21048 Wepak UST Closure Report 2019.03.01

■
hart ; • hackman
SMARTER ENVIRONMENTAL SOLUTIONS
Via E-Mail
March 1, 2019
North Carolina Department of Environmental Quality
Division of Waste Management — Brownfields Program
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Attn: Ms. Caroline Goodwin
Re: UST Closure Report
Former Wepak Facility
332 W. Bland Street
Charlotte, North Carolina
Brownfields Project No. 21048-17-060
H&H Job No. MGN-002
Dear Ms. Goodwin:
1.0 Introduction
On behalf of 332 West Bland Street, LLC (Prospective Developer or PD), Hart and Hickman, PC
(H&H) is providing this report to document in -place closure activities associated with three
underground storage tanks (USTs) recently discovered at the former Wepak facility located at
332 W. Bland Street in Charlotte, Mecklenburg County, North Carolina (Site). Redevelopment
activities at the Site include adaptive reuse of the existing Site buildings with new paved parking
areas along W. Bland Street in the west -central and southeastern portions of the Site. A Site
location map is included as Figure 1 and the Site and surrounding area are shown in Figure 2.
The Site was entered into the North Carolina Department of Environmental Quality (DEQ)
Brownfields Program (Brownfield Project No. 21048-17-060) via a Letter of Eligibility dated
October 25, 2017. Prior to beginning redevelopment activities at the Site, an Environmental
Management Plan (EMP) dated May 14, 2018 received DEQ Brownfields approval on June 13,
2423 SnuthTryen Street, Suits 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.€am
704.5B5.0007 main 419.647A241 main

Ms. Caroline Goodwin
March 1, 2019
Page 2
2018. In accordance with the Brownfields approved EMP, H&H notified the Brownfields
Program following discovery of the USTs on January 17, 2019.
The tanks were discovered in the west -central parking area in close proximity to W. Bland Street
during subsurface stormwater utility installation activities (Figure 2). On January 30, 2019,
DEQ Brownfields provided approval to close the USTs in -place due to close proximity to the W.
Bland Street right-of-way and locations of new and existing utilities. As part of the UST closure
activities, soil samples were collected adjacent to each UST to evaluate the potential for impact.
Details associated with the UST closure activities and soil assessment activities area provided in
the following sections.
2.0 UST Closure and Soil Sampling Activities
2.1 In -Place Closure Activities
On February 5 through February 7, 2019, H&H contracted with EVO Corporation (EVO) to
conduct in -place closure activities for three USTs discovered during utility installations in the
west -central portion of the Site. Initial activities included removal of overburden soil to expose
portions of the tops of the tanks and opening portals into the tanks for removal of residual fluids.
Residual fluids were removed from each UST utilizing a vacuum truck and the tanks were then
rinsed clean with a pressure washer. The rinse water was also removed from the tanks using the
vacuum truck.
Based on dimensions of the tanks and the volume of fluids removed from each UST, estimated
tank volumes included one 15,000-gallon diesel UST, one 12,000-gallon gasoline UST, and one
2,000-gallon heating oil UST. A total of approximately 25,500 gallons of non -hazardous water
and 350 gallons of petroleum sludge were removed from the three USTs and transported off -Site
for disposal at the EVO facility located at 1703 Vargrave Street in Winston-Salem, NC. Waste
manifests for the fluid disposal are provided in Appendix A.
44
S:WAA-Master Projects\Magnus Capital Partners (MGN)\314 W. Bland Street\UST Closure In hart ` ! h i c k m a n
Place\Final To DEQ\UST Closure Report Wepak (BPN 21048-17-060) 20190301.doc W
SMARTER ENVIRONMENTAL SOLUTIONS

Ms. Caroline Goodwin
March 1, 2019
Page 3
Upon completion of fluid removal and rinsing activities, the tanks were tested for explosive
vapors utilizing a lower explosive limit (LEL) meter under the supervision of the Charlotte -
Mecklenburg Fire Marshall. Upon verification that combustible vapors were adequately
removed from the three USTs, each tank was filled with concrete.
2.2 Soil Sampling Activities
On February 15 and February 18, 2019, H&H contracted Mid -South Environmental (MSE), a
North Carolina licensed driller, to advance a total of 10 soil borings (UST-1 through UST-10)
around the perimeter of the UST basins. The soil borings were advanced utilizing a hand auger
and a track -mounted direct push technology (DPT) drill rig to depths ranging from
approximately 8 to 12 feet below ground surface (ft bgs). The base of each UST was estimated
to be approximately 8 ft bgs. Based on lithological observations by field personnel at the time of
sampling and previous assessment conducted at the Site, the water table is estimated to be
approximately 10 ft bgs in the vicinity of the UST basins. Locations of the soil boring are shown
on Figure 3.
Continuous soil samples were collected from each boring from the center of the hand auger
bucket and from acetate -lined macrocore sleeves. Soil samples were logged for lithologic
description and screened using visual and olfactory methods for obvious evidence of staining,
unusual odors, and for the presence of volatile organic vapors using a calibrated photo -ionization
detector (PID). Boring logs, including lithologic descriptions and field screening results, are
provided in Appendix B.
Soil samples for laboratory analysis were collected at depths of 6 to 8 ft bgs which is above the
water table and near the base of each tank. Soil samples selected for laboratory analysis were
collected directly into laboratory supplied sample containers, labeled with the sample
identification, date, time, and requested analyses and placed in a laboratory supplied cooler with
ice. The samples were delivered to Pace Analytical under standard chain of custody protocols
14
S:WAA-Master Projects\Magnus Capital Partners (MGN)\314 W. Bland Street\UST Closure In hart ` ! h i c k m a n
Place\Pinal To DEQ\UST Closure Report Wepak (BPN 21048-17-060) 20190301.doc W
SMARTER ENVIRONMENTAL SOLUTIONS

Ms. Caroline Goodwin
March 1, 2019
Page 4
for laboratory analysis of volatile organic compounds (VOCs) by EPA Method 8260B and semi-
VOCs (SVOCs) by EPA Method 8270D. In addition, two samples (UST-1 and UST-7) were
also analyzed for Resource Conservation and Recovery Act (RCRA) EPA Methods
602013/747113. The laboratory analytical report and chain of custody record are provided in
Appendix C.
2.3 Soil Sample Analytical Results
A tabular summary of soil sample analytical results is provided in Table 1. The laboratory
analytical results were compared to the DEQ Inactive Hazardous Sites Branch (IHSB)
Residential and Industrial/Commercial Preliminary Soil Remediation Goals (PSRGs) dated
February 2018. In addition to the PSRGs, metals results were compared to Site -specific and
published concentrations for naturally occurring metals in North Carolina soil.
Laboratory analytical results indicate that several petroleum -related compounds were detected at
concentrations above the laboratory method detection limits in soil samples UST-1 through
UST-4 collected adjacent to the eastern sides of the USTs. Results indicate that benzene (up to
2.06 milligrams per kilogram [mg/kg]), 1,2,4-trimethylbenzene (up to 227 mg/kg), 1,3,5-
trimethylbenzene (up to 73 mg/kg) and total xylenes (up to 278 mg/kg) were detected at
concentrations above the IHSB Residential PSRGs in soil samples UST-1 and/or UST-2. As
shown in Table 2, ethylbenzene (52.9 mg/kg) and naphthalene (47 mg/kg) were detected in the
UST-1 soil sample at concentrations exceeding the IHSB Industrial/Commercial PSRGs of 27
mg/kg and 18 mg/kg, respectively. No other compounds were detected above IHSB Industrial
PSRGs in soil samples collected in the vicinity USTs.
44
S:WAA-Master Projects\Magnus Capital Partners (MGN)\314 W. Bland Street\UST Closure In hart ` ! h i c k m a n
Place\Pinal To DEQ\UST Closure Report Wepak (BPN 21048-17-060) 20190301.doc W
SMARTER ENVIRONMENTAL SOLUTIONS

Ms. Caroline Goodwin
March 1, 2019
Page 5
4.0 Summary
H&H has completed in -place closure of three USTs discovered during utility installation
activities at the former Wepak facility located in Charlotte, North Carolina. Prior to
abandonment, approximately 25,500 gallons of non -hazardous water and 350 gallons of
petroleum sludge were removed the USTs. Following removal of residual fluids, the USTs were
washed clean and purged of combustible vapors under supervision of the Charlotte -Mecklenburg
Fire Marshall. The USTs were then closed in -place by filling with flowable concrete fill.
To evaluate the potential for impact, soil assessment activities were completed adjacent to each
UST. Soil assessment activities consisted of collection of ten (10) soil samples for laboratory
analysis. Laboratory analytical results indicate that the petroleum -related compounds
ethylbenzene and naphthalene were detected at concentrations above the IHSB
Industrial/Commercial PSRGs in soil sample UST-1 collected adjacent to the eastern side of the
USTs. No other compounds were detected above IHSB Industrial/Commercial PSRGs.
Based on the results of UST soil assessment activities, the Brownfields plat is being updated to
include the locations of the USTs and information associated with the UST-1 soil sample.
Should you have any questions or need additional information, please do not hesitate to call me
at [phone].
Very truly yours,
Hart & Hickman, PC
Ralph McGee, PG
Senior Project Geologist
Attachments
��SSS00I t7oI Ito#ot,'v
C A y o rPrr
NO'��i.��"`.
SEAL w
2419 y
4
SAAAA-Master ProjectsMagnus Capital Partners (MGN)\314 W. Bland Street\UST Closure In hart 0_ i � ickman
Place\Final To DEQ\UST Closure Report _Wepak (BPN 21048-17-060)_20190301.doe W
SMARTER ENVIRONMENTAL SOLUTIONS

Table 1
Summary of Soil Analytical Data
Former Wepak Facility
Charlotte, North Carolina
H&H Job No. MGN-002
Sample ID
UST-1
UST-2
UST-3
UST-4
UST-5
UST-6
UST-7
UST-8
UST-9
UST-10
Residential
2
PSRG
Industrial /
Commercial
PSRG2
Sample Date
2/15/2019
2/15/2019
2/15/2019
2/15/2019
2/15/2019
2/15/2019
2/18/2019
2/15/2019
2/18/2019
2/18/2019
Sample Depth (ft bgs)
6-8
6-8
6-8
6-8
6-8
6-8
6-8
6-8
6-8
6-8
VOCs (8260B)
Acetone
<12.5
<10.6
0.0142 J
0.0314 J
<0.125
<0.112
0.0263 J
<0.0995
0.0272 J
<0.119
12,000
140,000
Benzene
2.06
1.24
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0133
1.2
5.4
n-Butylbenzene
16.5
<0.528
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0102
780
12,000
sec-Butylbenzene
4.79
0.852
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0055 J
1,600
23,000
Ethylbenzene
52.9
8.37
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0138
6.1
27
Isopropyl benzene (Cumene)
9.77
1.60
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0060
410
2,100
p-Isopropyltoluene
20.5
3.34
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0084
NE
NE
Naphthalene
47.0
8.45
0.0016 J
<0.0066
<0.0062
0.0014 J
<0.0048
<0.0050
<0.0050
0.0186
4.1
18
n-Propylbenzene
27.7
3.53
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0090
780
5,100
Toluene
45.8
9.35
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
<0.0059
990
9,700
1,2,4-Trimethyl benzene
227
13.9
0.0087
0.0039 J
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0187
63
370
1,3,5-Trimethyl benzene
73
9.41
0.0025 J
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
0.0031 J
56
320
Xylene (Total)
278
38.2
<0.0102
<0.0132
<0.0125
<0.0112
<0.0096
<0.0099
<0.0101
<0.0119
120
530
m&p-Xylene
210
28.4
0.0041 J
<0.0132
<0.0125
<0.0112
<0.0096
<0.0099
<0.0101
0.0077 J
240
1,020
o-Xylene
68.0
9.83
<0.0051
<0.0066
<0.0062
<0.0056
<0.0048
<0.0050
<0.0050
<0.0059
140
590
SVOCs (8270D)
Site Specific
Fluorene
1.03 J
<0.405
1.05 J
<0.406
<0.388
<0.399
<0.409
<0.387
<0.416
<0.427
480
6,000
1-Methyl naphthalene
15.2
<0.405
7.47
<0.406
<0.388
<0.399
<0.409
<0.387
<0.416
<0.427
18
73
Background Metals in
Regional Background Metals
2-Methyl naphthalene
28.4
<0.405
12.7
<0.406
<0.388
<0.399
<0.409
<0.387
<0.416
<0.427
48
600
Soil
in Soil
Naphthalene
33.0
<0.405
7.42
<0.406
<0.388
<0.399
<0.409
<0.387
<0.416
<0.427
4.1
18
Phenanthrene
1.42 J
<0.405
1.20 J
<0.406
<0.388
<0.399
<0.409
<0.387
<0.416
<0.427
NE
NE
Range
Range
Mean
Metals (6020B/7471A)
Arsenic
0.704
NA
NA
NA
NA
NA
1.06
NA
NA
NA
0.68
3
1.2 - 1.4
1.0 - 18
4.8
Barium
68.8
NA
NA
NA
NA
NA
121
NA
NA
NA
3,100
47,000
26 - 34
50 - 1,000
356
Cadmium
<0.0957
NA
NA
NA
NA
NA
<0.0984
NA
NA
NA
14
200
<0.014 - 0.054
1.0 - 10
4.3
Chromium (total)
2.52
NA
NA
NA
NA
NA
18.4
NA
NA
NA
23,000*
350,000*
12 - 14
7.0 - 300
65
Lead
9.05
NA
NA
NA
NA
NA
6.55
NA
NA
400
800
4.2 - 26
ND - 50
16
Mercury
<0.00335
NA
NA
NA
NA
NA
0.00781 J
NA
NA
NA
2.3
9.7
0.054 - 0.11
0.03 - 0.52
0.121
Selenium
0.571 J
NA
NA
NA
NA
NA
0.830
NA
NA
NA
78
1,200
<0.060 - 0.47
<0.1 - 0.8
0.42
Silver
<0.185
NA
NA
NA
NA
NA
<0.191
NA
NA
NA
78
1,200
0.035 - 0.040
ND - 5.0
NS
Notes
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (February 2018).
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.
Concentrations are reported in milligrams per kilogram (mg/kg).
Compound concentrations are reported to the laboratory method detection limits.
Bold values exceed Residential PSRGs
Underlined values exceed Industrial/Commercial PSRG
*Based on resutls of previous Site soil assessment activities, total chromium concentrations represent trivalent chromium concentrations. As such, the trivalent chromium IHSB PSRGs are used for comparison.
Laboratory analytical methods are shown in parentheses.
VOCs = volatile organic compounds; SVOCs = semi -volatile organic compounds; ft bgs= feet below ground surface
NA = Not Analyzed; NE = Not Established
J = compound was detected above the laboratory method detection limit but, below the laboratory reporting limit resulting in an estimated concentration.
Table 1 (Page 1 off 1)
SAAAA-Master Projects\Magnus Capital Partners (MGN(\314 W. Bland Street\UST Closure In Place\Tables\UST In -Platy Closure Soil SamLples rm Hart & Hickman, C

■ � W o ,t �: � 149
•TY-; LR SITE
L ' 4 Ip' �h r :•�..,
s> ne
77
¢4 � •y �� '.'' � ii' ��'" u
�• .... � � `� ITT !r"�_�^ .. �.. .�� 1%.
V
1 1 t3 5 i 1. a prp gna t'
qb
45�—� _-f• J /r L� ,fee � [� . � ,:V, �
f thleh
■ + -t Par pVE 4 �4
l i •,
APPROXIMATE
N 0 2000 4000
SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA, 1991
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)

LEGEND
BROWNFIELDS PROPERTY
BOUNDARY
APPROXIMATE EXTENT OF
UNDERGROUND STORAGE TANKS
• SOIL BORING LOCATION
gr
r ' i�v' • ; 'Qa'
` , R SB
SB-6 • • •-9 •
\ NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG CO. GIS
SB-4 SB 1 2. SOIL SAMPLES COLLECTED BY H&H ON 2/15/19 AND 2/1819.
's6-zAN-
,,� e ,-` • _ .fir, {+*;
4e
` {
'�• ' jj7 is •� 4 l�k. !TITLE
r ems'
t
t - ti �►•.
t � `
• � • Irify
10* t
0
APPROXIMATE
0 50 100
SCALE IN FEET
SITE MAP
ECT FORMER WEPAK FACILITY
314 W. BLAND STREET
CHARLOTTE, NORTH CAROLINA
dart hiekma� 2923South Tryon
thCarolina28203te 0
1. Charlotte, North Carolina 28203
704-586-0007(p) 704-586 03;3(t
SMARTER ENVIRONMENTAL SOLUTIONS i.icense # C-1269 / ± 245 Geoloa,
ATE: 3-1-19 REVISION NO. 0
OB NO. MGN-002 FIGURE NO. 2

•
UST-7
UST-8
` `'UST-9
UST-6 • `
C' `• UST-10
•UST-5 • UST-1
UST
• UST-2
• v
UST-3
X
LEGEND
BROWNFIELDS PROPERTY
BOUNDARY
APPROXIMATE EXTENT OF
UNDERGROUND STORAGE TANKS
• SOIL BORING LOCATION
NOTES:
1. UNDERGROUND STORAGE TANKS CLOSED IN -PLACE ON
FEBRUARY 5 THROUGH FEBRUARY 7 2019.
2. SOIL SAMPLES COLLECTED BY H&H ON 2/15/19 AND 2/1819.
0
APPROXIMATE
0 20
SCALE IN FEET
SAMPLE LOCATION MAP
40
FORMER WEPAK FACILITY
332 W. BLAND STREET
CHARLOTTE, NORTH CAROLINA
• 2923 South Tryon Street -Suite 100
hart h i c k m a n Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(�
SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
DATE: 3-1-19 REVISION NO. 0
JOB NO. MGN-002 FIGURE NO. 3

Appendix A
Waste Manifests
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

AERXIC3
CORPORATION
1703 Migpve Street
Winston-Salem, NO 27107
ph 338-725-W44
fax [phone]
CERTIFICATE OF DISPOSAL
Evo Corporation does hereby certify that 25,500 gallons of non -hazardous
contaminated Water received on 2/5/2019, 2/6/2019 and 2/7/2019 from;
Generator: West BIand Street, LLC
Originating at: 314 and 332 West Bland St.
Charlotte, NC
EC Waste ID #: 021908
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environmental Quality.
Signature
Thomas W. Hammett
CEO
Evo Corporation

CORPORATION
1703 Vargrave. Street
Winston-Salem, NC 27107
ph 336-725-5844
fax [phone]
A
Evo Corporation does hereby certify that 350 gallons of product received on
2/6/2019 from:
Generator: West Bland Street, LLC
Originating at: 314 and 332 West Bland St.
Charlotte, NC
EC Waste ID 4: 021908
has been disposed of by Evo Corporation in a manner approved by the..North
Carolina Department of Environmental Quality.
Signature

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 81010
Generator: West Bland Street L Phone:
1 `1 " 32 West Bland. St
Site Addres .
City/State: �1 _UP NYC Contact:
Gross Weight (lbs):
Empty Weight (Ibs):
Net Weight (lbs):
Material: 8l e
Contaminant: Gasoline
Quantity Ss D Tons Drums Pails Sacs Yards EEJ ONS
Transporter:Evo Co ration
Truck #:
Phone: [phone]
Contact: Tony Dishg�jr
As the transporter, I certify that the materials described above being shipped under this nonhazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
In commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Slgnature: �., L _L
EVO CORPORATION
1703 Vargrave Street
Winston-Salem, NC 27107
Date: A. g7'
Evo Project #: 02IL909
Phone: [phone]
Contact: Tony Disher _
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment ang/or disposal in a TAaaeQhat has been authorized by the State of North Carolina.
Facility SignatureL 114 ,,J J Date:
White/Facility Canary/Invoice Goldenrod/Generator Pin
Evo Corporation, 2008
rr- nn-

EV® CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 11431
GENERATOR INFORMATION �
Generator:
Wiest bland Street LLC Phone: [phone]
� Site Address: ° 332 Nest Bland St
City/State: Charlotte NC Contact: Vishat Arora
MATERIAL DESCRIPTION 1 QUANTITY I WEIGHT
Gross Weight (lbs):
Empty Weight (lbs):
Net Weight (lbs):
Quantity 30�
Material: water'
Contaminant: Fue
Tons Drums Pails Sacs Yards Other:
TRANSPORTER INFORMATION
Transporter: EVO C' Orpor t n
Truck #:
Phone;, —
336-725-5844
Contact: Tony :dishier
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Siqnature:
Date:
FA ILITY INFORMATION
Bvo Corporation
1�0 �Trrae Street
Winston-Salem"
inston-Salem WC
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment agdlor disposal)q-a-p--1pNer that has been authorized by tl)e Stat6 of North Carolina.
Facilitv Siqnature:
Date:
Ev°o Corporation, 2008

City/State
EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Charlotte NC
Contact: Vishal Amara
MATERIAL DESCRIPTION 1 QUANTITY / WEIGHT ,
Gross Weight (lbs): Material:
Empty Weight (lbs):
Net Weight (Ibs):
Quantity
Contaminant: Diesel Fuel
Tons Drums Pails Sacs Yards Other:
TRANSPORTER INFORMATION
Transporter: :Evo Cp1poratio n. Phone: 336-- 5-5$44
Truck #: Contact: To-nv Tiit%hF-_r
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Si nature: Date:
FACILITY INFORMATION
Eva Project #:
Evo Corgoratioi
1703 Var rave Street Phone:
wiUston-Salem NC Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment agd4pdisppsal in ja manner that has been authorized by the Stale of North Carolina.
Facilitv Signature:
Date:
NTHI IT- 1.
Evo Corparit€on, 2008
ce
er

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 11435
GENERATOR INFORMATION
Generator:
West Bland St eet LLB Phone: [phone]
Site Address: Yg�! 332 West Blanc. St
City/State: challotINC Contact: DOW .,A.rora
Gross Weight (lbs):
Empty Weight (lbs):
Net Weight (lbs):
MATERIAL DESCRIPTION 1 QUANTITY i WEIGHT
Material: Water
Contaminant
Diem Fuel
Quantity s-J-00 Tons Drums Palls Sacs Yards Dthr:
TRANSPORTER INFORMATION
Transporter: Evo.Corpo ration Phone: [phone]
Truck #: 26 Contact: Tony Dis$er
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature: - Date:
FACILITY INFORMATION
EV Coo ration
natoit-.Salem Bid
Evo Project #: 021908
Phone:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment anJ/or disposgj in a resat has been authorized by the, Statia of North Carolina.
Fac
Date: 0,
wrine/ramiry vanarynnvoice
Evo Corporation, 2008

EVO CORPORATION
1703 Vargrarre Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 11430
GENERATOR INFORMATION
Generator: West Bland Street LLC Phone:
art 332 meat Bland St
Site Address: 4J
City/State:
Grass Weight (lbs):
Empty Weight (lbs):
Net Weight (lbs):
Charlotte NC
Contact: Visha1 Arora
MATERIAL DESCRIPTION 1 QUANTITY !WEIGHT
Material: Water
Contaminant: Diem Fuel
Quantity Tons Drums Pails Sacs Yards 00the
TRANSPORTER INFORMATION
Transporter: Evo Corporation Phone:
Truck #: 2 c)� Contact: Ton D►bher
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature: Date: Z/5-
FACILITY INFORMATION
Evo Corporation
1703 Vaurgrave Street
Winston-Salem NC
Evo Project #: 02190
Phone:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment a9ld/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Sictnatu
Date:
Evo Corporwinn, 2009
Pink/Carrier

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 11434
GENERATOR INFORMATION
West Bland Street.L C
Generator: Phone:
Site Address: ,Ad 332 West, Bla n.d.St
City/State: Char Otte NC Contact: YU
MATERIAL. DESCRIPTION 1 QUANTITY 1 WEIGHT
Gross Weight (Ibs):
Empty Weight (lbs):
Net Weight (lbs):
Quantity©ram
Material:
Contaminant:
'water
Diesel Fuel
Tons Drums Pails Sacs Yards
TRANSPORTER INFORMATION
Transporter:
Eyo CoiT ortt o
Phone:
336-725-58
Truck #:
14a.-2-
Contact:
Tonv Disher
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Si nature: Date: ,� - G - ! 91
FACILITY INFORMATION
Eva Corporation
1703 Var rave. Street
Winston-Salem NC
Evo Project #:.__ -- 02190R
Phone:
Contact:
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facilitv Sianature:
Date:
nvo
Evn Corporation, 2008

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 11437
GENERATOR INFORMATION
West Bland Street LLC 64 6-790-5 3
Generator: Phone:
Site Address rlg, 332. West Bland St
City/State-
Gross Weight (lbs):
Empty Weight (Iles):
Net Weight (lbs):
Charlotte NC
Contact: Kkha . Axma,
MATERIAL DESCRIPTION / QUANTITY I WEIGHT
Material: Water
Contaminant: Diese: Fuel
Quantity--�j� Tons Drums Pails Sacs Yards Other C
TRANSPORTER INFORMATIDN
Transporter: Bvo Corporation Phone:
336-725-5844-
Truck #: _ 2G2 Contact: TjQny Diaber -
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Siqnature:
Date: Z/7/�
FACILITY INFORMATION I
Bvo Corporation
1703 �ia�rrvtrt
'Winston-Salem WC.
Evo Project #: 021909
Phone:
Contact:
1 certify that the carrier has delivered the materials described above to this facility,
material for treatment a d/or disposal in a manner that has been authorized by the Si
,;� -7
facility Siqnature: Date: c _/
and l hereby accept this
itwof North Carolina.
FY
Canary/Invoice
Cvo Corporation, 2009

EVO CORPORATION
1703 Vargrave Street, Winston-Salem, NC 27107
www.evocorp.net
NON -HAZARDOUS MATERIALS MANIFEST
Load # Manifest No. 11433
GENERATOR INFORMATION
West Bland Street L�
Generator: Phone:
Site Address: /Yqa= West Bland St
City/State: Charlotte NC Contact: - Vishal Arora
Gross Weight (lbs):
Empty Weight (Ibs):
Net Weight (Ibs):
MATERIAL DESCRIPTION 1 QUANTITY 1 WEIGHT
Material: �i
Contaminant: Biel fel
Quantity '350 Tons Drums Pails Sacs Yards �ther:
TRANSPORTER INFORMATION
Transporter: ,, //Evo Coateration
Truck #: �t 6
i '"
Contact:-i`IDny_plaher
As the transporter, I certify that the materials described above being shipped under this non -hazardous
materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport
in commerce under the applicable regulations governing transportation, and I hereby receive this material for
delivery to the facility designate.
Driver Signature: Date: 6—
F CILITY INFORMATION
E o Cor ►ration
170 V2rgraveS reet
Winston-Salem: KC
Evo Project #: 0210OR
Phone:
Contact:
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this
material for treatment anal/or dispolal in a manner that has been authorized by the State of North Carolina.
Facility Si nature: F Date: XIUIJV
White/Facility Canary/Invoice Pink/Carrier
Eva Corpomtion, 2008

Appendix B
Boring Logs
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

.
hart hickman
Client: Magnus Capital Partners
Project: MGN.002
BORING LOG
Boring No. SB-1
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 0211512019
Boring Depth (ft): 12.0
Drilling End Date: 02115/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
}
00
J
W
W
Z
O
(�
=
p
J
1-
ZW
d
Z
H
y
SOIL/ROCK VISUAL DESCRIPTION
n
N
E
a
W
a
O�
d
a
n
W
W
❑
2
J
Q
00O
N
E
H
L)
3
N
0
❑
m
�
❑
CJ
o
d
a
cn
m
a'
0 0
(0') Poorly graded GRAVEL with silt and sand (GP -GM); some medium sand
181.3
(1') SILT with sand (ML); trace clay, medium stiff, moist, orange and light brown gray
(2') Poorly graded SAND with silt (SP-SM); few clay, medium dense, moist,
reddish -gray, Angular gravel, trace brick fragments, strong odor
(4') SILT with sand (ML); very stiff, moist, gray, with angular gravel
602.3
(45) SILT (ML); some clay, medium stiff, moist, reddish -gray, strong odor
5
5
1,679
SB-1
(6'-8')
(8') Sandy SILT (ML); trace clay, medium stiff, moist, brown and tan, strong odor
1,768
(95) As Above: wet, some clay
10
1,465
10
(12') Boring terminated
15 15
NOTES: Hole precleared to 5.0' on 02/15/2019 using hand auger.
generated using GroundLogs.onhne

14
Client: Magnus Capital Partners
BORING LOG
hart hickman
Project: MGN.002
Boring No. SB-2
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/15/2019
Boring Depth (ft): 10.0
Drilling End Date: 02/15/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
L
....
�
O
Jp
LU
W
W
0F
E2
O2
d
H
a)
z
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
LU
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
d
J
0 0
(0') SILT (ML); little fine sand, some clay, stiff, moist, dark reddish -brown
7.2
(2') Sandy SILT (ML); trace fine gravel, little clay, very stiff, moist, red tan orange
4.4
(4') SILT (ML); trace clay, medium stiff, moist, orange tan
4.9
5
5
(6) Sandy SILT (ML); trace clay, medium stiff, moist, tan gray, strong odor
2,126
SB-2
(6'-8')
(8') SILT (ML); some clay, stiff, moist, gray and tan, manganese infill, strong odor
63.9
10
10
(10') Baring terminated
15 15
NOTES: Hole precleared to 5.0' on 02/15/2019 using hand auger.
generated using GroundLogs.onllne

14
Client: Magnus Capital Partners
BORING LOG
hart hickman
Project: MGN.002
Boring No. SB-3
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/15/2019
Boring Depth (ft): 10.0
Drilling End Date: 02/15/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
LU
Z
L
0F
....
V
�
O
Jp
W
W
E2
O2
d
H
a)
z
SOIL/ROCK VISUAL DESCRIPTION
n
E
LU
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
d
J
0 0
(0') SILT (ML); some clay, medium stiff, moist, orange and red
9.3
(2') As Above: pale orange
12.7
(4') SILT (ML); some fine sand, trace clay, stiff, moist, brown tan
9.6
5
5
(6) Sandy SILT (ML); trace clay, medium stiff, moist, brown white tan
10.3
SB-3
(6'-8')
77.1
10
10
(10') Baring terminated
15 15
NOTES: Hole precleared to 5.0' on 02/15/2019 using hand auger.
generated using GroundLogs.onllne

14
hart hickman
Client: Magnus Capital Partners
BORING LOG
Project: MGN.002
Boring No. SB-4
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/15/2019
Boring Depth (ft): 8.0
Drilling End Date: 02/15/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
L
....
�
O
Jp
LU
W
W
0F
E2
O2
d
H
a)
z
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
LU
2
J
Q
°gyp
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
d
J
0 0
(0') Sandy SILT (ML); few fine gravel, soft, moist, dark brown and black, with few
2.1
organics
(05) Sandy SILT (ML); some clay, soft, moist, orange and gray
(2') Sandy SILT (ML); some clay, soft, moist, orange and tan, with few clay peds
1.4
2.1
5
5
(6) SILT (ML); some clay, soft, moist, orange and tan with red mottling, with some
1.4
SB-4
(6'-8')
organics (roots)
(8') Boring terminated
10
10
15 15
NOTES: Hole precleared to 4.0' on 02/15/2019 using hand auger.
generated using GroundLogs.onlfne

14
Client: Magnus Capital Partners
BORING LOG
hart hickman
Project: MGN.002
Boring No. SB-5
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/15/2019
Boring Depth (ft): 8.0
Drilling End Date: 02/15/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
LU
Z
L
0F
....
V
�
O
Jp
W
W
O2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
LU
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
d
J
0 0
(0') Poorly graded SAND with silt (SP-SM); loose, moist, dark brown and black, with
0.7
some organics
(0.5') Sandy SILT (ML); some clay, soft, moist, brown and gray
(2') As Above: with white and black coloring
0.5
(4') Sandy SILT (ML); soft, moist, light tan and gray, with few red silty clay peds
0.4
5
5
(6) SILT (ML); few fine sand, some clay, stiff, moist, gray and orange and red
0.4
SB-5
(6'-8')
(8') Boring terminated
10
10
15 15
NOTES: Hole precleared to 5.0' on 02/15/2019 using hand auger.
generated using GroundLogs.onllne

14
Client: Magnus Capital Partners
BORING LOG
hart hickman
Project: MGN.002
Boring No. SB-6
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314+332 W. Bland Street, Charlotte, NC
Page: 1 of 1
Drilling Start Date: 02/15/2019
Boring Depth (ft): 8.0
Drilling End Date: 02/15/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
L
....
�
O
Jp
LU
W
W
0F
O2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
LU
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
d
J
0 0
(0') Sandy SILT (ML); few fine gravel, medium stiff, moist, tan and brown, few red stiff
2.3
silty clay peds
(2') Sandy SILT (ML); stiff, moist, brown, some silty clay peds
1.2
(4') SILT (ML); some clay, stiff, moist, gray brown red, with white mottling
1.4
5
5
(6) Sandy SILT (ML); little clay, stiff, moist, gray brown red, with white mottling
13.7
SB-6
(6'-8')
(8') Boring terminated
10
10
15 15
NOTES: Hole precleared to 5.0' on 02/15/2019 using hand auger.
generated using GroundLogs.onllne

.
hart hickman
Client: Magnus Capital Partners
Project: MGN.002
BORING LOG
Boring No. SB-7
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/18/2019
Boring Depth (ft): 8.0
Drilling End Date: 02/18/2019
Boring Diameter (in): 3.50
Drilling Company: Mid South Environmental
Sampling Method(s):
Drilling Method: Other
DTW During Drilling (ft):
Drilling Equipment: Hand Auger
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
L
....
O
Jp
Lu
W
W
0F
O2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
Lu
O
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
d
J
�
m
�
0 0
(0') Asphalt
16.7
(05) SILT (ML); some clay, medium stiff, moist, red brown with white mottling, fill
14.5
13.5
(3') As Above: trace roots
19.6
(4') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, brown and red,
5.9
fill
5
28.2
5
27.8
SB-7
(6'-8')
5.5
(8') Boring terminated
10
10
15 15
NOTES: Hole precleared to 8.0' on 02/18/2019 by Mid South Environmental using hand auger.
generated using GroundLogs.online

14
Client: Magnus Capital Partners
BORING LOG
hart hickman
Project: MGN.002
Boring No. SB-8
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/15/2019
Boring Depth (ft): 8.0
Drilling End Date: 02/15/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
L
....
�
O
Jp
LU
W
W
0F
O2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
LU
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
0
J
0 0
(0') Sandy SILT (ML); few fine gravel, some clay, medium stiff, moist, orange and
0.0
brown, with silty clay peds
(2') As Above: with trace gravel
0.0
(4') SILT (ML); little fine sand, some clay, medium stiff, moist, gray white brown
3.1
5
5
(6) Sandy SILT (ML); medium stiff, moist, gray brown
3.3
SB-8
(6'-8')
(8') Boring terminated
10
10
15 15
NOTES: Hole precleared to 5.0' on 02/15/2019 using hand auger.
generated using GroundLogs.onllne

14
Client: Magnus Capital Partners
BORING LOG
hart hickman
Project: MGN.002
Boring No. SB-9
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/18/2019
Boring Depth (ft): 8.0
Drilling End Date: 02/18/2019
Boring Diameter (in): 3.50
Drilling Company: Mid South Environmental
Sampling Method(s):
Drilling Method: Other
DTW During Drilling (ft):
Drilling Equipment: Hand Auger
DTW After Drilling (ft):
Driller:
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
L
....
O
Jp
w
W
W
�F
O2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
LU
O
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
d
J
0 0
(0') Asphalt
2.7
(0.5') SILT (ML); medium stiff, moist, light reddish -brown, fill
2.0
1.8
1.6
(3.5') As Above: some clay
4.5
(4.5') SILT (ML); medium stiff, moist, light gray, with red brown mottling, native
5
3.9
5
(6) As Above: abundent manganese nodules
3.2
SB-9
(6'-8')
7.1
(7.5') SILT (ML); stiff, moist, gray and black and white, slight odor
(8') Boring terminated
10
10
15 15
NOTES: Hole precleared to 8.0' on 02/18/2019 by Mid South Environmental using hand auger.
generated using GroundLogs.onlfne

14
hart hickman
Client: Magnus Capital Partners
BORING LOG
Project: MGN.002
Boring No. SB-10
SMARTER ENVIRONMENTAL SOLUTIONS
Address:314&332 W. Bland Street, Charlotte NC
Page: 1 of 1
Drilling Start Date: 02/18/2019
Boring Depth (ft): 8.0
Drilling End Date: 02/18/2019
Boring Diameter (in): 2.25
Drilling Company: Mid South Environmental
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 5400
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
O
....
O
Jp
w
W
W
�F
O2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
LU
O
2
J
Q
°�O
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
0
J
0 0
(0') Asphalt
14.6
(0.5') SILT (ML); little fine sand, some clay, soft, moist, brown, fill
15.1
(15) SILT (ML); soft, moist, gray, with moist, soft, red/brown, silty clay, odor, fill
21.1
19.6
6.1
(45) SILT (ML); stiff, moist, gray and white, with verticle manganese veins, native,
5
odor
5.9
5
11.6
SB-10
(6'-8')
(7') SILT (ML); stiff, moist, gray and white, odor
22.7
(8') Boring terminated
10
10
15 15
NOTES: Hole precleared to 5.0' on 02/18/2019 by Mid South Environmental using hand auger.
generated using GroundLogs.onlfne

