20094_Belmont Dyers_Stockpile Soil Characterization Report RV1_2019.04.23

i
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx
Stockpile Soil Characterization Report Former Belmont Dyers
18 Linestowe Drive
Belmont, North Carolina
H&H Job RPH-001
Table of Contents

Section Page No.
1.0 Introduction and Background .............................................................................................. 1
2.0 Export Soil Characterization Scope of Work ...................................................................... 3
3.0 Export Soil Characterization Sampling Methodology ....................................................... 4
4.0 Soil Characterization Sampling Results .............................................................................. 4
5.0 Quality Assurance/Quality Control ..................................................................................... 6
6.0 Investigation Derived Waste Management .......................................................................... 6
7.0 Stockpile Soil Characterization Summary .......................................................................... 6

Tables
Table 1 Summary of Stockpile Soil Analytical Results

Figures
Figure 1 Site Location Map
Figure 2 Stockpile Sample Location Map
Figure 3 Proposed Site Plan

List of Appendices
Appendix A Summary of Historical Soil Analytical Data (Tables and Figures)
Appendix B Laboratory Analytical Report

1
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx
Stockpile Soil Characterization Report Former Belmont Dyers
18 Linestowe Drive
Belmont, North Carolina
H&H Job RPH-001
1.0 Introduction and Background

On behalf of the Prospective Developer (PD), Aberfoyle, LLC, Hart & Hickman, PC (H&H) has
prepared this Stockpile Soil Characterization Report for the Former Belmont Dyers property
located at 18 Linestowe Drive in Belmont, Gaston County, North Carolina (Site). A Site
location map is included as Figure 1. The Site is in the North Carolina Department of
Environmental Quality (DEQ) Brownfields Program (Brownfields Project #20094-16-036). This
assessment was performed in accordance with the approved Export Soil Characterization Work
Plan dated March 28, 2019.

The subject Site is comprised of two parcels totaling approximately 11.32 acres situated on the
western bank of the Catawba River. The Site contains a vacant office building which is
approximately 2,000 square feet and two asphalt paved parking areas. The remainder of the Site
is vacant land. Grading and construction activities are currently underway at the Site in
accordance with the DEQ-approved Environmental Management Plan (EMP) dated July 26,
2017.

The Site is planned to be redeveloped with 70 townhouse units and 102 multi-family apartment
units, a leasing office, limited urban greenspace, asphalt-paved parking, and landscaped areas.
H&H understands that the redevelopment will result in a net export of soil from the Site.
Currently, three soil stockpiles consisting of approximately 750 cubic yards (CY) each are staged
in the southeastern portion of the Site (identified as Stockpile #1 through #3). Stockpile #1 was
generally cut from the central portion of the Site, Stockpile #2 was generally cut from the
northern portion of the Site, and Stockpile #3 was cut from the southwestern portion of the Site.
The sampling of stockpiled soil will be used to determine the suitability of the soil for use as
beneficial fill and to assist in identifying an appropriate destination for the proposed export soil.

2
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx

H&H understands that in addition to DEQ Brownfields, the DEQ Division of Waste
Management (DWM) Solid Waste Section (SWS) may be involved with review of this report to
determine if the proposed soil-import property is an appropriate destination for the stockpiled
soil. Stockpile soil characterization assessment activities are described in the following sections.

Background
The Site was developed with a textile mill prior to 1929. At that time, the Site contained a main
production building, a boiler building, an attached warehouse, caustic and sulphuric acid tanks,
gasoline underground storage tanks (USTs), a detached warehouse, and the current office
building. Two railroad spurs serviced the Site’s operations until the mid-1960s. An attached dye
house addition was completed by 1965. Former textile operations at the Site consisted of yarn
mercerizing, bleaching, and dyeing. The Site was occupied by the Belmont Processing Company
until the mid-1940s, when Aberfoyle Manufacturing Company took over operations at the Site.
The Site was operated by Belmont Dyers Company from the mid-1970s until 2003. During this
time period, Michelle Textiles also operated in a portion of the building. The former mill
buildings were razed beginning in mid-2007, and the Site has remained vacant since that time.

Soil and groundwater assessment have been conducted at the Site from 1991 to the present.
Assessment and remediation are currently being conducted by the Remediating Party, Meridian
Specialty Yarn Group, Inc. (Meridian), pursuant to a voluntary Administrative Agreement (AA)
with the DEQ Inactive Hazardous Sites Branch (IHSB) Registered Environmental Consultant
(REC) Program. Currently, a Remedial Investigation (RI) is being performed to define the
extent of compounds in environmental media.

Results of groundwater assessment indicate that groundwater impacts (primarily
tetrachloroethylene or PCE) are present in the central, southern, and eastern portions of the Site
at concentrations exceeding the 15A North Carolina Administrative Code 02L .0202
Groundwater Quality Standards (2L Standards). Analytical results of the most recent
groundwater sampling event conducted in November 2017 indicated concentrations of PCE,
trichloroethylene (TCE), 1,4-dichlorobenzene, and 1,1-dichloroethylene

3
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx
exceeding DEQ Residential and Non-Residential Vapor Intrusion Groundwater Screening Levels
(GWSLs) in the southern and eastern portions of the Site.

Limited soil assessment activities have been conducted at the Site by H&H and others. The
results of previous soil assessment conducted in September 2005 indicated PCE was detected in
one soil sample (GP-5) collected from the far southern portion of the Site at a concentration of
19 milligrams per kilogram (mg/kg), which is above the DEQ Residential Preliminary Soil
Remediation Goal (PSRG) of 17 mg/kg but below the Industrial/Commercial PSRG of 82 mg/kg.
The results of previous soil assessment conducted in November 2016 indicated two polycyclic
aromatic hydrocarbons (PAHs; benzo[a]pyrene and dibenzo[a,h]anthracene) were detected at
concentrations exceeding Residential PSRGs but below Industrial/Commercial PSRGs in a soil
boring advanced in the north-central portion of the Site (SB-2). Metals including arsenic and
manganese have been detected at the Site at concentrations above Residential PSRGs but within
the range of regional background metals concentrations.

2.0 Export Soil Characterization Scope of Work

H&H conducted soil characterization sampling of the stockpiled soil to determine the suitability
of the soil for use as beneficial fill and to assist in identifying an appropriate destination for the
proposed export soil. H&H collected stockpile soil samples on March 28, 2019. H&H collected
soil stockpile samples at a sampling rate of approximately one sample per 750 CY. Therefore,
one sample was collected from each of the three stockpiles for laboratory analysis. As indicated
on Table 1, the stockpile samples were collected for laboratory analysis of volatile organic
compounds (VOCs) by EPA Method 8260, semi-VOCs (SVOCs) by EPA Method 8270, and
Resource Conservation and Recovery Act (RCRA) metals plus hexavalent chromium by EPA
Methods 6020/7179/7196.

4
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx
3.0 Export Soil Characterization Sampling Methodology

The stockpile soil characterization activities were performed in general accordance with DEQ
IHSB’s Guidelines for Assessment and Cleanup (Guidelines) dated October 2015 and the most
recent version of the U.S. Environmental Protection Agency (EPA) Region IV Science and
Ecosystem Support (SESD) Field Branches Quality System and Technical Procedures guidance.

Soil characterization samples collected for analysis of SVOCs and metals were collected as
composite samples using a decontaminated stainless-steel hand auger. The composite samples
consisted of five sample aliquots that were combined in the field to form one sample for
laboratory analysis. Each aliquot was field screened for the presence of VOCs using a calibrated
photoionization detector (PID). VOC samples were collected as grab samples using a
decontaminated stainless-steel hand auger from the general area of the aliquot which exhibited
the highest indication of impact during field screening. Field screening indicated PID readings
that ranged from 0.1 parts per million by volume (ppmv) to 1.5 ppmv. The soil samples were
placed in dedicated laboratory-supplied sample containers, labelled with sample ID, date and
time and requested analysis, covered with ice, and shipped to a Prism Laboratories, Inc. (Prism)
under standard chain of custody protocols.

4.0 Soil Characterization Sampling Results

In Table 2, the soil laboratory analytical results are compared to the DEQ IHSB Protection of
Groundwater, Residential, and Industrial/Commercial PSRGs dated February 2018. Because
background metals data are not available for the subject Site, metal concentrations were
compared to regional background levels for North Carolina soils as published in Elements in
North American Soils by Dragun and Chekiri (2005) before comparison to the PSRGs.

H&H requested that Prism, a North Carolina-certified laboratory (NC Certification No. 402),
include a Level II Quality Assurance/Quality Control (QA/QC) data package for the laboratory
report. Additionally, H&H requested Prism report values to the laboratory-specified method

5
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx
detection limits using J-flags and that the laboratory method detection limits met the lower of the
PSRG values (to the extent feasible).

VOCs
Analytical results indicate that PCE was detected in Stockpile #3 at an estimated concentration of
0.0083 J mg/kg which is above the Protection of Groundwater PSRG of 0.0063 mg/kg, but below
the Residential PSRG of 17 mg/kg and the Industrial/Commercial PSRG of 82 mg/kg. No other
VOCs were detected at concentrations above PSRGs.

SVOCs
Analytical results indicate that no SVOCs were detected at concentrations exceeding PSRGs.

Metals
Analytical results indicate that metals concentrations in the stockpile soil samples are consistent
with regional background levels. Concentrations of arsenic were detected above the Residential
PSRG and Industrial/Commercial PSRG, but within the range of regional background levels of
arsenic.

Hexavalent chromium was detected in each of the three stockpiles are concentrations ranging
from 0.40 J mg/kg to 0.58 mg/kg, which are above the Residential PSRG of 0.31 mg/kg. The
hexavalent chromium detections were generally consistent in concentration and were cut from
depths ranging from zero to eight ft below ground surface (bgs) from across the Site. Although
the presence of hexavalent chromium in the environment may be the result of anthropogenic
activity, hexavalent chromium is potentially present in background soil. For example, the New
Jersey Department of Environmental Protection (NJ DEP) conducted a study of background
levels of hexavalent chromium in soil. Results indicated that of the 258 samples analyzed, 36%
contained detectable concentrations of hexavalent chromium, with a 75th percentile concentration
of 1.4 mg/kg and a 99th percentile concentration of 5.5 mg/kg1.

1 http://nemc.us/docs/2011/presentations/Presentation-NagourneyS-8-16-11-Tue-
PM%20[Compatibility%20Mode].pdf

6
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx
No other metals were detected at concentrations above PSRGs.

5.0 Quality Assurance/Quality Control

H&H utilized standard quality assurance/quality control (QA/QC) processes during the
Brownfields additional assessment activities. Non-dedicated sampling equipment, including the
hand auger, was decontaminated using Liquinox® detergent and deionized water prior to and
between each sampling location. H&H wore nitrile gloves while handling samples.

6.0 Investigation Derived Waste Management

No significant soil impacts were observed during field screening and sampling activities.
Therefore, investigation derived waste (IDW) soil cuttings were placed back into the soil
stockpile at each sample location.

7.0 Stockpile Soil Characterization Summary

H&H completed stockpile soil characterization activities at the Former Belmont Dyers
Brownfields property located at 18 Linestowe Drive in Belmont, Gaston County, North Carolina
on March 28, 2019. The assessment activities were conducted to determine the suitability of the
stockpiled soil for use as beneficial fill and to assist in identifying an appropriate destination for
the proposed export soil. Based on the results of the assessment activities, H&H concludes the
following:

• No VOCs or SVOCs were detected in Stockpile #1 or Stockpile #2 at concentrations
exceeding PSRGs.

• Stockpile #3 contained one VOC (PCE) at a concentration exceeding the Protection of
Groundwater PSRG but below the Residential and Industrial/Commercial PSRGs.

7
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Stockpile Soil Characterization Report.docx
• The metal arsenic was detected in each of the three stockpiles samples at concentrations
above the Residential and Industrial/Commercial PSRGs but within the range of regional
background levels of arsenic.

