08026_Fulflex Inc_Groundwater Monitoring Report_2019.01.29

Via Email and US Mail
January 29, 2019
North Carolina Department of Environmental Quality 1636 Mail Service Center
Raleigh, NC 27699-1636
Attention: Ms. Shristi Shrestha
Re: Groundwater Monitoring Report
Former Fulflex, Inc. Facility Scotland Neck, North Carolina Site ID Number NCD067187302 UIC Permit WI0500168 H&H Job No. FUL-006
Dear Shristi:
On behalf of Fulflex, Inc., Hart & Hickman, PC (H&H) is submitting the attached Groundwater
Monitoring Report for the former Fulflex facility located at 500 E 7th Street in Scotland Neck,
Halifax County, North Carolina.
If you have any questions concerning this information, please feel free to contact me.
Sincerely,
Hart & Hickman, PC
Matt Bramblett, PE
Principal
cc: Mr. Pete Johnson, Fulflex (via mail and email) Mr. Eric Rice, DEQ RRO (via email)
Mr. Andrew Rodak, D&D (via email)
#C-1269 Engineering #-245 Geology
Groundwater Monitoring Report
Former Fulflex Facility
IHSB # NCD067187302
Scotland Neck, North Carolina
H&H Job No. FUL-006
January 29, 2019
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Groundwater Monitoring Report Former Fulflex Facility
Scotland Neck, North Carolina H&H Job No. FUL-006
Table of Contents
Section Page No.
1.0 Introduction .............................................................................................................................1
1.1 Site History ............................................................................................................................1
1.2 Historical Remedial Activities ..............................................................................................2
2.0 Semi-Annual Groundwater Monitoring ...............................................................................5
2.1 Groundwater Elevation Data .................................................................................................5
2.2 Groundwater Sampling Procedures .......................................................................................5
2.3 Groundwater Analytical Results – VOCs ..............................................................................6
2.4 Groundwater Analytical Results – 1,4-Dioxane ....................................................................8
2.5 Groundwater Analytical Results – RCRA Metals .................................................................9
2.6 Groundwater Analytical Results – Injection Related and Geochemical Parameters...........10
2.7 Investigation Derived Waste ...............................................................................................12
3.0 Summary ................................................................................................................................13

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List of Tables

Table 1 Groundwater Monitoring Program
Table 2 Monitoring Well Construction and Water Level Measurements
Table 3 Groundwater Analytical Detections – October 2018
Table 4 RCRA Metals Results for Injection Area Wells
List of Figures
Figure 1 Site Location Map
Figure 2 Site Plan
Figure 3 Water Supply Well Location Map
Figure 4 PersulfOx Injection Well Locations
Figure 5 Shallow Groundwater Elevations (October 2018)
Figure 6 Post-PersulfOx Injection 1,1-DCE Groundwater Concentrations (October 2018)
Figure 7 Post-PersulfOx Injection 1,1,1-TCA Groundwater Concentrations (October 2018)
Figure 8 1,1-DCE Concentrations in Groundwater (October 2018)
Figure 9 1,4-Dioxane Concentrations in Groundwater (October 2018)
Figure 10 RCRA Metal Concentrations in Groundwater (October 2018)

List of Appendices Appendix A Groundwater Sampling Forms
Appendix B Laboratory Analytical Data
Appendix C Historical Groundwater Analytical Results Table
Appendix D Concentration vs Time Graphs
Appendix E IDW Disposal Documentation

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Groundwater Monitoring Report Former Fulflex Facility
Scotland Neck, North Carolina H&H Job No. FUL-006 1.0 Introduction
This report presents the results of groundwater monitoring activities conducted by
Hart & Hickman, PC (H&H) at the former Fulflex facility located at 500 East 7th Street in
Scotland Neck, North Carolina. Groundwater sampling has historically been conducted to monitor
volatile organic compound (VOC) concentrations as required by the North Carolina Department
of Environmental Quality (DEQ) Underground Injection Control (UIC) permits. Per the previous
UIC permit (Dated November 29th 2013, Permit number: WI0500168), H&H completed
three activated sodium persulfate solution (PersulfOx™) injections in March and April 2014 to
further remediate VOC-impacted groundwater in the vicinity of the former knife room (near
monitoring well MW-8). One year of quarterly post-injection groundwater monitoring followed
by semi-annual monitoring is required under the UIC permit. The year of quarterly post-injection
monitoring was completed between March 2014 and March 2015. This report describes the
eighth semi-annual sampling event, which was conducted in October 2018.

A site location map is provided as Figure 1. A site plan depicting the site and pertinent on-site
features is provided as Figure 2. The NC DEQ Facility ID number is NCD067187302. The site
is also in the NC DEQ Brownfields Program (08026-04-042).
1.1 Site History
The former Fulflex facility was used for the manufacturing of rubber products from the late 1960s
until it closed in 2002. The property is currently owned and occupied by AirBoss Rubber
Compounding, Inc. (AirBoss), a custom rubber manufacturer. Groundwater at the site is
impacted by chlorinated solvents, primarily 1,1,1-trichloroethane (1,1,1-TCA) and
1,1-dichloroethene (1,1-DCE), and the associated VOC 1,4-dioxane. 1,1,1-TCA was historically
used for cleaning industrial knives in the center of the manufacturing building in a room known as
the “knife room” (Figure 4). 1,1-DCE in groundwater is suspected to be an abiotic degradation
product of 1,1,1-TCA. 1,4-dioxane was previously used as a stabilizer for 1,1,1-TCA. The highest

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concentrations of chlorinated solvents in groundwater are detected in the vicinity of the former
knife room. 1,1-DCE impacts had historically migrated to a downgradient water supply well.
However, downgradient water supply wells of concern have since been abandoned (Figure 3).
1.2 Historical Remedial Activities

Fulflex previously conducted interim corrective action measures comprised of chemical oxidation
via injection of sodium persulfate in January and February 2005 to address the chlorinated solvent
impacts. The injection was conducted in an approximate 125 feet (ft) by 60 feet area in the vicinity
and downgradient of the former knife room. Downgradient of the knife room, 1,1-DCE impacts
exceeding North Carolina Administrative Code (NCAC) 2L groundwater standards (2L Standards)
were more widespread than 1,1,1-TCA exceedances. The injection treated both the source area
and the area of the highest 1,1-DCE concentrations. The injection process and subsequent
sampling events were documented in the Report of Post Injection Groundwater Monitoring dated
October 21, 2005.

In general, the sodium persulfate injection significantly reduced the mass of VOCs in groundwater
at the site. In particular, the concentration of the primary contaminant of concern (COC), 1,1-DCE,
was reduced in the vicinity of the former knife room from a high of 390,000 micrograms per liter
(µg/l) to non-detect (<1,000 µg/l) in January 2007. Significant reductions were also noted
downgradient of the source area compared to pre-injection concentrations. Concentrations of
1,1,1,-TCA downgradient of the knife room were reduced (although to a lesser extent than
1,1-DCE). However, high concentrations of 1,1,1-TCA remained in the former knife room area.

A limited membrane interface probe (MIP) investigation was conducted in August 2007 in the
former knife room area to estimate the vertical and horizontal distribution of the remaining
contaminant mass in relation to subsurface geology. The MIP investigation confirmed that the
majority of the remaining contaminant mass was in the immediate vicinity of the former knife
room in the 8 ft to 20 ft below ground surface (bgs) depth interval. Based on the MIP results,
additional chemical oxidant injections were conducted to address 1,1,1-TCA (and other
chlorinated solvent) concentrations in the vicinity of the former knife room.

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Two RegenOx™ injections were conducted in December 2007 in the immediate vicinity of
monitoring well MW-8, including the area of the former floor drain and sink areas of the former
knife room. A third RegenOx™ injection was conducted in the same vicinity in December 2008,
followed by a fourth injection in this area in February 2009.

At each location, the injection point consisted of a shallow injection interval (8 ft to 15 ft) and a
deeper injection interval (15 ft to 22 ft). RegenOx™ was selected as the chemical oxidant because
it is capable of treating a broad range of contaminants including 1,1,1-TCA and 1,1-DCE.

The UIC permit allowed for up to five injections of RegenOx™ to address residual VOC impacts
in the immediate vicinity of the former knife room (near MW-8). However, after four RegenOx™
injection events, the higher 1,1,1-TCA concentrations in MW-8 were sustained and the
fifth RegenOx™ injection event was not conducted. Performance monitoring was conducted on
a quarterly and then semi-annual basis to evaluate the effects of the RegenOx™ injections.

In 2013, the UIC permit was renewed and approved under the current UIC Permit (WI0500168)
for the injection of a catalyst-activated sodium persulfate solution (known as PersulfOx™).
PersulfOx™ was selected as the oxidant due to the relative success of the 2005 persulfate injection.
The catalyst was sodium hydroxide (NaOH). Eight permanent injection wells were installed
within a close area surrounding monitoring well MW-8 (Figure 4).

The oxidant mixture was injected into the subsurface over the course of three injection events
between March and April 2014. During these injections, field parameters did not indicate good
connectivity between the injection wells and source area monitoring well MW-8. Based on the
poor connectivity with the formation, MW-8 was abandoned and replaced with MW-8R to
continue monitoring the efficacy of the PersulfOx™ injection within the source area. The location
of MW-8R was installed approximately 4 ft south of MW-8 (Figure 4). The injections were
summarized in the PersulfOx™ Injection and Groundwater Monitoring Report dated
November 18, 2014.

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The UIC permit was renewed on August 7, 2018 and authorizes the injection of Klozur® SP
(sodium persulfate) and hydrogen peroxide. An injection event is planned during the first half of
2019.

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2.0 Semi-Annual Groundwater Monitoring
A semi-annual groundwater monitoring event was conducted by H&H in October 2018 to evaluate
groundwater conditions. H&H sampled on-site monitoring wells MW-1 through MW-10, MW-13,
MW-18, MW-19 and off-site monitoring wells MW-14, MW-15, MW-16, MW-17, MW-17D, and
MW-17DD. The semi-annual monitoring event included collection of water level elevations and
analysis of groundwater samples, as discussed below. A summary of the groundwater monitoring
program is provided as Table 1.
2.1 Groundwater Elevation Data
Water levels in the on-site and off-site monitoring wells were gauged on October 4, 2018. Current
and limited historical groundwater elevation data are summarized in Table 2. The October 2018
shallow groundwater elevation data are presented on Figure 5. The water levels may not have
been at equilibrium at the time of this gauging event. Based on historical results, the groundwater
flow direction is generally to the south and southwest. The October 2018 water levels were
approximately 3 ft lower compared to the levels in March 2018, which is attributed to seasonal
fluctuation.

2.2 Groundwater Sampling Procedures

During the monitoring event, sampled monitoring wells were purged using low-flow, low-volume
sampling methods with a peristaltic pump and dedicated tubing until field measurements of pH,
temperature, dissolved oxygen (DO), oxidation-reduction potential (ORP), specific conductivity,
and turbidity stabilized. Field parameters were measured using a YSI Pro Plus multi-meter with a
flow-through cell and Hach and MicroTPI Turbidimeters. Groundwater low-flow sampling
records are provided in Appendix A.

Upon stabilization of field parameters, groundwater samples were collected in laboratory-supplied
sample bottles. A chain-of-custody record was completed for samples collected and included
sample description, date collected, time collected, matrix, sample container information, and
analyses required. The chain-of-custody was signed by H&H and placed along with the samples
in iced coolers for delivery to the analytical laboratory. The coolers were sealed with a H&H

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representative’s signature and date such that potential disturbance of the cooler contents could be
detected by the laboratory.

The groundwater samples were analyzed by Pace Analytical Services Inc. (Pace) of Huntersville,
NC, a NC certified laboratory. Table 1 summarizes analytical parameters that are monitored, and
specific analytical methods are provided on Table 3. The laboratory report for the October 2018
monitoring event is provided in Appendix B.

2.3 Groundwater Analytical Results – VOCs

October 2018 Semi-Annual Results
VOCs were detected in groundwater above 2L Standards in ten of the 19 monitoring wells sampled
in October 2018 (Table 3), including source area well MW-8R. Historically, the primary
compounds of concern at the site have been 1,1,1-TCA, 1,1-DCE, and 1,4-dioxane. Source area
monitoring well MW-8R contained 1,1,1-TCA at a concentration of 24,900 µg/l, which exceeds
the 2L Standard of 200 µg/l. 1,1-DCE was detected in groundwater above its 2L Standard of
350 µg/l in monitoring wells MW-8R (2,770 µg/l) and MW-18 (404 µg/l). 1,4-Dioxane was
detected in groundwater above its standard of 3 µg/l in nine of the 19 monitoring wells sampled
(see Section 2.4 for additional discussion of 1,4-dioxane).

With natural biodegradation, 1,1-dichloroethane (1,1-DCA) has become more widespread as
1,1,1-TCA concentrations undergo reductive dechlorination. 1,1-DCA was detected in
groundwater above the 2L Standard of 6 µg/l in six of the 19 monitoring wells sampled. The
highest 1,1-DCA concentration detected was 4,390 µg/l in MW-8R.

During the October 2018 monitoring event, the following VOCs were detected in at least one
monitoring well above their respective 2L Standard: chloromethane, 1,1-DCA, 1,2-DCA,
1,1-DCE, methylene chloride, trichloroethene, 1,1,1,2-tetrachloroethane, 1,1,1-TCA, 1,1,2-TCA,
and 1,4-dioxane. Some of these compounds are reductive dechlorination daughter products and/or
abiotic degradation products of the parent COCs.

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Plume Extent
The extent of the chlorinated VOC plume is reasonably well defined. The plume originates in the
central portion of the subject property and extends approximately 1,000 ft to the south. The
downgradient extent of the plume is defined by the absence of chlorinated VOCs above laboratory
reporting limits in shallow monitoring wells MW-14, MW-15, and MW-16. The chlorinated VOC
plume extends vertically less than approximately 50 ft below grade based on the general historical
absence of chlorinated VOCs in MW-2D and MW-17DD. Plume maps for 1,1-DCE and
1,1,1-TCA in shallow groundwater are depicted on Figures 6 through 8. The extent of 1,4-dioxane
impacts for the October 2018 monitoring event is presented on Figure 9.

Source Area Concentration Trends
A tabular summary of historical groundwater analytical data is presented in Appendix C. Time
series concentration graphs of 1,1-DCE, 1,1,1-TCA, and 1,1-DCA for source area monitoring
wells MW-8/MW-8R and MW-18, as well as for downgradient monitoring wells MW-10, MW-19,
and MW-20 are provided in Appendix D.

As indicated on the graphs, significant decreases in 1,1-DCE concentrations were observed in the
source area wells following the sodium persulfate injection in 2005. Starting in July 2007,
apparent rebound in 1,1-DCE concentrations was observed. The RegenOx™ injections (two in
December 2007, one in December 2008, and one in February 2009) were conducted to address this
rebound. The RegenOx™ injections resulted in 1,1-DCE concentration decreases in downgradient
wells. While 1,1-DCE concentrations increased in source area well MW-8/8R initially following
the PersulfOx™ injections (March – April 2014), significant reductions (close to two orders of
magnitude) were observed in 1,1-DCE concentrations in 2015 and 2016 monitoring events, with
an increasing trend in more recent data. Concentrations of 1,1-DCE increased from 1,960 µg/L in
March 2018 to 2,770 µg/L in October 2018.

Seasonal fluctuations in 1,1-DCE concentrations in monitoring wells MW-18 and MW-19 have
been observed since semi-annual monitoring began in March 2015. These wells are located
downgradient of the source area. The 1,1-DCE concentrations in MW-18 have ranged from
404 µg/L (September 2015) to 1,070 µg/L (March 2015). In October 2018, MW-18 had a 1,1-DCE

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concentration of 404 µg/L, which is a historical low since the PersulfOxTM injections
(March – April 2014). In MW-19, the 1,1-DCE concentrations have ranged from 190 µg/L
(March 2015) to 1,460 µg/L (September 2015). In October 2018, MW-19 had a 1,1-DCE
concentration of 350 µg/L.

1,1,1-TCA also decreased over one order of magnitude in source area monitoring well MW-8/8R
following the 2014 injections based on 2015 through 2018 data. While 1,1,1-TCA concentrations
in MW-8 were in excess of 100,000 µg/L for many years, significant concentration reductions
were observed in MW-8/8R post injections with concentrations ranging from 8,550 µg/l
(March 2016) to 28,200 µg/L (September 2017). The recent data indicate some rebound in
concentrations in MW-8R.

Seasonal fluctuations of 1,1,1-TCA concentrations in downgradient monitoring wells MW-18 and
MW-19 have also been observed since semi-annual monitoring began in March 2015 with a
decreasing trend in the most recent data. The 1,1,1-TCA concentrations in MW-18 have ranged
from 6.6 µg/L (October 2018) to 802 µg/L (March 2015). The 1,1,1-TCA concentrations in
MW-19 have ranged from 22.9 µg/L (October 2018) to 146 µg/L (September 2015).

1,1-DCA concentrations have attenuated in source area monitoring well MW-8/8R after the
persulfate injections (January 2005 and March-April 2014) and recent data indicate stable
concentrations. 1,1-DCA concentrations in MW-18 and MW-19 have fluctuated over time, with
a decreasing trend in the most recent data.

2.4 Groundwater Analytical Results – 1,4-Dioxane
1,4-Dioxane is a solvent stabilizer that was historically added to chlorinated solvents, such as
1,1,1-TCA, to inhibit reactions that resulted in deterioration of the solvent. 1,4-Dioxane has
attracted interest among regulators because of its mobility and classification as a probable human
carcinogen.

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Concentrations of 1,4-dioxane detected during the October 2018 monitoring event are presented
on Table 3 and Figure 9. 1,4-Dioxane concentration graphs for source area monitoring wells
MW-8/MW-8R and MW-18, and downgradient wells MW-10 and MW-19 are provided in
Appendix D. As indicated on the graphs, concentrations across the plume remain relatively stable.
1,4-Dioxane was detected during the October 2018 monitoring event in 10 of the 19 monitoring
wells sampled at concentrations ranging from 2.2 µg/l (MW-5) to 4,740 µg/l (MW-8R). In general,
1,4-dioxane concentrations detected in October 2018 remained stable in comparison to previous
sampling events. While ISCO injections appear to reduce 1,4-dioxane concentrations, rebound
occurs as the aquifer materials release more contaminant post injection. The highest
concentrations were detected at monitoring wells located beneath and downgradient of the former
knife room. 1,4-Dioxane was not detected above its 2L Standard in downgradient monitoring
wells MW-14, MW-15, or MW-16, indicating that the horizontal extent of 1,4-dioxane in shallow
groundwater is defined.

During previous sampling events, 1,4-dioxane was detected at concentrations exceeding its
2L Standard of 3.0 µg/l at deeper monitoring wells MW-2D and MW-17DD, which are completed
at depths of 54 ft and 58 ft, respectively. MW-2D was not sampled during the October 2018
monitoring event. 1,4-Dioxane was last detected at monitoring well MW-2D during the
January 2010 monitoring event at a concentration of 9.5 µg/l, but it was not detected during the
subsequent April or July 2010 monitoring events. In October 2018, 1,4-dioxane was detected in
MW-17D at 33.2 µg/l; however, it was not detected above laboratory reporting limits in deeper
well MW-17DD (<2.0 µg/l). Based on these data, the vertical and horizontal extent of 1,4-dioxane
in deeper groundwater is defined.

2.5 Groundwater Analytical Results – RCRA Metals

In accordance with the Injection Permit, groundwater samples were collected from select
monitoring wells for analysis of RCRA metals in October 2018. Metals are monitored because
dissolved phase metal concentrations may fluctuate due to changes in groundwater chemistry
caused by the injections. The monitoring wells included upgradient/cross-gradient monitoring

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wells MW-9 and MW-13; injection zone wells MW-8/MW-8R, MW-18, and MW-19; and
downgradient well MW-10 (Table 4).

During the October 2018 monitoring event, the only RCRA metals detected above their respective
2L Standards were arsenic, chromium, and mercury. Arsenic was detected in injection zone
monitoring well MW-8R at a concentration of 0.343 mg/L, chromium was detected in injection
zone monitoring well MW-19 at a concentration of 0.0208 mg/L, and mercury was detected in
injection zone monitoring well MW-8R at a concentration of 0.0014 mg/L. The arsenic,
chromium, and mercury detections are consistent with historical results. With the exception of
monitoring well MW-8R, arsenic was not detected in any of the other monitoring wells sampled
for metals. With the exception of monitoring well MW-19, chromium was not detected in any of
the other monitoring wells sampled for metals. Mercury was detected in downgradient monitoring
well MW-10 at a concentration of 0.00048 mg/L, which is below its 2L Standard. Consistent with
historical results, barium was detected below its 2L Standard in upgradient monitoring well
MW-13 and cross-gradient monitoring well MW-9 during the October 2018 monitoring event. No
other RCRA metals were detected in upgradient monitoring well MW-13 or cross-gradient
monitoring well MW-9 during the October 2018 monitoring event.

In general, metals concentrations in injection area wells are consistent with the detections from the
July 2013 baseline sampling event. With the possible exception of sporadic detections of
chromium above the 2L Standard in downgradient monitoring well MW-10 during the March 2015
and March 2016 monitoring events, groundwater results indicate that elevated RCRA metals
concentrations in groundwater are not migrating outside of the injection zone. RCRA metal
detections for the October 2018 sampling event and the injection zone are depicted on Figure 10.

2.6 Groundwater Analytical Results – Injection Related and Geochemical Parameters

As discussed in the preceding sections, the primary indicator of a successful remediation
technology is decreasing concentrations of the contaminants of concern (COCs). With some
remediation technologies (i.e. enhanced anaerobic bioremediation), the production of degradation
byproduct species (aka, “daughter products”) can also indicate that remediation of the COCs is
occurring.

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Secondary performance indicators typically include injection specific parameters and geochemical
parameters. To monitor the ISCO reaction, chloride, sulfate, sodium, pH, ORP, DO, and specific
conductivity were monitored in and near the source area monitoring wells in October 2018 in
accordance with the UIC permit requirements. These constituents are either potential by-products
of the persulfate-based and/or RegenOx™ injection activities (chloride, sulfate, sodium) or are
geochemical parameters that are potentially affected by such injections (specific conductivity, DO,
ORP, and pH). Injection of PersulfOx™ typically results in increased chloride, sulfate, sodium,
conductivity, DO, and ORP. Typically, pH would decrease with the injection of PersulfOx™
alone; however, the addition of NaOH as the catalyst acts as a buffer and would initially increase
the pH. With dispersion, the levels of chloride, sulfate and sodium will decrease over time.

According to the 2013 UIC permit requirement, injection related constituents and geochemical
parameters are to be monitored until they reach concentrations detected at the Site prior to the
injections authorized by the 2007 UIC permit or do not exceed the 2L Standards. Chloride, sulfate,
and sodium concentrations appear to have been affected by prior injections within the injection
zone. Current and historical results are included on Table 3 and in Appendix C, respectively.

Chloride, sulfate, and sodium concentrations remain elevated within the injection zone. In October
2018, chloride and sulfate concentrations in monitoring well MW-8R were above their respective
2L Standard. Sodium concentrations are elevated in the injection zone, but there is no 2L Standard
specified for sodium.

Source area well MW-8/8R has demonstrated consistently high ORP and high specific
conductivity, indicating oxidizing conditions. The measured ORP value during the October 2018
monitoring event (488.3 mV) was higher than the previous March 2018 level (415.8 mV). DO
concentrations have remained low following the most recent ISCO injection. pH has fluctuated in
MW-8/8R over time and is currently at 3.72.

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2.7 Investigation Derived Waste
Non-hazardous purge water from the October 2018 sampling event was containerized in a
55-gallon drum and staged on-site. This drum was transported for off-site disposal on October 5,
2018. Disposal documentation for this drum is provided in Appendix E. The purge water was
previously profiled as non-hazardous based on a representative purge water sample from
September 2017.

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3.0 Summary
This report summarizes the post-injection groundwater monitoring event conducted in October
2018 at the former Fulflex facility in Scotland Neck, North Carolina. Chlorinated VOCs are
present in groundwater above standards. The source of the groundwater impacts appears to be the
former knife cleaning room.

• Groundwater impacts are present above 2L Standards and extend off-site. The primary
constituents of concern in the source area are 1,1,1-TCA, 1,1-DCA and 1,1-DCE.
Additionally, the compound 1,4-dioxane (which was historically added to 1,1,1-TCA as a
solvent stabilizer) has been detected beneath and downgradient of the subject property.

• 1,1,1-TCA was detected in source area monitoring well MW-8R at a concentration of
24,900 µg/L in October 2018. Although above the 2L Standard of 200 µg/L, this
concentration is a significant decrease from the concentration (260,000 µg/L in July 2013)
detected prior to the last PersulfOx™ injections in March and April 2014. Concentrations
in the source area well trended up March 2016 to September 2017, and then indicate a
stable trend from the September 2017 to October 2018 sampling events.

• Since the PersulfOx™ injections in March and April 2014, 1,1-DCE concentrations in
MW-8/MW-8R were reduced from 23,000 µg/L to 2,770 µg/L in October 2018. 1,1-DCE
remains above the 2L Standard of 350 µg/L.

• 1,1-DCA concentrations attenuated in the source area monitoring well MW-8/MW-8R
after the PersulfOx™ injections in March and April 2014 and generally remain stable.
1,1-DCA concentrations in MW-18 and MW-19 have fluctuated over time, with a
decreasing trend in the most recent data.

• 1,4-Dioxane was detected in groundwater above the 2L Standard of 3 µg/l in nine of the
19 monitoring wells sampled in October 2018. The highest 1,4-dioxane concentration
detected was 4,740 µg/l in source area monitoring well MW-8R, which is slightly lower
than the July 2013 pre-injection concentration of 4,900 µg/l in this location.

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• The lateral and vertical extent of the VOC plume is reasonably well defined. The plume
originates in the central portion of the subject property and extends approximately 1,000 ft
to the south. The southern portion of the 1,4-dioxane plume (downgradient) is outside of
the boundaries of the subject property, but the plume is defined by shallow off-site
monitoring wells MW-14, MW-15, and MW-16. Chlorinated VOCs and 1,4-dioxane were
not detected in these three shallow downgradient off-site monitoring wells during the
October 2018 monitoring event. The chlorinated VOC plume extends to less than
approximately 50 ft below grade.

• Concentrations of injection related constituents (chloride, sulfate, and sodium) and
potentially elevated metals related to changes in geochemistry appear to be present within
the injection zone. Arsenic, chromium, mercury, chloride, and sulfate exceed 2L Standards
in certain monitoring wells in the source area and injection zone. However, these
constituents are not present above 2L Standards downgradient of the injection zone.

The October 2018 monitoring event was the eighth semi-annual monitoring event following
completion of one year of quarterly monitoring for the UIC permit. H&H will continue with the
semi-annual monitoring events in March 2019 which will include sampling on-site and off-site
monitoring wells. A report will be completed following the March 2019 monitoring event. In
addition, another ISCO injection of sodium persulfate in the area of highest 1,1,1-TCA
groundwater concentrations is planned for the first half of 2019 and a DEQ permit for this injection
has been obtained.

Tables
Table 1Groundwater Monitoring ProgramFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006MW-1 to MW-7,MW-14 to MW-17, MW-17D and MW-17DDVOCs including 1,4-dioxane, FieldVOCs including 1,4-dioxane, FieldMW-8, MW-9, MW-10*, MW-13, MW-18, and MW-19VOCs including 1,4-dioxane, Sulfate, Sodium, Chloride, RCRA Metals, FieldVOCs including 1,4-dioxane, Sulfate, Sodium, Chloride, RCRA Metals, FieldNotes:1) Injection related parameters are to be sampled until concentrations return to pre-injection concentrations (2007) or below 2L Standards, whichever is higher.VOCs = Volatile Organic Compounds (Method 8260B)Field = Field measured parameters including dissolved oxygen, oxidation-reduction potential, conductivity, temperature, pH, and turbidity* UIC Program indicated MW-10 could be sampled instead of replacing MW-20, which was abandoned in January 2008 during soil excavation activities.RCRA metals include Arsenic, Barium, Cadmium, Chromium, Lead, Mercury, Selenium, and Silver by EPA Methods 6010/7470Monitoring will continue on a semi-annual basis for all monitoring wells listed after the March 2015 event. Monitoring WellsSemi-AnnualMonitoringJune and December 2014UIC Permit for PersulfOxQuarterly Sampling (June, September, and December 2014, March 2015)Semi-Annual Monitoring after March 20151S:\AAA-Master Projects\Fulflex - FUL\FUL-006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL-006 October 2018 Tables12/31/2018Table 1Hart & Hickman, PC
Table 2Monitoring Well Construction and Water Level MeasurementsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)DTW(ft)ELEV(ft)MW-1 12/20/02 18 8-18 100.00 6.52 93.48 3.21 96.79 2.85 97.15 5.22 94.78 3.46 96.54 8.71 91.29 1.94 98.06 2.92 97.08 3.86 96.14 6.84 93.16 2.53 97.47 5.27 94.73MW-2 12/20/02 17 7-17 99.07 5.62 93.45 2.38 96.69 1.91 97.16 4.34 94.73 2.5696.51 7.76 91.31 1.14 97.93 2.07 97.00 2.95 96.12 5.86 93.21 1.60 97.47 5.3893.69MW-3 02/25/03 18 8-18 101.66 8.10 93.56 4.90 96.76 4.81 96.85 6.83 94.83 5.09 96.57 10.23 91.43 3.53 98.13 4.69 96.97 5.45 96.21 8.38 93.28 4.17 97.49 6.89 94.77MW-4 02/26/03 18 8-18 100.77 7.25 93.52 3.48 97.29 3.76 97.01 5.96 94.81 4.21 96.56 10.43 90.34 2.63 98.14 3.64 97.13 4.58 96.19 7.53 93.24 3.22 97.55 7.72 93.05MW-5 02/26/03 20 10-20 100.73 7.11 93.62 3.87 96.86 3.94 96.79 NF -- 4.03 96.70 9.40 91.33 2.48 98.25 4.01 96.72 4.52 96.21 7.42 93.31 3.01 97.72 6.80 93.93MW-6 02/26/03 19 9-19 101.66 8.72 92.94 4.89 96.77 4.34 97.32 6.87 94.79 5.09 96.57 10.31 91.35 3.52 98.14 4.23 97.43 5.52 96.14 8.38 93.28 3.93 97.73 6.90 94.76MW-7 02/26/03 16 6-16 97.53 4.10 93.43 1.10 96.43 0.78 96.75 2.89 94.64 1.0296.51 6.20 91.33 Artesian -- 0.76 96.77 1.43 96.10 4.40 93.13 0.23 97.30 2.91 94.62MW-8 06/11/03 20 10-20 104.92 11.10 93.82 7.96 96.96 8.24 96.68 10.12 94.808.44 96.48MW-8R 02/01/15 20 10-20 104.73 NA -- NA -- NA -- NA -- NA -- 13.40 91.33 6.33 98.40 8.20 96.53 8.51 96.22 11.53 93.20 7.33 97.40 9.85 94.88MW-9 06/10/03 20 10-20 104.72 11.07 93.65 7.78 96.94 8.44 96.28 9.80 94.92 8.12 96.60 13.29 91.43 6.25 98.47 7.86 96.86 8.44 96.28 11.40 93.32 7.34 97.38 9.80 94.92MW-10 06/10/03 20 10-20 104.47 10.86 93.61 7.60 96.87 7.52 96.95 9.58 94.897.85 96.62 13.12 91.35 6.14 98.33 8.45 96.02 8.21 96.26 11.18 93.29 6.50 97.97 9.53 94.94MW-11 06/10/03 18 10-20 99.60 6.19 93.41 3.00 96.60 2.98 96.62 NM -- NM -- -- -- 2.11 97.49 2.97 96.63 3.49 96.11 6.54 93.06 2.35 97.25 NM --MW-12 06/10/03 20 10-20 101.11 6.68 94.43 3.65 97.46 NM -- NM -- NM -- -- -- NM --NM--NM--NM--NM--NM--MW-13 06/11/03 20 10-20 102.19 7.76 94.43 4.78 97.41 5.23 96.96 6.55 95.64 5.10 97.09 10.58 91.61 3.29 98.90 5.08 97.11 5.33 96.86 8.48 93.71 4.58 97.616.63 95.56MW-14 06/11/03 20 10-20 97.09 3.82 93.27 1.40 95.69 0.70 96.39 2.75 94.34 1.38 95.71 5.97 91.12 0.54 96.55 0.56 96.53 1.92 95.17 3.93 93.16 0.45 96.64 2.53 94.56MW-15 06/12/03 20 10-20 99.70 7.55 92.15 4.51 95.19 4.29 95.41 6.62 93.08 4.71 94.99 9.34 90.36 3.09 96.61 4.05 95.65 5.09 94.61 7.48 92.22 3.86 95.84 6.75 92.95MW-16 06/12/03 20 10-20 104.14 11.74 92.40 9.61 94.53 9.78 94.36 11.10 93.04 9.70 94.44 13.54 90.60 7.82 96.32 9.36 94.78 9.87 94.27 12.25 91.89 9.34 94.80 11.05 93.09MW-17 11/17/03 16 11-16 99.04 5.85 93.19 2.70 96.34 2.24 96.80 5.34 93.70 3.43 95.61 8.44 90.60 2.12 96.92 2.93 96.11 3.75 95.29 6.55 92.49 2.50 96.54 5.10 93.94MW-17D 11/17/03 28 23-28 99.00 5.87 93.13 2.76 96.24 2.31 96.69 5.00 94.00 3.28 95.72 8.29 90.71 2.05 96.95 2.77 96.23 3.62 95.38 6.41 92.59 3.40 95.60 4.91 94.09MW-17DD 06/03/04 58 53-58 99.05 5.89 93.16 2.76 96.29 2.41 96.64 5.42 93.633.42 95.63 7.97 91.08 1.99 97.06 2.47 96.58 3.35 95.70 6.11 92.94 2.89 96.165.56 93.49MW-18 01/18/05 20 10-20 104.64 10.96 93.68 7.80 96.84 7.71 96.93 9.73 94.918.06 96.58 13.23 91.41 6.23 98.41 8.03 96.61 8.36 96.28 11.38 93.26 7.46 97.18 9.79 94.85MW-19 01/18/05 20 10-20 104.74 11.13 93.61 7.88 96.86 7.82 96.92 9.94 94.808.14 96.60 13.40 91.34 6.35 98.39 8.14 96.60 8.48 96.26 11.51 93.23 7.33 97.41 9.72 95.02MW-20 01/18/05 20 10-20 104.72MW-2D 03/10/03 54 49-54 99.25 5.35 93.90 2.11 97.14 1.48 97.77 NM -- NM --7.5891.670.7398.522.0097.25 2.71 96.54 5.57 93.68 Artesian -- Artesian --Notes:Elevations based on arbitrary datum of 100 ft for MW-1 TOCTOC = top of casing, DTW = Depth to WaterNA = Not Applicable, NM = Not MeasuredWellInstallation DateWell Depth (ft)TOC Elevation (ft)Screen Interval (ft bls)12/9/20147/1/2013 6/11/20141/23/2013 9/17/20153/21/2016 9/22/2016 3/30/2017 9/21/2017 3/13/2018 10/4/20187/9/2012All well casing constructed with 2-inch PVC except MW-17 and 17D (1-inch PVC), MW-2D is a Type III well with 6-inch PVC surface casing to 32 ft bgs.MW-8 was abandonded on February 23, 2015. Replacement well MW-8R was installed on February 1, 2015 with the same construction details as MW-8.AbandonedAbandonedS:\AAA-Master Projects\Fulflex - FUL\FUL-006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL-006 October 2018 Tables T2 WL12/31/2018Table 2Hart & Hickman, PC
Table 3Groundwater Analytical Detections - October 2018Former Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDMW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8R MW-9 MW-10 MW-13 MW-14 MW-15 MW-16 MW-17 MW-17D MW-17DD MW-18 MW-19Sample Date 10/5/18 10/5/18 10/5/18 10/5/18 10/5/18 10/5/18 10/5/18 10/4/18 10/4/1810/4/18 10/4/18 10/4/18 10/4/18 10/4/18 10/4/18 10/4/18 10/4/18 10/4/1810/4/18VOCs (µg/L) - 8260Chloroform 70 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <200 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 4.3 <2.0Chloromethane 3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0699<1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.01,1-Dichloroethane 6 <1.0 <1.0 <1.0 <1.0 1.9 <1.016.0 4,390<1.022.7<1.0 <1.0 <1.0 <1.0 1.112.2<1.0389 1471,2-Dichloroethane 0.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.02.7 590<1.04.9<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.069.1 27.31,1-Dichloroethene 350 <1.0 4.2 <1.0 1.5 47.0 <1.0 99.32,7701.2 134 <1.0 <1.0 <1.0 <1.0 15.4 197 <1.0404349cis-1,2-Dichloroethene 70 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <200 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 6.4 3.0Methylene Chloride 5 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <400 <2.0 <4.0 <2.0<2.0 <2.0 <2.0 <2.0 <2.0 <2.06.9<4.01,1,1,2-Tetrachloroethane 1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <200 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.026.5 4.4Toluene 600 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <200 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 74.4 <1.0 <1.0 <2.5 <2.01,1,1-Trichloroethane 200 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.024,9003.9 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 6.6 22.91,1,2-Trichloroethane 0.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.03.8 657<1.03.1<1.0 <1.0 <1.0 <1.0 <1.02.7<1.045.0 19.0Trichloroethene 3 <1.03.7<1.0 <1.0 <1.0 <1.0 <1.0 <200 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.03.5<1.03.2<2.0Trichlorofluoromethane 2,000 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <200 <1.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.01,4-Dioxane (µg/L) - 8260 SIM1,4-Dioxane 3 <2.0 <2.06.7<2.0 2.2 <2.024.1 4,740 6.7 37.6<2.0 <2.0 <2.0 <2.04.0 33.2<2.0598 206Others (µg/L)Chloride 250,000 NA NA NA NA NA NA NA1,000,00088,500 66,300 36,100 NA NA NA NA NA NA 164,000 96,400Sulfate 250,000 NA NA NA NA NA NA NA2,060,0007,100 8,500 6,000 NA NA NA NA NA NA 93,100 148,000Sodium NS NANANANANANANA1,210,000 48,000 49,400 14,400 NANANANANANA143,000 98,200Field MeasurementsORP (mV) NS -153.6 47.3 32.6 118.2 87.1 118.9 -106.5 488.3 119.2 113.8 159.5 49.8 141.3 -92.5 -195.9 109.5 -85.0 -163.7 -83.1Temperature (oC)NS 26.1 20.1 23.0 20.9 18.5 19.0 24.8 26.5 22.1 21.4 28.4 23.2 26.0 24.4 30.3 20.1 18.8 25.4 24.1pH NS 6.09 5.02 4.61 3.81 4.27 3.79 4.85 3.72 4.04 4.03 3.63 4.49 3.93 4.46 6.06 4.82 7.03 4.00 4.06Conductivity (μS/cm) NS 125.5 128.0 124.8 85.7 140.8 165.7 285.7 7,202 419.7 345.1 172.5 160.3 99.3 70.3 254.4 182.3 277.3 899 745.0Dissolved Oxygen (mg/L) NS 0.15 0.80 1.42 1.08 1.94 2.32 0.19 0.20 1.22 2.35 1.00 4.56 1.90 3.68 0.12 1.83 0.43 0.27 2.01Turbidity (NTU) NS 9.41 23.94 3.77 13.58 669.2 10.89 4.12 5.48 3.27 8.55 6.08 5.93 21.53 1.88 6.05 60.60 30.91 3.52 1.59Persulfate (mg/L)2NS NA NA NA NA NA NA NA 35 NA NA NA NA NA NA NA NA NA 0.0 0.0Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L (April 1, 2013) 2) Measured using CHEMetrics test kits. Detection limit is 0.35 mg/LOnly those compounds detected above laboratory reporting limits are included in table.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardVOCs = Volatile Organic Compounds; NS = Not Specified; NA = Not AnalyzedNC Groundwater Standard1S:\AAA-Master Projects\Fulflex - FUL\FUL-006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL-006 October 2018 Tables T3 GW October 201812/31/2018Table 3 Hart & Hickman, PC
Table 4
RCRA Metals Results for Injection Area Wells
Former Fulflex Facility
Scotland Neck, North Carolina
H&H Project No. FUL-006
Mercury Arsenic Barium Cadmium Chromium Lead Selenium Silver
0.001 0.01 0.7 0.002 0.01 0.015 0.02 0.02
Sample ID Sample Date
12/8/2007 0.0023 0.45 <0.089 <0.089 <0.18 0.19 <0.36 <0.18
1/30/2008 0.0016 0.044 0.062 <0.005 0.15 0.013 <0.02 <0.01
7/16/2008 0.0019 0.27 <0.050 <0.05 <0.10 0.18 <0.20 <0.10
1/29/2009 0.0035 0.25 <0.050 <0.05 <0.10 0.097 <0.20 <0.050
7/2/2013 0.0014 <0.40 <0.10 <0.10 <0.20 0.14 <0.40 <0.20
6/11/2014 0.0019 <1.0 <0.25 <0.25 <0.50 <0.25 <1.0 <0.5
9/16/2014 0.0038 0.24 <0.050 <0.05 <0.10 0.1 <0.2 <0.1
12/9/2014 0.0038 0.166 <0.050 <0.01 <0.050 0.0969 <0.1 <0.050
3/13/2015 0.0003 <0.05 <0.025 <0.005 <0.025 <0.025 <0.05 <0.025
9/17/2015 0.0012 <0.50 <0.25 <0.05 <0.25 <0.25 <0.50 <0.25
3/21/2016 0.0014 <0.50 <0.25 <0.05 <0.25 <0.25 <0.50 <0.25
9/22/2016 0.00079 <0.50 <0.25 <0.05 <0.25 <0.25 <0.50 <0.25
3/29/2017 0.0012 <0.200 <0.100 <0.020 <0.100 <0.100 <0.200 <0.100
9/22/2017 0.0015 0.25 <0.100 <0.020 <0.100 <0.100 <0.200 <0.100
3/13/2018 0.0016 <0.50 <0.25 <0.05 <0.25 <0.25 <0.50 <0.25
10/4/2018 0.0014 0.343 <0.100 <0.020 <0.100 <0.100 <0.200 <0.100
7/2/2013 <0.002 <0.02 0.33 <0.005 <0.01 <0.005 <0.02 <0.01
6/12/2014 <0.0002 <0.02 0.37 <0.005 <0.01 <0.005 <0.02 <0.01
9/16/2014 <0.0002 <0.02 0.30 <0.005 <0.01 <0.005 <0.02 <0.01
12/9/2014 <0.0002 <0.01 0.278 <0.001 <0.005 <0.005 <0.01 <0.005
3/13/2015 <0.0002 <0.01 0.30 <0.001 <0.005 <0.005 <0.01 <0.005
9/17/2015 <0.0002 <0.01 0.328 <0.001 <0.005 <0.005 <0.01 <0.005
3/21/2016 <0.0002 <0.01 0.238 <0.001 <0.005 <0.005 <0.01 <0.005
9/23/2016 <0.0002 <0.01 0.270 <0.001 <0.005 <0.005 <0.01 <0.005
3/29/2017 <0.0002 <0.01 0.371 <0.001 <0.005 0.005 <0.01 <0.005
9/21/2017 <0.0002 <0.01 0.346 <0.001 <0.005 0.005 <0.01 <0.005
3/13/2018 <0.0002 <0.01 0.310 <0.001 <0.005 <0.005 <0.01 <0.005
10/4/2018 <0.0002 <0.01 0.322 <0.001 <0.005 <0.005 <0.01 <0.005
7/16/2008 0.00028 <0.02 0.27 <0.005 <0.01 <0.005 <0.02 <0.01
1/29/2009 <0.0002 <0.02 0.21 <0.005 <0.01 <0.005 <0.02 <0.01
7/2/2013 0.00028 <0.02 0.22 <0.005 <0.01 <0.005 <0.02 <0.01
6/12/2014 0.00032 <0.02 0.22 <0.005 <0.01 <0.005 <0.02 <0.01
9/16/2014 <0.0002 <0.02 0.15 <0.005 <0.01 <0.005 <0.02 <0.01
12/10/2014 0.00048 <0.01 0.222 <0.001 <0.005 <0.005 <0.01 <0.005
3/13/2015 <0.0002 <0.01 0.0973 <0.001 0.0426 <0.005 <0.01 <0.005
9/17/2015 0.00032 <0.01 0.250 <0.001 <0.005 <0.005 <0.01 <0.005
3/21/2016 <0.0002 <0.01 0.088 <0.001 0.0361 <0.005 <0.01 <0.005
9/22/2016 0.00036 <0.01 0.174 <0.001 <0.005 <0.005 <0.01 <0.005
3/29/2017 0.00055 <0.01 0.272 <0.001 <0.005 <0.005 <0.01 <0.005
9/22/2017 0.00052 <0.01 0.271 <0.001 <0.005 <0.005 <0.01 <0.005
3/14/2018 <0.0002 <0.01 0.0677 <0.001 <0.005 <0.005 <0.01 <0.005
10/4/2018 0.00048 <0.01 0.241 <0.001 <0.005 <0.005 <0.01 <0.005
7/1/2013 <0.002 <0.02 0.20 <0.005 <0.01 <0.005 <0.02 <0.01
6/13/2014 <0.0002 <0.02 0.22 <0.005 <0.01 <0.005 <0.020 <0.01
9/16/2014 <0.0002 <0.02 0.20 <0.005 <0.01 <0.005 <0.02 <0.01
12/10/2014 <0.0002 <0.01 0.183 <0.001 <0.005 <0.005 <0.01 <0.005
3/13/2015 <0.0002 <0.01 0.191 <0.001 <0.005 <0.005 <0.01 <0.005
9/18/2015 <0.0002 <0.01 0.193 <0.001 <0.005 <0.005 <0.01 <0.005
3/22/2016 <0.0002 <0.01 0.193 <0.001 <0.005 <0.005 <0.01 <0.005
9/22/2016 <0.0002 <0.01 0.174 <0.001 <0.005 <0.005 <0.01 <0.005
3/29/2017 <0.0002 <0.01 0.209 <0.001 <0.005 <0.005 <0.01 <0.005
9/22/2017 <0.0002 <0.01 0.188 <0.001 <0.005 <0.005 <0.01 <0.005
3/13/2018 <0.0002 <0.01 0.204 <0.001 <0.005 <0.005 <0.01 <0.005
10/4/2018 <0.0002 <0.01 0.188 <0.001 <0.005 <0.005 <0.01 <0.005
12/8/2007 0.0018 0.036 0.08 <0.005 0.038 0.044 <0.02 <0.01
1/30/2008 0.0013 0.026 0.02 <0.005 <0.03 0.012 0.03 <0.01
7/16/2008 0.0017 <0.02 0.03 <0.005 0.034 0.018 <0.02 <0.01
1/29/2009 0.0014 <0.02 0.04 <0.005 0.023 0.0066 <0.02 <0.01
7/2/2013 0.00041 <0.02 0.10 <0.005 0.01 0.01 <0.02 <0.01
6/11/2014 0.00026 <0.02 0.17 <0.005 <0.01 0.016 <0.02 <0.01
9/16/2014 0.00023 <0.02 0.09 <0.005 <0.01 0.012 <0.02 <0.01
12/9/2014 <0.0002 <0.01 0.0541 <0.001 <0.005 0.0055 <0.01 <0.005
3/13/2015 0.00069 <0.1 0.0611 <0.01 0.0652 <0.05 <0.1 <0.05
9/17/2015 0.00021 0.0105 0.0475 <0.001 0.0061 0.0079 <0.01 <0.005
3/21/2016 0.00049 <0.05 0.0262 <0.005 0.029 <0.05 <0.025 <0.025
9/22/2016 <0.0002 <0.05 0.197 <0.005 <0.025 <0.025 <0.05 <0.025
3/29/2017 <0.0002 <0.01 0.0665 <0.001 <0.005 0.007 <0.01 <0.005
9/21/2017 <0.0002 <0.01 0.0481 <0.001 <0.005 0.0098 <0.01 <0.005
3/13/2018 <0.0002 <0.01 0.0481 <0.001 <0.005 0.0077 <0.01 <0.005
10/4/2018 <0.0002 <0.01 0.0658 <0.001 <0.005 0.0058 <0.01 <0.005
12/8/2007 0.0032 <0.02 0.09 <0.005 0.13 0.035 <0.02 <0.01
1/30/2008 0.0013 <0.02 0.04 <0.005 0.10 0.0089 <0.02 <0.01
7/16/2008 0.001 <0.02 0.04 <0.005 0.11 0.0092 <0.02 <0.01
1/29/2009 0.00083 <0.02 0.05 <0.005 0.072 0.009 <0.02 <0.01
7/2/2013 0.00023 <0.02 0.04 <0.005 0.042 0.01 <0.02 <0.01
6/11/2014 0.00028 <0.02 0.03 <0.005 0.048 0.05 <0.02 <0.01
9/16/2014 <0.0002 <0.02 0.03 <0.005 0.040 0.035 <0.02 <0.01
12/9/2014 0.00032 <0.01 0.0243 <0.001 0.036 0.0152 <0.01 <0.005
3/13/2015 <0.0002 <0.01 0.0270 <0.001 0.0575 0.0148 <0.01 <0.005
9/17/2015 0.0016 <0.01 0.0338 <0.001 0.0389 0.0139 <0.01 <0.005
3/21/2016 <0.0002 <0.01 0.0404 <0.001 0.0359 0.0124 <0.01 <0.005
9/22/2016 0.00044 <0.01 0.0437 <0.001 0.0322 0.0094 <0.01 <0.005
3/29/2017 <0.0002 <0.01 0.0384 <0.001 0.0231 0.0138 <0.01 <0.005
9/21/2017 0.00026 <0.01 0.0458 <0.001 0.0294 0.0061 <0.01 <0.005
3/13/2018 0.00032 <0.01 0.0345 <0.001 0.0274 0.0096 <0.01 <0.005
10/4/2018 <0.0002 <0.01 0.0323 <0.001 0.0208 0.0080 <0.01 <0.005
12/8/2007 0.002 <0.02 0.06 <0.005 0.028 0.0097 <0.02 <0.01
1/22/2008 0.00055 <0.001 0.05 <0.005 0.033 <0.0050 <0.02 <0.01
Notes:
1) NC Groundwater Standard as indicated in 15A NCAC 2L; Bold indicates analyte concentration exceeds NC 2L Ground Water Standard (April 1 2013)
2) MW-20 was abandoned in January 2008.
MW-8 was abandoned on February 23, 2015. Replacement well MW-8R was installed on February 1, 2015.
Two RegenOx injection events were conducted on December 8 & 9, 2007 and December 27 & 28, 2007.
Three PersulfOx injections were conducted on March 8 & 9, 2014; March 29 & 30, 2014; and April 26 & 27, 2014.
MW-202
RCRA Metals (mg/L) - 6010B/7470A
NC Groundwater Standard1 (mg/L)
MW-8
MW-8R
MW-9
MW-10
MW-13
MW-18
MW-19
S:\AAA-Master Projects\Fulflex - FUL\FUL-006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL-006 October 2018 Tables T4 RCRA Metals1/28/2019
Table 4
Hart & Hickman, PC

