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HomeMy WebLinkAboutMO-88513_91340_CA_MRP_04012019_1st 2019 Semiannual ReportAPEX April 1, 2019 Ms. Trudy Beverly Hydrogeologist LIST Section — Corrective Action Branch Division of Waste Management — Mooresville Regional Office North Carolina Department of Environmental Quality 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 RE: Semiannual Groundwater Monitoring Report - Kannapolis Booster Station Colonial Pipeline Company, Concord, North Carolina Incident Number: 14414 & 91340 Dear Ms. Beverly: Apex Companies, LLC (Apex; dba Apex Engineering, P.C.) is pleased to submit the September 2018 — February 2019 Semiannual Groundwater Monitoring Report for the Colonial Pipeline Company Kannapolis Booster Station. Should you have any questions concerning this, please do not hesitate to contact the undersigned at 704-799-6390. Sincerely, Apex Companies, LLC Prepared By: Andrew Street, CHMM Senior Project Manager Enclosure cc: John Culbreath, Colonial Pipeline Company Jeff Morrison, Colonial Pipeline Company Apex Companies, LLC Reviewed By: Eric Wysong, P.G. Project Manager NC Geology License No. 2581 Apex Companies, LLC • 10610 Metromont Parkway, Suite 206 • Charlotte, NC 28269 • T 704.799.6390 • F 704.799.6395 apexcos.00m Prepared for: Pipeline Company PO Box 87 Paw Creek, North Carolina 28130 m Semiannual Groundwater Monitoring Report Kannapolis Booster Station Incident Number 14414 & 91340 September 2018 — February 2019 A APEX 10610 Metromont Parkway, Suite 206 Charlotte NC 28269 Prepared by: JZf9 wl� Andrew Street, CHMM Senior Project Manager April 1, 2019 •r` Q-,.: AGE N SEO.: (> Reviewed by: 2 SEAL , J 2581 U arc J. yt Eric Wysong, P.G. �'0414" `a« Project Manager NC Geology License No. 2581 Apex Companies, LLC • 10610 Metromont Parkway, Suite 206 • Chadotle, NC 28269 T 704.799.6390 - F 704.799.6395 apexcos.cwm t=1 Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page i TABLE OF CONTENTS 1.0 INTRODUCTION....................................................................................................................................1 2.0 PROJECT BACKGROUND..................................................................................................................1 2.1 Historic Site Impacts................................................................................................................. 1 2.2 Recent Site Impacts.................................................................................................................. 2 3.0 FIELD ACTIVITIES................................................................................................................................ 3 3.1 Groundwater Gauging.............................................................................................................. 3 3.2 Groundwater Sampling and Analysis....................................................................................... 3 4.0 FINDINGS...............................................................................................................................................4 4.1 Well Gauging Results and Groundwater Flow........................................................................ 4 4.2 Groundwater Analytical Results............................................................................................... 4 5.0 REMEDIATION SYSTEM PERFORMANCE........................................................................................ 6 5.1 Air Sparge Trench Remediation System................................................................................. 6 5.2 Bio-Sparge and Bio-Venting Systems..................................................................................... 6 6.0 CONCLUSIONS AND RECOMMENDATIONS.................................................................................... 6 Tables Table 1 Well Sampling and Analysis Program Table 2 Groundwater Elevation Summary Table 3 Recovery Well Gauging Data Table 4 Groundwater Analytical Data Figures Figure 1 Site Location Map Figure 2 Site Plan Figure 3 Recovery Well Locations — February 15, 2019 Figure 4 Groundwater Potentiometric Surface Map — Surficial Saprolite Unit — February 15, 2019 Figure 5 Benzene Isoconcentration Map — February 15, 2019 Appendices Appendix A Groundwater Sampling Field Logs Appendix B Laboratory Analytical Reports Appendix C Concentration Time Trend Series Graph — MW-13 APEX Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page 1 1.0 INTRODUCTION This report summarizes the semiannual groundwater monitoring activities performed at the Colonial Pipeline Company (CPC) Kannapolis Booster Station (the Site) located at 9301 Mooresville Road in Concord, North Carolina (Figure 1) from September 2018 through February 2019. This report also describes the remediation systems operations performed during the reporting period in accordance with the Corrective Action Plans (CAPs) for the Site approved by the North Carolina Department of Environmental Quality (NCDEQ). Apex Companies, LLC (Apex; dba Apex Engineering, P.C.) prepared this Semiannual Groundwater Monitoring Report on behalf of CPC for submittal to NCDEQ. 2.0 PROJECT BACKGROUND The facility consists of a control building, a switch gear building, eight large electric booster pumps, a 40-inch diameter pipeline for transporting gasoline products (Line 1), a 36-inch diameter pipeline for transporting kerosene, diesel fuel, and other fuel oil products (Line 2), and two 21,000-gallon above ground storage tanks and associated above -ground and below -ground piping and valves. The facility has been in operation since the 1970s. 2.1 Historic Site Impacts Formal assessment and remediation activities were initiated at the facility in 1995. Three areas of concern were identified at the facility including: (i) the Line 2 Manifold Area; (ii) the Line 1 Manifold Area; and, (iii) the Line 1 Pig Signal Area. Impacts identified during the 1995 assessment are included in Incident Number 14414 (Figure 2). Petroleum impacts in the Line 2 Manifold Area were the result of a kerosene release. Excavation of impacted soils were limited due to the presence of pumps, footings, and associated underground piping and valves. A light non -aqueous phase liquid (LNAPL) recovery system and a soil vapor extraction (SVE) system were installed and formerly operated in this area. A dissolved phase plume consisting of gasoline -related compounds was identified in the Line 1 Manifold Area. A limited amount of impacted soil was excavated in this area and an SVE system was installed and formerly operated in the Line 1 Manifold Area. `` APEX Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page 2 Gasoline impacted soil was also identified in the Line 1 Pig Signal Area as a result of a release from a leaking pipe fitting. Approximately 1,000 tons of soil was excavated and thermally treated from this area. The excavation extended to bedrock, removing the source material; however, the release resulted in dissolved phase groundwater impacts. An air sparge trench located near the downgradient property boundary and a non -discharge pump and treat system were installed in the late-1990s to prevent off -Site migration of petroleum hydrocarbons. The air sparge trench is currently in operation. The groundwater pump and treatment system were taken off-line in 2010, following approval from NCDEQ on April 12, 2010. The LNAPL recovery and SVE systems were taken off-line in 2010, following approval from NCDEQ on September 29, 2010. 2.2 Recent Site Impacts A 920-gallon petroleum release occurred at the Site on March 13, 2015 when a valve gasket failed near the Line 2, Unit 4 booster pump. Emergency response and abatement activities were performed from March 13, 2015 through August 11, 2015. On August 13, 2015, a three -quarter -inch nipple on Line 2 was struck by a piece of equipment during backfilling operations resulting in a 5,000- gallon petroleum release over the recently remediated area. Approximately 4,750-gallons of diesel fuel were recovered during initial response activities and subsequent recovery well evacuation efforts. Residual soil impacts were detected at areas where additional excavation was not feasible due to the presence of booster pumps, footings, and associated underground piping and valves. Approximately 750 tons of petroleum -impacted soil were removed from the release area during the initial response activities associated with both 2015 releases. Impacts identified during the 2015 assessment are included in Incident Number 91340. A CAP and CAP Addendum were submitted to NCDEQ on April 15, 2016 and July 12, 2016, respectively. The CAP documents specify installation and operation of a bio-venting and bio-sparge system to address residual soil impacts and dissolved phase groundwater impacts. The CAP was approved on May 6, 2016 and the CAP Addendum was approved on July 28, 2016. The semiannual groundwater monitoring program for the Site incorporates the groundwater monitoring programs associated with Incident Numbers 14414 and 91340. A summary of the Groundwater Monitoring Program for the Site is provided as Table 1. `` APEX Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page 3 3.0 FIELD ACTIVITIES 3.1 Groundwater Gauging Prior to sampling, groundwater monitoring wells were gauged to measure the depth to groundwater and LNAPL, if present. Upon arriving at the Site, wells were opened and allowed to equilibrate. Wells were gauged in accordance with the United States Environmental Protection Agency (USEPA) Region IV Science and Ecosystem Support Division Field Branches Quality System and Technical Procedures. The wells were gauged in order of potential impact, moving from upgradient wells, to downgradient wells and finally source area wells. Depths to groundwater and LNAPL were measured using an electronic oil/water interface probe capable of measuring to an accuracy of 0.01 feet. The interface probe was thoroughly decontaminated before collecting measurements at each subsequent monitoring well. A total of 10 monitoring wells (MW-1, MW-4, MW-5, MW-6, MW-8, MW-13, MW-23, MW-24, MW-25, and MW-25D) and 11 recovery wells (SB- 4, S13-6, S13-8, S13-9, SB-10, S13-11, S13-12, SB-15, SB-16, S13-18, and RW-1) were gauged during the February 2019 monitoring event. Two recovery wells (SB-14 and RW-2) were not able to be located. The location of each monitoring well is shown on Figure 2 and the location of each recovery well is shown on Figure 3. 