HomeMy WebLinkAboutFA-1_29001_M_RP_20030115.PDFPost Office Box 902
207 West Fourth Avenue
Red Springs, NC 28377
Telephone: (910) 843-4456
Fax (910) 843-5376
ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, INC.
Report of
Phase II Limited Site Assessment
Former Atlas Distributing Company Inc.
5510 Cliffdale Road
Fayetteville, Cumberland County, North Carolina
Prepared For:
Mr. John L. Beard
Atlas Distributing Company
1214 Morganton Road
Fayetteville, North Carolina 28305
Prepared By:
Environmental Hydrogeological Consultants, Inc.
Post Office Box 902
207 West Fourth Avenue
Red Springs, North Carolina 28377
EHC Project Number: 02-EV1209-3
January 15, 2003
RECEIVED
JAN 17 2003
DENR-FAYETiEMLLE REGIONAL OFRCE
Serving North & South Carolina
since 1986
www.environmentalnc.com
Phase II Limited Site Assessment Report
DATE OF REPORT: January 15, 2003
Facility I.D.: Unregistered
Site Name: Former Atlas Distributing
Site Location: 5510 Cliffdale Road,
Nearest City/Town: Fayetteville, NC
UST Owner: USTs have been removed
Address:
29001
UST Incident# (if known): Pcnditg
County: Cumberland
Phone:
UST Operator: C/O Mr. John Beard — Atlas Distributing Company
Address: 1214 Morganton Road, Fayetteville NC 28305 Phone: (910) 864-5000
Property Owner: C/O Mr. John Beard — Atlas Distributing Company
Address: 1214 Morganton Road, Fayetteville NC 28305 Phone: (910) 864-5000
Property Occupant: Harris Wholesale, Inc.
Address: 5510 Cliffdale Road, Fayetteville, NC 28305 Phone: (910)—860-1283
Consultant/Contractor: Environmental Hydrogeological Consultants, Inc.
Address: 207 West 4ch Ave, Red Springs, NC 28377 Phone: (910) 843-4456
Release Information
Date Discovered: August, 1994
Latitude: N 35' 3.554'
Longitude: W 78' 57.986'
Estimated Quantity of Release: Unknown
Cause of Release: Underground Storage Tank
Source of Release (e.g., Piping/UST): Unknown
Sizes and contents of UST system(s) from which the release occurred:
(2) 10,000 gallon gasoline (removed)
(1) 12,000 gallon diesel (removed)
1, 0 G a -� I�j ^ �✓� a Professional
one) of Environmental Hydrogeological Consultants,
contained in this report is correct and accurate to the be;
(Please Affix Seal and Signature)
Post Office Box 902
207 West Fourth Avenue
Red Springs, NC 28377
Telephone: (910) 843-4456
Fax (910) 843-5376
ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, INC.
11
January 15, 2003
Mr. Ken Currie
NCDENR — Fayetteville Regional Office
Systel Building, Ste 714
Fayetteville, NC 28301
Subject: Report of Phase II Limited Site Assessment
Former Atlas Distributing Company, Inc.
5510 Cliffdale Road
Fayetteville, North Carolina
EHC Project No. 02-EV1209-3
Dear Mr. Currie:
REC
JAN 17 2003
DENR - FAYETTEYIU.E REWA OR E
On behalf of Mr. John L. Beard, Environmental Hydrogeological Consultants (EHC) is
pleased to submit this Report of Phase II Limited Site Assessment conducted at the above
referenced location. This work was requested to address the possibility of groundwater
contamination.
In general, the assessment activities have included drilling of soil exploration borings and
collection of soil samples for description; installation of a groundwater monitoring wells;
collection of groundwater samples for chemical testing; and investigation of the geology and
hydrogeology in the vicinity of the site. The objective of our services was to provide a limited
assessment pertaining to the distribution of petroleum constituents in the groundwater, site
hydrogeology, and the potential for human exposure and to chemical contaminants. The
scope of work for this project is intended to comply with appropriate state environmental
regulations contained in 15 NCAC2L.
...........
Serving North & South Carolina
since 1986 www.environmentalnc.com
If any questions concerning this report or our findings, please contact us at (910) 843-4456.
We look forward to receiving your comments on this report.
Sincerely,
ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS, INC.
as Ammons David L. Brown, L.G.
Project Manager Senior Geologist
Enclosures
•
TABLE OF CONTENTS
COVER LETTER
1.0 INTRODUCTION............................................................................................................. 1
1.1 Purpose of Investigation.......................................................................................... 1
1.2 Scope of Work Summary........................................................................................ 2
2.0 SITE HISTORY................................................................................................................ 2
2.1 Underground Storage Tank Removal and Previous Environmental Work ............ 2
3.0 RISK CHARACTERIZATION........................................................................................ 4
4.0 POTENTIAL RECEPTORS AND MIGRATION PATHWAYS ................................... 7
4.1 Water Supply Wells................................................................................................. 7
4.2 Potential Receptors.................................................................................................. 7
4.2.1 Surface Water........................................................................................... 8
4.2.2 Wellhead Protection Areas...................................................................... 8
4.2.3 Deep Aquifers of the Coastal Plain Region ............................................. 8
4.2.4 Subsurface Structures............................................................................... 9
4.2.5 Area Land Use......................................................................................... 9
4.2.6 Property Owners and Occupants............................................................. 9
5.0 SITE TOPOGRAPHY, GEOLOGY AND HYDROGEOLOGY................................. 10
5.1 Topographic Conditions........................................................................................ 10
5.2 Regional Geology and Hydrogeology................................................................... 10
5.3 Site Geology.......................................................................................................... 11
5.4 Soil Borings and Sampling.................................................................................... 11
6.0 GROUND WATER INVESTIGATION........................................................................ 12
6.1 Site Hydrogeological Study Methods...................................................................... 12
6.1.1 Monitoring Well Installation.................................................................. 12
6.1.2 Ground -Water Gauging and Sampling .................................................. 13
7.0 RESULTS ...................
.. 14
7.1 Ground Water Flow Directions............................................................................. 14
7.2 Ground -Water Sample Analyses.......................................................................... 14
8.0 CONCLUSIONS............................................................................................................. 15
9.0 RECOMMENDATIONS................................................................................................ 16
•
Table of Contents (coot.)
REFERENCES
TABLES
Table 1 ADJACENT PROPERTY OWNERS
Table 2 GROUND WATER ELEVATION, WELL CONSTRUCTION AND FIELD
PARAMETER DATA
Table 3 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
FIGURES
Figure 1
USGS SITE TOPOGRAPHIC MAP
Figure 2
ADJACENT PROPERTY BOUNDARY MAP
Figure 3
SITE MAP WITH FORMER UST LOCATIONS
Figure 4
GROUNDWATER FLOW DIRECTION MAP
Figure 5
GROUNDWATER ANALYSIS RESULTS SUMMARY
APPENDICES
Appendix A NOTICE OF REGULATORY REQUIREMENTS
Appendix B SOIL BORING LOGS
Appendix C WELL CONSTUCTION RECORDS
Appendix D LABORATORY REPORT
Atlas Distributing Company, Phase H LSA
Final
January, 2003
0 1.0 INTRODUCTION
Mr. John L. Beard, contracted Environmental Hydrogeological Consultants (EHC) to conduct
a Phase II Limited Site Assessment (LSA) as outlined in EHC's Cost Proposal to Complete a
Phase H LSA dated September 26, 2002 at the Former Atlas Distributing Company, Inc. site
located at 5510 Cliffdale Road in Fayetteville, North Carolina (Figure 1). This scope of
services was required the North Carolina Department of Environment and Natural Resources
(NCDENR) Underground Storage Tank (UST) Section, Fayetteville Regional Office (FRO)
due to a risk based assessment assigned in a "Notice of Regulatory Requirements" (NORR)
dated September 5, 2002 that is included in Appendix A. The NORR is based on chemical
analysis results of samples collected from onsite monitoring well (MW-1) that indicated
concentrations of petroleum constituent -benzene, to be in excess of 10 times the North
Carolina Administrative Code (NCAC) 2L Standard. Therefore, a Phase II LSA was
conducted at the site.
The following report includes documentation of the methods utilized in this study and
presents the results of data analyses, conclusions and recommendations for achieving
compliance with state regulatory requirements.
0 1.1 Purpose of Investigation
The purpose of the Phase II LSA includes the following:
• To identify chemical constituents detected in ground water in the subject area
exceeding NCAC, Title 15A, Subchapter 2L (2L) Groundwater Standards;
• To identify chemical constituents which exceed gross contamination levels (GCLs)
and;
• Prepare a Phase II LSA report containing a description of our assessment activities,
results, and conclusions.
This report is designed to provide information required by the NCDENR, Division of Waste
Management (DWM), in accordance with the document entitled "Guidelines for Assessment
and Corrective Action — North Carolina Underground Storage Tank Section", dated April
2001, for a Phase II LSA. This document also addresses groundwater requirements as
provided in the Groundwater Section Guidelines for the investigation and Remediation for
• Soil and Groundwater dated July 2000 as provided in the North Carolina Administrative Code
1
Atlas Distributing Company, Phase II LSA Final
January, 2003
Title 15A Subchapter 2L Sections .0100, .0200 and .0300, "Classifications and Water Quality
Standards Applicable to the Groundwater of North Carolina".
The Phase II LSA scope of work is intended to provide additional data via drilling and
sampling of additional monitoring wells.
1.2 Scope of Work Summary
As part of the Phase II LSA activities, EHC conducted the following tasks:
• Construction of 2 type -II monitoring wells.
• Construction of a deep type -III monitoring well to assess the vertical extent of the
contamination.
• Sampling of the monitoring wells using required analysis methods.
• Survey of site monitoring wells.
• Preparation of a Ph. II LSA report of results and findings.
The results and conclusions of this LSA work are intended for use in the development of an
accurate site ranking and/or risk classification as required by the DWM. The specific methods
employed during performance of the project activities and the results, conclusions and
recommendations of the LSA are described within the following sections of this report.
2.0 SITE HISTORY
2.1 Underground Storage Tank Removal and Previous Environmental Work
A report dated April 4, 1991, by Carl M. Taylor and Sons Construction Company of Hope
Mills, NC documents the removal of USTs, associated piping and pump islands at the site
as follows:
Previous Underground Storage Tank Systems
Tank Number
Date of Installation
Capacity
Product
Date Closed
1
Unknown
10,000gal
Gasoline
3129191
2
Unknown
10, 000 gal
Gasoline
3129191
3
Unknown
12, 000 gal
Diesel
3129191
2
Atlas Distributing Company, Phase II LSA Final
January, 2003
• The report does not state if ground water was encountered in the excavation, however 10
confirmation soil samples were collected for laboratory analysis using Environmental
Protection Agency (EPA) Method 5030. Petroleum hydrocarbons were not detected above
the method detection limit of 5.0 milligrams per kilogram (mg/Kg) in the submitted samples.
Though not included in the closure report, a 550 gallon UST located near the diesel UST was
also removed at this time according to Atlas Distributing Company personnel. Details
concerning this 550 gallon UST were not available.
A Phase I Environmental Site Assessment (ESA) dated August 18, 1994 was prepared by
EHC for the site. The ESA recommended that additional sampling be performed and that
monitoring wells be constructed in the former UST basins.
The additional environmental work based on the recommendations is documented in EHC's
Phase II ESA dated August 23, 1994. The report details that 4 borings were advanced for soil
collection purposes, 3 borings were advanced to construct temporary monitoring wells (TAH-
1 through 3) and that 2 permanent monitoring wells (MW-1 and MW-2) were constructed.
According to the report, 135 tons of soil was excavated from the site for offsite remediation.
As documented in EHC's Phase H ESA Report, at least 5 sampling events were conducted on
MW-I, and MW-2 in July and August 1994. Gasoline constituents were demonstrated to
exceed the 2L Standards in each of the wells.
3
Atlas Distributing Company, Phase H LSA Final
January, 2003
• 3.0 RISK CHARACTERIZATION
The following sections are reproduced from the Limited Site Assessment Report format,
pages B-18 through B-21 of the Guidelines for the Assessment and Corrective,
Underground Storage Tank Section, April, 2001.
Limited Site Assessment Risk Classification and Land Use Form
Part I — Groundwater/Surface water/Vapor Impacts
High Risk
1. Has the discharge or release contaminated any water supply well including
any used for non -drinking purposes?
NO:
2. Is a water supply well used for drinking water located within 1000 feet of
the source area of the discharge or release?
NO:
• 3. Is a water supply well used for an purpose e. irrigation, washing cars
pp Y Y p� � g• g g ,
industrial cooling water, filling swimming pools) located within 250 feet of
the source area of the release or discharge?
NO:
•
4. Does the groundwater within 500 feet of the source area of the discharge or
release have the potential for future use in that there is no other source of
water supply other than the groundwater?
NO: Public water is currently supplied to the surrounding area by the
City of Fayetteville.
5. Do vapors from the discharge or release pose a threat of explosion because
of accumulation of the vapors in a confined space or pose any other serious
threat to public health, public safety or the environment.
NO:
4
Atlas Distributing Company, Phase H LSA
Final
January, 2003
. 6. Are there any other factors that would cause the discharge or release to pose
an imminent danger to public health, public safety, or the environment?
NO:
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the
discharge -release?
NO:
8. Is the source area of the discharge or release located with a designated
wellhead protection area as defined in 42 USC 300h(e)?
NO:
9. Is the release located in the Coastal Plain physiographic region as
designated on a map entitled "Geology of North Carolina" published by the
Department in 1985?
YES
. If yes, is the source area of the discharge located in an area in which there is
recharge to an unconfined or semi -confined aquifer that is being or may be
•
used as a source for drinking water?
UNKNOWN: It is unlikely that the source area could provide recharge
to the Upper Cape Fear Aquifer, however recharge cannot be
determined without further hydrogeologic study.
10. Do the levels of groundwater contamination for any contaminant exceed the
gross contamination levels (GCL) established (Table 7) by the Department?
NO:
Part II - Land Use
Property Containing Source Area of Release
1. Does the property contain one or more primary or secondary residences
(permanent or temporary)?
NO:
5
Atlas Distributing Company, Phase H LSA
Final
January, 2003
is park,
Does the property contain a school, daycare center, hospital, playground,
park, recreation area, church, nursing home, or other place of public
assembly?
NO:
3. Does the property contain a commercial or industrial enterprise, an inactive
commercial or enterprise, or is the land undeveloped?
YES: Commercial enterprise:
4. Do children visit the property?
NO:
5. Is the access to the property reliably restricted consistent with its use (e.g.
fences, security personnel or both)?
YES: Surrounded by chain link fence and automatic gates.
6. Do pavement, buildings, or other structures cap the contaminated soil?
YES: The soil is capped by asphalt in most areas, however the
. northern side of the parcel is not paved.
7. What is the zoning status of the property?
The facility is currently zoned as Commercial.
•
8. Is the use of the property likely to change in the next 20 years?
NO.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1000 feet of the source area of the release.
9. What is the distance from the source area of the release to the nearest
primary or secondary residence?
Residential housing is located on Cliffdale Road approximately 1,000
feet south of the source.
2
Atlas Distributing Company, Phase H LSA
Final
January, 2003
• 10. What is the distance from the source area of the release to the nearest
school, daycare center, hospital, playground, park, recreation area, church,
nursing home, or other place of public assembly?
A church is located approximately 1,000 feet south east of the site.
11. What is the zoning status of the properties in the surrounding area?
Commercial and Residential
11. Briefly characterize the use and activities of the land in the surrounding
area.
The site is near Skibo and Cliffdale Roads. Land use is light
commercial with retail stores and restraurants. A mobile home park is
located south of the site on Cliffdale Road.
4.0 POTENTIAL RECEPTORS AND MIGRATION PATHWAYS
As part of the Phase II LSA Investigation, EHC completed an evaluation of potential
• receptors, which is documented in the following section.
•
4.1 Water Supply Wells
Fayetteville city water and sewer service are both supplied to the surrounding area. Properties
visited were observed receiving these services. The site is located several miles south of
Glenville Lake and several miles west of the Cape Fear River. Public water is drawn from
intakes at Glenville Lake and the Cape Fear River.
4.2 Potential Receptors
Potential receptors considered, as part of this LSA, include identification of: adjacent property
owners; water supply wells within 1,000 feet of the source area; surface water bodies; surface
water intakes (for public water supplies and springs) that are within 0.5 miles; and
identification of subsurface structures and utilities.
7
Atlas Distributing Company, Phase II LSA
Final
January, 2003
• 4.2.1 Surface Water
Beaver Creek Pond and Beaver Creek is located approximately 1 mile west of the site.
Beaver Creek Pond is created by a artificial dam located near Mt. Gilead Church (Figure
1).
4.2.2 Wellhead Protection Areas
The Wellhead Protection Program (N.C. Division of Environmental Health, Public Water
Supply Section) was contacted to determine whether a wellhead protection area was
located near the site. There were no Wellhead Protection programs listed in Fayetteville.
The closest wellhead protection programs identified were located in Bladen County
(Bladenboro) and Robeson County (Lumberton, Parkton and Red Springs).
4.2.3 Deep Aquifers in the Coastal Plain Region
• According to Geologic Map of North Carolina, (1985), the site is located in the Atlantic
Coastal Plain Physiographic Province of North Carolina. The surficial materials at the site are
mapped as being near the boundary of the Cretaceous age Black Creek and Cape Fear
Formations. Sohl and Owens (1991) describe the Cape Fear Formation as being
"widespread in the sub -surface in North and South Carolina." Subsurface features are
described as "rhythmically interbedded sands that are green gray to bluish -green, thin
bedded to less commonly thick -bedded, and fine to coarse; and thin to thick bedded, dark
gray to greenish gray clays. Locally the sands are cross bedded but are for the most part,
massive and clayey, hence poorly sorted." Overlying the Cape Fear Formation is the Black
Creek Formation, which is commonly described as having silts/sands and clays as well as
beds of graded sands. These formations are part of primary water bearing units in the eastern
North Carolina area.
Hydraulic conductivity data for these aquifers and confining units in this area was not
available.
In the area near the site, the Cretaceous sand yields large quantities of water to wells (Schipf,
1961). The primary source of water for this aquifer is infiltrated rainfall. The surficial
0
deposits aquifer transmits water laterally to streams and serves as a source bed, holding the
Atlas Distributing Company, Phase II LSA
Final
January, 2003
• water that eventually moves downgradient to the deeper aquifers within recharge areas
(Winner and Coble, 1989).
4.2.4 Subsurface Structures
There were no basements identified during the receptor survey. The only underground
structures identified in the receptor survey were underground utilities. Most notable is the
storm drain located near MW-1. The storm drain appears to be entrenched above the water
table.
4.2.5 Area Land Use
The site is located in Fayetteville, adjacent to Cliffdale Road.
Site Specific Conditions
• Adults work at the facility, which is a beverage warehouse and distributorship.
• • The site is restricted via chain link fence and automatic gates. The groundwater is
separated from the employees by a 6-foot thick layer of soil, capped with concrete
and asphalt in most areas.
• The distance from the source area, which is the eastern UST location, to the nearest
residence or place of public assembly is approximately 1,000 feet.
• The zoning status of the site and surrounding area is mixed commercial and
residential.
•
4.2.6 Property Owners and Occupants
Properties adjacent to the site were cataloged and the owners' names and addresses were
recorded (Table 1) from Cumberland County tax records.
The results of the survey indicated 5 properties adjacent to the site. The properties were
either reported or observed to not contain supply wells. The property owners are listed in
Table 1 and the property boundaries are shown on Figure 2.
9
Atlas Distributing Company, Phase H LSA
Final
January, 2003
• 5.0 SITE TOPOGRAPHY, GEOLOGY AND HYDROGEOLOGY
The following sections describe the regional geologic conditions and the methods employed
to obtain physical data that support our discussion of the local geologic and environmental
conditions.
5.1 Topographic Conditions
As shown on Figure 1 (Delorme 3-D TopoQuads, 1999, Yarmouth), the topography of the
site is relatively flat. The elevations shown on Figure 1 indicate the property to be
approximately 230 feet above mean sea level (msl). Drainage in the vicinity of the source
area generally leaves the site via surface runoff. The site is generally located between
north -south trending valleys created by Buckhead Creek to the east and Beaver Creek to
the west.
5.2 Regional Geology and Hydrogeology
Suriiicial Aquifer - The groundwater head elevation (referenced from "above mean sea
• level or ASL") associated with the surficial aquifer monitored by the DWR in a well
located in Bladenboro, N.C. (well No. Z41U1) ranges from approximately 113 ft to
approximately 106 ft ASL and averages approximately 110 ft. The land surface elevation
at this well is 114.75 ft., resulting in a water level located approximately 43-feet below
grade.
Upper Cape Fear Aquifer - The groundwater head elevation associated with the Upper
Cape Fear Aquifer is monitored by the DWR in Bladenboro, N.C. (well No. Z 41U2) and
Boardman, N.0 (well No. AA 43 Q 1)
The groundwater head elevation in well No Z 41U2 has fallen from an elevation of
approximately 69 ft in 1975 to a current elevation of approximately 20 ft. The land surface
elevation at this well is 116.04 ft, resulting in a current water level located approximately
96 feet below grade.
The groundwater head elevation in well No. AA 43Q1 has fallen from an elevation of
approximately 75 ft in 1972 to a current elevation of approximately 20 ft. The land surface
elevation at this well is 80.46 ft, resulting in a current water level located approximately
• 60.5—feet below grade.
S
Atlas Distributing Company, Phase H LSA Final
January, 2003
The gradational decline in head elevation in the Upper Cape Fear Aquifer is consistent with
observations made by commercial well drillers and pump installers. They report an
estimated 1 to 2 foot per year drop in head elevations in deeper aquifers of the US Coastal
Plain since the 1960s (interviews with Olin, Guy, Roy and Jimmy Cribbs-Cribbs Well
Drilling, Mullins, S.C. and Fred and Wayne Grosch-Grosch Well Drilling, Dublin Ga.)