Figures
TITLE
PROJECT
SITE LOCATION MAP
FORMER FULFLEX FACILITYSCOTLAND NECK, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
11-05-18 0
1FUL-006
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
SCOTLAND NECK, NC 2013HOBGOOD, NC 2013
SITE
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704.586.0007(p) 704.586.0373(f)License # C-1269 / #C-245 Geology
VACANT
ABANDONED RAILROAD RIGHT-OF-WAYPOWER
SUBSTATION
AREA SUPPLIED WITH
CITY WATER AREA SUPPLIED WITH
CITY WATER
VACANT
VACANT
VACANT
FORMER
FULFLEX
AREA SUPPLIED WITH
CITY WATER
FORMER
HAZARDOUS
MATERIALS BUILDING
TRANSFORMERSCOOLING TOWER
DIRT ROAD
SOLAR
FARM
EDWARD
S

F
O
R
K CHESTNUT STREETGRACE STREETRAILROAD STREET7th STRE
E
T
FOOD LI
O
N

R
O
A
D

(
D
I
R
T
)
MW-9 MW-19
MW-17/17D/17DD
MW-12
MW-20
MW-10
MW-16
MW-14
MW-2D
MW-3
MW-7
MW-1
MW-6
MW-4 MW-5
MW-2
MW-11
MW-15
MW-13
MW-8R MW-18
MW-8
JOB NO. FUL-006
REVISION NO. 0DATE: 11-05-18
FIGURE NO. 2
FORMER FULFLEX FACILITY
SCOTLAND NECK, NORTH CAROLINA
SITE PLAN
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
LEGEND
DRAINAGE FEATURE
STREAM
PROPERTY LINE
SUBJECT PROPERTY LINE
FENCE LINES
POWER LINES
STORM SEWER
SANITARY SEWER
BUILDINGS
TREELINE
FUEL OIL AST BUILDING
PROPANE AST
MONITOR WELL
DEEP MONITOR WELL
ABANDONED MONITOR WELL
SEWER FLOW DIRECTION
VACANT
ABANDONED RAILROAD RIGHT-OF-WAYPOWER
SUBSTATION
AREA SUPPLIED WITH
CITY WATER AREA SUPPLIED WITH
CITY WATER
VACANT
VACANT
VACANT
FORMER
FULFLEX
AREA SUPPLIED WITH
CITY WATER
FORMER
HAZARDOUS
MATERIALS BUILDING
TRANSFORMERSCOOLING TOWER
DIRT ROAD
SOLAR
FARM
?
C
C
C
C
C
C
C
C
C
C
C
C
C
C
WSW-12
WSW-13
WSW-14
WSW-15 WSW-6
WSW-5
WSW-4
WSW-3
WSW-1
WSW-10
WSW-9
WSW-2 WSW-8
WSW-11
EDWARD
S

F
O
R
K CHESTNUT STREETGRACE STREETRAILROAD STREET7th STRE
E
T
FOOD LI
O
N

R
O
A
D

(
D
I
R
T
)
MW-9 MW-19
MW-17/17D/17DD
MW-12
MW-20
MW-10
MW-16
MW-14
MW-2D
MW-3
MW-7
MW-1
MW-6
MW-4 MW-5
MW-2
MW-11
MW-15
MW-13
WSW-7
MW-8R MW-18
MW-8
JOB NO. FUL-006
REVISION NO. 0DATE: 11-05-18
FIGURE NO. 3
FORMER FULFLEX FACILITY
SCOTLAND NECK, NORTH CAROLINA
WATER SUPPLY WELL LOCATION MAP
C
?
LEGEND
DRAINAGE FEATURE
STREAM
PROPERTY LINE
SUBJECT PROPERTY LINE
FENCE LINES
POWER LINES
STORM SEWER
SANITARY SEWER
BUILDINGS
TREELINE
FUEL OIL AST BUILDING
PROPANE AST
MONITOR WELL
DEEP MONITOR WELL
ABANDONED MONITOR WELL
SEWER FLOW DIRECTION
TAP PRESENT BUT NO MUNICIPAL
WATER ACCOUNT
ABANDONED WATER SUPPLY WELL
WATER SUPPLY WELL (USE
UNKNOWN)
CITY WATER CONNECTION
(INDIVIDUAL CONNECTIONS SHOWN
ONLY FOR SELECT PROPERTIES ON
FOOD LION ROAD, EDWARDS FORK
ROAD, AND RAILROAD STREET)
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.RECEPTOR SURVEY UPDATED 3/14/2018.
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)A Professional CorporationSTORAGEBUILDINGGRASSGRAVELASPHALTWOODED136MW TEXT136136
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
FOOD LIO
N

R
O
A
D

(
D
I
R
T
)
EDWARD
S

F
O
R
K
MW-2D
MW-3
MW-7
MW-1
MW-6
MW-5
FORMER
FULFLEX
MW-2
MW-4
7th STRE
E
T
CHESTNUT STREETGRACE STREETRAILROAD STREETPOWER
SUBSTATION
VACANT
ABANDONED RAILROAD RIGHT-OF-WAYSOLAR
FARM
AREA SUPPLIED WITH
CITY WATER AREA SUPPLIED WITH
CITY WATER
AREA SUPPLIED WITH
CITY WATER
MW-16
MW-14
MW-15
MW-8
MW-9
MW-13
MW-11
MW-12
MW-17/17D/17DD
MW-10
MW-19
MW-20
MW-18
VACANT
VACANT
VACANT
FORMER
HAZARDOUS
MATERIALS BUILDING
TRANSFORMERS
MW-8R
COOLING TOWER
DIRT ROAD
(NM)
(95.56)
(94.92)
(94.88)
(94.85)
(95.02)
(94.94)
(94.77)
(94.73)(NM)
(93.69)
(93.93)
(94.76)
(94.62)
(93.09)
(93.94)
(94.56)
(92.95)
(93.05)
JOB NO. FUL-006
REVISION NO. 0DATE: 1-28-19
FIGURE NO. 5
FORMER FULFLEX FACILITY
SCOTLAND NECK, NORTH CAROLINA
SHALLOW GROUNDWATER ELEVATIONS
(OCTOBER 2018)
(93.69)
LEGEND
DRAINAGE FEATURE
STREAM
PROPERTY LINE
SUBJECT PROPERTY LINE
FENCE LINES
POWER LINES
STORM SEWER
SANITARY SEWER
BUILDINGS
TREELINE
FUEL OIL AST BUILDING
PROPANE AST
MONITOR WELL
DEEP MONITOR WELL
ABANDONED MONITOR WELL
SEWER FLOW DIRECTION
GROUNDWATER ELEVATION (FT)
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.WATER LEVELS MEASURED ON 10/04/2018.
ELEVATIONS MAY NOT HAVE BEEN AT EQUILIBRIUM.
2.ELEVATIONS BASED ON ARBITRARY DATUM OF 100 FT
FOR MW-1 TOP OF CASING.
3.NM = NOT MEASURED
S:\AAA-Master Projects\Fulflex - FUL\FUL-006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Figures\Figures-20190128.dwg, FIG 5, 1/28/2019 2:08:15 PM,SVincent
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
FOOD LI
O
N

R
O
A
D

(
D
I
R
T
)
EDWARD
S

F
O
R
K
MW-2D
MW-7
MW-1
MW-6
FORMER
FULFLEX
MW-2
7th STR
E
E
T
CHESTNUT STREETGRACE STREETRAILROAD STREETPOWER
SUBSTATION
VACANT
ABANDONED RAILROAD RIGHT-OF-WAYSOLAR
FARM
AREA SUPPLIED WITH
CITY WATER AREA SUPPLIED WITH
CITY WATER
AREA SUPPLIED WITH
CITY WATER
MW-16
MW-14
MW-15
MW-9
MW-13
MW-11
MW-12
MW-17/17D/17DD
MW-19
MW-20
VACANT
VACANT
VACANT
FORMER
HAZARDOUS
MATERIALS BUILDING
TRANSFORMERSCOOLING TOWER
(<1.0)
(<1.0)
(<1.0)
(15.4/197/<1.0)
(99.3)
(<1.0)
(4.2)
(47.0)(1.5)
(<1.0)
(<1.0)
(NS)
(1.2)
(134)
(349)
(<1.0)
(NS)
DIRT ROAD
(NS)
MW-3
MW-4
MW-10
MW-5
MW-8
MW-18MW-8R (404)(2,770)
NOTES:
1.BOLD CONCENTRATIONS INDICATES AN EXCEEDANCE OF
THE 2L STANDARD (350 μg/L).
2.DCE = DICHLOROETHENE
NS = NOT SAMPLED
JOB NO. FUL-006
REVISION NO. 0DATE: 11-05-18
FIGURE NO. 8
FORMER FULFLEX FACILITY
SCOTLAND NECK, NORTH CAROLINA
1,1-DCE CONCENTRATIONS IN
GROUNDWATER (OCTOBER 2018)
(404)
LEGEND
DRAINAGE FEATURE
STREAM
PROPERTY LINE
SUBJECT PROPERTY LINE
FENCE LINES
POWER LINES
STORM SEWER
SANITARY SEWER
BUILDINGS
TREELINE
FUEL OIL AST BUILDING
PROPANE AST
MONITOR WELL
DEEP MONITOR WELL
ABANDONED MONITOR WELL
SEWER FLOW DIRECTION
1,1-DCE CONCENTRATION (μg/L)
>350 μg/L 1,1-DCE
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
VACANT
ABANDONED RAILROAD RIGHT-OF-WAYPOWER
SUBSTATION
AREA SUPPLIED WITH
CITY WATER AREA SUPPLIED WITH
CITY WATER
VACANT
VACANT
VACANT
FORMER
FULFLEX
AREA SUPPLIED WITH
CITY WATER
FORMER
HAZARDOUS
MATERIALS BUILDING
TRANSFORMERSCOOLING TOWER
DIRT ROAD
SOLAR
FARM
EDWARD
S

F
O
R
K CHESTNUT STREETGRACE STREETRAILROAD STREET7th STR
E
E
T
FOOD LI
O
N

R
O
A
D

(
D
I
R
T
)
(NS)
<2.0
(4,740)
(6.7)
(598)
(206)
(37.6)
(6.7)
(<2.0)
(<2.0)
(<2.0)
(2.2)
(<2.0)
(NS)
(24.1)
(NS)
(4.0/33.2/<2.0)
(<2.0)
(<2.0)
(<2.0)3003
3,000
MW-9 MW-19
MW-17/17D/17DD
MW-12
MW-20
MW-10
MW-16
MW-14
MW-2D
MW-3
MW-7
MW-1
MW-6
MW-4 MW-5
MW-2MW-11
MW-15
MW-13
MW-8R MW-18
MW-8
JOB NO. FUL-006
REVISION NO. 0DATE: 11-05-18
FIGURE NO. 9
FORMER FULFLEX FACILITY
SCOTLAND NECK, NORTH CAROLINA
1,4-DIOXANE CONCENTRATIONS IN
GROUNDWATER (OCTOBER 2018)
NOTES:
1.BOLD CONCENTRATIONS INDICATES AN EXCEEDANCE OF
THE 2L STANDARD (3 μg/L).
2.NS = NOT SAMPLED
(6.7)
LEGEND
DRAINAGE FEATURE
STREAM
PROPERTY LINE
SUBJECT PROPERTY LINE
FENCE LINES
POWER LINES
STORM SEWER
SANITARY SEWER
BUILDINGS
TREELINE
FUEL OIL AST BUILDING
PROPANE AST
MONITOR WELL
DEEP MONITOR WELL
ABANDONED MONITOR WELL
SEWER FLOW DIRECTION
1,4 DIOXANE CONCENTRATION (μg/L)
>3,000 μg/L 1,4-DIOXANE
>300 μg/L 1,4-DIOXANE
>3 μg/L 1,4-DIOXANE
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
BUILDING
MW-8
MW-9
MW-12
MW-19
MW-20
MW-18
MW-10
FORMER HAZARDOUS
MATERIALS BUILDING
MW-2D
MW-3
MW-7
MW-1
MW-6
MW-4 MW-5
MW-2
MW-11
MW-13
TRANSFORMERS
COOLING
TOWER
SOLAR FARM
MW-8R
ABANDONED RAILROAD RIGHT-OF-WAY7TH ST
R
E
E
T CHESTNUT STREETINJECTION ZONE
150FT BY 200FT
AND 40FT DEEP
MW-19 10/4/18 2L STANDARD
BARIUM 0.343 0.700
CHROMIUM
(TOTAL)0.0208 0.010
LEAD 0.0080 0.015
FORMER FULFLEX FACILITY
SCOTLAND NECK, NORTH CAROLINA
RCRA METAL CONCENTRATIONS
IN GROUNDWATER
(OCTOBER 2018)
PARKING
MW-13 10/4/18
BARIUM 0.188
MW-8R 10/4/18
MERCURY 0.0014
ARSENIC 0.343
MW-10 10/4/18
BARIUM 0.241
MERCURY 0.00048
MW-18 10/4/18
BARIUM 0.0658
LEAD 0.0058
MW-9 10/4/18
BARIUM 0.322
MW-19 10/4/18
BARIUM 0.0323
CHROMIUM
(TOTAL)0.0208
LEAD 0.0080
WELL ID
CONSTITUENT
CONCENTRATION
(mg/L)
SAMPLE DATE
NOTES:
1.ONLY DETECTED METALS SHOWN FOR EACH
MONITORING WELL.
2.BOLD CONCENTRATIONS EXCEED APPLICABLE NC
2L GROUNDWATER STANDARD.
JOB NO. FUL-006
REVISION NO. 0DATE: 11-05-18
FIGURE NO. 10
LEGEND
DRAINAGE FEATURE
PROPERTY LINE
SUBJECT PROPERTY LINE
FENCE LINES
POWER LINES
STORM SEWER
SANITARY SEWER
BUILDINGS
TREELINE
FUEL OIL AST BUILDING
PROPANE AST
MONITOR WELL
DEEP MONITOR WELL
ABANDONED MONITOR WELL
SEWER FLOW DIRECTION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
S:\American CAD Figures\FUL-006\Metal Concentrations in Groundwater-20181105.dwg, Fig 10, 1/3/2019 12:24:20 PM,SVincent

Appendix A Groundwater Sampling Forms
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/5/1820.00 5.27Chase GoodwinLPDE Poly18.00SUNNY 86°F10:5010:5511:0011:0511:1011:1511:205.956.036.036.026.036.036.030.290.220.200.170.170.150.1524.925.926.126.426.325.626.1103.2106.7117.8120.5127.0124.9125.55.986.016.066.086.096.096.09-191.0-197.8-183.6-171.7-160.1-161.7-153.621.3028.3623.1419.5415.3313.269.41YSI, Hach turbidimeterFedEx3-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIMPeristalticPVC2-inch11:20Pace AnalyticalMW-1
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/5/1817.005.38HNR1/4" OD Poly1210:4510:5010:5511:0011:055.405.435.445.445.440mL750150022503000150mL/min 2.001.250.910.780.8021.020.420.520.420.1133.9135.4134.5131.8128.05.274.944.965.025.0247.855.352.447.847.3138.6069.0936.4528.0423.94YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch11:05Pace Analytical MW-2717
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/5/1820.00 6.89Chase GoodwinLPDE Poly18.00SUNNY 77°F08:4508:5008:5509:0009:0509:1009:156.926.926.926.936.936.936.931.411.501.681.541.441.521.4221.722.122.422.422.522.523.0135.8129.0125.6124.1124.3124.7124.84.704.664.654.644.634.614.6124.529.037.639.232.926.432.649.9819.4238.6513.497.014.613.77YSI, Hach turbidimeterFedex3-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIMPeristalticPVC2-inch09:15Pace AnalyticalMW- 3
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/5/1818.007.72HNR1/4" OD Poly1311:2511:3011:3511:4011:457.787.767.757.757.750mL750150022503000150mL/min 2.691.141.020.971.0823.321.321.220.920.987.587.585.685.485.74.383.903.813.873.8173.0110.7119.5115.5118.238.0032.3219.1117.1713.58YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch11:45Pace Analytical MW-4818
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/5/1820.006.80HNR1/4" OD Poly1509:4509:5009:5510:0010:0510:106.846.876.896.906.906.900mL7501500225030003750150mL/min 2.871.621.681.751.801.9418.918.718.318.418.418.5145.1143.8143.9143.8142.5140.84.334.104.144.174.214.2792.1107.5103.795.090.987.150.6053.70103.50317.80388.50669.20YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch10:10Pace Analytical MW-51020
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/5/1819.006.90HNR1/4" OD Poly1408:4508:5008:5509:0009:0509:1009:157.387.718.138.007.987.957.950mL75015002250300037504500150mL/min 2.822.394.193.092.462.412.3219.018.918.818.818.919.019.0281.0243.7167.6165.5165.0165.4165.75.554.413.633.703.773.783.7929.984.7129.6126.2122.6120.2118.924.8322.4019.9414.1011.5011.0110.89YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch09:15Pace Analytical MW-6919
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006Former FulflexScotlandneck10/5/1820.00 2.91Chase G.18.00Sunny 82°F09:5009:5510:0010:0510:1010:1510:2010:252.942.942.942.942.942.942.942.940.500.310.260.250.210.190.210.1923.224.024.124.124.524.124.124.8281.7283.7284.7283.8285.3285.7285.3285.74.864.854.854.854.854.854.854.856.2-56.9-76.1-86.5-93.9-103.3-109.2-106.546.359.9110.648.114.994.835.294.12Ysi Pro. HACH 2100Q turbidimeterFedEx3-40mL vials with HCL FOR 8260, 3-40mL vials with HCL for 8260-SIMPeristaltic2"10:25Pace AnalyticalMW-7
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/4/1820.00 9.85Chase GoodwinLPDE Poly18.00High conductivity is causing WLM togive inconsistet readings. No readings taken.18:2518:3018:3518:4018:4518:5018:5519:000.530.360.250.230.200.180.180.2026.926.926.726.826.626.626.626.57,058.07,228.07,282.07,305.07,308.07,295.07,255.07,202.03.673.653.663.673.673.703.713.72368.0447.4465.3462.8492.0494.2484.8488.348.4540.9921.6618.3614.5410.798.445.48Sodium Persulfate. 35 mg/LYSI, Hach. TurbidimeterCourier3-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIM1-125mLplastic HNO3 for RCRA metals+NA, 1-125mLplastic umpres. for 300.0 sulfate, chloridePeristalticPVC2-inch19:00Pace AnalyticalMW-8R
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/4/1820.009.80HNR1/4" OD Poly1517:4017:4517:5017:5518:0018:0510.0110.4310.6410.8310.8510.860mL7501500225030003750150mL/min 5.333.181.911.481.321.2223.522.522.422.222.022.1433.3429.7427.6427.8428.1419.74.063.823.863.923.954.04128.2139.2135.0128.1124.0119.27.707.063.472.393.583.27YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch18:05Pace Analytical MW-91020
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/4/1820.009.53HNR1/4" OD Poly1518:3518:4018:4518:5018:5519:0019:059.699.699.699.699.699.699.690mL75015002250300037504500150mL/min 5.903.022.552.372.382.122.3522.721.721.621.521.421.321.4345.0346.2343.9343.7341.8343.7345.14.613.943.954.004.004.014.0388.7127.0123.3119.7119.0116.2113.827.4925.2214.1813.1513.3710.158.55YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch19:05Pace Analytical MW-101020
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/4/1820.006.63HNR1/4" OD Poly1516:3016:3516:4016:4516:5016:5517:007.197.767.757.757.757.757.750mL75015002250300037504500150mL/min 3.052.171.741.451.181.071.0029.629.029.329.128.828.528.4177.4170.1170.8170.6171.8173.0172.53.913.613.613.623.643.643.63136.7160.9166.6162.8151.5149.6159.538.3015.268.046.284.913.976.08YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch17:00Pace Analytical MW-131020
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/4/1820.00 2.53Chase GoodwinLPDE Poly18.00Sunny. 83°F11:1011:1511:2011:2511:3011:352.562.562.562.562.572.573.163.784.164.544.604.5622.823.523.423.223.123.2158.3156.4158.5160.8161.2160.34.784.634.524.484.484.4912.032.157.853.750.449.824.7728.7122.359.436.175.93YSI, HACH TURBIDIMETER3-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIMPeristalticPVC2-inch11:35Pace AnalyticalMW-14
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/4/1820.006.75HNR1/4" OD Poly1514:0014:0514:1014:1514:206.836.826.826.826.820mL750150022503000150mL/min 2.721.881.651.791.9031.227.226.626.426.0142.1101.9101.399.699.35.124.224.034.013.9377.3118.5140.5148.4141.350.84281.1051.9036.4721.53YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC4-inch14:20Pace Analytical MW-151020
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/4/1820.00 11.05Chase GoodwinLPDE Poly18.00Sunny 88°F14:1014:1514:2014:2514:3014:3514:4011.0911.1011.1011.1011.1011.1011.104.263.973.433.623.643.423.6826.625.725.825.925.925.724.471.170.970.470.270.170.970.34.474.404.474.474.474.474.46-4.6-57.3-72.9-83.4-87.8-91.3-92.515.507.714.683.171.621.883-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIMPeristalticPVC2-inch14:40Pace AnalyticalMW-16
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/4/1816.00 5.10Chase GoodwinLPDE Poly15.00Sunny. 88°FWell casing is broken one foot below ground surface. Concrete pad has been disturbed, possibly by mowing tractor in solar farm.12:1512:2012:2512:3012:3512:4012:4512:5012:5513:005.355.325.335.325.315.315.325.265.265.270.830.460.260.200.180.150.130.140.140.1227.728.028.027.928.228.328.229.130.330.3354.1347.9328.5314.2292.1286.6267.2262.0257.8254.45.886.026.056.066.066.066.066.066.066.06-178.2-191.2-195.8-193.5-216.1-201.0-192.4-201.3-193.9-195.964.5926.1419.2314.0210.549.068.406.386.766.05YSI, Hach turbidimeterFedEx3-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIMPeristalticPVC1-inch13:00Pace AnalyticalMW-17
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/4/1828.004.91HNR1/4" OD Poly12:2012:2512:3012:3512:404.985.045.125.275.280mL750150022503000150mL/min 2.201.781.771.871.8320.720.420.019.820.1188.4189.3187.5186.3182.35.294.994.874.894.8293.1108.3111.3109.3109.5136.5088.7760.6036.9060.60YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC1-inch12:40Pace Analytical MW-17D2328
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria3ULPDU\ 6HFRQGDU\S+XQLW '2PJO6 &RQG 253P9Turb. +/- 10% (<10 NTUsIRUPHWDOV)LOW-FLOW GROUNDWATER Other Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):SAMPLING RECORDWell Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________Well Diameter:Sampling Personnel:___________________________BBBBBBBBBBBBBBBBBBBBBBBBBB6FUHHQ,QWHUYDOIWEJVBBBBBBBBBBBBBBBBBBBBBBBBBBBType of Pump:____________________________ Tubing Material:____________________________ Pump/Tubing set at:__________________ ft.Weather Conditions:_______________________________________________________NOTES:*5281':$7(R SAMPLING PARAMETERSFUL-006FulflexScotland Neck, NC10/4/1858.005.56HNR1/4" OD Poly55.511:1011:1511:2011:2511:3011:3511:4011:4511:5011:5512:0012:055.595.645.735.866.056.826.886.926.926.926.926.920mL7501500225030003750450052506000675075008250150mL/min 1.630.890.560.590.720.680.520.470.450.440.410.4319.419.319.219.219.319.118.918.918.918.818.718.8107.3106.1112.6117.0139.6191.8225.2232.9245.1262.0272.2277.36.986.215.925.986.116.416.646.706.806.886.957.03-30.35.918.311.72.6-20.9-43.1-49.6-59.6-70.4-78.7-85.0101.6087.5653.9239.0932.9830.8432.6031.6231.8034.9434.8530.91YSI pro plus, MicroTPI turbidimeterFedExSee chainPeristalticPVC2-inch12:05Pace Analytical MW-17DD5358
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/4/1820.00 9.79Chase GoodwinLPDE Poly18.0017:0017:0517:1017:1517:2017:2517:3017:3517:4017:4517:5017:559.909.859.859.849.849.849.849.919.929.929.939.930.760.610.580.470.410.420.360.340.310.300.280.2725.726.326.226.226.126.126.125.525.425.425.425.4685.0702.0729.0752.0782.0810.0825.0856.0870.0886.0891.0899.04.094.094.084.074.064.044.044.024.014.014.004.00-99.5-125.7-133.1-132.2-130.6-135.0-133.7-132.2-141.8-155.0-158.5-163.751.9136.7726.2012.299.627.126.295.634.894.503.753.52Sodium Persulfate. 0.0 mg/L3-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIM1-125mLplastic HNO3 for RCRA metals+NA, 1-125mLplastic umpres. for 300.0 sulfate, chloridePeristalticPVC1-inch17:55Pace AnalyticalMW-18
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling RecordDate:1/21/2016Job No:Well ID:Well Location:Facility Name:Date:Top of Casing Elevation (ft msl):_______________ Casing Material:_______________ Volume of Water Per Well Volume:Total Well Depth (ft):_____________________Depth to Water (ft):_________________________________ Well Diameter:Sampling Personnel:___________________________,___________________________,________________________,________________________Type of Pump:____________________________ Tubing Material:______________________________ Pump/Tubing set at:____________________ ft.Weather Conditions:_______________________________________________________ NOTES:__________________________________________Water Volume Pumping DO Temp. S. Cond. pH ORP TurbidityTimeLevelPumpedRate(mg/l)(oC)(PS/cm)(SU)(mV)(NTU)Stabilization Criteria DO +/- 0.3 mg/lTurb. +/- 10% (<10 NTUs)S. Cond. +/- 3%ORP +/- 10 mVpH +/- 0.1 unitLOW-FLOW GROUNDWATER SAMPLING RECORDOther Sample Parameters:___________________________________________________________________________________________________ Sampled at:____________________________Parameters taken with:Sample Delivered to:________________________________ by ______________________________________ at ____________________________. Field Filtration: )Yes No If yes, which sample parameters were field filtered:_____________________________________________Sample Parameter Containers (Types, Number of Containers, Preservatives):GROUNDWATER SAMPLING PARAMETERSFUL.006FulFlexScotland Neck,NC10/4/1820.00 9.72Chase GoodwinLPDE Poly17.00Sunny 89°F15:4515:5015:5516:0016:0516:1016:1516:2016:2516:3016:359.859.859.869.869.869.879.879.879.879.879.873.143.022.812.812.562.652.462.522.142.042.0125.025.124.524.424.324.224.124.124.024.124.1808.0812.0815.0812.0803.0791.0777.0771.0756.0750.0745.04.764.064.084.054.054.054.054.054.064.064.066.4-36.2-45.8-60.0-42.9-38.4-54.4-54.8-74.3-78.6-83.132.6228.3217.929.615.783.654.391.981.762.381.59Sodium Persulfate 0.0 mg/LYsi, Hach turbidimeterFedex3-40mL amber vial HCL for 8260, 3-40mL amber vial for 8260 SIM1-125mLplastic HNO3 for RCRA metals+NA, 1-125mLplastic umpres. for 300.0 sulfate, chloridePeristalticPVC1-inch16:35Pace AnalyticalMW-19

