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HomeMy WebLinkAboutFA-1_29001_M_RP_20030115.PDFPost Office Box 902 207 West Fourth Avenue Red Springs, NC 28377 Telephone: (910) 843-4456 Fax (910) 843-5376 ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, INC. Report of Phase II Limited Site Assessment Former Atlas Distributing Company Inc. 5510 Cliffdale Road Fayetteville, Cumberland County, North Carolina Prepared For: Mr. John L. Beard Atlas Distributing Company 1214 Morganton Road Fayetteville, North Carolina 28305 Prepared By: Environmental Hydrogeological Consultants, Inc. Post Office Box 902 207 West Fourth Avenue Red Springs, North Carolina 28377 EHC Project Number: 02-EV1209-3 January 15, 2003 RECEIVED JAN 17 2003 DENR-FAYETiEMLLE REGIONAL OFRCE Serving North & South Carolina since 1986 www.environmentalnc.com Phase II Limited Site Assessment Report DATE OF REPORT: January 15, 2003 Facility I.D.: Unregistered Site Name: Former Atlas Distributing Site Location: 5510 Cliffdale Road, Nearest City/Town: Fayetteville, NC UST Owner: USTs have been removed Address: 29001 UST Incident# (if known): Pcnditg County: Cumberland Phone: UST Operator: C/O Mr. John Beard — Atlas Distributing Company Address: 1214 Morganton Road, Fayetteville NC 28305 Phone: (910) 864-5000 Property Owner: C/O Mr. John Beard — Atlas Distributing Company Address: 1214 Morganton Road, Fayetteville NC 28305 Phone: (910) 864-5000 Property Occupant: Harris Wholesale, Inc. Address: 5510 Cliffdale Road, Fayetteville, NC 28305 Phone: (910)—860-1283 Consultant/Contractor: Environmental Hydrogeological Consultants, Inc. Address: 207 West 4ch Ave, Red Springs, NC 28377 Phone: (910) 843-4456 Release Information Date Discovered: August, 1994 Latitude: N 35' 3.554' Longitude: W 78' 57.986' Estimated Quantity of Release: Unknown Cause of Release: Underground Storage Tank Source of Release (e.g., Piping/UST): Unknown Sizes and contents of UST system(s) from which the release occurred: (2) 10,000 gallon gasoline (removed) (1) 12,000 gallon diesel (removed) 1, 0 G a -� I�j ^ �✓� a Professional one) of Environmental Hydrogeological Consultants, contained in this report is correct and accurate to the be; (Please Affix Seal and Signature) Post Office Box 902 207 West Fourth Avenue Red Springs, NC 28377 Telephone: (910) 843-4456 Fax (910) 843-5376 ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, INC. 11 January 15, 2003 Mr. Ken Currie NCDENR — Fayetteville Regional Office Systel Building, Ste 714 Fayetteville, NC 28301 Subject: Report of Phase II Limited Site Assessment Former Atlas Distributing Company, Inc. 5510 Cliffdale Road Fayetteville, North Carolina EHC Project No. 02-EV1209-3 Dear Mr. Currie: REC JAN 17 2003 DENR - FAYETTEYIU.E REWA OR E On behalf of Mr. John L. Beard, Environmental Hydrogeological Consultants (EHC) is pleased to submit this Report of Phase II Limited Site Assessment conducted at the above referenced location. This work was requested to address the possibility of groundwater contamination. In general, the assessment activities have included drilling of soil exploration borings and collection of soil samples for description; installation of a groundwater monitoring wells; collection of groundwater samples for chemical testing; and investigation of the geology and hydrogeology in the vicinity of the site. The objective of our services was to provide a limited assessment pertaining to the distribution of petroleum constituents in the groundwater, site hydrogeology, and the potential for human exposure and to chemical contaminants. The scope of work for this project is intended to comply with appropriate state environmental regulations contained in 15 NCAC2L. ........... Serving North & South Carolina since 1986 www.environmentalnc.com If any questions concerning this report or our findings, please contact us at (910) 843-4456. We look forward to receiving your comments on this report. Sincerely, ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, INC. as Ammons David L. Brown, L.G. Project Manager Senior Geologist Enclosures • TABLE OF CONTENTS COVER LETTER 1.0 INTRODUCTION............................................................................................................. 1 1.1 Purpose of Investigation.......................................................................................... 1 1.2 Scope of Work Summary........................................................................................ 2 2.0 SITE HISTORY................................................................................................................ 2 2.1 Underground Storage Tank Removal and Previous Environmental Work ............ 2 3.0 RISK CHARACTERIZATION........................................................................................ 4 4.0 POTENTIAL RECEPTORS AND MIGRATION PATHWAYS ................................... 7 4.1 Water Supply Wells................................................................................................. 7 4.2 Potential Receptors.................................................................................................. 7 4.2.1 Surface Water........................................................................................... 8 4.2.2 Wellhead Protection Areas...................................................................... 8 4.2.3 Deep Aquifers of the Coastal Plain Region ............................................. 8 4.2.4 Subsurface Structures............................................................................... 9 4.2.5 Area Land Use......................................................................................... 9 4.2.6 Property Owners and Occupants............................................................. 9 5.0 SITE TOPOGRAPHY, GEOLOGY AND HYDROGEOLOGY................................. 10 5.1 Topographic Conditions........................................................................................ 10 5.2 Regional Geology and Hydrogeology................................................................... 10 5.3 Site Geology.......................................................................................................... 11 5.4 Soil Borings and Sampling.................................................................................... 11 6.0 GROUND WATER INVESTIGATION........................................................................ 12 6.1 Site Hydrogeological Study Methods...................................................................... 12 6.1.1 Monitoring Well Installation.................................................................. 12 6.1.2 Ground -Water Gauging and Sampling .................................................. 13 7.0 RESULTS ................... .. 14 7.1 Ground Water Flow Directions............................................................................. 14 7.2 Ground -Water Sample Analyses.......................................................................... 14 8.0 CONCLUSIONS............................................................................................................. 15 9.0 RECOMMENDATIONS................................................................................................ 16 • Table of Contents (coot.) REFERENCES TABLES Table 1 ADJACENT PROPERTY OWNERS Table 2 GROUND WATER ELEVATION, WELL CONSTRUCTION AND FIELD PARAMETER DATA Table 3 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS FIGURES Figure 1 USGS SITE TOPOGRAPHIC MAP Figure 2 ADJACENT PROPERTY BOUNDARY MAP Figure 3 SITE MAP WITH FORMER UST LOCATIONS Figure 4 GROUNDWATER FLOW DIRECTION MAP Figure 5 GROUNDWATER ANALYSIS RESULTS SUMMARY APPENDICES Appendix A NOTICE OF REGULATORY REQUIREMENTS Appendix B SOIL BORING LOGS Appendix C WELL CONSTUCTION RECORDS Appendix D LABORATORY REPORT Atlas Distributing Company, Phase H LSA Final January, 2003 0 1.0 INTRODUCTION Mr. John L. Beard, contracted Environmental Hydrogeological Consultants (EHC) to conduct a Phase II Limited Site Assessment (LSA) as outlined in EHC's Cost Proposal to Complete a Phase H LSA dated September 26, 2002 at the Former Atlas Distributing Company, Inc. site located at 5510 Cliffdale Road in Fayetteville, North Carolina (Figure 1). This scope of services was required the North Carolina Department of Environment and Natural Resources (NCDENR) Underground Storage Tank (UST) Section, Fayetteville Regional Office (FRO) due to a risk based assessment assigned in a "Notice of Regulatory Requirements" (NORR) dated September 5, 2002 that is included in Appendix A. The NORR is based on chemical analysis results of samples collected from onsite monitoring well (MW-1) that indicated concentrations of petroleum constituent -benzene, to be in excess of 10 times the North Carolina Administrative Code (NCAC) 2L Standard. Therefore, a Phase II LSA was conducted at the site. The following report includes documentation of the methods utilized in this study and presents the results of data analyses, conclusions and recommendations for achieving compliance with state regulatory requirements. 0 1.1 Purpose of Investigation The purpose of the Phase II LSA includes the following: • To identify chemical constituents detected in ground water in the subject area exceeding NCAC, Title 15A, Subchapter 2L (2L) Groundwater Standards; • To identify chemical constituents which exceed gross contamination levels (GCLs) and; • Prepare a Phase II LSA report containing a description of our assessment activities, results, and conclusions. This report is designed to provide information required by the NCDENR, Division of Waste Management (DWM), in accordance with the document entitled "Guidelines for Assessment and Corrective Action — North Carolina Underground Storage Tank Section", dated April 2001, for a Phase II LSA. This document also addresses groundwater requirements as provided in the Groundwater Section Guidelines for the investigation and Remediation for • Soil and Groundwater dated July 2000 as provided in the North Carolina Administrative Code 1 Atlas Distributing Company, Phase II LSA Final January, 2003 Title 15A Subchapter 2L Sections .0100, .0200 and .0300, "Classifications and Water Quality Standards Applicable to the Groundwater of North Carolina". The Phase II LSA scope of work is intended to provide additional data via drilling and sampling of additional monitoring wells. 1.2 Scope of Work Summary As part of the Phase II LSA activities, EHC conducted the following tasks: • Construction of 2 type -II monitoring wells. • Construction of a deep type -III monitoring well to assess the vertical extent of the contamination. • Sampling of the monitoring wells using required analysis methods. • Survey of site monitoring wells. • Preparation of a Ph. II LSA report of results and findings. The results and conclusions of this LSA work are intended for use in the development of an accurate site ranking and/or risk classification as required by the DWM. The specific methods employed during performance of the project activities and the results, conclusions and recommendations of the LSA are described within the following sections of this report. 2.0 SITE HISTORY 2.1 Underground Storage Tank Removal and Previous Environmental Work A report dated April 4, 1991, by Carl M. Taylor and Sons Construction Company of Hope Mills, NC documents the removal of USTs, associated piping and pump islands at the site as follows: Previous Underground Storage Tank Systems Tank Number Date of Installation Capacity Product Date Closed 1 Unknown 10,000gal Gasoline 3129191 2 Unknown 10, 000 gal Gasoline 3129191 3 Unknown 12, 000 gal Diesel 3129191 2 Atlas Distributing Company, Phase II LSA Final January, 2003 • The report does not state if ground water was encountered in the excavation, however 10 confirmation soil samples were collected for laboratory analysis using Environmental Protection Agency (EPA) Method 5030. Petroleum hydrocarbons were not detected above the method detection limit of 5.0 milligrams per kilogram (mg/Kg) in the submitted samples. Though not included in the closure report, a 550 gallon UST located near the diesel UST was also removed at this time according to Atlas Distributing Company personnel. Details concerning this 550 gallon UST were not available. A Phase I Environmental Site Assessment (ESA) dated August 18, 1994 was prepared by EHC for the site. The ESA recommended that additional sampling be performed and that monitoring wells be constructed in the former UST basins. The additional environmental work based on the recommendations is documented in EHC's Phase II ESA dated August 23, 1994. The report details that 4 borings were advanced for soil collection purposes, 3 borings were advanced to construct temporary monitoring wells (TAH- 1 through 3) and that 2 permanent monitoring wells (MW-1 and MW-2) were constructed. According to the report, 135 tons of soil was excavated from the site for offsite remediation. As documented in EHC's Phase H ESA Report, at least 5 sampling events were conducted on MW-I, and MW-2 in July and August 1994. Gasoline constituents were demonstrated to exceed the 2L Standards in each of the wells. 3 Atlas Distributing Company, Phase H LSA Final January, 2003 • 3.0 RISK CHARACTERIZATION The following sections are reproduced from the Limited Site Assessment Report format, pages B-18 through B-21 of the Guidelines for the Assessment and Corrective, Underground Storage Tank Section, April, 2001. Limited Site Assessment Risk Classification and Land Use Form Part I — Groundwater/Surface water/Vapor Impacts High Risk 1. Has the discharge or release contaminated any water supply well including any used for non -drinking purposes? NO: 2. Is a water supply well used for drinking water located within 1000 feet of the source area of the discharge or release? NO: • 3. Is a water supply well used for an purpose e. irrigation, washing cars pp Y Y p� � g• g g , industrial cooling water, filling swimming pools) located within 250 feet of the source area of the release or discharge? NO: • 4. Does the groundwater within 500 feet of the source area of the discharge or release have the potential for future use in that there is no other source of water supply other than the groundwater? NO: Public water is currently supplied to the surrounding area by the City of Fayetteville. 5. Do vapors from the discharge or release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety or the environment. NO: 4 Atlas Distributing Company, Phase H LSA Final January, 2003 . 6. Are there any other factors that would cause the discharge or release to pose an imminent danger to public health, public safety, or the environment? NO: Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the discharge -release? NO: 8. Is the source area of the discharge or release located with a designated wellhead protection area as defined in 42 USC 300h(e)? NO: 9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled "Geology of North Carolina" published by the Department in 1985? YES . If yes, is the source area of the discharge located in an area in which there is recharge to an unconfined or semi -confined aquifer that is being or may be • used as a source for drinking water? UNKNOWN: It is unlikely that the source area could provide recharge to the Upper Cape Fear Aquifer, however recharge cannot be determined without further hydrogeologic study. 10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels (GCL) established (Table 7) by the Department? NO: Part II - Land Use Property Containing Source Area of Release 1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO: 5 Atlas Distributing Company, Phase H LSA Final January, 2003 is park, Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? NO: 3. Does the property contain a commercial or industrial enterprise, an inactive commercial or enterprise, or is the land undeveloped? YES: Commercial enterprise: 4. Do children visit the property? NO: 5. Is the access to the property reliably restricted consistent with its use (e.g. fences, security personnel or both)? YES: Surrounded by chain link fence and automatic gates. 6. Do pavement, buildings, or other structures cap the contaminated soil? YES: The soil is capped by asphalt in most areas, however the . northern side of the parcel is not paved. 7. What is the zoning status of the property? The facility is currently zoned as Commercial. • 8. Is the use of the property likely to change in the next 20 years? NO. Property Surrounding Source Area of Release The questions below pertain to the area within 1000 feet of the source area of the release. 9. What is the distance from the source area of the release to the nearest primary or secondary residence? Residential housing is located on Cliffdale Road approximately 1,000 feet south of the source. 2 Atlas Distributing Company, Phase H LSA Final January, 2003 • 10. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? A church is located approximately 1,000 feet south east of the site. 11. What is the zoning status of the properties in the surrounding area? Commercial and Residential 11. Briefly characterize the use and activities of the land in the surrounding area. The site is near Skibo and Cliffdale Roads. Land use is light commercial with retail stores and restraurants. A mobile home park is located south of the site on Cliffdale Road. 4.0 POTENTIAL RECEPTORS AND MIGRATION PATHWAYS As part of the Phase II LSA Investigation, EHC completed an evaluation of potential • receptors, which is documented in the following section. • 4.1 Water Supply Wells Fayetteville city water and sewer service are both supplied to the surrounding area. Properties visited were observed receiving these services. The site is located several miles south of Glenville Lake and several miles west of the Cape Fear River. Public water is drawn from intakes at Glenville Lake and the Cape Fear River. 