3.2 Groundwater Sampling and Analysis Groundwater samples were collected from seven monitoring wells (MW-4, MW-6, MW-8, MW-13, MW-24, MW-25, and MW-25D) during the February 2019 monitoring event. At each monitoring well, a baseline set of water quality stabilization data were measured (temperature, pH, specific conductance, and oxidation reduction potential), and recorded. The total volume of water in each well was calculated and approximately three well volumes were purged from each well prior to collecting each sample. All monitoring wells were purged and sampled with disposable bailers. Groundwater sampling logs documenting the groundwater purging and sampling are provided as Appendix A. After purging an adequate volume of water from each well, a sample was retrieved and transferred to laboratory supplied, pre -preserved bottleware and immediately placed on ice and maintained at a temperature of approximately 4 degrees Celsius. Groundwater samples were transported under standard chain -of -custody procedures to Shealy Environmental Services, Inc. of West Columbia, South Carolina. Groundwater samples collected from monitoring wells MW-4, MW-6, MW-8, and MW-13 were analyzed for benzene, toluene, ethylbenzene, and xylenes (BTEX) and methyl tert- APEX Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page 4 butyl ether (MTBE) by Environmental Protection Agency (EPA) Method 602 — purgeable aromatics SM 6200B. Groundwater samples collected from monitoring wells MW-24, MW-25, and MW-25D were analyzed for BTEX by EPA Method 602 — purgeable aromatics SM 6200B; semi -volatile organic compounds by EPA Method 625; and Massachusetts Department of Environmental Protection (MADEP) extractable petroleum hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH) in consideration of the diesel releases that occurred on March 13, 2015 and August 13, 2015. 4.0 FINDINGS 4.1 Well Gauging Results and Groundwater Flow Depth to water and top of well casing elevation data from the monitoring wells were used to calculate groundwater elevations relative to an on -Site benchmark referenced to mean sea level datum. LNAPL was not detected in any of the monitoring wells during this sampling event. A summary of monitoring well gauging data is provided in Table 2. A groundwater potentiometric map for the surficial unit using water level elevation data from the February 2019 sampling event is provided as Figure 4. The potentiometric map depicts the direction of groundwater flow to the southeast. A hydraulic gradient of approximately 0.04 feet per foot was measured between the 720 feet potentiometric contour line near MW-23 and the 705 feet potentiometric contour line near MW-8. Groundwater flow patterns observed in February 2019 are consistent with historic sampling events. LNAPL was detected in 1 of the 13 recovery wells during the February 15, 2019 sampling event at SB-16 at a thickness of 0.02 feet. A summary of recovery well gauging data is provided as Table 3. 4.2 Groundwater Analytical Results Groundwater sampling activities performed at the Site focused on collecting analytical data from the upgradient, downgradient, and central plume areas to evaluate Constituents of Concern (COC) trends over time. The analytical results for groundwater samples collected during this monitoring period were compared to the 15A NCAC 2L .0202 Groundwater Quality Standards (21L Standards) and to the 15A NCAC 2B .0215 Surface Water Standards (213 Standards) for a Water Supply II, High Quality Waters surface water classification following the Risk Based Corrective Action Rules APEX Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page 5 for non -UST releases of petroleum under North Carolina House Bill 765. A groundwater concentration map showing the concentrations of benzene in groundwater monitoring wells during the February 2019 sampling event is provided as Figure 5. Laboratory analytical reports and chain -of -custody records for the groundwater samples are presented in Appendix B. The February 2019 groundwater sampling results indicate that the hydrocarbon plume is generally stable; however, concentrations of benzene in MW-13, and benzene, C5-C8 Aliphatics, C9-C-18 Aliphatics, and C9-C22 Aromatics in MW-24 were elevated compared to those recorded during recent sampling events. A summary of groundwater analytical results is provided in Table 4. Notable results from the February 2019 sampling event are summarized below: ■ Benzene was detected in MW-13 (48 pg/L) and in MW-24 (13 pg/L) above the 2L and 2B Standards of 1.0 pg/L and 1.19 pg/L, respectively. A concentration time trend graph for benzene in MW-13 is included as Appendix C ■ MTBE was detected in MW-8 (10 pg/L) and MW-13 (2.7 pg/L) during the sampling event. Concentrations were below the 2L and 2B Standards of 20 pg/L and 19 pg/L, respectively. ■ Ethylbenzene (1.6 and 14 pg/L), toluene (1.4 and 3.3 pg/L), and xylenes (2.0 and 7.4 pg/L) were detected in MW-13 and MW-24 at concentrations below their respective 2L and 2B Standards. ■ Acenaphthene (7.0 pg/L), anthracene (estimated concentration of 2.9 pg/L), fluoranthene (7.9 pg/L), phenanthrene (estimated concentration of 2.3 pg/L), and pyrene (6.2 pg/L) were detected in MW-24 during the sampling event at concentrations below their respective 2L and 2B Standards. ■ EPH and VPH were detected in MW-24 during the sampling event. Hydrocarbon fractions C9-C12 Aliphatics were detected at a concentration of 400 pg/L, above the 2B Standard of 180 pg/L. Hydrocarbon fractions C9-C18 Aliphatics were detected at a concentration of 260 pg/L, above the 2B Standard of 180 pg/L. Hydrocarbon fractions C5-C8 Aliphatics were detected at a concentration of 1,900 pg/L, above the 2L and 2B Standards. Hydrocarbon fractions C9-C10 Aromatics were detected at a concentration of 520 pg/L and C11-C22 Aromatics were detected at a concentration of 320 pg/L, exceeding their combined 2L Standard of 200 pg/L. APEX Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page 6 5.0 REMEDIATION SYSTEM PERFORMANCE 5.1 Air Sparge Trench Remediation System The air sparge trench remediation system was brought on-line in June 1998 to treat shallow groundwater prior to migration off -Site. The air sparge system continues to operate to aid in the removal of benzene and MTBE from groundwater in the vicinity of well MW-8 and MW-13. The air sparge trench operated continuously during the reporting period; however, it was shut down approximately two weeks prior to the February 15, 2019 groundwater sampling event to allow for collection of representative groundwater samples. 5.2 Bio-Sparge and Bio-Venting Systems The bio-sparge and bio-venting systems were brought on-line on March 7, 2017 to address soil and groundwater impacts associated with the 2015 diesel fuel releases. The bio-sparge system ran continuously during the reporting period. The bio-venting system ran approximately 50% of the time during the reporting period due to excessive water recovery due to prolonged wet weather conditions resulting in a wetting front moving downward through the soil column. The bio-sparge and bio-venting systems were shut down approximately two weeks prior to the February 15, 2019 groundwater sampling event to allow for collection of representative groundwater samples. 6.0 CONCLUSIONS AND RECOMMENDATIONS During the February 2019 monitoring event, with the exception of SB-16, residual LNAPL was not detected in recovery wells installed in response to the 2015 diesel fuel releases. Benzene, C5-Cl8 Aliphatics and C9-C22 Aromatics exhibited concentrations above the applicable 2B and/or 2L Standards in MW-24. This well is located approximately 360 feet from the surface water body. These detections are attributed to the 2015 diesel fuel releases. The recently installed bio-sparge and bioventing system will aid in the removal of these remaining hydrocarbon constituents from the subsurface. Monitoring wells MW-25 and MW-25D, located nearly 250 feet from the surface water body, continue to delineate the downgradient boundary of the plume in this area. Both monitoring wells were free of any detections during the February 2019 sampling event. Benzene was detected in MW-13 during the February 2019 sampling event at concentrations greater than the 2L and 2B Standards. Detections of benzene at MW-13 are associated with the 1995 release as historic groundwater analytical data indicates the presence of benzene in this well `` APEX Semiannual Groundwater Monitoring Report, September 2018 - February 2019 April 1, 2019 Colonial Pipeline Company, Kannapolis Booster Station Page 7 since February 1998. Benzene concentrations in MW-13 have generally been decreasing since 1998, with seasonal fluctuations; however, the benzene concentration during the February 2019 sampling event was one order of magnitude higher than the five preceding sampling events. The concentration time trend graph for benzene in monitoring well MW-13 shows an overall decreasing concentration trend. Although 2B Surface Water Standards were exceeded in MW-13, any discharge of the groundwater plume to surface water would not likely contravene the surface water standards within the surface water body itself. During the February 2019 sampling event, MTBE was detected in MW-8 (10 pg/L) and MW-13 (2.7 pg/L). Concentrations were below the 2L and 2B Standards of 20 pg/L and 19 pg/L, respectively. The historic concentration trends of MTBE show a continual decrease in both MW-8 and MW-13. The air sparge system in the vicinity of wells MW-8 and MW-13 continues to operate and aid in the removal of benzene and MTBE from groundwater. Apex proposes that based on the minimal LNAPL detections during the reporting period, and the generally stable and/or decreasing dissolved phase petroleum concentration trends observed at the Site since the historic and recent 2015 