Appendix B Laboratory Analytical Data
#=CL#
October 16, 2018
LIMS USE: FR - GREG KANELLIS
LIMS OBJECT ID: 92402488
92402488
Project:
Pace Project No.:
RE:
Greg Kanellis
Hart & Hickman
3921 Sunset Ridge Rd.
Suite 301
Raleigh, NC 27607
FUL.006
Dear Greg Kanellis:
Enclosed are the analytical results for sample(s) received by the laboratory on October 08, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 77
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92402488
FUL.006
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 77
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92402488
FUL.006
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92402488001 MW-1 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488002 MW-2 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488003 MW-3 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488004 MW-4 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488005 MW-5 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488006 MW-6 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488007 MW-7 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488008 MW-8R EPA 6010D 8 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8260B 63 PASI-CCL
EPA 8260B Mod.3 PASI-CDLK
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
92402488009 MW-9 EPA 6010D 8 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
92402488010 MW-10 EPA 6010D 8 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8260B 63 PASI-CCL
EPA 8260B Mod.3 PASI-CDLK
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
92402488011 MW-13 EPA 6010D 8 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
92402488012 MW-14 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488013 MW-15 EPA 8260B 63 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 77
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92402488
FUL.006
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8260B Mod.3 PASI-CDLK
92402488014 MW-16 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488015 MW-17 EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488016 MW-17D EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488017 MW-17DD EPA 8260B 63 PASI-CSAS
EPA 8260B Mod.3 PASI-CDLK
92402488018 MW-18 EPA 6010D 8 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8260B 63 PASI-CGAW
EPA 8260B Mod.3 PASI-CDLK
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
92402488019 MW-19 EPA 6010D 8 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8260B 63 PASI-CGAW
EPA 8260B Mod.3 PASI-CDLK
EPA 300.0 Rev 2.1 1993 2 PASI-ACDC
92402488020 TRIP BLANK EPA 8260B 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-1 Lab ID:92402488001 Collected:10/05/18 11:20 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 15:09 67-64-125.0 1
Benzene ND ug/L 10/09/18 15:09 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 15:09 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 15:09 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 15:09 75-27-41.0 1
Bromoform ND ug/L 10/09/18 15:09 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 15:09 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 15:09 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 15:09 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 15:09 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 15:09 75-00-31.0 1
Chloroform ND ug/L 10/09/18 15:09 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 15:09 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 15:09 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 15:09 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 15:09 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 15:09 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 15:09 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 15:09 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 15:09 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 15:09 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 15:09 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 15:09 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 15:09 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 15:09 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 15:09 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 15:09 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 15:09 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 15:09 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 15:09 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 15:09 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 15:09 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 15:09 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 15:09 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 15:09 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 15:09 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 15:09 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 15:09 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 15:09 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 15:09 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 15:09 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 15:09 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 15:09 91-20-31.0 1
Styrene ND ug/L 10/09/18 15:09 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 15:09 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 15:09 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 15:09 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-1 Lab ID:92402488001 Collected:10/05/18 11:20 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 15:09 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 15:09 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 15:09 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 15:09 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 15:09 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 15:09 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 15:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 15:09 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 15:09 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 15:09 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 15:09 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 15:09 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 15:09 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/09/18 15:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/09/18 15:09 17060-07-070-130 1
Toluene-d8 (S)108 %10/09/18 15:09 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/18 19:46 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/12/18 19:46 17060-07-050-150 1
Toluene-d8 (S)109 %10/12/18 19:46 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-2 Lab ID:92402488002 Collected:10/05/18 11:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 15:27 67-64-125.0 1
Benzene ND ug/L 10/09/18 15:27 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 15:27 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 15:27 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 15:27 75-27-41.0 1
Bromoform ND ug/L 10/09/18 15:27 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 15:27 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 15:27 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 15:27 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 15:27 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 15:27 75-00-31.0 1
Chloroform ND ug/L 10/09/18 15:27 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 15:27 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 15:27 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 15:27 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 15:27 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 15:27 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 15:27 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 15:27 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 15:27 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 15:27 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 15:27 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 15:27 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 15:27 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 15:27 107-06-21.0 1
1,1-Dichloroethene 4.2 ug/L 10/09/18 15:27 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 15:27 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 15:27 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 15:27 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 15:27 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 15:27 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 15:27 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 15:27 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 15:27 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 15:27 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 15:27 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 15:27 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 15:27 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 15:27 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 15:27 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 15:27 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 15:27 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 15:27 91-20-31.0 1
Styrene ND ug/L 10/09/18 15:27 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 15:27 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 15:27 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 15:27 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-2 Lab ID:92402488002 Collected:10/05/18 11:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 15:27 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 15:27 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 15:27 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 15:27 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 15:27 79-00-51.0 1
Trichloroethene 3.7 ug/L 10/09/18 15:27 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 15:27 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 15:27 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 15:27 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 15:27 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 15:27 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 15:27 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 15:27 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/09/18 15:27 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %10/09/18 15:27 17060-07-070-130 1
Toluene-d8 (S)107 %10/09/18 15:27 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/18 20:44 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %10/12/18 20:44 17060-07-050-150 1
Toluene-d8 (S)105 %10/12/18 20:44 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-3 Lab ID:92402488003 Collected:10/05/18 09:15 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 15:45 67-64-125.0 1
Benzene ND ug/L 10/09/18 15:45 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 15:45 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 15:45 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 15:45 75-27-41.0 1
Bromoform ND ug/L 10/09/18 15:45 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 15:45 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 15:45 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 15:45 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 15:45 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 15:45 75-00-31.0 1
Chloroform ND ug/L 10/09/18 15:45 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 15:45 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 15:45 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 15:45 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 15:45 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 15:45 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 15:45 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 15:45 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 15:45 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 15:45 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 15:45 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 15:45 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 15:45 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 15:45 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 15:45 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 15:45 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 15:45 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 15:45 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 15:45 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 15:45 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 15:45 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 15:45 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 15:45 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 15:45 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 15:45 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 15:45 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 15:45 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 15:45 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 15:45 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 15:45 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 15:45 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 15:45 91-20-31.0 1
Styrene ND ug/L 10/09/18 15:45 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 15:45 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 15:45 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 15:45 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-3 Lab ID:92402488003 Collected:10/05/18 09:15 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 15:45 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 15:45 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 15:45 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 15:45 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 15:45 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 15:45 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 15:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 15:45 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 15:45 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 15:45 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 15:45 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 15:45 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 15:45 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/09/18 15:45 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/09/18 15:45 17060-07-070-130 1
Toluene-d8 (S)105 %10/09/18 15:45 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)6.7 ug/L 10/12/18 21:03 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %10/12/18 21:03 17060-07-050-150 1
Toluene-d8 (S)108 %10/12/18 21:03 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-4 Lab ID:92402488004 Collected:10/05/18 11:45 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 16:03 67-64-125.0 1
Benzene ND ug/L 10/09/18 16:03 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 16:03 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 16:03 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 16:03 75-27-41.0 1
Bromoform ND ug/L 10/09/18 16:03 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 16:03 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 16:03 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 16:03 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 16:03 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 16:03 75-00-31.0 1
Chloroform ND ug/L 10/09/18 16:03 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 16:03 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 16:03 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 16:03 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 16:03 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 16:03 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 16:03 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 16:03 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 16:03 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 16:03 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 16:03 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 16:03 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 16:03 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 16:03 107-06-21.0 1
1,1-Dichloroethene 1.5 ug/L 10/09/18 16:03 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 16:03 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 16:03 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 16:03 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 16:03 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 16:03 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 16:03 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 16:03 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 16:03 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 16:03 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 16:03 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 16:03 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 16:03 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 16:03 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 16:03 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 16:03 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 16:03 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 16:03 91-20-31.0 1
Styrene ND ug/L 10/09/18 16:03 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 16:03 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 16:03 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 16:03 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-4 Lab ID:92402488004 Collected:10/05/18 11:45 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 16:03 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 16:03 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 16:03 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 16:03 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 16:03 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 16:03 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 16:03 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 16:03 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 16:03 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 16:03 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 16:03 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 16:03 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 16:03 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %10/09/18 16:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %10/09/18 16:03 17060-07-070-130 1
Toluene-d8 (S)106 %10/09/18 16:03 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/12/18 21:23 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %10/12/18 21:23 17060-07-050-150 1
Toluene-d8 (S)104 %10/12/18 21:23 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-5 Lab ID:92402488005 Collected:10/05/18 10:10 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 18:11 67-64-125.0 1
Benzene ND ug/L 10/09/18 18:11 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 18:11 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 18:11 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 18:11 75-27-41.0 1
Bromoform ND ug/L 10/09/18 18:11 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 18:11 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 18:11 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 18:11 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 18:11 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 18:11 75-00-31.0 1
Chloroform ND ug/L 10/09/18 18:11 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 18:11 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 18:11 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 18:11 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 18:11 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 18:11 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 18:11 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 18:11 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 18:11 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 18:11 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 18:11 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 18:11 75-71-81.0 1
1,1-Dichloroethane 1.9 ug/L 10/09/18 18:11 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 18:11 107-06-21.0 1
1,1-Dichloroethene 47.0 ug/L 10/09/18 18:11 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 18:11 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 18:11 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 18:11 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 18:11 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 18:11 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 18:11 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 18:11 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 18:11 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 18:11 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 18:11 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 18:11 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 18:11 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 18:11 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 18:11 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 18:11 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 18:11 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 18:11 91-20-31.0 1
Styrene ND ug/L 10/09/18 18:11 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 18:11 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 18:11 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 18:11 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-5 Lab ID:92402488005 Collected:10/05/18 10:10 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 18:11 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 18:11 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 18:11 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 18:11 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 18:11 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 18:11 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 18:11 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 18:11 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 18:11 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 18:11 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 18:11 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 18:11 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 18:11 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %10/09/18 18:11 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %10/09/18 18:11 17060-07-070-130 1
Toluene-d8 (S)110 %10/09/18 18:11 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)2.2 ug/L 10/15/18 13:36 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/15/18 13:36 17060-07-050-150 1
Toluene-d8 (S)108 %10/15/18 13:36 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-6 Lab ID:92402488006 Collected:10/05/18 09:15 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 17:35 67-64-125.0 1
Benzene ND ug/L 10/09/18 17:35 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 17:35 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 17:35 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 17:35 75-27-41.0 1
Bromoform ND ug/L 10/09/18 17:35 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 17:35 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 17:35 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 17:35 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 17:35 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 17:35 75-00-31.0 1
Chloroform ND ug/L 10/09/18 17:35 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 17:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 17:35 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 17:35 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 17:35 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 17:35 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 17:35 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 17:35 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 17:35 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 17:35 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 17:35 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 17:35 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 17:35 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 17:35 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 17:35 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 17:35 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 17:35 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 17:35 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 17:35 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 17:35 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 17:35 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 17:35 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 17:35 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 17:35 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 17:35 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 17:35 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 17:35 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 17:35 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 17:35 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 17:35 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 17:35 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 17:35 91-20-31.0 1
Styrene ND ug/L 10/09/18 17:35 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 17:35 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 17:35 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 17:35 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-6 Lab ID:92402488006 Collected:10/05/18 09:15 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 17:35 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 17:35 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 17:35 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 17:35 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 17:35 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 17:35 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 17:35 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 17:35 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 17:35 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 17:35 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 17:35 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 17:35 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 17:35 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/09/18 17:35 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %10/09/18 17:35 17060-07-070-130 1
Toluene-d8 (S)109 %10/09/18 17:35 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/15/18 13:56 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %10/15/18 13:56 17060-07-050-150 1
Toluene-d8 (S)111 %10/15/18 13:56 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-7 Lab ID:92402488007 Collected:10/05/18 10:25 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 19:40 67-64-125.0 1
Benzene ND ug/L 10/09/18 19:40 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 19:40 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 19:40 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 19:40 75-27-41.0 1
Bromoform ND ug/L 10/09/18 19:40 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 19:40 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 19:40 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 19:40 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 19:40 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 19:40 75-00-31.0 1
Chloroform ND ug/L 10/09/18 19:40 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 19:40 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 19:40 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 19:40 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 19:40 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 19:40 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 19:40 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 19:40 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 19:40 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 19:40 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 19:40 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 19:40 75-71-81.0 1
1,1-Dichloroethane 16.0 ug/L 10/09/18 19:40 75-34-31.0 1
1,2-Dichloroethane 2.7 ug/L 10/09/18 19:40 107-06-21.0 1
1,1-Dichloroethene 99.3 ug/L 10/09/18 19:40 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 19:40 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 19:40 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 19:40 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 19:40 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 19:40 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 19:40 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 19:40 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 19:40 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 19:40 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 19:40 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 19:40 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 19:40 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 19:40 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 19:40 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 19:40 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 19:40 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 19:40 91-20-31.0 1
Styrene ND ug/L 10/09/18 19:40 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 19:40 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 19:40 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 19:40 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-7 Lab ID:92402488007 Collected:10/05/18 10:25 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 19:40 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 19:40 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 19:40 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 19:40 71-55-61.0 1
1,1,2-Trichloroethane 3.8 ug/L 10/09/18 19:40 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 19:40 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 19:40 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 19:40 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 19:40 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 19:40 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 19:40 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 19:40 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 19:40 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/09/18 19:40 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/09/18 19:40 17060-07-070-130 1
Toluene-d8 (S)104 %10/09/18 19:40 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)24.1 ug/L 10/15/18 14:16 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %10/15/18 14:16 17060-07-050-150 1
Toluene-d8 (S)112 %10/15/18 14:16 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-8R Lab ID:92402488008 Collected:10/04/18 19:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic 343 ug/L 10/10/18 16:11 7440-38-2 M610/09/18 11:3020020
Barium ND ug/L 10/10/18 16:11 7440-39-3 D310/09/18 11:3010020
Cadmium ND ug/L 10/10/18 16:11 7440-43-9 D310/09/18 11:3020.0 20
Chromium ND ug/L 10/10/18 16:11 7440-47-3 D3,M610/09/18 11:3010020
Lead ND ug/L 10/10/18 16:11 7439-92-1 D3,M610/09/18 11:3010020
Selenium ND ug/L 10/10/18 16:11 7782-49-2 D310/09/18 11:3020020
Silver ND ug/L 10/10/18 16:11 7440-22-4 D3,M610/09/18 11:3010020
Sodium 1210000 ug/L 10/10/18 16:11 7440-23-5 M610/09/18 11:3010000020
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury 1.4 ug/L 10/10/18 12:49 7439-97-610/09/18 18:220.20 1
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/10/18 02:26 67-64-15000200
Benzene ND ug/L 10/10/18 02:26 71-43-2200200
Bromobenzene ND ug/L 10/10/18 02:26 108-86-1200200
Bromochloromethane ND ug/L 10/10/18 02:26 74-97-5200200
Bromodichloromethane ND ug/L 10/10/18 02:26 75-27-4200200
Bromoform ND ug/L 10/10/18 02:26 75-25-2200200
Bromomethane ND ug/L 10/10/18 02:26 74-83-9400200
2-Butanone (MEK)ND ug/L 10/10/18 02:26 78-93-31000200
Carbon tetrachloride ND ug/L 10/10/18 02:26 56-23-5200200
Chlorobenzene ND ug/L 10/10/18 02:26 108-90-7200200
Chloroethane ND ug/L 10/10/18 02:26 75-00-3200200
Chloroform ND ug/L 10/10/18 02:26 67-66-3200200
Chloromethane 699 ug/L 10/10/18 02:26 74-87-3200200
2-Chlorotoluene ND ug/L 10/10/18 02:26 95-49-8200200
4-Chlorotoluene ND ug/L 10/10/18 02:26 106-43-4200200
1,2-Dibromo-3-chloropropane ND ug/L 10/10/18 02:26 96-12-8400200
Dibromochloromethane ND ug/L 10/10/18 02:26 124-48-1200200
1,2-Dibromoethane (EDB)ND ug/L 10/10/18 02:26 106-93-4200200
Dibromomethane ND ug/L 10/10/18 02:26 74-95-3200200
1,2-Dichlorobenzene ND ug/L 10/10/18 02:26 95-50-1200200
1,3-Dichlorobenzene ND ug/L 10/10/18 02:26 541-73-1200200
1,4-Dichlorobenzene ND ug/L 10/10/18 02:26 106-46-7200200
Dichlorodifluoromethane ND ug/L 10/10/18 02:26 75-71-8200200
1,1-Dichloroethane 4390 ug/L 10/10/18 02:26 75-34-3200200
1,2-Dichloroethane 590 ug/L 10/10/18 02:26 107-06-2200200
1,1-Dichloroethene 2770 ug/L 10/10/18 02:26 75-35-4200200
cis-1,2-Dichloroethene ND ug/L 10/10/18 02:26 156-59-2200200
trans-1,2-Dichloroethene ND ug/L 10/10/18 02:26 156-60-5200200
1,2-Dichloropropane ND ug/L 10/10/18 02:26 78-87-5200200
1,3-Dichloropropane ND ug/L 10/10/18 02:26 142-28-9200200
2,2-Dichloropropane ND ug/L 10/10/18 02:26 594-20-7200200
1,1-Dichloropropene ND ug/L 10/10/18 02:26 563-58-6200200
cis-1,3-Dichloropropene ND ug/L 10/10/18 02:26 10061-01-5200200
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-8R Lab ID:92402488008 Collected:10/04/18 19:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 10/10/18 02:26 10061-02-6200200
Diisopropyl ether ND ug/L 10/10/18 02:26 108-20-3200200
Ethylbenzene ND ug/L 10/10/18 02:26 100-41-4200200
Hexachloro-1,3-butadiene ND ug/L 10/10/18 02:26 87-68-3200200
2-Hexanone ND ug/L 10/10/18 02:26 591-78-61000200
p-Isopropyltoluene ND ug/L 10/10/18 02:26 99-87-6200200
Methylene Chloride ND ug/L 10/10/18 02:26 75-09-2400200
4-Methyl-2-pentanone (MIBK)ND ug/L 10/10/18 02:26 108-10-11000200
Methyl-tert-butyl ether ND ug/L 10/10/18 02:26 1634-04-4200200
Naphthalene ND ug/L 10/10/18 02:26 91-20-3200200
Styrene ND ug/L 10/10/18 02:26 100-42-5200200
1,1,1,2-Tetrachloroethane ND ug/L 10/10/18 02:26 630-20-6200200
1,1,2,2-Tetrachloroethane ND ug/L 10/10/18 02:26 79-34-5200200
Tetrachloroethene ND ug/L 10/10/18 02:26 127-18-4200200
Toluene ND ug/L 10/10/18 02:26 108-88-3200200
1,2,3-Trichlorobenzene ND ug/L 10/10/18 02:26 87-61-6200200
1,2,4-Trichlorobenzene ND ug/L 10/10/18 02:26 120-82-1200200
1,1,1-Trichloroethane 24900 ug/L 10/10/18 02:26 71-55-6200200
1,1,2-Trichloroethane 657 ug/L 10/10/18 02:26 79-00-5200200
Trichloroethene ND ug/L 10/10/18 02:26 79-01-6200200
Trichlorofluoromethane ND ug/L 10/10/18 02:26 75-69-4200200
1,2,3-Trichloropropane ND ug/L 10/10/18 02:26 96-18-4200200
Vinyl acetate ND ug/L 10/10/18 02:26 108-05-4400200
Vinyl chloride ND ug/L 10/10/18 02:26 75-01-4200200
Xylene (Total)ND ug/L 10/10/18 02:26 1330-20-7200200
m&p-Xylene ND ug/L 10/10/18 02:26 179601-23-1400200
o-Xylene ND ug/L 10/10/18 02:26 95-47-6200200
Surrogates
4-Bromofluorobenzene (S)106 %10/10/18 02:26 460-00-470-130 200
1,2-Dichloroethane-d4 (S)94 %10/10/18 02:26 17060-07-070-130 200
Toluene-d8 (S)104 %10/10/18 02:26 2037-26-570-130 200
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)4740 ug/L 10/15/18 14:35 123-91-110050
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/15/18 14:35 17060-07-050-150 50
Toluene-d8 (S)113 %10/15/18 14:35 2037-26-550-150 50
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 1000 mg/L 10/10/18 00:40 16887-00-6 M639.0 39
Sulfate 2060 mg/L 10/10/18 00:40 14808-79-8 M639.0 39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-9 Lab ID:92402488009 Collected:10/04/18 18:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 10/09/18 22:57 7440-38-210/09/18 11:3010.0 1
Barium 322 ug/L 10/09/18 22:57 7440-39-310/09/18 11:305.0 1
Cadmium ND ug/L 10/09/18 22:57 7440-43-910/09/18 11:301.0 1
Chromium ND ug/L 10/09/18 22:57 7440-47-310/09/18 11:305.0 1
Lead ND ug/L 10/09/18 22:57 7439-92-110/09/18 11:305.0 1
Selenium ND ug/L 10/09/18 22:57 7782-49-210/09/18 11:3010.0 1
Silver ND ug/L 10/09/18 22:57 7440-22-410/09/18 11:305.0 1
Sodium 48000 ug/L 10/09/18 22:57 7440-23-510/09/18 11:3050001
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 10/10/18 12:51 7439-97-610/09/18 18:220.20 1
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 19:22 67-64-125.0 1
Benzene ND ug/L 10/09/18 19:22 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 19:22 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 19:22 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 19:22 75-27-41.0 1
Bromoform ND ug/L 10/09/18 19:22 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 19:22 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 19:22 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 19:22 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 19:22 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 19:22 75-00-31.0 1
Chloroform ND ug/L 10/09/18 19:22 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 19:22 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 19:22 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 19:22 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 19:22 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 19:22 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 19:22 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 19:22 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 19:22 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 19:22 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 19:22 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 19:22 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 19:22 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 19:22 107-06-21.0 1
1,1-Dichloroethene 1.2 ug/L 10/09/18 19:22 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 19:22 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 19:22 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 19:22 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 19:22 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 19:22 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 19:22 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 19:22 10061-01-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-9 Lab ID:92402488009 Collected:10/04/18 18:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 10/09/18 19:22 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 19:22 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 19:22 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 19:22 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 19:22 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 19:22 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 19:22 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 19:22 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 19:22 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 19:22 91-20-31.0 1
Styrene ND ug/L 10/09/18 19:22 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 19:22 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 19:22 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 19:22 127-18-41.0 1
Toluene ND ug/L 10/09/18 19:22 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 19:22 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 19:22 120-82-11.0 1
1,1,1-Trichloroethane 3.9 ug/L 10/09/18 19:22 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 19:22 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 19:22 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 19:22 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 19:22 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 19:22 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 19:22 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 19:22 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 19:22 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 19:22 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/09/18 19:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/09/18 19:22 17060-07-070-130 1
Toluene-d8 (S)104 %10/09/18 19:22 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)6.7 ug/L 10/15/18 14:55 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %10/15/18 14:55 17060-07-050-150 1
Toluene-d8 (S)116 %10/15/18 14:55 2037-26-550-150 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 88.5 mg/L 10/10/18 11:48 16887-00-61.0 1
Sulfate 7.1 mg/L 10/10/18 11:48 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-10 Lab ID:92402488010 Collected:10/04/18 19:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 10/09/18 23:00 7440-38-210/09/18 11:3010.0 1
Barium 241 ug/L 10/09/18 23:00 7440-39-310/09/18 11:305.0 1
Cadmium ND ug/L 10/09/18 23:00 7440-43-910/09/18 11:301.0 1
Chromium ND ug/L 10/09/18 23:00 7440-47-310/09/18 11:305.0 1
Lead ND ug/L 10/09/18 23:00 7439-92-110/09/18 11:305.0 1
Selenium ND ug/L 10/09/18 23:00 7782-49-210/09/18 11:3010.0 1
Silver ND ug/L 10/09/18 23:00 7440-22-410/09/18 11:305.0 1
Sodium 49400 ug/L 10/09/18 23:00 7440-23-510/09/18 11:3050001
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury 0.48 ug/L 10/10/18 12:53 7439-97-610/09/18 18:220.20 1
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/14/18 19:36 67-64-150.0 2
Benzene ND ug/L 10/14/18 19:36 71-43-22.0 2
Bromobenzene ND ug/L 10/14/18 19:36 108-86-12.0 2
Bromochloromethane ND ug/L 10/14/18 19:36 74-97-52.0 2
Bromodichloromethane ND ug/L 10/14/18 19:36 75-27-42.0 2
Bromoform ND ug/L 10/14/18 19:36 75-25-22.0 2
Bromomethane ND ug/L 10/14/18 19:36 74-83-94.0 2
2-Butanone (MEK)ND ug/L 10/14/18 19:36 78-93-310.0 2
Carbon tetrachloride ND ug/L 10/14/18 19:36 56-23-52.0 2
Chlorobenzene ND ug/L 10/14/18 19:36 108-90-72.0 2
Chloroethane ND ug/L 10/14/18 19:36 75-00-32.0 2
Chloroform ND ug/L 10/14/18 19:36 67-66-32.0 2
Chloromethane ND ug/L 10/14/18 19:36 74-87-32.0 2
2-Chlorotoluene ND ug/L 10/14/18 19:36 95-49-82.0 2
4-Chlorotoluene ND ug/L 10/14/18 19:36 106-43-42.0 2
1,2-Dibromo-3-chloropropane ND ug/L 10/14/18 19:36 96-12-84.0 2
Dibromochloromethane ND ug/L 10/14/18 19:36 124-48-12.0 2
1,2-Dibromoethane (EDB)ND ug/L 10/14/18 19:36 106-93-42.0 2
Dibromomethane ND ug/L 10/14/18 19:36 74-95-32.0 2
1,2-Dichlorobenzene ND ug/L 10/14/18 19:36 95-50-12.0 2
1,3-Dichlorobenzene ND ug/L 10/14/18 19:36 541-73-12.0 2
1,4-Dichlorobenzene ND ug/L 10/14/18 19:36 106-46-72.0 2
Dichlorodifluoromethane ND ug/L 10/14/18 19:36 75-71-82.0 2
1,1-Dichloroethane 22.7 ug/L 10/14/18 19:36 75-34-32.0 2
1,2-Dichloroethane 4.9 ug/L 10/14/18 19:36 107-06-22.0 2
1,1-Dichloroethene 134 ug/L 10/14/18 19:36 75-35-42.0 2
cis-1,2-Dichloroethene ND ug/L 10/14/18 19:36 156-59-22.0 2
trans-1,2-Dichloroethene ND ug/L 10/14/18 19:36 156-60-52.0 2
1,2-Dichloropropane ND ug/L 10/14/18 19:36 78-87-52.0 2
1,3-Dichloropropane ND ug/L 10/14/18 19:36 142-28-92.0 2
2,2-Dichloropropane ND ug/L 10/14/18 19:36 594-20-72.0 2
1,1-Dichloropropene ND ug/L 10/14/18 19:36 563-58-62.0 2
cis-1,3-Dichloropropene ND ug/L 10/14/18 19:36 10061-01-52.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-10 Lab ID:92402488010 Collected:10/04/18 19:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 10/14/18 19:36 10061-02-62.0 2
Diisopropyl ether ND ug/L 10/14/18 19:36 108-20-32.0 2
Ethylbenzene ND ug/L 10/14/18 19:36 100-41-42.0 2
Hexachloro-1,3-butadiene ND ug/L 10/14/18 19:36 87-68-32.0 2
2-Hexanone ND ug/L 10/14/18 19:36 591-78-610.0 2
p-Isopropyltoluene ND ug/L 10/14/18 19:36 99-87-62.0 2
Methylene Chloride ND ug/L 10/14/18 19:36 75-09-24.0 2
4-Methyl-2-pentanone (MIBK)ND ug/L 10/14/18 19:36 108-10-110.0 2
Methyl-tert-butyl ether ND ug/L 10/14/18 19:36 1634-04-42.0 2
Naphthalene ND ug/L 10/14/18 19:36 91-20-32.0 2
Styrene ND ug/L 10/14/18 19:36 100-42-52.0 2
1,1,1,2-Tetrachloroethane ND ug/L 10/14/18 19:36 630-20-62.0 2
1,1,2,2-Tetrachloroethane ND ug/L 10/14/18 19:36 79-34-52.0 2
Tetrachloroethene ND ug/L 10/14/18 19:36 127-18-42.0 2
Toluene ND ug/L 10/14/18 19:36 108-88-32.0 2
1,2,3-Trichlorobenzene ND ug/L 10/14/18 19:36 87-61-62.0 2
1,2,4-Trichlorobenzene ND ug/L 10/14/18 19:36 120-82-12.0 2
1,1,1-Trichloroethane ND ug/L 10/14/18 19:36 71-55-62.0 2
1,1,2-Trichloroethane 3.1 ug/L 10/14/18 19:36 79-00-52.0 2
Trichloroethene ND ug/L 10/14/18 19:36 79-01-62.0 2
Trichlorofluoromethane ND ug/L 10/14/18 19:36 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 10/14/18 19:36 96-18-42.0 2
Vinyl acetate ND ug/L 10/14/18 19:36 108-05-44.0 2
Vinyl chloride ND ug/L 10/14/18 19:36 75-01-42.0 2
Xylene (Total)ND ug/L 10/14/18 19:36 1330-20-72.0 2
m&p-Xylene ND ug/L 10/14/18 19:36 179601-23-14.0 2
o-Xylene ND ug/L 10/14/18 19:36 95-47-62.0 2
Surrogates
4-Bromofluorobenzene (S)103 %10/14/18 19:36 460-00-470-130 2
1,2-Dichloroethane-d4 (S)103 %10/14/18 19:36 17060-07-070-130 2
Toluene-d8 (S)97 %10/14/18 19:36 2037-26-570-130 2
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)37.6 ug/L 10/15/18 15:14 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %10/15/18 15:14 17060-07-050-150 1
Toluene-d8 (S)111 %10/15/18 15:14 2037-26-550-150 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 66.3 mg/L 10/10/18 12:06 16887-00-61.0 1
Sulfate 8.5 mg/L 10/10/18 12:06 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-13 Lab ID:92402488011 Collected:10/04/18 17:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 10/09/18 23:03 7440-38-210/09/18 11:3010.0 1
Barium 188 ug/L 10/09/18 23:03 7440-39-310/09/18 11:305.0 1
Cadmium ND ug/L 10/09/18 23:03 7440-43-910/09/18 11:301.0 1
Chromium ND ug/L 10/09/18 23:03 7440-47-310/09/18 11:305.0 1
Lead ND ug/L 10/09/18 23:03 7439-92-110/09/18 11:305.0 1
Selenium ND ug/L 10/09/18 23:03 7782-49-210/09/18 11:3010.0 1
Silver ND ug/L 10/09/18 23:03 7440-22-410/09/18 11:305.0 1
Sodium 14400 ug/L 10/09/18 23:03 7440-23-510/09/18 11:3050001
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 10/10/18 12:56 7439-97-610/09/18 18:220.20 1
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 16:20 67-64-125.0 1
Benzene ND ug/L 10/09/18 16:20 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 16:20 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 16:20 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 16:20 75-27-41.0 1
Bromoform ND ug/L 10/09/18 16:20 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 16:20 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 16:20 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 16:20 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 16:20 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 16:20 75-00-31.0 1
Chloroform ND ug/L 10/09/18 16:20 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 16:20 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 16:20 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 16:20 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 16:20 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 16:20 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 16:20 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 16:20 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 16:20 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 16:20 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 16:20 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 16:20 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 16:20 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 16:20 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 16:20 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 16:20 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 16:20 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 16:20 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 16:20 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 16:20 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 16:20 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 16:20 10061-01-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-13 Lab ID:92402488011 Collected:10/04/18 17:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 10/09/18 16:20 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 16:20 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 16:20 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 16:20 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 16:20 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 16:20 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 16:20 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 16:20 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 16:20 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 16:20 91-20-31.0 1
Styrene ND ug/L 10/09/18 16:20 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 16:20 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 16:20 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 16:20 127-18-41.0 1
Toluene ND ug/L 10/09/18 16:20 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 16:20 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 16:20 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 16:20 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 16:20 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 16:20 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 16:20 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 16:20 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 16:20 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 16:20 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 16:20 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 16:20 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 16:20 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/09/18 16:20 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/09/18 16:20 17060-07-070-130 1
Toluene-d8 (S)109 %10/09/18 16:20 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/15/18 15:34 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/15/18 15:34 17060-07-050-150 1
Toluene-d8 (S)117 %10/15/18 15:34 2037-26-550-150 1
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 36.1 mg/L 10/10/18 12:23 16887-00-61.0 1
Sulfate 6.0 mg/L 10/10/18 12:23 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-14 Lab ID:92402488012 Collected:10/04/18 11:35 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 16:38 67-64-125.0 1
Benzene ND ug/L 10/09/18 16:38 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 16:38 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 16:38 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 16:38 75-27-41.0 1
Bromoform ND ug/L 10/09/18 16:38 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 16:38 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 16:38 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 16:38 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 16:38 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 16:38 75-00-31.0 1
Chloroform ND ug/L 10/09/18 16:38 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 16:38 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 16:38 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 16:38 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 16:38 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 16:38 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 16:38 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 16:38 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 16:38 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 16:38 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 16:38 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 16:38 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 16:38 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 16:38 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 16:38 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 16:38 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 16:38 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 16:38 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 16:38 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 16:38 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 16:38 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 16:38 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 16:38 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 16:38 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 16:38 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 16:38 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 16:38 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 16:38 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 16:38 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 16:38 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 16:38 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 16:38 91-20-31.0 1
Styrene ND ug/L 10/09/18 16:38 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 16:38 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 16:38 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 16:38 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-14 Lab ID:92402488012 Collected:10/04/18 11:35 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 16:38 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 16:38 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 16:38 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 16:38 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 16:38 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 16:38 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 16:38 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 16:38 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 16:38 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 16:38 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 16:38 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 16:38 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 16:38 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/09/18 16:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %10/09/18 16:38 17060-07-070-130 1
Toluene-d8 (S)113 %10/09/18 16:38 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/15/18 15:53 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %10/15/18 15:53 17060-07-050-150 1
Toluene-d8 (S)116 %10/15/18 15:53 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-15 Lab ID:92402488013 Collected:10/04/18 14:20 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 17:17 67-64-125.0 1
Benzene ND ug/L 10/09/18 17:17 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 17:17 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 17:17 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 17:17 75-27-41.0 1
Bromoform ND ug/L 10/09/18 17:17 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 17:17 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 17:17 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 17:17 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 17:17 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 17:17 75-00-31.0 1
Chloroform ND ug/L 10/09/18 17:17 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 17:17 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 17:17 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 17:17 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 17:17 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 17:17 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 17:17 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 17:17 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 17:17 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 17:17 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 17:17 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 17:17 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 17:17 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 17:17 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 17:17 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 17:17 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 17:17 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 17:17 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 17:17 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 17:17 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 17:17 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 17:17 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 17:17 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 17:17 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 17:17 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 17:17 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 17:17 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 17:17 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 17:17 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 17:17 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 17:17 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 17:17 91-20-31.0 1
Styrene ND ug/L 10/09/18 17:17 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 17:17 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 17:17 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 17:17 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-15 Lab ID:92402488013 Collected:10/04/18 14:20 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 17:17 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 17:17 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 17:17 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 17:17 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 17:17 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 17:17 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 17:17 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 17:17 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 17:17 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 17:17 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 17:17 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 17:17 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 17:17 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %10/09/18 17:17 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/09/18 17:17 17060-07-070-130 1
Toluene-d8 (S)108 %10/09/18 17:17 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/15/18 16:13 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)102 %10/15/18 16:13 17060-07-050-150 1
Toluene-d8 (S)116 %10/15/18 16:13 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-16 Lab ID:92402488014 Collected:10/04/18 14:40 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 16:56 67-64-125.0 1
Benzene ND ug/L 10/09/18 16:56 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 16:56 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 16:56 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 16:56 75-27-41.0 1
Bromoform ND ug/L 10/09/18 16:56 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 16:56 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 16:56 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 16:56 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 16:56 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 16:56 75-00-31.0 1
Chloroform ND ug/L 10/09/18 16:56 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 16:56 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 16:56 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 16:56 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 16:56 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 16:56 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 16:56 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 16:56 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 16:56 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 16:56 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 16:56 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 16:56 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 16:56 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 16:56 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 16:56 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 16:56 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 16:56 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 16:56 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 16:56 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 16:56 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 16:56 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 16:56 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 16:56 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 16:56 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 16:56 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 16:56 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 16:56 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 16:56 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 16:56 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 16:56 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 16:56 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 16:56 91-20-31.0 1
Styrene ND ug/L 10/09/18 16:56 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 16:56 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 16:56 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 16:56 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-16 Lab ID:92402488014 Collected:10/04/18 14:40 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 16:56 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 16:56 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 16:56 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 16:56 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 16:56 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 16:56 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 16:56 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 16:56 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 16:56 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 16:56 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 16:56 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 16:56 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 16:56 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/09/18 16:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %10/09/18 16:56 17060-07-070-130 1
Toluene-d8 (S)106 %10/09/18 16:56 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/15/18 16:32 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)106 %10/15/18 16:32 17060-07-050-150 1
Toluene-d8 (S)119 %10/15/18 16:32 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-17 Lab ID:92402488015 Collected:10/04/18 13:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 18:29 67-64-125.0 1
Benzene ND ug/L 10/09/18 18:29 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 18:29 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 18:29 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 18:29 75-27-41.0 1
Bromoform ND ug/L 10/09/18 18:29 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 18:29 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 18:29 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 18:29 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 18:29 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 18:29 75-00-31.0 1
Chloroform ND ug/L 10/09/18 18:29 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 18:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 18:29 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 18:29 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 18:29 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 18:29 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 18:29 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 18:29 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 18:29 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 18:29 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 18:29 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 18:29 75-71-81.0 1
1,1-Dichloroethane 1.1 ug/L 10/09/18 18:29 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 18:29 107-06-21.0 1
1,1-Dichloroethene 15.4 ug/L 10/09/18 18:29 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 18:29 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 18:29 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 18:29 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 18:29 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 18:29 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 18:29 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 18:29 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 18:29 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 18:29 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 18:29 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 18:29 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 18:29 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 18:29 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 18:29 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 18:29 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 18:29 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 18:29 91-20-31.0 1
Styrene ND ug/L 10/09/18 18:29 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 18:29 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 18:29 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 18:29 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-17 Lab ID:92402488015 Collected:10/04/18 13:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene 74.4 ug/L 10/09/18 18:29 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 18:29 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 18:29 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 18:29 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 18:29 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 18:29 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 18:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 18:29 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 18:29 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 18:29 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 18:29 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 18:29 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 18:29 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)94 %10/09/18 18:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/09/18 18:29 17060-07-070-130 1
Toluene-d8 (S)102 %10/09/18 18:29 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)4.0 ug/L 10/15/18 16:52 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %10/15/18 16:52 17060-07-050-150 1
Toluene-d8 (S)112 %10/15/18 16:52 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-17D Lab ID:92402488016 Collected:10/04/18 12:40 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 19:58 67-64-125.0 1
Benzene ND ug/L 10/09/18 19:58 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 19:58 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 19:58 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 19:58 75-27-41.0 1
Bromoform ND ug/L 10/09/18 19:58 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 19:58 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 19:58 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 19:58 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 19:58 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 19:58 75-00-31.0 1
Chloroform ND ug/L 10/09/18 19:58 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 19:58 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 19:58 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 19:58 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 19:58 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 19:58 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 19:58 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 19:58 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 19:58 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 19:58 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 19:58 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 19:58 75-71-81.0 1
1,1-Dichloroethane 12.2 ug/L 10/09/18 19:58 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 19:58 107-06-21.0 1