4.2 Potential Receptors Potential receptors considered, as part of this LSA, include identification of: adjacent property owners; water supply wells within 1,000 feet of the source area; surface water bodies; surface water intakes (for public water supplies and springs) that are within 0.5 miles; and identification of subsurface structures and utilities. 7 Atlas Distributing Company, Phase II LSA Final January, 2003 • 4.2.1 Surface Water Beaver Creek Pond and Beaver Creek is located approximately 1 mile west of the site. Beaver Creek Pond is created by a artificial dam located near Mt. Gilead Church (Figure 1). 4.2.2 Wellhead Protection Areas The Wellhead Protection Program (N.C. Division of Environmental Health, Public Water Supply Section) was contacted to determine whether a wellhead protection area was located near the site. There were no Wellhead Protection programs listed in Fayetteville. The closest wellhead protection programs identified were located in Bladen County (Bladenboro) and Robeson County (Lumberton, Parkton and Red Springs). 4.2.3 Deep Aquifers in the Coastal Plain Region • According to Geologic Map of North Carolina, (1985), the site is located in the Atlantic Coastal Plain Physiographic Province of North Carolina. The surficial materials at the site are mapped as being near the boundary of the Cretaceous age Black Creek and Cape Fear Formations. Sohl and Owens (1991) describe the Cape Fear Formation as being "widespread in the sub -surface in North and South Carolina." Subsurface features are described as "rhythmically interbedded sands that are green gray to bluish -green, thin bedded to less commonly thick -bedded, and fine to coarse; and thin to thick bedded, dark gray to greenish gray clays. Locally the sands are cross bedded but are for the most part, massive and clayey, hence poorly sorted." Overlying the Cape Fear Formation is the Black Creek Formation, which is commonly described as having silts/sands and clays as well as beds of graded sands. These formations are part of primary water bearing units in the eastern North Carolina area. Hydraulic conductivity data for these aquifers and confining units in this area was not available. In the area near the site, the Cretaceous sand yields large quantities of water to wells (Schipf, 1961). The primary source of water for this aquifer is infiltrated rainfall. The surficial 0 deposits aquifer transmits water laterally to streams and serves as a source bed, holding the Atlas Distributing Company, Phase II LSA Final January, 2003 • water that eventually moves downgradient to the deeper aquifers within recharge areas (Winner and Coble, 1989). 4.2.4 Subsurface Structures There were no basements identified during the receptor survey. The only underground structures identified in the receptor survey were underground utilities. Most notable is the storm drain located near MW-1. The storm drain appears to be entrenched above the water table. 4.2.5 Area Land Use The site is located in Fayetteville, adjacent to Cliffdale Road. Site Specific Conditions • Adults work at the facility, which is a beverage warehouse and distributorship. • • The site is restricted via chain link fence and automatic gates. The groundwater is separated from the employees by a 6-foot thick layer of soil, capped with concrete and asphalt in most areas. • The distance from the source area, which is the eastern UST location, to the nearest residence or place of public assembly is approximately 1,000 feet. • The zoning status of the site and surrounding area is mixed commercial and residential. • 4.2.6 Property Owners and Occupants Properties adjacent to the site were cataloged and the owners' names and addresses were recorded (Table 1) from Cumberland County tax records. The results of the survey indicated 5 properties adjacent to the site. The properties were either reported or observed to not contain supply wells. The property owners are listed in Table 1 and the property boundaries are shown on Figure 2. 9 Atlas Distributing Company, Phase H LSA Final January, 2003 • 5.0 SITE TOPOGRAPHY, GEOLOGY AND HYDROGEOLOGY The following sections describe the regional geologic conditions and the methods employed to obtain physical data that support our discussion of the local geologic and environmental conditions. 5.1 Topographic Conditions As shown on Figure 1 (Delorme 3-D TopoQuads, 1999, Yarmouth), the topography of the site is relatively flat. The elevations shown on Figure 1 indicate the property to be approximately 230 feet above mean sea level (msl). Drainage in the vicinity of the source area generally leaves the site via surface runoff. The site is generally located between north -south trending valleys created by Buckhead Creek to the east and Beaver Creek to the west. 5.2 Regional Geology and Hydrogeology Suriiicial Aquifer - The groundwater head elevation (referenced from "above mean sea • level or ASL") associated with the surficial aquifer monitored by the DWR in a well located in Bladenboro, N.C. (well No. Z41U1) ranges from approximately 113 ft to approximately 106 ft ASL and averages approximately 110 ft. The land surface elevation at this well is 114.75 ft., resulting in a water level located approximately 43-feet below grade. Upper Cape Fear Aquifer - The groundwater head elevation associated with the Upper Cape Fear Aquifer is monitored by the DWR in Bladenboro, N.C. (well No. Z 41U2) and Boardman, N.0 (well No. AA 43 Q 1) The groundwater head elevation in well No Z 41U2 has fallen from an elevation of approximately 69 ft in 1975 to a current elevation of approximately 20 ft. The land surface elevation at this well is 116.04 ft, resulting in a current water level located approximately 96 feet below grade. The groundwater head elevation in well No. AA 43Q1 has fallen from an elevation of approximately 75 ft in 1972 to a current elevation of approximately 20 ft. The land surface elevation at this well is 80.46 ft, resulting in a current water level located approximately • 60.5—feet below grade. S Atlas Distributing Company, Phase H LSA Final January, 2003 The gradational decline in head elevation in the Upper Cape Fear Aquifer is consistent with observations made by commercial well drillers and pump installers. They report an estimated 1 to 2 foot per year drop in head elevations in deeper aquifers of the US Coastal Plain since the 1960s (interviews with Olin, Guy, Roy and Jimmy Cribbs-Cribbs Well Drilling, Mullins, S.C. and Fred and Wayne Grosch-Grosch Well Drilling, Dublin Ga.) Based on discussions with industrial and commercial well drillers operating in the region, the regional uses of the deeper aquifers are primarily municipal supply wells; wells associated with pork and poultry operations, and irrigation wells. 5.3 Site Geology On the basis of the soils encountered from vertical boring activities at the site, the following limited interpretation of the site geology was developed. The boring logs have been included as Appendix B. In general, the geologic material encountered from the ground surface was observed to be orange, brown to light gray sandy clay and clay to approximately 15 feet below land surface 40 (bls) in which, a silty, fine to coarse, sand is encountered to approximately 20 feet. Red orange, mottled, massive sandy clay was present to approximately 33 feet in which silty fine sand was observed to 38 feet. Soft, dark gray massive clay was observed from 38 to 40 feet bls. Borings were not advanced beyond 40 feet as part of this investigation. • 5.4 Soil Borings and Sampling As documented in the Site History Section, wells MW-1 and MW-2 were installed as part of the Phase II ESA in 1994. In December 2002, EHC drilled two soil borings (MW-3 and MW-4) to explore subsurface conditions and allow for type II monitoring well construction and deep well MW-2D (type III well) as part of Phase II LSA activities. The soil boring/wells were drilled using mechanical drilling equipment, hollow -stem auger (HSA) and mud rotary techniques. The locations of soil borings/monitoring wells are displayed as monitoring wells on the Site Map (Figure 3) including property boundaries, buildings, and former UST and pump island locations. 11 Atlas Distributing Company, Phase H LSA Final January, 2003 • 0 Mechanical drill rig soil samples were collected, via split spoon, at 5-foot intervals until boring termination. The soil samples and records of well construction details were logged in a field book by EHC personnel. Boring logs for each location are included as Appendix B. Ten soil samples were collected during tank removal activities in 1991 as Sample Test 1 through 10 for analysis using TPH 5030. Petroleum hydrocarbons were BDL in each of the samples. As part of Phase II LSA activities, a soil boring was advanced to the water table near MW- 2 for sampling purposes. The soil sample nearest to the water table (LSA-1, 3.0-4.0 feet) was submitted for analysis of volatile organic compounds (VOCs) using Environmental Protection Agency (EPA) Methods 8260 with 5035 preparation, semi -volatile compounds using EPA Method 8270, Massachusetts Department of Environmental Protection (MADEP) analysis of volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH). Petroleum compounds were "below detection limits" (BDL) in the submitted samples. Laboratory reports are included in Appendix D. 6.0 GROUNDWATER INVESTIGATION 6.1 Site Hydrogeological Study Methods A description of hydrogeologic and environmental conditions at the site was developed from information gathered from the soil boring logs, water level measurements, topographic maps, published information sources and groundwater sample analysis. The following sections describe the regional and site hydrogeology as it relates to groundwater movement and the detected petroleum compounds in ground water at the site. 6.1.1 Monitoring Well Installation The type II monitoring wells (MW-1, MW-2, MW-3, and MW-4) consists of a 10 feet length of two-inch inside diameter (ID), schedule 40 polyvinyl chloride (PVC) well screen with 0.01- inch slots attached by threaded joints to an appropriate length of two-inch ID, and schedule 40 PVC riser pipe. Clean quartz filter sand was placed in the annular space between the well and the borehole to a level at least one foot above the top of the well screen. Approximately two feet of a hydrated bentonite seal was placed above the filter sand pack. The remaining annular 12 Atlas Distributing Company, Phase H LSA Final January, 2003 is space was then backfilled to the ground surface with a cement-bentonite grout. EHC monitoring well construction details are provided in Appendix C. The Type III well (MW-2D) is a deep telescoping well, which includes inner, and outer casings. The Type III well was constructed by first installing an outer 6-inch casing to separate the upper and lower portions of the aquifer. The outer casing was then pressure grouted with a neat cement mixture, and allowed to cure for 24 hours thereby sealing the upper portions of the surficial aquifer. After 24 hours, the annulus of the outer casing was reamed out and drilling was continued to the desired depth of the lower portions of the surficial aquifer. After completion of the borehole, a 2-inch inner casing and well screen was constructed inside the casing and borehole in a manner similar to the type II well using a five- foot well screen. Monitoring well construction details for each of the site wells are provided in Appendix C. The wells were developed using a pre -cleaned disposable polyethylene bailer. Groundwater was removed until the water became reasonably clear. Field readings including pH/temperature and conductivity were taken to insure that reasonably stabilized ground -water parameters were achieved. 6.1.2 Groundwater Gauging and Sampling EHC personnel collected groundwater samples from monitoring wells MW-1, MW-2, MW- 2D, MW-3 and MW-4 on December 16, 2002 as part of the Ph. II LSA investigation. Prior to sampling, depth to groundwater was measured from the top of the PVC casing at the well. Depth to water readings and field measurements are included as Table 2. Water from the well was then purged using pre -cleaned, dedicated, high -density polyethylene disposable bailing equipment. Upon collection, the water samples were placed into laboratory -prepared containers, packed on ice in coolers and delivered via express courier to Environmental Science Corp. (ESC) in Mt. Juliet Tennessee (a North Carolina Certified Laboratory) for analysis. The samples were submitted for analysis of petroleum constituents via EPA Methods 6210D with iso-propyl ether (IPE), methyl tert-butyl ether (MTBE), ethylene di -bromide (EDB) and xylenes, semi- volatiles via EPA 625 plus 10 tentatively identified compounds (TICS), MADEP analysis of VPH and EPH and lead via EPA Method 6010/3030C preparation. Appropriate chain-of- 13 Atlas Distributing Company, Phase H LSA Final January, 2003 • custody records were maintained through the sample collection and shipment of each sample, and are attached with the laboratory reports as Appendix D. 7.0 RESULTS 7.1 Ground Water Flow Directions Ground water levels, obtained on December 16, 2002 were observed in site monitoring wells to range from approximately 6 feet BLS in the shallow portion of the surficial aquifer. Depth to water in Well MW-2D was gauged 22 feet below the top of casing. Ground water elevations, which are presented in Table 2, have been contoured on Figure 4. Please note that the elevations are relative to a temporary benchmark with assumed elevation of 100 feet and that the deep well is not included in the contours. The December 16, 2002 data suggest that ground water flow is to the north with a hydraulic gradient of approximately 0.005 ft/ft. • 7.2 Groundwater Sample Analyses A summary of ground water chemical analysis data as compared to the 2L Standards and GCL's is included as Table 3. Copies of the laboratory reports and chain -of -custody records for these analyses are included in Appendix D. A summary of selected petroleum constituent results including benzene, toluene, ethyl benzene, and total xylenes (BTEX) is included as Figure 5. As reported previously, chemical analysis of ground -water samples has been performed on wells MW-1 and MW-2 dating back to 1994. As shown on Table 4, several constituents including BTEX, and MTBE exceeded the 2L Standard. Chemical analysis of groundwater samples was collected on December 16, 2002 as part of the Ph. II LSA investigation from MW-2D, MW-3 and MW-4. As shown by the Table, the recent analyses indicate benzene exceeds the 2L Standard of 1.0 micrograms per liter (ug/1) in well MW-2 with the concentration of 1.4 ug/1 and in well MW-3 with the concentration of 14 ug/L. Chloroform was detected in well MW-2D with the concentration of 12 ug/L and lead was detected at 18 ug/L. The 2L Standard for chloroform and lead is • 0.19 ug/L and 15 ug/L respectively. The TIC library search identified several possible 14 Atlas Distributing Company, Phase H LSA Final January, 2003 • organic compounds in each of the wells including 1-ethyl-2 methyl benzene, 1,2,4- trimethylbenzene, indane, 2-ethyl-1,3-dimethyl benzene, hexadecanoic acid, and eicosane. A complete list is included in the laboratory reports in Appendix D. 2L Standards are not available for most of the TIC compounds. 8.0 CONCLUSIONS Site reconnaissance indicated the surrounding properties as supplied by public water. Water supply wells were not identified within a 1,000-foot radius around the site and impacts to potential receptors were found to be minimal. Additional receptors that may effect risk classification were not observed during Phase II LSA activities. Laboratory analysis of submitted soil samples from the MW-2 location for listed parameters including EPA Methods 8260/8270 and MADEP EPA/VPH indicated petroleum constituents to be BDL. The direction of ground -water flow on the site is north with an average hydraulic gradient • of approximately 0.005 ft/ft. Recent sampling data indicates benzene exceeds the NCAC 2L Standard in wells MW-2 and MW-3 with concentrations of 1.4 ug/1 and 14 ug/L respectively however, GCLs were not exceeded in the constituents analyzed for the 5 sampled wells. NCAC 2L Standards for chloroform and lead are exceeded in MW-2D. Metals occur naturally in soil and in dissolved phase in ground water. The turbidity (suspended sediment) of a ground water sample can affect the concentration of the metals detected. Analysis of metals by EPA Method 6010 or 3030C preparation requires the sample to be preserved by nitric acid at the time of collection. The nitric acid in the sample container may dissolve metals suspended in the sediments of a turbid sample causing and increase in the concentrations of those metals. Therefore, the lead detected in MW-2D may be naturally occurring rather than as the result of a release. Chloroform is associated with the chlorination and disinfection of the public water supply. The bentonite slurry mixture used to drill the well was mixed using the Fayetteville public water supply. It is therefore likely the chloroform came from that source. El 15 Atlas Distributing Company, Phase H LSA Final January, 2003 Downgradient well MW-3 was BDL indicating that it does not appear the plume is migration from the site with natural ground water flow. Based on limited receptors and migration pathways, commercial use, and concentrations of detected constituents that do not exceed the GCL, EHC concludes that the release at this site appears to pose limited risk to health and environment. According to risk -based rules for USTs, it appears this site should be considered as "low risk." 9.0 RECOMMENDATIONS On the basis of the data presented and our conclusions, EHC recommends the following: • Submit this Phase II LSA report to the NCDWM Fayetteville Regional Office for review, and comment. • • 16 • REFERENCES Delorme 3-D TopoQuads, 1999, Yarmouth, ME 04096, Fayetteville. Geologic Map of North Carolina, 1985, North Carolina Geological Survey. Schipf, Robert G., Geology and Ground -Water Resources of the Fayetteville Area, Ground - Water Bulletin Number 3, North Carolina Department of Water Resources -Division of Ground Water, Raleigh, 1961. Winner & Coble, 1989, U.S. Geological Survey, Open -File Report 87-690, Raleigh, North Carolina, 57 - 62 pp. • 0 • • • TABLES TABLE 1 ADJACENT PROPERTIES Atlas Distributing Company 5510 Cliffdale Road Fayetteville, NC ,/ ' IF /r � I /n ...: 0417-06-0763 Site - Fomer Atlas Distributing 5510 Cliffdale Rd. Fayetteville NC 28305 0417-06-6874 Marsh and Evans LD-Leisure Living 5500 Cliffdale Rd. Fayetteville NC 28314 0417-06-6207 New Sanford Milling Company PO Box 53186 Fayetteville NC 28305 0417-06-6874 Sharlene Williams PO Box 53646 Fayetteville NC 28305 0417-07-5002 Sharlene Williams PO Box 53646 Fayetteville NC 28305 0407-96-6586 March F. Riddle PO Box 53646 Fayetteville NC 28305 0407-97-7119 Triangle Builders Wholesale PO Box 53646 Fayetteville NC 28305 0417-07-1165 riang a Builders o esa a ox 5 4 ayettevl eNC 28305 Notes: Taken from Cumberland County Tax Records Prepared by: David Brown Map ID Number Corresponds to Figure 2. F:ProjectSites/Atlas Distributing/Adj Properties.xls • 0 0 C9-C1 0 Aromatics NA NA NA ND NA NA NA NA NA NA 130 ND ND 130 210 NS Ma OMIT w M11 77 U9777777 NAB. AJI :7NI . . .................. - m C9-C18 Aliphatics NA NA NA ND NA NA NA NA NA NA ND ND ND ND 4200 NS 7\0,, MI, IM11 CI 1 -C22 Aromatics NA NA NA I ND NA NA NA NA NA NA ND ND ND ND 210 NS r g N Results are presented in micrograms per liter (ugIL). ND = "Not Detected" above laboratory detection limits. Refer to laboratory reports for detection limits ISIS - No Standard NA = Not Analyzed H:Proiects%das%h20Chem Summ.xis • 0 FIGURES � 0 10 � 0 ; 77. ov .0 . , I '41 L 3-1) TopoQuads C1999 DeLorme, Yarmouth, ME 04096 Source Data: USGS FIGURE 1 1:24000 Detail 13-1 Datum WOS84 Topographic Map EHC Atlas Distributing, Inc. ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS 5510 Chffdale Road HYDROLOGY - GEOLOGY - EXPLORATION - ANALYTICAL Fayetteville, North Carolina 0417-06-6874- nfh*" � �<' 0407-96-6586 ��'�� a �,� r.,F J-` .�•��_ � -'--� - .. Aid Surrounding Properties Map s iV A Atlas Distfibu&g, Inc. e. x , ,. - • APPENDIX A NOTICE OF REGULATORY REQUIREMENTS • 09/12/02 THU 10:39 FAX 910 864 5329 _ DOUBLE EAGLE North Carolina Department of Environment and Natural Resources • Division of Waste Management Underground Storage Tank Section Fayetteville Regional Office Michael F. Easley, Governor William G. Ross Jr, Secretar}, Dexter R. Matthews, Director September 5, 2002 Mr. John L. Beard Atlas Distributing Company, Inc. 1214 Morganton Road Fayetteville, NC 28305 Re: Notice of Regulatory Requirements 15A NCAC 2L .0115(c) 00;j A7441illi*j AftRYA � NCDENR. Risk -based Assessment and Corrective Action for Petroleum Underground Storage Tanks Atlas Distributing Company (farmer location) 5510 Cliffidale Road Fayetteville, Cumberland County Facility ID #: unregistered Incident #: pending issuance Dear Mr. Beard: • Information received by this office on August 27, 2002 confirms a release or discharge from a petroleum underground storage tank (UST) system formerly located at the above -referenced location. Records indicate that Atlas Distributing Company, Inc., was the owner of this UST sys::m and is considered the responsible party for the release or discharge. This letter is a standard notice explaining the actions you must take as a result of the release or discharge in accordance with North Carolina statutes and rules. The UST Section of the Division of Waste Management administers the state's rules for USTs and the required response for petroleum releases. Those rules are located in Title 15A, Subchapter 2L and Title 15A, Subchapter 2N of the North Carolina Administrative Code (NCAC). As a responsible party, you are required to comply with the release response and corrective action requirements of 15A NCAC 2L .0115(c), which include the requirements established in 15A NCAC 2N. Listed is a general description of actions you must take to comply with State rules. For a detailed description of your requirements, please refer to the enclosed rules and the most rel:ent version of the UST Section Guidelines for Assessment and Corrective Action. The guidelines are available on the Internet at http://wastenot.enr.state.nc.us or may be purchased from the UST Section for a fee of $8.50. To purchase a copy of the guidelines, please send a check made payable to DUNR to: DENR / DWM / UST Section 1637 Mail Service Center Raleigh, NC 27699-1637 • 225 Grcen Street, Suite 714, Fayetteville, North Carolina 28301-5043 Phonc: 910-486-1541 / FAX: 910-486-0707 / Internet. http://w2stenot.enr.stitc.nc.us AN EQU:U.OPPORTUNrtY / At•TIRNIATWL AcrtON EMPLOYtiR / SOY. POsr CONSUMPR PAPER 0002 09/12/02 THU 10:39 FAX 910 864 5329 DOUBLE EAGLE 19003 • Required Actions: 1) If you have not already done so, you must take immediate action to prevent any fur -her release of the regulated substance into the environment and to identify and mitigate any tire, explosion and vapor hazards; remove any free product; and comply with the requiremen�.; of Rules .0601 through .0604 and .0701 through .0703 and .0705 of Subchapter 2N; 2) Incorporate the requirements of 15A NCAC 2N .0704 into the report to be submitte:1 in accordance with 15A NCAC 2L .0115 (c)(3) or (c)(4), whichever is applicable (see Item #3 below). This shall constitute compliance with the reporting requirements of 15A NCAC. 2N .0704(b); 3) If it can be demonstrated that localized soil contamination was cleaned up at the time of link removal, you may submit a Soil Contamination Report in accordance with 15A NCAC 2L.0115(c)(3). The Soil Contamination Report must demonstrate that the soil remainin;; in the sidewalls and at the base of the excavation is located in the unsaturated zone and does not exceed either the soil -to -groundwater or the residential maximum soil contaminant concentrations, whichever are lower. A Soil Contamination Report is not appropriate for sites where contamination is situated directly on top of bedrock or once a tank clo:�ure excavation has been back -filled. In both cases, a Limited Site Assessment Reporl is required. A Soil Contamination Report, if applicable, is due in this office no later than December 15, 2002. Upon approval of this report, the Department may issue a later indicating that no further action related to this incident is required; or, 4) If the requirements of 15A NCAC .0115(ex3) cannot be met as described in Item #3 above, • submit a Limited Site Assessment (LSA) Report in accordance with 15A NCAC 21, .0115(c)(4), containing information needed by the Department to classify the level of risk to human health and the environment posed by the discharge or release. The LSA Report is due in this office no later than January 15, 2003. Based on a review of the informal_ on submitted in the LSA, the Department will classify the risk of the discharge or release: as high, intermediate or low. At that time, the Department will also classify the land use of -:he site as either residential or industrial/commercial. You will be notified of the risk and land use classifications once review of your LSA Report is completed. 5) Please note that before you sell a property or request a "No Further Action" determination for a property that has not been remediated to below "unrestricted use" standards, you must fV-. a Notice of Residual Petroleum ("Notice") with the Register of Deeds in the county where the property is located (NCGS 14313-279.9 and 143B-279.11). Unrestricted use standards for groundwater and soil are the groundwater quality standards and interim standards contai:ed in 15A NCAC 2L .0202 and the residential maximum soil contaminant concentrati :lns established in 15A NCAC 2L .0115, respectively. The Notice must first be approved and notarized by the UST Section prior to conveyance of a property or prior to receiving a "No Further Action" determination, whichever occurs first. The Notice must contain a legal description of the property containing the source of contamination and legal description, of any other properties that you own (or control) that are contaminated by the release. '.'he Notice must include appropriate land use restrictions for these properties. In addition, the Notice must identify all other properties (adjacent, adjoining, downgradient, etc.) on which 0 DOUBLE EAGLE 0 004 contamination is known to exist at the time the Notice is prepared. If contamination. is located on more than one parcel or tract, the UST Section may require that a composite neap or plat be prepared. After the Notice is filed with the Register of Deeds, a certified coPy of the filed Notice must be submitted to the UST Section. Additional guidance including the language and format of the Notice is available by calling this regional office or visiting the UST Section web site at htip://wastenot.enr.state.nc.us. If you believe that any of the information requested above has already been submitted, please notify me of the date, title, and content of the documents that contain the information. Your prompt attention to the items described herein is required. Failure to comply with the State's rules in the manner and time specified may result in the assessment of civil penalties and /or the use of other enforcement mechanisms available to the State. Each day that a violation continues may be considered a separate violation. If you believe you are not the responsible party, notify the is ST Section within 15 days of receipt of this notice. Please note that performing assessment and cleanup work that is not required under 15A NC!kC 2L.0115 is not reimbursable from the Commercial or Noncommercial Leaking Petroletun Underground Storage Tank Cleanup Funds. If you have any questions regarding the actions that must be taken or the rules mentioned in -:zis letter, please contact me at the letterhead address or at (910) 486-1541. If you have any questims regarding trust fund eligibility or reimbursement, please contact the UST Section Trust Fund Bra::ch at (919) 733-8486. • Sincerely, Kenneth E. Currie UST Section Enclosures: 15A NCAC 2L .0115 Notice of Residual Petroleum Format and Instructions c: FRO Incident Management Files Mr. Scott Jurgcnsen Harrispark Properties P.O. Box 1190 Raleigh, NC 27602 Mr. James Joyner, Project Manager TRC Environmental Corp. 516 N. West Street Raleigh, NC 27603 0 • APPENDIX B 0 BORING LOGS 0 • • 0 BORING LOG RECORD Environmental Hydrogeological Consultants 207 West Fourth Avenue Red Springs, North Carolina 28377 Ph. (910) 843-4456 Fax (910)843-5376 E H C Inc. Depth Blows per 6" Rec (in.) Description Remarks (USCS Symbol) 1- 5-8-12-18 24 (5.0-7.0 feet) 5- Medium orange to red -brown, sandy CLAY. Stiff sc mottled. 3-4-4-6 18 (10.0 -12.0 feet) As above sc 10- 4-1-4-4 2 (15.0 -17.0 feet) Light brown to tan, silty, fine to coarse SAND. sm 15- Wet. 2-6-6-7 18 (20.0-22 feet) 20- Light tan to buff, sandy CLAY over gray, massive, cl mottled sandy CLAY. Boring Terminated at 23.0 feet. Notes: • I 0 Depth Blows per 6" Rec (in.) Description Remarks (USCS Symbol) 1- 5-7-12-18 24 (5.0-7.0 feet) 5- Red -orange, stiff, massive, mottled CLAY. sc 3-4-5-7 8 (10.0 -12.0 feet) Red orange to gray, mottled sandy CLAY. sc 10- - 5-5-7-5 12 (15.0 -17.0 feet) Yellow brown to red gray, silty, fine to coarse sm 15- SAND, poorly sorted, wet. Boring Terminated at 17.0 feet. 20- Notes: LJ 0 BORING LOG RECORD Environmental Hydrogeological Consultants 207 West Fourth Avenue E Red Springs, North Carolina 28377 H Ph. (910) 843-4456 C Inc. Fax (910)843-5376 Site Name Atlas Distributing rted !2�8142 Job Location Fayetteville,, NC ;, Gateomple#ed . 42�1a10� I Drilling Method Mud Rotary Latitude IN35 3.55,V I Longitude JW78. deg. 57.986' Depth Blows NA Description Remarks (USCS) Soil Screen (ppm) 1- 0.0-17 feet Boring paired with MW-2. Refer to the MW-2 NA 5- boring log. 10- 15- 10-10-16-17 (18.0-20.0 feet) 20- Brown to gray, massive, very silty fine SAND. sm Driller noted fat clay layer at 22' cl 23- 10-12-16-17 (23.0-25.0 feet) - As above sm Notes: Drilled by Mid -Atlantic Drilling na = Not Available • r LJ BORING LOG RECORD Environmental Hydrogeological Consultants 207 West Fourth Avenue E Red Springs, North Carolina 28377 H Ph. (910) 843-4456 C Inc. Fax (910)843-5376 Site Name Atlas Distributing Date Started s : ,12/91,02; Job Location Faye$eville; NG Date Compieted,_ 12fta/02 ". Boring Number MW 2D ;(Sheet 1) Depth to Water - Z41.42' =' , Geologist D. Brown lVeasulrePtr , Top of Casing Drilling Method Mud Rotary tit N35 3.554' FL40naitvde" W78 deq. 57986' Depth Blows 24 in Description Remarks (USCS) Soil Screen (ppm) 25- (28.0-30.0 feet) 1-5-5-4 Red gray to pink, soft, plastic CLAY. cl 30- - 2-4-7-7 (33.0-35.0 feet) 35- Clay slough and concretions Orange -red silty, fine, sand and sand stringers. sm (38.0-40.0 feet) 40- 4-4-5-7 Dark gray, soft, slightly sand, micaceous, plastic cl - CLAY. Boring Terminated at 40 feet. 45- 48- Notes: Drilled by Mid -Atlantic Drilling na = Not Available • APPENDIX C WELL CONSTRUCTION RECORDS • North Carolina - Department of Environment, Heallh, and Natural Resources Division of Environmental Management - Groundwater Section P.O. Box 29535 - Raleigh, N.C. 27626-0535 Phone (919) 733.3221 u, / FOR OFFICE USE ONLY pUAD. NO. SERIALNO. Long. RO Min" Basin WELL CONSTRUCTION RECORD Basin Code Basin coda `LLING CONTRACTOR: L%�C, 1 U/C-. Header Ent' GW-1 Ent STATE WELL CONSTRUCTION DRILLER REGISTRATION NUMBER: � D 2 9 PERMIT NUMBER: 1. WELL LOCATION: (Show sketch of the location below) Nearest Town: r �'=T�7'`f�'%C`` County: eU& (Road, Community. or Subdivision and Lot No.) �446-�-�' 2. OWNER 11tl �1U41; �ia _ .� ADDRESS c 421O (' -> ez',a (Street or Route No.) ,0 c 2,J`3403 CitjorTown State Zip Code 3. DATE DRILLED USE OF WELL%�[�f/%-�0�- 4. TOTAL DEPTH 2 v 5. CUTTINGS COLLECTED YES ❑ NOX 6. DOES WELL REPLACE EXISTING WELL? YES F NO ] 7. STATIC WATER LEVEL Below lop of Casing: _T FT. (Use "+' it Above Top of Casing) 8. TOP OF CASING ISM-2eAl 420.nftmus Land Surface* ' Casing Terminated aVor below land surface is illegal unless a variance Is Issued DEPTH From To s� /D Z0/2 J DRILLING LOG Formation Description J• � In accordance with 15A AC 2C .0118 9. YIELD (gpm): METHOD OF TEST l�,r/ I(io-�� F ascr • D.� o�. 10. WATER ZONES (depth): _ /4/^t e4,00cb.L•// /:1 ri, .CHLORINATION: Type 12. CASING: Depth Diameter From 0—To -L `= Ft. From To Ft. From To Ft. 13. GROUT: Depth From To _4 Ft From _46 To Ft 14. SCREEN: Amount If additional space is needed use back of form Wall Thickness LOCATION SKETCH or Weight/Fl. lApterial (Show direction and distance from at least two State UC— Roads, or other map reference points) Material Wthod e d4crYUu.t 4c I Depth Diameter Slot Size material From /O _ To 10 Ft in. •A2Z(.L in. From To Ft. in. in. �-� •�- .-. From To Ft. in. in. 15. SAND/GRAVEL PACK: _ Depth §ize Material ..�. .�.. `��• From To 20 Ft. 2A- ��)""L� 664r t>+c From To Ft. 16. REMARKS: -- — •1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER. SIGNATURE OF CONTRACTOR (A AGENT / 1 DATE GW-1 REV. 9191 Submit original to Division of Environmental Management and copy to well owner. North Carolina - Department of Environment. Health, and Natural Resources Division of Environmental Management - Groundwater Section P.O. Box 29535 - Raleigh, N.C. 27626.0535 Phone (919) 733-3221 WELL CONSTRUCTION RECORD &LING CONTRACTOR: FOR OFFICE USE ONLY QUAD. NO. SERIALNO. Lal. ,._ Long. RO Minor Basin Basin Coda Header Ent.4 Gw-1 Ent --� DRILLER REGISTRATION NUMBER: STATE WELL CONSTRUCTION f (�Z PERMIT NUMBER: 1. WELL LOCATIQLL SShow sketch of the location below) Nearest Town: - County:%�`^"� — — (Road, ( 2. OWNER ADORE: and or Route No.) DEPTH 6 m TO t!� �w •Sr 3. City orXown State Zip Code DATE DRILLED X%�Dti USE OF WELL A 2• S J 4. TOTAL DEPTH 5. CUTTINGS COLLECT D YES 0 NOCg --• O Z. (D 6. DOES WELL REPLACE EXISTING WELL? YES NC1tjj� 7. STATIC WATER LEVEL Below lop of Casing: FT. 8. �I (Use 't' if Above Top of Casing) TOP OF CASING IS _lam _ +**•theft Land Surface' ' Casing Terminated atlor below land surface Is Illegal unless a variance Is Issued In accordance with 15 2C .011 b 9. YIELD (gpm):_e� METHOD OF TEST WIA_• O — /O. u 10. WATER ZONES (depth):. 46LORINATION: Type 12. CASING: Depth Diameter From To Ft. From To Ft. From To Ft. 13. GROUT: DRILLING LOG Formation Description Q�ifSi�fc /"l.Rd—CoblWc.,f,,tcd r<LCt, d/'d�Ls.RJ �dlcclw f�/�O�,ow Amount If additional space is neec Wall Thickness LOCATION SKETCH of eMaterial (Show direction and distance from at least two State �C- Roads, or other map reference points) Depth Material Njqthod From To Ft. Wfjvou.c From To 3 Ft. 51, pu^ 14. SCREEN: Depth Diameter Slot Size M erial From _4 To Ft ? in. • azzl in. 1/L From To Ft. in. in. From To Ft. in. in. t 15. SAND/GRAVEL PACK: .'.—� ..� Depth S' e Material I From To ZV Ft. 4z' rr '= Iw & W �K IIIiO�d�:X tAa.t+rrt w1N. •11... O..�YIM y.4I From To Ft.� •"' 16. REMARKS: — — Of DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER. v SIGNATURE OF CONTRACTOR OR AGENT I /DATE GW-1 REV. 9,91 Submit original to Division of Environmental Management and copy to well owner. 0 ct, - LA WELL CONSTRUCTION RECORD Worth Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRACTOR (INDIVIDUAL) NAME (print) C.u-4 J 9AZ-1el— CERTIFICATION # z Iq s( WELL CONTRACTOR COMPANY NAME JL� � � PHONE # J%T 1 gq-?- NN jG STATE WELL CONSTRUCTION PERNIIT# 1• ASSOCIATED WQ PERMIT# N1.4 (if applicable) (if applicable) 1. WELL USE (C ck Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑ Monitoring IT Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use 2. WEt.L LOCATION: Topographic/Land .