Appendix C
Laboratory Analytical Report
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 21, 2019
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
RE: Project: MGN-002
Pace Project No.: 92418026
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on February 15, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
Per client request, report revised 2/21/19 to update sample IDs.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: MGN-002
Pace Project No.: 92418026
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 72

aceAnalytical
—pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: MGN-002
Pace Project No.: 92418026
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92418026001
UST-1
Solid
02/15/1911:20
02/15/1917:45
92418026002
UST-2
Solid
02/15/1912:25
02/15/1917:45
92418026003
UST-3
Solid
02/15/1911:50
02/15/1917:45
92418026004
UST-4
Solid
02/15/1915:45
02/15/1917:45
92418026005
UST-5
Solid
02/15/1915:55
02/15/1917:45
92418026006
UST-6
Solid
02/15/1913:40
02/15/1917:45
92418026007
UST-8
Solid
02/15/1915:15
02/15/1917:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
MGN-002
92418026
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92418026001
UST-1
EPA 8270D
RES
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418026002
UST-2
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418026003
UST-3
EPA 8270D
RES
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418026004
UST-4
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418026005
UST-5
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418026006
UST-6
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418026007
UST-8
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-1 Lab ID: 92418026001 Collected: 02/15/19 11:20 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
3960
912
10
02/15/19 20:33
02/20/19 10:23
83-32-9
Acenaphthylene
ND
ug/kg
3960
936
10
02/15/19 20:33
02/20/19 10:23
208-96-8
Aniline
ND
ug/kg
3960
1070
10
02/15/19 20:33
02/20/19 10:23
62-53-3
Anthracene
ND
ug/kg
3960
888
10
02/15/19 20:33
02/20/19 10:23
120-12-7
Benzo(a)anthracene
ND
ug/kg
3960
732
10
02/15/19 20:33
02/20/19 10:23
56-55-3
Benzo(a)pyrene
ND
ug/kg
3960
756
10
02/15/19 20:33
02/20/19 10:23
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
3960
684
10
02/15/19 20:33
02/20/19 10:23
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
3960
1010
10
02/15/19 20:33
02/20/19 10:23
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
3960
780
10
02/15/19 20:33
02/20/19 10:23
207-08-9
Benzoic Acid
ND
ug/kg
19800
720
10
02/15/19 20:33
02/20/19 10:23
65-85-0
Benzyl alcohol
ND
ug/kg
7920
792
10
02/15/19 20:33
02/20/19 10:23
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
3960
720
10
02/15/19 20:33
02/20/19 10:23
101-55-3
Butylbenzylphthalate
ND
ug/kg
3960
840
10
02/15/19 20:33
02/20/19 10:23
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
7920
816
10
02/15/19 20:33
02/20/19 10:23
59-50-7
4-Chloroaniline
ND
ug/kg
19800
1100
10
02/15/19 20:33
02/20/19 10:23
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
3960
924
10
02/15/19 20:33
02/20/19 10:23
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
3960
1010
10
02/15/19 20:33
02/20/19 10:23
111-44-4
2-Chloronaphthalene
ND
ug/kg
3960
780
10
02/15/19 20:33
02/20/19 10:23
91-58-7
2-Chlorophenol
ND
ug/kg
3960
1080
10
02/15/19 20:33
02/20/19 10:23
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
3960
816
10
02/15/19 20:33
02/20/19 10:23
7005-72-3
Chrysene
ND
ug/kg
3960
528
10
02/15/19 20:33
02/20/19 10:23
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
3960
840
10
02/15/19 20:33
02/20/19 10:23
53-70-3
Dibenzofuran
ND
ug/kg
3960
648
10
02/15/19 20:33
02/20/19 10:23
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
3960
1060
10
02/15/19 20:33
02/20/19 10:23
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
3960
900
10
02/15/19 20:33
02/20/19 10:23
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
3960
1120
10
02/15/19 20:33
02/20/19 10:23
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
19800
864
10
02/15/19 20:33
02/20/19 10:23
91-94-1
2,4-Dichlorophenol
ND
ug/kg
3960
864
10
02/15/19 20:33
02/20/19 10:23
120-83-2
Diethylphthalate
ND
ug/kg
3960
612
10
02/15/19 20:33
02/20/19 10:23
84-66-2
2,4-Dimethylphenol
ND
ug/kg
3960
1560
10
02/15/19 20:33
02/20/19 10:23
105-67-9
Dimethylphthalate
ND
ug/kg
3960
804
10
02/15/19 20:33
02/20/19 10:23
131-11-3
Di-n-butylphthalate
ND
ug/kg
3960
648
10
02/15/19 20:33
02/20/19 10:23
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
7920
792
10
02/15/19 20:33
02/20/19 10:23
534-52-1
2,4-Dinitrophenol
ND
ug/kg
19800
648
10
02/15/19 20:33
02/20/19 10:23
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
3960
744
10
02/15/19 20:33
02/20/19 10:23
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
3960
828
10
02/15/19 20:33
02/20/19 10:23
606-20-2
Di-n-octylphthalate
ND
ug/kg
3960
828
10
02/15/19 20:33
02/20/19 10:23
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
3960
1080
10
02/15/19 20:33
02/20/19 10:23
117-81-7
Fluoranthene
ND
ug/kg
3960
576
10
02/15/19 20:33
02/20/19 10:23
206-44-0
Fluorene
1030J
ug/kg
3960
816
10
02/15/19 20:33
02/20/19 10:23
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
3960
684
10
02/15/19 20:33
02/20/19 10:23
87-68-3
Hexachlorobenzene
ND
ug/kg
3960
504
10
02/15/19 20:33
02/20/19 10:23
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
3960
732
10
02/15/19 20:33
02/20/19 10:23
77-47-4
Hexachloroethane
ND
ug/kg
3960
1040
10
02/15/19 20:33
02/20/19 10:23
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
3960
816
10
02/15/19 20:33
02/20/19 10:23
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-1
Lab ID:
92418026001
Collected:
02/15/19 11:20
Received: 02/15/19
17:45 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270D Preparation Method:
EPA 3546
Isophorone
ND
ug/kg
3960
888
10
02/15/19 20:33
02/20/19 10:23
78-59-1
1-Methylnaphthalene
15200
ug/kg
3960
1030
10
02/15/19 20:33
02/20/19 10:23
90-12-0
2-Methylnaphthalene
28400
ug/kg
3960
852
10
02/15/19 20:33
02/20/19 10:23
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
3960
1200
10
02/15/19 20:33
02/20/19 10:23
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
3960
1560
10
02/15/19 20:33
02/20/19 10:23
15831-10-4
Naphthalene
33000
ug/kg
3960
972
10
02/15/19 20:33
02/20/19 10:23
91-20-3
2-Nitroaniline
ND
ug/kg
19800
1220
10
02/15/19 20:33
02/20/19 10:23
88-74-4
3-Nitroaniline
ND
ug/kg
19800
1080
10
02/15/19 20:33
02/20/19 10:23
99-09-2
4-Nitroaniline
ND
ug/kg
7920
1120
10
02/15/19 20:33
02/20/19 10:23
100-01-6
Nitrobenzene
ND
ug/kg
3960
1080
10
02/15/19 20:33
02/20/19 10:23
98-95-3
2-Nitrophenol
ND
ug/kg
3960
960
10
02/15/19 20:33
02/20/19 10:23
88-75-5
4-Nitrophenol
ND
ug/kg
19800
708
10
02/15/19 20:33
02/20/19 10:23
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
3960
1280
10
02/15/19 20:33
02/20/19 10:23
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
3960
756
10
02/15/19 20:33
02/20/19 10:23
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
3960
1180
10
02/15/19 20:33
02/20/19 10:23
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
3960
1060
10
02/15/19 20:33
02/20/19 10:23
108-60-1
Pentachlorophenol
ND
ug/kg
19800
720
10
02/15/19 20:33
02/20/19 10:23
87-86-5
Phenanthrene
1420J
ug/kg
3960
660
10
02/15/19 20:33
02/20/19 10:23
85-01-8
Phenol
ND
ug/kg
3960
1190
10
02/15/19 20:33
02/20/19 10:23
108-95-2
Pyrene
ND
ug/kg
3960
672
10
02/15/19 20:33
02/20/19 10:23
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
3960
768
10
02/15/19 20:33
02/20/19 10:23
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
3960
1220
10
02/15/19 20:33
02/20/19 10:23
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
3960
876
10
02/15/19 20:33
02/20/19 10:23
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
02/15/19 20:33
02/20/19 10:23
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
02/15/19 20:33
02/20/19 10:23
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
02/15/19 20:33
02/20/19 10:23
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
02/15/19 20:33
02/20/19 10:23
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
02/15/19 20:33
02/20/19 10:23
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
02/15/19 20:33
02/20/19 10:23
118-79-6
S4
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
12500
1250
100
02/18/19 10:37
02/18/19 20:01
67-64-1
Benzene
2060
ug/kg
627
201
100
02/18/19 10:37
02/18/19 20:01
71-43-2
Bromobenzene
ND
ug/kg
627
251
100
02/18/19 10:37
02/18/19 20:01
108-86-1
Bromochloromethane
ND
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
74-97-5
Bromodichloromethane
ND
ug/kg
627
238
100
02/18/19 10:37
02/18/19 20:01
75-27-4
Bromoform
ND
ug/kg
627
289
100
02/18/19 10:37
02/18/19 20:01
75-25-2
Bromomethane
ND
ug/kg
1250
314
100
02/18/19 10:37
02/18/19 20:01
74-83-9
2-Butanone (MEK)
ND
ug/kg
12500
364
100
02/18/19 10:37
02/18/19 20:01
78-93-3
n-Butylbenzene
16500
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
104-51-8
sec-Butylbenzene
4790
ug/kg
627
201
100
02/18/19 10:37
02/18/19 20:01
135-98-8
tert-Butyl benzene
ND
ug/kg
627
251
100
02/18/19 10:37
02/18/19 20:01
98-06-6
Carbon tetrachloride
ND
ug/kg
627
326
100
02/18/19 10:37
02/18/19 20:01
56-23-5
Chlorobenzene
ND
ug/kg
627
238
100
02/18/19 10:37
02/18/19 20:01
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-1 Lab ID: 92418026001 Collected: 02/15/19 11:20 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
1250
301
100
02/18/19 10:37
02/18/19 20:01
75-00-3
Chloroform
ND
ug/kg
627
201
100
02/18/19 10:37
02/18/19 20:01
67-66-3
Chloromethane
ND
ug/kg
1250
301
100
02/18/19 10:37
02/18/19 20:01
74-87-3
2-Chlorotoluene
ND
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
95-49-8
4-Chlorotoluene
ND
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
627
452
100
02/18/19 10:37
02/18/19 20:01
96-12-8
Dibromochloromethane
ND
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
106-93-4
Dibromomethane
ND
ug/kg
627
314
100
02/18/19 10:37
02/18/19 20:01
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
627
238
100
02/18/19 10:37
02/18/19 20:01
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
627
251
100
02/18/19 10:37
02/18/19 20:01
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
106-46-7
Dichlorodifluoromethane
ND
ug/kg
1250
452
100
02/18/19 10:37
02/18/19 20:01
75-71-8
1,1-Dichloroethane
ND
ug/kg
627
188
100
02/18/19 10:37
02/18/19 20:01
75-34-3
1,2-Dichloroethane
ND
ug/kg
627
276
100
02/18/19 10:37
02/18/19 20:01
107-06-2
1,1-Dichloroethene
ND
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
627
176
100
02/18/19 10:37
02/18/19 20:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
627
238
100
02/18/19 10:37
02/18/19 20:01
156-60-5
1,2-Dichloropropane
ND
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
78-87-5
1,3-Dichloropropane
ND
ug/kg
627
238
100
02/18/19 10:37
02/18/19 20:01
142-28-9
2,2-Dichloropropane
ND
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
594-20-7
1,1-Dichloropropene
ND
ug/kg
627
188
100
02/18/19 10:37
02/18/19 20:01
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
627
188
100
02/18/19 10:37
02/18/19 20:01
10061-02-6
Diisopropyl ether
ND
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
108-20-3
Ethylbenzene
52900
ug/kg
7840
2820
1250
02/18/19 10:37
02/19/1911:35
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
627
251
100
02/18/19 10:37
02/18/19 20:01
87-68-3
2-Hexanone
ND
ug/kg
6270
489
100
02/18/19 10:37
02/18/19 20:01
591-78-6
Isopropylbenzene (Cumene)
9770
ug/kg
627
238
100
02/18/19 10:37
02/18/19 20:01
98-82-8
p-Isopropyltoluene
20500
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
99-87-6
Methylene Chloride
ND
ug/kg
2510
376
100
02/18/19 10:37
02/18/19 20:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
6270
464
100
02/18/19 10:37
02/18/19 20:01
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
627
188
100
02/18/19 10:37
02/18/19 20:01
1634-04-4
Naphthalene
47000
ug/kg
7840
1880
1250
02/18/19 10:37
02/19/1911:35
91-20-3
n-Propylbenzene
27700
ug/kg
7840
2670
1250
02/18/19 10:37
02/19/1911:35
103-65-1
Styrene
ND
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
627
264
100
02/18/19 10:37
02/18/19 20:01
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
627
238
100
02/18/19 10:37
02/18/19 20:01
79-34-5
Tetrachloroethene
ND
ug/kg
627
213
100
02/18/19 10:37
02/18/19 20:01
127-18-4
Toluene
45800
ug/kg
7840
2820
1250
02/18/19 10:37
02/19/1911:35
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
627
276
100
02/18/19 10:37
02/18/19 20:01
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
627
201
100
02/18/19 10:37
02/18/19 20:01
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
627
226
100
02/18/19 10:37
02/18/19 20:01
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
627
264
100
02/18/19 10:37
02/18/19 20:01
79-00-5
Trichloroethene
ND
ug/kg
627
264
100
02/18/19 10:37
02/18/19 20:01
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-1 Lab ID: 92418026001 Collected: 02/15/19 11:20 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/21 /2019 04:18 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
627
276
100
02/18/19 10:37
02/18/19 20:01
75-69-4
ND
ug/kg
627
201
100
02/18/19 10:37
02/18/19 20:01
96-18-4
227000
ug/kg
7840
3140
1250
02/18/19 10:37
02/19/1911:35
95-63-6
73000
ug/kg
7840
2820
1250
02/18/19 10:37
02/19/1911:35
108-67-8
ND
ug/kg
6270
1100
100
02/18/19 10:37
02/18/19 20:01
108-05-4
ND
ug/kg
1250
226
100
02/18/19 10:37
02/18/19 20:01
75-01-4
278000
ug/kg
15700
5650
1250
02/18/19 10:37
02/19/1911:35
1330-20-7
210000
ug/kg
15700
5650
1250
02/18/19 10:37
02/19/1911:35
179601-23-1
68000
ug/kg
7840
2980
1250
02/18/19 10:37
02/19/1911:35
95-47-6
109 % 70-130
159 % 70-130
121 % 70-132
Analytical Method: ASTM D2974-87
16.1 % 0.10
100 02/18/19 10:37 02/18/19 20:01 2037-26-5
100 02/18/19 10:37 02/18/19 20:01 460-00-4 S1
100 02/18/19 10:37 02/18/19 20:01 17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/16/19 18:56
Page 8 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-2 Lab ID: 92418026002 Collected: 02/15/19 12:25 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
405
93.4
1
02/15/19 20:33
02/18/19 17:07
83-32-9
Acenaphthylene
ND
ug/kg
405
95.8
1
02/15/19 20:33
02/18/19 17:07
208-96-8
Aniline
ND
ug/kg
405
109
1
02/15/19 20:33
02/18/19 17:07
62-53-3
Anthracene
ND
ug/kg
405
90.9
1
02/15/19 20:33
02/18/19 17:07
120-12-7
Benzo(a)anthracene
ND
ug/kg
405
74.9
1
02/15/19 20:33
02/18/19 17:07
56-55-3
Benzo(a)pyrene
ND
ug/kg
405
77.4
1
02/15/19 20:33
02/18/19 17:07
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
405
70.0
1
02/15/19 20:33
02/18/19 17:07
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
405
103
1
02/15/19 20:33
02/18/19 17:07
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
405
79.9
1
02/15/19 20:33
02/18/19 17:07
207-08-9
Benzoic Acid
ND
ug/kg
2030
73.7
1
02/15/19 20:33
02/18/19 17:07
65-85-0
Benzyl alcohol
ND
ug/kg
811
81.1
1
02/15/19 20:33
02/18/19 17:07
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
405
73.7
1
02/15/19 20:33
02/18/19 17:07
101-55-3
Butylbenzylphthalate
ND
ug/kg
405
86.0
1
02/15/19 20:33
02/18/19 17:07
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
811
83.5
1
02/15/19 20:33
02/18/19 17:07
59-50-7
4-Chloroaniline
ND
ug/kg
2030
113
1
02/15/19 20:33
02/18/19 17:07
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
405
94.6
1
02/15/19 20:33
02/18/19 17:07
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
405
103
1
02/15/19 20:33
02/18/19 17:07
111-44-4
2-Chloronaphthalene
ND
ug/kg
405
79.9
1
02/15/19 20:33
02/18/19 17:07
91-58-7
2-Chlorophenol
ND
ug/kg
405
ill
1
02/15/19 20:33
02/18/19 17:07
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
405
83.5
1
02/15/19 20:33
02/18/19 17:07
7005-72-3
Chrysene
ND
ug/kg
405
54.1
1
02/15/19 20:33
02/18/19 17:07
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
405
86.0
1
02/15/19 20:33
02/18/19 17:07
53-70-3
Dibenzofuran
ND
ug/kg
405
66.3
1
02/15/19 20:33
02/18/19 17:07
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
405
108
1
02/15/19 20:33
02/18/19 17:07
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
405
92.1
1
02/15/19 20:33
02/18/19 17:07
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
405
114
1
02/15/19 20:33
02/18/19 17:07
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2030
88.5
1
02/15/19 20:33
02/18/19 17:07
91-94-1
2,4-Dichlorophenol
ND
ug/kg
405
88.5
1
02/15/19 20:33
02/18/19 17:07
120-83-2
Diethylphthalate
ND
ug/kg
405
62.7
1
02/15/19 20:33
02/18/19 17:07
84-66-2
2,4-Dimethylphenol
ND
ug/kg
405
160
1
02/15/19 20:33
02/18/19 17:07
105-67-9
Dimethylphthalate
ND
ug/kg
405
82.3
1
02/15/19 20:33
02/18/19 17:07
131-11-3
Di-n-butylphthalate
ND
ug/kg
405
66.3
1
02/15/19 20:33
02/18/19 17:07
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
811
81.1
1
02/15/19 20:33
02/18/19 17:07
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2030
66.3
1
02/15/19 20:33
02/18/19 17:07
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
405
76.2
1
02/15/19 20:33
02/18/19 17:07
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
405
84.8
1
02/15/19 20:33
02/18/19 17:07
606-20-2
Di-n-octylphthalate
ND
ug/kg
405
84.8
1
02/15/19 20:33
02/18/19 17:07
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
405
ill
1
02/15/19 20:33
02/18/19 17:07
117-81-7
Fluoranthene
ND
ug/kg
405
59.0
1
02/15/19 20:33
02/18/19 17:07
206-44-0
Fluorene
ND
ug/kg
405
83.5
1
02/15/19 20:33
02/18/19 17:07
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
405
70.0
1
02/15/19 20:33
02/18/19 17:07
87-68-3
Hexachlorobenzene
ND
ug/kg
405
51.6
1
02/15/19 20:33
02/18/19 17:07
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
405
74.9
1
02/15/19 20:33
02/18/19 17:07
77-47-4
Hexachloroethane
ND
ug/kg
405
107
1
02/15/19 20:33
02/18/19 17:07
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
405
83.5
1
02/15/19 20:33
02/18/19 17:07
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-2 Lab ID: 92418026002 Collected: 02/15/19 12:25 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
405
90.9
1
02/15/19 20:33
02/18/19 17:07
78-59-1
1-Methylnaphthalene
ND
ug/kg
405
106
1
02/15/19 20:33
02/18/19 17:07
90-12-0
2-Methylnaphthalene
ND
ug/kg
405
87.2
1
02/15/19 20:33
02/18/19 17:07
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
405
123
1
02/15/19 20:33
02/18/19 17:07
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
405
160
1
02/15/19 20:33
02/18/19 17:07
15831-10-4
Naphthalene
ND
ug/kg
405
99.5
1
02/15/19 20:33
02/18/19 17:07
91-20-3
2-Nitroaniline
ND
ug/kg
2030
125
1
02/15/19 20:33
02/18/19 17:07
88-74-4
3-Nitroaniline
ND
ug/kg
2030
ill
1
02/15/19 20:33
02/18/19 17:07
99-09-2
4-Nitroaniline
ND
ug/kg
811
114
1
02/15/19 20:33
02/18/19 17:07
100-01-6
Nitrobenzene
ND
ug/kg
405
ill
1
02/15/19 20:33
02/18/19 17:07
98-95-3
2-Nitrophenol
ND
ug/kg
405
98.3
1
02/15/19 20:33
02/18/19 17:07
88-75-5
4-Nitrophenol
ND
ug/kg
2030
72.5
1
02/15/19 20:33
02/18/19 17:07
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
405
131
1
02/15/19 20:33
02/18/19 17:07
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
405
77.4
1
02/15/19 20:33
02/18/19 17:07
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
405
120
1
02/15/19 20:33
02/18/19 17:07
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
405
108
1
02/15/19 20:33
02/18/19 17:07
108-60-1
Pentachlorophenol
ND
ug/kg
2030
73.7
1
02/15/19 20:33
02/18/19 17:07
87-86-5
Phenanthrene
ND
ug/kg
405
67.6
1
02/15/19 20:33
02/18/19 17:07
85-01-8
Phenol
ND
ug/kg
405
122
1
02/15/19 20:33
02/18/19 17:07
108-95-2
Pyrene
ND
ug/kg
405
68.8
1
02/15/19 20:33
02/18/19 17:07
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
405
78.6
1
02/15/19 20:33
02/18/19 17:07
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
405
125
1
02/15/19 20:33
02/18/19 17:07
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
405
89.7
1
02/15/19 20:33
02/18/19 17:07
88-06-2
Surrogates
Nitrobenzene-d5 (S)
70
%
23-110
1
02/15/19 20:33
02/18/19 17:07
4165-60-0
2-Fluorobiphenyl (S)
65
%
30-110
1
02/15/19 20:33
02/18/19 17:07
321-60-8
Terphenyl-d14 (S)
71
%
28-110
1
02/15/19 20:33
02/18/19 17:07
1718-51-0
Phenol-d6 (S)
63
%
22-110
1
02/15/19 20:33
02/18/19 17:07
13127-88-3
2-Fluorophenol (S)
56
%
13-110
1
02/15/19 20:33
02/18/19 17:07
367-12-4
2,4,6-Tribromophenol (S)
62
%
27-110
1
02/15/19 20:33
02/18/19 17:07
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation
Method:
EPA 5035A
Acetone
ND
ug/kg
10600
1060
100
02/18/19 10:46
02/18/19 20:20
67-64-1
Benzene
1240
ug/kg
528
169
100
02/18/19 10:46
02/18/19 20:20
71-43-2
Bromobenzene
ND
ug/kg
528
211
100
02/18/19 10:46
02/18/19 20:20
108-86-1
Bromochloromethane
ND
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
74-97-5
Bromodichloromethane
ND
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
75-27-4
Bromoform
ND
ug/kg
528
243
100
02/18/19 10:46
02/18/19 20:20
75-25-2
Bromomethane
ND
ug/kg
1060
264
100
02/18/19 10:46
02/18/19 20:20
74-83-9
2-Butanone (MEK)
ND
ug/kg
10600
306
100
02/18/19 10:46
02/18/19 20:20
78-93-3
n-Butylbenzene
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
104-51-8
sec-Butylbenzene
852
ug/kg
528
169
100
02/18/19 10:46
02/18/19 20:20
135-98-8
tert-Butyl benzene
ND
ug/kg
528
211
100
02/18/19 10:46
02/18/19 20:20
98-06-6
Carbon tetrachloride
ND
ug/kg
528
275
100
02/18/19 10:46
02/18/19 20:20
56-23-5
Chlorobenzene
ND
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-2 Lab ID: 92418026002 Collected: 02/15/19 12:25 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
1060
254
100
02/18/19 10:46
02/18/19 20:20
75-00-3
Chloroform
ND
ug/kg
528
169
100
02/18/19 10:46
02/18/19 20:20
67-66-3
Chloromethane
ND
ug/kg
1060
254
100
02/18/19 10:46
02/18/19 20:20
74-87-3
2-Chlorotoluene
ND
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
95-49-8
4-Chlorotoluene
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
528
380
100
02/18/19 10:46
02/18/19 20:20
96-12-8
Dibromochloromethane
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
106-93-4
Dibromomethane
ND
ug/kg
528
264
100
02/18/19 10:46
02/18/19 20:20
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
528
211
100
02/18/19 10:46
02/18/19 20:20
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
106-46-7
Dichlorodifluoromethane
ND
ug/kg
1060
380
100
02/18/19 10:46
02/18/19 20:20
75-71-8
1,1-Dichloroethane
ND
ug/kg
528
159
100
02/18/19 10:46
02/18/19 20:20
75-34-3
1,2-Dichloroethane
ND
ug/kg
528
232
100
02/18/19 10:46
02/18/19 20:20
107-06-2
1,1-Dichloroethene
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
528
148
100
02/18/19 10:46
02/18/19 20:20
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
156-60-5
1,2-Dichloropropane
ND
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
78-87-5
1,3-Dichloropropane
ND
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
142-28-9
2,2-Dichloropropane
ND
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
594-20-7
1,1-Dichloropropene
ND
ug/kg
528
159
100
02/18/19 10:46
02/18/19 20:20
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
528
159
100
02/18/19 10:46
02/18/19 20:20
10061-02-6
Diisopropyl ether
ND
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
108-20-3
Ethylbenzene
8370
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
528
211
100
02/18/19 10:46
02/18/19 20:20
87-68-3
2-Hexanone
ND
ug/kg
5280
412
100
02/18/19 10:46
02/18/19 20:20
591-78-6
Isopropylbenzene (Cumene)
1600
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
98-82-8
p-Isopropyltoluene
3340
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
99-87-6
Methylene Chloride
ND
ug/kg
2110
317
100
02/18/19 10:46
02/18/19 20:20
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
5280
391
100
02/18/19 10:46
02/18/19 20:20
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
528
159
100
02/18/19 10:46
02/18/19 20:20
1634-04-4
Naphthalene
8450
ug/kg
528
127
100
02/18/19 10:46
02/18/19 20:20
91-20-3
n-Propylbenzene
3530
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
103-65-1
Styrene
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
528
222
100
02/18/19 10:46
02/18/19 20:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
79-34-5
Tetrachloroethene
ND
ug/kg
528
180
100
02/18/19 10:46
02/18/19 20:20
127-18-4
Toluene
9350
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
528
232
100
02/18/19 10:46
02/18/19 20:20
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
528
169
100
02/18/19 10:46
02/18/19 20:20
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
528
222
100
02/18/19 10:46
02/18/19 20:20
79-00-5
Trichloroethene
ND
ug/kg
528
222
100
02/18/19 10:46
02/18/19 20:20
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-2 Lab ID: 92418026002 Collected: 02/15/19 12:25 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/21 /2019 04:18 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
528
232
100
02/18/19 10:46
02/18/19 20:20
75-69-4
ND
ug/kg
528
169
100
02/18/19 10:46
02/18/19 20:20
96-18-4
13900
ug/kg
1320
528
250
02/18/19 10:46
02/19/1912:13
95-63-6
9410
ug/kg
528
190
100
02/18/19 10:46
02/18/19 20:20
108-67-8
ND
ug/kg
5280
930
100
02/18/19 10:46
02/18/19 20:20
108-05-4
ND
ug/kg
1060
190
100
02/18/19 10:46
02/18/19 20:20
75-01-4
38200
ug/kg
1060
380
100
02/18/19 10:46
02/18/19 20:20
1330-20-7
28400
ug/kg
1060
380
100
02/18/19 10:46
02/18/19 20:20
179601-23-1
9830
ug/kg
528
201
100
02/18/19 10:46
02/18/19 20:20
95-47-6
96
%
70-130
100
02/18/19 10:46
02/18/19 20:20
2037-26-5
118
%
70-130
100
02/18/19 10:46
02/18/19 20:20
460-00-4
104
%
70-132
100
02/18/19 10:46
02/18/19 20:20
17060-07-0
Analytical Method: ASTM D2974-87
19.9 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/16/19 18:56
Page 12 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-3 Lab ID: 92418026003 Collected: 02/15/19 11:50 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
3860
889
10
02/15/19 20:33
02/20/19 14:12
83-32-9
Acenaphthylene
ND
ug/kg
3860
913
10
02/15/19 20:33
02/20/19 14:12
208-96-8
Aniline
ND
ug/kg
3860
1040
10
02/15/19 20:33
02/20/19 14:12
62-53-3
Anthracene
ND
ug/kg
3860
866
10
02/15/19 20:33
02/20/19 14:12
120-12-7
Benzo(a)anthracene
ND
ug/kg
3860
714
10
02/15/19 20:33
02/20/19 14:12
56-55-3
Benzo(a)pyrene
ND
ug/kg
3860
737
10
02/15/19 20:33
02/20/19 14:12
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
3860
667
10
02/15/19 20:33
02/20/19 14:12
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
3860
983
10
02/15/19 20:33
02/20/19 14:12
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
3860
761
10
02/15/19 20:33
02/20/19 14:12
207-08-9
Benzoic Acid
ND
ug/kg
19300
702
10
02/15/19 20:33
02/20/19 14:12
65-85-0
Benzyl alcohol
ND
ug/kg
7720
772
10
02/15/19 20:33
02/20/19 14:12
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
3860
702
10
02/15/19 20:33
02/20/19 14:12
101-55-3
Butylbenzylphthalate
ND
ug/kg
3860
819
10
02/15/19 20:33
02/20/19 14:12
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
7720
796
10
02/15/19 20:33
02/20/19 14:12
59-50-7
4-Chloroaniline
ND
ug/kg
19300
1080
10
02/15/19 20:33
02/20/19 14:12
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
3860
901
10
02/15/19 20:33
02/20/19 14:12
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
3860
983
10
02/15/19 20:33
02/20/19 14:12
111-44-4
2-Chloronaphthalene
ND
ug/kg
3860
761
10
02/15/19 20:33
02/20/19 14:12
91-58-7
2-Chlorophenol
ND
ug/kg
3860
1050
10
02/15/19 20:33
02/20/19 14:12
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
3860
796
10
02/15/19 20:33
02/20/19 14:12
7005-72-3
Chrysene
ND
ug/kg
3860
515
10
02/15/19 20:33
02/20/19 14:12
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
3860
819
10
02/15/19 20:33
02/20/19 14:12
53-70-3
Dibenzofuran
ND
ug/kg
3860
632
10
02/15/19 20:33
02/20/19 14:12
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
3860
1030
10
02/15/19 20:33
02/20/19 14:12
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
3860
878
10
02/15/19 20:33
02/20/19 14:12
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
3860
1090
10
02/15/19 20:33
02/20/19 14:12
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
19300
842
10
02/15/19 20:33
02/20/19 14:12
91-94-1
2,4-Dichlorophenol
ND
ug/kg
3860
842
10
02/15/19 20:33
02/20/19 14:12
120-83-2
Diethylphthalate
ND
ug/kg
3860
597
10
02/15/19 20:33
02/20/19 14:12
84-66-2
2,4-Dimethylphenol
ND
ug/kg
3860
1520
10
02/15/19 20:33
02/20/19 14:12
105-67-9
Dimethylphthalate
ND
ug/kg
3860
784
10
02/15/19 20:33
02/20/19 14:12
131-11-3
Di-n-butylphthalate
ND
ug/kg
3860
632
10
02/15/19 20:33
02/20/19 14:12
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
7720
772
10
02/15/19 20:33
02/20/19 14:12
534-52-1
2,4-Dinitrophenol
ND
ug/kg
19300
632
10
02/15/19 20:33
02/20/19 14:12
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
3860
725
10
02/15/19 20:33
02/20/19 14:12
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
3860
807
10
02/15/19 20:33
02/20/19 14:12
606-20-2
Di-n-octylphthalate
ND
ug/kg
3860
807
10
02/15/19 20:33
02/20/19 14:12
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
3860
1050
10
02/15/19 20:33
02/20/19 14:12
117-81-7
Fluoranthene
ND
ug/kg
3860
562
10
02/15/19 20:33
02/20/19 14:12
206-44-0
Fluorene
1050J
ug/kg
3860
796
10
02/15/19 20:33
02/20/19 14:12
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
3860
667
10
02/15/19 20:33
02/20/19 14:12
87-68-3
Hexachlorobenzene
ND
ug/kg
3860
491
10
02/15/19 20:33
02/20/19 14:12
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
3860
714
10
02/15/19 20:33
02/20/19 14:12
77-47-4
Hexachloroethane
ND
ug/kg
3860
1020
10
02/15/19 20:33
02/20/19 14:12
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
3860
796
10
02/15/19 20:33
02/20/19 14:12
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-3
Lab ID:
92418026003
Collected:
02/15/19
11:50
Received: 02/15/19
17:45 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
3860
866
10
02/15/19 20:33
02/20/19 14:12
78-59-1
1-Methylnaphthalene
7470
ug/kg
3860
1010
10
02/15/19 20:33
02/20/19 14:12
90-12-0
2-Methylnaphthalene
12700
ug/kg
3860
831
10
02/15/19 20:33
02/20/19 14:12
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
3860
1170
10
02/15/19 20:33
02/20/19 14:12
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
3860
1520
10
02/15/19 20:33
02/20/19 14:12
15831-10-4
Naphthalene
7420
ug/kg
3860
948
10
02/15/19 20:33
02/20/19 14:12
91-20-3
2-Nitroaniline
ND
ug/kg
19300
1190
10
02/15/19 20:33
02/20/19 14:12
88-74-4
3-Nitroaniline
ND
ug/kg
19300
1050
10
02/15/19 20:33
02/20/19 14:12
99-09-2
4-Nitroaniline
ND
ug/kg
7720
1090
10
02/15/19 20:33
02/20/19 14:12
100-01-6
Nitrobenzene
ND
ug/kg
3860
1050
10
02/15/19 20:33
02/20/19 14:12
98-95-3
2-Nitrophenol
ND
ug/kg
3860
936
10
02/15/19 20:33
02/20/19 14:12
88-75-5
4-Nitrophenol
ND
ug/kg
19300
690
10
02/15/19 20:33
02/20/19 14:12
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
3860
1250
10
02/15/19 20:33
02/20/19 14:12
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
3860
737
10
02/15/19 20:33
02/20/19 14:12
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
3860
1150
10
02/15/19 20:33
02/20/19 14:12
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
3860
1030
10
02/15/19 20:33
02/20/19 14:12
108-60-1
Pentachlorophenol
ND
ug/kg
19300
702
10
02/15/19 20:33
02/20/19 14:12
87-86-5
Phenanthrene
1200J
ug/kg
3860
644
10
02/15/19 20:33
02/20/19 14:12
85-01-8
Phenol
ND
ug/kg
3860
1160
10
02/15/19 20:33
02/20/19 14:12
108-95-2
Pyrene
ND
ug/kg
3860
655
10
02/15/19 20:33
02/20/19 14:12
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
3860
749
10
02/15/19 20:33
02/20/19 14:12
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
3860
1190
10
02/15/19 20:33
02/20/19 14:12
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
3860
854
10
02/15/19 20:33
02/20/19 14:12
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
02/15/19 20:33
02/20/19 14:12
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
02/15/19 20:33
02/20/19 14:12
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
02/15/19 20:33
02/20/19 14:12
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
02/15/19 20:33
02/20/19 14:12
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
02/15/19 20:33
02/20/19 14:12
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
02/15/19 20:33
02/20/19 14:12
118-79-6
S4
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B
Preparation Method:
EPA 5035A
Acetone
14.2J
ug/kg
102
10.2
1
02/18/19 10:42
02/18/19 20:40
67-64-1
Benzene
ND
ug/kg
5.1
1.6
1
02/18/19 10:42
02/18/19 20:40
71-43-2
Bromobenzene
ND
ug/kg
5.1
2.0
1
02/18/19 10:42
02/18/19 20:40
108-86-1
Bromochloromethane
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
74-97-5
Bromodichloromethane
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
75-27-4
Bromoform
ND
ug/kg
5.1
2.3
1
02/18/19 10:42
02/18/19 20:40
75-25-2
Bromomethane
ND
ug/kg
10.2
2.5
1
02/18/19 10:42
02/18/19 20:40
74-83-9
2-Butanone (MEK)
ND
ug/kg
102
2.9
1
02/18/19 10:42
02/18/19 20:40
78-93-3
n-Butylbenzene
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
104-51-8
sec-Butylbenzene
ND
ug/kg
5.1
1.6
1
02/18/19 10:42
02/18/19 20:40
135-98-8
tert-Butyl benzene
ND
ug/kg
5.1
2.0
1
02/18/19 10:42
02/18/19 20:40
98-06-6
Carbon tetrachloride
ND
ug/kg
5.1
2.6
1
02/18/19 10:42
02/18/19 20:40
56-23-5
Chlorobenzene
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-3 Lab ID: 92418026003 Collected: 02/15/19 11:50 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
10.2
2.4
1
02/18/19 10:42
02/18/19 20:40
75-00-3
Chloroform
ND
ug/kg
5.1
1.6
1
02/18/19 10:42
02/18/19 20:40
67-66-3
Chloromethane
ND
ug/kg
10.2
2.4
1
02/18/19 10:42
02/18/19 20:40
74-87-3
2-Chlorotoluene
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
95-49-8
4-Chlorotoluene
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.1
3.7
1
02/18/19 10:42
02/18/19 20:40
96-12-8
Dibromochloromethane
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
106-93-4
Dibromomethane
ND
ug/kg
5.1
2.5
1
02/18/19 10:42
02/18/19 20:40
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.1
2.0
1
02/18/19 10:42
02/18/19 20:40
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
106-46-7
Dichlorodifluoromethane
ND
ug/kg
10.2
3.7
1
02/18/19 10:42
02/18/19 20:40
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.1
1.5
1
02/18/19 10:42
02/18/19 20:40
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.1
2.2
1
02/18/19 10:42
02/18/19 20:40
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.1
1.4
1
02/18/19 10:42
02/18/19 20:40
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.1
1.5
1
02/18/19 10:42
02/18/19 20:40
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.1
1.5
1
02/18/19 10:42
02/18/19 20:40
10061-02-6
Diisopropyl ether
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
108-20-3
Ethylbenzene
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.1
2.0
1
02/18/19 10:42
02/18/19 20:40
87-68-3
2-Hexanone
ND
ug/kg
50.8
4.0
1
02/18/19 10:42
02/18/19 20:40
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
99-87-6
Methylene Chloride
ND
ug/kg
20.3
3.0
1
02/18/19 10:42
02/18/19 20:40
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
50.8
3.8
1
02/18/19 10:42
02/18/19 20:40
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.1
1.5
1
02/18/19 10:42
02/18/19 20:40
1634-04-4
Naphthalene
1.6J
ug/kg
5.1
1.2
1
02/18/19 10:42
02/18/19 20:40
91-20-3
n-Propylbenzene
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
103-65-1
Styrene
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.1
2.1
1
02/18/19 10:42
02/18/19 20:40
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
79-34-5
Tetrachloroethene
ND
ug/kg
5.1
1.7
1
02/18/19 10:42
02/18/19 20:40
127-18-4
Toluene
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.1
2.2
1
02/18/19 10:42
02/18/19 20:40
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.1
1.6
1
02/18/19 10:42
02/18/19 20:40
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.1
2.1
1
02/18/19 10:42
02/18/19 20:40
79-00-5
Trichloroethene
ND
ug/kg
5.1
2.1
1
02/18/19 10:42
02/18/19 20:40
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-3 Lab ID: 92418026003 Collected: 02/15/19 11:50 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/21 /2019 04:18 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
5.1
2.2
1
02/18/19 10:42
02/18/19 20:40
75-69-4
ND
ug/kg
5.1
1.6
1
02/18/19 10:42
02/18/19 20:40
96-18-4
8.7
ug/kg
5.1
2.0
1
02/18/19 10:42
02/18/19 20:40
95-63-6
2.5J
ug/kg
5.1
1.8
1
02/18/19 10:42
02/18/19 20:40
108-67-8
ND
ug/kg
50.8
8.9
1
02/18/19 10:42
02/18/19 20:40
108-05-4
ND
ug/kg
10.2
1.8
1
02/18/19 10:42
02/18/19 20:40
75-01-4
ND
ug/kg
10.2
3.7
1
02/18/19 10:42
02/18/19 20:40
1330-20-7
4.1J
ug/kg
10.2
3.7
1
02/18/19 10:42
02/18/19 20:40
179601-23-1
ND
ug/kg
5.1
1.9
1
02/18/19 10:42
02/18/19 20:40
95-47-6
119
%
70-130
1
02/18/19 10:42
02/18/19 20:40
2037-26-5
109
%
70-130
1
02/18/19 10:42
02/18/19 20:40
460-00-4
80
%
70-132
1
02/18/19 10:42
02/18/19 20:40
17060-07-0
Analytical Method: ASTM D2974-87
14.5 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/16/19 18:56
Page 16 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-4 Lab ID: 92418026004 Collected: 02/15/19 15:45 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
406
93.4
1
02/15/19 20:33
02/18/19 18:08
83-32-9
Acenaphthylene
ND
ug/kg
406
95.9
1
02/15/19 20:33
02/18/19 18:08
208-96-8
Aniline
ND
ug/kg
406
109
1
02/15/19 20:33
02/18/19 18:08
62-53-3
Anthracene
ND
ug/kg
406
91.0
1
02/15/19 20:33
02/18/19 18:08
120-12-7
Benzo(a)anthracene
ND
ug/kg
406
75.0
1
02/15/19 20:33
02/18/19 18:08
56-55-3
Benzo(a)pyrene
ND
ug/kg
406
77.4
1
02/15/19 20:33
02/18/19 18:08
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
406
70.1
1
02/15/19 20:33
02/18/19 18:08
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
406
103
1
02/15/19 20:33
02/18/19 18:08
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
406
79.9
1
02/15/19 20:33
02/18/19 18:08
207-08-9
Benzoic Acid
ND
ug/kg
2030
73.8
1
02/15/19 20:33
02/18/19 18:08
65-85-0
Benzyl alcohol
ND
ug/kg
811
81.1
1
02/15/19 20:33
02/18/19 18:08
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
406
73.8
1
02/15/19 20:33
02/18/19 18:08
101-55-3
Butylbenzylphthalate
ND
ug/kg
406
86.1
1
02/15/19 20:33
02/18/19 18:08
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
811
83.6
1
02/15/19 20:33
02/18/19 18:08
59-50-7
4-Chloroaniline
ND
ug/kg
2030
113
1
02/15/19 20:33
02/18/19 18:08
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
406
94.7
1
02/15/19 20:33
02/18/19 18:08
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
406
103
1
02/15/19 20:33
02/18/19 18:08
111-44-4
2-Chloronaphthalene
ND
ug/kg
406
79.9
1
02/15/19 20:33
02/18/19 18:08
91-58-7
2-Chlorophenol
ND
ug/kg
406
ill
1
02/15/19 20:33
02/18/19 18:08
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
406
83.6
1
02/15/19 20:33
02/18/19 18:08
7005-72-3
Chrysene
ND
ug/kg
406
54.1
1
02/15/19 20:33
02/18/19 18:08
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
406
86.1
1
02/15/19 20:33
02/18/19 18:08
53-70-3
Dibenzofuran
ND
ug/kg
406
66.4
1
02/15/19 20:33
02/18/19 18:08
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
406
108
1
02/15/19 20:33
02/18/19 18:08
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
406
92.2
1
02/15/19 20:33
02/18/19 18:08
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
406
114
1
02/15/19 20:33
02/18/19 18:08
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2030
88.5
1
02/15/19 20:33
02/18/19 18:08
91-94-1
2,4-Dichlorophenol
ND
ug/kg
406
88.5
1
02/15/19 20:33
02/18/19 18:08
120-83-2
Diethylphthalate
ND
ug/kg
406
62.7
1
02/15/19 20:33
02/18/19 18:08
84-66-2
2,4-Dimethylphenol
ND
ug/kg
406
160
1
02/15/19 20:33
02/18/19 18:08
105-67-9
Dimethylphthalate
ND
ug/kg
406
82.4
1
02/15/19 20:33
02/18/19 18:08
131-11-3
Di-n-butylphthalate
ND
ug/kg
406
66.4
1
02/15/19 20:33
02/18/19 18:08
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
811
81.1
1
02/15/19 20:33
02/18/19 18:08
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2030
66.4
1
02/15/19 20:33
02/18/19 18:08
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
406
76.2
1
02/15/19 20:33
02/18/19 18:08
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
406
84.8
1
02/15/19 20:33
02/18/19 18:08
606-20-2
Di-n-octylphthalate
ND
ug/kg
406
84.8
1
02/15/19 20:33
02/18/19 18:08
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
406
ill
1
02/15/19 20:33
02/18/19 18:08
117-81-7
Fluoranthene
ND
ug/kg
406
59.0
1
02/15/19 20:33
02/18/19 18:08
206-44-0
Fluorene
ND
ug/kg
406
83.6
1
02/15/19 20:33
02/18/19 18:08
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
406
70.1
1
02/15/19 20:33
02/18/19 18:08
87-68-3
Hexachlorobenzene
ND
ug/kg
406
51.6
1
02/15/19 20:33
02/18/19 18:08
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
406
75.0
1
02/15/19 20:33
02/18/19 18:08
77-47-4
Hexachloroethane
ND
ug/kg
406
107
1
02/15/19 20:33
02/18/19 18:08
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
406
83.6
1
02/15/19 20:33
02/18/19 18:08
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-4 Lab ID: 92418026004 Collected: 02/15/19 15:45 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
406
91.0
1
02/15/19 20:33
02/18/19 18:08
78-59-1
1-Methylnaphthalene
ND
ug/kg
406
106
1
02/15/19 20:33
02/18/19 18:08
90-12-0
2-Methylnaphthalene
ND
ug/kg
406
87.3
1
02/15/19 20:33
02/18/19 18:08
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
406
123
1
02/15/19 20:33
02/18/19 18:08
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
406
160
1
02/15/19 20:33
02/18/19 18:08
15831-10-4
Naphthalene
ND
ug/kg
406
99.6
1
02/15/19 20:33
02/18/19 18:08
91-20-3
2-Nitroaniline
ND
ug/kg
2030
125
1
02/15/19 20:33
02/18/19 18:08
88-74-4
3-Nitroaniline
ND
ug/kg
2030
ill
1
02/15/19 20:33
02/18/19 18:08
99-09-2
4-Nitroaniline
ND
ug/kg
811
114
1
02/15/19 20:33
02/18/19 18:08
100-01-6
Nitrobenzene
ND
ug/kg
406
ill
1
02/15/19 20:33
02/18/19 18:08
98-95-3
2-Nitrophenol
ND
ug/kg
406
98.3
1
02/15/19 20:33
02/18/19 18:08
88-75-5
4-Nitrophenol
ND
ug/kg
2030
72.5
1
02/15/19 20:33
02/18/19 18:08
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
406
132
1
02/15/19 20:33
02/18/19 18:08
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
406
77.4
1
02/15/19 20:33
02/18/19 18:08
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
406
120
1
02/15/19 20:33
02/18/19 18:08
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
406
108
1
02/15/19 20:33
02/18/19 18:08
108-60-1
Pentachlorophenol
ND
ug/kg
2030
73.8
1
02/15/19 20:33
02/18/19 18:08
87-86-5
Phenanthrene
ND
ug/kg
406
67.6
1
02/15/19 20:33
02/18/19 18:08
85-01-8
Phenol
ND
ug/kg
406
122
1
02/15/19 20:33
02/18/19 18:08
108-95-2
Pyrene
ND
ug/kg
406
68.8
1
02/15/19 20:33
02/18/19 18:08
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
406
78.7
1
02/15/19 20:33
02/18/19 18:08
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
406
125
1
02/15/19 20:33
02/18/19 18:08
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
406
89.7
1
02/15/19 20:33
02/18/19 18:08
88-06-2
Surrogates
Nitrobenzene-d5 (S)
75
%
23-110
1
02/15/19 20:33
02/18/19 18:08
4165-60-0
2-Fluorobiphenyl (S)
69
%
30-110
1
02/15/19 20:33
02/18/19 18:08
321-60-8
Terphenyl-d14 (S)
72
%
28-110
1
02/15/19 20:33
02/18/19 18:08
1718-51-0
Phenol-d6 (S)
72
%
22-110
1
02/15/19 20:33
02/18/19 18:08
13127-88-3
2-Fluorophenol (S)
63
%
13-110
1
02/15/19 20:33
02/18/19 18:08
367-12-4
2,4,6-Tribromophenol (S)
74
%
27-110
1
02/15/19 20:33
02/18/19 18:08
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
31 AJ
ug/kg
132
13.2
1
02/18/19 10:42
02/18/19 21:00
67-64-1
Benzene
ND
ug/kg
6.6
2.1
1
02/18/19 10:42
02/18/19 21:00
71-43-2
Bromobenzene
ND
ug/kg
6.6
2.6
1
02/18/19 10:42
02/18/19 21:00
108-86-1
Bromochloromethane
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
74-97-5
Bromodichloromethane
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
75-27-4
Bromoform
ND
ug/kg
6.6
3.0
1
02/18/19 10:42
02/18/19 21:00
75-25-2
Bromomethane
ND
ug/kg
13.2
3.3
1
02/18/19 10:42
02/18/19 21:00
74-83-9
2-Butanone (MEK)
ND
ug/kg
132
3.8
1
02/18/19 10:42
02/18/19 21:00
78-93-3
n-Butylbenzene
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
104-51-8
sec-Butylbenzene
ND
ug/kg
6.6
2.1
1
02/18/19 10:42
02/18/19 21:00
135-98-8
tert-Butyl benzene
ND
ug/kg
6.6
2.6
1
02/18/19 10:42
02/18/19 21:00
98-06-6
Carbon tetrachloride
ND
ug/kg
6.6
3.4
1
02/18/19 10:42
02/18/19 21:00
56-23-5
Chlorobenzene
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-4 Lab ID: 92418026004 Collected: 02/15/19 15:45 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
13.2
3.2
1
02/18/19 10:42
02/18/19 21:00
75-00-3
Chloroform
ND
ug/kg
6.6
2.1
1
02/18/19 10:42
02/18/19 21:00
67-66-3
Chloromethane
ND
ug/kg
13.2
3.2
1
02/18/19 10:42
02/18/19 21:00
74-87-3
2-Chlorotoluene
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
95-49-8
4-Chlorotoluene
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.6
4.7
1
02/18/19 10:42
02/18/19 21:00
96-12-8
Dibromochloromethane
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
106-93-4
Dibromomethane
ND
ug/kg
6.6
3.3
1
02/18/19 10:42
02/18/19 21:00
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.6
2.6
1
02/18/19 10:42
02/18/19 21:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
106-46-7
Dichlorodifluoromethane
ND
ug/kg
13.2
4.7
1
02/18/19 10:42
02/18/19 21:00
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.6
2.0
1
02/18/19 10:42
02/18/19 21:00
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.6
2.9
1
02/18/19 10:42
02/18/19 21:00
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.6
1.8
1
02/18/19 10:42
02/18/19 21:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.6
2.0
1
02/18/19 10:42
02/18/19 21:00
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.6
2.0
1
02/18/19 10:42
02/18/19 21:00
10061-02-6
Diisopropyl ether
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
108-20-3
Ethylbenzene
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.6
2.6
1
02/18/19 10:42
02/18/19 21:00
87-68-3
2-Hexanone
ND
ug/kg
65.9
5.1
1
02/18/19 10:42
02/18/19 21:00
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
99-87-6
Methylene Chloride
ND
ug/kg
26.4
4.0
1
02/18/19 10:42
02/18/19 21:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
65.9
4.9
1
02/18/19 10:42
02/18/19 21:00
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.6
2.0
1
02/18/19 10:42
02/18/19 21:00
1634-04-4
Naphthalene
ND
ug/kg
6.6
1.6
1
02/18/19 10:42
02/18/19 21:00
91-20-3
n-Propylbenzene
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
103-65-1
Styrene
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
6.6
2.8
1
02/18/19 10:42
02/18/19 21:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
79-34-5
Tetrachloroethene
ND
ug/kg
6.6
2.2
1
02/18/19 10:42
02/18/19 21:00
127-18-4
Toluene
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
6.6
2.9
1
02/18/19 10:42
02/18/19 21:00
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
6.6
2.1
1
02/18/19 10:42
02/18/19 21:00
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
6.6
2.8
1
02/18/19 10:42
02/18/19 21:00
79-00-5
Trichloroethene
ND
ug/kg
6.6
2.8
1
02/18/19 10:42
02/18/19 21:00
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-4 Lab ID: 92418026004 Collected: 02/15/19 15:45 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/21 /2019 04:18 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
6.6
2.9
1
02/18/19 10:42
02/18/19 21:00
75-69-4
ND
ug/kg
6.6
2.1
1
02/18/19 10:42
02/18/19 21:00
96-18-4
3.9J
ug/kg
6.6
2.6
1
02/18/19 10:42
02/18/19 21:00
95-63-6
ND
ug/kg
6.6
2.4
1
02/18/19 10:42
02/18/19 21:00
108-67-8
ND
ug/kg
65.9
11.6
1
02/18/19 10:42
02/18/19 21:00
108-05-4
ND
ug/kg
13.2
2.4
1
02/18/19 10:42
02/18/19 21:00
75-01-4
ND
ug/kg
13.2
4.7
1
02/18/19 10:42
02/18/19 21:00
1330-20-7
ND
ug/kg
13.2
4.7
1
02/18/19 10:42
02/18/19 21:00
179601-23-1
ND
ug/kg
6.6
2.5
1
02/18/19 10:42
02/18/19 21:00
95-47-6
118
%
70-130
1
02/18/19 10:42
02/18/19 21:00
2037-26-5
108
%
70-130
1
02/18/19 10:42
02/18/19 21:00
460-00-4
78
%
70-132
1
02/18/19 10:42
02/18/19 21:00
17060-07-0
Analytical Method: ASTM D2974-87
17.6 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/16/19 18:57
Page 20 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-5 Lab ID: 92418026005 Collected: 02/15/19 15:55 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
388
89.4
1
02/15/19 20:33
02/18/19 18:39
83-32-9
Acenaphthylene
ND
ug/kg
388
91.8
1
02/15/19 20:33
02/18/19 18:39
208-96-8
Aniline
ND
ug/kg
388
105
1
02/15/19 20:33
02/18/19 18:39
62-53-3
Anthracene
ND
ug/kg
388
87.1
1
02/15/19 20:33
02/18/19 18:39
120-12-7
Benzo(a)anthracene
ND
ug/kg
388
71.8
1
02/15/19 20:33
02/18/19 18:39
56-55-3
Benzo(a)pyrene
ND
ug/kg
388
74.1
1
02/15/19 20:33
02/18/19 18:39
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
388
67.1
1
02/15/19 20:33
02/18/19 18:39
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
388
98.8
1
02/15/19 20:33
02/18/19 18:39
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
388
76.5
1
02/15/19 20:33
02/18/19 18:39
207-08-9
Benzoic Acid
ND
ug/kg
1940
70.6
1
02/15/19 20:33
02/18/19 18:39
65-85-0
Benzyl alcohol
ND
ug/kg
777
77.7
1
02/15/19 20:33
02/18/19 18:39
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
388
70.6
1
02/15/19 20:33
02/18/19 18:39
101-55-3
Butylbenzylphthalate
ND
ug/kg
388
82.4
1
02/15/19 20:33
02/18/19 18:39
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
777
80.0
1
02/15/19 20:33
02/18/19 18:39
59-50-7
4-Chloroaniline
ND
ug/kg
1940
108
1
02/15/19 20:33
02/18/19 18:39
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
388
90.6
1
02/15/19 20:33
02/18/19 18:39
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
388
98.8
1
02/15/19 20:33
02/18/19 18:39
111-44-4
2-Chloronaphthalene
ND
ug/kg
388
76.5
1
02/15/19 20:33
02/18/19 18:39
91-58-7
2-Chlorophenol
ND
ug/kg
388
106
1
02/15/19 20:33
02/18/19 18:39
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
388
80.0
1
02/15/19 20:33
02/18/19 18:39
7005-72-3
Chrysene
ND
ug/kg
388
51.8
1
02/15/19 20:33
02/18/19 18:39
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
388
82.4
1
02/15/19 20:33
02/18/19 18:39
53-70-3
Dibenzofuran
ND
ug/kg
388
63.5
1
02/15/19 20:33
02/18/19 18:39
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
388
104
1
02/15/19 20:33
02/18/19 18:39
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
388
88.3
1
02/15/19 20:33
02/18/19 18:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
388
109
1
02/15/19 20:33
02/18/19 18:39
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1940
84.7
1
02/15/19 20:33
02/18/19 18:39
91-94-1
2,4-Dichlorophenol
ND
ug/kg
388
84.7
1
02/15/19 20:33
02/18/19 18:39
120-83-2
Diethylphthalate
ND
ug/kg
388
60.0
1
02/15/19 20:33
02/18/19 18:39
84-66-2
2,4-Dimethylphenol
ND
ug/kg
388
153
1
02/15/19 20:33
02/18/19 18:39
105-67-9
Dimethylphthalate
ND
ug/kg
388
78.8
1
02/15/19 20:33
02/18/19 18:39
131-11-3
Di-n-butylphthalate
ND
ug/kg
388
63.5
1
02/15/19 20:33
02/18/19 18:39
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
777
77.7
1
02/15/19 20:33
02/18/19 18:39
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1940
63.5
1
02/15/19 20:33
02/18/19 18:39
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
388
73.0
1
02/15/19 20:33
02/18/19 18:39
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
388
81.2
1
02/15/19 20:33
02/18/19 18:39
606-20-2
Di-n-octylphthalate
ND
ug/kg
388
81.2
1
02/15/19 20:33
02/18/19 18:39
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
388
106
1
02/15/19 20:33
02/18/19 18:39
117-81-7
Fluoranthene
ND
ug/kg
388
56.5
1
02/15/19 20:33
02/18/19 18:39
206-44-0
Fluorene
ND
ug/kg
388
80.0
1
02/15/19 20:33
02/18/19 18:39
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
388
67.1
1
02/15/19 20:33
02/18/19 18:39
87-68-3
Hexachlorobenzene
ND
ug/kg
388
49.4
1
02/15/19 20:33
02/18/19 18:39
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
388
71.8
1
02/15/19 20:33
02/18/19 18:39
77-47-4
Hexachloroethane
ND
ug/kg
388
102
1
02/15/19 20:33
02/18/19 18:39
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
388
80.0
1
02/15/19 20:33
02/18/19 18:39
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-5 Lab ID: 92418026005 Collected: 02/15/19 15:55 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
388
87.1
1
02/15/19 20:33
02/18/19 18:39
78-59-1
1-Methylnaphthalene
ND
ug/kg
388
101
1
02/15/19 20:33
02/18/19 18:39
90-12-0
2-Methylnaphthalene
ND
ug/kg
388
83.5
1
02/15/19 20:33
02/18/19 18:39
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
388
118
1
02/15/19 20:33
02/18/19 18:39
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
388
153
1
02/15/19 20:33
02/18/19 18:39
15831-10-4
Naphthalene
ND
ug/kg
388
95.3
1
02/15/19 20:33
02/18/19 18:39
91-20-3
2-Nitroaniline
ND
ug/kg
1940
120
1
02/15/19 20:33
02/18/19 18:39
88-74-4
3-Nitroaniline
ND
ug/kg
1940
106
1
02/15/19 20:33
02/18/19 18:39
99-09-2
4-Nitroaniline
ND
ug/kg
777
109
1
02/15/19 20:33
02/18/19 18:39
100-01-6
Nitrobenzene
ND
ug/kg
388
106
1
02/15/19 20:33
02/18/19 18:39
98-95-3
2-Nitrophenol
ND
ug/kg
388
94.1
1
02/15/19 20:33
02/18/19 18:39
88-75-5
4-Nitrophenol
ND
ug/kg
1940
69.4
1
02/15/19 20:33
02/18/19 18:39
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
388
126
1
02/15/19 20:33
02/18/19 18:39
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
388
74.1
1
02/15/19 20:33
02/18/19 18:39
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
388
115
1
02/15/19 20:33
02/18/19 18:39
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
388
104
1
02/15/19 20:33
02/18/19 18:39
108-60-1
Pentachlorophenol
ND
ug/kg
1940
70.6
1
02/15/19 20:33
02/18/19 18:39
87-86-5
Phenanthrene
ND
ug/kg
388
64.7
1
02/15/19 20:33
02/18/19 18:39
85-01-8
Phenol
ND
ug/kg
388
116
1
02/15/19 20:33
02/18/19 18:39
108-95-2
Pyrene
ND
ug/kg
388
65.9
1
02/15/19 20:33
02/18/19 18:39
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
388
75.3
1
02/15/19 20:33
02/18/19 18:39
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
388
120
1
02/15/19 20:33
02/18/19 18:39
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
388
85.9
1
02/15/19 20:33
02/18/19 18:39
88-06-2
Surrogates
Nitrobenzene-d5 (S)
43
%
23-110
1
02/15/19 20:33
02/18/19 18:39
4165-60-0
2-Fluorobiphenyl (S)
47
%
30-110
1
02/15/19 20:33
02/18/19 18:39
321-60-8
Terphenyl-d14 (S)
57
%
28-110
1
02/15/19 20:33
02/18/19 18:39
1718-51-0
Phenol-d6 (S)
41
%
22-110
1
02/15/19 20:33
02/18/19 18:39
13127-88-3
2-Fluorophenol (S)
35
%
13-110
1
02/15/19 20:33
02/18/19 18:39
367-12-4
2,4,6-Tribromophenol (S)
59
%
27-110
1
02/15/19 20:33
02/18/19 18:39
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
ND
ug/kg
125
12.5
1
02/18/19 10:42
02/18/19 21:20
67-64-1
Benzene
ND
ug/kg
6.2
2.0
1
02/18/19 10:42
02/18/19 21:20
71-43-2
Bromobenzene
ND
ug/kg
6.2
2.5
1
02/18/19 10:42
02/18/19 21:20
108-86-1
Bromochloromethane
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
74-97-5
Bromodichloromethane
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
75-27-4
Bromoform
ND
ug/kg
6.2
2.9
1
02/18/19 10:42
02/18/19 21:20
75-25-2
Bromomethane
ND
ug/kg
12.5
3.1
1
02/18/19 10:42
02/18/19 21:20
74-83-9
2-Butanone (MEK)
ND
ug/kg
125
3.6
1
02/18/19 10:42
02/18/19 21:20
78-93-3
n-Butylbenzene
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
104-51-8
sec-Butylbenzene
ND
ug/kg
6.2
2.0
1
02/18/19 10:42
02/18/19 21:20
135-98-8
tert-Butyl benzene
ND
ug/kg
6.2
2.5
1
02/18/19 10:42
02/18/19 21:20
98-06-6
Carbon tetrachloride
ND
ug/kg
6.2
3.2
1
02/18/19 10:42
02/18/19 21:20
56-23-5
Chlorobenzene
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-5 Lab ID: 92418026005 Collected: 02/15/19 15:55 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
12.5
3.0
1
02/18/19 10:42
02/18/19 21:20
75-00-3
Chloroform
ND
ug/kg
6.2
2.0
1
02/18/19 10:42
02/18/19 21:20
67-66-3
Chloromethane
ND
ug/kg
12.5
3.0
1
02/18/19 10:42
02/18/19 21:20
74-87-3
2-Chlorotoluene
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
95-49-8
4-Chlorotoluene
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.2
4.5
1
02/18/19 10:42
02/18/19 21:20
96-12-8
Dibromochloromethane
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
106-93-4
Dibromomethane
ND
ug/kg
6.2
3.1
1
02/18/19 10:42
02/18/19 21:20
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.2
2.5
1
02/18/19 10:42
02/18/19 21:20
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.5
4.5
1
02/18/19 10:42
02/18/19 21:20
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.2
1.9
1
02/18/19 10:42
02/18/19 21:20
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.2
2.7
1
02/18/19 10:42
02/18/19 21:20
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.2
1.7
1
02/18/19 10:42
02/18/19 21:20
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.2
1.9
1
02/18/19 10:42
02/18/19 21:20
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.2
1.9
1
02/18/19 10:42
02/18/19 21:20
10061-02-6
Diisopropyl ether
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
108-20-3
Ethylbenzene
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.2
2.5
1
02/18/19 10:42
02/18/19 21:20
87-68-3
2-Hexanone
ND
ug/kg
62.5
4.9
1
02/18/19 10:42
02/18/19 21:20
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
99-87-6
Methylene Chloride
ND
ug/kg
25.0
3.7
1
02/18/19 10:42
02/18/19 21:20
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
62.5
4.6
1
02/18/19 10:42
02/18/19 21:20
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.2
1.9
1
02/18/19 10:42
02/18/19 21:20
1634-04-4
Naphthalene
ND
ug/kg
6.2
1.5
1
02/18/19 10:42
02/18/19 21:20
91-20-3
n-Propylbenzene
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
103-65-1
Styrene
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
6.2
2.6
1
02/18/19 10:42
02/18/19 21:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
79-34-5
Tetrachloroethene
ND
ug/kg
6.2
2.1
1
02/18/19 10:42
02/18/19 21:20
127-18-4
Toluene
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
6.2
2.7
1
02/18/19 10:42
02/18/19 21:20
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
6.2
2.0
1
02/18/19 10:42
02/18/19 21:20
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
6.2
2.6
1
02/18/19 10:42
02/18/19 21:20
79-00-5
Trichloroethene
ND
ug/kg
6.2
2.6
1
02/18/19 10:42
02/18/19 21:20
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-5 Lab ID: 92418026005 Collected: 02/15/19 15:55 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/21 /2019 04:18 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
6.2
2.7
1
02/18/19 10:42
02/18/19 21:20
75-69-4
ND
ug/kg
6.2
2.0
1
02/18/19 10:42
02/18/19 21:20
96-18-4
ND
ug/kg
6.2
2.5
1
02/18/19 10:42
02/18/19 21:20
95-63-6
ND
ug/kg
6.2
2.2
1
02/18/19 10:42
02/18/19 21:20
108-67-8
ND
ug/kg
62.5
11.0
1
02/18/19 10:42
02/18/19 21:20
108-05-4
ND
ug/kg
12.5
2.2
1
02/18/19 10:42
02/18/19 21:20
75-01-4
ND
ug/kg
12.5
4.5
1
02/18/19 10:42
02/18/19 21:20
1330-20-7
ND
ug/kg
12.5
4.5
1
02/18/19 10:42
02/18/19 21:20
179601-23-1
ND
ug/kg
6.2
2.4
1
02/18/19 10:42
02/18/19 21:20
95-47-6
121
%
70-130
1
02/18/19 10:42
02/18/19 21:20
2037-26-5
108
%
70-130
1
02/18/19 10:42
02/18/19 21:20
460-00-4
78
%
70-132
1
02/18/19 10:42
02/18/19 21:20
17060-07-0
Analytical Method: ASTM D2974-87
15.6 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/16/19 18:57
Page 24 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-6 Lab ID: 92418026006 Collected: 02/15/19 13:40 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
399
91.8
1
02/15/19 20:33
02/18/19 19:10
83-32-9
Acenaphthylene
ND
ug/kg
399
94.2
1
02/15/19 20:33
02/18/19 19:10
208-96-8
Aniline
ND
ug/kg
399
108
1
02/15/19 20:33
02/18/19 19:10
62-53-3
Anthracene
ND
ug/kg
399
89.4
1
02/15/19 20:33
02/18/19 19:10
120-12-7
Benzo(a)anthracene
ND
ug/kg
399
73.7
1
02/15/19 20:33
02/18/19 19:10
56-55-3
Benzo(a)pyrene
ND
ug/kg
399
76.1
1
02/15/19 20:33
02/18/19 19:10
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
399
68.9
1
02/15/19 20:33
02/18/19 19:10
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
399
101
1
02/15/19 20:33
02/18/19 19:10
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
399
78.5
1
02/15/19 20:33
02/18/19 19:10
207-08-9
Benzoic Acid
ND
ug/kg
1990
72.5
1
02/15/19 20:33
02/18/19 19:10
65-85-0
Benzyl alcohol
ND
ug/kg
797
79.7
1
02/15/19 20:33
02/18/19 19:10
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
399
72.5
1
02/15/19 20:33
02/18/19 19:10
101-55-3
Butylbenzylphthalate
ND
ug/kg
399
84.6
1
02/15/19 20:33
02/18/19 19:10
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
797
82.1
1
02/15/19 20:33
02/18/19 19:10
59-50-7
4-Chloroaniline
ND
ug/kg
1990
ill
1
02/15/19 20:33
02/18/19 19:10
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
399
93.0
1
02/15/19 20:33
02/18/19 19:10
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
399
101
1
02/15/19 20:33
02/18/19 19:10
111-44-4
2-Chloronaphthalene
ND
ug/kg
399
78.5
1
02/15/19 20:33
02/18/19 19:10
91-58-7
2-Chlorophenol
ND
ug/kg
399
109
1
02/15/19 20:33
02/18/19 19:10
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
399
82.1
1
02/15/19 20:33
02/18/19 19:10
7005-72-3
Chrysene
ND
ug/kg
399
53.2
1
02/15/19 20:33
02/18/19 19:10
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
399
84.6
1
02/15/19 20:33
02/18/19 19:10
53-70-3
Dibenzofuran
ND
ug/kg
399
65.2
1
02/15/19 20:33
02/18/19 19:10
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
399
106
1
02/15/19 20:33
02/18/19 19:10
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
399
90.6
1
02/15/19 20:33
02/18/19 19:10
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
399
112
1
02/15/19 20:33
02/18/19 19:10
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1990
87.0
1
02/15/19 20:33
02/18/19 19:10
91-94-1
2,4-Dichlorophenol
ND
ug/kg
399
87.0
1
02/15/19 20:33
02/18/19 19:10
120-83-2
Diethylphthalate
ND
ug/kg
399
61.6
1
02/15/19 20:33
02/18/19 19:10
84-66-2
2,4-Dimethylphenol
ND
ug/kg
399
157
1
02/15/19 20:33
02/18/19 19:10
105-67-9
Dimethylphthalate
ND
ug/kg
399
80.9
1
02/15/19 20:33
02/18/19 19:10
131-11-3
Di-n-butylphthalate
ND
ug/kg
399
65.2
1
02/15/19 20:33
02/18/19 19:10
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
797
79.7
1
02/15/19 20:33
02/18/19 19:10