1,1-Dichloroethene 197 ug/L 10/09/18 19:58 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 19:58 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 19:58 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 19:58 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 19:58 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 19:58 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 19:58 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 19:58 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 19:58 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 19:58 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 19:58 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 19:58 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 19:58 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 19:58 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 19:58 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 19:58 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 19:58 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 19:58 91-20-31.0 1
Styrene ND ug/L 10/09/18 19:58 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 19:58 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 19:58 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 19:58 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-17D Lab ID:92402488016 Collected:10/04/18 12:40 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 19:58 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 19:58 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 19:58 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 19:58 71-55-61.0 1
1,1,2-Trichloroethane 2.7 ug/L 10/09/18 19:58 79-00-51.0 1
Trichloroethene 3.5 ug/L 10/09/18 19:58 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 19:58 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 19:58 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 19:58 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 19:58 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 19:58 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 19:58 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 19:58 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/09/18 19:58 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %10/09/18 19:58 17060-07-070-130 1
Toluene-d8 (S)106 %10/09/18 19:58 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)33.2 ug/L 10/15/18 17:31 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %10/15/18 17:31 17060-07-050-150 1
Toluene-d8 (S)116 %10/15/18 17:31 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-17DD Lab ID:92402488017 Collected:10/04/18 12:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/09/18 17:53 67-64-125.0 1
Benzene ND ug/L 10/09/18 17:53 71-43-21.0 1
Bromobenzene ND ug/L 10/09/18 17:53 108-86-11.0 1
Bromochloromethane ND ug/L 10/09/18 17:53 74-97-51.0 1
Bromodichloromethane ND ug/L 10/09/18 17:53 75-27-41.0 1
Bromoform ND ug/L 10/09/18 17:53 75-25-21.0 1
Bromomethane ND ug/L 10/09/18 17:53 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/09/18 17:53 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/09/18 17:53 56-23-51.0 1
Chlorobenzene ND ug/L 10/09/18 17:53 108-90-71.0 1
Chloroethane ND ug/L 10/09/18 17:53 75-00-31.0 1
Chloroform ND ug/L 10/09/18 17:53 67-66-31.0 1
Chloromethane ND ug/L 10/09/18 17:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/09/18 17:53 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/09/18 17:53 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/09/18 17:53 96-12-82.0 1
Dibromochloromethane ND ug/L 10/09/18 17:53 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/09/18 17:53 106-93-41.0 1
Dibromomethane ND ug/L 10/09/18 17:53 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/09/18 17:53 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/09/18 17:53 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/09/18 17:53 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/09/18 17:53 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/09/18 17:53 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/09/18 17:53 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/09/18 17:53 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/09/18 17:53 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/09/18 17:53 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/09/18 17:53 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/09/18 17:53 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/09/18 17:53 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/09/18 17:53 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/09/18 17:53 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/09/18 17:53 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/09/18 17:53 108-20-31.0 1
Ethylbenzene ND ug/L 10/09/18 17:53 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/09/18 17:53 87-68-31.0 1
2-Hexanone ND ug/L 10/09/18 17:53 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/09/18 17:53 99-87-61.0 1
Methylene Chloride ND ug/L 10/09/18 17:53 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/09/18 17:53 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/09/18 17:53 1634-04-41.0 1
Naphthalene ND ug/L 10/09/18 17:53 91-20-31.0 1
Styrene ND ug/L 10/09/18 17:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/09/18 17:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/09/18 17:53 79-34-51.0 1
Tetrachloroethene ND ug/L 10/09/18 17:53 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-17DD Lab ID:92402488017 Collected:10/04/18 12:05 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/09/18 17:53 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/09/18 17:53 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/09/18 17:53 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/09/18 17:53 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/09/18 17:53 79-00-51.0 1
Trichloroethene ND ug/L 10/09/18 17:53 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/09/18 17:53 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/09/18 17:53 96-18-41.0 1
Vinyl acetate ND ug/L 10/09/18 17:53 108-05-42.0 1
Vinyl chloride ND ug/L 10/09/18 17:53 75-01-41.0 1
Xylene (Total)ND ug/L 10/09/18 17:53 1330-20-71.0 1
m&p-Xylene ND ug/L 10/09/18 17:53 179601-23-12.0 1
o-Xylene ND ug/L 10/09/18 17:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)95 %10/09/18 17:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %10/09/18 17:53 17060-07-070-130 1
Toluene-d8 (S)108 %10/09/18 17:53 2037-26-570-130 1
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)ND ug/L 10/15/18 17:50 123-91-12.0 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %10/15/18 17:50 17060-07-050-150 1
Toluene-d8 (S)108 %10/15/18 17:50 2037-26-550-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-18 Lab ID:92402488018 Collected:10/04/18 17:55 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 10/09/18 23:06 7440-38-210/09/18 11:3010.0 1
Barium 65.8 ug/L 10/09/18 23:06 7440-39-310/09/18 11:305.0 1
Cadmium ND ug/L 10/09/18 23:06 7440-43-910/09/18 11:301.0 1
Chromium ND ug/L 10/09/18 23:06 7440-47-310/09/18 11:305.0 1
Lead 5.8 ug/L 10/09/18 23:06 7439-92-110/09/18 11:305.0 1
Selenium ND ug/L 10/09/18 23:06 7782-49-210/09/18 11:3010.0 1
Silver ND ug/L 10/09/18 23:06 7440-22-410/09/18 11:305.0 1
Sodium 143000 ug/L 10/10/18 15:34 7440-23-510/09/18 11:30250005
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 10/10/18 13:03 7439-97-610/09/18 18:220.20 1
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/11/18 03:43 67-64-162.5 2.5
Benzene ND ug/L 10/11/18 03:43 71-43-22.5 2.5
Bromobenzene ND ug/L 10/11/18 03:43 108-86-12.5 2.5
Bromochloromethane ND ug/L 10/11/18 03:43 74-97-52.5 2.5
Bromodichloromethane ND ug/L 10/11/18 03:43 75-27-42.5 2.5
Bromoform ND ug/L 10/11/18 03:43 75-25-22.5 2.5
Bromomethane ND ug/L 10/11/18 03:43 74-83-95.0 2.5
2-Butanone (MEK)ND ug/L 10/11/18 03:43 78-93-312.5 2.5
Carbon tetrachloride ND ug/L 10/11/18 03:43 56-23-52.5 2.5
Chlorobenzene ND ug/L 10/11/18 03:43 108-90-72.5 2.5
Chloroethane ND ug/L 10/11/18 03:43 75-00-32.5 2.5
Chloroform 4.3 ug/L 10/11/18 03:43 67-66-32.5 2.5
Chloromethane ND ug/L 10/11/18 03:43 74-87-32.5 2.5
2-Chlorotoluene ND ug/L 10/11/18 03:43 95-49-82.5 2.5
4-Chlorotoluene ND ug/L 10/11/18 03:43 106-43-42.5 2.5
1,2-Dibromo-3-chloropropane ND ug/L 10/11/18 03:43 96-12-85.0 2.5
Dibromochloromethane ND ug/L 10/11/18 03:43 124-48-12.5 2.5
1,2-Dibromoethane (EDB)ND ug/L 10/11/18 03:43 106-93-42.5 2.5
Dibromomethane ND ug/L 10/11/18 03:43 74-95-32.5 2.5
1,2-Dichlorobenzene ND ug/L 10/11/18 03:43 95-50-12.5 2.5
1,3-Dichlorobenzene ND ug/L 10/11/18 03:43 541-73-12.5 2.5
1,4-Dichlorobenzene ND ug/L 10/11/18 03:43 106-46-72.5 2.5
Dichlorodifluoromethane ND ug/L 10/11/18 03:43 75-71-82.5 2.5
1,1-Dichloroethane 389 ug/L 10/11/18 03:43 75-34-32.5 2.5
1,2-Dichloroethane 69.1 ug/L 10/11/18 03:43 107-06-22.5 2.5
1,1-Dichloroethene 404 ug/L 10/11/18 03:43 75-35-42.5 2.5
cis-1,2-Dichloroethene 6.4 ug/L 10/11/18 03:43 156-59-22.5 2.5
trans-1,2-Dichloroethene ND ug/L 10/11/18 03:43 156-60-52.5 2.5
1,2-Dichloropropane ND ug/L 10/11/18 03:43 78-87-52.5 2.5
1,3-Dichloropropane ND ug/L 10/11/18 03:43 142-28-92.5 2.5
2,2-Dichloropropane ND ug/L 10/11/18 03:43 594-20-72.5 2.5
1,1-Dichloropropene ND ug/L 10/11/18 03:43 563-58-62.5 2.5
cis-1,3-Dichloropropene ND ug/L 10/11/18 03:43 10061-01-52.5 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-18 Lab ID:92402488018 Collected:10/04/18 17:55 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 10/11/18 03:43 10061-02-62.5 2.5
Diisopropyl ether ND ug/L 10/11/18 03:43 108-20-32.5 2.5
Ethylbenzene ND ug/L 10/11/18 03:43 100-41-42.5 2.5
Hexachloro-1,3-butadiene ND ug/L 10/11/18 03:43 87-68-32.5 2.5
2-Hexanone ND ug/L 10/11/18 03:43 591-78-612.5 2.5
p-Isopropyltoluene ND ug/L 10/11/18 03:43 99-87-62.5 2.5
Methylene Chloride 6.9 ug/L 10/11/18 03:43 75-09-2 C95.0 2.5
4-Methyl-2-pentanone (MIBK)ND ug/L 10/11/18 03:43 108-10-112.5 2.5
Methyl-tert-butyl ether ND ug/L 10/11/18 03:43 1634-04-42.5 2.5
Naphthalene ND ug/L 10/11/18 03:43 91-20-32.5 2.5
Styrene ND ug/L 10/11/18 03:43 100-42-52.5 2.5
1,1,1,2-Tetrachloroethane 26.5 ug/L 10/11/18 03:43 630-20-62.5 2.5
1,1,2,2-Tetrachloroethane ND ug/L 10/11/18 03:43 79-34-52.5 2.5
Tetrachloroethene ND ug/L 10/11/18 03:43 127-18-42.5 2.5
Toluene ND ug/L 10/11/18 03:43 108-88-32.5 2.5
1,2,3-Trichlorobenzene ND ug/L 10/11/18 03:43 87-61-62.5 2.5
1,2,4-Trichlorobenzene ND ug/L 10/11/18 03:43 120-82-12.5 2.5
1,1,1-Trichloroethane 6.6 ug/L 10/11/18 03:43 71-55-62.5 2.5
1,1,2-Trichloroethane 45.0 ug/L 10/11/18 03:43 79-00-52.5 2.5
Trichloroethene 3.2 ug/L 10/11/18 03:43 79-01-62.5 2.5
Trichlorofluoromethane ND ug/L 10/11/18 03:43 75-69-42.5 2.5
1,2,3-Trichloropropane ND ug/L 10/11/18 03:43 96-18-42.5 2.5
Vinyl acetate ND ug/L 10/11/18 03:43 108-05-45.0 2.5
Vinyl chloride ND ug/L 10/11/18 03:43 75-01-42.5 2.5
Xylene (Total)ND ug/L 10/11/18 03:43 1330-20-72.5 2.5
m&p-Xylene ND ug/L 10/11/18 03:43 179601-23-15.0 2.5
o-Xylene ND ug/L 10/11/18 03:43 95-47-62.5 2.5
Surrogates
4-Bromofluorobenzene (S)101 %10/11/18 03:43 460-00-470-130 2.5
1,2-Dichloroethane-d4 (S)104 %10/11/18 03:43 17060-07-070-130 2.5
Toluene-d8 (S)101 %10/11/18 03:43 2037-26-570-130 2.5
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)598 ug/L 10/15/18 18:10 123-91-140.0 20
Surrogates
1,2-Dichloroethane-d4 (S)110 %10/15/18 18:10 17060-07-050-150 20
Toluene-d8 (S)119 %10/15/18 18:10 2037-26-550-150 20
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 164 mg/L 10/10/18 02:06 16887-00-67.0 7
Sulfate 93.1 mg/L 10/10/18 12:41 14808-79-81.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
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Page 40 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-19 Lab ID:92402488019 Collected:10/04/18 16:35 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 10/09/18 23:09 7440-38-210/09/18 11:3010.0 1
Barium 32.3 ug/L 10/09/18 23:09 7440-39-310/09/18 11:305.0 1
Cadmium ND ug/L 10/09/18 23:09 7440-43-910/09/18 11:301.0 1
Chromium 20.8 ug/L 10/09/18 23:09 7440-47-310/09/18 11:305.0 1
Lead 8.0 ug/L 10/09/18 23:09 7439-92-110/09/18 11:305.0 1
Selenium ND ug/L 10/09/18 23:09 7782-49-210/09/18 11:3010.0 1
Silver ND ug/L 10/09/18 23:09 7440-22-410/09/18 11:305.0 1
Sodium 98200 ug/L 10/10/18 15:37 7440-23-510/09/18 11:30250005
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 10/10/18 13:05 7439-97-610/09/18 18:220.20 1
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/11/18 03:27 67-64-150.0 2
Benzene ND ug/L 10/11/18 03:27 71-43-22.0 2
Bromobenzene ND ug/L 10/11/18 03:27 108-86-12.0 2
Bromochloromethane ND ug/L 10/11/18 03:27 74-97-52.0 2
Bromodichloromethane ND ug/L 10/11/18 03:27 75-27-42.0 2
Bromoform ND ug/L 10/11/18 03:27 75-25-22.0 2
Bromomethane ND ug/L 10/11/18 03:27 74-83-94.0 2
2-Butanone (MEK)ND ug/L 10/11/18 03:27 78-93-310.0 2
Carbon tetrachloride ND ug/L 10/11/18 03:27 56-23-52.0 2
Chlorobenzene ND ug/L 10/11/18 03:27 108-90-72.0 2
Chloroethane ND ug/L 10/11/18 03:27 75-00-32.0 2
Chloroform ND ug/L 10/11/18 03:27 67-66-32.0 2
Chloromethane ND ug/L 10/11/18 03:27 74-87-32.0 2
2-Chlorotoluene ND ug/L 10/11/18 03:27 95-49-82.0 2
4-Chlorotoluene ND ug/L 10/11/18 03:27 106-43-42.0 2
1,2-Dibromo-3-chloropropane ND ug/L 10/11/18 03:27 96-12-84.0 2
Dibromochloromethane ND ug/L 10/11/18 03:27 124-48-12.0 2
1,2-Dibromoethane (EDB)ND ug/L 10/11/18 03:27 106-93-42.0 2
Dibromomethane ND ug/L 10/11/18 03:27 74-95-32.0 2
1,2-Dichlorobenzene ND ug/L 10/11/18 03:27 95-50-12.0 2
1,3-Dichlorobenzene ND ug/L 10/11/18 03:27 541-73-12.0 2
1,4-Dichlorobenzene ND ug/L 10/11/18 03:27 106-46-72.0 2
Dichlorodifluoromethane ND ug/L 10/11/18 03:27 75-71-82.0 2
1,1-Dichloroethane 147 ug/L 10/11/18 03:27 75-34-32.0 2
1,2-Dichloroethane 27.3 ug/L 10/11/18 03:27 107-06-22.0 2
1,1-Dichloroethene 349 ug/L 10/11/18 03:27 75-35-42.0 2
cis-1,2-Dichloroethene 3.0 ug/L 10/11/18 03:27 156-59-22.0 2
trans-1,2-Dichloroethene ND ug/L 10/11/18 03:27 156-60-52.0 2
1,2-Dichloropropane ND ug/L 10/11/18 03:27 78-87-52.0 2
1,3-Dichloropropane ND ug/L 10/11/18 03:27 142-28-92.0 2
2,2-Dichloropropane ND ug/L 10/11/18 03:27 594-20-72.0 2
1,1-Dichloropropene ND ug/L 10/11/18 03:27 563-58-62.0 2
cis-1,3-Dichloropropene ND ug/L 10/11/18 03:27 10061-01-52.0 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:MW-19 Lab ID:92402488019 Collected:10/04/18 16:35 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
trans-1,3-Dichloropropene ND ug/L 10/11/18 03:27 10061-02-62.0 2
Diisopropyl ether ND ug/L 10/11/18 03:27 108-20-32.0 2
Ethylbenzene ND ug/L 10/11/18 03:27 100-41-42.0 2
Hexachloro-1,3-butadiene ND ug/L 10/11/18 03:27 87-68-32.0 2
2-Hexanone ND ug/L 10/11/18 03:27 591-78-610.0 2
p-Isopropyltoluene ND ug/L 10/11/18 03:27 99-87-62.0 2
Methylene Chloride ND ug/L 10/11/18 03:27 75-09-24.0 2
4-Methyl-2-pentanone (MIBK)ND ug/L 10/11/18 03:27 108-10-110.0 2
Methyl-tert-butyl ether ND ug/L 10/11/18 03:27 1634-04-42.0 2
Naphthalene ND ug/L 10/11/18 03:27 91-20-32.0 2
Styrene ND ug/L 10/11/18 03:27 100-42-52.0 2
1,1,1,2-Tetrachloroethane 4.4 ug/L 10/11/18 03:27 630-20-62.0 2
1,1,2,2-Tetrachloroethane ND ug/L 10/11/18 03:27 79-34-52.0 2
Tetrachloroethene ND ug/L 10/11/18 03:27 127-18-42.0 2
Toluene ND ug/L 10/11/18 03:27 108-88-32.0 2
1,2,3-Trichlorobenzene ND ug/L 10/11/18 03:27 87-61-62.0 2
1,2,4-Trichlorobenzene ND ug/L 10/11/18 03:27 120-82-12.0 2
1,1,1-Trichloroethane 22.9 ug/L 10/11/18 03:27 71-55-62.0 2
1,1,2-Trichloroethane 19.0 ug/L 10/11/18 03:27 79-00-52.0 2
Trichloroethene ND ug/L 10/11/18 03:27 79-01-62.0 2
Trichlorofluoromethane ND ug/L 10/11/18 03:27 75-69-42.0 2
1,2,3-Trichloropropane ND ug/L 10/11/18 03:27 96-18-42.0 2
Vinyl acetate ND ug/L 10/11/18 03:27 108-05-44.0 2
Vinyl chloride ND ug/L 10/11/18 03:27 75-01-42.0 2
Xylene (Total)ND ug/L 10/11/18 03:27 1330-20-72.0 2
m&p-Xylene ND ug/L 10/11/18 03:27 179601-23-14.0 2
o-Xylene ND ug/L 10/11/18 03:27 95-47-62.0 2
Surrogates
4-Bromofluorobenzene (S)96 %10/11/18 03:27 460-00-470-130 2
1,2-Dichloroethane-d4 (S)104 %10/11/18 03:27 17060-07-070-130 2
Toluene-d8 (S)100 %10/11/18 03:27 2037-26-570-130 2
Analytical Method: EPA 8260B Mod.8260 MSV SIM
1,4-Dioxane (p-Dioxane)206 ug/L 10/15/18 18:29 123-91-110.0 5
Surrogates
1,2-Dichloroethane-d4 (S)107 %10/15/18 18:29 17060-07-050-150 5
Toluene-d8 (S)116 %10/15/18 18:29 2037-26-550-150 5
Analytical Method: EPA 300.0 Rev 2.1 1993300.0 IC Anions 28 Days
Chloride 96.4 mg/L 10/10/18 12:58 16887-00-61.0 1
Sulfate 148 mg/L 10/10/18 02:23 14808-79-84.0 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:TRIP BLANK Lab ID:92402488020 Collected:10/04/18 00:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Acetone ND ug/L 10/10/18 00:13 67-64-125.0 1
Benzene ND ug/L 10/10/18 00:13 71-43-21.0 1
Bromobenzene ND ug/L 10/10/18 00:13 108-86-11.0 1
Bromochloromethane ND ug/L 10/10/18 00:13 74-97-51.0 1
Bromodichloromethane ND ug/L 10/10/18 00:13 75-27-41.0 1
Bromoform ND ug/L 10/10/18 00:13 75-25-21.0 1
Bromomethane ND ug/L 10/10/18 00:13 74-83-92.0 1
2-Butanone (MEK)ND ug/L 10/10/18 00:13 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/10/18 00:13 56-23-51.0 1
Chlorobenzene ND ug/L 10/10/18 00:13 108-90-71.0 1
Chloroethane ND ug/L 10/10/18 00:13 75-00-31.0 1
Chloroform ND ug/L 10/10/18 00:13 67-66-31.0 1
Chloromethane ND ug/L 10/10/18 00:13 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/10/18 00:13 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/10/18 00:13 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/10/18 00:13 96-12-82.0 1
Dibromochloromethane ND ug/L 10/10/18 00:13 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/10/18 00:13 106-93-41.0 1
Dibromomethane ND ug/L 10/10/18 00:13 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/10/18 00:13 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/10/18 00:13 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/10/18 00:13 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/10/18 00:13 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/10/18 00:13 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/10/18 00:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/10/18 00:13 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/10/18 00:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/10/18 00:13 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/10/18 00:13 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/10/18 00:13 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/10/18 00:13 594-20-71.0 1
1,1-Dichloropropene ND ug/L 10/10/18 00:13 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/10/18 00:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/10/18 00:13 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/10/18 00:13 108-20-31.0 1
Ethylbenzene ND ug/L 10/10/18 00:13 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/10/18 00:13 87-68-31.0 1
2-Hexanone ND ug/L 10/10/18 00:13 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/10/18 00:13 99-87-61.0 1
Methylene Chloride ND ug/L 10/10/18 00:13 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/10/18 00:13 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/10/18 00:13 1634-04-41.0 1
Naphthalene ND ug/L 10/10/18 00:13 91-20-31.0 1
Styrene ND ug/L 10/10/18 00:13 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/10/18 00:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/10/18 00:13 79-34-51.0 1
Tetrachloroethene ND ug/L 10/10/18 00:13 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 77
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92402488
FUL.006
Sample:TRIP BLANK Lab ID:92402488020 Collected:10/04/18 00:00 Received:10/08/18 09:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260B8260 MSV Low Level
Toluene ND ug/L 10/10/18 00:13 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/10/18 00:13 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/10/18 00:13 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/10/18 00:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/10/18 00:13 79-00-51.0 1
Trichloroethene ND ug/L 10/10/18 00:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/10/18 00:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/10/18 00:13 96-18-41.0 1
Vinyl acetate ND ug/L 10/10/18 00:13 108-05-42.0 1
Vinyl chloride ND ug/L 10/10/18 00:13 75-01-41.0 1
Xylene (Total)ND ug/L 10/10/18 00:13 1330-20-71.0 1
m&p-Xylene ND ug/L 10/10/18 00:13 179601-23-12.0 1
o-Xylene ND ug/L 10/10/18 00:13 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)106 %10/10/18 00:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)81 %10/10/18 00:13 17060-07-070-130 1
Toluene-d8 (S)112 %10/10/18 00:13 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435216
EPA 7470A
EPA 7470A
7470 Mercury
Associated Lab Samples:92402488008, 92402488009, 92402488010, 92402488011, 92402488018, 92402488019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2395830
Associated Lab Samples:92402488008, 92402488009, 92402488010, 92402488011, 92402488018, 92402488019
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 10/10/18 12:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2395831LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.72.5 107 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2395832MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402404001
2395833
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 103 75-12597 62.5ND 2.6 2.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 45 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435090
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples:92402488008, 92402488009, 92402488010, 92402488011, 92402488018, 92402488019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2395188
Associated Lab Samples:92402488008, 92402488009, 92402488010, 92402488011, 92402488018, 92402488019
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 10/09/18 22:31
Barium ug/L ND 5.0 10/09/18 22:31
Cadmium ug/L ND 1.0 10/09/18 22:31
Chromium ug/L ND 5.0 10/09/18 22:31
Lead ug/L ND 5.0 10/09/18 22:31
Selenium ug/L ND 10.0 10/09/18 22:31
Silver ug/L ND 5.0 10/09/18 22:31
Sodium ug/L ND 5000 10/09/18 22:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2395189LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 460500 92 80-120
Barium ug/L 490500 98 80-120
Cadmium ug/L 474500 95 80-120
Chromium ug/L 474500 95 80-120
Lead ug/L 460500 92 80-120
Selenium ug/L 470500 94 80-120
Silver ug/L 244250 97 80-120
Sodium ug/L 51005000 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2395190MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402488008
2395191
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L M65006375-12560 2500343658644
Barium ug/L 500 77 75-12575 2500ND390383
Cadmium ug/L 500 79 75-12578 2500ND395388
Chromium ug/L M65007575-12573 2500ND391383
Lead ug/L M65007175-12572 1500ND413419
Selenium ug/L 500 79 75-12576 4500ND397381
Silver ug/L M62507175-12569 2250ND177173
Sodium ug/L M65000-2370 75-125-2540 15000121000
0 1090000 1080000
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435194
EPA 8260B
EPA 8260B
8260 MSV Low Level
Associated Lab Samples:92402488001, 92402488002, 92402488003, 92402488004, 92402488005, 92402488006, 92402488007,
92402488009, 92402488011, 92402488012, 92402488013, 92402488014, 92402488015, 92402488016,
92402488017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2395705
Associated Lab Samples:92402488001, 92402488002, 92402488003, 92402488004, 92402488005, 92402488006, 92402488007,
92402488009, 92402488011, 92402488012, 92402488013, 92402488014, 92402488015, 92402488016,
92402488017
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/09/18 13:57
1,1,1-Trichloroethane ug/L ND 1.0 10/09/18 13:57
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/09/18 13:57
1,1,2-Trichloroethane ug/L ND 1.0 10/09/18 13:57
1,1-Dichloroethane ug/L ND 1.0 10/09/18 13:57
1,1-Dichloroethene ug/L ND 1.0 10/09/18 13:57
1,1-Dichloropropene ug/L ND 1.0 10/09/18 13:57
1,2,3-Trichlorobenzene ug/L ND 1.0 10/09/18 13:57
1,2,3-Trichloropropane ug/L ND 1.0 10/09/18 13:57
1,2,4-Trichlorobenzene ug/L ND 1.0 10/09/18 13:57
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/09/18 13:57
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/09/18 13:57
1,2-Dichlorobenzene ug/L ND 1.0 10/09/18 13:57
1,2-Dichloroethane ug/L ND 1.0 10/09/18 13:57
1,2-Dichloropropane ug/L ND 1.0 10/09/18 13:57
1,3-Dichlorobenzene ug/L ND 1.0 10/09/18 13:57
1,3-Dichloropropane ug/L ND 1.0 10/09/18 13:57
1,4-Dichlorobenzene ug/L ND 1.0 10/09/18 13:57
2,2-Dichloropropane ug/L ND 1.0 10/09/18 13:57
2-Butanone (MEK)ug/L ND 5.0 10/09/18 13:57
2-Chlorotoluene ug/L ND 1.0 10/09/18 13:57
2-Hexanone ug/L ND 5.0 10/09/18 13:57
4-Chlorotoluene ug/L ND 1.0 10/09/18 13:57
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/09/18 13:57
Acetone ug/L ND 25.0 10/09/18 13:57
Benzene ug/L ND 1.0 10/09/18 13:57
Bromobenzene ug/L ND 1.0 10/09/18 13:57
Bromochloromethane ug/L ND 1.0 10/09/18 13:57
Bromodichloromethane ug/L ND 1.0 10/09/18 13:57
Bromoform ug/L ND 1.0 10/09/18 13:57
Bromomethane ug/L ND 2.0 10/09/18 13:57
Carbon tetrachloride ug/L ND 1.0 10/09/18 13:57
Chlorobenzene ug/L ND 1.0 10/09/18 13:57
Chloroethane ug/L ND 1.0 10/09/18 13:57
Chloroform ug/L ND 1.0 10/09/18 13:57
Chloromethane ug/L ND 1.0 10/09/18 13:57
cis-1,2-Dichloroethene ug/L ND 1.0 10/09/18 13:57
cis-1,3-Dichloropropene ug/L ND 1.0 10/09/18 13:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2395705
Associated Lab Samples:92402488001, 92402488002, 92402488003, 92402488004, 92402488005, 92402488006, 92402488007,
92402488009, 92402488011, 92402488012, 92402488013, 92402488014, 92402488015, 92402488016,
92402488017
Matrix:Water
Analyzed
Dibromochloromethane ug/L ND 1.0 10/09/18 13:57
Dibromomethane ug/L ND 1.0 10/09/18 13:57
Dichlorodifluoromethane ug/L ND 1.0 10/09/18 13:57
Diisopropyl ether ug/L ND 1.0 10/09/18 13:57
Ethylbenzene ug/L ND 1.0 10/09/18 13:57
Hexachloro-1,3-butadiene ug/L ND 1.0 10/09/18 13:57
m&p-Xylene ug/L ND 2.0 10/09/18 13:57
Methyl-tert-butyl ether ug/L ND 1.0 10/09/18 13:57
Methylene Chloride ug/L ND 2.0 10/09/18 13:57
Naphthalene ug/L ND 1.0 10/09/18 13:57
o-Xylene ug/L ND 1.0 10/09/18 13:57
p-Isopropyltoluene ug/L ND 1.0 10/09/18 13:57
Styrene ug/L ND 1.0 10/09/18 13:57
Tetrachloroethene ug/L ND 1.0 10/09/18 13:57
Toluene ug/L ND 1.0 10/09/18 13:57
trans-1,2-Dichloroethene ug/L ND 1.0 10/09/18 13:57
trans-1,3-Dichloropropene ug/L ND 1.0 10/09/18 13:57
Trichloroethene ug/L ND 1.0 10/09/18 13:57
Trichlorofluoromethane ug/L ND 1.0 10/09/18 13:57
Vinyl acetate ug/L ND 2.0 10/09/18 13:57
Vinyl chloride ug/L ND 1.0 10/09/18 13:57
Xylene (Total)ug/L ND 1.0 10/09/18 13:57
1,2-Dichloroethane-d4 (S)%101 70-130 10/09/18 13:57
4-Bromofluorobenzene (S)%99 70-130 10/09/18 13:57
Toluene-d8 (S)%106 70-130 10/09/18 13:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2395706LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.050 98 80-125
1,1,1-Trichloroethane ug/L 46.150 92 71-129
1,1,2,2-Tetrachloroethane ug/L 49.350 99 79-124
1,1,2-Trichloroethane ug/L 48.850 98 85-125
1,1-Dichloroethane ug/L 48.650 97 73-126
1,1-Dichloroethene ug/L 47.050 94 66-135
1,1-Dichloropropene ug/L 45.950 92 74-135
1,2,3-Trichlorobenzene ug/L 56.150 112 73-135
1,2,3-Trichloropropane ug/L 54.050 108 75-130
1,2,4-Trichlorobenzene ug/L 51.850 104 75-134
1,2-Dibromo-3-chloropropane ug/L 50.950 102 71-133
1,2-Dibromoethane (EDB)ug/L 49.850 100 83-124
1,2-Dichlorobenzene ug/L 53.450 107 80-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2395706LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane ug/L 46.750 93 67-128
1,2-Dichloropropane ug/L 52.650 105 75-132
1,3-Dichlorobenzene ug/L 53.450 107 77-130
1,3-Dichloropropane ug/L 50.750 101 76-131
1,4-Dichlorobenzene ug/L 53.450 107 78-130
2,2-Dichloropropane ug/L 45.750 91 40-160
2-Butanone (MEK)ug/L 101100 101 61-144
2-Chlorotoluene ug/L 48.050 96 74-132
2-Hexanone ug/L 107100 107 68-143
4-Chlorotoluene ug/L 52.750 105 76-133
4-Methyl-2-pentanone (MIBK)ug/L 97.6100 98 72-135
Acetone ug/L 99.6100 100 48-146
Benzene ug/L 51.850 104 80-125
Bromobenzene ug/L 51.850 104 75-125
Bromochloromethane ug/L 49.250 98 71-125
Bromodichloromethane ug/L 51.950 104 78-124
Bromoform ug/L 45.350 91 71-128
Bromomethane ug/L 44.850 90 40-160
Carbon tetrachloride ug/L 46.750 93 69-131
Chlorobenzene ug/L 52.950 106 81-122
Chloroethane ug/L 43.250 86 39-148
Chloroform ug/L 45.850 92 73-127
Chloromethane ug/L 43.950 88 44-146
cis-1,2-Dichloroethene ug/L 48.650 97 74-124
cis-1,3-Dichloropropene ug/L 48.050 96 72-132
Dibromochloromethane ug/L 48.950 98 78-125
Dibromomethane ug/L 53.950 108 82-120
Dichlorodifluoromethane ug/L 53.150 106 34-157
Diisopropyl ether ug/L 44.150 88 69-135
Ethylbenzene ug/L 52.450 105 79-121
Hexachloro-1,3-butadiene ug/L 52.950 106 72-131
m&p-Xylene ug/L 110100 110 81-124
Methyl-tert-butyl ether ug/L 46.850 94 74-131
Methylene Chloride ug/L 44.050 88 64-133
Naphthalene ug/L 48.750 97 73-133
o-Xylene ug/L 56.650 113 79-131
p-Isopropyltoluene ug/L 47.950 96 80-131
Styrene ug/L 49.750 99 84-126
Tetrachloroethene ug/L 49.650 99 78-122
Toluene ug/L 48.450 97 80-121
trans-1,2-Dichloroethene ug/L 48.150 96 71-127
trans-1,3-Dichloropropene ug/L 47.950 96 69-141
Trichloroethene ug/L 49.350 99 78-122
Trichlorofluoromethane ug/L 40.050 80 53-137
Vinyl acetate ug/L 101100 101 40-160
Vinyl chloride ug/L 53.450 107 58-137
Xylene (Total)ug/L 167150 111 81-126
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2395706LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloroethane-d4 (S)%86 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%95 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2395707MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402132011
2395708
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L M11006870-13079 16100ND67.5 79.4
1,1,1-Trichloroethane ug/L 100 75 70-13087 15100ND75.1 87.5
1,1,2,2-Tetrachloroethane ug/L 100 70 70-13081 14100ND69.8 80.7
1,1,2-Trichloroethane ug/L 100 73 70-13083 13100ND72.5 82.7
1,1-Dichloroethane ug/L 100 71 70-13082 15100ND71.1 82.3
1,1-Dichloroethene ug/L 100 73 70-16696 27100ND73.1 95.5
1,1-Dichloropropene ug/L 100 73 70-13087 18100ND72.9 86.9
1,2,3-Trichlorobenzene ug/L 100 79 70-13090 13100ND78.6 89.8
1,2,3-Trichloropropane ug/L M11006870-13078 13100ND68.4 77.5
1,2,4-Trichlorobenzene ug/L 100 80 70-13091 12100ND80.3 90.8
1,2-Dibromo-3-chloropropane ug/L 100 70 70-13079 12100ND70.2 79.2
1,2-Dibromoethane (EDB)ug/L M11006670-13080 18100ND66.3 79.6
1,2-Dichlorobenzene ug/L 100 72 70-13085 16100ND72.1 84.8
1,2-Dichloroethane ug/L 100 70 70-13086 21100ND69.7 85.9
1,2-Dichloropropane ug/L 100 73 70-13086 16100ND72.9 85.8
1,3-Dichlorobenzene ug/L 100 72 70-13086 17100ND72.3 85.7
1,3-Dichloropropane ug/L M11006970-13083 18100ND69.0 83.0
1,4-Dichlorobenzene ug/L 100 72 70-13086 17100ND72.3 85.7
2,2-Dichloropropane ug/L M11006970-13081 16100ND68.7 81.0
2-Butanone (MEK)ug/L 200 79 70-13097 21200ND157194
2-Chlorotoluene ug/L 100 76 70-13086 13100ND75.8 86.5
2-Hexanone ug/L 200 74 70-13081 10200ND147162
4-Chlorotoluene ug/L 100 73 70-13086 17100ND73.1 86.3
4-Methyl-2-pentanone (MIBK)ug/L 200 75 70-13082 9200ND150163
Acetone ug/L 200 77 70-13092 17200ND154184
Benzene ug/L 100 75 70-14888 17100ND74.5 88.4
Bromobenzene ug/L 100 70 70-13085 18100ND70.2 84.5
Bromochloromethane ug/L M11006570-13079 20100ND64.6 78.6
Bromodichloromethane ug/L 100 70 70-13082 16100ND70.0 82.0
Bromoform ug/L M11006470-13073 14100ND63.6 73.3
Bromomethane ug/L 100 75 70-13083 10100ND75.4 83.1
Carbon tetrachloride ug/L 100 78 70-13088 13100ND77.7 88.4
Chlorobenzene ug/L 100 71 70-14683 16100ND70.7 83.1
Chloroethane ug/L 100 70 70-13089 23100ND70.1 88.5
Chloroform ug/L M11006970-13081 17100ND68.9 81.4
Chloromethane ug/L 100 72 70-13090 23100ND71.7 90.4
cis-1,2-Dichloroethene ug/L M11004370-13075 5100582625657
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2395707MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402132011
2395708
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
cis-1,3-Dichloropropene ug/L M11006870-13079 15100ND68.1 79.2
Dibromochloromethane ug/L M11006770-13079 16100ND67.1 78.9
Dibromomethane ug/L 100 74 70-13087 16100ND74.4 87.4
Dichlorodifluoromethane ug/L 100 79 70-13098 21100ND79.3 97.9
Diisopropyl ether ug/L M11006970-13081 15100ND69.3 80.7
Ethylbenzene ug/L 100 71 70-13084 17100ND71.2 84.5
Hexachloro-1,3-butadiene ug/L 100 90 70-13095 5100ND90.3 94.9
m&p-Xylene ug/L 200 72 70-13086 17200ND144172
Methyl-tert-butyl ether ug/L M11006370-13077 19100ND63.2 76.7
Methylene Chloride ug/L 100 75 70-13089 18100ND74.8 89.5
Naphthalene ug/L M11006970-13080 14100ND69.2 79.8
o-Xylene ug/L 100 71 70-13085 18100ND71.1 85.0
p-Isopropyltoluene ug/L 100 78 70-13088 11100ND78.4 87.7
Styrene ug/L M11006970-13082 18100ND69.0 82.3
Tetrachloroethene ug/L M11005070-13071 5100359409430
Toluene ug/L 100 70 70-15581 15100ND70.2 81.4
trans-1,2-Dichloroethene ug/L M11006870-13086 211008.8 76.7 94.8
trans-1,3-Dichloropropene ug/L 100 70 70-13081 14100ND69.9 80.8
Trichloroethene ug/L 100 74 69-15179 2100164239244
Trichlorofluoromethane ug/L 100 70 70-13084 18100ND69.9 83.9
Vinyl acetate ug/L 200 74 70-13087 16200ND149174
Vinyl chloride ug/L 100 78 70-13099 1910022.2 101 121
Xylene (Total)ug/L 300 72 70-13086 18300ND216257
1,2-Dichloroethane-d4 (S)%96 70-13097
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%100 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435301
EPA 8260B
EPA 8260B
8260 MSV Low Level
Associated Lab Samples:92402488008, 92402488020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2396195
Associated Lab Samples:92402488008, 92402488020
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/09/18 23:56
1,1,1-Trichloroethane ug/L ND 1.0 10/09/18 23:56
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/09/18 23:56
1,1,2-Trichloroethane ug/L ND 1.0 10/09/18 23:56
1,1-Dichloroethane ug/L ND 1.0 10/09/18 23:56
1,1-Dichloroethene ug/L ND 1.0 10/09/18 23:56
1,1-Dichloropropene ug/L ND 1.0 10/09/18 23:56
1,2,3-Trichlorobenzene ug/L ND 1.0 10/09/18 23:56
1,2,3-Trichloropropane ug/L ND 1.0 10/09/18 23:56
1,2,4-Trichlorobenzene ug/L ND 1.0 10/09/18 23:56
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/09/18 23:56
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/09/18 23:56
1,2-Dichlorobenzene ug/L ND 1.0 10/09/18 23:56
1,2-Dichloroethane ug/L ND 1.0 10/09/18 23:56
1,2-Dichloropropane ug/L ND 1.0 10/09/18 23:56
1,3-Dichlorobenzene ug/L ND 1.0 10/09/18 23:56
1,3-Dichloropropane ug/L ND 1.0 10/09/18 23:56
1,4-Dichlorobenzene ug/L ND 1.0 10/09/18 23:56
2,2-Dichloropropane ug/L ND 1.0 10/09/18 23:56
2-Butanone (MEK)ug/L ND 5.0 10/09/18 23:56
2-Chlorotoluene ug/L ND 1.0 10/09/18 23:56
2-Hexanone ug/L ND 5.0 10/09/18 23:56
4-Chlorotoluene ug/L ND 1.0 10/09/18 23:56
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/09/18 23:56
Acetone ug/L ND 25.0 10/09/18 23:56
Benzene ug/L ND 1.0 10/09/18 23:56
Bromobenzene ug/L ND 1.0 10/09/18 23:56
Bromochloromethane ug/L ND 1.0 10/09/18 23:56
Bromodichloromethane ug/L ND 1.0 10/09/18 23:56
Bromoform ug/L ND 1.0 10/09/18 23:56
Bromomethane ug/L ND 2.0 10/09/18 23:56
Carbon tetrachloride ug/L ND 1.0 10/09/18 23:56
Chlorobenzene ug/L ND 1.0 10/09/18 23:56
Chloroethane ug/L ND 1.0 10/09/18 23:56
Chloroform ug/L ND 1.0 10/09/18 23:56
Chloromethane ug/L ND 1.0 10/09/18 23:56
cis-1,2-Dichloroethene ug/L ND 1.0 10/09/18 23:56
cis-1,3-Dichloropropene ug/L ND 1.0 10/09/18 23:56
Dibromochloromethane ug/L ND 1.0 10/09/18 23:56
Dibromomethane ug/L ND 1.0 10/09/18 23:56
Dichlorodifluoromethane ug/L ND 1.0 10/09/18 23:56
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2396195
Associated Lab Samples:92402488008, 92402488020
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 10/09/18 23:56
Ethylbenzene ug/L ND 1.0 10/09/18 23:56
Hexachloro-1,3-butadiene ug/L ND 1.0 10/09/18 23:56
m&p-Xylene ug/L ND 2.0 10/09/18 23:56
Methyl-tert-butyl ether ug/L ND 1.0 10/09/18 23:56
Methylene Chloride ug/L ND 2.0 10/09/18 23:56
Naphthalene ug/L ND 1.0 10/09/18 23:56
o-Xylene ug/L ND 1.0 10/09/18 23:56
p-Isopropyltoluene ug/L ND 1.0 10/09/18 23:56
Styrene ug/L ND 1.0 10/09/18 23:56
Tetrachloroethene ug/L ND 1.0 10/09/18 23:56
Toluene ug/L ND 1.0 10/09/18 23:56
trans-1,2-Dichloroethene ug/L ND 1.0 10/09/18 23:56
trans-1,3-Dichloropropene ug/L ND 1.0 10/09/18 23:56
Trichloroethene ug/L ND 1.0 10/09/18 23:56
Trichlorofluoromethane ug/L ND 1.0 10/09/18 23:56
Vinyl acetate ug/L ND 2.0 10/09/18 23:56
Vinyl chloride ug/L ND 1.0 10/09/18 23:56
Xylene (Total)ug/L ND 1.0 10/09/18 23:56
1,2-Dichloroethane-d4 (S)%84 70-130 10/09/18 23:56
4-Bromofluorobenzene (S)%105 70-130 10/09/18 23:56
Toluene-d8 (S)%106 70-130 10/09/18 23:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2396196LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.550 103 80-125
1,1,1-Trichloroethane ug/L 51.050 102 71-129
1,1,2,2-Tetrachloroethane ug/L 45.350 91 79-124
1,1,2-Trichloroethane ug/L 50.350 101 85-125
1,1-Dichloroethane ug/L 44.750 89 73-126
1,1-Dichloroethene ug/L 46.650 93 66-135
1,1-Dichloropropene ug/L 54.550 109 74-135
1,2,3-Trichlorobenzene ug/L 38.950 78 73-135
1,2,3-Trichloropropane ug/L 44.550 89 75-130
1,2,4-Trichlorobenzene ug/L 44.250 88 75-134
1,2-Dibromo-3-chloropropane ug/L 43.350 87 71-133
1,2-Dibromoethane (EDB)ug/L 53.050 106 83-124
1,2-Dichlorobenzene ug/L 46.150 92 80-133
1,2-Dichloroethane ug/L 48.550 97 67-128
1,2-Dichloropropane ug/L 50.750 101 75-132
1,3-Dichlorobenzene ug/L 46.350 93 77-130
1,3-Dichloropropane ug/L 54.650 109 76-131
1,4-Dichlorobenzene ug/L 45.950 92 78-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2396196LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 48.950 98 40-160
2-Butanone (MEK)ug/L 90.7100 91 61-144
2-Chlorotoluene ug/L 45.250 90 74-132
2-Hexanone ug/L 78.8100 79 68-143
4-Chlorotoluene ug/L 45.950 92 76-133
4-Methyl-2-pentanone (MIBK)ug/L 78.1100 78 72-135
Acetone ug/L 81.2100 81 48-146
Benzene ug/L 50.850 102 80-125
Bromobenzene ug/L 48.450 97 75-125
Bromochloromethane ug/L 49.050 98 71-125
Bromodichloromethane ug/L 46.650 93 78-124
Bromoform ug/L 40.750 81 71-128
Bromomethane ug/L 37.850 76 40-160
Carbon tetrachloride ug/L 47.550 95 69-131
Chlorobenzene ug/L 48.750 97 81-122
Chloroethane ug/L 41.250 82 39-148
Chloroform ug/L 50.050 100 73-127
Chloromethane ug/L 39.850 80 44-146
cis-1,2-Dichloroethene ug/L 46.950 94 74-124
cis-1,3-Dichloropropene ug/L 51.550 103 72-132
Dibromochloromethane ug/L 51.550 103 78-125
Dibromomethane ug/L 47.450 95 82-120
Dichlorodifluoromethane ug/L 52.450 105 34-157
Diisopropyl ether ug/L 45.450 91 69-135
Ethylbenzene ug/L 46.950 94 79-121
Hexachloro-1,3-butadiene ug/L 44.850 90 72-131
m&p-Xylene ug/L 92.1100 92 81-124
Methyl-tert-butyl ether ug/L 49.550 99 74-131
Methylene Chloride ug/L 43.450 87 64-133
Naphthalene ug/L 40.450 81 73-133
o-Xylene ug/L 47.450 95 79-131
p-Isopropyltoluene ug/L 43.750 87 80-131
Styrene ug/L 46.550 93 84-126
Tetrachloroethene ug/L 51.350 103 78-122
Toluene ug/L 44.750 89 80-121
trans-1,2-Dichloroethene ug/L 47.350 95 71-127
trans-1,3-Dichloropropene ug/L 49.250 98 69-141
Trichloroethene ug/L 54.150 108 78-122
Trichlorofluoromethane ug/L 46.350 93 53-137
Vinyl acetate ug/L 98.1100 98 40-160
Vinyl chloride ug/L 51.250 102 58-137
Xylene (Total)ug/L 139150 93 81-126
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%93 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2396197MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401424003
2396198
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 102 70-130100 2200ND205201
1,1,1-Trichloroethane ug/L 200 110 70-130107 3200ND221214
1,1,2,2-Tetrachloroethane ug/L 200 92 70-13093 1200ND183186
1,1,2-Trichloroethane ug/L 200 98 70-130101 2200ND197202
1,1-Dichloroethane ug/L 200 100 70-13098 3200ND201196
1,1-Dichloroethene ug/L 200 109 70-166106 3200ND218213
1,1-Dichloropropene ug/L 200 117 70-130111 6200ND234222
1,2,3-Trichlorobenzene ug/L 200 78 70-13085 9200ND156171
1,2,3-Trichloropropane ug/L 200 93 70-13090 3200ND186181
1,2,4-Trichlorobenzene ug/L 200 95 70-13093 2200ND190185
1,2-Dibromo-3-chloropropane ug/L 200 90 70-13087 3200ND179173
1,2-Dibromoethane (EDB)ug/L 200 102 70-130101 2200ND205201
1,2-Dichlorobenzene ug/L 200 102 70-13099 3200ND204198
1,2-Dichloroethane ug/L 200 100 70-13094 6200ND200189
1,2-Dichloropropane ug/L 200 108 70-130107 1200ND216214
1,3-Dichlorobenzene ug/L 200 104 70-130102 2200ND207204
1,3-Dichloropropane ug/L 200 105 70-130103 1200ND209206
1,4-Dichlorobenzene ug/L 200 101 70-130103 2200ND202206
2,2-Dichloropropane ug/L 200 105 70-130100 5200ND211201
2-Butanone (MEK)ug/L 400 83 70-13081 3400ND334323
2-Chlorotoluene ug/L 200 105 70-130101 3200ND209202
2-Hexanone ug/L 400 83 70-13083 0400ND333333
4-Chlorotoluene ug/L 200 105 70-130101 4200ND209202
4-Methyl-2-pentanone (MIBK)ug/L 400 84 70-13083 1400ND335331
Acetone ug/L 400 86 70-13089 3400ND344356
Benzene ug/L 200 110 70-148105 5200ND221211
Bromobenzene ug/L 200 105 70-130104 1200ND211208
Bromochloromethane ug/L 200 108 70-130104 3200ND216209
Bromodichloromethane ug/L 200 100 70-13096 4200ND200192
Bromoform ug/L 200 80 70-13081 0200ND161161
Bromomethane ug/L 200 81 70-13074 9200ND162148
Carbon tetrachloride ug/L 200 108 70-130107 1200ND216215
Chlorobenzene ug/L 200 104 70-146105 0200ND209210
Chloroethane ug/L 200 120 70-130106 13200ND241212
Chloroform ug/L 200 93 70-13094 1200ND186188
Chloromethane ug/L 200 87 70-13085 2200ND174170
cis-1,2-Dichloroethene ug/L M120011270-13066 8200100012201130
cis-1,3-Dichloropropene ug/L 200 104 70-130104 0200ND208209
Dibromochloromethane ug/L 200 98 70-13096 2200ND197193
Dibromomethane ug/L 200 101 70-130103 2200ND201206
Dichlorodifluoromethane ug/L 200 109 70-130103 6200ND219206
Diisopropyl ether ug/L 200 91 70-13086 6200ND182171
Ethylbenzene ug/L 200 103 70-130102 1200ND206205
Hexachloro-1,3-butadiene ug/L 200 99 70-13097 2200ND197193
m&p-Xylene ug/L 400 103 70-130102 1400ND412408
Methyl-tert-butyl ether ug/L 200 86 70-13084 2200ND172169
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2396197MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92401424003
2396198
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 200 90 70-13087 4200ND181174
Naphthalene ug/L 200 83 70-13088 6200ND166176
o-Xylene ug/L 200 106 70-130102 3200ND211204
p-Isopropyltoluene ug/L 200 99 70-13098 2200ND199195
Styrene ug/L 200 102 70-130101 0200ND203203
Tetrachloroethene ug/L 200 120 70-130109 220085511001070
Toluene ug/L 200 102 70-155103 2200ND203206
trans-1,2-Dichloroethene ug/L 200 109 70-130103 5200ND218207
trans-1,3-Dichloropropene ug/L 200 98 70-13098 1200ND196195
Trichloroethene ug/L 200 127 69-151121 420080.6 334 322
Trichlorofluoromethane ug/L 200 113 70-130109 3200ND225218
Vinyl acetate ug/L 400 86 70-13082 5400ND345329
Vinyl chloride ug/L 200 113 70-130110 220010.8 236 232
Xylene (Total)ug/L 600 104 70-130102 2600ND623612
1,2-Dichloroethane-d4 (S)%90 70-13086
4-Bromofluorobenzene (S)%101 70-13097
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435528
EPA 8260B
EPA 8260B
8260 MSV Low Level
Associated Lab Samples:92402488018, 92402488019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2397278
Associated Lab Samples:92402488018, 92402488019
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/11/18 01:18
1,1,1-Trichloroethane ug/L ND 1.0 10/11/18 01:18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/11/18 01:18
1,1,2-Trichloroethane ug/L ND 1.0 10/11/18 01:18
1,1-Dichloroethane ug/L ND 1.0 10/11/18 01:18
1,1-Dichloroethene ug/L ND 1.0 10/11/18 01:18
1,1-Dichloropropene ug/L ND 1.0 10/11/18 01:18
1,2,3-Trichlorobenzene ug/L ND 1.0 10/11/18 01:18
1,2,3-Trichloropropane ug/L ND 1.0 10/11/18 01:18
1,2,4-Trichlorobenzene ug/L ND 1.0 10/11/18 01:18
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/11/18 01:18
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/11/18 01:18
1,2-Dichlorobenzene ug/L ND 1.0 10/11/18 01:18
1,2-Dichloroethane ug/L ND 1.0 10/11/18 01:18
1,2-Dichloropropane ug/L ND 1.0 10/11/18 01:18
1,3-Dichlorobenzene ug/L ND 1.0 10/11/18 01:18
1,3-Dichloropropane ug/L ND 1.0 10/11/18 01:18
1,4-Dichlorobenzene ug/L ND 1.0 10/11/18 01:18
2,2-Dichloropropane ug/L ND 1.0 10/11/18 01:18
2-Butanone (MEK)ug/L ND 5.0 10/11/18 01:18
2-Chlorotoluene ug/L ND 1.0 10/11/18 01:18
2-Hexanone ug/L ND 5.0 10/11/18 01:18
4-Chlorotoluene ug/L ND 1.0 10/11/18 01:18
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/11/18 01:18
Acetone ug/L ND 25.0 10/11/18 01:18
Benzene ug/L ND 1.0 10/11/18 01:18
Bromobenzene ug/L ND 1.0 10/11/18 01:18
Bromochloromethane ug/L ND 1.0 10/11/18 01:18
Bromodichloromethane ug/L ND 1.0 10/11/18 01:18
Bromoform ug/L ND 1.0 10/11/18 01:18
Bromomethane ug/L ND 2.0 10/11/18 01:18
Carbon tetrachloride ug/L ND 1.0 10/11/18 01:18
Chlorobenzene ug/L ND 1.0 10/11/18 01:18
Chloroethane ug/L ND 1.0 10/11/18 01:18
Chloroform ug/L ND 1.0 10/11/18 01:18
Chloromethane ug/L ND 1.0 10/11/18 01:18
cis-1,2-Dichloroethene ug/L ND 1.0 10/11/18 01:18
cis-1,3-Dichloropropene ug/L ND 1.0 10/11/18 01:18
Dibromochloromethane ug/L ND 1.0 10/11/18 01:18
Dibromomethane ug/L ND 1.0 10/11/18 01:18
Dichlorodifluoromethane ug/L ND 1.0 10/11/18 01:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2397278
Associated Lab Samples:92402488018, 92402488019
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 10/11/18 01:18
Ethylbenzene ug/L ND 1.0 10/11/18 01:18
Hexachloro-1,3-butadiene ug/L ND 1.0 10/11/18 01:18
m&p-Xylene ug/L ND 2.0 10/11/18 01:18
Methyl-tert-butyl ether ug/L ND 1.0 10/11/18 01:18
Methylene Chloride ug/L ND 2.0 10/11/18 01:18
Naphthalene ug/L ND 1.0 10/11/18 01:18
o-Xylene ug/L ND 1.0 10/11/18 01:18
p-Isopropyltoluene ug/L ND 1.0 10/11/18 01:18
Styrene ug/L ND 1.0 10/11/18 01:18
Tetrachloroethene ug/L ND 1.0 10/11/18 01:18
Toluene ug/L ND 1.0 10/11/18 01:18
trans-1,2-Dichloroethene ug/L ND 1.0 10/11/18 01:18
trans-1,3-Dichloropropene ug/L ND 1.0 10/11/18 01:18
Trichloroethene ug/L ND 1.0 10/11/18 01:18
Trichlorofluoromethane ug/L ND 1.0 10/11/18 01:18
Vinyl acetate ug/L ND 2.0 10/11/18 01:18
Vinyl chloride ug/L ND 1.0 10/11/18 01:18
Xylene (Total)ug/L ND 1.0 10/11/18 01:18
1,2-Dichloroethane-d4 (S)%105 70-130 10/11/18 01:18
4-Bromofluorobenzene (S)%96 70-130 10/11/18 01:18
Toluene-d8 (S)%101 70-130 10/11/18 01:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397279LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.050 104 80-125
1,1,1-Trichloroethane ug/L 53.050 106 71-129
1,1,2,2-Tetrachloroethane ug/L 50.950 102 79-124
1,1,2-Trichloroethane ug/L 49.550 99 85-125
1,1-Dichloroethane ug/L 49.650 99 73-126
1,1-Dichloroethene ug/L 57.450 115 66-135
1,1-Dichloropropene ug/L 53.550 107 74-135
1,2,3-Trichlorobenzene ug/L 47.350 95 73-135
1,2,3-Trichloropropane ug/L 51.550 103 75-130
1,2,4-Trichlorobenzene ug/L 49.450 99 75-134
1,2-Dibromo-3-chloropropane ug/L 51.150 102 71-133
1,2-Dibromoethane (EDB)ug/L 51.450 103 83-124
1,2-Dichlorobenzene ug/L 49.750 99 80-133
1,2-Dichloroethane ug/L 51.550 103 67-128
1,2-Dichloropropane ug/L 51.350 103 75-132
1,3-Dichlorobenzene ug/L 49.450 99 77-130
1,3-Dichloropropane ug/L 52.650 105 76-131
1,4-Dichlorobenzene ug/L 48.850 98 78-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2397279LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 49.950 100 40-160
2-Butanone (MEK)ug/L 115100 115 61-144
2-Chlorotoluene ug/L 49.750 99 74-132
2-Hexanone ug/L 117100 117 68-143
4-Chlorotoluene ug/L 49.050 98 76-133
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 72-135
Acetone ug/L 119100 119 48-146
Benzene ug/L 51.750 103 80-125
Bromobenzene ug/L 49.950 100 75-125
Bromochloromethane ug/L 52.450 105 71-125
Bromodichloromethane ug/L 53.850 108 78-124
Bromoform ug/L 51.850 104 71-128
Bromomethane ug/L 46.150 92 40-160
Carbon tetrachloride ug/L 54.050 108 69-131
Chlorobenzene ug/L 50.350 101 81-122
Chloroethane ug/L 44.650 89 39-148
Chloroform ug/L 53.050 106 73-127
Chloromethane ug/L 50.850 102 44-146
cis-1,2-Dichloroethene ug/L 52.050 104 74-124
cis-1,3-Dichloropropene ug/L 51.150 102 72-132
Dibromochloromethane ug/L 53.550 107 78-125
Dibromomethane ug/L 51.250 102 82-120
Dichlorodifluoromethane ug/L 53.150 106 34-157
Diisopropyl ether ug/L 53.650 107 69-135
Ethylbenzene ug/L 50.850 102 79-121
Hexachloro-1,3-butadiene ug/L 49.750 99 72-131
m&p-Xylene ug/L 103100 103 81-124
Methyl-tert-butyl ether ug/L 49.950 100 74-131
Methylene Chloride ug/L 58.950 118 64-133
Naphthalene ug/L 49.050 98 73-133
o-Xylene ug/L 51.550 103 79-131
p-Isopropyltoluene ug/L 50.550 101 80-131
Styrene ug/L 48.950 98 84-126
Tetrachloroethene ug/L 48.350 97 78-122
Toluene ug/L 47.250 94 80-121
trans-1,2-Dichloroethene ug/L 53.450 107 71-127
trans-1,3-Dichloropropene ug/L 51.550 103 69-141
Trichloroethene ug/L 51.450 103 78-122
Trichlorofluoromethane ug/L 51.950 104 53-137
Vinyl acetate ug/L 127100 127 40-160
Vinyl chloride ug/L 58.150 116 58-137
Xylene (Total)ug/L 154150 103 81-126
1,2-Dichloroethane-d4 (S)%105 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397329MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402544001
2397330
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 800 106 70-130110 4800ND844883
1,1,1-Trichloroethane ug/L 800 118 70-130116 2800ND944926
1,1,2,2-Tetrachloroethane ug/L 800 102 70-130107 5800ND817856
1,1,2-Trichloroethane ug/L 800 106 70-130105 1800ND846839
1,1-Dichloroethane ug/L 800 108 70-130108 0800ND868867
1,1-Dichloroethene ug/L 800 133 70-166131 2800ND10601050
1,1-Dichloropropene ug/L 800 118 70-130118 0800ND946943
1,2,3-Trichlorobenzene ug/L 800 97 70-130104 7800ND775828
1,2,3-Trichloropropane ug/L 800 107 70-130115 7800ND854916
1,2,4-Trichlorobenzene ug/L 800 98 70-130106 7800ND785846
1,2-Dibromo-3-chloropropane ug/L 800 98 70-130105 8800ND782844
1,2-Dibromoethane (EDB)ug/L 800 105 70-130111 6800ND842891
1,2-Dichlorobenzene ug/L 800 101 70-130109 8800ND810875
1,2-Dichloroethane ug/L 800 112 70-130111 1800ND893887
1,2-Dichloropropane ug/L 800 113 70-130112 1800ND905897
1,3-Dichlorobenzene ug/L 800 101 70-130108 6800ND810864
1,3-Dichloropropane ug/L 800 107 70-130115 7800ND853920
1,4-Dichlorobenzene ug/L 800 99 70-130107 8800ND791857
2,2-Dichloropropane ug/L 800 100 70-13095 4800ND796762
2-Butanone (MEK)ug/L 1600 122 70-130121 01600ND19501940
2-Chlorotoluene ug/L 800 103 70-130111 7800ND823885
2-Hexanone ug/L 1600 119 70-130127 61600ND19002030
4-Chlorotoluene ug/L 800 103 70-130110 7800ND824880
4-Methyl-2-pentanone (MIBK)ug/L 1600 118 70-130116 11600ND18801850
Acetone ug/L M1160013270-130129 31600ND21202060
Benzene ug/L 800 113 70-148112 1800ND907897
Bromobenzene ug/L 800 102 70-130113 10800ND817900
Bromochloromethane ug/L 800 113 70-130108 4800ND901865
Bromodichloromethane ug/L 800 111 70-130108 3800ND889867
Bromoform ug/L 800 94 70-130102 8800ND753815
Bromomethane ug/L 800 86 70-130100 14800ND692797
Carbon tetrachloride ug/L 800 120 70-130122 2800ND963978
Chlorobenzene ug/L 800 106 70-146112 5800ND847892
Chloroethane ug/L 800 120 70-130122 2800ND960979
Chloroform ug/L 800 114 70-130113 1800ND908902
Chloromethane ug/L 800 116 70-130117 1800ND926936
cis-1,2-Dichloroethene ug/L 800 114 70-130114 080013410501040
cis-1,3-Dichloropropene ug/L 800 104 70-130105 1800ND832843
Dibromochloromethane ug/L 800 105 70-130110 5800ND841880
Dibromomethane ug/L 800 110 70-130109 1800ND876870
Dichlorodifluoromethane ug/L 800 124 70-130122 2800ND991974
Diisopropyl ether ug/L 800 116 70-130114 2800ND928914
Ethylbenzene ug/L 800 109 70-130115 6800ND868922
Hexachloro-1,3-butadiene ug/L 800 99 70-130106 7800ND792846
m&p-Xylene ug/L 1600 108 70-130116 61600ND17301850
Methyl-tert-butyl ether ug/L 800 105 70-130104 1800ND839833
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2397329MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402544001
2397330
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 800 126 70-130124 1800ND1010995
Naphthalene ug/L 800 98 70-130105 780046.9 830 889
o-Xylene ug/L 800 107 70-130113 5800ND857903
p-Isopropyltoluene ug/L 800 105 70-130112 6800ND840896
Styrene ug/L 800 100 70-130105 5800ND804844
Tetrachloroethene ug/L 800 102 70-130109 7800ND813870
Toluene ug/L 800 104 70-155103 1800ND836827
trans-1,2-Dichloroethene ug/L 800 119 70-130119 1800ND948953
trans-1,3-Dichloropropene ug/L 800 102 70-130104 2800ND814832
Trichloroethene ug/L 800 105 69-151103 0800704078807860
Trichlorofluoromethane ug/L M180013570-130136 1800ND10801090
Vinyl acetate ug/L M1160013670-130135 11600ND21802160
Vinyl chloride ug/L M180013470-130133 1800ND10701060
Xylene (Total)ug/L 2400 108 70-130115 62400ND25902750
1,2-Dichloroethane-d4 (S)%100 70-130101
4-Bromofluorobenzene (S)%97 70-13099
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436152
EPA 8260B
EPA 8260B
8260 MSV Low Level
Associated Lab Samples:92402488010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399889
Associated Lab Samples:92402488010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/14/18 13:22
1,1,1-Trichloroethane ug/L ND 1.0 10/14/18 13:22
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/14/18 13:22
1,1,2-Trichloroethane ug/L ND 1.0 10/14/18 13:22
1,1-Dichloroethane ug/L ND 1.0 10/14/18 13:22
1,1-Dichloroethene ug/L ND 1.0 10/14/18 13:22
1,1-Dichloropropene ug/L ND 1.0 10/14/18 13:22
1,2,3-Trichlorobenzene ug/L ND 1.0 10/14/18 13:22
1,2,3-Trichloropropane ug/L ND 1.0 10/14/18 13:22
1,2,4-Trichlorobenzene ug/L ND 1.0 10/14/18 13:22
1,2-Dibromo-3-chloropropane ug/L ND 2.0 10/14/18 13:22
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/14/18 13:22
1,2-Dichlorobenzene ug/L ND 1.0 10/14/18 13:22
1,2-Dichloroethane ug/L ND 1.0 10/14/18 13:22
1,2-Dichloropropane ug/L ND 1.0 10/14/18 13:22
1,3-Dichlorobenzene ug/L ND 1.0 10/14/18 13:22
1,3-Dichloropropane ug/L ND 1.0 10/14/18 13:22
1,4-Dichlorobenzene ug/L ND 1.0 10/14/18 13:22
2,2-Dichloropropane ug/L ND 1.0 10/14/18 13:22
2-Butanone (MEK)ug/L ND 5.0 10/14/18 13:22
2-Chlorotoluene ug/L ND 1.0 10/14/18 13:22
2-Hexanone ug/L ND 5.0 10/14/18 13:22
4-Chlorotoluene ug/L ND 1.0 10/14/18 13:22
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/14/18 13:22
Acetone ug/L ND 25.0 10/14/18 13:22
Benzene ug/L ND 1.0 10/14/18 13:22
Bromobenzene ug/L ND 1.0 10/14/18 13:22
Bromochloromethane ug/L ND 1.0 10/14/18 13:22
Bromodichloromethane ug/L ND 1.0 10/14/18 13:22
Bromoform ug/L ND 1.0 10/14/18 13:22
Bromomethane ug/L ND 2.0 10/14/18 13:22
Carbon tetrachloride ug/L ND 1.0 10/14/18 13:22
Chlorobenzene ug/L ND 1.0 10/14/18 13:22
Chloroethane ug/L ND 1.0 10/14/18 13:22
Chloroform ug/L ND 1.0 10/14/18 13:22
Chloromethane ug/L ND 1.0 10/14/18 13:22
cis-1,2-Dichloroethene ug/L ND 1.0 10/14/18 13:22
cis-1,3-Dichloropropene ug/L ND 1.0 10/14/18 13:22
Dibromochloromethane ug/L ND 1.0 10/14/18 13:22
Dibromomethane ug/L ND 1.0 10/14/18 13:22
Dichlorodifluoromethane ug/L ND 1.0 10/14/18 13:22
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
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Huntersville, NC 28078
[phone]
Page 62 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399889
Associated Lab Samples:92402488010
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 10/14/18 13:22
Ethylbenzene ug/L ND 1.0 10/14/18 13:22
Hexachloro-1,3-butadiene ug/L ND 1.0 10/14/18 13:22
m&p-Xylene ug/L ND 2.0 10/14/18 13:22
Methyl-tert-butyl ether ug/L ND 1.0 10/14/18 13:22
Methylene Chloride ug/L ND 2.0 10/14/18 13:22
Naphthalene ug/L ND 1.0 10/14/18 13:22
o-Xylene ug/L ND 1.0 10/14/18 13:22
p-Isopropyltoluene ug/L ND 1.0 10/14/18 13:22
Styrene ug/L ND 1.0 10/14/18 13:22
Tetrachloroethene ug/L ND 1.0 10/14/18 13:22
Toluene ug/L ND 1.0 10/14/18 13:22
trans-1,2-Dichloroethene ug/L ND 1.0 10/14/18 13:22
trans-1,3-Dichloropropene ug/L ND 1.0 10/14/18 13:22
Trichloroethene ug/L ND 1.0 10/14/18 13:22
Trichlorofluoromethane ug/L ND 1.0 10/14/18 13:22
Vinyl acetate ug/L ND 2.0 10/14/18 13:22
Vinyl chloride ug/L ND 1.0 10/14/18 13:22
Xylene (Total)ug/L ND 1.0 10/14/18 13:22
1,2-Dichloroethane-d4 (S)%101 70-130 10/14/18 13:22
4-Bromofluorobenzene (S)%103 70-130 10/14/18 13:22
Toluene-d8 (S)%97 70-130 10/14/18 13:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399890LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.250 102 80-125
1,1,1-Trichloroethane ug/L 52.150 104 71-129
1,1,2,2-Tetrachloroethane ug/L 45.150 90 79-124
1,1,2-Trichloroethane ug/L 48.150 96 85-125
1,1-Dichloroethane ug/L 46.750 93 73-126
1,1-Dichloroethene ug/L 51.350 103 66-135
1,1-Dichloropropene ug/L 49.250 98 74-135
1,2,3-Trichlorobenzene ug/L 51.350 103 73-135
1,2,3-Trichloropropane ug/L 48.850 98 75-130
1,2,4-Trichlorobenzene ug/L 53.550 107 75-134
1,2-Dibromo-3-chloropropane ug/L 46.950 94 71-133
1,2-Dibromoethane (EDB)ug/L 47.650 95 83-124
1,2-Dichlorobenzene ug/L 48.950 98 80-133
1,2-Dichloroethane ug/L 49.350 99 67-128
1,2-Dichloropropane ug/L 47.450 95 75-132
1,3-Dichlorobenzene ug/L 48.450 97 77-130
1,3-Dichloropropane ug/L 47.550 95 76-131
1,4-Dichlorobenzene ug/L 48.650 97 78-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399890LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 50.950 102 40-160
2-Butanone (MEK)ug/L 86.0100 86 61-144
2-Chlorotoluene ug/L 47.950 96 74-132
2-Hexanone ug/L 91.6100 92 68-143
4-Chlorotoluene ug/L 46.850 94 76-133
4-Methyl-2-pentanone (MIBK)ug/L 91.6100 92 72-135
Acetone ug/L 88.3100 88 48-146
Benzene ug/L 47.650 95 80-125
Bromobenzene ug/L 48.550 97 75-125
Bromochloromethane ug/L 47.850 96 71-125
Bromodichloromethane ug/L 49.950 100 78-124
Bromoform ug/L 46.050 92 71-128
Bromomethane ug/L 40.050 80 40-160
Carbon tetrachloride ug/L 55.350 111 69-131
Chlorobenzene ug/L 49.650 99 81-122
Chloroethane ug/L 32.650 65 39-148
Chloroform ug/L 49.250 98 73-127
Chloromethane ug/L 36.750 73 44-146
cis-1,2-Dichloroethene ug/L 47.950 96 74-124
cis-1,3-Dichloropropene ug/L 49.750 99 72-132
Dibromochloromethane ug/L 51.450 103 78-125
Dibromomethane ug/L 49.750 99 82-120
Dichlorodifluoromethane ug/L 35.750 71 34-157
Diisopropyl ether ug/L 43.450 87 69-135
Ethylbenzene ug/L 50.450 101 79-121
Hexachloro-1,3-butadiene ug/L 57.750 115 72-131
m&p-Xylene ug/L 104100 104 81-124
Methyl-tert-butyl ether ug/L 44.750 89 74-131
Methylene Chloride ug/L 45.950 92 64-133
Naphthalene ug/L 46.350 93 73-133
o-Xylene ug/L 49.850 100 79-131
p-Isopropyltoluene ug/L 49.150 98 80-131
Styrene ug/L 48.950 98 84-126
Tetrachloroethene ug/L 52.650 105 78-122
Toluene ug/L 48.450 97 80-121
trans-1,2-Dichloroethene ug/L 48.250 96 71-127
trans-1,3-Dichloropropene ug/L 50.750 101 69-141
Trichloroethene ug/L 51.450 103 78-122
Trichlorofluoromethane ug/L 49.350 99 53-137
Vinyl acetate ug/L 97.0100 97 40-160
Vinyl chloride ug/L 44.850 90 58-137
Xylene (Total)ug/L 154150 102 81-126
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399891MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403223012
2399892
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 106 70-130100 6200ND211200
1,1,1-Trichloroethane ug/L 200 120 70-130109 10200ND240218
1,1,2,2-Tetrachloroethane ug/L 200 94 70-13095 2200ND188191
1,1,2-Trichloroethane ug/L 200 105 70-130104 1200ND210208
1,1-Dichloroethane ug/L 200 101 70-13093 9200ND203186
1,1-Dichloroethene ug/L 200 113 70-166107 6200ND227214
1,1-Dichloropropene ug/L 200 112 70-130104 8200ND224207
1,2,3-Trichlorobenzene ug/L 200 103 70-130105 2200ND206210
1,2,3-Trichloropropane ug/L 200 106 70-130106 0200ND213212
1,2,4-Trichlorobenzene ug/L 200 108 70-130107 1200ND215214
1,2-Dibromo-3-chloropropane ug/L 200 93 70-13095 1200ND186189
1,2-Dibromoethane (EDB)ug/L 200 100 70-130102 2200ND200205
1,2-Dichlorobenzene ug/L 200 104 70-130102 1200ND207205
1,2-Dichloroethane ug/L 200 104 70-130104 0200ND208207
1,2-Dichloropropane ug/L 200 103 70-13097 6200ND205194
1,3-Dichlorobenzene ug/L 200 107 70-130100 6200ND213200
1,3-Dichloropropane ug/L 200 101 70-130101 1200ND203202
1,4-Dichlorobenzene ug/L 200 104 70-13096 7200ND208193
2,2-Dichloropropane ug/L 200 98 70-13091 8200ND197182
2-Butanone (MEK)ug/L 400 96 70-13096 0400ND385384
2-Chlorotoluene ug/L 200 100 70-13090 11200ND201180
2-Hexanone ug/L 400 95 70-13098 4400ND378393
4-Chlorotoluene ug/L 200 97 70-13091 6200ND195183
4-Methyl-2-pentanone (MIBK)ug/L 400 98 70-130101 3400ND402414
Acetone ug/L 400 104 70-130106 2400ND414423
Benzene ug/L E,M120017170-14877 10200169020301850
Bromobenzene ug/L 200 103 70-130104 1200ND205207
Bromochloromethane ug/L 200 106 70-130102 5200ND213203
Bromodichloromethane ug/L 200 104 70-13097 6200ND207195
Bromoform ug/L 200 85 70-13090 5200ND170179
Bromomethane ug/L M12005770-13061 7200ND114122
Carbon tetrachloride ug/L 200 121 70-130116 4200ND241233
Chlorobenzene ug/L 200 108 70-146100 7200ND216201
Chloroethane ug/L 200 94 70-13084 10200ND187169
Chloroform ug/L 200 113 70-130100 12200ND226200
Chloromethane ug/L M12007870-13069 12200ND159141
cis-1,2-Dichloroethene ug/L 200 104 70-13097 6200ND208195
cis-1,3-Dichloropropene ug/L 200 104 70-13098 6200ND208196
Dibromochloromethane ug/L 200 101 70-13099 3200ND203197
Dibromomethane ug/L 200 107 70-130106 1200ND214212
Dichlorodifluoromethane ug/L 200 82 70-13076 7200ND163152
Diisopropyl ether ug/L 200 96 70-13091 5200ND191182
Ethylbenzene ug/L 200 129 70-13094 12200363621550
Hexachloro-1,3-butadiene ug/L 200 112 70-13096 15200ND224193
m&p-Xylene ug/L M140019070-13089 12400287036303230
Methyl-tert-butyl ether ug/L 200 110 70-130104 2200421641629
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399891MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92403223012
2399892
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 200 99 70-13089 11200ND198178
Naphthalene ug/L 200 98 70-130105 3200245441455
o-Xylene ug/L M120013670-13093 10200608879793
p-Isopropyltoluene ug/L M120013470-130115 16200ND268229
Styrene ug/L 200 103 70-13098 5200ND206197
Tetrachloroethene ug/L 200 114 70-130105 8200ND227209
Toluene ug/L 200 116 70-15597 10200175407369
trans-1,2-Dichloroethene ug/L 200 108 70-130100 8200ND215199
trans-1,3-Dichloropropene ug/L 200 105 70-130102 2200ND210205
Trichloroethene ug/L 200 114 69-151100 13200ND227200
Trichlorofluoromethane ug/L 200 118 70-130110 7200ND236220
Vinyl acetate ug/L 400 104 70-130104 0400ND416415
Vinyl chloride ug/L 200 101 70-13095 7200ND203190
Xylene (Total)ug/L MS60017270-13090 11600348045104020
1,2-Dichloroethane-d4 (S)%105 70-130100
4-Bromofluorobenzene (S)%100 70-130100
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435961
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92402488001, 92402488002, 92402488003, 92402488004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2399114
Associated Lab Samples:92402488001, 92402488002, 92402488003, 92402488004
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 10/12/18 11:59
1,2-Dichloroethane-d4 (S)%99 50-150 10/12/18 11:59
Toluene-d8 (S)%103 50-150 10/12/18 11:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2399115LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 20.820 104 71-125
1,2-Dichloroethane-d4 (S)%101 50-150
Toluene-d8 (S)%103 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2399116MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402488001
2399117
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 106 50-150111 420ND21.2 22.1
1,2-Dichloroethane-d4 (S)%103 50-150105
Toluene-d8 (S)%105 50-150107
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
436230
EPA 8260B Mod.
EPA 8260B Mod.
8260 MSV SIM
Associated Lab Samples:92402488005, 92402488006, 92402488007, 92402488008, 92402488009, 92402488010, 92402488011,
92402488012, 92402488013, 92402488014, 92402488015, 92402488016, 92402488017, 92402488018,
92402488019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2400347
Associated Lab Samples:92402488005, 92402488006, 92402488007, 92402488008, 92402488009, 92402488010, 92402488011,
92402488012, 92402488013, 92402488014, 92402488015, 92402488016, 92402488017, 92402488018,
92402488019
Matrix:Water
Analyzed
1,4-Dioxane (p-Dioxane)ug/L ND 2.0 10/15/18 13:17
1,2-Dichloroethane-d4 (S)%105 50-150 10/15/18 13:17
Toluene-d8 (S)%109 50-150 10/15/18 13:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2400348LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dioxane (p-Dioxane)ug/L 22.020 110 71-125
1,2-Dichloroethane-d4 (S)%101 50-150
Toluene-d8 (S)%106 50-150
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2400349MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
2610107032
2400350
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,4-Dioxane (p-Dioxane)ug/L 20 99 50-15098 120ND19.8 19.6
1,2-Dichloroethane-d4 (S)%112 50-150102
Toluene-d8 (S)%115 50-150116
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 77
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92402488
FUL.006
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
435111
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
300.0 IC Anions
Associated Lab Samples:92402488008, 92402488009, 92402488010, 92402488011, 92402488018, 92402488019
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2395256
Associated Lab Samples:92402488008, 92402488009, 92402488010, 92402488011, 92402488018, 92402488019
Matrix:Water
Analyzed
Chloride mg/L ND 1.0 10/09/18 13:58
Sulfate mg/L ND 1.0 10/09/18 13:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2395257LABORATORY CONTROL SAMPLE:
LCSSpike
Chloride mg/L 49.950 100 90-110
Sulfate mg/L 49.550 99 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2395258MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402488008
2395259
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride mg/L M6507490-11077 050100010401040
Sulfate mg/L M65039390-110578 450206022502340
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2395260MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92402337001
2395261
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chloride mg/L M6,R150-176 90-110-670 1525037428639.1
Sulfate mg/L 50 93 90-110101 55037.8 84.1 88.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92402488
FUL.006
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 77
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92402488
FUL.006
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92402488008 435090 435271MW-8R EPA 3010A EPA 6010D
92402488009 435090 435271MW-9 EPA 3010A EPA 6010D
92402488010 435090 435271MW-10 EPA 3010A EPA 6010D
92402488011 435090 435271MW-13 EPA 3010A EPA 6010D
92402488018 435090 435271MW-18 EPA 3010A EPA 6010D
92402488019 435090 435271MW-19 EPA 3010A EPA 6010D
92402488008 435216 435311MW-8R EPA 7470A EPA 7470A
92402488009 435216 435311MW-9 EPA 7470A EPA 7470A
92402488010 435216 435311MW-10 EPA 7470A EPA 7470A
92402488011 435216 435311MW-13 EPA 7470A EPA 7470A
92402488018 435216 435311MW-18 EPA 7470A EPA 7470A
92402488019 435216 435311MW-19 EPA 7470A EPA 7470A
92402488001 435194MW-1 EPA 8260B
92402488002 435194MW-2 EPA 8260B
92402488003 435194MW-3 EPA 8260B
92402488004 435194MW-4 EPA 8260B
92402488005 435194MW-5 EPA 8260B
92402488006 435194MW-6 EPA 8260B
92402488007 435194MW-7 EPA 8260B
92402488008 435301MW-8R EPA 8260B
92402488009 435194MW-9 EPA 8260B
92402488010 436152MW-10 EPA 8260B
92402488011 435194MW-13 EPA 8260B
92402488012 435194MW-14 EPA 8260B
92402488013 435194MW-15 EPA 8260B
92402488014 435194MW-16 EPA 8260B
92402488015 435194MW-17 EPA 8260B
92402488016 435194MW-17D EPA 8260B
92402488017 435194MW-17DD EPA 8260B
92402488018 435528MW-18 EPA 8260B
92402488019 435528MW-19 EPA 8260B
92402488020 435301TRIP BLANK EPA 8260B
92402488001 435961MW-1 EPA 8260B Mod.
92402488002 435961MW-2 EPA 8260B Mod.
92402488003 435961MW-3 EPA 8260B Mod.
92402488004 435961MW-4 EPA 8260B Mod.
92402488005 436230MW-5 EPA 8260B Mod.
92402488006 436230MW-6 EPA 8260B Mod.
92402488007 436230MW-7 EPA 8260B Mod.
92402488008 436230MW-8R EPA 8260B Mod.
92402488009 436230MW-9 EPA 8260B Mod.
92402488010 436230MW-10 EPA 8260B Mod.
92402488011 436230MW-13 EPA 8260B Mod.
92402488012 436230MW-14 EPA 8260B Mod.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 77
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92402488
FUL.006
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92402488013 436230MW-15 EPA 8260B Mod.
92402488014 436230MW-16 EPA 8260B Mod.
92402488015 436230MW-17 EPA 8260B Mod.
92402488016 436230MW-17D EPA 8260B Mod.
92402488017 436230MW-17DD EPA 8260B Mod.
92402488018 436230MW-18 EPA 8260B Mod.
92402488019 436230MW-19 EPA 8260B Mod.
92402488008 435111MW-8R EPA 300.0 Rev 2.1 1993
92402488009 435111MW-9 EPA 300.0 Rev 2.1 1993
92402488010 435111MW-10 EPA 300.0 Rev 2.1 1993
92402488011 435111MW-13 EPA 300.0 Rev 2.1 1993
92402488018 435111MW-18 EPA 300.0 Rev 2.1 1993
92402488019 435111MW-19 EPA 300.0 Rev 2.1 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/16/2018 12:44 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 77
Page 73 of 77
Page 74 of 77
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Page 76 of 77
Page 77 of 77