• The metal hexavalent chromium was detected in each of the three stockpile samples at
concentrations above the Residential PSRG but below the Protection of Groundwater and
Industrial/Commercial PSRGs.

Table
Table 1Summary of Stockpile Soil Analytical ResultsFormer Belmont Dyers18 Linestowe DriveBelmont, North CarolinaH&H Job No. RPH-001Sample IDDateRange Mean3/28/2019 3/28/2019 3/28/2019VOCs (8260B) mg/kg1,2,3-Trichlorobenzene0.33 13 190 -- --<0.000320.0040 J 0.0241,2,4-Trichlorobenzene4.1 12 55 -- --<0.000420.0076 J 0.31Acetone25 12,000 140,000 -- -- 0.074 0.026 J 0.027 JTetrachloroethylene 0.0063 17 82 -- --<0.00027 <0.000350.0083 JSVOCs (8270D) mg/kgBenzo(a)anthracene0.35 1.1 21-- -- 0.078 J<0.052 <0.051Benzo(a)pyrene0.12 0.11 2.1-- -- 0.060 J<0.043 <0.042Benzo(b)fluoranthene1.2 1.1 21-- -- 0.12 J<0.0460.046 JBenzo(g,h,i)perylene15,600 NS NS-- -- 0.049 J<0.044 <0.043Caprolactam20 6,300 82,000-- --<0.057 <0.060 <0.059Chrysene36 110 2,100-- -- 0.088 J<0.050 <0.049Fluoranthene670 480 6,000-- -- 0.13 J<0.0510.061 JIndeno(1,2,3-cd)pyrene3.9 1.1 21-- -- 0.055 J<0.046 <0.045Pyrene 440 360 4,500 -- -- 0.12 J<0.0530.061 JPhenanthrene 134 NS NS -- -- 0.050 J<0.052 <0.051Metals (6020C/7471B/7196A) mg/kgArsenic5.8 0.68 3.0 1.0 - 18.0 4.83.1 3.3 4.2Barium580 3,100 47,000 50 - 1,000 35677 98 93Cadmium3.0 14 200 1.0 - 10* 4.3<0.11 <0.12 <0.11Lead270 400 NS ND - 50 1615 19 15Mercury1.0 2.3 9.7 0.03 - 0.52 0.1210.25 0.24 0.29Selenium2.1 78 1,200 <0.1 - 0.8 0.421.1 1.3 1.3Silver3.4 78 1,200 ND - 5.0 NS<0.13 <0.14 <0.14Chromium (total)3.8 0.31 6.5 7.0 - 300 6534 36 36Hexavalent Chromium3.8 0.31 6.5 NS NS0.42 J 0.58 0.40 JTrivalent Chromium** 360,000 23,000 350,000 NS NS33.5835.42 35.60Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (February 2018)2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005* = Range and mean values of background metals for Southeastern USA soils** = Total Chromium - Hexavalent Chromium = Trivalent Chromiumunderlined values exceed Protection of Groundwater PSRGs Bold values exceed background levels for metals and Residential PSRGs Soil concentrations are reported in milligrams per kilogram (mg/kg)Laboratory analytical methods are shown in parenthesesNA = Not Analyzed; NS = Not Specified; -- = Not Applicable VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic CompoundsJ = estimated value between the laboratory detection limit and the laboratory reporting limitLess than values indicate laboratory method detection limitsRegional BackgroundRegional Background Metals in Soil (2)Stockpile SamplesNC DEQ PSRGs(1)SS-01 SS-02 SS-03Protection of GroundwaterResidential IndustrialS:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Task 2 - Brownfields\Stockpile\Soil Data Table4/17/2019Table 1 (Page 1 of 1)Hart & Hickman, PC

Figures
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
BELMONT, NORTH CAROLINA 1997
TITLE
PROJECT
SITE LOCATION MAP
FORMER BELMONT DYERS
18 LINESTOWE DRIVEBELMONT, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
2-12-17 0
1RPH-001
CATAWBA DRIVE
LIN
E
S
T
O
W
E

D
R
I
V
E
VOLK STREET
RIVER

DR
IVE
LI
N
E
S
T
OW
E

D
R
I
V
E
LINESTOWE DRIVE
GP-5
BACKGROUND
SB-2
SB-1
SB-5
SB-4
SB-3
GP-8
GP-9
GP-10
GP-7
GP-6 GP-1 GP-2
GP-3
GP-4
GP-5
BACKGROUND
SB-2
SB-1
SB-5
SB-3
HHSB-4HHSB-8
HHSB-5
HHSB-7
HHSB-3
HHSB-2
HHSB-1
HHSB-6
HHSB-9
JOB NO. RPH-001
REVISION NO. 0DATE: 4-9-19
FIGURE NO. 2
FORMER BELMONT DYERS
18 LINESTOWE DRIVE
BELMONT, NORTH CAROLINA
CATAWBA
RIVER
MULTI-FAMILY
RESIDENCES
CITY OF BELMONT
PUMP STATION
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
PARCEL NO.
126390
PARCEL NO.
126388
PARCEL NO.
126388
PARCEL NO.
126388
PARCEL NO.
126388
STOCKPILE SAMPLE LOCATION MAP
LEGEND
SOIL STOCKPILE
SITE PROPERTY BOUNDARY
APPROXIMATE AREA OF FILL
APPROXIMATE SOIL CUT DEPTH (<2')
APPROXIMATE SOIL CUT DEPTH (2-4')
APPROXIMATE SOIL CUT DEPTH (4-6')
APPROXIMATE SOIL CUT DEPTH (6-8')
SOIL BORING LOCATION (H&H; 2016)
SOIL BORING LOCATION
(MID-ATLANTIC ASSOCIATES; 2016)
SOIL BORING LOCATION
(MID-ATLANTIC ASSOCIATES; 2005)
SOIL SAMPLE COLLECTED BY H&H 5/16/17
STOCKPILE SAMPLE ALIQUOT (3/28/19)
NOTES:
1. NO SHADING INDICATES APPROXIMATE GRADE TO REMAIN.
2. STOCKPILE SOIL SAMPLES COLLECTED BY H&H ON 3/28/19.
STOCKPILE #3/SS-03
STOCKPILE #2/SS-02
STOCKPILE #1/SS-01
APPROXIMATE STOCKPILE #3
SOURCE AREA
APPROXIMATE STOCKPILE #1
SOURCE AREA
APPROXIMATE STOCKPILE #2
SOURCE AREA
S:\AAA-Master Projects\Ralph Falls (RPH)\RPH-001 - Belmont Dyers\Figures\Stockpile Sample Map.dwg, FIG 3 ALT, 4/9/2019 2:43:11 PM, erichardson
CATAWBA DRIVE
LIN
E
S
T
O
W
E

D
R
I
V
E
VOLK STREET
RIVER

DR
IVE
LI
N
E
S
T
OW
E

D
R
I
V
E
LINESTOWE DRIVE
PMW-1IR
PMW-1DR PMW-1SRPMW-2SR
PMW-5SR PMW-4SR
PMW-3SR
PMW-6IR PMW-6SR
LEGEND
SITE PROPERTY BOUNDARY
SHALLOW MONITORING WELL
LOCATION
DEEP MONITORING WELL
LOCATION
PROPOSED BUILDING FOOTPRINT
JOB NO. RPH-001
REVISION NO. 0DATE: 4-8-19
FIGURE NO. 3
FORMER BELMONT DYERS
18 LINESTOWE DRIVE
BELMONT, NORTH CAROLINA
PROPOSED SITE PLAN RIVER

DR
IVE
CATAWBA
RIVER
MULTI-FAMILY
RESIDENCES
CITY OF BELMONT
PUMP STATION
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
PARCEL NO.
126390
PARCEL NO.
126388
PARCEL NO.
126388
PARCEL NO.
126388
PARCEL NO.
126388
S:\AAA-Master Projects\Ralph Falls (RPH)\Task 2 - Brownfields\Work Plan\Figures\Sample Location Map.dwg, FIG 3, 6/14/2017 11:57:44 AM, zbarlow

Appendix A Summary of Historical Soil Analytical Data (Tables and Figures)
Table 1 (Page 1 of 1)
Summary of Soil Analytical Results
Former Belmont Dyers Facility
18 Linestowe Drive
Belmont, North Carolina
H&H Job No. RPH-001
S:\AAA-Master Projects\Ralph Falls (RPH)\Task 2 - Brownfields\Report\Soil Data Table
2/6/2017
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Sample ID Background-1 SB-1 SB-2 SB-3 SB-4 SB-5
Date 11/21/2016 11/21/2016 11/21/2016 11/21/2016 11/21/2016 11/21/2016
Depth (ft)Range Mean 2-4 0-2 1-3 1-3 3-5 2-4
VOCs (8260B) mg/kgAcetone 12,200 ----NA 0.0234 J <0.058 0.0152 J 0.0258 J 0.0162 J
SVOCs (8270D) mg/kg
Acenaphthylene NS ----NA <0.200 0.175 J <0.210 <0.200 <0.210
Anthracene 3,600 ----NA <0.200 0.209 <0.210 <0.200 <0.210
Benzo(a) anthracene 0.16 ----NA <0.200 0.61 <0.210 <0.200 <0.210
Benzo (a) pyrene 0.016 ----NA <0.200 0.622 <0.210 <0.200 <0.210
Benzo (b) fluoranthene 0.16 ----NA <0.200 0.567 <0.210 <0.200 <0.210
Benzo (g,h,i) perylene NS ----NA <0.200 0.493 <0.210 <0.200 <0.210
Benzo (k) fluoranthene 1.6 ----NA <0.200 0.587 <0.210 <0.200 <0.210
Chrysene 16 ----NA <0.200 0.629 <0.210 <0.200 <0.210
Dibenzo(a,h)anthracene 0.016 ----NA <0.200 0.111 J <0.210 <0.200 <0.210
Fluoranthene 480 ----NA <0.200 0.779 <0.210 <0.200 <0.210
Indeno(1,2,3-cd)pyrene 0.16 ----NA <0.200 0.534 <0.210 <0.200 <0.210
Phenanthrene NS ----NA <0.200 0.244 <0.210 <0.200 <0.210
Pyrene 360 ----NA <0.200 1.02 <0.210 <0.200 <0.210
Metals (6010C/7471B/7196A) mg/kg
Antimony 6.2 <1.0 - 8.8*0.76 <6.2 <5.8 <6.1 <5.8 <5.2 <6.1
Beryllium 32 ND - 2.0 0.11 <1.5 <1.5 <1.5 <1.5 <1.3 <1.5
Cadmium 14.2 1.0 - 10*4.3 <1.2 <1.2 <1.2 <1.2 <1.0 <1.2
Copper 620 3 - 100 34 65.0 82.4 80.0 83.0 53.7 59.0
Lead 400 ND - 50 16 <6.2 <5.8 <6.1 <5.8 <5.2 <6.1
Manganese 360 <2.0 - 7,000*640 111 624 265 241 527 171
Nickel 300 ND - 150 23 44.0 <12 <12 <12 26.9 <12
Selenium 78 <0.1 - 0.8 0.42 <6.2 <5.8 <6.1 <5.8 <5.2 <6.1
Silver 78 ND - 5.0 NS <3.1 <2.9 <3.1 <2.9 <2.6 <3.0
Zinc 4,600 25 - 124 56 30.2 69.7 35.0 42.7 87.5 50.5
Chromium (Total)NS 7.0 - 300 65 116 3.3 8.5 17.4 38.2 39.0
Hexavalent Chromium 0.3 NS NS <2.5 <2.3 <2.4 <2.5 <2.4 <2.5
Trivalent Chromium**24,000 NS NS 116 3.3 8.5 17.4 38.2 39.0
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB)
Preliminary Soil Remediation Goals (PSRGs) (April 2016)
2) Range and mean values of background metals for North Carolina soils taken from Elements in
North American Soils by Dragun and Chekiri, 2005
* = Range and mean values of background metals for Southeastern USA soils
** = Total Chromium - Hexavalent Chromium = Trivalent Chromium
Bold values exceed background levels for metals and Residential PSRGs
Soil concentrations are reported in milligrams per kilogram (mg/kg)
Laboratory analytical methods are shown in parentheses
NA = Not Analyzed; NS = Not Specified; -- = Not Applicable
VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds
J = estimated value between the laboratory detection limit and the laboratory reporting limit
Background Soil Borings
Residential
PSRGs (1)
(mg/kg)
Regional Background
Metals in Soil (2)
Table 1 (Page 1 of 1)Summary of Soil Analytical ResultsFormer Belmont Dyers Facility18 Linestowe DriveBelmont, North CarolinaH&H Job No. RPH-001Sample IDBackground-1* HHSB-1 HHSB-2 HHSB-4 HHSB-5 HHSB-6 HHSB-7 HHSB-8 HHSB-9Date11/21/2016 5/16/2017 5/16/2017 5/16/2017 5/16/2017 5/16/2017 5/16/2017 5/16/2017 5/16/2017 5/16/2017 5/16/2017Depth (ft)Range Mean2-42-42-46-8 4-6 0-2 2-4 4-6 6-8SVOCs (8270C) mg/kg-- -- ----NA NA NA NA NA ALL BRL NA NA NA NAPCBs (8082) mg/kg------NA ALL BRL ALL BRL ALL BRL ALL BRL ALL BRL ALL BRL ALL BRL ALL BRL ALL BRL ALL BRLPesticides (8081) mg/kgHexachlorobenzene0.21----NA<0.00710.00096 J<0.0072 <0.0072 <0.0085 <0.00730.0048 J<0.0079 <0.0070 <0.0070RCRA Metals (6020/7471) mg/kgArsenic0.68 1.0 - 18 4.8NANANANANANA2.6NANANANABarium3,000 50 - 1,000 356NANANANANANA58NANANANAChromium (Total)NS 7.0 - 300 65116NANANANANA38NANANANALead400 ND - 50 16<6.2 NANANANANA14NANANANAMercury2.20.03 - 0.52 0.121NANANANANANA0.085NANANANASelenium78 <0.1 - 0.8 0.42<6.2 NANANANANA1.2 JNANANANASilver78ND - 5.0 NS<3.1NANANANANA0.016 JNANANANANotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (October 2016)2) Range and mean values of background metals for North Carolina soils taken from Elements inNorth American Soils by Dragun and Chekiri, 2005Bold indicates concentration exceeds Residential PSRG (October 2016)Only compounds detected in at least one sample are shown* = Sample collected from an area on the Site that does not appear to have been impacted by historical operationsSoil concentrations are reported in milligrams per kilogram (mg/kg)Laboratory analytical methods are shown in parenthesesNA = Not Analyzed; NS = Not Specified; -- = Not Applicable VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic CompoundsJ = estimated value between the laboratory detection limit and the laboratory reporting limitBRL = below laboratory reporting limitBackgroundSoil BoringsResidential PSRGs (1)(mg/kg)Regional Background Metals in Soil (2)HHSB-3 / DUP-14-6S:\AAA‐Master Projects\Ralph Falls (RPH)\Tables\Data Tables6/12/2017Table 1 (Page 1 of 1)Hart & Hickman, PC
CATAWBA DRIVE
LIN
E
S
T
O
W
E