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1990
65.2
1
02/15/19 20:33
02/18/19 19:10
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
399
74.9
1
02/15/19 20:33
02/18/19 19:10
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
399
83.4
1
02/15/19 20:33
02/18/19 19:10
606-20-2
Di-n-octylphthalate
ND
ug/kg
399
83.4
1
02/15/19 20:33
02/18/19 19:10
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
399
109
1
02/15/19 20:33
02/18/19 19:10
117-81-7
Fluoranthene
ND
ug/kg
399
58.0
1
02/15/19 20:33
02/18/19 19:10
206-44-0
Fluorene
ND
ug/kg
399
82.1
1
02/15/19 20:33
02/18/19 19:10
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
399
68.9
1
02/15/19 20:33
02/18/19 19:10
87-68-3
Hexachlorobenzene
ND
ug/kg
399
50.7
1
02/15/19 20:33
02/18/19 19:10
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
399
73.7
1
02/15/19 20:33
02/18/19 19:10
77-47-4
Hexachloroethane
ND
ug/kg
399
105
1
02/15/19 20:33
02/18/19 19:10
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
399
82.1
1
02/15/19 20:33
02/18/19 19:10
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-6 Lab ID: 92418026006 Collected: 02/15/19 13:40 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
399
89.4
1
02/15/19 20:33
02/18/19 19:10
78-59-1
1-Methylnaphthalene
ND
ug/kg
399
104
1
02/15/19 20:33
02/18/19 19:10
90-12-0
2-Methylnaphthalene
ND
ug/kg
399
85.8
1
02/15/19 20:33
02/18/19 19:10
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
399
121
1
02/15/19 20:33
02/18/19 19:10
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
399
157
1
02/15/19 20:33
02/18/19 19:10
15831-10-4
Naphthalene
ND
ug/kg
399
97.8
1
02/15/19 20:33
02/18/19 19:10
91-20-3
2-Nitroaniline
ND
ug/kg
1990
123
1
02/15/19 20:33
02/18/19 19:10
88-74-4
3-Nitroaniline
ND
ug/kg
1990
109
1
02/15/19 20:33
02/18/19 19:10
99-09-2
4-Nitroaniline
ND
ug/kg
797
112
1
02/15/19 20:33
02/18/19 19:10
100-01-6
Nitrobenzene
ND
ug/kg
399
109
1
02/15/19 20:33
02/18/19 19:10
98-95-3
2-Nitrophenol
ND
ug/kg
399
96.6
1
02/15/19 20:33
02/18/19 19:10
88-75-5
4-Nitrophenol
ND
ug/kg
1990
71.3
1
02/15/19 20:33
02/18/19 19:10
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
399
129
1
02/15/19 20:33
02/18/19 19:10
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
399
76.1
1
02/15/19 20:33
02/18/19 19:10
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
399
118
1
02/15/19 20:33
02/18/19 19:10
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
399
106
1
02/15/19 20:33
02/18/19 19:10
108-60-1
Pentachlorophenol
ND
ug/kg
1990
72.5
1
02/15/19 20:33
02/18/19 19:10
87-86-5
Phenanthrene
ND
ug/kg
399
66.4
1
02/15/19 20:33
02/18/19 19:10
85-01-8
Phenol
ND
ug/kg
399
120
1
02/15/19 20:33
02/18/19 19:10
108-95-2
Pyrene
ND
ug/kg
399
67.6
1
02/15/19 20:33
02/18/19 19:10
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
399
77.3
1
02/15/19 20:33
02/18/19 19:10
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
399
123
1
02/15/19 20:33
02/18/19 19:10
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
399
88.2
1
02/15/19 20:33
02/18/19 19:10
88-06-2
Surrogates
Nitrobenzene-d5 (S)
82
%
23-110
1
02/15/19 20:33
02/18/19 19:10
4165-60-0
2-Fluorobiphenyl (S)
81
%
30-110
1
02/15/19 20:33
02/18/19 19:10
321-60-8
Terphenyl-d14 (S)
68
%
28-110
1
02/15/19 20:33
02/18/19 19:10
1718-51-0
Phenol-d6 (S)
69
%
22-110
1
02/15/19 20:33
02/18/19 19:10
13127-88-3
2-Fluorophenol (S)
62
%
13-110
1
02/15/19 20:33
02/18/19 19:10
367-12-4
2,4,6-Tribromophenol (S)
60
%
27-110
1
02/15/19 20:33
02/18/19 19:10
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
ND
ug/kg
112
11.2
1
02/18/19 10:42
02/18/19 21:40
67-64-1
Benzene
ND
ug/kg
5.6
1.8
1
02/18/19 10:42
02/18/19 21:40
71-43-2
Bromobenzene
ND
ug/kg
5.6
2.2
1
02/18/19 10:42
02/18/19 21:40
108-86-1
Bromochloromethane
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
74-97-5
Bromodichloromethane
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
75-27-4
Bromoform
ND
ug/kg
5.6
2.6
1
02/18/19 10:42
02/18/19 21:40
75-25-2
Bromomethane
ND
ug/kg
11.2
2.8
1
02/18/19 10:42
02/18/19 21:40
74-83-9
2-Butanone (MEK)
ND
ug/kg
112
3.2
1
02/18/19 10:42
02/18/19 21:40
78-93-3
n-Butylbenzene
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
104-51-8
sec-Butylbenzene
ND
ug/kg
5.6
1.8
1
02/18/19 10:42
02/18/19 21:40
135-98-8
tert-Butyl benzene
ND
ug/kg
5.6
2.2
1
02/18/19 10:42
02/18/19 21:40
98-06-6
Carbon tetrachloride
ND
ug/kg
5.6
2.9
1
02/18/19 10:42
02/18/19 21:40
56-23-5
Chlorobenzene
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-6 Lab ID: 92418026006 Collected: 02/15/19 13:40 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
11.2
2.7
1
02/18/19 10:42
02/18/19 21:40
75-00-3
Chloroform
ND
ug/kg
5.6
1.8
1
02/18/19 10:42
02/18/19 21:40
67-66-3
Chloromethane
ND
ug/kg
11.2
2.7
1
02/18/19 10:42
02/18/19 21:40
74-87-3
2-Chlorotoluene
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
95-49-8
4-Chlorotoluene
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.6
4.0
1
02/18/19 10:42
02/18/19 21:40
96-12-8
Dibromochloromethane
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
106-93-4
Dibromomethane
ND
ug/kg
5.6
2.8
1
02/18/19 10:42
02/18/19 21:40
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.6
2.2
1
02/18/19 10:42
02/18/19 21:40
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.2
4.0
1
02/18/19 10:42
02/18/19 21:40
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.6
1.7
1
02/18/19 10:42
02/18/19 21:40
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.6
2.5
1
02/18/19 10:42
02/18/19 21:40
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.6
1.6
1
02/18/19 10:42
02/18/19 21:40
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.6
1.7
1
02/18/19 10:42
02/18/19 21:40
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.6
1.7
1
02/18/19 10:42
02/18/19 21:40
10061-02-6
Diisopropyl ether
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
108-20-3
Ethylbenzene
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.6
2.2
1
02/18/19 10:42
02/18/19 21:40
87-68-3
2-Hexanone
ND
ug/kg
55.9
4.4
1
02/18/19 10:42
02/18/19 21:40
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
99-87-6
Methylene Chloride
ND
ug/kg
22.4
3.4
1
02/18/19 10:42
02/18/19 21:40
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
55.9
4.1
1
02/18/19 10:42
02/18/19 21:40
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.6
1.7
1
02/18/19 10:42
02/18/19 21:40
1634-04-4
Naphthalene
1AJ
ug/kg
5.6
1.3
1
02/18/19 10:42
02/18/19 21:40
91-20-3
n-Propylbenzene
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
103-65-1
Styrene
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.6
2.3
1
02/18/19 10:42
02/18/19 21:40
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
79-34-5
Tetrachloroethene
ND
ug/kg
5.6
1.9
1
02/18/19 10:42
02/18/19 21:40
127-18-4
Toluene
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.6
2.5
1
02/18/19 10:42
02/18/19 21:40
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.6
1.8
1
02/18/19 10:42
02/18/19 21:40
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.6
2.3
1
02/18/19 10:42
02/18/19 21:40
79-00-5
Trichloroethene
ND
ug/kg
5.6
2.3
1
02/18/19 10:42
02/18/19 21:40
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-6 Lab ID: 92418026006 Collected: 02/15/19 13:40 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/21 /2019 04:18 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
5.6
2.5
1
02/18/19 10:42
02/18/19 21:40
75-69-4
ND
ug/kg
5.6
1.8
1
02/18/19 10:42
02/18/19 21:40
96-18-4
ND
ug/kg
5.6
2.2
1
02/18/19 10:42
02/18/19 21:40
95-63-6
ND
ug/kg
5.6
2.0
1
02/18/19 10:42
02/18/19 21:40
108-67-8
ND
ug/kg
55.9
9.8
1
02/18/19 10:42
02/18/19 21:40
108-05-4
ND
ug/kg
11.2
2.0
1
02/18/19 10:42
02/18/19 21:40
75-01-4
ND
ug/kg
11.2
4.0
1
02/18/19 10:42
02/18/19 21:40
1330-20-7
ND
ug/kg
11.2
4.0
1
02/18/19 10:42
02/18/19 21:40
179601-23-1
ND
ug/kg
5.6
2.1
1
02/18/19 10:42
02/18/19 21:40
95-47-6
119
%
70-130
1
02/18/19 10:42
02/18/19 21:40
2037-26-5
108
%
70-130
1
02/18/19 10:42
02/18/19 21:40
460-00-4
78
%
70-132
1
02/18/19 10:42
02/18/19 21:40
17060-07-0
Analytical Method: ASTM D2974-87
18.6 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/16/19 18:57
Page 28 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-8 Lab ID: 92418026007 Collected: 02/15/19 15:15 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
387
89.1
1
02/15/19 20:33
02/18/19 19:41
83-32-9
Acenaphthylene
ND
ug/kg
387
91.4
1
02/15/19 20:33
02/18/19 19:41
208-96-8
Aniline
ND
ug/kg
387
104
1
02/15/19 20:33
02/18/19 19:41
62-53-3
Anthracene
ND
ug/kg
387
86.7
1
02/15/19 20:33
02/18/19 19:41
120-12-7
Benzo(a)anthracene
ND
ug/kg
387
71.5
1
02/15/19 20:33
02/18/19 19:41
56-55-3
Benzo(a)pyrene
ND
ug/kg
387
73.8
1
02/15/19 20:33
02/18/19 19:41
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
387
66.8
1
02/15/19 20:33
02/18/19 19:41
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
387
98.4
1
02/15/19 20:33
02/18/19 19:41
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
387
76.2
1
02/15/19 20:33
02/18/19 19:41
207-08-9
Benzoic Acid
ND
ug/kg
1930
70.3
1
02/15/19 20:33
02/18/19 19:41
65-85-0
Benzyl alcohol
ND
ug/kg
773
77.3
1
02/15/19 20:33
02/18/19 19:41
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
387
70.3
1
02/15/19 20:33
02/18/19 19:41
101-55-3
Butylbenzylphthalate
ND
ug/kg
387
82.0
1
02/15/19 20:33
02/18/19 19:41
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
773
79.7
1
02/15/19 20:33
02/18/19 19:41
59-50-7
4-Chloroaniline
ND
ug/kg
1930
108
1
02/15/19 20:33
02/18/19 19:41
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
387
90.2
1
02/15/19 20:33
02/18/19 19:41
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
387
98.4
1
02/15/19 20:33
02/18/19 19:41
111-44-4
2-Chloronaphthalene
ND
ug/kg
387
76.2
1
02/15/19 20:33
02/18/19 19:41
91-58-7
2-Chlorophenol
ND
ug/kg
387
105
1
02/15/19 20:33
02/18/19 19:41
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
387
79.7
1
02/15/19 20:33
02/18/19 19:41
7005-72-3
Chrysene
ND
ug/kg
387
51.6
1
02/15/19 20:33
02/18/19 19:41
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
387
82.0
1
02/15/19 20:33
02/18/19 19:41
53-70-3
Dibenzofuran
ND
ug/kg
387
63.3
1
02/15/19 20:33
02/18/19 19:41
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
387
103
1
02/15/19 20:33
02/18/19 19:41
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
387
87.9
1
02/15/19 20:33
02/18/19 19:41
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
387
109
1
02/15/19 20:33
02/18/19 19:41
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1930
84.4
1
02/15/19 20:33
02/18/19 19:41
91-94-1
2,4-Dichlorophenol
ND
ug/kg
387
84.4
1
02/15/19 20:33
02/18/19 19:41
120-83-2
Diethylphthalate
ND
ug/kg
387
59.8
1
02/15/19 20:33
02/18/19 19:41
84-66-2
2,4-Dimethylphenol
ND
ug/kg
387
152
1
02/15/19 20:33
02/18/19 19:41
105-67-9
Dimethylphthalate
ND
ug/kg
387
78.5
1
02/15/19 20:33
02/18/19 19:41
131-11-3
Di-n-butylphthalate
ND
ug/kg
387
63.3
1
02/15/19 20:33
02/18/19 19:41
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
773
77.3
1
02/15/19 20:33
02/18/19 19:41
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1930
63.3
1
02/15/19 20:33
02/18/19 19:41
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
387
72.6
1
02/15/19 20:33
02/18/19 19:41
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
387
80.9
1
02/15/19 20:33
02/18/19 19:41
606-20-2
Di-n-octylphthalate
ND
ug/kg
387
80.9
1
02/15/19 20:33
02/18/19 19:41
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
387
105
1
02/15/19 20:33
02/18/19 19:41
117-81-7
Fluoranthene
ND
ug/kg
387
56.2
1
02/15/19 20:33
02/18/19 19:41
206-44-0
Fluorene
ND
ug/kg
387
79.7
1
02/15/19 20:33
02/18/19 19:41
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
387
66.8
1
02/15/19 20:33
02/18/19 19:41
87-68-3
Hexachlorobenzene
ND
ug/kg
387
49.2
1
02/15/19 20:33
02/18/19 19:41
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
387
71.5
1
02/15/19 20:33
02/18/19 19:41
77-47-4
Hexachloroethane
ND
ug/kg
387
102
1
02/15/19 20:33
02/18/19 19:41
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
387
79.7
1
02/15/19 20:33
02/18/19 19:41
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-8 Lab ID: 92418026007 Collected: 02/15/19 15:15 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
387
86.7
1
02/15/19 20:33
02/18/19 19:41
78-59-1
1-Methylnaphthalene
ND
ug/kg
387
101
1
02/15/19 20:33
02/18/19 19:41
90-12-0
2-Methylnaphthalene
ND
ug/kg
387
83.2
1
02/15/19 20:33
02/18/19 19:41
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
387
117
1
02/15/19 20:33
02/18/19 19:41
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
387
152
1
02/15/19 20:33
02/18/19 19:41
15831-10-4
Naphthalene
ND
ug/kg
387
94.9
1
02/15/19 20:33
02/18/19 19:41
91-20-3
2-Nitroaniline
ND
ug/kg
1930
120
1
02/15/19 20:33
02/18/19 19:41
88-74-4
3-Nitroaniline
ND
ug/kg
1930
105
1
02/15/19 20:33
02/18/19 19:41
99-09-2
4-Nitroaniline
ND
ug/kg
773
109
1
02/15/19 20:33
02/18/19 19:41
100-01-6
Nitrobenzene
ND
ug/kg
387
105
1
02/15/19 20:33
02/18/19 19:41
98-95-3
2-Nitrophenol
ND
ug/kg
387
93.7
1
02/15/19 20:33
02/18/19 19:41
88-75-5
4-Nitrophenol
ND
ug/kg
1930
69.1
1
02/15/19 20:33
02/18/19 19:41
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
387
125
1
02/15/19 20:33
02/18/19 19:41
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
387
73.8
1
02/15/19 20:33
02/18/19 19:41
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
387
115
1
02/15/19 20:33
02/18/19 19:41
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
387
103
1
02/15/19 20:33
02/18/19 19:41
108-60-1
Pentachlorophenol
ND
ug/kg
1930
70.3
1
02/15/19 20:33
02/18/19 19:41
87-86-5
Phenanthrene
ND
ug/kg
387
64.4
1
02/15/19 20:33
02/18/19 19:41
85-01-8
Phenol
ND
ug/kg
387
116
1
02/15/19 20:33
02/18/19 19:41
108-95-2
Pyrene
ND
ug/kg
387
65.6
1
02/15/19 20:33
02/18/19 19:41
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
387
75.0
1
02/15/19 20:33
02/18/19 19:41
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
387
120
1
02/15/19 20:33
02/18/19 19:41
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
387
85.5
1
02/15/19 20:33
02/18/19 19:41
88-06-2
Surrogates
Nitrobenzene-d5 (S)
79
%
23-110
1
02/15/19 20:33
02/18/19 19:41
4165-60-0
2-Fluorobiphenyl (S)
68
%
30-110
1
02/15/19 20:33
02/18/19 19:41
321-60-8
Terphenyl-d14 (S)
73
%
28-110
1
02/15/19 20:33
02/18/19 19:41
1718-51-0
Phenol-d6 (S)
63
%
22-110
1
02/15/19 20:33
02/18/19 19:41
13127-88-3
2-Fluorophenol (S)
57
%
13-110
1
02/15/19 20:33
02/18/19 19:41
367-12-4
2,4,6-Tribromophenol (S)
68
%
27-110
1
02/15/19 20:33
02/18/19 19:41
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
ND
ug/kg
99.5
9.9
1
02/18/19 10:42
02/18/19 22:00
67-64-1
Benzene
ND
ug/kg
5.0
1.6
1
02/18/19 10:42
02/18/19 22:00
71-43-2
Bromobenzene
ND
ug/kg
5.0
2.0
1
02/18/19 10:42
02/18/19 22:00
108-86-1
Bromochloromethane
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
74-97-5
Bromodichloromethane
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
75-27-4
Bromoform
ND
ug/kg
5.0
2.3
1
02/18/19 10:42
02/18/19 22:00
75-25-2
Bromomethane
ND
ug/kg
9.9
2.5
1
02/18/19 10:42
02/18/19 22:00
74-83-9
2-Butanone (MEK)
ND
ug/kg
99.5
2.9
1
02/18/19 10:42
02/18/19 22:00
78-93-3
n-Butylbenzene
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
104-51-8
sec-Butylbenzene
ND
ug/kg
5.0
1.6
1
02/18/19 10:42
02/18/19 22:00
135-98-8
tert-Butyl benzene
ND
ug/kg
5.0
2.0
1
02/18/19 10:42
02/18/19 22:00
98-06-6
Carbon tetrachloride
ND
ug/kg
5.0
2.6
1
02/18/19 10:42
02/18/19 22:00
56-23-5
Chlorobenzene
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-8 Lab ID: 92418026007 Collected: 02/15/19 15:15 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
9.9
2.4
1
02/18/19 10:42
02/18/19 22:00
75-00-3
Chloroform
ND
ug/kg
5.0
1.6
1
02/18/19 10:42
02/18/19 22:00
67-66-3
Chloromethane
ND
ug/kg
9.9
2.4
1
02/18/19 10:42
02/18/19 22:00
74-87-3
2-Chlorotoluene
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
95-49-8
4-Chlorotoluene
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.0
3.6
1
02/18/19 10:42
02/18/19 22:00
96-12-8
Dibromochloromethane
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
106-93-4
Dibromomethane
ND
ug/kg
5.0
2.5
1
02/18/19 10:42
02/18/19 22:00
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.0
2.0
1
02/18/19 10:42
02/18/19 22:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
106-46-7
Dichlorodifluoromethane
ND
ug/kg
9.9
3.6
1
02/18/19 10:42
02/18/19 22:00
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.0
1.5
1
02/18/19 10:42
02/18/19 22:00
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.0
2.2
1
02/18/19 10:42
02/18/19 22:00
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.0
1.4
1
02/18/19 10:42
02/18/19 22:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.0
1.5
1
02/18/19 10:42
02/18/19 22:00
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.0
1.5
1
02/18/19 10:42
02/18/19 22:00
10061-02-6
Diisopropyl ether
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
108-20-3
Ethylbenzene
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.0
2.0
1
02/18/19 10:42
02/18/19 22:00
87-68-3
2-Hexanone
ND
ug/kg
49.7
3.9
1
02/18/19 10:42
02/18/19 22:00
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
99-87-6
Methylene Chloride
ND
ug/kg
19.9
3.0
1
02/18/19 10:42
02/18/19 22:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
49.7
3.7
1
02/18/19 10:42
02/18/19 22:00
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.0
1.5
1
02/18/19 10:42
02/18/19 22:00
1634-04-4
Naphthalene
ND
ug/kg
5.0
1.2
1
02/18/19 10:42
02/18/19 22:00
91-20-3
n-Propylbenzene
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
103-65-1
Styrene
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.0
2.1
1
02/18/19 10:42
02/18/19 22:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
79-34-5
Tetrachloroethene
ND
ug/kg
5.0
1.7
1
02/18/19 10:42
02/18/19 22:00
127-18-4
Toluene
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.0
2.2
1
02/18/19 10:42
02/18/19 22:00
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.0
1.6
1
02/18/19 10:42
02/18/19 22:00
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.0
2.1
1
02/18/19 10:42
02/18/19 22:00
79-00-5
Trichloroethene
ND
ug/kg
5.0
2.1
1
02/18/19 10:42
02/18/19 22:00
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418026
Sample: UST-8 Lab ID: 92418026007 Collected: 02/15/19 15:15 Received: 02/15/19 17:45 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/21 /2019 04:18 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
5.0
2.2
1
02/18/19 10:42
02/18/19 22:00
75-69-4
ND
ug/kg
5.0
1.6
1
02/18/19 10:42
02/18/19 22:00
96-18-4
ND
ug/kg
5.0
2.0
1
02/18/19 10:42
02/18/19 22:00
95-63-6
ND
ug/kg
5.0
1.8
1
02/18/19 10:42
02/18/19 22:00
108-67-8
ND
ug/kg
49.7
8.8
1
02/18/19 10:42
02/18/19 22:00
108-05-4
ND
ug/kg
9.9
1.8
1
02/18/19 10:42
02/18/19 22:00
75-01-4
ND
ug/kg
9.9
3.6
1
02/18/19 10:42
02/18/19 22:00
1330-20-7
ND
ug/kg
9.9
3.6
1
02/18/19 10:42
02/18/19 22:00
179601-23-1
ND
ug/kg
5.0
1.9
1
02/18/19 10:42
02/18/19 22:00
95-47-6
120
%
70-130
1
02/18/19 10:42
02/18/19 22:00
2037-26-5
106
%
70-130
1
02/18/19 10:42
02/18/19 22:00
460-00-4
75
%
70-132
1
02/18/19 10:42
02/18/19 22:00
17060-07-0
Analytical Method: ASTM D2974-87
15.2 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
02/16/19 18:57
Page 32 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
QC Batch: 458674 Analysis Method: EPA 8260B
QC Batch Method: EPA 5035A Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92418026001
METHOD BLANK: 2500319
Associated Lab Samples: 92418026001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.3
2.2
02/18/19 12:23
1,1,1-Trichloroethane
ug/kg
ND
5.3
1.9
02/18/19 12:23
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.3
2.0
02/18/19 12:23
1,1,2-Trichloroethane
ug/kg
ND
5.3
2.2
02/18/19 12:23
1,1-Dichloroethane
ug/kg
ND
5.3
1.6
02/18/19 12:23
1,1-Dichloroethene
ug/kg
ND
5.3
1.9
02/18/19 12:23
1,1-Dichloropropene
ug/kg
ND
5.3
1.6
02/18/19 12:23
1,2,3-Trichlorobenzene
ug/kg
ND
5.3
2.3
02/18/19 12:23
1,2,3-Trichloropropane
ug/kg
ND
5.3
1.7
02/18/19 12:23
1,2,4-Trichlorobenzene
ug/kg
ND
5.3
1.7
02/18/19 12:23
1,2,4-Trimethylbenzene
ug/kg
ND
5.3
2.1
02/18/19 12:23
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.3
3.8
02/18/19 12:23
1,2-Dibromoethane (EDB)
ug/kg
ND
5.3
1.9
02/18/19 12:23
1,2-Dichlorobenzene
ug/kg
ND
5.3
2.0
02/18/19 12:23
1,2-Dichloroethane
ug/kg
ND
5.3
2.3
02/18/19 12:23
1,2-Dichloropropane
ug/kg
ND
5.3
1.8
02/18/19 12:23
1,3,5-Trimethylbenzene
ug/kg
ND
5.3
1.9
02/18/19 12:23
1,3-Dichlorobenzene
ug/kg
ND
5.3
2.1
02/18/19 12:23
1,3-Dichloropropane
ug/kg
ND
5.3
2.0
02/18/19 12:23
1,4-Dichlorobenzene
ug/kg
ND
5.3
1.8
02/18/19 12:23
2,2-Dichloropropane
ug/kg
ND
5.3
1.8
02/18/19 12:23
2-Butanone (MEK)
ug/kg
ND
106
3.1
02/18/19 12:23
2-Chlorotoluene
ug/kg
ND
5.3
1.8
02/18/19 12:23
2-Hexanone
ug/kg
ND
53.0
4.1
02/18/19 12:23
4-Chlorotoluene
ug/kg
ND
5.3
1.9
02/18/19 12:23
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
53.0
3.9
02/18/19 12:23
Acetone
ug/kg
ND
106
10.6
02/18/19 12:23
Benzene
ug/kg
ND
5.3
1.7
02/18/19 12:23
Bromobenzene
ug/kg
ND
5.3
2.1
02/18/19 12:23
Bromochloromethane
ug/kg
ND
5.3
1.8
02/18/19 12:23
Bromodichloromethane
ug/kg
ND
5.3
2.0
02/18/19 12:23
Bromoform
ug/kg
ND
5.3
2.4
02/18/19 12:23
Bromomethane
ug/kg
ND
10.6
2.6
02/18/19 12:23
Carbon tetrachloride
ug/kg
ND
5.3
2.8
02/18/19 12:23
Chlorobenzene
ug/kg
ND
5.3
2.0
02/18/19 12:23
Chloroethane
ug/kg
ND
10.6
2.5
02/18/19 12:23
Chloroform
ug/kg
ND
5.3
1.7
02/18/19 12:23
Chloromethane
ug/kg
ND
10.6
2.5
02/18/19 12:23
cis-1,2-Dichloroethene
ug/kg
ND
5.3
1.5
02/18/19 12:23
cis-1,3-Dichloropropene
ug/kg
ND
5.3
1.9
02/18/19 12:23
Dibromochloromethane
ug/kg
ND
5.3
1.9
02/18/19 12:23
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
METHOD BLANK: 2500319
Associated Lab Samples: 92418026001
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromomethane
ug/kg
ND
5.3
2.6
02/18/19 12:23
Dichlorodifluoromethane
ug/kg
ND
10.6
3.8
02/18/19 12:23
Diisopropyl ether
ug/kg
ND
5.3
1.8
02/18/19 12:23
Ethylbenzene
ug/kg
ND
5.3
1.9
02/18/19 12:23
Hexachloro-1,3-butadiene
ug/kg
ND
5.3
2.1
02/18/19 12:23
Isopropylbenzene (Cumene)
ug/kg
ND
5.3
2.0
02/18/19 12:23
m&p-Xylene
ug/kg
ND
10.6
3.8
02/18/19 12:23
Methyl-tert-butyl ether
ug/kg
ND
5.3
1.6
02/18/19 12:23
Methylene Chloride
ug/kg
ND
21.2
3.2
02/18/19 12:23
n-Butylbenzene
ug/kg
ND
5.3
1.9
02/18/19 12:23
n-Propylbenzene
ug/kg
ND
5.3
1.8
02/18/19 12:23
Naphthalene
ug/kg
ND
5.3
1.3
02/18/19 12:23
o-Xylene
ug/kg
ND
5.3
2.0
02/18/19 12:23
p-Isopropyltoluene
ug/kg
ND
5.3
1.8
02/18/19 12:23
sec-Butylbenzene
ug/kg
ND
5.3
1.7
02/18/19 12:23
Styrene
ug/kg
ND
5.3
1.9
02/18/19 12:23
tert-Butyl benzene
ug/kg
ND
5.3
2.1
02/18/19 12:23
Tetrachloroethene
ug/kg
ND
5.3
1.8
02/18/19 12:23
Toluene
ug/kg
ND
5.3
1.9
02/18/19 12:23
trans-1,2-Dichloroethene
ug/kg
ND
5.3
2.0
02/18/19 12:23
trans- 1,3-Dichloropropene
ug/kg
ND
5.3
1.6
02/18/19 12:23
Trichloroethene
ug/kg
ND
5.3
2.2
02/18/19 12:23
Trichlorofluoromethane
ug/kg
ND
5.3
2.3
02/18/19 12:23
Vinyl acetate
ug/kg
ND
53.0
9.3
02/18/19 12:23
Vinyl chloride
ug/kg
ND
10.6
1.9
02/18/19 12:23
Xylene (Total)
ug/kg
ND
10.6
3.8
02/18/19 12:23
1,2-Dichloroethane-d4 (S)
%
75
70-132
02/18/19 12:23
4-Bromofluorobenzene (S)
%
107
70-130
02/18/19 12:23
Toluene-d8 (S)
%
115
70-130
02/18/19 12:23
Qualifiers
LABORATORY CONTROL SAMPLE:
2500320
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
51.8
54.1
105
70-130
1,1,1-Trichloroethane
ug/kg
51.8
54.7
106
70-130
1,1,2,2-Tetrachloroethane
ug/kg
51.8
45.7
88
55-130
1,1,2-Trichloroethane
ug/kg
51.8
54.2
105
70-130
1,1-Dichloroethane
ug/kg
51.8
52.6
102
68-130
1,1-Dichloroethene
ug/kg
51.8
52.1
101
70-130
1,1-Dichloropropene
ug/kg
51.8
47.6
92
70-130
1,2,3-Trichlorobenzene
ug/kg
51.8
52.1
101
70-130
1,2,3-Trichloropropane
ug/kg
51.8
54.9
106
70-130
1,2,4-Trichlorobenzene
ug/kg
51.8
51.6
100
70-130
1,2,4-Trimethylbenzene
ug/kg
51.8
52.8
102
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
LABORATORY CONTROL SAMPLE:
Parameter
2500320
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/kg
51.8
52.2
101
57-141
1,2-Dibromoethane (EDB)
ug/kg
51.8
56.6
109
70-130
1,2-Dichlorobenzene
ug/kg
51.8
52.9
102
70-130
1,2-Dichloroethane
ug/kg
51.8
53.6
104
70-130
1,2-Dichloropropane
ug/kg
51.8
56.3
109
70-130
1,3,5-Trimethylbenzene
ug/kg
51.8
53.4
103
70-130
1,3-Dichlorobenzene
ug/kg
51.8
53.1
103
70-130
1,3-Dichloropropane
ug/kg
51.8
51.0
99
70-130
1,4-Dichlorobenzene
ug/kg
51.8
52.0
100
70-130
2,2-Dichloropropane
ug/kg
51.8
54.6
106
70-130
2-Butanone (MEK)
ug/kg
104
93.6J
90
60-130
2-Chlorotoluene
ug/kg
51.8
53.2
103
70-130
2-Hexanone
ug/kg
104
113
110
70-132
4-Chlorotoluene
ug/kg
51.8
53.4
103
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
104
104
101
69-130
Acetone
ug/kg
104
103J
99
49-148
Benzene
ug/kg
51.8
56.0
108
70-130
Bromobenzene
ug/kg
51.8
51.8
100
70-130
Bromochloromethane
ug/kg
51.8
51.9
100
70-130
Bromodichloromethane
ug/kg
51.8
56.7
109
70-130
Bromoform
ug/kg
51.8
55.1
106
68-136
Bromomethane
ug/kg
51.8
53.5
103
60-140
Carbon tetrachloride
ug/kg
51.8
54.5
105
70-130
Chlorobenzene
ug/kg
51.8
53.3
103
70-130
Chloroethane
ug/kg
51.8
53.9
104
51-147
Chloroform
ug/kg
51.8
49.1
95
70-130
Chloromethane
ug/kg
51.8
48.4
94
48-130
cis-1,2-Dichloroethene
ug/kg
51.8
52.0
100
70-130
cis-1,3-Dichloropropene
ug/kg
51.8
51.9
100
70-130
Dibromochloromethane
ug/kg
51.8
50.5
98
70-130
Dibromomethane
ug/kg
51.8
52.1
101
70-130
Dichlorodifluoromethane
ug/kg
51.8
49.2
95
49-130
Diisopropyl ether
ug/kg
51.8
47.6
92
66-130
Ethylbenzene
ug/kg
51.8
53.0
102
70-130
Hexachloro-1,3-butadiene
ug/kg
51.8
49.6
96
70-130
Isopropylbenzene (Cumene)
ug/kg
51.8
53.3
103
70-130
m&p-Xylene
ug/kg
104
105
101
70-130
Methyl-tert-butyl ether
ug/kg
51.8
46.4
90
70-130
Methylene Chloride
ug/kg
51.8
49.1
95
50-137
n-Butylbenzene
ug/kg
51.8
53.0
102
70-130
n-Propylbenzene
ug/kg
51.8
53.6
104
70-130
Naphthalene
ug/kg
51.8
54.0
104
70-131
o-Xylene
ug/kg
51.8
53.6
104
70-130
p-Isopropyltoluene
ug/kg
51.8
52.8
102
70-130
sec-Butylbenzene
ug/kg
51.8
54.0
104
70-130
Styrene
ug/kg
51.8
53.3
103
70-130
tert-Butyl benzene
ug/kg
51.8
52.9
102
69-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
LABORATORY CONTROL SAMPLE:
2500320
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Tetrachloroethene
ug/kg
51.8
33.4
65
56-130
Toluene
ug/kg
51.8
50.9
98
70-130
trans-1,2-Dichloroethene
ug/kg
51.8
53.5
103
70-130
trans- 1,3-Dichloropropene
ug/kg
51.8
51.5
99
70-130
Trichloroethene
ug/kg
51.8
55.4
107
70-141
Trichlorofluoromethane
ug/kg
51.8
49.4
95
67-130
Vinyl acetate
ug/kg
104
73.4
71
10-136
Vinyl chloride
ug/kg
51.8
49.6
96
67-130
Xylene (Total)
ug/kg
155
158
102
70-130
1,2-Dichloroethane-d4 (S)
%
99
70-132
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE SAMPLE:
2500322
35448215004
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
0.0040U mg/kg
21.8
22.3
103
52-133
1,1,1-Trichloroethane
ug/kg
0.00341-1 mg/kg
21.8
24.2
111
49-137
1,1,2,2-Tetrachloroethane
ug/kg
0.00361-1 mg/kg
21.8
24.1
111
39-150
1,1,2-Trichloroethane
ug/kg
0.0040U mg/kg
21.8
22.3
103
48-140
1,1-Dichloroethane
ug/kg
0.00291-1 mg/kg
21.8
23.6
109
46-135
1,1-Dichloroethene
ug/kg
0.00341-1 mg/kg
21.8
25.1
116
38-149
1,1-Dichloropropene
ug/kg
0.00291-1 mg/kg
21.8
21.2
98
41-140
1,2,3-Trichlorobenzene
ug/kg
0.00421-1 mg/kg
21.8
22.1
102
10-158
1,2,3-Trichloropropane
ug/kg
0.0030U mg/kg
21.8
23.2
107
33-157
1,2,4-Trichlorobenzene
ug/kg
0.0030U mg/kg
21.8
21.6
99
10-155
1,2,4-Trimethylbenzene
ug/kg
0.020 mg/kg
21.8
22.2
11
24-154 M1
1,2-Dibromo-3-chloropropane
ug/kg
0.00691-1 mg/kg
21.8
22.6
104
33-158
1,2-Dibromoethane (EDB)
ug/kg
0.00341-1 mg/kg
21.8
20.8
96
40-136
1,2-Dichlorobenzene
ug/kg
0.00361-1 mg/kg
21.8
22.1
102
27-146
1,2-Dichloroethane
ug/kg
0.00421-1 mg/kg
21.8
23.1
106
49-140
1,2-Dichloropropane
ug/kg
0.00321-1 mg/kg
21.8
23.1
107
44-143
1,3,5-Trimethylbenzene
ug/kg
0.0071J mg/kg
21.8
22.5
71
40-144
1,3-Dichlorobenzene
ug/kg
0.00381-1 mg/kg
21.8
23.1
107
33-140
1,3-Dichloropropane
ug/kg
0.00361-1 mg/kg
21.8
21.8
100
47-147
1,4-Dichlorobenzene
ug/kg
0.00321-1 mg/kg
21.8
23.1
106
35-139
2,2-Dichloropropane
ug/kg
0.00321-1 mg/kg
21.8
23.7
109
41-140
2-Butanone (MEK)
ug/kg
0.023J mg/kg
43.4
44.6J
51
10-181
2-Chlorotoluene
ug/kg
0.00321-1 mg/kg
21.8
23.0
106
38-147
2-Hexanone
ug/kg
0.00741-1 mg/kg
43.4
46.8J
108
18-169
4-Chlorotoluene
ug/kg
0.00341-1 mg/kg
21.8
22.6
104
36-145
4-Methyl-2-pentanone (MIBK)
ug/kg
0.0070U mg/kg
43.4
47.9J
110
16-175
Acetone
ug/kg
0.077J mg/kg
43.4
54.3J
-52
10-200 M1
Benzene
ug/kg
0.0030U mg/kg
21.8
23.4
108
46-136
Bromobenzene
ug/kg
0.00381-1 mg/kg
21.8
21.9
101
38-149
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
MATRIX SPIKE SAMPLE:
2500322
35448215004
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/kg
0.0032U mg/kg
21.8
23.7
109
44-142
Bromodichloromethane
ug/kg
0.0036U mg/kg
21.8
23.2
107
41-140
Bromoform
ug/kg
0.0044U mg/kg
21.8
22.0
101
34-145
Bromomethane
ug/kg
0.0048U mg/kg
21.8
24.8
114
14-162
Carbon tetrachloride
ug/kg
0.0050U mg/kg
21.8
23.6
109
44-141
Chlorobenzene
ug/kg
0.0036U mg/kg
21.8
23.0
106
39-141
Chloroethane
ug/kg
0.0046U mg/kg
21.8
26.1
120
10-182
Chloroform
ug/kg
0.0030U mg/kg
21.8
22.4
103
45-140
Chloromethane
ug/kg
0.0046U mg/kg
21.8
22.0
101
19-149
cis-1,2-Dichloroethene
ug/kg
0.0027U mg/kg
21.8
23.2
107
38-150
cis-1,3-Dichloropropene
ug/kg
0.0034U mg/kg
21.8
20.7
95
30-144
Dibromochloromethane
ug/kg
0.0034U mg/kg
21.8
21.0
97
36-145
Dibromomethane
ug/kg
0.0048U mg/kg
21.8
23.3
108
41-145
Dichlorodifluoromethane
ug/kg
0.0069U mg/kg
21.8
23.1
107
16-146
Diisopropyl ether
ug/kg
0.0032U mg/kg
21.8
21.4
98
41-143
Ethylbenzene
ug/kg
0.0034U mg/kg
21.8
24.0
110
35-144
Hexachloro-1,3-butadiene
ug/kg
0.0038U mg/kg
21.8
21.4
99
10-160
Isopropylbenzene (Cumene)
ug/kg
0.0036U mg/kg
21.8
24.1
111
30-152
m&p-Xylene
ug/kg
0.0069U mg/kg
43.4
47.2
97
33-145
Methyl-tert-butyl ether
ug/kg
0.0029U mg/kg
21.8
21.4
98
49-140
Methylene Chloride
ug/kg
0.0057U mg/kg
21.8
23.7
109
10-174
n-Butylbenzene
ug/kg
0.0037J mg/kg
21.8
23.3
90
10-160
n-Propylbenzene
ug/kg
0.0032U mg/kg
21.8
23.6
98
24-159
Naphthalene
ug/kg
0.0073J mg/kg
21.8
23.3
74
10-171
o-Xylene
ug/kg
0.0036U mg/kg
21.8
23.8
109
31-150
p-Isopropyltoluene
ug/kg
0.0066J mg/kg
21.8
23.6
78
21-154
sec-Butylbenzene
ug/kg
0.0030U mg/kg
21.8
23.4
96
19-159
Styrene
ug/kg
0.0034U mg/kg
21.8
22.8
105
15-152
tert-Butyl benzene
ug/kg
0.0038U mg/kg
21.8
22.7
105
31-141
Tetrachloroethene
ug/kg
0.037 mg/kg
21.8
14.4
-105
19-141 M1
Toluene
ug/kg
0.0034U mg/kg
21.8
23.8
110
31-146
trans-1,2-Dichloroethene
ug/kg
0.0036U mg/kg
21.8
23.4
108
28-157
trans- 1,3-Dichloropropene
ug/kg
0.0029U mg/kg
21.8
20.5
94
25-146
Trichloroethene
ug/kg
0.0040U mg/kg
21.8
21.1
97
34-149
Trichlorofluoromethane
ug/kg
0.0042U mg/kg
21.8
23.3
107
10-167
Vinyl acetate
ug/kg
0.0171-1 mg/kg
43.4
62.4
144
10-200
Vinyl chloride
ug/kg
0.0034U mg/kg
21.8
23.5
108
36-155
Xylene (Total)
ug/kg
0.0069U mg/kg
65.2
71.0
109
29-148
1,2-Dichloroethane-d4 (S)
%
99
70-132
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
SAMPLE DUPLICATE: 2500321
35448215001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
0.0022U
ND
30
mg/kg
1,1,1-Trichloroethane
ug/kg
0.0019U
ND
30
mg/kg
1,1,2,2-Tetrachloroethane
ug/kg
0.0020U
ND
30
mg/kg
1,1,2-Trichloroethane
ug/kg
0.0022U
ND
30
mg/kg
1,1-Dichloroethane
ug/kg
0.0016U
ND
30
mg/kg
1,1-Dichloroethene
ug/kg
0.0019U
ND
30
mg/kg
1,1-Dichloropropene
ug/kg
0.0016U
ND
30
mg/kg
1,2,3-Trichlorobenzene
ug/kg
0.0023U
ND
30
mg/kg
1,2,3-Trichloropropane
ug/kg
0.0017U
ND
30
mg/kg
1,2,4-Trichlorobenzene
ug/kg
0.0017U
ND
30
mg/kg
1,2,4-Trimethylbenzene
ug/kg
0.0021U
ND
30
mg/kg
1,2-Dibromo-3-chloropropane
ug/kg
0.0037U
ND
30
mg/kg
1,2-Dibromoethane (EDB)
ug/kg
0.0019U
ND
30
mg/kg
1,2-Dichlorobenzene
ug/kg
0.0020U
ND
30
mg/kg
1,2-Dichloroethane
ug/kg
0.0023U
ND
30
mg/kg
1,2-Dichloropropane
ug/kg
0.0018U
ND
30
mg/kg
1,3,5-Trimethylbenzene
ug/kg
0.0019U
ND
30
mg/kg
1,3-Dichlorobenzene
ug/kg
0.0021U
ND
30
mg/kg
1,3-Dichloropropane
ug/kg
0.0020U
ND
30
mg/kg
1,4-Dichlorobenzene
ug/kg
0.0018U
ND
30
mg/kg
2,2-Dichloropropane
ug/kg
0.0018U
ND
30
mg/kg
2-Butanone (MEK)
ug/kg
0.0030U
ND
30
mg/kg
2-Chlorotoluene
ug/kg
0.0018U
ND
30
mg/kg
2-Hexanone
ug/kg
0.0040U
ND
30
mg/kg
4-Chlorotoluene
ug/kg
0.0019U
ND
30
mg/kg
4-Methyl-2-pentanone (MIBK)
ug/kg
0.0038U
ND
30
mg/kg
Acetone
ug/kg
0.010U mg/kg
ND
30
Benzene
ug/kg
0.0017U
ND
30
mg/kg
Results presented on this
page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
SAMPLE DUPLICATE: 2500321
Parameter
Units
35448215001
Result
Dup
Result
Bromobenzene
ug/kg
0.0021U
ND
mg/kg
Bromochloromethane
ug/kg
0.0018U
ND
mg/kg
Bromodichloromethane
ug/kg
0.0020U
ND
mg/kg
Bromoform
ug/kg
0.0024U
ND
mg/kg
Bromomethane
ug/kg
0.0026U
ND
mg/kg
Carbon tetrachloride
ug/kg
0.0027U
ND
mg/kg
Chlorobenzene
ug/kg
0.0020U
ND
mg/kg
Chloroethane
ug/kg
0.0025U
ND
mg/kg
Chloroform
ug/kg
0.0017U
ND
mg/kg
Chloromethane
ug/kg
0.0025U
ND
mg/kg
cis-1,2-Dichloroethene
ug/kg
0.0014U
ND
mg/kg
cis-1,3-Dichloropropene
ug/kg
0.0019U
ND
mg/kg
Dibromochloromethane
ug/kg
0.0019U
ND
mg/kg
Dibromomethane
ug/kg
0.0026U
ND
mg/kg
Dichlorodifluoromethane
ug/kg
0.0037U
ND
mg/kg
Diisopropyl ether
ug/kg
0.0018U
ND
mg/kg
Ethylbenzene
ug/kg
0.0019U
ND
mg/kg
Hexachloro-1,3-butadiene
ug/kg
0.0021U
ND
mg/kg
Isopropylbenzene (Cumene)
ug/kg
0.0020U
ND
mg/kg
m&p-Xylene
ug/kg
0.0037U
ND
mg/kg
Methyl-tert-butyl ether
ug/kg
0.0016U
ND
mg/kg
Methylene Chloride
ug/kg
0.0031U
ND
mg/kg
n-Butylbenzene
ug/kg
0.0019U
ND
mg/kg
n-Propylbenzene
ug/kg
0.0018U
ND
mg/kg
Naphthalene
ug/kg
0.0012U
ND
mg/kg
o-Xylene
ug/kg
0.0020U
ND
mg/kg
p-Isopropyltoluene
ug/kg
0.0018U
ND
mg/kg
Max
RPD RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC.
Page 39 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
SAMPLE DUPLICATE: 2500321
Parameter
Units
35448215001
Result
Dup
Result
sec-Butylbenzene
ug/kg
0.0017U
ND
mg/kg
Styrene
ug/kg
0.0019U
ND
mg/kg
tert-Butyl benzene
ug/kg
0.0021U
ND
mg/kg
Tetrachloroethene
ug/kg
0.0038J
3.1 J
mg/kg
Toluene
ug/kg
0.0019U
ND
mg/kg
trans-1,2-Dichloroethene
ug/kg
0.0020U
ND
mg/kg
trans- 1,3-Dichloropropene
ug/kg
0.0016U
ND
mg/kg
Trichloroethene
ug/kg
0.0022U
ND
mg/kg
Trichlorofluoromethane
ug/kg
0.0023U
ND
mg/kg
Vinyl acetate
ug/kg
0.0091U
ND
mg/kg
Vinyl chloride
ug/kg
0.0019U
ND
mg/kg
Xylene (Total)
ug/kg
0.0037U
ND
mg/kg
1,2-Dichloroethane-d4 (S)
%
90
81
4-Bromofluorobenzene (S)
%
112
107
Toluene-d8 (S)
%
118
112
Max
RPD RPD Qualifiers
1
7
7
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
QC Batch: 458676 Analysis Method: EPA 8260B
QC Batch Method: EPA 5035A Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92418026002, 92418026003, 92418026004, 92418026005, 92418026006, 92418026007
METHOD BLANK: 2500328 Matrix: Solid
Associated Lab Samples: 92418026002, 92418026003, 92418026004, 92418026005, 92418026006, 92418026007
Blank Reporting
Parameter Units Result Limit MDL Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.2
2.2
02/18/19 12:04
1,1,1-Trichloroethane
ug/kg
ND
5.2
1.9
02/18/19 12:04
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.2
2.0
02/18/19 12:04
1,1,2-Trichloroethane
ug/kg
ND
5.2
2.2
02/18/19 12:04
1,1-Dichloroethane
ug/kg
ND
5.2
1.6
02/18/19 12:04
1,1-Dichloroethene
ug/kg
ND
5.2
1.9
02/18/19 12:04
1,1-Dichloropropene
ug/kg
ND
5.2
1.6
02/18/19 12:04
1,2,3-Trichlorobenzene
ug/kg
ND
5.2
2.3
02/18/19 12:04
1,2,3-Trichloropropane
ug/kg
ND
5.2
1.7
02/18/19 12:04
1,2,4-Trichlorobenzene
ug/kg
ND
5.2
1.7
02/18/19 12:04
1,2,4-Trimethylbenzene
ug/kg
ND
5.2
2.1
02/18/19 12:04
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.2
3.7
02/18/19 12:04
1,2-Dibromoethane (EDB)
ug/kg
ND
5.2
1.9
02/18/19 12:04
1,2-Dichlorobenzene
ug/kg
ND
5.2
2.0
02/18/19 12:04
1,2-Dichloroethane
ug/kg
ND
5.2
2.3
02/18/19 12:04
1,2-Dichloropropane
ug/kg
ND
5.2
1.8
02/18/19 12:04
1,3,5-Trimethylbenzene
ug/kg
ND
5.2
1.9
02/18/19 12:04
1,3-Dichlorobenzene
ug/kg
ND
5.2
2.1
02/18/19 12:04
1,3-Dichloropropane
ug/kg
ND
5.2
2.0
02/18/19 12:04
1,4-Dichlorobenzene
ug/kg
ND
5.2
1.8
02/18/19 12:04
2,2-Dichloropropane
ug/kg
ND
5.2
1.8
02/18/19 12:04
2-Butanone (MEK)
ug/kg
ND
104
3.0
02/18/19 12:04
2-Chlorotoluene
ug/kg
ND
5.2
1.8
02/18/19 12:04
2-Hexanone
ug/kg
ND
51.9
4.0
02/18/19 12:04
4-Chlorotoluene
ug/kg
ND
5.2
1.9
02/18/19 12:04
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
51.9
3.8
02/18/19 12:04
Acetone
ug/kg
ND
104
10.4
02/18/19 12:04
Benzene
ug/kg
ND
5.2
1.7
02/18/19 12:04
Bromobenzene
ug/kg
ND
5.2
2.1
02/18/19 12:04
Bromochloromethane
ug/kg
ND
5.2
1.8
02/18/19 12:04
Bromodichloromethane
ug/kg
ND
5.2
2.0
02/18/19 12:04
Bromoform
ug/kg
ND
5.2
2.4
02/18/19 12:04
Bromomethane
ug/kg
ND
10.4
2.6
02/18/19 12:04
Carbon tetrachloride
ug/kg
ND
5.2
2.7
02/18/19 12:04
Chlorobenzene
ug/kg
ND
5.2
2.0
02/18/19 12:04
Chloroethane
ug/kg
ND
10.4
2.5
02/18/19 12:04
Chloroform
ug/kg
ND
5.2
1.7
02/18/19 12:04
Chloromethane
ug/kg
ND
10.4
2.5
02/18/19 12:04
cis-1,2-Dichloroethene
ug/kg
ND
5.2
1.5
02/18/19 12:04
cis-1,3-Dichloropropene
ug/kg
ND
5.2
1.9
02/18/19 12:04
Dibromochloromethane
ug/kg
ND
5.2
1.9
02/18/19 12:04
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
METHOD BLANK: 2500328 Matrix: Solid
Associated Lab Samples: 92418026002, 92418026003, 92418026004, 92418026005, 92418026006, 92418026007
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Dibromomethane
ug/kg
ND
5.2
2.6
02/18/19 12:04
Dichlorodifluoromethane
ug/kg
ND
10.4
3.7
02/18/19 12:04
Diisopropyl ether
ug/kg
ND
5.2
1.8
02/18/19 12:04
Ethylbenzene
ug/kg
ND
5.2
1.9
02/18/19 12:04
Hexachloro-1,3-butadiene
ug/kg
ND
5.2
2.1
02/18/19 12:04
Isopropylbenzene (Cumene)
ug/kg
ND
5.2
2.0
02/18/19 12:04
m&p-Xylene
ug/kg
ND
10.4
3.7
02/18/19 12:04
Methyl-tert-butyl ether
ug/kg
ND
5.2
1.6
02/18/19 12:04
Methylene Chloride
ug/kg
ND
20.7
3.1
02/18/19 12:04
n-Butylbenzene
ug/kg
ND
5.2
1.9
02/18/19 12:04
n-Propylbenzene
ug/kg
ND
5.2
1.8
02/18/19 12:04
Naphthalene
ug/kg
ND
5.2
1.2
02/18/19 12:04
o-Xylene
ug/kg
ND
5.2
2.0
02/18/19 12:04
p-Isopropyltoluene
ug/kg
ND
5.2
1.8
02/18/19 12:04
sec-Butylbenzene
ug/kg
ND
5.2
1.7
02/18/19 12:04
Styrene
ug/kg
ND
5.2
1.9
02/18/19 12:04
tert-Butyl benzene
ug/kg
ND
5.2
2.1
02/18/19 12:04
Tetrachloroethene
ug/kg
ND
5.2
1.8
02/18/19 12:04
Toluene
ug/kg
ND
5.2
1.9
02/18/19 12:04
trans-1,2-Dichloroethene
ug/kg
ND
5.2
2.0
02/18/19 12:04
trans- 1,3-Dichloropropene
ug/kg
ND
5.2
1.6
02/18/19 12:04
Trichloroethene
ug/kg
ND
5.2
2.2
02/18/19 12:04
Trichlorofluoromethane
ug/kg
ND
5.2
2.3
02/18/19 12:04
Vinyl acetate
ug/kg
ND
51.9
9.1
02/18/19 12:04
Vinyl chloride
ug/kg
ND
10.4
1.9
02/18/19 12:04
Xylene (Total)
ug/kg
ND
10.4
3.7
02/18/19 12:04
1,2-Dichloroethane-d4 (S)
%
75
70-132
02/18/19 12:04
4-Bromofluorobenzene (S)
%
112
70-130
02/18/19 12:04
Toluene-d8 (S)
%
114
70-130
02/18/19 12:04
Qualifiers
LABORATORY CONTROL SAMPLE:
2500329
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50.9
53.8
106
70-130
1,1,1-Trichloroethane
ug/kg
50.9
54.1
106
70-130
1,1,2,2-Tetrachloroethane
ug/kg
50.9
49.5
97
55-130
1,1,2-Trichloroethane
ug/kg
50.9
53.6
105
70-130
1,1-Dichloroethane
ug/kg
50.9
49.9
98
68-130
1,1-Dichloroethene
ug/kg
50.9
50.4
99
70-130
1,1-Dichloropropene
ug/kg
50.9
47.9
94
70-130
1,2,3-Trichlorobenzene
ug/kg
50.9
50.8
100
70-130
1,2,3-Trichloropropane
ug/kg
50.9
55.2
108
70-130
1,2,4-Trichlorobenzene
ug/kg
50.9
49.2
97
70-130
1,2,4-Trimethylbenzene
ug/kg
50.9
51.7
102
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
LABORATORY CONTROL SAMPLE:
Parameter
2500329
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/kg
50.9
52.2
103
57-141
1,2-Dibromoethane (EDB)
ug/kg
50.9
57.1
112
70-130
1,2-Dichlorobenzene
ug/kg
50.9
50.9
100
70-130
1,2-Dichloroethane
ug/kg
50.9
52.4
103
70-130
1,2-Dichloropropane
ug/kg
50.9
55.2
109
70-130
1,3,5-Trimethylbenzene
ug/kg
50.9
52.5
103
70-130
1,3-Dichlorobenzene
ug/kg
50.9
50.8
100
70-130
1,3-Dichloropropane
ug/kg
50.9
52.6
103
70-130
1,4-Dichlorobenzene
ug/kg
50.9
50.2
99
70-130
2,2-Dichloropropane
ug/kg
50.9
55.0
108
70-130
2-Butanone (MEK)
ug/kg
102
102J
100
60-130
2-Chlorotoluene
ug/kg
50.9
52.1
102
70-130
2-Hexanone
ug/kg
102
121
118
70-132
4-Chlorotoluene
ug/kg
50.9
52.1
102
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
102
109
107
69-130
Acetone
ug/kg
102
97.9J
96
49-148
Benzene
ug/kg
50.9
53.9
106
70-130
Bromobenzene
ug/kg
50.9
50.8
100
70-130
Bromochloromethane
ug/kg
50.9
50.0
98
70-130
Bromodichloromethane
ug/kg
50.9
55.1
108
70-130
Bromoform
ug/kg
50.9
58.4
115
68-136
Bromomethane
ug/kg
50.9
50.5
99
60-140
Carbon tetrachloride
ug/kg
50.9
53.7
105
70-130
Chlorobenzene
ug/kg
50.9
53.2
104
70-130
Chloroethane
ug/kg
50.9
51.2
101
51-147
Chloroform
ug/kg
50.9
48.4
95
70-130
Chloromethane
ug/kg
50.9
45.7
90
48-130
cis-1,2-Dichloroethene
ug/kg
50.9
50.4
99
70-130
cis-1,3-Dichloropropene
ug/kg
50.9
51.4
101
70-130
Dibromochloromethane
ug/kg
50.9
51.4
101
70-130
Dibromomethane
ug/kg
50.9
50.1
98
70-130
Dichlorodifluoromethane
ug/kg
50.9
47.8
94
49-130
Diisopropyl ether
ug/kg
50.9
47.7
94
66-130
Ethylbenzene
ug/kg
50.9
53.6
105
70-130
Hexachloro-1,3-butadiene
ug/kg
50.9
47.3
93
70-130
Isopropylbenzene (Cumene)
ug/kg
50.9
53.8
106
70-130
m&p-Xylene
ug/kg
102
105
103
70-130
Methyl-tert-butyl ether
ug/kg
50.9
48.3
95
70-130
Methylene Chloride
ug/kg
50.9
47.8
94
50-137
n-Butylbenzene
ug/kg
50.9
51.7
101
70-130
n-Propylbenzene
ug/kg
50.9
52.1
102
70-130
Naphthalene
ug/kg
50.9
53.2
104
70-131
o-Xylene
ug/kg
50.9
52.2
103
70-130
p-Isopropyltoluene
ug/kg
50.9
51.8
102
70-130
sec-Butylbenzene
ug/kg
50.9
52.6
103
70-130
Styrene
ug/kg
50.9
53.0
104
70-130
tert-Butyl benzene
ug/kg
50.9
50.7
100
69-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
LABORATORY CONTROL SAMPLE:
Parameter
2500329
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
ug/kg
50.9
33.7
66
56-130
Toluene
ug/kg
50.9
48.4
95
70-130
trans-1,2-Dichloroethene
ug/kg
50.9
50.9
100
70-130
trans- 1,3-Dichloropropene
ug/kg
50.9
52.1
102
70-130
Trichloroethene
ug/kg
50.9
52.7
103
70-141
Trichlorofluoromethane
ug/kg
50.9
47.5
93
67-130
Vinyl acetate
ug/kg
102
91.9
90
10-136
Vinyl chloride
ug/kg
50.9
48.4
95
67-130
Xylene (Total)
ug/kg
153
158
103
70-130
1,2-Dichloroethane-d4 (S)
%
102
70-132
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
94
70-130
MATRIX SPIKE SAMPLE:
Parameter
2500331
Units
92418026006
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
22.2
22.3
100
52-133
1,1,1-Trichloroethane
ug/kg
ND
22.2
23.5
106
49-137
1,1,2,2-Tetrachloroethane
ug/kg
ND
22.2
23.8
108
39-150
1,1,2-Trichloroethane
ug/kg
ND
22.2
22.3
101
48-140
1,1-Dichloroethane
ug/kg
ND
22.2
24.7
111
46-135
1,1-Dichloroethene
ug/kg
ND
22.2
25.2
114
38-149
1,1-Dichloropropene
ug/kg
ND
22.2
19.5
88
41-140
1,2,3-Trichlorobenzene
ug/kg
ND
22.2
21.2
95
10-158
1,2,3-Trichloropropane
ug/kg
ND
22.2
23.1
104
33-157
1,2,4-Trichlorobenzene
ug/kg
ND
22.2
21.5
97
10-155
1,2,4-Trimethylbenzene
ug/kg
ND
22.2
22.8
98
24-154
1,2-Dibromo-3-chloropropane
ug/kg
ND
22.2
22.4
101
33-158
1,2-Dibromoethane (EDB)
ug/kg
ND
22.2
21.1
95
40-136
1,2-Dichlorobenzene
ug/kg
ND
22.2
22.3
100
27-146
1,2-Dichloroethane
ug/kg
ND
22.2
23.1
104
49-140
1,2-Dichloropropane
ug/kg
ND
22.2
21.9
99
44-143
1,3,5-Trimethylbenzene
ug/kg
ND
22.2
22.4
101
40-144
1,3-Dichlorobenzene
ug/kg
ND
22.2
22.6
102
33-140
1,3-Dichloropropane
ug/kg
ND
22.2
20.5
92
47-147
1,4-Dichlorobenzene
ug/kg
ND
22.2
21.6
97
35-139
2,2-Dichloropropane
ug/kg
ND
22.2
24.7
111
41-140
2-Butanone (MEK)
ug/kg
ND
44.3
35.8J
81
10-181
2-Chlorotoluene
ug/kg
ND
22.2
22.7
102
38-147
2-Hexanone
ug/kg
ND
44.3
42AJ
96
18-169
4-Chlorotoluene
ug/kg
ND
22.2
22.6
102
36-145
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
44.3
45.5J
103
16-175
Acetone
ug/kg
ND
44.3
55.8J
126
10-200
Benzene
ug/kg
ND
22.2
22.3
101
46-136
Bromobenzene
ug/kg
ND
22.2
21.1
95
38-149
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
MATRIX SPIKE SAMPLE:
2500331
92418026006
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/kg
ND
22.2
23.7
107
44-142
Bromodichloromethane
ug/kg
ND
22.2
22.9
103
41-140
Bromoform
ug/kg
ND
22.2
21.5
97
34-145
Bromomethane
ug/kg
ND
22.2
26.9
122
14-162
Carbon tetrachloride
ug/kg
ND
22.2
24.2
109
44-141
Chlorobenzene
ug/kg
ND
22.2
22.1
100
39-141
Chloroethane
ug/kg
ND
22.2
27.1
122
10-182
Chloroform
ug/kg
ND
22.2
23.3
105
45-140
Chloromethane
ug/kg
ND
22.2
23.0
104
19-149
cis-1,2-Dichloroethene
ug/kg
ND
22.2
23.4
105
38-150
cis-1,3-Dichloropropene
ug/kg
ND
22.2
19.8
89
30-144
Dibromochloromethane
ug/kg
ND
22.2
20.5
93
36-145
Dibromomethane
ug/kg
ND
22.2
23.8
107
41-145
Dichlorodifluoromethane
ug/kg
ND
22.2
22.8
103
16-146
Diisopropyl ether
ug/kg
ND
22.2
20.9
94
41-143
Ethylbenzene
ug/kg
ND
22.2
23.5
106
35-144
Hexachloro-1,3-butadiene
ug/kg
ND
22.2
21.0
95
10-160
Isopropylbenzene (Cumene)
ug/kg
ND
22.2
24.3
109
30-152
m&p-Xylene
ug/kg
ND
44.3
48.6
110
33-145
Methyl-tert-butyl ether
ug/kg
ND
22.2
19.8
89
49-140
Methylene Chloride
ug/kg
ND
22.2
24.8
112
10-174
n-Butylbenzene
ug/kg
ND
22.2
22.6
102
10-160
n-Propylbenzene
ug/kg
ND
22.2
22.6
102
24-159
Naphthalene
ug/kg
1 AJ
22.2
22.7
96
10-171
o-Xylene
ug/kg
ND
22.2
24.3
110
31-150
p-Isopropyltoluene
ug/kg
ND
22.2
23.0
104
21-154
sec-Butylbenzene
ug/kg
ND
22.2
23.4
106
19-159
Styrene
ug/kg
ND
22.2
21.5
97
15-152
tert-Butyl benzene
ug/kg
ND
22.2
22.9
103
31-141
Tetrachloroethene
ug/kg
ND
22.2
14.0
63
19-141
Toluene
ug/kg
ND
22.2
22.8
103
31-146
trans-1,2-Dichloroethene
ug/kg
ND
22.2
23.9
108
28-157
trans- 1,3-Dichloropropene
ug/kg
ND
22.2
20.8
94
25-146
Trichloroethene
ug/kg
ND
22.2
20.1
91
34-149
Trichlorofluoromethane
ug/kg
ND
22.2
24.3
110
10-167
Vinyl acetate
ug/kg
ND
44.3
ND
13
10-200
Vinyl chloride
ug/kg
ND
22.2
24.6
111
36-155
Xylene (Total)
ug/kg
ND
66.6
73.0
110
29-148
1,2-Dichloroethane-d4 (S)
%
97
70-132
4-Bromofluorobenzene (S)
%
105
70-130
Toluene-d8 (S)
%
105
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
SAMPLE DUPLICATE: 2500330
Parameter
Units
92418026004
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
3.9J
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
31AJ
22.6J
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
SAMPLE DUPLICATE: 2500330
Parameter
Units
92418026004
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
6.9J
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
78
85
4-Bromofluorobenzene (S)
%
108
112
Toluene-d8 (S)
%
118
117
Max
RPD RPD Qualifiers
22
27
31
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC.
Page 47 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
QC Batch: 458472 Analysis Method: EPA 8270D
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92418026001, 92418026002, 92418026003, 92418026004, 92418026005, 92418026006, 92418026007
METHOD BLANK: 2499453 Matrix: Solid
Associated Lab Samples: 92418026001, 92418026002, 92418026003, 92418026004, 92418026005, 92418026006, 92418026007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
333
64.6
02/18/19 13:35
1,2-Dichlorobenzene
ug/kg
ND
333
88.9
02/18/19 13:35
1,3-Dichlorobenzene
ug/kg
ND
333
75.8
02/18/19 13:35
1,4-Dichlorobenzene
ug/kg
ND
333
93.9
02/18/19 13:35
1-Methylnaphthalene
ug/kg
ND
333
86.9
02/18/19 13:35
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
333
88.9
02/18/19 13:35
2,4,5-Trichlorophenol
ug/kg
ND
333
103
02/18/19 13:35
2,4,6-Trichlorophenol
ug/kg
ND
333
73.7
02/18/19 13:35
2,4-Dichlorophenol
ug/kg
ND
333
72.7
02/18/19 13:35
2,4-Dimethylphenol
ug/kg
ND
333
131
02/18/19 13:35
2,4-Dinitrophenol
ug/kg
ND
1670
54.5
02/18/19 13:35
2,4-Dinitrotoluene
ug/kg
ND
333
62.6
02/18/19 13:35
2,6-Dinitrotoluene
ug/kg
ND
333
69.7
02/18/19 13:35
2-Chloronaphthalene
ug/kg
ND
333
65.7
02/18/19 13:35
2-Chlorophenol
ug/kg
ND
333
90.9
02/18/19 13:35
2-Methylnaphthalene
ug/kg
ND
333
71.7
02/18/19 13:35
2-Methylphenol(o-Cresol)
ug/kg
ND
333
101
02/18/19 13:35
2-Nitroaniline
ug/kg
ND
1670
103
02/18/19 13:35
2-Nitrophenol
ug/kg
ND
333
80.8
02/18/19 13:35
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
333
131
02/18/19 13:35
3,3'-Dichlorobenzidine
ug/kg
ND
1670
72.7
02/18/19 13:35
3-Nitroaniline
ug/kg
ND
1670
90.9
02/18/19 13:35
4,6-Dinitro-2-methyl phenol
ug/kg
ND
667
66.7
02/18/19 13:35
4-Bromophenylphenyl ether
ug/kg
ND
333
60.6
02/18/19 13:35
4-ChIoro-3-methyl phenol
ug/kg
ND
667
68.7
02/18/19 13:35
4-Chloroaniline
ug/kg
ND
1670
92.9
02/18/19 13:35
4-Chlorophenylphenyl ether
ug/kg
ND
333
68.7
02/18/19 13:35
4-Nitroaniline
ug/kg
ND
667
93.9
02/18/19 13:35
4-Nitrophenol
ug/kg
ND
1670
59.6
02/18/19 13:35
Acenaphthene
ug/kg
ND
333
76.8
02/18/19 13:35
Acenaphthylene
ug/kg
ND
333
78.8
02/18/19 13:35
Aniline
ug/kg
ND
333
89.9
02/18/19 13:35
Anthracene
ug/kg
ND
333
74.7
02/18/19 13:35
Benzo(a)anthracene
ug/kg
ND
333
61.6
02/18/19 13:35
Benzo(a)pyrene
ug/kg
ND
333
63.6
02/18/19 13:35
Benzo(b)fluoranthene
ug/kg
ND
333
57.6
02/18/19 13:35
Benzo(g,h,i)perylene
ug/kg
ND
333
84.8
02/18/19 13:35
Benzo(k)fluoranthene
ug/kg
ND
333
65.7
02/18/19 13:35
Benzoic Acid
ug/kg
ND
1670
60.6
02/18/19 13:35
Benzyl alcohol
ug/kg
ND
667
66.7
02/18/19 13:35
bis(2-Chloroethoxy)methane
ug/kg
ND
333
77.8
02/18/19 13:35
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
METHOD BLANK: 2499453 Matrix: Solid
Associated Lab Samples: 92418026001, 92418026002, 92418026003, 92418026004, 92418026005, 92418026006, 92418026007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
bis(2-Chloroethyl) ether
ug/kg
ND
333
84.8
02/18/19 13:35
bis(2-Ethylhexyl)phthalate
ug/kg
ND
333
90.9
02/18/19 13:35
Butylbenzylphthalate
ug/kg
ND
333
70.7
02/18/19 13:35
Chrysene
ug/kg
ND
333
44.4
02/18/19 13:35
Di-n-butylphthalate
ug/kg
ND
333
54.5
02/18/19 13:35
Di-n-octylphthalate
ug/kg
ND
333
69.7
02/18/19 13:35
Dibenz(a,h)anthracene
ug/kg
ND
333
70.7
02/18/19 13:35
Dibenzofuran
ug/kg
ND
333
54.5
02/18/19 13:35
Diethylphthalate
ug/kg
ND
333
51.5
02/18/19 13:35
Dimethylphthalate
ug/kg
ND
333
67.7
02/18/19 13:35
Fluoranthene
ug/kg
ND
333
48.5
02/18/19 13:35
Fluorene
ug/kg
ND
333
68.7
02/18/19 13:35
Hexachloro-1,3-butadiene
ug/kg
ND
333
57.6
02/18/19 13:35
Hexachlorobenzene
ug/kg
ND
333
42.4
02/18/19 13:35
Hexachlorocyclopentadiene
ug/kg
ND
333
61.6
02/18/19 13:35
Hexachloroethane
ug/kg
ND
333
87.9
02/18/19 13:35
Indeno(1,2,3-cd)pyrene
ug/kg
ND
333
68.7
02/18/19 13:35
Isophorone
ug/kg
ND
333
74.7
02/18/19 13:35
N-Nitroso-di-n-propylamine
ug/kg
ND
333
63.6
02/18/19 13:35
N-Nitrosodimethylamine
ug/kg
ND
333
108
02/18/19 13:35
N-Nitrosodiphenylamine
ug/kg
ND
333
99.0
02/18/19 13:35
Naphthalene
ug/kg
ND
333
81.8
02/18/19 13:35
Nitrobenzene
ug/kg
ND
333
90.9
02/18/19 13:35
Pentachlorophenol
ug/kg
ND
1670
60.6
02/18/19 13:35
Phenanthrene
ug/kg
ND
333
55.6
02/18/19 13:35
Phenol
ug/kg
ND
333
100
02/18/19 13:35
Pyrene
ug/kg
ND
333
56.6
02/18/19 13:35
2,4,6-Tribromophenol (S)
%
56
27-110
02/18/19 13:35
2-Fluorobiphenyl (S)
%
57
30-110
02/18/19 13:35
2-Fluorophenol (S)
%
58
13-110
02/18/19 13:35
Nitrobenzene-d5 (S)
%
71
23-110
02/18/19 13:35
Phenol-d6 (S)
%
60
22-110
02/18/19 13:35
Terphenyl-d14 (S)
%
62
28-110
02/18/19 13:35
LABORATORY CONTROL SAMPLE:
2499454
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1690
993
59
52-130
1,2-Dichlorobenzene
ug/kg
1690
1090
65
51-130
1,3-Dichlorobenzene
ug/kg
1690
1040
61
50-130
1,4-Dichlorobenzene
ug/kg
1690
1040
62
49-130
1-Methylnaphthalene
ug/kg
1690
1150
68
55-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1690
1410
84
30-130
2,4,5-Trichlorophenol
ug/kg
1690
952
56
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
LABORATORY CONTROL SAMPLE:
Parameter
2499454
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,6-TrichIorophenol
ug/kg
1690
1010
60
57-130
2,4-DichIorophenol
ug/kg
1690
1050
62
56-130
2,4-Dimethylphenol
ug/kg
1690
1320
78
51-130
2,4-Dinitrophenol
ug/kg
8450
6480
77
27-133
2,4-Dinitrotoluene
ug/kg
1690
1110
66
61-130
2,6-Dinitrotoluene
ug/kg
1690
1130
67
60-130
2-Chloronaphthalene
ug/kg
1690
1050
62
52-130
2-Chlorophenol
ug/kg
1690
1130
67
54-130
2-Methylnaphthalene
ug/kg
1690
1140
68
54-130
2-Methylphenol(o-Cresol)
ug/kg
1690
1210
71
51-130
2-Nitroaniline
ug/kg
3380
2490
74
51-130
2-Nitrophenol
ug/kg
1690
1080
64
49-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1690
1210
72
11-163
3,3'-Dichlorobenzidine
ug/kg
3380
1820
54
10-132
3-Nitroaniline
ug/kg
3380
1930
57
55-130
4,6-Dinitro-2-methyl phenol
ug/kg
3380
2610
77
47-142
4-Bromophenylphenyl ether
ug/kg
1690
1100
65
59-130
4-Chloro-3-methylphenol
ug/kg
3380
2720
81
55-130
4-Chloroaniline
ug/kg
3380
2180
65
54-130
4-Chlorophenylphenyl ether
ug/kg
1690
1160
68
58-130
4-Nitroaniline
ug/kg
3380
2160
64
54-130
4-Nitrophenol
ug/kg
8450
6530
77
48-130
Acenaphthene
ug/kg
1690
1160
69
60-130
Acenaphthylene
ug/kg
1690
1290
76
60-130
Aniline
ug/kg
1690
999
59
43-130
Anthracene
ug/kg
1690
1160
68
63-130
Benzo(a)anthracene
ug/kg
1690
1250
74
59-130
Benzo(a)pyrene
ug/kg
1690
1160
69
57-130
Benzo(b)fluoranthene
ug/kg
1690
1100
65
54-130
Benzo(g,h,i)perylene
ug/kg
1690
1090
64
59-130
Benzo(k)fluoranthene
ug/kg
1690
1110
66
54-130
Benzoic Acid
ug/kg
8450
6050
72
19-130
Benzyl alcohol
ug/kg
3380
2450
73
50-130
bis(2-Chloroethoxy)methane
ug/kg
1690
1210
71
54-130
bis(2-Chloroethyl) ether
ug/kg
1690
1150
68
48-130
bis(2-Ethylhexyl)phthalate
ug/kg
1690
1370
81
45-134
Butylbenzylphthalate
ug/kg
1690
1430
85
46-138
Chrysene
ug/kg
1690
1190
70
58-130
Di-n-butylphthalate
ug/kg
1690
1160
69
60-130
Di-n-octylphthalate
ug/kg
1690
1340
79
53-130
Dibenz(a,h)anthracene
ug/kg
1690
1030
61
59-130
Dibenzofuran
ug/kg
1690
1120
66
60-130
Diethylphthalate
ug/kg
1690
1190
71
60-130
Dimethylphthalate
ug/kg
1690
1120
66
60-130
Fluoranthene
ug/kg
1690
1180
70
65-130
Fluorene
ug/kg
1690
1220
72
63-130
Hexachloro-1,3-butadiene
ug/kg
1690
1120
67
46-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
LABORATORY CONTROL SAMPLE:
Parameter
2499454
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachlorobenzene
ug/kg
1690
1030
61
58-130
Hexachlorocyclopentadiene
ug/kg
1690
892
53
23-130
Hexachloroethane
ug/kg
1690
1170
69
47-130
Indeno(1,2,3-cd)pyrene
ug/kg
1690
1070
63
60-130
Isophorone
ug/kg
1690
1220
72
49-130
N-Nitroso-di-n-propylamine
ug/kg
1690
1360
81
47-130
N-Nitrosodimethylamine
ug/kg
1690
1360
81
45-130
N-Nitrosodiphenylamine
ug/kg
1690
1170
69
59-130
Naphthalene
ug/kg
1690
1220
72
55-130
Nitrobenzene
ug/kg
1690
1240
73
49-130
Pentachlorophenol
ug/kg
3380
2010
60
10-132
Phenanthrene
ug/kg
1690
1180
70
62-130
Phenol
ug/kg
1690
1170
69
46-130
Pyrene
ug/kg
1690
1480
88
53-130
2,4,6-Tribromophenol (S)
%
64
27-110
2-Fluorobiphenyl (S)
%
58
30-110
2-Fluorophenol(S)
%
69
13-110
Nitrobenzene-d5 (S)
%
76
23-110
Phenol-d6 (S)
%
73
22-110
Terphenyl-d14 (S)
%
74
28-110
MATRIX SPIKE SAMPLE:
Parameter
2499455
Units
92417701001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
2300
1790
78
18-130
1,2-Dichlorobenzene
ug/kg
ND
2300
1710
75
14-130
1,3-Dichlorobenzene
ug/kg
ND
2300
1680
73
12-130
1,4-Dichlorobenzene
ug/kg
ND
2300
1750
76
10-130
1-Methylnaphthalene
ug/kg
ND
2300
1950
85
12-130
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
2300
2160
94
10-130
2,4,5-Trichlorophenol
ug/kg
ND
2300
2060
90
13-130
2,4,6-Trichlorophenol
ug/kg
ND
2300
2190
95
17-130
2,4-Dichlorophenol
ug/kg
ND
2300
1800
78
10-130
2,4-Dimethylphenol
ug/kg
ND
2300
2010
88
10-130
2,4-Dinitrophenol
ug/kg
ND
11500
3680
32
10-130
2,4-Dinitrotoluene
ug/kg
ND
2300
1880
82
24-130
2,6-Dinitrotoluene
ug/kg
ND
2300
1900
83
23-130
2-Chloronaphthalene
ug/kg
ND
2300
1820
79
19-130
2-Chlorophenol
ug/kg
ND
2300
1770
77
10-130
2-Methylnaphthalene
ug/kg
ND
2300
1970
86
18-130
2-Methylphenol(o-Cresol)
ug/kg
ND
2300
1920
84
10-130
2-Nitroaniline
ug/kg
ND
4590
4970
108
17-130
2-Nitrophenol
ug/kg
ND
2300
1650
72
10-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
2300
1790
78
10-130
3,3'-Dichlorobenzidine
ug/kg
ND
4590
3290
72
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
MATRIX SPIKE SAMPLE:
2499455
92417701001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
3-Nitroaniline
ug/kg
ND
4590
3470
76
24-130
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4590
3370
73
10-152
4-Bromophenylphenyl ether
ug/kg
ND
2300
1740
76
29-130
4-Chloro-3-methylphenol
ug/kg
ND
4590
4000
87
17-130
4-Chloroaniline
ug/kg
ND
4590
3550
77
14-130
4-Chlorophenylphenyl ether
ug/kg
ND
2300
2040
89
25-130
4-Nitroaniline
ug/kg
ND
4590
3650
79
22-130
4-Nitrophenol
ug/kg
ND
11500
12800
111
10-130
Acenaphthene
ug/kg
ND
2300
2030
89
20-130
Acenaphthylene
ug/kg
ND
2300
2190
95
25-130
Aniline
ug/kg
ND
2300
1530
66
10-130
Anthracene
ug/kg
ND
2300
1970
86
29-130
Benzo(a)anthracene
ug/kg
ND
2300
2040
89
19-130
Benzo(a)pyrene
ug/kg
ND
2300
2060
90
12-130
Benzo(b)fluoranthene
ug/kg
ND
2300
2010
88
14-130
Benzo(g,h,i)perylene
ug/kg
ND
2300
1820
79
10-130
Benzo(k)fluoranthene
ug/kg
ND
2300
2040
89
14-130
Benzoic Acid
ug/kg
ND
11500
854J
7
10-130 M1
Benzyl alcohol
ug/kg
ND
4590
3720
81
13-130
bis(2-Chloroethoxy)methane
ug/kg
ND
2300
1850
81
16-130
bis(2-Chloroethyl) ether
ug/kg
ND
2300
1790
78
11-130
bis(2-Ethylhexyl)phthalate
ug/kg
ND
2300
2060
90
21-130
Butylbenzylphthalate
ug/kg
ND
2300
2010
87
23-130
Chrysene
ug/kg
ND
2300
1960
85
22-130
Di-n-butylphthalate
ug/kg
ND
2300
2020
88
30-130
Di-n-octylphthalate
ug/kg
ND
2300
2020
88
23-142
Dibenz(a,h)anthracene
ug/kg
ND
2300
1910
83
10-130
Dibenzofuran
ug/kg
ND
2300
1950
85
24-130
Diethylphthalate
ug/kg
ND
2300
2130
93
26-130
Dimethylphthalate
ug/kg
ND
2300
2030
88
22-130
Fluoranthene
ug/kg
ND
2300
2110
92
33-130
Fluorene
ug/kg
ND
2300
2180
95
22-130
Hexachloro-1,3-butadiene
ug/kg
ND
2300
1870
81
13-130
Hexachlorobenzene
ug/kg
ND
2300
1610
70
29-130
Hexachlorocyclopentadiene
ug/kg
ND
2300
1790
78
10-130
Hexachloroethane
ug/kg
ND
2300
1760
77
10-130
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2300
1880
82
10-130
Isophorone
ug/kg
ND
2300
1970
86
13-130
N-Nitroso-di-n-propylamine
ug/kg
ND
2300
2060
90
12-130
N-Nitrosodimethylamine
ug/kg
ND
2300
2000
87
11-130
N-Nitrosodiphenylamine
ug/kg
ND
2300
1900
83
15-130
Naphthalene
ug/kg
ND
2300
1950
85
15-130
Nitrobenzene
ug/kg
ND
2300
1890
82
12-130
Pentachlorophenol
ug/kg
ND
4590
2920
64
10-130
Phenanthrene
ug/kg
ND
2300
1950
85
27-130
Phenol
ug/kg
ND
2300
1740
76
10-130
Pyrene
ug/kg
ND
2300
2170
94
19-130
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: MGN-002
Pace Project No.: 92418026
MATRIX SPIKE SAMPLE:
Parameter
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
2499455
Units
92417701001 Spike MS MS
Result Conc. Result % Rec
% Rec
Limits
%
74
27-110
%
89
30-110
%
72
13-110
%
84
23-110
%
80
22-110
%
78
28-110
SAMPLE DUPLICATE: 2499456
Parameter
Units
92417701002
Result
Dup
Result RPD
Max
RPD
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
1-Methylnaphthalene
ug/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
30
2,4,5-Trichlorophenol
ug/kg
ND
ND
30
2,4,6-Trichlorophenol
ug/kg
ND
ND
30
2,4-Dichlorophenol
ug/kg
ND
ND
30
2,4-Dimethylphenol
ug/kg
ND
ND
30
2,4-Dinitrophenol
ug/kg
ND
ND
30
2,4-Dinitrotoluene
ug/kg
ND
ND
30
2,6-Dinitrotoluene
ug/kg
ND
ND
30
2-Chloronaphthalene
ug/kg
ND
ND
30
2-Chlorophenol
ug/kg
ND
ND
30
2-Methylnaphthalene
ug/kg
ND
ND
30
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
30
2-Nitroaniline
ug/kg
ND
ND
30
2-Nitrophenol
ug/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
30
3,3'-Dichlorobenzidine
ug/kg
ND
ND
30
3-Nitroaniline
ug/kg
ND
ND
30
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
30
4-Bromophenylphenyl ether
ug/kg
ND
ND
30
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
30
4-Chloroaniline
ug/kg
ND
ND
30
4-Chlorophenylphenyl ether
ug/kg
ND
ND
30
4-Nitroaniline
ug/kg
ND
ND
30
4-Nitrophenol
ug/kg
ND
ND
30
Acenaphthene
ug/kg
ND
ND
30
Acenaphthylene
ug/kg
ND
ND
30
Aniline
ug/kg
ND
ND
30
Anthracene
ug/kg
ND
ND
30
Benzo(a)anthracene
ug/kg
ND
ND
30
Benzo(a)pyrene
ug/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
SAMPLE DUPLICATE: 2499456
Parameter
Units
92417701002
Result
Dup
Result
RPD
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
76
68
10
2-Fluorobiphenyl (S)
%
53
56
7
2-Fluorophenol(S)
%
42
54
26
Nitrobenzene-d5 (S)
%
60
66
11
Phenol-d6 (S)
%
51
63
23
Terphenyl-d14 (S)
%
83
73
12
Max
RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418026
QC Batch: 458526 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92418026001, 92418026002, 92418026003, 92418026004, 92418026005, 92418026006, 92418026007
SAMPLE DUPLICATE: 2499893
92417612001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 20.4 18.6 10 25
SAMPLE DUPLICATE: 2499894
92417659001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 47.7 39.1 20 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: MGN-002
Pace Project No.: 92418026
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
S1 Surrogate recovery outside laboratory control limits (confirmed by re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/21 /2019 04:18 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
MGN-002
92418026
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92418026001
UST-1
EPA 3546
458472
EPA 8270D
458699
92418026002
UST-2
EPA 3546
458472
EPA 8270D
458699
92418026003
UST-3
EPA 3546
458472
EPA 8270D
458699
92418026004
UST-4
EPA 3546
458472
EPA 8270D
458699
92418026005
UST-5
EPA 3546
458472
EPA 8270D
458699
92418026006
UST-6
EPA 3546
458472
EPA 8270D
458699
92418026007
UST-8
EPA 3546
458472
EPA 8270D
458699
92418026001
UST-1
EPA 5035A
458674
EPA 8260B
458695
92418026002
UST-2
EPA 5035A
458676
EPA 8260B
458696
92418026003
UST-3
EPA 5035A
458676
EPA 8260B
458696
92418026004
UST-4
EPA 5035A
458676
EPA 8260B
458696
92418026005
UST-5
EPA 5035A
458676
EPA 8260B
458696
92418026006
UST-6
EPA 5035A
458676
EPA 8260B
458696
92418026007
UST-8
EPA 5035A
458676
EPA 8260B
458696
92418026001
UST-1
ASTM D2974-87
458526
92418026002
UST-2
ASTM D2974-87
458526
92418026003
UST-3
ASTM D2974-87
458526
92418026004
UST-4
ASTM D2974-87
458526
92418026005
UST-5
ASTM D2974-87
458526
92418026006
UST-6
ASTM D2974-87
458526
92418026007
UST-8
ASTM D2974-87
458526
Date: 02/21 /2019 04:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 57 of 72