Appendix C Historical Groundwater Analytical Results Table
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date 12/20/02 02/28/03 01/19/05 04/21/05 07/18/05 10/20/05 01/30/06 07/25/06 01/31/07 07/12/07 01/29/08 07/16/08 01/28/0907/27/09 01/12/10 07/21/10 01/18/11 07/13/11 01/24/12 07/10/12 01/24/1307/02/13 06/12/14 12/10/14 09/18/15 03/22/16 09/23/16 03/30/17 09/22/17 03/14/18 10/05/18VOCs (µg/l)6230D 6230D 601 601 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BAcetone 6,000 NA NA NA NA NA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 18J <50 <50 <50<50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0Benzene 1 <0.5<0.5NANANANANANANA<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Bromochloromethane NS <0.5 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Bromodichloromethane 0.6 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Bromoform 4 ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Bromomethane 10 <0.5 <0.5 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0 <2.0 <2.0<2.0 <2.0 <2.0tert-Butylbenzene 70 <0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 NA NA NA NA NA NA NA NAn-Butylbenzene 70 <0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NACarbon Disulfide 700 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NACarbon Tetrachloride 0.3 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Chlorobenzene 50 ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Chloroethane 3,000 ND ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Chloroform 70 <0.5 1.2 1.2 1.4 1.0 <1.0 <1.0 0.56J 2.4 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 2.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0Chloromethane 3 <2.5 <2.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0Dibromomethane 70 <0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,2-Dichlorobenzene 20 <0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,3-Dichlorobenzene 200 ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,4-Dichlorobenzene 6 <0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,1-Dichloroethane 6 0.538.4 6.24.4 1.5 <1.0 <1.0 <1.0181.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.01,2-Dichloroethane 0.4 <0.50.78<1.00.52J<1.0 <1.0 <1.0 <1.03.8<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,1-Dichloroethene 350 9.9 160 190 75 43 12 17 1053025 2.4 3.1 1.1 <1.0 <1.0 0.82 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.8 <1.0 <1.0 1.3 <1.0 <1.0 <1.0 <1.0 <1.0cis-1,2-Dichloroethene 70 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0trans-1,2-Dichloroethene 100 <0.5 <0.5<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,2-Dichloropropane 0.6 <0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.01,3-Dichloropropane 0.4 ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Ethylbenzene 600 <0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.02-Butanone (MEK) 4,000 NA NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10<10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0Methylene Chloride 5 <2.0 <2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.04-Methyl 2-pentanone (MIBK) NS NA NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0Naphthalene 6 <0.5 0.54 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,1,1,2-Tetrachloroethane 1 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.01,1,2,2-Tetrachloroethane 0.2 ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0Tetrachloroethene 0.7 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Toluene 600 <0.5 <0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,2,3-Trichlorobenzene NS ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,2,4-Trichlorobenzene 70 <0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,1,1-Trichloroethane 200 <0.5 0.70 <1.0 0.24J <1.0 <1.0 <1.0 <1.0 2.00 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,1,2-Trichloroethane 0.6 <0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.02.60<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Trichloroethene 3 <0.5 1.6 <1.0 0.89J <1.0 <1.0 <1.0 <1.0 1.20 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Trichlorofluoromethane 2,000 4.6 48 16 19 16 <5.0 5.3 <5.0 23 13 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,2,3-Trichloropropane 0.005 ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,2,4-Trimethylbenzene 400 <0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA1,3,5-Trimethylbenzene 400 <0.5 0.52 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NAVinyl Chloride 0.03 ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Total Xylenes 500 <0.5 0.81 NA NA NA NA NA NA NA <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0<3.0 <1.0 <3.0 <2.0 <1.0<1.0<1.0 <1.0 <1.01,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0 NANANANANANANANANA9.3<4.010.0 8.5<4.0 <4.03.8<3.0 <3.0 <3.0 <3.0 <3.0 <3.05.2<2.0 <2.0 <2.0 <2.0 <2.0 <2.0<2.0 <2.0Others (µg/l)Chloride 250,000 NA 110,000 97,000120,000 130,000 44,000 98,000 77,000 76,000 110,000 47,000 30,000 28,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Sulfate 250,000 NA 1,900 18,000 22,000 16,000 17,000 10,000 13,000 <5,00010,000 28,000 23,000 37,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Sodium NS NA NA 67,000 71,000 72,000 32,000 54,000 54,000 46,000 62,000 42,000 30,000 39,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Iron, Total 300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANANA NA Nitrate 10,000 NA 6,900 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA Methane NS NA <26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANANA NA Total Organic Carbon NS NA NA NA NA NA 4,040 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NANA NANA NA Field MeasurementsFerrous Iron (mg/l) NS NM <0.1 NM NM 0.2 0.4 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ORP (mV) NS NM NM NM 80 266 306 261 173 252 261 284.8 -2.9 56.2 -27.1 142.2 120.5 8.0 140.0 173.3 84.4 148.6 82.5 2.0 66.0 53.3 138.4 52.3 66.6 1.0 458.5 -153.6Temperature (oC) NS 16.7 13.6 12.0 16.3 19.4 20.7 16.1 19.6 13.9 19.5 17.80 20.40 16.67 20.62 14.77 20.58 13.93 20.02 16.16 19.5015.19 22.23 19.88 16.83 21.17 15.30 24.20 13.20 26.50 12.40 26.1pH NS 5.8 5.21 4.34 5.70 4.71 5.49 5.31 5.22 5.5 5.34 4.92 5.28 5.74 5.77 5.50 5.14 6.03 5.52 5.44 5.92 5.31 5.31 5.88 4.97 5.59 6.12 5.95 5.62 5.85 6.07 6.09Conductivity (µS/cm) NS 327.0 428.0 293.3 460.3 402.5 238.0 404.6 338 356318.3 229 204 198 126 219 277 92 134 122 96 109 108 222 193 136 98.1 63.0 124.9 121.7 105.3 125.5Dissolved Oxygen (mg/l) NS NM 1.36 NM2.75 1.02 0.67 0.400.58 1.56 0.31 0.55 0.13 0.74 0.58 1.24 0.577.25 0.11 0.74 2.34 0.56 0.23 0.25 1.88 0.21 0.98 0.25 1.21 0.29 1.63 0.15Turbidity (NTU) NS NMNMNMNMNMNMNMNMNMNM4.72.8510.79.458.925.839.45 14.68 8.01 8.28 7.3 20.48 0.00 33.3 8.33 63.7 54.1 42.5 29.9 41.8 9.41Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointNorth Carolina Groundwater Standard 1MW-1S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 1 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 112/20/02 02/28/03 01/19/05 04/21/05 07/18/05 10/20/05 01/30/06 07/25/06 01/31/07 07/12/07 01/29/08 07/16/08 01/28/0907/27/09 01/12/10 07/21/10 01/19/11 07/13/11 01/25/12 07/10/12 01/24/1307/02/13 06/12/14 12/10/14 09/18/15 03/22/16 09/23/16 03/30/17 09/22/17 03/14/18 10/05/186230D 6230D 601 601 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 NA NA NA NA <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0<2.0<2.0<2.0<2.0<2.0<2.0<2.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANANA<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 1.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 0.39<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2.5 <2.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5<2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.010 9.95.7 4.8 4.16.25.2 5.3 5.5 4.8 2.8 2.5 <1.0 2.0 1.4 1.6 0.92J 1.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.2 1.2 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.056 150 82 85 77 84 68 36 89 90 36 28 8.2 13 15 22 4.9 5.4 2.5 4.0 2.2 <1.0 15 14.7 24.025.4 <1.0 6.8 9.2 1.5 4.2<0.5 <0.5 <1.0 0.86J <1.0 1.30 1.4 <1.0 <1.0 1.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 <0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.52.1 1.6 1.1 1.7 1.9 2.50.61J1.3 1.4<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0<1.0<1.0<1.0<1.0<1.04.4 2.5 1.2 1.4 1.5 1.4 0.86J 3.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.42 0.35J<1.0 <1.0 <1.0 2.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.034 130 56 50 54 72 44 23 74 42 7.2 6.71.83.1 4.7 6.31.4 1.0 <1.0 1.2 <1.0 <1.04.4 3.7 6.1 9.2<1.03.2 3.2<1.03.7<0.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0NANANANANANANA<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0NANANANANANANAND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <0.5 NA NA NA NA NA NA NA <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0<3.0 <1.0 <3.0 <2.0 <1.0<1.0<1.0<1.0<1.0NA NA NA NA NA NA NA NA NA <4.0 <4.0 <4.0 <4.0<4.0 <4.04.1<3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <2.0 <2.0 3.0 <2.0 <2.0 <2.0 <2.0 <2.0NA 54,000 46,000 39,000 37,000 35,00033,000 29,000 45,000 30,000 23,000 23,000 26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1,500 18,000 20,000 17,000 19,000 7,800 20,000 <5,000 12,000 26,000 10,000 8,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 26,000 24,000 23,000 20,000 21,000 19,000 29,000 20,000 15,000 14,000 14,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NM NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1,000 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NM <0.1 NM NM 0.4 0.2 0.4 <0.2 <0.2 <0.2 0.3 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NANANANANANANANANM NM NM -50 41 358 354 275 330 351 309.2 19.2 71.4 149.2 171.4 293.6 60.6 164.4226.1 151.1 306.7 182.6 319 250 269 -56.3 271.7 104.5 159.4 470.8 47.315.4 12.5 13.1 17.9 19.2 20.9 15.5 20.9 13.6 19.7 16.2 20.7 15.4 20.9 12.9 21.0 14.3 20.7 15.5 20.1 14.022.3 19.0 16.8 21.9 16.523.9 12.4 26.0 11.3 20.15.31 5.38 4.39 5.56 5.01 4.81 4.45 4.52 4.92 4.51 4.354.30 5.09 4.04 4.40 4.42 4.86 4.46 4.45 4.82 4.34 5.21 2.81 4.24 4.64 5.63 4.75 5.20 5.08 5.73 5.02175.0 428.0 162.0 192.2 186.2 198.6188.9 153 238 185.0 126 131 111 155 177 148 114 141 120 108 76 101 254 113 136 149.7 137.2 122.6 93.4 101.4 128.0NM 2.12 NM 2.48 1.35 0.50 2.42 1.72 2.51 1.28 0.69 0.291.51 0.26 2.56 0.74 2.21 0.35 1.08 0.29 1.94 2.04 0.00 2.31 0.24 0.43 0.39 2.19 0.26 4.26 0.80NM NM NM NM NM NM NM NM NM NM 2.9 4.47 1.81 2.79 4.72 0.78 10.02 0.41 1.12 1.41 7.01 19.63 0.0 9.6 7.34 26.378.30 55.60 9.51 62.61 23.94Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-2S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 2 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 103/11/03 01/28/09 07/27/09 01/12/10 04/07/10 07/21/10 02/28/03 01/19/05 04/21/05 07/18/05 10/20/05 01/30/06 07/25/06 01/31/07 07/12/07 01/29/08 07/16/08 01/28/09 07/27/09 01/12/10 07/21/1001/18/11 07/13/11 01/25/12 07/11/12 01/25/13 07/02/13 06/12/14 12/10/1409/18/15 03/22/16 09/23/16 03/29/17 09/22/1703/14/18 10/05/186230D 8260 8260B 8260B 8260B 8260B 6230D 601 601 601 601 601 601 601 8260 82608260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B8260B 8260B 8260B 8260B 8260B 8260B 8260B<0.5 <50 <50 <50 <50 <50 NA NA NA NA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<0.5 NA NA NA <1.0 <1.0 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND ND NDND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <0.5 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND ND NDND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 ND ND ND NDND ND ND ND <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.016 <5.0 <5.0 <5.0 <5.0 <5.0 1.0 1.2 1.0 <1.0 1.4 1.4 9.1 8.0 9.5 5.1 <5.0 <5.0 <5.0 <5.0 5.1 4.6J <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 2.5 2.0 3.3 1.9 1.6 1.4 1.2 <1.0<0.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND ND NDND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0184.011<1.0 <1.0 <1.0 <1.0 1.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.06.4<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.02.9<1.01.5<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.0<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.062097 110 16 7 1.8 1.5 35 1.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 18.7 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 0.92 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND NA NA NANA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NA <10 <10 <10 <10 <10 NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10<10 <10 <10 <10 <10.0 <5.0 <5.0<5.0<5.0<5.0<5.0<5.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA <10 <10 <10 <10 <10 NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10<10 <10 <10 <10 <10.0 <5.0 <5.0<5.0<5.0<5.0<5.0<5.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <0.5 NA NANA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND ND NDND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.01.7<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <0.5 NA NANA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND NA NA NANA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 5.3 <1.0 8.5 <1.0 1.9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.03.5<1.00.96J<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 1.4 <1.0 1.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 14 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND NA NA NANA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 NA NANA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND ND NDND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <3.0<3.0 <3.0<3.0 <3.0<0.5 NA NA NA NA NA NA NA <3.0 <3.0<3.0 <3.0<3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 <1.0 <3.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA <4.0 <4.09.5<4.0 <4.0NA NA NA NA NA NA NA NA26 21 16 129<4.04.1 4.7<3.05.1 12 5.7 6.5 7.2 4.7 3.0 42.3 6.1 6.0 5.5 9.9 6.7NA NA NA NA NA NA 39,000 42,000 45,00044,000 42,000 38,000 24,000 24,000 28,000 28,000 23,000 25,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA 1,400 4,400 30,000 19,000 14,000 3,400 15,000 9,600 7,400 14,000 5,200 5,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NM 26,000 30,000 29,000 26,000 26,000 21,000 21,000 21,000 21,000 20,000 20,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANA NA NANA NA NA NA NA NA 7,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NANA NA NA NA NA NA <26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NANA NANA NANANA NA NA NA NA 1,060 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA 0.20 NA NA NA NA <0.1 NM NM 0.4 0.4 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NANANANANANANANANANANA 7.4 -197.5 108.6 -177.1 -91.4 NM NM112 273 299 315 281 311 343 345.5 50.8 66.2 57.4 178.8 293.5 23.4 178.8 265.2155.2 292.8 333.0 167 311 356.3 332.3 237.3 110.4 242.1 54.9 32.6NA 13.59 20.32 14.36 17.80 19.56 14.2 13.8 17.5 19.0 21.6 16.7 20.4 14.9 19.717.1 21.1 16.8 21.3 14.6 21.5 14.8 20.4 16.5 19.3 15.2 21.7 19.4 17.0 20.8 10.823.417.526.312.923.0NA 7.68 6.86 6.71 7.60 7.024.81 4.17 5.25 4.55 4.98 4.5 4.58 5.01 4.60 4.41 4.39 5.19 4.42 4.59 4.31 4.604.22 4.21 4.62 4.50 3.90 4.84 3.72 4.10 4.55 4.51 3.92 4.52 4.75 4.61NA 154 0.130 149 290 199 221.0 140.7 197.2 179.9 188.0 182.6 158 145 146.7 132124 112 108 131 126 116 133 131 127 89 120 125 131 134 227.9 132.2 147.6 108.4 128.5 124.8NA 0.53 0.07 1.27 0.32 1.622.12 NM 2.35 1.25 3.61 1.801.72 2.94 1.24 1.44 1.582.321.641.851.421.971.161.681.27 1.41 1.27 2.53 2.51 1.03 1.02 1.29 1.32 1.38 1.86 1.42NA17.0 9.89 22.97 63.76 3.07 NM NM NM NM NM NMNM NM NM 0.00 1.78 1.40 1.69 2.28 3.11 1.23 0.00 0.09 0.62 0.88 2.56 0.0 6.0 2.09 55.10 13.10 18.10 5.28 9.89 3.77Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-2DSouth of BuildingMW-3S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 3 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 102/28/03 01/19/05 04/21/05 07/18/05 10/20/05 01/30/06 07/25/06 01/31/07 07/12/07 01/29/08 07/16/08 01/28/09 07/27/0901/12/10 07/21/10 01/19/11 07/13/11 01/25/12 07/12/12 01/25/13 07/02/1306/12/14 12/11/14 09/18/15 03/22/16 09/23/16 03/29/17 09/22/17 03/14/18 10/05/186230D 601 601 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <20.0<25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANANA<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.51 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 1.3 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 1.3 <1.0 <1.0 <1.0 <1.0 <1.0<2.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5<2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.07.04.6 2.7 1.7 2.0 3.2 0.51J 5.9 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 1.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.5 <1.0 <1.0 <1.0 <1.0 <1.00.65<1.0 0.31J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.4<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0210 80 78 51 56 54 37 120 34 15 7.7 <1.0 4.6 8.4 40 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 12.4 38.2 <1.0 <1.0 <1.0 <1.0 1.51.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 1.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.03.2 1.1 1.1<1.0 <1.01.8<1.02.4<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.5 <1.0 0.27J <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.97<1.0 0.32J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 0.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0230 38 49 6.2 4.3 15 16 792.2 <1.0 <1.0 <1.0 <1.0 <1.07.5<1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.03.9 25.6<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANA<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANAND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <1.0 <3.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA NA <4.0 <4.0 <4.0 <4.0<4.0 <4.06.8<3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <2.0 <2.07.4<2.0 <2.0 <2.0 <2.0 <2.0NA 32,000 50,000 18,000 20,000 20,00022,000 49,000 12,000 27,000 7,700 8,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA 28,000 18,000 34,000 38,000 18,000 22,000 <5,000 21,000 13,000 18,000 18,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA 18,000 32,000 12,000 11,000 12,000 9,900 30,000 8,200 10,000 6,500 6,000NANANANANANANANANANANANANANANANA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA9,400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA 1,740 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.1 NM NM 1.4 0.2 0.6 1.9 <0.2 <0.2 0.9 0.9-1.0 0.25 NA NA NA NA NA NA NA NA NA NA NANANANANANANANANM NM 62 263 291 292 210 339 309 236.5 16.262.7 171.9 178.9 260.6 63.8 172.5 259.8 140.9 271.8 314.3 296 326 66.7310.8 -31.7 101.2 284.8 400.2 118.214.1 12.0 17.0 18.6 20.9 16.1 19.8 14.1 18.8 16.2 21.1 16.3 21.1 14.6 20.8 15.3 20.5 15.8 19.8 14.0 21.1 20.0 13.720.9 16.9 22.6 17.1 23.2 10.3 20.94.84 4.25 5.17 4.49 4.85 4.42 4.46 4.82 4.54 4.40 4.305.06 4.11 4.16 4.06 4.49 4.27 4.02 4.47 4.36 3.44 2.66 3.22 5.28 4.74 4.42 3.81 4.34 4.62 3.81270.0 143.5 255.4 120.4 134.9 144.2 149262 105.8 124 90 74 78 89 150 58 63 76 8450 70 159 55 89 215.2 49.3 76.8 57.2 57.3 85.72.02 NM 1.74 0.39 4.18 0.321.53 1.82 0.59 1.00 0.26 0.83 0.37 1.63 0.53 1.23 0.42 0.51 0.94 0.56 0.31 0.00 3.36 1.59 1.18 0.57 0.55 0.44 0.81 1.08NM NM NM NM NM NM NM NM NM 6.7 2.30 16.70 2.71 3.98 8.49 2.72 0.37 0.99 3.45 0.71 13.57 35.2 14.9 55.72 9.648.14 9.10 21.20 7.69 13.58Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-4S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 4 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 102/28/03 01/19/05 04/21/05 07/18/05 10/20/05 01/30/06 07/25/06 01/30/07 07/12/07 01/29/08 07/16/08 01/28/09 07/28/0901/12/10 07/21/10 01/19/11 07/13/11 01/25/12 07/12/12 01/24/13 07/01/1306/12/14 12/11/14 09/18/15 03/22/16 09/23/16 03/29/17 09/22/17 03/14/18 10/05/186230D 601 601 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 NS <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 NA NA NA NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS <1.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.06.5NANANANANANANA<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA NA NA NA NA NA NA NA1.8NANANANANANANA<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5<2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 0.27J <1.0 2.6 2.6 <1.0 2.6 <1.0 3.2 1.9 5.0 1.9 4.3 <1.0 3.4 1.7 7.7 5.1 4.9153.1 NS 4.0 3.1 3.1 2.8 1.3 2.5 1.9 1.91.5<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.026 6.6 30 76 62 16 67 2.5 73 44 150 39 100 1.6 81 28 140 100 100 100 63 NS 118 85.7 59.3 69.3 26.2 69.7 50.4 47.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.61 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 NS <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS <5.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 NS <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.01.7NANANANANANANA<5.0<5.0<5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.2<1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.63 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.95 <1.0 <1.0 1.9 <1.0 <1.0 0.65J <1.0 1.6 <1.0 2.1 <1.0 1.7 <1.0 0.95 <1.0 1.1 <1.0 <1.0 2.5 <1.0 NS <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 0.36 <1.0 <1.0 <1.0 <1.01.6<1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0 1.2 <1.0NS<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NS<1.0NANANANANANANA<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NS<1.0NANANANANANANAND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.03.4NANANANANANANA<3.0<3.0<3.0 <3.0<3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0<3.0 <3.0 NS <1.0 <3.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA NA8.8 7.3 9.5 107.7<4.012<3.015 20 19 12 10NS6.2 3.9 5.4 4.12.83.4 3.92.211,000 9,400 11,000 14,000 18,000 10,000 16,000 6,300 12,000 12,000 13,000 12,000 NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA 43,000 21,000 24,000 8,10022,000 5,700 12,000 8,900<5,000 10,000 <5,000<5,000 NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA 3,100 4,300 6,800 8,000 3,800 6,5006,200 6,400 4,700 7,500 4,600 NA NA NANA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA 4,800 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA <26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA NA <1,000 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA <0.1 NM NM 0.2 <0.1 <0.2 <0.2 <0.2 <0.2 0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NS NANANANANANANANA NM NM 45 271 435 343 402 253 391 337.7 69.271.4 170.4 150.5 274.6 55.2 159.5 175.6 141.0 337.3 472.5 NS 353.0 317.420.1 27.1 366.9 225.8 101.8 87.112.1 13.9 15.4 16.9 18.6 15.6 16.6 13.2 16.4 16.1 17.4 15.8 16.8 13.6 25.3 14.9 17.3 15.7 16.6 14.4 17.4 NS 14.318.1 14.4 21.2 16.3 19.5 9.1 18.55.84 4.07 5.55 4.76 4.89 4.40 4.45 5.33 4.68 4.35 4.355.12 4.14 4.81 4.74 5.21 4.90 4.89 4.93 4.39 3.41 NS 3.73 4.60 4.80 4.56 4.34 4.46 4.94 4.27143.3 96.6 128.0 119.4 149.1 132.5 120127 129.7 103 110 100 97 108 131 94 130 124 121 88 109 NS 131 128 125.7 125.2 124.9 102.2 121.4 140.84.17 NM 3.15 2.14 2.82 3.323.65 5.04 3.95 3.39 2.79 4.24 0.85 0.54 0.94 3.69 0.93 1.78 1.91 3.33 1.95 NS 5.19 3.30 0.95 1.10 4.86 2.24 3.51 1.94NM NM NM NM NM NM NM NM NM 2.2 1.67 4.95 294.7 107.2 >1,100 67.44 40.32 37.04 28.7 22.19 NM NS 37.00 136 122.8 27.2 4.5 308.0 214 669.2Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointSoutheast of BuildingMW-5S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 5 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 102/28/03 01/19/05 04/21/05 07/18/05 10/20/05 01/30/06 07/25/06 01/30/07 07/12/07 01/29/08 07/16/08 01/28/09 7/28/09 1/12/10 7/21/10 1/19/11 7/13/11 1/25/12 7/11/12 1/24/13 7/1/13 6/13/14 12/11/14 9/18/15 3/22/16 9/23/16 3/29/17 9/22/17 3/14/18 10/5/186230D 601 601 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <100 <50 <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <2.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <1.0<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0<1.0<1.0NANANANANANANANA<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0<1.0<1.0NANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0<5.0 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 0.71 0.38J 0.38J <10 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5<2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <5.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.018 6.0 <1.0 <1.0 3.2 3.29.633.33.620<1.0 3.8 1.517 21 13 8.42.2 4.411 6.8 9.82.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.01.2<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.36 0.32J <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0210 99 36 35 63 48 150 49 56 70 240 15 50 25 240 330 56 170 45 110 180 93 186 59.4 8.4 19.9 12.9 <1.0 1.9 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <20 <10 <10 <10 <10 <10.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA NA NA NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <20 <10 <10 <10 <10 <10.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.53 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.01.1<1.0 <1.0 <1.00.82 1.7 1.2<2.0 <1.0 <1.0 <1.0 <1.01.1<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.09.2 1.8 <1.0 <1.0 <1.0 0.77J 1.2 1.2 <1.0 <1.0 2.3 <1.0 <1.0 <1.0 1.2 1.6 1.2 <2.0 <1.0 1.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.1<1.0 <1.0 <1.0 <1.0 <1.01<1.0 <1.0 <1.02.1<1.0 <1.0 <1.01.9 2.3 1.4<2.0 <1.0 <1.01.1<1.01.1<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.86 <1.0 <1.0 <1.0 <1.0 <1.0 0.95J <1.0<1.0 <1.0 1.3 2.1 <1.0 <1.0 1.1 1.5 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <5.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANA<0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANAND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <3.0 <3.0<3.0 <3.0<3.0 <3.0<3.0 <3.0 <3.0 <6.0 <3.0<3.0 <3.0 <3.0 <1.0 <3.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA NA8.6 15 83 8.417<4.0140 73 29 32 13 50 37 43 30.1 9.8 4.62.6 2.4 <2.0 <2.0 <2.026,000 12,000 11,000 13,000 13,000 13,000 17,000 12,000 11,000 15,000 31,000 30,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA10,000 16,000 21,000 20,00025,000 3,300 15,000 <5,000 6,400 12,000 <5,000 7,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA 4,400 3,300 4,700 5,100 5,500 9,5005,800 5,400 7,400 17,000 20,000 NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA4,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA <1,000 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA1.0 NM NM <0.2 <0.1 <0.2 <0.2 <0.2 <0.2 0.4 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NANANANANANANANANM NM 147 321 462 345 361 318 465 372.9 46.854.0 165.0 177.0 182.5 48.9 202.5 223.4 169.9 355.9 404.8 568 420 363.5 -73.4 92.6 122.6 253.9 21.4 118.912.7 13.3 15.9 16.3 18.0 14.9 17.5 13.5 16.7 15.7 17.5 15.4 17.5 13.5 23.7 15.2 17.2 16.2 16.8 15.1 19.8 19.3 14.319.3 17.1 21.4 16.9 21.6 12.3 19.04.79 4.16 4.96 4.39 4.60 4.40 4.78 4.81 4.42 4.19 4.265.27 4.13 4.18 4.48 4.37 4.31 4.04 4.39 4.20 4.03 2.36 3.28 4.14 5.28 3.90 3.59 4.16 4.42 3.79163.7 82.6 111.7 125.1 130.5 132.1118 132 129.2 109 151 139 175 187 197 152 161 149 137 106 138 385 150 142 227.1135.1 146.3 106.1 128.1 165.73.98 NM 3.67 2.26 2.68 3.843.94 4.06 3.82 2.97 0.81 2.54 1.06 2.04 1.17 2.05 2.19 3.02 3.31 2.10 2.20 0.18 3.90 2.94 0.34 2.89 1.99 2.82 2.16 2.32NM NM NM NM NM NM NM NM NM 5.9 1.27 1.71 3.75 2.89 4.85 1.61 0.00 0.57 4.05 10.10 28.90 14.2 13.6 5.90 4.85 8.87 26.20 6.72 10.20 10.89Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-6Southeast of BuildingS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 6 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 102/28/03 11/19/03 01/19/05 04/21/05 07/18/05 10/20/05 01/30/06 07/24/06 01/31/07 07/12/07 01/29/08 07/16/08 01/29/09 7/27/09 1/12/10 7/20/10 1/18/11 7/13/11 1/24/12 7/11/12 1/24/13 7/2/13 6/12/14 12/10/14 9/18/15 3/22/16 9/23/16 3/30/17 9/22/17 3/14/18 10/5/186230D 6230D 601 601 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA NA NA NA NA <50 <50 <50 <50 <250 <50 <50 <50 <50 <50 <50 <50 <50 <50 <20 <25.0 <25.0 <25.0 <50.0 <25.0 <25.0 <25.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<2.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <25 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0 <2.0 <4.0 <2.0 <2.0 <2.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANANA<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<2.0<1.0<1.0<1.0ND ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 <1.0 0.57J <1.0 <1.0 0.66J ND <1.0 <5.0 <5.0 <5.0 <5.0 <25 <5.0 1.7 0.99J <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 2.8 2.5 1.7 2.3 2.3 2.5 2.8 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5 <2.5 <12 <2.5 <2.5<2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0<1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.030 47 21 31 20 21 23 23 23 20 12 14 7.2 14 29 8.6 9.2 10 5.2 125.29.7 9.8 10.2 18.2 29.2 31.5 25.2 20.0 19.2 16.02.9<0.51.7 2.0 1.2<1.0 <1.01.0 2.2<1.01.5 1.5<1.0 <5.05.7 1.7 1.7 1.8<1.02.4 1.0 1.9 2.0 2.2 3.3 4.5 5.0 4.8 3.1 3.8 2.7460340 280 170 210 270 220 260 300 190 190360110 310690150 160 170 100 240 110 160 95 137 175 144 159 172 140 172 99.31.4 0.76 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 1.8 <1.0 0.50J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.00.56 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <5.0 1.4 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0<1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA NA NA <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 <5.0<2.0 <2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <25 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0 <2.0 <4.0 <2.0 <2.0 <2.0NA NA NA NA NA NA NA NA NA <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <10.0 <5.0 <5.0 <5.0<0.5 <0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.00.690.72<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0<1.0<2.0<1.0<1.0<1.01.2 <0.5 <1.0 0.61J <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <5.0 3.9 1.8 0.91J 1.8 <1.0 1.4 <1.0 1.2 <1.0 <1.0 1.7 7.2 5.0 4.2 4.2 1.5 <1.01.7<0.51.3 0.80J<1.0 <1.0 <1.01.7 1.1<1.0 <1.0 <1.0 <1.0 <5.03.9 1.1 1.3 1.3<1.01.8<1.01.6<1.01.4 2.3 3.7 3.9 4.3 2.6 2.8 3.82.8 2.2 1.8 2.3 1.3 2.43.82.9 1.7 1.2 <1.0 <1.0 <1.0 <5.0 2.1 0.37 0.65J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.052 33 37 28 24 26 14 21 15 10 12 11 6.7 <25 17 17 8.5 20 5.7 8.1 2.8 9.0 <5.0 5.7 6.1 7.85.25.74.75.2<1.0ND ND NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0<1.0<2.0<1.0<1.0<1.0<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0NANANANANANANA<0.5 <0.5 NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0NANANANANANANAND ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0<1.0<0.5 <0.5 NA NA NA NA NA NA NA <3.0 <3.0<3.0 <3.0<15.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <1.0 <3.0<2.0 <1.0 <2.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA NA NA26 12 22 1322 26 35 19 10 15 30 13 16 18 11.7 17.9 23.3 24.4 25.4 18.4 35.6 24.175,000 NA 99,000 100,000 100,000 100,00049,000 63,000 51,000 65,000 68,000 68,000 61,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 7,300 NA 26,000 26,000 37,000 15,00011,000 12,000 8,500 15,000 25,000 12,000 21,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 72,000 54,000 68,000 55,000 35,000 43,000 37,000 44,000 48,000 45,000 45,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 5,700 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1,280 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <0.1NMNMNM<0.20.2<0.2<0.2NM<0.2<0.2<0.1<0.1NANANANANANANANANANANA NA NA NA NA NA NA NA NM NM NM 76 209 363 293 173 269 332 318.1 20.1 29.6 65.1 -105.1 285.6 -36.4 154.9 296.5 131.0 285.5 351.0 218 378 227.6312.3 201.6 99.6 261.8 525.3 -106.514.3 18.2 10.3 17.4 19.4 20.3 15.9 19.6 14.1 19.5 15.2 19.5 12.5 21.9 13.7 20.3 11.3 20.8 14.9 21.4 14.121.6 18.8 16.9 27.9 17.427.1 13.2 25.8 11.3 24.85.16 5.17 4.83 5.67 5.18 5.08 5.02 5.22 5.35 4.99 4.764.68 6.01 4.70 4.70 4.63 5.00 4.72 4.42 4.84 4.52 4.51 5.02 3.89 4.56 4.92 4.76 4.65 4.68 4.88 4.85329.0 NM 279.5 389.2 440.5 395.0 240.8 338 263 310.9 281 283 229 276 269 380 285 351 347 313 222 299 307 318 307 412.5367.3 386.7 337.6 316.1 285.71.81 1.19 NM 2.12 1.37 2.182.15 2.05 2.46 1.08 1.72 1.13 3.02 1.74 1.73 0.72 2.18 0.78 2.42 0.46 0.65 0.43 0.44 2.44 0.67 0.51 0.43 0.38 0.32 0.37 0.19NM NM NM NM NM NM NM NM NM NM 5.3 4.31 3.05 2.03 8.02 7.27 5.84 0.29 0.34 8.5 8.10 8.04 0.0 47.5 17.9 32.7 22.3 15.9 7.00 75.83 4.12Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-7South of Building Near Drainage FeatureS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 7 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 106/12/03 11/19/03 01/19/05 03/14/05 04/21/05 07/19/05 10/21/05 01/31/06 07/25/06 01/31/07 07/12/07 12/08/07 01/30/0804/29/08 07/16/08 10/14/08 01/29/09 7/28/09 10/20/09 1/13/10 4/7/10 7/21/10 10/19/10 1/20/11 7/14/116230D 6230D 601 601 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260B 8260B 8260B 8260 8260B 8260B 8260B 8260BNA NA NA NA <1,000 <10,000 <4,000 <40,000 <40,000 <50,0009,0002,000 1,600 <5,000 <500,000 <120,000<5,000 <50,000 <120,000 1400 <250,000 <250,000 <250,000 <100,000 <50,000<50 <50 NA NA97J<1000 <400 <4,000 <4,000 <1,000460 380 120 100<10,0003,000 150 1,500<2,500120<14001,100<5,000150<1,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,000 NA <20 NA NA NA <2,500 NA NA <2,500 NA NA NA NA NA NA<50 <50 <400 <400 <100 <1000 <400 <4,000 <4,000 <1,000 <1.0 <20 1.8 <100 <10,000 <2,500 <100 <1,000 <2,500 <201.0<5,000 <5,000 <20 <1,000ND ND ND ND ND ND ND ND ND ND <1.0 <202.2<100 <10,000 <2,500 <100 <1,000 <2,500 <20 <1.0 <5,000 <5,000 <20 <1,000<50 <50 <2,000 <2,0002,400 4,400 1,200<12,000 <12,000 <1,00050<100 <5.0 <500 <50,000 <5,000 <500 <5,000 <5,000 <10013<1,000,000 <25,00089J<5,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,000 <1.0 <20 <1.0 <100 <10,000<2,500 <100 <1,000 <2,500 <20 <1.0 <5,000 <5,000 <20 <1,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,000 <1.0 <20 <1.0 <100 <10,000<2,500 <100 <1,000 <2,500 <20 <1.0 <5,000 <5,000 <20 <1,000NA NA NA NA <500 <5000 <2000 <20,000 <20,000 <1,000 NA NA NA NA NA NA NA NA NA NA NANANANANA<502,100<400 <400 <200120,000<800 <8,000 <8,000 <1,000 <1.0 <208,800 7,500<10,000 <2,500 <100 <1,000 <2,500<20 <1.0 <5,000 <5,000 <20 <1,000ND ND ND ND ND ND ND ND ND ND95 6431 <100 <10,000 <2,500 <100 <1,000 <2,500 40 38 <5,000 <5,000 35 <1,000ND ND ND ND ND ND ND ND ND ND 130 140 86 <500 <50,000 <5,000 <500 <5,000 <12,000 <100 51 0 <25,000 <100 <5,0001,600 420<400 <400220<1000 <400 <4,000 <4,000 <1,000160 190 99<500 <50,000 <5,000 <500 <5,000 <12,000130<25,000 <25,000 <25,000130<5,000<50 <50 <2,000 <2,00015,000 39,000 22,00017,000 35,000 50,000<1.016,000 8,800 9,100<25,00020,000 9,200 5,800 7,800 3,700 3,800 15,000<13,0002,800 2,800<50 <50 <400 <400 <100 <1000 <400 <4,000 <4,000 <1,000 <1.0 <20 <1.0 <100 <10,000 <2,500 <100 <1,000 <2,500<20 0.7 <5,000 <5,000 <20 <1,000<50 <50 <400 <400 92J <1000 <400 <4,000<4,000 <1,000 110 42 34 <100 <10,000 <2,500 <100 <1,000 <2,50071 73<5,000 <5,00090<1,000ND ND ND ND ND ND ND ND ND ND 3.6 <20 1.2 <100<10,000 <2,500 <100 <1,000 <2,500 <20 2.7 <5,000 <5,000 <20 <1,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,000 <1.0 <20 2.0 <100 <10,000 <2,500 <100 <1,000 <2,500 <1004.7 <5,000 <5,000 <20 <1,00014,000 18,000 24,000 1,100 25,000 35,000 18,000 6,900 22,000 27,000 24,000 13,000 7,700 6,700 17,000 18,000 13,000 13,000 16,000 10,000 16,000 47,000 12,000 13,000 14,0003,800 14,000 7,500 3805,200 6,700 3,300<4,0004,300 5,100 4,000 2,900 1,500 1,600<10,0003,400 2,800 2,900<2,5002,200 2,900 9,300<5,0002,400 2,00099,000 230,000 390,000 460 380<1000 <400 <4,000 <4,000 <1,0008,400 1,900 1,200 830<10,000 <2,5001,400 24,000 4,500 4,400 12,000 27,000 26,000 22,000 12,000240 580<400 <400310<1000 <400 <4,000 <4,0002400 260 170 89<100 <10,000 <2,500 <100 <1,000 <2,500110<5,000 <5,000 <5,000110<1,000<50940<400 <400 64J <1000 <400 <4,000 <4,000<1,000 47 39 <1.0 <100 <10,000 <2,500<100 <1,000 <2,500 27 49 <5,000 <5,000 26 <1,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,00022<2010<100 <10,000 <2,500 <100 <1,000 <2,500 <2018<5,000 <5,00016J<1,000ND ND NA NA ND ND ND ND ND ND50 28 14<100 <10,000 <2,500 <100 <1,000 <2,50029 31<5,000 <5,00031<1,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,000 <1.0 <20 <1.0 <100 <10,000<2,500 <100 <1,000 <2,500 <20 0.48 <5,000 <5,000 <20 <1,000NA NA NA NA ND ND ND ND ND ND <10 1,500 970 <100 <10,000 <2,500 <100 <1,0000 <2,500 610 <10 <50,000 <50,000 <200 <10,000<200 <200 <2,000 <2,000100J<1000 <400 <4,000 <4,000 <1,000400 240 130<500 <50,000 <5,000 <500 <5,000 <12,000230<25,000 <25,000 <25,000260<5,000NA NA NA NA ND ND ND ND ND ND 17 <200 <10 <1,000 <100,000 <10,000 <1,000 <10,000<25,000 <200 11 <25,000<25,000 <100 <5,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,000 <5.0 <20 <5.0 <500 <50,000<5,000 <500 <5,000 <12,000 <1000.61 <25,000 <25,000 <100 <5,000<50 <50 <400 <400 <100 <1000 <400 <4,000 <4,000 <1,000360 230 140 100<10,000 <2,500240<1,000 <2,500260<5,000 <5,000 <5,000240<1,000ND ND ND ND ND ND ND ND ND ND41<203.0<100 <10,000 <2,500 <100 <1,000 <2,50021 35<5,000 <5,00025<1,00076 130<400 <40079J<1000 <400 <4,000 <4,000 <1,00082 38 26<100 <10,000 <2,500 <100 <1,000 <2,50052 48<5,000 <5,00055<1,0006,000 11,000NA NA 60J <1000 <400 <4,000 <4,000 <1,000 <5.0 <100 22 <500 <50,000 <5,000 <500 <5,000 <12,000 <100 <25,000 <5,000 <5,000 230 <5,000ND ND NA NA ND ND ND ND ND ND 2.1 <20 <1.0 <100 <10,000 <2,500 <100 <1,000 <2,500<20 <1.0 <5,000 <5,000 <20 <1,000<50 <50 NA NA <100 <1000 <400 <4,000 <4,000 <1,000 <1.0 <20 <1.0 <100 <10,000<2,500 <100 <1,000 <2,500 <20 <1.0 <5,000 <5,000 <20 <1,000410,000 390,000 330,000 68,000 450,000670,000 350,000 75,000 440,000 490,000 360,000 270,000 66,000 54,000240,000 180,000 250,000 320,000 190,000 100,000 210,000 470,000200,000 220,000 220,0001,200 3,100<400 <4002,900 4,600 1,900<4,0003200J 5,100 4,400 2,200 1,500 1,100<10,000 2,7003,300 3,600 2,900 2,000 3,700 11,000 2,400J 3,100 2,300190 480<400 <40080J<1000 <400 <4,000 <4,000 <1,00075 36 24<100 <10,000 <2,500 <100 <1,000 <2,50070 74<5,000 <5,00070<1,000<50 <50 <2000 <2000 <200 <2000 <800 <8,000 <8,000 <1,000 <1.0 <100 <5.0 <500<50,000 <5,000 <500 <5,000 <12,000 <100 <5.0 <25,000 <25,000 <100 <5,000ND ND NA NA ND ND ND ND ND ND11<20 <1.0 <100 <10,000 <2,500 <100 <1,000 <2,500 <20 <1.0 <5,000 <5,000 <20 <1,000<50 <50 NA NA <100 <1,000 <400 <4,000 <4,000 <1,000 <1.0 <20 <1.0 <100 <10,000 <2,500 <100 <1,000 <2,500 <20 <1.0 <5,000 <5,000 <20 <1,000<50 <50 NA NA <100 <1,000 <400 <4,000 <4,000 <1,000 <1.0 <20 <1.0 <100 <10,000 <2,500 <100 <1,000 <2,500 <20 <1.0 <5,000 <5,000 <20 <1,000ND ND ND ND ND ND ND ND ND ND8.4<20 <1.0 <100 <10,000 <2,500 <100 <1,000 <2,500 <203.5<5,000 <5,000 <20 <1,000<50 <50 NA NA <300 <3000 <1200 <8000 <8000 <3000 <3.0 <60 <3.0<300 <30,000 <3,000 <300<3,000 <7,500 <60 <3.0 <15,000 <15,000 <60 <3,000NA NA NA NA NA NA NA NA NA NA <1000 NA7,800NA1,600NA7,0004,300 10,000 6,300 5,0007,700 9,500 6,200 4,1002,200,000NA300,000 1,400,000 2,800,000 2,500,000 2,300,0001,300,000 2,100,000 2,500,000 2,700,000NA 150,000 NA2,600,000NA2,200,000 2,400,000NA1,600,000NA2,400,000NA2,000,000 2,000,00016,000 NA 1929,000,000 3,100,000 2,200,000 2,000,000 5,000,000 2,700,000 3,400,000 3,400,000NA3,400,000 2,500,000 3,600,000 3,400,000 3,400,000 5,100,000 4,200,0003,200,000 4,500,000 4,800,0004,000,000 3,800,000 4,000,000NA NA 37 29,000,000 5,700,000 2,600,000 2,900,000 4,200,000 2,200,000 1,400,000 440,000 1,400,0004,200,000 3,300,000 2,100,000 2,000,000 2,500,000 2,400,000 2,000,000 540,000 2,100,000 2,100,000 2,000,000 2,400,000 1,900,000NA NA NA790,000NA NA NA NA NA NA NA <1,8006,800.0 750.00<2,000 430,000 <1,000 <2,000 <100 <100440 1,100 540J<5,000 <1,0003,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA66,000 NA NA NA NA NA 311,000 NA NA NA NA NA NA NANA NA NANA NA NA NA NA NA NA NA2.2 NM NM NM NM <0.1 0.4 <0.2 <0.2 <0.2 <0.2 NA 0.4 NA <0.1 <0.1 <0.1 NA NA NA NA <0.1 <0.1 <0.1 <0.1NM NM NM NM 246 499 494 379 433 526 500 447.1 218.8 144.0 443.5 502.3 428.3 514.6 405.0 221.7 432.7 513.5 480.8 7.0 421.325.6 NM 18.7 19.5 23.8 22.322.3 21.0 22.2 21.2 24.921.9 20.6 22.5 24.6 23.5 21.5 26.9 22.2 20.0 22.0 25.9 24.3 20.6 23.55.37 NM 3.77 11.2 7.82 3.44 3.94 4.05 3.54 3.7 3.30 3.74 7.95 6.47 3.69 3.46 4.45 3.41 4.45 5.94 3.823.14 3.70 3.56 3.571,742 NM 608.0 47,000 25,190 13,220 9,680 15,260 NM 1,170 11,690 10,960 15,040 10,550 11,640 10,950 11,990 11,06011,740 12,300 12,070 12,200 10,84010,540 10,7200.62 NM NM NM 2.68 0.07 0.66 NM NM 0.98 5.27 NA 13.97* 16.24* 37.07* 1.25 26.65* 18.13 2.52 8.05 2.636.23 20.85* 2.94 33.62*NM NM NM NM NM NM NM NM NM NM NM 3.19 15 2.12 26.33 5.45 37.59 110.6 NA 35.27 159.52.45 1.53 3.20 5.29Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-8Knife Room (Source Area)S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 8 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 11/24/12 7/11/12 1/25/13 7/2/13 6/11/14 9/16/14 12/9/14 3/13/15 9/17/15 3/21/16 9/22/16 3/29/179/22/17 3/13/18 10/4/1806/12/03 01/19/05 04/21/05 07/19/05 07/02/13 06/12/14 09/16/14 12/09/1403/13/15 09/17/15 03/21/16 09/23/16 03/29/17 09/21/17 03/13/18 10/04/188260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 6230D 601 601 601 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B<100,000 <2,500 <100,000 <50,000 <250,000 <250,000 1,240 222 381 <1250 <2500 <2500 <5000 <5000 <5000 NA NA NA NA <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<2,000420<2,000 <1,000 <5,000 <5,000355 35.6 49.8<50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA 30.2 <1.0 5.9 <50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,0004.2<1.0 <1.0 <50.0 <100 <100 <200 <200 <200 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000 <1.0 <1.0 <1.0 <50.0 <100 <100 <200 <200 <200 ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<10,000 <250 <10,000 <5,000 <25,000 <25,00085.4 14.9 29.3<100 <200 <200 <400 <400 <400 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<2,000 <50 <2,000 <1,000 <5,000 <5,000 NA NA NA NA NA NA NA NA NA <0.5 NA NA NA <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA<2,000 <50 <2,000 <1,000 <5,000 <5,000 NA NA NA NA NA NA NA NA NA <0.5 NA NA NA <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NANANANANANANA<10.0NANANANANANANANANANANANANANANANANANANANANANANANA<2,000 <50 <2,000 <1,000 <5,000 <5,000 <1.0 <1.08.8<1.0 <100 <100 <200 <200 <200 <0.5 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <50.