release incidents, the reporting schedule for the Site be modified from semiannual to annual. Following NCDEQ approval, one annual report will be submitted on or before October 1st of each year detailing the semiannual monitoring well sampling and annual water supply well sampling results. The next semiannual groundwater sampling event is scheduled to occur in August 2019. `` APEX TABLES i APEX Table 1 Well Sampling and Analysis Program Colonial Pipeline Company Kannapolis Booster Station Concord, NC Top of Casing Screen Total Depth Analysis Well ID Elevation Interval Sampling Frequency (ft. BGS) (Following Establishment of COCs) (ft. MSL) (ft. BGS) MW-1 717.24 23.5 3.5 - 23.5 NA NA MW-2 708.52 103 88 - 103 NA NA (MW-2D) MW-3 716.64 24 4 - 24 NA NA MW-4 729.9 28 8 - 28 BTEX and MTBE by EPA Method 602 Semiannual MW-5 726.87 19 4 -19 NA NA MW-6 724.61 13 3 -13 BTEX and MTBE by EPA Method 602 Semiannual MW-7 725.1 58 53 -58 NA NA (MW-6D) MW-8 710.26 20 10 - 20 BTEX and MTBE by EPA Method 602 Semiannual MW-13 707.35 22 2 - 22 BTEX and MTBE by EPA Method 602 Semiannual MW-14 707.03 15 3-15 NA NA (MW-17) MW-15 706.23 109 -- NA NA MW-16 -- -- NA NA MW-17 707.45 NA NA (MW-TR1U) MW-18 706.79 -- -- NA NA (MW-TR1D) MW-23 726.70 15 5-15 NA NA Page 1 of 2 Table 1 Well Sampling and Analysis Program Colonial Pipeline Company Kannapolis Booster Station Concord, NC Top of Casing Total Depth Screen Analysis Well ID Elevation (ft. BGS) Interval (Following Establishment of COCs) Sampling Frequency (ft. MSL) (ft. BGS) BTEX by EPA Method 602; MW-24 724.61 10 10 - 20 SVOCs by EPA Method 625; MADEP VPH Semiannual and EPH BTEX by EPA Method 602; MW-25 724.32 17 7 - 17 SVOCs by EPA Method 625; MADEP VPH Semiannual and EPH BTEX by EPA Method 602; MW-25D 724.00 74 69 - 74 SVOCs by EPA Method 625; MADEP VPH Semiannual and EPH Notes: -- - unknown ft. - Feet ft. MSL - Feet above mean sea level BGS - Below ground surface COCs - Constituents of Concern NA - Not Applicable BTEX - Benzene, toluene, ethylbenzene, and xylenes MTBE - Methyl tert-butyl ether EPA - United States Environmental Protection Agency SVOCs - Semi -volatile Organic Compounds MADEP - Massachusetts Department of Environmental Protection VPH - Volatile Petroleum Hydrocarbons EPH - Extricable Petroleum Hydrocarbons Page 2 of 2 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-1 1/31/2001 717.24 6.70 710.54 2/7/2001 6.84 710.40 2/8/2001 6.80 710.44 2/9/2001 6.74 710.50 2/14/2001 6.22 711.02 2/21 /2001 6.54 710.70 8/16/2001 6.75 710.49 2/27/2002 6.32 710.92 8/28/2002 7.43 709.81 2/18/2003 5.15 712.09 8/18/2003 5.63 711.61 2/19/2004 5.45 711.79 8/17/2004 6.34 710.90 2/23/2005 5.64 711.60 8/16/2005 6.50 710.74 2/22/2006 5.85 711.39 8/16/2006 4.05 713.19 2/20/2007 5.78 711.46 8/15/2007 7.08 710.16 2/25/2008 6.20 711.04 8/27/2008 4.85 712.39 8/12/2010 6.18 711.06 9/8/2011 7.15 710.09 2/13/2012 6.14 711.10 8/3/2012 NM NM 2/4/2013 6.3 710.94 2/19/2014 5.06 712.18 8/25/2014 6.67 710.57 2/23/2015 5.96 711.28 8/18/2015 7.57 709.67 12/3/2015 5.10 712.14 2/16/2016 4.29 712.95 8/19/2016 6.71 710.53 2/7/2017 6.46 710.78 8/15/2017 7.00 710.24 2/1/2018 6.29 710.95 8/16/2018 6.32 710.92 2/15/2019 5.95 711.29 MW-2 (MW-2D) 1/31/2001 708.52 3.40 705.12 2/7/2001 13.80 694.72 2/8/2001 13.50 695.02 2/9/2001 12.97 695.55 2/14/2001 13.25 695.27 2/21 /2001 13.72 694.80 7/23/2001 14.15 694.37 8/16/2001 14.30 694.22 8/20/2001 5.83 702.69 8/22/2001 9.20 699.32 2/27/2002 10.50 698.02 8/28/2002 10.60 697.92 2/18/2003 9.63 698.89 8/18/2003 6.68 701.84 2/19/2004 11.35 697.17 8/17/2004 4.70 703.82 2/23/2005 12.49 696.03 12/3/2015 3.58 704.94 Page 1 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-3 1 /31 /2001 716.64 11.48 705.16 2/7/2001 11.86 704.78 2/8/2001 12.15 704.49 2/9/2001 12.48 704.16 2/14/2001 13.04 703.60 2/21 /2001 13.40 703.24 8/16/2001 13.30 703.34 2/27/2002 11.15 705.49 8/28/2002 13.95 702.69 2/18/2003 10.28 706.36 8/18/2003 9.17 707.47 2/19/2004 9.28 707.36 8/17/2004 10.61 706.03 2/23/2005 10.77 705.87 12/3/2015 9.33 707.31 MW-4 1/31/2001 729.9 15.57 714.33 2/7/2001 15.58 714.32 2/8/2001 15.51 714.39 2/9/2001 14.90 715.00 2/12/2001 14.07 715.83 2/14/2001 13.45 716.45 2/16/2001 12.80 717.10 2/21 /2001 7.00 722.90 2/27/2001 6.70 723.20 3/2/2001 6.85 723.05 3/9/2001 4.97 724.93 3/19/2001 5.02 724.88 3/26/2001 5.65 724.25 4/2/2001 5.00 724.90 4/9/2001 3.80 726.10 4/16/2001 5.00 724.90 4/23/2001 4.04 725.86 4/27/2001 3.65 726.25 5/1/2001 4.35 725.55 5/21/2001 5.33 724.57 6/13/2001 4.75 725.15 7/3/2001 3.64 726.26 7/19/2001 4.10 725.80 7/23/2001 3.58 726.32 7/30/2001 4.30 725.60 8/14/2001 3.55 726.35 8/16/2001 3.30 726.60 9/5/2001 4.62 725.28 9/11/2001 4.50 725.40 10/11/2001 5.20 724.70 11 /7/2001 5.62 724.28 11 /21 /2001 5.26 724.64 12/18/2001 3.35 726.55 12/27/2001 4.65 725.25 1/17/2002 6.16 723.74 2/26/2002 4.50 725.40 2/27/2002 4.75 725.15 3/14/2002 5.40 724.50 4/26/2002 6.75 723.15 5/10/2002 5.70 724.20 5/28/2002 3.80 726.10 6/19/2002 4.90 725.00 7/3/2002 5.85 724.05 8/20/2002 5.80 724.10 Page 2 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-4 continued 8/28/2002 729.9 5.80 724.10 2/18/2003 4.38 725.52 3/17/2003 3.55 726.35 4/28/2003 3.80 726.10 5/19/2003 3.30 726.60 6/5/2003 3.75 726.15 7/7/2003 4.38 725.52 8/18/2003 4.73 725.17 9/5/2003 5.10 724.80 10/6/2003 4.70 725.20 11 /21 /2003 4.90 725.00 12/8/2003 4.30 725.60 1 /29/2004 4.48 725.42 2/19/2004 4.50 725.40 3/9/2004 4.90 725.00 4/6/2004 4.00 725.90 5/7/2004 4.64 725.26 6/8/2004 4.66 725.24 7/22/2004 7.62 722.28 8/10/2004 7.15 722.75 8/17/2004 7.73 722.17 9/9/2004 6.40 723.50 2/23/2005 3.51 726.39 3/23/2005 6.95 722.95 4/11/2005 4.35 725.55 5/5/2005 3.94 725.96 6/23/2005 3.80 726.10 7/7/2005 3.90 726.00 8/16/2005 5.50 724.40 9/9/2005 5.40 724.50 10/18/2005 5.82 724.08 11 /9/2005 6.70 723.20 12/20/2005 3.55 726.35 1/18/2006 4.33 725.57 2/22/2006 5.32 724.58 2/20/2007 5.54 724.36 8/15/2007 8.45 721.45 2/25/2008 4.46 725.44 8/27/2008 4.90 725.00 2/11/2009 8.66 721.24 8/20/2009 9.08 720.82 2/4/2010 6.06 723.84 8/12/2010 9.87 720.03 2/15/2011 11.73 718.17 9/8/2011 13.82 716.08 2/13/2012 10.76 719.14 8/3/2012 12.87 717.03 2/4/2013 13.12 716.78 2/19/2014 10.12 719.78 8/25/2014 11.03 718.87 2/23/2015 11.39 718.51 8/18/2015 13.96 715.94 12/3/2015 10.26 719.64 2/16/2016 8.46 721.44 8/19/2016 11.34 718.56 2/7/2017 12.01 717.89 8/15/2017 11.74 718.16 2/1/2018 13.56 716.34 8/16/2018 12.2 717.70 2/15/2019 7.79 722.11 Page 3 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-5 2/23/2001 726.87 13.27 713.60 2/27/2002 10.35 716.52 2/18/2003 9.50 717.37 8/17/2004 9.85 717.02 2/23/2005 9.24 717.63 8/12/2010 10.32 716.55 9/8/2011 12.34 714.53 2/13/2012 10.97 715.90 8/3/2012 NM NM 2/4/2013 12.39 714.48 2/19/2014 10.76 716.11 8/25/2014 11.68 715.19 2/23/2015 11.41 715.46 8/18/2015 13.14 713.73 12/3/2015 10.02 716.85 2/16/2016 9.65 717.22 8/19/2016 11.22 715.65 2/7/2017 12.02 714.85 8/15/2017 11.94 714.93 2/1/2018 12.76 714.11 8/16/2018 11.02 715.85 2/15/2019 9.73 717.14 Page 4 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-6 1 /31 /2001 724.61 15.10 709.51 2/7/2001 15.18 709.43 2/8/2001 15.17 709.44 2/9/2001 15.18 709.43 2/14/2001 15.18 709.43 2/21 /2001 15.18 709.43 8/16/2001 15.52 709.09 2/27/2002 14.00 710.61 8/28/2002 30.45 694.16 2/18/2003 13.17 711.44 8/18/2003 11.62 712.99 2/19/2004 12.17 712.44 8/17/2004 12.98 711.63 2/23/2005 13.28 711.33 8/16/2005 12.97 711.64 2/22/2006 11.98 712.63 8/16/2006 12.55 712.06 2/20/2007 11.90 712.71 8/15/2007 14.23 710.38 2/25/2008 13.10 711.51 8/27/2008 12.78 711.83 2/11/2009 13.27 711.34 8/20/2009 13.86 710.75 2/4/2010 13.75 710.86 8/12/2010 12.15 712.46 2/15/2011 13.09 711.52 9/8/2011 DRY DRY 2/13/2012 12.42 712.19 8/3/2012 13.66 710.95 2/4/2013 13.61 711.00 2/19/2014 12.02 712.59 8/25/2014 13.31 711.30 2/23/2015 13.01 711.60 8/18/2015 14.50 710.11 12/3/2015 11.63 712.98 2/16/2016 11.24 713.37 8/19/2016 13.05 711.56 2/7/2017 13.35 711.26 8/15/2017 13.36 711.25 2/1/2018 14.28 710.33 8/16/2018 12.93 711.68 2/15/2019 11.67 712.94 Page 5 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-7 (MW-6D) 1/31/2001 725.52 21.40 704.12 2/7/2001 30.48 695.04 2/8/2001 30.40 695.12 2/9/2001 29.23 696.29 2/14/2001 30.12 695.40 2/21 /2001 30.60 694.92 7/23/2001 31.02 694.50 8/16/2001 31.15 694.37 8/20/2001 22.75 702.77 8/22/2001 26.12 699.40 2/27/2002 27.40 698.12 8/28/2002 14.62 710.90 2/18/2003 26.50 699.02 8/18/2003 23.60 701.92 2/19/2004 28.17 697.35 8/17/2004 21.69 703.83 2/23/2005 29.37 696.15 8/16/2005 28.75 696.77 2/22/2006 25.10 700.42 8/16/2006 28.75 696.77 2/20/2007 26.68 698.84 8/15/2007 28.68 696.84 2/25/2008 13.10 712.42 8/27/2008 28.60 696.92 9/8/2011 23.76 701.76 2/13/2012 21.12 704.40 8/3/2012 NM NM 2/4/2013 21.69 703.83 8/18/2015 NM NM 12/3/2015 20.38 705.14 Page 6 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-8 1 /31 /2001 710.26 6.72 703.54 2/7/2001 6.80 703.46 2/8/2001 6.97 703.29 2/9/2001 7.08 703.18 2/14/2001 7.20 703.06 2/21 /2001 7.37 702.89 8/16/2001 7.75 702.51 2/27/2002 6.65 703.61 8/28/2002 8.60 701.66 2/18/2003 6.25 704.01 8/18/2003 6.13 704.13 2/19/2004 6.00 704.26 8/17/2004 6.36 703.90 2/23/2005 6.28 703.98 8/16/2005 6.55 703.71 2/22/2006 5.75 704.51 8/16/2006 7.08 703.18 2/20/2007 6.70 703.56 8/15/2007 15.80 694.46 2/25/2008 7.50 702.76 8/27/2008 10.30 699.96 2/11/2009 6.13 704.13 8/20/2009 7.90 702.36 2/4/2010 6.00 704.26 8/12/2010 6.52 703.74 2/15/2011 6.69 703.57 9/8/2011 8.82 701.44 2/13/2012 6.23 704.03 8/3/2012 7.12 703.14 2/4/2013 6.72 703.54 2/19/2014 6.08 704.18 8/25/2014 4.67 705.59 2/23/2015 6.62 703.64 8/18/2015 7.87 702.39 12/3/2015 6.22 704.04 2/16/2016 5.82 704.44 8/19/2016 7.25 703.01 2/7/2017 6.48 703.78 8/15/2017 7.14 703.12 2/1/2018 6.44 703.82 8/16/2018 7.14 703.12 2/15/2019 6.43 703.83 MW-9 (MW-9D) 1/31/2001 711.84 7.78 704.06 2/7/2001 12.24 699.60 2/8/2001 15.85 695.99 2/9/2001 15.64 696.20 2/14/2001 15.83 696.01 2/21 /2001 16.25 695.59 8/16/2001 16.95 694.89 8/20/2001 9.20 702.64 8/22/2001 12.25 699.59 2/27/2002 13.20 698.64 8/28/2002 16.40 695.44 2/18/2003 12.46 699.38 8/18/2003 6.94 704.90 2/19/2004 12.75 699.09 8/17/2004 8.04 703.80 2/23/2005 15.13 696.71 Page 7 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-10 (MW-10D) 1/31/2001 706.24 3.70 702.54 