D
R
I
V
E
VOLK STREET
RIVER

DR
IVE
LI
N
E
S
T
OW
E

D
R
I
V
E
LINESTOWE DRIVE
GP-5
BACKGROUND
SB-2
SB-1
SB-5
SB-4
SB-3
GP-8
GP-9
GP-10
GP-7
GP-6 GP-1 GP-2
GP-3
GP-4
GP-5
BH101 BH102
BH105BH110BH111
BH106
TF-2
D-1
FT-2
BH104
BH103
TF-3
BH100
BH107
BH108
BH109
TF-1
GT-1
GT-2
DL-.05
DL-1
TF1-S/
TF1-6
TA-1
TA-2
BACKGROUND
SB-2
SB-1
SB-5
SB-3
HHSB-4HHSB-8
HHSB-5
HHSB-7
HHSB-3
HHSB-2
HHSB-1
HHSB-6
HHSB-9
JOB NO. RPH-001
REVISION NO. 0DATE: 6-12-17
FIGURE NO. 2
FORMER BELMONT DYERS
18 LINESTOWE DRIVE
BELMONT, NORTH CAROLINA
CATAWBA
RIVER
MULTI-FAMILY
RESIDENCES
CITY OF BELMONT
PUMP STATION
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
PARCEL NO.
126390
PARCEL NO.
126388
PARCEL NO.
126388
PARCEL NO.
126388
PARCEL NO.
126388
CUT/FILL ANALYSIS WITH
SOIL SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
FORMER BUILDING FOOTPRINT
APPROXIMATE AREA OF FILL
APPROXIMATE SOIL CUT DEPTH (<2')
APPROXIMATE SOIL CUT DEPTH (2-4')
APPROXIMATE SOIL CUT DEPTH (4-6')
APPROXIMATE SOIL CUT DEPTH (6-8')
SOIL BORING LOCATION (H&H; 2016)
SOIL BORING LOCATION (MID-ATLANTIC
ASSOCIATES; 2016)
SOIL BORING LOCATION (MID-ATLANTIC
ASSOCIATES; 2005)
SOIL BORING LOCATION
NOTES:
1. NO SHADING INDICATES APPROXIMATE GRADE TO REMAIN.
2. SOIL SAMPLES COLLECTED BY H&H ON 5/16/17.S:\AAA-Master Projects\Ralph Falls (RPH)\Task 2 - Brownfields\Work Plan\Figures\Sample Location Map.dwg, FIG 2, 6/12/2017 10:39:42 AM, zbarlow