Based on discussions with industrial and commercial well drillers operating in the region,
the regional uses of the deeper aquifers are primarily municipal supply wells; wells
associated with pork and poultry operations, and irrigation wells.
5.3 Site Geology
On the basis of the soils encountered from vertical boring activities at the site, the following
limited interpretation of the site geology was developed. The boring logs have been included
as Appendix B.
In general, the geologic material encountered from the ground surface was observed to be
orange, brown to light gray sandy clay and clay to approximately 15 feet below land surface
40 (bls) in which, a silty, fine to coarse, sand is encountered to approximately 20 feet. Red
orange, mottled, massive sandy clay was present to approximately 33 feet in which silty fine
sand was observed to 38 feet. Soft, dark gray massive clay was observed from 38 to 40 feet
bls. Borings were not advanced beyond 40 feet as part of this investigation.
•
5.4 Soil Borings and Sampling
As documented in the Site History Section, wells MW-1 and MW-2 were installed as part of
the Phase II ESA in 1994.
In December 2002, EHC drilled two soil borings (MW-3 and MW-4) to explore subsurface
conditions and allow for type II monitoring well construction and deep well MW-2D (type III
well) as part of Phase II LSA activities. The soil boring/wells were drilled using mechanical
drilling equipment, hollow -stem auger (HSA) and mud rotary techniques. The locations of
soil borings/monitoring wells are displayed as monitoring wells on the Site Map (Figure 3)
including property boundaries, buildings, and former UST and pump island locations.
11
Atlas Distributing Company, Phase H LSA Final
January, 2003
•
0
Mechanical drill rig soil samples were collected, via split spoon, at 5-foot intervals until
boring termination. The soil samples and records of well construction details were logged in a
field book by EHC personnel. Boring logs for each location are included as Appendix B.
Ten soil samples were collected during tank removal activities in 1991 as Sample Test 1
through 10 for analysis using TPH 5030. Petroleum hydrocarbons were BDL in each of the
samples.
As part of Phase II LSA activities, a soil boring was advanced to the water table near MW-
2 for sampling purposes. The soil sample nearest to the water table (LSA-1, 3.0-4.0 feet)
was submitted for analysis of volatile organic compounds (VOCs) using Environmental
Protection Agency (EPA) Methods 8260 with 5035 preparation, semi -volatile compounds
using EPA Method 8270, Massachusetts Department of Environmental Protection (MADEP)
analysis of volatile petroleum hydrocarbons (VPH) and extractable petroleum
hydrocarbons (EPH). Petroleum compounds were "below detection limits" (BDL) in the
submitted samples. Laboratory reports are included in Appendix D.
6.0 GROUNDWATER INVESTIGATION
6.1 Site Hydrogeological Study Methods
A description of hydrogeologic and environmental conditions at the site was developed from
information gathered from the soil boring logs, water level measurements, topographic maps,
published information sources and groundwater sample analysis. The following sections
describe the regional and site hydrogeology as it relates to groundwater movement and the
detected petroleum compounds in ground water at the site.
6.1.1 Monitoring Well Installation
The type II monitoring wells (MW-1, MW-2, MW-3, and MW-4) consists of a 10 feet length
of two-inch inside diameter (ID), schedule 40 polyvinyl chloride (PVC) well screen with 0.01-
inch slots attached by threaded joints to an appropriate length of two-inch ID, and schedule 40
PVC riser pipe. Clean quartz filter sand was placed in the annular space between the well and
the borehole to a level at least one foot above the top of the well screen. Approximately two
feet of a hydrated bentonite seal was placed above the filter sand pack. The remaining annular
12
Atlas Distributing Company, Phase H LSA Final
January, 2003
is
space was then backfilled to the ground surface with a cement-bentonite grout. EHC
monitoring well construction details are provided in Appendix C.
The Type III well (MW-2D) is a deep telescoping well, which includes inner, and outer
casings. The Type III well was constructed by first installing an outer 6-inch casing to
separate the upper and lower portions of the aquifer. The outer casing was then pressure
grouted with a neat cement mixture, and allowed to cure for 24 hours thereby sealing the
upper portions of the surficial aquifer. After 24 hours, the annulus of the outer casing was
reamed out and drilling was continued to the desired depth of the lower portions of the
surficial aquifer. After completion of the borehole, a 2-inch inner casing and well screen was
constructed inside the casing and borehole in a manner similar to the type II well using a five-
foot well screen. Monitoring well construction details for each of the site wells are provided
in Appendix C.
The wells were developed using a pre -cleaned disposable polyethylene bailer. Groundwater
was removed until the water became reasonably clear. Field readings including
pH/temperature and conductivity were taken to insure that reasonably stabilized ground -water
parameters were achieved.
6.1.2 Groundwater Gauging and Sampling
EHC personnel collected groundwater samples from monitoring wells MW-1, MW-2, MW-
2D, MW-3 and MW-4 on December 16, 2002 as part of the Ph. II LSA investigation. Prior to
sampling, depth to groundwater was measured from the top of the PVC casing at the well.
Depth to water readings and field measurements are included as Table 2. Water from the well
was then purged using pre -cleaned, dedicated, high -density polyethylene disposable bailing
equipment.
Upon collection, the water samples were placed into laboratory -prepared containers, packed
on ice in coolers and delivered via express courier to Environmental Science Corp. (ESC) in
Mt. Juliet Tennessee (a North Carolina Certified Laboratory) for analysis. The samples were
submitted for analysis of petroleum constituents via EPA Methods 6210D with iso-propyl
ether (IPE), methyl tert-butyl ether (MTBE), ethylene di -bromide (EDB) and xylenes, semi-
volatiles via EPA 625 plus 10 tentatively identified compounds (TICS), MADEP analysis of
VPH and EPH and lead via EPA Method 6010/3030C preparation. Appropriate chain-of-
13
Atlas Distributing Company, Phase H LSA Final
January, 2003
• custody records were maintained through the sample collection and shipment of each sample,
and are attached with the laboratory reports as Appendix D.
7.0 RESULTS
7.1 Ground Water Flow Directions
Ground water levels, obtained on December 16, 2002 were observed in site monitoring wells
to range from approximately 6 feet BLS in the shallow portion of the surficial aquifer. Depth
to water in Well MW-2D was gauged 22 feet below the top of casing.
Ground water elevations, which are presented in Table 2, have been contoured on Figure 4.
Please note that the elevations are relative to a temporary benchmark with assumed elevation
of 100 feet and that the deep well is not included in the contours. The December 16, 2002
data suggest that ground water flow is to the north with a hydraulic gradient of approximately
0.005 ft/ft.
• 7.2 Groundwater Sample Analyses
A summary of ground water chemical analysis data as compared to the 2L Standards and
GCL's is included as Table 3. Copies of the laboratory reports and chain -of -custody
records for these analyses are included in Appendix D. A summary of selected petroleum
constituent results including benzene, toluene, ethyl benzene, and total xylenes (BTEX) is
included as Figure 5.
As reported previously, chemical analysis of ground -water samples has been performed on
wells MW-1 and MW-2 dating back to 1994. As shown on Table 4, several constituents
including BTEX, and MTBE exceeded the 2L Standard.
Chemical analysis of groundwater samples was collected on December 16, 2002 as part of
the Ph. II LSA investigation from MW-2D, MW-3 and MW-4. As shown by the Table,
the recent analyses indicate benzene exceeds the 2L Standard of 1.0 micrograms per liter
(ug/1) in well MW-2 with the concentration of 1.4 ug/1 and in well MW-3 with the
concentration of 14 ug/L. Chloroform was detected in well MW-2D with the concentration
of 12 ug/L and lead was detected at 18 ug/L. The 2L Standard for chloroform and lead is
• 0.19 ug/L and 15 ug/L respectively. The TIC library search identified several possible
14
Atlas Distributing Company, Phase H LSA Final
January, 2003
• organic compounds in each of the wells including 1-ethyl-2 methyl benzene, 1,2,4-
trimethylbenzene, indane, 2-ethyl-1,3-dimethyl benzene, hexadecanoic acid, and eicosane.
A complete list is included in the laboratory reports in Appendix D. 2L Standards are not
available for most of the TIC compounds.
8.0 CONCLUSIONS
Site reconnaissance indicated the surrounding properties as supplied by public water.
Water supply wells were not identified within a 1,000-foot radius around the site and
impacts to potential receptors were found to be minimal. Additional receptors that may
effect risk classification were not observed during Phase II LSA activities.
Laboratory analysis of submitted soil samples from the MW-2 location for listed parameters
including EPA Methods 8260/8270 and MADEP EPA/VPH indicated petroleum constituents
to be BDL.
The direction of ground -water flow on the site is north with an average hydraulic gradient
• of approximately 0.005 ft/ft.
Recent sampling data indicates benzene exceeds the NCAC 2L Standard in wells MW-2 and
MW-3 with concentrations of 1.4 ug/1 and 14 ug/L respectively however, GCLs were not
exceeded in the constituents analyzed for the 5 sampled wells.
NCAC 2L Standards for chloroform and lead are exceeded in MW-2D. Metals occur
naturally in soil and in dissolved phase in ground water. The turbidity (suspended
sediment) of a ground water sample can affect the concentration of the metals detected.
Analysis of metals by EPA Method 6010 or 3030C preparation requires the sample to be
preserved by nitric acid at the time of collection. The nitric acid in the sample container
may dissolve metals suspended in the sediments of a turbid sample causing and increase in
the concentrations of those metals. Therefore, the lead detected in MW-2D may be
naturally occurring rather than as the result of a release. Chloroform is associated with the
chlorination and disinfection of the public water supply. The bentonite slurry mixture used to
drill the well was mixed using the Fayetteville public water supply. It is therefore likely the
chloroform came from that source.
El
15
Atlas Distributing Company, Phase H LSA
Final
January, 2003
Downgradient well MW-3 was BDL indicating that it does not appear the plume is migration
from the site with natural ground water flow.
Based on limited receptors and migration pathways, commercial use, and concentrations of
detected constituents that do not exceed the GCL, EHC concludes that the release at this
site appears to pose limited risk to health and environment. According to risk -based rules
for USTs, it appears this site should be considered as "low risk."
9.0 RECOMMENDATIONS
On the basis of the data presented and our conclusions, EHC recommends the following:
• Submit this Phase II LSA report to the NCDWM Fayetteville Regional Office for review,
and comment.
•
•
16
• REFERENCES
Delorme 3-D TopoQuads, 1999, Yarmouth, ME 04096, Fayetteville.
Geologic Map of North Carolina, 1985, North Carolina Geological Survey.
Schipf, Robert G., Geology and Ground -Water Resources of the Fayetteville Area, Ground -
Water Bulletin Number 3, North Carolina Department of Water Resources -Division of
Ground Water, Raleigh, 1961.
Winner & Coble, 1989, U.S. Geological Survey, Open -File Report 87-690, Raleigh, North
Carolina, 57 - 62 pp.
•
0
•
•
•
TABLES
TABLE 1
ADJACENT PROPERTIES
Atlas Distributing Company
5510 Cliffdale Road
Fayetteville, NC
,/ '
IF
/r � I /n
...:
0417-06-0763
Site - Fomer Atlas Distributing
5510 Cliffdale Rd. Fayetteville NC 28305
0417-06-6874
Marsh and Evans LD-Leisure Living
5500 Cliffdale Rd.
Fayetteville NC 28314
0417-06-6207
New Sanford Milling Company
PO Box 53186
Fayetteville NC 28305
0417-06-6874
Sharlene Williams
PO Box 53646
Fayetteville NC 28305
0417-07-5002
Sharlene Williams
PO Box 53646
Fayetteville NC 28305
0407-96-6586
March F. Riddle
PO Box 53646
Fayetteville NC 28305
0407-97-7119
Triangle Builders Wholesale
PO Box 53646
Fayetteville NC 28305
0417-07-1165
riang a Builders o esa a
ox 5 4
ayettevl eNC 28305
Notes: Taken from Cumberland County Tax Records
Prepared by: David Brown
Map ID Number Corresponds
to Figure 2.
F:ProjectSites/Atlas Distributing/Adj Properties.xls
•
0
0
C9-C1 0 Aromatics
NA
NA
NA
ND
NA
NA
NA
NA
NA
NA
130
ND
ND
130
210
NS
Ma OMIT w
M11
77
U9777777
NAB.
AJI
:7NI
. . ..................
-
m
C9-C18 Aliphatics
NA
NA
NA
ND
NA
NA
NA
NA
NA
NA
ND
ND
ND
ND
4200
NS
7\0,,
MI,
IM11
CI 1 -C22 Aromatics
NA
NA
NA
I ND
NA
NA
NA
NA
NA
NA
ND
ND
ND
ND
210
NS
r
g
N
Results are presented in micrograms per liter (ugIL).
ND = "Not Detected" above laboratory detection limits. Refer to laboratory reports for detection limits
ISIS - No Standard
NA = Not Analyzed
H:Proiects%das%h20Chem Summ.xis
•
0
FIGURES
� 0
10
� 0
; 77.
ov
.0 . , I
'41
L
3-1) TopoQuads C1999 DeLorme, Yarmouth, ME 04096
Source Data: USGS FIGURE 1
1:24000 Detail 13-1 Datum WOS84
Topographic Map
EHC Atlas Distributing, Inc.
ENVIRONMENTAL HYDROGEOLOGICAL CONSULTANTS 5510 Chffdale Road
HYDROLOGY - GEOLOGY - EXPLORATION - ANALYTICAL Fayetteville, North Carolina
0417-06-6874-
nfh*" � �<' 0407-96-6586 ��'�� a �,� r.,F J-` .�•��_ � -'--� - ..
Aid
Surrounding Properties Map
s
iV
A Atlas Distfibu&g, Inc.
e. x , ,. -
•
APPENDIX A
NOTICE OF REGULATORY REQUIREMENTS
•
09/12/02 THU 10:39 FAX 910 864 5329 _ DOUBLE EAGLE
North Carolina
Department of Environment and Natural Resources
• Division of Waste Management
Underground Storage Tank Section
Fayetteville Regional Office
Michael F. Easley, Governor
William G. Ross Jr, Secretar},
Dexter R. Matthews, Director
September 5, 2002
Mr. John L. Beard
Atlas Distributing Company, Inc.
1214 Morganton Road
Fayetteville, NC 28305
Re: Notice of Regulatory Requirements
15A NCAC 2L .0115(c)
00;j
A7441illi*j
AftRYA �
NCDENR.
Risk -based Assessment and Corrective Action for Petroleum Underground Storage Tanks
Atlas Distributing Company (farmer location)
5510 Cliffidale Road
Fayetteville, Cumberland County
Facility ID #: unregistered
Incident #: pending issuance
Dear Mr. Beard:
• Information received by this office on August 27, 2002 confirms a release or discharge from a
petroleum underground storage tank (UST) system formerly located at the above -referenced
location. Records indicate that Atlas Distributing Company, Inc., was the owner of this UST sys::m
and is considered the responsible party for the release or discharge. This letter is a standard notice
explaining the actions you must take as a result of the release or discharge in accordance with North
Carolina statutes and rules. The UST Section of the Division of Waste Management administers the
state's rules for USTs and the required response for petroleum releases. Those rules are located in
Title 15A, Subchapter 2L and Title 15A, Subchapter 2N of the North Carolina Administrative Code
(NCAC).
As a responsible party, you are required to comply with the release response and corrective action
requirements of 15A NCAC 2L .0115(c), which include the requirements established in 15A NCAC
2N. Listed is a general description of actions you must take to comply with State rules. For a
detailed description of your requirements, please refer to the enclosed rules and the most rel:ent
version of the UST Section Guidelines for Assessment and Corrective Action. The guidelines are
available on the Internet at http://wastenot.enr.state.nc.us or may be purchased from the UST Section
for a fee of $8.50. To purchase a copy of the guidelines, please send a check made payable to DUNR
to:
DENR / DWM / UST Section
1637 Mail Service Center
Raleigh, NC 27699-1637
• 225 Grcen Street, Suite 714, Fayetteville, North Carolina 28301-5043
Phonc: 910-486-1541 / FAX: 910-486-0707 / Internet. http://w2stenot.enr.stitc.nc.us
AN EQU:U.OPPORTUNrtY / At•TIRNIATWL AcrtON EMPLOYtiR / SOY. POsr CONSUMPR PAPER
0002
09/12/02 THU 10:39 FAX 910 864 5329 DOUBLE EAGLE
19003
• Required Actions:
1) If you have not already done so, you must take immediate action to prevent any fur -her
release of the regulated substance into the environment and to identify and mitigate any tire,
explosion and vapor hazards; remove any free product; and comply with the requiremen�.; of
Rules .0601 through .0604 and .0701 through .0703 and .0705 of Subchapter 2N;
2) Incorporate the requirements of 15A NCAC 2N .0704 into the report to be submitte:1 in
accordance with 15A NCAC 2L .0115 (c)(3) or (c)(4), whichever is applicable (see Item #3
below). This shall constitute compliance with the reporting requirements of 15A NCAC. 2N
.0704(b);
3) If it can be demonstrated that localized soil contamination was cleaned up at the time of link
removal, you may submit a Soil Contamination Report in accordance with 15A NCAC
2L.0115(c)(3). The Soil Contamination Report must demonstrate that the soil remainin;; in
the sidewalls and at the base of the excavation is located in the unsaturated zone and does not
exceed either the soil -to -groundwater or the residential maximum soil contaminant
concentrations, whichever are lower. A Soil Contamination Report is not appropriate for
sites where contamination is situated directly on top of bedrock or once a tank clo:�ure
excavation has been back -filled. In both cases, a Limited Site Assessment Reporl is
required. A Soil Contamination Report, if applicable, is due in this office no later than
December 15, 2002. Upon approval of this report, the Department may issue a later
indicating that no further action related to this incident is required; or,
4) If the requirements of 15A NCAC .0115(ex3) cannot be met as described in Item #3 above,
• submit a Limited Site Assessment (LSA) Report in accordance with 15A NCAC 21,
.0115(c)(4), containing information needed by the Department to classify the level of risk to
human health and the environment posed by the discharge or release. The LSA Report is due
in this office no later than January 15, 2003. Based on a review of the informal_ on
submitted in the LSA, the Department will classify the risk of the discharge or release: as
high, intermediate or low. At that time, the Department will also classify the land use of -:he
site as either residential or industrial/commercial. You will be notified of the risk and land
use classifications once review of your LSA Report is completed.
5) Please note that before you sell a property or request a "No Further Action" determination for
a property that has not been remediated to below "unrestricted use" standards, you must fV-. a
Notice of Residual Petroleum ("Notice") with the Register of Deeds in the county where the
property is located (NCGS 14313-279.9 and 143B-279.11). Unrestricted use standards for
groundwater and soil are the groundwater quality standards and interim standards contai:ed
in 15A NCAC 2L .0202 and the residential maximum soil contaminant concentrati :lns
established in 15A NCAC 2L .0115, respectively. The Notice must first be approved and
notarized by the UST Section prior to conveyance of a property or prior to receiving a "No
Further Action" determination, whichever occurs first. The Notice must contain a legal
description of the property containing the source of contamination and legal description, of
any other properties that you own (or control) that are contaminated by the release. '.'he
Notice must include appropriate land use restrictions for these properties. In addition, the
Notice must identify all other properties (adjacent, adjoining, downgradient, etc.) on which
0
DOUBLE EAGLE
0 004
contamination is known to exist at the time the Notice is prepared. If contamination. is
located on more than one parcel or tract, the UST Section may require that a composite neap
or plat be prepared. After the Notice is filed with the Register of Deeds, a certified coPy of
the filed Notice must be submitted to the UST Section. Additional guidance including the
language and format of the Notice is available by calling this regional office or visiting the
UST Section web site at htip://wastenot.enr.state.nc.us.
If you believe that any of the information requested above has already been submitted, please notify
me of the date, title, and content of the documents that contain the information.
Your prompt attention to the items described herein is required. Failure to comply with the State's
rules in the manner and time specified may result in the assessment of civil penalties and /or the use
of other enforcement mechanisms available to the State. Each day that a violation continues may be
considered a separate violation. If you believe you are not the responsible party, notify the is ST
Section within 15 days of receipt of this notice.
Please note that performing assessment and cleanup work that is not required under 15A NC!kC
2L.0115 is not reimbursable from the Commercial or Noncommercial Leaking Petroletun
Underground Storage Tank Cleanup Funds.
If you have any questions regarding the actions that must be taken or the rules mentioned in -:zis
letter, please contact me at the letterhead address or at (910) 486-1541. If you have any questims
regarding trust fund eligibility or reimbursement, please contact the UST Section Trust Fund Bra::ch
at (919) 733-8486.
• Sincerely,
Kenneth E. Currie
UST Section
Enclosures: 15A NCAC 2L .0115
Notice of Residual Petroleum Format and Instructions
c: FRO Incident Management Files
Mr. Scott Jurgcnsen
Harrispark Properties
P.O. Box 1190
Raleigh, NC 27602
Mr. James Joyner, Project Manager
TRC Environmental Corp.
516 N. West Street
Raleigh, NC 27603
0
•
APPENDIX B
0
BORING LOGS
0
•
•
0
BORING LOG RECORD
Environmental Hydrogeological Consultants
207 West Fourth Avenue
Red Springs, North Carolina 28377
Ph. (910) 843-4456
Fax (910)843-5376
E
H
C Inc.
Depth
Blows
per 6"
Rec
(in.)
Description
Remarks
(USCS Symbol)
1-
5-8-12-18
24
(5.0-7.0 feet)
5-
Medium orange to red -brown, sandy CLAY. Stiff
sc
mottled.
3-4-4-6
18
(10.0 -12.0 feet)
As above
sc
10-
4-1-4-4
2
(15.0 -17.0 feet)
Light brown to tan, silty, fine to coarse SAND.
sm
15-
Wet.
2-6-6-7
18
(20.0-22 feet)
20-
Light tan to buff, sandy CLAY over gray, massive,
cl
mottled sandy CLAY.