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000 98.1 8.2 20.1 <50.0 <100 <100 <200 <200 <200 ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<10,000 <250 <10,000 <5,000 <25,000<25,000 34.0 3.6 9.7 <50.0 <100 <100 <200 <200 <200 ND ND ND ND <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<10,000260<10,000 <5,000 <25,000 <25,00013727.3 60 <50.0 <100 <100 <200 <200 <200 <0.5 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0<1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0<2,0003,200<5,000 <2,500 <12,000 <12,00071,300 547 686 728 1,050 1,050 1,020 831 699<0.5 <5.0 <5.0 <5.0 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,0002.3 <1.0 1.4 <50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,00083<2,000 <1,000 <5,000 <5,00010416.459.6<50.0 <100 <100 <200 <200 <200 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000 NA <1.0 2.9 <50.0 <100 <100 <200 <200<200 ND ND ND ND <1.0 <1.0 <1.0 NA <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,0006.41.1 3.9 <50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.016,000 10,000 7,200 13,00014,000 10,000 14,700 1,8703,950 2,750 2,710 3,800 4,140 3,720 4,390<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.4 1.5 <1.0<1.0 <1.0 <1.0 <1.0 <1.02,400 4,500<2,0001,900<5,000 <5,000 <10,000301 661 460 431 628 714 673 590<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.017,000 13,000 16,000 23,000 18,000<5,000 <10,000 220516 358 826 1,390 2,010 1,960 2,770<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 1.2<2,000260<2,000 <1,000 <5,000 <5,000 98.0 13.5 21.2 <50.0 <100 <100 <200 <200 <200 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000220<2,000 <1,000 <5,000 <5,000 <1.0 <1.0 4 <50.0 <100 <100 <200 <200 <200 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,00018.5<1.06.4<50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000 NA4.8 13.3<50.0 <100 <100 <200 <200 <200 ND NA NA NA <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000 <1.0 <1.0 <1.0 <50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<20,000 630 <20,000 <10,000 <50,000 <50,000 <10.0 52.1 85 <250 <500 <500 <1000 <1000 <1000 NA NA NA NA <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0<10,000460<10,000 <5,000 <25,000 <25,000199 61.7 133 107<200 <200 <400 <400 <400 <2.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0 <2.0<2.0<2.0<2.0<2.0<2.0<10,000 <500 <20,000 <5,000 <50,000 <50,000 <10.0 <5.0 <5.0 <250 <500 <500<1000 <1000 <1000 NA NA NA NA <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<10,000 <250 <10,000 <5,000 <25,000 <25,000 NA <1.0 <1.0 <50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <5.0 <5.0 <5.0NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000230<2,000 <1,000 <5,000 <5,000255 51.6 195 74.9<100255 <200 <200<200 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<2,000 <50 <2,000 <1,000 <5,000 <5,00026.4 2.0 6.0<50.0 <100 <100 <200 <200 <200 ND ND ND ND <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,00067<2,000 <1,000 <5,000 <5,00073.5 12.0 37.9<50.0 <100 <100 <200 <200 <200 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<10,000650<10,000 <5,000 <25,000 <25,000 6.1 4.926 <50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000NA <1.0 <1.0 <50.0 <100 <100 <200 <200 <200 ND NA NA NA <1.0 <1.0 <1.0 NA <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000NA <1.0 <1.0 <50.0 <100 <100 <200 <200 <200 <0.5 NA NA NA <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0310,000 230,000 86,000 260,000 330,000200,000 393,000 9,130 14,900 8,550 13,100 19,200 28,200 20,200 24,900<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1 114 41.5 13.2 6.8 4.8 3.6 1.7 3.93,100 2,800<2,0002,500<5,000 <5,000 <10,000288 739 504 402 709 652 675 657<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.5<1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0<2,00093<2,000 <1,000 <5,000 <5,00077.1 8.2 21.4<50.0 <100 <100 <200 <200 <200 <0.5 <1.0 0.74J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<10,000 <250 <250 <5,000 <25,000 <25,000 <1.0 <1.0 <1.0 <50.0 <100 <100 <200 <200 <200 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <120 <2,000 <1,000 <12,000 <12,000 9.4 1.34.3<50.0 <100 <100 <200 <200 <200 ND NA NA NA <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<2,000 <50 <2,000 <1,000 <5,000 <5,000 <1.0 NA NA NA NA NA NA NA NA <0.5 NA NA NA<1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA<2,000 <50 <2,000 <1,000 <5,000 <5,000 <1.0 NA NA NA NA NA NA NA NA <0.5 NA NA NA<1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA<2,000 <50 <2,000 <1,000 <5,000 <5,000 <1.0 <1.02.3<50.0 <100 <100 <200 <200 <200ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<6,000 <150 <6,000 <3,000 <15,000 <15,000 <1.0 <2.0 <3.0 <100 <100 <100 <200 <200 <200 <0.5 NA NA NA<3.0 <3.0 <3.0 <1.0 <2.0 <2.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.05,200 4,000 5,500 4,900 5,100 2,300 3,090 1,360 3,790 2,680 2,270 3,180 3,810 3,880 4,740NA NA NA NA9.4 15 11 8.5 12.7 7.87.15.28.05.88.06.72,100,000 2,000,00017,0001,800,000 1,800,000 1,800,000 1,930,000 406,000 1,030,000 708,000 622,000 851,000 1,100,000976,000 1,000,000NA 71,000 60,000 96,000 76,000 75,00058,000 68,200 65,200 65,400 60,800 74,800 71,800 103,000 71,400 88,5003,800,000 3,800,000 3,900,000 3,400,000 5,000,000 7,700,000 4,300,000869,000 2,140,000 1,670,000 1,230,000 1,730,0001,940,000 1,780,000 2,060,000370,000 3,300 10,000 15,000 120,000 13,000 10,000 7,100 8,000 5,000 5,9004,900 6,300 8,000 7,200 7,1001,700,000 1,500,000 1,600,000 1,600,000 3,600,000 2,700,000 3,020,000740,000 1,380,000 1,160,000 880,0001,020,000 985,000 1,300,000 1,210,000 NA 42,000 41,000 57,000 47,000 58,000 37,000 38,600 36,100 42,200 31,000 40,800 50,400 56,000 40,400 48,0001000.0<1,000 <1,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 5,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA1,620 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.1 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NA NA 1.2 NM NM 0.2 NA NA NA NA NA NA NA NA NANANANA512.0 323.7 480.1 503.0 550 518 463 329561.3 348.1 138.2 156.2 582.9 415.8 488.3 NM NM 166 278 394.5 232 145 407 399 324.6 307.2 -46.7 319.7 154.9 131.2 119.221.0 23.7 21.0 24.6 28.9 24.3 22.9 20.5 24.5 20.2 27.0 20.6 24.6 19.5 26.5 18.6 15.1 18.3 19.6 21.6 20.922.0 18.0 14.5 23.1 17.922.5 20.1 27.0 16.4 22.13.04 3.42 3.61 3.34 2.21 3.69 2.89 6.13 4.27 5.04 4.173.54 3.89 4.23 3.72 5.01 4.47 5.36 4.38 3.56 4.63 4.61 4.07 4.67 6.56 5.23 5.46 4.40 4.32 4.70 4.0410,670 9,853 7,630 9,18832,300 16,580 15,400 3,9257,784 5,022 4,799 6,895 7,173 6,902 7,202 148.0 255.0 337.0440.1 362.0 371 347 333 255 351 284.5 355.9 384.2 428 347.5 419.71.36 36.17 10.85 1.27 0.31 0.93 1.80 0.36 0.33 0.86 0.28 0.36 0.36 0.47 0.20 2.52 NM 3.04 3.43 0.49 0.21 0.69 2.51 2.66 0.70 3.57 1.59 2.83 0.32 2.34 1.222.48 1.20 1.05 6.40 82.0 8.5 26.4 6.9 18.3 59.2 24.6 4.9 38.8 7.0 5.48 NM NM NM NM 0.06 0.0 0.0 0.2 0.7 0.38 2.46 6.37 0.51 2.63 0.78 3.27Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-8RKnife Room (Source Area)MW-9SW Corner of BuildingMW-8 (Cont'd)Knife Room (Source Area)S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 9 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 106/12/03 01/19/05 03/14/05 04/21/05 07/19/05 10/20/05 01/30/06 07/25/06 01/31/07 07/12/07 01/30/08 04/29/08 07/16/08 10/14/08 01/29/09 7/28/09 10/20/09 1/13/10 4/7/10 7/21/10 10/19/10 1/19/11 7/14/11 1/25/12 7/11/12 1/25/13 7/2/13 6/12/14 9/16/14 12/10/14 3/13/15 9/17/15 3/21/16 9/22/16 3/29/17 9/22/173/14/18 10/4/186230D 601 601 601 601 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260B 8260B 8260B 8260 8260 8260 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8620B 8260B 8260B 8260BNA NA NA NA NA <100 <1000 <1000 <50 <50 <50 <250 <250 <250 <50 <50 <50 <50 <50 <50<50 <50 <50 <50 <50 <50 <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <50.0 <25.0 <50.0<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<2.0<1.0<2.0<0.5 NA NA NA NA <10 <100 <100 NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 <10 <10 <10 <10 <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.04.5<1.05.3<1.0 <1.0 <2.0 <1.0 <2.0<0.5 <50 <50 <50 <50 <50 <500 <500 <5.0 <5.0 <5.0 <25 <25 <25 <5.0 <5.0 <5.0 <5.0<5.0<5.0<5.0<5.0<5.0<5.0<5.0<5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0 <2.0 <2.0 <1.0 <4.0 <1.0 <4.0<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NANA NA NA NA NA <50 <500 <500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA<0.5 <10 <10 <10 <10 <20 <200 <200 <1.045<1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 <1.0 <2.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0<1.0 <2.0ND ND ND ND ND ND ND ND ND <1.0 <5.0 <25 <25 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <2.0 <1.0<2.08.9 <10 <10 <10 <10 <10 <100 <100 <5.0 5.3 <5.0 <25 <25 <25 <5.0 <5.0 <5.0 <5.0 2.6 2.6 2.3J 2.3J <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 2.3 2.9 2.8 2 1.7 2.2 2.4 <1.0<2.0<0.5 <50 <50 <50 <50 <50 <500 <500 2.735<2.5 <12 <12 <12 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 1.7 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 NA NA NA NA <10 <100 <100 1.4 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <2.0 <1.0 <2.02.7 <10 <10 <10 <10 <10 <100 <100 <1.0 1.8 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<2.0<1.0<2.0310 230 200 220 260 270 250 140 85 160 14 12 21 123.2 3.2 2.3 2.5 4.9 5.9 5.2 3.1 4.1 3.66.73.3 5.918 16 22.1 99.6 40.0 74.530.1 35.9 41.7 9.4 22.747 38 18 34 43 60<100 <10014 33<5.0 <5.0 <5.0 <5.0<5.0 <1.0 <1.0 <1.01.4 1.1 1.0 0.93<1.0 <1.01.3<1.01.2 3.5 2.4 4.3 13.9 7.0 10.5 4.2 6.2 7.4 1.8 4.96,200 4,800 3,700 3,4004,200 5,200 5,100 3,100<1.02,000290 240480310 79 55 63 68 87 130 120 60 100 81 160 71 130 190 33 232 28.4 288.0 55.2 137 171 282 95.9 13420 16 14 12 16 21 <100 <100 2.5 <20 1.1 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.46 0.44J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.2 <1.0 1.5 1.6 2.0 1.3 <1.0 <1.0 <2.0 <1.0 <2.015 <10 <10 <10 <10 <10 <100 <100 <1.0 4.1 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<2.0<1.0<2.0ND NA NA NA NA ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<2.0<1.0<2.0NA NA NA NA NA ND ND ND ND <10 <10 <50 <50 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10<10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10.0 <5.0 <10.0<2.0 <50 <50 <50 <50 <50 <500 <500 <5.0 <5.0 <5.0 <25 <25 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0 <2.0 <2.0 <2.0 <4.0 <2.0 <4.0NA NA NA NA NA ND ND ND ND <10 <10 <50 <50 <50 <10 <10 <10 <10 <1.4 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <10.0 <5.0 <10.0<0.5 NA NA NA NA <10 <100 <100 <5.0 <5.0 <5.0 <25 <25 <25 <5.0 6.0 <5.0 <5.0 <5.0<5.0 1.8J <5.0 <5.0 <5.0 8.6 <5.012<5.0 <5.0 NA <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <2.0<0.5 <10 <10 <10 <10 <10 <100 <100 <1.0 <20 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.02.6<1.01.9<1.0 <1.0 <2.0 <1.0 <2.0ND ND ND ND ND ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0<1.0<2.03.5<10 <10 <10 <10 <10 <100 <100 <1.01.7<1.0 <5.0 <5.0 <5.0<1.0 <1.0 <1.0 <1.00.82 1.1 0.78J 0.72J<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 NA NA NA NA <10 <100 <100 <5.0 <5.0 <5.0 <25 <25 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0ND NA NA NA NA ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 NA NA NA NA <20 <200 <200 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0NA <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.066 27 17 25 25 19 <100 <100 <1.0 <20 12 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.6 <1.0 26.4 3.4 19.0 3.4 3.3 2.6 <1.0 <2.031 29 9.6J 17 26 39<100 <1009.1 22<5.0 <5.0 <5.0 <5.0<5.0 <1.0 <1.0 <1.01.1 0.64 0.65J 0.78J<1.0 <1.0 <1.0 <1.0 <1.02.4 2.0 2.4 10.1 5.0 8.3 3.1 4.8 4.7<1.03.18.6<10 <108.4J<10 <10 <100 <100 1.13.8<1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.2 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 <50 <50 <50 <50 <50 <500 <500 <1.0 <1.0 <5.0 <25 <25 <25 <5.0 <5.0 <5.0 <5.00.45<5.0<5.0<5.0<5.0<5.0<5.0<5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <2.0ND NA NA NA NA ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0<1.0 <2.0<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 1.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0NANANANANANANANA<0.5 NA NA NA NA <10 <100 <100 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NAND ND ND ND ND ND ND ND ND <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ,1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <2.0 <1.0 <2.0<0.5 NA NA NA NA <30 <300 <300 <3.0 <3.0 <3.0<15 <15 <15<3.0 <3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <1.0 <2.0 <2.0<2.0 <1.0 <1.0 <2.0 <1.0 <2.0NA NA NA NA NA NA NA NA NA300 25NA29NA169.5 9.4 8.3 14 27 39 18 9.8 15 19 20 19 38 1824.7 82.3 42.3 80.532.5 39.3 50.8 12.1 37.6NA 50,000 45,000 46,000 71,000 63,00065,000 46,000 53,000 65,000 37,000 NA 37,000 NA 26,000 28,000 NA 29,000 NA34,000 NA 33,000 34,000 35,000 40,00036,000 32,000 48,000 29,000 43,600 58,800 56,800 60,400 52,200 66,300 70,000 14,700 66,3007,000 24,000 16,000 19,000 21,000 17,000 8,100 25,000 140,000 10,000 10,000 17,000 <5,000 <5,000 <5,000 <5,000 <5,000 5,100 14,000 2,400 21,000 1,800J <5,000 <5,000 <5,000 <5,00010,000 16,000 50,0005,400 129,000 20,70095,300 24,900 8,900 7,500 15,100 8,500NA 44,000 34,000 34,000 57,000 46,00051,000 41,000 140,000 49,000 33,00032,000 29,000 27,000 21,000 23,000 20,000 30,000 29,000 27,000 26,000 25,000 28,000 26,000 32,000 29,000 16,00043,000 41,000 30,800 87,100 44,90069,300 44,900 57,300 47,400 19,500 49,400NA NA 1,400 NA NA NA NA NA NA NA NA1,400<200 <100 <100 <100 <100 <100 30 19 140 <100 <100 <100 <100 <100 NA NA NA NA NA NANA NA NA NA NA NA 8,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANA NA NA 4000.0 NA NA NA NA <1,000 NA NA NA NA NA NANA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2.2 NM NM NM 0.2 0.4 <0.2 <0.2 <0.2 <0.2 <0.2 NA <0.1 <0.1 <0.1 NA NA NA NA <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NA NA NM NM NM 204 299 412 358 280 388 365 378.8 217.5 45.8 306.7 236.6 219.5 119.4 169.2 300.1 331.9 249.9 65.1 238.4 241.2 185.1 339.1 452.1 230 84 267 458 298.7383.0 47.3 360.0 228.4 79.3 113.824.5 15.0 17.0 18.5 20.0 21.6 19.2 20.0 17.8 20.5 20.1 18.4 22.7 21.4 18.0 25.7 20.9 18.3 18.9 22.6 22.819.0 20.8 19.9 21.6 17.3 20.6 20.0 24.0 17.8 16.5 23.8 18.4 25.6 20.4 22.4 12.9 21.44.6 4.33 4.28 5.07 4.26 4.73 4.49 4.54 4.62 4.47 4.40 4.36 4.35 4.33 4.56 4.194.17 4.45 4.16 4.04 4.48 4.43 4.22 4.15 4.45 4.37 3.134.79 5.61 4.57 4.65 7.05 4.56 4.64 4.37 4.29 5.90 4.03263.0 232.1 255.0 256.6 358.7 340.0341.8 286 936 337.4 193 190 203 187 161 146 150 176 211 201 197 175 194 196 226 150 194 267 327 256 517 319 510.4 306.8 374.1 326.1 155.6 345.11.45 NM NM 1.21 0.73 1.02 0.97 2.50 2.49 1.37 0.75 1.690.67 1.31 2.64 1.00 1.261.211.061.030.541.140.690.781.82 0.94 0.63 0.46 0.99 3.81 3.08 0.93 3.16 2.03 1.98 1.88 7.58 2.35NM NM NM NM NM NM NM NM NM NM 6.0 5.90 2.34 3.24 2.06 2.20 NA 4.40 5.36 4.19 2.65 1.78 0.00 5.73 1.22 0.89 5.44 0.0 0.0 4.3 2.0 9.59 1.13 17.90 0.58 1.24 9.13 8.55Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-10SE Corner of BuildingS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 10 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 1MW-126/12/03 1/19/05 4/21/057/18/05 1/29/09 7/27/091/12/10 7/20/10 6/12/031/19/05 4/21/05 7/18/05 6/12/03 1/19/05 4/21/05 7/19/05 7/1/13 6/13/14 9/16/14 12/10/14 3/13/159/18/15 3/22/16 9/22/163/29/17 9/22/17 3/13/1810/4/186230D 601 601 601 8260 8260B 8260B 8260B 6230D 601 601 601 6230D 601 601 601 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B6,000 NA NA NA <50 <50 <50 <50 NA NA NA NA NA NA NA NA <50 <50 <50 <20.0 <25.0 <25.0<25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA <0.5 NA NA NA <0.5 NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND <1.0 <1.0 <1.0 <1.0 ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <0.5 <5.0 <5.0<5.0 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NA NA NA <0.5 NA NA NA <1.0 <1.0 <1.0 NA NA NANANANANANANA<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NA NA NA <0.5 NA NA NA <1.0 <1.0 <1.0 NA NA NANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND <1.0 <1.0 <1.0 <1.0 ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND <5.0 <5.0 <5.0 <5.0 ND ND ND ND ND ND ND ND <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <2.5 <2.5 <2.5 <2.5 <0.5 <5.0 <5.0<5.0 <0.5 <5.0 <5.0 <5.0 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND <1.0 <1.0 <1.0 <1.0 ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.4 NA NA NA <1.0 <1.0 <1.0 <1.0 ND NA NA NA ND NA NA NA <1.0 <1.0 <1.0 NA <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA <10 <10 <10 <10 NA NA NA NA NA NA NA NA <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <5.0 <5.0<5.0 <2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA NA NA NA <10 <10 <10 <10 NA NA NA NA NA NA NA NA <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 NA NA NA <5.0 <5.0 <5.0 <5.0 <0.5 NANA NA <0.5 NA NA NA <5.0 <5.0 <5.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND <1.0 <1.0 <1.0 <1.0 ND ND ND ND ND ND ND ND <1.0 <1.0 < 1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <5.0 <5.0 <5.0 <5.0 <0.5 NANA NA <0.5 NA NA NA <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA <1.0 <1.0 <1.0 <1.0 ND NA NA NA ND NA NA NA <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 NA <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 9.8 9.8 <0.5 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <0.5 <1.0 <1.0<1.0 <0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 0.79J <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <0.5 <1.0 0.60J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <0.5 <5.0 <5.0<5.0 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA <1.0 <1.0 <1.0 <1.0 ND NA NA NA ND NA NA NA <2.5 <2.5 <2.5 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 NANANANANANANANA<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <0.5 NANA NA <0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 NANANANANANANANAND ND ND ND <1.0 <1.0 <1.0 <1.0 ND ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <3.0 <3.0 <3.0 <3.0 <0.5 NA NA NA <0.5 NA NA NA<3.0 <3.0 <3.0 <1.0 <2.0 <2.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA <4.0<4.0 <4.0 <4.0NA NA NA NA NA NA NA NA<3.0 <3.0 <3.0 <2.0 2.8 <2.0<2.0 <2.0 <2.0 2.5 <2.0 <2.0NA 21,000 18,000 18,000 NA NA NA NA NA 15,000 12,000 13,000 NA 42,000 39,000 40,000 36,000 35,000 33,000 39,300 35,100 36,500 38,700 38,200 35,700 37,100 35,000 36,1009,400 18,000 5,100 16,000 NA NA NA NA 16,000 32,000 30,000 17,000 4,600 18,000 19,000 17,000 7,000 7,70011,000 4,600 5,100 5,2004,400 4,000 4,700 6,600 5,600 6,000NA 8,700 7,400 8,700 NA NA NA NA NA 8,400 5,800 5,100 NA 19,000 17,000 17,000 150,000 18,000 14,000 16,400 15,200 15,200 15,600 16,400 16,800 13,800 16,000 14,400NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 3,300 NA NA NA NA NA NA NA 1,400 NA NA NA 300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 3,620 NA NA NA NA NA NA NA 1,120 NA NA NA 3,960 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0.8NMNM1.4 0.3 NA NA NA 1.6NMNM0.4 1.6NMNM0.8 NA NANANANANANANANANANANA NM NM 147 199 40.3 82.5 154.3 201.9 NM NM -176 301 NM NM 119 272 295.8 331.0 -27.2 375 400 167.2 32.7 264.5406.4 197.3 187.8 159.526.1 12.8 15.9 17.5 14.8318.65 15.44 18.74 19.6 13.518.1 17.0 26.7 10.2 20.2 21.8 23.7 22.8 27.5 21.4 15.9 25.8 20.0 27.9 21.3 26.4 15.6 28.44.2 4.73 5.49 4.94 5.53 4.60 4.77 4.63 4.25 3.80 5.70 4.45 4.34 4.18 4.79 4.174.00 2.53 4.49 3.50 4.47 3.904.42 4.27 4.12 4.20 4.33 3.6380.0 72.2 88.9 84.0 84.0 82 120 124 127.0 97.9 91.0 82.9 119.0 140.9 160.7 156.2 172 352 155 172 121 141 162.1 165.7 160 130 159.6 172.51.05 NM 1.14 1.19 2.39 0.150.85 1.17 2.02 NM 2.51 2.971.33 NM 0.66 0.06 0.34 0.44 0.25 2.10 1.75 0.82 0.340.271.900.261.631.00NM NM NM NM 5.25 2.53 3.88 4.02 NM NM NM NMNM NM NM NM 2.14 0.00 0.0 1.9 4.7 1.95 4.73 2.53 0.48 3.12 1.21 6.08Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointSW Corner of Site Eastern Section of SiteMW-11MW-13Northern Portion of Site S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 11 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 16/12/03 10/20/05 1/31/067/24/06 1/30/07 7/12/071/29/08 7/16/08 1/28/09 7/27/09 1/11/10 7/20/101/19/11 7/12/11 1/24/127/10/12 1/24/13 7/1/136/11/14 12/10/14 9/17/153/21/16 9/22/16 3/30/179/21/17 3/13/18 10/4/186230D 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0<2.0<2.0<2.0<2.0<2.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NANANANANANANANA<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <2.5<2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 14 <10.0 <5.0 <5.0<5.0<5.0<5.0<5.0<5.0<2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0<2.0<2.0<2.0<2.0<2.0NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 5.2 <1.0 <1.0 <1.0 <1.0 <1.01.4 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANA<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANAND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <3.0 <3.0<3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <1.0 <2.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA <4.0 <4.0 <4.0 <4.0<4.0 <4.0 <4.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <2.0<2.0 <2.0 <2.0 <2.0 <2.0<2.0<2.0NA 29,000 21,000 20,000 15,000 24,000 28,000 26,000 28,.000 NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA 26,000 39,000 19,000 16,00010,000 28,000 48,000 25,000 32,000 NA NA NA NA NANANANANANANANANANANANA NA NA NA 3,300 8,300 9,700 9,800 5,000 3,400 3,300 2,600 NA NA NA NA NA NA NA NA NA NA NANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 6,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1,910 NA NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1.8 0.4 <0.2 <0.2 <0.2 NM <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANA NM 396 326 286 298 341 362.9 284.9 254.8 186.1 177.3 329.0 27.8 199.4 350.3 149.4 266.2 459.6 312.0 310 383.9 -42.3 228.9 316.4 241.1 356.8 49.820.8 20.4 13.8 18.5 12.5 19.7 15.0 18.8 14.5 19.5 12.9 19.7 12.3 19.3 14.5 20.1 13.6 20.1 27.5 15.3 22.7 16.9 25.7 16.0 25.0 11.6 23.25.42 4.69 4.86 4.91 5.12 4.73 4.24 4.25 4.33 3.96 4.534.19 4.47 4.18 4.00 4.80 4.16 3.51 3.14 4.40 4.40 4.934.334.674.194.864.49261.0 268.0 183.40 154 150 203.2 203 195 246 164 150 223 198 174 212 186 117 189352 147 259 146.2 194.3 139.2 143.5 144 160.30.83 5.59 2.56 4.65 4.11 5.37 6.31 5.19 7.80 4.90 2.985.89 6.51 4.86 9.99 4.18 4.22 6.33 2.66 1.77 6.67 1.954.572.246.092.684.56NM NM NM NM NM NM 6.0 8.4 3.10 1.40 2.16 2.21 1.93 0.30 0.45 0.71 1.11 0.73 0.00 2.7 2.97 6.53 8.12 2.93 3.38 4.02 5.93Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-14Off Site S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 12 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 16/12/03 10/20/05 1/31/067/25/06 1/30/07 7/12/071/30/08 7/16/08 1/28/09 7/27/09 1/11/10 7/20/101/18/11 7/12/11 1/23/127/10/12 1/24/13 7/1/136/12/14 12/11/14 9/18/153/22/16 9/23/16 3/29/179/21/17 3/13/18 10/4/186230D 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0<2.0<2.0<2.0<2.0<2.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NANANANANANANANA<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.01.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <1.0 1.3 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5<2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0<2.0<2.0<2.0<2.0<2.0NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 8.9 <1.0 <1.0 <1.0 <1.0 3.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANA<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANAND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <3.0 <3.0<3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <1.0 <2.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA <4.0 <4.0 <4.0 <4.0<4.0 <4.0 <4.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <2.0<2.0 <2.0 <2.0 <2.0 <2.0<2.0<2.0NA 9,300 9,100 9,400 6,700 7,400 8,100 7,800 8,300 NA NA NA NA NA NA NA NA NA NA NANANANANANA NA NA 13,000 20,000 12,000 20,00012,000 14,000 24,000 13,000 22,000 NA NA NA NA NANANANANANANANANANANANA NA NA NA 7,800 11,000 10,000 9,0009,900 12,000 11,000 13,000 NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 330 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1,590 NA NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1.8 0.6 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANA NM 311 359 256 287 345 294.7 225.6 172.7171.0 172.7 312.8 -78.4 166.0 199.4 154.4 239.1 420.0 372.0 391 257.3 59.3 230.4 307.5 240.0 421.2 141.318.0 22.5 15.8 20.6 14.323.1 16.76 21.07 17.51 22.6815.3 23.0 14.3 22.9 16.3 21.7 13.0 22.1 20.9 16.2 23.115.9 23.7 18.2 24.8 13.0 26.05.15 4.94 4.89 4.77 5 4.66 4.41 4.38 4.66 4.08 4.69 4.10 4.51 3.95 4.20 4.68 4.25 3.49 2.94 3.97 4.27 4.894.56 4.40 3.99 4.80 3.9392.0 85.5 88.62 87 90 94.71 95 87 130 95 125 106 132 106 147 113 89 114 180 99 68 72.3 81.6 76.2 64.8 88.3 99.30.38 0.43 0.46 1.42 2.41 2.18 1.07 2.99 2.75 2.58 1.992.52 2.10 1.01 2.57 1.06 1.87 1.37 0.51 1.48 0.96 0.841.301.331.001.421.90NM NM NM NM NM NM 1.5 3.81 2.09 3.80 6.1410.42 18.21 1.16 2.166.57 5.21 1.58 27.10 4.0 13.75 7.15 9.575.86 4.43 6.88 21.53Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointOff SiteMW-15S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 13 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 16/12/03 10/20/05 1/31/067/25/06 1/30/07 7/12/071/30/08 7/16/08 1/28/09 7/27/09 1/11/10 7/20/101/18/11 7/12/11 1/23/127/10/12 1/24/13 7/1/136/12/14 12/11/14 9/18/153/22/16 9/23/16 3/29/179/21/17 3/14/18 10/4/186230D 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA NA NA NA <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <2.0 <2.0<2.0<2.0<2.0<2.0<2.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NANANANANANANANA<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <2.5<2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <2.0 <2.0<2.0<2.0<2.0<2.0<2.0NA NA NA NA NA <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 NA NA NA NA <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 6.9 <1.0 16 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<0.5 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANA<0.5 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0NANANANANANANAND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 NA NA NA NA <3.0 <3.0<3.0 <3.0<3.0 <3.0 <3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 <3.0 <1.0 <2.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA <4.0 <4.0 <4.0 <4.0<4.0 <4.0 1.6 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0<2.0 <2.0NA 15,000 9,500 8,400 6,50010,000 12,000 6,800 7,200 NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA 2,900 13,000 4,200 <2,000 <5,000 <5,00012,000 <5,000 <5,000 NA NA NA NA NA NA NA NA NANANANANANANANA NA NA NA 10,000 6,300 6,400 6,2009,900 4,800 6,100 5,800 NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 3,090 NA NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2.2 <0.1 0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANA NM 367 360 293 289 368 398.1 238 217.9 194.5 190.7 338.2 -128.7 205.5 242.9 167.0 285.4 520.3 260.0 370 329 121.8 252.4 330.5 184.3 538.8 -92.518.2 19.1 15.9 19.6 13.8 19.4 16.9 19.0 17.6 20.5 15.7 20.1 15.1 20.3 16.2 19.6 16.1 19.3 18.6 13.2 20.4 14.4 20.5 18.9 24.1 10.2 24.43.73 4.53 4.40 4.52 4.74 4.48 4.07 4.17 4.35 3.93 4.403.76 4.27 3.79 3.91 4.44 4.03 2.08 4.54 4.35 3.82 4.624.074.224.104.554.4688.0 103.7 88.75 116 85 92.39 94 62 81 76 8381 78 71 79 74 54 64 63 81 73 73.6 68.4 72.3 65.6 70 70.34.27 1.05 5.64 8.38 5.48 5.75 1.47 5.14 5.60 4.70 5.625.52 5.20 4.29 5.49 4.78 4.55 4.64 3.43 4.79 2.53 4.713.814.435.524.923.68NM NM NM NM NM NM 0.45 4.97 2.04 1.70 3.352.06 1.67 0.29 0.821.32 1.68 0.13 0.00 <1.0 4.91 3.01 7.25 0.98 1.32 0.00 1.88Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-16Off SiteS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 14 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 111/19/03 6/3/04 7/18/0510/20/05 1/31/06 7/24/061/30/07 7/12/07 1/29/08 7/16/08 1/28/09 7/28/091/13/10 7/20/10 1/19/117/13/11 1/24/12 7/10/12 1/24/13 7/1/13 6/12/1412/10/14 9/17/15 3/21/169/22/16 3/30/17 9/21/17 3/13/18 10/4/186230D 8260 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA <5.0 NA NA NA NA NA <50 <50 <50 <50 <500 <250 <50 <50 <50 <50 <50 <100 <50 <50 3,190 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA <5.0 <5.0 <5.0 <5.0<5.0 <50 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <1.0 <2.0 <2.0<2.0 <1.0 <2.0 <2.0 <2.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 NA NA NA NA NA NA NA NA<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 NA NA NA NA NA NA NA NANA <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <50 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0<50 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5 <2.5<25 <12 <2.5 <2.5 <2.5 <2.5 <2.5 <5.0 <2.5 <2.5 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.09.9 6.3 9.8 25 35 17 9.3 12 16 14 28 20 16 12 12 144.416 115.57.8 11.8 7.9 11.4 11.2 7.9 7.24.4 1.1<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.087110 98 320 310 160 120 120 190 210450240 260 160 170 97 58 240 130 74 96 176 120 155 161 107 106 62.8 15.4<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0NA ND NA NA NA NA NA <10 <10 <10 <10 <100 <50 <10 <10 <10 <10 <10 <20 <10 32 2,180 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 <2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<50 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <5.0 <2.0<2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA ND NA NA NA NA NA <10 <10 <10 <10 <100 <50 <10 <10 <10 <10 <10 <20 <10 <10 <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<0.5 <1.0 NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <50 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <10<5.0 <5.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.02.2<1.0 <1.0 <1.0 <1.0 <1.01.1<10 <5.00.720.44J <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <50 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <10<5.0 <5.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 74.4ND ND NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 NA <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.03.4 <1.0 8.9 7.8 13 4.2 3.1 7.4 3.5 <1.0 6.5 <10 9.7 <1.0 1.4 1.6 <1.0 1.7 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.00.541.1<1.0 <1.01.9 1.3<1.0 <1.01.1 1.1 2.2<10 <5.01.0 1.2<1.0 <1.01.2<2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.03.04.2 4.2 8.3 8.0 6.12.6 2.83.12.64.2<10 <5.0 2.8 1.6 1.8 <1.03.12.9 1.65.1 4.9 8.3 9.0 5.4 4.52.3 1.6 <1.0<0.5 <1.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <1.0 <5.0 <5.0<50 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <10 <5.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <2.5 <5.0 <1.0 <2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NAND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <10 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <3.0 <3.0<3.0 <3.0<30 <15 <3.0 <3.0 <3.0 <3.0<3.0 <6.0 <3.0 <3.0 <1.0 <2.0<2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA NA31 28 23 8246 27 52 43 25 17 44 41 38 31 28.8 19.3 31.2 31.4 22.5 20.7 16.3 4.0NA NA 18,000 18,000 19,000 19,000 17,000 18000 20000 19,000 20,000 NA NA NA NANANANANANANANANANANANANA NA NA NA NA 28,000 29,000 14,000 22,000 16,000 17000 19000 16,000 18,000 NA NA NA NANANANANANANANANANANANANA NA NA NA NA 13,000 12,000 14,000 17,000 15,000 14000 14000 13,000 13,000 NA NA NA NANANANANANANANANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1,000 NA NA NA NA NANA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <0.1 0.4 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NANM 212 214 366 289 289 286 277 302.5 196.3243.0 182.3 169.6 264.9 44.6 168.0 319.4 142.1 266.6 450.2 521.0 162 261.3140.0 147.3 252.9 189.9 256.1 -195.917.6 15.5 17.0 18.7 15.8 18.0 14.1 17.1 16.6 18.9 16.7 18.2 14.5 22.3 15.3 19.4 16.7 18.4 14.2 18.7 19.6 16.5 21.3 14.2 24.7 15.6 25.0 13.6 30.35.29 5.09 5.73 5.64 5.17 4.99 5.21 5.10 4.81 4.66 4.903.91 4.83 4.76 4.90 4.99 4.67 5.15 4.46 3.60 2.94 4.73 5.47 5.10 5.71 5.54 5.30 5.82 6.06NM 139.3 174.2 191.7 173.8 170 190 192.9 174 196.3 201 155 226 226 199 225 272 203 141 190 500 232 299 235.7 322.8 287.5 227.6 314.1 254.42.95 2.72 3.18 2.05 3.10 5.22 5.51 3.90 3.56 2.91 3.072.97 3.82 3.34 3.31 2.67 4.81 2.63 3.49 3.98 3.15 3.15 1.56 2.28 1.16 1.80 2.40 2.29 0.12NM NM NM NM NM NM NM NM 5.6 4.07 2.48 7.90 6.27 6.91 3.43 0.72 0.92 0.58 0.85 2.390.00 <1.0 2.12 2.56 5.79 1.71 0.50 8.70 6.05Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-17South & Offsite S:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 15 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 111/19/03 6/3/04 7/18/0510/20/05 1/31/06 7/24/061/30/07 7/12/07 1/29/08 7/16/08 1/29/09 7/28/091/13/10 7/20/10 1/19/117/13/11 1/24/12 7/11/12 1/24/13 7/1/13 6/12/1412/10/14 9/17/15 3/21/169/22/16 3/30/17 9/21/17 3/13/18 10/4/186230D 8260 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA <5.0 NA NA NA NA NA <50 <50 <50 <50 <250 <250 <50 <50 <250 <100 <50 <100 <1006,8001,880 <25.0 <50.0 <50.0 <25.0 <50.0 <25.0 <25.