Appendix B
Laboratory Analytical Report
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
4/11/19 11:59
Hart & Hickman (Charlotte)
Brett Lawrence
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: RPH-001
Lab Submittal Date: 03/28/2019
Prism Work Order: 9030455
This is a Revised Report and supercedes the original laboratory report dated 04/02/19. This report has
results for samples SS-01, SS-02, and SS-03.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
MI Matrix spike outside of the control limits. Matrix interference suspected.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Receipt Summary
04/11/2019
Prism Work Order: 9030455
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
9030455-01 03/28/19 12:55SS-01 03/28/19 17:18Solid
9030455-02 03/28/19 13:10SS-02 03/28/19 17:18Solid
9030455-03 03/28/19 13:25SS-03 03/28/19 17:18Solid
Samples were received in good condition at 4.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 9030455
04/11/2019
Summary of Detections
0.078 J mg/kg dry9030455-01 SS-01 Benzo(a)anthracene 8270D
0.060 J mg/kg dry9030455-01 SS-01 Benzo(a)pyrene 8270D
0.12 J mg/kg dry9030455-01 SS-01 Benzo(b)fluoranthene 8270D
0.049 J mg/kg dry9030455-01 SS-01 Benzo(g,h,i)perylene 8270D
0.088 J mg/kg dry9030455-01 SS-01 Chrysene 8270D
0.13 J mg/kg dry9030455-01 SS-01 Fluoranthene 8270D
0.055 J mg/kg dry9030455-01 SS-01 Indeno(1,2,3-cd)pyrene 8270D
0.050 J mg/kg dry9030455-01 SS-01 Phenanthrene 8270D
0.12 J mg/kg dry9030455-01 SS-01 Pyrene 8270D
0.42 J mg/kg dry9030455-01 SS-01 Hexavalent Chromium 7196A
0.25 mg/kg dry9030455-01 SS-01 Mercury 7471B
3.1 mg/kg dry9030455-01 SS-01 Arsenic 6020B
77 mg/kg dry9030455-01 SS-01 Barium 6020B
34 mg/kg dry9030455-01 SS-01 Chromium 6020B
15 mg/kg dry9030455-01 SS-01 Lead 6020B
1.1 mg/kg dry9030455-01 SS-01 Selenium 6020B
0.074 mg/kg dry9030455-01 SS-01 Acetone 8260B
0.58 mg/kg dry9030455-02 SS-02 Hexavalent Chromium 7196A
0.24 mg/kg dry9030455-02 SS-02 Mercury 7471B
3.3 mg/kg dry9030455-02 SS-02 Arsenic 6020B
98 mg/kg dry9030455-02 SS-02 Barium 6020B
36 mg/kg dry9030455-02 SS-02 Chromium 6020B
19 mg/kg dry9030455-02 SS-02 Lead 6020B
1.3 mg/kg dry9030455-02 SS-02 Selenium 6020B
0.0040 J mg/kg dry9030455-02 SS-02 1,2,3-Trichlorobenzene 8260B
0.0076 J mg/kg dry9030455-02 SS-02 1,2,4-Trichlorobenzene 8260B
0.026 J mg/kg dry9030455-02 SS-02 Acetone 8260B
0.046 J mg/kg dry9030455-03 SS-03 Benzo(b)fluoranthene 8270D
0.061 J mg/kg dry9030455-03 SS-03 Fluoranthene 8270D
0.061 J mg/kg dry9030455-03 SS-03 Pyrene 8270D
0.40 J mg/kg dry9030455-03 SS-03 Hexavalent Chromium 7196A
0.29 mg/kg dry9030455-03 SS-03 Mercury 7471B
4.2 mg/kg dry9030455-03 SS-03 Arsenic 6020B
93 mg/kg dry9030455-03 SS-03 Barium 6020B
36 mg/kg dry9030455-03 SS-03 Chromium 6020B
15 mg/kg dry9030455-03 SS-03 Lead 6020B
1.3 mg/kg dry9030455-03 SS-03 Selenium 6020B
0.024 mg/kg dry9030455-03 SS-03 1,2,3-Trichlorobenzene 8260B
0.31 mg/kg dry9030455-03 SS-03 1,2,4-Trichlorobenzene 8260B
0.027 J mg/kg dry9030455-03 SS-03 Acetone 8260B
0.0083 J mg/kg dry9030455-03 SS-03 Tetrachloroethylene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-01
Prism Sample ID: 9030455-01
Prism Work Order: 9030455
Time Collected: 03/28/19 12:55
Time Submitted: 03/28/19 17:18
General Chemistry Parameters
87.6 SM2540 G P9C059310.100 4/1/19 8:53 KBS% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0311,1’-Biphenyl
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0582,3,4,6-Tetrachlorophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0712,4,5-Trichlorophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0702,4,6-Trichlorophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0732,4-Dichlorophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0582,4-Dimethylphenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0522,4-Dinitrophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0462,4-Dinitrotoluene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0502,6-Dinitrotoluene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0542-Chloronaphthalene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0532-Chlorophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0602-Methylnaphthalene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0482-Methylphenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0682-Nitroaniline
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0682-Nitrophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0743,3’-Dichlorobenzidine
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0463/4-Methylphenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0653-Nitroaniline
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0564,6-Dinitro-2-methylphenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0644-Bromophenyl phenyl ether
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0534-Chloro-3-methylphenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0454-Chloroaniline
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0494-Chlorophenyl phenyl ether
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0684-Nitroaniline
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.0584-Nitrophenol
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.051Acenaphthene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.054Acenaphthylene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.063Acetophenone
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.060Anthracene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.058Atrazine
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.033Benzaldehyde
0.078 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.049Benzo(a)anthracene
0.060 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.041Benzo(a)pyrene
0.12 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.044Benzo(b)fluoranthene
0.049 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.041Benzo(g,h,i)perylene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.049Benzo(k)fluoranthene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.065bis(2-Chloroethoxy)methane
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.064Bis(2-chloroisopropyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-01
Prism Sample ID: 9030455-01
Prism Work Order: 9030455
Time Collected: 03/28/19 12:55
Time Submitted: 03/28/19 17:18
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.056Bis(2-Ethylhexyl)phthalate
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.053Butyl benzyl phthalate
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.057Caprolactam
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.058Carbazole
0.088 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.047Chrysene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.057Dibenzofuran
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.052Diethyl phthalate
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.050Dimethyl phthalate
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.053Di-n-butyl phthalate
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.046Di-n-octyl phthalate
0.13 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.048Fluoranthene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.054Fluorene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.060Hexachlorobenzene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.067Hexachlorobutadiene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.067Hexachlorocyclopentadiene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.063Hexachloroethane
0.055 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.043Indeno(1,2,3-cd)pyrene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.051Isophorone
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.060Naphthalene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.053Nitrobenzene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.059N-Nitroso-di-n-propylamine
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.057N-Nitrosodiphenylamine
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.044Pentachlorophenol
0.050 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.049Phenanthrene
BRL 8270D P9C058010.38 3/29/19 18:24 JMVmg/kg dry 0.055Phenol
0.12 8270D P9C058010.38 3/29/19 18:24 JMVJmg/kg dry 0.050Pyrene
Surrogate Recovery Control Limits
37-13157 %2,4,6-Tribromophenol
47-13076 %2-Fluorobiphenyl
44-11770 %2-Fluorophenol
45-12166 %Nitrobenzene-d5
37-12769 %Phenol-d5
38-13574 %Terphenyl-d14
Total Metals
0.42 7196A P9D003010.46 4/2/19 11:00 BMSJmg/kg dry 0.11Hexavalent Chromium
0.25 7471B P9D000310.057 4/1/19 10:58 MMRmg/kg dry 0.020Mercury
3.1 6020B P9C0571101.1 3/29/19 16:01 JABmg/kg dry 0.37Arsenic
77 6020B P9C057110113/29/19 16:01 JABmg/kg dry 0.39Barium
BRL 6020B P9C0571100.57 3/29/19 16:01 JABmg/kg dry 0.11Cadmium
34 6020B P9C0571101.1 3/29/19 16:01 JABmg/kg dry 0.30Chromium
15 6020B P9C0571101.1 3/29/19 16:01 JABmg/kg dry 0.22Lead
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-01
Prism Sample ID: 9030455-01
Prism Work Order: 9030455
Time Collected: 03/28/19 12:55
Time Submitted: 03/28/19 17:18
1.1 6020B P9C0571101.1 3/29/19 16:01 JABmg/kg dry 0.31Selenium
BRL 6020B P9C0571100.57 3/29/19 16:01 JABmg/kg dry 0.13Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000271,1,1-Trichloroethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000381,1,2,2-Tetrachloroethane
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.000421,1,2-Trichloro-1,2,2-trifluoroethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000501,1,2-Trichloroethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000421,2-Dibromo-3-chloropropane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.000271,2-Dichlorobenzene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000341,2-Dichloroethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P9D000710.11 3/29/19 17:52 JLBmg/kg dry 0.0111,4-Dioxane
0.074 8260B P9D000710.023 3/29/19 17:52 JLBmg/kg dry 0.0014Acetone
BRL 8260B P9D000710.0034 3/29/19 17:52 JLBmg/kg dry 0.00033Benzene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00031Bromochloromethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00032Bromodichloromethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00064Bromoform
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00070Bromomethane
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00028Carbon disulfide
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00030Chlorobenzene
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00047Chloroethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00041Chloroform
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00038Chloromethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00037Cyclohexane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00026Dichlorodifluoromethane
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00022Ethylbenzene
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00033Isopropylbenzene (Cumene)
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00052m,p-Xylenes
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00085Methyl Acetate
BRL 8260B P9D000710.057 3/29/19 17:52 JLBmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00048Methylcyclohexane
BRL 8260B P9D000710.023 3/29/19 17:52 JLBmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-01
Prism Sample ID: 9030455-01
Prism Work Order: 9030455
Time Collected: 03/28/19 12:55
Time Submitted: 03/28/19 17:18
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00048Methyl Isobutyl Ketone
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00032Methylene Chloride
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00023o-Xylene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00034Styrene
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00032Toluene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00037Trichloroethylene
BRL 8260B P9D000710.0057 3/29/19 17:52 JLBmg/kg dry 0.00037Trichlorofluoromethane
BRL 8260B P9D000710.011 3/29/19 17:52 JLBmg/kg dry 0.00027Vinyl chloride
BRL 8260B P9D000710.017 3/29/19 17:52 JLBmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12995 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-02
Prism Sample ID: 9030455-02
Prism Work Order: 9030455
Time Collected: 03/28/19 13:10
Time Submitted: 03/28/19 17:18
General Chemistry Parameters