Boring Terminated at 23.0 feet.
Notes:
•
I 0
Depth
Blows
per 6"
Rec
(in.)
Description
Remarks
(USCS Symbol)
1-
5-7-12-18
24
(5.0-7.0 feet)
5-
Red -orange, stiff, massive, mottled CLAY.
sc
3-4-5-7
8
(10.0 -12.0 feet)
Red orange to gray, mottled sandy CLAY.
sc
10-
-
5-5-7-5
12
(15.0 -17.0 feet)
Yellow brown to red gray, silty, fine to coarse
sm
15-
SAND, poorly sorted, wet.
Boring Terminated at 17.0 feet.
20-
Notes:
LJ
0
BORING LOG RECORD
Environmental Hydrogeological Consultants
207 West Fourth Avenue E
Red Springs, North Carolina 28377 H
Ph. (910) 843-4456 C Inc.
Fax (910)843-5376
Site Name Atlas Distributing rted !2�8142
Job Location Fayetteville,, NC ;, Gateomple#ed . 42�1a10�
I Drilling Method Mud Rotary Latitude IN35 3.55,V
I Longitude JW78. deg. 57.986'
Depth
Blows
NA
Description
Remarks
(USCS)
Soil Screen
(ppm)
1-
0.0-17 feet
Boring paired with MW-2. Refer to the MW-2
NA
5-
boring log.
10-
15-
10-10-16-17
(18.0-20.0 feet)
20-
Brown to gray, massive, very silty fine SAND.
sm
Driller noted fat clay layer at 22'
cl
23-
10-12-16-17
(23.0-25.0 feet)
-
As above
sm
Notes:
Drilled by Mid -Atlantic Drilling
na = Not Available
•
r
LJ
BORING LOG RECORD
Environmental Hydrogeological Consultants
207 West Fourth Avenue E
Red Springs, North Carolina 28377 H
Ph. (910) 843-4456 C Inc.
Fax (910)843-5376
Site Name
Atlas Distributing
Date Started s
: ,12/91,02;
Job Location
Faye$eville; NG
Date Compieted,_
12fta/02 ".
Boring Number
MW 2D ;(Sheet 1)
Depth to Water
- Z41.42' =' ,
Geologist
D. Brown
lVeasulrePtr ,
Top of Casing
Drilling Method
Mud Rotary
tit
N35 3.554'
FL40naitvde"
W78 deq. 57986'
Depth
Blows
24 in
Description
Remarks
(USCS)
Soil Screen
(ppm)
25-
(28.0-30.0 feet)
1-5-5-4
Red gray to pink, soft, plastic CLAY.
cl
30-
-
2-4-7-7
(33.0-35.0 feet)
35-
Clay slough and concretions
Orange -red silty, fine, sand and sand stringers.
sm
(38.0-40.0 feet)
40-
4-4-5-7
Dark gray, soft, slightly sand, micaceous, plastic
cl
-
CLAY.
Boring Terminated at 40 feet.
45-
48-
Notes:
Drilled by Mid -Atlantic Drilling
na = Not Available
•
APPENDIX C
WELL CONSTRUCTION RECORDS
•
North Carolina - Department of Environment, Heallh, and Natural Resources
Division of Environmental Management - Groundwater Section
P.O. Box 29535 - Raleigh, N.C. 27626-0535
Phone (919) 733.3221 u, /
FOR OFFICE USE ONLY
pUAD. NO. SERIALNO.
Long. RO
Min"
Basin
WELL CONSTRUCTION RECORD Basin Code
Basin coda
`LLING CONTRACTOR: L%�C, 1 U/C-. Header Ent' GW-1 Ent
STATE WELL CONSTRUCTION
DRILLER REGISTRATION NUMBER: � D 2 9 PERMIT NUMBER:
1. WELL LOCATION: (Show sketch of the location below)
Nearest Town: r �'=T�7'`f�'%C`` County: eU&
(Road, Community. or Subdivision and Lot No.)
�446-�-�'
2. OWNER 11tl �1U41; �ia _ .�
ADDRESS c 421O (' -> ez',a
(Street or Route No.)
,0 c 2,J`3403
CitjorTown State Zip Code
3. DATE DRILLED USE OF WELL%�[�f/%-�0�-
4. TOTAL DEPTH 2 v
5. CUTTINGS COLLECTED YES ❑ NOX
6. DOES WELL REPLACE EXISTING WELL? YES F NO ]
7. STATIC WATER LEVEL Below lop of Casing: _T FT.
(Use "+' it Above Top of Casing)
8. TOP OF CASING ISM-2eAl 420.nftmus Land Surface*
' Casing Terminated aVor below land surface is illegal unless a variance Is Issued
DEPTH
From To
s� /D
Z0/2
J
DRILLING LOG
Formation Description
J• �
In accordance with 15A AC 2C .0118
9. YIELD (gpm): METHOD OF TEST l�,r/ I(io-�� F ascr • D.� o�.
10. WATER ZONES (depth): _ /4/^t e4,00cb.L•// /:1 ri,
.CHLORINATION: Type
12. CASING:
Depth Diameter
From 0—To -L `= Ft.
From To Ft.
From To Ft.
13. GROUT:
Depth
From To _4 Ft
From _46 To Ft
14. SCREEN:
Amount If additional space is needed use back of form
Wall Thickness LOCATION SKETCH
or Weight/Fl. lApterial (Show direction and distance from at least two State
UC— Roads, or other map reference points)
Material Wthod
e d4crYUu.t
4c
I
Depth Diameter Slot Size material
From /O _ To 10 Ft in. •A2Z(.L in.
From To Ft. in. in. �-� •�- .-.
From To Ft. in. in.
15. SAND/GRAVEL PACK: _
Depth §ize Material ..�. .�.. `��•
From To 20 Ft. 2A- ��)""L� 664r t>+c
From To Ft.
16. REMARKS: -- —
•1 DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
SIGNATURE OF CONTRACTOR (A AGENT / 1 DATE
GW-1 REV. 9191 Submit original to Division of Environmental Management and copy to well owner.
North Carolina - Department of Environment. Health, and Natural Resources
Division of Environmental Management - Groundwater Section
P.O. Box 29535 - Raleigh, N.C. 27626.0535
Phone (919) 733-3221
WELL CONSTRUCTION RECORD
&LING CONTRACTOR:
FOR OFFICE USE ONLY
QUAD. NO. SERIALNO.
Lal. ,._ Long. RO
Minor Basin
Basin Coda
Header Ent.4 Gw-1 Ent
--� DRILLER REGISTRATION NUMBER: STATE WELL CONSTRUCTION
f (�Z PERMIT NUMBER:
1. WELL LOCATIQLL SShow sketch of the location below)
Nearest Town: - County:%�`^"� — —
(Road, (
2. OWNER
ADORE:
and
or Route No.)
DEPTH
6 m TO
t!�
�w •Sr
3.
City orXown State Zip Code
DATE DRILLED X%�Dti USE OF WELL A
2• S J
4.
TOTAL DEPTH
5.
CUTTINGS COLLECT D YES 0 NOCg
--• O Z. (D
6.
DOES WELL REPLACE EXISTING WELL? YES NC1tjj�
7.
STATIC WATER LEVEL Below lop of Casing: FT.
8.
�I (Use 't' if Above Top of Casing)
TOP OF CASING IS
_lam _ +**•theft Land Surface'
' Casing Terminated atlor below land surface Is Illegal unless a variance Is Issued
In accordance with 15 2C .011 b
9.
YIELD (gpm):_e� METHOD OF TEST WIA_•
O — /O. u
10. WATER ZONES (depth):.
46LORINATION: Type
12. CASING:
Depth Diameter
From To Ft.
From To Ft.
From To Ft.
13. GROUT:
DRILLING LOG
Formation Description
Q�ifSi�fc /"l.Rd—CoblWc.,f,,tcd
r<LCt,
d/'d�Ls.RJ �dlcclw f�/�O�,ow
Amount If additional space is neec
Wall Thickness
LOCATION SKETCH
of eMaterial (Show direction and distance from at least two State
�C- Roads, or other map reference points)
Depth Material Njqthod
From To Ft. Wfjvou.c
From To 3 Ft. 51, pu^
14. SCREEN:
Depth Diameter Slot Size M erial
From _4 To Ft ? in. • azzl in. 1/L
From To Ft. in. in.
From To Ft. in. in.
t
15. SAND/GRAVEL PACK:
.'.—� ..�
Depth S' e Material I
From To ZV Ft. 4z'
rr '= Iw & W �K IIIiO�d�:X tAa.t+rrt w1N. •11... O..�YIM y.4I
From To Ft.� •"'
16. REMARKS: — —
Of DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
v SIGNATURE OF CONTRACTOR OR AGENT I /DATE
GW-1 REV. 9,91 Submit original to Division of Environmental Management and copy to well owner.
0 ct, - LA WELL CONSTRUCTION RECORD
Worth Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME (print) C.u-4 J 9AZ-1el— CERTIFICATION # z Iq
s(
WELL CONTRACTOR COMPANY NAME JL� � � PHONE # J%T 1 gq-?- NN jG
STATE WELL CONSTRUCTION PERNIIT# 1• ASSOCIATED WQ PERMIT# N1.4
(if applicable) (if applicable)
1. WELL USE (C ck Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring IT Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use
2. WEt.L LOCATION: Topographic/Land .�e: ' setting�
Nearest Town: I.Z. County ���-r+t���Ci �� ❑Ridge ❑Slope ❑Valley 13Flat
t! 6 (• F d — 0 6 e , ' t— X� , (check appropriate box)
(Street Name. Numbers, Community, ubdivision. Lot No.. Zip Code) L tit n ttftde,of well location
3. OWNER: �c[�0 l , (-C35 �y Lv rs � -7. g
) .
(degrees/minutes/seconds)
Address u c Latitude/longitude source:t?rPS❑Topographic map
p (Street or R uteN .) r (check box)
X=1 F r�DEPTH DRILLING LOG
City or Town St a Zip Cosa From TQ Fo at' n Description
Area code- Phone number s 1 5
4. DATE. DRILLE! LLUZ-
5. TOTAL DEPTH:
6. DOES WELL REPLACE EXISTING WELL? YES0 L!r ; i6
7. STATIC WATER LEVEL Below Top of Casing: FT.
( Use --- if Above Top of Casing) A
• S. TOP OF CASING IS ' 'V, u 4-- FT. Above Land Surface*
-Top of casin; terminated at/or below land surface requires a
variance in •accordant w th I5:\ NCAC 2C .01ld. -
9. FIELD (epm): 4- j�-N METHOD OFTEN
10. WATER ZONES (depth): <:T` I S
LOCATION SKETCH
1 1. DISINFECTION. Type ti 14 Amount Show direction and distance in miles from at least
t'_. CASING: Nall Thickness two State Roads or County Roads. Include the road
Dcpth�� Diameter or Wei_ht'Ft.Material numbers and common road names.
From To Ft._-')— S< < 4c) VV_
From To Ft.
From To Ft.
13. GROUT: Depth Material /+ I thud
From d Tom_ Ft. Sfc),-,- IN
From To Ft. L'
14. SCREEN: Depth Diameter Slot Size laSerial
From eZ To Ft. in. i OIC• in.
From To Ft. in. in. w 1
OL
15. SANDiGRAVEL PACK:
Depth. t laterial
From 3 To k 77— Ft.
From To Ft.
•
16. REMARKS: `1 io."
I DO H - 1" CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STAtNDARD,0. AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
cv—
SIGNATURE OF PERSON CONSTRUCTING THE WELL
v'
DATE
e.
Submit the original to the Division of NN ater Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, INC
27699-1636 Phone No. (919) 733-3221. within 30 days. GW-I REV. 07/2001
w-3
WELL CONSTRUCTION RECORD
dWorth Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME (print) w CERTIFICATION # •29st
NVELL CONTRACTOR COMPANY NAME r= He— _) IX PHON,EI # �(D) $�/3• �/y �C�
S'rA-f E WELL CONSTRICTION PER.N11T# _ ri/1i ASSOCIATED WQ PERMIT#
(if applicable) (if applicable)
1. WELL USE (Cbeck Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use
2. WELL LOCATION:
Topographic/Land setting
Nearest Town: .'� ' Ifz County `v-wt�--z�U ❑Ridge ❑Slope ❑Valley lat
(• F� ex" rtt �C �GS� (check appropriate box)
(Street Name. Numbers. Community, ubdivision, Lot No.. Zip Code) Lvitu je/I n Itude,of well location
cur
3. OWNER: f • ) 1/ d—' �'"S 0.5t. w (degrees/minutes/seconds)
Address I Q Latitude/longitude source: E2 PS❑TopoLraphic map
(Street or R ute Nq.) (check box)
r',Ue-U. )I, i✓(_ Z -3cr, DEPTH DRILLING LOG
To Town St a jd,Zip Code Fro T,� Formation Description
If
Area rude- Phone number +`
4. DATE DRILLED 12 /41G2- L
5. TOTAL DEPTH: Z-; ` L;
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO C7� -;:I
7. STATIC WATER LEVEL Below Top of Casing: AFT.
(USe --- if Above Top of Casing)
• S. TOP OF CASING IS - 'y� e.��- FT. Above Land Surface*
*Top of casing terminated at/or below land surface requires a
variance in accordant with 1 NCAC 2C .0118.
9. YIELD (,-,pm): OF TEST
10. WATER ZONES (depth):
( Piea,&� I LOCATION SKETCH
11. DISINFECTION. Tvpc ti 6 Amount Show direction and distance in miles from at least
12. CASING: Wall Thickness two State Roads or County Roads. Include the road
Depth Diameter or We11-1htF1. Maierial numbers and common road names.
From U To (3 Ft. Si i 4c) ►' 4-
From To— Ft.
From To Ft.
13. GROUT: Depth Nlateri# M (hod
From To E Ft. i�G`� I �•
From To Ft. -rA
14. SCREEN: Depth Diamzfer Slot Size laSerial �
From t_To�Ft. � in. ;-OkC in. 1. V)
From To Ft. in. in.
15. SAND/GRAVEL PACK:
Depth t laterial
From �'I To Z) Ft._ • (t C e-
From To Ft.
16. RENIARKS:
I DO HEREBYCERTIFYTHAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTIO, TA DARDS, ND THA A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
cC
SIGNATURE OF PERSON CONSTRUCTING THE WELL DATE
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, NC
27699-1636 I'lionc No. (919) 733-3221.,*%ithin 30 dues. GW-I REV. 07/2001
'. -V\.j C
01 ��
WELL CONSTRUCTION RECORD
•North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME (print)_ (.L„: J �!� ✓/`, CERTIFICATION # Z95
WELL CONTRACTOR COMPANY NAME E ni PHONE # fYl�) S43- (Iq SG
i v -
STATE WELL CONSTRUCTION PERMIT# Jv� ASSOCIATED WQ PERMIT#
(if a licable) (if applicable)
1. WELL USE (C ck Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use
2. WELL LOCATION:
Nearest Town: A e: I1z County �u-S tb-,, a
(Street Name. Numbers, Community, tubdivision, Lot No.. Zip Code) /
3. OWNER: !- ax 44L—S 6.'J. (-c
Address I XJ
Q (Street or R ute N
t , City 5 p��✓ State -b Zip Code
Area code- Phone number
4. DATE DRILLED 12- r - I ZI002—
5. TOTAL DEPTH: Ll0, o , r
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO I]T
7. STATIC WATER LEVEL Below Top of Casing:.? •ti.L* FT.
( Use "+" if Above Top of Casing)
• S. TOP OF CASING IS ' 'v-, G +- FT. Above Land Surface*
'Tup of rasing terminated at/or below land surface requires a
variance in accordanc with.I5A NCAC 2C .0118. J
9. YIELD (gpm): G� METHOD OF TEST
10. WATER ZONES (depth): 33 G - �?L
•
11.
DISINFECTION. Type
ti Amount
l'_.
CASING:
Wall Thickness
Depth
Diameter or WeightlFt. 1 enal
From 0
To 31
Ft.. S< < 4r} �-
From G
To 10
Ft. C
From
To
Ft.
13.
GROUT:
Depth
Material 1 thod
From Q
To�
Ft.. Q✓m;�
From
To
Ft. ►-e_A -
14.
SCREEN:
Depth
Diameter Slot Size �ta4erial
From'723
To 'iF,
Ft.in. GICt in. L
From
To
Ft. in. in.
15.
SAND/GRAVEL PACK:
Depth
Pi3q laterial
From 3 X. To_U Ft. t C 6-
From
To
Ftt..
16.
REMARKS:
1 "
�N e__ _ ` ` t 4C 1 C- I c_cv
Topographic/Land setting
❑Ridge ❑Slope ❑Valley lat
(check appropriate box)
L�y, itu�e/l deof well loation
y �" cv�;3s.
$�
T (degrees/minutes/seconds)
Latitude/longitude source:f6PS❑Topographic map
(check box)
DEPTH DRILLING LOG
From To Formation Description
Z - i3
:3 -5- 31--'
LOCATION SKETCH
Show direction and distance in miles from at least
two State Roads or County Roads. Include the road
numbers and common road names. ki
�1 w
�t 5to-1�-
1
GI►r=Fd,�
1 DO HEREB ' TIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRU TION TANDARf�S, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
SIGNATURE OF PERSON CONSTRUCTING THE WELL DATE
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, NC
27699-1636 Phone No. (919) 733-3221, within 30 dais. GW-I REV. 0712001
M
•
�J
0
Monitoring Well Construction Record
Type 11
Environmental Hydrogeological Consultants
207 West Fourth Avenue
Red Springs, North Carolina 28377
Ph. (910) 843-4456
Fax(910)843-5376
Former Atlas Distributing Company, Inc.
Well Number
MW-1
Date of Installation 7/19/94
Job Location
Fayetteville, North Carolina
Well Material 2" I.D. Sch 40
Top of Casing
98.58 Feet
Lock Number Twist Lock
Ground Surface
98.70 Feet
Sandpack Material #2 Well Pack
Geologist
B. Bright
Static Water Level 5.70
Lock Number
Twist Lock
jDate Measured 12/16/02
Sandpack Material
#2 Well Pack
Latitude N35 3.554'
Drilling Method
Hollow Stem Auger
ILongitude W78 57.986'
Steel -Flush Mount Cover
Locking Well Cap
Top Of Grout —0.5 feet
Bentonite Seal 6.0 feet
Borehole Diameter Unknown
Top of Sandpack 8.0 feet
Top of Well Screen 10.0 feet
Depth of Borehole 20.0'
Bottom of Screen 20.0 feet
Notes:
Static Water Level Measured From the Top of Casing (TOC)
•
•
r 1
L_.J
Monitoring Well Construction Record
Type II
Environmental Hydrogeological Consultants
207 West Fourth Avenue
Red Springs, North Carolina 28377
Ph. (910) 843-4456
Fax(910)843-5376
Former Atlas Distributing Company, Inc.
Well Number
MW-2
Date of Installation 7/19194
Job Location
Fayetteville, North Carolina
Well Material 2" I.D. Sch 40
Top of Casing
98.48 Feet
Lock Number Twist Lock
Ground Surface
98.58 Feet
Sandpack Material #2 Well Pack
Geologist
B. Bright
Static Water Level 6.11'
Lock Number
Twist Lock
Date Measured 12/16/02
Sandpack Material
#2 Well Pack
Latitude N35 3.554'
Drilling Method
Hollow Stem Auger
Longitude W78 57.986'
Steel -Flush Mount Cover
Locking Well Cap
Top Of Grout —0.5 feet
Bentonite Seal 2.0 feet
Borehole Diameter
Unknown
Top of Sandpack 3.0 feet
Top of Well Screen 4 feet
Depth of Borehole
14'
Bottom of Screen 14.0 feet
Notes:
Free Product in well.
r1
0
Monitoring Well Construction Record
Type II
Environmental Hydrogeological Consultants
207 West Fourth Avenue
Red Springs, North Carolina 28377
Ph. (910) 843-4456
Fax(910)843-5376
Former Atlas Distributing Company, Inc.