UOGUmenL Name: ""- --- - -
Page 1 of 2
Condition Upon Recelpt(SCUR) issuing Authority:
Document No.:
r 16A o PC n7O O-- Ae Pace Carolinas Qua[ity Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvill- F1 Raleigh[]Mechanicsville❑
-Sample- Condition Client Name: # TWO# • 9241 V O26
Upon Receipt I Project
6ouPieri ❑Fed Ex ❑UPS ❑Other:. ClientICI
❑ Commercial ❑Pace ❑ 92418026
Custody Seal Present? []yes No Seals intact? ❑Yes [ No 14
patellnitials Person Examining Contents: % -
/
Packing Material: ❑Bubble Wrap ubhle Bags ❑None El other Tissue Frozen?
Other ❑yes ❑No ❑N']A
Thermometer; j g�Ta�g Type of Ice: et ❑Glue ❑None
Q R Gun ID:
Cooler Temp (°C): , Correction Factor: Add/Subtract (°C) 0.0 Temp should be above freezing to VC
Cooler Temp [orrected (°C):— ❑Samples cut of temp criteria. Samples on Ice, cooling process
has begun
USDA Regulated Soil (❑ N/A, water sample)
Did sarripies origin m a quarantine zone within the'United States: CA, NY, or SC (check maps)? Did samples originate from a fareigh source (internationally,
❑Yes
including Hawaii and Puerto Rico)? ❑Yes . I2�
cnmmentslbiscrepancy:
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Raid Time Anaiysis (<72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Cortect Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis. Samples Field Filtered?
Sample Labels Match COO
-Includes
[]NO ❑N/A S.
[]No ❑NIA 6,
[]No [I N/A 7.
❑No -- N/A 8.
[]No ❑NIA 9-
Fleadspace in VOA Vials(>5-5mm)? "Yes Lu N9, LfJ141A
Trip Blank Present? ❑Yes ' Na ❑NIA
Trio BlankCustodv Seals Present? ❑yes ❑No NIA
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Date/Time:
Lot ID of split containers:
Field Data Required? Dyes []No
Project Manager SCURF Review: Oate: L
r � Date:
Project Manager SRF Review:--
Page 58 of 72