83.1 SM2540 G P9C059310.100 4/1/19 8:53 KBS% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0331,1’-Biphenyl
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0612,3,4,6-Tetrachlorophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0752,4,5-Trichlorophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0742,4,6-Trichlorophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0772,4-Dichlorophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0612,4-Dimethylphenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0552,4-Dinitrophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0482,4-Dinitrotoluene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0572-Chloronaphthalene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0562-Chlorophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0632-Methylnaphthalene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0512-Methylphenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0722-Nitroaniline
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0722-Nitrophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0783,3’-Dichlorobenzidine
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0683-Nitroaniline
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0684-Bromophenyl phenyl ether
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0564-Chloro-3-methylphenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0724-Nitroaniline
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.0614-Nitrophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.054Acenaphthene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.057Acenaphthylene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.066Acetophenone
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.064Anthracene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.062Atrazine
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.035Benzaldehyde
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.052Benzo(a)anthracene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.052Benzo(k)fluoranthene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.069bis(2-Chloroethoxy)methane
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-02
Prism Sample ID: 9030455-02
Prism Work Order: 9030455
Time Collected: 03/28/19 13:10
Time Submitted: 03/28/19 17:18
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.057Butyl benzyl phthalate
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.060Caprolactam
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.061Carbazole
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.050Chrysene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.060Dibenzofuran
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.052Dimethyl phthalate
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.056Di-n-butyl phthalate
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.051Fluoranthene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.057Fluorene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.063Hexachlorobenzene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.071Hexachlorobutadiene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.071Hexachlorocyclopentadiene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.066Hexachloroethane
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.054Isophorone
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.064Naphthalene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.056Nitrobenzene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.060N-Nitrosodiphenylamine
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.047Pentachlorophenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.052Phenanthrene
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.059Phenol
BRL 8270D P9C058010.40 3/29/19 17:39 JMVmg/kg dry 0.053Pyrene
Surrogate Recovery Control Limits
37-13166 %2,4,6-Tribromophenol
47-13081 %2-Fluorobiphenyl
44-11773 %2-Fluorophenol
45-12168 %Nitrobenzene-d5
37-12773 %Phenol-d5
38-13582 %Terphenyl-d14
Total Metals
0.58 7196A P9D003010.48 4/2/19 11:00 BMSmg/kg dry 0.12Hexavalent Chromium
0.24 7471B P9D000310.060 4/1/19 11:16 MMRmg/kg dry 0.021Mercury
3.3 6020B P9C0571101.2 3/29/19 16:19 JABmg/kg dry 0.39Arsenic
98 6020B P9C057110123/29/19 16:19 JABmg/kg dry 0.41Barium
BRL 6020B P9C0571100.60 3/29/19 16:19 JABmg/kg dry 0.12Cadmium
36 6020B P9C0571101.2 3/29/19 16:19 JABmg/kg dry 0.31Chromium
19 6020B P9C0571101.2 3/29/19 16:19 JABmg/kg dry 0.23Lead
1.3 6020B P9C0571101.2 3/29/19 16:19 JABmg/kg dry 0.32Selenium
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-02
Prism Sample ID: 9030455-02
Prism Work Order: 9030455
Time Collected: 03/28/19 13:10
Time Submitted: 03/28/19 17:18
BRL 6020B P9C0571100.60 3/29/19 16:19 JABmg/kg dry 0.14Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000361,1,1-Trichloroethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000501,1,2,2-Tetrachloroethane
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.000551,1,2-Trichloro-1,2,2-trifluoroethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000651,1,2-Trichloroethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000201,1-Dichloroethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000321,1-Dichloroethylene
0.0040 8260B P9D000710.015 3/29/19 18:22 JLBJmg/kg dry 0.000421,2,3-Trichlorobenzene
0.0076 8260B P9D000710.015 3/29/19 18:22 JLBJmg/kg dry 0.000551,2,4-Trichlorobenzene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000541,2-Dibromo-3-chloropropane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000291,2-Dibromoethane
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.000341,2-Dichlorobenzene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000441,2-Dichloroethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.000451,2-Dichloropropane
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.000491,3-Dichlorobenzene
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.000291,4-Dichlorobenzene
BRL 8260B P9D000710.15 3/29/19 18:22 JLBmg/kg dry 0.0151,4-Dioxane
0.026 8260B P9D000710.029 3/29/19 18:22 JLBJmg/kg dry 0.0018Acetone
BRL 8260B P9D000710.0044 3/29/19 18:22 JLBmg/kg dry 0.00043Benzene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00040Bromochloromethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00041Bromodichloromethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00083Bromoform
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00091Bromomethane
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00036Carbon disulfide
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00037Carbon Tetrachloride
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00039Chlorobenzene
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00061Chloroethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00053Chloroform
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00049Chloromethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00031cis-1,2-Dichloroethylene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00025cis-1,3-Dichloropropylene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00048Cyclohexane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00030Dibromochloromethane
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00033Dichlorodifluoromethane
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00028Ethylbenzene
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00043Isopropylbenzene (Cumene)
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00068m,p-Xylenes
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.0011Methyl Acetate
BRL 8260B P9D000710.073 3/29/19 18:22 JLBmg/kg dry 0.00066Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00062Methylcyclohexane
BRL 8260B P9D000710.029 3/29/19 18:22 JLBmg/kg dry 0.00066Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00062Methyl Isobutyl Ketone
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-02
Prism Sample ID: 9030455-02
Prism Work Order: 9030455
Time Collected: 03/28/19 13:10
Time Submitted: 03/28/19 17:18
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00041Methylene Chloride
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00023Methyl-tert-Butyl Ether
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00030o-Xylene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00044Styrene
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00035Tetrachloroethylene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00042Toluene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00044trans-1,2-Dichloroethylene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00039trans-1,3-Dichloropropylene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00048Trichloroethylene
BRL 8260B P9D000710.0073 3/29/19 18:22 JLBmg/kg dry 0.00047Trichlorofluoromethane
BRL 8260B P9D000710.015 3/29/19 18:22 JLBmg/kg dry 0.00036Vinyl chloride
BRL 8260B P9D000710.022 3/29/19 18:22 JLBmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-03
Prism Sample ID: 9030455-03
Prism Work Order: 9030455
Time Collected: 03/28/19 13:25
Time Submitted: 03/28/19 17:18
General Chemistry Parameters
84.5 SM2540 G P9C059310.100 4/1/19 8:53 KBS% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0321,1’-Biphenyl
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0602,3,4,6-Tetrachlorophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0732,4,5-Trichlorophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0732,4,6-Trichlorophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0752,4-Dichlorophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0602,4-Dimethylphenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0542,4-Dinitrophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0472,4-Dinitrotoluene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0522,6-Dinitrotoluene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0562-Chloronaphthalene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0552-Chlorophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0622-Methylnaphthalene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0502-Methylphenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0702-Nitroaniline
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0712-Nitrophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0773,3’-Dichlorobenzidine
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0483/4-Methylphenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0673-Nitroaniline
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0584,6-Dinitro-2-methylphenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0674-Bromophenyl phenyl ether
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0554-Chloro-3-methylphenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0474-Chloroaniline
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0714-Nitroaniline
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.0604-Nitrophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.053Acenaphthene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.056Acenaphthylene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.065Acetophenone
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.063Anthracene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.060Atrazine
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.034Benzaldehyde
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.051Benzo(a)anthracene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.042Benzo(a)pyrene
0.046 8270D P9C058010.39 3/29/19 18:01 JMVJmg/kg dry 0.045Benzo(b)fluoranthene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.051Benzo(k)fluoranthene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.067bis(2-Chloroethoxy)methane
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.055Bis(2-Chloroethyl)ether
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.066Bis(2-chloroisopropyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-03
Prism Sample ID: 9030455-03
Prism Work Order: 9030455
Time Collected: 03/28/19 13:25
Time Submitted: 03/28/19 17:18
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.055Butyl benzyl phthalate
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.059Caprolactam
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.060Carbazole
