20074_East 7th Street_2018 Redevelopment Report_2019.01.21

REDEVELOPMENT SUMMARY REPORT
EAST 7TH STREET STORAGE CHARLOTTE MECKLENBURG COUNTY
NORTH CAROLINA SUMMIT PROJECT NO. 3586.11 BROWNFIELDS PROJECT NO. 20074-16-060
Prepared For: East 7th Street, LLC 1420 East 7th Street
Suite 150 Charlotte, NC 29204 Prepared By:
SUMMIT ENGINEERING, LABRATORY & TESTING, Inc. 3575 Centre Circle Fort Mill, South Carolina 29715 704-504-1717

January 21, 2019

SUMMIT Engineering, Laboratory & Testing, P.C. 3575 Centre Circle Fort Mill, South Carolina 29715 www.SUMMIT-companies.com Phone: [phone] Fax: [phone] January 21, 2019
Ms. Hayley Irick North Carolina Department of Environmental Quality DWM - Brownfields 217 W. Jones Street
Raleigh, North Carolina 27699
Subject: 2018 Redevelopment Summary Report
East 7th Street Storage
East 7th Street Charlotte, Mecklenburg County, North Carolina Brownfields No. 20074-16-060 SUMMIT Project No. 3586.11
Dear Ms. Irick:
SUMMIT ENGINEERING, LABRATORY & TESTING, P.C . (SUMMIT) is pleased to submit the
following Redevelopment Summary Report pursuant to Land Use Restriction 8 of the Notice of
Brownfields Property. This report is completed to document development activities taken place at the property through December 2018. If you have any questions regarding our report, please do not hesitate to call us at [phone]. Sincerely, SUMMIT

Patrick W. Lowery, PG Michael D. Zavislak, NRCC-EAC, CIH, PE
Senior Environmental Manager Environmental Department Manager
NC LG No: 2421 SUMMIT’s NC Engineering Firm License No. C-2530
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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TABLE OF CONTENTS
1.0 INTRODUCTION .................................................................................................................... 1
1.1. PURPOSE .......................................................................................................................................... 1
1.2. SITE DESCRIPTION ........................................................................................................................ 1
1.3. PRE-DEVELOPMENT CONDITIONS ........................................................................................... 1
1.4. ENVIRONMENTAL MANAGEMENT PLAN ............................................................................... 1
1.5. CURRENT DEVELOPMENT STATUS .......................................................................................... 2
2.0 DEVELOPMENT SCHEDULE............................................................................................... 3
3.0 SITE GRADING & SOIL MANAGEMENT .......................................................................... 4
3.1. MATERIAL EXPORT ....................................................................................................................... 4
3.1.1. SOIL ............................................................................................................................. 4
3.1.2. DEBRIS ........................................................................................................................ 4
3.2. EXISTING SOILS CUT/FILL .......................................................................................................... 5
3.3. BARROW SOURCE ......................................................................................................................... 5
3.4. MATERIAL IMPORT ....................................................................................................................... 6
3.5. WATER .............................................................................................................................................. 6
3.6. UTILITY TRENCHES ...................................................................................................................... 7
4.0 UNDERGROUND STORAGE TANK .................................................................................... 8
5.0 POST DEVELOPMENT SAMPLING .................................................................................. 10
5.1. FINAL GRADE SAMPLES ............................................................................................................ 10
6.0 SUMMARY ............................................................................................................................ 11

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map Figure 3: Cut/Fill Placement
APPENDICES
Appendix A: Site/Field Reports Appendix B: NCDEQ Approvals Appendix C: UST Soil Sampling Letter Appendix D: Special Waste Profile Appendix E: Republic Soil Disposal Manifests Appendix F: Import Tickets
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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1.0 INTRODUCTION
1.1. PURPOSE

SUMMIT prepared this Redevelopment Summary Report to document redevelopment activities
occurring from January 1, 2018 through December 31, 2018 at the at the East 7th Street Storage
property located at 969 East 7th Street in Charlotte, Mecklenburg County, North Carolina. This report
has been prepared in accordance with requirements set forth in the Brownfields Agreement for the
site (the “Property”)

1.2. SITE DESCRIPTION

The Property is triangular in shape and was noted to be comprised of approximately 1.062 acres,
situated along the eastern site for East 7th Street, 300 feet south of its intersection with N. McDowell
Street in Charlotte, Mecklenburg County, North Carolina. The Property can be identified by
Mecklenburg Tax Parcel ID 08010175. Refer to the Site Location Map shown in Figure 1 for the
location of the Property. Refer to the Site map shown in Figure 2 for a detail view of the Property
development.

1.3. PRE-DEVELOPMENT CONDITIONS

The Property was undeveloped, grassed and partially wooded land prior to starting development
activities in January 2018. No structures, pavement or concrete slab foundations were present on the
site prior to redevelopment.

1.4. ENVIRONMENTAL MANAGEMENT PLAN

SUMMIT prepared an Environmental Management Plan (EMP) in accordance with NCDEQ
guidance and October 23, 2014 EMP format. The EMP was submitted to NCDEQ Brownfields on
January 10, 2018. The EMP was approved on January 22, 2018.

Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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1.5. CURRENT DEVELOPMENT STATUS

Redevelopment of the Property began in January 2018. Development activities completed by
December 31, 2018 include site grading, stormwater and utility system installation, foundation and
segmental retaining wall installation and vertical construction. The proposed development is
approximately 80% complete. Exterior components will be installed in early 2019 with interior
finishes following. A current planned date of occupancy is in June 2019.
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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2.0 DEVELOPMENT SCHEDULE

The Property is approximately 80% developed with a planned occupancy date in June of 2019. The
following timeline details the development progress for the Property. Site Reports completed by the
project management team (JLL) and SUMMIT field reports can be viewed in Appendix A of this
report.

Date Development Status January 23, 2018 Clearing and stripping of existing top soil materials and stockpiling for disposal off-site. February & March 2018 Haul off top soil materials, prepare sub-grade and haul in fill materials. Place fill materials in preparation of foundation installation.
May 2018 Excavate and install foundation footers. Prepare for foundation poured wall installation.
June 2018 Continue footer and foundation system installations. Start elevator
column installation.
July 2018 Install Storm Drain system (80%) and start retaining wall installation.
August 2018 Install underground detention system and install sewer main (waiting on tap).
September 2018 Install sewer line (waiting on tap) and start of vertical construction (framing 1st floor).
October – December 2018 Continue vertical construction with framing of 1st through 5th floors. Rough grade Property.

Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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3.0 SITE GRADING & SOIL MANAGEMENT

3.1. MATERIAL EXPORT
3.1.1. SOIL

The initial phase of redevelopment of the Property included the clearing of vegetation and stripping
of topsoil materials. It was determined that the stripped topsoil materials were unsuitable for re-use
as structural fill due to the presence of high organic materials and therefore were transported for
disposal at Republic Services CMS Landfill (speedway). A Special Waste profile was submitted and
approved by Republic Services prior to disposal of any materials. Copies of the waste profile approval
is included in Appendix D of this report. Republic Services provided Non-Hazardous Waste
Manifests for the material under profile 5010-18-0937. The grading contractor, SiteWorks provided
the transportation to the landfill.

Initial grading activities began in January of 2018. Topsoil materials were stockpiled in the central
portion of the site awaiting transport for disposal. Topsoil materials were transported to Republic
Services CMS Landfill on February 27, 2018, February 28, 2018 and March 2, 2018. Seventy-nine
(79) truck loads of soil were transported to the landfill for disposal. 1,273.67 tons of soil export was
conducted during the initial grading phase of redevelopment. Copies of the Non-Hazardous Waste
Manifests can be viewed in Appendix E of this report.

No other soil export has occurred for this redevelopment.

3.1.2. DEBRIS

Asphalt and various inert debris materials (concrete cobbles, wood, etc) were encountered at shallow
depths in the eastern portions of the site, adjacent to Interstate 277. This material could not be
adequately segregated from the topsoil materials and therefore was disposed of along with the topsoil
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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materials described above in section 2.1.1 of this report. Crushed heating oil USTs were identified in
the northeastern portion of the property. These tanks are discussed in Section 4.0 of this report.

3.2. EXISTING SOILS CUT/FILL

The topography of the Property prior to development sloped steeply from west to east with a relief of
approximately 25 feet. The grading plan and construction design for the redevelopment included
utilizing the elevated western portions of the property for ingress/egress (parking/driveway) and
backfilling the lower elevation portions of the Property with cut soils and import materials utilizing
structural retaining walls situated along the eastern property boundary. Following stripping of the
upper 0.5-1 ft bgs of organic laden topsoil, two (2) areas of existing soil required excavation (cut) and
placement adjacent to the cut areas, utilized as structural backfill. These areas are depicted on Figure
3A of this report. Max cut depths were 6 feet in the western portion of the site. No other soils were
cut and placed at other locations on the Property.

3.3. BARROW SOURCE

Import was anticipated on an as needed basis. For the development, the PD identified the following
quarry:

Martin Marietta 4551 Beatties Ford Road Charlotte, North Carolina
According to the quarry, the quarry generates rock, rock materials (granite dust, gravel, etc) and soil
mined from the residuum over the rock. The Beatties Ford quarry does not accept outside materials
and is a 100 percent export site.

On January 17, 2018 SUMMIT received approval from DEQ to import soils from the identified
quarry without further testing obligations. This quarry was considered approved by DEQ as a
Brownfields site import source. A copy of this approval is included in Appendix B of this report.
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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3.4. MATERIAL IMPORT

Property redevelopment planned for import in order to bring the site up to development grades. Soil
import was conducted by the grading contractor, SiteWorks. Material was loaded from the approved
barrow source (Beatties Ford Rd Quarry) and transported to the site for placement as structural fill.
A summary of the soil import activities is provided below:

Date Total Import (Cubic Yards) Purpose
3/16/18 652
Structural Fill for development.
3/19/18 608
3/27/18 980
3/28/18 906
3/29/18 67
8/6/18 346 Import to bring site to grade
10/9/18 80 Import to bring site to grade
Total 3,639 CY
As indicated in section 3.2 of this report, topography of the Property prior to development sloped
steeply from west to east with a relief of approximately 25 feet. The grading plan and construction
design for the redevelopment included utilizing the elevated western portions of the property for
ingress/egress (parking/driveway) and backfilling the lower elevation portions of the Property with
cut soils and import materials utilizing structural retaining walls situated along the eastern property
boundary. The retaining walls average approximately 12 feet in height along the eastern boundary.
Import fill was placed at thicknesses ranging from 12 feet in the eastern portion of the property to 4
feet in the western portion of the property.

Copies of soil import tickets can be viewed in Appendix F of this report. Refer to the Import Fill
Map, Figure 3B for reference of placed materials and approximate placement depths.

3.5. WATER

Groundwater was not encountered in any excavation conducted during site grading activities.
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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Following rain events, small pools of storm water would accumulate in the excavations on-site.
Surface water accumulated from rain events were allowed to infiltrate on-site and were not pumped
to storm drains or transported off-site.

3.6. UTILITY TRENCHES

Utility installation was completed following grading and import of fill material used to balance the
Property elevations in August and September 2018. The water utilities were installed at depths that
did not encounter native soils. Stormwater and sewer line installation was complete by trenching in
a combination of import fill material and native soils. Excavated soils from the utility trenches were
used as backfill of the utility trenches using the last out/first in practice. No environmental concerns
were noted in the excavation of native soils.

Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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4.0 UNDERGROUND STORAGE TANK

On February 9, 2018, grading activities in the eastern portion of the site encountered shallow buried
metal objects. Further excavation identified this material to consist of four (4) crushed Underground
Storage Tank (UST) partially buried in the upper 1 foot of the Property. The USTs were similar in
size and construction to residential home heating oil USTs. These USTs were free of any liquids. On
February 9, 2018 SUMMIT notified NCDEQ Project Manager of the discovery by phone. The USTs
were removed from the excavation and stored on-site for disposal at a steel recycling facility. Two
(2) soil samples were collected by SUMMIT following the removal from ground in accordance with
the EMP. A Letter of Soil Sampling, dated February 26, 2018 details the sampling and analysis for
these encountered USTs. This letter is included in Appendix C of this report. A UST Location Map
is included as Figure 5 of this report and sample locations can be viewed in Figure 1 of the Letter of
Soil Sampling located in Appendix C of the report. Detections were compared to the October 2017
IHSB PSRG at the time of sampling. A summary of analytical results is provided below:

• Tetrachloroethene was detected in sample USTP-1B at a level of 0.0083 mg/kg, below the
Commercial PSRG of 82 mg/kg and above the Protection of Groundwater PSRG of .0063
mg/kg.
• Benzo(a)anthracene and Benzo(b)fluoranthene were detected below the Commercial
PSRGs of 21 mg/kg and above the Protection of Groundwater standards in sample USTP-
1B.
• Benzo(a)pyrene was detected in sample USTP-1B at a level of 3.1 mg/kg, above the
Industrial/Commercial PSRG of 2.1 mg/kg.

Sample results indicate the presence of PAH compounds Benzo(a)anthracene, Benzo(a)pyrene and
Benzo(b)fluoranthene and VOC compound Tetrachloroethene (PCE) above IHSB Protection of
Groundwater October 2017 values. Benzo(a)pyrene additionally exceeded the PSRG for
Commercial soils, while all other detections were below the Commercial PSRGs. With the exception
of PCE, soil detections appeared similar to PAH concentrations identified in previous soil
assessments.
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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The resulting location of the removed USTs was subsequently backfilled and covered by greater than
9 feet of import soils for the backfill of foundation and structural retaining walls. Following backfill,
the area was capped with asphalt and concrete pavement surface materials for use as a dumpster pad
in the redevelopment of the Property.
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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5.0 POST DEVELOPMENT SAMPLING

5.1. FINAL GRADE SAMPLES

Final Grade samples have not been collected at the time of this report. This information will be
included in the final Redevelopment Summary Report.

Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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6.0 SUMMARY

The East 7th Street Storage redevelopment began construction activities in January 2018. Initial
stripping of soils across the Property resulted in the transport and disposal of 1,273 tons of topsoil
materials. During initial grading activities four (4) crush home heating oil USTs were discovered by
the grading contractor. In accordance with the Environmental Management Plan (EMP), the grading
contractor contacted SUMMIT for evaluation of the USTs. The USTs were empty and crushed.
SUMMIT contacted NCDEQ Project Manager by phone in accordance with the EMP. Two (2) soil
samples were collected from the beneath the USTs and the USTs were hauled off-site for disposal.
Sample results indicate the presence of PAH compounds Benzo(a)anthracene, Benzo(a)pyrene and
Benzo(b)fluoranthene and VOC compound Tetrachloroethene (PCE) above IHSB Protection of
Groundwater October 2017 values. Benzo(a)pyrene additionally exceeded the PSRG for
Commercial soils, while all other detections were below the Commercial PSRGs. With the exception
of PCE, soil detections appeared similar to PAH concentrations identified in previous soil
assessments.

Soil export and import was conducted in February and March of 2018. As indicated above, 1,273
tons of topsoil material stripped from the upper 1 foot of the Property was properly disposed of at
Republic Services CMS Landfill. Approximately 3,600 CY of import soils were transport to the
subject site as structural fill from the Martin Marietta Beatties Ford Quarry. All transport of soils was
completed by SiteWorks, the grading contractor for the redevelopment of the Property.

Following export and import, foundation systems, stormwater conveyance systems, and utility
installations were completed by September 2018. Vertical construction of the storage facility began
in September 2018. The Property is approximately 80 % developed with a planned occupancy date
of June 2018.

Final Grade sampling will be conducted in February 2019 with results included in the final
Redevelopment Report for the Property.
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11
Charlotte, North Carolina January 21, 2019

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FIGURES
Source:Delorme Prepared By\Date:PL/12/16
Checked By\Date:MZ/12/16
Scale
Figure 1
1420 East 7th Street, Suite 150 As Shown
Charlotte, NC 28204
Subject Property Topography
E. 7th Street StorageE. 7th Street
Charlotte, North Carolina
East 7th Street, LLC
N
Subject Property
Source: Drawn by SUMMIT.
Prepared By\Date:PL/12/16Checked By\Date:MZ 12/16
Scale
Figure 2As Shown
Charlotte, North Carolina
Subject Property Aerial East 7th Street, LLC
E. 7th Street Storage 1420 East 7th Street, Suite 150
E. 7th Street Charlotte, NC 28204
N
Subject Property
Little Sugar Creek
NOVANT Health
Residential/Commerical
Source: Drawn by SUMMIT.
Prepared By\Date:PL/01/19Checked By\Date:MZ 01/19
Scale
Figure 3AAs Shown
Charlotte, North Carolina
Existing Site Soils Cut/Fill Map East 7th Street, LLC
E. 7th Street Storage 1420 East 7th Street, Suite 150
E. 7th Street Charlotte, NC 28204
N
Max Cut = 6'
Max Cut = 2'
Cut soils used as structural fill to balance site adjacent to cut, placed on existing grade
prior to import of additional soils.
KEY
Area of Cut soils
Area of placed cut soils
Source: Drawn by SUMMIT.
Prepared By\Date:PL/01/19Checked By\Date:MZ 01/19
Scale
Figure 3BAs Shown
Charlotte, North Carolina
Import Fill Map East 7th Street, LLC
E. 7th Street Storage 1420 East 7th Street, Suite 150
E. 7th Street Charlotte, NC 28204
N
Wall Height = 12'
Approx. Location of Retaining Wall
KEY
Area import fill placement
Approx. thickness of import
fill
Wall Height = 12'
8'
12'
9'
10'
7'
6'
4'
4'
9'
3'
Source: Drawn by SUMMIT.
Prepared By\Date:PL/01/19Checked By\Date:MZ 01/19
Scale
Figure 4As Shown
Charlotte, North Carolina
Utility Map East 7th Street, LLC
E. 7th Street Storage 1420 East 7th Street, Suite 150
E. 7th Street Charlotte, NC 28204
N
KEY
Sewer Utility
Water Utility
Stormwater Utility
Sewer Connection to existing SS
CLT Water Tap
Stormwater Detention
Stormwater Outfall
Hydrant
Notes:
-Water Utilities installed in import
fill material.
-Sewer and Stormwater trenching
conducted in import and existing
soils. Last Out/First In practice
followed for trenching in existing
soils.
Source: Drawn by SUMMIT.
Prepared By\Date:PL/01/19Checked By\Date:MZ 01/19
Scale
Figure 5As Shown
Charlotte, North Carolina
UST Location Map East 7th Street, LLC
E. 7th Street Storage 1420 East 7th Street, Suite 150
E. 7th Street Charlotte, NC 28204
N
Notes:
-Approximately 4 crushed
residential heating oil USTs found
buried 1' bgs during stripping of
the site.
-Location of USTs located beneath
approximately 9' of import fill and
asphalt pavement.
Location of crushed USTs
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina January 21, 2019

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APPENDIX A
SITE/FIELD REPORTS

Phase I ESA, E 7th Street Storage SUMMIT Project No.3586.11 Charlotte, North Carolina Photograph Date: March 8, 2018

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SITE PHOTOGRAPHS
View looking west along the sites northern boundary.
View looking east along the sites northern boundary.
Phase I ESA, E 7th Street Storage SUMMIT Project No.3586.11 Charlotte, North Carolina Photograph Date: April 4, 2018

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SITE PHOTOGRAPHS
View north through the site.
View looking east along the sites southern boundary.
Phase I ESA, E 7th Street Storage SUMMIT Project No.3586.11 Charlotte, North Carolina Photograph Date: April 4, 2018

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View looking west along through the site.
View looking north through the site.

Site Visit Report
Client Name:
Project Name:E 7th St
Project Number:
JLL Project Manager:Martha Fakadej
Date of Visit:5/3/2018 11:49
General Notes
Site Visit
- Footing excavation in progress
- Concrete footing pour in progress
- Rebar placement in progress
- Additional Geotech borings in progress
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5 6
7 8
9 10
11 12
13 14
15 16
19 20
17 18
Site Visit Report
Client Name:
Project Name:E 7th
Project Number:
JLL Project Manager:Martha Fakadej
Date of Visit:06/13/2018 02:02:32 PM GMT-04:00
General Notes
COMPLETED
•Elevator #1 #2 waterproofing complete,•French drains at Foundation wall - Complete
CURRENT
•Building footings – 95% complete, •Pour slab on grade – 60% complete, •Building foundation
wall form prep – 85% complete, •Building foundation wall poured - 75% complete, •Storm Drain -
80% complete,•Underslab back fill - 90% complete
UPCOMING
•Import and Back fill for Foundation wall – Late June,•Building foundation wall waterproofing -
June, •CMU Stair installation –July, •CMU Elevator Tower installation – July, •SOB - Completion
Target July 5, 2018
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9 10
11 12
13 14
15 16
19 20
17 18
Site Visit Report
Client Name:E 7th LLC
Project Name:
Project Number:
JLL Project Manager:Martha Fakadej
Date of Visit:7/18/2018 14:26
General Notes - Site Visit
COMPLETED - Under slab back fill ,Building footings, Pour slab on grade, Building foundation wall form
prep, Building foundation wall poured ,
CURRENT - Storm Drain - 80% complete, Foundation waterproofing - 95% complete, Import and Back fill
for Retaining wall - 10% complete, CMU Stair installation –10% complete, CMU Elevator Tower
installation – 10% complete, Retaining wall installation - 20% complete
UPCOMING - Backfill Drive - Early Aug. start, Site Utilities - Aug start, Storm Detention Installation - Late
July start, Steel Mobilization - Late Aug. Start, Steel Delivery - Early Sep.
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Page 1 of 5
5 6
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9 10
Page 2 of 5
11 12
13 14
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Page 3 of 5
19 20 New Duke power pole location
17 18
Page 4 of 5
Key Plan
Page 5 of 5
Site Visit Report
Client Name:East 7th Street LLC
Project Name:E 7th St
Project Number:
JLL Project Manager:Martha Fakadej
Date of Visit:8/8/2018 13:50
General Notes
COMPLETED - Retaining Wall installation, Import and Backfill for Retaining wall, Charlotte Water
waterline extension, Duke Energy power pole installation,
CURRENT - Storm Drain – 80% Complete, (2) CMU stair towers – 55% complete, (2) CMU Elevator
towers – 45% complete, Underground detention system installation – 65% , complete, IMP shop
drawings in review
UPCOMING - Install of Sewer underground line – Late Aug., Import and rough grade site – Late Aug.,
Curb and gutter – Late Aug., Steel delivery – Aug 27, Steel Framing Leve 2 – Sep.
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19 20
17 18
Site Visit Report
Client Name:
Project Name:E 7th st
Project Number:
JLL Project Manager:
Date of Visit:9/5/2018 13:58
General Notes
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3 4
COMPLETED - Building foundation wall poured, Import and Back fill for Retaining wall ,Foundation
waterproofing,Storm Detention system,Water line and meter – Set,Temp. Power ,CMU Stair
installation,CMU Elevator Tower installation,Curb and gutter,Proof rolling ,Binder,
CURRENT - Sanitary Sewer underground (waiting on tie in)– 95% complete, 7 th St Retaining wall
installation – 95 % complete, Steel framing installation - 1st floor in progress,
UPCOMING - As built for Storm Detention system - Oct., Fire line and hydrant installation – Early Sep.,
Brick Installation – Early Sep., Fire proofing – Early Sep.., Elec. Misspelled WordMech rough – Oct.
9 10
7 8
5 6
15 16
13 14
11 12
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17 18
Site Visit Report
Client Name:
Project Name:E 7th Street LLC
Project Number:
JLL Project Manager:Martha Fakadej
Date of Visit:10/9/2018 13:31
General Notes
COMPLETED -Temp. Power ,CMU Stair installation,CMU Elevator Tower installation, Proof rolling,
Binder, slab on grade pour, 2nd floor slab pour
CURRENT - Sanitary Sewer underground (waiting on tie in)– 95% complete, 7 th St Retaining wall
installation – 95 % complete,
Steel framing installation - 2nd floor in progress, Steel Stair #2 - 10% complete, Level 3 metal deck - 95
% complete, Level 3 steel framing - in progress, Fire line and hydrant installation - 95% complete
UPCOMING - As built for Storm Detention system - Oct., Brick Installation – Oct., Fire proofing – Oct.,
Elec. Mech rough – Oct., Exterior light gauge framing - Oct. Upper floors steel framing, upper floors
deck and slab pour
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Site Visit Report
Client Name:PDP
Project Name:E 7th
Project Number:
JLL Project Manager:Martha Fakadej
Date of Visit:11/14/2018 14:37
General Notes
COMPLETED -Temp. Power ,CMU Stair installation, CMU Elevator Tower installation, Proof rolling,
Binder, slab on grade pour, 4th floor concrete slab pour (Nov.8th)
CURRENT - Sanitary Sewer underground (waiting on tie in)– 95% complete, 7 th St Retaining wall
installation – 95 % complete, Fire proofing – 15% complete, Elec. Rough – 20% complete, in progress on
1,2 and 3 floors, Light gauge Metal framing 2nd floor 10% complete
Steel framing installation – 5th floor columns and beams in progress, Steel Stair #1 and #2 (Floors 1-4)-
30% complete,
UPCOMING - Level 5 metal deck (Target Nov. 17th), As built for Storm Detention system – Dec., Mech
Rough – week of Nov. 19th., Fire Sprinkler – week of Nov. 19th Exterior light gauge framing – Dec.,
Elevator Meeting on site (Target Nov. 17th) Upper floors steel framing, upper floors deck and slab pour
2 - 2nd floor office 1 - 2nd floor office
3 - 2nd floor office 4 - Eletrical room
5 - Transformer pad 6 - 2nd floor Steel (x bracing)
7 - 1st floor spray fireproofing 8 - 1st floor spray fireproofing
9 - 1st floor Electrical rough 10 - 1st floor Electrical rough
11 - 4th floor slab (5th floor steel column and beams)12 - 4th floor slab (5th floor steel column and
beams)
13 - 4th floor slab 14 - 4th floor slab
15 - Stair #2 16 - Stair #2
Phase I ESA, E 7th Street Storage SUMMIT Project No.3586.11 Charlotte, North Carolina Photograph Date: January 14, 2019

D:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\Redevelopment Report\Site Photographs 1-14-19.doc 1
SITE PHOTOGRAPHS
View of the self-storage building.
View looking east along the site’s southern boundary.
Phase I ESA, E 7th Street Storage SUMMIT Project No.3586.11 Charlotte, North Carolina Photograph Date: January 14, 2019

D:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\Redevelopment Report\Site Photographs 1-14-19.doc 2
View looking north along retaining wall.
View looking west through the site from the building.

Redevelopment Summary Report – Highland Mill #3 – North Brevard Street Site SUMMIT Project No. 1820.59 Charlotte, North Carolina January 30, 2018

D:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\Redevelopment Report\1-21-19 Draft\Appendix B - Approvals.rtf

APPENDIX B
APPROVALS

APPROVAL SIGNATURES
Prospective Developer
Printed Name/Title/Com pany
Consultant
Printed
PatrickW. Lowery, P.G.
Senior Environmental Manager
SUMMIT ELT, PC
Date
U22t20t8
EMP Form ver.L. October 23.2014
L2
1
Patrick Lowery
From:Irick, Hayley M <[e-mail]>
Sent:Wednesday, January 17, 2018 11:41 AM
To:Patrick Lowery
Subject:RE: [External] FW: 7th Street Storage Import Source
Hey Patrick – You are correct, the Martin Marietta ‐ Beatties Ford Quarry has been sampled extensively for our program 
and therefore does not need to be sampled prior to import at the East 7th Street site.   

Thanks,  
Hayley 

Hayley M. Irick
Project Manager
Division of Waste Management – Brownfields Program
NC Department of Environmental Quality

919 707 8294 direct line
[e-mail]

217 W Jones Street
1646 Mail Service Center
Raleigh, NC 27699

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Patrick Lowery [mailto:plowery@summit‐companies.com]  
Sent: Wednesday, January 17, 2018 11:00 AM 
To: Irick, Hayley M <[e-mail]> 
Subject: [External] FW: 7th Street Storage Import Source 

CAUTION: External email. Do not click links or open attachments unless verified. Send all suspicious email as an attachment to 
[e-mail]. 

Hayley, 
The contractor with Siteworks has informed me that the import for the E. 7th Street project will be sourced from the 
Martin Marietta‐Beatties Ford Quarry.   

I believe Joselyn has approved soils for other area projects from this quarry.  Can you please review your files and let me 
know if you need import confirmation samples from this quarry.   If so, please let me know your preference on sample # 
vs import quantity.   

2
Thanks! 
Patrick 

From: Jeff Crump [mailto:JCrump@siteworks‐llc.com]  
Sent: Wednesday, January 17, 2018 10:47 AM 
To: Patrick Lowery <plowery@summit‐companies.com> 
Cc: Greg Rodden ([e-mail]) <[e-mail]> 
Subject: 7th Street Storage Import Source 

Patrick, 

I wanted to confirm that our import source will be Martin Marietta‐ Beatties Ford Quarry.   Approximately 11,000 cubic 
yards. 

Let me know if you need any additional information.  

Thanks 

Jeff Crump
Siteworks, LLC
Project Manager

12034 Goodrich Drive
Charlotte, NC 28273
704-588-3055 office
704-588-3056 fax
704-622-2605 mobile

1
Patrick Lowery
From:Patrick Lowery
Sent:Tuesday, January 23, 2018 2:26 PM
To:Irick, Hayley M
Cc:Fakadej, Martha; Will Andrews
Subject:East 7th Street Storage - Notification of Start
Hayley, 
Please let this email serve as notification that construction activities are starting at the East 7th Street Storage (20074‐16‐
060) property.  If you have any questions or concerns please let us know. 
Thank you, 
Patrick 

Patrick W. Lowery, PG 
Senior Environmental Manager 
plowery@summit‐companies.com  
Columbia Office | 101 Rice Bent Way, Unit 9 | Columbia, SC 29229  
803.708.7945 Office | 803.708.7946 Fax | 803.230.5087 Cell 
www.summit‐companies.com 
Charlotte‐HQ | Raleigh | Columbia | Greenville | Charleston 

Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina January 21, 2019

D:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\Redevelopment Report\1-21-19 Draft\Appendix C - UST Soil Sampling Letter.rtf

APPENDIX C
UST SOIL SAMPLING LETTER

February 26, 2018 Ms. Hayley Irick NC Department of Environmental Quality Division of Waste Management – Brownfields Program 1646 Mail Service Center Raleigh, NC 27699 Subject: Letter of Soil Sampling E. 7th Street Storage 969 E. 7th Street Charlotte, Mecklenburg County, North Carolina SUMMIT Project No. 3586.11 Brownfields Project No. 20074-16-060
SUMMIT ENGINEERING, LABORATORY & TESTING, P.C. (SUMMIT) completed soil sampling
conducted at the E. 7th Street Storage Brownfields site in accordance with the NCDEQ approved Environmental Management Plan (EMP). The subject site is located at 969 E. 7th Street, in Charlotte, Mecklenburg County, North Carolina. Preliminary grading of the subject site for storm-water infrastructure installation began on January 23, 2018. On February 9, 2018, Edifice (General Contractor) contacted SUMMIT to report the discovery of approximately four (4) crushed heating oil underground storage tanks (USTs). The USTs were discovered to be buried approximately 2 feet below ground surface (bgs) in the northeastern portion of the site. The USTs were empty and did not contain liquids. The crushed USTs were removed from the ground and placed on-site for transport and disposal at a recycling
facility. SUMMIT personnel (Patrick Lowery) collected two (2) soil samples from the soils located beneath the discovered USTs. Samples were collected from each end of the pit containing the USTs (USTP-1A and USTP-1B). Soil samples were collected via a decontaminated stainless steel hand auger. Collected soils were
transferred to laboratory provided vials/jars and placed on ice for transport to the laboratory. Details for the collected soil samples are provided below.
Soil Sample Summary Table Sample ID GPS Lat/Long Sample Depth Sample Analysis USTP-1A 35o 13.57’/-80o 49.793 0-2 ’ bgs VOCs, SVOCs, RCRA Metals
USTP-1B 35o 13.57’/-80o 49.793 0-2 ’ bgs VOCs, SVOCs, RCRA Metals
SUMMIT did not observe soil staining or encounter petroleum odors in the UST pit.
Soil samples were submitted to Shealy Environmental Services on February 13, 2018 for the analysis of Volatile Organic Compounds, Semi-Volatile Organic Compounds and RCRA Metals. A copy of the results and chain-of-custody records are attached to this letter. Table 1.0 attached to this letter summarizes the laboratory
detections. Reportable detections were compared to the October 2017 NC DEQ Preliminary Soil Remediation Goals (PSRGs) for Industrial/Commercial properties and the Protection of Groundwater standards.
Letter of Soil Sampling and Analysis – E. 7th Street Storage SUMMIT Project No. 3586.11 Charlotte, Mecklenburg County, North Carolina February 26, 2018

Results reported above a NC DEQ PSRG standards are detailed below.
• Tetrachloroethene was detected in sample USTP-1B at a level of 0.0083 mg/kg, below the Commercial PSRG of 82 mg/kg and above the Protection of Groundwater PSRG of .0063 mg/kg.
• Benzo(a)anthracene and Benzo(b)fluoranthene were detected below the Commercial PSRGs of 21 mg/kg and above the Protection of Groundwater standards in sample USTP-1B.
• Benzo(a)pyrene was detected in sample USTP-1B at a level of 3.1 mg/kg, above the Industrial/Commercial PSRG of 2.1 mg/kg. Detections reported from USTP-1A did not exceed the Commercial PSRG or Soil to Groundwater PSRG standards. With the exception of Tetrachloroethene, concentrations reported in this soil sample analysis are reported at similar concentrations detected in previous site assessments.
This letter includes a description of the methodology of our investigation and a summary of our findings. If you have any questions regarding our assessment of the subject property, or our conclusions or
recommendations, please do not hesitate to call us at [phone]. Sincerely, SUMMIT Patrick W. Lowery, PG Senior Environmental Manager Attachments: Table 1.0 – Soil Sample Detection Summary Table Sample Location Map Site Photographs Laboratory Analytical Report
Source: Drawn by SUMMIT.
Prepared By\Date:PL/02/18
Checked By\Date:MZ 02/18
Scale
Figure 1As ShownCharlotte, North Carolina
Sampling Location Map 2/9/18 East 7th Street, LLC
E. 7th Street Storage 1355 Greenwood Cliff, Suite 150
E. 7th Street Charlotte, NC 28204
N
Subject Property
Crushed USTs
USTP-1A USTP-1B
Page 1 of 1
E. 7th Street StorageCharlotte, NC February 26, 2018SUMMIT Project No: 3586.11
CAS VOC Analyte
PSRG-
Industrial
Protection
of GW Result RL Result RL
67-64-1 Acetone 1.00E+05 2.50E+01 0.038 0.02 0.1 0.022
127-18-4 Tetrachloroethene 8.20E+01 6.30E-03 BRL 0.005 0.0083 0.005
127-18-4 SVOC Analyte
PSRG-
Industrial
Protection
of GW Result RL Result RL
83-32-9 Acenaphthene 9.00E+03 1.60E+01 BRL 0.066 0.17 0.071
120-12-7 Anthracene 4.50E+04 1.30E+03 BRL 0.066 0.64 0.071
56-55-3 Benzo(a)anthracene 2.10E+01 3.50E-01 0.11 0.066 2.6 0.07150-32-8 Benzo(a)pyrene 2.10E+00 1.20E-01 0.11 0.066 3.1 0.071
205-99-2 Benzo(b)fluoranthene 2.10E+01 1.20E+00 0.19 0.066 4.4 0.071
191-24-2 Benzo(g,h,i)perylene NA 1.56E+04 BRL 0.066 0.72 0.071
207-08-9 Benzo(k)fluoranthene 2.10E+02 1.20E+01 BRL 0.066 1.6 0.071
218-01-9 Chrysene 2.10E+03 3.60E+01 BRL 0.066 2.1 0.071
206-44-0 Fluoranthene 6.00E+03 6.70E+02 0.1 0.066 5 0.071
86-73-7 Fluorene 6.00E+03 1.10E+02 BRL 0.066 0.15 0.071
193-39-5 lndeno(1,2,3-c,d)pyrene 2.10E+01 3.90E+00 BRL 0.066 0.85 0.07185-01-8 Phenanthrene NA 1.34E+02 BRL 0.066 2.4 0.071
129-00-0 Pyrene 4.50E+03 4.40E+02 0.094 0.066 3.6 0.071
CAS Metals
PSRG-Industrial Protection of GW Result RL Result RL
7440-38-2 Arsenic 3.00E+00 5.80E+00 2.1 0.78 2.9 0.78
7440-39-3 Barium 4.70E+04 5.80E+02 81 1.3 110 1.4
7440-43-9 Cadmium 2.00E+02 3.00E+00 BRL 0.026 0.55 0.26
7440-47-3 Chromium NA 3.60E+05 43 0.52 40 0.52
7439-92-1 Lead NA 2.70E+02 38 0.52 83 0.52
7439-97-6 Mercury 3.13E+00 1.00E+00 BRL 0.095 0.66 0.1
BRL = Below Reporting Limit J = Estimated Concentration BOLD = Concentration Above Reference Values
NT = Not Tested RL = Lab Reporting Limit
0-2' bgsAll Values in mg/kg
NCDEQ Reference Values
USTP-1A USTP-1B
0-2' bgs
Table 1.0: Soil Sample Detection Summary Table
2/9/2018 2/9/2018
E. 7th Street Storage SUMMIT Project No.3586.11
Charlotte, North Carolina February 26, 2018

E:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\EMP\Site Visit 2-9-18 UST\3586.11 - Site Photographs.doc 1
SITE PHOTOGRAPHS
View approximately 4 crushed heating oil USTs discovered on-site.
View approximately 4 crushed heating oil USTs discovered on-site.
E. 7th Street Storage SUMMIT Project No.3586.11
Charlotte, North Carolina February 26, 2018

E:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\EMP\Site Visit 2-9-18 UST\3586.11 - Site Photographs.doc 2
View approximately 4 crushed heating oil USTs discovered on-site.
View area USTs were discovered and soil samples collected.

SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
SUMMIT Engineering,Laboratory &Testing,P.C.
3575 Centre Circle
Fort Mill,SC 28715
Attention:Patrick Lowery
Project Name:E.7th St.
Project Number:3586.11
Lot Number:TB13013
Date Completed:02/21/2018
02/21/2018 11:02 AM
Approved and released by:
Project Manager:Lucas Odom
Page 1 of 30
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
SUMMIT Engineering,Laboratory &Testing,P.C.
Lot Number:TB13013
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.
The sample receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved NELAC
standards,the Shealy Environmental Services,Inc.("Shealy")Quality Assurance Management Plan (QAMP),standard operating
procedures (SOPs),and Shealy policies.Any exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the
results page or discussed below.
Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W"qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
SVOCs by GC/MS
Due to the large number of spiked analytes,there is a high probability that one or more analytes will recover outside acceptance limits.
The laboratory's SOP allows for 10%of analytes to recover marginally outside criteria.The following analytes recovered marginallyoutsideLCScriteria:4-nitroaniline.
The laboratory control sample (LCS)for prep batch 64527 exceeded acceptance criteria for the following analytes:Pyridine.These
analytes were biased high and were not detected in the samples affected:TB13013-001,TB13013-002.
Page 2 of 30
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TB13013

Sample Number Sample ID Matrix Date Sampled Date Received
001 02/09/2018 1500USTP-1A Solid 02/13/2018
002 02/09/2018 1510USTP-1B Solid 02/13/2018
(2 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 30
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TB13013

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 USTP-1A Solid Acetone 8260B 38 ug/kg 5
001 USTP-1A Solid Benzo(a)anthracene 8270D 110 ug/kg 6
001 USTP-1A Solid Benzo(a)pyrene 8270D 110 ug/kg 6
001 USTP-1A Solid Benzo(b)fluoranthene 8270D 190 ug/kg 6
001 USTP-1A Solid Fluoranthene 8270D 100 ug/kg 7
001 USTP-1A Solid Pyrene 8270D 94 ug/kg 8
001 USTP-1A Solid Arsenic 6010D 2.1 mg/kg 8
001 USTP-1A Solid Barium 6010D 81 mg/kg 8
001 USTP-1A Solid Chromium 6010D 43 mg/kg 8
001 USTP-1A Solid Lead 6010D 38 mg/kg 8
002 USTP-1B Solid Acetone 8260B 100 ug/kg 9
002 USTP-1B Solid Tetrachloroethene 8260B 8.3 ug/kg 9
002 USTP-1B Solid Acenaphthene 8270D 170 ug/kg 10
002 USTP-1B Solid Anthracene 8270D 640 ug/kg 10
002 USTP-1B Solid Benzo(a)anthracene 8270D 2600 ug/kg 10
002 USTP-1B Solid Benzo(a)pyrene 8270D 3100 ug/kg 10
002 USTP-1B Solid Benzo(b)fluoranthene 8270D 4400 ug/kg 10
002 USTP-1B Solid Benzo(g,h,i)perylene 8270D 720 ug/kg 10
002 USTP-1B Solid Benzo(k)fluoranthene 8270D 1600 ug/kg 10
002 USTP-1B Solid Chrysene 8270D 2100 ug/kg 11
002 USTP-1B Solid Fluoranthene 8270D 5000 ug/kg 11
002 USTP-1B Solid Fluorene 8270D 150 ug/kg 11
002 USTP-1B Solid Indeno(1,2,3-c,d)pyrene 8270D 850 ug/kg 11
002 USTP-1B Solid Phenanthrene 8270D 2400 ug/kg 12
002 USTP-1B Solid Pyrene 8270D 3600 ug/kg 12
002 USTP-1B Solid Arsenic 6010D 2.9 mg/kg 12
002 USTP-1B Solid Barium 6010D 110 mg/kg 12
002 USTP-1B Solid Cadmium 6010D 0.55 mg/kg 12
002 USTP-1B Solid Chromium 6010D 40 mg/kg 12
002 USTP-1B Solid Lead 6010D 83 mg/kg 12
002 USTP-1B Solid Mercury 7471B 0.66 mg/kg 12
(31 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1A
TB13013-001
02/09/2018 1500
02/13/2018
Solid
% Solids:81.3 02/13/2018 2108
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/14/2018 1534 JM1 64493 6.04
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acetone 67-64-1 8260B 38 1ug/kg20
Benzene 71-43-2 8260B ND 1ug/kg5.1
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.1
Bromoform 75-25-2 8260B ND 1ug/kg5.1
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.1
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg10
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.1
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.1
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.1
Chloroethane 75-00-3 8260B ND 1ug/kg5.1
Chloroform 67-66-3 8260B ND 1ug/kg5.1
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.1
Cyclohexane 110-82-7 8260B ND 1ug/kg5.1
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.1
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.1
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.1
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.1
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.1
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.1
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.1
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.1
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.1
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.1
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.1
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.1
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.1
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.1
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.1
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.1
2-Hexanone 591-78-6 8260B ND 1ug/kg10
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.1
Methyl acetate 79-20-9 8260B ND 1ug/kg5.1
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.1
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg10
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.1
Methylene chloride 75-09-2 8260B ND 1ug/kg5.1
Styrene 100-42-5 8260B ND 1ug/kg5.1
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.1
Tetrachloroethene 127-18-4 8260B ND 1ug/kg5.1
Toluene 108-88-3 8260B ND 1ug/kg5.1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1A
TB13013-001
02/09/2018 1500
02/13/2018
Solid
% Solids:81.3 02/13/2018 2108
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/14/2018 1534 JM1 64493 6.04
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.1
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.1
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.1
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.1
Trichloroethene 79-01-6 8260B ND 1ug/kg5.1
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.1
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.1
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.1
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 89 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 107 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 02/20/2018 1229 CMP2 02/14/2018 1745 64527
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 8270D ND 1ug/kg66
Acenaphthylene 208-96-8 8270D ND 1ug/kg66
Acetophenone 98-86-2 8270D ND 1ug/kg320
Anthracene 120-12-7 8270D ND 1ug/kg66
Atrazine 1912-24-9 8270D ND 1ug/kg320
Benzaldehyde 100-52-7 8270D ND 1ug/kg320
Benzo(a)anthracene 56-55-3 8270D 110 1ug/kg66
Benzo(a)pyrene 50-32-8 8270D 110 1ug/kg66
Benzo(b)fluoranthene 205-99-2 8270D 190 1ug/kg66
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg66
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg66
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg320
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg320
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg320
Caprolactam 105-60-2 8270D ND 1ug/kg320
Carbazole 86-74-8 8270D ND 1ug/kg320
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg320
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg320
4-Chloroaniline 106-47-8 8270D ND 1ug/kg320
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg320
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1A
TB13013-001
02/09/2018 1500
02/13/2018
Solid
% Solids:81.3 02/13/2018 2108
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 02/20/2018 1229 CMP2 02/14/2018 1745 64527
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg320
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg320
2-Chlorophenol 95-57-8 8270D ND 1ug/kg320
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg320
Chrysene 218-01-9 8270D ND 1ug/kg66
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg66
Dibenzofuran 132-64-9 8270D ND 1ug/kg320
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg320
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg320
Diethylphthalate 84-66-2 8270D ND 1ug/kg320
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg320
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg320
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg320
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg1600
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg1600
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg660
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg660
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg320
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg320
Fluoranthene 206-44-0 8270D 100 1ug/kg66
Fluorene 86-73-7 8270D ND 1ug/kg66
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg320
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg320
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1600
Hexachloroethane 67-72-1 8270D ND 1ug/kg320
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg66
Isophorone 78-59-1 8270D ND 1ug/kg320
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg66
2-Methylphenol 95-48-7 8270D ND 1ug/kg320
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg660
Naphthalene 91-20-3 8270D ND 1ug/kg66
2-Nitroaniline 88-74-4 8270D ND 1ug/kg660
3-Nitroaniline 99-09-2 8270D ND 1ug/kg660
4-Nitroaniline 100-01-6 8270D ND 1ug/kg660
Nitrobenzene 98-95-3 8270D ND 1ug/kg320
2-Nitrophenol 88-75-5 8270D ND 1ug/kg660
4-Nitrophenol 100-02-7 8270D ND 1ug/kg1600
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg320
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg320
Pentachlorophenol 87-86-5 8270D ND 1ug/kg1600
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1A
TB13013-001
02/09/2018 1500
02/13/2018
Solid
% Solids:81.3 02/13/2018 2108
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 02/20/2018 1229 CMP2 02/14/2018 1745 64527
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Phenanthrene 85-01-8 8270D ND 1ug/kg66
Phenol 108-95-2 8270D ND 1ug/kg320
Pyrene 129-00-0 8270D 94 1ug/kg66
Pyridine 110-86-1 8270D ND 1ug/kg320
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg320
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg320
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 44 33-102
2-Fluorophenol 37 35-115
Nitrobenzene-d5 59 22-109
Phenol-d5 42 33-122
Terphenyl-d14 48 41-120
2,4,6-Tribromophenol 38 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 02/14/2018 0938 CJZ 02/13/2018 1548 64355
1 7471B 7471B 1 02/14/2018 1616 SLS 02/14/2018 1404 64390
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Arsenic 7440-38-2 6010D 2.1 1mg/kg0.78
Barium 7440-39-3 6010D 81 1mg/kg1.3
Cadmium 7440-43-9 6010D ND 1mg/kg0.26
Chromium 7440-47-3 6010D 43 1mg/kg0.52
Lead 7439-92-1 6010D 38 1mg/kg0.52
Mercury 7439-97-6 7471B ND 1mg/kg0.095
Selenium 7782-49-2 6010D ND 1mg/kg1.0
Silver 7440-22-4 6010D ND 1mg/kg0.52
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1B
TB13013-002
02/09/2018 1510
02/13/2018
Solid
% Solids:74.9 02/13/2018 2108
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/14/2018 1557 JM1 64493 6.14
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acetone 67-64-1 8260B 100 1ug/kg22
Benzene 71-43-2 8260B ND 1ug/kg5.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg5.4
Bromoform 75-25-2 8260B ND 1ug/kg5.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg5.4
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg11
Carbon disulfide 75-15-0 8260B ND 1ug/kg5.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg5.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg5.4
Chloroethane 75-00-3 8260B ND 1ug/kg5.4
Chloroform 67-66-3 8260B ND 1ug/kg5.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg5.4
Cyclohexane 110-82-7 8260B ND 1ug/kg5.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg5.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg5.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg5.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg5.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg5.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg5.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg5.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg5.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg5.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg5.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg5.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg5.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg5.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg5.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg5.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg5.4
2-Hexanone 591-78-6 8260B ND 1ug/kg11
Isopropylbenzene 98-82-8 8260B ND 1ug/kg5.4
Methyl acetate 79-20-9 8260B ND 1ug/kg5.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg5.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg11
Methylcyclohexane 108-87-2 8260B ND 1ug/kg5.4
Methylene chloride 75-09-2 8260B ND 1ug/kg5.4
Styrene 100-42-5 8260B ND 1ug/kg5.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg5.4
Tetrachloroethene 127-18-4 8260B 8.3 1ug/kg5.4
Toluene 108-88-3 8260B ND 1ug/kg5.4
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1B
TB13013-002
02/09/2018 1510
02/13/2018
Solid
% Solids:74.9 02/13/2018 2108
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 02/14/2018 1557 JM1 64493 6.14
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg5.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg5.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg5.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg5.4
Trichloroethene 79-01-6 8260B ND 1ug/kg5.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg5.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg5.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg5.4
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 92 53-142
Bromofluorobenzene 87 47-138
Toluene-d8 112 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 02/20/2018 1254 CMP2 02/14/2018 1745 64527
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acenaphthene 83-32-9 8270D 170 1ug/kg71
Acenaphthylene 208-96-8 8270D ND 1ug/kg71
Acetophenone 98-86-2 8270D ND 1ug/kg340
Anthracene 120-12-7 8270D 640 1ug/kg71
Atrazine 1912-24-9 8270D ND 1ug/kg340
Benzaldehyde 100-52-7 8270D ND 1ug/kg340
Benzo(a)anthracene 56-55-3 8270D 2600 1ug/kg71
Benzo(a)pyrene 50-32-8 8270D 3100 1ug/kg71
Benzo(b)fluoranthene 205-99-2 8270D 4400 1ug/kg71
Benzo(g,h,i)perylene 191-24-2 8270D 720 1ug/kg71
Benzo(k)fluoranthene 207-08-9 8270D 1600 1ug/kg71
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg340
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg340
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg340
Caprolactam 105-60-2 8270D ND 1ug/kg340
Carbazole 86-74-8 8270D ND 1ug/kg340
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg340
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg340
4-Chloroaniline 106-47-8 8270D ND 1ug/kg340
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg340
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1B
TB13013-002
02/09/2018 1510
02/13/2018
Solid
% Solids:74.9 02/13/2018 2108
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 02/20/2018 1254 CMP2 02/14/2018 1745 64527
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg340
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg340
2-Chlorophenol 95-57-8 8270D ND 1ug/kg340
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg340
Chrysene 218-01-9 8270D 2100 1ug/kg71
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg71
Dibenzofuran 132-64-9 8270D ND 1ug/kg340
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg340
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg340
Diethylphthalate 84-66-2 8270D ND 1ug/kg340
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg340
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg340
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg340
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg1800
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg1800
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg710
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg710
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg340
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg340
Fluoranthene 206-44-0 8270D 5000 1ug/kg71
Fluorene 86-73-7 8270D 150 1ug/kg71
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg340
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg340
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1800
Hexachloroethane 67-72-1 8270D ND 1ug/kg340
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 850 1ug/kg71
Isophorone 78-59-1 8270D ND 1ug/kg340
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg71
2-Methylphenol 95-48-7 8270D ND 1ug/kg340
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg710
Naphthalene 91-20-3 8270D ND 1ug/kg71
2-Nitroaniline 88-74-4 8270D ND 1ug/kg710
3-Nitroaniline 99-09-2 8270D ND 1ug/kg710
4-Nitroaniline 100-01-6 8270D ND 1ug/kg710
Nitrobenzene 98-95-3 8270D ND 1ug/kg340
2-Nitrophenol 88-75-5 8270D ND 1ug/kg710
4-Nitrophenol 100-02-7 8270D ND 1ug/kg1800
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg340
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg340
Pentachlorophenol 87-86-5 8270D ND 1ug/kg1800
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 30
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
USTP-1B
TB13013-002
02/09/2018 1510
02/13/2018
Solid
% Solids:74.9 02/13/2018 2108
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 02/20/2018 1254 CMP2 02/14/2018 1745 64527
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Phenanthrene 85-01-8 8270D 2400 1ug/kg71
Phenol 108-95-2 8270D ND 1ug/kg340
Pyrene 129-00-0 8270D 3600 1ug/kg71
Pyridine 110-86-1 8270D ND 1ug/kg340
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg340
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg340
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 51 33-102
2-Fluorophenol 50 35-115
Nitrobenzene-d5 66 22-109
Phenol-d5 61 33-122
Terphenyl-d14 50 41-120
2,4,6-Tribromophenol 43 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 02/14/2018 0943 CJZ 02/13/2018 1548 64355
1 7471B 7471B 1 02/14/2018 1623 SLS 02/14/2018 1404 64390
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Arsenic 7440-38-2 6010D 2.9 1mg/kg0.78
Barium 7440-39-3 6010D 110 1mg/kg1.4
Cadmium 7440-43-9 6010D 0.55 1mg/kg0.26
Chromium 7440-47-3 6010D 40 1mg/kg0.52
Lead 7439-92-1 6010D 83 1mg/kg0.52
Mercury 7439-97-6 7471B 0.66 1mg/kg0.10
Selenium 7782-49-2 6010D ND 1mg/kg1.0
Silver 7440-22-4 6010D ND 1mg/kg0.52
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 30
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 13 of 30
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ64493-001
64493 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Acetone ND 02/14/2018 113020ug/kg1
Benzene ND 02/14/2018 11305.0 ug/kg1
Bromodichloromethane ND 02/14/2018 11305.0 ug/kg1
Bromoform ND 02/14/2018 11305.0 ug/kg1
Bromomethane (Methyl bromide)ND 02/14/2018 11305.0 ug/kg1
2-Butanone (MEK)ND 02/14/2018 113010ug/kg1
Carbon disulfide ND 02/14/2018 11305.0 ug/kg1
Carbon tetrachloride ND 02/14/2018 11305.0 ug/kg1
Chlorobenzene ND 02/14/2018 11305.0 ug/kg1
Chloroethane ND 02/14/2018 11305.0 ug/kg1
Chloroform ND 02/14/2018 11305.0 ug/kg1
Chloromethane (Methyl chloride)ND 02/14/2018 11305.0 ug/kg1
Cyclohexane ND 02/14/2018 11305.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 02/14/2018 11305.0 ug/kg1
Dibromochloromethane ND 02/14/2018 11305.0 ug/kg1
1,2-Dibromoethane (EDB)ND 02/14/2018 11305.0 ug/kg1
1,2-Dichlorobenzene ND 02/14/2018 11305.0 ug/kg1
1,3-Dichlorobenzene ND 02/14/2018 11305.0 ug/kg1
1,4-Dichlorobenzene ND 02/14/2018 11305.0 ug/kg1
Dichlorodifluoromethane ND 02/14/2018 11305.0 ug/kg1
1,1-Dichloroethane ND 02/14/2018 11305.0 ug/kg1
1,2-Dichloroethane ND 02/14/2018 11305.0 ug/kg1
1,1-Dichloroethene ND 02/14/2018 11305.0 ug/kg1
cis-1,2-Dichloroethene ND 02/14/2018 11305.0 ug/kg1
trans-1,2-Dichloroethene ND 02/14/2018 11305.0 ug/kg1
1,2-Dichloropropane ND 02/14/2018 11305.0 ug/kg1
cis-1,3-Dichloropropene ND 02/14/2018 11305.0 ug/kg1
trans-1,3-Dichloropropene ND 02/14/2018 11305.0 ug/kg1
Ethylbenzene ND 02/14/2018 11305.0 ug/kg1
2-Hexanone ND 02/14/2018 113010ug/kg1
Isopropylbenzene ND 02/14/2018 11305.0 ug/kg1
Methyl acetate ND 02/14/2018 11305.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 02/14/2018 11305.0 ug/kg1
4-Methyl-2-pentanone ND 02/14/2018 113010ug/kg1
Methylcyclohexane ND 02/14/2018 11305.0 ug/kg1
Methylene chloride ND 02/14/2018 11305.0 ug/kg1
Styrene ND 02/14/2018 11305.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 02/14/2018 11305.0 ug/kg1
Tetrachloroethene ND 02/14/2018 11305.0 ug/kg1
Toluene ND 02/14/2018 11305.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/14/2018 11305.0 ug/kg1
1,2,4-Trichlorobenzene ND 02/14/2018 11305.0 ug/kg1
1,1,1-Trichloroethane ND 02/14/2018 11305.0 ug/kg1
1,1,2-Trichloroethane ND 02/14/2018 11305.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 30
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ64493-001
64493 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Trichloroethene ND 02/14/2018 11305.0 ug/kg1
Trichlorofluoromethane ND 02/14/2018 11305.0 ug/kg1
Vinyl chloride ND 02/14/2018 11305.0 ug/kg1
Xylenes (total)ND 02/14/2018 11305.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 92 53-142
Bromofluorobenzene 100 47-138
Toluene-d8 100 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 30
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ64493-002
64493 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 83 02/14/2018 10218310060-1401
Benzene 52 02/14/2018 10211055070-1301
Bromodichloromethane 53 02/14/2018 10211055070-1301
Bromoform 52 02/14/2018 10211045070-1301
Bromomethane (Methyl bromide)50 02/14/2018 10211005070-1301
2-Butanone (MEK)93 02/14/2018 10219310060-1401
Carbon disulfide 59 02/14/2018 10211185070-1301
Carbon tetrachloride 52 02/14/2018 10211045070-1301
Chlorobenzene 52 02/14/2018 10211045070-1301
Chloroethane 46 02/14/2018 1021925070-1301
Chloroform 54 02/14/2018 10211085070-1301
Chloromethane (Methyl chloride)51 02/14/2018 10211015060-1401
Cyclohexane 50 02/14/2018 10211005070-1301
1,2-Dibromo-3-chloropropane (DBCP)48 02/14/2018 1021965070-1301
Dibromochloromethane 53 02/14/2018 10211055070-1301
1,2-Dibromoethane (EDB)52 02/14/2018 10211055070-1301
1,2-Dichlorobenzene 52 02/14/2018 10211045070-1301
1,3-Dichlorobenzene 50 02/14/2018 10211015070-1301
1,4-Dichlorobenzene 50 02/14/2018 10211005070-1301
Dichlorodifluoromethane 43 02/14/2018 1021875060-1401
1,1-Dichloroethane 54 02/14/2018 10211085070-1301
1,2-Dichloroethane 54 02/14/2018 10211075070-1301
1,1-Dichloroethene 55 02/14/2018 10211105070-1301
cis-1,2-Dichloroethene 55 02/14/2018 10211105070-1301
trans-1,2-Dichloroethene 55 02/14/2018 10211095070-1301
1,2-Dichloropropane 53 02/14/2018 10211065070-1301
cis-1,3-Dichloropropene 53 02/14/2018 10211065070-1301
trans-1,3-Dichloropropene 52 02/14/2018 10211035070-1301
Ethylbenzene 51 02/14/2018 10211025070-1301
2-Hexanone 85 02/14/2018 10218510070-1301
Isopropylbenzene 52 02/14/2018 10211035070-1301
Methyl acetate 60 02/14/2018 10211205070-1301
Methyl tertiary butyl ether (MTBE)55 02/14/2018 10211115070-1301
4-Methyl-2-pentanone 100 02/14/2018 102110010070-1301
Methylcyclohexane 48 02/14/2018 1021975070-1301
Methylene chloride 54 02/14/2018 10211075070-1301
Styrene 52 02/14/2018 10211045070-1301
1,1,2,2-Tetrachloroethane 49 02/14/2018 1021985070-1301
Tetrachloroethene 51 02/14/2018 10211025070-1301
Toluene 52 02/14/2018 10211055070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 50 02/14/2018 10211005070-1301
1,2,4-Trichlorobenzene 47 02/14/2018 1021955070-1301
1,1,1-Trichloroethane 53 02/14/2018 10211075070-1301
1,1,2-Trichloroethane 50 02/14/2018 10211005070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 30
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ64493-002
64493 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 52 02/14/2018 10211045070-1301
Trichlorofluoromethane 45 02/14/2018 1021915070-1301
Vinyl chloride 46 02/14/2018 1021925070-1301
Xylenes (total)100 02/14/2018 102110110070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 94 53-142
Bromofluorobenzene 101 47-138
Toluene-d8 100 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 17 of 30
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ64527-001
64527 3546
02/14/2018 1745Analytical Method:8270D
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Acenaphthene ND 02/20/2018 10512.7 ug/kg1
Acenaphthylene ND 02/20/2018 10512.7 ug/kg1
Acetophenone ND 02/20/2018 105113ug/kg1
Anthracene ND 02/20/2018 10512.7 ug/kg1
Atrazine ND 02/20/2018 105113ug/kg1
Benzaldehyde ND 02/20/2018 105113ug/kg1
Benzo(a)anthracene ND 02/20/2018 10512.7 ug/kg1
Benzo(a)pyrene ND 02/20/2018 10512.7 ug/kg1
Benzo(b)fluoranthene ND 02/20/2018 10512.7 ug/kg1
Benzo(g,h,i)perylene ND 02/20/2018 10512.7 ug/kg1
Benzo(k)fluoranthene ND 02/20/2018 10512.7 ug/kg1
1,1'-Biphenyl ND 02/20/2018 105113ug/kg1
4-Bromophenyl phenyl ether ND 02/20/2018 105113ug/kg1
Butyl benzyl phthalate ND 02/20/2018 105113ug/kg1
Caprolactam ND 02/20/2018 105113ug/kg1
Carbazole ND 02/20/2018 105113ug/kg1
bis (2-Chloro-1-methylethyl) ether ND 02/20/2018 105113ug/kg1
4-Chloro-3-methyl phenol ND 02/20/2018 105113ug/kg1
4-Chloroaniline ND 02/20/2018 105113ug/kg1
bis(2-Chloroethoxy)methane ND 02/20/2018 105113ug/kg1
bis(2-Chloroethyl)ether ND 02/20/2018 105113ug/kg1
2-Chloronaphthalene ND 02/20/2018 105113ug/kg1
2-Chlorophenol ND 02/20/2018 105113ug/kg1
4-Chlorophenyl phenyl ether ND 02/20/2018 105113ug/kg1
Chrysene ND 02/20/2018 10512.7 ug/kg1
Dibenzo(a,h)anthracene ND 02/20/2018 10512.7 ug/kg1
Dibenzofuran ND 02/20/2018 105113ug/kg1
3,3'-Dichlorobenzidine ND 02/20/2018 105113ug/kg1
2,4-Dichlorophenol ND 02/20/2018 105113ug/kg1
Diethylphthalate ND 02/20/2018 105113ug/kg1
Dimethyl phthalate ND 02/20/2018 105113ug/kg1
2,4-Dimethylphenol ND 02/20/2018 105113ug/kg1
Di-n-butyl phthalate ND 02/20/2018 105113ug/kg1
4,6-Dinitro-2-methylphenol ND 02/20/2018 105167ug/kg1
2,4-Dinitrophenol ND 02/20/2018 105167ug/kg1
2,4-Dinitrotoluene ND 02/20/2018 105127ug/kg1
2,6-Dinitrotoluene ND 02/20/2018 105127ug/kg1
Di-n-octylphthalate ND 02/20/2018 105113ug/kg1
bis(2-Ethylhexyl)phthalate 25 02/20/2018 105113ug/kg1
Fluoranthene ND 02/20/2018 10512.7 ug/kg1
Fluorene ND 02/20/2018 10512.7 ug/kg1
Hexachlorobenzene ND 02/20/2018 105113ug/kg1
Hexachlorobutadiene ND 02/20/2018 105113ug/kg1
Hexachlorocyclopentadiene ND 02/20/2018 105167ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 18 of 30
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ64527-001
64527 3546
02/14/2018 1745Analytical Method:8270D
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Hexachloroethane ND 02/20/2018 105113ug/kg1
Indeno(1,2,3-c,d)pyrene ND 02/20/2018 10512.7 ug/kg1
Isophorone ND 02/20/2018 105113ug/kg1
2-Methylnaphthalene ND 02/20/2018 10512.7 ug/kg1
2-Methylphenol ND 02/20/2018 105113ug/kg1
3+4-Methylphenol ND 02/20/2018 105127ug/kg1
Naphthalene ND 02/20/2018 10512.7 ug/kg1
2-Nitroaniline ND 02/20/2018 105127ug/kg1
3-Nitroaniline ND 02/20/2018 105127ug/kg1
4-Nitroaniline ND 02/20/2018 105127ug/kg1
Nitrobenzene ND 02/20/2018 105113ug/kg1
2-Nitrophenol ND 02/20/2018 105127ug/kg1
4-Nitrophenol ND 02/20/2018 105167ug/kg1
N-Nitrosodi-n-propylamine ND 02/20/2018 105113ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 02/20/2018 105113ug/kg1
Pentachlorophenol ND 02/20/2018 105167ug/kg1
Phenanthrene ND 02/20/2018 10512.7 ug/kg1
Phenol ND 02/20/2018 105113ug/kg1
Pyrene ND 02/20/2018 10512.7 ug/kg1
Pyridine ND 02/20/2018 105113ug/kg1
2,4,5-Trichlorophenol ND 02/20/2018 105113ug/kg1
2,4,6-Trichlorophenol ND 02/20/2018 105113ug/kg1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 58 33-102
2-Fluorophenol 69 35-115
Nitrobenzene-d5 74 22-109
Phenol-d5 80 33-122
Terphenyl-d14 92 41-120
2,4,6-Tribromophenol 54 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 19 of 30
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ64527-002
64527 3546
02/14/2018 1745Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acenaphthene 88 02/20/2018 11156613012-1111
Acenaphthylene 86 02/20/2018 11156513018-901
Acetophenone 98 02/20/2018 11157413030-1301
Anthracene 91 02/20/2018 11156913016-1221
Atrazine 80 02/20/2018 11156013030-1301
Benzaldehyde 130 02/20/2018 11159513030-1301
Benzo(a)anthracene 98 02/20/2018 11157413040-1211
Benzo(a)pyrene 120 02/20/2018 11158713036-1141
Benzo(b)fluoranthene 110 02/20/2018 11157913038-1231
Benzo(g,h,i)perylene 120 02/20/2018 11159213043-1201
Benzo(k)fluoranthene 110 02/20/2018 11158513040-1261
1,1'-Biphenyl 83 02/20/2018 11156213045-1281
4-Bromophenyl phenyl ether 82 02/20/2018 11156213030-1301
Butyl benzyl phthalate 120 02/20/2018 11158913048-1241
Caprolactam 89 02/20/2018 11156713040-1171
Carbazole 91 02/20/2018 11156913047-1251
bis (2-Chloro-1-methylethyl) ether 100 02/20/2018 11157613041-1131
4-Chloro-3-methyl phenol 88 02/20/2018 11156613048-1201
4-Chloroaniline 40 02/20/2018 11153013017-1061
bis(2-Chloroethoxy)methane 96 02/20/2018 11157213038-1151
bis(2-Chloroethyl)ether 99 02/20/2018 11157413046-1221
2-Chloronaphthalene 83 02/20/2018 11156213037-1061
2-Chlorophenol 100 02/20/2018 11157813044-1221
4-Chlorophenyl phenyl ether 80 02/20/2018 11156013032-1071
Chrysene 91 02/20/2018 11156813041-1241
Dibenzo(a,h)anthracene 110 02/20/2018 11158513038-1251
Dibenzofuran 84 02/20/2018 11156313045-1281
3,3'-Dichlorobenzidine 37 02/20/2018 11152813010-1191
2,4-Dichlorophenol 78 02/20/2018 11155913030-961
Diethylphthalate 96 02/20/2018 11157213030-1301
Dimethyl phthalate 91 02/20/2018 11156813024-1271
2,4-Dimethylphenol 140 02/20/2018 111510613030-1301
Di-n-butyl phthalate 100 02/20/2018 11157613035-1081
4,6-Dinitro-2-methylphenol 78 02/20/2018 11155913053-1501
2,4-Dinitrophenol 110 02/20/2018 11154227032-1151
2,4-Dinitrotoluene 87 02/20/2018 11156513040-1301
2,6-Dinitrotoluene 88 02/20/2018 11156613046-1181
Di-n-octylphthalate 120 02/20/2018 11158713049-1181
bis(2-Ethylhexyl)phthalate 130 02/20/2018 11159513033-1231
Fluoranthene 87 02/20/2018 11156613026-1331
Fluorene 88 02/20/2018 11156613019-1081
Hexachlorobenzene 93 02/20/2018 11157013010-1251
Hexachlorobutadiene 68 02/20/2018 11155113047-1161
Hexachlorocyclopentadiene 420 02/20/2018 11156467048-1271
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 20 of 30
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ64527-002
64527 3546
02/14/2018 1745Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Hexachloroethane 85 02/20/2018 11156413018-1541
Indeno(1,2,3-c,d)pyrene 130 02/20/2018 11159513042-1231
Isophorone 100 02/20/2018 11157913030-1301
2-Methylnaphthalene 83 02/20/2018 11156213010-1071
2-Methylphenol 110 02/20/2018 11158213033-1031
3+4-Methylphenol 110 02/20/2018 11158213018-1211
Naphthalene 87 02/20/2018 11156513010-1121
2-Nitroaniline 81 02/20/2018 11156113046-1281
3-Nitroaniline 40 02/20/2018 11153013030-1301
4-Nitroaniline 65 02/20/2018 1115N4913051-1291
Nitrobenzene 100 02/20/2018 11157713049-1421
2-Nitrophenol 89 02/20/2018 11156713033-1141
4-Nitrophenol 250 02/20/2018 11159427027-1381
N-Nitrosodi-n-propylamine 130 02/20/2018 11159613045-1121
N-Nitrosodiphenylamine (Diphenylamine)81 02/20/2018 11156113049-1231
Pentachlorophenol 160 02/20/2018 11156127036-1081
Phenanthrene 91 02/20/2018 11156813016-1231
Phenol 130 02/20/2018 11159413039-1081
Pyrene 100 02/20/2018 11157513034-1211
Pyridine 130 02/20/2018 1115N9613010-741
2,4,5-Trichlorophenol 82 02/20/2018 11156213032-1051
2,4,6-Trichlorophenol 73 02/20/2018 11155513031-1021
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 61 33-102
2-Fluorophenol 71 35-115
Nitrobenzene-d5 73 22-109
Phenol-d5 84 33-122
Terphenyl-d14 78 41-120
2,4,6-Tribromophenol 62 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 21 of 30
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ64355-001
64355 3050B
02/13/2018 1548Analytical Method:6010D
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Arsenic ND 02/14/2018 08540.75 mg/kg1
Barium ND 02/14/2018 08541.3 mg/kg1
Cadmium ND 02/14/2018 08540.25 mg/kg1
Chromium ND 02/14/2018 08540.50 mg/kg1
Lead ND 02/14/2018 08540.50 mg/kg1
Selenium ND 02/14/2018 08541.0 mg/kg1
Silver ND 02/14/2018 08540.50 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 22 of 30
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ64355-002
64355 3050B
02/13/2018 1548Analytical Method:6010D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Arsenic 240 02/14/2018 08599725080-1201
Barium 510 02/14/2018 085910350080-1201
Cadmium 49 02/14/2018 0859985080-1201
Chromium 250 02/14/2018 085910025080-1201
Lead 260 02/14/2018 085910525080-1201
Selenium 49 02/14/2018 0859995080-1201
Silver 48 02/14/2018 0859965080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 23 of 30
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ64390-001
64390 7471B
02/14/2018 1404Analytical Method:7471B
Matrix:Solid
Parameter Result Q LOQ Units Analysis DateDil
Mercury ND 02/14/2018 15460.083 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 24 of 30
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ64390-002
64390 7471B
02/14/2018 1404Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Mercury 0.88 02/14/2018 15481050.83 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 25 of 30
RCRA Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:TB13013-001MS
64390 7471B
02/14/2018 1404Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Mercury 1.2 02/14/2018 1619N1220.99 80-120ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 26 of 30
RCRA Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:TB13013-001MD
64390 7471B
02/14/2018 1404Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/kg)(mg/kg)(mg/kg)
Mercury 1.2 02/14/2018 16211181.0 80-1203.0 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 27 of 30
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 28 of 30
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 29 of 30
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 30 of 30
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina January 21, 2019

D:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\Redevelopment Report\1-21-19 Draft\Appendix D - Soil Profile.rtf

APPENDIX D
SOIL PROFILE

Customer Master Detail List
CUSTOMER
Phone :
Contact Name :
Sales Rep :
Contract No. :
Contract Date :
Expiration Date :
Alpha Sort :
Customer Type :
Tax Jurisdiction :
Fax :
PO BOX 7248
[phone]
() -
333497 - SITE WORKS
Address:SITEWORK
TAXABLE
3rd Party
P.O. No. :
Bill To Type : Consolidated
CHARLOTTE NC 28241
Credit Limit :
Credit Warning :
$ 0.00
$ 0.00
Currency : U.S. Dollar
Email :
Broker :
Intercompany:
CONTRACT DETAILS
Customer:
Contract:5010180937
Start Date:
Expiration Date:
January 24, 2018
July 31, 2018
1
Spriggle, Jill
From:Hill, Ron (South Carolina)
Sent:Thursday, January 25, 2018 8:31 AM
To:Spriggle, Jill; Keller, Bartow; Springs, Quanta; Samples, Amanda; Marston, John
Subject:Re: 5010180937 - East 7th Street, LLC
Approved
Sent via the Samsung Galaxy S®6 active, an AT&T 4G LTE smartphone
-------- Original message --------
From: "Spriggle, Jill" <[e-mail]>
Date: 1/25/18 8:15 AM (GMT-05:00)
To: "Keller, Bartow" <[e-mail]>, "Springs, Quanta"
<[e-mail]>, "Samples, Amanda" <[e-mail]>, "Marston,
John" <[e-mail]>
Cc: "Hill, Ron (South Carolina)" <[e-mail]>
Subject: 5010180937 - East 7th Street, LLC
Bart,
Need landfill approval for the attached new profile.
Ron,
Need LOA approval. See below:
$31.50/ton @ 2,100 tons (1,050 cy) = $66,150.00
Thanks,
Jill Spriggle
Sales Coordinator - Special Waste
1220 Commerce St SW, Suite A
Conover, NC 28613
e [e-mail]
o 828.695.2051
f 828.464.6922 w www.RepublicServices.com
2
1
Spriggle, Jill
From:Keller, Bartow
Sent:Thursday, January 25, 2018 8:18 AM
To:Spriggle, Jill
Cc:Springs, Quanta; Samples, Amanda; Marston, John; Hill, Ron (South Carolina)
Subject:Re: 5010180937 - East 7th Street, LLC
Approved
Sent from my iPhone
> On Jan 25, 2018, at 8:15 AM, Spriggle, Jill <[e-mail]> wrote:
>
> Bart,
>
> Need landfill approval for the attached new profile.
>
> Ron,
>
> Need LOA approval. See below:
>
> $31.50/ton @ 2,100 tons (1,050 cy) = $66,150.00
>
> Thanks,
> Jill Spriggle
> Sales Coordinator - Special Waste
>
> 1220 Commerce St SW, Suite A
> Conover, NC 28613
> e
>[e-mail]<mailto:[e-mail]>
> o 828.695.2051
> f 828.464.6922 w www.RepublicServices.com<http://www.RepublicServices.com/>
>
> [RS_EMAIL_SIGNATURE_LOCKUP_1]
>
> <5010180937_East 7th Street, LLC_2018-01-18.pdf> <image003.jpg>
Contract Number:
Landfill :
Sales Rep
Bill To:
Acct #:Transporter Information:
TBD
Generator Name:
Origin:Additional Notes:
Waste Name:
Trux Waste Code
Inbound Rate:31.50$UOM:Tons
Minimum:31.50$Fee/Taxes
(ERF/FRF/Admin/Local)
Other Charges:
(Trans, Backfill, App, etc.)
East 7th Street, LLC
Mecklenburg, NC
No fees
Name:
Address
Address
Phone
Special Waste Summary Report
Cont. Soil-VG
Site Works
333497
5010 - CMS
5010180937
Impacted Soil
116 - John Marston
ADDITIONALLY APPROVED BY:_____________________________ DATE:______________
ENTERED BY: ______________________________________ DATE:______________Jill Spriggle 1/25/2018
May 2009
SPECIAL WASTE INSPECTION SHEET
Initial Random Suspicious Recertification
Disposal Facility: 5010 - CMS Waste Profile # 5010180937
Generator Name: East 7th Street, LLC
Name of Waste: Impacted Soil
Transporter Name:
Transporter Phone Number:
Driver Name:
Vehicle License Plate Number and State:
Physical Screening
INDICATE YES OR NO FOR EACH OF THE FOLLOWING TESTS AND NOTE ANY DESCREPANCIES. DO THE
CHARACTERISTICS OF THE WASTE MATCH THE PROVIDED INFORMATION ON THE SPECIAL WASTE PROFILE?
Characteristics Profile Yes No Comments and/or Observations:
Color Orange/Tan
Odor None
Physical State Solid
Free Liquids No
Is a Photograph Attached?Initial Load Must Include Photograph
IF WASTE FAILS ONE OR MORE OF THE PHYSICAL SCREENING TESTS, THE WASTE IS DEEMEDUNACCEPTABLE FOR DISPOSAL AND SHOULD BE REJECTED.
Waste Accepted
Inspector Signature Date
Waste Rejected (If Rejected then a Photograph MUST be attached.)
Reasons for RejectionExtraneous and/or Unauthorized Material Suspected Hazardous Waste Suspected PCB Waste
Suspected PCB Waste Free Liquids Does Not Match Profile
Comments
Inspector Signature Date
General Manager or Designee Date
Date:
Time:
Republic Services, Inc.
18500 N. Allied Way, Phoenix, AZ 85054
SPECIAL WASTE DEPARTMENT DECISION
Waste Profile #5010180937 Expiration Date7/31/2018
I. Decision Request:Initial Recertification Change
Disposal Facility: 5010 - CMS Landfill
Generator Name: East 7th Street, LLC
Generator Site Address: 969 East 7th Street
City: Charlotte County: State: NC Zip:
Name of Waste:Impacted Soil
Estimated Annual Volume: 1050 Cubic Yards
II. Special Waste Department Decision:Approved Rejected
Management Method(s): Landfill Solidification Bioremediation Transfer Facility
Problematic Special Waste according to Republic? Yes No
If yes, which one?
Approved by Special Waste Review Committee? Yes No Not Applicable
Precautions, Conditions or Limitations on Approval


Special Waste Analyst Signature: ____________________________Name (Printed):Lynette Gehring
Date: 1/24/2018
III. Facility Decision:Approved Rejected
Precautions, Conditions or Limitations on Approval

By signing below, the General Manager or Designee agrees that a fully executed Special Waste Service Agreement is on file for this profile and that the special waste file is complete.
General Manager or Designee: _____________________________ Name (Printed): _____________________________
Date: 1/24/2018
, PO Box 7248 5010-18-0937 116
5010-18-0937
SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
SUMMIT Engineering,Laboratory &Testing,P.C.
3575 Centre Circle
Fort Mill,SC 28715
Attention:Patrick Lowery
Project Name:E 7th Street Storage
Lot Number:TA19129
Date Completed:01/24/2018
01/24/2018 12:04 PM
Approved and released by:
Project Manager:Lucas Odom
Page 1 of 11
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
SUMMIT Engineering,Laboratory &Testing,P.C.
Lot Number:TA19129
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.
The sample receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved NELAC
standards,the Shealy Environmental Services,Inc.("Shealy")Quality Assurance Management Plan (QAMP),standard operating
procedures (SOPs),and Shealy policies.Any exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the
results page or discussed below.
Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W"qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page 2 of 11
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TA19129