UU6UNIMUL NaIii ,
Condition Upon Receil
Document No.:
F-CAR-CS=033-Rev.06
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: vOA,Coliforrn, TOC, Oil and Grease, DRO/8015 (water) HOC, LLHg
**Sottom half of box is to list number of bottle
1
2
3
A
S
6
S
9
to
it
12
Project IWO# • 9241e VQ26
PM: KRIN Due Date: 02/22/19
CLIENT: 92—Hart Hick
Z
CI
E
[��[
.-i
ca
k
�
(n
c
7
a
E
N
N
M
m
Z
v'
H
Cl.O
E
O
yr
N
m
6
:
a
N
G
a
w
—
�+
�
m
U
V
2
`C"
E
N
tI
Y
m
V
=
0.
m
O
7-
=
E
O
L"
N
M
m
n
S
�
y
�u
E
Ln -
N
m
'
U
A
2
a
Z
E
Ln
N
rIi
m
d
@
o.
c-
7
p
N
=
��,
7i
�
z,
a)
a
E
G
±v
rl
7
U
4
ry
=
4
QJ
Ua¢
C
°
=
rt
S
U'
4
Z
N
N
of
Lr'
N
7
l7
d
^y
V
CL
'J
Wry
N
a
N
(U
.-1
V5
C9
C
rJ
v
7-
Q-
�¢
d
a
N
V7
l7
Q
_
Z
=
Z
v
E
"'
O
d
d
Q
.
=
Q
OO
J
E
Q
=
O
Q
Z
n5
0
M
z
a
]
J
E
F-
}
d
z6aE
O
7
J
E
V
9
`Z
_
dM
Ou
O
1
c
It
6ch
�T
0
`
z
N
m
-
0d
C
d
u
N-
aaye
a
=
m
,
00.
7
p
m
i'
aTa
—
E
N
Irri
iai6
I
z
m—
J
E
N
1
N
m
n
°1
cfI
Li
Q
z
'+m
pO
E
rq
d
"�
�
azz
d
E
a
a
7
l9
d
E
o
7
to
}
a
ro
N
E
I E
l
pH Adjustment Log for Preserved Samples
H upon receipt Date preservation adjusted Time pressrvation Amount of Preservative Eat fk
Sample ID Type of Preservative p P P adjusted added
Noth Carolina compliance samplas, a copy of this form will be sent to the North Carolina DEHNR Certification Office OA
Note: Whenever there is a discrepancy affecting
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 59 of 72