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.049Chrysene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.047Dibenzo(a,h)anthracene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.059Dibenzofuran
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.054Diethyl phthalate
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.051Dimethyl phthalate
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.055Di-n-butyl phthalate
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.048Di-n-octyl phthalate
0.061 8270D P9C058010.39 3/29/19 18:01 JMVJmg/kg dry 0.050Fluoranthene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.056Fluorene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.062Hexachlorobenzene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.070Hexachlorobutadiene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.069Hexachlorocyclopentadiene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.065Hexachloroethane
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.053Isophorone
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.063Naphthalene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.055Nitrobenzene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.061N-Nitroso-di-n-propylamine
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.059N-Nitrosodiphenylamine
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.046Pentachlorophenol
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.051Phenanthrene
BRL 8270D P9C058010.39 3/29/19 18:01 JMVmg/kg dry 0.057Phenol
0.061 8270D P9C058010.39 3/29/19 18:01 JMVJmg/kg dry 0.051Pyrene
Surrogate Recovery Control Limits
37-13161 %2,4,6-Tribromophenol
47-13078 %2-Fluorobiphenyl
44-11769 %2-Fluorophenol
45-12166 %Nitrobenzene-d5
37-12769 %Phenol-d5
38-13580 %Terphenyl-d14
Total Metals
0.40 7196A P9D003010.47 4/2/19 11:00 BMSJmg/kg dry 0.12Hexavalent Chromium
0.29 7471B P9D000310.059 4/1/19 11:21 MMRmg/kg dry 0.020Mercury
4.2 6020B P9C0571101.2 3/29/19 16:26 JABmg/kg dry 0.39Arsenic
93 6020B P9C057110123/29/19 16:26 JABmg/kg dry 0.40Barium
BRL 6020B P9C0571100.59 3/29/19 16:26 JABmg/kg dry 0.11Cadmium
36 6020B P9C0571101.2 3/29/19 16:26 JABmg/kg dry 0.31Chromium
15 6020B P9C0571101.2 3/29/19 16:26 JABmg/kg dry 0.22Lead
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-03
Prism Sample ID: 9030455-03
Prism Work Order: 9030455
Time Collected: 03/28/19 13:25
Time Submitted: 03/28/19 17:18
1.3 6020B P9C0571101.2 3/29/19 16:26 JABmg/kg dry 0.32Selenium
BRL 6020B P9C0571100.59 3/29/19 16:26 JABmg/kg dry 0.14Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000471,1,1-Trichloroethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000651,1,2,2-Tetrachloroethane
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.000721,1,2-Trichloro-1,2,2-trifluoroethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000861,1,2-Trichloroethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000271,1-Dichloroethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000431,1-Dichloroethylene
0.024 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.000551,2,3-Trichlorobenzene
0.31 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.000721,2,4-Trichlorobenzene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000721,2-Dibromo-3-chloropropane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000391,2-Dibromoethane
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.000451,2-Dichlorobenzene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000581,2-Dichloroethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.000601,2-Dichloropropane
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.000641,3-Dichlorobenzene
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.000381,4-Dichlorobenzene
BRL 8260B P9D000710.19 3/29/19 17:22 JLBmg/kg dry 0.0201,4-Dioxane
0.027 8260B P9D000710.039 3/29/19 17:22 JLBJmg/kg dry 0.0024Acetone
BRL 8260B P9D000710.0058 3/29/19 17:22 JLBmg/kg dry 0.00056Benzene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00053Bromochloromethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00054Bromodichloromethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.0011Bromoform
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.0012Bromomethane
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00047Carbon disulfide
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00048Carbon Tetrachloride
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00051Chlorobenzene
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00081Chloroethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00070Chloroform
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00065Chloromethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00041cis-1,2-Dichloroethylene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00032cis-1,3-Dichloropropylene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00063Cyclohexane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00040Dibromochloromethane
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00044Dichlorodifluoromethane
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00037Ethylbenzene
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00057Isopropylbenzene (Cumene)
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00089m,p-Xylenes
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.0015Methyl Acetate
BRL 8260B P9D000710.097 3/29/19 17:22 JLBmg/kg dry 0.00087Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00082Methylcyclohexane
BRL 8260B P9D000710.039 3/29/19 17:22 JLBmg/kg dry 0.00087Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
04/11/2019
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Sample Matrix: Solid
Client Sample ID: SS-03
Prism Sample ID: 9030455-03
Prism Work Order: 9030455
Time Collected: 03/28/19 13:25
Time Submitted: 03/28/19 17:18
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00082Methyl Isobutyl Ketone
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00054Methylene Chloride
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00031Methyl-tert-Butyl Ether
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00040o-Xylene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00058Styrene
0.0083 8260B P9D000710.019 3/29/19 17:22 JLBJmg/kg dry 0.00046Tetrachloroethylene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00055Toluene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00058trans-1,2-Dichloroethylene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00051trans-1,3-Dichloropropylene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00063Trichloroethylene
BRL 8260B P9D000710.0097 3/29/19 17:22 JLBmg/kg dry 0.00062Trichlorofluoromethane
BRL 8260B P9D000710.019 3/29/19 17:22 JLBmg/kg dry 0.00047Vinyl chloride
BRL 8260B P9D000710.029 3/29/19 17:22 JLBmg/kg dry 0.0018Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9D0007 - 5035
Blank (P9D0007-BLK1)Prepared & Analyzed: 03/29/19
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wetBRL0.010
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2-Dibromo-3-chloropropane mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.010
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.010
1,4-Dichlorobenzene mg/kg wetBRL0.010
1,4-Dioxane mg/kg wetBRL0.10
Acetone mg/kg wetBRL0.020
Benzene mg/kg wetBRL0.0030
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon disulfide mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Cyclohexane mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.010
m,p-Xylenes mg/kg wetBRL0.010
Methyl Acetate mg/kg wetBRL0.0050
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methylcyclohexane mg/kg wetBRL0.0050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.010
Methylene Chloride mg/kg wet0.00247 0.010 J
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.010
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9D0007 - 5035
Blank (P9D0007-BLK1)Prepared & Analyzed: 03/29/19
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.3
ug/L 50.00 76-129Surrogate: Toluene-d8 9849.0
LCS (P9D0007-BS1)Prepared & Analyzed: 03/29/19
1,1,1-Trichloroethane mg/kg wet0.0478 0.0050 0.05000 67-13196
1,1,2,2-Tetrachloroethane mg/kg wet0.0467 0.0050 0.05000 56-12693
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0502 0.010 0.05000 70-130100
1,1,2-Trichloroethane mg/kg wet0.0470 0.0050 0.05000 70-13394
1,1-Dichloroethane mg/kg wet0.0482 0.0050 0.05000 74-12796
1,1-Dichloroethylene mg/kg wet0.0501 0.0050 0.05000 67-149100
1,2,3-Trichlorobenzene mg/kg wet0.0472 0.010 0.05000 68-13094
1,2,4-Trichlorobenzene mg/kg wet0.0466 0.010 0.05000 66-12593
1,2-Dibromo-3-chloropropane mg/kg wet0.0482 0.0050 0.05000 55-15796
1,2-Dibromoethane mg/kg wet0.0474 0.0050 0.05000 70-13295
1,2-Dichlorobenzene mg/kg wet0.0452 0.010 0.05000 72-12390
1,2-Dichloroethane mg/kg wet0.0455 0.0050 0.05000 68-12891
1,2-Dichloropropane mg/kg wet0.0483 0.0050 0.05000 73-13097
1,3-Dichlorobenzene mg/kg wet0.0453 0.010 0.05000 71-12091
1,4-Dichlorobenzene mg/kg wet0.0456 0.010 0.05000 71-12391
1,4-Dioxane mg/kg wet0.525 0.10 0.5000 70-130105
Acetone mg/kg wet0.137 0.020 0.1000 29-198137
Benzene mg/kg wet0.0478 0.0030 0.05000 74-12796
Bromochloromethane mg/kg wet0.0466 0.0050 0.05000 72-13493
Bromodichloromethane mg/kg wet0.0461 0.0050 0.05000 75-12292
Bromoform mg/kg wet0.0473 0.0050 0.05000 66-13595
Bromomethane mg/kg wet0.0471 0.010 0.05000 20-18094
Carbon disulfide mg/kg wet0.0461 0.010 0.05000 61-12992
Carbon Tetrachloride mg/kg wet0.0495 0.0050 0.05000 64-14399
Chlorobenzene mg/kg wet0.0462 0.0050 0.05000 74-11892
Chloroethane mg/kg wet0.0547 0.010 0.05000 33-149109
Chloroform mg/kg wet0.0461 0.0050 0.05000 73-12792
Chloromethane mg/kg wet0.0480 0.010 0.05000 45-14396
cis-1,2-Dichloroethylene mg/kg wet0.0477 0.0050 0.05000 76-13495
cis-1,3-Dichloropropylene mg/kg wet0.0486 0.0050 0.05000 71-12597
Cyclohexane mg/kg wet0.0510 0.0050 0.05000 70-130102
Dibromochloromethane mg/kg wet0.0472 0.0050 0.05000 73-12294
Dichlorodifluoromethane mg/kg wet0.0429 0.010 0.05000 26-14686
Ethylbenzene mg/kg wet0.0484 0.0050 0.05000 74-12897
Isopropylbenzene (Cumene)mg/kg wet0.0478 0.010 0.05000 68-12696
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9D0007 - 5035
LCS (P9D0007-BS1)Prepared & Analyzed: 03/29/19
m,p-Xylenes mg/kg wet0.0963 0.010 0.1000 75-12496
Methyl Acetate mg/kg wet0.0450 0.0050 0.05000 70-13090
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0534 0.050 0.05000 61-157107
Methylcyclohexane mg/kg wet0.0502 0.0050 0.05000 70-130100
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0599 0.020 0.05000 63-149120
Methyl Isobutyl Ketone mg/kg wet0.0472 0.010 0.05000 57-16294
Methylene Chloride mg/kg wet0.0468 0.010 0.05000 74-12994
Methyl-tert-Butyl Ether mg/kg wet0.0475 0.0050 0.05000 70-13095
o-Xylene mg/kg wet0.0484 0.0050 0.05000 74-12697
Styrene mg/kg wet0.0476 0.0050 0.05000 77-12195
Tetrachloroethylene mg/kg wet0.0491 0.010 0.05000 68-13098
Toluene mg/kg wet0.0485 0.0050 0.05000 71-12997
trans-1,2-Dichloroethylene mg/kg wet0.0479 0.0050 0.05000 73-13296
trans-1,3-Dichloropropylene mg/kg wet0.0494 0.0050 0.05000 68-12399
Trichloroethylene mg/kg wet0.0480 0.0050 0.05000 75-13396
Trichlorofluoromethane mg/kg wet0.0488 0.0050 0.05000 44-14698
Vinyl chloride mg/kg wet0.0458 0.010 0.05000 48-14792
Xylenes, total mg/kg wet0.145 0.015 0.1500 74-12696
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9547.6
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.7
LCS Dup (P9D0007-BSD1)Prepared & Analyzed: 03/29/19
1,1,1-Trichloroethane mg/kg wet0.0489 0.0050 0.05000 2067-13198 2
1,1,2,2-Tetrachloroethane mg/kg wet0.0481 0.0050 0.05000 2056-12696 3
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0501 0.010 0.05000 2070-130100 0.1
1,1,2-Trichloroethane mg/kg wet0.0500 0.0050 0.05000 2070-133100 6
1,1-Dichloroethane mg/kg wet0.0492 0.0050 0.05000 2074-12798 2
1,1-Dichloroethylene mg/kg wet0.0505 0.0050 0.05000 2067-149101 0.8
1,2,3-Trichlorobenzene mg/kg wet0.0485 0.010 0.05000 2068-13097 3
1,2,4-Trichlorobenzene mg/kg wet0.0482 0.010 0.05000 2066-12596 3
1,2-Dibromo-3-chloropropane mg/kg wet0.0499 0.0050 0.05000 2055-157100 3
1,2-Dibromoethane mg/kg wet0.0499 0.0050 0.05000 2070-132100 5
1,2-Dichlorobenzene mg/kg wet0.0465 0.010 0.05000 2072-12393 3
1,2-Dichloroethane mg/kg wet0.0471 0.0050 0.05000 2068-12894 4