2/7/2001 3.22 703.02 2/8/2001 3.14 703.10 2/9/2001 3.02 703.22 2/14/2001 3.40 702.84 2/21 /2001 2.50 703.74 8/16/2001 5.75 700.49 2/27/2002 3.80 702.44 8/28/2002 6.90 699.34 2/18/2003 2.30 703.94 2/19/2004 3.55 702.69 2/20/2004 4.55 701.69 8/17/2004 5.03 701.21 2/23/2005 3.54 702.70 MW-11 Abandoned MW-12 (MW-12D) 1/31/2001 715.94 8.10 707.84 2/7/2001 8.37 707.57 2/8/2001 8.34 707.60 2/9/2001 8.35 707.59 2/14/2001 8.15 707.79 2/21 /2001 7.52 708.42 8/16/2001 9.77 706.17 2/27/2002 7.20 708.74 8/28/2002 10.87 705.07 2/18/2003 5.60 710.34 8/18/2003 6.25 709.69 2/19/2004 5.40 710.54 8/17/2004 9.25 706.69 2/23/2005 5.75 710.19 Page 8 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL M W-13 1 /31 /2001 707.35 4.00 703.35 2/7/2001 4.63 702.72 2/8/2001 4.75 702.60 2/9/2001 4.75 702.60 2/14/2001 4.69 702.66 2/21 /2001 4.67 702.68 2/27/2002 4.85 702.50 8/28/2002 6.50 700.85 2/18/2003 4.66 702.69 8/18/2003 4.95 702.40 2/19/2004 4.15 703.20 8/17/2004 5.06 702.29 2/23/2005 4.25 703.10 8/16/2005 4.65 702.70 2/22/2006 4.02 703.33 8/16/2006 3.80 703.55 2/20/2007 4.30 703.05 8/15/2007 5.80 701.55 2/25/2008 3.90 703.45 8/27/2008 3.68 703.67 2/11/2009 4.30 703.05 8/20/2009 5.36 701.99 2/4/2010 3.87 703.48 8/12/2010 4.91 702.44 2/15/2011 3.98 703.37 9/8/2011 5.10 702.25 2/13/2012 4.12 703.23 8/3/2012 NM N M 2/4/2013 3.88 703.47 2/19/2014 3.86 703.49 8/25/2014 4.85 702.50 2/23/2015 4.65 702.70 8/18/2015 5.63 701.72 12/3/2015 3.55 703.80 2/16/2016 3.55 703.80 8/19/2016 4.99 702.36 2/7/2017 4.32 703.03 8/15/2017 4.71 702.64 2/1/2018 3.69 703.66 8/16/2018 4.6 702.75 2/15/2019 3.91 703.44 MW-14 (MW-17) 1/31/2001 707.15 4.02 703.13 2/7/2001 4.20 702.95 2/8/2001 4.25 702.90 2/9/2001 4.18 702.97 2/14/2001 4.05 703.10 2/21 /2001 4.15 703.00 8/16/2001 4.80 702.35 2/27/2002 4.35 702.80 8/28/2002 6.10 701.05 2/18/2003 4.00 703.15 8/18/2003 4.25 702.90 2/19/2004 4.50 702.65 8/17/2004 4.55 702.60 2/23/2005 3.53 703.62 12/3/2015 3.51 703.64 Page 9 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-15 (MW-17D) 1/31/2001 706.23 2.30 703.93 2/7/2001 23.10 683.13 2/8/2001 22.30 683.93 2/9/2001 16.82 689.41 2/14/2001 21.60 684.63 2/21 /2001 22.90 683.33 7/23/2001 15.15 691.08 8/16/2001 15.20 691.03 8/20/2001 3.60 702.63 8/22/2001 7.85 698.38 2/27/2002 11.00 695.23 2/18/2003 9.70 696.53 8/18/2003 5.90 700.33 2/19/2004 12.58 693.65 8/17/2004 4.00 702.23 2/23/2005 14.80 691.43 8/16/2005 12.20 694.03 2/22/2006 7.95 698.28 8/16/2006 12.20 694.03 2/20/2007 9.82 696.41 8/15/2007 11.90 694.33 8/27/2008 12.60 693.63 2/11/2009 3.04 703.19 MW-16 (Crowe Well) 1/31/2001 718.48 15.10 703.38 2/7/2001 18.40 700.08 2/8/2001 18.95 699.53 2/9/2001 18.60 699.88 2/14/2001 18.80 699.68 2/21 /2001 18.85 699.63 8/16/2001 20.05 698.43 8/20/2001 16.22 702.26 8/22/2001 18.07 700.41 2/27/2002 17.98 700.50 8/28/2002 20.78 697.70 2/18/2003 16.82 701.66 8/18/2003 13.60 704.88 2/19/2004 16.25 702.23 8/17/2004 15.24 703.24 2/23/2005 18.00 700.48 8/16/2005 18.40 700.08 2/22/2006 15.00 703.48 8/16/2006 18.65 699.83 2/20/2007 16.37 702.11 8/15/2007 19.48 699.00 2/25/2008 16.95 701.53 8/27/2008 19.30 699.18 MW-17 (MW-TR1U) 2/23/2001 707.45 4.45 703.00 8/16/2001 5.10 702.35 2/27/2002 4.15 703.30 8/28/2002 6.35 701.10 2/18/2003 4.35 703.10 2/19/2004 4.00 703.45 8/17/2004 4.71 702.74 2/23/2005 3.68 703.77 12/3/2015 3.51 703.94 Page 10 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-18 (MW-TR1D) 2/23/2001 706.79 3.88 702.91 8/16/2001 4.52 702.27 2/27/2002 4.10 702.69 8/28/2002 5.75 701.04 2/18/2003 3.75 703.04 2/19/2004 3.50 703.29 8/17/2004 4.12 702.67 2/23/2005 3.19 703.60 12/3/2015 3.32 703.47 MW-19 (MW-TR2U) 2/23/2001 707.97 5.18 702.79 8/16/2001 5.77 702.20 2/27/2002 5.45 702.52 8/28/2002 6.95 701.02 2/18/2003 5.05 702.92 2/19/2004 4.60 703.37 8/17/2004 5.62 702.35 2/23/2005 4.19 703.78 MW-20 (MW-TR2D) 2/23/2001 707.46 4.77 702.69 8/16/2001 5.71 701.75 2/27/2002 5.40 702.06 8/28/2002 7.00 700.46 2/18/2003 4.30 703.16 2/19/2004 4.18 703.28 8/17/2004 5.18 702.28 2/23/2005 4.42 703.04 8/19/2010 5.61 701.85 2/19/2014 4.93 702.53 8/25/2014 5.39 702.07 2/23/2015 4.74 702.72 MW-21 (MW-MU) 2/23/2001 711.47 7.46 704.01 8/16/2001 7.90 703.57 2/27/2002 7.00 704.47 8/28/2002 8.60 702.87 2/18/2003 6.85 704.62 2/19/2004 6.80 704.67 8/17/2004 6.86 704.61 2/23/2005 6.80 704.67 MW-22 (MW-TR3D) 2/23/2001 710.84 7.65 703.19 8/16/2001 8.13 702.71 2/27/2002 7.60 703.24 8/28/2002 9.00 701.84 2/18/2003 6.70 704.14 2/19/2004 6.50 704.34 8/17/2004 6.80 704.04 2/23/2005 6.73 704.11 MW-23 12/3/2015 726.70 7.72 718.98 2/16/2016 6.48 720.22 8/19/2016 8.82 717.88 2/7/2017 9.67 717.03 8/15/2017 9.49 717.21 2/1/2018 11.11 715.59 8/16/2018 9.07 717.63 2/15/2019 6.03 720.67 MW-24 12/3/2015 724.61 6.54 718.07 2/16/2016 6.16 718.45 8/19/2016 7.46 717.15 2/7/2017 8.49 716.12 8/15/2017 7.92 716.69 2/1/2018 9.07 715.54 8/16/2018 7.23 717.38 2/15/2019 5.91 718.70 Page 11 of 12 Table 2 Groundwater Elevation Summary Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Number Date Elevation of TOC (ft. MSL) Depth to Water (ft.) Groundwater Elevation ft. MSL MW-25 12/3/2015 724.32 8.34 715.98 2/16/2016 8.11 716.21 8/19/2016 9.28 715.04 2/7/2017 10.60 713.72 8/15/2017 10.28 714.04 2/1/2018 10.61 713.71 8/16/2018 8.91 715.41 2/15/2019 8.06 716.26 MW-25D 12/3/2015 724.00 19.70 704.30 2/16/2016 19.13 704.87 8/19/2016 22.77 701.23 2/7/2017 20.57 703.43 8/15/2017 22.04 701.96 2/1/2018 11.80 712.20 8/16/2018 21.63 702.37 2/15/2019 18.99 705.01 Notes: TOC elevations obtained from ESP Associates survey (4/2001) and TWT survey (12/2015), with the exception of MW-15. Monitor well numbers modified January 2001. Former well designations in parenthesis. TOC - Top of casing ft. - Feet ft. MSL - Feet above mean sea level Page 12 of 12 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Date Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) 'Corrected Groundwater Elevation (ft. MSL) S13-1 8/14/2015 NM 5.0 2.67 4.03 1.36 8/15/2015 3.79 4.05 0.26 8/17/2015 3.60 4.10 0.50 8/18/2015 DRY S13-2 8/14/2015 NM 5.0 2.16 3.78 1.62 8/15/2015 3.22 4.00 0.78 8/17/2015 3.65 3.85 0.20 8/18/2015 DRY S13-3 8/14/2015 NM 5.0 0.99 4.03 3.04 8/15/2015 2.64 4.20 1.56 8/17/2015 3.99 4.20 0.21 8/18/2015 3.95 4.20 0.25 - 8/19/2015 DRY S13-4 8/15/2015 722.57 13.55 7.13 13.27 6.14 713.72 8/17/2015 7.51 13.26 5.75 713.45 8/18/2015 8.48 9.42 0.94 713.83 8/19/2015 8.70 9.40 0.70 713.67 8/20/2015 8.59 9.40 0.81 713.75 8/21 /2015 8.80 9.10 0.30 713.69 8/24/2015 8.50 8.58 0.08 714.05 8/27/2015 8.84 9.01 0.17 713.68 12/16/2015 7.03 7.05 0.02 715.53 2/16/2016 ND 3.45 NA 719.12 8/19/2016 ND 4.42 NA 718.15 2/7/2017 ND 5.91 NA 716.66 8/15/2017 ND 5.64 NA 716.93 2/1/2018 ND 5.33 NA 717.24 8/16/2018 ND 4.21 NA 718.36 2/15/2019 ND 3.32 NA 719.25 S13-5 (Converted to RW-01) 8/15/2015 NM 11.43 7.11 9.57 2.46 8/17/2015 7.49 9.65 2.16 - 8/18/2015 8.61 9.66 1.05 8/19/2015 8.92 10.92 2.00 8/20/2015 2.50 3.90 1.40 8/21 /2015 1.45 1.95 0.50 - S13-6 8/15/2015 723.17 14.7 8.68 10.05 1.37 714.11 8/17/2015 8.44 11.92 3.48 713.76 8/18/2015 8.88 10.04 1.16 713.97 8/19/2015 9.31 9.55 0.24 713.79 8/20/2015 5.64 8.50 2.86 716.73 8/21 /2015 9.04 10.06 1.02 713.84 8/24/2015 8.92 10.47 1.55 713.82 8/27/2015 9.34 9.60 0.26 713.76 12/16/2015 7.03 7.05 0.02 716.13 2/16/2016 ND 5.73 NA 717.44 8/19/2016 6.76 6.77 0.01 716.41 2/7/2017 ND 8.10 NA 715.07 8/15/2017 8.45 8.56 0.11 714.69 2/1/2018 8.01 8.02 0.01 715.16 8/16/2018 ND 6.32 NA 716.85 2/15/2019 ND 5.15 NA 718.02 Page 1 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Date Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) 'Corrected Groundwater Elevation (ft. MSL) S13-7 8/15/2015 723.33 9.35 ND 7.50 NA 715.83 8/17/2015 7.68 7.72 0.04 715.64 8/18/2015 7.67 8.09 0.42 715.54 8/19/2015 8.23 8.24 0.01 715.10 8/20/2015 8.29 8.30 0.01 715.04 8/21/2015 ND 8.35 NA 714.98 8/24/2015 8.32 8.33 0.01 715.01 8/27/2015 ND 8.12 NA 715.21 12/16/2015 ND 6.05 NA 717.28 2/16/2016 ND 2.88 NA 720.45 8/19/2016 ND 3.32 NA 720.01 2/7/2017 ND 5.55 NA 717.78 Well Abandoned S13-8 8/17/2015 722.60 12.76 ND 8.41 NA 714.19 8/18/2015 ND 8.49 NA 714.11 8/19/2015 ND 8.70 NA 713.90 8/20/2015 ND 8.60 NA 714.00 8/21/2015 ND 8.62 NA 713.98 8/24/2015 ND 8.56 NA 714.04 8/27/2015 ND 8.75 NA 713.85 12/16/2015 ND 6.22 NA 716.38 2/16/2016 ND 4.70 NA 717.90 8/19/2016 ND 6.13 NA 716.47 2/7/2017 ND 6.89 NA 715.71 8/15/2017 ND 2.51 NA 720.09 2/1/2018 ND 3.60 NA 719.00 8/16/2018 ND 2.61 NA 719.99 2/15/2019 ND 2.68 NA 719.92 S13-9 8/17/2015 722.62 9.75 7.45 9.75 2.30 714.53 8/18/2015 7.91 9.48 1.57 714.27 8/19/2015 8.41 9.48 1.07 713.91 8/20/2015 8.33 9.75 1.42 713.89 8/21/2015 8.43 9.47 1.04 713.90 8/24/2015 8.37 9.54 1.17 713.92 8/27/2015 8.46 9.45 0.99 713.88 12/16/2015 ND 5.96 NA 716.66 2/16/2016 ND 3.60 NA 719.02 8/19/2016 ND 4.28 NA 718.34 2/7/2017 ND 5.64 NA 716.98 8/15/2017 ND 5.34 NA 717.28 2/1/2018 ND 6.37 NA 716.25 8/16/2018 ND 3.94 NA 718.68 2/15/2019 ND 3.63 NA 718.99 SB-10 8/17/2015 724.35 15.35 ND 10.53 NA 713.82 8/18/2015 ND 10.30 NA 714.05 8/19/2015 ND 10.45 NA 713.90 8/20/2015 ND 10.38 NA 713.97 8/21/2015 ND 10.40 NA 713.95 8/24/2015 ND 10.32 NA 714.03 8/27/2015 ND 10.50 NA 713.85 12/16/2015 ND 7.99 NA 716.36 2/16/2016 ND 6.49 NA 717.86 8/19/2016 ND 7.75 NA 716.60 2/7/2017 ND 8.73 NA 715.62 8/18/2017 ND 9.49 NA 714.86 2/1/2018 ND 9.13 NA 715.22 8/16/2018 ND 7.34 NA 717.01 2/15/2019 ND 6.29 NA 718.06 Page 2 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Date Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) 'Corrected Groundwater Elevation (ft. MSL) SB-11 8/18/2015 725.36 15.19 ND 11.18 NA 714.18 8/19/2015 ND 11.30 NA 714.06 8/20/2015 ND 12.27 NA 713.09 8/21/2015 ND 11.35 NA 714.01 8/24/2015 ND 11.40 NA 713.96 8/27/2015 ND 11.55 NA 713.81 12/16/2015 ND 8.58 NA 716.78 2/16/2016 ND 6.29 NA 719.07 8/19/2016 ND 8.40 NA 716.96 2/7/2017 ND 8.90 NA 716.46 8/15/2017 ND 9.21 NA 716.15 2/1/2018 ND 9.58 NA 715.78 8/16/2018 ND 8.94 NA 716.42 2/15/2019 ND 6.07 NA 719.29 SB-12 8/18/2015 722.03 15.8 ND 7.75 NA 714.28 8/19/2015 ND 7.88 NA 714.15 8/20/2015 ND 7.36 NA 714.67 8/21/2015 ND 7.86 NA 714.17 8/24/2015 ND 7.89 NA 714.14 8/27/2015 ND 9.13 NA 712.90 12/16/2015 ND 5.96 NA 716.07 2/16/2016 ND 4.83 NA 717.20 8/19/2016 ND 6.46 NA 715.57 2/7/2017 ND 6.77 NA 715.26 8/15/2017 