Sample Number Sample ID Matrix Date Sampled Date Received
001 01/19/2018 0700BG-1 Solid 01/19/2018
(1 sample)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 11
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TA19129

Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 11
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
TA19129-001
01/19/2018 0700
01/19/2018
Solid
TCLP Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3010A 6010D 10 01/23/2018 2056 CJZ 01/23/2018 1116 62586 01/22/2018 1728
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Lead 7439-92-1 6010D ND 1mg/L0.10
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 11
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 11
TCLP Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ62586-001
62586 1311/3010A
01/23/2018 1116Analytical Method:6010D
Matrix:Solid
Leachate Date:01/22/2018 1728
Parameter Result Q LOQ Units Analysis DateDil
Lead ND 01/23/2018 20460.10 mg/L10
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 11
TCLP Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ62586-002
62586 1311/3010A
01/23/2018 1116Analytical Method:6010D
Matrix:Solid
Leachate Date:01/22/2018 1728
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Lead 5.4 01/23/2018 20511095.0 80-12010
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 11
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 11
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 11
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 11
SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
SUMMIT Engineering,Laboratory &Testing,P.C.
3575 Centre Circle
Fort Mill,SC 28715
Attention:Patrick Lowery
Project Name:East 7th Street Storage
Project Number:3586.11
Lot Number:SA17067
Date Completed:01/19/2018
Revision Date:01/19/2018
01/22/2018 9:50 AM
Approved and released by:
Project Manager:Lucas Odom
Page 1 of 98
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
SUMMIT Engineering,Laboratory &Testing,P.C.
Lot Number:SA17067
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.
The sample receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved NELAC
standards,the Shealy Environmental Services,Inc.("Shealy")Quality Assurance Management Plan (QAMP),standard operating
procedures (SOPs),and Shealy policies.Any exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the
results page or discussed below.
Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W"qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
SVOCs by GC/MS
The method blank associated with batch 32300 yielded a detection for Bis2-(ethylhexylphthalate).No corrective action is required as all
associated samples are non-detect for this compound.There was one "J"value detection but this is an estimated value recovered
below the PQL.
Report Revision
Per client request,Pyridine has been added to SVOC analysis.
Page 2 of 98
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: SA17067

Sample Number Sample ID Matrix Date Sampled Date Received
001 01/16/2017 1100SB-1-SS Solid 01/17/2017
002 01/16/2017 1145SB-1-SB Solid 01/17/2017
003 01/16/2017 1600SB-2-SS Solid 01/17/2017
004 01/16/2017 1520SB-3-SS Solid 01/17/2017
005 01/16/2017 1520SB-3 DUP Solid 01/17/2017
006 01/16/2017 1420SB-4-SS Solid 01/17/2017
007 01/16/2017 1400SB-5-SB Solid 01/17/2017
008 01/16/2017 1440BG-1 Solid 01/17/2017
009 01/16/2017 1200EQUIPMENT BLANK Aqueous 01/17/2017
010 01/16/2017 1330FIELD BLANK Aqueous 01/17/2017
011 01/16/2017TRIP BLANK Aqueous 01/17/2017
(11 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 98
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: SA17067