�e: ' setting� Nearest Town: I.Z. County ���-r+t���Ci �� ❑Ridge ❑Slope ❑Valley 13Flat t! 6 (• F d — 0 6 e , ' t— X� , (check appropriate box) (Street Name. Numbers, Community, ubdivision. Lot No.. Zip Code) L tit n ttftde,of well location 3. OWNER: �c[�0 l , (-C35 �y Lv rs � -7. g ) . (degrees/minutes/seconds) Address u c Latitude/longitude source:t?rPS❑Topographic map p (Street or R uteN .) r (check box) X=1 F r�DEPTH DRILLING LOG City or Town St a Zip Cosa From TQ Fo at' n Description Area code- Phone number s 1 5 4. DATE. DRILLE! LLUZ- 5. TOTAL DEPTH: 6. DOES WELL REPLACE EXISTING WELL? YES0 L!r ; i6 7. STATIC WATER LEVEL Below Top of Casing: FT. ( Use --- if Above Top of Casing) A • S. TOP OF CASING IS ' 'V, u 4-- FT. Above Land Surface* -Top of casin; terminated at/or below land surface requires a variance in •accordant w th I5:\ NCAC 2C .01ld. - 9. FIELD (epm): 4- j�-N METHOD OFTEN 10. WATER ZONES (depth): <:T` I S LOCATION SKETCH 1 1. DISINFECTION. Type ti 14 Amount Show direction and distance in miles from at least t'_. CASING: Nall Thickness two State Roads or County Roads. Include the road Dcpth�� Diameter or Wei_ht'Ft.Material numbers and common road names. From To Ft._-')— S< < 4c) VV_ From To Ft. From To Ft. 13. GROUT: Depth Material /+ I thud From d Tom_ Ft. Sfc),-,- IN From To Ft. L' 14. SCREEN: Depth Diameter Slot Size laSerial From eZ To Ft. in. i OIC• in. From To Ft. in. in. w 1 OL 15. SANDiGRAVEL PACK: Depth. t laterial From 3 To k 77— Ft. From To Ft. • 16. REMARKS: `1 io." I DO H - 1" CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STAtNDARD,0. AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER cv— SIGNATURE OF PERSON CONSTRUCTING THE WELL v' DATE e. Submit the original to the Division of NN ater Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, INC 27699-1636 Phone No. (919) 733-3221. within 30 days. GW-I REV. 07/2001 w-3 WELL CONSTRUCTION RECORD dWorth Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRACTOR (INDIVIDUAL) NAME (print) w CERTIFICATION # •29st NVELL CONTRACTOR COMPANY NAME r= He— _) IX PHON,EI # �(D) $�/3• �/y �C� S'rA-f E WELL CONSTRICTION PER.N11T# _ ri/1i ASSOCIATED WQ PERMIT# (if applicable) (if applicable) 1. WELL USE (Cbeck Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑ Monitoring Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use 2. WELL LOCATION: Topographic/Land setting Nearest Town: .'� ' Ifz County `v-wt�--z�U ❑Ridge ❑Slope ❑Valley lat (• F� ex" rtt �C �GS� (check appropriate box) (Street Name. Numbers. Community, ubdivision, Lot No.. Zip Code) Lvitu je/I n Itude,of well location cur 3. OWNER: f • ) 1/ d—' �'"S 0.5t. w (degrees/minutes/seconds) Address I Q Latitude/longitude source: E2 PS❑TopoLraphic map (Street or R ute Nq.) (check box) r',Ue-U. )I, i✓(_ Z -3cr, DEPTH DRILLING LOG To Town St a jd,Zip Code Fro T,� Formation Description If Area rude- Phone number +` 4. DATE DRILLED 12 /41G2- L 5. TOTAL DEPTH: Z-; ` L; 6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO C7� -;:I 7. STATIC WATER LEVEL Below Top of Casing: AFT. (USe --- if Above Top of Casing) • S. TOP OF CASING IS - 'y� e.��- FT. Above Land Surface* *Top of casing terminated at/or below land surface requires a variance in accordant with 1 NCAC 2C .0118. 9. YIELD (,-,pm): OF TEST 10. WATER ZONES (depth): ( Piea,&� I LOCATION SKETCH 11. DISINFECTION. Tvpc ti 6 Amount Show direction and distance in miles from at least 12. CASING: Wall Thickness two State Roads or County Roads. Include the road Depth Diameter or We11-1htF1. Maierial numbers and common road names. From U To (3 Ft. Si i 4c) ►' 4- From To— Ft. From To Ft. 13. GROUT: Depth Nlateri# M (hod From To E Ft. i�G`� I �• From To Ft. -rA 14. SCREEN: Depth Diamzfer Slot Size laSerial � From t_To�Ft. � in. ;-OkC in. 1. V) From To Ft. in. in. 15. SAND/GRAVEL PACK: Depth t laterial From �'I To Z) Ft._ • (t C e- From To Ft. 16. RENIARKS: I DO HEREBYCERTIFYTHAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTIO, TA DARDS, ND THA A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER cC SIGNATURE OF PERSON CONSTRUCTING THE WELL DATE Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, NC 27699-1636 I'lionc No. (919) 733-3221.,*%ithin 30 dues. GW-I REV. 07/2001 '. -V\.j C 01 �� WELL CONSTRUCTION RECORD •North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRACTOR (INDIVIDUAL) NAME (print)_ (.L„: J �!� ✓/`, CERTIFICATION # Z95 WELL CONTRACTOR COMPANY NAME E ni PHONE # fYl�) S43- (Iq SG i v - STATE WELL CONSTRUCTION PERMIT# Jv� ASSOCIATED WQ PERMIT# (if a licable) (if applicable) 1. WELL USE (C ck Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑ Monitoring Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use 2. WELL LOCATION: Nearest Town: A e: I1z County �u-S tb-,, a (Street Name. Numbers, Community, tubdivision, Lot No.. Zip Code) / 3. OWNER: !- ax 44L—S 6.'J. (-c Address I XJ Q (Street or R ute N t , City 5 p��✓ State -b Zip Code Area code- Phone number 4. DATE DRILLED 12- r - I ZI002— 5. TOTAL DEPTH: Ll0, o , r 6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO I]T 7. STATIC WATER LEVEL Below Top of Casing:.? •ti.L* FT. ( Use "+" if Above Top of Casing) • S. TOP OF CASING IS ' 'v-, G +- FT. Above Land Surface* 'Tup of rasing terminated at/or below land surface requires a variance in accordanc with.I5A NCAC 2C .0118. J 9. YIELD (gpm): G� METHOD OF TEST 10. WATER ZONES (depth): 33 G - �?L • 11. DISINFECTION. Type ti Amount l'_. CASING: Wall Thickness Depth Diameter or WeightlFt. 1 enal From 0 To 31 Ft.. S< < 4r} �- From G To 10 Ft. C From To Ft. 13. GROUT: Depth Material 1 thod From Q To� Ft.. Q✓m;� From To Ft. ►-e_A - 14. SCREEN: Depth Diameter Slot Size �ta4erial From'723 To 'iF, Ft.in. GICt in. L From To Ft. in. in. 15. SAND/GRAVEL PACK: Depth Pi3q laterial From 3 X. To_U Ft. t C 6- From To Ftt.. 16. REMARKS: 1 " �N e__ _ ` ` t 4C 1 C- I c_cv Topographic/Land setting ❑Ridge ❑Slope ❑Valley lat (check appropriate box) L�y, itu�e/l deof well loation y �" cv�;3s. $� T (degrees/minutes/seconds) Latitude/longitude source:f6PS❑Topographic map (check box) DEPTH DRILLING LOG From To Formation Description Z - i3 :3 -5- 31--' LOCATION SKETCH Show direction and distance in miles from at least two State Roads or County Roads. Include the road numbers and common road names. ki �1 w �t 5to-1�- 1 GI►r=Fd,� 1 DO HEREB ' TIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRU TION TANDARf�S, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER SIGNATURE OF PERSON CONSTRUCTING THE WELL DATE Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, NC 27699-1636 Phone No. (919) 733-3221, within 30 dais. GW-I REV. 0712001 M • �J 0 Monitoring Well Construction Record Type 11 Environmental Hydrogeological Consultants 207 West Fourth Avenue Red Springs, North Carolina 28377 Ph. (910) 843-4456 Fax(910)843-5376 Former Atlas Distributing Company, Inc. Well Number MW-1 Date of Installation 7/19/94 Job Location Fayetteville, North Carolina Well Material 2" I.D. Sch 40 Top of Casing 98.58 Feet Lock Number Twist Lock Ground Surface 98.70 Feet Sandpack Material #2 Well Pack Geologist B. Bright Static Water Level 5.70 Lock Number Twist Lock jDate Measured 12/16/02 Sandpack Material #2 Well Pack Latitude N35 3.554' Drilling Method Hollow Stem Auger ILongitude W78 57.986' Steel -Flush Mount Cover Locking Well Cap Top Of Grout —0.5 feet Bentonite Seal 6.0 feet Borehole Diameter Unknown Top of Sandpack 8.0 feet Top of Well Screen 10.0 feet Depth of Borehole 20.0' Bottom of Screen 20.0 feet Notes: Static Water Level Measured From the Top of Casing (TOC) • • r 1 L_.J Monitoring Well Construction Record Type II Environmental Hydrogeological Consultants 207 West Fourth Avenue Red Springs, North Carolina 28377 Ph. (910) 843-4456 Fax(910)843-5376 Former Atlas Distributing Company, Inc. Well Number MW-2 Date of Installation 7/19194 Job Location Fayetteville, North Carolina Well Material 2" I.D. Sch 40 Top of Casing 98.48 Feet Lock Number Twist Lock Ground Surface 98.58 Feet Sandpack Material #2 Well Pack Geologist B. Bright Static Water Level 6.11' Lock Number Twist Lock Date Measured 12/16/02 Sandpack Material #2 Well Pack Latitude N35 3.554' Drilling Method Hollow Stem Auger Longitude W78 57.986' Steel -Flush Mount Cover Locking Well Cap Top Of Grout —0.5 feet Bentonite Seal 2.0 feet Borehole Diameter Unknown Top of Sandpack 3.0 feet Top of Well Screen 4 feet Depth of Borehole 14' Bottom of Screen 14.0 feet Notes: Free Product in well. r1 0 Monitoring Well Construction Record Type II Environmental Hydrogeological Consultants 207 West Fourth Avenue Red Springs, North Carolina 28377 Ph. (910) 843-4456 Fax(910)843-5376 Former Atlas Distributing Company, Inc. Well Number MW-3 Date of Installation 12/4/02 Job Location Fayetteville, North Carolina Well Material 2" I.D. Sch 40 Top of Casing 99.79 Feet Lock Number Twist Lock Ground Surface 99.82 Feet Sandpack Material #2 Well Pack Geologist D. Brown Static Water Level 7.72' Lock Number Twist Lock Date Measured 12/16/02 Sandpack Material #2 Well Pack Latitude N35 3.554' Drilling Method Hollow Stem Auger Longitude W78 57.986' Steel -Flush Mount Cover Locking Well Cap Top Of Grout -0.5 feet Bentonite Seal 6.0 feet Borehole Diameter Approx 8" Top of Sandpack 9.0 feet Top of Well Screen 13 feet Depth of Borehole 23' Bottom of Screen 23 feet Notes: Static Water Level Measured From the Top of Casing (TOC) C] Monitoring Well Construction Record Type II Environmental Hydrogeological Consultants 207 West Fourth Avenue Red Springs, North Carolina 28377 Ph. (910) 843- 456 Fax(910)843-5376 Atlas Distributing Well Number MW-4 Date of Installation 1214/02 Job Location Fayetteville, North Carolina Well Material 2" I.D. Sch 40 Top of Casing 97.45 Feet Lock Number Twist Lock Ground Surface 97.65 Feet Sandpack Material #2 Well Pack Geologist D. Brown Static Water Level 6.12' Lock Number Twist Lock Date Measured 12/16/02 Sandpack Material #2 Well Pack Latitude N35 3.554' Drilling Method Hollow Stem Auger Longitude W78 57.986' Steel -Flush Mount Cover Locking Well Cap Top Of Grout -0.5 feet Bentonite Seal 1.0 feet Borehole Diameter Approx 8" Top of Sandpack 3.0 feet Top of Well Screen 5.0 feet Depth of Borehole 17.0' Bottom of Screen 15.0 feet Notes: Static Water Level Measured From the Top of Casing (TOC) I• 16 0 Monitoring Well Construction Record Type III Environmental Hydrogeological Consultants 207 West Fourth Avenue Red Springs, North Carolina 28377 Ph. (910)843-4456 Fax(910)843-5376 Atlas Distributing Job Location Fayetteville, North Carolina Well Material Sch 40 Top of Casing 99.11 Feet Screen Size 0.0101, Ground Surface 99.22 Feet Sandpack Material #2 Well Pack Geologist D. Brown Static Water Level 24.42' Lock Number Master 0536 Date Measured 10/02/02 Sandpack Material 1#2 Well Pack Latitude N35 5.554' Drilling Method lRotary Wash Longitude W79 57.986' Steel -Flush Mount Cover Outer Casing (6") Outer Borehole Diameter =12" Borehole Diameter Approx 6" Bottom of Outer Casing 30.0' IDepth of Borehole 40' Water Level Measured From the Top of Casing (TOC) Locking Well Cap Top Of Grout —0.5 feet Inner Casing ed Outer Casing Bentonite Seal 26 feet of SandDack 32 feet of Screen 38feet • APPENDIX D • LABORATORY REPORTS LJ SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 Ah1ALYT I CAL F2EPOF -F ENVIRONMENTAL HYDROGEOLOGICAL 5309 CONSULTANTS P.O. BOX 902 RED SPRINGS, NC 28377 Sample: NiW # 1 C T� ATLAS DISTRIBUTING Sampler: P S I CHAEL LAi M Date Collected: 7/11/94 Time Collected: Sample type: Water Site I.D.: Analyte Result Units POL -------------------------------- ------ --- 0 Benzene Toluene Ethylbenzene Xylenes, total Methyl-t-butylether ** Surrogate Recoveries Surrogate ------------- BTEX/GRO Surrogate 0 Lab Number-: 94-AO34300 State Certification: 387 Date Received: 7/13/94 Time Received: 9:00 Preservative: HC1 Date Time Analyst Method -------- --------------- ------ 3.0 ug/l 1.0 7/14/94 13:44 G.Norton 602 90.0 ug/l 45.0 7/14/94 13:44 G.Norton 602 590. ug/1 45.0 7/14/94 13:44 G.Norton 602 4920 ug/l 45.0 7/14/94 13:44 G.Norton 602 < 10.0 ug/l 10.0 7/14/94 13:44 G.Norton 602 % Recovery Target Range 105. 70 - 130 Labor; Cory Supervisor SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 ENVIRONMENTAL HYDROGEOLOGICAL 5309 CONSULTANTS P.O. BOX 902 FED SPRINGS, NC 28377 Sample: MW #2 rP.eXMtU&ltri) ATLAS D STRIBUTING Sampler: t � I CHAEL LAMM Date Collected: 7/11/94 Time Collected: Sample type: Water Site I.U.: Analyte i---- Benzene Toluene Ethylbenzene Xylenes, total methyl-t-butyl ether ANAL.YT I CAL FtEF="OFtT Lab Number: 94-AO34301 State Certification: 387 Date Received: 7/13/94 Time Received: 9:00 Preservative: HC1 Result Units FQL Date Time Analyst Method -------------- ------ ------------- --------------- ------ * Surrogate Recoveries ** Surrogate ------------- BTEX/GRO Surrogate 0 4490 ug/l 90.0 7/14/94 13:44 G.Norton 602 18900 ug/l 90.0 7/14/94 13:44 G.Norton 602 2120 ug/l 90.0 7/14/94 13:44 G.Norton 602 12700 ug/l 90.0 7/14/94 13:44 G.Norton 602 900. ug/1 900. 7/14/94 13:44 G.Norton 602 % Recovery Target Range 94. 70 - 130 Labor—tol-y Supervisor SPECIALIZED ASSAYS ENVIRONMENTAL REFERRING CLIENT 300 12th Ave., South Nashville, TN 37203 Entsonmental Hydrogeological L,5 0� 615-726-0177 FAX 615/726-3404 - ju Thomas Ammons 207 W. 4th Avenue, Red Springs, NC 28377 Ph: 910-843-4456 Fax: 910-843-5376 ILLING CONTROL NUMBER (FOR LAB USE ONLY) (� l� PROJECT # P.O. # AMPLERS (Signature -Please Print) PROJECT NAME FOR LAB USE ONLY n ACC# SAMPLE DESCRIPTION DATE TIME U U ANALYSIS REQUESTED As�sS+• Z T ����9� T3 F, X ryi Ai 1 As 3A it- Z p1Ti-. p� I ) TA A y r, U M vi 0 1 A+ 1,4 5 P� ; 47 . 33b1 Mw Z. 'ein e _ azure) Time e eceived by: (Si nature) Received for Laboratory by D to / Time relinquished by: (Signature) Date i Time Received by: Signature) gemarks Fax results to 910-843-5376 Mail COC/results to client QUOTE # 40894JBO relinquished by: (Signature) Date /Time Received by: (Signature) :elinf d by: (Signature) Date ! Time Received by: (Signature) For further assistance in completing the chain of custody form please refer to the instructions found on the nnnosite side = 3= "E" Q � SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 ENVIRONMENTAL HYDROGEOLOG I CAL 5309 CONSULTANTS P.O. BOX 902 RED SPRINGS, DC 28377 V Sample: ATLAS DIST..-%eAWACCC�AfeZ ATLAS DISTRIBUTING Sampler: THOMAS AMMONS Date Collected: 7/19/94 Time Collected: Sample type: Water Site I.D.: AIVAI_YT I CAL FtEF}CFt-r Lab Number: 94-AO36006 State Certification: 387 Date Received: 7/21/94 Time Received: 10:00 Preservative: Analyse Result Units POL Date Time Analyst Method --------------------- • ----------- -- ----- -------- ----- ---------- -------- enzene 23.0 ug/l 1.0 7/25/94 8:19 S. Wani 602 Toluene 11.0 ug/l 1.0 7/25/94 8:18 S. Wani 602 Ethylbenzene 71.0 ug/l 1.0 7/25/94 8:18 S. Wani 602 Xylenes, total 110. ug/l 1.0 7/25/94 8:18 S. Wani 602 Methyl-t-butylether :: 10.0 Ug/l 10.0 7/25/94 8:18 S. 'Wani 602 ** Surrogate Recoveries Surrogate ------------- ETEX/6RO Surrogate Recovery Target Range 85 . 70 - 13i y Laboratory upervisor COPY 1 SPECIALIZED ASSAYS ENVIRONMENTAL 300 /26x.m" s""m Nashville, Tennessee 37203 ENVIRONMENTAL HYDROGEOLOGICAL 5309 CONSULTANTS P.O. BOX 902 RED SPRINGS, NC 28377 Sample: ATLAS DIST. ATLAS DISTRIBUTING Sampler: THOMAS AMMONS Date Collected: 7/19/94 Time Collected: Sample type: Water Site I.D.: Analyte Result ~~~Benzene Toluene Ethylbenzene Xylenes, total Methyl-t-butylether ** Surrogate Recoveries ** Surrogate _____________ BTEX/GRO Surrogate 0 Lab Number: 94-A036005 State Certification: 387 Date Received: 7/21/94 Time Received: 10:00 Preservative: Units PQL Date Time Analyst Method ------ ----- -------- ----- ---------- -------- 2380 ug/l 45.0 7/25/94 8:18 S. Wani 602 10700 ug/l 45.0 7/25/94 8:18 S. Wani 602 1210 ug/l 45.0 7/25/94 8:18 S. Wani 602 7380 ug/l 45.0 7/25/94 8:18 S. Wani 602 459. ug/l 450. 7/25/94 8:18 S. Wani 602 % Recovery Target Range ---------- ------------ 87. 70 - 130 SPECIALIZED ASSAYS ENVIRONMENTAL REFERRING CLIENT 300 12th Ave.. South Nashville, TN 37203 rr;. T r..r. � c,nm�nt,r� 1. ,rwtir.c.q4�l.p�, i.t;.�:l. 615-726-0177 t �: A mmc) n c FAX 615/726-3404 S vri ngs , NC' 18377 n: �i 1.V.i -84:3 - 4 4 5 6 4 1-1 x: 9 1.0 - ?43 -1) 376 3ILLING CONTROL NUMBER (FOR LAB USE ONLA� I PROJECT # P.O. # SAMPLERS (Signature -Please Print) PROJECT NAME 1� 'rl b � A 3 )57i {l FOR LAB USE ONLY 2 < ACC# SAMPLE DESCRIPTION DATE TIME O V ANALYSIS REQUESTED 0 }) A s D; st. hTT� A 1 �i 11 b-5 GA SO l i ---e, Lcw A+IA.5 telinquishe r �:�(Sicnat Da ime Receiv d by: (Si_ ture) RfcejviX for Laborat bv: Date / Time telinquished by: (Signature) Date / Time Received by: (Signature) Rem M:Z tI_ I i17 j.Pr 1•. telinquished by: (Signature) Date / Time Received by: (Signature) `"' "' ' 4 �{ 'elinquished by: (Signature) Date / Time Received by: (Signature) For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side 3 �; r t /w,11 SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 ENVIRONMENTAL HYDROGEOLOG I CAL 5309 CONSULTANTS P.O. BOX 902 RED SPRINGS, NC 22e377 Sample: ATLAS -jSA_ 0WV wWVi -- ATLAS DISTRIBUTI`dG Sampler: M I CHAEL LAM; Date Collected: 7/21/94 Time Collected: Sample type: Water Site I.D.. Analyse - ------ -------------- Benzene Toluene Ethylbenzene Xylenes, total Methyl-t-butylether * Surrogate Recoveries* Surrogate ------------- BTEX ./GRO Surrogate AM4=6L_`YT I GAL FxL=POFZT Lad Number: 94-AO36436 State Certification: 387 Date Received: 7/23/94 Time Received: 10:00 Preservative: HC1 Result Units POL Date Time Analyst Method 6.0 ug/l 1.0 7/25/94 16:17 G.Norton 602 27.0 ug/l 1.0 7/25/94 16:17 G.Norton 602 4.0 ug/l 1.0 7/25/94 16:17 G.Norton 602 3.0 ug/l 1.0 7/25/94 16:17 G.Norton 602 <:: 10.0 ug/l 10.0 7/25/94 16:17 G.Norton 602 ** UST Spike/Duplicate Results ** % Recovery Target Range ------------ 70 - 130 Precision Compound -------------------- %.Recovery --------- Target Range ---------------- RPD --------- Target Range ---------------- Benzene 91. 70 - 130 5.3 0 - 20.0 410 luene 90. 70 - 130 6.5 G - 20.0 �.yl benzene 91. 70 - 130 5.3 0 - 20.0 Xylene 93. 70 - 130 7.3 0 - 20.0 COPY 1 SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 AIVAILYT I CAI_ REF*C3FtT ENVIRONMENTAL HYDROGEOLOG I CAL 5309 COI SULTANTS P.O. BOX 902 REED SPRINGS, NC 28377 Sample: ATLAS p.