Well Number
MW-3
Date of Installation 12/4/02
Job Location
Fayetteville, North Carolina
Well Material 2" I.D. Sch 40
Top of Casing
99.79 Feet
Lock Number Twist Lock
Ground Surface
99.82 Feet
Sandpack Material #2 Well Pack
Geologist
D. Brown
Static Water Level 7.72'
Lock Number
Twist Lock
Date Measured 12/16/02
Sandpack Material
#2 Well Pack
Latitude N35 3.554'
Drilling Method
Hollow Stem Auger
Longitude W78 57.986'
Steel -Flush Mount Cover
Locking Well Cap
Top Of Grout -0.5 feet
Bentonite Seal 6.0 feet
Borehole Diameter Approx 8"
Top of Sandpack 9.0 feet
Top of Well Screen 13 feet
Depth of Borehole 23'
Bottom of Screen 23 feet
Notes:
Static Water Level Measured From the Top of Casing (TOC)
C]
Monitoring Well Construction Record
Type II
Environmental Hydrogeological Consultants
207 West Fourth Avenue
Red Springs, North Carolina 28377
Ph. (910) 843- 456
Fax(910)843-5376
Atlas Distributing
Well Number
MW-4
Date of Installation 1214/02
Job Location
Fayetteville, North Carolina
Well Material 2" I.D. Sch 40
Top of Casing
97.45 Feet
Lock Number Twist Lock
Ground Surface
97.65 Feet
Sandpack Material #2 Well Pack
Geologist
D. Brown
Static Water Level 6.12'
Lock Number
Twist Lock
Date Measured 12/16/02
Sandpack Material
#2 Well Pack
Latitude N35 3.554'
Drilling Method
Hollow Stem Auger
Longitude W78 57.986'
Steel -Flush Mount Cover
Locking Well Cap
Top Of Grout -0.5 feet
Bentonite Seal 1.0 feet
Borehole Diameter Approx 8"
Top of Sandpack 3.0 feet
Top of Well Screen 5.0 feet
Depth of Borehole 17.0'
Bottom of Screen 15.0 feet
Notes:
Static Water Level Measured From the Top of Casing (TOC)
I•
16
0
Monitoring Well Construction Record
Type III
Environmental Hydrogeological Consultants
207 West Fourth Avenue
Red Springs, North Carolina 28377
Ph. (910)843-4456
Fax(910)843-5376
Atlas Distributing
Job Location
Fayetteville, North Carolina
Well Material Sch 40
Top of Casing
99.11 Feet
Screen Size 0.0101,
Ground Surface
99.22 Feet
Sandpack Material #2 Well Pack
Geologist
D. Brown
Static Water Level 24.42'
Lock Number
Master 0536
Date Measured 10/02/02
Sandpack Material
1#2 Well Pack
Latitude N35 5.554'
Drilling Method
lRotary Wash
Longitude W79 57.986'
Steel -Flush Mount Cover
Outer Casing (6")
Outer Borehole Diameter =12"
Borehole Diameter Approx 6"
Bottom of Outer Casing 30.0'
IDepth of Borehole 40'
Water Level Measured From the Top of Casing (TOC)
Locking Well Cap
Top Of Grout —0.5 feet
Inner Casing
ed Outer Casing
Bentonite Seal 26 feet
of SandDack 32 feet
of Screen 38feet
•
APPENDIX D
•
LABORATORY REPORTS
LJ
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
Ah1ALYT I CAL F2EPOF -F
ENVIRONMENTAL HYDROGEOLOGICAL 5309
CONSULTANTS
P.O. BOX 902
RED SPRINGS, NC 28377
Sample: NiW # 1 C
T�
ATLAS DISTRIBUTING
Sampler: P S I CHAEL LAi M
Date Collected: 7/11/94
Time Collected:
Sample type: Water
Site I.D.:
Analyte Result Units POL
-------------------------------- ------ ---
0
Benzene
Toluene
Ethylbenzene
Xylenes, total
Methyl-t-butylether
** Surrogate Recoveries
Surrogate
-------------
BTEX/GRO Surrogate
0
Lab Number-: 94-AO34300
State Certification: 387
Date Received: 7/13/94
Time Received: 9:00
Preservative: HC1
Date Time Analyst Method
-------- --------------- ------
3.0
ug/l
1.0
7/14/94
13:44
G.Norton
602
90.0
ug/l
45.0
7/14/94
13:44
G.Norton
602
590.
ug/1
45.0
7/14/94
13:44
G.Norton
602
4920
ug/l
45.0
7/14/94
13:44
G.Norton
602
< 10.0
ug/l
10.0
7/14/94
13:44
G.Norton
602
% Recovery Target Range
105. 70 - 130
Labor; Cory Supervisor
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
ENVIRONMENTAL HYDROGEOLOGICAL 5309
CONSULTANTS
P.O. BOX 902
FED SPRINGS, NC 28377
Sample: MW #2 rP.eXMtU<ri)
ATLAS D STRIBUTING
Sampler: t � I CHAEL LAMM
Date Collected: 7/11/94
Time Collected:
Sample type: Water
Site I.U.:
Analyte
i----
Benzene
Toluene
Ethylbenzene
Xylenes, total
methyl-t-butyl ether
ANAL.YT I CAL FtEF="OFtT
Lab Number: 94-AO34301
State Certification: 387
Date Received: 7/13/94
Time Received: 9:00
Preservative: HC1
Result Units FQL Date Time Analyst Method
-------------- ------ ------------- --------------- ------
* Surrogate Recoveries **
Surrogate
-------------
BTEX/GRO Surrogate
0
4490
ug/l
90.0
7/14/94
13:44
G.Norton
602
18900
ug/l
90.0
7/14/94
13:44
G.Norton
602
2120
ug/l
90.0
7/14/94
13:44
G.Norton
602
12700
ug/l
90.0
7/14/94
13:44
G.Norton
602
900.
ug/1
900.
7/14/94
13:44
G.Norton
602
% Recovery Target Range
94. 70 - 130
Labor—tol-y Supervisor
SPECIALIZED ASSAYS
ENVIRONMENTAL
REFERRING CLIENT
300 12th Ave., South
Nashville, TN 37203
Entsonmental
Hydrogeological L,5 0�
615-726-0177
FAX 615/726-3404 -
ju
Thomas Ammons
207 W. 4th Avenue,
Red Springs, NC 28377
Ph: 910-843-4456 Fax: 910-843-5376
ILLING CONTROL NUMBER (FOR LAB USE ONLY) (�
l�
PROJECT #
P.O. #
AMPLERS (Signature -Please Print)
PROJECT NAME
FOR LAB USE ONLY
n
ACC#
SAMPLE DESCRIPTION
DATE
TIME
U
U
ANALYSIS REQUESTED
As�sS+•
Z
T
����9�
T3 F, X ryi
Ai 1 As
3A
it- Z
p1Ti-.
p�
I )
TA A
y r, U
M vi 0 1
A+ 1,4 5 P� ; 47 .
33b1
Mw Z.
'ein e _ azure)
Time e
eceived by: (Si nature)
Received for Laboratory by
D to / Time
relinquished by: (Signature)
Date i Time
Received by: Signature)
gemarks
Fax results to 910-843-5376
Mail COC/results to client
QUOTE # 40894JBO
relinquished by: (Signature)
Date /Time
Received by: (Signature)
:elinf d by: (Signature)
Date ! Time
Received by: (Signature)
For further assistance in completing the chain of custody form please refer to the instructions found on the nnnosite side
= 3= "E"
Q
�
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
ENVIRONMENTAL HYDROGEOLOG I CAL 5309
CONSULTANTS
P.O. BOX 902
RED SPRINGS, DC 28377 V
Sample: ATLAS DIST..-%eAWACCC�AfeZ
ATLAS DISTRIBUTING
Sampler: THOMAS AMMONS
Date Collected: 7/19/94
Time Collected:
Sample type: Water
Site I.D.:
AIVAI_YT I CAL FtEF}CFt-r
Lab Number: 94-AO36006
State Certification: 387
Date Received: 7/21/94
Time Received: 10:00
Preservative:
Analyse
Result
Units
POL
Date
Time
Analyst
Method
---------------------
•
-----------
--
-----
--------
-----
----------
--------
enzene
23.0
ug/l
1.0
7/25/94
8:19
S.
Wani
602
Toluene
11.0
ug/l
1.0
7/25/94
8:18
S.
Wani
602
Ethylbenzene
71.0
ug/l
1.0
7/25/94
8:18
S.
Wani
602
Xylenes, total
110.
ug/l
1.0
7/25/94
8:18
S.
Wani
602
Methyl-t-butylether
:: 10.0
Ug/l
10.0
7/25/94
8:18
S.
'Wani
602
** Surrogate Recoveries
Surrogate
-------------
ETEX/6RO Surrogate
Recovery Target Range
85 . 70 - 13i y
Laboratory upervisor
COPY 1
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 /26x.m" s""m
Nashville, Tennessee 37203
ENVIRONMENTAL HYDROGEOLOGICAL 5309
CONSULTANTS
P.O. BOX 902
RED SPRINGS, NC 28377
Sample: ATLAS DIST.
ATLAS DISTRIBUTING
Sampler: THOMAS AMMONS
Date Collected: 7/19/94
Time Collected:
Sample type: Water
Site I.D.:
Analyte Result
~~~Benzene
Toluene
Ethylbenzene
Xylenes, total
Methyl-t-butylether
** Surrogate Recoveries **
Surrogate
_____________
BTEX/GRO Surrogate
0
Lab Number: 94-A036005
State Certification: 387
Date Received: 7/21/94
Time Received: 10:00
Preservative:
Units PQL Date Time Analyst Method
------ ----- -------- ----- ---------- --------
2380
ug/l
45.0
7/25/94
8:18
S.
Wani
602
10700
ug/l
45.0
7/25/94
8:18
S.
Wani
602
1210
ug/l
45.0
7/25/94
8:18
S.
Wani
602
7380
ug/l
45.0
7/25/94
8:18
S.
Wani
602
459.
ug/l
450.
7/25/94
8:18
S.
Wani
602
% Recovery Target Range
---------- ------------
87. 70 - 130
SPECIALIZED ASSAYS
ENVIRONMENTAL
REFERRING CLIENT
300 12th Ave.. South
Nashville, TN 37203
rr;. T
r..r. � c,nm�nt,r� 1. ,rwtir.c.q4�l.p�, i.t;.�:l.
615-726-0177
t �: A mmc) n c
FAX 615/726-3404
S vri ngs , NC' 18377
n: �i 1.V.i -84:3 - 4 4 5 6 4 1-1 x: 9 1.0 - ?43 -1) 376
3ILLING CONTROL NUMBER (FOR LAB USE ONLA� I
PROJECT #
P.O. #
SAMPLERS (Signature -Please Print)
PROJECT NAME 1�
'rl b
�
A 3 )57i
{l
FOR LAB USE ONLY
2
<
ACC#
SAMPLE DESCRIPTION
DATE
TIME
O
V
ANALYSIS REQUESTED
0 }) A s D; st.
hTT� A 1 �i
11
b-5 GA SO l i ---e,
Lcw
A+IA.5
telinquishe r �:�(Sicnat
Da ime
Receiv d by: (Si_ ture)
RfcejviX for Laborat bv:
Date / Time
telinquished by: (Signature)
Date / Time
Received by: (Signature)
Rem
M:Z tI_ I i17 j.Pr 1•.
telinquished by: (Signature)
Date / Time
Received by: (Signature)
`"' "' ' 4 �{
'elinquished by: (Signature)
Date / Time
Received by: (Signature)
For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side
3 �; r t /w,11
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
ENVIRONMENTAL HYDROGEOLOG I CAL 5309
CONSULTANTS
P.O. BOX 902
RED SPRINGS, NC 22e377
Sample: ATLAS -jSA_ 0WV wWVi --
ATLAS DISTRIBUTI`dG
Sampler: M I CHAEL LAM;
Date Collected: 7/21/94
Time Collected:
Sample type: Water
Site I.D..
Analyse
- ------ --------------
Benzene
Toluene
Ethylbenzene
Xylenes, total
Methyl-t-butylether
* Surrogate Recoveries*
Surrogate
-------------
BTEX ./GRO Surrogate
AM4=6L_`YT I GAL FxL=POFZT
Lad Number: 94-AO36436
State Certification: 387
Date Received: 7/23/94
Time Received: 10:00
Preservative: HC1
Result
Units
POL
Date
Time
Analyst
Method
6.0
ug/l
1.0
7/25/94
16:17
G.Norton
602
27.0
ug/l
1.0
7/25/94
16:17
G.Norton
602
4.0
ug/l
1.0
7/25/94
16:17
G.Norton
602
3.0
ug/l
1.0
7/25/94
16:17
G.Norton
602
<:: 10.0
ug/l
10.0
7/25/94
16:17
G.Norton
602
** UST Spike/Duplicate Results **
% Recovery
Target Range
------------
70 - 130
Precision
Compound
--------------------
%.Recovery
---------
Target Range
----------------
RPD
---------
Target Range
----------------
Benzene
91.
70 - 130
5.3
0 - 20.0
410 luene
90.
70 - 130
6.5
G - 20.0
�.yl benzene
91.
70 - 130
5.3
0 - 20.0
Xylene
93.
70 - 130
7.3
0 - 20.0
COPY 1
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
AIVAILYT I CAI_ REF*C3FtT
ENVIRONMENTAL HYDROGEOLOG I CAL 5309
COI SULTANTS
P.O. BOX 902
REED SPRINGS, NC 28377
Sample: ATLAS p.('Wa,�` %(�Z
ATLAS DISTRIBUTING
Sa.mp 1 er- : M I CHAEL LAI' M
Date Collected: 7/21/94
Time Collected:
Sample type: Water
Site I.D.,
* Polyaromatic Hydrocarbon Control Results ***
Lab Numb ei- : 94-AO36436
State Cer-tification: 387
Date Received: 7/23/94
Time Received: 10:00
Preservative: HC1
- p0Lind% Recovery Target Range
----
---------------
-----------------------------
•
i
Labor-ator Supel-viSor-
COPY 1
ENVIRONMENTAL
300 12th A%c.. South
Nash%ille. TN 37203
615-726-0177
FAX 615-726-3404
REFERRING CLIENT
Aj 7.
)ILLING CONTROL NUMBER (FOR LABVSLQNLY)
PROJECT #
P.O.
;AMPLERS (Signature -Please Print)
WICI\Ael
t.AMWA
PROJECT NAME
D',5+r-s't>v+.v-%j
FOR LAB USE ONLY
ACC#
SAMPLE DESCRIPTION
DATE
TIME
P=
<
ANALYSIS REQUESTED
V3
tel nquis (Signature)
D al ck! e
N�,
Received by: (jignature)
ceived or LaboratoryDate
Time
telinquished by: (Signature)
Date Time
i'e0cc'-t7v_ed by: (Signature)
R
telinquished by: (Signature)
Date Time
Received by: (Signature)
telinquished by: (Signature)
Date Time
Received by: (Signature)
w
For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12thx.enu South
Nashville, Tennessee 37203
ENVIRONMENTAL HYDROGEOLOGICAL 5309
CONSULTANTS
P.O. BOX 902
RED SPRINGS, NC 28377
� J#
Sample: A �
ATLAS DISTRIBUTING
Sampler: MICHAEL LAMM
Date Collected: 7/28/94
Time Collected:
Sample type: Water
Site I.D.:
Analyte
_______________________
0-
uenzene
Toluene
EthyIbenzene
Xylenes, total
Nsthyl-t-butylether
** Surrogate Recoveries **
| Surrogate
� --_--___--__-
BTEX/GR0 Surrogate
0
Lab Number: 94-A037693
State Certification: 387
Date Received: 7/30/94
Time Received: 11:00
Preservative: HCl
Result
___________
Units
______
PQL
_____
Date
________
Time
_____
Analyst
__________
Method
______
< 1.O
ug/l
1.0
8/
1/94
8:17
S.
Wani
602
< 1.0
ug/l
1.0
8/
1 /9 4
8:17
S.
Wani
602
< 1.0
og/l
1.0
8/
1/94
8:17
S.
Wani
602
< 1.0
ug/l
1.0
8/
1/94
8:17
S.
Wani
602
< 10.0
ug/l
10.0
8/
1/94
8:17
S.
Wani
602
% Recovery Target Range
---------- ------------
95. 70 - 130
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
ENVIRONMENTAL HYDROGEOLOGICAL 5309
CONSULTANTS
P.O. BOX 902
RED SPRINGS, NC 28377
Sample: A-m;,
ATLAS DISTRIBUTING
Sampler: MICHAEL LAMM
Date Collected: 7/28/94
Time Collected:
Sample tyoe: Water
Site I.D.:
Lab Number: 94-A037692
State Certification: 387
Date Received: 7/30/94
Time Received: 11:00
Preservative: HCl
Analyte
Result
Units
PQL
Date
Time
Analyst
Method
----------------------
-----------
------
-----
--------
-----
----------
--------
Benzene
743.
ug/l
10.0
8/
1/94
8:17
S.
Wani
602
Toluene
3650
ug/l
10.0
8/
1/94
8:17
S.
Wani
602
Ethylbenzene
415.
ug/l
10.0
8/
1/94
8:17
S.
Wani
602
Xylenes, total
284O
ug/l
10.0
8/
1/94
8:17
S.
Wani
602
Methyl -t-butylether
1490
ug/l
1O0.
8/
1/94
8:17
S.
Wani
602
** Surrogate Recoveries **
\ Surrogate % Recovery Target Range
� ------------- ---------- ---__----__-
0
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Ave., South
MmNashville, TN 37203
wo 615-726-0177
FAX 615/726-3404
"Jr
Specialized Assays: (800) 765-0980
REFERRING CLIENT
count: 5309
ironmental Hydrogeological
homas Ammons
207 W. 4th Avenue
Red Springs, NC 28377
.0-84 -4456 F x: 910-843-5376
ILLING CONTROL NUMBER (FOR LAB USE ONLY)
PROJECT #
P.O. #
aINPLERS (Signaturr.Please Print)
Mia\'Wj i�Rm
PROJECT NAME
FOR LAB USE ONLY
ACC#
SAMPLE DESCRIPTION
DATE
TIME
i
U
<
U
8
o
ANALYSIS REQUESTED
�� `�
��
1�►�X 1 YnT13E
A
uI 1
I
re)
D ime
Re ived : (S natur) r�')�
r Vi/
�
Received f Laboratory by "p I 'W
Date / Time
"�9y
xlinquished by: (Signature)
Date / Time
eceived by: (Signature)
Rem rks
Quote # 40894JBO
elinquished by: (Signature)
Date / Time
Received by: (Signature)
elfin wished by: (Signature)
Date / Time
Received by: (Signature)
For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side
•
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
ENVIRONMENTAL H`/DROGEOLOG I GAL 5309
CONSULTANTS
P.O. LOX 902
RED SPRINGS„ NC 2e377
Sample: MW-2 BEFORE
ATLAS DISTRIBUTING
Sampler: M I CHAEL LAMt
Date Collected: 8/11/94
Time Collected:
Sample type: Water
Site I.D..
AIVALYT I CAL f;tEF=-MF2T
Lab Number: 94-AO40197
State Certification: 387
Date Received: 8/12/94
Time Received: 9:20
Preservative:
Analyte
Result
Units
POL
Date
Time
Analyst
Method
•------------------------
-----------
------
-----
--------
-----
----------
--------
Benzene
2.0
ug/1
1.0
8/15/94
13:50
G.Norton
602
Toluene
7.0
ug/l
1.0
6/15/94
13:50
G.Norton
602
Ethylbenzene
4.0
ug/l
1.0
8/15/94
13:50
G.Norton
602
Xylenes, total
55.0
ug/1
1.0
8/15/94
13:50
G.Norton
602
Methyl-t-butylether
< 10.0
ug/l
10.0
8/15/94
13:50
G.Norton
602
** Surrogate Recoveries **
Surrogate % Recovery Target Range
-----------------------------------
BTEX./GRO Surrogate 98. 70 - 130
Laboratory upervisor-
COPY 1
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 12th Avenue South
Nashville, Tennessee 37203
ENVIRONMENTAL HYDROGEOLOG I CAL 5309
CO `NSULTANTS
P.O. LOX 9o2
RED SPRINGS, NC 28377
Sample: MW-2 AFTER
ATLAS DISTRIBUTING
Samp 1 ei- : M I CHAEL LAB M
Date Collected: 8/11/94
Time Collected:
Sample type: Water
Site I.D..
Analyte
---------------------
Benzene
Toluene
Ethyibenzene
Xylenes, total
Methyl-t-butylether
Surrogate Recoveries
Surrogate
-------------
STEX/GRO Surrogate
•
Ah1ALYT I CAL_ F2EF'OF -r
Lad Numbei- : 94-AO40198
State Certification: 387
Date Received: 8/12/94
Time Received: 9:20
Preservative:
Result
-----------
Units
------
POL
-----
Date
--------
Time
-----
Analyst
----------
Method
--------
5.0
uq/1
1.0
8/15/94
13:50
G.Norton
602
41.0
ua/l
1.0
8/15/94
13:50
G.Norton
602
6.0
ua/1
1.0
8/15/94
13:50
G.Norton
602
42.0
uQ/l
1.0
8/15/94
13:50
G.Norton
602
<:: 10.0
ug/l
10.0
8/15/94
13:50
G.Norton
602
% Recovery Target Range
105 . 70 - 13� y
Laboratory Eytpervisor
COPY 1
SPECIALIZED ASSAYS
ENVIRONMENTAL
300 l2th Ave., South
Nashville, TN 37203
615-726-0177
FAX 615/726-3404 -
REFERRING CLIENT
Ovironmental Hydrogeological
Thomas Ammons
207 W. 4th Avenue,
Red Springs, NC 28377
910-843-4456 Fax: 910-843-5376
TILLING CONTROL NUMBER (FOR L4B USE ONLY)
33S
PROJECT #
P.O. #
+AMPLERS (Signature -Please Print)
icanAe� �4 Imn�
PROJECT NAME
,A-}-IAs �i `t,bv�-rn
FOR LAB USE ONLY
ACC#
SAMPLE DESCRIPTION
DATE
TIME
O
¢
v
g
ANALYSIS REQUESTED
y c�ti
+IA5
rnw W z B4f'd«
� �
4� ��,��
1
z
E i-g 9
g-�— x rn
AflAS
W Z A4v
�n P
•
eli uish ture)
D Time
Reced�)-A%iurcy((—�� +fa
(! : 3
Re ved or Laboratory b .
Date /Time
elinquished by: (Signature)
Date / Time
Received by: (Signature)
Re r
Fax results to 910-843-5376
Mail COC /results to client
QUOTE # 40894JB0
elinquished by: (Signature)
Date ! Time
Received by: (Signature)
e9hed by: (Signature)
Date / Time
Received by: (Signature)
For further assistance in completing the chain of custody form please refer to the instructions found on the opposite side
(Jc4 yo19
ENVIRONMENTAL
SCIENCE CORP.
•
•
0
REPORT OF ANALYSIS
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing 1
Sample ID A9W—i" r11.. - ( ��' *S•a� �en�.,
Collected By David Brown
Collection Date 12/16/02 13:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-02
Site ID :
Project #
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
Lead
14.
5.0
ug/l
6010B
12/20/02
1
volatile Petroleum Hydrocarbons
BDL
100
ug/l
MADEPV
12/21/02
1
C5-C8 Aliphatics
BDL
100
ug/l
MADEPV
12/21/02
1
C9-C12 Aliphatics
BDL
100
ug/l
MADEPV
12/21/02
1
C9-C10 Aromatics
BDL
100
ug/l
MADEPV
12/21/02
1
Surrogate Recovery
2,5-Dibromotoluene(FID)
94.0
% Rec.