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SB-1-SS Solid Acenaphthene 8270D 3.6 ug/kg 8
001 SB-1-SS Solid Acenaphthylene 8270D 10 ug/kg 8
001 SB-1-SS Solid Acetophenone 8270D 4.3 J ug/kg 8
001 SB-1-SS Solid Anthracene 8270D 22 ug/kg 8
001 SB-1-SS Solid Benzo(a)anthracene 8270D 84 ug/kg 8
001 SB-1-SS Solid Benzo(a)pyrene 8270D 85 ug/kg 8
001 SB-1-SS Solid Benzo(b)fluoranthene 8270D 110 ug/kg 8
001 SB-1-SS Solid Benzo(g,h,i)perylene 8270D 32 ug/kg 9
001 SB-1-SS Solid Benzo(k)fluoranthene 8270D 47 ug/kg 9
001 SB-1-SS Solid Carbazole 8270D 14 J ug/kg 9
001 SB-1-SS Solid Chrysene 8270D 83 ug/kg 9
001 SB-1-SS Solid Dibenzofuran 8270D 11 J ug/kg 9
001 SB-1-SS Solid Fluoranthene 8270D 170 ug/kg 9
001 SB-1-SS Solid Fluorene 8270D 4.8 ug/kg 9
001 SB-1-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 33 ug/kg 9
001 SB-1-SS Solid 2-Methylnaphthalene 8270D 17 ug/kg 9
001 SB-1-SS Solid Naphthalene 8270D 21 ug/kg 10
001 SB-1-SS Solid Phenanthrene 8270D 95 ug/kg 10
001 SB-1-SS Solid Pyrene 8270D 140 ug/kg 10
001 SB-1-SS Solid Arsenic 6010C 2.2 mg/kg 10
001 SB-1-SS Solid Barium 6010C 71 mg/kg 10
001 SB-1-SS Solid Cadmium 6010C 0.053 J mg/kg 10
001 SB-1-SS Solid Chromium 6010C 46 mg/kg 10
001 SB-1-SS Solid Lead 6010C 20 mg/kg 10
001 SB-1-SS Solid Mercury 7471B 0.080 J mg/kg 10
002 SB-1-SB Solid Arsenic 6010C 1.3 J mg/kg 15
002 SB-1-SB Solid Barium 6010C 27 mg/kg 15
002 SB-1-SB Solid Chromium 6010C 0.96 J mg/kg 15
003 SB-2-SS Solid Acenaphthylene 8270D 1.2 J ug/kg 18
003 SB-2-SS Solid Anthracene 8270D 1.1 J ug/kg 18
003 SB-2-SS Solid Benzo(a)anthracene 8270D 4.6 ug/kg 18
003 SB-2-SS Solid Benzo(a)pyrene 8270D 4.8 ug/kg 18
003 SB-2-SS Solid Benzo(b)fluoranthene 8270D 8.3 ug/kg 18
003 SB-2-SS Solid Benzo(g,h,i)perylene 8270D 3.4 ug/kg 19
003 SB-2-SS Solid Benzo(k)fluoranthene 8270D 2.3 J ug/kg 19
003 SB-2-SS Solid Chrysene 8270D 5.6 ug/kg 19
003 SB-2-SS Solid Fluoranthene 8270D 6.7 ug/kg 19
003 SB-2-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 2.6 J ug/kg 19
003 SB-2-SS Solid 2-Methylnaphthalene 8270D 17 ug/kg 19
003 SB-2-SS Solid Naphthalene 8270D 13 ug/kg 20
003 SB-2-SS Solid Phenanthrene 8270D 9.9 ug/kg 20
003 SB-2-SS Solid Pyrene 8270D 6.2 ug/kg 20
003 SB-2-SS Solid Arsenic 6010C 2.8 J mg/kg 20
003 SB-2-SS Solid Barium 6010C 93 mg/kg 20
003 SB-2-SS Solid Chromium 6010C 61 mg/kg 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 98
Detection Summary (Continued)
Lot Number: SA17067
Sample Sample ID Matrix Parameter Method Result Q Units Page
003 SB-2-SS Solid Lead 6010C 16 mg/kg 20
003 SB-2-SS Solid Mercury 7471B 0.056 J mg/kg 20
004 SB-3-SS Solid Anthracene 8270D 1.1 J ug/kg 23
004 SB-3-SS Solid Benzaldehyde 8270D 4.0 J ug/kg 23
004 SB-3-SS Solid Benzo(a)anthracene 8270D 5.6 ug/kg 23
004 SB-3-SS Solid Benzo(a)pyrene 8270D 6.4 ug/kg 23
004 SB-3-SS Solid Benzo(b)fluoranthene 8270D 10 ug/kg 23
004 SB-3-SS Solid Benzo(g,h,i)perylene 8270D 3.0 J ug/kg 24
004 SB-3-SS Solid Benzo(k)fluoranthene 8270D 3.1 ug/kg 24
004 SB-3-SS Solid Chrysene 8270D 7.1 ug/kg 24
004 SB-3-SS Solid Fluoranthene 8270D 9.7 ug/kg 24
004 SB-3-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 2.6 J ug/kg 24
004 SB-3-SS Solid 2-Methylnaphthalene 8270D 7.3 ug/kg 24
004 SB-3-SS Solid Naphthalene 8270D 5.3 ug/kg 25
004 SB-3-SS Solid Phenanthrene 8270D 8.8 ug/kg 25
004 SB-3-SS Solid Pyrene 8270D 8.7 ug/kg 25
004 SB-3-SS Solid Arsenic 6010C 2.4 J mg/kg 25
004 SB-3-SS Solid Barium 6010C 37 mg/kg 25
004 SB-3-SS Solid Chromium 6010C 75 mg/kg 25
004 SB-3-SS Solid Lead 6010C 8.6 mg/kg 25
004 SB-3-SS Solid Mercury 7471B 0.051 J mg/kg 25
005 SB-3 DUP Solid Benzaldehyde 8270D 5.3 J ug/kg 28
005 SB-3 DUP Solid Benzo(a)anthracene 8270D 4.1 ug/kg 28
005 SB-3 DUP Solid Benzo(a)pyrene 8270D 3.5 ug/kg 28
005 SB-3 DUP Solid Benzo(b)fluoranthene 8270D 6.3 ug/kg 28
005 SB-3 DUP Solid Benzo(g,h,i)perylene 8270D 1.9 J ug/kg 29
005 SB-3 DUP Solid Chrysene 8270D 3.3 ug/kg 29
005 SB-3 DUP Solid Fluoranthene 8270D 4.5 ug/kg 29
005 SB-3 DUP Solid Indeno(1,2,3-c,d)pyrene 8270D 1.6 J ug/kg 29
005 SB-3 DUP Solid 2-Methylnaphthalene 8270D 4.4 ug/kg 29
005 SB-3 DUP Solid Naphthalene 8270D 3.1 J ug/kg 30
005 SB-3 DUP Solid Phenanthrene 8270D 4.3 ug/kg 30
005 SB-3 DUP Solid Pyrene 8270D 4.1 ug/kg 30
005 SB-3 DUP Solid Arsenic 6010C 2.8 J mg/kg 30
005 SB-3 DUP Solid Barium 6010C 40 mg/kg 30
005 SB-3 DUP Solid Chromium 6010C 93 mg/kg 30
005 SB-3 DUP Solid Lead 6010C 14 mg/kg 30
005 SB-3 DUP Solid Mercury 7471B 0.24 mg/kg 30
006 SB-4-SS Solid Acenaphthene 8270D 190 ug/kg 33
006 SB-4-SS Solid Anthracene 8270D 270 ug/kg 33
006 SB-4-SS Solid Benzo(a)anthracene 8270D 820 ug/kg 33
006 SB-4-SS Solid Benzo(a)pyrene 8270D 760 ug/kg 33
006 SB-4-SS Solid Benzo(b)fluoranthene 8270D 1100 ug/kg 34
006 SB-4-SS Solid Benzo(g,h,i)perylene 8270D 140 ug/kg 34
006 SB-4-SS Solid Benzo(k)fluoranthene 8270D 340 ug/kg 34
006 SB-4-SS Solid 1,1'-Biphenyl 8270D 9.1 J ug/kg 34
006 SB-4-SS Solid Carbazole 8270D 160 ug/kg 34
006 SB-4-SS Solid Chrysene 8270D 800 ug/kg 34
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 98
Detection Summary (Continued)
Lot Number: SA17067
Sample Sample ID Matrix Parameter Method Result Q Units Page
006 SB-4-SS Solid Dibenzofuran 8270D 81 ug/kg 34
006 SB-4-SS Solid Fluoranthene 8270D 2000 ug/kg 34
006 SB-4-SS Solid Fluorene 8270D 140 ug/kg 34
006 SB-4-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 160 ug/kg 34
006 SB-4-SS Solid 2-Methylnaphthalene 8270D 33 ug/kg 35
006 SB-4-SS Solid Naphthalene 8270D 71 ug/kg 35
006 SB-4-SS Solid Phenanthrene 8270D 1700 ug/kg 35
006 SB-4-SS Solid Pyrene 8270D 1500 ug/kg 35
006 SB-4-SS Solid Arsenic 6010C 1.3 mg/kg 35
006 SB-4-SS Solid Barium 6010C 36 mg/kg 35
006 SB-4-SS Solid Chromium 6010C 6.8 mg/kg 35
006 SB-4-SS Solid Lead 6010C 6.4 mg/kg 36
006 SB-4-SS Solid Mercury 7471B 0.019 J mg/kg 36
007 SB-5-SB Solid 2-Methylnaphthalene 8270D 2.2 J ug/kg 39
007 SB-5-SB Solid Naphthalene 8270D 2.0 J ug/kg 40
007 SB-5-SB Solid Arsenic 6010C 0.97 mg/kg 40
007 SB-5-SB Solid Barium 6010C 27 mg/kg 40
007 SB-5-SB Solid Chromium 6010C 1.3 mg/kg 40
007 SB-5-SB Solid Lead 6010C 2.0 mg/kg 40
008 BG-1 Solid Acenaphthylene 8270D 8.4 ug/kg 43
008 BG-1 Solid Anthracene 8270D 12 ug/kg 43
008 BG-1 Solid Benzaldehyde 8270D 5.6 J ug/kg 43
008 BG-1 Solid Benzo(a)anthracene 8270D 100 ug/kg 43
008 BG-1 Solid Benzo(a)pyrene 8270D 93 ug/kg 43
008 BG-1 Solid Benzo(b)fluoranthene 8270D 180 ug/kg 43
008 BG-1 Solid Benzo(g,h,i)perylene 8270D 17 ug/kg 44
008 BG-1 Solid Benzo(k)fluoranthene 8270D 60 ug/kg 44
008 BG-1 Solid Chrysene 8270D 94 ug/kg 44
008 BG-1 Solid bis(2-Ethylhexyl)phthalate 8270D 4.0 BJ ug/kg 44
008 BG-1 Solid Fluoranthene 8270D 170 ug/kg 44
008 BG-1 Solid Fluorene 8270D 1.6 J ug/kg 44
008 BG-1 Solid Indeno(1,2,3-c,d)pyrene 8270D 21 ug/kg 44
008 BG-1 Solid 2-Methylnaphthalene 8270D 11 ug/kg 44
008 BG-1 Solid Naphthalene 8270D 9.8 ug/kg 45
008 BG-1 Solid Phenanthrene 8270D 41 ug/kg 45
008 BG-1 Solid Pyrene 8270D 140 ug/kg 45
008 BG-1 Solid Arsenic 6010C 2.6 mg/kg 45
008 BG-1 Solid Barium 6010C 160 mg/kg 45
008 BG-1 Solid Cadmium 6010C 0.23 J mg/kg 45
008 BG-1 Solid Chromium 6010C 25 mg/kg 45
008 BG-1 Solid Lead 6010C 130 mg/kg 45
008 BG-1 Solid Mercury 7471B 0.18 mg/kg 45
010 FIELD BLANK Aqueous Acetone 8260B 2.2 J ug/L 52
(136 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/25/2017 0100 ECP 32474 5.79
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1321
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1358 ECB 31997 5.24
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.723
Benzene 71-43-2 8260B ND 1ug/kg2.35.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.35.8
Bromoform 75-25-2 8260B ND 1ug/kg2.35.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.35.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.723
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.35.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.35.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.35.8
Chloroethane 75-00-3 8260B ND 1ug/kg2.35.8
Chloroform 67-66-3 8260B ND 1ug/kg2.35.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.35.8
Cyclohexane 110-82-7 8260B ND 1ug/kg2.35.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.35.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.35.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.35.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.35.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.35.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.35.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.35.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.35.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.35.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.35.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.35.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.35.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.35.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.35.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.35.8
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1358 ECB 31997 5.24
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.712
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.35.8
Methyl acetate 79-20-9 8260B ND 1ug/kg2.35.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.35.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.712
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.35.8
Methylene chloride 75-09-2 8260B ND 1ug/kg2.35.8
Styrene 100-42-5 8260B ND 1ug/kg2.35.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.35.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.35.8
Toluene 108-88-3 8260B ND 1ug/kg2.35.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.35.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.35.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.35.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.35.8
Trichloroethene 79-01-6 8260B ND 1ug/kg2.35.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.35.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.35.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.712
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 106 47-138
Toluene-d8 107 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1650 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D 3.6 1ug/kg1.03.3
Acenaphthylene 208-96-8 8270D 10 1ug/kg1.23.3
Acetophenone 98-86-2 8270D 4.3 J 1ug/kg1.716
Anthracene 120-12-7 8270D 22 1ug/kg0.623.3
Atrazine 1912-24-9 8270D ND 1ug/kg1.216
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.216
Benzo(a)anthracene 56-55-3 8270D 84 1ug/kg0.723.3
Benzo(a)pyrene 50-32-8 8270D 85 1ug/kg0.813.3
Benzo(b)fluoranthene 205-99-2 8270D 110 1ug/kg0.613.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1650 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D 32 1ug/kg0.803.3
Benzo(k)fluoranthene 207-08-9 8270D 47 1ug/kg0.593.3
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.216
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.116
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8516
Caprolactam 105-60-2 8270D ND 1ug/kg2.916
Carbazole 86-74-8 8270D 14 J 1ug/kg1.016
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.616
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.316
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.516
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8616
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.316
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg3.116
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.616
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9816
Chrysene 218-01-9 8270D 83 1ug/kg0.553.3
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.623.3
Dibenzofuran 132-64-9 8270D 11 J 1ug/kg1.216
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.416
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.616
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9816
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg9.116
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.716
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.416
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.482
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg4.082
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.933
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.633
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2916
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5516
Fluoranthene 206-44-0 8270D 170 1ug/kg0.513.3
Fluorene 86-73-7 8270D 4.8 1ug/kg0.703.3
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.216
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.116
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.682
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.316
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 33 1ug/kg1.23.3
Isophorone 78-59-1 8270D ND 1ug/kg1.516
2-Methylnaphthalene 91-57-6 8270D 17 1ug/kg1.23.3
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.316
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1650 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg4.033
Naphthalene 91-20-3 8270D 21 1ug/kg1.23.3
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.533
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.533
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.933
Nitrobenzene 98-95-3 8270D ND 1ug/kg2.016
2-Nitrophenol 88-75-5 8270D ND 1ug/kg2.033
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2582
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.316
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.216
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.582
Phenanthrene 85-01-8 8270D 95 1ug/kg0.883.3
Phenol 108-95-2 8270D ND 1ug/kg1.516
Pyrene 129-00-0 8270D 140 1ug/kg0.613.3
Pyridine 110-86-1 8270D ND 1ug/kg16
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.116
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.216
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 61 33-102
2-Fluorophenol 63 35-115
Nitrobenzene-d5 55 22-109
Phenol-d5 73 33-122
Terphenyl-d14 58 41-120
2,4,6-Tribromophenol 65 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1843 SLS 01/17/2017 2128 31784
1 3050B 6010C 2 01/20/2017 2127 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 2.2 1mg/kg0.411.3
Barium 7440-39-3 6010C 71 1mg/kg0.252.3
Cadmium 7440-43-9 6010C 0.053 J 1mg/kg0.0440.44
Chromium 7440-47-3 6010C 46 1mg/kg0.130.89
Lead 7439-92-1 6010C 20 1mg/kg0.390.89
Mercury 7439-97-6 7471B 0.080 J 1mg/kg0.00690.091
Selenium 7782-49-2 6010C ND 1mg/kg0.721.8
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1843 SLS 01/17/2017 2128 31784
1 3050B 6010C 2 01/20/2017 2127 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/kg0.140.89
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/20/2017 1641 ECB 32172 5.55
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1219
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 108 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1421 ECB 31997 5.04
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.221
Benzene 71-43-2 8260B ND 1ug/kg2.15.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.15.2
Bromoform 75-25-2 8260B ND 1ug/kg2.15.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.15.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.221
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.15.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.15.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.15.2
Chloroethane 75-00-3 8260B ND 1ug/kg2.15.2
Chloroform 67-66-3 8260B ND 1ug/kg2.15.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.15.2
Cyclohexane 110-82-7 8260B ND 1ug/kg2.15.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.15.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.15.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.15.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.15.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.15.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.15.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.15.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.15.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.15.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.15.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.15.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.15.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.15.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.15.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.15.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.15.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1421 ECB 31997 5.04
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.210
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.15.2
Methyl acetate 79-20-9 8260B ND 1ug/kg2.15.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.15.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.210
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.15.2
Methylene chloride 75-09-2 8260B ND 1ug/kg2.15.2
Styrene 100-42-5 8260B ND 1ug/kg2.15.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.15.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.15.2
Toluene 108-88-3 8260B ND 1ug/kg2.15.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.15.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.15.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.15.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.15.2
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.15.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.15.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.210
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 106 47-138
Toluene-d8 104 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1714 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.852.8
Acenaphthylene 208-96-8 8270D ND 1ug/kg0.972.8
Acetophenone 98-86-2 8270D ND 1ug/kg1.413
Anthracene 120-12-7 8270D ND 1ug/kg0.522.8
Atrazine 1912-24-9 8270D ND 1ug/kg1.013
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.013
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg0.602.8
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg0.672.8
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg0.512.8
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 13 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1714 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg0.662.8
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg0.492.8
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg0.9713
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg0.9413
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.7013
Caprolactam 105-60-2 8270D ND 1ug/kg2.513
Carbazole 86-74-8 8270D ND 1ug/kg0.8613
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.313
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.113
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.213
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.7113
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.113
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.613
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.113
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.8213
Chrysene 218-01-9 8270D ND 1ug/kg0.462.8
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.522.8
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.013
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.013
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.313
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.8213
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg7.613
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.213
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.013
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.068
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.468
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.528
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.128
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2513
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.4613
Fluoranthene 206-44-0 8270D ND 1ug/kg0.432.8
Fluorene 86-73-7 8270D ND 1ug/kg0.582.8
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.013
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg1.713
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.368
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.113
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg1.02.8
Isophorone 78-59-1 8270D ND 1ug/kg1.213
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg1.02.8
2-Methylphenol 95-48-7 8270D ND 1ug/kg3.613
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1714 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.428
Naphthalene 91-20-3 8270D ND 1ug/kg0.992.8
2-Nitroaniline 88-74-4 8270D ND 1ug/kg3.828
3-Nitroaniline 99-09-2 8270D ND 1ug/kg3.828
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.128
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.613
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.628
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2168
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.113
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.013
Pentachlorophenol 87-86-5 8270D ND 1ug/kg5.468
Phenanthrene 85-01-8 8270D ND 1ug/kg0.742.8
Phenol 108-95-2 8270D ND 1ug/kg1.213
Pyrene 129-00-0 8270D ND 1ug/kg0.512.8
Pyridine 110-86-1 8270D ND 1ug/kg13
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg0.8913
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg0.9813
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 50 33-102
2-Fluorophenol 56 35-115
Nitrobenzene-d5 46 22-109
Phenol-d5 65 33-122
Terphenyl-d14 51 41-120
2,4,6-Tribromophenol 53 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1850 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2132 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 1.3 J 1mg/kg0.812.7
Barium 7440-39-3 6010C 27 1mg/kg0.514.6
Cadmium 7440-43-9 6010C ND 1mg/kg0.0890.89
Chromium 7440-47-3 6010C 0.96 J 1mg/kg0.261.8
Lead 7439-92-1 6010C ND 1mg/kg0.771.8
Mercury 7439-97-6 7471B ND 1mg/kg0.00640.084
Selenium 7782-49-2 6010C ND 1mg/kg1.43.5
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1850 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2132 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/kg0.281.8
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/20/2017 1703 ECB 32172 5.41
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1423
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 105 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1443 ECB 31997 5.46
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.623
Benzene 71-43-2 8260B ND 1ug/kg2.35.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.35.8
Bromoform 75-25-2 8260B ND 1ug/kg2.35.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.35.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.623
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.35.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.35.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.35.8
Chloroethane 75-00-3 8260B ND 1ug/kg2.35.8
Chloroform 67-66-3 8260B ND 1ug/kg2.35.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.35.8
Cyclohexane 110-82-7 8260B ND 1ug/kg2.35.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.35.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.35.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.35.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.35.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.35.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.35.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.35.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.35.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.35.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.35.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.35.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.35.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.35.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.35.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.35.8
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 17 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1443 ECB 31997 5.46
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.612
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.35.8
Methyl acetate 79-20-9 8260B ND 1ug/kg2.35.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.35.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.612
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.35.8
Methylene chloride 75-09-2 8260B ND 1ug/kg2.35.8
Styrene 100-42-5 8260B ND 1ug/kg2.35.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.35.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.35.8
Toluene 108-88-3 8260B ND 1ug/kg2.35.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.35.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.35.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.35.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.35.8
Trichloroethene 79-01-6 8260B ND 1ug/kg2.35.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.35.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.35.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.612
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 53-142
Bromofluorobenzene 107 47-138
Toluene-d8 106 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1738 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D ND 1ug/kg1.03.3
Acenaphthylene 208-96-8 8270D 1.2 J 1ug/kg1.23.3
Acetophenone 98-86-2 8270D ND 1ug/kg1.716
Anthracene 120-12-7 8270D 1.1 J 1ug/kg0.633.3
Atrazine 1912-24-9 8270D ND 1ug/kg1.216
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.216
Benzo(a)anthracene 56-55-3 8270D 4.6 1ug/kg0.733.3
Benzo(a)pyrene 50-32-8 8270D 4.8 1ug/kg0.823.3
Benzo(b)fluoranthene 205-99-2 8270D 8.3 1ug/kg0.623.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 18 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1738 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D 3.4 1ug/kg0.803.3
Benzo(k)fluoranthene 207-08-9 8270D 2.3 J 1ug/kg0.593.3
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.216
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.116
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8516
Caprolactam 105-60-2 8270D ND 1ug/kg3.016
Carbazole 86-74-8 8270D ND 1ug/kg1.016
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.616
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.416
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.516
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8616
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.416
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg3.116
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.616
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9916
Chrysene 218-01-9 8270D 5.6 1ug/kg0.563.3
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.633.3
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.216
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.516
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.616
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9916
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg9.116
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.716
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.516
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.583
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg4.183
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg3.033
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.633
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.3016
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5616
Fluoranthene 206-44-0 8270D 6.7 1ug/kg0.523.3
Fluorene 86-73-7 8270D ND 1ug/kg0.703.3
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.216
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.116
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.683
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.416
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 2.6 J 1ug/kg1.23.3
Isophorone 78-59-1 8270D ND 1ug/kg1.516
2-Methylnaphthalene 91-57-6 8270D 17 1ug/kg1.23.3
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.316
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 19 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1738 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg4.133
Naphthalene 91-20-3 8270D 13 1ug/kg1.23.3
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.633
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.633
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.933
Nitrobenzene 98-95-3 8270D ND 1ug/kg2.016
2-Nitrophenol 88-75-5 8270D ND 1ug/kg2.033
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2683
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.416
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.216
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.583
Phenanthrene 85-01-8 8270D 9.9 1ug/kg0.893.3
Phenol 108-95-2 8270D ND 1ug/kg1.516
Pyrene 129-00-0 8270D 6.2 1ug/kg0.623.3
Pyridine 110-86-1 8270D ND 1ug/kg16
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.116
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.216
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 52 33-102
2-Fluorophenol 53 35-115
Nitrobenzene-d5 48 22-109
Phenol-d5 60 33-122
Terphenyl-d14 53 41-120
2,4,6-Tribromophenol 57 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1853 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2136 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 2.8 J 1mg/kg1.23.9
Barium 7440-39-3 6010C 93 1mg/kg0.746.7
Cadmium 7440-43-9 6010C ND 1mg/kg0.131.3
Chromium 7440-47-3 6010C 61 1mg/kg0.372.6
Lead 7439-92-1 6010C 16 1mg/kg1.12.6
Mercury 7439-97-6 7471B 0.056 J 1mg/kg0.00710.094
Selenium 7782-49-2 6010C ND 1mg/kg2.15.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 20 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1853 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2136 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/kg0.412.6
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 21 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/25/2017 0038 ECP 32474 4.63
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1524
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1506 ECB 31997 5.55
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.120
Benzene 71-43-2 8260B ND 1ug/kg2.05.1
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.05.1
Bromoform 75-25-2 8260B ND 1ug/kg2.05.1
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.05.1
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.120
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.05.1
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.05.1
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.05.1
Chloroethane 75-00-3 8260B ND 1ug/kg2.05.1
Chloroform 67-66-3 8260B ND 1ug/kg2.05.1
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.05.1
Cyclohexane 110-82-7 8260B ND 1ug/kg2.05.1
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.05.1
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.05.1
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.05.1
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.05.1
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.05.1
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.05.1
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.05.1
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.05.1
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.05.1
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.1
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.05.1
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.05.1
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.05.1
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.05.1
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.05.1
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.05.1
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 22 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1506 ECB 31997 5.55
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.110
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.05.1
Methyl acetate 79-20-9 8260B ND 1ug/kg2.05.1
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.05.1
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.110
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.05.1
Methylene chloride 75-09-2 8260B ND 1ug/kg2.05.1
Styrene 100-42-5 8260B ND 1ug/kg2.05.1
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.05.1
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.05.1
Toluene 108-88-3 8260B ND 1ug/kg2.05.1
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.05.1
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.05.1
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.05.1
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.05.1
Trichloroethene 79-01-6 8260B ND 1ug/kg2.05.1
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.05.1
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.05.1
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.110
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 104 47-138
Toluene-d8 105 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1803 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.943.1
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.1
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D 1.1 J 1ug/kg0.583.1
Atrazine 1912-24-9 8270D ND 1ug/kg1.115
Benzaldehyde 100-52-7 8270D 4.0 J 1ug/kg1.115
Benzo(a)anthracene 56-55-3 8270D 5.6 1ug/kg0.673.1
Benzo(a)pyrene 50-32-8 8270D 6.4 1ug/kg0.753.1
Benzo(b)fluoranthene 205-99-2 8270D 10 1ug/kg0.573.1
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 23 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1803 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D 3.0 J 1ug/kg0.743.1
Benzo(k)fluoranthene 207-08-9 8270D 3.1 1ug/kg0.543.1
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.015
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.7815
Caprolactam 105-60-2 8270D ND 1ug/kg2.715
Carbazole 86-74-8 8270D ND 1ug/kg0.9515
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.215
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.7915
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.215
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.815
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.415
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9115
Chrysene 218-01-9 8270D 7.1 1ug/kg0.513.1
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.583.1
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.115
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9115
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.415
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.515
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.376
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.776
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.731
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.431
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2715
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5115
Fluoranthene 206-44-0 8270D 9.7 1ug/kg0.483.1
Fluorene 86-73-7 8270D ND 1ug/kg0.653.1
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.115
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg1.915
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.576
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.215
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 2.6 J 1ug/kg1.13.1
Isophorone 78-59-1 8270D ND 1ug/kg1.415
2-Methylnaphthalene 91-57-6 8270D 7.3 1ug/kg1.13.1
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.015
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 24 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1803 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.731
Naphthalene 91-20-3 8270D 5.3 1ug/kg1.13.1
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.231
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.231
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.531
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.815
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.831
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2376
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.215
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.115
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.076
Phenanthrene 85-01-8 8270D 8.8 1ug/kg0.823.1
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D 8.7 1ug/kg0.573.1
Pyridine 110-86-1 8270D ND 1ug/kg15
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg0.9915
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 52 33-102
2-Fluorophenol 56 35-115
Nitrobenzene-d5 48 22-109
Phenol-d5 63 33-122
Terphenyl-d14 48 41-120
2,4,6-Tribromophenol 56 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1855 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/23/2017 1426 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 2.4 J 1mg/kg0.903.0
Barium 7440-39-3 6010C 37 1mg/kg0.565.1
Cadmium 7440-43-9 6010C ND 1mg/kg0.0980.98
Chromium 7440-47-3 6010C 75 1mg/kg0.282.0
Lead 7439-92-1 6010C 8.6 1mg/kg0.862.0
Mercury 7439-97-6 7471B 0.051 J 1mg/kg0.00680.090
Selenium 7782-49-2 6010C ND 1mg/kg1.63.9
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 25 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1855 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/23/2017 1426 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/kg0.312.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 26 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/25/2017 0015 ECP 32474 5.86
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1321
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 107 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1528 ECB 31997 5.88
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.221
Benzene 71-43-2 8260B ND 1ug/kg2.15.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.15.2
Bromoform 75-25-2 8260B ND 1ug/kg2.15.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.15.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.221
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.15.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.15.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.15.2
Chloroethane 75-00-3 8260B ND 1ug/kg2.15.2
Chloroform 67-66-3 8260B ND 1ug/kg2.15.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.15.2
Cyclohexane 110-82-7 8260B ND 1ug/kg2.15.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.15.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.15.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.15.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.15.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.15.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.15.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.15.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.15.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.15.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.15.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.15.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.15.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.15.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.15.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.15.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.15.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 27 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1528 ECB 31997 5.88
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.210
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.15.2
Methyl acetate 79-20-9 8260B ND 1ug/kg2.15.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.15.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.210
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.15.2
Methylene chloride 75-09-2 8260B ND 1ug/kg2.15.2
Styrene 100-42-5 8260B ND 1ug/kg2.15.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.15.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.15.2
Toluene 108-88-3 8260B ND 1ug/kg2.15.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.15.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.15.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.15.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.15.2
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.15.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.15.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.210
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 105 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1828 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.993.2
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.2
Acetophenone 98-86-2 8270D ND 1ug/kg1.716
Anthracene 120-12-7 8270D ND 1ug/kg0.613.2
Atrazine 1912-24-9 8270D ND 1ug/kg1.216
Benzaldehyde 100-52-7 8270D 5.3 J 1ug/kg1.216
Benzo(a)anthracene 56-55-3 8270D 4.1 1ug/kg0.703.2
Benzo(a)pyrene 50-32-8 8270D 3.5 1ug/kg0.793.2
Benzo(b)fluoranthene 205-99-2 8270D 6.3 1ug/kg0.603.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 28 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1828 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D 1.9 J 1ug/kg0.783.2
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg0.573.2
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.116
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.116
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8216
Caprolactam 105-60-2 8270D ND 1ug/kg2.916
Carbazole 86-74-8 8270D ND 1ug/kg1.016
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.616
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.316
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.416
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8416
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.316
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg3.016
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.516
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9616
Chrysene 218-01-9 8270D 3.3 1ug/kg0.543.2
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.613.2
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.216
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.416
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.616
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9616
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.816
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.616
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.416
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.480
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.980
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.932
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.532
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2916
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5416
Fluoranthene 206-44-0 8270D 4.5 1ug/kg0.503.2
Fluorene 86-73-7 8270D ND 1ug/kg0.683.2
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.216
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.016
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.680
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.316
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 1.6 J 1ug/kg1.23.2
Isophorone 78-59-1 8270D ND 1ug/kg1.416
2-Methylnaphthalene 91-57-6 8270D 4.4 1ug/kg1.23.2
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.216
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 29 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1828 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.932
Naphthalene 91-20-3 8270D 3.1 J 1ug/kg1.23.2
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.432
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.432
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.832
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.916
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.932
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2580
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.316
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.216
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.380
Phenanthrene 85-01-8 8270D 4.3 1ug/kg0.863.2
Phenol 108-95-2 8270D ND 1ug/kg1.416
Pyrene 129-00-0 8270D 4.1 1ug/kg0.603.2
Pyridine 110-86-1 8270D ND 1ug/kg16
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.016
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.116
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 56 33-102
2-Fluorophenol 54 35-115
Nitrobenzene-d5 53 22-109
Phenol-d5 59 33-122
Terphenyl-d14 51 41-120
2,4,6-Tribromophenol 58 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1857 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2145 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 2.8 J 1mg/kg1.24.0
Barium 7440-39-3 6010C 40 1mg/kg0.767.0
Cadmium 7440-43-9 6010C ND 1mg/kg0.131.3
Chromium 7440-47-3 6010C 93 1mg/kg0.392.7
Lead 7439-92-1 6010C 14 1mg/kg1.22.7
Mercury 7439-97-6 7471B 0.24 1mg/kg0.00760.10
Selenium 7782-49-2 6010C ND 1mg/kg2.25.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 30 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1857 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2145 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/kg0.422.7
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 31 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/24/2017 2353 ECP 32474 6.13
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1219
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1551 ECB 31997 5.47
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.322
Benzene 71-43-2 8260B ND 1ug/kg2.25.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.25.4
Bromoform 75-25-2 8260B ND 1ug/kg2.25.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.25.4
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.322
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.25.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.25.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.25.4
Chloroethane 75-00-3 8260B ND 1ug/kg2.25.4
Chloroform 67-66-3 8260B ND 1ug/kg2.25.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.25.4
Cyclohexane 110-82-7 8260B ND 1ug/kg2.25.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.25.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.25.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.25.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.25.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.25.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.25.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.25.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.25.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.25.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.25.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.25.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.25.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.25.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.25.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.25.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.25.4
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 32 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1551 ECB 31997 5.47
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.311
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.25.4
Methyl acetate 79-20-9 8260B ND 1ug/kg2.25.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.25.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.311
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.25.4
Methylene chloride 75-09-2 8260B ND 1ug/kg2.25.4
Styrene 100-42-5 8260B ND 1ug/kg2.25.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.25.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.25.4
Toluene 108-88-3 8260B ND 1ug/kg2.25.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.25.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.25.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.25.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.25.4
Trichloroethene 79-01-6 8260B ND 1ug/kg2.25.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.25.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.25.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.311
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 53-142
Bromofluorobenzene 103 47-138
Toluene-d8 103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1852 JCG 01/23/2017 1403 32300
2 3546 8270D 10 01/25/2017 1021 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D 190 1ug/kg0.953.1
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.1
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D 270 1ug/kg0.583.1
Atrazine 1912-24-9 8270D ND 1ug/kg1.115
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.115
Benzo(a)anthracene 56-55-3 8270D 820 2ug/kg6.731
Benzo(a)pyrene 50-32-8 8270D 760 2ug/kg7.531
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 33 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1852 JCG 01/23/2017 1403 32300
2 3546 8270D 10 01/25/2017 1021 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(b)fluoranthene 205-99-2 8270D 1100 2ug/kg5.731
Benzo(g,h,i)perylene 191-24-2 8270D 140 1ug/kg0.743.1
Benzo(k)fluoranthene 207-08-9 8270D 340 1ug/kg0.553.1
1,1'-Biphenyl 92-52-4 8270D 9.1 J 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.015
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.7915
Caprolactam 105-60-2 8270D ND 1ug/kg2.715
Carbazole 86-74-8 8270D 160 1ug/kg0.9615
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.315
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8015
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.315
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.815
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.415
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9115
Chrysene 218-01-9 8270D 800 2ug/kg5.131
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.583.1
Dibenzofuran 132-64-9 8270D 81 1ug/kg1.115
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9115
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.415
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.515
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.376
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.876
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.731
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.431
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2715
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5115
Fluoranthene 206-44-0 8270D 2000 2ug/kg4.831
Fluorene 86-73-7 8270D 140 1ug/kg0.653.1
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.115
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg1.915
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.576
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.315
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 160 1ug/kg1.13.1
Isophorone 78-59-1 8270D ND 1ug/kg1.415
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 34 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1852 JCG 01/23/2017 1403 32300
2 3546 8270D 10 01/25/2017 1021 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Methylnaphthalene 91-57-6 8270D 33 1ug/kg1.13.1
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.015
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.831
Naphthalene 91-20-3 8270D 71 1ug/kg1.13.1
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.231
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.231
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.631
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.815
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.831
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2476
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.315
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.115
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.076
Phenanthrene 85-01-8 8270D 1700 2ug/kg8.231
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D 1500 2ug/kg5.731
Pyridine 110-86-1 8270D ND 1ug/kg15
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg0.9915
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
2-Fluorobiphenyl 57 33-102 76 33-102
2-Fluorophenol 56 35-115 57 35-115
Nitrobenzene-d5 52 22-109 66 22-109
Phenol-d5 63 33-122 65 33-122
Terphenyl-d14 48 41-120 84 41-120
2,4,6-Tribromophenol 61 30-117 46 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1900 SLS 01/17/2017 2128 31784
1 3050B 6010C 1 01/20/2017 2150 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 1.3 1mg/kg0.230.76
Barium 7440-39-3 6010C 36 1mg/kg0.141.3
Cadmium 7440-43-9 6010C ND 1mg/kg0.0250.25
Chromium 7440-47-3 6010C 6.8 1mg/kg0.0730.51
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 35 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1900 SLS 01/17/2017 2128 31784
1 3050B 6010C 1 01/20/2017 2150 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Lead 7439-92-1 6010C 6.4 1mg/kg0.220.51
Mercury 7439-97-6 7471B 0.019 J 1mg/kg0.00690.091
Selenium 7782-49-2 6010C ND 1mg/kg0.411.0
Silver 7440-22-4 6010C ND 1mg/kg0.0800.51
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 36 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/24/2017 2330 ECP 32474 4.96
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1524
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 118 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1613 ECB 31997 5.14
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.723
Benzene 71-43-2 8260B ND 1ug/kg2.35.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.35.9
Bromoform 75-25-2 8260B ND 1ug/kg2.35.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.35.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.723
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.35.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.35.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.35.9
Chloroethane 75-00-3 8260B ND 1ug/kg2.35.9
Chloroform 67-66-3 8260B ND 1ug/kg2.35.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.35.9
Cyclohexane 110-82-7 8260B ND 1ug/kg2.35.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.35.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.35.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.35.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.35.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.35.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.35.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.35.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.35.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.35.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.35.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.35.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.35.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.35.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.35.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.35.9
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 37 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1613 ECB 31997 5.14
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.712
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.35.9
Methyl acetate 79-20-9 8260B ND 1ug/kg2.35.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.35.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.712
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.35.9
Methylene chloride 75-09-2 8260B ND 1ug/kg2.35.9
Styrene 100-42-5 8260B ND 1ug/kg2.35.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.35.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.35.9
Toluene 108-88-3 8260B ND 1ug/kg2.35.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.35.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.35.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.35.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.35.9
Trichloroethene 79-01-6 8260B ND 1ug/kg2.35.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.35.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.35.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.712
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 53-142
Bromofluorobenzene 109 47-138
Toluene-d8 103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1917 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.973.2
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.2
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D ND 1ug/kg0.603.2
Atrazine 1912-24-9 8270D ND 1ug/kg1.215
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.215
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg0.693.2
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg0.773.2
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg0.593.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 38 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1917 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg0.763.2
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg0.563.2
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.115
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8115
Caprolactam 105-60-2 8270D ND 1ug/kg2.815
Carbazole 86-74-8 8270D ND 1ug/kg0.9915
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.315
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8215
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.315
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.915
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.515
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9415
Chrysene 218-01-9 8270D ND 1ug/kg0.533.2
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.603.2
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.215
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9415
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.715
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.615
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.379
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.979
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.832
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.532
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2815
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5315
Fluoranthene 206-44-0 8270D ND 1ug/kg0.493.2
Fluorene 86-73-7 8270D ND 1ug/kg0.673.2
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.215
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.015
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.579
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.315
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg1.23.2
Isophorone 78-59-1 8270D ND 1ug/kg1.415
2-Methylnaphthalene 91-57-6 8270D 2.2 J 1ug/kg1.23.2
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.115
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 39 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1917 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.932
Naphthalene 91-20-3 8270D 2.0 J 1ug/kg1.13.2
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.332
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.332
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.732
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.915
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.932
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2479
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.315
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.215
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.279
Phenanthrene 85-01-8 8270D ND 1ug/kg0.853.2
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D ND 1ug/kg0.593.2
Pyridine 110-86-1 8270D ND 1ug/kg15
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.015
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 52 33-102
2-Fluorophenol 61 35-115
Nitrobenzene-d5 49 22-109
Phenol-d5 65 33-122
Terphenyl-d14 53 41-120
2,4,6-Tribromophenol 55 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1902 SLS 01/17/2017 2128 31784
1 3050B 6010C 1 01/20/2017 2154 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 0.97 1mg/kg0.230.74
Barium 7440-39-3 6010C 27 1mg/kg0.141.3
Cadmium 7440-43-9 6010C ND 1mg/kg0.0250.25
Chromium 7440-47-3 6010C 1.3 1mg/kg0.0710.50
Lead 7439-92-1 6010C 2.0 1mg/kg0.220.50
Mercury 7439-97-6 7471B ND 1mg/kg0.00740.097
Selenium 7782-49-2 6010C ND 1mg/kg0.400.99
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 40 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1902 SLS 01/17/2017 2128 31784
1 3050B 6010C 1 01/20/2017 2154 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/kg0.0780.50
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 41 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/24/2017 2308 ECP 32474 4.65
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1525
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 113 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1636 ECB 31997 5.54
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/kg4.221
Benzene 71-43-2 8260B ND 1ug/kg2.15.3
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.15.3
Bromoform 75-25-2 8260B ND 1ug/kg2.15.3
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.15.3
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.221
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.15.3
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.15.3
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.15.3
Chloroethane 75-00-3 8260B ND 1ug/kg2.15.3
Chloroform 67-66-3 8260B ND 1ug/kg2.15.3
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.15.3
Cyclohexane 110-82-7 8260B ND 1ug/kg2.15.3
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.15.3
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.15.3
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.15.3
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.15.3
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.15.3
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.15.3
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.15.3
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.15.3
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.15.3
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.15.3
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.15.3
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.15.3
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.15.3
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.15.3
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.15.3
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.15.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 42 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1636 ECB 31997 5.54
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.211
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.15.3
Methyl acetate 79-20-9 8260B ND 1ug/kg2.15.3
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.15.3
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.211
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.15.3
Methylene chloride 75-09-2 8260B ND 1ug/kg2.15.3
Styrene 100-42-5 8260B ND 1ug/kg2.15.3
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.15.3
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.15.3
Toluene 108-88-3 8260B ND 1ug/kg2.15.3
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.15.3
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.15.3
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.15.3
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.15.3
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.3
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.15.3
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.15.3
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.211
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 100 47-138
Toluene-d8 103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1941 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.973.2
Acenaphthylene 208-96-8 8270D 8.4 1ug/kg1.13.2
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D 12 1ug/kg0.603.2
Atrazine 1912-24-9 8270D ND 1ug/kg1.215
Benzaldehyde 100-52-7 8270D 5.6 J 1ug/kg1.215
Benzo(a)anthracene 56-55-3 8270D 100 1ug/kg0.693.2
Benzo(a)pyrene 50-32-8 8270D 93 1ug/kg0.773.2
Benzo(b)fluoranthene 205-99-2 8270D 180 1ug/kg0.583.2
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 43 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1941 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D 17 1ug/kg0.763.2
Benzo(k)fluoranthene 207-08-9 8270D 60 1ug/kg0.563.2
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.115
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8115
Caprolactam 105-60-2 8270D ND 1ug/kg2.815
Carbazole 86-74-8 8270D ND 1ug/kg0.9815
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.315
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8215
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.315
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.915
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.515
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9415
Chrysene 218-01-9 8270D 94 1ug/kg0.533.2
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.603.2
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.215
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9415
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.715
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.615
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.378
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.978
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.832
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.532
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2815
bis(2-Ethylhexyl)phthalate 117-81-7 8270D 4.0 BJ 1ug/kg0.5315
Fluoranthene 206-44-0 8270D 170 1ug/kg0.493.2
Fluorene 86-73-7 8270D 1.6 J 1ug/kg0.673.2
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.115
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.015
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.578
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.315
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 21 1ug/kg1.23.2
Isophorone 78-59-1 8270D ND 1ug/kg1.415
2-Methylnaphthalene 91-57-6 8270D 11 1ug/kg1.23.2
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.115
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 44 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1941 JCG 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.932
Naphthalene 91-20-3 8270D 9.8 1ug/kg1.13.2
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.332
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.332
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.732
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.915
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.932
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2478
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.315
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.215
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.278
Phenanthrene 85-01-8 8270D 41 1ug/kg0.843.2
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D 140 1ug/kg0.583.2
Pyridine 110-86-1 8270D ND 1ug/kg15
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.015
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 56 33-102
2-Fluorophenol 59 35-115
Nitrobenzene-d5 51 22-109
Phenol-d5 63 33-122
Terphenyl-d14 54 41-120
2,4,6-Tribromophenol 60 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1904 SLS 01/17/2017 2128 31784
1 3050B 6010C 2 01/20/2017 2159 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C 2.6 1mg/kg0.300.99
Barium 7440-39-3 6010C 160 1mg/kg0.191.7
Cadmium 7440-43-9 6010C 0.23 J 1mg/kg0.0330.33
Chromium 7440-47-3 6010C 25 1mg/kg0.0950.66
Lead 7439-92-1 6010C 130 1mg/kg0.290.66
Mercury 7439-97-6 7471B 0.18 1mg/kg0.00640.084
Selenium 7782-49-2 6010C ND 1mg/kg0.541.3
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 45 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1904 SLS 01/17/2017 2128 31784
1 3050B 6010C 2 01/20/2017 2159 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/kg0.100.66
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 46 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS (SIM)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B (SIM)1 01/18/2017 1126 TML 31846
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/L1.03.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 40-170
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1036 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/L2.020
Benzene 71-43-2 8260B ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.401.0
Bromoform 75-25-2 8260B ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.401.0
Chloroethane 75-00-3 8260B ND 1ug/L0.402.0
Chloroform 67-66-3 8260B ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.401.0
Cyclohexane 110-82-7 8260B ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.402.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 47 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1036 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Hexanone 591-78-6 8260B ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260B ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.401.0
Styrene 100-42-5 8260B ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.401.0
Toluene 108-88-3 8260B ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 70-130
Bromofluorobenzene 103 70-130
Toluene-d8 99 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 01/23/2017 1737 RBH 01/19/2017 1436 32000
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 8270D ND 1ug/L0.0400.20
Acenaphthylene 208-96-8 8270D ND 1ug/L0.0400.20
Acetophenone 98-86-2 8270D ND 1ug/L0.231.0
Anthracene 120-12-7 8270D ND 1ug/L0.0600.20
Atrazine 1912-24-9 8270D ND 1ug/L0.201.0
Benzaldehyde 100-52-7 8270D ND 1ug/L0.275.0
Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.0400.20
Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.0700.20
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.0400.20
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 48 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 01/23/2017 1737 RBH 01/19/2017 1436 32000
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.0400.20
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L0.0400.20
1,1'-Biphenyl 92-52-4 8270D ND 1ug/L0.211.0
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L0.151.0
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L0.215.0
Caprolactam 105-60-2 8270D ND 1ug/L0.715.0
Carbazole 86-74-8 8270D ND 1ug/L0.0401.0
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L0.261.0
4-Chloroaniline 106-47-8 8270D ND 1ug/L0.131.0
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L0.0601.0
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L0.161.0
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/L0.171.0
2-Chloronaphthalene 91-58-7 8270D ND 1ug/L0.151.0
2-Chlorophenol 95-57-8 8270D ND 1ug/L0.151.0
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L0.161.0
Chrysene 218-01-9 8270D ND 1ug/L0.0300.20
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L0.0300.20
Dibenzofuran 132-64-9 8270D ND 1ug/L0.161.0
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L0.815.0
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/L0.191.0
Diethylphthalate 84-66-2 8270D ND 1ug/L0.195.0
Dimethyl phthalate 131-11-3 8270D ND 1ug/L0.185.0
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/L0.151.0
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L0.425.0
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L0.895.0
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/L1.35.0
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L0.362.0
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L0.342.0
Di-n-octylphthalate 117-84-0 8270D ND 1ug/L0.485.0
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/L0.385.0
Fluoranthene 206-44-0 8270D ND 1ug/L0.0770.20
Fluorene 86-73-7 8270D ND 1ug/L0.0300.20
Hexachlorobenzene 118-74-1 8270D ND 1ug/L0.151.0
Hexachlorobutadiene 87-68-3 8270D ND 1ug/L0.171.0
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L1.15.0
Hexachloroethane 67-72-1 8270D ND 1ug/L0.171.0
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L0.0400.20
Isophorone 78-59-1 8270D ND 1ug/L0.221.0
1-Methylnaphthalene 90-12-0 8270D ND 1ug/L0.0300.20
2-Methylnaphthalene 91-57-6 8270D ND 1ug/L0.0400.20
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 49 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 01/23/2017 1737 RBH 01/19/2017 1436 32000
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Methylphenol 95-48-7 8270D ND 1ug/L0.211.0
3+4-Methylphenol 106-44-5 8270D ND 1ug/L0.462.0
Naphthalene 91-20-3 8270D ND 1ug/L0.0500.20
2-Nitroaniline 88-74-4 8270D ND 1ug/L0.662.0
3-Nitroaniline 99-09-2 8270D ND 1ug/L0.152.0
4-Nitroaniline 100-01-6 8270D ND 1ug/L1.32.0
Nitrobenzene 98-95-3 8270D ND 1ug/L0.171.0
2-Nitrophenol 88-75-5 8270D ND 1ug/L0.442.0
4-Nitrophenol 100-02-7 8270D ND 1ug/L2.15.0
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L0.281.0
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/L0.841.0
Pentachlorophenol 87-86-5 8270D ND 1ug/L1.35.0
Phenanthrene 85-01-8 8270D ND 1ug/L0.0600.20
Phenol 108-95-2 8270D ND 1ug/L0.191.0
Pyrene 129-00-0 8270D ND 1ug/L0.0750.20
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L0.191.0
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L0.221.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 53 37-129
2-Fluorophenol 50 24-127
Nitrobenzene-d5 54 38-127
Phenol-d5 54 28-128
Terphenyl-d14 63 10-148
2,4,6-Tribromophenol 58 41-144
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 01/18/2017 1636 COH 01/18/2017 1222 31803
1 3005A 6010C 1 01/19/2017 2151 CJZ 01/18/2017 0917 31799
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Arsenic 7440-38-2 6010C ND 1mg/L0.00220.015
Barium 7440-39-3 6010C ND 1mg/L0.00190.025
Cadmium 7440-43-9 6010C ND 1mg/L0.000540.0050
Chromium 7440-47-3 6010C ND 1mg/L0.000720.010
Lead 7439-92-1 6010C ND 1mg/L0.00470.010
Mercury 7439-97-6 7470A ND 1mg/L0.0000280.00010
Selenium 7782-49-2 6010C ND 1mg/L0.00850.020
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 50 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 01/18/2017 1636 COH 01/18/2017 1222 31803
1 3005A 6010C 1 01/19/2017 2151 CJZ 01/18/2017 0917 31799
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Silver 7440-22-4 6010C ND 1mg/L0.00210.010
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 51 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
FIELD BLANK
SA17067-010
01/16/2017 1330
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1059 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B 2.2 J 1ug/L2.020
Benzene 71-43-2 8260B ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.401.0
Bromoform 75-25-2 8260B ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.401.0
Chloroethane 75-00-3 8260B ND 1ug/L0.402.0
Chloroform 67-66-3 8260B ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.401.0
Cyclohexane 110-82-7 8260B ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.402.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260B ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260B ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.401.0
Styrene 100-42-5 8260B ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.401.0
Toluene 108-88-3 8260B ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 52 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
FIELD BLANK
SA17067-010
01/16/2017 1330
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1059 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 70-130
Bromofluorobenzene 99 70-130
Toluene-d8 99 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 53 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TRIP BLANK
SA17067-011
01/16/2017
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1123 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acetone 67-64-1 8260B ND 1ug/L2.020
Benzene 71-43-2 8260B ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.401.0
Bromoform 75-25-2 8260B ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.401.0
Chloroethane 75-00-3 8260B ND 1ug/L0.402.0
Chloroform 67-66-3 8260B ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.401.0
Cyclohexane 110-82-7 8260B ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.402.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.401.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260B ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260B ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.401.0
Styrene 100-42-5 8260B ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.401.0
Toluene 108-88-3 8260B ND 1ug/L0.401.0
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
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Page 54 of 98
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TRIP BLANK
SA17067-011
01/16/2017
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1123 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 90 70-130
Bromofluorobenzene 99 70-130
Toluene-d8 100 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
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Page 55 of 98
QC Summary
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Page 56 of 98
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31828-001
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 01/18/2017 0947202.0 ug/L1
Benzene ND 01/18/2017 09471.0 0.40 ug/L1
Bromodichloromethane ND 01/18/2017 09471.0 0.40 ug/L1
Bromoform ND 01/18/2017 09471.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 01/18/2017 09472.0 0.40 ug/L1
2-Butanone (MEK)ND 01/18/2017 0947102.0 ug/L1
Carbon disulfide ND 01/18/2017 09471.0 0.40 ug/L1
Carbon tetrachloride ND 01/18/2017 09471.0 0.40 ug/L1
Chlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
Chloroethane ND 01/18/2017 09472.0 0.40 ug/L1
Chloroform ND 01/18/2017 09471.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 01/18/2017 09471.0 0.40 ug/L1
Cyclohexane ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/18/2017 09471.0 0.40 ug/L1
Dibromochloromethane ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
1,3-Dichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
1,4-Dichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
Dichlorodifluoromethane ND 01/18/2017 09472.0 0.40 ug/L1
1,1-Dichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
1,1-Dichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dichloropropane ND 01/18/2017 09471.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 01/18/2017 09471.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 01/18/2017 09471.0 0.40 ug/L1
Ethylbenzene ND 01/18/2017 09471.0 0.40 ug/L1
2-Hexanone ND 01/18/2017 0947102.0 ug/L1
Isopropylbenzene ND 01/18/2017 09471.0 0.40 ug/L1
Methyl acetate ND 01/18/2017 09471.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 01/18/2017 09471.0 0.40 ug/L1
4-Methyl-2-pentanone ND 01/18/2017 0947102.0 ug/L1
Methylcyclohexane ND 01/18/2017 09475.0 0.40 ug/L1
Methylene chloride ND 01/18/2017 09471.0 0.40 ug/L1
Styrene ND 01/18/2017 09471.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 01/18/2017 09471.0 0.40 ug/L1
Tetrachloroethene ND 01/18/2017 09471.0 0.40 ug/L1
Toluene ND 01/18/2017 09471.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/18/2017 09471.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
1,1,1-Trichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
1,1,2-Trichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 57 of 98
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31828-001
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Trichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
Trichlorofluoromethane ND 01/18/2017 09471.0 0.40 ug/L1
Vinyl chloride ND 01/18/2017 09471.0 0.40 ug/L1
Xylenes (total)ND 01/18/2017 09471.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 91 70-130
Bromofluorobenzene 100 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 58 of 98
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31828-002
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 100 01/18/2017 084210010060-1401
Benzene 48 01/18/2017 0842965070-1301
Bromodichloromethane 49 01/18/2017 0842975070-1301
Bromoform 39 01/18/2017 0842795070-1301
Bromomethane (Methyl bromide)52 01/18/2017 08421045060-1401
2-Butanone (MEK)99 01/18/2017 08429910060-1401
Carbon disulfide 50 01/18/2017 0842995060-1401
Carbon tetrachloride 48 01/18/2017 0842965070-1301
Chlorobenzene 49 01/18/2017 0842995070-1301
Chloroethane 50 01/18/2017 0842995060-1401
Chloroform 46 01/18/2017 0842935070-1301
Chloromethane (Methyl chloride)48 01/18/2017 0842975060-1401
Cyclohexane 46 01/18/2017 0842915070-1301
1,2-Dibromo-3-chloropropane (DBCP)43 01/18/2017 0842865070-1301
Dibromochloromethane 49 01/18/2017 0842975070-1301
1,2-Dibromoethane (EDB)48 01/18/2017 0842965070-1301
1,2-Dichlorobenzene 47 01/18/2017 0842945070-1301
1,3-Dichlorobenzene 47 01/18/2017 0842945070-1301
1,4-Dichlorobenzene 45 01/18/2017 0842905070-1301
Dichlorodifluoromethane 62 01/18/2017 08421245060-1401
1,1-Dichloroethane 49 01/18/2017 0842975070-1301
1,2-Dichloroethane 48 01/18/2017 0842955070-1301
1,1-Dichloroethene 48 01/18/2017 0842965070-1301
cis-1,2-Dichloroethene 48 01/18/2017 0842955070-1301
trans-1,2-Dichloroethene 47 01/18/2017 0842945070-1301
1,2-Dichloropropane 49 01/18/2017 0842995070-1301
cis-1,3-Dichloropropene 47 01/18/2017 0842945070-1301
trans-1,3-Dichloropropene 45 01/18/2017 0842915070-1301
Ethylbenzene 52 01/18/2017 08421045070-1301
2-Hexanone 98 01/18/2017 08429810060-1401
Isopropylbenzene 47 01/18/2017 0842945070-1301
Methyl acetate 51 01/18/2017 08421015015-1281
Methyl tertiary butyl ether (MTBE)47 01/18/2017 0842935070-1301
4-Methyl-2-pentanone 96 01/18/2017 08429610060-1401
Methylcyclohexane 47 01/18/2017 0842945070-1301
Methylene chloride 45 01/18/2017 0842905070-1301
Styrene 46 01/18/2017 0842935070-1301
1,1,2,2-Tetrachloroethane 46 01/18/2017 0842935060-1401
Tetrachloroethene 52 01/18/2017 08421035070-1301
Toluene 51 01/18/2017 08421025070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 47 01/18/2017 0842945070-1301
1,2,4-Trichlorobenzene 45 01/18/2017 0842915070-1301
1,1,1-Trichloroethane 48 01/18/2017 0842955070-1301
1,1,2-Trichloroethane 48 01/18/2017 0842955070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 59 of 98
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31828-002
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 48 01/18/2017 0842975070-1301
Trichlorofluoromethane 52 01/18/2017 08421045070-1301
Vinyl chloride 51 01/18/2017 08421035070-1301
Xylenes (total)98 01/18/2017 08429810070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 85 70-130
Bromofluorobenzene 104 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 60 of 98
Volatile Organic Compounds by GC/MS (SIM) - MB
Batch:Prep Method:
Sample ID:SQ31846-001
31846 5030B
Analytical Method:8260B (SIM)
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
1,4-Dioxane ND 01/18/2017 10533.0 1.0 ug/L1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 102 40-170
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 61 of 98
Volatile Organic Compounds by GC/MS (SIM) - LCS
Batch:Prep Method:
Sample ID:SQ31846-002
31846 5030B
Analytical Method:8260B (SIM)
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,4-Dioxane 55 01/18/2017 10191105070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 102 40-170
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 62 of 98
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31997-001
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acetone ND 01/19/2017 1026204.0 ug/kg1
Benzene ND 01/19/2017 10265.0 2.0 ug/kg1
Bromodichloromethane ND 01/19/2017 10265.0 2.0 ug/kg1
Bromoform ND 01/19/2017 10265.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 01/19/2017 10265.0 2.0 ug/kg1
2-Butanone (MEK)ND 01/19/2017 1026204.0 ug/kg1
Carbon disulfide ND 01/19/2017 10265.0 2.0 ug/kg1
Carbon tetrachloride ND 01/19/2017 10265.0 2.0 ug/kg1
Chlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
Chloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
Chloroform ND 01/19/2017 10265.0 2.0 ug/kg1
Chloromethane (Methyl chloride)ND 01/19/2017 10265.0 2.0 ug/kg1
Cyclohexane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/19/2017 10265.0 2.0 ug/kg1
Dibromochloromethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dibromoethane (EDB)ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
1,3-Dichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
1,4-Dichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
Dichlorodifluoromethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,1-Dichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,1-Dichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
cis-1,2-Dichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
trans-1,2-Dichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dichloropropane ND 01/19/2017 10265.0 2.0 ug/kg1
cis-1,3-Dichloropropene ND 01/19/2017 10265.0 2.0 ug/kg1
trans-1,3-Dichloropropene ND 01/19/2017 10265.0 2.0 ug/kg1
Ethylbenzene ND 01/19/2017 10265.0 2.0 ug/kg1
2-Hexanone ND 01/19/2017 1026104.0 ug/kg1
Isopropylbenzene ND 01/19/2017 10265.0 2.0 ug/kg1
Methyl acetate ND 01/19/2017 10265.0 2.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 01/19/2017 10265.0 2.0 ug/kg1
4-Methyl-2-pentanone ND 01/19/2017 1026104.0 ug/kg1
Methylcyclohexane ND 01/19/2017 10265.0 2.0 ug/kg1
Methylene chloride ND 01/19/2017 10265.0 2.0 ug/kg1
Styrene ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
Tetrachloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
Toluene ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2,4-Trichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,1-Trichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,2-Trichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 63 of 98
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31997-001
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Trichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
Trichlorofluoromethane ND 01/19/2017 10265.0 2.0 ug/kg1
Vinyl chloride ND 01/19/2017 10265.0 2.0 ug/kg1
Xylenes (total)ND 01/19/2017 1026104.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 112 47-138
Toluene-d8 106 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 64 of 98
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31997-002
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 01/19/2017 092710010060-1401
Benzene 45 01/19/2017 0927905069-1231
Bromodichloromethane 49 01/19/2017 0927995069-1211
Bromoform 47 01/19/2017 0927945061-1191
Bromomethane (Methyl bromide)59 01/19/2017 09271175010-1681
2-Butanone (MEK)88 01/19/2017 09278810057-1481
Carbon disulfide 49 01/19/2017 0927985058-1221
Carbon tetrachloride 47 01/19/2017 0927955058-1361
Chlorobenzene 50 01/19/2017 09271005059-1291
Chloroethane 52 01/19/2017 09271055060-1401
Chloroform 47 01/19/2017 0927955071-1251
Chloromethane (Methyl chloride)48 01/19/2017 0927965034-1341
Cyclohexane 46 01/19/2017 0927925053-1391
1,2-Dibromo-3-chloropropane (DBCP)44 01/19/2017 0927875055-1251
Dibromochloromethane 49 01/19/2017 0927995066-1191
1,2-Dibromoethane (EDB)47 01/19/2017 0927945074-1241
1,2-Dichlorobenzene 49 01/19/2017 0927985057-1311
1,3-Dichlorobenzene 48 01/19/2017 0927975051-1341
1,4-Dichlorobenzene 49 01/19/2017 0927985052-1331
Dichlorodifluoromethane 60 01/19/2017 09271205010-1571
1,1-Dichloroethane 48 01/19/2017 0927955071-1271
1,2-Dichloroethane 49 01/19/2017 0927995067-1291
1,1-Dichloroethene 44 01/19/2017 0927885069-1381
cis-1,2-Dichloroethene 45 01/19/2017 0927915070-1221
trans-1,2-Dichloroethene 47 01/19/2017 0927935068-1311
1,2-Dichloropropane 48 01/19/2017 0927965072-1241
cis-1,3-Dichloropropene 49 01/19/2017 0927985070-1261
trans-1,3-Dichloropropene 50 01/19/2017 09271005070-1241
Ethylbenzene 48 01/19/2017 0927965059-1281
2-Hexanone 92 01/19/2017 09279210054-1371
Isopropylbenzene 50 01/19/2017 0927995050-1361
Methyl acetate 44 01/19/2017 0927885059-1371
Methyl tertiary butyl ether (MTBE)45 01/19/2017 0927895070-1301
4-Methyl-2-pentanone 95 01/19/2017 09279510060-1341
Methylcyclohexane 45 01/19/2017 0927895041-1441
Methylene chloride 47 01/19/2017 0927955070-1301
Styrene 50 01/19/2017 09271005054-1361
1,1,2,2-Tetrachloroethane 46 01/19/2017 0927915069-1321
Tetrachloroethene 49 01/19/2017 0927985045-1501
Toluene 49 01/19/2017 0927975061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 48 01/19/2017 0927965049-1361
1,2,4-Trichlorobenzene 46 01/19/2017 0927935034-1451
1,1,1-Trichloroethane 47 01/19/2017 0927955063-1281
1,1,2-Trichloroethane 47 01/19/2017 0927945055-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 65 of 98
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31997-002
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 45 01/19/2017 0927915062-1261
Trichlorofluoromethane 48 01/19/2017 0927965045-1381
Vinyl chloride 50 01/19/2017 09271005042-1321
Xylenes (total)100 01/19/2017 092710310058-1281
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 95 53-142
Bromofluorobenzene 110 47-138
Toluene-d8 107 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 66 of 98
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-001DU
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Acetone 5.5 01/19/2017 182820020ND1
Benzene ND 01/19/2017 18280.00 20ND1
Bromodichloromethane ND 01/19/2017 18280.00 20ND1
Bromoform ND 01/19/2017 18280.00 20ND1
Bromomethane (Methyl bromide)ND 01/19/2017 18280.00 20ND1
2-Butanone (MEK)ND 01/19/2017 18280.00 20ND1
Carbon disulfide ND 01/19/2017 18280.00 20ND1
Carbon tetrachloride ND 01/19/2017 18280.00 20ND1
Chlorobenzene ND 01/19/2017 18280.00 20ND1
Chloroethane ND 01/19/2017 18280.00 20ND1
Chloroform ND 01/19/2017 18280.00 20ND1
Chloromethane (Methyl chloride)ND 01/19/2017 18280.00 20ND1
Cyclohexane ND 01/19/2017 18280.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/19/2017 18280.00 20ND1
Dibromochloromethane ND 01/19/2017 18280.00 20ND1
1,2-Dibromoethane (EDB)ND 01/19/2017 18280.00 20ND1
1,2-Dichlorobenzene ND 01/19/2017 18280.00 20ND1
1,3-Dichlorobenzene ND 01/19/2017 18280.00 20ND1
1,4-Dichlorobenzene ND 01/19/2017 18280.00 20ND1
Dichlorodifluoromethane ND 01/19/2017 18280.00 20ND1
1,1-Dichloroethane ND 01/19/2017 18280.00 20ND1
1,2-Dichloroethane ND 01/19/2017 18280.00 20ND1
1,1-Dichloroethene ND 01/19/2017 18280.00 20ND1
cis-1,2-Dichloroethene ND 01/19/2017 18280.00 20ND1
trans-1,2-Dichloroethene ND 01/19/2017 18280.00 20ND1
1,2-Dichloropropane ND 01/19/2017 18280.00 20ND1
cis-1,3-Dichloropropene ND 01/19/2017 18280.00 20ND1
trans-1,3-Dichloropropene ND 01/19/2017 18280.00 20ND1
Ethylbenzene ND 01/19/2017 18280.00 20ND1
2-Hexanone ND 01/19/2017 18280.00 20ND1
Isopropylbenzene ND 01/19/2017 18280.00 20ND1
Methyl acetate ND 01/19/2017 18280.00 20ND1
Methyl tertiary butyl ether (MTBE)ND 01/19/2017 18280.00 20ND1
4-Methyl-2-pentanone ND 01/19/2017 18280.00 20ND1
Methylcyclohexane ND 01/19/2017 18280.00 20ND1
Methylene chloride ND 01/19/2017 18280.00 20ND1
Styrene ND 01/19/2017 18280.00 20ND1
1,1,2,2-Tetrachloroethane ND 01/19/2017 18280.00 20ND1
Tetrachloroethene ND 01/19/2017 18280.00 20ND1
Toluene ND 01/19/2017 18280.00 20ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/19/2017 18280.00 20ND1
1,2,4-Trichlorobenzene ND 01/19/2017 18280.00 20ND1
1,1,1-Trichloroethane ND 01/19/2017 18280.00 20ND1
1,1,2-Trichloroethane ND 01/19/2017 18280.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 67 of 98
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-001DU
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Trichloroethene ND 01/19/2017 18280.00 20ND1
Trichlorofluoromethane ND 01/19/2017 18280.00 20ND1
Vinyl chloride ND 01/19/2017 18280.00 20ND1
Xylenes (total)ND 01/19/2017 18280.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 107 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 68 of 98
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-002MS
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 94 01/19/2017 18511088760-140ND1
Benzene 39 01/19/2017 1851914369-123ND1
Bromodichloromethane 43 01/19/2017 18511004369-121ND1
Bromoform 42 01/19/2017 1851964361-119ND1
Bromomethane (Methyl bromide)50 01/19/2017 18511164335-144ND1
2-Butanone (MEK)77 01/19/2017 1851898757-148ND1
Carbon disulfide 43 01/19/2017 1851994358-122ND1
Carbon tetrachloride 46 01/19/2017 18511074358-136ND1
Chlorobenzene 43 01/19/2017 18511004359-129ND1
Chloroethane 44 01/19/2017 18511024350-132ND1
Chloroform 40 01/19/2017 1851934371-125ND1
Chloromethane (Methyl chloride)43 01/19/2017 18511004334-134ND1
Cyclohexane 44 01/19/2017 18511024353-139ND1
1,2-Dibromo-3-chloropropane (DBCP)41 01/19/2017 1851954355-125ND1
Dibromochloromethane 42 01/19/2017 1851984366-119ND1
1,2-Dibromoethane (EDB)40 01/19/2017 1851924374-124ND1
1,2-Dichlorobenzene 42 01/19/2017 1851974357-131ND1
1,3-Dichlorobenzene 42 01/19/2017 1851974351-134ND1
1,4-Dichlorobenzene 42 01/19/2017 1851974352-133ND1
Dichlorodifluoromethane 57 01/19/2017 18511314310-157ND1
1,1-Dichloroethane 39 01/19/2017 1851914371-127ND1
1,2-Dichloroethane 44 01/19/2017 18511024367-129ND1
1,1-Dichloroethene 38 01/19/2017 1851894369-138ND1
cis-1,2-Dichloroethene 37 01/19/2017 1851864370-122ND1
trans-1,2-Dichloroethene 39 01/19/2017 1851914368-131ND1
1,2-Dichloropropane 40 01/19/2017 1851924372-124ND1
cis-1,3-Dichloropropene 41 01/19/2017 1851944370-126ND1
trans-1,3-Dichloropropene 41 01/19/2017 1851944370-124ND1
Ethylbenzene 43 01/19/2017 1851994359-128ND1
2-Hexanone 85 01/19/2017 1851988754-137ND1
Isopropylbenzene 45 01/19/2017 18511054350-136ND1
Methyl acetate 40 01/19/2017 1851924359-137ND1
Methyl tertiary butyl ether (MTBE)34 01/19/2017 1851804370-130ND1
4-Methyl-2-pentanone 85 01/19/2017 1851988760-134ND1
Methylcyclohexane 45 01/19/2017 18511034341-144ND1
Methylene chloride 38 01/19/2017 1851884377-129ND1
Styrene 43 01/19/2017 18511004354-136ND1
1,1,2,2-Tetrachloroethane 40 01/19/2017 1851924369-132ND1
Tetrachloroethene 46 01/19/2017 18511074370-130ND1
Toluene 42 01/19/2017 1851984361-129ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane 46 01/19/2017 18511054349-136ND1
1,2,4-Trichlorobenzene 40 01/19/2017 1851924334-145ND1
1,1,1-Trichloroethane 43 01/19/2017 18511004363-128ND1
1,1,2-Trichloroethane 39 01/19/2017 1851904355-128ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 69 of 98
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-002MS
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Trichloroethene 42 01/19/2017 1851984362-126ND1
Trichlorofluoromethane 45 01/19/2017 18511034345-138ND1
Vinyl chloride 44 01/19/2017 18511034342-132ND1
Xylenes (total)90 01/19/2017 18511048758-128ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 113 47-138
Toluene-d8 105 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 70 of 98
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ32172-001
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
1,4-Dioxane ND 01/20/2017 13192012ug/kg1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 71 of 98
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ32172-002
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
1,4-Dioxane 110 01/20/2017 123411410070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 72 of 98
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-002MS
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
1,4-Dioxane 95 01/20/2017 1941999670-130ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 117 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 73 of 98
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-003DU
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
1,4-Dioxane ND 01/20/2017 19180.00 40ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 74 of 98
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ32474-001
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
1,4-Dioxane ND 01/24/2017 22292012ug/kg1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 111 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 75 of 98
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ32474-002
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
1,4-Dioxane 120 01/24/2017 213112110070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 76 of 98
Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-007MS
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
1,4-Dioxane 130 01/25/2017 014511612070-130ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 118 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 77 of 98
Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-008DU
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
1,4-Dioxane ND 01/25/2017 01230.00 40ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 115 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 78 of 98
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-001
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 01/23/2017 16470.20 0.040 ug/L1
Acenaphthylene ND 01/23/2017 16470.20 0.040 ug/L1
Acetophenone ND 01/23/2017 16471.0 0.23 ug/L1
Anthracene ND 01/23/2017 16470.20 0.060 ug/L1
Atrazine ND 01/23/2017 16471.0 0.20 ug/L1
Benzaldehyde ND 01/23/2017 16475.0 0.27 ug/L1
Benzo(a)anthracene ND 01/23/2017 16470.20 0.040 ug/L1
Benzo(a)pyrene ND 01/23/2017 16470.20 0.070 ug/L1
Benzo(b)fluoranthene ND 01/23/2017 16470.20 0.040 ug/L1
Benzo(g,h,i)perylene ND 01/23/2017 16470.20 0.040 ug/L1
Benzo(k)fluoranthene ND 01/23/2017 16470.20 0.040 ug/L1
1,1'-Biphenyl ND 01/23/2017 16471.0 0.21 ug/L1
4-Bromophenyl phenyl ether ND 01/23/2017 16471.0 0.15 ug/L1
Butyl benzyl phthalate ND 01/23/2017 16475.0 0.21 ug/L1
Caprolactam ND 01/23/2017 16475.0 0.71 ug/L1
Carbazole ND 01/23/2017 16471.0 0.040 ug/L1
4-Chloro-3-methyl phenol ND 01/23/2017 16471.0 0.26 ug/L1
4-Chloroaniline ND 01/23/2017 16471.0 0.13 ug/L1
bis(2-Chloroethoxy)methane ND 01/23/2017 16471.0 0.060 ug/L1
bis(2-Chloroethyl)ether ND 01/23/2017 16471.0 0.16 ug/L1
bis (2-Chloro-1-methylethyl) ether ND 01/23/2017 16471.0 0.17 ug/L1
2-Chloronaphthalene ND 01/23/2017 16471.0 0.15 ug/L1
2-Chlorophenol ND 01/23/2017 16471.0 0.15 ug/L1
4-Chlorophenyl phenyl ether ND 01/23/2017 16471.0 0.16 ug/L1
Chrysene ND 01/23/2017 16470.20 0.030 ug/L1
Dibenzo(a,h)anthracene ND 01/23/2017 16470.20 0.030 ug/L1
Dibenzofuran ND 01/23/2017 16471.0 0.16 ug/L1
3,3'-Dichlorobenzidine ND 01/23/2017 16475.0 0.81 ug/L1
2,4-Dichlorophenol ND 01/23/2017 16471.0 0.19 ug/L1
Diethylphthalate ND 01/23/2017 16475.0 0.19 ug/L1
Dimethyl phthalate ND 01/23/2017 16475.0 0.18 ug/L1
2,4-Dimethylphenol ND 01/23/2017 16471.0 0.15 ug/L1
Di-n-butyl phthalate ND 01/23/2017 16475.0 0.42 ug/L1
4,6-Dinitro-2-methylphenol ND 01/23/2017 16475.0 0.89 ug/L1
2,4-Dinitrophenol ND 01/23/2017 16475.0 1.3 ug/L1
2,4-Dinitrotoluene ND 01/23/2017 16472.0 0.36 ug/L1
2,6-Dinitrotoluene ND 01/23/2017 16472.0 0.34 ug/L1
Di-n-octylphthalate ND 01/23/2017 16475.0 0.48 ug/L1
bis(2-Ethylhexyl)phthalate ND 01/23/2017 16475.0 0.38 ug/L1
Fluoranthene ND 01/23/2017 16470.20 0.077 ug/L1
Fluorene ND 01/23/2017 16470.20 0.030 ug/L1
Hexachlorobenzene ND 01/23/2017 16471.0 0.15 ug/L1
Hexachlorobutadiene ND 01/23/2017 16471.0 0.17 ug/L1
Hexachlorocyclopentadiene ND 01/23/2017 16475.0 1.1 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 79 of 98
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-001
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Hexachloroethane ND 01/23/2017 16471.0 0.17 ug/L1
Indeno(1,2,3-c,d)pyrene ND 01/23/2017 16470.20 0.040 ug/L1
Isophorone ND 01/23/2017 16471.0 0.22 ug/L1
1-Methylnaphthalene ND 01/23/2017 16470.20 0.030 ug/L1
2-Methylnaphthalene ND 01/23/2017 16470.20 0.040 ug/L1
2-Methylphenol ND 01/23/2017 16471.0 0.21 ug/L1
3+4-Methylphenol ND 01/23/2017 16472.0 0.46 ug/L1
Naphthalene ND 01/23/2017 16470.20 0.050 ug/L1
2-Nitroaniline ND 01/23/2017 16472.0 0.66 ug/L1
3-Nitroaniline ND 01/23/2017 16472.0 0.15 ug/L1
4-Nitroaniline ND 01/23/2017 16472.0 1.3 ug/L1
Nitrobenzene ND 01/23/2017 16471.0 0.17 ug/L1
2-Nitrophenol ND 01/23/2017 16472.0 0.44 ug/L1
4-Nitrophenol ND 01/23/2017 16475.0 2.1 ug/L1
N-Nitrosodi-n-propylamine ND 01/23/2017 16471.0 0.28 ug/L1
N-Nitrosodiphenylamine (Diphenylamine)ND 01/23/2017 16471.0 0.84 ug/L1
Pentachlorophenol ND 01/23/2017 16475.0 1.3 ug/L1
Phenanthrene ND 01/23/2017 16470.20 0.060 ug/L1
Phenol ND 01/23/2017 16471.0 0.19 ug/L1
Pyrene ND 01/23/2017 16470.20 0.075 ug/L1
2,4,5-Trichlorophenol ND 01/23/2017 16471.0 0.19 ug/L1
2,4,6-Trichlorophenol ND 01/23/2017 16471.0 0.22 ug/L1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 66 37-129
2-Fluorophenol 61 24-127
Nitrobenzene-d5 65 38-127
Phenol-d5 68 28-128
Terphenyl-d14 81 10-148
2,4,6-Tribromophenol 72 41-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 80 of 98
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-002
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acenaphthene 7.1 01/23/2017 1712711054-1181
Acenaphthylene 7.3 01/23/2017 1712731048-1551
Acetophenone 7.4 01/23/2017 1712741052-1251
Anthracene 7.7 01/23/2017 1712771055-1221
Atrazine 7.6 01/23/2017 1712761025-1211
Benzaldehyde 6.9 01/23/2017 1712691045-1151
Benzo(a)anthracene 7.5 01/23/2017 1712751056-1231
Benzo(a)pyrene 6.8 01/23/2017 1712681054-1241
Benzo(b)fluoranthene 7.2 01/23/2017 1712721055-1361
Benzo(g,h,i)perylene 9.0 01/23/2017 1712901042-1291
Benzo(k)fluoranthene 6.9 01/23/2017 1712691053-1321
1,1'-Biphenyl 6.6 01/23/2017 1712661042-1201
4-Bromophenyl phenyl ether 7.2 01/23/2017 1712721055-1211
Butyl benzyl phthalate 8.9 01/23/2017 1712891054-1351
Caprolactam 7.3 01/23/2017 1712731044-1521
Carbazole 8.2 01/23/2017 1712821045-1011
4-Chloro-3-methyl phenol 8.0 01/23/2017 1712801058-1251
4-Chloroaniline 7.6 01/23/2017 1712761010-1281
bis(2-Chloroethoxy)methane 7.1 01/23/2017 1712711044-1271
bis(2-Chloroethyl)ether 6.2 01/23/2017 1712621046-1201
bis (2-Chloro-1-methylethyl) ether 6.3 01/23/2017 1712631042-1241
2-Chloronaphthalene 6.6 01/23/2017 1712661046-1001
2-Chlorophenol 6.6 01/23/2017 1712661050-1171
4-Chlorophenyl phenyl ether 7.1 01/23/2017 1712711055-1211
Chrysene 7.5 01/23/2017 1712751054-1201
Dibenzo(a,h)anthracene 7.5 01/23/2017 1712751050-1271
Dibenzofuran 7.6 01/23/2017 1712761058-1181
2,4-Dichlorophenol 7.2 01/23/2017 1712721055-1171
Diethylphthalate 8.2 01/23/2017 1712821060-1251
Dimethyl phthalate 7.9 01/23/2017 1712791060-1221
2,4-Dimethylphenol 8.8 01/23/2017 1712881036-1701
Di-n-butyl phthalate 8.1 01/23/2017 1712811060-1311
4,6-Dinitro-2-methylphenol 9.4 01/23/2017 1712941056-1281
2,4-Dinitrophenol 18 01/23/2017 1712902047-1331
2,4-Dinitrotoluene 8.3 01/23/2017 1712831059-1271
2,6-Dinitrotoluene 7.8 01/23/2017 1712781059-1261
Di-n-octylphthalate 6.5 01/23/2017 1712651050-1361
bis(2-Ethylhexyl)phthalate 7.5 01/23/2017 1712751056-1281
Fluoranthene 7.7 01/23/2017 1712771058-1241
Fluorene 7.5 01/23/2017 1712751057-1191
Hexachlorobenzene 7.0 01/23/2017 1712701055-1181
Hexachlorobutadiene 5.5 01/23/2017 1712551053-1161
Hexachlorocyclopentadiene 19 01/23/2017 1712385016-961
Hexachloroethane 5.2 01/23/2017 1712521031-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 81 of 98
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-002
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Indeno(1,2,3-c,d)pyrene 8.5 01/23/2017 1712851048-1261
Isophorone 7.0 01/23/2017 1712701057-1231
1-Methylnaphthalene 6.8 01/23/2017 1712681041-1251
2-Methylnaphthalene 6.9 01/23/2017 1712691057-11151
2-Methylphenol 7.0 01/23/2017 1712701056-1191
3+4-Methylphenol 7.4 01/23/2017 1712741053-1191
Naphthalene 6.9 01/23/2017 1712691052-1091
2-Nitroaniline 8.0 01/23/2017 1712801060-1241
3-Nitroaniline 7.8 01/23/2017 1712781043-1231
4-Nitroaniline 8.0 01/23/2017 1712801060-1351
Nitrobenzene 6.8 01/23/2017 1712681051-1221
2-Nitrophenol 7.5 01/23/2017 1712751051-1181
4-Nitrophenol 16 01/23/2017 1712792053-1301
N-Nitrosodi-n-propylamine 7.2 01/23/2017 1712721054-1271
N-Nitrosodiphenylamine (Diphenylamine)7.6 01/23/2017 1712761035-1461
Pentachlorophenol 16 01/23/2017 1712782042-1311
Phenanthrene 7.6 01/23/2017 1712761056-1191
Phenol 6.1 01/23/2017 1712611049-1171
Pyrene 8.1 01/23/2017 1712811055-1271
2,4,5-Trichlorophenol 7.5 01/23/2017 1712751056-1181
2,4,6-Trichlorophenol 6.9 01/23/2017 1712691055-1211
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 66 37-129
2-Fluorophenol 59 24-127
Nitrobenzene-d5 68 38-127
Phenol-d5 65 28-128
Terphenyl-d14 71 10-148
2,4,6-Tribromophenol 77 41-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 82 of 98
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-001
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 01/24/2017 09292.7 0.83 ug/kg1
Acenaphthylene ND 01/24/2017 09292.7 0.95 ug/kg1
Acetophenone ND 01/24/2017 0929131.4 ug/kg1
Anthracene ND 01/24/2017 09292.7 0.51 ug/kg1
Atrazine ND 01/24/2017 0929131.0 ug/kg1
Benzaldehyde ND 01/24/2017 0929131.0 ug/kg1
Benzo(a)anthracene ND 01/24/2017 09292.7 0.59 ug/kg1
Benzo(a)pyrene ND 01/24/2017 09292.7 0.66 ug/kg1
Benzo(b)fluoranthene ND 01/24/2017 09292.7 0.50 ug/kg1
Benzo(g,h,i)perylene ND 01/24/2017 09292.7 0.65 ug/kg1
Benzo(k)fluoranthene ND 01/24/2017 09292.7 0.48 ug/kg1
1,1'-Biphenyl ND 01/24/2017 0929130.95 ug/kg1
4-Bromophenyl phenyl ether ND 01/24/2017 0929130.92 ug/kg1
Butyl benzyl phthalate ND 01/24/2017 0929130.69 ug/kg1
Caprolactam 9.0 01/24/2017 0929J132.4 ug/kg1
Carbazole ND 01/24/2017 0929130.84 ug/kg1
bis (2-Chloro-1-methylethyl) ether ND 01/24/2017 0929131.3 ug/kg1
4-Chloro-3-methyl phenol ND 01/24/2017 0929131.1 ug/kg1
4-Chloroaniline ND 01/24/2017 0929131.2 ug/kg1
bis(2-Chloroethoxy)methane ND 01/24/2017 0929130.70 ug/kg1
bis(2-Chloroethyl)ether ND 01/24/2017 0929131.1 ug/kg1
2-Chloronaphthalene ND 01/24/2017 0929132.5 ug/kg1
2-Chlorophenol ND 01/24/2017 0929132.1 ug/kg1
4-Chlorophenyl phenyl ether ND 01/24/2017 0929130.80 ug/kg1
Chrysene ND 01/24/2017 09292.7 0.45 ug/kg1
Dibenzo(a,h)anthracene ND 01/24/2017 09292.7 0.51 ug/kg1
Dibenzofuran ND 01/24/2017 0929131.0 ug/kg1
3,3'-Dichlorobenzidine ND 01/24/2017 0929132.0 ug/kg1
2,4-Dichlorophenol ND 01/24/2017 0929131.3 ug/kg1
Diethylphthalate ND 01/24/2017 0929130.80 ug/kg1
Dimethyl phthalate ND 01/24/2017 0929137.4 ug/kg1
2,4-Dimethylphenol ND 01/24/2017 0929132.2 ug/kg1
Di-n-butyl phthalate ND 01/24/2017 0929132.0 ug/kg1
4,6-Dinitro-2-methylphenol ND 01/24/2017 0929672.0 ug/kg1
2,4-Dinitrophenol ND 01/24/2017 0929673.3 ug/kg1
2,4-Dinitrotoluene ND 01/24/2017 0929272.4 ug/kg1
2,6-Dinitrotoluene ND 01/24/2017 0929272.1 ug/kg1
Di-n-octylphthalate ND 01/24/2017 0929130.24 ug/kg1
bis(2-Ethylhexyl)phthalate 20 01/24/2017 0929130.45 ug/kg1
Fluoranthene ND 01/24/2017 09292.7 0.42 ug/kg1
Fluorene ND 01/24/2017 09292.7 0.57 ug/kg1
Hexachlorobenzene ND 01/24/2017 0929130.98 ug/kg1
Hexachlorobutadiene ND 01/24/2017 0929131.7 ug/kg1
Hexachlorocyclopentadiene ND 01/24/2017 0929671.3 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 83 of 98
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-001
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Hexachloroethane ND 01/24/2017 0929131.1 ug/kg1
Indeno(1,2,3-c,d)pyrene ND 01/24/2017 09292.7 1.0 ug/kg1
Isophorone ND 01/24/2017 0929131.2 ug/kg1
2-Methylnaphthalene ND 01/24/2017 09292.7 0.99 ug/kg1
2-Methylphenol ND 01/24/2017 0929133.5 ug/kg1
3+4-Methylphenol ND 01/24/2017 0929273.3 ug/kg1
Naphthalene ND 01/24/2017 09292.7 0.97 ug/kg1
2-Nitroaniline ND 01/24/2017 0929273.7 ug/kg1
3-Nitroaniline ND 01/24/2017 0929273.7 ug/kg1
4-Nitroaniline ND 01/24/2017 0929274.0 ug/kg1
Nitrobenzene ND 01/24/2017 0929131.6 ug/kg1
2-Nitrophenol ND 01/24/2017 0929271.6 ug/kg1
4-Nitrophenol ND 01/24/2017 09296721ug/kg1
N-Nitrosodi-n-propylamine ND 01/24/2017 0929131.1 ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 01/24/2017 0929131.0 ug/kg1
Pentachlorophenol ND 01/24/2017 0929675.3 ug/kg1
Phenanthrene ND 01/24/2017 09292.7 0.72 ug/kg1
Phenol ND 01/24/2017 0929131.2 ug/kg1
Pyrene ND 01/24/2017 09292.7 0.50 ug/kg1
Pyridine 0.00 01/24/2017 0929J130.00 ug/kg1
2,4,5-Trichlorophenol ND 01/24/2017 0929130.87 ug/kg1
2,4,6-Trichlorophenol ND 01/24/2017 0929130.96 ug/kg1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 68 33-102
2-Fluorophenol 76 35-115
Nitrobenzene-d5 66 22-109
Phenol-d5 85 33-122
Terphenyl-d14 74 41-120
2,4,6-Tribromophenol 69 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 84 of 98
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-002
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acenaphthene 85 01/24/2017 09536413012-1111
Acenaphthylene 89 01/24/2017 09536713018-901
Acetophenone 90 01/24/2017 09536713030-1301
Anthracene 92 01/24/2017 09536913016-1221
Atrazine 89 01/24/2017 09536713030-1301
Benzaldehyde 60 01/24/2017 09534513030-1301
Benzo(a)anthracene 95 01/24/2017 09537213040-1211
Benzo(a)pyrene 99 01/24/2017 09537413036-1141
Benzo(b)fluoranthene 98 01/24/2017 09537413038-1231
Benzo(g,h,i)perylene 100 01/24/2017 09537713043-1201
Benzo(k)fluoranthene 96 01/24/2017 09537213040-1261
1,1'-Biphenyl 82 01/24/2017 09536213045-1281
4-Bromophenyl phenyl ether 87 01/24/2017 09536613030-1301
Butyl benzyl phthalate 100 01/24/2017 09537913048-1241
Caprolactam 110 01/24/2017 09538113040-1171
Carbazole 110 01/24/2017 09538013047-1251
bis (2-Chloro-1-methylethyl) ether 88 01/24/2017 09536613041-1131
4-Chloro-3-methyl phenol 97 01/24/2017 09537313048-1201
4-Chloroaniline 54 01/24/2017 09534013031-1271
bis(2-Chloroethoxy)methane 87 01/24/2017 09536613038-1151
bis(2-Chloroethyl)ether 89 01/24/2017 09536713046-1221
2-Chloronaphthalene 83 01/24/2017 09536213037-1061
2-Chlorophenol 91 01/24/2017 09536813044-1221
4-Chlorophenyl phenyl ether 86 01/24/2017 09536413032-1071
Chrysene 95 01/24/2017 09537113041-1241
Dibenzo(a,h)anthracene 88 01/24/2017 09536613038-1251
Dibenzofuran 93 01/24/2017 09537013045-1281
3,3'-Dichlorobenzidine 71 01/24/2017 09535413039-1081
2,4-Dichlorophenol 88 01/24/2017 09536613030-961
Diethylphthalate 95 01/24/2017 09537213030-1301
Dimethyl phthalate 95 01/24/2017 09537113024-1271
2,4-Dimethylphenol 100 01/24/2017 09537613030-1301
Di-n-butyl phthalate 100 01/24/2017 09537613035-1081
4,6-Dinitro-2-methylphenol 78 01/24/2017 09535813053-1501
2,4-Dinitrophenol 120 01/24/2017 09534527032-1151
2,4-Dinitrotoluene 90 01/24/2017 09536813040-1301
2,6-Dinitrotoluene 91 01/24/2017 09536813046-1181
Di-n-octylphthalate 100 01/24/2017 09537513049-1181
bis(2-Ethylhexyl)phthalate 120 01/24/2017 09539013033-1231
Fluoranthene 94 01/24/2017 09537113026-1331
Fluorene 90 01/24/2017 09536813019-1081
Hexachlorobenzene 85 01/24/2017 09536413010-1251
Hexachlorobutadiene 74 01/24/2017 09535513047-1161
Hexachlorocyclopentadiene 360 01/24/2017 09535567048-1271
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 85 of 98
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-002
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Hexachloroethane 68 01/24/2017 09535113018-1541
Indeno(1,2,3-c,d)pyrene 99 01/24/2017 09537513042-1231
Isophorone 90 01/24/2017 09536713030-1301
2-Methylnaphthalene 86 01/24/2017 09536513010-1071
2-Methylphenol 100 01/24/2017 09537713033-1031
3+4-Methylphenol 100 01/24/2017 09537713018-1211
Naphthalene 85 01/24/2017 09536413010-1121
2-Nitroaniline 95 01/24/2017 09537213046-1281
3-Nitroaniline 62 01/24/2017 09534713030-1301
4-Nitroaniline 88 01/24/2017 09536613051-1291
Nitrobenzene 81 01/24/2017 09536113049-1421
2-Nitrophenol 88 01/24/2017 09536613033-1141
4-Nitrophenol 140 01/24/2017 09535427027-1381
N-Nitrosodi-n-propylamine 100 01/24/2017 09537613045-1121
N-Nitrosodiphenylamine (Diphenylamine)95 01/24/2017 09537113049-1231
Pentachlorophenol 180 01/24/2017 09536627036-1081
Phenanthrene 92 01/24/2017 09536913016-1231
Phenol 97 01/24/2017 09537313039-1081
Pyrene 97 01/24/2017 09537313034-1211
Pyridine 89 01/24/2017 09536713010-741
2,4,5-Trichlorophenol 90 01/24/2017 09536813032-1051
2,4,6-Trichlorophenol 88 01/24/2017 09536613031-1021
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 57 33-102
2-Fluorophenol 66 35-115
Nitrobenzene-d5 59 22-109
Phenol-d5 72 33-122
Terphenyl-d14 64 41-120
2,4,6-Tribromophenol 63 30-117
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 86 of 98
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31799-001
31799 3005A
01/18/2017 917Analytical Method:6010C
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Arsenic ND 01/19/2017 21420.015 0.0022 mg/L1
Barium ND 01/19/2017 21420.025 0.0019 mg/L1
Cadmium ND 01/19/2017 21420.0050 0.00054 mg/L1
Chromium ND 01/19/2017 21420.010 0.00072 mg/L1
Lead ND 01/19/2017 21420.010 0.0047 mg/L1
Selenium ND 01/19/2017 21420.020 0.0085 mg/L1
Silver ND 01/19/2017 21420.010 0.0021 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 87 of 98
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31799-002
31799 3005A
01/18/2017 917Analytical Method:6010C
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Arsenic 0.42 01/19/2017 21461060.40 80-1201
Barium 2.1 01/19/2017 21461042.0 80-1201
Cadmium 0.43 01/19/2017 21461070.40 80-1201
Chromium 2.1 01/19/2017 21461072.0 80-1201
Lead 0.42 01/19/2017 21461060.40 80-1201
Selenium 0.43 01/19/2017 21461070.40 80-1201
Silver 0.41 01/19/2017 21461020.40 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 88 of 98
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31801-001
31801 3050B
01/18/2017 949Analytical Method:6010C
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Arsenic ND 01/20/2017 20410.75 0.23 mg/kg1
Barium ND 01/20/2017 20411.3 0.14 mg/kg1
Cadmium ND 01/20/2017 20410.25 0.025 mg/kg1
Chromium ND 01/20/2017 20410.50 0.072 mg/kg1
Lead ND 01/20/2017 20410.50 0.22 mg/kg1
Selenium ND 01/20/2017 20411.0 0.41 mg/kg1
Silver ND 01/20/2017 20410.50 0.079 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 89 of 98
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31801-002
31801 3050B
01/18/2017 949Analytical Method:6010C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Arsenic 240 01/20/2017 20469625080-1201
Barium 470 01/20/2017 20469450080-1201
Cadmium 50 01/20/2017 2046995080-1201
Chromium 250 01/20/2017 204610225080-1201
Lead 240 01/20/2017 20469625080-1201
Selenium 46 01/20/2017 2046915080-1201
Silver 46 01/20/2017 2046935080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 90 of 98
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31784-001
31784 7471B
01/17/2017 2128Analytical Method:7471B
Matrix:Solid
Parameter Result Q LOQ DL Units Analysis DateDil
Mercury ND 01/18/2017 18340.083 0.0063 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 91 of 98
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31784-002
31784 7471B
01/17/2017 2128Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Mercury 0.84 01/18/2017 18361010.83 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 92 of 98
RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31803-001
31803 7470A
01/18/2017 1222Analytical Method:7470A
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Mercury ND 01/18/2017 16290.00010 0.000028 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 93 of 98
RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31803-002
31803 7470A
01/18/2017 1222Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Mercury 0.0020 01/18/2017 16311020.0020 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 94 of 98
Chain of Custody
and
Miscellaneous Documents
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Shealy Environmental Services, Inc.