ND 7.14 NA 714.89 2/1/2018 ND 7.08 NA 714.95 8/16/2018 ND 6.13 NA 715.9 2/15/2019 ND 4.87 NA 717.16 SB-13 8/19/2015 721.26 9 7.29 8.53 1.24 713.62 8/20/2015 7.33 8.45 1.12 713.62 8/21/2015 7.58 8.65 1.07 713.38 8/24/2015 7.33 8.00 0.67 713.74 8/27/2015 7.45 8.55 1.10 713.50 12/16/2015 ND 5.30 NA 715.96 2/16/2016 ND 1.86 NA 719.40 8/19/2016 ND 3.10 NA 718.16 2/7/2017 ND 4.72 NA 716.54 Well Abandoned SB-14 8/19/2015 721.69 18 7.81 8.10 0.29 713.80 8/20/2015 7.65 8.90 1.25 713.69 8/21/2015 7.75 7.80 0.05 713.93 8/24/2015 7.86 8.28 0.42 713.71 8/27/2015 7.80 8.33 0.53 713.74 12/16/2015 ND 5.80 NA 715.89 2/16/2016 ND 3.23 NA 718.46 8/19/2016 4.48 4.65 0.17 717.16 2/7/2017 5.50 6.10 0.60 716.02 8/15/2017 ND 5.83 NA 715.86 2/1/2018 ND 5.41 NA 716.28 8/16/2018 ND 3.87 NA 717.82 2/15/2019 Well not located Page 3 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Date Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) 'Corrected Groundwater Elevation (ft. MSL) SB-15 8/19/2015 722.76 17.2 8.64 10.28 1.64 713.66 8/20/2015 8.68 9.33 0.65 713.90 8/21/2015 8.78 8.90 0.12 713.95 8/24/2015 8.79 8.84 0.05 713.96 8/27/2015 ND 8.95 NA 713.81 12/16/2015 ND 6.46 NA 716.30 2/16/2016 ND 5.00 NA 717.76 8/19/2016 ND 6.41 NA 716.35 2/7/2017 ND 7.47 NA 715.29 8/15/2017 ND 7.88 NA 714.88 2/1/2018 ND 7.60 NA 715.16 8/16/2018 ND 5.85 NA 716.91 2/15/2019 ND 4.52 NA 718.24 SB-16 8/20/2015 722.88 12.5 ND 8.90 NA 713.98 8/21/2015 ND 8.85 NA 714.03 8/24/2015 ND 8.80 NA 714.08 8/27/2015 ND 9.00 NA 713.88 12/16/2015 ND 6.47 NA 716.41 2/16/2016 ND 3.24 NA 719.64 8/19/2016 ND 5.21 NA 717.67 2/7/2017 ND 7.21 NA 715.67 8/15/2017 ND 7.76 NA 715.12 2/1/2018 ND 7.53 NA 715.35 8/16/2018 ND 5.48 NA 717.40 2/15/2019 4.35 4.37 0.02 718.52 SB-17 8/20/2015 722.88 13.8 ND 8.95 NA 713.93 8/21/2015 ND 8.95 NA 713.93 8/24/2015 ND 8.88 NA 714.00 8/27/2015 ND 9.09 NA 713.79 12/16/2015 ND 6.90 NA 715.98 2/16/2016 ND 5.79 NA 717.09 8/19/2016 ND 6.80 NA 716.08 2/7/2017 7.57 7.58 0.01 715.31 Well Abandoned SB-18 8/21/2015 721.87 15.8 ND 8.45 NA 713.42 8/24/2015 ND 8.38 NA 713.49 8/27/2015 ND 8.68 NA 713.19 12/16/2015 5.50 8.83 3.33 715.44 2/16/2016 4.20 4.21 0.01 717.67 8/19/2016 6.10 6.35 0.25 715.70 2/7/2017 6.06 6.89 0.83 715.58 8/15/2017 ND 3.20 NA 718.67 2/1/2018 ND 3.12 NA 718.75 8/16/2018 ND 2.32 NA 719.55 2/15/2019 ND 4.34 NA 717.53 Page 4 of 5 Table 3 Recovery Well Gauging Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Well Date Top of Casing Elevation (ft. MSL) Well Depth (ft. BLS) Depth to LNAPL (ft. TOC) Depth to Water (ft. TOC) LNAPL Thickness (ft.) 'Corrected Groundwater Elevation (ft. MSL) SB-19 8/21/2015 723.66 13.33 9.65 10.45 0.80 713.79 8/24/2015 9.67 10.06 0.39 713.88 8/27/2015 9.80 10.00 0.20 713.80 12/16/2015 7.52 7.57 0.05 716.13 2/16/2016 ND 4.42 NA 719.24 8/19/2016 5.80 5.95 0.15 717.82 2/7/2017 ND 7.43 NA 716.23 Well Abandoned RW-1 8/24/2015 722.98 14.3 9.03 9.91 0.88 713.70 8/27/2015 9.20 10.20 1.00 713.50 12/16/2015 ND 6.86 NA 716.12 2/16/2016 ND 4.11 NA 718.87 8/19/2016 ND 5.10 NA 717.88 2/7/2017 ND 7.50 NA 715.48 8/15/2017 ND 6.90 NA 716.08 2/1/2018 ND 8.22 NA 714.76 8/16/2018 ND 4.96 NA 718.02 2/15/2019 ND 2.72 NA 720.26 RW-2 8/24/2015 723.14 15 ND 9.25 NA 713.89 8/27/2015 ND 9.45 NA 713.69 12/16/2015 ND 7.05 NA 716.09 2/16/2016 ND 5.25 NA 717.89 8/19/2016 ND 6.63 NA 716.51 2/7/2017 ND 7.97 NA 715.17 8/15/817 ND 8.06 NA 715.08 2/1/2018 ND 8.53 NA 714.61 8/16/2018 Well not located 2/15/2019 Well not located Notes: ft. - Feet ft. TOC - Feet below top of casing ft. BLS - Feet below ground surface ft. MSL - Feet above mean sea level LNAPL - Light non -aqueous phase liquid ND - None detected NA - Not applicable 1 - Corrected groundwater elevations calculated for wells with LNAPL detections Page 5 of 5 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 01 d d t Sample ID Sample Data m Q y N 2 i K m m m .u-. R M ra s' A y c r m m m a t t m Q E O E O N O H i a+ d C 2. t i Q to .Q' Q .Q' Q Q Q y N N G V L C C c M U co N_ co O _ N N d C L m C L t N N N i � C U U U U V = N L a+ 7 O O T a+ N y V C C N L N_ O 7 O 3 N t T T r T T 1n T r r m W H X Q Q In Q I LL E: I a. I d U L) L) L) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 1 3 1 300 300 200 200 10,000* 700* 400* 200* Surface Water Standard u /L WS-II, HQW 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 10.32(1)1 20 LL 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-1 2/25/1998 ND ND ND ND 85 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/1998 ND ND ND ND 97 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 ND ND ND ND 14 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 110 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 160 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 9.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 58 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 58 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 17.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 1.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 40 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 19 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 16 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 8.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 6.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 Page 1 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, INC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 0) d d t Sample ID Sample Data m Q y N 2 i K m m m L)R M ra s' y c r m m m a t t m E O E O N H a+ C 2. to Q Q Q Q = y 07 N _ G V L LU C C c M U 00 N_ O_ N 0) d 7 C T W m M y >4 t O C N �' i O 0) O W C L) L) L) L) U C 07 L a+ O Q T - 0) V C (D L .�.. N_ 7 3 0) t T T r T M 1n M r r m W H X M Q Q In Q I LL E: a (L U L) L) L) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,00W 700* 400* 200* Surface Water Standard u /L WS-II, HQW 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 0.32 ' 20 ' 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-2 (MW-2D) 10/20/1997 ND ND ND ND 2,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/1998 ND ND ND ND 3,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18-19/98 ND ND ND ND 2,700 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 ND ND ND ND 4,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 3,800 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/23/1999 ND ND ND ND 5,900 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 6,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 1.1 <1.0 6.5 4,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1/31/2001 <1.0 <1.0 <1.0 <3.0 1,400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 430 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 5.2 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <75 <100 MW-3 2/25/1998 ND ND ND ND 21 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 ND ND ND ND 590 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/1999 ND ND ND ND 170 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 1,400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 52 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 22 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1 <1 <1 <3 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1 <1 <1 <3 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1 <1 <1 <3 <5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 0.83J <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 Page 2 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, INC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH Sample ID Sample Data = N N = 07 m y C N CDd Q i .+ W d 7 O H f6 p H N C N T X d r d � 16 '�" W r m N M O m G @ y V Q m V t C Q N m LT .5.+ G (D m y = N �` L U a� @ � L ? x N s >. t ll.l .N... N_ Q d c r C i O 7 U- C O 3 U- y C s` c d t a C T (L N L)U fL6 O ._ Q O M U T r U 1 t Q a0 L) T L) U f6 t Q N_ L) T L) N 'U R L a 00 L) 1n L) 2 i6 E O Q L) O1 U u lC O L Q U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000* 700* 400* 200* Surface Water Standard u /L WS-II, HQW 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 0.32 ' 20 ' 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-4 1/31/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 15.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/27/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2015 <0.5 <0.5 <0.5 <1.5 <0.5 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <4.9 <200 <200 <100 <100 <100 <200 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 151 <75 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2019 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Page 3 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, INC Sample ID Sample Data Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH = 0) C 07 m N 4)07 L a+ W d 7 O H ra H N C Q T X L d d s' _ T W - m 0) M y c a+ G M y V Q C V >4 t C Q m i r 2. O C (D In N �' L 0) t Q K m L LU .�.. N_ Q m C i O 7 I LL C 0) O 3 E: m c W 0) t a C T (L y m a to M U T r U m t Q 00 L) T L) m t Q N_ L) M L) N L)R m L) 1n L) 2 E O Q O_ L) M U M E O Q N U r r U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,00W 700* 400* 200* Surface Water Standard u /L WS-II, HQ!! 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 0.32 ' 20 ' 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-5 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 MW-6 2/17/2000 2,000 1500 7,300 14,000 30,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 2,000 700 3,200 12,000 29,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 9 37 27 240 8,100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 160 27 32 570 2,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <20.0 <20.0 <20.0 <20.0 3,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 354 <1.0 24.9 209 1,560 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 22 <1.0 <1.0 <3.0 400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 260 13 4.6 4.4 410 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 260 46 10 31 340 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 160 52 <10 <30 76 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 370 110 19 30 84 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 110 47 <10 <30 120 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 240 33 9.8 J 17 58 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 150 32 <10 <30 <50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 310 63 17 31 68 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 130 37 4.5 14.9 95 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 170 28 3.3 8.9 230 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 13.2 <1.0 <1.0 <2.0 23 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 73.7 5 1.4 <2.0 33.