1,2-Dichloropropane mg/kg wet0.0495 0.0050 0.05000 2073-13099 2
1,3-Dichlorobenzene mg/kg wet0.0467 0.010 0.05000 2071-12093 3
1,4-Dichlorobenzene mg/kg wet0.0464 0.010 0.05000 2071-12393 2
1,4-Dioxane mg/kg wet0.540 0.10 0.5000 2070-130108 3
Acetone mg/kg wet0.0875 0.020 0.1000 20 D29-19887 44
Benzene mg/kg wet0.0485 0.0030 0.05000 2074-12797 1
Bromochloromethane mg/kg wet0.0468 0.0050 0.05000 2072-13494 0.4
Bromodichloromethane mg/kg wet0.0478 0.0050 0.05000 2075-12296 4
Bromoform mg/kg wet0.0498 0.0050 0.05000 2066-135100 5
Bromomethane mg/kg wet0.0482 0.010 0.05000 2020-18096 2
Carbon disulfide mg/kg wet0.0467 0.010 0.05000 2061-12993 1
Carbon Tetrachloride mg/kg wet0.0487 0.0050 0.05000 2064-14397 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P9D0007 - 5035
LCS Dup (P9D0007-BSD1)Prepared & Analyzed: 03/29/19
Chlorobenzene mg/kg wet0.0486 0.0050 0.05000 2074-11897 5
Chloroethane mg/kg wet0.0563 0.010 0.05000 2033-149113 3
Chloroform mg/kg wet0.0477 0.0050 0.05000 2073-12795 3
Chloromethane mg/kg wet0.0496 0.010 0.05000 2045-14399 3
cis-1,2-Dichloroethylene mg/kg wet0.0482 0.0050 0.05000 2076-13496 1
cis-1,3-Dichloropropylene mg/kg wet0.0500 0.0050 0.05000 2071-125100 3
Cyclohexane mg/kg wet0.0518 0.0050 0.05000 2070-130104 1
Dibromochloromethane mg/kg wet0.0495 0.0050 0.05000 2073-12299 5
Dichlorodifluoromethane mg/kg wet0.0427 0.010 0.05000 2026-14685 0.5
Ethylbenzene mg/kg wet0.0499 0.0050 0.05000 2074-128100 3
Isopropylbenzene (Cumene)mg/kg wet0.0489 0.010 0.05000 2068-12698 2
m,p-Xylenes mg/kg wet0.0995 0.010 0.1000 2075-124100 3
Methyl Acetate mg/kg wet0.0477 0.0050 0.05000 2070-13095 6
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0505 0.050 0.05000 2061-157101 5
Methylcyclohexane mg/kg wet0.0510 0.0050 0.05000 2070-130102 2
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0490 0.020 0.05000 2063-14998 20
Methyl Isobutyl Ketone mg/kg wet0.0491 0.010 0.05000 2057-16298 4
Methylene Chloride mg/kg wet0.0473 0.010 0.05000 2074-12995 1
Methyl-tert-Butyl Ether mg/kg wet0.0480 0.0050 0.05000 2070-13096 1
o-Xylene mg/kg wet0.0499 0.0050 0.05000 2074-126100 3
Styrene mg/kg wet0.0492 0.0050 0.05000 2077-12198 3
Tetrachloroethylene mg/kg wet0.0498 0.010 0.05000 2068-130100 2
Toluene mg/kg wet0.0495 0.0050 0.05000 2071-12999 2
trans-1,2-Dichloroethylene mg/kg wet0.0485 0.0050 0.05000 2073-13297 1
trans-1,3-Dichloropropylene mg/kg wet0.0512 0.0050 0.05000 2068-123102 4
Trichloroethylene mg/kg wet0.0486 0.0050 0.05000 2075-13397 1
Trichlorofluoromethane mg/kg wet0.0495 0.0050 0.05000 2044-14699 1
Vinyl chloride mg/kg wet0.0467 0.010 0.05000 2048-14793 2
Xylenes, total mg/kg wet0.149 0.015 0.1500 2074-126100 3
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.6
ug/L 50.00 76-129Surrogate: Toluene-d8 10150.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9C0580 - 3546
Blank (P9C0580-BLK1)Prepared & Analyzed: 03/29/19
1,1’-Biphenyl mg/kg wetBRL0.33
2,3,4,6-Tetrachlorophenol mg/kg wetBRL0.33
2,4,5-Trichlorophenol mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitroaniline mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
3-Nitroaniline mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitroaniline mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Acetophenone mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Atrazine mg/kg wetBRL0.33
Benzaldehyde mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Caprolactam mg/kg wetBRL0.33
Carbazole mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9C0580 - 3546
Blank (P9C0580-BLK1)Prepared & Analyzed: 03/29/19
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 1023.41
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 1121.86
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 1103.65
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 1021.70
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 1073.57
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 1171.96
LCS (P9C0580-BS1)Prepared & Analyzed: 03/29/19
2,4,5-Trichlorophenol mg/kg wet1.47 0.33 1.667 41-12488
2,4,6-Trichlorophenol mg/kg wet1.64 0.33 1.667 39-12699
2,4-Dichlorophenol mg/kg wet1.41 0.33 1.667 40-12285
2,4-Dimethylphenol mg/kg wet1.81 0.33 1.667 30-127108
2,4-Dinitrophenol mg/kg wet0.965 0.33 1.667 27-12958
2,4-Dinitrotoluene mg/kg wet1.64 0.33 1.667 48-12699
2,6-Dinitrotoluene mg/kg wet1.67 0.33 1.667 46-124100
2-Chloronaphthalene mg/kg wet1.61 0.33 1.667 41-11497
2-Chlorophenol mg/kg wet1.59 0.33 1.667 34-12195
2-Methylnaphthalene mg/kg wet1.38 0.33 1.667 38-12283
2-Methylphenol mg/kg wet1.68 0.33 1.667 32-122101
2-Nitroaniline mg/kg wet1.60 0.33 1.667 44-12796
2-Nitrophenol mg/kg wet1.30 0.33 1.667 36-12378
3,3’-Dichlorobenzidine mg/kg wet1.65 0.33 1.667 22-12199
3/4-Methylphenol mg/kg wet1.50 0.33 1.667 34-11990
3-Nitroaniline mg/kg wet1.63 0.33 1.667 33-11998
4,6-Dinitro-2-methylphenol mg/kg wet1.30 0.33 1.667 29-13278
4-Bromophenyl phenyl ether mg/kg wet1.60 0.33 1.667 46-12496
4-Chloro-3-methylphenol mg/kg wet1.46 0.33 1.667 45-12287
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9C0580 - 3546
LCS (P9C0580-BS1)Prepared & Analyzed: 03/29/19
4-Chloroaniline mg/kg wet1.32 0.33 1.667 17-10679
4-Chlorophenyl phenyl ether mg/kg wet1.67 0.33 1.667 45-121100
4-Nitroaniline mg/kg wet1.72 0.33 1.667 63-147103
4-Nitrophenol mg/kg wet1.64 0.33 1.667 30-13299
Acenaphthene mg/kg wet1.68 0.33 1.667 40-123101
Acenaphthylene mg/kg wet1.68 0.33 1.667 32-132101
Acetophenone mg/kg wet1.35 0.33 1.667 33-11581
Anthracene mg/kg wet1.79 0.33 1.667 47-123108
Benzo(a)anthracene mg/kg wet1.67 0.33 1.667 49-126100
Benzo(a)pyrene mg/kg wet1.70 0.33 1.667 45-129102
Benzo(b)fluoranthene mg/kg wet1.70 0.33 1.667 45-132102
Benzo(g,h,i)perylene mg/kg wet1.70 0.33 1.667 43-134102
Benzo(k)fluoranthene mg/kg wet1.82 0.33 1.667 47-132109
bis(2-Chloroethoxy)methane mg/kg wet1.39 0.33 1.667 36-12183
Bis(2-Chloroethyl)ether mg/kg wet1.32 0.33 1.667 31-12079
Bis(2-chloroisopropyl)ether mg/kg wet1.48 0.33 1.667 33-13189
Bis(2-Ethylhexyl)phthalate mg/kg wet1.73 0.33 1.667 51-133104
Butyl benzyl phthalate mg/kg wet1.67 0.33 1.667 48-132100
Carbazole mg/kg wet1.83 0.33 1.667 50-123110
Chrysene mg/kg wet1.71 0.33 1.667 50-124103
Dibenzo(a,h)anthracene mg/kg wet1.72 0.33 1.667 45-134103
Dibenzofuran mg/kg wet1.62 0.33 1.667 44-12097
Diethyl phthalate mg/kg wet1.73 0.33 1.667 50-124104
Dimethyl phthalate mg/kg wet1.69 0.33 1.667 48-124101
Di-n-butyl phthalate mg/kg wet1.74 0.33 1.667 51-128104
Di-n-octyl phthalate mg/kg wet1.72 0.33 1.667 45-140103
Fluoranthene mg/kg wet1.73 0.33 1.667 50-127104
Fluorene mg/kg wet1.76 0.33 1.667 43-125106
Hexachlorobenzene mg/kg wet1.55 0.33 1.667 45-12293
Hexachlorobutadiene mg/kg wet1.34 0.33 1.667 32-12380
Hexachlorocyclopentadiene mg/kg wet1.44 0.33 1.667 32-11787
Hexachloroethane mg/kg wet1.32 0.33 1.667 28-11779
Indeno(1,2,3-cd)pyrene mg/kg wet2.09 0.33 1.667 45-133125
Isophorone mg/kg wet1.34 0.33 1.667 30-12281
Naphthalene mg/kg wet1.36 0.33 1.667 35-12382
Nitrobenzene mg/kg wet1.33 0.33 1.667 34-12280
N-Nitroso-di-n-propylamine mg/kg wet1.44 0.33 1.667 36-12086
N-Nitrosodiphenylamine mg/kg wet1.95 0.33 1.667 38-127117
Pentachlorophenol mg/kg wet1.79 0.33 1.667 25-133108
Phenanthrene mg/kg wet1.78 0.33 1.667 50-121107
Phenol mg/kg wet1.58 0.33 1.667 34-12195
Pyrene mg/kg wet1.73 0.33 1.667 47-127104
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 993.31
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 981.63
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 963.21
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 791.32
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9C0580 - 3546
LCS (P9C0580-BS1)Prepared & Analyzed: 03/29/19
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 943.13
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 1011.68
LCS (P9C0580-BS2)Prepared & Analyzed: 03/29/19
1,1’-Biphenyl mg/kg wet1.43 0.33 1.667 40-11786
2,3,4,6-Tetrachlorophenol mg/kg wet1.64 0.33 1.667 44-12598
Atrazine mg/kg wet1.72 0.33 1.667 47-127103
Benzaldehyde mg/kg wet1.02 0.33 1.667 35-11561
Caprolactam mg/kg wet1.25 0.33 1.667 46-11775
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 973.24
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 1031.71
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 1043.45
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 951.59
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 1003.34
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 1061.77
LCS Dup (P9C0580-BSD1)Prepared & Analyzed: 03/29/19
2,4,5-Trichlorophenol mg/kg wet1.47 0.33 1.667 2041-12488 0.1
2,4,6-Trichlorophenol mg/kg wet1.64 0.33 1.667 2039-12698 0.1
2,4-Dichlorophenol mg/kg wet1.44 0.33 1.667 2040-12286 2
2,4-Dimethylphenol mg/kg wet1.81 0.33 1.667 2030-127109 0.3
2,4-Dinitrophenol mg/kg wet0.968 0.33 1.667 2027-12958 0.3
2,4-Dinitrotoluene mg/kg wet1.63 0.33 1.667 2048-12698 0.5
2,6-Dinitrotoluene mg/kg wet1.67 0.33 1.667 2046-124100 0.2
2-Chloronaphthalene mg/kg wet1.63 0.33 1.667 2041-11498 1
2-Chlorophenol mg/kg wet1.63 0.33 1.667 2034-12198 2
2-Methylnaphthalene mg/kg wet1.41 0.33 1.667 2038-12285 2
2-Methylphenol mg/kg wet1.69 0.33 1.667 2032-122101 0.5
2-Nitroaniline mg/kg wet1.59 0.33 1.667 2044-12796 0.7
2-Nitrophenol mg/kg wet1.32 0.33 1.667 2036-12379 2
3,3’-Dichlorobenzidine mg/kg wet1.65 0.33 1.667 2022-12199 0.2
3/4-Methylphenol mg/kg wet1.48 0.33 1.667 2034-11989 1
3-Nitroaniline mg/kg wet1.58 0.33 1.667 2033-11995 3
4,6-Dinitro-2-methylphenol mg/kg wet1.31 0.33 1.667 2029-13278 0.1
4-Bromophenyl phenyl ether mg/kg wet1.60 0.33 1.667 2046-12496 0.2
4-Chloro-3-methylphenol mg/kg wet1.47 0.33 1.667 2045-12288 0.8
4-Chloroaniline mg/kg wet1.34 0.33 1.667 2017-10681 2
4-Chlorophenyl phenyl ether mg/kg wet1.65 0.33 1.667 2045-12199 1
4-Nitroaniline mg/kg wet1.69 0.33 1.667 2063-147102 2
4-Nitrophenol mg/kg wet1.65 0.33 1.667 2030-13299 0.6
Acenaphthene mg/kg wet1.68 0.33 1.667 2040-123101 0.3
Acenaphthylene mg/kg wet1.69 0.33 1.667 2032-132102 0.8
Acetophenone mg/kg wet1.34 0.33 1.667 2033-11581 0.4
Anthracene mg/kg wet1.79 0.33 1.667 2047-123107 0.4
Benzo(a)anthracene mg/kg wet1.70 0.33 1.667 2049-126102 2
Benzo(a)pyrene mg/kg wet1.73 0.33 1.667 2045-129104 2
Benzo(b)fluoranthene mg/kg wet1.71 0.33 1.667 2045-132103 0.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9C0580 - 3546
LCS Dup (P9C0580-BSD1)Prepared & Analyzed: 03/29/19
Benzo(g,h,i)perylene mg/kg wet1.72 0.33 1.667 2043-134103 0.7
Benzo(k)fluoranthene mg/kg wet1.82 0.33 1.667 2047-132109 0.1
bis(2-Chloroethoxy)methane mg/kg wet1.41 0.33 1.667 2036-12185 1
Bis(2-Chloroethyl)ether mg/kg wet1.53 0.33 1.667 2031-12092 15
Bis(2-chloroisopropyl)ether mg/kg wet1.44 0.33 1.667 2033-13187 2
Bis(2-Ethylhexyl)phthalate mg/kg wet1.70 0.33 1.667 2051-133102 2
Butyl benzyl phthalate mg/kg wet1.66 0.33 1.667 2048-132100 0.2
Carbazole mg/kg wet1.80 0.33 1.667 2050-123108 2
Chrysene mg/kg wet1.74 0.33 1.667 2050-124104 2
Dibenzo(a,h)anthracene mg/kg wet1.72 0.33 1.667 2045-134103 0.1
Dibenzofuran mg/kg wet1.63 0.33 1.667 2044-12098 0.3
Diethyl phthalate mg/kg wet1.68 0.33 1.667 2050-124101 3
Dimethyl phthalate mg/kg wet1.67 0.33 1.667 2048-124100 0.7
Di-n-butyl phthalate mg/kg wet1.72 0.33 1.667 2051-128103 1
Di-n-octyl phthalate mg/kg wet1.72 0.33 1.667 2045-140103 0.1
Fluoranthene mg/kg wet1.73 0.33 1.667 2050-127104 0.3
Fluorene mg/kg wet1.75 0.33 1.667 2043-125105 0.9
Hexachlorobenzene mg/kg wet1.55 0.33 1.667 2045-12293 0.1
Hexachlorobutadiene mg/kg wet1.39 0.33 1.667 2032-12383 4
Hexachlorocyclopentadiene mg/kg wet1.44 0.33 1.667 2032-11787 0.1
Hexachloroethane mg/kg wet1.32 0.33 1.667 2028-11779 0.5
Indeno(1,2,3-cd)pyrene mg/kg wet2.10 0.33 1.667 2045-133126 0.5
Isophorone mg/kg wet1.36 0.33 1.667 2030-12282 1
Naphthalene mg/kg wet1.39 0.33 1.667 2035-12384 2
Nitrobenzene mg/kg wet1.35 0.33 1.667 2034-12281 1
N-Nitroso-di-n-propylamine mg/kg wet1.49 0.33 1.667 2036-12090 4
N-Nitrosodiphenylamine mg/kg wet1.95 0.33 1.667 2038-127117 0.2
Pentachlorophenol mg/kg wet1.74 0.33 1.667 2025-133104 3
Phenanthrene mg/kg wet1.77 0.33 1.667 2050-121106 0.4
Phenol mg/kg wet1.59 0.33 1.667 2034-12196 1
Pyrene mg/kg wet1.75 0.33 1.667 2047-127105 1
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 993.30