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0<2.0<1.0<2.0<1.0<1.0<0.5 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <0.60 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA <5.0 <5.0 <5.0 <5.0<5.0 <25 <25 <5.0 <5.0 <25 <10 <5.0 <10<10 <10 <1.0 <2.0 <4.0 <4.0 <2.0 <4.0 <2.0 <2.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0<2.0<2.0NANANANANANANANA<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0<2.0<2.0NANANANANANANANANA <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0<1.0<2.0<1.0<2.0<1.0<1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <5.0 <25 <25 <5.0 <5.0 <25 <10 <5.0 <10 <10 <10<1.0 <1.0 <2.0 <2.0<1.0 <2.0 <1.0 <1.01.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <5.0 <5.0 <25 <25 0.48 0.31J <25 <10 <5.0 <10 <10 <10 <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <2.5 <2.5<12 <12 <2.5 <2.5 <12 <5.0 <2.5 <5.0 <5.0 <5.0 <1.0 <1.0<2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0<2.0<1.0<2.0<1.0<1.0<0.5 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0<2.0<1.0<2.0<1.0<1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 NA <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA <1.0 <1.0 <1.0 <1.0<1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0<2.0<1.0<2.0<1.0<1.0515.615 32 40 23 23 27<1.019 14 14 20 16 22 18 23 19 14 16 14 21.316.6 14.7 17.1 14.4 13.3 12.1 12.2<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <5.00.82 0.50J<5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0<1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0370110 200400 370190 300360<1.0 270 180 200 350 200 290 240 300 250 180 210 160 289 197 180 223 194 188 196 197<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <5.0 0.34 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0<2.0<2.0<1.0<2.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0<2.0<2.0<1.0<2.0<1.0<1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0<2.0<2.0<1.0<2.0<1.0<1.0ND ND NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 NA <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0<2.0<1.0<2.0<1.0<1.0NA ND NA NA NA NA NA <10 <10 <10 <10 <50 <50 <10 <10 <50 <20 <10 <20 <204,2001,780 <5.0 <10.0 <10.0 <5.0 <10.0 <5.0 <5.0<2.0 <2.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<25 <25 <5.0 <5.0 <25 <10 <5.0 <10 <10 <10 <5.0 <2.05.1<4.0 <2.0 <4.0 <2.0 <2.0NA ND NA NA NA NA NA <10 <10 <10 <10 <50 <50 <10 <10 <50 <20 <10 <20 <20 <20 <10.0 <5.0 <10.0 <10.0 <5.0 <10.0 <5.0 <5.0<0.5 <1.0 NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <25 <25 <5.0 <5.0 <25 <10 <5.0 <10 <10 <10 NA <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0<2.0<2.0<1.0<2.0<1.0<1.0ND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <0.50 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.01.3<1.0 <1.0 <1.02.3 1.1 1.1<1.0 <1.0 <1.0 <1.0 <5.0 <5.00.8 0.83J<5.0 <2.0 <1.0 <2.0 <2.0 <2.01.0<1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <5.0 <5.0 <5.0 <5.0 <25 <25 <5.0 <5.0 <25 <10 <5.0 <10 <10 <10 <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0ND ND NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 NA <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 NA <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.021 <1.0 5.1 13 16 4.8 6.2 6.7 <1.0 8.4 <1.0 <5.0 8.6 <1.0 2.7 <5.0 2.7 1.5 <2.0 <2.0 <2.0 1.7 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.02.5 0.98J 0.63J 1.2 2.6 1.6 1.4 1.9<1.01.0<1.0 <5.0 <5.01.2 1.9<5.0 <2.01.4<2.0 <2.0 <2.01.5 1.2<2.0 <2.0 1.1 <2.0 <1.02.719 32 22 24 15 16 12 14<1.021 13 14 12 16 4.4 6.7 5.0 7.5 8.0 6.6 9.5 6.9 8.8 5.6 4.7 7.1<2.0 1.43.5<0.5 <1.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <5.0 <5.0 <5.0<25 <25 <5.0 <5.0 <25 <10 <5.0 <10 <10 <10 <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0ND ND NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <2.5 <5.0 <5.0 <5.0 <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0<2.0<2.0<1.0NANANANANANANA<0.5 <1.0 NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0<2.0<2.0<1.0NANANANANANANAND ND ND ND ND ND ND <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <5.0 <2.0 <1.0 <2.0 <2.0 <2.0 <1.0 <1.0 <2.0 <2.0 <1.0 <2.0 <1.0 <1.0<0.5 <1.0 NA NA NA NA NA <3.0 <3.0<3.0 <3.0<15 <15 <3.0 <3.0 <15 <6.0<3.0<6.0 <6.0 <6.0 <1.0 <2.0 <4.0 <2.0 <1.0 <2.0 <1.0 <1.0NA NA NA NA NA NA NA66 35 56 39284.4496833804448626044.136.3 41.0 47.8 33.6 46.5 40.1 33.2NA NA 18,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 16,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 15,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0.8 0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NANANANANANANANANM 268 184 290 224 260 232 120 226.1 116.5 52.9 156.3 -22.8 217.0 46.1 153.9 234.4 105.9 247.0 441.0 279.0 215 28279.3 -25.2 249.2 146.7 353.3 109.517.4 15.3 16.1 18.0 15.8 17.2 15.1 17.8 16.5 19.5 15.7 18.7 15.8 18.3 15.6 19.1 17.1 19.1 14.7 19.2 22.1 16.1 21.4 12.1 23.1 14.2 24.3 13.2 20.16.00 5.62 5.63 6.19 5.61 5.52 5.7 5.69 5.33 5.34 6.10 4.88 5.35 5.15 5.52 5.065.17 5.45 4.85 4.60 3.96 4.97 5.45 5.50 5.28 5.25 5.27 5.46 4.82NM 114.0 134.5 167.0 145.8 138.0 138.9 141.6 124 118 120 114 160 153 136 149 161 158 112 141 346 166 174 169.4 169.7 170.4 130 156 182.33.83 2.29 2.61 2.11 3.61 3.05 4.42 2.50 1.62 1.38 2.451.62 1.64 2.57 1.70 1.11 1.84 1.57 1.69 1.44 0.91 0.91 0.83 1.18 1.01 1.16 0.87 1.11 1.83NM NM NM NM NM NM NM NM 2.4 7.92 1.14 6.10 5.29 6.80 2.78 0.00 0.09 2.53 3.18 2.04242.00 <1.0 3.19 3.95 10.90 2.54 6.33 54.59 60.60Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-17DSouth and OffsiteS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 16 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 16/3/04 7/18/05 10/20/051/31/06 7/25/06 1/30/077/12/07 1/29/08 7/16/081/29/09 7/28/09 1/11/10 4/7/10 7/20/10 1/19/11 7/12/11 1/24/12 7/10/12 1/24/13 7/1/13 6/12/14 12/10/14 9/17/15 3/21/16 9/22/16 3/30/17 9/21/17 3/13/18 10/4/188260 601 601 601 601 601 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B14 NA NA NA NA NA <50 <502200<50 <50 <50 <50 <50 <50 <50 <50 <50 <50 <50 NS <20.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0 <25.0<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS <1.0 <1.0 <1.0 <1.0 <1.0<1.0<1.0<1.01.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 NS <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA <5.0 <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 NS <1.0 <2.0 <2.0<2.0 <2.0 <2.0 <2.0 <2.0<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NSNANANANANANANANA<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NSNANANANANANANANA<1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND ND <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND ND ND ND ND ND <1.0 <5.0 <25 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.027 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <5.0 <5.0 <5.0 <5.0 <1.0 <1.0 <2.5 <12 <1.0 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5<2.5 <2.5 <2.5 <2.5 NS <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA <1.0 <1.0 <1.0 <5.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND ND <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA <1.0 <1.0 <1.0 <5.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.718<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.01.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0ND NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 NS <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<2.0 NA NA NA NA <5.0 <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 NS <5.0 <2.0 <2.0<2.0 <2.0 <2.0 <2.0 <2.0ND NA NA NA NA NA <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 NS <10.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<1.0 NA NA NA NA NA <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0ND ND ND ND ND ND <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <0.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0 NA NA NA NA NA <5.0 <5.0 <25 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 NS <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS NA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.9 <5.0 <1.0 <1.0 <1.0 <1.0 3.5 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 NS <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01.2<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.020<5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <1.0 <5.0 <25 <1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0<5.0 <5.0 <5.0 <5.0 NS <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0ND NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.5 <2.5 <2.5 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NS<1.0NANANANANANANA<1.0 NA NA NA NA NA <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0NS<1.0NANANANANANANAND ND ND ND ND ND <1.0 <1.0 <5.0 <1.0 <1.0<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 NS <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0<1.0 NA NA NA NA NA <3.0 <3.0<15<3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 <3.0<3.0 <3.0 <3.0 NS <1.0 <2.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0NA NA NA NA NA NA <4.0 <4.04.3<4.0<4.034<4.0 <4.03.2<3.0 <3.0 <3.0 <3.0 <3.0 NS <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0NA 5,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA 59,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA 67,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANA NA NA NA NA NA NA NS NA NA NA NA NA NA NA NA NM 0.2 1.0 1.2 <0.2 <0.2 0.5 <0.2 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NS NA NA NA NANANANANA63 112 115 31 238 253 214 104.7 -9.9 -8.1 -97.4 96.7 -115.5 90.5 45.4 187.2 -98.9 -102.7 -75.4 -69.0 NS -148.0 -183.8 -165.3 -141.1 160.1 -116.3 142.6 -85.017.7 17.5 17.0 15.8 19.8 13.2 20.5 16.3 18.8 14.8 19.7 14.5 16.8 18.9 15.0 19.2 16.1 19.0 15.2 20.5 NS 15.2 22.1 15.1 28.0 13.9 20.4 14.5 18.88.7 6.61 7.09 6.54 7.32 5.33 7.35 7.38 7.27 8.00 6.46 6.72 7.51 6.88 7.27 7.086.89 7.13 6.56 7.26 NS 7.10 7.857.51 7.27 5.99 7.21 6.98 7.0350.4 499.6 405.0 389.0 357 127 367.1 309 288 289 290 352 365 353 269 258 364 345247 314 NS 367 347 326.6 331.977.6 278.1 157.6 277.34.42 0.005 0.76 4.42 5.89 5.76 5.31 2.29 1.62 0.38 0.41 0.69 0.55 1.87 6.45 4.20 1.19 0.33 0.40 0.37 NS 0.36 0.19 0.19 0.23 0.59 0.14 0.58 0.43NM NM NM NM NM NM NM 2.0 5.54 5.31 3.90 2.437.150.662.261.782.393.094.261.36 NS 115.00 42.35 30.59 37.60 2.77 19.80 57.02 30.91Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-17DDSouth & OffsiteS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 17 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 11/19/05 3/14/05 4/21/057/19/05 10/21/05 1/31/067/25/06 1/31/07 7/12/07 12/8/07 12/27/07 1/30/08 4/29/08 7/16/08 10/14/08 1/29/09 7/28/09 10/20/09 1/13/10 4/7/10 7/21/10 10/19/10 1/20/11 7/14/11 1/23/12 7/11/12 1/25/13 7/2/13 6/11/14 9/16/14 12/9/14 3/13/15 9/17/15 3/21/16 9/22/16 3/29/17 9/21/17 3/13/18 10/4/18601 601 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA 85 140 57 <400 <400 52 200 <250 <250 220 53 <2,500 <1,200 <500 <250 <50 <1,000 58 <500 <500 <5,000 <1,000 <1,000 <500 <250 <500 <500 <500 23 <25.0 <25.0<62.5 <250 <125 <250 <125 <62.5NA NA <1.0 0.71J <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.02.1<1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5NANA3.64.76.1<40<40<1.0NANANANANANANANANANANANANANANANANANANANANA NA 2.3 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5<100 <11.2<1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 0.35 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <0.60 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <1.06.8<50 <25 <10 <5.0 <1.0 <20 2 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5<500 4.5J17 188.9 <120 <12014<5.0 <25 <25 <5.0 5.2 <250 <120 <50 <25 <5.0 <100 <5.0 <50 <50 <50 <100 <100 <50<25 <50 <50 <50 <1.0 <2.0 <2.0 <5.0 <20.0 <10.0 <20.0 <10.0 <5.0NA NA <1.0 <1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0<20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 NA NA NA NA NA NA NA NA NANA NA <1.0 <1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0<20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 NA NA NA NA NA NA NA NA NANA NA 0.99J <5.0 <5.0 <200 <200 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA<100 <1 <2.03.7<2.0 <80 <80 <2 53 <5.0 <5.0 2.2 <1.0 <50 <25 <10 <5.02.3<20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.05.0<1.0 <1.0 <10.0 <5.0 <10.0 <5.0 <2.5ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 <1.0 <10<10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5ND ND ND ND ND ND ND ND <1.0 <25 <25 6.5 <5.0 <250 <25 <50 <25 <5.0 <100 <5.0 <50 <50 <50 <100 <100 <50 <25 <50 <50 <50 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5<100 19 33 36 36 30J <40 8.8 19 35 29 26 14 <250 <25 <50 <25 22 <100 15 22 34J 24J <100 <100 <50 <25 <50 <50 <50 14.5 18.7 11.7 9.1 12 9.9 16.1 10.8 4.3<50055 65 98 92 180<80690 180 490 140 200 230<120220 87 71 51<50100 60 120 91 53 98 36 40 32<25 <2535.9 33.12.59.4<10.05.6<10.0 <5.0 <2.5NA NA 0.79J 2.9 <1.0 <40 <40 <1.0 1.8 <5.0 <5.0 1.2 <1.0 <50 <25 <10 <5.0 1.4 <201.4 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5<100 0.63 1.6 7.6 4.8 <40 <40 <1.0 8.4 5.5 7.5 5.0 1.6 <50 <25 <10 <5.0 3.4 <20 4.4 7.5 13 12 <20 <20 <10 <5.0 <10 <10 <10 6.4 5.4 4.5 2.9 <10.0 <5.0 <10.0 <5.0 <2.5ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 <1.0 <10<10 <10 <20 <20 <10 <5.0 <10 <10 <10 NA <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5<100 8.4 <1.0 <1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.53,300 370 640 1,800 2,000 1,300 620 220 1,500 1,500 2,200 1,700 760 1,700 2,000 1,000 1,700 1,200 670 720 1,700 2,8002,300 2,200 2,400 970 1,900 1,300 840 740 1,280 937 703 459 1,050 703 1,090 661 389520 69 100 290 340 230 94 53 320 340 270 200 120 250 310 120 160 170 100 130 290 450370 310 380 150 300 110 140 110 174 156 120 78.5 162 111 178 123 69.143,000<1.0 <1.03,900 590<40720<1.0990100440 1,00013 <50 140470140950 2,300<5.0 1901,600 1,800 940 2,000 700 920 740 540 430 900 1,070 423 499 819 652 1,050 711 404130 14 2.2 32 13 <40 <40 2.6 28 27 27 22 8.5 <50<25 1712 19 23 8.6 16 33 27 20 32 12 19 14 <10 <10 12.0 12.4 8.2 5.6 13.2 9.7 16.4 10.9 6.4<100 <1 0.79J 8.9 3.9 <80 <80 <1.0 4.5 <5.0 5.2 4.1 <1.0 <50 <25 <10 <5.0 4.0 <202.0 <10 8.1J 4.8J <20 <20 <10 <5.0 <10 <10 <10 2.2 2.4 1.7 <2.5 <10.0 <5.0 <10.0<5.0 <2.5<100 0.98J <1.01.5<1.0 <40 <40 <1.0 <1.0 <5.0 <5.01.3<1.0 <50 <25 <10 <5.01.0<20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.01.5<1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5NA NA ND ND ND ND ND ND <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 0.58 <102.9J <10 <20 <20 <10 <5.0 <10 <10 <10 NA1.0<1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5NA NA <1.0 <1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0<20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0<10.0 <5.0 <2.5NA NA ND ND ND ND ND ND 120 70 <50 34 12 <500 <250 <100 <50 <10 <200 7.2 <50 35J 75J <200 <200 <100 <50 <100 <100 <100 20.4 7.6 7.6 <12.5 <50.0 <25.0 <50.0 <25.0 <12.5<5009.54.69.2 9.3<80 <807.2 5.7<25 <2512 11<250 <120 <50 <257.1<10012 10 20J 18J<100 <100 <50 <25 <50 <50 <5012.6 22.34.212.2<20.012.6<20.0 <106.9NA NA ND ND ND ND ND ND <10 <50 <50 <10 <10 <500 <250 <100 <50 <10 <200 <10 <100 <100 <100 <200 <200 <100 <50 <100 <100 <100<10.0 <5.0 <5.0 <12.5 <50.0 <25.0 <50.0 <25.0 <12.5NA NA <1.0 <1.0 <1.0 <40 <40 <1.0 <5.0 <25 <25 <5.0 <5.0 <250 <250 <50 <25 <10 <100 <5.0 <50 <50 <50 <100 <100 <50 <25 <50 <50 <50 NA <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5<100 <118 29 32<40 <401628 3 404526<5046 18 23 22<2032 110 210 120 100 160 82 150 99 81 63 99.2 39.9 72.6 17.7 64.2 48.4 69.4 47.2 26.5ND ND ND ND ND ND ND ND <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 <1.0 <10<10 <10 <20 <20 <10 <5.0 <10 <10 <101.3<1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5<1001.4 0.84J 4.6 3.7<40 <40 <1.03.8<5.05.5 3.9 1.3<50 <25 <10 <5.03.3<202.4 4.1 7.7J 6.1<20 <20 <10 <5.0 <10 <10 <103.7 5.7 2.9 2.6<10.0 <5.0 <10.0 <5.0 <2.5NA NA <1.0 13 <1.0 <40 <40 <1.0 15 <25 <25 <5.0 <5.0 <250 <120 <50 <25 <5.0 <100 1.3 3.9 30J 35J <100 <100 <50 <25 <50 <50 <50 18.1 3.7 10.5 <2.5 11.1 5.7 13.9 <5.0<2.5NA NA ND ND ND ND ND ND <1.0 <5.0 <5.0 <1.0 <1.0 <50 <1.0 <10 <5.0 <1.0 <20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 NA <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5NA NA 0.64J <1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <1.0 <10 <5.0 <1.0 <20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 NA <1.0 <1.0 <2.5 <10.0 <5.0<10.0 <5.0 <2.568011 200 17 26 37J <40560 810 52017 8033055 49 34 19 22 38 64 <10 13 <10 <20 26 11 14 10 23 46 11980226.837839.6 27.8 24.7 18.2 6.6330 49 73 170 210 140 60 50 160 180 180 160 70 150 190 89 110 110 89 82 190 310 270 180 250 130 220 120 100 84 128 122 90.9 65.4 113 85.9 120 80.4 45.0<100 <1 1.7J17 16<80 <80 1.31191311<1.0 <50 <25 <105.2 7.9<204.4 11 20 15<20 <20 <1012<10 <10 <107.3 7.0 5.22.7 <10.0 <5.0 <10.05.7 3.2<500 <5 <2.0 <2.0 <2.0 <80 <80 <1.0 <5.0 <25 <25 <5.0 <5.0 <250 <120 <50 <25 <5.0 <100 <5.0 <50 <50 <50 <100 <100 <50 <25 <50 <50 <50 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5NA NA ND ND ND ND ND ND <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 <1.0 <10<10 <10 <20 <20 <25 <12 <25 <25 <25 <1.0 <1.0 <1.0 <2.5 <10.0 <5.0 <10.0 <5.0 <2.5NA NA <1.0 <1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0<20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.0 NA NA NA NA NA NA NA NANA NA <1.0 <1.0 <1.0 <40 <40 <1.0 <1.0 <5.0 <5.0 <1.0 <1.0 <50 <25 <10 <5.0 <1.0<20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10 <1.0 NA NA NA NA NA NA NA NAND ND ND ND ND ND ND ND <1.0 <5.0120<1.0 <1.0 <50 <25 <10 <5.0 <1.0 <20 <1.0 <10 <10 <10 <20 <20 <10 <5.0 <10 <10 <10<1.0 <1.0 <1.0<2.5 <10.0 <5.0 <10.0 <5.0 <2.5NA NA <3.0 <3.0 <3.0 <80 <80 <3.0 <3.0 <15 <15 <3.0 <3.0<150<75<30<15 <3.0 <60 <3.0 <30 <30 <30 <60 <60 <30 <15 <30 <30 <30 <1.0 <2.0 <2.0 <5.0 <10.0 <5.0 <10.0 <5.0 <2.5NA NA NA NA NA NA NA NA1700NA NA960NA800NA500490 630 370460 3,200 5,600 2,600 1,300 2,900 1,200 2,200 1,600 1,600 710 1,070 969 778585 1,430 940 1,160 1,010 598120,000 100,000 97,000 140,000 120,000140,000 190,000 93,000 230,000 NANA 180,000 NA 190,000 NA 130,000 190,000 NA 68,000 NA320,000NA310,000 340,000 360,00027,000350,000 310,000 260,000 260,000 283,000191,000 207,000 182,000301,000 244,000 347,000 234,000164,00013,000660,000 970,000 570,000420,000 610,000 780,000240,000870,000NA280,000 490,000 300,000 470,000 490,000220,000330,000 300,00096,000440,000 370,000 360,000230,000300,000240,000 22,000310,000 200,000160,000 200,000123,000642,000164,000454,000119,000 104,000 120,000 108,000 93,10039,000 1,500,000 1,200,000 760,000590,000 640,000 480,000 160,000 290,000 250,000 620,000 240,000 190,000260,000 260,000 150,000 200,000 180,000 160,000220,000 240,000 250,000 210,000 260,000 230,000 200,000 230,000 210,000200,000 190,000205,000 239,000 184,000 98,100 188,000233,000 193,000 183,000 143,000NA 37,000 NA NA NA NA NA NA NA 8,000 310 <100 410 <200 <100 <100 <100 <100 <100540 56 82J <100 <100 220 170 <100 NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANANA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANANA NA NANA NA NA NA 4,520 NA NA NA NA NA NA NA NANA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANM NM NM <0.1 0.2 <0.2 <0.2 <0.2 <0.2 NA NA <0.2 NA <0.1 <0.1 <0.1 NA NA NA NA <0.1<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 NA NA NA NA NA NA NA NA NA NA NA NANM NM 182 304 305 331 338 473 433 NA 506.2349.4 270.3 284.9 437.0 432.1 529.5 343.8 342.2441.5 573.7 465.9 6.5 371.9307.4 245.7 498.6 489.4494.0 291 376 492 405.7 503.0 72.1 124.1 218.5 180.5 -163.717.3 18.5 22.0 22.0 22.5 21.4 22.0 20.4 23.9 NA 21.621.0 22.9 24.9 23.4 21.4 22.9 23.0 21.221.8 24.4 24.5 21.5 23.5 22.1 23.4 21.3 23.123.5 24.1 21.4 20.8 24.4 20.4 26.2 20.6 25.1 19.9 25.44.64 5.01 6.37 5.65 5.32 5.10 4.25 4.30 3.88 NA 3.85 3.86 3.72 3.78 3.73 4.02 3.63 3.94 3.873.97 3.47 3.66 3.69 3.78 3.64 4.05 3.73 3.81.84 3.99 3.36 3.72 3.83 3.81 3.81 3.30 3.71 3.99 4.00361.3 6,100 5,704 3,050 22.5 2,957 2,333 1,146 2,315 NA 1,882 1,510 1,129 1,836 1,673 1,008 1,390 1,106 1,0951,288 1,935 2,011 1,487 1,803 1,750 1,339 1,396 1,3982,970 1,053 1,420 1,883 1,239 1,621 1,445 1,169 1,399 1,202 899NM NM 1.21 0.96 1.28 3.97 1.32 3.55 2.29 NA 5.23 6.572.82 6.57 5.64 11.28 10.01 10.92 8.433.44 3.64 3.80 3.02 1.25 0.84 0.55 5.01 0.360.38 0.54 2.45 0.41 0.19 0.73 0.28 0.33 0.42 0.26 0.27NM NM NM NM NM NM NM NM NM NA 8.80 0.35 7.781.03 1.42 2.00 2.23NA 6.86 4.12 7.82 3.24 2.47 2.81 3.63 2.18 1.39 9.05 0.00 0.0 <1.0 4.2 0.60 9.61 9.59 3.07 2.05 3.46 3.52Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-18Approx 30 ft Downgradient of Knife RoomS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 18 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 11/19/05 3/14/05 4/21/057/19/05 10/21/05 1/31/067/25/06 1/31/07 7/12/07 12/8/07 12/27/08 1/30/08 4/29/08 7/16/08 10/14/08 1/29/09 7/28/09 10/20/09 1/13/10 4/7/10 7/21/10 10/19/10 1/20/11 7/14/11 1/23/12 7/11/12 1/25/13 7/2/13 6/11/14 9/16/14 12/9/14 3/13/15 9/18/15 3/21/16 9/22/16 3/29/17 9/21/17 3/13/18 10/4/18601 601 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260BNA NA <100 8.4J <100 <10 <10 <50 130 <50 <500 <500 <50 <50 <500 <500 <250 <50 <500 33 <250 <1,000 <1,000 <50 <500 <50 <500<500 <500 <500 <20.0 <25.0 <25.0 <25.0 <250 <100 <125 <100 <50.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <101.0<1.01.6<1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA <1.0 <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0<10 <10 <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0<1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <0.60 <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0ND ND ND ND ND ND ND ND <1.0 <1.0 <10 <105.4<1.0 <10 <10 <5.0 <1.0 <10 2.9 <5.0 <20 <1.0 <1.0 <10 1.1 <10 <10 <10 <10 1.6 <1.06.5<1.0 <10.0 <4.0 <5.0 <4.0 <2.0<10 <10 <10 1.4J <30 <3 <3 <3 <5.0 <5.0 <50 <50 <5.0 <5.0 <50 <50 <25 <5.0 <50 1.3<25 <100 <5.0 <5.0 <50 <5.0 <50 <50 <50 <50 <1.0 <2.0 <2.0 <2.0 <20.0 <8.0 <10.0 <8.0 <4.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 NA NA NA NA NA NA NA NA NANA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 NA NA NA NA NA NA NA NA NANA NA <10 <1.0 <10 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANANANANANANANA<10 <10 <106.9<20<2<2<236 2.5<10 <10 <1.0 <1.0 <10 <10 <5.01.9<10 <1.0 <5.0 <20 <1.0 <1.0 <101.2<10 <10 <10 <103.2 1.4 4<2.5 <10.0 <4.0 <5.0 <4.0 <2.0ND ND ND ND ND ND ND ND <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0<20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <1.0 <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0<2.0ND ND ND ND ND ND ND ND 7 <5.0 <50 <50 <5.0 <5.0 <50 <50 <25 <5.0 <50 1.2 <25 <100 <5.0 <5.0 <50 <5.0 <50 <50 <50 <50 <1.0 <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0<10 <10 <10 6.0 21 3.3 12 <5.0 36 22 <50 <50 8.2 16 <50 <50 <25 11 <50 4.6 6.4 8.2J 5.1 6.4 <50 5.0 <50 <50 <50 <50 11.2 8.3 15.0 3.5 10.5 4.0 6.6 5.9 <2.0<50 <50 <508.0<205.6 7.2 120 530 92 38 34 10 25 25<25 <125.4 29 120 38<503.1 5.6<258.8<25 <25 <25 <2526.3 14.1 3.12.9 <10.0 <4.0 <5.0 <4.0 <2.0NA NA <10 <1.0 <10 <1.0 0.64J <1.0 <1.0 <1.0 <10 <10 <1.0 1.9 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <1.0 <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0<10 <10 <10 <1.0 <10 <1.0 <1.0 <1.0 6.0 1.4 <10 <10 <1.0 3.1 <10 <10 <5.0 2.1 <100.46 <5.0 <20 1.1 1.0 <10 1.1 <10 <10 <10 <10 4.7 1.7 6.9 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0ND ND ND ND ND ND ND ND <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0<20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 NA <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0<10 <10 <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0<1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <1.0 <1.0 <1.0 <1.0 <10.0<4.0 <5.0 <4.0 <2.0290 150 130 110 630 65 300 39 1,600 460 620 860 290 730 810 640 450 390 140 95 240 300 260 220 200 290 290 790 880 310 851 305 759 176 744 244 315 241 14751 12 28 19 99 9.7 60 7.3 240 110 77 130 48 120 140 100 74 83 21 23 45 50 36 43 33 32 44 110 140 46 118 64.2 149 27.0113 40.4 50.6 43.4 27.36,200 2,00058 <1.0610<1.0 300 <1.08803370 700<1.01,000 2,300 6,800 5,700 4,300 1,200<5.02,600 2,400 1,500 1,900 1,4001,100 510 1,500 890 380 1,5202741,4601901,270 440 771 45934919 10J <10 <1.0 14 <1.0 5.3 <1.0 32 6.3 14 23 2.8 29 34 38 31 26 <10 0.73 11 14J 10 1311 6.2 <10 18 14 <10 14 6.9 18 2.8 12.9 <4.0 5.6 4.5 3.012 <10 <10 <1.0 <10 <1.0 1.2J <1.0 6.1 1.3 <10 <10 <1.0 6.4 <10 <10 6.7 7.2 <10 0.37 3.5 <20 2.7 3.6 <10 1.9 <10 <10 <10 <108.2 1.3 5.1 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0<10 <10 <10 <1.0 <10 <1.0 <1.0 <1.02.3<1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0<10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <1.0 <1.01.2<1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA ND ND ND ND NDND 1.7 <1.0<10 <10 <1.0 <1.0 <10 <10<5.0 <1.0<10 0.36<5.0<20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 NA <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <1.0 <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA ND ND ND ND ND ND 92 <10 <100 <100 <10 <10 <100 <100 <50 <10 <100 6.9 <50 <50 <5.0 <5.0 <50 <10 <50 <50 <100 <100 <10.0 <5.0 <5.0 <5.0 <50.0 <20.0 <25.0 <20.0 <10.0<50 <50 <50 1.1J <20 <2.0 <2.0 <5.020<5.0 <50 <50 <5.05.7<50 <50 <25 <5.0 <508.1<25 <200 1.2J <5.0 <50 <5.0 <50 <50 <50 <509.5 9.2 7.33.6 <20.08.6<10.0 <8.0 <4.0NA NA ND ND ND ND ND ND <10 <10 <100 <100 <10 <10 <100 <100 <50 <10 <100 <10 <50 <200 <10 <10 <100 <10 <100 <100 <100 <100 <10.0 <5.0 <5.0 <5.0 <50.0 <20.0 <25.0 <20.0 <10.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <5.0 <5.0 <50 <50 <5.0 <5.0 <50 <50 <25 <5.0 <50 <5.0 <25 <100 <5.0 <5.0 <50 <5.0 <50 <50 <50 <50 NA <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0<10 <10 <103.6 19 2.90.94J3.5 140 18 11<103.0 6.8<10 <10 <5.0 <10 <1010 4.5<20 0.58J1.4<1011 14 33 59 13 39.7 13.7 50.6 6.4 24.2<4.010.2 9.0 4.4ND ND ND ND ND ND ND ND1.1<1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <100.32<5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <101.2<1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.01.4 1.4 <10 <1.0 <10 <1.0 <1.0 <1.04.4 1.8<10 <10 <1.03.6<10 <10 <5.03.6<10 0.322.2<201.6J 1.8<102.1<10 <10 <10 <103.8 1.7 5.9<1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <5.0 <5.0 <50 <50 <5.0 <5.0 <50 <50 <25 <1.0 <50 <1.0 <5.0 <100 <5.0 <5.0 <50 <5.0 <50 <50 <50 <50 2.3 <1.0 4 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA ND ND ND ND ND ND <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0<20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 NA <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 NA <1.0 <1.0 <1.0 <10.0 <4.0<5.0 <4.0 <2.0200 87 73 30 33 14 24 120300180 23 <10 27 56 36 <10 <5.0 2.5 67 94 46 16J <20 4.4 <10 31 23 120 120 180 163 113 146 38.6 163 50.7 62.9 31.7 22.938 49 18 16 66 7.5 44 8 180 69 58 89 31 87 91 68 56 42 21 22 31 35 25 24 21 29 33 74 110 35 87 48.7 113 22.5 84.429.8 34.9 30.2 19.0<10 <1011J<2.029<2.0 1.8J <1.0112.8 <1010<1.09.4 11 13 9.8 9.2<10 <1.0 <5.0 <203.7 4.2<103.4<10 <10 <10 <106.72.910.11.4 <10.0 <4.0 <5.0 <4.0 <2.0<50 <50 <20 <2.0 <20 <2.0 <2.0 <1.0 <1.0<5.0 <50 <50 <5.0 <5.0 <50 <50 <25 <1.0<50 <1.0 <5.0 <100 <5.0 <5.0 <50 <5.0 <50 <50 <50 <50 <1.0 <1.0 <1.0 <1.0 <10.0<4.0 <5.0 <4.0 <2.0NA NA ND ND ND ND ND ND <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0<20 <1.0 <1.0 <10 <2.5 <10 <10 <25 <25 <1.0 <1.0 <1.0 <1.0 <10.0 <4.0 <5.0 <4.0<2.0NA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <1.0 NA NA NA NA NA NA NA NANA NA <10 <1.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <10 <10 <1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10 <1.0 NA NA NA NA NA NA NA NAND ND ND ND ND ND ND ND <1.0 <1.044 15<1.0 <1.0 <10 <10 <5.0 <1.0 <10 <1.0 <5.0 <20 <1.0 <1.0 <10 <1.0 <10 <10 <10 <10<1.0 <1.0 <1.0<1.0 <10.0 <4.0 <5.0 <4.0 <2.0NA NA <30 <3.0 <30 <3.0 <3.0 <3.0 <3.0 <3.0 <30 <30<3.0 <3.0<30<30<15 <3.0 <30 <3.0 <15 <60 <3.0 <3.0 <30 <3.0 <30 <30 <30 <30 <1.0 <2.0 <2.0 <2.0<10.0 <4.0 <5.0 <4.0 <2.0NA NA NA NA NA NA NA NA1,300NA NA480NA610NA710520 380 130 22 420 590 290 180 220 210 290 880 1,200 260 775 441 992 246 975 300 77.0 317 20651,000 46,000 43,000 55,000 67,00064,000 79,000 54,000 150000 NA NA 110000 NA 110,000 NA 75,000 71,000 NA 70,000NA 70,000 NA 74,000 74,000 85,000 9,100 8,800 140,000 190,00070,000 181,000 106,000270,00068,200 158,000 72,500 137,000 105,000 96,40011,000 49,000 100,000450,000 740,000 820,000750,000 390,000 350,000NA 220,000330,000 520,000 250,000230,000 160,000 160,000 110,000410,000 460,000 410,000130,000 150,000 150,000 150,000 20,000 190,000 160,000340,000<5,000 163,000 205,000 135,000 153,00081,700 133,000 93,800 174,000 148,00027,000 75,000 170,000 570,000 500,000660,000 480,000 170,000 170,000 200,000 310,000 190,000 270,000 160,000150,000 100,000 94,000 80,000 170,000 180,000 170,000 100,000 91,000 98,000 110,000 110,000 110,000 140,000 210,000 89,000 120,000 114,000 148,000 74,900 101,000 84,300 114,000 125,000 98,200NA 13,000 NA NA NA NA NA NA NA 3,300 200 <100 240 <100 <100 <100 <100 <100 <600 170 170 45J <100 <100 <100 100 <100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NANANANANANA NA NA NA NA NA NA 4,230 NA NA NA NA NA NA NANA NANANANA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NM NM NM <0.1 0.2 <0.2 <0.2 <0.2 <0.2 NA NA <0.2 NA <0.1 <0.10 <0.1 NA NA NA NA <0.1<0.1<0.1<0.1<0.1<0.1<0.1NA NANANANANANANANANANANANM NM 272 470 416 488 356 508 449 NA 511.9459.1 396.0 257.9 450.0 411.4 455.9 291.1 310.0 462.6 450.0 389.6 -25.7 298.7 365.0 205.9 472.4 450.8 323.0 247.6 366 390 448.6 398.5 -193.9 124.0 226.7 170.7 -83.116.7 16.4 20.9 21.2 21.8 21.0 21.6 21.0 22.5 NA 21.020.7 22.0 22.9 22.1 21.2 22.2 22.3 20.8 20.8 22.4 23.2 20.4 22.4 21.7 22.4 21.422.9 23.9 23.3 22.0 20.523.1 19.9 25.2 20.2 23.6 20.3 24.15.27 4.65 4.88 3.76 3.89 3.77 4.15 4.03 3.88 NA 3.92 3.91 3.62 3.83 3.81 4.07 3.76 4.13 3.83 4.06 3.7 3.93 3.88 4.02 3.47 4.13 3.87 3.93 4.06 4.19 3.51 4.02 3.82 4.10 3.91 3.46 3.82 4.14 4.06206.2 2,009 1,001 2,771 2,580 3,502 2,215 1,459 1,500 NA 1,188 1,101 1,566 1,000 893 715 612 521 1,306 1,327 733 698 649 667 720 721 615 930 1,470 857 1,120789 1,030 6.76 927 765 768 885 745NM NM 1.3 3.97 1.78 3.99 NM 2.48 1.14 NA 1.2 0.49 1.90 0.94 0.81 1.08 1.47 1.73 1.62 1.04 4.39 5.66 3.02 4.91 6.35 8.01 4.43 5.30 0.48 0.39 2.47 0.44 1.19 1.061.57 1.07 4.91 2.62 2.01NM NM NM NM NM NM NM NM NM NA 8.0 0.10 3.31 0.97 1.08 2.39 1.56 NA 4.79 9.01 2.36 0.83 0.72 0.10 3.28 3.12 1.561.82 0.00 0 <1.0 2.7 0.78 5.02 6.35 3.35 1.56 2.18 1.59Notes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointMW-19Approx 60 ft Downgradient of Knife RoomS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 19 of 20)Hart & Hickman, PC
Appendix CHistorical Groundwater Analytical ResultsFormer Fulflex FacilityScotland Neck, North CarolinaH&H Project No. FUL-006Sample IDLocationSample Date VOCs (µg/l)Acetone 6,000Benzene 1Bromochloromethane NSBromodichloromethane 0.6Bromoform 4Bromomethane 10tert-Butylbenzene 70n-Butylbenzene 70Carbon Disulfide 700Carbon Tetrachloride 0.3Chlorobenzene 50Chloroethane 3,000Chloroform 70Chloromethane 3Dibromomethane 701,2-Dichlorobenzene 201,3-Dichlorobenzene 2001,4-Dichlorobenzene 61,1-Dichloroethane 61,2-Dichloroethane 0.41,1-Dichloroethene 350cis-1,2-Dichloroethene 70trans-1,2-Dichloroethene 1001,2-Dichloropropane 0.61,3-Dichloropropane 0.4Ethylbenzene 6002-Butanone (MEK) 4,000Methylene Chloride 54-Methyl 2-pentanone (MIBK) NSNaphthalene 61,1,1,2-Tetrachloroethane 11,1,2,2-Tetrachloroethane 0.2Tetrachloroethene 0.7Toluene 6001,2,3-Trichlorobenzene NS1,2,4-Trichlorobenzene 701,1,1-Trichloroethane 2001,1,2-Trichloroethane 0.6Trichloroethene 3Trichlorofluoromethane 2,0001,2,3-Trichloropropane 0.0051,2,4-Trimethylbenzene 4001,3,5-Trimethylbenzene 400Vinyl Chloride 0.03Total Xylenes 5001,4-Dioxane (µg/l) - 8260 SIM1,4-Dioxane 3.0Others (µg/l)Chloride 250,000Sulfate 250,000Sodium NSIron, Total 300Nitrate 10,000Methane NSTotal Organic Carbon NSField MeasurementsFerrous Iron (mg/l) NSORP (mV) NSTemperature (oC) NSpH NSConductivity (µS/cm) NSDissolved Oxygen (mg/l) NSTurbidity (NTU) NSNorth Carolina Groundwater Standard 1PS-3 (20 FT) PS-19 (20 FT)1/19/05 3/14/05 4/21/057/19/05 10/21/05 1/31/067/25/06 1/31/07 7/12/07 12/8/07 12/27/07 1/22/08 1/31/07 1/31/07601 601 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260 8260NA NA 36J <100 <10 <10 <10 <2500 62 <500 <5000 <50 <2500 2,500NA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50NA NA <10 <10 4.7 <10 <10 <50 NA NA NA NA <50 <50<10 <10 <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50ND ND ND ND ND ND ND ND10<10 <100 <1.0 ND ND<10 <10 <10 <10 3.8 <10 <10 <250 <5.0 <50 <500 <5.0 <250 <250NA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50NA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50NA NA <10 <10 <1.0 <10 <10 NA NA NA NA NA NA NA<10 <10 <1038<2.0 <20 <20 <50 <1.0 <10 <1001.2<50 <50ND ND ND ND ND ND ND ND <1.0 <10 <100 <1.0 NDND ND ND ND ND ND ND ND <1.0 <50 <500 <5.0 ND ND<10 <10 5.7J 15 12 9.2J 6.4J <250 12 <50 <500 18 <250 <250<50 <50 <5029 30 26<20810 69 26<25030 6,100 12,000NA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50<10 <10 <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 4.5 <50 <50ND ND ND ND ND ND ND ND <1.0 <10 <100 <1.0 ND ND<10 <10 <10 <10 1.2 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50370 170 160 310 280 230 270 400 190 950 740 530 1,600 2,90061 10 32 62 55 43 54 81 31 180 110 140 420 1,4007,2001301,900 2,100 810 500 1,700 1,300<1.06,400 6,900 3,200<50 <5023 <10 9.5J 13 11 7.4J 18 <50 1.9 54 <100 50 <50 <5015 <10 <10 <10 3.7 <20 <20 <50 <1.0 <10 <100 19 <50 <50<10 <10 <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50NA NA ND ND ND ND ND ND <1.0 <10 <100 <1.0 ND NDNA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50NA NA ND ND ND ND ND ND <10 <100 <1000 <10 ND ND<50 <50 <50 <20 2.8 <10 <10 <50 <5.0 <50 <500 <5.0 <50490NA NA ND ND ND ND ND ND <10 <100 <1000 <10 ND NDNA NA <10 <10 <1.0 <10 <10 <50 <5.0 <50 <500 <5.0 <50 <50NA NA <1024 19<10 <10 <5010<10 <1002.8<50 <50ND ND ND ND ND ND ND ND <1.0 <10 <100 <1.0 ND ND<10 <10 <10 <101.5<10 <10 <50 <1.0 <10 <1004.4<50 <50NA NA <10 <10 <1.0 <10 <10 <50 <5.0 <50 <500 <5.0 <50 <50NA NA ND ND ND ND ND ND <1.0 <10 <100 <1.0 ND NDNA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50110 48 53 110 89 63 26 770 40 340 <100 302,80020047<1023 44 41 31 31 60 17 93<100100 140 6011<10 <20 <2034<20 <20 <50 <1.016<10015<50 <50<50 <50 <20 <20 <2.0 <20 <20 <50 <1.0 <50 <500 <5.0 <50 <50NA NA ND ND ND ND ND ND <1.0 <10 <100 <1.0 ND NDNA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 1.5 <50 <50NA NA <10 <10 <1.0 <10 <10 <50 <1.0 <10 <100 <1.0 <50 <50ND ND ND ND ND ND ND ND <1.0 <10 <100 <1.0 ND NDNA NA <30 <30 <3.0 <30 <30 <150 <3.0 <30 <300 <3.0 <150 <150NA NA NA NA NA NA NA NA46NA NA1,800NA NA46,000 51,000 55,000 75,00068,000 65,000 90,000 73,000 95,000 NA NA NA NA NA15,000 210,000 110,000180,000 100,000 210,000270,000130,000390,000NA 130,000 200,000 NA NA27,000 360,000 180,000 390,000 150,000180,000 110,000 110,000 220,000 110,000 190,000 120,000 NA NANA88,000NA NA NA NA NA NA NA860 2,500 260,000NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA NANA NA NA NA 4,240 NA NA NA NA NA NA NA NA NANM NM NM 0.4 0.4 <0.2 NM <0.2 <0.2 NA NA NA <0.2 5.4NM NM 112 425 340 379 NM 337 516 NA 508.1 346.3 570 -19215.5 17.1 20.4 20.8 21.0 20.4 NM 20 23.9 NA 19.7 20.05 20.4 20.35.01 5.18 6.07 4.98 4.88 4.70 NM5.25 4.43 NA 4.09 4.35 3.34 6.37184.9 1,781 1,016 1,824 970 1,150NM 738 1,587 NA 822 861 2,356 2,060NM NM 1.07 1.30 0.70 0.70 NMNM 12.64 NA 1.27 0.86 NM NMNM NM NM NM NM NM NM NM NM NA 9.5 2.9 NM NMNotes:1) NC Groundwater Standard as indicated in 15A NCAC 2L Only those compounds detected above method detection limits are included in table.In December 2014, MW-18 had a detection of iodomethane (methyl iodide) of 1.6 μg/L. There is no NC 2L Groundwater Standard for this compound.Bold indicates analyte concentration exceeds NC 2L Groundwater StandardDirections in reference to manufacturing portion of Fulflex facility.VOCs - Volatile Organic Compounds; NS - Not Specified; NA - Not AnalyzedJ = Estimated value below the lowest calibration pointKnife Room AreaMW-20 (Abandoned)Approx 90 ft Downgradient of Knife RoomS:\AAA‐Master Projects\Fulflex ‐ FUL\FUL‐006 Fulflex Scotland Neck 2018\October 2018 Monitoring\Tables\FUL‐006 October 2018 Tables Appendix C GW Historical 12/31/2018Appendix C (Page 20 of 20)Hart & Hickman, PC