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 <1.0 <1.0 <1.0 <3.0 10.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 6.5 <1.0 <1.0 <2.0 4.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 INS INS INS INS INS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 3.6 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 <2.0 <2.0 7.3J <2.0 <2.0 <2.0 <2.0 <100 <100 <75 10J <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 <0.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 <1.0 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA NA NA NA NA NA NA NA NA NA NA NA IN NA 2/15/2019 <0.50 <0.50 <0.50 <0.50 <0.50 NA NA I NA I NA NA I NA NA NA NA NA NA NA NA IN NA Page 4 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, INC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 0) d d t Sample ID Sample Data m Q y N 2 i K m m m L)R M ra s' y c r m m m a t t m E O E O N H a+ C 2. to Q Q Q Q = 4)07 N _ G V L LU C C c M U 00 N_ O_ N 0) d 7 C T W m M y >4 t O C N �' i O 0) O W C L) L) L) L) U C 07 L a+ O Q T - 0) V C (D L .�.. N_ 7 3 0) t T T r T M 1n M r r m W H X M Q Q In Q I LL E: a (L U L) L) L) U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,00W 700* 400* 200* Surface Water Standard u /L WS-II, HQW 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 0.32 ' 20 ' 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-7 (MW-6D) 10/25/1995 ND ND ND ND 57,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/12/95 ND ND ND ND 80,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 04/15/97 ND ND ND ND 40,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 07/16/97 ND ND ND ND 42,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/20/97 ND ND ND ND 43,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/9/1999 ND ND ND ND 25,900 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/23/1999 ND ND ND ND 10,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1/31/2001 <1.0 <1.0 <1.0 <3.0 17,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 22,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 4 <1.0 <1.0 <3.0 12,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 7.1 <1.0 <1.0 <3.0 15,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <50.0 <50.0 <50.0 <50.0 4,120 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 5.1 <1.0 <1.0 <1.0 2,890 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 38 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 6.5 <1.0 <1.0 <3.0 1,800 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1 <1.0 <1.0 <3.0 2.7 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 <0.5 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 2.8 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 12J <25 <100 Page 5 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, INC Sample ID Sample Data Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH = 0) C 07 m N y L a+ W 07 d 7 O H ra H N C Q T X L d d s' _ T W - m 0) M y c a+ G M y V Q C V >4 t C Q m i r 2. O C (D In N �' L 0) t Q K m L LU .�.. N_ Q m C i O 7 I LL C 0) O 3 E: m c W 0) t a C T (L y m a to M U T r U m t Q 00 L) T L) m t Q N_ L) M L) N L)R m L) 1n L) 2 E O Q O_ L) M U M E O Q N U r r U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,00W 700* 400* 200* Surface Water Standard u /L WS-II, HQW 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 0.32 ' 20 ' 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-8 2/17/2000 ND ND ND ND 13,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 26,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 1 <3.0 500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 69 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 680 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 <1.0 <1.0 <1.0 <1.0 68.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 2,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 <1.0 <1.0 <1.0 <3.0 13,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 <1.0 <1.0 <1.0 <3.0 80 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 340 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 <10 <10 <10 <30 130 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2005 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 <1.0 <1.0 <1.0 <3.0 9,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 860 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 <1.0 <1.0 <1.0 <3.0 2,800 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 <1.0 <1.0 <1.0 <3.0 1,600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 <0.5 <1.0 <1.0 <3.0 580 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 <0.5 <1.0 <1.0 <3.0 640 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 <1.0 <1.0 <1.0 <2.0 722 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 <1.0 <1.0 <1.0 <2.0 475 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 <1.0 <1.0 <1.0 <2.0 231 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 <2.0 <2.0 <2.0 <6.0 215 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 <1.0 <1.0 <1.0 <2.0 404 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 <1.0 <1.0 <1.0 <2.0 37.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 <1.0 <1.0 <1.0 <3.0 28.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 <1.0 <1.0 <1.0 <2.0 43.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 <1.0 <1.0 <1.0 <2.0 27.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 <1.0 <1.0 <1.0 <2.0 22.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 <1.0 <1.0 <1.0 <2.0 3.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 <1.0 <1.0 <1.0 <2.0 27.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 <1.0 <1.0 <1.0 <2.0 24.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2015 <0.5 <0.5 <0.5 <1.5 <0.5 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <200 <200 <100 <100 <100 <200 12/4/2015 <1.0 <1.0 <1.0 <1.0 18 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 191 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 16 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 7.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 <1.0 <1.0 <1.0 <3.0 9.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 <0.50 <0.50 <0.50 <0.50 7.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 <0.50 <0.50 <0.50 <0.50 11 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 <0.50 <0.50 <0.50 <0.50 6.6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA �NA 2/15/2019 <0.50 <0.50 <0.50 <0.50 10 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Page 6 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, INC Sample ID Sample Data Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH = 0) C 07 m N y L a+ W 07 d 7 O H ra H N C Q T X L d d s' _ T W - m 0) M y c a+ G M y V Q C V >4 t C Q m i r 2. O C (D In N �' L 0) t Q K m L LU .�.. N_ Q m C i O 7 I LL C 0) O 3 E: m c W 0) t a C T (L y m a to M U T r U m t Q 00 L) T L) m t Q N_ L) M L) N L)R m L) 1n L) 2 E O Q O_ L) M U M E O Q N U r r U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,00W 700* 400* 200* Surface Water Standard u /L WS-II, HQW 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 0.32 ' 20 ' 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-13 10/20/1997 ND ND ND ND 23,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/1998 190 ND ND ND 31,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18-19/98 3 ND ND ND 4,300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 9 ND ND ND 10,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 530 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 1,200 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 1.8 <1.0 <1.0 <3.0 510 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 2.9 <1.0 <1.0 <3.0 410 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 5.2 <1.0 <1.0 <3.0 290 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 1.2 <1.0 <1.0 <3.0 160 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2002 3.3 <1.0 <1.0 <1.0 134 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/18/2003 <1.0 <1.0 <1.0 <1.0 1.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2003 8.3 <1.0 <1.0 <3.0 45 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2004 1.0 <1.0 <1.0 <3.0 3.8 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2004 <1.0 <1.0 <1.0 <3.0 18 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2005 1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/17/2005 2.6 <1.0 <1.0 <3.0 5.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/22/2006 86 3.5 2.4 1.2 14.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2006 <1.0 <1.0 <1.0 <3.0 2.6 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/20/2007 3.5 <1.0 <1.0 <3.0 6.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2007 31 <1.0 <1.0 <3.0 6.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/25/2008 10 <1.0 <1.0 <3.0 2.9J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/28/2008 7.6 <1.0 <1.0 <3.0 3.8J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/11/2009 <1.0 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/20/2009 5.7 <1.0 <1.0 <2.0 1.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2010 2.1 <1.0 <1.0 <2.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/12/2010 8.3 <1.0 <1.0 <3.0 3.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2011 7.8 <1.0 <1.0 <2.0 6.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 9/8/2011 25.4 <1.0 <1.0 <2.0 1.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/13/2012 27.5 <1.0 <1.0 <3.0 3.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/3/2012 NS INS INS INS INS NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/4/2013 17.6 <1.0 <1.0 <2.0 2.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/29/2013 1.4 <1.0 <1.0 <2.0 1.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/19/2014 6.6 <1.0 <1.0 <2.0 3.8 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/25/2014 14.0 <1.0 <1.0 <2.0 4.