MADEPV
12/21/02
1
2,5-Dibromotoluene(PID)
93.0
% Rec.
MADEPV
12/21/02
1
Volatile Organics
Acetone
BDL
50.
ug/l
6210D
12/23/02
1
Acrolein
BDL
50.
ug/1
6210D
12/23/02
1
Acrylonitrile
BDL
50.
ug/l
6210D
12/23/02
1
Benzene
BDL
1.0
ug/l
6210D
12/23/02
1
Bromobenzene
BDL
1.0
ug/l
6210D
12/23/02
1
Bromodichloromethane
BDL
1.0
ug/l
6210D
12/23/02
1
Bromoform
BDL
1.0
ug/l
6210D
12/23/02
1
Bromomethane
BDL
1.0
ug/l
6210D
12/23/02
1
n-Butylbenzene
BDL
1.0
ug/l
6210D
12/23/02
1
sec-Butylbenzene
BDL
1.0
ug/l
6210D
12/23/02
1
tert-Butylbenzene
BDL
1.0
ug/l
6210D
12/23/02
1
Carbon tetrachloride
BDL
1.0
ug/l
6210D
12/23/02
1
Chlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
1
Chlorodibromomethane
BDL
1.0
ug/l
6210D
12/23/02
1
Chloroethane
BDL
1.0
ug/l
6210D
12/23/02
1
Chloroform
BDL
5.0
ug/l
6210D
12/23/02
1
Chloromethane
BDL
1.0
ug/l
6210D
12/23/02
1
2-Chlorotoluene
BDL
1.0
ug/l
6210D
12/23/02
1
4-Chlorotoluene
BDL
1.0
ug/l
6210D
12/23/02
1
1,2-Dibromo-3-Chloropropane
BDL
2.0
ug/l
6210D
12/23/02
1
1,2-Dibromoethane
BDL
1.0
ug/l
6210D
12/23/02
1
Dibromomethane
BDL
1.0
ug/l
6210D
12/23/02
1
1,2-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
1
1,3-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
1
1,4-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
1
Dichlorodifluoromethane
BDL
1.0
ug/l
6210D
12/23/02
1
1,1-Dichloroethane
BDL
1.0
ug/l
6210D
12/23/02
1
1,2-Dichloroethane
BDL
1.0
ug/l
6210D
12/23/02
1
1,1-Dichloroethene
BDL
1.0
ug/l
6210D
12/23/02
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 5 of 26
Lebanon R
0
Mtt..
J 3uliet, TN 7122
ENVIRONMENTAL
(615)
758-5858
1-800-767-5859
SCIENCE CORP.
Fax
(615) 758-5859
Tax
I.D. 62-0814289
Est.
1970
REPORT
OF ANALYSIS
Mr. David Brown
December 26,2002
EHC, Inc.
PO Box 902
Red Springs, NC 28377
ESC
Sample #
L99295-02
Date Received December 19, 2002
Description Atlas Distributing
Site
ID
Sample ID 14W-2
Project
#
Collected By David Brown
Collection Date 12/16/02 13:00
Parameter
Result
Det. Limit
Units
Method
Date
cis-1,2-Dichloroethene
BDL
1.0
ug/1
6210D
12/23/02
trans-1,2-Dichloroethene
BDL
1.0
ug/1
6210D
12/23/02
1,2-Dichloropropane
BDL
1.0
ug/1
6210D
12/23/02
1,1-Dichloropropene
BDL
1.0
ug/1
6210D
12/23/02
1,3-Dichloropropane
BDL
1.0
ug/1
6210D
12/23/02
2,2-Dichloropropane
BDL
1.0
ug/1
6210D
12/23/02
Di -isopropyl ether
BDL
1.0
ug/l
6210D
12/23/02
Ethylbenzene
BDL
1.0
ug/l
6210D
12/23/02
Hexachlorobutadiene
BDL
1.0
ug/l
6210D
12/23/02
Isopropylbenzene
BDL
1.0
ug/l
6210D
12/23/02
p-Isopropyltoluene
BDL
1.0
ug/l
6210D
12/23/02
2-Butanone (MEK)
BDL
50.
ug/l
6210D
12/23/02
Methylene Chloride
BDL
5.0
ug/l
6210D
12/23/02
4-Methyl-2-pentanone (MIBK)
BDL
50.
ug/l
6210D
12/23/02
Methyl tert-butyl ether
BDL
1.0
ug/l
6210D
12/23/02
•
Naphthalene
BDL
5.0
ug/l
6210D
12/23/02
n-Propylbenzene
BDL
1.0
ug/l
6210D
12/23/02
Styrene
BDL
1.0
ug/l
6210D
12/23/02
1,1,1,2-Tetrachloroethane
BDL
1.0
ug/1
6210D
12/23/02
1,1,2,2-Tetrachloroethane
BDL
1.0
ug/1
6210D
12/23/02
Tetrachloroethene
BDL
1.0
ug/l
6210D
12/23/02
Toluene
BDL
5.0
ug/1
6210D
12/23/02
1,2,3-Trichlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
1,2,4-Trichlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
1,1,1-Trichloroethane
BDL
1.0
ug/l
6210D
12/23/02
1,1,2-Trichloroethane
BDL
1.0
ug/l
6210D
12/23/02
Trichloroethene
BDL
1.0
ug/l
6210D
12/23/02
Trichlorofluoromethane
BDL
1.0
ug/l
6210D
12/23/02
1,2,3-Trichloropropane
BDL
1.0
ug/l
6210D
12/23/02
1,2,4-Trimethylbenzene
BDL
1.0
ug/l
6210D
12/23/02
1,3,5-Trimethylbenzene
BDL
1.0
ug/1
6210D
12/23/02
Vinyl chloride
BDL
1.0
ug/l
6210D
12/23/02
o-Xylene
BDL
1.0
ug/l
6210D
12/23/02
m&p-Xylenes
BDL
2.0
ug/l
6210D
12/23/02
Surrogate Recovery
Toluene-d8
98.
% Rec.
6210D
12/23/02
Dibromofluoromethane
100
96 Rec.
6210D
12/23/02
4-Bromofluorobenzene
98.
% Rec.
6210D
12/23/02
0
Dil.
1
1
1
Extractable Petroleum Hydrocarb BDL 100 ug/l MADEPE 12/26/02 1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 6 of 26
ENVIRONMENTAL
SCIENCE CORP.
•
E
REPORT OF ANALYSIS
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID *MW-2 V^ w
Collected By David Brown
Collection Date 12/16/02 13:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-02
Site ID :
Project #
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
C9-C18 Aliphatics
BDL
100
ug/l
MADEPE
12/26/02
1
C19-C36 Aliphatics
BDL
100
ug/l
MADEPE
12/26/02
1
Cll-C22 Aromatics
BDL
100
ug/l
MADEPE
12/26/02
1
Surrogate Recovery
o-Terphenyl
74.0
%- Rec.
MADEPE
12/26/02
1
1-Chloro-octadecane
74.0
% Rec.
MADEPE
12/26/02
1
2-Fluorobiphenyl
79.0
& Rec.
MADEPE
12/26/02
1
2-Bromonaphthanene
79.0
%- Rec.
MADEPE
12/26/02
1
625 Base/Neutrals w/ TIC
Acenaphthene
BDL
10.
ug/l
625
12/21/02
1
Acenaphthylene
BDL
10.
ug/l
625
12/21/02
1
Anthracene
BDL
10.
ug/l
625
12/21/02
1
Benzidine
BDL
50.
ug/l
625
12/21/02
1
Benzo(a)anthracene
BDL
10.
ug/l
625
12/21/02
1
Benzo(b)fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Benzo(k)fluoranthene
BDL
10.
ug/1
625
12/21/02
1
Benzo(g,h,i)perylene
BDL
10.
ug/1
625
12/21/02
1
Benzo(a)pyrene
BDL
10.
ug/1
625
12/21/02
1
Bis(2-chlorethoxy)methane
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chloroethyl)ether
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chloroisopropyl)ether
BDL
10.
ug/l
625
12/21/02
1
4-Bromophenyl-phenylether
BDL
10.
ug/l
625
12/21/02
1
2-Chloronaphthalene
BDL
10.
ug/1
625
12/21/02
1
4-Chlorophenyl-phenylether
BDL
10.
ug/1
625
12/21/02
1
Chrysene
BDL
10.
ug/l
625
12/21/02
1
Dibenz(a,h)anthracene
BDL
10.
ug/l
625
12/21/02
1
3,3-Dichlorobenzidine
BDL
10.
ug/l
625
12/21/02
1
2,4-Dinitrotoluene
BDL
10.
ug/1
625
12/21/02
1
2,6-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
1
Fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Fluorene
BDL
10.
ug/1
625
12/21/02
1
Hexachlorobenzene
BDL
10.
ug/l
625
12/21/02
1
Hexachloro-1,3-butadiene
BDL
10.
ug/l
625
12/21/02
1
Hexachlorocyclopentadiene
BDL
10.
ug/l
625
12/21/02
1
Hexachloroethane
BDL
10.
ug/l
625
12/21/02
1
Indeno(1,2,3-cd)pyrene
BDL
10.
ug/l
625
12/21/02
1
Isophorone
BDL
10.
ug/1
625
12/21/02
1
Naphthalene
BDL
10.
ug/l
625
12/21/02
1
Nitrobenzene
BDL
10.
ug/l
625
12/21/02
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 7 of 26
ENVIRONMENTAL
. SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received
Description
Sample ID
Collected By
Collection Date
Parameter
December 19, 2002
Atlas Distributing
494-2 h1 w -'
David Brown
12/16/02 13:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # : L99295-02
Site ID :
Project #
Result Det. Limit Units Method Date Dil.
n-Nitrosodimethylamine
BDL
10.
ug/l
625
12/21/02
n-Nitrosodiphenylamine
BDL
10.
ug/l
625
12/21/02
n-Nitrosodi-n-propylamine
BDL
10.
ug/l
625
12/21/02
Phenanthrene
BDL
10.
ug/l
625
12/21/02
Benzylbutyl phthalate
BDL
10.
ug/l
625
12/21/02
Bis(2-ethylhexyl)phthalate
BDL
10.
ug/l
625
12/21/02
Di-n-butyl phthalate
BDL
10.
ug/l
625
12/21/02
Diethyl phthalate
BDL
10.
ug/l
625
12/21/02
Dimethyl phthalate
BDL
10.
ug/l
625
12/21/02
Di-n-octyl phthalate
BDL
10.
ug/l
625
12/21/02
Pyrene
BDL
10.
ug/1
625
12/21/02
1,2,4-Trichlorobenzene
BDL
10.
ug/l
625
12/21/02
Acid Extractables
4-Chloro-3-methylphenol
BDL
10.
ug/l
625
12/21/02
2-Chlorophenol
BDL
10.
ug/l
625
12/21/02
2,4-Dichlorophenol
•
BDL
10.
ug/l
625
12/21/02
2,4-Dimethylphenol
BDL
10.
ug/l
625
12/21/02
4,6-Dinitro-2-methylphenol
BDL
10.
ug/1
625
12/21/02
2,4-Dinitrophenol
BDL
10.
ug/l
625
12/21/02
2-Nitrophenol
BDL
10.
ug/l
625
12/21/02
4-Nitrophenol
BDL
10.
ug/l
625
12/21/02
Pentachlorophenol
BDL
10.
ug/l
625
12/21/02
Phenol
BDL
10.
ug/l
625
12/21/02
2,4,6-Trichlorophenol
BDL
10.
ug/l
625
12/21/02
Surrogate Recovery
Nitrobenzene-d5
62.
$ Rec.
625
12/21/02
2-Fluorobiphenyl
72.
96 Rec.
625
12/21/02
p-Terphenyl-dl4
94.
% Rec.
625
12/21/02
Phenol-d5
24.
% Rec.
625
12/21/02
2-Fluorophenol
31.
% Rec.
625
12/21/02
2,4,6-Tribromophenol
72.
% Rec.
625
12/21/02
( dWjJ1zCk0
Terrie Fudge,t ESC T
presentative
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
The reported analytical results relate only to the sample submitted.
• This report shall not be reproduced, except in full, without the written approval from ESC.
Page 8 of 26
ENVIRONMENTAL
• SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received
Description
Sample ID
Collected By
Collection Date
Parameter
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # : L99295-01
December 19, 2002
Atlas Distributing 1
David Brown
12/16/02 12:00
Result Det. Limit Units
REPORT OF ANALYSIS
Site ID :
Project # :
Method Date
Lead
13.
5.0
ug/1
6010B
12/20/02
Volatile Petroleum Hydrocarbons
320
100
ug/1
MADEPV
12/19/02
C5-C8 Aliphatics
200
100
ug/l
MADEPV
12/19/02
C9-C12 Aliphatics
250
100
ug/l
MADEPV
12/19/02
C9-C10 Aromatics
130
100
ug/l
MADEPV
12/19/02
Surrogate Recovery
2,5-Dibromotoluene(FID)
118.
% Rec.
MADEPV
12/19/02
2,5-Dibromotoluene(PID)
114.
% Rec.
MADEPV
12/19/02
Volatile Organics
Acetone
BDL
50.
ug/l
6210D
12/23/02
Acrolein
BDL
50.
ug/l
6210D
12/23/02
Acrylonitrile
BDL
50.
ug/l
6210D
12/23/02
Benzene
1.4
1.0
ug/l
6210D
12/23/02
Bromobenzene
•
BDL
1.0
ug/l
6210D
12/23/02
Bromodichloromethane
BDL
1.0
ug/l
6210D
12/23/02
Bromoform
BDL
1.0
ug/l
6210D
12/23/02
Bromomethane
BDL
1.0
ug/l
6210D
12/23/02
n-Butylbenzene
BDL
1.0
ug/l
6210D
12/23/02
sec-Butylbenzene
BDL
1.0
ug/l
6210D
12/23/02
tert-Butylbenzene
BDL
1.0
ug/l
6210D
12/23/02
Carbon tetrachloride
BDL
1.0
ug/l
6210D
12/23/02
Chlorobenzene
BDL
1.0
ug/1
6210D
12/23/02
Chlorodibromomethane
BDL
1.0
ug/l
6210D
12/23/02
Chloroethane
BDL
1.0
ug/l
6210D
12/23/02
Chloroform
BDL
5.0
ug/l
6210D
12/23/02
Chloromethane
BDL
1.0
ug/l
6210D
12/23/02
2-Chlorotoluene
BDL
1.0
ug/l
6210D
12/23/02
4-Chlorotoluene
BDL
1.0
ug/l
6210D
12/23/02
1,2-Dibromo-3-Chloropropane
BDL
2.0
ug/1
6210D
12/23/02
1,2-Dibromoethane
BDL
1.0
ug/1
6210D
12/23/02
Dibromomethane
BDL
1.0
ug/l
6210D
12/23/02
1,2-Dichlorobenzene
BDL
1.0
ug/1
6210D
12/23/02
1,3-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
1,4-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/23/02
Dichlorodifluoromethane
BDL
1.0
ug/l
6210D
12/23/02
1,1-Dichloroethane
BDL
1.0
ug/l
6210D
12/23/02
1,2-Dichloroethane
BDL
1.0
ug/l
6210D
12/23/02
1,1-Dichloroethene
BDL
1.0
ug/1
6210D
12/23/02
Dil.
1
1
1
1
1
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 1 of 26
•
0
ENVIRONMENTAL
SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC
28377
Date Received
December 19, 2002
Description
Atlas Distributing
Sample ID
m -1 V' ••- -
Collected By
David Brown
Collection Date
12/16/02 12:00
Parameter
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
m&p-Xylenes
Surrogate Recovery
Toluene-d8
Dibromofluoromethane
4-Bromofluorobenzene
REPORT OF ANALYSIS
Result
BDL
BDL
BDL
BDL
BDL
BDL
BDL
20.
BDL
BDL
BDL
BDL
BDL
BDL
BDL
5.2
1.6
BDL
BDL
BDL
BDL
17.
BDL
BDL
BDL
BDL
BDL
BDL
BDL
22.
6.4
BDL
8.9
71.
96.
100
98.
Det. Limit
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
50.
5.0
50.
1.0
5.0
1.0
1.0
1.0
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
1.0
2.0
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-01
Site ID :
Project #
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/1
ug/1
ug/1
ug/l
% Rec.
Rec.
96 Rec.
Method
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
6210D
Date
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
12/23/02
Dil.
1
1
1
Extractable Petroleum Hydrocarb BDL 100 ug/l MADEPE 12/26/02 1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 2 of 26
ENVIRONMENTAL
SCIENCE CORP.
REPORT OF ANALYSIS
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID UN-4 IVIL
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-01
Site ID :
Collected By David Brown
Collection Date 12/16/02 12:00
Parameter Result
Det. Limit
Project #
Units Method
Date
Dil.
C9-C18 Aliphatics
BDL
100
ug/l
MADEPE
12/26/02
1
C19-C36 Aliphatics
BDL
100
ug/l
MADEPE
12/26/02
1
Cll-C22 Aromatics
BDL
100
ug/l
MADEPE
12/26/02
1
Surrogate Recovery
o-Terphenyl
88.0
% Rec.
MADEPE
12/26/02
1
1-Chloro-octadecane
74.0
% Rec.
MADEPE
12/26/02
1
2-Fluorobiphenyl
96.0
% Rec.
MADEPE
12/26/02
1
2-Bromonaphthanene
95.0
% Rec.
MADEPE
12/26/02
1
625 Base/Neutrals w/ TIC
Acenaphthene
BDL
10.
ug/l
625
12/21/02
1
Acenaphthylene
BDL
10.
ug/l
625
12/21/02
1
Anthracene
BDL
10.
ug/l
625
12/21/02
1
Benzidine
BDL
50.
ug/1
625
12/21/02
1
Benzo(a)anthracene
BDL
10.
ug/1
625
12/21/02
1
Benzo(b)fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Benzo(k)fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Benzo(g,h,i)perylene
BDL
10.
ug/l
625
12/21/02
1
Benzo(a)pyrene
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chlorethoxy)methane
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chloroethyl)ether
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chloroisopropyl)ether
BDL
10.
ug/l
625
12/21/02
1
4-Bromophenyl-phenylether
BDL
10.
ug/l
625
12/21/02
1
2-Chloronaphthalene
BDL
10.
ug/l
625
12/21/02
1
4-Chlorophenyl-phenylether
BDL
10.
ug/l
625
12/21/02
1
Chrysene
BDL
10.
ug/l
625
12/21/02
1
Dibenz(a,h)anthracene
BDL
10.
ug/l
625
12/21/02
1
3,3-Dichlorobenzidine
BDL
10.
ug/l
625
12/21/02
1
2,4-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
1
2,6-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
1
Fluoranthene
BDL
10.
ug/1
625
12/21/02
1
Fluorene
BDL
10.
ug/l
625
12/21/02
1
Hexachlorobenzene
BDL
10.
ug/l
625
12/21/02
1
Hexachloro-1,3-butadiene
BDL
10.
ug/l
625
12/21/02
1
Hexachlorocyclopentadiene
BDL
10.
ug/l
625
12/21/02
1
Hexachloroethane
BDL
10.
ug/l
625
12/21/02
1
Indeno(1,2,3-cd)pyrene
BDL
10.
ug/l
625
12/21/02
1
Isophorone
BDL
10.
ug/l
625
12/21/02
1
Naphthalene
BDL
10.
ug/l
625
12/21/02
1
Nitrobenzene
BDL
10.
ug/l
625
12/21/02
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation
Limit(EQL)
Laboratory Certification
Numbers:
A2LA - 1461-01, AIHA - 100789,
AL - 40660, CA -
I-2327, CT- PH-0197, FL
- E87487, GA -
923, IN -
C-TN-01
KY - 90010, KYUST - 0016, NC
- ENV375,DW21704,
ND - R-140,
SC - 84004,
TN - 2006, VA
- 00109, WV - 233
Page
3 of 26
0
ENVIRONMENTAL
• SCIENCE CORP.
:7
•
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID MW---1 hn "- -
Collected By David Brown
Collection Date 12/16/02 12:00
Parameter
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
Nitrobenzene-d5
2-Fluorobiphenyl
p-Terphenyl-d14
Phenol-d5
2-Fluorophenol
2,4,6-Tribromophenol
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-01
Site ID :
Project #
Result Det. Limit Units Method Date Dil.
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
69.
% Rec.
625
12/21/02 1
77.
% Rec.
625
12/21/02 1
81.
% Rec.
625
12/21/02 1
31.
% Rec.
625
12/21/02 1
43.
% Rec.
625
12/21/02 1
80.
% Rec.
625
12/21/02 1
Terrie Fudge, ESC /Z44
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Page 4 of 26
ENVIRONMENTAL
• SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
•
•
Date Received December 19, 2002
Description Atlas Distributing
Sample ID MW-2D
Collected By David Brown
Collection Date 12/16/02 14:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # : L99295-03
Site ID :
Project #
Parameter Result Det. Limit Units Method Date Dil.
Lead
18.
5.0
ug/1
6010B
12/20/02
Volatile Petroleum Hydrocarbons
BDL
100
ug/l
MADEPV
12/19/02
C5-C8 Aliphatics
BDL
100
ug/l
MADEPV
12/19/02
C9-C12 Aliphatics
BDL
100
ug/l
MADEPV
12/19/02
C9-C10 Aromatics
BDL
100
ug/l
MADEPV
12/19/02
Surrogate Recovery
2,5-Dibromotoluene(FID)
119.
% Rec.
MADEPV
12/19/02
2,5-Dibromotoluene(PID)
116.
% Rec.