('Wa,�` %(�Z ATLAS DISTRIBUTING Sa.mp 1 er- : M I CHAEL LAI' M Date Collected: 7/21/94 Time Collected: Sample type: Water Site I.D., * Polyaromatic Hydrocarbon Control Results *** Lab Numb ei- : 94-AO36436 State Cer-tification: 387 Date Received: 7/23/94 Time Received: 10:00 Preservative: HC1 - p0Lind% Recovery Target Range ---- --------------- ----------------------------- • i Labor-ator Supel-viSor- COPY 1 ENVIRONMENTAL 300 12th A%c.. South Nash%ille. TN 37203 615-726-0177 FAX 615-726-3404 REFERRING CLIENT Aj 7. )ILLING CONTROL NUMBER (FOR LABVSLQNLY) PROJECT # P.O. ;AMPLERS (Signature -Please Print) WICI\Ael t.AMWA PROJECT NAME D',5+r-s't>v+.v-%j FOR LAB USE ONLY ACC# SAMPLE DESCRIPTION DATE TIME P= < ANALYSIS REQUESTED V3 tel nquis (Signature) D al ck! e N�, Received by: (jignature) ceived or LaboratoryDate Time telinquished by: (Signature) Date Time i'e0cc'-t7v_ed by: (Signature) R telinquished by: (Signature) Date Time Received by: (Signature) telinquished by: (Signature) Date Time Received by: (Signature) w For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side SPECIALIZED ASSAYS ENVIRONMENTAL 300 12thx.enu South Nashville, Tennessee 37203 ENVIRONMENTAL HYDROGEOLOGICAL 5309 CONSULTANTS P.O. BOX 902 RED SPRINGS, NC 28377 � J# Sample: A � ATLAS DISTRIBUTING Sampler: MICHAEL LAMM Date Collected: 7/28/94 Time Collected: Sample type: Water Site I.D.: Analyte _______________________ 0- uenzene Toluene EthyIbenzene Xylenes, total Nsthyl-t-butylether ** Surrogate Recoveries ** | Surrogate � --_--___--__- BTEX/GR0 Surrogate 0 Lab Number: 94-A037693 State Certification: 387 Date Received: 7/30/94 Time Received: 11:00 Preservative: HCl Result ___________ Units ______ PQL _____ Date ________ Time _____ Analyst __________ Method ______ < 1.O ug/l 1.0 8/ 1/94 8:17 S. Wani 602 < 1.0 ug/l 1.0 8/ 1 /9 4 8:17 S. Wani 602 < 1.0 og/l 1.0 8/ 1/94 8:17 S. Wani 602 < 1.0 ug/l 1.0 8/ 1/94 8:17 S. Wani 602 < 10.0 ug/l 10.0 8/ 1/94 8:17 S. Wani 602 % Recovery Target Range ---------- ------------ 95. 70 - 130 SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 ENVIRONMENTAL HYDROGEOLOGICAL 5309 CONSULTANTS P.O. BOX 902 RED SPRINGS, NC 28377 Sample: A-m;, ATLAS DISTRIBUTING Sampler: MICHAEL LAMM Date Collected: 7/28/94 Time Collected: Sample tyoe: Water Site I.D.: Lab Number: 94-A037692 State Certification: 387 Date Received: 7/30/94 Time Received: 11:00 Preservative: HCl Analyte Result Units PQL Date Time Analyst Method ---------------------- ----------- ------ ----- -------- ----- ---------- -------- Benzene 743. ug/l 10.0 8/ 1/94 8:17 S. Wani 602 Toluene 3650 ug/l 10.0 8/ 1/94 8:17 S. Wani 602 Ethylbenzene 415. ug/l 10.0 8/ 1/94 8:17 S. Wani 602 Xylenes, total 284O ug/l 10.0 8/ 1/94 8:17 S. Wani 602 Methyl -t-butylether 1490 ug/l 1O0. 8/ 1/94 8:17 S. Wani 602 ** Surrogate Recoveries ** \ Surrogate % Recovery Target Range � ------------- ---------- ---__----__- 0 SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Ave., South MmNashville, TN 37203 wo 615-726-0177 FAX 615/726-3404 "Jr Specialized Assays: (800) 765-0980 REFERRING CLIENT count: 5309 ironmental Hydrogeological homas Ammons 207 W. 4th Avenue Red Springs, NC 28377 .0-84 -4456 F x: 910-843-5376 ILLING CONTROL NUMBER (FOR LAB USE ONLY) PROJECT # P.O. # aINPLERS (Signaturr.Please Print) Mia\'Wj i�Rm PROJECT NAME FOR LAB USE ONLY ACC# SAMPLE DESCRIPTION DATE TIME i U < U 8 o ANALYSIS REQUESTED �� `� �� 1�►�X 1 YnT13E A uI 1 I re) D ime Re ived : (S natur) r�')� r Vi/ � Received f Laboratory by "p I 'W Date / Time "�9y xlinquished by: (Signature) Date / Time eceived by: (Signature) Rem rks Quote # 40894JBO elinquished by: (Signature) Date / Time Received by: (Signature) elfin wished by: (Signature) Date / Time Received by: (Signature) For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side • SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 ENVIRONMENTAL H`/DROGEOLOG I GAL 5309 CONSULTANTS P.O. LOX 902 RED SPRINGS„ NC 2e377 Sample: MW-2 BEFORE ATLAS DISTRIBUTING Sampler: M I CHAEL LAMt Date Collected: 8/11/94 Time Collected: Sample type: Water Site I.D.. AIVALYT I CAL f;tEF=-MF2T Lab Number: 94-AO40197 State Certification: 387 Date Received: 8/12/94 Time Received: 9:20 Preservative: Analyte Result Units POL Date Time Analyst Method •------------------------ ----------- ------ ----- -------- ----- ---------- -------- Benzene 2.0 ug/1 1.0 8/15/94 13:50 G.Norton 602 Toluene 7.0 ug/l 1.0 6/15/94 13:50 G.Norton 602 Ethylbenzene 4.0 ug/l 1.0 8/15/94 13:50 G.Norton 602 Xylenes, total 55.0 ug/1 1.0 8/15/94 13:50 G.Norton 602 Methyl-t-butylether < 10.0 ug/l 10.0 8/15/94 13:50 G.Norton 602 ** Surrogate Recoveries ** Surrogate % Recovery Target Range ----------------------------------- BTEX./GRO Surrogate 98. 70 - 130 Laboratory upervisor- COPY 1 SPECIALIZED ASSAYS ENVIRONMENTAL 300 12th Avenue South Nashville, Tennessee 37203 ENVIRONMENTAL HYDROGEOLOG I CAL 5309 CO `NSULTANTS P.O. LOX 9o2 RED SPRINGS, NC 28377 Sample: MW-2 AFTER ATLAS DISTRIBUTING Samp 1 ei- : M I CHAEL LAB M Date Collected: 8/11/94 Time Collected: Sample type: Water Site I.D.. Analyte --------------------- Benzene Toluene Ethyibenzene Xylenes, total Methyl-t-butylether Surrogate Recoveries Surrogate ------------- STEX/GRO Surrogate • Ah1ALYT I CAL_ F2EF'OF -r Lad Numbei- : 94-AO40198 State Certification: 387 Date Received: 8/12/94 Time Received: 9:20 Preservative: Result ----------- Units ------ POL ----- Date -------- Time ----- Analyst ---------- Method -------- 5.0 uq/1 1.0 8/15/94 13:50 G.Norton 602 41.0 ua/l 1.0 8/15/94 13:50 G.Norton 602 6.0 ua/1 1.0 8/15/94 13:50 G.Norton 602 42.0 uQ/l 1.0 8/15/94 13:50 G.Norton 602 <:: 10.0 ug/l 10.0 8/15/94 13:50 G.Norton 602 % Recovery Target Range 105 . 70 - 13� y Laboratory Eytpervisor COPY 1 SPECIALIZED ASSAYS ENVIRONMENTAL 300 l2th Ave., South Nashville, TN 37203 615-726-0177 FAX 615/726-3404 - REFERRING CLIENT Ovironmental Hydrogeological Thomas Ammons 207 W. 4th Avenue, Red Springs, NC 28377 910-843-4456 Fax: 910-843-5376 TILLING CONTROL NUMBER (FOR L4B USE ONLY) 33S PROJECT # P.O. # +AMPLERS (Signature -Please Print) icanAe� �4 Imn� PROJECT NAME ,A-}-IAs �i `t,bv�-rn FOR LAB USE ONLY ACC# SAMPLE DESCRIPTION DATE TIME O ¢ v g ANALYSIS REQUESTED y c�ti +IA5 rnw W z B4f'd« � � 4� ��,�� 1 z E i-g 9 g-�— x rn AflAS W Z A4v �n P • eli uish ture) D Time Reced�)-A%iurcy((—�� +fa (! : 3 Re ved or Laboratory b . Date /Time elinquished by: (Signature) Date / Time Received by: (Signature) Re r Fax results to 910-843-5376 Mail COC /results to client QUOTE # 40894JB0 elinquished by: (Signature) Date ! Time Received by: (Signature) e9hed by: (Signature) Date / Time Received by: (Signature) For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side (Jc4 yo19 ENVIRONMENTAL SCIENCE CORP. • • 0 REPORT OF ANALYSIS Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing 1 Sample ID A9W—i" r11.. - ( ��' *S•a� �en�., Collected By David Brown Collection Date 12/16/02 13:00 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-02 Site ID : Project # Parameter Result Det. Limit Units Method Date Dil. Lead 14. 5.0 ug/l 6010B 12/20/02 1 volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 12/21/02 1 C5-C8 Aliphatics BDL 100 ug/l MADEPV 12/21/02 1 C9-C12 Aliphatics BDL 100 ug/l MADEPV 12/21/02 1 C9-C10 Aromatics BDL 100 ug/l MADEPV 12/21/02 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 94.0 % Rec. MADEPV 12/21/02 1 2,5-Dibromotoluene(PID) 93.0 % Rec. MADEPV 12/21/02 1 Volatile Organics Acetone BDL 50. ug/l 6210D 12/23/02 1 Acrolein BDL 50. ug/1 6210D 12/23/02 1 Acrylonitrile BDL 50. ug/l 6210D 12/23/02 1 Benzene BDL 1.0 ug/l 6210D 12/23/02 1 Bromobenzene BDL 1.0 ug/l 6210D 12/23/02 1 Bromodichloromethane BDL 1.0 ug/l 6210D 12/23/02 1 Bromoform BDL 1.0 ug/l 6210D 12/23/02 1 Bromomethane BDL 1.0 ug/l 6210D 12/23/02 1 n-Butylbenzene BDL 1.0 ug/l 6210D 12/23/02 1 sec-Butylbenzene BDL 1.0 ug/l 6210D 12/23/02 1 tert-Butylbenzene BDL 1.0 ug/l 6210D 12/23/02 1 Carbon tetrachloride BDL 1.0 ug/l 6210D 12/23/02 1 Chlorobenzene BDL 1.0 ug/l 6210D 12/23/02 1 Chlorodibromomethane BDL 1.0 ug/l 6210D 12/23/02 1 Chloroethane BDL 1.0 ug/l 6210D 12/23/02 1 Chloroform BDL 5.0 ug/l 6210D 12/23/02 1 Chloromethane BDL 1.0 ug/l 6210D 12/23/02 1 2-Chlorotoluene BDL 1.0 ug/l 6210D 12/23/02 1 4-Chlorotoluene BDL 1.0 ug/l 6210D 12/23/02 1 1,2-Dibromo-3-Chloropropane BDL 2.0 ug/l 6210D 12/23/02 1 1,2-Dibromoethane BDL 1.0 ug/l 6210D 12/23/02 1 Dibromomethane BDL 1.0 ug/l 6210D 12/23/02 1 1,2-Dichlorobenzene BDL 1.0 ug/l 6210D 12/23/02 1 1,3-Dichlorobenzene BDL 1.0 ug/l 6210D 12/23/02 1 1,4-Dichlorobenzene BDL 1.0 ug/l 6210D 12/23/02 1 Dichlorodifluoromethane BDL 1.0 ug/l 6210D 12/23/02 1 1,1-Dichloroethane BDL 1.0 ug/l 6210D 12/23/02 1 1,2-Dichloroethane BDL 1.0 ug/l 6210D 12/23/02 1 1,1-Dichloroethene BDL 1.0 ug/l 6210D 12/23/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 5 of 26 Lebanon R 0 Mtt.. J 3uliet, TN 7122 ENVIRONMENTAL (615) 758-5858 1-800-767-5859 SCIENCE CORP. Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. David Brown December 26,2002 EHC, Inc. PO Box 902 Red Springs, NC 28377 ESC Sample # L99295-02 Date Received December 19, 2002 Description Atlas Distributing Site ID Sample ID 14W-2 Project # Collected By David Brown Collection Date 12/16/02 13:00 Parameter Result Det. Limit Units Method Date cis-1,2-Dichloroethene BDL 1.0 ug/1 6210D 12/23/02 trans-1,2-Dichloroethene BDL 1.0 ug/1 6210D 12/23/02 1,2-Dichloropropane BDL 1.0 ug/1 6210D 12/23/02 1,1-Dichloropropene BDL 1.0 ug/1 6210D 12/23/02 1,3-Dichloropropane BDL 1.0 ug/1 6210D 12/23/02 2,2-Dichloropropane BDL 1.0 ug/1 6210D 12/23/02 Di -isopropyl ether BDL 1.0 ug/l 6210D 12/23/02 Ethylbenzene BDL 1.0 ug/l 6210D 12/23/02 Hexachlorobutadiene BDL 1.0 ug/l 6210D 12/23/02 Isopropylbenzene BDL 1.0 ug/l 6210D 12/23/02 p-Isopropyltoluene BDL 1.0 ug/l 6210D 12/23/02 2-Butanone (MEK) BDL 50. ug/l 6210D 12/23/02 Methylene Chloride BDL 5.0 ug/l 6210D 12/23/02 4-Methyl-2-pentanone (MIBK) BDL 50. ug/l 6210D 12/23/02 Methyl tert-butyl ether BDL 1.0 ug/l 6210D 12/23/02 • Naphthalene BDL 5.0 ug/l 6210D 12/23/02 n-Propylbenzene BDL 1.0 ug/l 6210D 12/23/02 Styrene BDL 1.0 ug/l 6210D 12/23/02 1,1,1,2-Tetrachloroethane BDL 1.0 ug/1 6210D 12/23/02 1,1,2,2-Tetrachloroethane BDL 1.0 ug/1 6210D 12/23/02 Tetrachloroethene BDL 1.0 ug/l 6210D 12/23/02 Toluene BDL 5.0 ug/1 6210D 12/23/02 1,2,3-Trichlorobenzene BDL 1.0 ug/l 6210D 12/23/02 1,2,4-Trichlorobenzene BDL 1.0 ug/l 6210D 12/23/02 1,1,1-Trichloroethane BDL 1.0 ug/l 6210D 12/23/02 1,1,2-Trichloroethane BDL 1.0 ug/l 6210D 12/23/02 Trichloroethene BDL 1.0 ug/l 6210D 12/23/02 Trichlorofluoromethane BDL 1.0 ug/l 6210D 12/23/02 1,2,3-Trichloropropane BDL 1.0 ug/l 6210D 12/23/02 1,2,4-Trimethylbenzene BDL 1.0 ug/l 6210D 12/23/02 1,3,5-Trimethylbenzene BDL 1.0 ug/1 6210D 12/23/02 Vinyl chloride BDL 1.0 ug/l 6210D 12/23/02 o-Xylene BDL 1.0 ug/l 6210D 12/23/02 m&p-Xylenes BDL 2.0 ug/l 6210D 12/23/02 Surrogate Recovery Toluene-d8 98. % Rec. 6210D 12/23/02 Dibromofluoromethane 100 96 Rec. 6210D 12/23/02 4-Bromofluorobenzene 98. % Rec. 6210D 12/23/02 0 Dil. 1 1 1 Extractable Petroleum Hydrocarb BDL 100 ug/l MADEPE 12/26/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 6 of 26 ENVIRONMENTAL SCIENCE CORP. • E REPORT OF ANALYSIS Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID *MW-2 V^ w Collected By David Brown Collection Date 12/16/02 13:00 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-02 Site ID : Project # Parameter Result Det. Limit Units Method Date Dil. C9-C18 Aliphatics BDL 100 ug/l MADEPE 12/26/02 1 C19-C36 Aliphatics BDL 100 ug/l MADEPE 12/26/02 1 Cll-C22 Aromatics BDL 100 ug/l MADEPE 12/26/02 1 Surrogate Recovery o-Terphenyl 74.0 %- Rec. MADEPE 12/26/02 1 1-Chloro-octadecane 74.0 % Rec. MADEPE 12/26/02 1 2-Fluorobiphenyl 79.0 & Rec. MADEPE 12/26/02 1 2-Bromonaphthanene 79.0 %- Rec. MADEPE 12/26/02 1 625 Base/Neutrals w/ TIC Acenaphthene BDL 10. ug/l 625 12/21/02 1 Acenaphthylene BDL 10. ug/l 625 12/21/02 1 Anthracene BDL 10. ug/l 625 12/21/02 1 Benzidine BDL 50. ug/l 625 12/21/02 1 Benzo(a)anthracene BDL 10. ug/l 625 12/21/02 1 Benzo(b)fluoranthene BDL 10. ug/l 625 12/21/02 1 Benzo(k)fluoranthene BDL 10. ug/1 625 12/21/02 1 Benzo(g,h,i)perylene BDL 10. ug/1 625 12/21/02 1 Benzo(a)pyrene BDL 10. ug/1 625 12/21/02 1 Bis(2-chlorethoxy)methane BDL 10. ug/l 625 12/21/02 1 Bis(2-chloroethyl)ether BDL 10. ug/l 625 12/21/02 1 Bis(2-chloroisopropyl)ether BDL 10. ug/l 625 12/21/02 1 4-Bromophenyl-phenylether BDL 10. ug/l 625 12/21/02 1 2-Chloronaphthalene BDL 10. ug/1 625 12/21/02 1 4-Chlorophenyl-phenylether BDL 10. ug/1 625 12/21/02 1 Chrysene BDL 10. ug/l 625 12/21/02 1 Dibenz(a,h)anthracene BDL 10. ug/l 625 12/21/02 1 3,3-Dichlorobenzidine BDL 10. ug/l 625 12/21/02 1 2,4-Dinitrotoluene BDL 10. ug/1 625 12/21/02 1 2,6-Dinitrotoluene BDL 10. ug/l 625 12/21/02 1 Fluoranthene BDL 10. ug/l 625 12/21/02 1 Fluorene BDL 10. ug/1 625 12/21/02 1 Hexachlorobenzene BDL 10. ug/l 625 12/21/02 1 Hexachloro-1,3-butadiene BDL 10. ug/l 625 12/21/02 1 Hexachlorocyclopentadiene BDL 10. ug/l 625 12/21/02 1 Hexachloroethane BDL 10. ug/l 625 12/21/02 1 Indeno(1,2,3-cd)pyrene BDL 10. ug/l 625 12/21/02 1 Isophorone BDL 10. ug/1 625 12/21/02 1 Naphthalene BDL 10. ug/l 625 12/21/02 1 Nitrobenzene BDL 10. ug/l 625 12/21/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 7 of 26 ENVIRONMENTAL . SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received Description Sample ID Collected By Collection Date Parameter December 19, 2002 Atlas Distributing 494-2 h1 w -' David Brown 12/16/02 13:00 REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # : L99295-02 Site ID : Project # Result Det. Limit Units Method Date Dil. n-Nitrosodimethylamine BDL 10. ug/l 625 12/21/02 n-Nitrosodiphenylamine BDL 10. ug/l 625 12/21/02 n-Nitrosodi-n-propylamine BDL 10. ug/l 625 12/21/02 Phenanthrene BDL 10. ug/l 625 12/21/02 Benzylbutyl phthalate BDL 10. ug/l 625 12/21/02 Bis(2-ethylhexyl)phthalate BDL 10. ug/l 625 12/21/02 Di-n-butyl phthalate BDL 10. ug/l 625 12/21/02 Diethyl phthalate BDL 10. ug/l 625 12/21/02 Dimethyl phthalate BDL 10. ug/l 625 12/21/02 Di-n-octyl phthalate BDL 10. ug/l 625 12/21/02 Pyrene BDL 10. ug/1 625 12/21/02 1,2,4-Trichlorobenzene BDL 10. ug/l 625 12/21/02 Acid Extractables 4-Chloro-3-methylphenol BDL 10. ug/l 625 12/21/02 2-Chlorophenol BDL 10. ug/l 625 12/21/02 2,4-Dichlorophenol • BDL 10. ug/l 625 12/21/02 2,4-Dimethylphenol BDL 10. ug/l 625 12/21/02 4,6-Dinitro-2-methylphenol BDL 10. ug/1 625 12/21/02 2,4-Dinitrophenol BDL 10. ug/l 625 12/21/02 2-Nitrophenol BDL 10. ug/l 625 12/21/02 4-Nitrophenol BDL 10. ug/l 625 12/21/02 Pentachlorophenol BDL 10. ug/l 625 12/21/02 Phenol BDL 10. ug/l 625 12/21/02 2,4,6-Trichlorophenol BDL 10. ug/l 625 12/21/02 Surrogate Recovery Nitrobenzene-d5 62. $ Rec. 625 12/21/02 2-Fluorobiphenyl 72. 96 Rec. 625 12/21/02 p-Terphenyl-dl4 94. % Rec. 625 12/21/02 Phenol-d5 24. % Rec. 625 12/21/02 2-Fluorophenol 31. % Rec. 625 12/21/02 2,4,6-Tribromophenol 72. % Rec. 625 12/21/02 ( dWjJ1zCk0 Terrie Fudge,t ESC T presentative BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: The reported analytical results relate only to the sample submitted. • This report shall not be reproduced, except in full, without the written approval from ESC. Page 8 of 26 ENVIRONMENTAL • SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received Description Sample ID Collected By Collection Date Parameter 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # : L99295-01 December 19, 2002 Atlas Distributing 1 David Brown 12/16/02 12:00 Result Det. Limit Units REPORT OF ANALYSIS Site ID : Project # : Method Date Lead 13. 5.0 ug/1 6010B 12/20/02 Volatile Petroleum Hydrocarbons 320 100 ug/1 MADEPV 12/19/02 C5-C8 Aliphatics 200 100 ug/l MADEPV 12/19/02 C9-C12 Aliphatics 250 100 ug/l MADEPV 12/19/02 C9-C10 Aromatics 130 100 ug/l MADEPV 12/19/02 Surrogate Recovery 2,5-Dibromotoluene(FID) 118. % Rec. MADEPV 12/19/02 2,5-Dibromotoluene(PID) 114. % Rec. MADEPV 12/19/02 Volatile Organics Acetone BDL 50. ug/l 6210D 12/23/02 Acrolein BDL 50. ug/l 6210D 12/23/02 Acrylonitrile BDL 50. ug/l 6210D 12/23/02 Benzene 1.4 1.0 ug/l 6210D 12/23/02 Bromobenzene • BDL 1.0 ug/l 6210D 12/23/02 Bromodichloromethane BDL 1.0 ug/l 6210D 12/23/02 Bromoform BDL 1.0 ug/l 6210D 12/23/02 Bromomethane BDL 1.0 ug/l 6210D 12/23/02 n-Butylbenzene BDL 1.0 ug/l 6210D 12/23/02 sec-Butylbenzene BDL 1.0 ug/l 6210D 12/23/02 tert-Butylbenzene BDL 1.0 ug/l 6210D 12/23/02 Carbon tetrachloride BDL 1.0 ug/l 6210D 12/23/02 Chlorobenzene BDL 1.0 ug/1 6210D 12/23/02 Chlorodibromomethane BDL 1.0 ug/l 6210D 12/23/02 Chloroethane BDL 1.0 ug/l 6210D 12/23/02 Chloroform BDL 5.0 ug/l 6210D 12/23/02 Chloromethane BDL 1.0 ug/l 6210D 12/23/02 2-Chlorotoluene BDL 1.0 ug/l 6210D 12/23/02 4-Chlorotoluene BDL 1.0 ug/l 6210D 12/23/02 1,2-Dibromo-3-Chloropropane BDL 2.0 ug/1 6210D 12/23/02 1,2-Dibromoethane BDL 1.0 ug/1 6210D 12/23/02 Dibromomethane BDL 1.0 ug/l 6210D 12/23/02 1,2-Dichlorobenzene BDL 1.0 ug/1 6210D 12/23/02 1,3-Dichlorobenzene BDL 1.0 ug/l 6210D 12/23/02 1,4-Dichlorobenzene BDL 1.0 ug/l 6210D 12/23/02 Dichlorodifluoromethane BDL 1.0 ug/l 6210D 12/23/02 1,1-Dichloroethane BDL 1.0 ug/l 6210D 12/23/02 1,2-Dichloroethane BDL 1.0 ug/l 6210D 12/23/02 1,1-Dichloroethene BDL 1.0 ug/1 6210D 12/23/02 Dil. 1 1 1 1 1 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 1 of 26 • 0 ENVIRONMENTAL SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID m -1 V' ••- - Collected By David Brown Collection Date 12/16/02 12:00 Parameter cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,1-Dichloropropene 1,3-Dichloropropane 2,2-Dichloropropane Di -isopropyl ether Ethylbenzene Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene 2-Butanone (MEK) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene m&p-Xylenes Surrogate Recovery Toluene-d8 Dibromofluoromethane 4-Bromofluorobenzene REPORT OF ANALYSIS Result BDL BDL BDL BDL BDL BDL BDL 20. BDL BDL BDL BDL BDL BDL BDL 5.2 1.6 BDL BDL BDL BDL 17. BDL BDL BDL BDL BDL BDL BDL 22. 6.4 BDL 8.9 71. 96. 100 98. Det. Limit 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 50. 5.0 50. 1.0 5.0 1.0 1.0 1.0 1.0 1.0 5.