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2015 4.6 <1.0 <1.0 <2.0 5.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/18/2015 6.4 <0.5 <0.5 <1.5 1.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <200 <200 <100 53.9J <100 <200 12/4/2015 7.1 <1.0 <1.0 <1.0 9.0 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 191 130 <25 <100 2/16/2016 32 1.3 0.85 1.00 5.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 6.6 <1.0 <1.0 <3.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/7/2017 1.3 <1.0 <1.0 <3.0 3.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/15/2017 0.69 <0.50 <0.50 <0.50 8.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2018 1.9 <0.50 <0.50 <0.50 0.87 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2018 5.2 <0.50 <0.50 <0.50 2.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/15/2019 48 1.6 1.4 2.0 2.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Page 7 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, INC Sample ID Sample Data Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH = 0) C 07 m N y L a+ W 07 d 7 O H ra H N C Q T X L d d s' _ T W - m 0) M y c a+ G M y V Q C V >4 t C Q m i r 2. O C (D In N �' L 0) t Q K m L LU .�.. N_ Q m C i O 7 I LL C 0) O 3 E: m c W 0) t a C T (L y m a to M U T r U m t Q 00 L) T L) m t Q N_ L) M L) N L)R m L) 1n L) 2 E O Q O_ L) M U M E O Q N U r r U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,00W 700* 400* 200* Surface Water Standard u /L WS-II, HQ!! 1.19 68 ' 11 670 Z 19 Z 70 ' 300 ' 0.0028 0.32 ' 20 ' 50 ' NE 20 ' S 180 S Z 180 S Z 125 S Z NE NE MW-17 (MW-TR1U) 8/18/1998 38 ND ND ND 3,500 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 57 ND ND ND 2,400 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 23 ND ND ND 370 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 86 18 6 ND 170 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 50 7.9 2.2 <3.0 100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 21 1.9 1.6 <3.0 21 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 16 1.4 <1.0 <3.0 20 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 11 <1.0 <1.0 <3.0 12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 0.55J <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 110 <75 71 J <25 <100 MW-18 (MW-TR1D) 8/18-19/98 ND ND ND ND 240 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/1999 ND ND ND ND 70 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/1999 ND ND ND ND 20 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/17/2000 ND ND ND ND 5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2000 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/23/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/16/2001 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/27/2002 <1.0 <1.0 <1.0 <3.0 <5.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 12/4/2015 <1.0 <1.0 <1.0 <1.0 0.43J <2.0 <2.0 1 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 1 <25 <100 MW-23 12/3/2015 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <2.0 1 <2.0 1 <2.0 1 <10 <2.0 <2.0 <2.0 <2.0 <100 140 <75 1 <75 1 <25 <100 MW-24 12/4/2015 1.01 14 <5.0 <5.0 <5.0 14 4.3J 1.9J 1.2J <50 9.3J 2.8J 7.4J 7.3J <100 160 640 1,100 750 410 2/16/2016 8.7 8.7 2.0 J 3.9 <2.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 4.2 4.1 1.4 <3.0 NA 10.2 4.9J <0.33 <0.21 <0.79 11.5 2.1 J 8.7 6.3 <100 <100 393 2,050 730 276 2/7/2017 4.7 4.8 1.3 <3.0 NA 9.2 4.8J 1.OJ <0.21 <0.79 10.6 1.5J 7.3 6.6 <100 101 564 1,520 783 244 8/15/2017 1.4 3.9 0.53 0.88 NA 4.8J 1.9J 0.77J 0.29J <8.0 6.8J <8.0 1.5J 5.5J <120 <120 340 660 280 180 2/1/2018 t 1.7 1.8 0.63 0.75 NA 8.6J 2AJ <16 <16 <16 8.9J <16 <16 7.1J <100 <100 280 620 280 160 8/16/2018 2.0 1.8 0.64 1.2 NA 5.7J 2.2J <16 <16 <16 4.1 J <16 2.1 J 3.1 J <100 <100 410 740 330 130 2/15/2019 13 14 3.3 7.4 NA 7.0 2.9 J <3.2 <3.2 <16 7.9 <3.2 2.3 J 6.2 190 260 400 1,900 520 320 MW-25 12/4/2015 <1.0 <1.0 <1.0 <1.0 1.1 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 1.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 2/7/2017 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 8/15/2017 0.61 <0.50 <0.50 <0.50 NA <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 0.62J <110 <110 <75 <75 <25 <110 2/1/2018 <0.50 <0.50 <0.50 <0.50 NA <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 0.68J <100 <100 <75 <75 <25 <100 8/16/2018 <0.50 <0.50 <0.50 <0.50 NA <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 <8.0 0.51 J <100 <100 <75 <75 <25 <100 2/15/2019 <0.50 <0.50 <0.50 <0.50 NA <1.6 <1.6 <1.6 <1.6 <8.0 <1.6 <1.6 <1.6 <1.6 <100 <100 <75 <75 <25 <100 MW-25D 12/4/2015 <1.0 <1.0 <1.0 <1.0 1.2 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 100 <75 <75 <25 <100 2/16/2016 <0.5 <0.5 <0.5 <0.5 1.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8/19/2016 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 2/7/2017 <1.0 <1.0 <1.0 <3.0 NA <0.25 <0.14 <0.33 <0.21 <0.79 <0.21 <0.21 <0.22 <0.19 <100 <100 <50.0 <50.0 <50.0 <100 8/15/2017 <0.50 <0.50 <0.50 <0.50 <0.50 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <1.6 <100 <100 <75 <75 <25 <100 2/1/2018 t <0.50 <0.50 <0.50 <0.50 <0.50 <1.6 <1.6 <1.6 <1.6 0.75J <1.6 <1.6 <1.6 <1.6 <100 <100 <75 <75 <25 <100 8/16/2018 <0.50 <0.50 <0.50 <0.50 NA <1.6 <1.6 <1.6 <1.6 <8.0 <1.6 <1.6 <1.6 <1.6 <100 <100 <75 <75 <25 <100 2/15/2019 <0.50 <0.50 <0.50 <0.50 NA <1.6 <1.6 <1.6 <1.6 <8.0 <1.6 <1.6 <1.6 <1.6 NA NA <75 <75 <25 NA Page 8 of 9 Table 4 Groundwater Analytical Data Colonial Pipeline Company Kannapolis Booster Station Concord, NC Volatile Organic Compounds Method 6200B Semi Volatile Organic Compounds Method 625 MADEP-EPH/VPH L 0) d d t Sample ID Sample Data CD m Q yU 0 N 2 a� L m G t L R E E d N L Q Q Q Q Q N y 07 N '�" T W Q. <�,1 @ lJl C C C M U 00 N_00 _O N d 7 C 0) r m y t N �' i O 0) O C 4) U U U U V = 07 L a+ O T 0) V C c (D L .N.. N_ 7 3 0) t T O1 T T LO M m W H X M Q Q In I U m V_ LL ILa U U U U U U NCAC 2L Standard (ug/L) 1 600 600 500 20 80 2,000 0.05 5 3 300 300 200 200 10,000* 700* 400* 200* Surface Water Standard u /L WS-II, HQW 1.19 1 68 ' 11 1 670 z 19 z 70 ' 300 ' 0.0028 0.32(1)1 20 ' 50 ' NE 20 ' S 180 (S)(2) 1 180 (S)(2) 125 (S)(2) NE NE Quality Assurance / Qualit Control Samples Dup-1 (MW-4) 8/18/2015 <0.5 <0.5 <0.5 <1.5 <0.5 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <4.8 <190 <190 <100 <100 <100 <190 Dup120415 (MW-25D) 12/4/2015 <1.0 <1.0 <1.0 <1.0 1.1 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 <100 <75 <75 <25 <100 Dup12032015 (MW-2) 12/3/2015 <1.0 <1.0 <1.0 <1.0 5.2 <2.0 <2.0 <2.0 <2.0 <10 <2.0 <2.0 <2.0 <2.0 <100 100 <75 <75 <25 <100 KSDUP (MW-24) 2/16/2016 7.7 12 2.1 J 3.8 <2.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP081916 (MW-8) 8/19/2016 <1.0 <1.0 <1.0 <3.0 7.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP020717 (MW-8) 2/7/2017 <1.0 <1.0 <1.0 <3.0 9.5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP08152017(MW-13) 8/15/2017 0.75 <0.50 <0.50 <0.50 7.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP-1 (MW-8) 2/1/2018 <0.50 <0.50 <0.50 <0.50 9.7 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA DUP-1(MW-24) 8/16/2018 1.8 1.9 0.61 1.1 <0.50 5.9J 2.1J <16 <16 <80 3.7J <16 1.9J 28J <100 <100 340 700 360 110 DUP21519(MW-13) 02/15/19 48 1.6 1.3 2.0 3.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA Notes: All concentrations reported in micrograms per liter (Ng/L) MADEP = Massachusetts Department of Environmental Protection EPH = Extractable Petroleum Hydrocarbons VPH = Volatile Petroleum Hydrocarbons WS-II = Water Supply Class II HQW = High Quality Waters NE = No standard established NA = Not analyzed ND = Not detected Bold = Detection exceeds North Carolina Administrative Code (NCAC) 2L Groundwater Standard Gray fill indicates detection above the applicable Surface Water Standards (Indicated with superscript numerals 1 and 2) No superscript numeral indicates the NCAC 213 Surface Water Standard for Water Supply (WS) ll, High Quality Waters (HQW) classification (') = Environmental Protection Agency Nationally Recommended Water Quality Criteria for Aquatic Life and Human Health. (2) = North Carolina Protective Values for Surface Waters = Analyte was not detected at or above the reporting limit shown. Final and interim groundwater quality standards "J" = Estimated concentration between the method detection limit and the reporting limit. "S" = Solubility exceeds toxicity; therefore, standard is met if no sheen is present on water surface or shoreline t = Additional analytes were detected in these wells during the sampling event flagged: MW-24: Benzo(a)pyrene at an estimated concentration of 1.0 pg/L which is above the 2L Standard of 0.005 pg/L and 213 Standard of 0.0028 pg/L for Total PAHs combined. MW-25D: Di-n-butyl phthalate at an estimated concentration of 0.44 tag/L which is below the 2L Standard of 700 pg/L and the 2B Standard of 20 pg/L. Monitor Well naming convention was modified January 2001. Former well designation in parentheses. Page 9 of 9 FIGURES i APEX SITE LOCATION N ;U.SGS The National Map: National Boundaries Dataset, 3DEP Elevation Program, Geographic Names Information System, National Hydrography Dataset, National Land Cover Database, National Structures Dataset, and National Transportation Dataset; USGS Global Ecosystems; U.S. Census Bureau;TTIGER/Line data; USFS Road Data; Natural Earth Data; U.S. 0 1,000 2,000 Department of State -Humanitarian Information Unit; and NOAA National Centers _for Environmental Information, U.S. Coastal Relief Model. Data Feet refreshed October 2018. CHECK BY: AS FIGURE DRAWN BY: SP SITE LOCATION MAP DATE: 3/13/19 SCALE: AS SHOWN COLONIAL PIPELINE COMPANY CAD NO.: CPC19014.001 KANNAPOLIS BOOSTER STATION r CONCORD, NORTH CAROLINA L PRJ NO.: CPC19014.001 A x J x r��,'. •. s MW-4 `�S•_ Q�MW-23 1i• _ l.ynN,�'a•• �.; F`t•- .Iirr�� !� ASPHALTPgyED _- I r 1 r`•T • F`'". ,�. l ICUPOWER COMPA Y o \ � •t , �.1 `` �Cr'1 , •`; • y �• .•x-I; SUBSTATION MW-24 r •� _ . !.. ,may, ,! \1�, • rQ-6 LINE 2 �•` ~ 'I .F _ ,�i� ,y MANIFOLd',•'- cc 1 — A A � y- t `• ,1i \� 1° 1 .•zG, . M W-25 1 � . A �� f [ YMW-25D I � r MW-5 24" CMP .y r • .