MADEPV
12/19/02
Volatile Organics
Acetone
BDL
50.
ug/l
6210D
12/24/02
Acrolein
BDL
50.
ug/l
6210D
12/24/02
Acrylonitrile
BDL
50.
ug/l
6210D
12/24/02
Benzene
BDL
1.0
ug/l
6210D
12/24/02
Bromobenzene
BDL
1.0
ug/1
6210D
12/24/02
Bromodichloromethane
BDL
1.0
ug/l
6210D
12/24/02
Bromoform
BDL
1.0
ug/l
6210D
12/24/02
Bromomethane
BDL
1.0
ug/l
6210D
12/24/02
n-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
sec-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
tert-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
Carbon tetrachloride
BDL
1.0
ug/l
6210D
12/24/02
Chlorobenzene
BDL
1.0
ug/1
6210D
12/24/02
Chlorodibromomethane
BDL
1.0
ug/1
6210D
12/24/02
Chloroethane
BDL
1.0
ug/l
6210D
12/24/02
Chloroform
12.
5.0
ug/l
6210D
12/24/02
Chloromethane
BDL
1.0
ug/l
6210D
12/24/02
2-Chlorotoluene
BDL
1.0
ug/l
6210D
12/24/02
4-Chlorotoluene
BDL
1.0
ug/l
6210D
12/24/02
1,2-Dibromo-3-Chloropropane
BDL
2.0
ug/l
6210D
12/24/02
1,2-Dibromoethane
BDL
1.0
ug/1
6210D
12/24/02
Dibromomethane
BDL
1.0
ug/1
6210D
12/24/02
1,2-Dichlorobenzene
BDL
1.0
ug/1
6210D
12/24/02
1,3-Dichlorobenzene
BDL
1.0
ug/1
6210D
12/24/02
1,4-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/24/02
Dichlorodifluoromethane
BDL
1.0
ug/l
6210D
12/24/02
1,1-Dichloroethane
BDL
1.0
ug/l
6210D
12/24/02
1,2-Dichloroethane
BDL
1.0
ug/l
6210D
12/24/02
1,1-Dichloroethene
BDL
1.0
ug/l
6210D
12/24/02
1
1
1
1
1
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 9 of 26
ENVIRONMENTAL
• SCIENCE CORP.
•
is
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID MW-2D
Collected By David Brown
Collection Date 12/16/02 14:00
Parameter
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
m&p-Xylenes
Surrogate Recovery
Toluene-d8
Dibromofluoromethane
4-Bromofluorobenzene
Extractable Petroleum Hydrocarb
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-03
Site ID :
Project #
Result Det. Limit Units Method Date Dil.
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
50.
ug/l
6210D
12/24/02
BDL
5.0
ug/l
6210D
12/24/02
BDL
50.
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
5.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/1
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
5.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
2.0
ug/l
6210D
12/24/02
95.
% Rec.
6210D
12/24/02
100
% Rec.
6210D
12/24/02
93.
% Rec.
6210D
12/24/02
BDL
100
ug/l
MADEPE
12/26/02
1
1
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 10 of 26
ENVIRONMENTAL
• SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
E
Date Received December 19, 2002
Description Atlas Distributing
Sample ID MW-2D
Collected By David Brown
Collection Date 12/16/02 14:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-03
Site ID :
Project #
Parameter Result Det. Limit Units Method Date Dil.
C9-C18 Aliphatics
BDL
100
ug/l
MADEPE
12/26/02
C19-C36 Aliphatics
BDL
100
ug/l
MADEPE
12/26/02
Cll-C22 Aromatics
BDL
100
ug/l
MADEPE
12/26/02
Surrogate Recovery
o-Terphenyl
84.0
% Rec.
MADEPE
12/26/02
1-Chloro-octadecane
56.0
% Rec.
MADEPE
12/26/02
2-Fluorobiphenyl
91.0
% Rec.
MADEPE
12/26/02
2-Bromonaphthanene
80.0
% Rec.
MADEPE
12/26/02
625 Base/Neutrals w/ TIC
Acenaphthene
BDL
10.
ug/l
625
12/21/02
Acenaphthylene
BDL
10.
ug/1
625
12/21/02
Anthracene
BDL
10.
ug/l
625
12/21/02
Benzidine
BDL
50.
ug/l
625
12/21/02
Benzo(a)anthracene
BDL
10.
ug/l
625
12/21/02
Benzo(b)fluoranthene
BDL
10.
ug/l
625
12/21/02
Benzo(k)fluoranthene
BDL
10.
ug/l
625
12/21/02
Benzo(g,h,i)perylene
BDL
10.
ug/l
625
12/21/02
Benzo(a)pyrene
BDL
10.
ug/1
625
12/21/02
Bis(2-chlorethoxy)methane
BDL
10.
ug/l
625
12/21/02
Bis(2-chloroethyl)ether
BDL
10.
ug/l
625
12/21/02
Bis(2-chloroisopropyl)ether
BDL
10.
ug/l
625
12/21/02
4-Bromophenyl-phenylether
BDL
10.
ug/l
625
12/21/02
2-Chloronaphthalene
BDL
10.
ug/l
625
12/21/02
4-Chlorophenyl-phenylether
BDL
10.
ug/l
625
12/21/02
Chrysene
BDL
10.
ug/l
625
12/21/02
Dibenz(a,h)anthracene
BDL
10.
ug/l
625
12/21/02
3,3-Dichlorobenzidine
BDL
10.
ug/l
625
12/21/02
2,4-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
2,6-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
Fluoranthene
BDL
10.
ug/l
625
12/21/02
Fluorene
BDL
10.
ug/l
625
12/21/02
Hexachlorobenzene
BDL
10.
ug/l
625
12/21/02
Hexachloro-1,3-butadiene
BDL
10.
ug/l
625
12/21/02
Hexachlorocyclopentadiene
BDL
10.
ug/l
625
12/21/02
Hexachloroethane
BDL
10.
ug/l
625
12/21/02
Indeno(1,2,3-cd)pyrene
BDL
10.
ug/l
625
12/21/02
Isophorone
BDL
10.
ug/l
625
12/21/02
Naphthalene
BDL
10.
ug/l
625
12/21/02
Nitrobenzene
BDL
10.
ug/l
625
12/21/02
1
1
1
1
1
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 11 of 26
Lebanon R
0
Mtt.. J 3uliet, TN 7122
ENVIRONMENTAL
(615) 758-5858
1-800-767-5859
SCIENCE CORP.
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
REPORT
OF ANALYSIS
Mr. David Brown
December 26,2002
EHC, Inc.
PO Box 902
Red Springs, NC 28377
ESC
Sample
# L99295-03
Date Received December 19, 2002
Description Atlas Distributing
Site
ID
Sample ID MW-21)
Project
#
Collected By David Brown
Collection Date 12/16/02 14:00
Parameter
Result
Det. Limit
Units
Method Date
Dil.
n-Nitrosodimethylamine
BDL
10.
ug/1
625
12/21/02
1
n-Nitrosodiphenylamine
BDL
10.
ug/l
625
12/21/02
1
n-Nitrosodi-n-propylamine
BDL
10.
ug/l
625
12/21/02
1
Phenanthrene
BDL
10.
ug/l
625
12/21/02
1
Benzylbutyl phthalate
BDL
10.
ug/1
625
12/21/02
1
Bis(2-ethylhexyl)phthalate
BDL
10.
ug/l
625
12/21/02
1
Di-n-butyl phthalate
BDL
10.
ug/l
625
12/21/02
1
Diethyl phthalate
BDL
10.
ug/1
625
12/21/02
1
Dimethyl phthalate
BDL
10.
ug/l
625
12/21/02
1
Di-n-octyl phthalate
BDL
10.
ug/1
625
12/21/02
1
Pyrene
BDL
10.
ug/l
625
12/21/02
1
1,2,4-Trichlorobenzene
BDL
10.
ug/l
625
12/21/02
1
Acid Extractables
4-Chloro-3-methylphenol
BDL
10.
ug/l
625
12/21/02
1
2-Chlorophenol
•
BDL
10.
ug/l
625
12/21/02
1
2,4-Dichlorophenol
BDL
10.
ug/l
625
12/21/02
1
2,4-Dimethylphenol
BDL
10.
ug/l
625
12/21/02
1
4,6-Dinitro-2-methylphenol
BDL
10.
ug/l
625
12/21/02
1
2,4-Dinitrophenol
BDL
10.
ug/l
625
12/21/02
1
2-Nitrophenol
BDL
10.
ug/1
625
12/21/02
1
4-Nitrophenol
BDL
10.
ug/l
625
12/21/02
1
Pentachlorophenol
BDL
10.
ug/l
625
12/21/02
1
Phenol
BDL
10.
ug/l
625
12/21/02
1
2,4,6-Trichlorophenol
BDL
10.
ug/l
625
12/21/02
1
Surrogate Recovery
Nitrobenzene-d5
76.
% Rec.
625
12/21/02
1
2-Fluorobiphenyl
85.
% Rec.
625
12/21/02
1
p-Terphenyl-dl4
100
% Rec.
625
12/21/02
1
Phenol-d5
39.
% Rec.
625
12/21/02
1
2-Fluorophenol
42.
% Rec.
625
12/21/02
1
2,4,6-Tribromophenol
68.
% Rec.
625
12/21/02
1
Y-JA-A J-1 '&J,
Terrie Fudge, ERepkesentative
BDL - Below Detection Limit U
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A21A - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Page 12 of 26
ENVIRONMENTAL
SCIENCE CORP.
•
•
•
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received
Description
Sample ID
Collected By
Collection Date
Parameter
December 19, 2002
Atlas Distributing
MW-p N_ G„
David Brown
12/16/02 15:00
REPORT OF ANALYSIS
Result
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-04
Site ID :
Project #
Det. Limit Units Method Date Dil.
Lead
BDL
5.0
ug/1
6010B
12/20/02
1
volatile Petroleum Hydrocarbons
510
100
ug/l
MADEPV
12/19/02
1
C5-C8 Aliphatics
370
100
ug/l
MADEPV
12/19/02
1
C9-C12 Aliphatics
270
100
ug/l
MADEPV
12/19/02
1
C9-C10 Aromatics
130
100
ug/l
MADEPV
12/19/02
1
Surrogate Recovery
2,5-Dibromotoluene(FID)
128.
96 Rec.
MADEPV
12/19/02
1
2,5-Dibromotoluene(PID)
123.
96 Rec.
MADEPV
12/19/02
1
Volatile Organics
Acetone
BDL
50.
ug/1
6210D
12/24/02
1
Acrolein
BDL
50.
ug/l
6210D
12/24/02
1
Acrylonitrile
BDL
50.
ug/l
6210D
12/24/02
1
Benzene
14.
1.0
ug/l
6210D
12/24/02
1
Bromobenzene
BDL
1.0
ug/l
6210D
12/24/02
1
Bromodichloromethane
BDL
1.0
ug/l
6210D
12/24/02
1
Bromoform
BDL
1.0
ug/l
6210D
12/24/02
1
Bromomethane
BDL
1.0
ug/1
6210D
12/24/02
1
n-Butylbenzene
BDL
1.0
ug/1
6210D
12/24/02
1
sec-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
1
tert-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
1
Carbon tetrachloride
BDL
1.0
ug/l
6210D
12/24/02
1
Chlorobenzene
BDL
1.0
ug/l
6210D
12/24/02
1
Chlorodibromomethane
BDL
1.0
ug/l
6210D
12/24/02
1
Chloroethane
BDL
1.0
ug/l
6210D
12/24/02
1
Chloroform
BDL
5.0
ug/1
6210D
12/24/02
1
Chloromethane
BDL
1.0
ug/l
6210D
12/24/02
1
2-Chlorotoluene
BDL
1.0
ug/l
6210D
12/24/02
1
4-Chlorotoluene
BDL
1.0
ug/1
6210D
12/24/02
1
1,2-Dibromo-3-Chloropropane
BDL
2.0
ug/l
6210D
12/24/02
1
1,2-Dibromoethane
BDL
1.0
ug/l
6210D
12/24/02
1
Dibromomethane
BDL
1.0
ug/1
6210D
12/24/02
1
1,2-Dichlorobenzene
BDL
1.0
ug/1
6210D
12/24/02
1
1,3-Dichlorobenzene
BDL
1.0
ug/1
6210D
12/24/02
1
1,4-Dichlorobenzene
BDL
1.0
ug/1
6210D
12/24/02
1
Dichlorodifluoromethane
BDL
1.0
ug/1
6210D
12/24/02
1
1,1-Dichloroethane
BDL
1.0
ug/l
6210D
12/24/02
1
1,2-Dichloroethane
BDL
1.0
ug/l
6210D
12/24/02
1
1,1-Dichloroethene
BDL
1.0
ug/1
6210D
12/24/02
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation
Limit(EQL)
Laboratory Certification
Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA -
I-2327, CT-
PH-0197, FL
- E87487, GA -
923, IN -
C-TN-01
KY - 90010, KYUST - 0016, NC -
ENV375,DW21704,
ND - R-140,
SC - 84004,
TN - 2006, VA
- 00109,
WV - 233
Page
13 of 26
ENVIRONMENTAL
• SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
r
LJ
0
Date Received December 19, 2002
Description Atlas Distributing
Sample ID MW-14
Collected By David Brown
Collection Date 12/16/02 15:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-04
Site ID :
Project #
Parameter Result Det. Limit Units Method Date Dil.
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
m&p-Xylenes
Surrogate Recovery
Toluene-d8
Dibromofluoromethane
4-Bromofluorobenzene
Extractable Petroleum Hydrocarb
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
3.4
1.0
ug/l
6210D
12/24/02
18.
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
50.
ug/l
6210D
12/24/02
BDL
5.0
ug/l
6210D
12/24/02
BDL
50.
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
5.0
ug/l
6210D
12/24/02
1.9
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
55.
5.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
17.
1.0
ug/l
6210D
12/24/02
4.6
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
24.
1.0
ug/l
6210D
12/24/02
60.
2.0
ug/l
6210D
12/24/02
98.
% Rec.
6210D
12/24/02
100
% Rec.
6210D
12/24/02
99.
% Rec.
6210D
12/24/02
BDL
100
ug/l
MADEPE
12/26/02
1
1
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 14 of 26
ENVIRONMENTAL
• SCIENCE CORP.
•
0
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC
28377
Date Received
December 19, 2002
Description
Atlas Distributing
Sample ID
MW pq
Collected By
David Brown
Collection Date
12/16/02 15:00
Parameter
REPORT OF ANALYSIS
Result Det. Limit Units
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-04
Site ID :
Project #
Method Date Dil.
C9-C18 Aliphatics
BDL
100
ug/l
MADEPE
12/26/02
1
C19-C36 Aliphatics
BDL
100
ug/1
MADEPE
12/26/02
1
Cll-C22 Aromatics
BDL
100
ug/l
MADEPE
12/26/02
1
Surrogate Recovery
o-Terphenyl
80.0
% Rec.
MADEPE
12/26/02
1
1-Chloro-octadecane
74.0
% Rec.
MADEPE
12/26/02
1
2-Fluorobiphenyl
84.0
% Rec.
MADEPE
12/26/02
1
2-Bromonaphthanene
74.0
% Rec.
MADEPE
12/26/02
1
625 Base/Neutrals w/ TIC
Acenaphthene
BDL
10.
ug/l
625
12/21/02
1
Acenaphthylene
BDL
10.
ug/l
625
12/21/02
1
Anthracene
BDL
10.
ug/l
625
12/21/02
1
Benzidine
BDL
50.
ug/l
625
12/21/02
1
Benzo(a)anthracene
BDL
10.
ug/l
625
12/21/02
1
Benzo(b)fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Benzo(k)fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Benzo(g,h,i)perylene
BDL
10.
ug/l
625
12/21/02
1
Benzo(a)pyrene
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chlorethoxy)methane
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chloroethyl)ether
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chloroisopropyl)ether
BDL
10.
ug/l
625
12/21/02
1
4-Bromophenyl-phenylether
BDL
10.
ug/l
625
12/21/02
1
2-Chloronaphthalene
BDL
10.
ug/l
625
12/21/02
1
4-Chlorophenyl-phenylether
BDL
10.
ug/l
625
12/21/02
1
Chrysene
BDL
10.
ug/l
625
12/21/02
1
Dibenz(a,h)anthracene
BDL
10.
ug/l
625
12/21/02
1
3,3-Dichlorobenzidine
BDL
10.
ug/l
625
12/21/02
1
2,4-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
1
2,6-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
1
Fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Fluorene
BDL
10.
ug/l
625
12/21/02
1
Hexachlorobenzene
BDL
10.
ug/l
625
12/21/02
1
Hexachloro-1,3-butadiene
BDL
10.
ug/l
625
12/21/02
1
Hexachlorocyclopentadiene
BDL
10.
ug/l
625
12/21/02
1
Hexachloroethane
BDL
10.
ug/l
625
12/21/02
1
Indeno(1,2,3-cd)pyrene
BDL
10.
ug/l
625
12/21/02
1
Isophorone
BDL
10.
ug/l
625
12/21/02
1
Naphthalene
BDL
10.
ug/l
625
12/21/02
1
Nitrobenzene
BDL
10.
ug/1
625
12/21/02
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification
Numbers:
A2LA - 1461-01, AIHA - 100789,
AL - 40660, CA -
I-2327, CT-
PH-0197, FL
- E87487, GA -
923, IN -
C-TN-01
KY - 90010, KYUST - 0016, NC
- ENV375,DW21704,
ND - R-140,
SC - 84004,
TN - 2006, VA
- 00109,
WV - 233
Page 15 of 26
ENVIRONMENTAL
• SCIENCE CORP.
0
•
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC
28377
Date Received
December 19, 2002
Description
Atlas Distributing
Sample ID
MW -�Lf
Collected By
David Brown
Collection Date
12/16/02 15:00
Parameter
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
Nitrobenzene-d5
2-Fluorobiphenyl
p-Terphenyl-d14
Phenol-d5
2-Fluorophenol
2,4,6-Tribromophenol
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-04
Site ID :
Project #
Result Det. Limit Units Method Date Dil.
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
67.
Rec.
625
12/21/02 1
72.
Rec.
625
12/21/02 1
89.
Rec.
625
12/21/02 1
35.
Rec.
625
12/21/02 1
46.
96 Rec.
625
12/21/02 1
81.
% Rec.
625
12/21/02 1
cl,.-"� d()
Terrie Fudge, ISC Re esentative
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Page 16 of 26
ENVIRONMENTAL
• SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received
Description
Sample ID
Collected By
Collection Date
December 19, 2002
Atlas Distributing
Mw-� v?(,)3
David Brown
12/16/02 16:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-05
Site ID :
Project #
Parameter Result Det. Limit Units Method Date Dil.
Lead
BDL
5.0
ug/l
6010B
12/20/02
Volatile Petroleum Hydrocarbons
BDL
100
ug/l
MADEPV
12/19/02
C5-C8 Aliphatics
BDL
100
ug/l
MADEPV
12/19/02
C9-C12 Aliphatics
BDL
100
ug/l
MADEPV
12/19/02
C9-C10 Aromatics
BDL
100
ug/l
MADEPV
12/19/02
Surrogate Recovery
2,5-Dibromotoluene(FID)
127.
% Rec.
MADEPV
12/19/02
2,5-Dibromotoluene(PID)
124.
% Rec.
MADEPV
12/19/02
Volatile Organics
Acetone
BDL
50.
ug/l
6210D
12/24/02
Acrolein
BDL
50.
ug/l
6210D
12/24/02
Acrylonitrile
BDL
50.
ug/l
6210D
12/24/02
Benzene
BDL
1.0
ug/l
6210D
12/24/02
Bromobenzene
BDL
1.0
ug/l
6210D
12/24/02
Bromodichloromethane
BDL
1.0
ug/1
6210D
12/24/02
Bromoform
BDL
1.0
ug/l
6210D
12/24/02
Bromomethane
BDL
1.0
ug/l
6210D
12/24/02
n-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
sec-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
tert-Butylbenzene
BDL
1.0
ug/l
6210D
12/24/02
Carbon tetrachloride
BDL
1.0
ug/l
6210D
12/24/02
Chlorobenzene
BDL
1.0
ug/l
6210D
12/24/02
Chlorodibromomethane
BDL
1.0
ug/l
6210D
12/24/02
Chloroethane
BDL
1.0
ug/l
6210D
12/24/02
Chloroform
BDL
5.0
ug/l
6210D
12/24/02
Chloromethane
BDL
1.0
ug/l
6210D
12/24/02
2-Chlorotoluene
BDL
1.0
ug/l
6210D
12/24/02
4-Chlorotoluene
BDL
1.0
ug/l
6210D
12/24/02
1,2-Dibromo-3-Chloropropane
BDL
2.0
ug/l
6210D
12/24/02
1,2-Dibromoethane
BDL
1.0
ug/l
6210D
12/24/02
Dibromomethane
BDL
1.0
ug/l
6210D
12/24/02
1,2-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/24/02
1,3-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/24/02
1,4-Dichlorobenzene
BDL
1.0
ug/l
6210D
12/24/02
Dichlorodifluoromethane
BDL
1.0
ug/l
6210D
12/24/02
1,1-Dichloroethane
BDL
1.0
ug/l
6210D
12/24/02
1,2-Dichloroethane
BDL
1.0
ug/l
6210D
12/24/02
1,1-Dichloroethene
BDL
1.0
ug/l
6210D
12/24/02
1
1
1
1
1
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 17 of 26
0
0
ENVIRONMENTAL
• SCIENCE CORP.
r�
0
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID MW-P ?
Collected By David Brown
Collection Date 12/16/02 16:00
Parameter
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachlorobutadiene
Isopropylbenzene
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
o-Xylene
m&p-Xylenes
Surrogate Recovery
Toluene-d8
Dibromofluoromethane
4-Bromofluorobenzene
Extractable Petroleum Hydrocarb
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-05
Site ID :
Project #
Result Det. Limit Units
Method Date
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
50.
ug/l
6210D
12/24/02
BDL
5.0
ug/1
6210D
12/24/02
BDL
50.
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
5.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
5.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/1
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
1.0
ug/l
6210D
12/24/02
BDL
2.0
ug/1
6210D
12/24/02
96.
% Rec.
6210D
12/24/02
110
% Rec.
6210D
12/24/02
94.
% Rec.