Page 95 of 98
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 96 of 98
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 97 of 98
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 98 of 98
Republic Services, Inc.
18500 N. Allied Way, Phoenix, AZ 85054 FAX
INCOMPLETE FILE TRANSMITTAL
TO: Jill Spriggle LOG NO.: 5010180937
FAX: File Received: 1/18/2018
From: Special Waste Dept.Response Date: 1/18/2018
Re: East 7th Street, LLC / Impacted Soil
SECTION I SECTION II SECTION III SECTION IV SECTION V SECTION VI
DisposalFacility TransporterName NameOfWaste USEPA CharacteristicComponents GenAuthSignature
GeneratorName TransporterSiteAddress ProcessGeneratingWaste SampleDate FreeLiquids GenCoName
GeneratorSiteAddress TransporterCityStateZip TypeOfWaste CompositeGrab YesNo NoStateLetter
GeneratorCityStateZip TransporterMailingAddress PhysicalState SampleID pH_Flash Name_Title
GeneratorMailingAddress TransporterContactName MethodOfShipment SignatureDate
GeneratorContactName TransporterTelFax EstimatedAnnualVolume
GeneratorTelFax Frequency
GeneratorStateID DisposalConsideration
WasteCodeTexas
ANALYTICALS TCLP TOTAL METALS TCLP VOLATILES TCLP SEMI-VOLATILES PESTICIDES / HERBICIDE
TotalCyanide Arsenic Benzene Cresols Chlordane LabLetterhead
ReactiveCyanide Barium CarbonTetrachloride DichlorobenzeneOne Endrin ChainOfCustody
TotalSulfide Cadmium Chlorobenzene DinitrotolueneTwo Heptachlor NoLabSignature
ReactiveSulfide Chromium Chloroform Hexachlorobenzene HeptachlorEpoxide ReportOneYearOldPlus
TotalPCB Copper DichloroethaneOne Nitrobenzene Lindane NoThirdPartyLab
TOX_EOX LeadDichloroehyleneTwo Pentachlorophenol Methoxychlor MissingReportPages
Phenols Mercury MethylEthylKetone PyridineToxaphene MissingMSDSPages
FlashPoint Selenium Tetrachloroethylene TrichlorophenolFive TwoFourD TotalSulfates
pH Silver Trichlorethylene TrichlorphenolSix TwoFourFiveTP TotalSulfur
PaintFilter Zinc VinylChloride WrongProfile
TPH
BTEX GeneratorIncomplete
Notes:
The Total Lead result for Sample ID# BG-1 is 130 mg/kg. This value exceeds the Maximum Theoretical Concentration of 100 mg/kg for Lead. Please have the generator provide TCLP Lead on Sample ID# BG-1.
The lab did not report the results for Pyridine on the 8270 analysis for any of the samples. Since Pyridine is a RCRA TCLP volatile (D038), please have the generator contact the lab to have them report the results for Pyridine.Lynette
1/24/2018 - Attached is lab report TA19129. SUMMIT resampled BG-1 and ran Lead TCLP as requested. Also attached is
lab report SA17067. This report was revised to include Pyridine. - JS

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Summit Engineering and Construction Services, Inc.
3575 Centre Circle
Fort Mill, SC 28715
Attention: Patrick Lowery
SA17067Lot Number:
3586.11Project Number:
East 7th Street StorageProject Name:
01/25/2017Date Completed:
Lucas Odom
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 87
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SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Summit Engineering and Construction Services, Inc.
Lot Number: SA17067
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
SVOCs by GC/MS
The method blank associated with batch 32300 yielded a detection for Bis2-(ethylhexylphthalate). No corrective action is required as all associated
samples are non-detect for this compound. There was one "J" value detection but this is an estimated value recovered below the PQL.
Page: 2 of 87
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Summit Engineering and Construction Services, Inc.
Lot Number: SA17067

Sample Number Sample ID Matrix Date Sampled Date Received
001 01/16/2017 1100SB-1-SS Solid 01/17/2017
002 01/16/2017 1145SB-1-SB Solid 01/17/2017
003 01/16/2017 1600SB-2-SS Solid 01/17/2017
004 01/16/2017 1520SB-3-SS Solid 01/17/2017
005 01/16/2017 1520SB-3 DUP Solid 01/17/2017
006 01/16/2017 1420SB-4-SS Solid 01/17/2017
007 01/16/2017 1400SB-5-SB Solid 01/17/2017
008 01/16/2017 1440BG-1 Solid 01/17/2017
009 01/16/2017 1200EQUIPMENT BLANK Aqueous 01/17/2017
010 01/16/2017 1330FIELD BLANK Aqueous 01/17/2017
011 01/16/2017TRIP BLANK Aqueous 01/17/2017
(11 samples)
Page: 3 of 87
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Summit Engineering and Construction Services, Inc.
Lot Number: SA17067

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 SB-1-SS Solid Acenaphthene 8270D 3.6 ug/kg 8
001 SB-1-SS Solid Acenaphthylene 8270D 10 ug/kg 8
001 SB-1-SS Solid Acetophenone 8270D 4.3 J ug/kg 8
001 SB-1-SS Solid Anthracene 8270D 22 ug/kg 8
001 SB-1-SS Solid Benzo(a)anthracene 8270D 84 ug/kg 8
001 SB-1-SS Solid Benzo(a)pyrene 8270D 85 ug/kg 8
001 SB-1-SS Solid Benzo(b)fluoranthene 8270D 110 ug/kg 8
001 SB-1-SS Solid Benzo(g,h,i)perylene 8270D 32 ug/kg 9
001 SB-1-SS Solid Benzo(k)fluoranthene 8270D 47 ug/kg 9
001 SB-1-SS Solid Carbazole 8270D 14 J ug/kg 9
001 SB-1-SS Solid Chrysene 8270D 83 ug/kg 9
001 SB-1-SS Solid Dibenzofuran 8270D 11 J ug/kg 9
001 SB-1-SS Solid Fluoranthene 8270D 170 ug/kg 9
001 SB-1-SS Solid Fluorene 8270D 4.8 ug/kg 9
001 SB-1-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 33 ug/kg 9
001 SB-1-SS Solid 2-Methylnaphthalene 8270D 17 ug/kg 9
001 SB-1-SS Solid Naphthalene 8270D 21 ug/kg 10
001 SB-1-SS Solid Phenanthrene 8270D 95 ug/kg 10
001 SB-1-SS Solid Pyrene 8270D 140 ug/kg 10
001 SB-1-SS Solid Arsenic 6010C 2.2 mg/kg 10
001 SB-1-SS Solid Barium 6010C 71 mg/kg 10
001 SB-1-SS Solid Cadmium 6010C 0.053 J mg/kg 10
001 SB-1-SS Solid Chromium 6010C 46 mg/kg 10
001 SB-1-SS Solid Lead 6010C 20 mg/kg 10
001 SB-1-SS Solid Mercury 7471B 0.080 J mg/kg 10
002 SB-1-SB Solid Arsenic 6010C 1.3 J mg/kg 14
002 SB-1-SB Solid Barium 6010C 27 mg/kg 14
002 SB-1-SB Solid Chromium 6010C 0.96 J mg/kg 14
003 SB-2-SS Solid Acenaphthylene 8270D 1.2 J ug/kg 16
003 SB-2-SS Solid Anthracene 8270D 1.1 J ug/kg 16
003 SB-2-SS Solid Benzo(a)anthracene 8270D 4.6 ug/kg 16
003 SB-2-SS Solid Benzo(a)pyrene 8270D 4.8 ug/kg 16
003 SB-2-SS Solid Benzo(b)fluoranthene 8270D 8.3 ug/kg 16
003 SB-2-SS Solid Benzo(g,h,i)perylene 8270D 3.4 ug/kg 17
003 SB-2-SS Solid Benzo(k)fluoranthene 8270D 2.3 J ug/kg 17
003 SB-2-SS Solid Chrysene 8270D 5.6 ug/kg 17
003 SB-2-SS Solid Fluoranthene 8270D 6.7 ug/kg 17
003 SB-2-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 2.6 J ug/kg 17
003 SB-2-SS Solid 2-Methylnaphthalene 8270D 17 ug/kg 17
003 SB-2-SS Solid Naphthalene 8270D 13 ug/kg 18
003 SB-2-SS Solid Phenanthrene 8270D 9.9 ug/kg 18
003 SB-2-SS Solid Pyrene 8270D 6.2 ug/kg 18
003 SB-2-SS Solid Arsenic 6010C 2.8 J mg/kg 18
003 SB-2-SS Solid Barium 6010C 93 mg/kg 18
003 SB-2-SS Solid Chromium 6010C 61 mg/kg 18
Page: 4 of 87
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Shealy Environmental Services, Inc.

Executive Summary (Continued)
Lot Number: SA17067
Sample Sample ID Matrix Parameter Method Result Q Units Page
003 SB-2-SS Solid Lead 6010C 16 mg/kg 18
003 SB-2-SS Solid Mercury 7471B 0.056 J mg/kg 18
004 SB-3-SS Solid Anthracene 8270D 1.1 J ug/kg 20
004 SB-3-SS Solid Benzaldehyde 8270D 4.0 J ug/kg 20
004 SB-3-SS Solid Benzo(a)anthracene 8270D 5.6 ug/kg 20
004 SB-3-SS Solid Benzo(a)pyrene 8270D 6.4 ug/kg 20
004 SB-3-SS Solid Benzo(b)fluoranthene 8270D 10 ug/kg 20
004 SB-3-SS Solid Benzo(g,h,i)perylene 8270D 3.0 J ug/kg 21
004 SB-3-SS Solid Benzo(k)fluoranthene 8270D 3.1 ug/kg 21
004 SB-3-SS Solid Chrysene 8270D 7.1 ug/kg 21
004 SB-3-SS Solid Fluoranthene 8270D 9.7 ug/kg 21
004 SB-3-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 2.6 J ug/kg 21
004 SB-3-SS Solid 2-Methylnaphthalene 8270D 7.3 ug/kg 21
004 SB-3-SS Solid Naphthalene 8270D 5.3 ug/kg 22
004 SB-3-SS Solid Phenanthrene 8270D 8.8 ug/kg 22
004 SB-3-SS Solid Pyrene 8270D 8.7 ug/kg 22
004 SB-3-SS Solid Arsenic 6010C 2.4 J mg/kg 22
004 SB-3-SS Solid Barium 6010C 37 mg/kg 22
004 SB-3-SS Solid Chromium 6010C 75 mg/kg 22
004 SB-3-SS Solid Lead 6010C 8.6 mg/kg 22
004 SB-3-SS Solid Mercury 7471B 0.051 J mg/kg 22
005 SB-3 DUP Solid Benzaldehyde 8270D 5.3 J ug/kg 24
005 SB-3 DUP Solid Benzo(a)anthracene 8270D 4.1 ug/kg 24
005 SB-3 DUP Solid Benzo(a)pyrene 8270D 3.5 ug/kg 24
005 SB-3 DUP Solid Benzo(b)fluoranthene 8270D 6.3 ug/kg 24
005 SB-3 DUP Solid Benzo(g,h,i)perylene 8270D 1.9 J ug/kg 25
005 SB-3 DUP Solid Chrysene 8270D 3.3 ug/kg 25
005 SB-3 DUP Solid Fluoranthene 8270D 4.5 ug/kg 25
005 SB-3 DUP Solid Indeno(1,2,3-c,d)pyrene 8270D 1.6 J ug/kg 25
005 SB-3 DUP Solid 2-Methylnaphthalene 8270D 4.4 ug/kg 25
005 SB-3 DUP Solid Naphthalene 8270D 3.1 J ug/kg 26
005 SB-3 DUP Solid Phenanthrene 8270D 4.3 ug/kg 26
005 SB-3 DUP Solid Pyrene 8270D 4.1 ug/kg 26
005 SB-3 DUP Solid Arsenic 6010C 2.8 J mg/kg 26
005 SB-3 DUP Solid Barium 6010C 40 mg/kg 26
005 SB-3 DUP Solid Chromium 6010C 93 mg/kg 26
005 SB-3 DUP Solid Lead 6010C 14 mg/kg 26
005 SB-3 DUP Solid Mercury 7471B 0.24 mg/kg 26
006 SB-4-SS Solid Acenaphthene 8270D 190 ug/kg 28
006 SB-4-SS Solid Anthracene 8270D 270 ug/kg 28
006 SB-4-SS Solid Benzo(a)anthracene 8270D 820 ug/kg 28
006 SB-4-SS Solid Benzo(a)pyrene 8270D 760 ug/kg 28
006 SB-4-SS Solid Benzo(b)fluoranthene 8270D 1100 ug/kg 29
006 SB-4-SS Solid Benzo(g,h,i)perylene 8270D 140 ug/kg 29
006 SB-4-SS Solid Benzo(k)fluoranthene 8270D 340 ug/kg 29
006 SB-4-SS Solid 1,1'-Biphenyl 8270D 9.1 J ug/kg 29
006 SB-4-SS Solid Carbazole 8270D 160 ug/kg 29
006 SB-4-SS Solid Chrysene 8270D 800 ug/kg 29
Page: 5 of 87
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Shealy Environmental Services, Inc.