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 2.0 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-01 Site ID : Project # Units ug/l ug/l ug/l ug/l ug/l ug/1 ug/1 ug/l ug/l ug/l ug/l ug/l ug/1 ug/1 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/1 ug/l ug/l ug/l ug/l ug/1 ug/l ug/l ug/l ug/1 ug/1 ug/1 ug/l % Rec. Rec. 96 Rec. Method 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D 6210D Date 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 12/23/02 Dil. 1 1 1 Extractable Petroleum Hydrocarb BDL 100 ug/l MADEPE 12/26/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 2 of 26 ENVIRONMENTAL SCIENCE CORP. REPORT OF ANALYSIS Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID UN-4 IVIL 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-01 Site ID : Collected By David Brown Collection Date 12/16/02 12:00 Parameter Result Det. Limit Project # Units Method Date Dil. C9-C18 Aliphatics BDL 100 ug/l MADEPE 12/26/02 1 C19-C36 Aliphatics BDL 100 ug/l MADEPE 12/26/02 1 Cll-C22 Aromatics BDL 100 ug/l MADEPE 12/26/02 1 Surrogate Recovery o-Terphenyl 88.0 % Rec. MADEPE 12/26/02 1 1-Chloro-octadecane 74.0 % Rec. MADEPE 12/26/02 1 2-Fluorobiphenyl 96.0 % Rec. MADEPE 12/26/02 1 2-Bromonaphthanene 95.0 % Rec. MADEPE 12/26/02 1 625 Base/Neutrals w/ TIC Acenaphthene BDL 10. ug/l 625 12/21/02 1 Acenaphthylene BDL 10. ug/l 625 12/21/02 1 Anthracene BDL 10. ug/l 625 12/21/02 1 Benzidine BDL 50. ug/1 625 12/21/02 1 Benzo(a)anthracene BDL 10. ug/1 625 12/21/02 1 Benzo(b)fluoranthene BDL 10. ug/l 625 12/21/02 1 Benzo(k)fluoranthene BDL 10. ug/l 625 12/21/02 1 Benzo(g,h,i)perylene BDL 10. ug/l 625 12/21/02 1 Benzo(a)pyrene BDL 10. ug/l 625 12/21/02 1 Bis(2-chlorethoxy)methane BDL 10. ug/l 625 12/21/02 1 Bis(2-chloroethyl)ether BDL 10. ug/l 625 12/21/02 1 Bis(2-chloroisopropyl)ether BDL 10. ug/l 625 12/21/02 1 4-Bromophenyl-phenylether BDL 10. ug/l 625 12/21/02 1 2-Chloronaphthalene BDL 10. ug/l 625 12/21/02 1 4-Chlorophenyl-phenylether BDL 10. ug/l 625 12/21/02 1 Chrysene BDL 10. ug/l 625 12/21/02 1 Dibenz(a,h)anthracene BDL 10. ug/l 625 12/21/02 1 3,3-Dichlorobenzidine BDL 10. ug/l 625 12/21/02 1 2,4-Dinitrotoluene BDL 10. ug/l 625 12/21/02 1 2,6-Dinitrotoluene BDL 10. ug/l 625 12/21/02 1 Fluoranthene BDL 10. ug/1 625 12/21/02 1 Fluorene BDL 10. ug/l 625 12/21/02 1 Hexachlorobenzene BDL 10. ug/l 625 12/21/02 1 Hexachloro-1,3-butadiene BDL 10. ug/l 625 12/21/02 1 Hexachlorocyclopentadiene BDL 10. ug/l 625 12/21/02 1 Hexachloroethane BDL 10. ug/l 625 12/21/02 1 Indeno(1,2,3-cd)pyrene BDL 10. ug/l 625 12/21/02 1 Isophorone BDL 10. ug/l 625 12/21/02 1 Naphthalene BDL 10. ug/l 625 12/21/02 1 Nitrobenzene BDL 10. ug/l 625 12/21/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 3 of 26 0 ENVIRONMENTAL • SCIENCE CORP. :7 • Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID MW---1 hn "- - Collected By David Brown Collection Date 12/16/02 12:00 Parameter n-Nitrosodimethylamine n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine Phenanthrene Benzylbutyl phthalate Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene Acid Extractables 4-Chloro-3-methylphenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol Surrogate Recovery Nitrobenzene-d5 2-Fluorobiphenyl p-Terphenyl-d14 Phenol-d5 2-Fluorophenol 2,4,6-Tribromophenol REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-01 Site ID : Project # Result Det. Limit Units Method Date Dil. BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 69. % Rec. 625 12/21/02 1 77. % Rec. 625 12/21/02 1 81. % Rec. 625 12/21/02 1 31. % Rec. 625 12/21/02 1 43. % Rec. 625 12/21/02 1 80. % Rec. 625 12/21/02 1 Terrie Fudge, ESC /Z44 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Page 4 of 26 ENVIRONMENTAL • SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 • • Date Received December 19, 2002 Description Atlas Distributing Sample ID MW-2D Collected By David Brown Collection Date 12/16/02 14:00 REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # : L99295-03 Site ID : Project # Parameter Result Det. Limit Units Method Date Dil. Lead 18. 5.0 ug/1 6010B 12/20/02 Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 12/19/02 C5-C8 Aliphatics BDL 100 ug/l MADEPV 12/19/02 C9-C12 Aliphatics BDL 100 ug/l MADEPV 12/19/02 C9-C10 Aromatics BDL 100 ug/l MADEPV 12/19/02 Surrogate Recovery 2,5-Dibromotoluene(FID) 119. % Rec. MADEPV 12/19/02 2,5-Dibromotoluene(PID) 116. % Rec. MADEPV 12/19/02 Volatile Organics Acetone BDL 50. ug/l 6210D 12/24/02 Acrolein BDL 50. ug/l 6210D 12/24/02 Acrylonitrile BDL 50. ug/l 6210D 12/24/02 Benzene BDL 1.0 ug/l 6210D 12/24/02 Bromobenzene BDL 1.0 ug/1 6210D 12/24/02 Bromodichloromethane BDL 1.0 ug/l 6210D 12/24/02 Bromoform BDL 1.0 ug/l 6210D 12/24/02 Bromomethane BDL 1.0 ug/l 6210D 12/24/02 n-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 sec-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 tert-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 Carbon tetrachloride BDL 1.0 ug/l 6210D 12/24/02 Chlorobenzene BDL 1.0 ug/1 6210D 12/24/02 Chlorodibromomethane BDL 1.0 ug/1 6210D 12/24/02 Chloroethane BDL 1.0 ug/l 6210D 12/24/02 Chloroform 12. 5.0 ug/l 6210D 12/24/02 Chloromethane BDL 1.0 ug/l 6210D 12/24/02 2-Chlorotoluene BDL 1.0 ug/l 6210D 12/24/02 4-Chlorotoluene BDL 1.0 ug/l 6210D 12/24/02 1,2-Dibromo-3-Chloropropane BDL 2.0 ug/l 6210D 12/24/02 1,2-Dibromoethane BDL 1.0 ug/1 6210D 12/24/02 Dibromomethane BDL 1.0 ug/1 6210D 12/24/02 1,2-Dichlorobenzene BDL 1.0 ug/1 6210D 12/24/02 1,3-Dichlorobenzene BDL 1.0 ug/1 6210D 12/24/02 1,4-Dichlorobenzene BDL 1.0 ug/l 6210D 12/24/02 Dichlorodifluoromethane BDL 1.0 ug/l 6210D 12/24/02 1,1-Dichloroethane BDL 1.0 ug/l 6210D 12/24/02 1,2-Dichloroethane BDL 1.0 ug/l 6210D 12/24/02 1,1-Dichloroethene BDL 1.0 ug/l 6210D 12/24/02 1 1 1 1 1 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 9 of 26 ENVIRONMENTAL • SCIENCE CORP. • is Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID MW-2D Collected By David Brown Collection Date 12/16/02 14:00 Parameter cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,1-Dichloropropene 1,3-Dichloropropane 2,2-Dichloropropane Di -isopropyl ether Ethylbenzene Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene 2-Butanone (MEK) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene m&p-Xylenes Surrogate Recovery Toluene-d8 Dibromofluoromethane 4-Bromofluorobenzene Extractable Petroleum Hydrocarb REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-03 Site ID : Project # Result Det. Limit Units Method Date Dil. BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 50. ug/l 6210D 12/24/02 BDL 5.0 ug/l 6210D 12/24/02 BDL 50. ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 5.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/1 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 5.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 2.0 ug/l 6210D 12/24/02 95. % Rec. 6210D 12/24/02 100 % Rec. 6210D 12/24/02 93. % Rec. 6210D 12/24/02 BDL 100 ug/l MADEPE 12/26/02 1 1 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 10 of 26 ENVIRONMENTAL • SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 E Date Received December 19, 2002 Description Atlas Distributing Sample ID MW-2D Collected By David Brown Collection Date 12/16/02 14:00 REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-03 Site ID : Project # Parameter Result Det. Limit Units Method Date Dil. C9-C18 Aliphatics BDL 100 ug/l MADEPE 12/26/02 C19-C36 Aliphatics BDL 100 ug/l MADEPE 12/26/02 Cll-C22 Aromatics BDL 100 ug/l MADEPE 12/26/02 Surrogate Recovery o-Terphenyl 84.0 % Rec. MADEPE 12/26/02 1-Chloro-octadecane 56.0 % Rec. MADEPE 12/26/02 2-Fluorobiphenyl 91.0 % Rec. MADEPE 12/26/02 2-Bromonaphthanene 80.0 % Rec. MADEPE 12/26/02 625 Base/Neutrals w/ TIC Acenaphthene BDL 10. ug/l 625 12/21/02 Acenaphthylene BDL 10. ug/1 625 12/21/02 Anthracene BDL 10. ug/l 625 12/21/02 Benzidine BDL 50. ug/l 625 12/21/02 Benzo(a)anthracene BDL 10. ug/l 625 12/21/02 Benzo(b)fluoranthene BDL 10. ug/l 625 12/21/02 Benzo(k)fluoranthene BDL 10. ug/l 625 12/21/02 Benzo(g,h,i)perylene BDL 10. ug/l 625 12/21/02 Benzo(a)pyrene BDL 10. ug/1 625 12/21/02 Bis(2-chlorethoxy)methane BDL 10. ug/l 625 12/21/02 Bis(2-chloroethyl)ether BDL 10. ug/l 625 12/21/02 Bis(2-chloroisopropyl)ether BDL 10. ug/l 625 12/21/02 4-Bromophenyl-phenylether BDL 10. ug/l 625 12/21/02 2-Chloronaphthalene BDL 10. ug/l 625 12/21/02 4-Chlorophenyl-phenylether BDL 10. ug/l 625 12/21/02 Chrysene BDL 10. ug/l 625 12/21/02 Dibenz(a,h)anthracene BDL 10. ug/l 625 12/21/02 3,3-Dichlorobenzidine BDL 10. ug/l 625 12/21/02 2,4-Dinitrotoluene BDL 10. ug/l 625 12/21/02 2,6-Dinitrotoluene BDL 10. ug/l 625 12/21/02 Fluoranthene BDL 10. ug/l 625 12/21/02 Fluorene BDL 10. ug/l 625 12/21/02 Hexachlorobenzene BDL 10. ug/l 625 12/21/02 Hexachloro-1,3-butadiene BDL 10. ug/l 625 12/21/02 Hexachlorocyclopentadiene BDL 10. ug/l 625 12/21/02 Hexachloroethane BDL 10. ug/l 625 12/21/02 Indeno(1,2,3-cd)pyrene BDL 10. ug/l 625 12/21/02 Isophorone BDL 10. ug/l 625 12/21/02 Naphthalene BDL 10. ug/l 625 12/21/02 Nitrobenzene BDL 10. ug/l 625 12/21/02 1 1 1 1 1 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 11 of 26 Lebanon R 0 Mtt.. J 3uliet, TN 7122 ENVIRONMENTAL (615) 758-5858 1-800-767-5859 SCIENCE CORP. Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. David Brown December 26,2002 EHC, Inc. PO Box 902 Red Springs, NC 28377 ESC Sample # L99295-03 Date Received December 19, 2002 Description Atlas Distributing Site ID Sample ID MW-21) Project # Collected By David Brown Collection Date 12/16/02 14:00 Parameter Result Det. Limit Units Method Date Dil. n-Nitrosodimethylamine BDL 10. ug/1 625 12/21/02 1 n-Nitrosodiphenylamine BDL 10. ug/l 625 12/21/02 1 n-Nitrosodi-n-propylamine BDL 10. ug/l 625 12/21/02 1 Phenanthrene BDL 10. ug/l 625 12/21/02 1 Benzylbutyl phthalate BDL 10. ug/1 625 12/21/02 1 Bis(2-ethylhexyl)phthalate BDL 10. ug/l 625 12/21/02 1 Di-n-butyl phthalate BDL 10. ug/l 625 12/21/02 1 Diethyl phthalate BDL 10. ug/1 625 12/21/02 1 Dimethyl phthalate BDL 10. ug/l 625 12/21/02 1 Di-n-octyl phthalate BDL 10. ug/1 625 12/21/02 1 Pyrene BDL 10. ug/l 625 12/21/02 1 1,2,4-Trichlorobenzene BDL 10. ug/l 625 12/21/02 1 Acid Extractables 4-Chloro-3-methylphenol BDL 10. ug/l 625 12/21/02 1 2-Chlorophenol • BDL 10. ug/l 625 12/21/02 1 2,4-Dichlorophenol BDL 10. ug/l 625 12/21/02 1 2,4-Dimethylphenol BDL 10. ug/l 625 12/21/02 1 4,6-Dinitro-2-methylphenol BDL 10. ug/l 625 12/21/02 1 2,4-Dinitrophenol BDL 10. ug/l 625 12/21/02 1 2-Nitrophenol BDL 10. ug/1 625 12/21/02 1 4-Nitrophenol BDL 10. ug/l 625 12/21/02 1 Pentachlorophenol BDL 10. ug/l 625 12/21/02 1 Phenol BDL 10. ug/l 625 12/21/02 1 2,4,6-Trichlorophenol BDL 10. ug/l 625 12/21/02 1 Surrogate Recovery Nitrobenzene-d5 76. % Rec. 625 12/21/02 1 2-Fluorobiphenyl 85. % Rec. 625 12/21/02 1 p-Terphenyl-dl4 100 % Rec. 625 12/21/02 1 Phenol-d5 39. % Rec. 625 12/21/02 1 2-Fluorophenol 42. % Rec. 625 12/21/02 1 2,4,6-Tribromophenol 68. % Rec. 625 12/21/02 1 Y-JA-A J-1 '&J, Terrie Fudge, ERepkesentative BDL - Below Detection Limit U Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A21A - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Page 12 of 26 ENVIRONMENTAL SCIENCE CORP. • • • Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received Description Sample ID Collected By Collection Date Parameter December 19, 2002 Atlas Distributing MW-p N_ G„ David Brown 12/16/02 15:00 REPORT OF ANALYSIS Result 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-04 Site ID : Project # Det. Limit Units Method Date Dil. Lead BDL 5.0 ug/1 6010B 12/20/02 1 volatile Petroleum Hydrocarbons 510 100 ug/l MADEPV 12/19/02 1 C5-C8 Aliphatics 370 100 ug/l MADEPV 12/19/02 1 C9-C12 Aliphatics 270 100 ug/l MADEPV 12/19/02 1 C9-C10 Aromatics 130 100 ug/l MADEPV 12/19/02 1 Surrogate Recovery 2,5-Dibromotoluene(FID) 128. 96 Rec. MADEPV 12/19/02 1 2,5-Dibromotoluene(PID) 123. 96 Rec. MADEPV 12/19/02 1 Volatile Organics Acetone BDL 50. ug/1 6210D 12/24/02 1 Acrolein BDL 50. ug/l 6210D 12/24/02 1 Acrylonitrile BDL 50. ug/l 6210D 12/24/02 1 Benzene 14. 1.0 ug/l 6210D 12/24/02 1 Bromobenzene BDL 1.0 ug/l 6210D 12/24/02 1 Bromodichloromethane BDL 1.0 ug/l 6210D 12/24/02 1 Bromoform BDL 1.0 ug/l 6210D 12/24/02 1 Bromomethane BDL 1.0 ug/1 6210D 12/24/02 1 n-Butylbenzene BDL 1.0 ug/1 6210D 12/24/02 1 sec-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 1 tert-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 1 Carbon tetrachloride BDL 1.0 ug/l 6210D 12/24/02 1 Chlorobenzene BDL 1.0 ug/l 6210D 12/24/02 1 Chlorodibromomethane BDL 1.0 ug/l 6210D 12/24/02 1 Chloroethane BDL 1.0 ug/l 6210D 12/24/02 1 Chloroform BDL 5.0 ug/1 6210D 12/24/02 1 Chloromethane BDL 1.0 ug/l 6210D 12/24/02 1 2-Chlorotoluene BDL 1.0 ug/l 6210D 12/24/02 1 4-Chlorotoluene BDL 1.0 ug/1 6210D 12/24/02 1 1,2-Dibromo-3-Chloropropane BDL 2.0 ug/l 6210D 12/24/02 1 1,2-Dibromoethane BDL 1.0 ug/l 6210D 12/24/02 1 Dibromomethane BDL 1.0 ug/1 6210D 12/24/02 1 1,2-Dichlorobenzene BDL 1.0 ug/1 6210D 12/24/02 1 1,3-Dichlorobenzene BDL 1.0 ug/1 6210D 12/24/02 1 1,4-Dichlorobenzene BDL 1.0 ug/1 6210D 12/24/02 1 Dichlorodifluoromethane BDL 1.0 ug/1 6210D 12/24/02 1 1,1-Dichloroethane BDL 1.0 ug/l 6210D 12/24/02 1 1,2-Dichloroethane BDL 1.0 ug/l 6210D 12/24/02 1 1,1-Dichloroethene BDL 1.0 ug/1 6210D 12/24/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 13 of 26 ENVIRONMENTAL • SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 r LJ 0 Date Received December 19, 2002 Description Atlas Distributing Sample ID MW-14 Collected By David Brown Collection Date 12/16/02 15:00 REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-04 Site ID : Project # Parameter Result Det. Limit Units Method Date Dil. cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,1-Dichloropropene 1,3-Dichloropropane 2,2-Dichloropropane Di -isopropyl ether Ethylbenzene Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene 2-Butanone (MEK) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene m&p-Xylenes Surrogate Recovery Toluene-d8 Dibromofluoromethane 4-Bromofluorobenzene Extractable Petroleum Hydrocarb BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 3.4 1.0 ug/l 6210D 12/24/02 18. 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 50. ug/l 6210D 12/24/02 BDL 5.0 ug/l 6210D 12/24/02 BDL 50. ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 5.0 ug/l 6210D 12/24/02 1.9 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 55. 5.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 17. 1.0 ug/l 6210D 12/24/02 4.6 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 24. 1.0 ug/l 6210D 12/24/02 60. 2.0 ug/l 6210D 12/24/02 98. % Rec. 6210D 12/24/02 100 % Rec. 6210D 12/24/02 99. % Rec. 6210D 12/24/02 BDL 100 ug/l MADEPE 12/26/02 1 1 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 14 of 26 ENVIRONMENTAL • SCIENCE CORP. • 0 Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID MW pq Collected By David Brown Collection Date 12/16/02 15:00 Parameter REPORT OF ANALYSIS Result Det. Limit Units 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-04 Site ID : Project # Method Date Dil. C9-C18 Aliphatics BDL 100 ug/l MADEPE 12/26/02 1 C19-C36 Aliphatics BDL 100 ug/1 MADEPE 12/26/02 1 Cll-C22 Aromatics BDL 100 ug/l MADEPE 12/26/02 1 Surrogate Recovery o-Terphenyl 80.0 % Rec. MADEPE 12/26/02 1 1-Chloro-octadecane 74.0 % Rec. MADEPE 12/26/02 1 2-Fluorobiphenyl 84.0 % Rec. MADEPE 12/26/02 1 2-Bromonaphthanene 74.0 % Rec. MADEPE 12/26/02 1 625 Base/Neutrals w/ TIC Acenaphthene BDL 10. ug/l 625 12/21/02 1 Acenaphthylene BDL 10. ug/l 625 12/21/02 1 Anthracene BDL 10. ug/l 625 12/21/02 1 Benzidine BDL 50. ug/l 625 12/21/02 1 Benzo(a)anthracene BDL 10. ug/l 625 12/21/02 1 Benzo(b)fluoranthene BDL 10. ug/l 625 12/21/02 1 Benzo(k)fluoranthene BDL 10. ug/l 625 12/21/02 1 Benzo(g,h,i)perylene BDL 10. ug/l 625 12/21/02 1 Benzo(a)pyrene BDL 10. ug/l 625 12/21/02 1 Bis(2-chlorethoxy)methane BDL 10. ug/l 625 12/21/02 1 Bis(2-chloroethyl)ether BDL 10. ug/l 625 12/21/02 1 Bis(2-chloroisopropyl)ether BDL 10. ug/l 625 12/21/02 1 4-Bromophenyl-phenylether BDL 10. ug/l 625 12/21/02 1 2-Chloronaphthalene BDL 10. ug/l 625 12/21/02 1 4-Chlorophenyl-phenylether BDL 10. ug/l 625 12/21/02 1 Chrysene BDL 10. ug/l 625 12/21/02 1 Dibenz(a,h)anthracene BDL 10. ug/l 625 12/21/02 1 3,3-Dichlorobenzidine BDL 10. ug/l 625 12/21/02 1 2,4-Dinitrotoluene BDL 10. ug/l 625 12/21/02 1 2,6-Dinitrotoluene BDL 10. ug/l 625 12/21/02 1 Fluoranthene BDL 10. ug/l 625 12/21/02 1 Fluorene BDL 10. ug/l 625 12/21/02 1 Hexachlorobenzene BDL 10. ug/l 625 12/21/02 1 Hexachloro-1,3-butadiene BDL 10. ug/l 625 12/21/02 1 Hexachlorocyclopentadiene BDL 10. ug/l 625 12/21/02 1 Hexachloroethane BDL 10. ug/l 625 12/21/02 1 Indeno(1,2,3-cd)pyrene BDL 10. ug/l 625 12/21/02 1 Isophorone BDL 10. ug/l 625 12/21/02 1 Naphthalene BDL 10. ug/l 625 12/21/02 1 Nitrobenzene BDL 10. ug/1 625 12/21/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 15 of 26 ENVIRONMENTAL • SCIENCE CORP. 0 • Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID MW -�Lf Collected By David Brown Collection Date 12/16/02 15:00 Parameter n-Nitrosodimethylamine n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine Phenanthrene Benzylbutyl phthalate Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene Acid Extractables 4-Chloro-3-methylphenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol Surrogate Recovery Nitrobenzene-d5 2-Fluorobiphenyl p-Terphenyl-d14 Phenol-d5 2-Fluorophenol 2,4,6-Tribromophenol REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-04 Site ID : Project # Result Det. Limit Units Method Date Dil. BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 67. Rec. 625 12/21/02 1 72. Rec. 625 12/21/02 1 89. Rec. 625 12/21/02 1 35. Rec. 625 12/21/02 1 46. 96 Rec. 625 12/21/02 1 81. % Rec. 625 12/21/02 1 cl,.-"� d() Terrie Fudge, ISC Re esentative BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Page 16 of 26 ENVIRONMENTAL • SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received Description Sample ID Collected By Collection Date December 19, 2002 Atlas Distributing Mw-� v?