Appendix D Concentration vs Time Graph
01101001,00010,000100,0001,000,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,1,1-TCA Source Area Groundwater Concentrations(MW-8/MW-8R and MW-18)MW-8/MW-8RMW-18NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
01101001,00010,000100,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,1-DCA Source Area Groundwater Concentrations(MW-8/MW-8R and MW-18)MW-8/MW-8RMW-18NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
01101001,00010,000100,0001,000,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,1-DCE Source Area Groundwater Concentrations(MW-8/MW-8R and MW-18)MW-8/MW-8RMW-18NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
0100200300400500600700800Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,1,1-TCA Groundwater Concentrations(MW-10, MW-19, MW-20)MW-10MW-19MW-20NC 2L GroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
02004006008001,0001,2001,4001,600Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,1-DCA Groundwater Concentrations(MW-10, MW-19, MW-20)MW-10MW-19MW-20 (Abandoned)NC 2L GroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
01,0002,0003,0004,0005,0006,0007,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,1-DCE Groundwater Concentrations(MW-10, MW-19, MW-20)MW-10MW-19MW-20(Abandoned)NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
1101001,00010,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,4 - Dioxane Groundwater Concentrations- Source Area(MW-8/MW-8R and MW-18)MW-8/MW-8RMW-18NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
1101001,00010,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)Date1,4 - Dioxane Groundwater Concentrations- Downgradient of Injection Wells(MW-10 and MW-19)MW-19MW-10NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
0500,0001,000,0001,500,0002,000,0002,500,0003,000,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)DateChloride Groundwater Concentrations- Source Area(MW-8/MW-8R and MW-18)MW-8/MW-8RMW-18NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.- UIC permit limit established pre-12/7/2007 injection, supersedes NC 2L Standard based on background concentrations.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
050,000100,000150,000200,000250,000300,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)DateChloride Groundwater Concentrations- Downgradient of Injection Wells(MW-10 and MW-19)MW-19MW-10NC 2LGroundwaterStandardNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx Injections
05,000,00010,000,00015,000,00020,000,00025,000,00030,000,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)DateSulfate Groundwater Concentrations- Source Area(MW-8/MW-8R and MW-18)MW-8/MW-8RMW-18NC 2LGroundwaterStandardInitial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx InjectionsNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.- UIC permit limit established pre-12/7/2007 injection, supersedes NC 2L Standard based on background concentrations.
0100,000200,000300,000400,000500,000600,000700,000800,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)DateSulfate Groundwater Concentrations- Downgradient of Injection Wells(MW-10 and MW-19)MW-10MW-19NC 2L GroundwaterStandardInitial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx InjectionsNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- UIC permit limit established pre-12/7/2007 injection, supersedes NC 2L Standard based on background concentrations.
05,000,00010,000,00015,000,00020,000,00025,000,00030,000,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)DateSodium Groundwater Concentrations- Source Area(MW-8/MW-8R and MW-18)MW-8/MW-8RMW-18Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx InjectionsNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.- No NC 2L Standard is established for sodium, UIC permit limit established pre-12/7/2007 injection.
0100,000200,000300,000400,000500,000600,000700,000Mar-03
Jul-04
Oct-05
Feb-07
Jun-08
Sep-09
Jan-11
Apr-12
Aug-13
Dec-14
Mar-16
Jul-17
Oct-18
Concentration (µg/L)DateSodium Groundwater Concentrations- Downgradient of Injection Wells(MW-10 and MW-19)MW-10MW-19Initial SodiumPersulfate InjectionFirst and Second RegenOx InjectionThird and Fourth RegenOx InjectionPersulfOx InjectionsNotes:- Concentrations below the laboratory reporting limit are shown at half the reporting limit concentration.- MW-8 was replaced by MW-8R in February 2015. MW-8R was first sampled on March 13, 2015.- No NC 2L Standard is established for sodium, UIC permit limit established pre-12/7/2007 injection.

Appendix E
IDW Disposal Documentation