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 981.64
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 963.21
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 791.32
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 933.10
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 1001.66
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P9C0580 - 3546
LCS Dup (P9C0580-BSD2)Prepared & Analyzed: 03/29/19
1,1’-Biphenyl mg/kg wet1.27 0.33 1.667 2040-11776 12
2,3,4,6-Tetrachlorophenol mg/kg wet1.51 0.33 1.667 2044-12591 8
Atrazine mg/kg wet1.52 0.33 1.667 2047-12791 12
Benzaldehyde mg/kg wet0.897 0.33 1.667 2035-11554 13
Caprolactam mg/kg wet1.13 0.33 1.667 2046-11768 9
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 862.88
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 891.49
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 872.89
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 801.33
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 872.88
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 941.56
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P9C0571 - 3050B
Blank (P9C0571-BLK1)Prepared & Analyzed: 03/29/19
Arsenic mg/kg wetBRL1.0
Barium mg/kg wetBRL10
Cadmium mg/kg wetBRL0.50
Chromium mg/kg wetBRL1.0
Lead mg/kg wetBRL1.0
Selenium mg/kg wetBRL1.0
Silver mg/kg wetBRL0.50
LCS (P9C0571-BS1)Prepared & Analyzed: 03/29/19
Arsenic mg/kg wet12.4 1.0 12.50 80-12099
Barium mg/kg wet12.1 10 12.50 80-12097
Cadmium mg/kg wet12.6 0.50 12.50 80-120101
Chromium mg/kg wet13.7 1.0 12.50 80-120110
Lead mg/kg wet12.9 1.0 12.50 80-120103
Selenium mg/kg wet12.3 1.0 12.50 80-12099
Silver mg/kg wet5.01 0.50 5.000 80-120100
Matrix Spike (P9C0571-MS1)Prepared & Analyzed: 03/29/19 Source: 9030455-01
Arsenic mg/kg dry12.8 1.1 14.27 3.06 M75-12569
Barium mg/kg dry87.1 11 14.27 77.3 MC75-12568
Cadmium mg/kg dry12.0 0.57 14.27 BRL 75-12584
Chromium mg/kg dry44.1 1.1 14.27 34.2 M75-12569
Lead mg/kg dry26.9 1.1 14.27 15.2 75-12582
Selenium mg/kg dry11.7 1.1 14.27 1.15 M75-12574
Silver mg/kg dry4.72 0.57 5.708 BRL 75-12583
Matrix Spike Dup (P9C0571-MSD1)Prepared & Analyzed: 03/29/19 Source: 9030455-01
Arsenic mg/kg dry14.8 1.1 14.27 3.06 2075-12582 14
Barium mg/kg dry10411 14.27 77.3 20 MC75-125187 18
Cadmium mg/kg dry13.9 0.57 14.27 BRL 2075-12597 14
Chromium mg/kg dry46.9 1.1 14.27 34.2 2075-12589 6
Lead mg/kg dry28.9 1.1 14.27 15.2 2075-12596 7
Selenium mg/kg dry13.3 1.1 14.27 1.15 2075-12585 13
Silver mg/kg dry5.44 0.57 5.708 BRL 2075-12595 14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P9C0571 - 3050B
Post Spike (P9C0571-PS1)Prepared & Analyzed: 03/29/19 Source: 9030455-01
Arsenic ug/L109 100.0 10.7 80-12098
Barium ug/L374 100.0 271 80-120103
Cadmium ug/L99.8 100.0 0.283 80-120100
Chromium ug/L220 100.0 120 80-120100
Lead ug/L154 100.0 53.2 80-120101
Selenium ug/L102 100.0 4.01 80-12098
Silver ug/L99.8 100.0 0.102 80-120100
Batch P9D0003 - 7471B
Blank (P9D0003-BLK1)Prepared & Analyzed: 04/01/19
Mercury mg/kg wetBRL0.050
LCS (P9D0003-BS1)Prepared & Analyzed: 04/01/19
Mercury mg/kg wet0.433 0.050 0.4167 80-120104
Matrix Spike (P9D0003-MS1)Prepared & Analyzed: 04/01/19 Source: 9030455-01
Mercury mg/kg dry0.783 0.057 0.4757 0.250 80-120112
Matrix Spike Dup (P9D0003-MSD1)Prepared & Analyzed: 04/01/19 Source: 9030455-01
Mercury mg/kg dry0.604 0.057 0.4757 0.250 20 D, MI80-12074 26
Batch P9D0030 - 3060A
Blank (P9D0030-BLK1)Prepared & Analyzed: 04/02/19
Hexavalent Chromium mg/kg wetBRL0.40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P9D0030 - 3060A
LCS (P9D0030-BS1)Prepared & Analyzed: 04/02/19
Hexavalent Chromium mg/kg wet15.5 0.40 16.00 80-12097
Matrix Spike (P9D0030-MS1)Prepared & Analyzed: 04/02/19 Source: 9030455-01
Hexavalent Chromium mg/kg dry17.9 0.46 18.27 0.418 60-11996
Matrix Spike Dup (P9D0030-MSD1)Prepared & Analyzed: 04/02/19 Source: 9030455-01
Hexavalent Chromium mg/kg dry18.9 0.46 18.27 0.418 2060-119101 6
Post Spike (P9D0030-PS1)Prepared & Analyzed: 04/02/19 Source: 9030455-01
Hexavalent Chromium mg/kg0.399 0.4000 0.00915 85-11598
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
4/11/19
Level II QC Report
2923 South Tryon St. Ste 100
Project: RPH-001Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Brett Lawrence
Prism Work Order: 9030455
Time Submitted: 3/28/2019 5:18:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P9C0593 - Solids, Dry Weight
Duplicate (P9C0593-DUP1)Prepared: 03/29/19 Analyzed: 04/01/19 Source: 9030455-02
% Solids % by Weight83.1 0.100 83.1 200.08
Duplicate (P9C0593-DUP2)Prepared: 03/29/19 Analyzed: 04/01/19 Source: 9030455-07
% Solids % by Weight79.1 0.100 82.4 204
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P9C05939030455-01 03/29/19 16:393030gg
P9C05939030455-02 03/29/19 16:393030gg
P9C05939030455-03 03/29/19 16:393030gg
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P9C05809030455-01 03/29/19 11:4530.12 1g mL
P9C05809030455-02 03/29/19 11:4530.02 1g mL
P9C05809030455-03 03/29/19 11:4530.14 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P9C05719030455-01 03/29/19 8:50250gmL
P9C05719030455-02 03/29/19 8:50250gmL
P9C05719030455-03 03/29/19 8:50250gmL
Prep Method: 3060A
Lab Number Batch Date/TimeInitialFinal
P9D00309030455-01 04/02/19 8:102.5 100g mL
P9D00309030455-02 04/02/19 8:102.5 100g mL
P9D00309030455-03 04/02/19 8:102.5 100g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P9D00039030455-01 04/01/19 8:250.6 50g mL
P9D00039030455-02 04/01/19 8:250.6 50g mL
P9D00039030455-03 04/01/19 8:250.6 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P9D00079030455-01 03/29/19 9:595.05 5g mL
P9D00079030455-02 03/29/19 9:594.1 5g mL
P9D00079030455-03 03/29/19 9:593.06 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
WORK ORDER
9030455
Printed: 04/11/2019 11:47 am
RPH-001Project:
Project Number:
Project Manager:Angela D. Overcash
449 Springbrook Road
Charlotte, NC 28217
Phone: [phone]
www.prismlabs.com
Hart & Hickman (Charlotte)
Accounts Payable
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Phone: [phone]
Fax: [phone]
Hart & Hickman (Charlotte)
Brett Lawrence
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Phone: [phone]
Fax: [phone]
Report To: Invoice To:
Logged In By:Talon Yelton
Samples Received at:4.6C
PROPER PRESERVATIVES indicated?
Sample INTACT upon arrival?
Received ON WET ICE?
Received WITHIN HOLDING TIMES?
Yes
Yes
Yes
Yes
VOLATILES recd W/OUT HEADSPACE?
PROPER CONTAINERS used?
No
Yes
Date Due:04/02/2019 (2 day TAT)
Cooler Data
Received By:Date Received:Talon Yelton03/28/2019 05:18 PM
Date Logged In:03/28/2019 05:24 PM
Analysis Due TAT Expires Comments
9030455-01 SS-01 [Solid] Sampled 3/28/2019 12:55:00PM
2 04/11/2019 12:5504/02/2019 17:008260 (TCL)
2 04/11/2019 12:5504/02/2019 17:008270 (TCL - 3546)
2 09/24/2019 12:5504/02/2019 17:00Arsenic by ICP/MS 6020
2 09/24/2019 12:5504/02/2019 17:00Barium by ICP/MS 6020
2 09/24/2019 12:5504/02/2019 17:00Cadmium by ICP/MS 6020
2 09/24/2019 12:5504/02/2019 17:00Chromium by ICP/MS 6020
2 04/27/2019 12:5504/02/2019 17:00Hexavalent Chromium
2 09/24/2019 12:5504/02/2019 17:00Lead by ICP/MS 6020
2 04/25/2019 12:5504/02/2019 17:00Mercury 7470/7471
2 09/24/2019 12:5504/02/2019 17:00RCRA Metals (6020 + Hg)
2 09/24/2019 12:5504/02/2019 17:00Selenium by ICP/MS 6020
2 09/24/2019 12:5504/02/2019 17:00Silver by ICP/MS 6020
2 04/11/2019 12:5504/02/2019 17:00Solids, Dry Weight
9030455-02 SS-02 [Solid] Sampled 3/28/2019 1:10:00PM
2 04/11/2019 13:1004/02/2019 17:008260 (TCL)
2 04/11/2019 13:1004/02/2019 17:008270 (TCL - 3546)
2 09/24/2019 13:1004/02/2019 17:00Arsenic by ICP/MS 6020
2 09/24/2019 13:1004/02/2019 17:00Barium by ICP/MS 6020
2 09/24/2019 13:1004/02/2019 17:00Cadmium by ICP/MS 6020
2 09/24/2019 13:1004/02/2019 17:00Chromium by ICP/MS 6020
2 04/27/2019 13:1004/02/2019 17:00Hexavalent Chromium
2 09/24/2019 13:1004/02/2019 17:00Lead by ICP/MS 6020
2 04/25/2019 13:1004/02/2019 17:00Mercury 7470/7471
2 09/24/2019 13:1004/02/2019 17:00RCRA Metals (6020 + Hg)
2 09/24/2019 13:1004/02/2019 17:00Selenium by ICP/MS 6020
2 09/24/2019 13:1004/02/2019 17:00Silver by ICP/MS 6020
2 04/11/2019 13:1004/02/2019 17:00Solids, Dry Weight
WORK ORDER
9030455
Printed: 04/11/2019 11:47 am
RPH-001Project:
Project Number:
Project Manager:Angela D. Overcash
(Continued)
449 Springbrook Road
Charlotte, NC 28217
Phone: [phone]
www.prismlabs.com
Analysis Due TAT Expires Comments
9030455-03 SS-03 [Solid] Sampled 3/28/2019 1:25:00PM
2 04/11/2019 13:2504/02/2019 17:008260 (TCL)
2 04/11/2019 13:2504/02/2019 17:008270 (TCL - 3546)
2 09/24/2019 13:2504/02/2019 17:00Arsenic by ICP/MS 6020
2 09/24/2019 13:2504/02/2019 17:00Barium by ICP/MS 6020
2 09/24/2019 13:2504/02/2019 17:00Cadmium by ICP/MS 6020
2 09/24/2019 13:2504/02/2019 17:00Chromium by ICP/MS 6020
2 04/27/2019 13:2504/02/2019 17:00Hexavalent Chromium
2 09/24/2019 13:2504/02/2019 17:00Lead by ICP/MS 6020
2 04/25/2019 13:2504/02/2019 17:00Mercury 7470/7471
2 09/24/2019 13:2504/02/2019 17:00RCRA Metals (6020 + Hg)
2 09/24/2019 13:2504/02/2019 17:00Selenium by ICP/MS 6020
2 09/24/2019 13:2504/02/2019 17:00Silver by ICP/MS 6020
2 04/11/2019 13:2504/02/2019 17:00Solids, Dry Weight
9030455-04 BKG-01 River Rd [Solid] Sampled 3/28/2019 1:55:00PM
2 09/24/2019 13:5504/02/2019 17:00Arsenic by ICP/MS 6020
2 09/24/2019 13:5504/02/2019 17:00Barium by ICP/MS 6020
2 09/24/2019 13:5504/02/2019 17:00Cadmium by ICP/MS 6020
2 09/24/2019 13:5504/02/2019 17:00Chromium by ICP/MS 6020
2 04/27/2019 13:5504/02/2019 17:00Hexavalent Chromium
2 09/24/2019 13:5504/02/2019 17:00Lead by ICP/MS 6020
2 04/25/2019 13:5504/02/2019 17:00Mercury 7470/7471
2 09/24/2019 13:5504/02/2019 17:00RCRA Metals (6020 + Hg)
2 09/24/2019 13:5504/02/2019 17:00Selenium by ICP/MS 6020
2 09/24/2019 13:5504/02/2019 17:00Silver by ICP/MS 6020
2 04/11/2019 13:5504/02/2019 17:00Solids, Dry Weight
9030455-05 BKG-02 River Rd [Solid] Sampled 3/28/2019 2:05:00PM
2 09/24/2019 14:0504/02/2019 17:00Arsenic by ICP/MS 6020
2 09/24/2019 14:0504/02/2019 17:00Barium by ICP/MS 6020
2 09/24/2019 14:0504/02/2019 17:00Cadmium by ICP/MS 6020
2 09/24/2019 14:0504/02/2019 17:00Chromium by ICP/MS 6020
2 04/27/2019 14:0504/02/2019 17:00Hexavalent Chromium
2 09/24/2019 14:0504/02/2019 17:00Lead by ICP/MS 6020
2 04/25/2019 14:0504/02/2019 17:00Mercury 7470/7471
2 09/24/2019 14:0504/02/2019 17:00RCRA Metals (6020 + Hg)
2 09/24/2019 14:0504/02/2019 17:00Selenium by ICP/MS 6020
2 09/24/2019 14:0504/02/2019 17:00Silver by ICP/MS 6020
2 04/11/2019 14:0504/02/2019 17:00Solids, Dry Weight
9030455-06 BKG-01 Quarry [Solid] Sampled 3/28/2019 2:45:00PM
2 09/24/2019 14:4504/02/2019 17:00Arsenic by ICP/MS 6020
2 09/24/2019 14:4504/02/2019 17:00Barium by ICP/MS 6020
2 09/24/2019 14:4504/02/2019 17:00Cadmium by ICP/MS 6020
2 09/24/2019 14:4504/02/2019 17:00Chromium by ICP/MS 6020
2 04/27/2019 14:4504/02/2019 17:00Hexavalent Chromium
2 09/24/2019 14:4504/02/2019 17:00Lead by ICP/MS 6020
2 04/25/2019 14:4504/02/2019 17:00Mercury 7470/7471
2 09/24/2019 14:4504/02/2019 17:00RCRA Metals (6020 + Hg)
2 09/24/2019 14:4504/02/2019 17:00Selenium by ICP/MS 6020
2 09/24/2019 14:4504/02/2019 17:00Silver by ICP/MS 6020
2 04/11/2019 14:4504/02/2019 17:00Solids, Dry Weight
WORK ORDER
9030455
Printed: 04/11/2019 11:47 am
RPH-001Project:
Project Number:
Project Manager:Angela D. Overcash
(Continued)
449 Springbrook Road
Charlotte, NC 28217
Phone: [phone]
www.prismlabs.com
Analysis Due TAT Expires Comments
9030455-07 BKG-02 Quarry [Solid] Sampled 3/28/2019 2:55:00PM
2 09/24/2019 14:5504/02/2019 17:00Arsenic by ICP/MS 6020
2 09/24/2019 14:5504/02/2019 17:00Barium by ICP/MS 6020
2 09/24/2019 14:5504/02/2019 17:00Cadmium by ICP/MS 6020
2 09/24/2019 14:5504/02/2019 17:00Chromium by ICP/MS 6020
2 04/27/2019 14:5504/02/2019 17:00Hexavalent Chromium
2 09/24/2019 14:5504/02/2019 17:00Lead by ICP/MS 6020
2 04/25/2019 14:5504/02/2019 17:00Mercury 7470/7471
2 09/24/2019 14:5504/02/2019 17:00RCRA Metals (6020 + Hg)
2 09/24/2019 14:5504/02/2019 17:00Selenium by ICP/MS 6020
2 09/24/2019 14:5504/02/2019 17:00Silver by ICP/MS 6020
2 04/11/2019 14:5504/02/2019 17:00Solids, Dry Weight
RCRA Metals (6020 + Hg)
Silver by ICP/MS 6020 Selenium by ICP/MS 6020 Mercury 7470/7471 Lead by ICP/MS 6020 Chromium by ICP/MS 6020
Cadmium by ICP/MS 6020 Barium by ICP/MS 6020 Arsenic by ICP/MS 6020