Executive Summary (Continued)
Lot Number: SA17067
Sample Sample ID Matrix Parameter Method Result Q Units Page
006 SB-4-SS Solid Dibenzofuran 8270D 81 ug/kg 29
006 SB-4-SS Solid Fluoranthene 8270D 2000 ug/kg 29
006 SB-4-SS Solid Fluorene 8270D 140 ug/kg 29
006 SB-4-SS Solid Indeno(1,2,3-c,d)pyrene 8270D 160 ug/kg 29
006 SB-4-SS Solid 2-Methylnaphthalene 8270D 33 ug/kg 30
006 SB-4-SS Solid Naphthalene 8270D 71 ug/kg 30
006 SB-4-SS Solid Phenanthrene 8270D 1700 ug/kg 30
006 SB-4-SS Solid Pyrene 8270D 1500 ug/kg 30
006 SB-4-SS Solid Arsenic 6010C 1.3 mg/kg 30
006 SB-4-SS Solid Barium 6010C 36 mg/kg 30
006 SB-4-SS Solid Chromium 6010C 6.8 mg/kg 30
006 SB-4-SS Solid Lead 6010C 6.4 mg/kg 30
006 SB-4-SS Solid Mercury 7471B 0.019 J mg/kg 31
007 SB-5-SB Solid 2-Methylnaphthalene 8270D 2.2 J ug/kg 34
007 SB-5-SB Solid Naphthalene 8270D 2.0 J ug/kg 35
007 SB-5-SB Solid Arsenic 6010C 0.97 mg/kg 35
007 SB-5-SB Solid Barium 6010C 27 mg/kg 35
007 SB-5-SB Solid Chromium 6010C 1.3 mg/kg 35
007 SB-5-SB Solid Lead 6010C 2.0 mg/kg 35
008 BG-1 Solid Acenaphthylene 8270D 8.4 ug/kg 37
008 BG-1 Solid Anthracene 8270D 12 ug/kg 37
008 BG-1 Solid Benzaldehyde 8270D 5.6 J ug/kg 37
008 BG-1 Solid Benzo(a)anthracene 8270D 100 ug/kg 37
008 BG-1 Solid Benzo(a)pyrene 8270D 93 ug/kg 37
008 BG-1 Solid Benzo(b)fluoranthene 8270D 180 ug/kg 37
008 BG-1 Solid Benzo(g,h,i)perylene 8270D 17 ug/kg 38
008 BG-1 Solid Benzo(k)fluoranthene 8270D 60 ug/kg 38
008 BG-1 Solid Chrysene 8270D 94 ug/kg 38
008 BG-1 Solid bis(2-Ethylhexyl)phthalate 8270D 4.0 BJ ug/kg 38
008 BG-1 Solid Fluoranthene 8270D 170 ug/kg 38
008 BG-1 Solid Fluorene 8270D 1.6 J ug/kg 38
008 BG-1 Solid Indeno(1,2,3-c,d)pyrene 8270D 21 ug/kg 38
008 BG-1 Solid 2-Methylnaphthalene 8270D 11 ug/kg 38
008 BG-1 Solid Naphthalene 8270D 9.8 ug/kg 39
008 BG-1 Solid Phenanthrene 8270D 41 ug/kg 39
008 BG-1 Solid Pyrene 8270D 140 ug/kg 39
008 BG-1 Solid Arsenic 6010C 2.6 mg/kg 39
008 BG-1 Solid Barium 6010C 160 mg/kg 39
008 BG-1 Solid Cadmium 6010C 0.23 J mg/kg 39
008 BG-1 Solid Chromium 6010C 25 mg/kg 39
008 BG-1 Solid Lead 6010C 130 mg/kg 39
008 BG-1 Solid Mercury 7471B 0.18 mg/kg 39
010 FIELD BLANK Aqueous Acetone 8260B 2.2 J ug/L 45
(136 detections)
Page: 6 of 87
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Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/25/2017 0100 ECP 32474 5.79
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1321
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1358 ECB 31997 5.24
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.723
Benzene 71-43-2 8260B ND 1ug/kg2.35.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.35.8
Bromoform 75-25-2 8260B ND 1ug/kg2.35.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.35.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.723
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.35.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.35.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.35.8
Chloroethane 75-00-3 8260B ND 1ug/kg2.35.8
Chloroform 67-66-3 8260B ND 1ug/kg2.35.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.35.8
Cyclohexane 110-82-7 8260B ND 1ug/kg2.35.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.35.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.35.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.35.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.35.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.35.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.35.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.35.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.35.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.35.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.35.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.35.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.35.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.35.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.35.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.35.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 87
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Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1358 ECB 31997 5.24
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.712
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.35.8
Methyl acetate 79-20-9 8260B ND 1ug/kg2.35.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.35.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.712
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.35.8
Methylene chloride 75-09-2 8260B ND 1ug/kg2.35.8
Styrene 100-42-5 8260B ND 1ug/kg2.35.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.35.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.35.8
Toluene 108-88-3 8260B ND 1ug/kg2.35.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.35.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.35.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.35.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.35.8
Trichloroethene 79-01-6 8260B ND 1ug/kg2.35.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.35.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.35.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.712
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 106 47-138
Toluene-d8 107 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1650 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D 3.6 1ug/kg1.03.3
Acenaphthylene 208-96-8 8270D 10 1ug/kg1.23.3
Acetophenone 98-86-2 8270D 4.3 J 1ug/kg1.716
Anthracene 120-12-7 8270D 22 1ug/kg0.623.3
Atrazine 1912-24-9 8270D ND 1ug/kg1.216
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.216
Benzo(a)anthracene 56-55-3 8270D 84 1ug/kg0.723.3
Benzo(a)pyrene 50-32-8 8270D 85 1ug/kg0.813.3
Benzo(b)fluoranthene 205-99-2 8270D 110 1ug/kg0.613.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1650 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D 32 1ug/kg0.803.3
Benzo(k)fluoranthene 207-08-9 8270D 47 1ug/kg0.593.3
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.216
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.116
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8516
Caprolactam 105-60-2 8270D ND 1ug/kg2.916
Carbazole 86-74-8 8270D 14 J 1ug/kg1.016
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.616
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.316
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.516
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8616
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.316
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg3.116
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.616
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9816
Chrysene 218-01-9 8270D 83 1ug/kg0.553.3
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.623.3
Dibenzofuran 132-64-9 8270D 11 J 1ug/kg1.216
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.416
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.616
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9816
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg9.116
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.716
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.416
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.482
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg4.082
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.933
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.633
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2916
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5516
Fluoranthene 206-44-0 8270D 170 1ug/kg0.513.3
Fluorene 86-73-7 8270D 4.8 1ug/kg0.703.3
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.216
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.116
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.682
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.316
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 33 1ug/kg1.23.3
Isophorone 78-59-1 8270D ND 1ug/kg1.516
2-Methylnaphthalene 91-57-6 8270D 17 1ug/kg1.23.3
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.316
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SS
SA17067-001
01/16/2017 1100
01/17/2017
Solid
% Solids:81.7 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1650 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg4.033
Naphthalene 91-20-3 8270D 21 1ug/kg1.23.3
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.533
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.533
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.933
Nitrobenzene 98-95-3 8270D ND 1ug/kg2.016
2-Nitrophenol 88-75-5 8270D ND 1ug/kg2.033
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2582
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.316
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.216
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.582
Phenanthrene 85-01-8 8270D 95 1ug/kg0.883.3
Phenol 108-95-2 8270D ND 1ug/kg1.516
Pyrene 129-00-0 8270D 140 1ug/kg0.613.3
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.116
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.216
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 61 33-102
2-Fluorophenol 63 35-115
Nitrobenzene-d5 55 22-109
Phenol-d5 73 33-122
Terphenyl-d14 58 41-120
2,4,6-Tribromophenol 65 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1843 SLS 01/17/2017 2128 31784
1 3050B 6010C 2 01/20/2017 2127 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 2.2 1mg/kg0.411.3
Barium 7440-39-3 6010C 71 1mg/kg0.252.3
Cadmium 7440-43-9 6010C 0.053 J 1mg/kg0.0440.44
Chromium 7440-47-3 6010C 46 1mg/kg0.130.89
Lead 7439-92-1 6010C 20 1mg/kg0.390.89
Mercury 7439-97-6 7471B 0.080 J 1mg/kg0.00690.091
Selenium 7782-49-2 6010C ND 1mg/kg0.721.8
Silver 7440-22-4 6010C ND 1mg/kg0.140.89
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/20/2017 1641 ECB 32172 5.55
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1219
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 108 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1421 ECB 31997 5.04
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.221
Benzene 71-43-2 8260B ND 1ug/kg2.15.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.15.2
Bromoform 75-25-2 8260B ND 1ug/kg2.15.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.15.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.221
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.15.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.15.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.15.2
Chloroethane 75-00-3 8260B ND 1ug/kg2.15.2
Chloroform 67-66-3 8260B ND 1ug/kg2.15.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.15.2
Cyclohexane 110-82-7 8260B ND 1ug/kg2.15.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.15.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.15.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.15.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.15.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.15.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.15.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.15.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.15.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.15.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.15.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.15.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.15.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.15.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.15.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.15.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.15.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1421 ECB 31997 5.04
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.210
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.15.2
Methyl acetate 79-20-9 8260B ND 1ug/kg2.15.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.15.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.210
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.15.2
Methylene chloride 75-09-2 8260B ND 1ug/kg2.15.2
Styrene 100-42-5 8260B ND 1ug/kg2.15.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.15.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.15.2
Toluene 108-88-3 8260B ND 1ug/kg2.15.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.15.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.15.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.15.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.15.2
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.15.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.15.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.210
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 53-142
Bromofluorobenzene 106 47-138
Toluene-d8 104 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1714 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.852.8
Acenaphthylene 208-96-8 8270D ND 1ug/kg0.972.8
Acetophenone 98-86-2 8270D ND 1ug/kg1.413
Anthracene 120-12-7 8270D ND 1ug/kg0.522.8
Atrazine 1912-24-9 8270D ND 1ug/kg1.013
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.013
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg0.602.8
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg0.672.8
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg0.512.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1714 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg0.662.8
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg0.492.8
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg0.9713
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg0.9413
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.7013
Caprolactam 105-60-2 8270D ND 1ug/kg2.513
Carbazole 86-74-8 8270D ND 1ug/kg0.8613
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.313
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.113
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.213
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.7113
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.113
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.613
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.113
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.8213
Chrysene 218-01-9 8270D ND 1ug/kg0.462.8
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.522.8
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.013
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.013
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.313
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.8213
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg7.613
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.213
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.013
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.068
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.468
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.528
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.128
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2513
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.4613
Fluoranthene 206-44-0 8270D ND 1ug/kg0.432.8
Fluorene 86-73-7 8270D ND 1ug/kg0.582.8
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.013
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg1.713
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.368
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.113
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg1.02.8
Isophorone 78-59-1 8270D ND 1ug/kg1.213
2-Methylnaphthalene 91-57-6 8270D ND 1ug/kg1.02.8
2-Methylphenol 95-48-7 8270D ND 1ug/kg3.613
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-1-SB
SA17067-002
01/16/2017 1145
01/17/2017
Solid
% Solids:94.8 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1714 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.428
Naphthalene 91-20-3 8270D ND 1ug/kg0.992.8
2-Nitroaniline 88-74-4 8270D ND 1ug/kg3.828
3-Nitroaniline 99-09-2 8270D ND 1ug/kg3.828
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.128
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.613
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.628
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2168
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.113
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.013
Pentachlorophenol 87-86-5 8270D ND 1ug/kg5.468
Phenanthrene 85-01-8 8270D ND 1ug/kg0.742.8
Phenol 108-95-2 8270D ND 1ug/kg1.213
Pyrene 129-00-0 8270D ND 1ug/kg0.512.8
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg0.8913
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg0.9813
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 50 33-102
2-Fluorophenol 56 35-115
Nitrobenzene-d5 46 22-109
Phenol-d5 65 33-122
Terphenyl-d14 51 41-120
2,4,6-Tribromophenol 53 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1850 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2132 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 1.3 J 1mg/kg0.812.7
Barium 7440-39-3 6010C 27 1mg/kg0.514.6
Cadmium 7440-43-9 6010C ND 1mg/kg0.0890.89
Chromium 7440-47-3 6010C 0.96 J 1mg/kg0.261.8
Lead 7439-92-1 6010C ND 1mg/kg0.771.8
Mercury 7439-97-6 7471B ND 1mg/kg0.00640.084
Selenium 7782-49-2 6010C ND 1mg/kg1.43.5
Silver 7440-22-4 6010C ND 1mg/kg0.281.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/20/2017 1703 ECB 32172 5.41
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1423
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 105 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1443 ECB 31997 5.46
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.623
Benzene 71-43-2 8260B ND 1ug/kg2.35.8
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.35.8
Bromoform 75-25-2 8260B ND 1ug/kg2.35.8
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.35.8
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.623
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.35.8
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.35.8
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.35.8
Chloroethane 75-00-3 8260B ND 1ug/kg2.35.8
Chloroform 67-66-3 8260B ND 1ug/kg2.35.8
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.35.8
Cyclohexane 110-82-7 8260B ND 1ug/kg2.35.8
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.8
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.35.8
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.35.8
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.35.8
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.35.8
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.35.8
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.35.8
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.35.8
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.35.8
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.35.8
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.35.8
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.35.8
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.35.8
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.35.8
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.35.8
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.35.8
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1443 ECB 31997 5.46
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.612
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.35.8
Methyl acetate 79-20-9 8260B ND 1ug/kg2.35.8
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.35.8
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.612
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.35.8
Methylene chloride 75-09-2 8260B ND 1ug/kg2.35.8
Styrene 100-42-5 8260B ND 1ug/kg2.35.8
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.35.8
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.35.8
Toluene 108-88-3 8260B ND 1ug/kg2.35.8
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.35.8
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.35.8
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.35.8
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.35.8
Trichloroethene 79-01-6 8260B ND 1ug/kg2.35.8
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.35.8
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.35.8
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.612
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 97 53-142
Bromofluorobenzene 107 47-138
Toluene-d8 106 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1738 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg1.03.3
Acenaphthylene 208-96-8 8270D 1.2 J 1ug/kg1.23.3
Acetophenone 98-86-2 8270D ND 1ug/kg1.716
Anthracene 120-12-7 8270D 1.1 J 1ug/kg0.633.3
Atrazine 1912-24-9 8270D ND 1ug/kg1.216
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.216
Benzo(a)anthracene 56-55-3 8270D 4.6 1ug/kg0.733.3
Benzo(a)pyrene 50-32-8 8270D 4.8 1ug/kg0.823.3
Benzo(b)fluoranthene 205-99-2 8270D 8.3 1ug/kg0.623.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1738 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D 3.4 1ug/kg0.803.3
Benzo(k)fluoranthene 207-08-9 8270D 2.3 J 1ug/kg0.593.3
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.216
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.116
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8516
Caprolactam 105-60-2 8270D ND 1ug/kg3.016
Carbazole 86-74-8 8270D ND 1ug/kg1.016
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.616
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.416
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.516
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8616
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.416
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg3.116
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.616
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9916
Chrysene 218-01-9 8270D 5.6 1ug/kg0.563.3
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.633.3
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.216
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.516
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.616
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9916
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg9.116
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.716
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.516
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.583
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg4.183
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg3.033
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.633
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.3016
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5616
Fluoranthene 206-44-0 8270D 6.7 1ug/kg0.523.3
Fluorene 86-73-7 8270D ND 1ug/kg0.703.3
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.216
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.116
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.683
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.416
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 2.6 J 1ug/kg1.23.3
Isophorone 78-59-1 8270D ND 1ug/kg1.516
2-Methylnaphthalene 91-57-6 8270D 17 1ug/kg1.23.3
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.316
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-2-SS
SA17067-003
01/16/2017 1600
01/17/2017
Solid
% Solids:79.3 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1738 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg4.133
Naphthalene 91-20-3 8270D 13 1ug/kg1.23.3
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.633
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.633
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.933
Nitrobenzene 98-95-3 8270D ND 1ug/kg2.016
2-Nitrophenol 88-75-5 8270D ND 1ug/kg2.033
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2683
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.416
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.216
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.583
Phenanthrene 85-01-8 8270D 9.9 1ug/kg0.893.3
Phenol 108-95-2 8270D ND 1ug/kg1.516
Pyrene 129-00-0 8270D 6.2 1ug/kg0.623.3
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.116
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.216
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 52 33-102
2-Fluorophenol 53 35-115
Nitrobenzene-d5 48 22-109
Phenol-d5 60 33-122
Terphenyl-d14 53 41-120
2,4,6-Tribromophenol 57 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1853 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2136 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 2.8 J 1mg/kg1.23.9
Barium 7440-39-3 6010C 93 1mg/kg0.746.7
Cadmium 7440-43-9 6010C ND 1mg/kg0.131.3
Chromium 7440-47-3 6010C 61 1mg/kg0.372.6
Lead 7439-92-1 6010C 16 1mg/kg1.12.6
Mercury 7439-97-6 7471B 0.056 J 1mg/kg0.00710.094
Selenium 7782-49-2 6010C ND 1mg/kg2.15.2
Silver 7440-22-4 6010C ND 1mg/kg0.412.6
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/25/2017 0038 ECP 32474 4.63
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1524
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1506 ECB 31997 5.55
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.120
Benzene 71-43-2 8260B ND 1ug/kg2.05.1
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.05.1
Bromoform 75-25-2 8260B ND 1ug/kg2.05.1
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.05.1
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.120
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.05.1
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.05.1
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.05.1
Chloroethane 75-00-3 8260B ND 1ug/kg2.05.1
Chloroform 67-66-3 8260B ND 1ug/kg2.05.1
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.05.1
Cyclohexane 110-82-7 8260B ND 1ug/kg2.05.1
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.05.1
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.05.1
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.05.1
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.05.1
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.05.1
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.05.1
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.05.1
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.05.1
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.05.1
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.05.1
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.05.1
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.05.1
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.05.1
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.05.1
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.05.1
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.05.1
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1506 ECB 31997 5.55
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.110
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.05.1
Methyl acetate 79-20-9 8260B ND 1ug/kg2.05.1
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.05.1
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.110
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.05.1
Methylene chloride 75-09-2 8260B ND 1ug/kg2.05.1
Styrene 100-42-5 8260B ND 1ug/kg2.05.1
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.05.1
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.05.1
Toluene 108-88-3 8260B ND 1ug/kg2.05.1
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.05.1
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.05.1
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.05.1
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.05.1
Trichloroethene 79-01-6 8260B ND 1ug/kg2.05.1
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.05.1
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.05.1
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.110
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 104 47-138
Toluene-d8 105 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1803 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.943.1
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.1
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D 1.1 J 1ug/kg0.583.1
Atrazine 1912-24-9 8270D ND 1ug/kg1.115
Benzaldehyde 100-52-7 8270D 4.0 J 1ug/kg1.115
Benzo(a)anthracene 56-55-3 8270D 5.6 1ug/kg0.673.1
Benzo(a)pyrene 50-32-8 8270D 6.4 1ug/kg0.753.1
Benzo(b)fluoranthene 205-99-2 8270D 10 1ug/kg0.573.1
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1803 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D 3.0 J 1ug/kg0.743.1
Benzo(k)fluoranthene 207-08-9 8270D 3.1 1ug/kg0.543.1
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.015
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.7815
Caprolactam 105-60-2 8270D ND 1ug/kg2.715
Carbazole 86-74-8 8270D ND 1ug/kg0.9515
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.215
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.7915
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.215
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.815
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.415
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9115
Chrysene 218-01-9 8270D 7.1 1ug/kg0.513.1
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.583.1
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.115
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9115
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.415
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.515
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.376
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.776
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.731
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.431
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2715
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5115
Fluoranthene 206-44-0 8270D 9.7 1ug/kg0.483.1
Fluorene 86-73-7 8270D ND 1ug/kg0.653.1
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.115
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg1.915
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.576
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.215
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 2.6 J 1ug/kg1.13.1
Isophorone 78-59-1 8270D ND 1ug/kg1.415
2-Methylnaphthalene 91-57-6 8270D 7.3 1ug/kg1.13.1
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.015
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3-SS
SA17067-004
01/16/2017 1520
01/17/2017
Solid
% Solids:88.2 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1803 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.731
Naphthalene 91-20-3 8270D 5.3 1ug/kg1.13.1
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.231
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.231
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.531
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.815
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.831
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2376
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.215
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.115
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.076
Phenanthrene 85-01-8 8270D 8.8 1ug/kg0.823.1
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D 8.7 1ug/kg0.573.1
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg0.9915
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 52 33-102
2-Fluorophenol 56 35-115
Nitrobenzene-d5 48 22-109
Phenol-d5 63 33-122
Terphenyl-d14 48 41-120
2,4,6-Tribromophenol 56 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1855 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/23/2017 1426 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 2.4 J 1mg/kg0.903.0
Barium 7440-39-3 6010C 37 1mg/kg0.565.1
Cadmium 7440-43-9 6010C ND 1mg/kg0.0980.98
Chromium 7440-47-3 6010C 75 1mg/kg0.282.0
Lead 7439-92-1 6010C 8.6 1mg/kg0.862.0
Mercury 7439-97-6 7471B 0.051 J 1mg/kg0.00680.090
Selenium 7782-49-2 6010C ND 1mg/kg1.63.9
Silver 7440-22-4 6010C ND 1mg/kg0.312.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/25/2017 0015 ECP 32474 5.86
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1321
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 107 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1528 ECB 31997 5.88
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.221
Benzene 71-43-2 8260B ND 1ug/kg2.15.2
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.15.2
Bromoform 75-25-2 8260B ND 1ug/kg2.15.2
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.15.2
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.221
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.15.2
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.15.2
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.15.2
Chloroethane 75-00-3 8260B ND 1ug/kg2.15.2
Chloroform 67-66-3 8260B ND 1ug/kg2.15.2
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.15.2
Cyclohexane 110-82-7 8260B ND 1ug/kg2.15.2
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.15.2
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.15.2
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.15.2
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.15.2
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.15.2
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.15.2
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.15.2
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.15.2
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.15.2
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.15.2
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.15.2
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.15.2
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.15.2
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.15.2
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.15.2
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.15.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 23 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1528 ECB 31997 5.88
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.210
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.15.2
Methyl acetate 79-20-9 8260B ND 1ug/kg2.15.2
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.15.2
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.210
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.15.2
Methylene chloride 75-09-2 8260B ND 1ug/kg2.15.2
Styrene 100-42-5 8260B ND 1ug/kg2.15.2
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.15.2
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.15.2
Toluene 108-88-3 8260B ND 1ug/kg2.15.2
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.15.2
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.15.2
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.15.2
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.15.2
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.2
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.15.2
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.15.2
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.210
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 105 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1828 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.993.2
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.2
Acetophenone 98-86-2 8270D ND 1ug/kg1.716
Anthracene 120-12-7 8270D ND 1ug/kg0.613.2
Atrazine 1912-24-9 8270D ND 1ug/kg1.216
Benzaldehyde 100-52-7 8270D 5.3 J 1ug/kg1.216
Benzo(a)anthracene 56-55-3 8270D 4.1 1ug/kg0.703.2
Benzo(a)pyrene 50-32-8 8270D 3.5 1ug/kg0.793.2
Benzo(b)fluoranthene 205-99-2 8270D 6.3 1ug/kg0.603.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 24 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1828 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D 1.9 J 1ug/kg0.783.2
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg0.573.2
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.116
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.116
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8216
Caprolactam 105-60-2 8270D ND 1ug/kg2.916
Carbazole 86-74-8 8270D ND 1ug/kg1.016
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.616
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.316
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.416
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8416
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.316
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg3.016
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.516
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9616
Chrysene 218-01-9 8270D 3.3 1ug/kg0.543.2
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.613.2
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.216
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.416
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.616
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9616
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.816
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.616
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.416
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.480
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.980
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.932
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.532
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2916
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5416
Fluoranthene 206-44-0 8270D 4.5 1ug/kg0.503.2
Fluorene 86-73-7 8270D ND 1ug/kg0.683.2
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.216
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.016
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.680
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.316
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 1.6 J 1ug/kg1.23.2
Isophorone 78-59-1 8270D ND 1ug/kg1.416
2-Methylnaphthalene 91-57-6 8270D 4.4 1ug/kg1.23.2
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.216
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 25 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-3 DUP
SA17067-005
01/16/2017 1520
01/17/2017
Solid
% Solids:81.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1828 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.932
Naphthalene 91-20-3 8270D 3.1 J 1ug/kg1.23.2
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.432
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.432
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.832
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.916
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.932
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2580
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.316
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.216
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.380
Phenanthrene 85-01-8 8270D 4.3 1ug/kg0.863.2
Phenol 108-95-2 8270D ND 1ug/kg1.416
Pyrene 129-00-0 8270D 4.1 1ug/kg0.603.2
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.016
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.116
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 56 33-102
2-Fluorophenol 54 35-115
Nitrobenzene-d5 53 22-109
Phenol-d5 59 33-122
Terphenyl-d14 51 41-120
2,4,6-Tribromophenol 58 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1857 SLS 01/17/2017 2128 31784
1 3050B 6010C 5 01/20/2017 2145 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 2.8 J 1mg/kg1.24.0
Barium 7440-39-3 6010C 40 1mg/kg0.767.0
Cadmium 7440-43-9 6010C ND 1mg/kg0.131.3
Chromium 7440-47-3 6010C 93 1mg/kg0.392.7
Lead 7439-92-1 6010C 14 1mg/kg1.22.7
Mercury 7439-97-6 7471B 0.24 1mg/kg0.00760.10
Selenium 7782-49-2 6010C ND 1mg/kg2.25.3
Silver 7440-22-4 6010C ND 1mg/kg0.422.7
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 26 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/24/2017 2353 ECP 32474 6.13
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1219
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1551 ECB 31997 5.47
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.322
Benzene 71-43-2 8260B ND 1ug/kg2.25.4
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.25.4
Bromoform 75-25-2 8260B ND 1ug/kg2.25.4
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.25.4
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.322
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.25.4
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.25.4
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.25.4
Chloroethane 75-00-3 8260B ND 1ug/kg2.25.4
Chloroform 67-66-3 8260B ND 1ug/kg2.25.4
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.25.4
Cyclohexane 110-82-7 8260B ND 1ug/kg2.25.4
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.25.4
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.25.4
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.25.4
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.25.4
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.25.4
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.25.4
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.25.4
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.25.4
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.25.4
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.25.4
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.25.4
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.25.4
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.25.4
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.25.4
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.25.4
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.25.4
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 27 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1551 ECB 31997 5.47
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.311
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.25.4
Methyl acetate 79-20-9 8260B ND 1ug/kg2.25.4
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.25.4
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.311
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.25.4
Methylene chloride 75-09-2 8260B ND 1ug/kg2.25.4
Styrene 100-42-5 8260B ND 1ug/kg2.25.4
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.25.4
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.25.4
Toluene 108-88-3 8260B ND 1ug/kg2.25.4
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.25.4
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.25.4
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.25.4
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.25.4
Trichloroethene 79-01-6 8260B ND 1ug/kg2.25.4
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.25.4
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.25.4
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.311
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 53-142
Bromofluorobenzene 103 47-138
Toluene-d8 103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1852 RBH 01/23/2017 1403 32300
2 3546 8270D 10 01/25/2017 1021 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D 190 1ug/kg0.953.1
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.1
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D 270 1ug/kg0.583.1
Atrazine 1912-24-9 8270D ND 1ug/kg1.115
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.115
Benzo(a)anthracene 56-55-3 8270D 820 2ug/kg6.731
Benzo(a)pyrene 50-32-8 8270D 760 2ug/kg7.531
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 28 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1852 RBH 01/23/2017 1403 32300
2 3546 8270D 10 01/25/2017 1021 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(b)fluoranthene 205-99-2 8270D 1100 2ug/kg5.731
Benzo(g,h,i)perylene 191-24-2 8270D 140 1ug/kg0.743.1
Benzo(k)fluoranthene 207-08-9 8270D 340 1ug/kg0.553.1
1,1'-Biphenyl 92-52-4 8270D 9.1 J 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.015
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.7915
Caprolactam 105-60-2 8270D ND 1ug/kg2.715
Carbazole 86-74-8 8270D 160 1ug/kg0.9615
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.315
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8015
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.315
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.815
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.415
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9115
Chrysene 218-01-9 8270D 800 2ug/kg5.131
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.583.1
Dibenzofuran 132-64-9 8270D 81 1ug/kg1.115
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9115
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.415
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.515
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.376
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.876
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.731
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.431
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2715
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5115
Fluoranthene 206-44-0 8270D 2000 2ug/kg4.831
Fluorene 86-73-7 8270D 140 1ug/kg0.653.1
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.115
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg1.915
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.576
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.315
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 160 1ug/kg1.13.1
Isophorone 78-59-1 8270D ND 1ug/kg1.415
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 29 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1852 RBH 01/23/2017 1403 32300
2 3546 8270D 10 01/25/2017 1021 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Methylnaphthalene 91-57-6 8270D 33 1ug/kg1.13.1
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.015
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.831
Naphthalene 91-20-3 8270D 71 1ug/kg1.13.1
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.231
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.231
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.631
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.815
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.831
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2476
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.315
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.115
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.076
Phenanthrene 85-01-8 8270D 1700 2ug/kg8.231
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D 1500 2ug/kg5.731
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg0.9915
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
2-Fluorobiphenyl 57 33-102 76 33-102
2-Fluorophenol 56 35-115 57 35-115
Nitrobenzene-d5 52 22-109 66 22-109
Phenol-d5 63 33-122 65 33-122
Terphenyl-d14 48 41-120 84 41-120
2,4,6-Tribromophenol 61 30-117 46 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1900 SLS 01/17/2017 2128 31784
1 3050B 6010C 1 01/20/2017 2150 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 1.3 1mg/kg0.230.76
Barium 7440-39-3 6010C 36 1mg/kg0.141.3
Cadmium 7440-43-9 6010C ND 1mg/kg0.0250.25
Chromium 7440-47-3 6010C 6.8 1mg/kg0.0730.51
Lead 7439-92-1 6010C 6.4 1mg/kg0.220.51
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 30 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-4-SS
SA17067-006
01/16/2017 1420
01/17/2017
Solid
% Solids:84.9 01/17/2017 2213
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1900 SLS 01/17/2017 2128 31784
1 3050B 6010C 1 01/20/2017 2150 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Mercury 7439-97-6 7471B 0.019 J 1mg/kg0.00690.091
Selenium 7782-49-2 6010C ND 1mg/kg0.411.0
Silver 7440-22-4 6010C ND 1mg/kg0.0800.51
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 31 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/24/2017 2330 ECP 32474 4.96
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1524
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 118 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1613 ECB 31997 5.14
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.723
Benzene 71-43-2 8260B ND 1ug/kg2.35.9
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.35.9
Bromoform 75-25-2 8260B ND 1ug/kg2.35.9
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.35.9
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.723
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.35.9
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.35.9
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.35.9
Chloroethane 75-00-3 8260B ND 1ug/kg2.35.9
Chloroform 67-66-3 8260B ND 1ug/kg2.35.9
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.35.9
Cyclohexane 110-82-7 8260B ND 1ug/kg2.35.9
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.35.9
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.35.9
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.35.9
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.35.9
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.35.9
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.35.9
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.35.9
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.35.9
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.35.9
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.35.9
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.35.9
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.35.9
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.35.9
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.35.9
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.35.9
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.35.9
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 32 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1613 ECB 31997 5.14
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.712
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.35.9
Methyl acetate 79-20-9 8260B ND 1ug/kg2.35.9
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.35.9
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.712
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.35.9
Methylene chloride 75-09-2 8260B ND 1ug/kg2.35.9
Styrene 100-42-5 8260B ND 1ug/kg2.35.9
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.35.9
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.35.9
Toluene 108-88-3 8260B ND 1ug/kg2.35.9
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.35.9
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.35.9
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.35.9
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.35.9
Trichloroethene 79-01-6 8260B ND 1ug/kg2.35.9
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.35.9
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.35.9
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.712
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 53-142
Bromofluorobenzene 109 47-138
Toluene-d8 103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1917 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.973.2
Acenaphthylene 208-96-8 8270D ND 1ug/kg1.13.2
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D ND 1ug/kg0.603.2
Atrazine 1912-24-9 8270D ND 1ug/kg1.215
Benzaldehyde 100-52-7 8270D ND 1ug/kg1.215
Benzo(a)anthracene 56-55-3 8270D ND 1ug/kg0.693.2
Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg0.773.2
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/kg0.593.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 33 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1917 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg0.763.2
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg0.563.2
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.115
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8115
Caprolactam 105-60-2 8270D ND 1ug/kg2.815
Carbazole 86-74-8 8270D ND 1ug/kg0.9915
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.315
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8215
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.315
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.915
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.515
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9415
Chrysene 218-01-9 8270D ND 1ug/kg0.533.2
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.603.2
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.215
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9415
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.715
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.615
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.379
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.979
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.832
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.532
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2815
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg0.5315
Fluoranthene 206-44-0 8270D ND 1ug/kg0.493.2
Fluorene 86-73-7 8270D ND 1ug/kg0.673.2
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.215
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.015
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.579
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.315
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg1.23.2
Isophorone 78-59-1 8270D ND 1ug/kg1.415
2-Methylnaphthalene 91-57-6 8270D 2.2 J 1ug/kg1.23.2
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.115
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 34 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
SB-5-SB
SA17067-007
01/16/2017 1400
01/17/2017
Solid
% Solids:83.0 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1917 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.932
Naphthalene 91-20-3 8270D 2.0 J 1ug/kg1.13.2
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.332
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.332
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.732
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.915
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.932
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2479
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.315
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.215
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.279
Phenanthrene 85-01-8 8270D ND 1ug/kg0.853.2
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D ND 1ug/kg0.593.2
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.015
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 52 33-102
2-Fluorophenol 61 35-115
Nitrobenzene-d5 49 22-109
Phenol-d5 65 33-122
Terphenyl-d14 53 41-120
2,4,6-Tribromophenol 55 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1902 SLS 01/17/2017 2128 31784
1 3050B 6010C 1 01/20/2017 2154 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 0.97 1mg/kg0.230.74
Barium 7440-39-3 6010C 27 1mg/kg0.141.3
Cadmium 7440-43-9 6010C ND 1mg/kg0.0250.25
Chromium 7440-47-3 6010C 1.3 1mg/kg0.0710.50
Lead 7439-92-1 6010C 2.0 1mg/kg0.220.50
Mercury 7439-97-6 7471B ND 1mg/kg0.00740.097
Selenium 7782-49-2 6010C ND 1mg/kg0.400.99
Silver 7440-22-4 6010C ND 1mg/kg0.0780.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 35 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B (SIM)1 01/24/2017 2308 ECP 32474 4.65
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/kg1525
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 113 70-130
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1636 ECB 31997 5.54
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/kg4.221
Benzene 71-43-2 8260B ND 1ug/kg2.15.3
Bromodichloromethane 75-27-4 8260B ND 1ug/kg2.15.3
Bromoform 75-25-2 8260B ND 1ug/kg2.15.3
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg2.15.3
2-Butanone (MEK)78-93-3 8260B ND 1ug/kg4.221
Carbon disulfide 75-15-0 8260B ND 1ug/kg2.15.3
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg2.15.3
Chlorobenzene 108-90-7 8260B ND 1ug/kg2.15.3
Chloroethane 75-00-3 8260B ND 1ug/kg2.15.3
Chloroform 67-66-3 8260B ND 1ug/kg2.15.3
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg2.15.3
Cyclohexane 110-82-7 8260B ND 1ug/kg2.15.3
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/kg2.15.3
Dibromochloromethane 124-48-1 8260B ND 1ug/kg2.15.3
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg2.15.3
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg2.15.3
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg2.15.3
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg2.15.3
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg2.15.3
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg2.15.3
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg2.15.3
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg2.15.3
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg2.15.3
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg2.15.3
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg2.15.3
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg2.15.3
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg2.15.3
Ethylbenzene 100-41-4 8260B ND 1ug/kg2.15.3
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 36 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 01/19/2017 1636 ECB 31997 5.54
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/kg4.211
Isopropylbenzene 98-82-8 8260B ND 1ug/kg2.15.3
Methyl acetate 79-20-9 8260B ND 1ug/kg2.15.3
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/kg2.15.3
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg4.211
Methylcyclohexane 108-87-2 8260B ND 1ug/kg2.15.3
Methylene chloride 75-09-2 8260B ND 1ug/kg2.15.3
Styrene 100-42-5 8260B ND 1ug/kg2.15.3
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg2.15.3
Tetrachloroethene 127-18-4 8260B ND 1ug/kg2.15.3
Toluene 108-88-3 8260B ND 1ug/kg2.15.3
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/kg2.15.3
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg2.15.3
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg2.15.3
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg2.15.3
Trichloroethene 79-01-6 8260B ND 1ug/kg2.15.3
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg2.15.3
Vinyl chloride 75-01-4 8260B ND 1ug/kg2.15.3
Xylenes (total)1330-20-7 8260B ND 1ug/kg4.211
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 100 47-138
Toluene-d8 103 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1941 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/kg0.973.2
Acenaphthylene 208-96-8 8270D 8.4 1ug/kg1.13.2
Acetophenone 98-86-2 8270D ND 1ug/kg1.615
Anthracene 120-12-7 8270D 12 1ug/kg0.603.2
Atrazine 1912-24-9 8270D ND 1ug/kg1.215
Benzaldehyde 100-52-7 8270D 5.6 J 1ug/kg1.215
Benzo(a)anthracene 56-55-3 8270D 100 1ug/kg0.693.2
Benzo(a)pyrene 50-32-8 8270D 93 1ug/kg0.773.2
Benzo(b)fluoranthene 205-99-2 8270D 180 1ug/kg0.583.2
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 37 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1941 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D 17 1ug/kg0.763.2
Benzo(k)fluoranthene 207-08-9 8270D 60 1ug/kg0.563.2
1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg1.115
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg1.115
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg0.8115
Caprolactam 105-60-2 8270D ND 1ug/kg2.815
Carbazole 86-74-8 8270D ND 1ug/kg0.9815
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg1.515
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg1.315
4-Chloroaniline 106-47-8 8270D ND 1ug/kg1.415
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg0.8215
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg1.315
2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg2.915
2-Chlorophenol 95-57-8 8270D ND 1ug/kg2.515
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg0.9415
Chrysene 218-01-9 8270D 94 1ug/kg0.533.2
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg0.603.2
Dibenzofuran 132-64-9 8270D ND 1ug/kg1.215
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg2.315
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg1.515
Diethylphthalate 84-66-2 8270D ND 1ug/kg0.9415
Dimethyl phthalate 131-11-3 8270D ND 1ug/kg8.715
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg2.615
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg2.315
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg2.378
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg3.978
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg2.832
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg2.532
Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg0.2815
bis(2-Ethylhexyl)phthalate 117-81-7 8270D 4.0 BJ 1ug/kg0.5315
Fluoranthene 206-44-0 8270D 170 1ug/kg0.493.2
Fluorene 86-73-7 8270D 1.6 J 1ug/kg0.673.2
Hexachlorobenzene 118-74-1 8270D ND 1ug/kg1.115
Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg2.015
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg1.578
Hexachloroethane 67-72-1 8270D ND 1ug/kg1.315
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D 21 1ug/kg1.23.2
Isophorone 78-59-1 8270D ND 1ug/kg1.415
2-Methylnaphthalene 91-57-6 8270D 11 1ug/kg1.23.2
2-Methylphenol 95-48-7 8270D ND 1ug/kg4.115
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 38 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
BG-1
SA17067-008
01/16/2017 1440
01/17/2017
Solid
% Solids:85.5 01/17/2017 2213
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 1 01/24/2017 1941 RBH 01/23/2017 1403 32300
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
3+4-Methylphenol 106-44-5 8270D ND 1ug/kg3.932
Naphthalene 91-20-3 8270D 9.8 1ug/kg1.13.2
2-Nitroaniline 88-74-4 8270D ND 1ug/kg4.332
3-Nitroaniline 99-09-2 8270D ND 1ug/kg4.332
4-Nitroaniline 100-01-6 8270D ND 1ug/kg4.732
Nitrobenzene 98-95-3 8270D ND 1ug/kg1.915
2-Nitrophenol 88-75-5 8270D ND 1ug/kg1.932
4-Nitrophenol 100-02-7 8270D ND 1ug/kg2478
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg1.315
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg1.215
Pentachlorophenol 87-86-5 8270D ND 1ug/kg6.278
Phenanthrene 85-01-8 8270D 41 1ug/kg0.843.2
Phenol 108-95-2 8270D ND 1ug/kg1.415
Pyrene 129-00-0 8270D 140 1ug/kg0.583.2
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg1.015
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg1.115
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 56 33-102
2-Fluorophenol 59 35-115
Nitrobenzene-d5 51 22-109
Phenol-d5 63 33-122
Terphenyl-d14 54 41-120
2,4,6-Tribromophenol 60 30-117
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7471B 7471B 1 01/18/2017 1904 SLS 01/17/2017 2128 31784
1 3050B 6010C 2 01/20/2017 2159 CJZ 01/18/2017 0949 31801
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C 2.6 1mg/kg0.300.99
Barium 7440-39-3 6010C 160 1mg/kg0.191.7
Cadmium 7440-43-9 6010C 0.23 J 1mg/kg0.0330.33
Chromium 7440-47-3 6010C 25 1mg/kg0.0950.66
Lead 7439-92-1 6010C 130 1mg/kg0.290.66
Mercury 7439-97-6 7471B 0.18 1mg/kg0.00640.084
Selenium 7782-49-2 6010C ND 1mg/kg0.541.3
Silver 7440-22-4 6010C ND 1mg/kg0.100.66
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 39 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS (SIM)
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B (SIM)1 01/18/2017 1126 TML 31846
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,4-Dioxane 123-91-1 8260B (SIM)ND 1ug/L1.03.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 40-170
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1036 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L2.020
Benzene 71-43-2 8260B ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.401.0
Bromoform 75-25-2 8260B ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.401.0
Chloroethane 75-00-3 8260B ND 1ug/L0.402.0
Chloroform 67-66-3 8260B ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.401.0
Cyclohexane 110-82-7 8260B ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.402.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.401.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 40 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1036 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Hexanone 591-78-6 8260B ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260B ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.401.0
Styrene 100-42-5 8260B ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.401.0
Toluene 108-88-3 8260B ND 1ug/L0.401.0
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 70-130
Bromofluorobenzene 103 70-130
Toluene-d8 99 70-130
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 01/23/2017 1737 RBH 01/19/2017 1436 32000
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acenaphthene 83-32-9 8270D ND 1ug/L0.0400.20
Acenaphthylene 208-96-8 8270D ND 1ug/L0.0400.20
Acetophenone 98-86-2 8270D ND 1ug/L0.231.0
Anthracene 120-12-7 8270D ND 1ug/L0.0600.20
Atrazine 1912-24-9 8270D ND 1ug/L0.201.0
Benzaldehyde 100-52-7 8270D ND 1ug/L0.275.0
Benzo(a)anthracene 56-55-3 8270D ND 1ug/L0.0400.20
Benzo(a)pyrene 50-32-8 8270D ND 1ug/L0.0700.20
Benzo(b)fluoranthene 205-99-2 8270D ND 1ug/L0.0400.20
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 41 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 01/23/2017 1737 RBH 01/19/2017 1436 32000
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/L0.0400.20
Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/L0.0400.20
1,1'-Biphenyl 92-52-4 8270D ND 1ug/L0.211.0
4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/L0.151.0
Butyl benzyl phthalate 85-68-7 8270D ND 1ug/L0.215.0
Caprolactam 105-60-2 8270D ND 1ug/L0.715.0
Carbazole 86-74-8 8270D ND 1ug/L0.0401.0
4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/L0.261.0
4-Chloroaniline 106-47-8 8270D ND 1ug/L0.131.0
bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/L0.0601.0
bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/L0.161.0
bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/L0.171.0
2-Chloronaphthalene 91-58-7 8270D ND 1ug/L0.151.0
2-Chlorophenol 95-57-8 8270D ND 1ug/L0.151.0
4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/L0.161.0
Chrysene 218-01-9 8270D ND 1ug/L0.0300.20
Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/L0.0300.20
Dibenzofuran 132-64-9 8270D ND 1ug/L0.161.0
3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/L0.815.0
2,4-Dichlorophenol 120-83-2 8270D ND 1ug/L0.191.0
Diethylphthalate 84-66-2 8270D ND 1ug/L0.195.0
Dimethyl phthalate 131-11-3 8270D ND 1ug/L0.185.0
2,4-Dimethylphenol 105-67-9 8270D ND 1ug/L0.151.0
Di-n-butyl phthalate 84-74-2 8270D ND 1ug/L0.425.0
4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/L0.895.0
2,4-Dinitrophenol 51-28-5 8270D ND 1ug/L1.35.0
2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/L0.362.0
2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/L0.342.0
Di-n-octylphthalate 117-84-0 8270D ND 1ug/L0.485.0
bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/L0.385.0
Fluoranthene 206-44-0 8270D ND 1ug/L0.0770.20
Fluorene 86-73-7 8270D ND 1ug/L0.0300.20
Hexachlorobenzene 118-74-1 8270D ND 1ug/L0.151.0
Hexachlorobutadiene 87-68-3 8270D ND 1ug/L0.171.0
Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/L1.15.0
Hexachloroethane 67-72-1 8270D ND 1ug/L0.171.0
Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/L0.0400.20
Isophorone 78-59-1 8270D ND 1ug/L0.221.0
1-Methylnaphthalene 90-12-0 8270D ND 1ug/L0.0300.20
2-Methylnaphthalene 91-57-6 8270D ND 1ug/L0.0400.20
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 42 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270D 1 01/23/2017 1737 RBH 01/19/2017 1436 32000
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
2-Methylphenol 95-48-7 8270D ND 1ug/L0.211.0
3+4-Methylphenol 106-44-5 8270D ND 1ug/L0.462.0
Naphthalene 91-20-3 8270D ND 1ug/L0.0500.20
2-Nitroaniline 88-74-4 8270D ND 1ug/L0.662.0
3-Nitroaniline 99-09-2 8270D ND 1ug/L0.152.0
4-Nitroaniline 100-01-6 8270D ND 1ug/L1.32.0
Nitrobenzene 98-95-3 8270D ND 1ug/L0.171.0
2-Nitrophenol 88-75-5 8270D ND 1ug/L0.442.0
4-Nitrophenol 100-02-7 8270D ND 1ug/L2.15.0
N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/L0.281.0
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/L0.841.0
Pentachlorophenol 87-86-5 8270D ND 1ug/L1.35.0
Phenanthrene 85-01-8 8270D ND 1ug/L0.0600.20
Phenol 108-95-2 8270D ND 1ug/L0.191.0
Pyrene 129-00-0 8270D ND 1ug/L0.0750.20
2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/L0.191.0
2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/L0.221.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 53 37-129
2-Fluorophenol 50 24-127
Nitrobenzene-d5 54 38-127
Phenol-d5 54 28-128
Terphenyl-d14 63 10-148
2,4,6-Tribromophenol 58 41-144
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 01/18/2017 1636 COH 01/18/2017 1222 31803
1 3005A 6010C 1 01/19/2017 2151 CJZ 01/18/2017 0917 31799
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Arsenic 7440-38-2 6010C ND 1mg/L0.00220.015
Barium 7440-39-3 6010C ND 1mg/L0.00190.025
Cadmium 7440-43-9 6010C ND 1mg/L0.000540.0050
Chromium 7440-47-3 6010C ND 1mg/L0.000720.010
Lead 7439-92-1 6010C ND 1mg/L0.00470.010
Mercury 7439-97-6 7470A ND 1mg/L0.0000280.00010
Selenium 7782-49-2 6010C ND 1mg/L0.00850.020
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 43 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
EQUIPMENT BLANK
SA17067-009
01/16/2017 1200
01/17/2017
Aqueous
RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 01/18/2017 1636 COH 01/18/2017 1222 31803
1 3005A 6010C 1 01/19/2017 2151 CJZ 01/18/2017 0917 31799
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Silver 7440-22-4 6010C ND 1mg/L0.00210.010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 44 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
FIELD BLANK
SA17067-010
01/16/2017 1330
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1059 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B 2.2 J 1ug/L2.020
Benzene 71-43-2 8260B ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.401.0
Bromoform 75-25-2 8260B ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.401.0
Chloroethane 75-00-3 8260B ND 1ug/L0.402.0
Chloroform 67-66-3 8260B ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.401.0
Cyclohexane 110-82-7 8260B ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.402.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260B ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260B ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.401.0
Styrene 100-42-5 8260B ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.401.0
Toluene 108-88-3 8260B ND 1ug/L0.401.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 45 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
FIELD BLANK
SA17067-010
01/16/2017 1330
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1059 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 91 70-130
Bromofluorobenzene 99 70-130
Toluene-d8 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 46 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
TRIP BLANK
SA17067-011
01/16/2017
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1123 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
Acetone 67-64-1 8260B ND 1ug/L2.020
Benzene 71-43-2 8260B ND 1ug/L0.401.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L0.401.0
Bromoform 75-25-2 8260B ND 1ug/L0.401.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L0.402.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L2.010
Carbon disulfide 75-15-0 8260B ND 1ug/L0.401.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.401.0
Chloroethane 75-00-3 8260B ND 1ug/L0.402.0
Chloroform 67-66-3 8260B ND 1ug/L0.401.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L0.401.0
Cyclohexane 110-82-7 8260B ND 1ug/L0.401.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L0.401.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.401.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L0.402.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L0.401.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L0.401.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L0.401.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L0.401.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L0.401.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L0.401.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.401.0
2-Hexanone 591-78-6 8260B ND 1ug/L2.010
Isopropylbenzene 98-82-8 8260B ND 1ug/L0.401.0
Methyl acetate 79-20-9 8260B ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.401.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L2.010
Methylcyclohexane 108-87-2 8260B ND 1ug/L0.405.0
Methylene chloride 75-09-2 8260B ND 1ug/L0.401.0
Styrene 100-42-5 8260B ND 1ug/L0.401.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L0.401.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L0.401.0
Toluene 108-88-3 8260B ND 1ug/L0.401.0
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 47 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Summit Engineering and Construction Services, Inc.
TRIP BLANK
SA17067-011
01/16/2017
01/17/2017
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/18/2017 1123 PAP 31828
AnalyticalCAS
Parameter Number Method Result Q PQL Units RunMDL
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L0.401.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L0.401.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L0.401.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L0.401.0
Trichloroethene 79-01-6 8260B ND 1ug/L0.401.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L0.401.0
Vinyl chloride 75-01-4 8260B ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 90 70-130
Bromofluorobenzene 99 70-130
Toluene-d8 100 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 48 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