g
G' � rr-
z rn
a i a
-+ z y
In m m
D D
N
al al a1 >
J
w
m
TEMP in C
Received an
Ice
{YIN)
Custody
Sealed
\
Cooler
YIN
Samples
r•
(YIN)
a
j ITEM #
n ma°
'm " N
`-• o
-
.�
s+
w
w
i
o.
m
ao
m
cn
;
o
N
3 z
d C 7
¢ n
U3to
0
m
r3
J
r�
0 W
ogvWWP.0
e
H
6
v
F
°a
a y
d
m
p Kv
x
F
a
�g2�omv��os
v -A o
- _
01
m m
�F
v E0
co
�• a
A °
°m
at
o o
„i
o CL m
3 O Z
m n
# h 1
9 r
v
�
S
i o
MATRIX CODE (see valid codes to left)
SAMPLE TYPE (G=GRAB C=COMP)
z
o fi
N
m
n
-A
7
5
�V
- j
m
a
m
Z
0
k
SAMPLE TEMP AT COLLECTIO
Residual Chlorine (YIN)
Rn
o
N
^� {7
In _
n a
n �
� m
i Z
o O
C TI
N r
m w m a o g r m tia C
a g a n r
a m 0
n�e r
to °�° m C }
°n
m N C
m <_. Z z
f r
YIN �}
c CD
N TCT
CD
C
10 C ❑
a O
n x or C1
a rD _
w a 33
L Ca
e cD rt
n �
n p a
� 1 CAS
2 C'
c
v
N '
f/l @ N
w c
m y
z r- o
n
G
nn
O
Page 60 of 72
N
^� {7
In _
n a
n �
� m
i Z
o O
C TI
N r
m w m a o g r m tia C
a g a n r
a m 0
n�e r
to °�° m C }
°n
m N C
m <_. Z z
f r
YIN �}
c CD
N TCT
CD
C
10 C ❑
a O
n x or C1
a rD _
w a 33
L Ca
e cD rt
n �
n p a
� 1 CAS
2 C'
c
v
N '
f/l @ N
w c
m y
z r- o
n
G
nn
O
Page 60 of 72

O
�FaceAnalytical o
National Center for Testing & Innovation
P
a
ANALYTICAL REPORT
February 21, 2019
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1071331
Samples Received: 02/19/2019
Project Number: 92418026
Description: MGN-002
Site: 001
Report To: Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By: �vUnn v�,, �.
L111-�
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
V
It 49
it
Page 61 of 72

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Fn
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
SB-1 L1071331-01
5
[Cn]
Qc: Quality Control Summary
6
Total Solids by Method 2540 G-2011
6
Fr
Mercury by Method 7471B
7
Metals (ICPMS) by Method 6020B
8
RC
Gl: Glossary of Terms
9
F
Al: Accreditations & Locations
10
Sc: Sample Chain of Custody
11
rAl
FSC
Page 62 of 72
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Pace Analytical - Huntersville, INC 92418026 L1071331
02/21/19 07:48
2 of 12

S13-1 L1071331-01 Solid
Method
Total Solids by Method 2540 G-2011
Mercury by Method 7471B
Metals (ICPMS) by Method 6020B
SAMPLE SUMMARY
Collected by
Batch
WG1239165
WG1239242
WG1239524
Dilution Preparation
date/time
1 02/19/1913:11
1 02/19/1914:21
5 02/20/1918:30
ONE LAB. NATIONWIDE.
Collected date/time
Received date/time
02/15/1911:20
02/19/19 09:00
FP1
Analysis
Analyst
date/time
FTC
02/19/1913:19
JD
02/19/19
TCT
20/19 23:1
02/20/19 23:12
LD
[Cn]
FSr
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG:
Pace Analytical - Huntersville, NC 92418026 L1071331
Page 63 of 72
DATE/TIME: PAGE:
02/21/19 07:48 3 of 12

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
VV VV� � �t La�'_
Nancy McLain
Project Manager
FP1
FTC
FSS
FSr
FC-1
F,
FAI
FSC
Page 64 of 72
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92418026 L1071331 02/21/19 07:48 4 of 12

SB-1
Collected date/time: 02/15/19 11:20
Total Solids by Method 2540 G-2011
SAMPLE RESULTS - 01
L1071331
Result Qualifier Dilution Analysis
Analyte % date / time
Total Solids 83.6 1 02/19/201913:19
Mercury by Method 7471B
Batch
WG1239165
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Mercury
U
0.00335
0.0239
1
02/19/201919:46
WG12392
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier
MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date/time
Arsenic
0.704
0.149
0.598
5
02/20/2019 23:12
WG123952
Barium
68.8
01
0.191
1.20
5
02/20/2019 23:12
WG123952
Cadmium
U
0.0957
0.598
5
02/20/2019 23:12
WG123952
Chromium
2.52
0.323
1.20
5
02/20/2019 23:12
WG123952
Lead
9.05
01
0.144
0.598
5
02/20/2019 23:12
WG123952
Selenium
0.571
J
0.227
0.598
5
02/20/2019 23:12
WG123952
Silver
U
0.185
0.598
5
02/20/2019 23:12
WG123952
ONE LAB. NATIONWIDE.
42
Fp
FTC
FSS
4
Cn
1qc
4
4
Fq
4
4
FAI4
4
4
FSC
Page 65 of 72
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92418026 L1071331 02/21/19 07:48 5 of 12

WG1239165
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3385288-1 02/19/19 13:19
MB Result
Analyte %
Total Solids 0.00100
MB Qualifier MB MDL MB RDL
L1071307-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1071307-01 02/19/19 13:19 • (DUP) R3385288-3 02/19/19 13:19
Original Result DUP Result Dilution DUP RPD
Analyte % % %
Total Solids 78.1 78.0 1 0.104
Laboratory Control Sample (LCS)
(LCS) R3385288-2 02/19/19 13:19
Spike Amount LCS Result LCS Rec.
Analyte % %_ %
Total Solids 50.0 50.0 100
QUALITY CONTROL SUMMARY
L1071331-01
DUP Qualifier DUP RPD
Limits
10
Rec. Limits LCS Qualifier
o/
85.0-115
ONE LAB. NATIONWIDE.
— I
Cp
FTc
FSS
4
— Cn
FSr
— �GI
FAI
[Sc
Page 66 of 72
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92418026 L1071331 02/21/19 07:48 6 of 12

WG1239242
Mercury by Method 7471B
Method Blank (MB)
(MB) R3385177-1 02/19/1919:08
MB Result
Analyte mg/kg
Mercury U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.00280 0.0200
QUALITY CONTROL SUMMARY
L1071331-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3385177-2 02/19/1919:11 • (LCSD) R3385177-3 02/19/1919:13
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg % % % % %
Mercury 0.500 0.496 0.509 99.3 102 80.0-120 2.55 20
L1069846-21 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE.
(OS) L1069846-21 02/19/1919:16 • (MS) R3385177-4 02/19/1919:18 • (MSD) R3385177-5 02/19/1919:21
Spike Amount Original Result
MS Result (dry)
MSD Result MS Rec. MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry) (dry)
(dry)
Analyte mg/kg mg/kg
mg/kg
mg/kg % %
%
% %
Mercury 0.602 0.0393
0.617
0.593 96.0 92.0
1 75.0-125
3.99 20
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical - Huntersville, NC
92418026
L1071331
02/21/19 07:48
— I
Cp
FTc
FSS
4
— Cn
FSr
— �GI
FAI
[Sc
Page 67 of 72
PAGE:
7of12

WG1239524
Metals (ICPMS) by Method 6020B
Method Blank (MB)
(MB) R3385608-1 02/20/19 22:59
MB Result
Analyte mg/kg
Arsenic U
Barium U
Cadmium U
Chromium U
Lead U
Selenium U
Silver U
MB Qualifier MB MDL
mg/kg
0.125
0.160
0.0800
0.270
0.120
0.190
0.155
MB RDL
mg/kg
0.500
1.00
0.500
1.00
0.500
0.500
0.500
QUALITY CONTROL SUMMARY
L1071331-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3385608-2 02/20/19 23:03 • (LCSD) R3385608-3 02/20/19 23:08
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
Analyte
mg/kg
mg/kg
mg/kg
%
%
%
%
Arsenic
100
95.5
93.7
95.5
93.7
80.0-120
1.83
Barium
100
92.7
90.8
92.7
90.8
80.0-120
2.03
Cadmium
100
98.3
96.7
98.3
96.7
80.0-120
1.67
Chromium
100
97.3
96.0
97.3
96.0
80.0-120
1.28
Lead
100
101
97.2
101
97.2
80.0-120
3.69
Selenium
100
97.4
94.7
97.4
94.7
80.0-120
2.73
Silver
20.0
21.0
19.4
105
97.1
80.0-120
7.71
L1071331-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1071331-01 02/20/19 23:12 • (MS) R3385608-6 02/20/19 23:25 • (MSD) R3385608-7 02/20/19 23:29
Spike Amount
Original Result
MS Result (dry)
MSD Result
MS Rec.
MSD Rec.
(dry)
(dry)
(dry)
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
Arsenic
23.9
0.704
118
109
98.3
90.6
Barium
23.9
68.8
183
178
95.8
91.6
Cadmium
23.9
U
124
115
104
96.1
Chromium
23.9
2.52
126
117
103
96.1
Lead
23.9
9.05
132
125
103
96.7
Selenium
23.9
0.571
125
114
104
95.0
Silver
4.78
U
25.0
24.2
105
101
RPD Limits
20
20
20
20
20
20
20
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
5
75.0-125
8.11
5
75.0-125
2.76
5
75.0-125
7.84
5
75.0-125
6.70
5
75.0-125
5.72
5
75.0-125
8.67
5
75.0-125
3.44
ONE LAB. NATIONWIDE.
RPD Limits
20
20
20
20
20
20
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
[Sc
Page 68 of 72
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92418026 L1071331 02/21/19 07:48 8 of 12

GLOSSARY OF TERMS
ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
(dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry) Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry) Reported Detection Limit.
Rec. Recovery.
RPD Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
01
The analyte failed the method required serial dilution test and/or subsequent post -spike criteria. These failures indicate
matrix interference.
Page 69 of 72
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville,
INC 92418026 L1071331 02/21/19 07:48 9 of 12

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT NO
OR MN
T ID T WI NY
SD
WY MI
NV
T NE IA OH T PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
W 11110
� NM O� AR N Sc
T MS A`7L GA
T TX * LA
T
AK T T
q FL
wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME:
Pace Analytical - Huntersville, NC 92418026 L1071331 02/21/19 07:48
ME
Page 70 of 72
PAGE:
10 of 12

Chain of Custody
1248 aceAnalytical m
www pacelabs. com
t
i
w_..._...a..... nnA1an0a 1h1.-. L—weinr Hama- Results Requested By: 2/22/2019
Report 1 Invoice To
Kevin Godwin
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
Phone [phone]
Email: [e-mail]
State of Sample Origin: NC
Item I Sample ID
1 SB-1
2
3
4
5
Transfers Released By
1 / t (?
2
3
Cooler Temperature on R
P.O. 1
l2eJ(g.s LPioo�a., R
� i/2 Z
t7
m
Z
m
Collect
DatelTime Lab ID Matrix
2I1512019 11:20 192418026001 1 Solid I i
0 67jS
DatelTime [Received By
)A, (-)o I If1hli'- 41.,
Seal Y or N
v
2
E
a
u
cc
rved Containers I^
n
N
N
O
DatelTime
iced on Ice or N
An
LAB USE ONLY
_In-71331-0
Comments
Samples Intact ly or
Monday, February 18. 2019 6:37:01 AM FMT-ALL-C-002rev,00 24March2009 Pag&7ji3Df172f 1

Pace Analytical Nationalfor : Innovation
CoolerReceipt Form
Client: � SDG#:
Cooler Received/Opened On: 2 /tq /19 Temperature: G {o
Receives# By: Malik Tisdale
Signature:
Receipt Check List NP
Yes
No
COC Seal Present / Intact?
COC Signed / Accurate?
r
bottles arrive intact?
r
Correct bottles used?
Sufficient volume sent?
s
if Applicable
VOA Zero headspace?
Preservation Correct / Checked?
Page 72 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 22, 2019
Ralph McGee
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
RE: Project: MGN-002
Pace Project No.: 92418130
Dear Ralph McGee:
Enclosed are the analytical results for sample(s) received by the laboratory on February 18, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: MGN-002
Pace Project No.: 92418130
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 45