(,)3 David Brown 12/16/02 16:00 REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-05 Site ID : Project # Parameter Result Det. Limit Units Method Date Dil. Lead BDL 5.0 ug/l 6010B 12/20/02 Volatile Petroleum Hydrocarbons BDL 100 ug/l MADEPV 12/19/02 C5-C8 Aliphatics BDL 100 ug/l MADEPV 12/19/02 C9-C12 Aliphatics BDL 100 ug/l MADEPV 12/19/02 C9-C10 Aromatics BDL 100 ug/l MADEPV 12/19/02 Surrogate Recovery 2,5-Dibromotoluene(FID) 127. % Rec. MADEPV 12/19/02 2,5-Dibromotoluene(PID) 124. % Rec. MADEPV 12/19/02 Volatile Organics Acetone BDL 50. ug/l 6210D 12/24/02 Acrolein BDL 50. ug/l 6210D 12/24/02 Acrylonitrile BDL 50. ug/l 6210D 12/24/02 Benzene BDL 1.0 ug/l 6210D 12/24/02 Bromobenzene BDL 1.0 ug/l 6210D 12/24/02 Bromodichloromethane BDL 1.0 ug/1 6210D 12/24/02 Bromoform BDL 1.0 ug/l 6210D 12/24/02 Bromomethane BDL 1.0 ug/l 6210D 12/24/02 n-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 sec-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 tert-Butylbenzene BDL 1.0 ug/l 6210D 12/24/02 Carbon tetrachloride BDL 1.0 ug/l 6210D 12/24/02 Chlorobenzene BDL 1.0 ug/l 6210D 12/24/02 Chlorodibromomethane BDL 1.0 ug/l 6210D 12/24/02 Chloroethane BDL 1.0 ug/l 6210D 12/24/02 Chloroform BDL 5.0 ug/l 6210D 12/24/02 Chloromethane BDL 1.0 ug/l 6210D 12/24/02 2-Chlorotoluene BDL 1.0 ug/l 6210D 12/24/02 4-Chlorotoluene BDL 1.0 ug/l 6210D 12/24/02 1,2-Dibromo-3-Chloropropane BDL 2.0 ug/l 6210D 12/24/02 1,2-Dibromoethane BDL 1.0 ug/l 6210D 12/24/02 Dibromomethane BDL 1.0 ug/l 6210D 12/24/02 1,2-Dichlorobenzene BDL 1.0 ug/l 6210D 12/24/02 1,3-Dichlorobenzene BDL 1.0 ug/l 6210D 12/24/02 1,4-Dichlorobenzene BDL 1.0 ug/l 6210D 12/24/02 Dichlorodifluoromethane BDL 1.0 ug/l 6210D 12/24/02 1,1-Dichloroethane BDL 1.0 ug/l 6210D 12/24/02 1,2-Dichloroethane BDL 1.0 ug/l 6210D 12/24/02 1,1-Dichloroethene BDL 1.0 ug/l 6210D 12/24/02 1 1 1 1 1 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 17 of 26 0 0 ENVIRONMENTAL • SCIENCE CORP. r� 0 Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID MW-P ? Collected By David Brown Collection Date 12/16/02 16:00 Parameter cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,1-Dichloropropene 1,3-Dichloropropane 2,2-Dichloropropane Di -isopropyl ether Ethylbenzene Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene 2-Butanone (MEK) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl chloride o-Xylene m&p-Xylenes Surrogate Recovery Toluene-d8 Dibromofluoromethane 4-Bromofluorobenzene Extractable Petroleum Hydrocarb REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-05 Site ID : Project # Result Det. Limit Units Method Date BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 50. ug/l 6210D 12/24/02 BDL 5.0 ug/1 6210D 12/24/02 BDL 50. ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 5.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 5.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/1 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 1.0 ug/l 6210D 12/24/02 BDL 2.0 ug/1 6210D 12/24/02 96. % Rec. 6210D 12/24/02 110 % Rec. 6210D 12/24/02 94. % Rec. 6210D 12/24/02 BDL 100 ug/l MADEPE 12/26/02 Dil. 1 1 1 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 18 of 26 ENVIRONMENTAL • SCIENCE CORP. • 0 REPORT OF ANALYSIS Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID MW/.5 Collected By David Brown Collection Date 12/16/02 16:00 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-05 Site ID : Project # Parameter Result Det. Limit Units Method Date Dil. C9-C18 Aliphatics BDL 100 ug/1 MADEPE 12/26/02 1 C19-C36 Aliphatics BDL 100 ug/1 MADEPE 12/26/02 1 C11-C22 Aromatics BDL 100 ug/1 MADEPE 12/26/02 1 Surrogate Recovery o-Terphenyl 79.0 % Rec. MADEPE 12/26/02 1 1-Chloro-octadecane 63.0 % Rec. MADEPE 12/26/02 1 2-Fluorobiphenyl 88.0 % Rec. MADEPE 12/26/02 1 2-Bromonaphthanene 88.0 % Rec. MADEPE 12/26/02 1 625 Base/Neutrals w/ TIC Acenaphthene BDL 10. ug/l 625 12/21/02 1 Acenaphthylene BDL 10. ug/l 625 12/21/02 1 Anthracene BDL 10. ug/l 625 12/21/02 1 Benzidine BDL 50. ug/l 625 12/21/02 1 Benzo(a)anthracene BDL 10. ug/l 625 12/21/02 1 Benzo(b)fluoranthene BDL 10. ug/l 625 12/21/02 1 Benzo(k)fluoranthene BDL 10. ug/l 625 12/21/02 1 Benzo(g,h,i)perylene BDL 10. ug/l 625 12/21/02 1 Benzo(a)pyrene BDL 10. ug/1 625 12/21/02 1 Bis(2-chlorethoxy)methane BDL 10. ug/l 625 12/21/02 1 Bis(2-chloroethyl)ether BDL 10. ug/1 625 12/21/02 1 Bis(2-chloroisopropyl)ether BDL 10. ug/1 625 12/21/02 1 4-Bromophenyl-phenylether BDL 10. ug/1 625 12/21/02 1 2-Chloronaphthalene BDL 10. ug/l 625 12/21/02 1 4-Chlorophenyl-phenylether BDL 10. ug/1 625 12/21/02 1 Chrysene BDL 10. ug/1 625 12/21/02 1 Dibenz(a,h)anthracene BDL 10. ug/1 625 12/21/02 1 3,3-Dichlorobenzidine BDL 10. ug/l 625 12/21/02 1 2,4-Dinitrotoluene BDL 10. ug/1 625 12/21/02 1 2,6-Dinitrotoluene BDL 10. ug/l 625 12/21/02 1 Fluoranthene BDL 10. ug/1 625 12/21/02 1 Fluorene BDL 10. ug/l 625 12/21/02 1 Hexachlorobenzene BDL 10. ug/l 625 12/21/02 1 Hexachloro-1,3-butadiene BDL 10. ug/l 625 12/21/02 1 Hexachlorocyclopentadiene BDL 10. ug/1 625 12/21/02 1 Hexachloroethane BDL 10. ug/l 625 12/21/02 1 Indeno(1,2,3-cd)pyrene BDL 10. ug/1 625 12/21/02 1 Isophorone BDL 10. ug/l 625 12/21/02 1 Naphthalene BDL 10. ug/l 625 12/21/02 1 Nitrobenzene BDL 10. ug/1 625 12/21/02 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Page 19 of 26 C. • ENVIRONMENTAL SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID Collected By Collection Date Parameter MW-f 3 David Brown 12/16/02 16:00 n-Nitrosodimethylamine n-Nitrosodiphenylamine n-Nitrosodi-n-propylamine Phenanthrene Benzylbutyl phthalate Bis(2-ethylhexyl)phthalate Di-n-butyl phthalate Diethyl phthalate Dimethyl phthalate Di-n-octyl phthalate Pyrene 1,2,4-Trichlorobenzene Acid Extractables 4-Chloro-3-methylphenol 2-Chlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 4,6-Dinitro-2-methylphenol 2,4-Dinitrophenol 2-Nitrophenol 4-Nitrophenol Pentachlorophenol Phenol 2,4,6-Trichlorophenol Surrogate Recovery Nitrobenzene-d5 2-Fluorobiphenyl p-Terphenyl-dl4 Phenol-d5 2-Fluorophenol 2,4,6-Tribromophenol REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 December 26,2002 ESC Sample # L99295-05 Site ID : Project # Result Det. Limit Units Method Date Dil. BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 BDL 10. ug/1 625 12/21/02 1 BDL 10. ug/l 625 12/21/02 1 71. % Rec. 625 12/21/02 1 76. % Rec. 625 12/21/02 1 100 % Rec. 625 12/21/02 1 37. % Rec. 625 12/21/02 1 50. % Rec. 625 12/21/02 1 88. % Rec. 625 12/21/02 1 C-yj�e�- 11200 Terrie Fudge, ZSC Re resentative BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Page 20 of 26 ENVIRONMENTAL • SCIENCE CORP. REPORT OF ANALYSIS Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID LSA-1 3-4 FT Collected By David Brown Collection Date 12/17/02 00:00 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 - January 08,2003 ESC Sample # L99295-06 Site ID Project # Parameter Dry Result Det. Limit Units Method Date Dil. Total Solids 87.5 % 254OG 12/20/02 1 Volatile Petroleum Hydrocarbons BDL 5.7 mg/kg MADEPV 12/24/02 50 C5-C8 Aliphatics BDL 5.7 mg/kg MADEPV 12/24/02 50 C9-C12 Aliphatics BDL 5.7 mg/kg MADEPV 12/24/02 50 C9-C10 Aromatics BDL 5.7 mg/kg MADEPV 12/24/02 50 Surrogate Recovery 2,5-Dibromotoluene(FID) 114. °s Rec. MADEPV 12/24/02 1 2,5-Dibromotoluene(PID) 109. °s Rec. MADEPV 12/24/02 1 Volatile Organics Acetone BDL 0.057 mg/kg 8260B 12/23/02 1 Benzene BDL 0.0011 mg/kg 8260B 12/23/02 1 Bromodichloromethane BDL 0.0011 mg/kg 8260B 12/23/02 1 • Bromoform Bromomethane BDL BDL 0.0011 0.0011 mg/kg mg/kg 8260B 8260B 12/23/02 12/23/02 1 1 Carbon tetrachloride BDL 0.0011 mg/kg 8260B 12/23/02 1 Chlorobenzene BDL 0.0011 mg/kg 8260B 12/23/02 1 Chlorodibromomethane BDL 0.0011 mg/kg 8260B 12/23/02 1 Chloroethane BDL 0.0011 mg/kg 8260B 12/23/02 1 2-Chloroethyl vinyl ether BDL 0.057 mg/kg 8260B 12/23/02 1 Chloroform BDL 0.0057 mg/kg 8260B 12/23/02 1 Chloromethane BDL 0.0011 mg/kg 8260B 12/23/02 1 1,2-Dichlorobenzene BDL 0.0011 mg/kg 8260B 12/23/02 1 1,3-Dichlorobenzene BDL 0.0011 mg/kg 8260E 12/23/02 1 1,4-Dichlorobenzene BDL 0.0011 mg/kg 8260B 12/23/02 1 Dichlorodifluoromethane BDL 0.0011 mg/kg 8260B 12/23/02 1 1,1-Dichloroethane BDL 0.0011 mg/kg 8260B 12/23/02 1 1,2-Dichloroethane BDL 0.0011 mg/kg 8260B 12/23/02 1 1,1-Dichloroethene BDL 0.0011 mg/kg 8260E 12/23/02 1 cis-1,2-Dichloroethene BDL 0.0011 mg/kg 8260E 12/23/02 1 trans-1,2-Dichloroethene BDL 0.0011 mg/kg 8260B 12/23/02 1 1,2-Dichloropropane BDL 0.0011 mg/kg 8260B 12/23/02 1 cis-1,3-Dichloropropene BDL 0.0011 mg/kg 8260B 12/23/02 1 trans-1,3-Dichloropropene BDL 0.0011 mg/kg 8260B 12/23/02 1 Di -isopropyl ether BDL 0.0011 mg/kg 8260B 12/23/02 1 Ethylbenzene BDL 0.0011 mg/kg 8260B 12/23/02 1 2-Butanone (MEK) BDL 0.057 mg/kg 8260B 12/23/02 1 Methylene Chloride BDL 0.0057 mg/kg 8260B 12/23/02 1 4-Methyl-2-pentanone (MIBK) BDL 0.057 mg/kg 8260B 12/23/02 1 Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted 0 Page 21 of 26 ENVIRONMENTAL • SCIENCE CORP. Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 Date Received December 19, 2002 Description Atlas Distributing Sample ID LSA-1 3-4 FT Collected By David Brown Collection Date 12/17/02 00:00 REPORT OF ANALYSIS 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 January 08,2003 ESC Sample # L99295-06 Site ID Project # Parameter Dry Result Det. Limit Units Method Date Dil. Methyl tert-butyl ether BDL 0.057 mg/kg 8260B 12/23/02 1 1,1,2,2-Tetrachloroethane BDL 0.0011 mg/kg 8260B 12/23/02 1 Tetrachloroethene BDL 0.0011 mg/kg 8260E 12/23/02 1 Toluene BDL 0.0057 mg/kg 8260B 12/23/02 1 1,1,1-Trichloroethane BDL 0.0011 mg/kg 8260B 12/23/02 1 1,1,2-Trichloroethane BDL 0.0011 mg/kg 8260B 12/23/02 1 Trichloroethene BDL 0.0011 mg/kg 8260B 12/23/02 1 Trichlorofluoromethane BDL 0.0011 mg/kg 8260B 12/23/02 1 Vinyl chloride BDL 0.0011 mg/kg 8260B 12/23/02 1 Xylenes, Total BDL 0.0034 mg/kg 8260B 12/23/02 1 Surrogate Recovery Toluene-d8 99. % Rec. 8260B 12/23/02 1 Dibromofluoromethane 100 % Rec. 8260B 12/23/02 1 4-Bromofluorobenzene 85. % Rec. 8260B 12/23/02 1 • Extractable Petroleum Hydrocarb BDL 6.3 mg/kg MADEPE 12/23/02 1 C9-C18 Aliphatics BDL 6.3 mg/kg MADEPE 12/23/02 1 C19-C36 Aliphatics BDL 6.3 mg/kg MADEPE 12/23/02 1 C11-C22 Aromatics BDL 6.3 mg/kg MADEPE 12/23/02 1 Surrogate Recovery o-Terphenyl 69.0 % Rec. MADEPE 12/23/02 1 1-Chloro-octadecane 79.0 % Rec. MADEPE 12/23/02 1 2-Fluorobiphenyl 77.0 % Rec. MADEPE 12/23/02 1 2-Bromonaphthanene 42.0 °s Rec. MADEPE 12/23/02 1 Base/Neutral Extractables Acenaphthene BDL 0.38 mg/kg 8270C 12/20/02 1 Acenaphthylene BDL 0.38 mg/kg 8270C 12/20/02 1 Anthracene BDL 0.38 mg/kg 8270C 12/20/02 1 Benzidine BDL 0.38 mg/kg 8270C 12/20/02 1 Benzo(a)anthracene BDL 0.38 mg/kg 8270C 12/20/02 1 Benzo(b)fluoranthene BDL 0.38 mg/kg 8270C 12/20/02 1 Benzo(k)fluoranthene BDL 0.38 mg/kg 8270C 12/20/02 1 Benzo(g,h,i)perylene BDL 0.38 mg/kg 8270C 12/20/02 1 Benzo(a)pyrene BDL 0.38 mg/kg 8270C 12/20/02 1 Bis(2-chlorethoxy)methane BDL 0.38 mg/kg 8270C 12/20/02 1 Bis(2-chloroethyl)ether BDL 0.38 mg/kg 8270C 12/20/02 1 Bis(2-chloroisopropyl)ether BDL 0.38 mg/kg 8270C 12/20/02 1 4-Bromophenyl-phenylether BDL 0.38 mg/kg 8270C 12/20/02 1 2-Chloronaphthalene BDL 0.38 mg/kg 8270C 12/20/02 1 Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted • Page 22 of 26 Lebanon R 0 Mt. 3 Mt. Juliet, TN 7122 ENVIRONMENTAL (615) 758-5858 1-800-767-5859 SCIENCE CORP. Fax (615) 758-5859 • Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. David Brown January 08,2003 EHC, Inc. PO Box 902 Red Springs, NC 28377 ESC Sample # L99295-06 Date Received December 19, 2002 Description Atlas Distributing Site ID Sample ID LSA-1 3-4 FT Project # Collected By David Brown Collection Date 12/17/02 00:00 Parameter Dry Result Det. Limit Units Method Date Dil. 4-Chlorophenyl-phenylether BDL 0.38 mg/kg 8270C 12/20/02 1 Chrysene BDL 0.38 mg/kg 8270C 12/20/02 1 Dibenz(a,h)anthracene BDL 0.38 mg/kg 8270C 12/20/02 1 3,3-Dichlorobenzidine BDL 0.38 mg/kg 8270C 12/20/02 1 2,4-Dinitrotoluene BDL 0.38 mg/kg 8270C 12/20/02 1 2,6-Dinitrotoluene BDL 0.38 mg/kg 8270C 12/20/02 1 Fluoranthene BDL 0.38 mg/kg 8270C 12/20/02 1 Fluorene BDL 0.38 mg/kg 8270C 12/20/02 1 Hexachlorobenzene BDL 0.38 mg/kg 8270C 12/20/02 1 Hexachloro-1,3-butadiene BDL 0.38 mg/kg 8270C 12/20/02 1 Hexachlorocyclopentadiene BDL 0.38 mg/kg 8270C 12/20/02 1 Hexachloroethane BDL 0.38 mg/kg 8270C 12/20/02 1 Indeno(1,2,3-cd)pyrene BDL 0.38 mg/kg 8270C 12/20/02 1 Isophorone BDL 0.38 mg/kg 8270C 12/20/02 1 Naphthalene BDL 0.38 mg/kg 8270C 12/20/02 1 Nitrobenzene BDL 0.38 mg/kg 8270C 12/20/02 1 • n-Nitrosodimethylamine BDL 0.38 mg/kg 8270C 12/20/02 1 n-Nitrosodiphenylamine BDL 0.38 mg/kg 8270C 12/20/02 1 n-Nitrosodi-n-propylamine BDL 0.38 mg/kg 8270C 12/20/02 1 Phenanthrene BDL 0.38 mg/kg 8270C 12/20/02 1 Benzylbutyl phthalate BDL 0.38 mg/kg 8270C 12/20/02 1 Bis(2-ethylhexyl)phthalate BDL 0.38 mg/kg 8270C 12/20/02 1 Di-n-butyl phthalate BDL 0.38 mg/kg 8270C 12/20/02 1 Diethyl phthalate BDL 0.38 mg/kg 8270C 12/20/02 1 Dimethyl phthalate BDL 0.38 mg/kg 8270C 12/20/02 1 Di-n-octyl phthalate BDL 0.38 mg/kg 8270C 12/20/02 1 Pyrene BDL 0.38 mg/kg 8270C 12/20/02 1 1,2,4-Trichlorobenzene BDL 0.38 mg/kg 8270C 12/20/02 1 Acid Extractables 4-Chloro-3-methylphenol BDL 0.38 mg/kg 8270C 12/20/02 1 2-Chlorophenol BDL 0.38 mg/kg 8270C 12/20/02 1 2,4-Dichlorophenol BDL 0.38 mg/kg 8270C 12/20/02 1 2,4-Dimethylphenol BDL 0.38 mg/kg 8270C 12/20/02 1 4,6-Dinitro-2-methylphenol BDL 0.38 mg/kg 8270C 12/20/02 1 2,4-Dinitrophenol BDL 0.38 mg/kg 8270C 12/20/02 1 2-Nitrophenol BDL 0.38 mg/kg 8270C 12/20/02 1 4-Nitrophenol BDL 0.38 mg/kg 8270C 12/20/02 1 Pentachlorophenol BDL 0.38 mg/kg 8270C 12/20/02 1 Phenol BDL 0.38 mg/kg 8270C 12/20/02 1 2,4,6-Trichlorophenol BDL 0.38 mg/kg 8270C 12/20/02 1 Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: This report shall not be reproduced, except in full, without the written approval from ESC. The reported analytical results relate only to the sample submitted 0 Page 23 of 26 0 ENVIRONMENTAL SCIENCE CORP. • REPORT OF ANALYSIS Mr. David Brown EHC, Inc. PO Box 902 Red Springs, NC 28377 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 January 08,2003 ESC Sample # : L99295-06 Date Received December 19, 2002 Description Atlas Distributing Site ID Sample ID LSA-1 3-4 FT Project # Collected By David Brown Collection Date 12/17/02 00:00 Parameter Dry Result Det. Limit Units Method Date Dil. Surrogate Recovery Nitrobenzene-d5 69. % Rec. 8270C 12/20/02 1 2-Fluorobiphenyl 84. % Rec. 8270C 12/20/02 1 p-Terphenyl-d14 100 % Rec. 8270C 12/20/02 1 Phenol-d5 72. % Rec. 8270C 12/20/02 1 2-Fluorophenol 68. % Rec. 8270C 12/20/02 1 2,4,6-Tribromophenol 110 % Rec. 8270C 12/20/02 1 • Terrie Fudge, ES Repr sentative Results listed are dry weight basis. BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Laboratory Certification Numbers: A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01 KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233 Note: This report shall not be reproduced, except in full, without the written approval from ESC. • The reported analytical results relate only to the sample submitted Page 24 of 26 Attachment A List of Analytes with QC Qualifiers • Sample # Analyte Qualifier L99295-01 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-02 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-03 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-04 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-05 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-06 Benzidine J4 4-Nitrophenol J4 2-Chloroethyl vinyl ether J3J4 • Page 25 of 26 Attachment B Explanation of QC Qualifier Codes • Qualifier Meaning J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable unless qualified as 'R, (Rejected). Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. • Control Limits 2-Fluorophenol 31-119 Nitrobenzene-d5 43-118 Dibromfluoromethane 72-125 Phenol-d5 12-134 2-Fluorobiphenyl 45-128 Toluene-d8 79-120 2,4,6-Tribromophenol 51-141 Terphenyl-d14 43-137 4-Bromofluorobenzene 66-131 TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. • Page 26 of 26 Attachment A List of Analytes with QC Qualifiers C, C J • Sample # Analyte Qualifier L99295-01 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-02 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-03 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-04 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-05 Acrolein J4 Benzene J4 Bis(2-chlorethoxy)methane J3 Bis(2-chloroisopropyl)ether J3 Isophorone J3 Naphthalene J3 n-Nitrosodi-n-propylamine J3 1,2,4-Trichlorobenzene J3 L99295-06 Benzidine J4 4-Nitrophenol J4 2-Chloroethyl vinyl ether J3J4 Page 25 of 26 Attachment B Explanation of QC Qualifier Codes Qualifier Meaning • J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable unless qualified as 'R' (Rejected). Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. • Control Limits 2-Fluorophenol 31-119 Nitrobenzene-d5 43-118 Dibromfluoromethane 72-125 Phenol-d5 12-134 2-Fluorobiphenyl 45-128 Toluene-d8 79-120 2,4,6-Tribromophenol 51-141 Terphenyl-d14 43-137 4-Bromofluorobenzene 66-131 TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. • Page 26 of 26 • Client Name: Project Name: Site Location: VPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued EHC, Inc. Atlas Distributing nir• Laboratory Name: NC Certification # (LAB) Environmental Science Corporation 375 Sample Identification L99295-01 1-99295-03 L99295-04 L99295-05 Sample Description — MW-1 MW-2D WATER WATER N/A N/A 12/16/02 12/16/02 12/19/02 12/19/02 N/A N/A 12/19/02 12/19/02 N/A N/A MW-3 WATER MW-4 Sample Matrix WATER Collection Option (for soil)* N/A 12/16/02 12/19/02 N/A Date Collected 12/16/02 Date Received 12/19/02 N/A Date Extracted N/A 12/19/02 N/A Date Analyzed 12/19/02 Dry Weight % Dilution Factor N/A 200 e 1 <100 ' 1 370 1 <100 1 _ CS-C8 Aliphatics* in ug/L C9-C12 Aliphatics* in ug/L 250 1 <100 1 270 1 <100 1 C9-C10 Aromatics* in ug/L 130 1 <100 1 130 1 <100 1 Surrogate %Recovery -FID 118% 114% 119% 116% 128% 123% 127% Surrogate % Recovery - PID 124% * Option 1=Established fill line on vial Option 2=Sampling Device (indicate brand, e.g. EnCore) Option 3=Field weight of soil. ** Range results should exclude any surrogates, internal standards, or Target PAH analytes. Percent Recovery - Fortified Blank (Spike) - PID Relative Percent Difference - PID Duplicate Percent Recovery - Fortified Blank (Spike) - FID Relative Percent Difference - FID Duplicate Initial Calibration Date ration Ranges and Limits Attachment 2 VPH Laboratory Reporting Form 12/19/2002 NOTE: Please include units as appropriate Method of Quantitation (Circle one) C Curve > Average Response Factor Calibration Concentration Levels • 0.075 mg/L CS-C8 0.375 mg/L Coef of Det (r^2) Aliphatics 0.750 mg/L 1.00 7.5 mg/L Linear Fit 11.25 mg/L i 0.055 mg/L C9-C12 I 0.275 mg/L Coef of Det (r^2) j - 0.550 mg/L 13.5 Aliphatics 5.50 mg/L ;RSD - 8.25 mg/L 0.010 mg/L C9-C10 0.050 mg/L Coef of Det (r^2) Aromatics 0.100 mg/L 1.00 1.00 mg/L Linear Fit 1.50 mg/L NOTE: Please indicate units as appropriate. Calibration Check Date Calibration 12/19/2002 CS-C8 Aliphatics 0.75 6.5 .8 C9-C12 Aliphatics .55 9.5 .5 C9-C10 Aromatics 0.10 9.5 .11 MDL = Method Detection Limit RPD = Relative Percent Difference ML = Minimum Limit %RSD = Percent Relative Standard Deviation RL = Reportable Limit CCC = Correlation Coefficient of Curve 0EHC, Inc. Atlas Distributing NC L99295-01 Client Name: Project Name: Site Location: VPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued EHC, Inc. Laboratory Name: Environmental Science Corporation Atlas Distributing NC NC Certification # (LAB) 375 Sample Identification L99295-02 Sample Description MW-2 Sample Matrix WATER Collection Option (for soil)* N/A Date Collected 12/16/02 12/19/02 Date Received Date Extracted N/A - 12/21/02 N/A - - ---- ---- Date Analyzed Dry Weight % Dilution Factor C5-C8 Aliphatics* in ug/L <100 1 - uilt ah C9-C12 Aliphatics* in ug/L <100 1 C9-C10 Aromatics* in ug/L <100 1 Surrogate % Recovery - FID 94% 93% Surrogate % Recovery - PID * Option 1=Established fill line on vial Option 2=Sampling Device (indicate brand, e.g. EnCore) Option 3=Field weight of soil. ** Range results should exclude any surrogates, internal standards, or Target PAH analytes. Percent Recovery - Fortified Blank (Spike) - PID Relative Percent Difference - PID Duplicate Percent Recovery - Fortified Blank (Spike) - FID Relative Percent Difference - FID Duplicate Attachment 2 VPH Laboratory Reporting Form PInitial Calibration Date 12/23/2002 alibration Ranges and Limits CS-C8 Aliphatics 0.0062 mg/L70.02g/L 0.1 mg/L C9-C12 Aliphatics 0.0032 mg/Lg/L 0.1 mg/L C9-C10 Aromatics 0.0011 mg/L 0.003 mg/L 0.1 mg/L NOTE: Please include units as appropriate Method of Quantitation (Circle one) C Curve j Average Response Factor Calibration Concentration Levels — • 0.075 mg/L CS-C8 0.375 mg/L Coef of Det (r^2) Aliphatics 0.750 mg/L .998 7.5 mg/L Linear Fit 11.25 mg/L j 0.055 mg/L C9-C12 �_ 0.275 mg/L Coef of Det (r^2) 0.550 mg/L 1.000 Aliphatics 5.50 mg/L Linear Fit 8.25 mg/L 0.010 mg/L C9-C10 0.050 mg/L Coef of Det (r^2) Aromatics 0.100 mg/L 1.00 1.00 mg/L Linear Fit 1.50 mg/L NOTE: Please indicate units as appropriate. Calibration Check Date 12/19/2002 Calibration t �0 SIR 11"It" �t �2 • .77 Aromatics MDL = Method Detection Limit ML = Minimum Limit RL = Reportable Limit 0- EHC, Inc. Atlas Distributing NC L99295-02 RPD = Relative Percent Difference %RSD = Percent Relative Standard Deviation CCC = Correlation Coefficient of Curve Client Name: Project Name: Site Location: Sample Identification Sample Description Sample Matrix Collection Option (for soil)* Date Collected Date Received Date Extracted Date Analyzed _ _ _— Dry Weight % Dilution Factor C5-C8 Aliphatics* in mg/kg C9-C12 Aliphatics* in mg/kg C9-C10 Aromatics* in mg/kg Surrogate % Recovery - FID Surrogate % Recovery - PID VPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued EHC, Inc.__ Atlas Distributing NC Laboratory Name: Environmental Science Corporation NC Certification # (LAB) 375 L99295-06 LSA-1 3-4 FT SOIL Encore-- ------ --- - 12/17/02 12/19/02 -- _- 12/ 17/02 12/24/02 87.5% 50 114% 109% * Option 1=Established fill line on vial Option 2=Sampling Device (indicate brand, e.g. EnCore) Option 3=Field weight of soil. ** Range results should exclude any surrogates, internal standards, or Target PAH analytes. Percent Recovery - Fortified Blank (Spike) - PID Relative Percent Difference - PID Duplicate Percent Recovery - Fortified Blank (Spike) - FID Relative Percent Difference - FID Duplicate Initial Calibration Date bration Ranges and Limits Attachment 2 VPH Laboratory Reporting Form 12/23/2002 CS-C8 Aliphatics 0.0062 mg/L 0.02 mg/L 0.1 mg/L C9-Cl2 Aliphatics 0.0032 mg/L 0.01 mg/L 0.1 mg/L C9-C10 Aromatics 0.0011 mg/L 0.003 mg/L 0.1 mg/L NOTE: Please include units as appropriate Method of Quantitation (Circle one) Curve j Average Response Factor Calibration Concentration Levels -- • 0.075 mg/L MMIM C5-C8 0.375 mg/L Coef of Det (r^2) Aliphatics 0.750 mg/L - 3.7 7.5 mg/L RSD 11.25 mg/L 0.055 mg/L C9-C12 0.275 mg/L Coef of Det (r^2) 0.550 mg/L 9•3 Aliphatics , 5.50 mg/L RSD 8.25 mg/L 0.010 mg/L C9-C10 0.050 mg/L I Coef of Det (r^2) Aromatics ! 0.100 mg/L 21.0 _ 1.00 mg/L RSD 1.50 mg/L Ii NOTE: Please indicate units as appropriate. Calibration Check Date 12/24/2002 Calibration MDL = Method Detection Limit ML = Minimum Limit RL = Reportable Limit go EHC, Inc. Atlas Distributing NC L99295-06 RPD = Relative Percent Difference %RSD = Percent Relative Standard Deviation CCC = Correlation Coefficient of Curve 0 EPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued Client Name: EHC, Inc. Laboratory Name: Environmental Science Corporation Project Name: Atlas Distributing NC Certification # (LAB) 375 Site Location: NC Now Sample Identification L99295-01 . .. ........... L99295-02 L99295-03 L99295-04 L99296-05 Sample Description MW-1 M.W-2 WATER MW-2D WATER MW-3 MW-4 Sample Matrix WATER WATER WATER Date Collected 12/16/02 12/19/02 N/A 12/26/02 N/A 12/16/02 12/19/02 N/A 12/26/02 N/A 12/16/02 12/16/02 12/16/02 Date Received Date Extracted Date Analyzed Dry Weight % 12/19/02 12/19/02 N/A 12/19/02 N/A N/A 12/26/02 12/26/02 N/A 12/26/02 NIA N/A <100 I Dilution Factor C9-C18 Alliphatics* in ug/L <100 1 <100 1 <100 <100 I C119-C36 Aliphatics* in ug/L <100 1 <100 1 <100 1 <100 1 <100 C1 I -C22 Aromatics* in ug/L <100 1 <100 1 <100 1 <100 1 <100 OTP '0' 2F13F 2BN Surrogate % Recovery 88% 74% 74% 79% 79% 84% 80% 79% Surrogate% Recovery Fractionation Surrogate %Rec. 74% 96% 95% --- 56% ... 91 % 80% 74% 63% 84% 88% Fractionation Surrogate % Rec. 74% 88% Range results should exclude any surrogates, internal standards, or Target PAH analytes. ** Blank correction has been applied per method guidance. Percent Recovery - Fortified Blank (Spike) 161% 99% 841%1. 9 Relative Percent Difference - Sample Duplicates 7 8 9 Attachment 2 EPH Laboratory Reporting Form Initial Calibration Date 12/3/2002 ration Ranges and Limits C9-C18 Aliphatics 0.009341727 mg/L 0.029706691 mg/L 0.1 mg/L C19-C36 Aliphatics 0.013788582 mg/L 0.043847692 mg/L 0.1 mg/L C11-C22 Aromatics 0.004464143 mg/L 0.014195974 mg/L 0.1 mg/L NOTE: Please include units as appropriate Method of Quantitation (Circle one) Curve Average Response Factor Calibration Concentration Levels • 0.080 mg/L C9-C18 0.375 mg/L Coef of Det (r^2) 0.750 mg/L Aliphatics 4.6%rsd 6.0 mg/L Linear Fit 12.0 mg/L 0.055 mg/L C19-C36 0.275 mg/L —I Coef of Det (r^2) Aliphatics- 0.550 mg/L 4.40 mg/L - — 3.78%rsd Linear Fit 8.0 mg/L 0.010 mg/L C11-C22 0.050 mg/L — Coef of Det (r^2) Aromatics j _ 0.100 mg/L 9.1 %rsd 0.800 mg/L Linear Fit 1.60 mg/L NOTE: Please indicate units as appropriate. Calibration Check Date Calibration • EHC, Inc. Atlas Distributing NC L99295-01 11 /7/2002 MDL = Method Detection Limit ML = Minimum Limit RL = Reportable Limit RPD = Relative Percent Difference %RSD = Percent Relative Standard Deviation CCC = Correlation Coefficient of Curve Client Name: Project Name: Site Location: EPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued EHC, Inc. Atlas Distributing NC Laboratory Name: NC Certification # (LAB) Environmental Science Corporation 375 Sample Identification L99295-06 Sample Description LSA-1 3-4 FT Sample Matrix SOIL Date Collected --- - 12/17/02 ----...-------------- Date Received Date Extracted Date Analyzed Dry Weight % Dilution Factor 12/19/02 12/19/02 12/23/02 87.50 <6.3 1 MOM C9-C18 Aliphatics" in mg/kg C19-C36 Aliphatics' in mg/kg <6.3 _ 1 -- --- ---- --- C11-C22 Aromatics' in mg/kg <6.3 1 - ---- °TP COD 2FBF 26N Surrogate % Recovery 69% Surrogate % Recovery 79% 84.4% 42% Fractionation Surrogate % Rec. Fractionation Surrogate % Rec. " Range results should exclude any surrogates, internal standards, or Target PAH analytes. "* Blank correction has been applied per method guidance. t Percent Recovery - Fortified Blank (Spike) 73% 110% 98% Relative Percent Difference - Sample Duplicates 6 11 2 Initial Calibration Date ration Ranges and Limits 12/3/2002 Attachment 2 EPH Laboratory Reporting Form C9-C18 Aliphatics 0.009341727 mg/L 0.029706691 mg/L 0.1 mg/L C19-C36 Aliphatics 0.013788582 mg/L 0.043847692 mg/L 0.1 mg/L C11-C22 Aromatics 0.004464143 mg/L 0.014195974 mg/L 0.1 mg/L NOTE: Please include units as appropriate Method of Quantitation (Circle one) Curve Average Response Factor Calibration Concentration Levels • 0.080 mg/L C9-C18 0.375 mg/L i Coef of Det (r^2) Aliphatics 0.750 mg/L 4.6%rsd 6.0 mg/L Linear Fit 12.0 mg/L 0.055 mg/L C19-C36 0.275 mg/L Coef of Det (r^2) 0.550 mg/L 3.78%rsd Aliphatics - - - 4.40 mg/L - Linear Fit 8.0 mg/L 0.010 mg/L C11-C22 0.050 mg/L Coef of Det (r^2) Aromatics 0.100 mg/L _' 9.1 %rsd 0.800 mg/L Linear Fit - 1.60 mg/L NOTE: Please indicate units as appropriate. Calibration Check Date Calibration • EHC, Inc. Atlas Distributing NC L99295-06 11 /7/2002 MDL = Method Detection Limit ML = Minimum Limit RL = Reportable Limit RPD = Relative Percent Difference %RSD = Percent Relative Standard Deviation CCC = Correlation Coefficient of Curve Environmental Science Corp. • SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS 0 • SAMPLE ID. Client Name: EHC, Inc. MW-1 Contract: Matrix (soil/water): WATER ESC Sample No: L99295-01 Date Collected: 12/16/2002 Lab File ID: 1220 22.D Dilution Factor: 1.0 Date Analyzed: 12/21/2002 Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds . Therefore, not all TIC's are identified and quantitated using individual standards . TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard . from the total ion chromatogram . TIC's are identified and quantitated only if the peak area is 10 % or more of that of the nearest internal standard . CONCENTRATION UNITS: Number TICS found: 8 mg/L CAS NO. COMPOUND RT EST. CONC. Q 000108-88-3 Toluene 4.60 8.0391 000100-41-4 Ethylbenzene 6.20 3.8648 000106-42-3 p-Xylene 6.71 9.9219 000611-14-3 Benzene, 1-ethyl-2-methyl- 7.69 3.6734 000095-36-3 1,2,4-Trimethylbenzene 8.14 1.2218 000095-36-3 1,2,4-Trimethylbenzene 8.52 1.2120 000496-11-7 Indane 8.73 6.5606 002870-04-4 Benzene, 2-ethyl-1,3-dimethyl- 1 8.92 3.1891 Comments: All compounds reported have a match quality of 80% or higher FORM I SV-1 Sw-846 8270 Environmental Science Corp. • SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS • SAMPLE ID. Client Name: EHC, Inc. MW-2 Contract: Matrix (soil/water): WATER ESC Sample No: L99295-02 Date Collected: 12/16/2002 Lab File ID: 1220 23.D Dilution Factor: 1.0 Date Analyzed: 12/21/2002 Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds . Therefore, not all TIC's are identified and quantitated using individual standards . TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard . from the total ion chromatogram . TIC's are identified and quantitated only if the peak area is 10 % or more of that of the nearest internal standard . Number TICS found: 4 CONCENTRATION UNITS: mg/L CAS NO. COMPOUND RT EST. CONC. Q 000108-88-3 Toluene 4.60 0..31 000135-01-3 Benzene, 1,2-diethyl- 8.81 3.3348 000084-69-5 1,2-Benzenedicarboxylic acid, bis(2-meth 16.14 1.0637 000057-10-3 Hexadecanoic acid 16.68 1 3.7780 Comments: All compounds reported have a match quality of 80% or higher FORM I SV-1 SW-846 8270 Environmental Science Corp. • SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS • Client Name: EHC. Inc. Contract: SAMPLE ID. MW-2D Matrix (soil/water): WATER ESC Sample No: L99295-03 Date Collected: 12/16/2002 Lab File ID: 1220 24.D Dilution Factor: 1.0 Date Analyzed: 12/21/2002 Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds . Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard . from the total ion chromatogram . TIC's are identified and quantitated only if the peak area is 10 % or more of that of the nearest internal standard . Number TICS found: 3 CONCENTRATION UNITS: mg/L CAS NO. COMPOUND RT EST. CONC. Q 000108-88-3 Toluene 4.60 16740013659 000112-95-8 Eicosane 21.41 3.3579 000112-95-8 Eicosane 21.96 3.5302 Comments: All compounds reported have a match quality of 80% or higher FORM I SV-1 SW-846 8270 Environmental Science Corp. • SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Client Name: EHC, Inc. Contract: Matrix (soil/water): WATER Date Collected: 12/16/2002 Date Analyzed: 12/21/2002 ESC Sample No: Lab File ID: Dilution Factor: Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds . Therefore, not all TIC's are identified and quantitated using individual standards . TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard. from the total ion chromatogram. TIC's are identified and quantitated only if the peak area is 10 % or more of that of the nearest internal standard . Number TICS found: 8 SAMPLE ID. MW-3 L99295-04 1220_25.D CONCENTRATION UNITS: mg/L CAS NO. COMPOUND RT EST. CONC. Q 000108-88-3 Toluene 4.60 0.0408 001462-03-9 Cyclopentanol, 1-methyl- 5.03 9.2712 000100-41-4 Ethylbenzene 6.20 2.1008 000106-42-3 p-Xylene 6.71 3.1133 000611-14-3 Benzene, 1-ethyl-2-methyl- 7.69 1.5554 000095-36-3 1,2,4-Trimethylbenzene 8.15 3.1777 000526-73-8 Benzene, 1,2,3-trimethyl- 8.52 9.7711 000496-11-7 1 Indane 8.73 9.6214 Comments: All compounds reported have a match quality of 80% or higher FORM I SV-1 SW-846 8270 Environmental Science Corp. • SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS • SAMPLE ID. Client Name: EHC, Inc. MW-4 Contract: Matrix (soil/water): WATER ESC Sample No: L99295-05 Date Collected: 12/16/2002 Lab File ID: 1220 26.D Dilution Factor: 1.0 Date Analyzed: 12/21/2002 Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds . Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard . from the total ion chromatogram. TIC's are identified and quantitated only if the peak area is 10 % or more of that of the nearest internal standard . Number TICS found: 4 CONCENTRATION UNITS: mg/L CAS NO. COMPOUND RT EST. CONC. Q 000108-88-3 Toluene 4.60 2.7532 000140-66-9 Phenol, 4-(1,1,3,3-tetramethylbutyl)- 15.00 2.1839 025154-52-3 Phenol, nonyl- 15.11 2.2939 054932-78-4 Phenol, 4-(2,2,3,3-tetramethylbutyl)- 15.36 2.2734 Comments: All compounds reported have a match quality of 80% or higher FORM I SV-1 SW-846 8270 Environmental Science Corp. • SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS C J r1 L.J Client Name: EHC, Inc. Contract: Matrix (soil/water): WATER ESC Sample No: Lab File ID: Date Collected: Dilution Factor: Date Analyzed: 12/20/2002 Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds . Therefore, not all TIC's are identified and quantitated using individual standards. TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard . from the total ion chromatogram . TIC's are identified and quantitated only if the peak area is 10 % or more of that of the nearest internal standard . Number TICS found: 0 SAMPLE ID. MB94572 SBLK02 1220_03.D CONCENTRATION UNITS: mg/L CAS NO. COMPOUND RT EST. CONC. Q Comments: All compounds reported have a match quality of 80% or higher FORM I SV-1 SOP-846 8270 Environmental Science Corp. • SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Client Name: EHC, Inc. Contract: Matrix (soil/water): Date Collected: Date Analyzed: WATER 12/20/2002 SAMPLE ID. MB94572 ESC Sample No: SBLK03 Lab File ID: 1220 04.D Dilution Factor: 1.0 Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds . Therefore, not all TIC's are identified and quantitated using individual standards . TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard . from the total ion chromatogram . TIC's are identified and quantitated only if the peak area is 10 % or more of that of the nearest internal standard . Number TICS found: 0 CONCENTRATION UNITS: mg/L CAS NO. COMPOUND RT EST. CONC. Q • • Comments: All compounds reported have a match quality of 80% or higher FORM I SV-1 SW-846 8270 �a. � nc•4c !Inc�`J` PO Box 902 Red S rin s NC 28377 p g ' Alternate billing information: :_ � c Anal sis/Container/Preservative in of Cuslop -�-`t- Prepared by: ENVIRONMENTAL SCIENCE CORP. 12065 Lebanon Road Mt. Juliet, TN 37122 Phone (615) 758-5858 Phone (800) 767-5859 FAX (615) 758-5859 I ! J J 3 i i � $ j ijaI �.) �� � �--, t 1 J i I O v1 v l i I I i , - 1 N ( I �^ ! �� Report: /' I8 f ., ��"� Project name: 1-L 3 `I -r Phone(910) 843-4456 FAX: (910) 843-5376 Client Project #: ESC Key: Collected by: (print): w�i , d �wV\ Site/Facility ID#: P.O.#: — , V n ' riV )d�0,� CoCode: ENVHYD (lab use only) Template/Prelogin Cooler # Shipped Via: Collected by (signature): ���---L._----- Rush? ( Lab MUST Be Notified) Same Day ....... 200% Next Day........ 100% Two Day .........50% Date Results Needed: N0 of o Yes Sample ID Comp/Grab Matrix' Depth Date Time Cntrs Remarks/Contaminant Sample # (lab only) ." C—L� iZllWoZ �2Eo 2 2. -2,1 2, ti w,a C-w --� 2iZ►- ooIts rK w- L4 C-� j IZ/,16z t� -�i 2, L I I I � � �-y . 0 So -�1 t2ir 710 �S i1i Lf o 'Matrix: SS - Soil/Solid GW - Groundwater WW - Waste Water DW - Drinking Water OT - Other. Remarks: j �� ej �-1 .2 a c, �-o t IV - pit flow Temp Other Relinqu' he y, ( gature ( Date: / z Time: Received by: (Signature) mp es re urne via: UPS kFedEx❑Courier p Condition: lab use only) ( .00 Relinquished by: (Signature) Received by: (Signature) A Date: Time: Tem : Bottles Received: vtaG Relinquished by: (Signature) Date: Time: Received for I b Dat Time: pH Checked: NCF: (Signature) �olp l'Li (�% ILL tomL 2