QC Summary
Page: 49 of 87
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31828-001
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 01/18/2017 0947202.0 ug/L1
Benzene ND 01/18/2017 09471.0 0.40 ug/L1
Bromodichloromethane ND 01/18/2017 09471.0 0.40 ug/L1
Bromoform ND 01/18/2017 09471.0 0.40 ug/L1
Bromomethane (Methyl bromide)ND 01/18/2017 09472.0 0.40 ug/L1
2-Butanone (MEK)ND 01/18/2017 0947102.0 ug/L1
Carbon disulfide ND 01/18/2017 09471.0 0.40 ug/L1
Carbon tetrachloride ND 01/18/2017 09471.0 0.40 ug/L1
Chlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
Chloroethane ND 01/18/2017 09472.0 0.40 ug/L1
Chloroform ND 01/18/2017 09471.0 0.40 ug/L1
Chloromethane (Methyl chloride)ND 01/18/2017 09471.0 0.40 ug/L1
Cyclohexane ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/18/2017 09471.0 0.40 ug/L1
Dibromochloromethane ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
1,3-Dichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
1,4-Dichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
Dichlorodifluoromethane ND 01/18/2017 09472.0 0.40 ug/L1
1,2-Dichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
1,1-Dichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
cis-1,2-Dichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
trans-1,2-Dichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
1,1-Dichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
1,2-Dichloropropane ND 01/18/2017 09471.0 0.40 ug/L1
cis-1,3-Dichloropropene ND 01/18/2017 09471.0 0.40 ug/L1
trans-1,3-Dichloropropene ND 01/18/2017 09471.0 0.40 ug/L1
Ethylbenzene ND 01/18/2017 09471.0 0.40 ug/L1
2-Hexanone ND 01/18/2017 0947102.0 ug/L1
Isopropylbenzene ND 01/18/2017 09471.0 0.40 ug/L1
Methyl acetate ND 01/18/2017 09471.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 01/18/2017 09471.0 0.40 ug/L1
4-Methyl-2-pentanone ND 01/18/2017 0947102.0 ug/L1
Methylcyclohexane ND 01/18/2017 09475.0 0.40 ug/L1
Methylene chloride ND 01/18/2017 09471.0 0.40 ug/L1
Styrene ND 01/18/2017 09471.0 0.40 ug/L1
1,1,2,2-Tetrachloroethane ND 01/18/2017 09471.0 0.40 ug/L1
Tetrachloroethene ND 01/18/2017 09471.0 0.40 ug/L1
Toluene ND 01/18/2017 09471.0 0.40 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/18/2017 09471.0 0.40 ug/L1
1,2,4-Trichlorobenzene ND 01/18/2017 09471.0 0.40 ug/L1
1,1,1-Trichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
1,1,2-Trichloroethane ND 01/18/2017 09471.0 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 50 of 87
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31828-001
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 01/18/2017 09471.0 0.40 ug/L1
Trichlorofluoromethane ND 01/18/2017 09471.0 0.40 ug/L1
Vinyl chloride ND 01/18/2017 09471.0 0.40 ug/L1
Xylenes (total)ND 01/18/2017 09471.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 91 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 51 of 87
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31828-002
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 100 01/18/2017 084210010060-1401
Benzene 48 01/18/2017 0842965070-1301
Bromodichloromethane 49 01/18/2017 0842975070-1301
Bromoform 39 01/18/2017 0842795070-1301
Bromomethane (Methyl bromide)52 01/18/2017 08421045060-1401
2-Butanone (MEK)99 01/18/2017 08429910060-1401
Carbon disulfide 50 01/18/2017 0842995060-1401
Carbon tetrachloride 48 01/18/2017 0842965070-1301
Chlorobenzene 49 01/18/2017 0842995070-1301
Chloroethane 50 01/18/2017 0842995060-1401
Chloroform 46 01/18/2017 0842935070-1301
Chloromethane (Methyl chloride)48 01/18/2017 0842975060-1401
Cyclohexane 46 01/18/2017 0842915070-1301
1,2-Dibromo-3-chloropropane (DBCP)43 01/18/2017 0842865070-1301
Dibromochloromethane 49 01/18/2017 0842975070-1301
1,2-Dibromoethane (EDB)48 01/18/2017 0842965070-1301
1,2-Dichlorobenzene 47 01/18/2017 0842945070-1301
1,3-Dichlorobenzene 47 01/18/2017 0842945070-1301
1,4-Dichlorobenzene 45 01/18/2017 0842905070-1301
Dichlorodifluoromethane 62 01/18/2017 08421245060-1401
1,2-Dichloroethane 48 01/18/2017 0842955070-1301
1,1-Dichloroethane 49 01/18/2017 0842975070-1301
cis-1,2-Dichloroethene 48 01/18/2017 0842955070-1301
trans-1,2-Dichloroethene 47 01/18/2017 0842945070-1301
1,1-Dichloroethene 48 01/18/2017 0842965070-1301
1,2-Dichloropropane 49 01/18/2017 0842995070-1301
cis-1,3-Dichloropropene 47 01/18/2017 0842945070-1301
trans-1,3-Dichloropropene 45 01/18/2017 0842915070-1301
Ethylbenzene 52 01/18/2017 08421045070-1301
2-Hexanone 98 01/18/2017 08429810060-1401
Isopropylbenzene 47 01/18/2017 0842945070-1301
Methyl acetate 51 01/18/2017 08421015015-1281
Methyl tertiary butyl ether (MTBE)47 01/18/2017 0842935070-1301
4-Methyl-2-pentanone 96 01/18/2017 08429610060-1401
Methylcyclohexane 47 01/18/2017 0842945070-1301
Methylene chloride 45 01/18/2017 0842905070-1301
Styrene 46 01/18/2017 0842935070-1301
1,1,2,2-Tetrachloroethane 46 01/18/2017 0842935060-1401
Tetrachloroethene 52 01/18/2017 08421035070-1301
Toluene 51 01/18/2017 08421025070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 47 01/18/2017 0842945070-1301
1,2,4-Trichlorobenzene 45 01/18/2017 0842915070-1301
1,1,1-Trichloroethane 48 01/18/2017 0842955070-1301
1,1,2-Trichloroethane 48 01/18/2017 0842955070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 52 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31828-002
31828 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 48 01/18/2017 0842975070-1301
Trichlorofluoromethane 52 01/18/2017 08421045070-1301
Vinyl chloride 51 01/18/2017 08421035070-1301
Xylenes (total)98 01/18/2017 08429810070-1301
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 104 70-130
1,2-Dichloroethane-d4 85 70-130
Toluene-d8 100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 53 of 87
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Volatile Organic Compounds by GC/MS (SIM) - MB
Batch:Prep Method:
Sample ID:SQ31846-001
31846 5030B
Analytical Method:8260B (SIM)
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,4-Dioxane ND 01/18/2017 10533.0 1.0 ug/L1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 102 40-170
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 54 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS (SIM) - LCS
Batch:Prep Method:
Sample ID:SQ31846-002
31846 5030B
Analytical Method:8260B (SIM)
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,4-Dioxane 55 01/18/2017 10191105070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 102 40-170
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 55 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31997-001
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Acetone ND 01/19/2017 1026204.0 ug/kg1
Benzene ND 01/19/2017 10265.0 2.0 ug/kg1
Bromodichloromethane ND 01/19/2017 10265.0 2.0 ug/kg1
Bromoform ND 01/19/2017 10265.0 2.0 ug/kg1
Bromomethane (Methyl bromide)ND 01/19/2017 10265.0 2.0 ug/kg1
2-Butanone (MEK)ND 01/19/2017 1026204.0 ug/kg1
Carbon disulfide ND 01/19/2017 10265.0 2.0 ug/kg1
Carbon tetrachloride ND 01/19/2017 10265.0 2.0 ug/kg1
Chlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
Chloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
Chloroform ND 01/19/2017 10265.0 2.0 ug/kg1
Chloromethane (Methyl chloride)ND 01/19/2017 10265.0 2.0 ug/kg1
Cyclohexane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/19/2017 10265.0 2.0 ug/kg1
Dibromochloromethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dibromoethane (EDB)ND 01/19/2017 10265.0 2.0 ug/kg1
1,4-Dichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
1,3-Dichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
Dichlorodifluoromethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,1-Dichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
trans-1,2-Dichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
cis-1,2-Dichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
1,1-Dichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
1,2-Dichloropropane ND 01/19/2017 10265.0 2.0 ug/kg1
trans-1,3-Dichloropropene ND 01/19/2017 10265.0 2.0 ug/kg1
cis-1,3-Dichloropropene ND 01/19/2017 10265.0 2.0 ug/kg1
Ethylbenzene ND 01/19/2017 10265.0 2.0 ug/kg1
2-Hexanone ND 01/19/2017 1026104.0 ug/kg1
Isopropylbenzene ND 01/19/2017 10265.0 2.0 ug/kg1
Methyl acetate ND 01/19/2017 10265.0 2.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 01/19/2017 10265.0 2.0 ug/kg1
4-Methyl-2-pentanone ND 01/19/2017 1026104.0 ug/kg1
Methylcyclohexane ND 01/19/2017 10265.0 2.0 ug/kg1
Methylene chloride ND 01/19/2017 10265.0 2.0 ug/kg1
Styrene ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,2,2-Tetrachloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
Tetrachloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
Toluene ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,2,4-Trichlorobenzene ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,2-Trichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
1,1,1-Trichloroethane ND 01/19/2017 10265.0 2.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 56 of 87
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Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ31997-001
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Trichloroethene ND 01/19/2017 10265.0 2.0 ug/kg1
Trichlorofluoromethane ND 01/19/2017 10265.0 2.0 ug/kg1
Vinyl chloride ND 01/19/2017 10265.0 2.0 ug/kg1
Xylenes (total)ND 01/19/2017 1026104.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 112 47-138
1,2-Dichloroethane-d4 98 53-142
Toluene-d8 106 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 57 of 87
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31997-002
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 01/19/2017 092710010060-1401
Benzene 45 01/19/2017 0927905069-1231
Bromodichloromethane 49 01/19/2017 0927995069-1211
Bromoform 47 01/19/2017 0927945061-1191
Bromomethane (Methyl bromide)59 01/19/2017 09271175010-1681
2-Butanone (MEK)88 01/19/2017 09278810057-1481
Carbon disulfide 49 01/19/2017 0927985058-1221
Carbon tetrachloride 47 01/19/2017 0927955058-1361
Chlorobenzene 50 01/19/2017 09271005059-1291
Chloroethane 52 01/19/2017 09271055060-1401
Chloroform 47 01/19/2017 0927955071-1251
Chloromethane (Methyl chloride)48 01/19/2017 0927965034-1341
Cyclohexane 46 01/19/2017 0927925053-1391
1,2-Dibromo-3-chloropropane (DBCP)44 01/19/2017 0927875055-1251
Dibromochloromethane 49 01/19/2017 0927995066-1191
1,2-Dibromoethane (EDB)47 01/19/2017 0927945074-1241
1,4-Dichlorobenzene 49 01/19/2017 0927985052-1331
1,3-Dichlorobenzene 48 01/19/2017 0927975051-1341
1,2-Dichlorobenzene 49 01/19/2017 0927985057-1311
Dichlorodifluoromethane 60 01/19/2017 09271205010-1571
1,2-Dichloroethane 49 01/19/2017 0927995067-1291
1,1-Dichloroethane 48 01/19/2017 0927955071-1271
trans-1,2-Dichloroethene 47 01/19/2017 0927935068-1311
cis-1,2-Dichloroethene 45 01/19/2017 0927915070-1221
1,1-Dichloroethene 44 01/19/2017 0927885069-1381
1,2-Dichloropropane 48 01/19/2017 0927965072-1241
trans-1,3-Dichloropropene 50 01/19/2017 09271005070-1241
cis-1,3-Dichloropropene 49 01/19/2017 0927985070-1261
Ethylbenzene 48 01/19/2017 0927965059-1281
2-Hexanone 92 01/19/2017 09279210054-1371
Isopropylbenzene 50 01/19/2017 0927995050-1361
Methyl acetate 44 01/19/2017 0927885059-1371
Methyl tertiary butyl ether (MTBE)45 01/19/2017 0927895070-1301
4-Methyl-2-pentanone 95 01/19/2017 09279510060-1341
Methylcyclohexane 45 01/19/2017 0927895041-1441
Methylene chloride 47 01/19/2017 0927955070-1301
Styrene 50 01/19/2017 09271005054-1361
1,1,2,2-Tetrachloroethane 46 01/19/2017 0927915069-1321
Tetrachloroethene 49 01/19/2017 0927985045-1501
Toluene 49 01/19/2017 0927975061-1291
1,1,2-Trichloro-1,2,2-Trifluoroethane 48 01/19/2017 0927965049-1361
1,2,4-Trichlorobenzene 46 01/19/2017 0927935034-1451
1,1,2-Trichloroethane 47 01/19/2017 0927945055-1281
1,1,1-Trichloroethane 47 01/19/2017 0927955063-1281
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 58 of 87
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Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ31997-002
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Trichloroethene 45 01/19/2017 0927915062-1261
Trichlorofluoromethane 48 01/19/2017 0927965045-1381
Vinyl chloride 50 01/19/2017 09271005042-1321
Xylenes (total)100 01/19/2017 092710310058-1281
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 110 47-138
1,2-Dichloroethane-d4 95 53-142
Toluene-d8 107 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 59 of 87
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Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-001DU
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Acetone 5.5 01/19/2017 182820020ND1
Benzene ND 01/19/2017 18280.00 20ND1
Bromodichloromethane ND 01/19/2017 18280.00 20ND1
Bromoform ND 01/19/2017 18280.00 20ND1
Bromomethane (Methyl bromide)ND 01/19/2017 18280.00 20ND1
2-Butanone (MEK)ND 01/19/2017 18280.00 20ND1
Carbon disulfide ND 01/19/2017 18280.00 20ND1
Carbon tetrachloride ND 01/19/2017 18280.00 20ND1
Chlorobenzene ND 01/19/2017 18280.00 20ND1
Chloroethane ND 01/19/2017 18280.00 20ND1
Chloroform ND 01/19/2017 18280.00 20ND1
Chloromethane (Methyl chloride)ND 01/19/2017 18280.00 20ND1
Cyclohexane ND 01/19/2017 18280.00 20ND1
1,2-Dibromo-3-chloropropane (DBCP)ND 01/19/2017 18280.00 20ND1
Dibromochloromethane ND 01/19/2017 18280.00 20ND1
1,2-Dibromoethane (EDB)ND 01/19/2017 18280.00 20ND1
1,2-Dichlorobenzene ND 01/19/2017 18280.00 20ND1
1,3-Dichlorobenzene ND 01/19/2017 18280.00 20ND1
1,4-Dichlorobenzene ND 01/19/2017 18280.00 20ND1
Dichlorodifluoromethane ND 01/19/2017 18280.00 20ND1
1,1-Dichloroethane ND 01/19/2017 18280.00 20ND1
1,2-Dichloroethane ND 01/19/2017 18280.00 20ND1
1,1-Dichloroethene ND 01/19/2017 18280.00 20ND1
cis-1,2-Dichloroethene ND 01/19/2017 18280.00 20ND1
trans-1,2-Dichloroethene ND 01/19/2017 18280.00 20ND1
1,2-Dichloropropane ND 01/19/2017 18280.00 20ND1
cis-1,3-Dichloropropene ND 01/19/2017 18280.00 20ND1
trans-1,3-Dichloropropene ND 01/19/2017 18280.00 20ND1
Ethylbenzene ND 01/19/2017 18280.00 20ND1
2-Hexanone ND 01/19/2017 18280.00 20ND1
Isopropylbenzene ND 01/19/2017 18280.00 20ND1
Methyl acetate ND 01/19/2017 18280.00 20ND1
Methyl tertiary butyl ether (MTBE)ND 01/19/2017 18280.00 20ND1
4-Methyl-2-pentanone ND 01/19/2017 18280.00 20ND1
Methylcyclohexane ND 01/19/2017 18280.00 20ND1
Methylene chloride ND 01/19/2017 18280.00 20ND1
Styrene ND 01/19/2017 18280.00 20ND1
1,1,2,2-Tetrachloroethane ND 01/19/2017 18280.00 20ND1
Tetrachloroethene ND 01/19/2017 18280.00 20ND1
Toluene ND 01/19/2017 18280.00 20ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 01/19/2017 18280.00 20ND1
1,2,4-Trichlorobenzene ND 01/19/2017 18280.00 20ND1
1,1,1-Trichloroethane ND 01/19/2017 18280.00 20ND1
1,1,2-Trichloroethane ND 01/19/2017 18280.00 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 60 of 87
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Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-001DU
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
Trichloroethene ND 01/19/2017 18280.00 20ND1
Trichlorofluoromethane ND 01/19/2017 18280.00 20ND1
Vinyl chloride ND 01/19/2017 18280.00 20ND1
Xylenes (total)ND 01/19/2017 18280.00 20ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 102 47-138
Toluene-d8 107 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 61 of 87
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Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-002MS
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Acetone 94 01/19/2017 18511088760-140ND1
Benzene 39 01/19/2017 1851914369-123ND1
Bromodichloromethane 43 01/19/2017 18511004369-121ND1
Bromoform 42 01/19/2017 1851964361-119ND1
Bromomethane (Methyl bromide)50 01/19/2017 18511164335-144ND1
2-Butanone (MEK)77 01/19/2017 1851898757-148ND1
Carbon disulfide 43 01/19/2017 1851994358-122ND1
Carbon tetrachloride 46 01/19/2017 18511074358-136ND1
Chlorobenzene 43 01/19/2017 18511004359-129ND1
Chloroethane 44 01/19/2017 18511024350-132ND1
Chloroform 40 01/19/2017 1851934371-125ND1
Chloromethane (Methyl chloride)43 01/19/2017 18511004334-134ND1
Cyclohexane 44 01/19/2017 18511024353-139ND1
1,2-Dibromo-3-chloropropane (DBCP)41 01/19/2017 1851954355-125ND1
Dibromochloromethane 42 01/19/2017 1851984366-119ND1
1,2-Dibromoethane (EDB)40 01/19/2017 1851924374-124ND1
1,2-Dichlorobenzene 42 01/19/2017 1851974357-131ND1
1,3-Dichlorobenzene 42 01/19/2017 1851974351-134ND1
1,4-Dichlorobenzene 42 01/19/2017 1851974352-133ND1
Dichlorodifluoromethane 57 01/19/2017 18511314310-157ND1
1,1-Dichloroethane 39 01/19/2017 1851914371-127ND1
1,2-Dichloroethane 44 01/19/2017 18511024367-129ND1
1,1-Dichloroethene 38 01/19/2017 1851894369-138ND1
cis-1,2-Dichloroethene 37 01/19/2017 1851864370-122ND1
trans-1,2-Dichloroethene 39 01/19/2017 1851914368-131ND1
1,2-Dichloropropane 40 01/19/2017 1851924372-124ND1
cis-1,3-Dichloropropene 41 01/19/2017 1851944370-126ND1
trans-1,3-Dichloropropene 41 01/19/2017 1851944370-124ND1
Ethylbenzene 43 01/19/2017 1851994359-128ND1
2-Hexanone 85 01/19/2017 1851988754-137ND1
Isopropylbenzene 45 01/19/2017 18511054350-136ND1
Methyl acetate 40 01/19/2017 1851924359-137ND1
Methyl tertiary butyl ether (MTBE)34 01/19/2017 1851804370-130ND1
4-Methyl-2-pentanone 85 01/19/2017 1851988760-134ND1
Methylcyclohexane 45 01/19/2017 18511034341-144ND1
Methylene chloride 38 01/19/2017 1851884377-129ND1
Styrene 43 01/19/2017 18511004354-136ND1
1,1,2,2-Tetrachloroethane 40 01/19/2017 1851924369-132ND1
Tetrachloroethene 46 01/19/2017 18511074370-130ND1
Toluene 42 01/19/2017 1851984361-129ND1
1,1,2-Trichloro-1,2,2-Trifluoroethane 46 01/19/2017 18511054349-136ND1
1,2,4-Trichlorobenzene 40 01/19/2017 1851924334-145ND1
1,1,1-Trichloroethane 43 01/19/2017 18511004363-128ND1
1,1,2-Trichloroethane 39 01/19/2017 1851904355-128ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 62 of 87
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Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-002MS
31997 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
Trichloroethene 42 01/19/2017 1851984362-126ND1
Trichlorofluoromethane 45 01/19/2017 18511034345-138ND1
Vinyl chloride 44 01/19/2017 18511034342-132ND1
Xylenes (total)90 01/19/2017 18511048758-128ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 101 53-142
Bromofluorobenzene 113 47-138
Toluene-d8 105 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 63 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ32172-001
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
1,4-Dioxane ND 01/20/2017 13192012ug/kg1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 64 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ32172-002
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
1,4-Dioxane 110 01/20/2017 123411410070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 97 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 65 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-002MS
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
1,4-Dioxane 95 01/20/2017 1941999670-130ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 117 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 66 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-003DU
32172 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
1,4-Dioxane ND 01/20/2017 19180.00 40ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 67 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:SQ32474-001
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
1,4-Dioxane ND 01/24/2017 22292012ug/kg1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 111 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 68 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:SQ32474-002
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
1,4-Dioxane 120 01/24/2017 213112110070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 69 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - MS
Batch:Prep Method:
Sample ID:SA17067-007MS
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)(ug/kg)
1,4-Dioxane 130 01/25/2017 014511612070-130ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 118 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 70 of 87
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Shealy Environmental Services, Inc.

Volatile Organic Compounds by GC/MS - Duplicate
Batch:Prep Method:
Sample ID:SA17067-008DU
32474 5035
Analytical Method:8260B (SIM)
Matrix:Solid
Parameter
Result
Q Analysis Date% RPD
% RPD
Limit
Sample
Amount
Dil(ug/kg)(ug/kg)
1,4-Dioxane ND 01/25/2017 01230.00 40ND1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 115 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 71 of 87
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Shealy Environmental Services, Inc.

Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-001
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
1,1'-Biphenyl ND 01/23/2017 16471.0 0.21 ug/L1
1-Methylnaphthalene ND 01/23/2017 16470.20 0.030 ug/L1
2,4,5-Trichlorophenol ND 01/23/2017 16471.0 0.19 ug/L1
2,4,6-Trichlorophenol ND 01/23/2017 16471.0 0.22 ug/L1
2,4-Dichlorophenol ND 01/23/2017 16471.0 0.19 ug/L1
2,4-Dimethylphenol ND 01/23/2017 16471.0 0.15 ug/L1
2,4-Dinitrophenol ND 01/23/2017 16475.0 1.3 ug/L1
2,4-Dinitrotoluene ND 01/23/2017 16472.0 0.36 ug/L1
2,6-Dinitrotoluene ND 01/23/2017 16472.0 0.34 ug/L1
2-Chloronaphthalene ND 01/23/2017 16471.0 0.15 ug/L1
2-Chlorophenol ND 01/23/2017 16471.0 0.15 ug/L1
2-Methylnaphthalene ND 01/23/2017 16470.20 0.040 ug/L1
2-Methylphenol ND 01/23/2017 16471.0 0.21 ug/L1
2-Nitroaniline ND 01/23/2017 16472.0 0.66 ug/L1
2-Nitrophenol ND 01/23/2017 16472.0 0.44 ug/L1
3+4-Methylphenol ND 01/23/2017 16472.0 0.46 ug/L1
3,3'-Dichlorobenzidine ND 01/23/2017 16475.0 0.81 ug/L1
3-Nitroaniline ND 01/23/2017 16472.0 0.15 ug/L1
4,6-Dinitro-2-methylphenol ND 01/23/2017 16475.0 0.89 ug/L1
4-Bromophenyl phenyl ether ND 01/23/2017 16471.0 0.15 ug/L1
4-Chloro-3-methyl phenol ND 01/23/2017 16471.0 0.26 ug/L1
4-Chloroaniline ND 01/23/2017 16471.0 0.13 ug/L1
4-Chlorophenyl phenyl ether ND 01/23/2017 16471.0 0.16 ug/L1
4-Nitroaniline ND 01/23/2017 16472.0 1.3 ug/L1
4-Nitrophenol ND 01/23/2017 16475.0 2.1 ug/L1
Acenaphthene ND 01/23/2017 16470.20 0.040 ug/L1
Acenaphthylene ND 01/23/2017 16470.20 0.040 ug/L1
Acetophenone ND 01/23/2017 16471.0 0.23 ug/L1
Anthracene ND 01/23/2017 16470.20 0.060 ug/L1
Atrazine ND 01/23/2017 16471.0 0.20 ug/L1
Benzaldehyde ND 01/23/2017 16475.0 0.27 ug/L1
Benzo(a)anthracene ND 01/23/2017 16470.20 0.040 ug/L1
Benzo(a)pyrene ND 01/23/2017 16470.20 0.070 ug/L1
Benzo(b)fluoranthene ND 01/23/2017 16470.20 0.040 ug/L1
Benzo(g,h,i)perylene ND 01/23/2017 16470.20 0.040 ug/L1
Benzo(k)fluoranthene ND 01/23/2017 16470.20 0.040 ug/L1
bis (2-Chloro-1-methylethyl) ether ND 01/23/2017 16471.0 0.17 ug/L1
bis(2-Chloroethoxy)methane ND 01/23/2017 16471.0 0.060 ug/L1
bis(2-Chloroethyl)ether ND 01/23/2017 16471.0 0.16 ug/L1
bis(2-Ethylhexyl)phthalate ND 01/23/2017 16475.0 0.38 ug/L1
Butyl benzyl phthalate ND 01/23/2017 16475.0 0.21 ug/L1
Caprolactam ND 01/23/2017 16475.0 0.71 ug/L1
Carbazole ND 01/23/2017 16471.0 0.040 ug/L1
Chrysene ND 01/23/2017 16470.20 0.030 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 72 of 87
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Shealy Environmental Services, Inc.

Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-001
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Di-n-butyl phthalate ND 01/23/2017 16475.0 0.42 ug/L1
Di-n-octylphthalate ND 01/23/2017 16475.0 0.48 ug/L1
Dibenzo(a,h)anthracene ND 01/23/2017 16470.20 0.030 ug/L1
Dibenzofuran ND 01/23/2017 16471.0 0.16 ug/L1
Diethylphthalate ND 01/23/2017 16475.0 0.19 ug/L1
Dimethyl phthalate ND 01/23/2017 16475.0 0.18 ug/L1
Fluoranthene ND 01/23/2017 16470.20 0.077 ug/L1
Fluorene ND 01/23/2017 16470.20 0.030 ug/L1
Hexachlorobenzene ND 01/23/2017 16471.0 0.15 ug/L1
Hexachlorobutadiene ND 01/23/2017 16471.0 0.17 ug/L1
Hexachlorocyclopentadiene ND 01/23/2017 16475.0 1.1 ug/L1
Hexachloroethane ND 01/23/2017 16471.0 0.17 ug/L1
Indeno(1,2,3-c,d)pyrene ND 01/23/2017 16470.20 0.040 ug/L1
Isophorone ND 01/23/2017 16471.0 0.22 ug/L1
N-Nitrosodi-n-propylamine ND 01/23/2017 16471.0 0.28 ug/L1
N-Nitrosodiphenylamine (Diphenylamine)ND 01/23/2017 16471.0 0.84 ug/L1
Naphthalene ND 01/23/2017 16470.20 0.050 ug/L1
Nitrobenzene ND 01/23/2017 16471.0 0.17 ug/L1
Pentachlorophenol ND 01/23/2017 16475.0 1.3 ug/L1
Phenanthrene ND 01/23/2017 16470.20 0.060 ug/L1
Phenol ND 01/23/2017 16471.0 0.19 ug/L1
Pyrene ND 01/23/2017 16470.20 0.075 ug/L1
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 72 41-144
2-Fluorobiphenyl 66 37-129
2-Fluorophenol 61 24-127
Nitrobenzene-d5 65 38-127
Phenol-d5 68 28-128
Terphenyl-d14 81 10-148
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 73 of 87
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Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-002
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1'-Biphenyl 6.6 01/23/2017 1712661042-1201
1-Methylnaphthalene 6.8 01/23/2017 1712681041-1251
2,4,5-Trichlorophenol 7.5 01/23/2017 1712751056-1181
2,4,6-Trichlorophenol 6.9 01/23/2017 1712691055-1211
2,4-Dichlorophenol 7.2 01/23/2017 1712721055-1171
2,4-Dimethylphenol 8.8 01/23/2017 1712881036-1701
2,4-Dinitrophenol 18 01/23/2017 1712902047-1331
2,4-Dinitrotoluene 8.3 01/23/2017 1712831059-1271
2,6-Dinitrotoluene 7.8 01/23/2017 1712781059-1261
2-Chloronaphthalene 6.6 01/23/2017 1712661046-1001
2-Chlorophenol 6.6 01/23/2017 1712661050-1171
2-Methylnaphthalene 6.9 01/23/2017 1712691057-11151
2-Methylphenol 7.0 01/23/2017 1712701056-1191
2-Nitroaniline 8.0 01/23/2017 1712801060-1241
2-Nitrophenol 7.5 01/23/2017 1712751051-1181
3+4-Methylphenol 7.4 01/23/2017 1712741053-1191
3-Nitroaniline 7.8 01/23/2017 1712781043-1231
4,6-Dinitro-2-methylphenol 9.4 01/23/2017 1712941056-1281
4-Bromophenyl phenyl ether 7.2 01/23/2017 1712721055-1211
4-Chloro-3-methyl phenol 8.0 01/23/2017 1712801058-1251
4-Chloroaniline 7.6 01/23/2017 1712761010-1281
4-Chlorophenyl phenyl ether 7.1 01/23/2017 1712711055-1211
4-Nitroaniline 8.0 01/23/2017 1712801060-1351
4-Nitrophenol 16 01/23/2017 1712792053-1301
Acenaphthene 7.1 01/23/2017 1712711054-1181
Acenaphthylene 7.3 01/23/2017 1712731048-1551
Acetophenone 7.4 01/23/2017 1712741052-1251
Anthracene 7.7 01/23/2017 1712771055-1221
Atrazine 7.6 01/23/2017 1712761025-1211
Benzaldehyde 6.9 01/23/2017 1712691045-1151
Benzo(a)anthracene 7.5 01/23/2017 1712751056-1231
Benzo(a)pyrene 6.8 01/23/2017 1712681054-1241
Benzo(b)fluoranthene 7.2 01/23/2017 1712721055-1361
Benzo(g,h,i)perylene 9.0 01/23/2017 1712901042-1291
Benzo(k)fluoranthene 6.9 01/23/2017 1712691053-1321
bis (2-Chloro-1-methylethyl) ether 6.3 01/23/2017 1712631042-1241
bis(2-Chloroethoxy)methane 7.1 01/23/2017 1712711044-1271
bis(2-Chloroethyl)ether 6.2 01/23/2017 1712621046-1201
bis(2-Ethylhexyl)phthalate 7.5 01/23/2017 1712751056-1281
Butyl benzyl phthalate 8.9 01/23/2017 1712891054-1351
Caprolactam 7.3 01/23/2017 1712731044-1521
Carbazole 8.2 01/23/2017 1712821045-1011
Chrysene 7.5 01/23/2017 1712751054-1201
Di-n-butyl phthalate 8.1 01/23/2017 1712811060-1311
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 74 of 87
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Shealy Environmental Services, Inc.

Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32000-002
32000 3520C
01/19/2017 1436Analytical Method:8270D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Di-n-octylphthalate 6.5 01/23/2017 1712651050-1361
Dibenzo(a,h)anthracene 7.5 01/23/2017 1712751050-1271
Dibenzofuran 7.6 01/23/2017 1712761058-1181
Diethylphthalate 8.2 01/23/2017 1712821060-1251
Dimethyl phthalate 7.9 01/23/2017 1712791060-1221
Fluoranthene 7.7 01/23/2017 1712771058-1241
Fluorene 7.5 01/23/2017 1712751057-1191
Hexachlorobenzene 7.0 01/23/2017 1712701055-1181
Hexachlorobutadiene 5.5 01/23/2017 1712551053-1161
Hexachlorocyclopentadiene 19 01/23/2017 1712385016-961
Hexachloroethane 5.2 01/23/2017 1712521031-1101
Indeno(1,2,3-c,d)pyrene 8.5 01/23/2017 1712851048-1261
Isophorone 7.0 01/23/2017 1712701057-1231
N-Nitrosodi-n-propylamine 7.2 01/23/2017 1712721054-1271
N-Nitrosodiphenylamine (Diphenylamine)7.6 01/23/2017 1712761035-1461
Naphthalene 6.9 01/23/2017 1712691052-1091
Nitrobenzene 6.8 01/23/2017 1712681051-1221
Pentachlorophenol 16 01/23/2017 1712782042-1311
Phenanthrene 7.6 01/23/2017 1712761056-1191
Phenol 6.1 01/23/2017 1712611049-1171
Pyrene 8.1 01/23/2017 1712811055-1271
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 77 41-144
2-Fluorobiphenyl 66 37-129
2-Fluorophenol 59 24-127
Nitrobenzene-d5 68 38-127
Phenol-d5 65 28-128
Terphenyl-d14 71 10-148
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 75 of 87
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Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-001
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
1,1'-Biphenyl ND 01/24/2017 0929130.95 ug/kg1
2,4,5-Trichlorophenol ND 01/24/2017 0929130.87 ug/kg1
2,4,6-Trichlorophenol ND 01/24/2017 0929130.96 ug/kg1
2,4-Dichlorophenol ND 01/24/2017 0929131.3 ug/kg1
2,4-Dimethylphenol ND 01/24/2017 0929132.2 ug/kg1
2,4-Dinitrophenol ND 01/24/2017 0929673.3 ug/kg1
2,4-Dinitrotoluene ND 01/24/2017 0929272.4 ug/kg1
2,6-Dinitrotoluene ND 01/24/2017 0929272.1 ug/kg1
2-Chloronaphthalene ND 01/24/2017 0929132.5 ug/kg1
2-Chlorophenol ND 01/24/2017 0929132.1 ug/kg1
2-Methylnaphthalene ND 01/24/2017 09292.7 0.99 ug/kg1
2-Methylphenol ND 01/24/2017 0929133.5 ug/kg1
2-Nitroaniline ND 01/24/2017 0929273.7 ug/kg1
2-Nitrophenol ND 01/24/2017 0929271.6 ug/kg1
3+4-Methylphenol ND 01/24/2017 0929273.3 ug/kg1
3,3'-Dichlorobenzidine ND 01/24/2017 0929132.0 ug/kg1
3-Nitroaniline ND 01/24/2017 0929273.7 ug/kg1
4,6-Dinitro-2-methylphenol ND 01/24/2017 0929672.0 ug/kg1
4-Bromophenyl phenyl ether ND 01/24/2017 0929130.92 ug/kg1
4-Chloro-3-methyl phenol ND 01/24/2017 0929131.1 ug/kg1
4-Chloroaniline ND 01/24/2017 0929131.2 ug/kg1
4-Chlorophenyl phenyl ether ND 01/24/2017 0929130.80 ug/kg1
4-Nitroaniline ND 01/24/2017 0929274.0 ug/kg1
4-Nitrophenol ND 01/24/2017 09296721ug/kg1
Acenaphthene ND 01/24/2017 09292.7 0.83 ug/kg1
Acenaphthylene ND 01/24/2017 09292.7 0.95 ug/kg1
Acetophenone ND 01/24/2017 0929131.4 ug/kg1
Anthracene ND 01/24/2017 09292.7 0.51 ug/kg1
Atrazine ND 01/24/2017 0929131.0 ug/kg1
Benzaldehyde ND 01/24/2017 0929131.0 ug/kg1
Benzo(a)anthracene ND 01/24/2017 09292.7 0.59 ug/kg1
Benzo(a)pyrene ND 01/24/2017 09292.7 0.66 ug/kg1
Benzo(b)fluoranthene ND 01/24/2017 09292.7 0.50 ug/kg1
Benzo(g,h,i)perylene ND 01/24/2017 09292.7 0.65 ug/kg1
Benzo(k)fluoranthene ND 01/24/2017 09292.7 0.48 ug/kg1
bis (2-Chloro-1-methylethyl) ether ND 01/24/2017 0929131.3 ug/kg1
bis(2-Chloroethoxy)methane ND 01/24/2017 0929130.70 ug/kg1
bis(2-Chloroethyl)ether ND 01/24/2017 0929131.1 ug/kg1
bis(2-Ethylhexyl)phthalate 20 01/24/2017 0929130.45 ug/kg1
Butyl benzyl phthalate ND 01/24/2017 0929130.69 ug/kg1
Caprolactam 9.0 01/24/2017 0929J132.4 ug/kg1
Carbazole ND 01/24/2017 0929130.84 ug/kg1
Chrysene ND 01/24/2017 09292.7 0.45 ug/kg1
Di-n-butyl phthalate ND 01/24/2017 0929132.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 76 of 87
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Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-001
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Di-n-octylphthalate ND 01/24/2017 0929130.24 ug/kg1
Dibenzo(a,h)anthracene ND 01/24/2017 09292.7 0.51 ug/kg1
Dibenzofuran ND 01/24/2017 0929131.0 ug/kg1
Diethylphthalate ND 01/24/2017 0929130.80 ug/kg1
Dimethyl phthalate ND 01/24/2017 0929137.4 ug/kg1
Fluoranthene ND 01/24/2017 09292.7 0.42 ug/kg1
Fluorene ND 01/24/2017 09292.7 0.57 ug/kg1
Hexachlorobenzene ND 01/24/2017 0929130.98 ug/kg1
Hexachlorobutadiene ND 01/24/2017 0929131.7 ug/kg1
Hexachlorocyclopentadiene ND 01/24/2017 0929671.3 ug/kg1
Hexachloroethane ND 01/24/2017 0929131.1 ug/kg1
Indeno(1,2,3-c,d)pyrene ND 01/24/2017 09292.7 1.0 ug/kg1
Isophorone ND 01/24/2017 0929131.2 ug/kg1
N-Nitrosodi-n-propylamine ND 01/24/2017 0929131.1 ug/kg1
N-Nitrosodiphenylamine (Diphenylamine)ND 01/24/2017 0929131.0 ug/kg1
Naphthalene ND 01/24/2017 09292.7 0.97 ug/kg1
Nitrobenzene ND 01/24/2017 0929131.6 ug/kg1
Pentachlorophenol ND 01/24/2017 0929675.3 ug/kg1
Phenanthrene ND 01/24/2017 09292.7 0.72 ug/kg1
Phenol ND 01/24/2017 0929131.2 ug/kg1
Pyrene ND 01/24/2017 09292.7 0.50 ug/kg1
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 69 30-117
2-Fluorobiphenyl 68 33-102
2-Fluorophenol 76 35-115
Nitrobenzene-d5 66 22-109
Phenol-d5 85 33-122
Terphenyl-d14 74 41-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 77 of 87
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Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-002
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
1,1'-Biphenyl 82 01/24/2017 09536213045-1281
2,4,5-Trichlorophenol 90 01/24/2017 09536813032-1051
2,4,6-Trichlorophenol 88 01/24/2017 09536613031-1021
2,4-Dichlorophenol 88 01/24/2017 09536613030-961
2,4-Dimethylphenol 100 01/24/2017 09537613030-1301
2,4-Dinitrophenol 120 01/24/2017 09534527032-1151
2,4-Dinitrotoluene 90 01/24/2017 09536813040-1301
2,6-Dinitrotoluene 91 01/24/2017 09536813046-1181
2-Chloronaphthalene 83 01/24/2017 09536213037-1061
2-Chlorophenol 91 01/24/2017 09536813044-1221
2-Methylnaphthalene 86 01/24/2017 09536513010-1071
2-Methylphenol 100 01/24/2017 09537713033-1031
2-Nitroaniline 95 01/24/2017 09537213046-1281
2-Nitrophenol 88 01/24/2017 09536613033-1141
3+4-Methylphenol 100 01/24/2017 09537713018-1211
3,3'-Dichlorobenzidine 71 01/24/2017 09535413039-1081
3-Nitroaniline 62 01/24/2017 09534713030-1301
4,6-Dinitro-2-methylphenol 78 01/24/2017 09535813053-1501
4-Bromophenyl phenyl ether 87 01/24/2017 09536613030-1301
4-Chloro-3-methyl phenol 97 01/24/2017 09537313048-1201
4-Chloroaniline 54 01/24/2017 09534013031-1271
4-Chlorophenyl phenyl ether 86 01/24/2017 09536413032-1071
4-Nitroaniline 88 01/24/2017 09536613051-1291
4-Nitrophenol 140 01/24/2017 09535427027-1381
Acenaphthene 85 01/24/2017 09536413012-1111
Acenaphthylene 89 01/24/2017 09536713018-901
Acetophenone 90 01/24/2017 09536713030-1301
Anthracene 92 01/24/2017 09536913016-1221
Atrazine 89 01/24/2017 09536713030-1301
Benzaldehyde 60 01/24/2017 09534513030-1301
Benzo(a)anthracene 95 01/24/2017 09537213040-1211
Benzo(a)pyrene 99 01/24/2017 09537413036-1141
Benzo(b)fluoranthene 98 01/24/2017 09537413038-1231
Benzo(g,h,i)perylene 100 01/24/2017 09537713043-1201
Benzo(k)fluoranthene 96 01/24/2017 09537213040-1261
bis (2-Chloro-1-methylethyl) ether 88 01/24/2017 09536613041-1131
bis(2-Chloroethoxy)methane 87 01/24/2017 09536613038-1151
bis(2-Chloroethyl)ether 89 01/24/2017 09536713046-1221
bis(2-Ethylhexyl)phthalate 120 01/24/2017 09539013033-1231
Butyl benzyl phthalate 100 01/24/2017 09537913048-1241
Caprolactam 110 01/24/2017 09538113040-1171
Carbazole 110 01/24/2017 09538013047-1251
Chrysene 95 01/24/2017 09537113041-1241
Di-n-butyl phthalate 100 01/24/2017 09537613035-1081
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 78 of 87
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Shealy Environmental Services, Inc.

Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ32300-002
32300 3546
01/23/2017 1403Analytical Method:8270D
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Di-n-octylphthalate 100 01/24/2017 09537513049-1181
Dibenzo(a,h)anthracene 88 01/24/2017 09536613038-1251
Dibenzofuran 93 01/24/2017 09537013045-1281
Diethylphthalate 95 01/24/2017 09537213030-1301
Dimethyl phthalate 95 01/24/2017 09537113024-1271
Fluoranthene 94 01/24/2017 09537113026-1331
Fluorene 90 01/24/2017 09536813019-1081
Hexachlorobenzene 85 01/24/2017 09536413010-1251
Hexachlorobutadiene 74 01/24/2017 09535513047-1161
Hexachlorocyclopentadiene 360 01/24/2017 09535567048-1271
Hexachloroethane 68 01/24/2017 09535113018-1541
Indeno(1,2,3-c,d)pyrene 99 01/24/2017 09537513042-1231
Isophorone 90 01/24/2017 09536713030-1301
N-Nitrosodi-n-propylamine 100 01/24/2017 09537613045-1121
N-Nitrosodiphenylamine (Diphenylamine)95 01/24/2017 09537113049-1231
Naphthalene 85 01/24/2017 09536413010-1121
Nitrobenzene 81 01/24/2017 09536113049-1421
Pentachlorophenol 180 01/24/2017 09536627036-1081
Phenanthrene 92 01/24/2017 09536913016-1231
Phenol 97 01/24/2017 09537313039-1081
Pyrene 97 01/24/2017 09537313034-1211
Surrogate Q % Rec Acceptance
Limit
2,4,6-Tribromophenol 63 30-117
2-Fluorobiphenyl 57 33-102
2-Fluorophenol 66 35-115
Nitrobenzene-d5 59 22-109
Phenol-d5 72 33-122
Terphenyl-d14 64 41-120
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 79 of 87
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Shealy Environmental Services, Inc.

RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31799-001
31799 3005A
01/18/2017 917Analytical Method:6010C
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Arsenic ND 01/19/2017 21420.015 0.0022 mg/L1
Barium ND 01/19/2017 21420.025 0.0019 mg/L1
Cadmium ND 01/19/2017 21420.0050 0.00054 mg/L1
Chromium ND 01/19/2017 21420.010 0.00072 mg/L1
Lead ND 01/19/2017 21420.010 0.0047 mg/L1
Selenium ND 01/19/2017 21420.020 0.0085 mg/L1
Silver ND 01/19/2017 21420.010 0.0021 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 80 of 87
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RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31799-002
31799 3005A
01/18/2017 917Analytical Method:6010C
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Arsenic 0.42 01/19/2017 21461060.40 80-1201
Barium 2.1 01/19/2017 21461042.0 80-1201
Cadmium 0.43 01/19/2017 21461070.40 80-1201
Chromium 2.1 01/19/2017 21461072.0 80-1201
Lead 0.42 01/19/2017 21461060.40 80-1201
Selenium 0.43 01/19/2017 21461070.40 80-1201
Silver 0.41 01/19/2017 21461020.40 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 81 of 87
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RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31801-001
31801 3050B
01/18/2017 949Analytical Method:6010C
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Arsenic ND 01/20/2017 20410.75 0.23 mg/kg1
Barium ND 01/20/2017 20411.3 0.14 mg/kg1
Cadmium ND 01/20/2017 20410.25 0.025 mg/kg1
Chromium ND 01/20/2017 20410.50 0.072 mg/kg1
Lead ND 01/20/2017 20410.50 0.22 mg/kg1
Selenium ND 01/20/2017 20411.0 0.41 mg/kg1
Silver ND 01/20/2017 20410.50 0.079 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 82 of 87
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Shealy Environmental Services, Inc.

RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31801-002
31801 3050B
01/18/2017 949Analytical Method:6010C
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Arsenic 240 01/20/2017 20469625080-1201
Barium 470 01/20/2017 20469450080-1201
Cadmium 50 01/20/2017 2046995080-1201
Chromium 250 01/20/2017 204610225080-1201
Lead 240 01/20/2017 20469625080-1201
Selenium 46 01/20/2017 2046915080-1201
Silver 46 01/20/2017 2046935080-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 83 of 87
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RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31784-001
31784 7471B
01/17/2017 2128Analytical Method:7471B
Matrix:Solid
Parameter Result Q PQL MDL Units Analysis DateDil
Mercury ND 01/18/2017 18340.083 0.0063 mg/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 84 of 87
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Shealy Environmental Services, Inc.

RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31784-002
31784 7471B
01/17/2017 2128Analytical Method:7471B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
Mercury 0.84 01/18/2017 18361010.83 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 85 of 87
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RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:SQ31803-001
31803 7470A
01/18/2017 1222Analytical Method:7470A
Matrix:Aqueous
Parameter Result Q PQL MDL Units Analysis DateDil
Mercury ND 01/18/2017 16290.00010 0.000028 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 86 of 87
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Shealy Environmental Services, Inc.

RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:SQ31803-002
31803 7470A
01/18/2017 1222Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Mercury 0.0020 01/18/2017 16311020.0020 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the MDL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 87 of 87
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Chain of Custody
and
Miscellaneous Documents
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Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

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Shealy Environmental Services, Inc.

Page 1 of 2
East 7th Street Storage
Brownfield Project No:20074-16-060
March 9, 2017
SUMMIT Project No: 3586.11
CAS SVOC Analyte
PSRG-
Industrial
Protection
of GW Result RL Result RL Result RL Result RL
83-32-9 Acenaphthene 9.00E+03 8.40E+00 0.0036 0.003 BRL 0.003 BRL 0.003 BRL 0.003
208-96-8 Acenaphthylene NA 2.10E+01 0.01 0.003 BRL 0.003 0.0012 J 0.003 BRL 0.003
98-86-2 Acetophenone 2.52E+03 3.50E+00 0.0043 J 0.016 BRL 0.016 BRL 0.016 BRL 0.015
120-12-7 Anthracene 4.60E+04 6.60E+02 0.022 0.003 BRL 0.003 0.0011 J 0.003 0.0011 J 0.003
100-52-7 Benzaldehyde 8.20E+02 3.00E+00 BRL 0.003 BRL 0.003 BRL 0.003 0.004 J 0.015
56-55-3 Benzo(a)anthracene 2.90E+00 1.80E-01 0.084 0.003 BRL 0.003 0.0046 0.003 0.0056 0.003
50-32-8 Benzo(a)pyrene 2.90E-01 5.90E-02 0.085 0.003 BRL 0.003 0.0048 0.003 0.0064 0.003
205-99-2 Benzo(b)fluoranthene 2.90E+00 6.00E-01 0.11 0.003 BRL 0.003 0.0083 0.003 0.01 0.003
191-24-2 Benzo(g,h,i)perylene NA 7.80E+03 0.032 0.003 BRL 0.003 0.0034 0.003 0.003 J 0.003
204-08-9 Benzo(k)fluoranthene 2.90E+01 5.90E+00 0.047 0.003 BRL 0.003 0.0023 J 0.003 0.0031 0.003
92-52-4 1,1'-Biphenyl 4.00E+01 4.30E+01 BRL 0.016 BRL 0.016 BRL 0.016 BRL 0.015
86-74-8 Carbazole NA 3.70E-01 0.014 J 0.016 BRL 0.016 BRL 0.016 BRL 0.015
218-01-9 Chrysene 2.90E+02 1.80E+01 0.083 0.003 BRL 0.003 0.0056 0.003 0.0071 0.003
132-64-9 Dibenzofuran 2.00E+02 5.20E+00 0.011 J 0.016 BRL 0.016 BRL 0.016 BRL 0.015
117-81-7 bis(2-Ethylhexyl)phthalate 1.60E+02 7.20E+00 BRL 0.016 BRL 0.016 BRL 0.016 BRL 0.015
206-44-0 Fluoranthene 6.00E+03 3.30E+02 0.17 0.003 BRL 0.003 0.0067 0.003 0.0097 0.003
86-73-7 Fluorene 6.00E+03 5.60E+01 0.0048 0.003 BRL 0.003 BRL 0.003 BRL 0.003
193-39-5 lndeno(1,2,3-c,d)pyrene 2.90E+00 2.00E+00 0.033 0.003 BRL 0.003 0.0026 J 0.003 0.0026 J 0.003
91-57-6 2-Methylnaphthalene 6.00E+02 1.60E+00 0.017 0.003 BRL 0.003 0.017 0.003 0.0073 0.003
91-20-3 Naphthalene 1.70E+01 2.10E-01 0.021 0.003 BRL 0.003 0.013 0.003 0.0053 0.003
85-01-8 Phenanthrene NA 6.80E+01 0.095 0.003 BRL 0.003 0.0099 0.003 0.0088 0.003
129-00-0 Pyrene 4.60E+03 2.20E+02 0.14 0.033 BRL 0.003 0.0062 0.003 0.0087 0.003
CAS RCRA Metals
PSRG-
Industrial
Protection
of GW Result RL Result RL Result RL Result RL
7440-38-2 Arsenic 3.00E+00 5.80E+00 2.2 1.3 1.3 J 2.7 2.8 J 3.9 2.4 J 3.0
7440-39-3 Barium 4.40E+04 5.80E+02 71 2.3 27 4.6 93 6.7 37 5.1
7440-43-9 Cadmium 1.96E+02 3.00E+00 0.053 J 0.44 BRL 0.89 BRL 1.3 BRL 0.98
7440-47-3 Chromium NA NA 46 0.89 0.96 1.8 61 2.6 75 2.0
7439-92-1 Lead 8.00E+02 2.70E+02 20 0.89 BRL 1.8 16 2.6 8.6 2.0
7439-97-6 Mercury 3.13E+00 1.00E+00 0.08 J 0.091 BRL 0.084 0.56 J 0.094 0.051 J 0.09
BRL = Below Reporting Limit J = Estimated Concentration RL = Lab Reporting Limit
BOLD = Concentration Above Reference Values
Jan. 16, 2017
0-2' bgs
SB-1-SB
4-6' bgs
Jan. 16, 2017 Jan. 16, 2017 Jan. 16, 2017
All Values in mg/kg
Table 1A: Soil Sample Detection Summary Table
SB-2-SS
0-2' bgs
SB-3-SS
0-2' bgs
NCDEQ Reference Values
SB-1-SS
Page 2 of 2
East 7th Street Storage
Brownfield Project No:20074-16-060
March 9, 2017
SUMMIT Project No: 3586.11
CAS SVOC Analyte
PSRG-
Industrial
Protection
of GW Result RL Result RL Result RL Result RL
83-32-9 Acenaphthene 9.00E+03 8.40E+00 BRL 0.003 0.19 0.003 BRL 0.003 BRL 0.003
208-96-8 Acenaphthylene NA 2.10E+01 BRL 0.003 BRL 0.003 BRL 0.003 0.0084 0.003
98-86-2 Acetophenone 2.52E+03 3.50E+00 BRL 0.016 BRL 0.015 BRL 0.015 BRL 0.015
120-12-7 Anthracene 4.60E+04 6.60E+02 BRL 0.003 0.27 0.003 BRL 0.003 0.012 0.003
100-52-7 Benzaldehyde 8.20E+02 3.00E+00 0.0053 J 0.016 BRL 0.015 BRL 0.015 0.0056 J 0.016
56-55-3 Benzo(a)anthracene 2.90E+00 1.80E-01 0.0041 0.003 0.82 0.003 BRL 0.003 0.1 0.003
50-32-8 Benzo(a)pyrene 2.90E-01 5.90E-02 0.0035 0.003 0.76 0.003 BRL 0.003 0.093 0.003
205-99-2 Benzo(b)fluoranthene 2.90E+00 6.00E-01 0.0063 0.003 1.1 0.003 BRL 0.003 0.18 0.003
191-24-2 Benzo(g,h,i)perylene NA 7.80E+03 0.0019 0.003 0.14 0.003 BRL 0.003 0.017 0.003
204-08-9 Benzo(k)fluoranthene 2.90E+01 5.90E+00 BRL 0.003 0.34 0.003 BRL 0.003 0.06 0.003
92-52-4 1,1'-Biphenyl 4.00E+01 4.30E+01 BRL 0.016 0.0091 J 0.015 BRL 0.015 BRL 0.015
86-74-8 Carbazole NA 3.70E-01 BRL 0.016 0.16 0.015 BRL 0.015 BRL 0.015
218-01-9 Chrysene 2.90E+02 1.80E+01 0.0033 0.003 0.8 0.003 BRL 0.003 0.094 0.003
132-64-9 Dibenzofuran 2.00E+02 5.20E+00 BRL 0.016 0.081 0.015 BRL 0.015 BRL 0.015
117-81-7 bis(2-Ethylhexyl)phthalate 1.60E+02 7.20E+00 BRL 0.016 2.0 0.015 BRL 0.015 0.004 BJ 0.015
206-44-0 Fluoranthene 6.00E+03 3.30E+02 0.0045 0.003 0.14 0.003 BRL 0.003 0.17 0.003
86-73-7 Fluorene 6.00E+03 5.60E+01 BRL 0.003 BRL 0.003 BRL 0.003 0.0016 J 0.003
193-39-5 lndeno(1,2,3-c,d)pyrene 2.90E+00 2.00E+00 0.0016 J 0.003 0.16 0.003 BRL 0.003 0.021 0.003
91-57-6 2-Methylnaphthalene 6.00E+02 1.60E+00 0.0044 0.003 0.033 0.003 0.0022 J 0.003 0.011 0.003
91-20-3 Naphthalene 1.70E+01 2.10E-01 0.0031 J 0.003 0.071 0.003 0.002 J 0.003 0.0098 0.003
85-01-8 Phenanthrene NA 6.80E+01 0.0043 0.003 1.7 0.003 BRL 0.003 0.041 0.003
129-00-0 Pyrene 4.60E+03 2.20E+02 0.0041 0.033 1.5 0.003 BRL 0.003 0.14 0.003
CAS RCRA Metals
PSRG-
Industrial
Protection
of GW Result RL Result RL Result RL Result RL
7440-38-2 Arsenic 3.00E+00 5.80E+00 2.8 J 4.0 1.3 0.76 0.97 0.74 2.6 0.99
7440-39-3 Barium 4.40E+04 5.80E+02 40 7.0 36 1.3 27 1.3 160 1.7
7440-43-9 Cadmium 1.96E+02 3.00E+00 BRL 1.3 BRL 0.25 BRL 0.25 0.23 J 0.33
7440-47-3 Chromium NA NA 93 2.7 6.8 0.51 1.3 0.5 25 0.66
7439-92-1 Lead 8.00E+02 2.70E+02 14 2.7 6.4 0.51 2.0 0.5 130 0.66
7439-97-6 Mercury 3.13E+00 1.00E+00 0.24 0.1 0.19 J 0.091 BRL 0.097 0.18 0.084
BRL = Below Reporting Limit J = Estimated Concentration RL = Lab Reporting LimitBOLD = Concentration Above Reference Values
Jan. 16, 2017 Jan. 16, 2017 Jan. 16, 2017 Jan. 16, 2017
Table 1A: Soil Sample Detection Summary Table
NCDEQ Reference Values
SB-3-DUP SB-4-SS SB-5-SB BG-1
All Values in mg/kg 0-2' bgs 0-2' bgs 4-6' bgs 0-2' bgs
1
Spriggle, Jill
From:Jeff Crump <[e-mail]>
Sent:Wednesday, January 24, 2018 3:57 PM
To:Spriggle, Jill; Marston, John
Subject:RE: East 7th st
Attachments:Agent Agreement Signed Siteworks 7th Street.pdf
Please see attached signed agreement. We’ll probably have someone from SW stop by and pickup the manifest once
printed.
Let me know if you need anything else.
Thanks,
From:Spriggle, Jill [mailto:[e-mail]]
Sent:Wednesday, January 24, 2018 3:36 PM
To:Marston, John <[e-mail]>; Jeff Crump <[e-mail]>
Subject:FW: East 7th st
The profile has been approved. I need the service agreement signed/returned so that I can finish
the data entry.
Thanks,
Jill Spriggle
Sales Coordinator - Special Waste
1220 Commerce St SW, Suite A
Conover, NC 28613
e [e-mail]
o 828.695.2051
f 828.464.6922 w www.RepublicServices.com
From:Marston, John
Sent:Monday, January 22, 2018 12:29 PM
To:Jeff Crump ([e-mail])
Cc:Spriggle, Jill
Subject:East 7th st
Jeff
2
I think this is what we had discussed. Please sign these and return them while we wait for the
approval. Jill have you seen anything on this yet. I think it was sent in when you were snowed
in?
John Marston Manufacturing Environmental Services Executive
5105 Morehead Rd Concord, NC 28027
e [e-mail]
o 704 262 6003 c 704 622 1769
f 704 782 2177 w republicservices.com
0937

Terms and Conditions of Agent Special Waste Service Agreement
BROKER: ________________ COMPANY: ________________ May 2009
5. The Agreement. This agreement of the parties (“Agreement”) for the disposal of Special Waste
shall consist of this Agreement, riders to the Agreement (if any) and any Application, permit and
approval that may be applicable to such Waste.

6. Waste Accepted at Facility. Agent represents, warrants and covenants that the Waste delivered
to Company at its Facility hereunder will be Acceptable Waste and will not contain any
unacceptable quantity of hazardous materials or substances, radioactive materials or
substances, or toxic waste or substances, as defined by applicable federal, state, local or
provincial laws or regulations. Any Waste which does not meet these requirements shall
hereinafter be referred to as “Unacceptable Waste”. The Agent shall in all matters relating to the
collection, transportation and disposal of the Waste hereunder, comply with all applicable
federal, state and local laws, regulations, rules and orders regarding the same. The word
“Facility” shall mean any landfill, transfer station or other location used to transfer, process or
otherwise dispose of such Waste.

7. Special Waste. Agent represents, warrants and covenants that the Waste delivered to Company
hereunder (i) will not contain any Special Waste that is not specifically described on any
Application which is attached hereto and which is subsequently approved by the Company, (ii)
will meet the material description as set forth in any Application and otherwise in all significant
respects and (iii) will not contain Unacceptable Waste. The parties may incorporate additional
Special Waste as part of this Agreement if prior to delivery of such Waste to Company, Agent
has provided an Application for such Waste and Company has approved disposal of such Waste
within the limitations and conditions contained in Company’s written notice of approval of Special
Waste. Title to acceptable waste shall transfer to Company upon final acceptance of such
waste. At no time shall Company take title to unacceptable waste.

8. Rights of Refusal/Rejection. The Agent shall inspect all Waste at the place(s) of collection and
shall remove any and all Unacceptable Waste. Company has the right to refuse, or to reject
after acceptance, any load(s) of Waste(s) delivered to its Facility including if the Company
believes the Agent has breached (or is breaching) its representations, warranties, covenants or
agreements hereunder, or any applicable federal, state or local laws, regulations, rules or orders,
even if only a portion of such Waste load is unacceptable. The Company shall have the right to
inspect all vehicles of Waste haulers, including the Agent’s vehicles, in order to determine
whether the Waste is Acceptable Waste or Unacceptable Waste pursuant to this Agreement and
all applicable federal, state and local laws, rules and regulations. The Company’s exercise, or
failure to exercise, its rights hereunder shall not operate to relieve the Agent of its responsibilities
or liability under this Agreement. The Agent shall be responsible for, and bear all reasonable
expenses and damages incurred by the Company, as a result of the Unacceptable Waste and in
the reloading and removal of Unacceptable Waste disposed in the Facility. The Company, may
also, in its sole discretion, require the Agent to promptly remove the Unacceptable Waste.

9. Limited License to Enter. This Agreement provides Agent with a license to enter the Facility for
the limited purpose of, and only to the extent necessary for, off-loading Acceptable Waste at the
Facility in the manner directed by Company. Except in an emergency, Agent’s personnel shall
not leave the immediate vicinity of their vehicle. After off-loading the Waste, Agent’s personnel
shall promptly leave the Facility. Under no circumstances shall Agent or its personnel engage in
any scavenging of Waste or other materials at the Facility. The Company reserves the right to
make and enforce reasonable rules and regulations concerning the operation of the Facility, the
conduct of the drivers and others on the Facility premises, quantities and sources of Waste, and
any other matters necessary or desirable for the safe, legal and efficient operation of the Facility
including, but not limited to, speed limits on haul roads imposed by the Company, and the
wearing of hard hats and other personal protection equipment by all individuals allowed on the
Facility premises. Agent agrees to conform to such rules and regulations as they may be
established and amended from time to time. Company may refuse to accept Waste from and
shall deny an entrance license to, any of Agent’s personnel whom Company believes is under
the influence of alcohol or other chemical substances. Agent shall be solely responsible for its
employees and subcontractors performing their obligations in a safe manner when at the facility
of Company.

10. Charges and Payment. Payment shall be made by Agent within thirty (30) days after receipt of
invoice from Company. In the event that any amount is overdue, the Company may terminate
this Agreement. Agent agrees to pay a finance charge equal to the maximum interest rate
permitted by law. Agent shall be liable for all taxes, fees, or other charges imposed upon the
disposal of the Waste by federal, state, local or provincial laws and regulations. Company, from
time to time, may modify its rates upon sixty (60) days written notice to Agent. Agent hereby
agrees that the Company’s right to receive payments under this Agreement is unconditional and
is not conditioned upon Agent first receiving payment from Generator or any other party.

11. Termination. Agent’s obligations, representations, warranties and covenants regarding the
Waste delivered and all indemnities shall survive termination of this Agreement. Should Agent
materially default in any of its obligations hereunder, then Company may immediately terminate
this Agreement and Agent shall be liable for all costs and damages incurred by the Company.

12. Driver’s Knowledge and Authority. Agent represents, warrants and covenants that its drivers
who deliver Waste to Company’s Facility have been advised by Agent of the Company’s
prohibition on deliveries of hazardous materials or substances, radioactive materials or
substances, or toxic waste or substances or any other Unacceptable Waste to the Facility, of
Company’s restrictions on deliveries of Special Waste to the Facility of the definitions of
“Hazardous Waste and Hazardous Substances” as provided by applicable federal, state and
local law, rules and regulations and “Special Waste” as provided herein, and of the terms of this
license to enter Company’s Facility.

13. Indemnification. Agent shall indemnify, defend and hold harmless the Company and its
subsidiaries, affiliates and parent corporations, as applicable and their respective officers,
directors, lenders, employees, subcontractors and agents from and against any and all claims,
suits, losses, liabilities, assessments, damages, fines, costs and expenses, including reasonable
attorneys fees arising under federal, state or local laws, regulations or ordinances, or relating to
the content of the Waste, or arising out of or in connection with any breach of this Agreement or
arising out of the negligent collection, transportation and disposal of Waste by Agent or Agent’s
employees, agents, subcontractors or representatives thereof. Agent shall also be responsible
for increased inspection, testing, study and analysis costs made necessary due to reasonable
concerns of the Company as to the content of the Waste following discovery of potentially
Unacceptable Waste. This indemnification and other obligations stated in this paragraph shall
survive the termination of this Agreement.

14. Insurance. Agent shall maintain in full force and effect throughout the term of this Agreement the
following types of insurance in at least the amounts specified below:

Coverages Minimum Amounts of Insurance
Worker’s Compensation Statutory
General Liability $500,000 combined single limit
Automobile Liability $500,000 combined single limit

All insurance will be by insurers authorized to do business in the state in which the Facility is located. Prior
to Agent being allowed on Facility premises, Agent shall provide the Company with certificates of
insurance or other satisfactory evidence that such insurance has been procured and is in force. Said
policies shall not thereafter be canceled, be permitted to expire, or be changed without thirty (30) days
advance written notice to the Company. Agent warrants that it will secure the above minimum amounts of
insurance from any transportation of the Waste to the Facility.

15. Failure to Perform. Neither party hereto shall be liable for its failure to perform hereunder due to
circumstances not its fault and beyond its reasonable control, including, but not limited to, strikes or other
labor disputes, riots, protests, civil disturbances or sabotage, changes in law, fires, floods, compliance with
government requests, explosions, accidents, weather, lack of required natural resources, or acts of God
affecting either party hereto. In the event of any of the circumstances provided for in the preceding
sentence, including, but not limited, to whether any federal, state or local court or governmental authority
takes any action which would (i) close or restrict operations at the Facility, (ii) limit the quantity or prohibit
the disposal of Waste at the Facility, or (iii) limit the ability of or prohibit Agent from delivering Waste to the
Facility, the Company shall have the right, at its option, to reduce, suspend or terminate Agent’s access to
the Facility immediately, without prior notice and without any additional liabilities between the parties, other
than Agent’s payment obligation hereunder. Neither Party is required hereunder to settle any labor dispute
against its own best judgment.

16. Other Termination. The occurrence of any of the following events shall also constitute an event of default
by the Agent and shall give the Company the right to immediately terminate this Agreement:

(A) A petition for reorganization or bankruptcy filed by or against the Agent.

(B) Failure by Agent to pay any amounts due to Company.

(C) Any breach by Agent of any of its obligations pursuant to the Agreement.

Agent shall be liable for and shall indemnify, defend and hold harmless Company from any losses, claims
expenses or damages incurred by the Company as a result of termination hereunder.

17. Assignment. Agent may not assign, transfer or otherwise vest in any other Company, entity or person, in
whole or in part, any of its rights or obligations under the Agreement without the prior written consent of the
Company, provided, however, that the Company may without any such prior written consent, assign its
rights and/or obligations under the Agreement to a subsidiary or affiliate corporation.

18. Right of Disposal. This Agreement does not grant any rights to dispose of Waste other than in accordance
herewith. The Company reserves the right to immediately terminate access to the Facility by Agent and
Agent’s personnel in the event of breach or violation by Agent of any of the terms of this Agreement, the
Company’s operating rules or payment policies or any applicable laws or regulations.

19. Continuing Compliance. The Agent has a continuing obligation to inform the Company of any new
information, or information not previously provided to the Company by Agent and/or Generator which may
affect the acceptability of the Waste by the Company. Further, the Agent shall comply with all Company
requests for evidence of Agent’s continuing compliance with the terms of the Agreement including but not
limited to the following: (i) providing new, updated Waste profiles on the Waste(s) offered for disposal or,
(ii) providing appropriate certification that the Waste being offered for disposal is accurately reflected by
the appropriate Application or, (iii) re-sample the Waste at Agent’s expense if reasonable cause exists as
to its acceptability under the terms of this Agreement or, (iv) allow the Company to re-sample the Waste at
Agent’s expense if reasonable cause exists as to its acceptability under the terms of this Agreement or (v)
all of the above.

20. Miscellaneous.

(A) This Agreement shall be governed by the laws of the State in which the Facility is located.

(B) No waiver of a breach of any of the obligations contained in the Agreement shall be construed to be a
waiver of any prior or succeeding breach of the same obligation or of any other obligation of this
Agreement.

(C) No modification, release, discharge or waiver of any provision or obligation hereof shall be of any
force, or effect, unless in writing signed by all parties to this Agreement.

(D) Agent shall treat as confidential and not disclose to others during or subsequent to the terms of this
Agreement, except as is necessary to perform this Agreement, or to comply with any applicable law
or regulation any information (including any technical information, experience or date) regarding the
Company’s plans, programs, plants, processes, products, costs, equipment or operations which may
come within the knowledge of the Agent or its employees in the performance of this Agreement,
without in each instance securing the prior written consent of the other Company.

(E) If any term, phrase, obligation or provision of this Agreement shall be held to be invalid, illegal or
unenforceable in any respect, this Agreement shall remain in effect and be construed without regard
to such term, phrase, obligation or provision.

(F) This Agreement constitutes the entire understanding between the parties, replacing and amending
any prior agreements between the parties, and shall be binding upon all parties hereto, their
successors, heirs, representatives and assigns. Any provision, term or condition in any
acknowledgement, purchase order or other response by Agent which is in addition to or different from
the provisions of this Agreement shall be deemed objected to by the Company and shall be of no
effect.

(G) Agent represents, warrants and covenants that it is and during the term of this Agreement, will
remain, in compliance with and will perform its obligations pursuant to all applicable laws and
regulations and shall indemnify, defend and hold harmless the Company from any breach thereof.

(H) It is the understanding and agreement of the parties that the Company is an independent contractor,
and is not an agent, nor an authorized representative of the Agent. It is the further understanding and
agreement of the parties that Agent is an authorized representative of Generator.

21. Notices. All notices herein provided for shall be considered as having been given upon being placed in the
mail, certified postage prepaid addressed to the Company or Agent at the address herein set forth in this
Agreement or to such other address as may be given to the other party in writing.

22. Liquidated Damages. In the event that this Agreement is terminated by the Agent in a manner not in
accordance with paragraph 4 hereof, or terminated due to a breach of this Agreement by the Agent, the
Agent shall pay, as liquidated damages, and not as a penalty, the greater of an amount equal to six (6)
months’ service charges or the Agent’s most recent monthly charge multiplied by six (6). The Agent shall
be given credit for any advance payments made hereunder, however, in computing the amount owed as
liquidated damages hereunder. The Agent acknowledges that this liquidated damages clause is
reasonable and is applicable to recover damages related to its investment in equipment, development of
landfills and hiring of employees undertaken by the Company to service its customers including the Agent.
This liquidated damages clause in no way relieves the Agent from its obligations and liability for other cost
or damages as set forth elsewhere in this Agreement.
0937
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina January 21, 2019

D:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\Redevelopment Report\1-21-19 Draft\Appendix E - Waste Manifests.rtf

APPENDIX E
REPUBLIC SOIL DISPOSAL MANIFESTS

Date Weight (ton)Manifest #Date Weight (ton)Manifest #
2/27/2018 17.02 6072 2/28/2018 16.88 6024
2/27/2018 17.81 6070 2/28/2018 12.64 6009
2/27/2018 9.92 6077 2/28/2018 14.45 6007
2/27/2018 17.41 6029 2/28/2018 15.84 6017
2/27/2018 17.15 6078 2/28/2018 15.77 6016
2/27/2018 15.66 6035 2/28/2018 18.2 6018
2/27/2018 21.14 6069 2/28/2018 12.94 6023
2/27/2018 14.39 6066 2/28/2018 15.22 6015
2/27/2018 17.94 6002 2/28/2018 17.91 6013
2/27/2018 14.95 6003 2/28/2018 15.23 6057
2/27/2018 9.72 6027 2/28/2018 14.23 6012
2/27/2018 14.67 6004 2/28/2018 11.27 6014
2/27/2018 21.71 6006 2/28/2018 15.77 6061
2/27/2018 12.25 6005 3/2/2018 14.16 6049
2/27/2018 17.12 6028 3/2/2018 14.68 6041
2/27/2018 18.64 6001 3/2/2018 19.52 6042
2/27/2018 14.65 6026 3/2/2018 15.77 6044
2/27/2018 14.83 6025 3/2/2018 14.64 6043
2/27/2018 14.47 6065 3/2/2018 18.97 6045
2/27/2018 20.82 6031 3/2/2018 14.75 6047
2/27/2018 18.06 6030 3/2/2018 14.91 6046
2/27/2018 16.35 6075 3/2/2018 13.31 6051
2/27/2018 13.57 6073 3/2/2018 17.6 6048
2/27/2018 9.6 6074 3/2/2018 13.57 6038
2/27/2018 17.73 6076 3/2/2018 15.73 6011
2/27/2018 17.78 6032 3/2/2018 16.87 6050
2/27/2018 20.13 6062 3/2/2018 18.48 6037
2/27/2018 18.14 6033 3/2/2018 15.02 6036
2/27/2018 22.93 6071 3/2/2018 14.94 6053
2/27/2018 15.03 6034 3/2/2018 14.06 6052
2/27/2018 18.42 6067 3/2/2018 17.54 6040
2/27/2018 15.65 6080 3/2/2018 14.75 6055
2/27/2018 18.05 6079 3/2/2018 21.84 6054
2/27/2018 14.66 6064 3/2/2018 14.48 6039
2/27/2018 17.66 6059 Total 1273.67
2/27/2018 24.69 6060
2/27/2018 13.74 6056
2/27/2018 16.78 6058
2/27/2018 18.08 6068
2/28/2018 13.95 6021
2/28/2018 14.56 6020
2/28/2018 16.07 6019
2/28/2018 15.11 6022
2/28/2018 15.99 6008
2/28/2018 16.73 6010
Manifest Summary
Redevelopment Summary Report – East 7th Street Storage SUMMIT Project No. 3586.11 Charlotte, North Carolina January 21, 2019

D:\Project Forms\Projects\3586.11 Charlotte Self-Storage - Phase II\Redevelopment Report\1-21-19 Draft\Appendix F - Import.rtf

APPENDIX F
IMPORT TICKETS