aceAnalytical
—pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: MGN-002
Pace Project No.: 92418130
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92418130001
UST-7
Solid
02/18/19 09:50
02/18/19 16:20
92418130002
UST-9
Solid
02/18/19 09:30
02/18/19 16:20
92418130003
UST-10
Solid
02/18/19 09:10
02/18/19 16:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
MGN-002
92418130
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92418130001
UST-7
EPA 8270D
RES
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418130002
UST-9
EPA 8270D
RES
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92418130003
UST-10
EPA 8270D
RES
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-7 Lab ID: 92418130001 Collected: 02/18/19 09:50 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
409
94.2
1
02/19/19 17:50
02/20/19 17:16
83-32-9
Acenaphthylene
ND
ug/kg
409
96.7
1
02/19/19 17:50
02/20/19 17:16
208-96-8
Aniline
ND
ug/kg
409
110
1
02/19/19 17:50
02/20/19 17:16
62-53-3
Anthracene
ND
ug/kg
409
91.7
1
02/19/19 17:50
02/20/19 17:16
120-12-7
Benzo(a)anthracene
ND
ug/kg
409
75.6
1
02/19/19 17:50
02/20/19 17:16
56-55-3
Benzo(a)pyrene
ND
ug/kg
409
78.1
1
02/19/19 17:50
02/20/19 17:16
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
409
70.6
1
02/19/19 17:50
02/20/19 17:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
409
104
1
02/19/19 17:50
02/20/19 17:16
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
409
80.6
1
02/19/19 17:50
02/20/19 17:16
207-08-9
Benzoic Acid
ND
ug/kg
2050
74.4
1
02/19/19 17:50
02/20/19 17:16
65-85-0
Benzyl alcohol
ND
ug/kg
818
81.8
1
02/19/19 17:50
02/20/19 17:16
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
409
74.4
1
02/19/19 17:50
02/20/19 17:16
101-55-3
Butylbenzylphthalate
ND
ug/kg
409
86.8
1
02/19/19 17:50
02/20/19 17:16
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
818
84.3
1
02/19/19 17:50
02/20/19 17:16
59-50-7
4-Chloroaniline
ND
ug/kg
2050
114
1
02/19/19 17:50
02/20/19 17:16
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
409
95.4
1
02/19/19 17:50
02/20/19 17:16
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
409
104
1
02/19/19 17:50
02/20/19 17:16
111-44-4
2-Chloronaphthalene
ND
ug/kg
409
80.6
1
02/19/19 17:50
02/20/19 17:16
91-58-7
2-Chlorophenol
ND
ug/kg
409
112
1
02/19/19 17:50
02/20/19 17:16
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
409
84.3
1
02/19/19 17:50
02/20/19 17:16
7005-72-3
Chrysene
ND
ug/kg
409
54.5
1
02/19/19 17:50
02/20/19 17:16
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
409
86.8
1
02/19/19 17:50
02/20/19 17:16
53-70-3
Dibenzofuran
ND
ug/kg
409
66.9
1
02/19/19 17:50
02/20/19 17:16
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
409
109
1
02/19/19 17:50
02/20/19 17:16
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
409
93.0
1
02/19/19 17:50
02/20/19 17:16
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
409
115
1
02/19/19 17:50
02/20/19 17:16
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2050
89.2
1
02/19/19 17:50
02/20/19 17:16
91-94-1
2,4-Dichlorophenol
ND
ug/kg
409
89.2
1
02/19/19 17:50
02/20/19 17:16
120-83-2
Diethylphthalate
ND
ug/kg
409
63.2
1
02/19/19 17:50
02/20/19 17:16
84-66-2
2,4-Dimethylphenol
ND
ug/kg
409
161
1
02/19/19 17:50
02/20/19 17:16
105-67-9
Dimethylphthalate
ND
ug/kg
409
83.0
1
02/19/19 17:50
02/20/19 17:16
131-11-3
Di-n-butylphthalate
ND
ug/kg
409
66.9
1
02/19/19 17:50
02/20/19 17:16
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
818
81.8
1
02/19/19 17:50
02/20/19 17:16
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2050
66.9
1
02/19/19 17:50
02/20/19 17:16
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
409
76.8
1
02/19/19 17:50
02/20/19 17:16
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
409
85.5
1
02/19/19 17:50
02/20/19 17:16
606-20-2
Di-n-octylphthalate
ND
ug/kg
409
85.5
1
02/19/19 17:50
02/20/19 17:16
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
409
112
1
02/19/19 17:50
02/20/19 17:16
117-81-7
Fluoranthene
ND
ug/kg
409
59.5
1
02/19/19 17:50
02/20/19 17:16
206-44-0
Fluorene
ND
ug/kg
409
84.3
1
02/19/19 17:50
02/20/19 17:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
409
70.6
1
02/19/19 17:50
02/20/19 17:16
87-68-3
Hexachlorobenzene
ND
ug/kg
409
52.1
1
02/19/19 17:50
02/20/19 17:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
409
75.6
1
02/19/19 17:50
02/20/19 17:16
77-47-4
Hexachloroethane
ND
ug/kg
409
108
1
02/19/19 17:50
02/20/19 17:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
409
84.3
1
02/19/19 17:50
02/20/19 17:16
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-7 Lab ID: 92418130001 Collected: 02/18/19 09:50 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
409
91.7
1
02/19/19 17:50
02/20/19 17:16
78-59-1
1-Methylnaphthalene
ND
ug/kg
409
107
1
02/19/19 17:50
02/20/19 17:16
90-12-0
2-Methylnaphthalene
ND
ug/kg
409
88.0
1
02/19/19 17:50
02/20/19 17:16
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
409
124
1
02/19/19 17:50
02/20/19 17:16
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
409
161
1
02/19/19 17:50
02/20/19 17:16
15831-10-4
Naphthalene
ND
ug/kg
409
100
1
02/19/19 17:50
02/20/19 17:16
91-20-3
2-Nitroaniline
ND
ug/kg
2050
126
1
02/19/19 17:50
02/20/19 17:16
88-74-4
3-Nitroaniline
ND
ug/kg
2050
112
1
02/19/19 17:50
02/20/19 17:16
99-09-2
4-Nitroaniline
ND
ug/kg
818
115
1
02/19/19 17:50
02/20/19 17:16
100-01-6
Nitrobenzene
ND
ug/kg
409
112
1
02/19/19 17:50
02/20/19 17:16
98-95-3
2-Nitrophenol
ND
ug/kg
409
99.2
1
02/19/19 17:50
02/20/19 17:16
88-75-5
4-Nitrophenol
ND
ug/kg
2050
73.1
1
02/19/19 17:50
02/20/19 17:16
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
409
133
1
02/19/19 17:50
02/20/19 17:16
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
409
78.1
1
02/19/19 17:50
02/20/19 17:16
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
409
121
1
02/19/19 17:50
02/20/19 17:16
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
409
109
1
02/19/19 17:50
02/20/19 17:16
108-60-1
Pentachlorophenol
ND
ug/kg
2050
74.4
1
02/19/19 17:50
02/20/19 17:16
87-86-5
Phenanthrene
ND
ug/kg
409
68.2
1
02/19/19 17:50
02/20/19 17:16
85-01-8
Phenol
ND
ug/kg
409
123
1
02/19/19 17:50
02/20/19 17:16
108-95-2
Pyrene
ND
ug/kg
409
69.4
1
02/19/19 17:50
02/20/19 17:16
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
409
79.3
1
02/19/19 17:50
02/20/19 17:16
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
409
126
1
02/19/19 17:50
02/20/19 17:16
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
409
90.5
1
02/19/19 17:50
02/20/19 17:16
88-06-2
Surrogates
Nitrobenzene-d5 (S)
72
%
23-110
1
02/19/19 17:50
02/20/19 17:16
4165-60-0
2-Fluorobiphenyl (S)
65
%
30-110
1
02/19/19 17:50
02/20/19 17:16
321-60-8
Terphenyl-d14 (S)
79
%
28-110
1
02/19/19 17:50
02/20/19 17:16
1718-51-0
Phenol-d6 (S)
75
%
22-110
1
02/19/19 17:50
02/20/19 17:16
13127-88-3
2-Fluorophenol (S)
72
%
13-110
1
02/19/19 17:50
02/20/19 17:16
367-12-4
2,4,6-Tribromophenol (S)
77
%
27-110
1
02/19/19 17:50
02/20/19 17:16
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
26.3J
ug/kg
96.5
9.6
1
02/19/19 09:39
02/19/19 16:11
67-64-1
Benzene
ND
ug/kg
4.8
1.5
1
02/19/19 09:39
02/19/19 16:11
71-43-2
Bromobenzene
ND
ug/kg
4.8
1.9
1
02/19/19 09:39
02/19/19 16:11
108-86-1
Bromochloromethane
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
74-97-5
Bromodichloromethane
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
75-27-4
Bromoform
ND
ug/kg
4.8
2.2
1
02/19/19 09:39
02/19/19 16:11
75-25-2
Bromomethane
ND
ug/kg
9.6
2.4
1
02/19/19 09:39
02/19/19 16:11
74-83-9
2-Butanone (MEK)
ND
ug/kg
96.5
2.8
1
02/19/19 09:39
02/19/19 16:11
78-93-3
n-Butylbenzene
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
104-51-8
sec-Butylbenzene
ND
ug/kg
4.8
1.5
1
02/19/19 09:39
02/19/19 16:11
135-98-8
tert-Butyl benzene
ND
ug/kg
4.8
1.9
1
02/19/19 09:39
02/19/19 16:11
98-06-6
Carbon tetrachloride
ND
ug/kg
4.8
2.5
1
02/19/19 09:39
02/19/19 16:11
56-23-5
Chlorobenzene
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-7 Lab ID: 92418130001 Collected: 02/18/19 09:50 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
9.6
2.3
1
02/19/19 09:39
02/19/19 16:11
75-00-3
Chloroform
ND
ug/kg
4.8
1.5
1
02/19/19 09:39
02/19/19 16:11
67-66-3
Chloromethane
ND
ug/kg
9.6
2.3
1
02/19/19 09:39
02/19/19 16:11
74-87-3
2-Chlorotoluene
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
95-49-8
4-Chlorotoluene
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
4.8
3.5
1
02/19/19 09:39
02/19/19 16:11
96-12-8
Dibromochloromethane
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
106-93-4
Dibromomethane
ND
ug/kg
4.8
2.4
1
02/19/19 09:39
02/19/19 16:11
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4.8
1.9
1
02/19/19 09:39
02/19/19 16:11
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
106-46-7
Dichlorodifluoromethane
ND
ug/kg
9.6
3.5
1
02/19/19 09:39
02/19/19 16:11
75-71-8
1,1-Dichloroethane
ND
ug/kg
4.8
1.4
1
02/19/19 09:39
02/19/19 16:11
75-34-3
1,2-Dichloroethane
ND
ug/kg
4.8
2.1
1
02/19/19 09:39
02/19/19 16:11
107-06-2
1,1-Dichloroethene
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
4.8
1.4
1
02/19/19 09:39
02/19/19 16:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
156-60-5
1,2-Dichloropropane
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
78-87-5
1,3-Dichloropropane
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
142-28-9
2,2-Dichloropropane
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
594-20-7
1,1-Dichloropropene
ND
ug/kg
4.8
1.4
1
02/19/19 09:39
02/19/19 16:11
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
4.8
1.4
1
02/19/19 09:39
02/19/19 16:11
10061-02-6
Diisopropyl ether
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
108-20-3
Ethylbenzene
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
4.8
1.9
1
02/19/19 09:39
02/19/19 16:11
87-68-3
2-Hexanone
ND
ug/kg
48.2
3.8
1
02/19/19 09:39
02/19/19 16:11
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
98-82-8
p-Isopropyltoluene
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
99-87-6
Methylene Chloride
ND
ug/kg
19.3
2.9
1
02/19/19 09:39
02/19/19 16:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
48.2
3.6
1
02/19/19 09:39
02/19/19 16:11
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
4.8
1.4
1
02/19/19 09:39
02/19/19 16:11
1634-04-4
Naphthalene
ND
ug/kg
4.8
1.2
1
02/19/19 09:39
02/19/19 16:11
91-20-3
n-Propylbenzene
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
103-65-1
Styrene
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
4.8
2.0
1
02/19/19 09:39
02/19/19 16:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
79-34-5
Tetrachloroethene
ND
ug/kg
4.8
1.6
1
02/19/19 09:39
02/19/19 16:11
127-18-4
Toluene
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
4.8
2.1
1
02/19/19 09:39
02/19/19 16:11
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
4.8
1.5
1
02/19/19 09:39
02/19/19 16:11
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
4.8
2.0
1
02/19/19 09:39
02/19/19 16:11
79-00-5
Trichloroethene
ND
ug/kg
4.8
2.0
1
02/19/19 09:39
02/19/19 16:11
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-7 Lab ID: 92418130001 Collected: 02/18/19 09:50 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/22/2019 12:51 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
4.8
2.1
1
02/19/19 09:39
02/19/19 16:11
75-69-4
ND
ug/kg
4.8
1.5
1
02/19/19 09:39
02/19/19 16:11
96-18-4
ND
ug/kg
4.8
1.9
1
02/19/19 09:39
02/19/19 16:11
95-63-6
ND
ug/kg
4.8
1.7
1
02/19/19 09:39
02/19/19 16:11
108-67-8
ND
ug/kg
48.2
8.5
1
02/19/19 09:39
02/19/19 16:11
108-05-4 L1
ND
ug/kg
9.6
1.7
1
02/19/19 09:39
02/19/19 16:11
75-01-4
ND
ug/kg
9.6
3.5
1
02/19/19 09:39
02/19/19 16:11
1330-20-7
ND
ug/kg
9.6
3.5
1
02/19/19 09:39
02/19/19 16:11
179601-23-1
ND
ug/kg
4.8
1.8
1
02/19/19 09:39
02/19/19 16:11
95-47-6
119
%
70-130
1
02/19/19 09:39
02/19/19 16:11
2037-26-5
112
%
70-130
1
02/19/19 09:39
02/19/19 16:11
460-00-4
80
%
70-132
1
02/19/19 09:39
02/19/19 16:11
17060-07-0
Analytical Method: ASTM D2974-87
18.5 % 0.10 0.10 1 02/18/1917:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-9 Lab ID: 92418130002 Collected: 02/18/19 09:30 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
416
95.9
1
02/19/19 17:50
02/20/19 17:44
83-32-9
Acenaphthylene
ND
ug/kg
416
98.4
1
02/19/19 17:50
02/20/19 17:44
208-96-8
Aniline
ND
ug/kg
416
112
1
02/19/19 17:50
02/20/19 17:44
62-53-3
Anthracene
ND
ug/kg
416
93.4
1
02/19/19 17:50
02/20/19 17:44
120-12-7
Benzo(a)anthracene
ND
ug/kg
416
77.0
1
02/19/19 17:50
02/20/19 17:44
56-55-3
Benzo(a)pyrene
ND
ug/kg
416
79.5
1
02/19/19 17:50
02/20/19 17:44
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
416
71.9
1
02/19/19 17:50
02/20/19 17:44
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
416
106
1
02/19/19 17:50
02/20/19 17:44
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
416
82.0
1
02/19/19 17:50
02/20/19 17:44
207-08-9
Benzoic Acid
ND
ug/kg
2080
75.7
1
02/19/19 17:50
02/20/19 17:44
65-85-0
Benzyl alcohol
ND
ug/kg
833
83.3
1
02/19/19 17:50
02/20/19 17:44
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
416
75.7
1
02/19/19 17:50
02/20/19 17:44
101-55-3
Butylbenzylphthalate
ND
ug/kg
416
88.3
1
02/19/19 17:50
02/20/19 17:44
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
833
85.8
1
02/19/19 17:50
02/20/19 17:44
59-50-7
4-Chloroaniline
ND
ug/kg
2080
116
1
02/19/19 17:50
02/20/19 17:44
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
416
97.2
1
02/19/19 17:50
02/20/19 17:44
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
416
106
1
02/19/19 17:50
02/20/19 17:44
111-44-4
2-Chloronaphthalene
ND
ug/kg
416
82.0
1
02/19/19 17:50
02/20/19 17:44
91-58-7
2-Chlorophenol
ND
ug/kg
416
114
1
02/19/19 17:50
02/20/19 17:44
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
416
85.8
1
02/19/19 17:50
02/20/19 17:44
7005-72-3
Chrysene
ND
ug/kg
416
55.5
1
02/19/19 17:50
02/20/19 17:44
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
416
88.3
1
02/19/19 17:50
02/20/19 17:44
53-70-3
Dibenzofuran
ND
ug/kg
416
68.2
1
02/19/19 17:50
02/20/19 17:44
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
416
ill
1
02/19/19 17:50
02/20/19 17:44
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
416
94.7
1
02/19/19 17:50
02/20/19 17:44
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
416
117
1
02/19/19 17:50
02/20/19 17:44
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2080
90.9
1
02/19/19 17:50
02/20/19 17:44
91-94-1
2,4-Dichlorophenol
ND
ug/kg
416
90.9
1
02/19/19 17:50
02/20/19 17:44
120-83-2
Diethylphthalate
ND
ug/kg
416
64.4
1
02/19/19 17:50
02/20/19 17:44
84-66-2
2,4-Dimethylphenol
ND
ug/kg
416
164
1
02/19/19 17:50
02/20/19 17:44
105-67-9
Dimethylphthalate
ND
ug/kg
416
84.6
1
02/19/19 17:50
02/20/19 17:44
131-11-3
Di-n-butylphthalate
ND
ug/kg
416
68.2
1
02/19/19 17:50
02/20/19 17:44
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
833
83.3
1
02/19/19 17:50
02/20/19 17:44
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2080
68.2
1
02/19/19 17:50
02/20/19 17:44
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
416
78.3
1
02/19/19 17:50
02/20/19 17:44
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
416
87.1
1
02/19/19 17:50
02/20/19 17:44
606-20-2
Di-n-octylphthalate
ND
ug/kg
416
87.1
1
02/19/19 17:50
02/20/19 17:44
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
416
114
1
02/19/19 17:50
02/20/19 17:44
117-81-7
Fluoranthene
ND
ug/kg
416
60.6
1
02/19/19 17:50
02/20/19 17:44
206-44-0
Fluorene
ND
ug/kg
416
85.8
1
02/19/19 17:50
02/20/19 17:44
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
416
71.9
1
02/19/19 17:50
02/20/19 17:44
87-68-3
Hexachlorobenzene
ND
ug/kg
416
53.0
1
02/19/19 17:50
02/20/19 17:44
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
416
77.0
1
02/19/19 17:50
02/20/19 17:44
77-47-4
Hexachloroethane
ND
ug/kg
416
110
1
02/19/19 17:50
02/20/19 17:44
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
416
85.8
1
02/19/19 17:50
02/20/19 17:44
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-9 Lab ID: 92418130002 Collected: 02/18/19 09:30 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
416
93.4
1
02/19/19 17:50
02/20/19 17:44
78-59-1
1-Methylnaphthalene
ND
ug/kg
416
109
1
02/19/19 17:50
02/20/19 17:44
90-12-0
2-Methylnaphthalene
ND
ug/kg
416
89.6
1
02/19/19 17:50
02/20/19 17:44
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
416
126
1
02/19/19 17:50
02/20/19 17:44
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
416
164
1
02/19/19 17:50
02/20/19 17:44
15831-10-4
Naphthalene
ND
ug/kg
416
102
1
02/19/19 17:50
02/20/19 17:44
91-20-3
2-Nitroaniline
ND
ug/kg
2080
129
1
02/19/19 17:50
02/20/19 17:44
88-74-4
3-Nitroaniline
ND
ug/kg
2080
114
1
02/19/19 17:50
02/20/19 17:44
99-09-2
4-Nitroaniline
ND
ug/kg
833
117
1
02/19/19 17:50
02/20/19 17:44
100-01-6
Nitrobenzene
ND
ug/kg
416
114
1
02/19/19 17:50
02/20/19 17:44
98-95-3
2-Nitrophenol
ND
ug/kg
416
101
1
02/19/19 17:50
02/20/19 17:44
88-75-5
4-Nitrophenol
ND
ug/kg
2080
74.5
1
02/19/19 17:50
02/20/19 17:44
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
416
135
1
02/19/19 17:50
02/20/19 17:44
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
416
79.5
1
02/19/19 17:50
02/20/19 17:44
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
416
124
1
02/19/19 17:50
02/20/19 17:44
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
416
ill
1
02/19/19 17:50
02/20/19 17:44
108-60-1
Pentachlorophenol
ND
ug/kg
2080
75.7
1
02/19/19 17:50
02/20/19 17:44
87-86-5
Phenanthrene
ND
ug/kg
416
69.4
1
02/19/19 17:50
02/20/19 17:44
85-01-8
Phenol
ND
ug/kg
416
125
1
02/19/19 17:50
02/20/19 17:44
108-95-2
Pyrene
ND
ug/kg
416
70.7
1
02/19/19 17:50
02/20/19 17:44
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
416
80.8
1
02/19/19 17:50
02/20/19 17:44
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
416
129
1
02/19/19 17:50
02/20/19 17:44
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
416
92.1
1
02/19/19 17:50
02/20/19 17:44
88-06-2
Surrogates
Nitrobenzene-d5 (S)
63
%
23-110
1
02/19/19 17:50
02/20/19 17:44
4165-60-0
2-Fluorobiphenyl (S)
57
%
30-110
1
02/19/19 17:50
02/20/19 17:44
321-60-8
Terphenyl-d14 (S)
73
%
28-110
1
02/19/19 17:50
02/20/19 17:44
1718-51-0
Phenol-d6 (S)
63
%
22-110
1
02/19/19 17:50
02/20/19 17:44
13127-88-3
2-Fluorophenol (S)
62
%
13-110
1
02/19/19 17:50
02/20/19 17:44
367-12-4
2,4,6-Tribromophenol (S)
67
%
27-110
1
02/19/19 17:50
02/20/19 17:44
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
27.2J
ug/kg
101
10.1
1
02/19/19 09:39
02/19/19 16:52
67-64-1
Benzene
ND
ug/kg
5.0
1.6
1
02/19/19 09:39
02/19/19 16:52
71-43-2
Bromobenzene
ND
ug/kg
5.0
2.0
1
02/19/19 09:39
02/19/19 16:52
108-86-1
Bromochloromethane
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
74-97-5
Bromodichloromethane
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
75-27-4
Bromoform
ND
ug/kg
5.0
2.3
1
02/19/19 09:39
02/19/19 16:52
75-25-2
Bromomethane
ND
ug/kg
10.1
2.5
1
02/19/19 09:39
02/19/19 16:52
74-83-9
2-Butanone (MEK)
ND
ug/kg
101
2.9
1
02/19/19 09:39
02/19/19 16:52
78-93-3
n-Butylbenzene
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
104-51-8
sec-Butylbenzene
ND
ug/kg
5.0
1.6
1
02/19/19 09:39
02/19/19 16:52
135-98-8
tert-Butyl benzene
ND
ug/kg
5.0
2.0
1
02/19/19 09:39
02/19/19 16:52
98-06-6
Carbon tetrachloride
ND
ug/kg
5.0
2.6
1
02/19/19 09:39
02/19/19 16:52
56-23-5
Chlorobenzene
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-9 Lab ID: 92418130002 Collected: 02/18/19 09:30 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
10.1
2.4
1
02/19/19 09:39
02/19/19 16:52
75-00-3
Chloroform
ND
ug/kg
5.0
1.6
1
02/19/19 09:39
02/19/19 16:52
67-66-3
Chloromethane
ND
ug/kg
10.1
2.4
1
02/19/19 09:39
02/19/19 16:52
74-87-3
2-Chlorotoluene
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
95-49-8
4-Chlorotoluene
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.0
3.6
1
02/19/19 09:39
02/19/19 16:52
96-12-8
Dibromochloromethane
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
106-93-4
Dibromomethane
ND
ug/kg
5.0
2.5
1
02/19/19 09:39
02/19/19 16:52
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.0
2.0
1
02/19/19 09:39
02/19/19 16:52
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
106-46-7
Dichlorodifluoromethane
ND
ug/kg
10.1
3.6
1
02/19/19 09:39
02/19/19 16:52
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.0
1.5
1
02/19/19 09:39
02/19/19 16:52
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.0
2.2
1
02/19/19 09:39
02/19/19 16:52
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.0
1.4
1
02/19/19 09:39
02/19/19 16:52
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.0
1.5
1
02/19/19 09:39
02/19/19 16:52
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.0
1.5
1
02/19/19 09:39
02/19/19 16:52
10061-02-6
Diisopropyl ether
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
108-20-3
Ethylbenzene
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.0
2.0
1
02/19/19 09:39
02/19/19 16:52
87-68-3
2-Hexanone
ND
ug/kg
50.3
3.9
1
02/19/19 09:39
02/19/19 16:52
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
99-87-6
Methylene Chloride
ND
ug/kg
20.1
3.0
1
02/19/19 09:39
02/19/19 16:52
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
50.3
3.7
1
02/19/19 09:39
02/19/19 16:52
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.0
1.5
1
02/19/19 09:39
02/19/19 16:52
1634-04-4
Naphthalene
ND
ug/kg
5.0
1.2
1
02/19/19 09:39
02/19/19 16:52
91-20-3
n-Propylbenzene
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
103-65-1
Styrene
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.0
2.1
1
02/19/19 09:39
02/19/19 16:52
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
79-34-5
Tetrachloroethene
ND
ug/kg
5.0
1.7
1
02/19/19 09:39
02/19/19 16:52
127-18-4
Toluene
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.0
2.2
1
02/19/19 09:39
02/19/19 16:52
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.0
1.6
1
02/19/19 09:39
02/19/19 16:52
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.0
2.1
1
02/19/19 09:39
02/19/19 16:52
79-00-5
Trichloroethene
ND
ug/kg
5.0
2.1
1
02/19/19 09:39
02/19/19 16:52
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-9 Lab ID: 92418130002 Collected: 02/18/19 09:30 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/22/2019 12:51 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
5.0
2.2
1
02/19/19 09:39
02/19/19 16:52
75-69-4
ND
ug/kg
5.0
1.6
1
02/19/19 09:39
02/19/19 16:52
96-18-4
ND
ug/kg
5.0
2.0
1
02/19/19 09:39
02/19/19 16:52
95-63-6
ND
ug/kg
5.0
1.8
1
02/19/19 09:39
02/19/19 16:52
108-67-8
ND
ug/kg
50.3
8.8
1
02/19/19 09:39
02/19/19 16:52
108-05-4 L1
ND
ug/kg
10.1
1.8
1
02/19/19 09:39
02/19/19 16:52
75-01-4
ND
ug/kg
10.1
3.6
1
02/19/19 09:39
02/19/19 16:52
1330-20-7
ND
ug/kg
10.1
3.6
1
02/19/19 09:39
02/19/19 16:52
179601-23-1
ND
ug/kg
5.0
1.9
1
02/19/19 09:39
02/19/19 16:52
95-47-6
114
%
70-130
1
02/19/19 09:39
02/19/19 16:52
2037-26-5
ill
%
70-130
1
02/19/19 09:39
02/19/19 16:52
460-00-4
79
%
70-132
1
02/19/19 09:39
02/19/19 16:52
17060-07-0
Analytical Method: ASTM D2974-87
21.6 % 0.10 0.10 1 02/18/1917:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-10 Lab ID: 92418130003 Collected: 02/18/19 09:10 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
427
98.4
1
02/19/19 17:50
02/20/19 18:12
83-32-9
Acenaphthylene
ND
ug/kg
427
101
1
02/19/19 17:50
02/20/19 18:12
208-96-8
Aniline
ND
ug/kg
427
115
1
02/19/19 17:50
02/20/19 18:12
62-53-3
Anthracene
ND
ug/kg
427
95.8
1
02/19/19 17:50
02/20/19 18:12
120-12-7
Benzo(a)anthracene
ND
ug/kg
427
79.0
1
02/19/19 17:50
02/20/19 18:12
56-55-3
Benzo(a)pyrene
ND
ug/kg
427
81.6
1
02/19/19 17:50
02/20/19 18:12
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
427
73.8
1
02/19/19 17:50
02/20/19 18:12
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
427
109
1
02/19/19 17:50
02/20/19 18:12
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
427
84.2
1
02/19/19 17:50
02/20/19 18:12
207-08-9
Benzoic Acid
ND
ug/kg
2140
77.7
1
02/19/19 17:50
02/20/19 18:12
65-85-0
Benzyl alcohol
ND
ug/kg
855
85.5
1
02/19/19 17:50
02/20/19 18:12
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
427
77.7
1
02/19/19 17:50
02/20/19 18:12
101-55-3
Butylbenzylphthalate
ND
ug/kg
427
90.6
1
02/19/19 17:50
02/20/19 18:12
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
855
88.0
1
02/19/19 17:50
02/20/19 18:12
59-50-7
4-Chloroaniline
ND
ug/kg
2140
119
1
02/19/19 17:50
02/20/19 18:12
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
427
99.7
1
02/19/19 17:50
02/20/19 18:12
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
427
109
1
02/19/19 17:50
02/20/19 18:12
111-44-4
2-Chloronaphthalene
ND
ug/kg
427
84.2
1
02/19/19 17:50
02/20/19 18:12
91-58-7
2-Chlorophenol
ND
ug/kg
427
117
1
02/19/19 17:50
02/20/19 18:12
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
427
88.0
1
02/19/19 17:50
02/20/19 18:12
7005-72-3
Chrysene
ND
ug/kg
427
57.0
1
02/19/19 17:50
02/20/19 18:12
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
427
90.6
1
02/19/19 17:50
02/20/19 18:12
53-70-3
Dibenzofuran
ND
ug/kg
427
69.9
1
02/19/19 17:50
02/20/19 18:12
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
427
114
1
02/19/19 17:50
02/20/19 18:12
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
427
97.1
1
02/19/19 17:50
02/20/19 18:12
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
427
120
1
02/19/19 17:50
02/20/19 18:12
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2140
93.2
1
02/19/19 17:50
02/20/19 18:12
91-94-1
2,4-Dichlorophenol
ND
ug/kg
427
93.2
1
02/19/19 17:50
02/20/19 18:12
120-83-2
Diethylphthalate
ND
ug/kg
427
66.0
1
02/19/19 17:50
02/20/19 18:12
84-66-2
2,4-Dimethylphenol
ND
ug/kg
427
168
1
02/19/19 17:50
02/20/19 18:12
105-67-9
Dimethylphthalate
ND
ug/kg
427
86.8
1
02/19/19 17:50
02/20/19 18:12
131-11-3
Di-n-butylphthalate
ND
ug/kg
427
69.9
1
02/19/19 17:50
02/20/19 18:12
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
855
85.5
1
02/19/19 17:50
02/20/19 18:12
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2140
69.9
1
02/19/19 17:50
02/20/19 18:12
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
427
80.3
1
02/19/19 17:50
02/20/19 18:12
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
427
89.3
1
02/19/19 17:50
02/20/19 18:12
606-20-2
Di-n-octylphthalate
ND
ug/kg
427
89.3
1
02/19/19 17:50
02/20/19 18:12
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
427
117
1
02/19/19 17:50
02/20/19 18:12
117-81-7
Fluoranthene
ND
ug/kg
427
62.2
1
02/19/19 17:50
02/20/19 18:12
206-44-0
Fluorene
ND
ug/kg
427
88.0
1
02/19/19 17:50
02/20/19 18:12
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
427
73.8
1
02/19/19 17:50
02/20/19 18:12
87-68-3
Hexachlorobenzene
ND
ug/kg
427
54.4
1
02/19/19 17:50
02/20/19 18:12
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
427
79.0
1
02/19/19 17:50
02/20/19 18:12
77-47-4
Hexachloroethane
ND
ug/kg
427
113
1
02/19/19 17:50
02/20/19 18:12
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
427
88.0
1
02/19/19 17:50
02/20/19 18:12
193-39-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-10 Lab ID: 92418130003 Collected: 02/18/19 09:10 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Isophorone
ND
ug/kg
427
95.8
1
02/19/19 17:50
02/20/19 18:12
78-59-1
1-Methylnaphthalene
ND
ug/kg
427
ill
1
02/19/19 17:50
02/20/19 18:12
90-12-0
2-Methylnaphthalene
ND
ug/kg
427
91.9
1
02/19/19 17:50
02/20/19 18:12
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
427
129
1
02/19/19 17:50
02/20/19 18:12
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
427
168
1
02/19/19 17:50
02/20/19 18:12
15831-10-4
Naphthalene
ND
ug/kg
427
105
1
02/19/19 17:50
02/20/19 18:12
91-20-3
2-Nitroaniline
ND
ug/kg
2140
132
1
02/19/19 17:50
02/20/19 18:12
88-74-4
3-Nitroaniline
ND
ug/kg
2140
117
1
02/19/19 17:50
02/20/19 18:12
99-09-2
4-Nitroaniline
ND
ug/kg
855
120
1
02/19/19 17:50
02/20/19 18:12
100-01-6
Nitrobenzene
ND
ug/kg
427
117
1
02/19/19 17:50
02/20/19 18:12
98-95-3
2-Nitrophenol
ND
ug/kg
427
104
1
02/19/19 17:50
02/20/19 18:12
88-75-5
4-Nitrophenol
ND
ug/kg
2140
76.4
1
02/19/19 17:50
02/20/19 18:12
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
427
139
1
02/19/19 17:50
02/20/19 18:12
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
427
81.6
1
02/19/19 17:50
02/20/19 18:12
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
427
127
1
02/19/19 17:50
02/20/19 18:12
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
427
114
1
02/19/19 17:50
02/20/19 18:12
108-60-1
Pentachlorophenol
ND
ug/kg
2140
77.7
1
02/19/19 17:50
02/20/19 18:12
87-86-5
Phenanthrene
ND
ug/kg
427
71.2
1
02/19/19 17:50
02/20/19 18:12
85-01-8
Phenol
ND
ug/kg
427
128
1
02/19/19 17:50
02/20/19 18:12
108-95-2
Pyrene
ND
ug/kg
427
72.5
1
02/19/19 17:50
02/20/19 18:12
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
427
82.9
1
02/19/19 17:50
02/20/19 18:12
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
427
132
1
02/19/19 17:50
02/20/19 18:12
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
427
94.5
1
02/19/19 17:50
02/20/19 18:12
88-06-2
Surrogates
Nitrobenzene-d5 (S)
75
%
23-110
1
02/19/19 17:50
02/20/19 18:12
4165-60-0
2-Fluorobiphenyl (S)
70
%
30-110
1
02/19/19 17:50
02/20/19 18:12
321-60-8
Terphenyl-d14 (S)
69
%
28-110
1
02/19/19 17:50
02/20/19 18:12
1718-51-0
Phenol-d6 (S)
77
%
22-110
1
02/19/19 17:50
02/20/19 18:12
13127-88-3
2-Fluorophenol (S)
75
%
13-110
1
02/19/19 17:50
02/20/19 18:12
367-12-4
2,4,6-Tribromophenol (S)
79
%
27-110
1
02/19/19 17:50
02/20/19 18:12
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
ND
ug/kg
119
11.9
1
02/19/19 09:39
02/19/19 17:11
67-64-1
Benzene
13.3
ug/kg
5.9
1.9
1
02/19/19 09:39
02/19/19 17:11
71-43-2
Bromobenzene
ND
ug/kg
5.9
2.4
1
02/19/19 09:39
02/19/19 17:11
108-86-1
Bromochloromethane
ND
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
74-97-5
Bromodichloromethane
ND
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
75-27-4
Bromoform
ND
ug/kg
5.9
2.7
1
02/19/19 09:39
02/19/19 17:11
75-25-2
Bromomethane
ND
ug/kg
11.9
3.0
1
02/19/19 09:39
02/19/19 17:11
74-83-9
2-Butanone (MEK)
ND
ug/kg
119
3.4
1
02/19/19 09:39
02/19/19 17:11
78-93-3
n-Butylbenzene
10.2
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
104-51-8
sec-Butylbenzene
5.51
ug/kg
5.9
1.9
1
02/19/19 09:39
02/19/19 17:11
135-98-8
tert-Butyl benzene
ND
ug/kg
5.9
2.4
1
02/19/19 09:39
02/19/19 17:11
98-06-6
Carbon tetrachloride
ND
ug/kg
5.9
3.1
1
02/19/19 09:39
02/19/19 17:11
56-23-5
Chlorobenzene
ND
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
108-90-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-10 Lab ID: 92418130003 Collected: 02/18/19 09:10 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Chloroethane
ND
ug/kg
11.9
2.9
1
02/19/19 09:39
02/19/19 17:11
75-00-3
Chloroform
ND
ug/kg
5.9
1.9
1
02/19/19 09:39
02/19/19 17:11
67-66-3
Chloromethane
ND
ug/kg
11.9
2.9
1
02/19/19 09:39
02/19/19 17:11
74-87-3
2-Chlorotoluene
ND
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
95-49-8
4-Chlorotoluene
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.9
4.3
1
02/19/19 09:39
02/19/19 17:11
96-12-8
Dibromochloromethane
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
106-93-4
Dibromomethane
ND
ug/kg
5.9
3.0
1
02/19/19 09:39
02/19/19 17:11
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.9
2.4
1
02/19/19 09:39
02/19/19 17:11
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.9
4.3
1
02/19/19 09:39
02/19/19 17:11
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.9
1.8
1
02/19/19 09:39
02/19/19 17:11
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.9
2.6
1
02/19/19 09:39
02/19/19 17:11
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.9
1.7
1
02/19/19 09:39
02/19/19 17:11
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.9
1.8
1
02/19/19 09:39
02/19/19 17:11
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.9
1.8
1
02/19/19 09:39
02/19/19 17:11
10061-02-6
Diisopropyl ether
ND
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
108-20-3
Ethylbenzene
13.8
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.9
2.4
1
02/19/19 09:39
02/19/19 17:11
87-68-3
2-Hexanone
ND
ug/kg
59.5
4.6
1
02/19/19 09:39
02/19/19 17:11
591-78-6
Isopropylbenzene (Cumene)
6.0
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
98-82-8
p-Isopropyltoluene
8.4
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
99-87-6
Methylene Chloride
ND
ug/kg
23.8
3.6
1
02/19/19 09:39
02/19/19 17:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
59.5
4.4
1
02/19/19 09:39
02/19/19 17:11
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.9
1.8
1
02/19/19 09:39
02/19/19 17:11
1634-04-4
Naphthalene
18.6
ug/kg
5.9
1.4
1
02/19/19 09:39
02/19/19 17:11
91-20-3
n-Propylbenzene
9.0
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
103-65-1
Styrene
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.9
2.5
1
02/19/19 09:39
02/19/19 17:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
79-34-5
Tetrachloroethene
ND
ug/kg
5.9
2.0
1
02/19/19 09:39
02/19/19 17:11
127-18-4
Toluene
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.9
2.6
1
02/19/19 09:39
02/19/19 17:11
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.9
1.9
1
02/19/19 09:39
02/19/19 17:11
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.9
2.5
1
02/19/19 09:39
02/19/19 17:11
79-00-5
Trichloroethene
ND
ug/kg
5.9
2.5
1
02/19/19 09:39
02/19/19 17:11
79-01-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MGN-002
Pace Project No.: 92418130
Sample: UST-10 Lab ID: 92418130003 Collected: 02/18/19 09:10 Received: 02/18/19 16:20 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 02/22/2019 12:51 PM
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
ND
ug/kg
5.9
2.6
1
02/19/19 09:39
02/19/19 17:11
75-69-4
ND
ug/kg
5.9
1.9
1
02/19/19 09:39
02/19/19 17:11
96-18-4
18.7
ug/kg
5.9
2.4
1
02/19/19 09:39
02/19/19 17:11
95-63-6
3.1J
ug/kg
5.9
2.1
1
02/19/19 09:39
02/19/19 17:11
108-67-8
ND
ug/kg
59.5
10.5
1
02/19/19 09:39
02/19/19 17:11
108-05-4 L1
ND
ug/kg
11.9
2.1
1
02/19/19 09:39
02/19/19 17:11
75-01-4
ND
ug/kg
11.9
4.3
1
02/19/19 09:39
02/19/19 17:11
1330-20-7
7.7J
ug/kg
11.9
4.3
1
02/19/19 09:39
02/19/19 17:11
179601-23-1
ND
ug/kg
5.9
2.3
1
02/19/19 09:39
02/19/19 17:11
95-47-6
99
%
70-130
1
02/19/19 09:39
02/19/19 17:11
2037-26-5
105
%
70-130
1
02/19/19 09:39
02/19/19 17:11
460-00-4
80
%
70-132
1
02/19/19 09:39
02/19/19 17:11
17060-07-0
Analytical Method: ASTM D2974-87
22.0 % 0.10 0.10 1 02/18/1917:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
QC Batch: 458880 Analysis Method: EPA 8260B
QC Batch Method: EPA 5035A Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92418130001, 92418130002, 92418130003
METHOD BLANK: 2501065 Matrix:
Associated Lab Samples: 92418130001, 92418130002, 92418130003
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.3
2.2
02/19/19 11:16
1,1,1-Trichloroethane
ug/kg
ND
5.3
1.9
02/19/19 11:16
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.3
2.0
02/19/19 11:16
1,1,2-Trichloroethane
ug/kg
ND
5.3
2.2
02/19/19 11:16
1,1-Dichloroethane
ug/kg
ND
5.3
1.6
02/19/19 11:16
1,1-Dichloroethene
ug/kg
ND
5.3
1.9
02/19/19 11:16
1,1-Dichloropropene
ug/kg
ND
5.3
1.6
02/19/19 11:16
1,2,3-Trichlorobenzene
ug/kg
ND
5.3
2.3
02/19/19 11:16
1,2,3-Trichloropropane
ug/kg
ND
5.3
1.7
02/19/19 11:16
1,2,4-Trichlorobenzene
ug/kg
ND
5.3
1.7
02/19/19 11:16
1,2,4-Trimethylbenzene
ug/kg
ND
5.3
2.1
02/19/19 11:16
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.3
3.8
02/19/19 11:16
1,2-Dibromoethane (EDB)
ug/kg
ND
5.3
1.9
02/19/19 11:16
1,2-Dichlorobenzene
ug/kg
ND
5.3
2.0
02/19/19 11:16
1,2-Dichloroethane
ug/kg
ND
5.3
2.3
02/19/19 11:16
1,2-Dichloropropane
ug/kg
ND
5.3
1.8
02/19/19 11:16
1,3,5-Trimethylbenzene
ug/kg
ND
5.3
1.9
02/19/19 11:16
1,3-Dichlorobenzene
ug/kg
ND
5.3
2.1
02/19/19 11:16
1,3-Dichloropropane
ug/kg
ND
5.3
2.0
02/19/19 11:16
1,4-Dichlorobenzene
ug/kg
ND
5.3
1.8
02/19/19 11:16
2,2-Dichloropropane
ug/kg
ND
5.3
1.8
02/19/19 11:16
2-Butanone (MEK)
ug/kg
ND
106
3.1
02/19/19 11:16
2-Chlorotoluene
ug/kg
ND
5.3
1.8
02/19/19 11:16
2-Hexanone
ug/kg
ND
53.1
4.1
02/19/19 11:16
4-Chlorotoluene
ug/kg
ND
5.3
1.9
02/19/19 11:16
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
53.1
3.9
02/19/19 11:16
Acetone
ug/kg
ND
106
10.6
02/19/19 11:16
Benzene
ug/kg
ND
5.3
1.7
02/19/19 11:16
Bromobenzene
ug/kg
ND
5.3
2.1
02/19/19 11:16
Bromochloromethane
ug/kg
ND
5.3
1.8
02/19/19 11:16
Bromodichloromethane
ug/kg
ND
5.3
2.0
02/19/19 11:16
Bromoform
ug/kg
ND
5.3
2.4
02/19/19 11:16
Bromomethane
ug/kg
ND
10.6
2.7
02/19/19 11:16
Carbon tetrachloride
ug/kg
ND
5.3
2.8
02/19/19 11:16
Chlorobenzene
ug/kg
ND
5.3
2.0
02/19/19 11:16
Chloroethane
ug/kg
ND
10.6
2.5
02/19/19 11:16
Chloroform
ug/kg
ND
5.3
1.7
02/19/19 11:16
Chloromethane
ug/kg
ND
10.6
2.5
02/19/19 11:16
cis-1,2-Dichloroethene
ug/kg
ND
5.3
1.5
02/19/19 11:16
cis-1,3-Dichloropropene
ug/kg
ND
5.3
1.9
02/19/19 11:16
Dibromochloromethane
ug/kg
ND
5.3
1.9
02/19/19 11:16
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
METHOD BLANK: 2501065 Matrix:
Associated Lab Samples: 92418130001, 92418130002, 92418130003
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromomethane
ug/kg
ND
5.3
2.7
02/19/19 11:16
Dichlorodifluoromethane
ug/kg
ND
10.6
3.8
02/19/19 11:16
Diisopropyl ether
ug/kg
ND
5.3
1.8
02/19/19 11:16
Ethylbenzene
ug/kg
ND
5.3
1.9
02/19/19 11:16
Hexachloro-1,3-butadiene
ug/kg
ND
5.3
2.1
02/19/19 11:16
Isopropylbenzene (Cumene)
ug/kg
ND
5.3
2.0
02/19/19 11:16
m&p-Xylene
ug/kg
ND
10.6
3.8
02/19/19 11:16
Methyl-tert-butyl ether
ug/kg
ND
5.3
1.6
02/19/19 11:16
Methylene Chloride
ug/kg
ND
21.2
3.2
02/19/19 11:16
n-Butylbenzene
ug/kg
ND
5.3
1.9
02/19/19 11:16
n-Propylbenzene
ug/kg
ND
5.3
1.8
02/19/19 11:16
Naphthalene
ug/kg
ND
5.3
1.3
02/19/19 11:16
o-Xylene
ug/kg
ND
5.3
2.0
02/19/19 11:16
p-Isopropyltoluene
ug/kg
ND
5.3
1.8
02/19/19 11:16
sec-Butylbenzene
ug/kg
ND
5.3
1.7
02/19/19 11:16
Styrene
ug/kg
ND
5.3
1.9
02/19/19 11:16
tert-Butyl benzene
ug/kg
ND
5.3
2.1
02/19/19 11:16
Tetrachloroethene
ug/kg
ND
5.3
1.8
02/19/19 11:16
Toluene
ug/kg
ND
5.3
1.9
02/19/19 11:16
trans-1,2-Dichloroethene
ug/kg
ND
5.3
2.0
02/19/19 11:16
trans- 1,3-Dichloropropene
ug/kg
ND
5.3
1.6
02/19/19 11:16
Trichloroethene
ug/kg
ND
5.3
2.2
02/19/19 11:16
Trichlorofluoromethane
ug/kg
ND
5.3
2.3
02/19/19 11:16
Vinyl acetate
ug/kg
ND
53.1
9.3
02/19/19 11:16
Vinyl chloride
ug/kg
ND
10.6
1.9
02/19/19 11:16
Xylene (Total)
ug/kg
ND
10.6
3.8
02/19/19 11:16
1,2-Dichloroethane-d4 (S)
%
77
70-132
02/19/19 11:16
4-Bromofluorobenzene (S)
%
108
70-130
02/19/19 11:16
Toluene-d8 (S)
%
116
70-130
02/19/19 11:16
Qualifiers
LABORATORY CONTROL SAMPLE:
2501066
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
52.9
62.6
118
70-130
1,1,1-Trichloroethane
ug/kg
52.9
64.3
122
70-130
1,1,2,2-Tetrachloroethane
ug/kg
52.9
63.9
121
55-130
1,1,2-Trichloroethane
ug/kg
52.9
66.0
125
70-130
1,1-Dichloroethane
ug/kg
52.9
57.9
110
68-130
1,1-Dichloroethene
ug/kg
52.9
58.0
110
70-130
1,1-Dichloropropene
ug/kg
52.9
56.2
106
70-130
1,2,3-Trichlorobenzene
ug/kg
52.9
64.3
122
70-130
1,2,3-Trichloropropane
ug/kg
52.9
65.9
125
70-130
1,2,4-Trichlorobenzene
ug/kg
52.9
65.9
125
70-130
1,2,4-Trimethylbenzene
ug/kg
52.9
64.8
123
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
LABORATORY CONTROL SAMPLE:
Parameter
2501066
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/kg
52.9
69.8
132
57-141
1,2-Dibromoethane (EDB)
ug/kg
52.9
64.3
122
70-130
1,2-Dichlorobenzene
ug/kg
52.9
65.4
124
70-130
1,2-Dichloroethane
ug/kg
52.9
61.1
116
70-130
1,2-Dichloropropane
ug/kg
52.9
64.2
121
70-130
1,3,5-Trimethylbenzene
ug/kg
52.9
65.1
123
70-130
1,3-Dichlorobenzene
ug/kg
52.9
64.7
122
70-130
1,3-Dichloropropane
ug/kg
52.9
59.6
113
70-130
1,4-Dichlorobenzene
ug/kg
52.9
64.5
122
70-130
2,2-Dichloropropane
ug/kg
52.9
64.7
122
70-130
2-Butanone (MEK)
ug/kg
106
117
111
60-130
2-Chlorotoluene
ug/kg
52.9
63.8
121
70-130
2-Hexanone
ug/kg
106
139
132
70-132
4-Chlorotoluene
ug/kg
52.9
64.2
122
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
106
129
122
69-130
Acetone
ug/kg
106
121
114
49-148
Benzene
ug/kg
52.9
61.4
116
70-130
Bromobenzene
ug/kg
52.9
62.9
119
70-130
Bromochloromethane
ug/kg
52.9
58.6
111
70-130
Bromodichloromethane
ug/kg
52.9
65.7
124
70-130
Bromoform
ug/kg
52.9
65.8
125
68-136
Bromomethane
ug/kg
52.9
57.7
109
60-140
Carbon tetrachloride
ug/kg
52.9
61.7
117
70-130
Chlorobenzene
ug/kg
52.9
60.7
115
70-130
Chloroethane
ug/kg
52.9
58.4
110
51-147
Chloroform
ug/kg
52.9
56.5
107
70-130
Chloromethane
ug/kg
52.9
51.3
97
48-130
cis-1,2-Dichloroethene
ug/kg
52.9
58.1
110
70-130
cis-1,3-Dichloropropene
ug/kg
52.9
59.9
113
70-130
Dibromochloromethane
ug/kg
52.9
60.2
114
70-130
Dibromomethane
ug/kg
52.9
59.2
112
70-130
Dichlorodifluoromethane
ug/kg
52.9
56.2
106
49-130
Diisopropyl ether
ug/kg
52.9
53.9
102
66-130
Ethylbenzene
ug/kg
52.9
61.9
117
70-130
Hexachloro-1,3-butadiene
ug/kg
52.9
63.5
120
70-130
Isopropylbenzene (Cumene)
ug/kg
52.9
63.4
120
70-130
m&p-Xylene
ug/kg
106
121
115
70-130
Methyl-tert-butyl ether
ug/kg
52.9
54.4
103
70-130
Methylene Chloride
ug/kg
52.9
53.8
102
50-137
n-Butylbenzene
ug/kg
52.9
66.9
127
70-130
n-Propylbenzene
ug/kg
52.9
64.2
121
70-130
Naphthalene
ug/kg
52.9
67.3
127
70-131
o-Xylene
ug/kg
52.9
61.7
117
70-130
p-Isopropyltoluene
ug/kg
52.9
65.3
123
70-130
sec-Butylbenzene
ug/kg
52.9
65.1
123
70-130
Styrene
ug/kg
52.9
62.8
119
70-130
tert-Butyl benzene
ug/kg
52.9
63.1
119
69-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
LABORATORY CONTROL SAMPLE:
Parameter
2501066
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
ug/kg
52.9
36.7
69
56-130
Toluene
ug/kg
52.9
56.8
108
70-130
trans-1,2-Dichloroethene
ug/kg
52.9
59.1
112
70-130
trans- 1,3-Dichloropropene
ug/kg
52.9
61.9
117
70-130
Trichloroethene
ug/kg
52.9
59.3
112
70-141
Trichlorofluoromethane
ug/kg
52.9
55.7
105
67-130
Vinyl acetate
ug/kg
106
148
140
10-136 L1
Vinyl chloride
ug/kg
52.9
55.7
105
67-130
Xylene (Total)
ug/kg
159
183
115
70-130
1,2-Dichloroethane-d4 (S)
%
103
70-132
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE SAMPLE:
Parameter
2501068
Units
92418130001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
27
25.6
95
52-133
1,1,1-Trichloroethane
ug/kg
ND
27
26.2
97
49-137
1,1,2,2-Tetrachloroethane
ug/kg
ND
27
28.3
105
39-150
1,1,2-Trichloroethane
ug/kg
ND
27
26.3
97
48-140
1,1-Dichloroethane
ug/kg
ND
27
27.7
103
46-135
1,1-Dichloroethene
ug/kg
ND
27
29.5
109
38-149
1,1-Dichloropropene
ug/kg
ND
27
21.4
79
41-140
1,2,3-Trichlorobenzene
ug/kg
ND
27
21.5
80
10-158
1,2,3-Trichloropropane
ug/kg
ND
27
27.4
102
33-157
1,2,4-Trichlorobenzene
ug/kg
ND
27
21.5
80
10-155
1,2,4-Trimethylbenzene
ug/kg
ND
27
25.0
93
24-154
1,2-Dibromo-3-chloropropane
ug/kg
ND
27
25.3
94
33-158
1,2-Dibromoethane (EDB)
ug/kg
ND
27
23.7
88
40-136
1,2-Dichlorobenzene
ug/kg
ND
27
25.5
94
27-146
1,2-Dichloroethane
ug/kg
ND
27
25.8
96
49-140
1,2-Dichloropropane
ug/kg
ND
27
24.5
91
44-143
1,3,5-Trimethylbenzene
ug/kg
ND
27
25.2
94
40-144
1,3-Dichlorobenzene
ug/kg
ND
27
25.4
94
33-140
1,3-Dichloropropane
ug/kg
ND
27
22.9
85
47-147
1,4-Dichlorobenzene
ug/kg
ND
27
25.2
93
35-139
2,2-Dichloropropane
ug/kg
ND
27
25.6
95
41-140
2-Butanone (MEK)
ug/kg
ND
54
45.9J
85
10-181
2-Chlorotoluene
ug/kg
ND
27
27.0
100
38-147
2-Hexanone
ug/kg
ND
54
49.OJ
91
18-169
4-Chlorotoluene
ug/kg
ND
27
26.1
97
36-145
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
54
52.8J
98
16-175
Acetone
ug/kg
26.3J
54
1111
157
10-200
Benzene
ug/kg
ND
27
26.7
99
46-136
Bromobenzene
ug/kg
ND
27
25.2
93
38-149
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
MATRIX SPIKE SAMPLE:
2501068
92418130001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/kg
ND
27
25.5
95
44-142
Bromodichloromethane
ug/kg
ND
27
25.9
96
41-140
Bromoform
ug/kg
ND
27
25.7
95
34-145
Bromomethane
ug/kg
ND
27
33.1
123
14-162
Carbon tetrachloride
ug/kg
ND
27
26.5
98
44-141
Chlorobenzene
ug/kg
ND
27
26.8
99
39-141
Chloroethane
ug/kg
ND
27
33.8
125
10-182
Chloroform
ug/kg
ND
27
25.1
93
45-140
Chloromethane
ug/kg
ND
27
27.4
102
19-149
cis-1,2-Dichloroethene
ug/kg
ND
27
26.7
99
38-150
cis-1,3-Dichloropropene
ug/kg
ND
27
22.2
82
30-144
Dibromochloromethane
ug/kg
ND
27
23.6
88
36-145
Dibromomethane
ug/kg
ND
27
27.5
102
41-145
Dichlorodifluoromethane
ug/kg
ND
27
27.2
101
16-146
Diisopropyl ether
ug/kg
ND
27
24.0
89
41-143
Ethylbenzene
ug/kg
ND
27
28.4
105
35-144
Hexachloro-1,3-butadiene
ug/kg
ND
27
20.5
76
10-160
Isopropylbenzene (Cumene)
ug/kg
ND
27
29.2
108
30-152
m&p-Xylene
ug/kg
ND
54
57.3
106
33-145
Methyl-tert-butyl ether
ug/kg
ND
27
22.1
82
49-140
Methylene Chloride
ug/kg
ND
27
22.9J
85
10-174
n-Butylbenzene
ug/kg
ND
27
24.7
92
10-160
n-Propylbenzene
ug/kg
ND
27
27.3
101
24-159
Naphthalene
ug/kg
ND
27
23.0
85
10-171
o-Xylene
ug/kg
ND
27
28.4
105
31-150
p-Isopropyltoluene
ug/kg
ND
27
25.9
96
21-154
sec-Butylbenzene
ug/kg
ND
27
27.3
101
19-159
Styrene
ug/kg
ND
27
26.0
97
15-152
tert-Butyl benzene
ug/kg
ND
27
27.4
101
31-141
Tetrachloroethene
ug/kg
ND
27
16.1
60
19-141
Toluene
ug/kg
ND
27
28.5
106
31-146
trans-1,2-Dichloroethene
ug/kg
ND
27
26.5
98
28-157
trans- 1,3-Dichloropropene
ug/kg
ND
27
22.8
85
25-146
Trichloroethene
ug/kg
ND
27
22.8
85
34-149
Trichlorofluoromethane
ug/kg
ND
27
29.4
109
10-167
Vinyl acetate
ug/kg
ND
54
12.5J
23
10-200
Vinyl chloride
ug/kg
ND
27
29.3
108
36-155
Xylene (Total)
ug/kg
ND
80.9
85.7
106
29-148
1,2-Dichloroethane-d4 (S)
%
96
70-132
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
103
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
SAMPLE DUPLICATE: 2501067
Parameter
Units
92418104001
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
ND
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
ND
ND
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
SAMPLE DUPLICATE: 2501067
Parameter
Units
92418104001
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
79
81
4-Bromofluorobenzene (S)
%
106
109
Toluene-d8 (S)
%
116
114
Max
RPD RPD Qualifiers
9
9
5
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 45