6210D
12/24/02
BDL 100 ug/l MADEPE 12/26/02
Dil.
1
1
1
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Page 18 of 26
ENVIRONMENTAL
• SCIENCE CORP.
•
0
REPORT OF ANALYSIS
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC
28377
Date Received
December 19, 2002
Description
Atlas Distributing
Sample ID
MW/.5
Collected By
David Brown
Collection Date
12/16/02 16:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-05
Site ID :
Project #
Parameter
Result
Det. Limit
Units
Method
Date
Dil.
C9-C18 Aliphatics
BDL
100
ug/1
MADEPE
12/26/02
1
C19-C36 Aliphatics
BDL
100
ug/1
MADEPE
12/26/02
1
C11-C22 Aromatics
BDL
100
ug/1
MADEPE
12/26/02
1
Surrogate Recovery
o-Terphenyl
79.0
% Rec.
MADEPE
12/26/02
1
1-Chloro-octadecane
63.0
% Rec.
MADEPE
12/26/02
1
2-Fluorobiphenyl
88.0
% Rec.
MADEPE
12/26/02
1
2-Bromonaphthanene
88.0
% Rec.
MADEPE
12/26/02
1
625 Base/Neutrals w/ TIC
Acenaphthene
BDL
10.
ug/l
625
12/21/02
1
Acenaphthylene
BDL
10.
ug/l
625
12/21/02
1
Anthracene
BDL
10.
ug/l
625
12/21/02
1
Benzidine
BDL
50.
ug/l
625
12/21/02
1
Benzo(a)anthracene
BDL
10.
ug/l
625
12/21/02
1
Benzo(b)fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Benzo(k)fluoranthene
BDL
10.
ug/l
625
12/21/02
1
Benzo(g,h,i)perylene
BDL
10.
ug/l
625
12/21/02
1
Benzo(a)pyrene
BDL
10.
ug/1
625
12/21/02
1
Bis(2-chlorethoxy)methane
BDL
10.
ug/l
625
12/21/02
1
Bis(2-chloroethyl)ether
BDL
10.
ug/1
625
12/21/02
1
Bis(2-chloroisopropyl)ether
BDL
10.
ug/1
625
12/21/02
1
4-Bromophenyl-phenylether
BDL
10.
ug/1
625
12/21/02
1
2-Chloronaphthalene
BDL
10.
ug/l
625
12/21/02
1
4-Chlorophenyl-phenylether
BDL
10.
ug/1
625
12/21/02
1
Chrysene
BDL
10.
ug/1
625
12/21/02
1
Dibenz(a,h)anthracene
BDL
10.
ug/1
625
12/21/02
1
3,3-Dichlorobenzidine
BDL
10.
ug/l
625
12/21/02
1
2,4-Dinitrotoluene
BDL
10.
ug/1
625
12/21/02
1
2,6-Dinitrotoluene
BDL
10.
ug/l
625
12/21/02
1
Fluoranthene
BDL
10.
ug/1
625
12/21/02
1
Fluorene
BDL
10.
ug/l
625
12/21/02
1
Hexachlorobenzene
BDL
10.
ug/l
625
12/21/02
1
Hexachloro-1,3-butadiene
BDL
10.
ug/l
625
12/21/02
1
Hexachlorocyclopentadiene
BDL
10.
ug/1
625
12/21/02
1
Hexachloroethane
BDL
10.
ug/l
625
12/21/02
1
Indeno(1,2,3-cd)pyrene
BDL
10.
ug/1
625
12/21/02
1
Isophorone
BDL
10.
ug/l
625
12/21/02
1
Naphthalene
BDL
10.
ug/l
625
12/21/02
1
Nitrobenzene
BDL
10.
ug/1
625
12/21/02
1
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification
Numbers:
A2LA - 1461-01, AIHA - 100789,
AL - 40660, CA -
I-2327, CT- PH-0197, FL
- E87487, GA -
923, IN -
C-TN-01
KY - 90010, KYUST - 0016, NC
- ENV375,DW21704,
ND - R-140,
SC - 84004,
TN - 2006, VA
- 00109,
WV - 233
Page
19 of 26
C.
•
ENVIRONMENTAL
SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID
Collected By
Collection Date
Parameter
MW-f 3
David Brown
12/16/02 16:00
n-Nitrosodimethylamine
n-Nitrosodiphenylamine
n-Nitrosodi-n-propylamine
Phenanthrene
Benzylbutyl phthalate
Bis(2-ethylhexyl)phthalate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
Acid Extractables
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,6-Trichlorophenol
Surrogate Recovery
Nitrobenzene-d5
2-Fluorobiphenyl
p-Terphenyl-dl4
Phenol-d5
2-Fluorophenol
2,4,6-Tribromophenol
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
December 26,2002
ESC Sample # L99295-05
Site ID :
Project #
Result Det. Limit Units Method Date Dil.
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
BDL
10.
ug/1
625
12/21/02 1
BDL
10.
ug/l
625
12/21/02 1
71.
% Rec.
625
12/21/02 1
76.
% Rec.
625
12/21/02 1
100
% Rec.
625
12/21/02 1
37.
% Rec.
625
12/21/02 1
50.
% Rec.
625
12/21/02 1
88.
% Rec.
625
12/21/02 1
C-yj�e�- 11200
Terrie Fudge, ZSC Re resentative
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
The reported analytical results relate only to the sample submitted.
This report shall not be reproduced, except in full, without the written approval from ESC.
Page 20 of 26
ENVIRONMENTAL
• SCIENCE CORP.
REPORT OF ANALYSIS
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID LSA-1 3-4 FT
Collected By David Brown
Collection Date 12/17/02 00:00
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970 -
January 08,2003
ESC Sample # L99295-06
Site ID
Project #
Parameter
Dry Result
Det. Limit
Units
Method
Date
Dil.
Total Solids
87.5
%
254OG
12/20/02
1
Volatile Petroleum Hydrocarbons
BDL
5.7
mg/kg
MADEPV
12/24/02
50
C5-C8 Aliphatics
BDL
5.7
mg/kg
MADEPV
12/24/02
50
C9-C12 Aliphatics
BDL
5.7
mg/kg
MADEPV
12/24/02
50
C9-C10 Aromatics
BDL
5.7
mg/kg
MADEPV
12/24/02
50
Surrogate Recovery
2,5-Dibromotoluene(FID)
114.
°s Rec.
MADEPV
12/24/02
1
2,5-Dibromotoluene(PID)
109.
°s Rec.
MADEPV
12/24/02
1
Volatile Organics
Acetone
BDL
0.057
mg/kg
8260B
12/23/02
1
Benzene
BDL
0.0011
mg/kg
8260B
12/23/02
1
Bromodichloromethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
•
Bromoform
Bromomethane
BDL
BDL
0.0011
0.0011
mg/kg
mg/kg
8260B
8260B
12/23/02
12/23/02
1
1
Carbon tetrachloride
BDL
0.0011
mg/kg
8260B
12/23/02
1
Chlorobenzene
BDL
0.0011
mg/kg
8260B
12/23/02
1
Chlorodibromomethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
Chloroethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
2-Chloroethyl vinyl ether
BDL
0.057
mg/kg
8260B
12/23/02
1
Chloroform
BDL
0.0057
mg/kg
8260B
12/23/02
1
Chloromethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
1,2-Dichlorobenzene
BDL
0.0011
mg/kg
8260B
12/23/02
1
1,3-Dichlorobenzene
BDL
0.0011
mg/kg
8260E
12/23/02
1
1,4-Dichlorobenzene
BDL
0.0011
mg/kg
8260B
12/23/02
1
Dichlorodifluoromethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
1,1-Dichloroethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
1,2-Dichloroethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
1,1-Dichloroethene
BDL
0.0011
mg/kg
8260E
12/23/02
1
cis-1,2-Dichloroethene
BDL
0.0011
mg/kg
8260E
12/23/02
1
trans-1,2-Dichloroethene
BDL
0.0011
mg/kg
8260B
12/23/02
1
1,2-Dichloropropane
BDL
0.0011
mg/kg
8260B
12/23/02
1
cis-1,3-Dichloropropene
BDL
0.0011
mg/kg
8260B
12/23/02
1
trans-1,3-Dichloropropene
BDL
0.0011
mg/kg
8260B
12/23/02
1
Di -isopropyl ether
BDL
0.0011
mg/kg
8260B
12/23/02
1
Ethylbenzene
BDL
0.0011
mg/kg
8260B
12/23/02
1
2-Butanone (MEK)
BDL
0.057
mg/kg
8260B
12/23/02
1
Methylene Chloride
BDL
0.0057
mg/kg
8260B
12/23/02
1
4-Methyl-2-pentanone (MIBK)
BDL
0.057
mg/kg
8260B
12/23/02
1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
0
Page 21 of 26
ENVIRONMENTAL
• SCIENCE CORP.
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
Date Received December 19, 2002
Description Atlas Distributing
Sample ID LSA-1 3-4 FT
Collected By David Brown
Collection Date 12/17/02 00:00
REPORT OF ANALYSIS
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
January 08,2003
ESC Sample # L99295-06
Site ID
Project #
Parameter
Dry Result
Det. Limit
Units
Method
Date
Dil.
Methyl tert-butyl ether
BDL
0.057
mg/kg
8260B
12/23/02
1
1,1,2,2-Tetrachloroethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
Tetrachloroethene
BDL
0.0011
mg/kg
8260E
12/23/02
1
Toluene
BDL
0.0057
mg/kg
8260B
12/23/02
1
1,1,1-Trichloroethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
1,1,2-Trichloroethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
Trichloroethene
BDL
0.0011
mg/kg
8260B
12/23/02
1
Trichlorofluoromethane
BDL
0.0011
mg/kg
8260B
12/23/02
1
Vinyl chloride
BDL
0.0011
mg/kg
8260B
12/23/02
1
Xylenes, Total
BDL
0.0034
mg/kg
8260B
12/23/02
1
Surrogate Recovery
Toluene-d8
99.
% Rec.
8260B
12/23/02
1
Dibromofluoromethane
100
% Rec.
8260B
12/23/02
1
4-Bromofluorobenzene
85.
% Rec.
8260B
12/23/02
1
• Extractable Petroleum Hydrocarb
BDL
6.3
mg/kg
MADEPE
12/23/02
1
C9-C18 Aliphatics
BDL
6.3
mg/kg
MADEPE
12/23/02
1
C19-C36 Aliphatics
BDL
6.3
mg/kg
MADEPE
12/23/02
1
C11-C22 Aromatics
BDL
6.3
mg/kg
MADEPE
12/23/02
1
Surrogate Recovery
o-Terphenyl
69.0
% Rec.
MADEPE
12/23/02
1
1-Chloro-octadecane
79.0
% Rec.
MADEPE
12/23/02
1
2-Fluorobiphenyl
77.0
% Rec.
MADEPE
12/23/02
1
2-Bromonaphthanene
42.0
°s Rec.
MADEPE
12/23/02
1
Base/Neutral Extractables
Acenaphthene
BDL
0.38
mg/kg
8270C
12/20/02
1
Acenaphthylene
BDL
0.38
mg/kg
8270C
12/20/02
1
Anthracene
BDL
0.38
mg/kg
8270C
12/20/02
1
Benzidine
BDL
0.38
mg/kg
8270C
12/20/02
1
Benzo(a)anthracene
BDL
0.38
mg/kg
8270C
12/20/02
1
Benzo(b)fluoranthene
BDL
0.38
mg/kg
8270C
12/20/02
1
Benzo(k)fluoranthene
BDL
0.38
mg/kg
8270C
12/20/02
1
Benzo(g,h,i)perylene
BDL
0.38
mg/kg
8270C
12/20/02
1
Benzo(a)pyrene
BDL
0.38
mg/kg
8270C
12/20/02
1
Bis(2-chlorethoxy)methane
BDL
0.38
mg/kg
8270C
12/20/02
1
Bis(2-chloroethyl)ether
BDL
0.38
mg/kg
8270C
12/20/02
1
Bis(2-chloroisopropyl)ether
BDL
0.38
mg/kg
8270C
12/20/02
1
4-Bromophenyl-phenylether
BDL
0.38
mg/kg
8270C
12/20/02
1
2-Chloronaphthalene
BDL
0.38
mg/kg
8270C
12/20/02
1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
• Page 22 of 26
Lebanon R
0
Mt. 3
Mt. Juliet, TN 7122
ENVIRONMENTAL
(615)
758-5858
1-800-767-5859
SCIENCE CORP.
Fax (615)
758-5859
•
Tax I.D.
62-0814289
Est.
1970
REPORT
OF ANALYSIS
Mr. David Brown
January
08,2003
EHC, Inc.
PO Box 902
Red Springs, NC 28377
ESC
Sample #
L99295-06
Date Received December 19, 2002
Description Atlas Distributing
Site
ID
Sample ID LSA-1 3-4 FT
Project
#
Collected By David Brown
Collection Date 12/17/02 00:00
Parameter Dry
Result
Det. Limit
Units
Method
Date
Dil.
4-Chlorophenyl-phenylether
BDL
0.38
mg/kg
8270C
12/20/02
1
Chrysene
BDL
0.38
mg/kg
8270C
12/20/02
1
Dibenz(a,h)anthracene
BDL
0.38
mg/kg
8270C
12/20/02
1
3,3-Dichlorobenzidine
BDL
0.38
mg/kg
8270C
12/20/02
1
2,4-Dinitrotoluene
BDL
0.38
mg/kg
8270C
12/20/02
1
2,6-Dinitrotoluene
BDL
0.38
mg/kg
8270C
12/20/02
1
Fluoranthene
BDL
0.38
mg/kg
8270C
12/20/02
1
Fluorene
BDL
0.38
mg/kg
8270C
12/20/02
1
Hexachlorobenzene
BDL
0.38
mg/kg
8270C
12/20/02
1
Hexachloro-1,3-butadiene
BDL
0.38
mg/kg
8270C
12/20/02
1
Hexachlorocyclopentadiene
BDL
0.38
mg/kg
8270C
12/20/02
1
Hexachloroethane
BDL
0.38
mg/kg
8270C
12/20/02
1
Indeno(1,2,3-cd)pyrene
BDL
0.38
mg/kg
8270C
12/20/02
1
Isophorone
BDL
0.38
mg/kg
8270C
12/20/02
1
Naphthalene
BDL
0.38
mg/kg
8270C
12/20/02
1
Nitrobenzene
BDL
0.38
mg/kg
8270C
12/20/02
1
•
n-Nitrosodimethylamine
BDL
0.38
mg/kg
8270C
12/20/02
1
n-Nitrosodiphenylamine
BDL
0.38
mg/kg
8270C
12/20/02
1
n-Nitrosodi-n-propylamine
BDL
0.38
mg/kg
8270C
12/20/02
1
Phenanthrene
BDL
0.38
mg/kg
8270C
12/20/02
1
Benzylbutyl phthalate
BDL
0.38
mg/kg
8270C
12/20/02
1
Bis(2-ethylhexyl)phthalate
BDL
0.38
mg/kg
8270C
12/20/02
1
Di-n-butyl phthalate
BDL
0.38
mg/kg
8270C
12/20/02
1
Diethyl phthalate
BDL
0.38
mg/kg
8270C
12/20/02
1
Dimethyl phthalate
BDL
0.38
mg/kg
8270C
12/20/02
1
Di-n-octyl phthalate
BDL
0.38
mg/kg
8270C
12/20/02
1
Pyrene
BDL
0.38
mg/kg
8270C
12/20/02
1
1,2,4-Trichlorobenzene
BDL
0.38
mg/kg
8270C
12/20/02
1
Acid Extractables
4-Chloro-3-methylphenol
BDL
0.38
mg/kg
8270C
12/20/02
1
2-Chlorophenol
BDL
0.38
mg/kg
8270C
12/20/02
1
2,4-Dichlorophenol
BDL
0.38
mg/kg
8270C
12/20/02
1
2,4-Dimethylphenol
BDL
0.38
mg/kg
8270C
12/20/02
1
4,6-Dinitro-2-methylphenol
BDL
0.38
mg/kg
8270C
12/20/02
1
2,4-Dinitrophenol
BDL
0.38
mg/kg
8270C
12/20/02
1
2-Nitrophenol
BDL
0.38
mg/kg
8270C
12/20/02
1
4-Nitrophenol
BDL
0.38
mg/kg
8270C
12/20/02
1
Pentachlorophenol
BDL
0.38
mg/kg
8270C
12/20/02
1
Phenol
BDL
0.38
mg/kg
8270C
12/20/02
1
2,4,6-Trichlorophenol
BDL
0.38
mg/kg
8270C
12/20/02
1
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
The reported analytical results relate only to the sample submitted
0
Page 23 of 26
0
ENVIRONMENTAL
SCIENCE CORP.
•
REPORT OF ANALYSIS
Mr. David Brown
EHC, Inc.
PO Box 902
Red Springs, NC 28377
12065 Lebanon Rd.
Mt. Juliet, TN 37122
(615) 758-5858
1-800-767-5859
Fax (615) 758-5859
Tax I.D. 62-0814289
Est. 1970
January 08,2003
ESC
Sample # :
L99295-06
Date Received
December 19, 2002
Description
Atlas Distributing
Site
ID
Sample ID
LSA-1 3-4 FT
Project
#
Collected By
David Brown
Collection Date
12/17/02 00:00
Parameter
Dry
Result
Det. Limit Units
Method
Date
Dil.
Surrogate Recovery
Nitrobenzene-d5
69.
%
Rec.
8270C
12/20/02
1
2-Fluorobiphenyl
84.
%
Rec.
8270C
12/20/02
1
p-Terphenyl-d14
100
%
Rec.
8270C
12/20/02
1
Phenol-d5
72.
%
Rec.
8270C
12/20/02
1
2-Fluorophenol
68.
%
Rec.
8270C
12/20/02
1
2,4,6-Tribromophenol
110
%
Rec.
8270C
12/20/02
1
•
Terrie Fudge, ES Repr sentative
Results listed are dry weight basis.
BDL - Below Detection Limit
Det. Limit - Estimated Quantitation Limit(EQL)
Laboratory Certification Numbers:
A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - I-2327, CT- PH-0197, FL - E87487, GA - 923, IN - C-TN-01
KY - 90010, KYUST - 0016, NC - ENV375,DW21704, ND - R-140, SC - 84004, TN - 2006, VA - 00109, WV - 233
Note:
This report shall not be reproduced, except in full, without the written approval from ESC.
• The reported analytical results relate only to the sample submitted
Page 24 of 26
Attachment A
List of Analytes with QC Qualifiers
•
Sample #
Analyte
Qualifier
L99295-01
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-02
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-03
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-04
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-05
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-06
Benzidine
J4
4-Nitrophenol
J4
2-Chloroethyl vinyl ether
J3J4
• Page 25 of 26
Attachment B
Explanation of QC Qualifier Codes
•
Qualifier Meaning
J3 The associated batch QC was outside the established quality control range
for precision.
J4 The associated batch QC was outside the established quality control range
for accuracy.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R, (Rejected).
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
• Control Limits
2-Fluorophenol 31-119 Nitrobenzene-d5 43-118 Dibromfluoromethane 72-125
Phenol-d5 12-134 2-Fluorobiphenyl 45-128 Toluene-d8 79-120
2,4,6-Tribromophenol 51-141 Terphenyl-d14 43-137 4-Bromofluorobenzene 66-131
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
•
Page 26 of 26
Attachment A
List of Analytes with QC Qualifiers
C,
C J
•
Sample #
Analyte
Qualifier
L99295-01
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-02
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-03
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-04
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-05
Acrolein
J4
Benzene
J4
Bis(2-chlorethoxy)methane
J3
Bis(2-chloroisopropyl)ether
J3
Isophorone
J3
Naphthalene
J3
n-Nitrosodi-n-propylamine
J3
1,2,4-Trichlorobenzene
J3
L99295-06
Benzidine
J4
4-Nitrophenol
J4
2-Chloroethyl vinyl ether
J3J4
Page 25 of 26
Attachment B
Explanation of QC Qualifier Codes
Qualifier Meaning
• J3 The associated batch QC was outside the established quality control range
for precision.
J4 The associated batch QC was outside the established quality control range
for accuracy.
Qualifier Report Information
ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and
as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted
by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical
results. Each qualifier is designated in the qualifier explanation as either EPA or ESC.
Data qualifiers are intended to provide the ESC client with more detailed information concerning
the potential bias of reported data. Because of the wide range of constituents and variety of
matrices incorporated by most EPA methods,it is common for some compounds to fall outside of
established ranges. These exceptions are evaluated and all reported data is valid and useable
unless qualified as 'R' (Rejected).
Definitions
Accuracy - The relationship of the observed value of a known sample to the
true value of a known sample. Represented by percent recovery and
relevant to samples such as: control samples, matrix spike recoveries,
surrogate recoveries, etc.
Precision - The agreement between a set of samples or between duplicate samples.
Relates to how close together the results are and is represented by
Relative Percent Differrence.
Surrogate - Organic compounds that are similar in chemical composition, extraction,
and chromotography to analytes of interest. The surrogates are used to
determine the probable response of the group of analytes that are chem-
ically related to the surrogate compound. Surrogates are added to the
sample and carried through all stages of preparation and analyses.
• Control Limits
2-Fluorophenol 31-119 Nitrobenzene-d5 43-118 Dibromfluoromethane 72-125
Phenol-d5 12-134 2-Fluorobiphenyl 45-128 Toluene-d8 79-120
2,4,6-Tribromophenol 51-141 Terphenyl-d14 43-137 4-Bromofluorobenzene 66-131
TIC - Tentatively Identified Compound: Compounds detected in samples that are
not target compounds, internal standards, system monitoring compounds,
or surrogates.
•
Page 26 of 26
•
Client Name:
Project Name:
Site Location:
VPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued
EHC, Inc.
Atlas Distributing
nir•
Laboratory Name:
NC Certification # (LAB)
Environmental Science Corporation
375
Sample Identification
L99295-01
1-99295-03
L99295-04
L99295-05
Sample Description
—
MW-1 MW-2D
WATER WATER
N/A N/A
12/16/02 12/16/02
12/19/02 12/19/02
N/A N/A
12/19/02 12/19/02
N/A N/A
MW-3
WATER
MW-4
Sample Matrix
WATER
Collection Option (for soil)*
N/A
12/16/02
12/19/02
N/A
Date Collected
12/16/02
Date Received
12/19/02
N/A
Date Extracted
N/A
12/19/02
N/A
Date Analyzed
12/19/02
Dry Weight %
Dilution Factor
N/A
200
e
1 <100
'
1
370
1
<100
1
_
CS-C8 Aliphatics* in ug/L
C9-C12 Aliphatics* in ug/L
250
1
<100
1
270
1
<100
1
C9-C10 Aromatics* in ug/L
130
1
<100
1
130
1
<100
1
Surrogate %Recovery -FID
118%
114%
119%
116%
128%
123%
127%
Surrogate % Recovery - PID
124%
* Option 1=Established fill line on vial Option 2=Sampling Device (indicate brand, e.g. EnCore) Option 3=Field weight of soil.
** Range results should exclude any surrogates, internal standards, or Target PAH analytes.
Percent Recovery - Fortified Blank (Spike) - PID
Relative Percent Difference - PID Duplicate
Percent Recovery - Fortified Blank (Spike) - FID
Relative Percent Difference - FID Duplicate
Initial Calibration Date
ration Ranges and Limits
Attachment 2
VPH Laboratory Reporting Form
12/19/2002
NOTE: Please include units as appropriate
Method of Quantitation (Circle one) C Curve > Average Response Factor
Calibration Concentration Levels
•
0.075 mg/L
CS-C8
0.375 mg/L
Coef of Det (r^2)
Aliphatics
0.750 mg/L
1.00
7.5 mg/L
Linear Fit
11.25 mg/L
i
0.055 mg/L
C9-C12
I
0.275 mg/L
Coef of Det (r^2)
j
-
0.550 mg/L
13.5
Aliphatics
5.50 mg/L
;RSD
-
8.25 mg/L
0.010 mg/L
C9-C10
0.050 mg/L
Coef of Det (r^2)
Aromatics
0.100 mg/L
1.00
1.00 mg/L
Linear Fit
1.50 mg/L
NOTE: Please indicate units as appropriate.
Calibration Check Date
Calibration
12/19/2002
CS-C8 Aliphatics
0.75
6.5
.8
C9-C12 Aliphatics
.55
9.5
.5
C9-C10 Aromatics
0.10
9.5
.11
MDL = Method Detection Limit RPD = Relative Percent Difference
ML = Minimum Limit %RSD = Percent Relative Standard Deviation
RL = Reportable Limit CCC = Correlation Coefficient of Curve
0EHC, Inc.
Atlas Distributing
NC
L99295-01
Client Name:
Project Name:
Site Location:
VPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued
EHC, Inc. Laboratory Name: Environmental Science Corporation
Atlas Distributing
NC
NC Certification # (LAB)
375
Sample Identification
L99295-02
Sample Description
MW-2
Sample Matrix
WATER
Collection Option (for soil)*
N/A
Date Collected
12/16/02
12/19/02
Date Received
Date Extracted
N/A
-
12/21/02
N/A
- - ---- ----
Date Analyzed
Dry Weight %
Dilution Factor
C5-C8 Aliphatics* in ug/L
<100
1
-
uilt
ah
C9-C12 Aliphatics* in ug/L
<100
1
C9-C10 Aromatics* in ug/L
<100
1
Surrogate % Recovery - FID
94%
93%
Surrogate % Recovery - PID
* Option 1=Established fill line on vial Option 2=Sampling Device (indicate brand, e.g. EnCore) Option 3=Field weight of soil.
** Range results should exclude any surrogates, internal standards, or Target PAH analytes.
Percent Recovery - Fortified Blank (Spike) - PID
Relative Percent Difference - PID Duplicate
Percent Recovery - Fortified Blank (Spike) - FID
Relative Percent Difference - FID Duplicate
Attachment 2
VPH Laboratory Reporting Form
PInitial Calibration Date 12/23/2002
alibration Ranges and Limits
CS-C8 Aliphatics 0.0062 mg/L70.02g/L 0.1 mg/L
C9-C12 Aliphatics 0.0032 mg/Lg/L 0.1 mg/L
C9-C10 Aromatics 0.0011 mg/L 0.003 mg/L 0.1 mg/L
NOTE: Please include units as appropriate
Method of Quantitation (Circle one) C Curve j Average Response Factor
Calibration Concentration Levels —
•
0.075 mg/L
CS-C8
0.375 mg/L
Coef of Det (r^2)
Aliphatics
0.750 mg/L
.998
7.5 mg/L
Linear Fit
11.25 mg/L
j
0.055 mg/L
C9-C12 �_
0.275 mg/L
Coef of Det (r^2)
0.550 mg/L
1.000
Aliphatics
5.50 mg/L
Linear Fit
8.25 mg/L
0.010 mg/L
C9-C10
0.050 mg/L
Coef of Det (r^2)
Aromatics
0.100 mg/L
1.00
1.00 mg/L
Linear Fit
1.50 mg/L
NOTE: Please indicate units as appropriate.
Calibration Check Date 12/19/2002
Calibration
t �0
SIR
11"It"
�t
�2
• .77
Aromatics
MDL = Method Detection Limit
ML = Minimum Limit
RL = Reportable Limit
0-
EHC, Inc.
Atlas Distributing
NC
L99295-02
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
Client Name:
Project Name:
Site Location:
Sample Identification
Sample Description
Sample Matrix
Collection Option (for soil)*
Date Collected
Date Received
Date Extracted
Date Analyzed _ _ _—
Dry Weight %
Dilution Factor
C5-C8 Aliphatics* in mg/kg
C9-C12 Aliphatics* in mg/kg
C9-C10 Aromatics* in mg/kg
Surrogate % Recovery - FID
Surrogate % Recovery - PID
VPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued
EHC, Inc.__
Atlas Distributing
NC
Laboratory Name: Environmental Science Corporation
NC Certification # (LAB) 375
L99295-06
LSA-1 3-4 FT
SOIL
Encore-- ------ --- -
12/17/02
12/19/02 -- _-
12/ 17/02
12/24/02
87.5%
50
114%
109%
* Option 1=Established fill line on vial Option 2=Sampling Device (indicate brand, e.g. EnCore) Option 3=Field weight of soil.
** Range results should exclude any surrogates, internal standards, or Target PAH analytes.
Percent Recovery - Fortified Blank (Spike) - PID
Relative Percent Difference - PID Duplicate
Percent Recovery - Fortified Blank (Spike) - FID
Relative Percent Difference - FID Duplicate
Initial Calibration Date
bration Ranges and Limits
Attachment 2
VPH Laboratory Reporting Form
12/23/2002
CS-C8 Aliphatics
0.0062 mg/L
0.02 mg/L
0.1 mg/L
C9-Cl2 Aliphatics
0.0032 mg/L
0.01 mg/L
0.1 mg/L
C9-C10 Aromatics
0.0011 mg/L
0.003 mg/L
0.1 mg/L
NOTE: Please include units as appropriate
Method of Quantitation (Circle one) Curve j Average Response Factor
Calibration Concentration Levels --
•
0.075 mg/L
MMIM
C5-C8
0.375 mg/L
Coef of Det (r^2)
Aliphatics
0.750 mg/L
-
3.7
7.5 mg/L
RSD
11.25 mg/L
0.055 mg/L
C9-C12
0.275 mg/L
Coef of Det (r^2)
0.550 mg/L
9•3
Aliphatics
,
5.50 mg/L
RSD
8.25 mg/L
0.010 mg/L
C9-C10
0.050 mg/L
I Coef of Det (r^2)
Aromatics
! 0.100 mg/L
21.0
_
1.00 mg/L
RSD
1.50 mg/L
Ii
NOTE: Please indicate units as appropriate.
Calibration Check Date 12/24/2002
Calibration
MDL = Method Detection Limit
ML = Minimum Limit
RL = Reportable Limit
go
EHC, Inc.
Atlas Distributing
NC
L99295-06
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
0
EPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued
Client Name: EHC, Inc.
Laboratory Name:
Environmental Science Corporation
Project Name: Atlas Distributing NC Certification # (LAB) 375
Site Location: NC
Now
Sample Identification
L99295-01
. .. ...........
L99295-02 L99295-03
L99295-04
L99296-05
Sample Description
MW-1
M.W-2
WATER
MW-2D
WATER
MW-3
MW-4
Sample Matrix
WATER
WATER
WATER
Date Collected
12/16/02
12/19/02
N/A
12/26/02
N/A
12/16/02
12/19/02
N/A
12/26/02
N/A
12/16/02
12/16/02
12/16/02
Date Received
Date Extracted
Date Analyzed
Dry Weight %
12/19/02
12/19/02
N/A
12/19/02
N/A
N/A
12/26/02
12/26/02
N/A
12/26/02
NIA
N/A
<100 I
Dilution Factor
C9-C18 Alliphatics* in ug/L
<100
1
<100 1
<100
<100
I
C119-C36 Aliphatics* in ug/L
<100
1
<100
1
<100
1
<100
1
<100
C1 I -C22 Aromatics* in ug/L
<100
1
<100
1
<100
1
<100
1
<100
OTP
'0'
2F13F
2BN
Surrogate % Recovery
88%
74%
74%
79%
79%
84%
80%
79%
Surrogate% Recovery
Fractionation Surrogate %Rec.
74%
96%
95%
--- 56% ...
91 %
80%
74%
63%
84%
88%
Fractionation Surrogate % Rec.
74%
88%
Range results should exclude any surrogates, internal standards, or Target PAH analytes.
** Blank correction has been applied per method guidance.
Percent Recovery - Fortified Blank (Spike) 161% 99% 841%1. 9
Relative Percent Difference - Sample Duplicates 7 8 9
Attachment 2
EPH Laboratory Reporting Form
Initial Calibration Date 12/3/2002
ration Ranges and Limits
C9-C18 Aliphatics 0.009341727 mg/L 0.029706691 mg/L 0.1 mg/L
C19-C36 Aliphatics 0.013788582 mg/L 0.043847692 mg/L 0.1 mg/L
C11-C22 Aromatics 0.004464143 mg/L 0.014195974 mg/L 0.1 mg/L
NOTE: Please include units as appropriate
Method of Quantitation (Circle one) Curve Average Response Factor
Calibration Concentration Levels
•
0.080 mg/L
C9-C18
0.375 mg/L
Coef of Det (r^2)
0.750 mg/L
Aliphatics
4.6%rsd
6.0 mg/L
Linear Fit
12.0 mg/L
0.055 mg/L
C19-C36
0.275 mg/L —I
Coef of Det (r^2)
Aliphatics-
0.550 mg/L
4.40 mg/L
- —
3.78%rsd
Linear Fit
8.0 mg/L
0.010 mg/L
C11-C22
0.050 mg/L —
Coef of Det (r^2)
Aromatics
j _ 0.100 mg/L
9.1 %rsd
0.800 mg/L
Linear Fit
1.60 mg/L
NOTE: Please indicate units as appropriate.
Calibration Check Date
Calibration
•
EHC, Inc.
Atlas Distributing
NC
L99295-01
11 /7/2002
MDL = Method Detection Limit
ML = Minimum Limit
RL = Reportable Limit
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
Client Name:
Project Name:
Site Location:
EPH (Aliphatics/Aromatics) Laboratory Reporting Form Continued
EHC, Inc.
Atlas Distributing
NC
Laboratory Name:
NC Certification # (LAB)
Environmental Science Corporation
375
Sample Identification
L99295-06
Sample Description
LSA-1 3-4 FT
Sample Matrix
SOIL
Date Collected
--- -
12/17/02
----...--------------
Date Received
Date Extracted
Date Analyzed
Dry Weight %
Dilution Factor
12/19/02
12/19/02
12/23/02
87.50
<6.3
1
MOM
C9-C18 Aliphatics" in mg/kg
C19-C36 Aliphatics' in mg/kg
<6.3
_
1
-- --- ---- ---
C11-C22 Aromatics' in mg/kg
<6.3
1
-
----
°TP
COD
2FBF
26N
Surrogate % Recovery
69%
Surrogate % Recovery
79%
84.4%
42%
Fractionation Surrogate % Rec.
Fractionation Surrogate % Rec.
" Range results should exclude any surrogates, internal standards, or Target PAH analytes.
"* Blank correction has been applied per method guidance.
t
Percent Recovery - Fortified Blank (Spike) 73% 110% 98%
Relative Percent Difference - Sample Duplicates 6 11 2
Initial Calibration Date
ration Ranges and Limits
12/3/2002
Attachment 2
EPH Laboratory Reporting Form
C9-C18 Aliphatics
0.009341727 mg/L
0.029706691 mg/L
0.1 mg/L
C19-C36 Aliphatics
0.013788582 mg/L
0.043847692 mg/L
0.1 mg/L
C11-C22 Aromatics
0.004464143 mg/L
0.014195974 mg/L
0.1 mg/L
NOTE: Please include units as appropriate
Method of Quantitation (Circle one) Curve Average Response Factor
Calibration Concentration Levels
•
0.080 mg/L
C9-C18
0.375 mg/L
i Coef of Det (r^2)
Aliphatics
0.750 mg/L
4.6%rsd
6.0 mg/L
Linear Fit
12.0 mg/L
0.055 mg/L
C19-C36
0.275 mg/L
Coef of Det (r^2)
0.550 mg/L
3.78%rsd
Aliphatics
-
- -
4.40 mg/L
-
Linear Fit
8.0 mg/L
0.010 mg/L
C11-C22
0.050 mg/L
Coef of Det (r^2)
Aromatics
0.100 mg/L
_' 9.1 %rsd
0.800 mg/L
Linear Fit
-
1.60 mg/L
NOTE: Please indicate units as appropriate.
Calibration Check Date
Calibration
•
EHC, Inc.
Atlas Distributing
NC
L99295-06
11 /7/2002
MDL = Method Detection Limit
ML = Minimum Limit
RL = Reportable Limit
RPD = Relative Percent Difference
%RSD = Percent Relative Standard Deviation
CCC = Correlation Coefficient of Curve
Environmental Science Corp.
• SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
0
•
SAMPLE ID.
Client Name: EHC, Inc. MW-1
Contract:
Matrix (soil/water): WATER ESC Sample No: L99295-01
Date Collected: 12/16/2002 Lab File ID: 1220 22.D
Dilution Factor: 1.0
Date Analyzed: 12/21/2002
Tentatively Identified compounds (TIC) refers to substances not present in the list
of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards . TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist. Quantitation is accomplished
by relative peak area of the TIC compared to that of the nearest internal standard .
from the total ion chromatogram . TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
CONCENTRATION UNITS:
Number TICS found: 8 mg/L
CAS NO.
COMPOUND
RT
EST. CONC.
Q
000108-88-3
Toluene
4.60
8.0391
000100-41-4
Ethylbenzene
6.20
3.8648
000106-42-3
p-Xylene
6.71
9.9219
000611-14-3
Benzene, 1-ethyl-2-methyl-
7.69
3.6734
000095-36-3
1,2,4-Trimethylbenzene
8.14
1.2218
000095-36-3
1,2,4-Trimethylbenzene
8.52
1.2120
000496-11-7
Indane
8.73
6.5606
002870-04-4
Benzene, 2-ethyl-1,3-dimethyl-
1 8.92
3.1891
Comments: All compounds reported have a match quality of 80% or higher
FORM I SV-1 Sw-846 8270
Environmental Science Corp.
• SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
•
SAMPLE ID.
Client Name: EHC, Inc. MW-2
Contract:
Matrix (soil/water): WATER ESC Sample No: L99295-02
Date Collected: 12/16/2002 Lab File ID: 1220 23.D
Dilution Factor: 1.0
Date Analyzed: 12/21/2002
Tentatively Identified compounds (TIC) refers to substances not present in the list
of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards . TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist. Quantitation is accomplished
by relative peak area of the TIC compared to that of the nearest internal standard .
from the total ion chromatogram . TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
Number TICS found: 4
CONCENTRATION UNITS:
mg/L
CAS NO.
COMPOUND
RT
EST. CONC.
Q
000108-88-3
Toluene
4.60
0..31
000135-01-3
Benzene, 1,2-diethyl-
8.81
3.3348
000084-69-5
1,2-Benzenedicarboxylic acid, bis(2-meth
16.14
1.0637
000057-10-3
Hexadecanoic acid
16.68
1 3.7780
Comments: All compounds reported have a match quality of 80% or higher
FORM I SV-1 SW-846 8270
Environmental Science Corp.
• SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
•
Client Name: EHC. Inc.
Contract:
SAMPLE ID.
MW-2D
Matrix (soil/water): WATER ESC Sample No: L99295-03
Date Collected: 12/16/2002 Lab File ID: 1220 24.D
Dilution Factor: 1.0
Date Analyzed: 12/21/2002
Tentatively Identified compounds (TIC) refers to substances not present in the list
of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards. TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist. Quantitation is accomplished
by relative peak area of the TIC compared to that of the nearest internal standard .
from the total ion chromatogram . TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
Number TICS found: 3
CONCENTRATION UNITS:
mg/L
CAS NO.
COMPOUND
RT
EST. CONC.
Q
000108-88-3
Toluene
4.60
16740013659
000112-95-8
Eicosane
21.41
3.3579
000112-95-8
Eicosane
21.96
3.5302
Comments: All compounds reported have a match quality of 80% or higher
FORM I SV-1 SW-846 8270
Environmental Science Corp.
• SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Name: EHC, Inc.
Contract:
Matrix (soil/water): WATER
Date Collected: 12/16/2002
Date Analyzed: 12/21/2002
ESC Sample No:
Lab File ID:
Dilution Factor:
Tentatively Identified compounds (TIC) refers to substances not present in the list
of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards . TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist. Quantitation is accomplished
by relative peak area of the TIC compared to that of the nearest internal standard.
from the total ion chromatogram. TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
Number TICS found: 8
SAMPLE ID.
MW-3
L99295-04
1220_25.D
CONCENTRATION UNITS:
mg/L
CAS NO.
COMPOUND
RT
EST. CONC.
Q
000108-88-3
Toluene
4.60
0.0408
001462-03-9
Cyclopentanol, 1-methyl-
5.03
9.2712
000100-41-4
Ethylbenzene
6.20
2.1008
000106-42-3
p-Xylene
6.71
3.1133
000611-14-3
Benzene, 1-ethyl-2-methyl-
7.69
1.5554
000095-36-3
1,2,4-Trimethylbenzene
8.15
3.1777
000526-73-8
Benzene, 1,2,3-trimethyl-
8.52
9.7711
000496-11-7
1 Indane
8.73
9.6214
Comments: All compounds reported have a match quality of 80% or higher
FORM I SV-1 SW-846 8270
Environmental Science Corp.
• SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
•
SAMPLE ID.
Client Name: EHC, Inc. MW-4
Contract:
Matrix (soil/water): WATER ESC Sample No: L99295-05
Date Collected: 12/16/2002 Lab File ID: 1220 26.D
Dilution Factor: 1.0
Date Analyzed: 12/21/2002
Tentatively Identified compounds (TIC) refers to substances not present in the list
of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards. TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist. Quantitation is accomplished
by relative peak area of the TIC compared to that of the nearest internal standard .
from the total ion chromatogram. TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
Number TICS found: 4
CONCENTRATION UNITS:
mg/L
CAS NO.
COMPOUND
RT
EST. CONC.
Q
000108-88-3
Toluene
4.60
2.7532
000140-66-9
Phenol, 4-(1,1,3,3-tetramethylbutyl)-
15.00
2.1839
025154-52-3
Phenol, nonyl-
15.11
2.2939
054932-78-4
Phenol, 4-(2,2,3,3-tetramethylbutyl)-
15.36
2.2734
Comments: All compounds reported have a match quality of 80% or higher
FORM I SV-1 SW-846 8270
Environmental Science Corp.
• SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
C J
r1
L.J
Client Name: EHC, Inc.
Contract:
Matrix (soil/water): WATER ESC Sample No:
Lab File ID:
Date Collected:
Dilution Factor:
Date Analyzed: 12/20/2002
Tentatively Identified compounds (TIC) refers to substances not present in the list
of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards. TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist. Quantitation is accomplished
by relative peak area of the TIC compared to that of the nearest internal standard .
from the total ion chromatogram . TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
Number TICS found: 0
SAMPLE ID.
MB94572
SBLK02
1220_03.D
CONCENTRATION UNITS:
mg/L
CAS NO. COMPOUND RT EST. CONC. Q
Comments: All compounds reported have a match quality of 80% or higher
FORM I SV-1 SOP-846 8270
Environmental Science Corp.
• SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Client Name: EHC, Inc.
Contract:
Matrix (soil/water):
Date Collected:
Date Analyzed:
WATER
12/20/2002
SAMPLE ID.
MB94572
ESC Sample No: SBLK03
Lab File ID: 1220 04.D
Dilution Factor: 1.0
Tentatively Identified compounds (TIC) refers to substances not present in the list
of target compounds . Therefore, not all TIC's are identified and quantitated
using individual standards . TIC listings are prepared utilizing a computerized
library search routine of electron impact mass spectral data and evaluation of the
relevant data by a mass spectral data specialist. Quantitation is accomplished
by relative peak area of the TIC compared to that of the nearest internal standard .
from the total ion chromatogram . TIC's are identified and quantitated only if the
peak area is 10 % or more of that of the nearest internal standard .
Number TICS found: 0
CONCENTRATION UNITS:
mg/L
CAS NO. COMPOUND RT EST. CONC. Q
•
• Comments: All compounds reported have a match quality of 80% or higher
FORM I SV-1 SW-846 8270
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PO Box 902
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Phone (615) 758-5858
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Date
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