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
QC Batch: 459014 Analysis Method: EPA 8270D
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92418130001, 92418130002, 92418130003
METHOD BLANK: 2501730 Matrix:
Associated Lab Samples: 92418130001, 92418130002, 92418130003
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
328
63.6
02/20/19 14:54
1,2-Dichlorobenzene
ug/kg
ND
328
87.4
02/20/19 14:54
1,3-Dichlorobenzene
ug/kg
ND
328
74.5
02/20/19 14:54
1,4-Dichlorobenzene
ug/kg
ND
328
92.4
02/20/19 14:54
1-Methylnaphthalene
ug/kg
ND
328
85.4
02/20/19 14:54
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
328
87.4
02/20/19 14:54
2,4,5-Trichlorophenol
ug/kg
ND
328
101
02/20/19 14:54
2,4,6-Trichlorophenol
ug/kg
ND
328
72.5
02/20/19 14:54
2,4-Dichlorophenol
ug/kg
ND
328
71.5
02/20/19 14:54
2,4-Dimethylphenol
ug/kg
ND
328
129
02/20/19 14:54
2,4-Dinitrophenol
ug/kg
ND
1640
53.6
02/20/19 14:54
2,4-Dinitrotoluene
ug/kg
ND
328
61.6
02/20/19 14:54
2,6-Dinitrotoluene
ug/kg
ND
328
68.5
02/20/19 14:54
2-Chloronaphthalene
ug/kg
ND
328
64.6
02/20/19 14:54
2-Chlorophenol
ug/kg
ND
328
89.4
02/20/19 14:54
2-Methylnaphthalene
ug/kg
ND
328
70.5
02/20/19 14:54
2-Methylphenol(o-Cresol)
ug/kg
ND
328
99.3
02/20/19 14:54
2-Nitroaniline
ug/kg
ND
1640
101
02/20/19 14:54
2-Nitrophenol
ug/kg
ND
328
79.5
02/20/19 14:54
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
328
129
02/20/19 14:54
3,3'-Dichlorobenzidine
ug/kg
ND
1640
71.5
02/20/19 14:54
3-Nitroaniline
ug/kg
ND
1640
89.4
02/20/19 14:54
4,6-Dinitro-2-methyl phenol
ug/kg
ND
656
65.6
02/20/19 14:54
4-Bromophenylphenyl ether
ug/kg
ND
328
59.6
02/20/19 14:54
4-ChIoro-3-methyl phenol
ug/kg
ND
656
67.5
02/20/19 14:54
4-Chloroaniline
ug/kg
ND
1640
91.4
02/20/19 14:54
4-Chlorophenylphenyl ether
ug/kg
ND
328
67.5
02/20/19 14:54
4-Nitroaniline
ug/kg
ND
656
92.4
02/20/19 14:54
4-Nitrophenol
ug/kg
ND
1640
58.6
02/20/19 14:54
Acenaphthene
ug/kg
ND
328
75.5
02/20/19 14:54
Acenaphthylene
ug/kg
ND
328
77.5
02/20/19 14:54
Aniline
ug/kg
ND
328
88.4
02/20/19 14:54
Anthracene
ug/kg
ND
328
73.5
02/20/19 14:54
Benzo(a)anthracene
ug/kg
ND
328
60.6
02/20/19 14:54
Benzo(a)pyrene
ug/kg
ND
328
62.6
02/20/19 14:54
Benzo(b)fluoranthene
ug/kg
ND
328
56.6
02/20/19 14:54
Benzo(g,h,i)perylene
ug/kg
ND
328
83.4
02/20/19 14:54
Benzo(k)fluoranthene
ug/kg
ND
328
64.6
02/20/19 14:54
Benzoic Acid
ug/kg
ND
1640
59.6
02/20/19 14:54
Benzyl alcohol
ug/kg
ND
656
65.6
02/20/19 14:54
bis(2-Chloroethoxy)methane
ug/kg
ND
328
76.5
02/20/19 14:54
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
METHOD BLANK: 2501730 Matrix:
Associated Lab Samples: 92418130001, 92418130002, 92418130003
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
bis(2-Chloroethyl) ether
ug/kg
ND
328
83.4
02/20/19 14:54
bis(2-Ethylhexyl)phthalate
ug/kg
ND
328
89.4
02/20/19 14:54
Butylbenzylphthalate
ug/kg
ND
328
69.5
02/20/19 14:54
Chrysene
ug/kg
ND
328
43.7
02/20/19 14:54
Di-n-butylphthalate
ug/kg
ND
328
53.6
02/20/19 14:54
Di-n-octylphthalate
ug/kg
ND
328
68.5
02/20/19 14:54
Dibenz(a,h)anthracene
ug/kg
ND
328
69.5
02/20/19 14:54
Dibenzofuran
ug/kg
ND
328
53.6
02/20/19 14:54
Diethylphthalate
ug/kg
ND
328
50.7
02/20/19 14:54
Dimethylphthalate
ug/kg
ND
328
66.6
02/20/19 14:54
Fluoranthene
ug/kg
ND
328
47.7
02/20/19 14:54
Fluorene
ug/kg
ND
328
67.5
02/20/19 14:54
Hexachloro-1,3-butadiene
ug/kg
ND
328
56.6
02/20/19 14:54
Hexachlorobenzene
ug/kg
ND
328
41.7
02/20/19 14:54
Hexachlorocyclopentadiene
ug/kg
ND
328
60.6
02/20/19 14:54
Hexachloroethane
ug/kg
ND
328
86.4
02/20/19 14:54
Indeno(1,2,3-cd)pyrene
ug/kg
ND
328
67.5
02/20/19 14:54
Isophorone
ug/kg
ND
328
73.5
02/20/19 14:54
N-Nitroso-di-n-propylamine
ug/kg
ND
328
62.6
02/20/19 14:54
N-Nitrosodimethylamine
ug/kg
ND
328
106
02/20/19 14:54
N-Nitrosodiphenylamine
ug/kg
ND
328
97.4
02/20/19 14:54
Naphthalene
ug/kg
ND
328
80.5
02/20/19 14:54
Nitrobenzene
ug/kg
ND
328
89.4
02/20/19 14:54
Pentachlorophenol
ug/kg
ND
1640
59.6
02/20/19 14:54
Phenanthrene
ug/kg
ND
328
54.6
02/20/19 14:54
Phenol
ug/kg
ND
328
98.3
02/20/19 14:54
Pyrene
ug/kg
ND
328
55.6
02/20/19 14:54
2,4,6-Tribromophenol (S)
%
76
27-110
02/20/19 14:54
2-Fluorobiphenyl (S)
%
75
30-110
02/20/19 14:54
2-Fluorophenol(S)
%
79
13-110
02/20/19 14:54
Nitrobenzene-d5 (S)
%
79
23-110
02/20/19 14:54
Phenol-d6 (S)
%
80
22-110
02/20/19 14:54
Terphenyl-d14 (S)
%
84
28-110
02/20/19 14:54
Qualifiers
LABORATORY CONTROL SAMPLE:
2501731
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1680
1340
80
52-130
1,2-Dichlorobenzene
ug/kg
1680
1400
83
51-130
1,3-Dichlorobenzene
ug/kg
1680
1370
82
50-130
1,4-Dichlorobenzene
ug/kg
1680
1410
84
49-130
1-Methylnaphthalene
ug/kg
1680
1560
93
55-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1680
1510
90
30-130
2,4,5-Trichlorophenol
ug/kg
1680
1340
80
55-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
LABORATORY CONTROL SAMPLE:
Parameter
2501731
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,6-TrichIorophenol
ug/kg
1680
1450
86
57-130
2,4-DichIorophenol
ug/kg
1680
1430
86
56-130
2,4-Dimethylphenol
ug/kg
1680
1470
88
51-130
2,4-Dinitrophenol
ug/kg
8390
7060
84
27-133
2,4-Dinitrotoluene
ug/kg
1680
1450
87
61-130
2,6-Dinitrotoluene
ug/kg
1680
1540
91
60-130
2-Chloronaphthalene
ug/kg
1680
1610
96
52-130
2-Chlorophenol
ug/kg
1680
1430
85
54-130
2-Methylnaphthalene
ug/kg
1680
1540
92
54-130
2-Methylphenol(o-Cresol)
ug/kg
1680
1430
85
51-130
2-Nitroaniline
ug/kg
3360
2860
85
51-130
2-Nitrophenol
ug/kg
1680
1400
83
49-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1680
1430
86
11-163
3,3'-Dichlorobenzidine
ug/kg
3360
2630
78
10-132
3-Nitroaniline
ug/kg
3360
2880
86
55-130
4,6-Dinitro-2-methyl phenol
ug/kg
3360
2990
89
47-142
4-Bromophenylphenyl ether
ug/kg
1680
1410
84
59-130
4-Chloro-3-methylphenol
ug/kg
3360
2960
88
55-130
4-Chloroaniline
ug/kg
3360
2840
85
54-130
4-Chlorophenylphenyl ether
ug/kg
1680
1510
90
58-130
4-Nitroaniline
ug/kg
3360
2910
87
54-130
4-Nitrophenol
ug/kg
8390
7100
85
48-130
Acenaphthene
ug/kg
1680
1570
94
60-130
Acenaphthylene
ug/kg
1680
1660
99
60-130
Aniline
ug/kg
1680
1270
76
43-130
Anthracene
ug/kg
1680
1470
88
63-130
Benzo(a)anthracene
ug/kg
1680
1590
95
59-130
Benzo(a)pyrene
ug/kg
1680
1650
98
57-130
Benzo(b)fluoranthene
ug/kg
1680
1740
104
54-130
Benzo(g,h,i)perylene
ug/kg
1680
1630
97
59-130
Benzo(k)fluoranthene
ug/kg
1680
1630
97
54-130
Benzoic Acid
ug/kg
8390
6850
82
19-130
Benzyl alcohol
ug/kg
3360
2970
89
50-130
bis(2-Chloroethoxy)methane
ug/kg
1680
1470
88
54-130
bis(2-Chloroethyl) ether
ug/kg
1680
1450
87
48-130
bis(2-Ethylhexyl)phthalate
ug/kg
1680
1570
93
45-134
Butylbenzylphthalate
ug/kg
1680
1660
99
46-138
Chrysene
ug/kg
1680
1560
93
58-130
Di-n-butylphthalate
ug/kg
1680
1440
86
60-130
Di-n-octylphthalate
ug/kg
1680
1610
96
53-130
Dibenz(a,h)anthracene
ug/kg
1680
1610
96
59-130
Dibenzofuran
ug/kg
1680
1430
85
60-130
Diethylphthalate
ug/kg
1680
1490
89
60-130
Dimethylphthalate
ug/kg
1680
1480
88
60-130
Fluoranthene
ug/kg
1680
1470
88
65-130
Fluorene
ug/kg
1680
1580
94
63-130
Hexachloro-1,3-butadiene
ug/kg
1680
1350
80
46-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
LABORATORY CONTROL SAMPLE:
Parameter
2501731
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Hexachlorobenzene
ug/kg
1680
1370
81
58-130
Hexachlorocyclopentadiene
ug/kg
1680
1370
81
23-130
Hexachloroethane
ug/kg
1680
1370
82
47-130
Indeno(1,2,3-cd)pyrene
ug/kg
1680
1660
99
60-130
Isophorone
ug/kg
1680
1480
88
49-130
N-Nitroso-di-n-propylamine
ug/kg
1680
1500
90
47-130
N-Nitrosodimethylamine
ug/kg
1680
1460
87
45-130
N-Nitrosodiphenylamine
ug/kg
1680
1360
81
59-130
Naphthalene
ug/kg
1680
1540
92
55-130
Nitrobenzene
ug/kg
1680
1380
83
49-130
Pentachlorophenol
ug/kg
3360
2630
78
10-132
Phenanthrene
ug/kg
1680
1480
88
62-130
Phenol
ug/kg
1680
1490
89
46-130
Pyrene
ug/kg
1680
1710
102
53-130
2,4,6-Tribromophenol (S)
%
86
27-110
2-Fluorobiphenyl (S)
%
80
30-110
2-Fluorophenol(S)
%
88
13-110
Nitrobenzene-d5(S)
%
84
23-110
Phenol-d6 (S)
%
89
22-110
Terphenyl-d14 (S)
%
92
28-110
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MGN-002
Pace Project No.: 92418130
QC Batch: 458808 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92418130001, 92418130002, 92418130003
SAMPLE DUPLICATE: 2500894
92418090001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 0.10 ND 25
SAMPLE DUPLICATE: 2500895
92418129007 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 34.1 32.5 5 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: MGN-002
Pace Project No.: 92418130
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/22/2019 12:51 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 45

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MGN-002
Pace Project No.: 92418130
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92418130001
UST-7
EPA 3546
459014
EPA 8270D
459201
92418130002
UST-9
EPA 3546
459014
EPA 8270D
459201
92418130003
UST-10
EPA 3546
459014
EPA 8270D
459201
92418130001
UST-7
EPA 5035A
458880
EPA 8260B
458892
92418130002
UST-9
EPA 5035A
458880
EPA 8260B
458892
92418130003
UST-10
EPA 5035A
458880
EPA 8260B
458892
92418130001
UST-7
ASTM D2974-87
458808
92418130002
UST-9
ASTM D2974-87
458808
92418130003
UST-10
ASTM D2974-87
458808
Date: 02/22/2019 12:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 30 of 45

Laboratory receiving samples:
Asheville 0 Eden❑ Greenwood ❑ Huntersville Q Raleigh[] Mechanicsville[]
SampleClient Name: IWO# • 9241 V 13O
.. Receipt ` Project fi
I I I I
Courier: []Fed Ex []UPS ❑LISPS ❑Cllent III III I' I II II I1� II I III
Corti ❑ mercial ❑Pate other: 1�241$1;10 111 I 11
Custody Seal Present? ❑Yes []No . seats Intact? ❑Yes - -❑No
pate/Initials Person Examining Cantents:
Packing Material: ❑Bubble Wrap bubble Bags ❑None ❑ Other Biological Tissue Frozen?
❑Yes ❑No ❑N%A
ifierrnome 1l92TO48 Type of Ice: .Mwet []Blue ❑None
L. ❑IRGun ID;
Cooler Temp JT): ( Correction Factor: Add/Subtract (°C) 0.0
Temp should be above freezing to VC
Cooler temp Corrected (°C): []Samples out of temp criteria. Samples on ice, caoling process
has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the'United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
i IYPs l—ltdn including Hawaii and Puerto Rico)? []Yes . ❑No
Cam meets/Discrepancy:
Chain of Castbdy Present?
L[fYes
❑Na
❑NIA
1.
Samples Arrived within Hold lime?.yYes
[]No
El N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
❑No
❑NIA
3.
Rush Tern Around rime Requested?
[]Yes
[]No
❑NIA
4.
Sufficient Volume?
❑Yes
El No
❑NIA
5.
Correct Containers Used?
-Pace Containers Used?
[]yes
❑Yes
[]No
[]No
El N/A
El NIA
5.
Containers Intact?
❑Yes
❑No
El N/A
7.
Dissolved analysN: Samples Field Filtered?
[]Yes
❑No
.❑NIA
8.
Sample Labels Match COC?
-Includes Date/TiirneliD/Analysis Matrix:
[]Yes
❑No
[]NIA
9.
Headspace in VOA Vials (>S-timm)?
❑Yes
[]No_
NIA
Trip Blank Present?
Trip Blank Custody Seals Present?
[-]Yes
❑Yes
[]No
❑No
❑4/a
❑N/A
11.
COMMENTSI.SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? []Yes []No
Person contacted: Datelrime:
Project Manager SCURF Review: ��� Date. 2
c
Project Manager SRF_ Review:
Date:
Page 31 of 45

Sample Condition Upon Receipt(SCutt)
C�fjllc?I�'flCal Document No.: Issuing Authority:
r roe }•e nee o...1 nc pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorinatiort is
verified and within the acceptance range for Preservation
samples.
Exceptions: VOA,Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to iist number of bottle
Project # �Wo#� 3„ 813a
(W
PM: KRG Dupe Date: 02/25/19
CLIENT: 92—Hart Hick
E.
z
m
c
7
V
R
IL
E
to
,N-i
7
a
m
z
al
c
n
V
m
o.
E'
O
r�cv
7
M
m
z
V
�-
�
V
m
a
E
O
7
ry
m
,doY
at
aV'i
C CL
y
�,
r
r+
m
S
O
N
U
a
E
ut
cr
m
N
V
O
i
0
N
ro
a
J
E
O
LM
N
2
m
m
A
°
Z
a
�
++
Q
S
�
R
a
J
E
L
N
. N.
Q
m
�"
N
ri
A
2
S
Z
V
w
m
0.
J
E
-Ln
N
'i
U
v
m
m
N
¢
C_
a
_`m
m
V
�
a
E
l
_�a
u.
C7
Z
.�
y
Z
aN
C
�
°
¢
=
r{
]
t7
a
N
Y
a.
_
V
Y
a
¢
=
ri
Y
.{
C9
a
?
'O
a
ii
d-
v
a
E
o
N
r4
C7
a
N
V
S
O
N
�
a
E
m
y
ei
yr
l7
a
N
V V
Y 2
a
ci
r E
J
Ql E
E uoi
.4
"'�
E ran
Ln S>
N 6
ut 6
l7 l7
a a
Z
Y
�
S
p
>
J
E
d
V
x
d�
e7
A
Q
4r44r
Cn
Q
Cq
N
�
z
Q
a
J
E
p
h
m
l7
7
2
C
a
O
7
J
E
O
V
a�
l9
7
a
z
2 Ln
O
In
s Y
O a
>
J N
E �
0 La
d
oc a
q a
Q
z
Y
]
�+
d
w
a
en
Y
j
Q
U
ro
0.
�
E
sn
N
.�
F'
cn
n
t
Z
a
m
_
V
r'
G
o
Ln
N
Fc-
N
h
V
O
Z
u
h
a
J
E
L
ry
can
a
m
a
Z z
o
V
v v
N y
>
7
-0 Y .O
E E
Q Cn
1 J
E
o O a
n1 �i
7 7
O [7 ai
t7 En l7
Q > 0
2-
3
12
PH Adjustment Log for Preserved Samples
Sample la Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot k
adiwt I added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm will Ee sent to the North Carolina [IEHNR Certification Office (Le -
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 32 of 45

m T 3
n a
o
n m'
ni
s
o
m
oo
ti
m
m
A
w
N
s
ITEM #
��, 'm
o
v`--'
o
0 n
2
0
n
0 g
N NO
WM
V
L
0
v m
W
J
o,
y
3
O
Ci
•�
p, eSi
- 3
0
c n
m
_
n
r-
(_ '
`'
`.
m
tl
\
n
c a
?I
r
1 m
�.
F
q
-0 7? j)
i.= 0
.Ti
w in
o o
o
m
M m
_
2
#z y�
n, p
a
m
o
W
lip
m 0
�i
nl
O
I
z
MATRIXCODE (see valid codes to iefl)
A ,7�,
d
on
cC:-'
j
SAMPLE TYPE (G=GRAB C=COMP)
CD
3
s
m
a
x
L N
N
_
A
r"
"J"
rr,.
m
i.,
Irl
0
m
F"
M
�.
D
m
mJ
m
n
y
4
re
v
IN.
�0
_
f3i1
m
z
o
r4
z
0
m
SAMPLETEMPAT COLLECTION
M�
Rrl
D
A
n
rn
m,
n
c NmnpN
a OF
m
(�'
�?�
Unpreserved
N
M
m
o'
0
n
H2SO4
It
m
HNO3
�D
v
t
�
HGI
(D
w
R
v
l
�
NaOH
N
(D
f
—
—'
Na25203
N
j
t,
m
Methanol
f�
Other
ID
S
Analyses Test
YIN
m
'
8260f5035
o
D
o
m
n
a270
m
z
A
a
RCRA S Metals (602017471 )
m
7
-
W
5��
Q
y
t
Ao
_
m
3
3
Z
m
5
TEMP in C
`
�'
nA h ry
ic
Residual CHI Ine (YIN)
0
$
E
m
0
D
Received on
Ice
(YIN)
\
usto y
Sealed
cam'
O
Q
Cooler
\v
YIN
I
J
f
Samples
Intact
(YIN)
r"o
n
CD
nn
a
m
�• Z
O
ur �
0 n
a C
N• N
m -4
r 0
m
�D
n �
r
1
as
C
� p1
M
Z'<
.>
C
m
v SD
m CD
o. y
3v
O
Cr
C
a3
-a
m
C
0
0
C
d
rn
Page 33 of 45

O
�FaceAnalytical o
National Center for Testing & Innovation
P
a
ANALYTICAL REPORT
February 22, 2019
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1071961
Samples Received: 02/20/2019
Project Number: 92418130
Description: MGN-002
Site: 001
Report To: Kevin Godwin
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Entire Report Reviewed By: �vUnn �v, �. L
L111-�
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304.
V
it
Page 34 of 45

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Fn
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
SB-7 (6-8) L1071961-01
5
[Cn]
Qc: Quality Control Summary
6
Total Solids by Method 2540 G-2011
6
Fr
Mercury by Method 7471B
7
Metals (ICPMS) by Method 6020B
8
RC
Gl: Glossary of Terms
9
F
Al: Accreditations & Locations
10
Sc: Sample Chain of Custody
11
rAl
FSC
Page 35 of 45
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Pace Analytical - Huntersville, INC 92418130 L1071961
02/22/19 11:45
2 of 12

S13-7 (6-8) L1071961-01 Solid
SAMPLE
SUMMARY
Collected by
ONE LAB. NATIONWIDE.
Collected date/time Received date/time
02/18/1909:50 02/20/1909:45
FP1
Method
Batch
Dilution Preparation
Analysis
Analyst
date/time
date/time
FTC
Total Solids by Method 2540 G-2011
WG1240241
1 02/21/1912:31
02/21/1912:41
JD
Mercury by Method 7471B
WG1240058
1 02/20/1917:51
02/21/1910:20
ABL
Metals (ICPMS) by Method 6020B
WG1240206
5 02/21/19 09:46
02/21/1914:51
LAT
[Cn]
FSr
RC
F,
FAI
FSC
Page 36 of 45
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Pace Analytical - Huntersville, NC
92418130
L1071961
02/22/19 11:45
3 of 12

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
VV VV� � �t La�'_
Nancy McLain
Project Manager
FP1
FTC
FSS
FSr
FC-1
F,
FAI
FSC
Page 37 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92418130 L1071961 02/22/19 11:45 4 of 12

SB-7 (6-8)
Collected date/time: 02/18/19 09:50
Total Solids by Method 2540 G-2011
SAMPLE RESULTS - 01
L1071961
Result Qualifier Dilution Analysis
Analyte % date / time
Total Solids 81.3 1 02/21/201912:41
Mercury by Method 7471B
Batch
WG1240241
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date / time
Mercury
0.00781
J 0.00344
0.0246
1
02/21/201910:20
WG12400
Metals (ICPMS) by Method 6020B
Result (dry)
Qualifier MDL (dry)
RDL (dry)
Dilution
Analysis
Batch
Analyte
mg/kg
mg/kg
mg/kg
date/time
Arsenic
1.06
0.154
0.615
5
02/21/201914:51
WG12402
06
ONE LAB. NATIONWIDE.Cp2Tc3Ss58
1qc
06 Fq
06
06
06 FAI
06
06 FSC
Page 38 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92418130 L1071961 02/22/19 11:45 5 of 12
Page 38 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92418130 L1071961 02/22/19 11:45 5 of 12

WG1240241
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3386101-1 02/21/1912:41
MB Result MB Qualifier MB MDL
Analyte % %
Total Solids 0.00100
L1071692-03 Original Sample (OS) • Duplicate (DUP)
MB RDL
(OS) L1071692-03 02/21/19 12:41 • (DUP) R3386101-3 02/21/1912:41
Original Result DUP Result Dilution DUP RPD
Analyte % % %
Total Solids 87.2 87.2 1 0.00952
Laboratory Control Sample (LCS)
(LCS) R3386101-2 02/21/1912:41
Spike Amount LCS Result LCS Rec.
Analyte % %_ %
Total Solids 50.0 50.0 100
QUALITY CONTROL SUMMARY
L1071961-01
DUP Qualifier DUP RPD
Limits
10
Rec. Limits LCS Qualifier
o/
85.0-115
ONE LAB. NATIONWIDE.
- I
Cp
FTc
FSS
4
— Cn
FSr
— 7G1
FAI
[Sc
Page 39 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92418130 L1071961 02/22/19 11:45 6 of 12

WG1240058 QUALITY CONTROL SUMMARY
Mercury by Method 7471B L1071961-01
Method Blank (MB)
(MB) R3385789-1 02/21/19 09:09
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Mercury U 0.00280 0.0200
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3385789-2 02/21/19 09:11 • (LCSD) R3385789-3 02/21/19 09:14
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg % % % % %
Mercury 0.500 0.498 0.514 99.6 103 80.0-120 3.13 20
L1071638-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1071638-01 02/21/19 09:16 • (MS) R3385789-4 02/21/19 09:19 • (MSD) R3385789-5 02/21/19 09:22
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Mercury 0.500 ND 0.482 0.500 96.5 100 1 75.0-125 3.69
ONE LAB. NATIONWIDE.
RPD Limits
20
- I
Cp
FTc
FSS
4
— Cn
FSr
— 7G1
— $AI
[Sc
Page 40 of 45
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92418130 L1071961 02/22/19 11:45 7 of 12

WG1240206 QUALITY CONTROL SUMMARY
Metals (ICPMS) by Method 6020B L1071961-01
Method Blank (MB)
(MB) R3385852-1 02/21/1913:58
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
Arsenic U
0.125
0.500
Barium U
0.160
1.00
Cadmium U
0.0800
0.500
Chromium U
0.270
1.00
Lead U
0.120
0.500
Selenium U
0.190
0.500
Silver U
0.155
0.500
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3385852-2 02/21/1914:03 • (LCSD) R3385852-3 02/21/1914:07
Spike Amount
LCS Result
LCSD Result
LCS Rec.
Analyte
mg/kg
mg/kg
mg/kg
%
Arsenic
100
90.9
94.1
90.9
Barium
100
93.6
96.5
93.6
Cadmium
100
90.2
94.4
90.2
Chromium
100
93.0
96.2
93.0
Lead
100
92.8
99.8
92.8
Selenium
100
93.7
96.2
93.7
Silver
20.0
19.9
20.8
99.3
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
94.1
80.0-120
3.53
20
96.5
80.0-120
2.97
20
94.4
80.0-120
4.56
20
96.2
80.0-120
3.30
20
99.8
80.0-120
7.27
20
96.2
80.0-120
2.63
20
104
80.0-120
4.88
20
L1071849-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1071849-01 02/21/1914:11 • (MS) R3385852-6 02/21/1914:24 • (MSD) R3385852-7 02/21/1914:29
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
Arsenic
20.0
18.1
110
104
92.3
85.6
Barium
20.0
439
563
546
124
106
Cadmium
20.0
24.8
124
118
99.2
92.8
Chromium
20.0
86.7
176
163
89.7
76.3
Lead
20.0
1240
1380
1250
144
14.0
Selenium
20.0
4.92
95.3
89.0
90.4
84.1
Silver
4.00
2.55
23.0
22.2
102
98.2
Dilution Rec. Limits
5 75.0-125
5 75.0-125
5 75.0-125
5 75.0-125
5 75.0-125
5 75.0-125
5 75.0-125
ONE LAB. NATIONWIDE.
MS Qualifier MSD Qualifier RPD RPD Limits
6.27 20
3.21 20
5.26 20
7.92 20
V V
9.86 20
6.84 20
3.38 20
FP1
FTc
FSS
4
Cn
FSr
7G1
FAI
[Sc
ACCOUNT: PROJECT: SDG:
Pace Analytical - Huntersville, NC 92418130 L1071961
Page 41 of 45
DATE/TIME: PAG E:
02/22/19 11:45 8 of 12

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
and Definitions
CP
IP
FTCAbbreviations
(dry)
Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
FS
MDL (dry)
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
[Cn]
RDL (dry)
Reported Detection Limit.
Rec.
Recovery.
Fr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
U
Not detected at the Reporting Limit (or MDL where applicable).
Fc
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
9
duplicated within these ranges.
SC
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
v
The sample concentration is too high to evaluate accurate spike recoveries.
Page 42 of 45
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville,
INC 92418130 L1071961 02/22/19 11:45 9 of 12

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT NO
OR MN
T ID T WI NY
SD
WY MI
NV
T NE IA OH T PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
W 11110
� NM O� AR N Sc
T MS A`7L GA
T TX * LA
T
AK T T
q FL
wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME:
Pace Analytical - Huntersville, NC 92418130 L1071961 02/22/19 11:45
ME
Page 43 of 45
PAGE:
10 of 12

Chain of Custody
aceAnafytical
C 33 wwwpaaelabs cam
cJ !
Workorder: 92418130 Workorder Name: MGN-002 Results Requested By: 2/25/2019
Report I Invoice To
Subcontract To
Re nested Analysis
Kevin Godwin
Pace Analytical Charlotte
�] j
e P.O.
9800 Kincey Ave. Suite 100
r2,—1
Huntersville, NC 28078
Phone [phone]
�� �� l� ^,(/ 3�/
Email: [e-mail]
U
State of Sample Origin: NC
Preserved Containers
a
n
a
0
Collect
�
mL
o
10 11
Item
Sample ID
DatelTime
Lab ID
Matrix
LAB USE ONLY
1
SB-7 (6-8)
2/18/2019 09:50
92418130001
Solid
X
2
3
4
5
Comments
Transfers
Released By
Date./Time
Received By
Date/Time
t t� L
1
-7 -7
2
3
Cooler Temperature on Receipt Qqh{h
°C Custody Seal Y or Nj
Received on Ice
Y or N
Samples Intact Y or N
qi�.l" U 1 1 LI i[�—i
F23
Tuesday, February 19, 2019 7:51:07 AM FMT-ALL-C-002rev.00 24March2009 Pag�,J$,of4}� 1

Pace Analytical Nationalfor •
Cooler Receipt F•
Client: ppsc(, SDG#:
•
Cooler Received/Opened On: 2 / A/19 Temperature:
Y� f
Received By: Jeremy Webb
Signature:
Receipt Check List NF
Yes
No
COC Seal Present / Intact?
COC Signed / Accurate?
Bottles arrive intact?
Correct bottles used?
f'
Sufficient volume sent?
If Applicable
VOA Zero headspace?
Preservation Correct / Checked?
Page 45 of 45