� LINE 1 — MANIFOLD 1 x 1MW-31'ttit � 7[C I PZ-4 '• MW-6 x I ' 1. I J / / AITRENCHE� U r ;T TRENCH �pl PZ_3 I s / x M W-1 SPAR GE 4 " ' SYSTEM PAD I M�W-22 I TREATMENT c U SYSTEM PAD LINE 1 t PIG SIGNAL k POTABLE WATER MW-19Q�PZ-2 I ! 10 SUPPLY WELL MAllZ "p'-• CHECK BY AS DRAWN BY SP Y ' DATE 3/13/19 SITE PLAN SCALE AS SHOWN COLONIAL PIPELINE COMPANY CAD NO. CPC19014.001 KANNAPOLIS BOOSTER STATION PRJ NO. CPC19014.001 CONCORD, NORTH CAROLINA LEGEND - - - PROPERTY LINE —x FENCE LINE -G COLONIAL PIPELINE? ANCILLARY PIPING e MW-1 SHALLOW MONITORING WELL MW-2 DEEP MONITORING WELL MW-11 ABANDONED MONITORING WELL I9 RW-15 RECOVERY WELL 0 PZ-1 PIEZOMETER 0 PIG -SIGNAL SCALE IN FEET 0 40 80 160 WELL DESIGNATION UPDATE FORMER WELL NAME NEW WELL NAME MW-1 MW-1 MW-2 ABANDONED — MW-2D MW-2 MW-3 MW-3 MW-4 MW-4 MW-5 MW-5 MW-6 MW-6 MW-6D MW-7 MW-7 ABANDONED — MW-8 MW-8 MW-9D MW-9 MW-1 OD MW-10 MW-11 ABANDONED MW-11 ABANDONED MW-12D MW-12 MW-13 MW-13 MW-14 ABANDONED — MW-15 ABANDONED — MW-16 ABANDONED — MW-17 MW-14 MW-17D RECOVERY WELL MW-15 CROWE WELL MW-16 TR-1U MW-17 TR—iD MW-18 TR-2U MW-19 TR-2D MW-20 TR-3U MW-21 TR-3D MW-22 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. FIGURE 2 APEX LEGEND — — PROPERTY LINE X FENCE LINE c COLONIAL PIPELINE' ANCILLARY PIPING' ASPHALT PAVED SB-1 RECOVERY WELL 1W SB-7 RECOVERY WELL ABANDONED FREE PRODUCT EXTENT SB-11 BV-1 BIO—VENTING WELL BS-1 BIO—SPARGE WELL ®BV-1 BS-1 ® BV-3 (SVE-5) BV-2 SB-14 SB-6� SB- Ig SB-10 19 RW-02 BV-4 SSB/ SB-157 BS-3 SB-1 (�� c CD • - SB-5 RW-01 "SB-1 SB-13 BS-2 0 SB-12 B-19 1w SB-7 B-17 CHECK BY AS DRAWN BY SP DATE 3/18/19 SCALE AS SHOWN CAD NO. CPC19014.001 PRJ NO. CPC19014.001 RECOVERY WELL LOCATIONS FEBRUARY 15, 2019 COLONIAL PIPELINE COMPANY KANNAPOLIS BOOSTER STATION CONCORD, NORTH CAROLINA SCALE IN FEET 0 10 20 40 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. FIGURE .� 3 APEX LEGEND i i 1 1 I 1 I 1 1 DUKE POWER COMPANY I 1 I 1 I 1 24" I 1 I I 1 1 I 1 } 1 3 I 1 O I 1 K I i a 1 W 1 � IO 1 1 I 1 1 L _-- PZ- 703.44 f� i w-1s x 1 CHECK BY AS DRAWN BY SP DATE 3/13/19 SCALE AS SHOWN CAD NO. CPC19014.001 PRJ NO. CPC19014.001 POND — — PROPERTY LINE X FENCE LINE COLONIAL PIPELINE' ANCILLARY PIPING' 0 MW-1 SHALLOW MONITORING WELL MW-2 DEEP MONITORING WELL MW-11 ABANDONED MONITORING WELL 19 RW-15 RECOVERY WELL 0 PZ-1 PIEZOMETER 0 PIG —SIGNAL GROUNDWATER POTENTIOMETRIC CONTOUR (FT. MSL) (DASHED WHERE INFERRED) 718.70 GROUNDWATER ELEVATION (FT. MSL) y ESTIMATED GROUNDWATER FLOW DIRECTION SCALE IN FEET 0 40 80 160 WELL DESIGNATION UPDATE FORMER WELL NAME NEW WELL NAME MW-1 MW-1 MW-2 ABANDONED MW-2D MW-2 MW-3 MW-3 MW-4 MW-4 MW-5 MW-5 MW-6 MW-6 MW-6D MW-7 MW-7 ABANDONED - MW-8 MW-8 MW-9D MW-9 MW-10D MW-10 MW-11 ABANDONED MW-11 ABANDONED MW-12D MW-12 MW-13 MW-13 MW-14 ABANDONED MW-15 ABANDONED MW-16 ABANDONED MW-17 MW-14 MW-17D RECOVERY WELL MW-15 CROWE WELL MW-16 TR-1U MW-17 TR-1D MW-18 TR-2U MW-19 TR-2D MW-20 TR-3U MW-21 TR-3D MW-22 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. GROUNDWATER POTENTIOMETRIC SURFACE MAP SURFICIAL SAPROLITE UNIT — FEBRUARY 15, 2019 COLONIAL PIPELINE COMPANY KANNAPOLIS BOOSTER STATION CONCORD, NORTH CAROLINA APEX FIGURE 4 DUKE POWER COMPANY IIII ' I I 1 �x x-x-x� I I1 1 1 I MW-4 1 1qv x Q MW-230.50 � 1 x 1 Ix ASPHALT PAYED I 1 O BV-1 1 0 _I_ B SUB STATION 1 x _ _ I 2 M13 J 13 LINE MANIFOLD B\ 1 n I BS-3 E? - x m BV-3 (SVE- NW 1 G7 I MW-5 1 24" CMP o I _ LINE 1 - - - - - MANIFOLD x 1 1 MW-, I M W-6<0.50 x 1 1 I 1 1 x I MW-1 I 1 Ix MW-12 1 LINE 1 RETENTION POND Plc SIGNAL x POTABLE WATER Q, 1 SUPPLY WELL MW IPZ- 425 i W-18 BMW-14 or) MW-15 �� X (RW-15) _ 1 PRJ NO. CPC19014.001 BENZENE ISOCONCENTRATION MAP FEBRUARY 15, 2019 I COLONIAL PIPELINE COMPANY KANNAPOLIS BOOSTER STATION CONCORD, NORTH CAROLINA LEGEND - - PROPERTY LINE x FENCE LINE COLONIAL PIPELINE' ANCILLARY PIPING' 0 MW-1 SHALLOW MONITORING WELL MW-2 DEEP MONITORING WELL MW-11 ABANDONED MONITORING WELL * RW-1 RECOVERY WELL O PZ-1 PIEZOMETER 0 PIG -SIGNAL ® BV-1 BIO-VENTING WELL BS-1 BIO-SPARGE WELL !'1 — BENZENE ISOCONTOUR (DASHED WHERE INFERRED) 13 BENZENE CONCENTRATION (ug/L) 2B STANDARD FOR BENZENE IS 1.19 MICROGRAM PER LITER (ug/L) 2L STANDARD FOR BENZENE IS 1 ug/L <0.50 BENZENE NOT DETECTED AT OR ABOVE REPORTING LIMIT 1�1 SCALE IN FEET 0 40 80 160 WELL DESIGNATION UPDATE FORMER WELL NAME NEW WELL NAME MW-1 MW-1 MW-2 ABANDONED MW-2D MW-2 MW-3 MW-3 MW-4 MW-4 MW-5 MW-5 MW-6 MW-6 MW-6D MW-7 MW-7 ABANDONED MW-8 MW-8 MW-9D MW-9 MW-10D MW-10 MW-11 ABANDONED MW-11 ABANDONED MW-12D MW-12 MW-13 MW-13 MW-14 ABANDONED - MW-15 ABANDONED - MW-16 ABANDONED MW-17 MW-14 MW-17D RECOVERY WELL MW-15 CROWE WELL MW-16 TR-1U MW-17 TR-1D MW-18 TR-2U MW-19 TR-2D MW-20 TR-3U MW-21 TR-3D MW-22 NOTES: 1. ANCILLARY PIPING AND COLONIAL PIPELINE LOCATIONS ARE APPROXIMATE AND ARE FOR FIGURE PURPOSES ONLY. 2. MAP BASED OFF DRAWING ENTITLED "FACILITY MAP" DATED APRIL 1, 2014 COMPLETED BY PROGRESSIVE ENGINEERING AND CONSTRUCTION, INC. FIGURE vA "" 5 APEX GROUNDWATER SAMPLING FIELD LOGS i APEX C) O J J J W Q Q y 2 F 0 Q Q j O cc C7 O ° N FV a c � N c � O a 0 o o U m c o io � E a N a LL E E U o i N1f an d �' ro N Z ;m✓ o N m r s U o N c c m w ° a a v a a o ° N m y N U .o m `6 3 3 a' a ' O z N 2` o mo F Z E Co Icz U�zz >. Q .N m 0 uo. f rn U s r. J L m •�"x. Of- a XN JNro :. CN N Qzo . r(y •q �"' ° 9 ll _ O o a? a° o m E mu 0 A I f .N. aKi croi s m 0aai U a 0 J0 J J a w� C0 O W U � aW p 6 Z 7 cc V me 'J N U a m T � y- N O 0 �J o42 o c m U d m 17- o � m E U a z o m E o y S r E V5 N j UL6O N N > E O a m m r s pro 'c U O ui N N U -a)a m W m a N ~O z N c E jVl m � ❑ E � � +. ¢ z z } r� z� LL 2i d 2i m e co J a �n N � r a O N ILO O) NI lN. TO O N N a J N `U^• C N m N m z ❑ J ao 0 E2 �? m a 3 n o m o C ro P, a y Y a m d E F c E 'BE Q m U ® v o aroi a m o ro d m r a O J U C7 J J W ZIL M N M H 0a 0 Q j O C9 2 o N C � N C � O C � 8 m � 3 o 12 R Y E r w a a i Z R fl R U p U >' N E 'c o j rn a m .. = o N o m � R c o .. J O m O y E o o E _' w d E 3 m d m x ._ E E 3 3 L ' o z a +. d 'c Ch7 o o a K Z' E y ,E: m m ❑ ,,E. o m ¢ z z 'a E: .. m E - uj R ~ Y C M 3 R 3 OJ > N c JE J C^. cL E N N �) V O2 N O c R R E N R O pm > p a a .R �rE «❑0W) +Z C«3' . 5 3roHE h maO ° . . > U cC ❑ ❑ F 3> 3 H } O Z m } N o N v d R � E N N d R 4 a R E 1 n ce N �r E R 3 a 0 0 00 J J W Q QLu y a oc O� U IL 0 m 0 a r o d « 1 � d o a LL o. w' Z m«' d r E1d m E o �rS o E o tron 3 m d > m t� o o U 'c `o O O in 6 w .. y O O C O -P" ? J a d a O 1N N O O O a co `%" m F ri n a' w � 3 z y a a F o � J a m z a ¢ > r s. o O E � 'v, Cao°3 r c m o d ro 0.. d �j� \ * ll 3 N O. CO U czy M N U S E F sa 3 d a p 0 3> 5 o 0 a a c: Vj IN 0 Nn i E E O N E o 2 U ro ro o, Z ,o: LL > jr4 c y w a o m E m c a n .y rn o C ca R d m m n n o o¢ 9 u ow co)3 3 3 O Z 3 'O C � R Uj C �`r O a o 0 O c fn � R � R U R CJ R w m a m o a a a aci E E w o uS g Z rn d 0 3 m d _ c R a m 3 0 L p E ` " 3 gm a R t o 0 c R g L m R E o u `o m o J as a y E O olid O di d R y m U a `R = m IL a O z° w `— E _ Li R E o O m Z J N + Car 0 w o O � _ O > J U) U Y + v 11T a N I rr ¢ V 0 J i a J.. 1 ^ V, O o d y NE2 ❑ ! �� O r co N c d O` R L ? N O C o o R d, o y m ¢¢ a 3 O U 'a R C 2 N C (7 O a 0 o O flyN r OO R R E R N N ^4 U R R N Lu 3 E > 0 o CO 3 R d N t L O U m R 0 O O E a Y R a a R ro c H n W E 3 3 3 a' a- O z A � + o n ,Z F Z' E E W R ro U m � E E V o Q z z _ e m D m>0>>0 m a ° o) l U U U c _` M ci H � R c m D z a R to Li c a o 0 r E `o O O N U C j AA U. o a 9 0 0 o° �. 3 0 Y O Z 3 9 co } I O O J J0 J J Ca w aIL M H O Q U IL O cc C9 O 'a O d c N J c CJ C IV a.._ U ,.t. a y f of E R d N a N a a d E N a s' o � a` 0 W Z d ry m awo N m 3 o (A m L O .E O O N ¢ W N N O l0 a .n m n G w w E D S .- R w3 d m z N s c J m ❑ �I\J K] o H u z cc z z a a > o m a �S N o J •.. ri+ 3 a ° J F c LL orn ,d o^_ o r o S ¢ > d �+ J N E 0 S II .. _ ci c > 'm co .A o' o // �4`0 3 o Z a N a o U � .c .c ❑ � ¢ E IE T8 I R k m c m 7 9 x C nn N N E U ) N APPENDIX B LABORATORY ANALYTICAL REPORTS i APEX SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis Apex Companies, LLC 10610 Metromont Parkway Suite 206 Charlotte, NC 28269 Attention: Andrew Street Project Name: CPC-Kannapolis Project Number: CPC19014 Lot Number:UB18028 Date Completed:02/28/2019 03/01 /2019 9:32 AM Approved and released by: Lab Director - Greenville: Lucas Odom PCCRFp 4 / AM AC CF ED I T E D 11900 eLAa The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 62 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative Apex Companies, LLC Lot Number: UB18028 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. SVOCs by GC/MS The following samples werediluted due to the nature of the sample matrix: UB18028-003, UB18028-006. The LOQ has been elevated to reflect the dilution. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 62 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary Apex Companies, LLC Lot Number: UB18028 Sample Number Sample ID Matrix Date Sampled Date Received 001 MW-25D Aqueous 02/15/2019 0930 02/18/2019 002 MW-4 Aqueous 02/15/20191005 02/18/2019 003 MW-25 Aqueous 02/15/20191015 02/18/2019 004 MW-6 Aqueous 02/15/20191030 02/18/2019 005 MW-8 Aqueous 02/15/20191115 02/18/2019 006 MW-24 Aqueous 02/15/20191230 02/18/2019 007 MW-13 Aqueous 02/15/20191235 02/18/2019 008 EB-1 Aqueous 02/15/20191030 02/18/2019 009 DUP21519 Aqueous 02/15/2019 02/18/2019 010 TB Aqueous 02/15/2019 02/18/2019 (10 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 62 SHEALY ENVIRONMENTAL SERVICES, INC. Detection Summary Apex Companies, LLC Lot Number: UB18028 Sample Sample ID Matrix Parameter Method Result Q Units Page 005 MW-8 Aqueous Methyl tertiary butyl ether SM 6200B- 10 ug/L 15 006 MW-24 Aqueous Benzene SM 6200B- 13 ug/L 16 006 MW-24 Aqueous Ethylbenzene SM 6200B- 14 ug/L 16 006 MW-24 Aqueous Toluene SM 6200B- 3.3 ug/L 16 006 MW-24 Aqueous Xylenes (total) SM 6200B- 7.4 ug/L 16 006 MW-24 Aqueous Acenaphthene 625.1 7.0 ug/L 16 006 MW-24 Aqueous Anthracene 625.1 2.9 J ug/L 16 006 MW-24 Aqueous Fluoranthene 625.1 7.9 ug/L 17 006 MW-24 Aqueous 1-Methylnaphthalene 625.1 4.1 ug/L 17 006 MW-24 Aqueous Naphthalene 625.1 4.5 ug/L 17 006 MW-24 Aqueous Phenanthrene 625.1 2.3 J ug/L 17 006 MW-24 Aqueous Pyrene 625.1 6.2 ug/L 17 006 MW-24 Aqueous C11 - C22 Aromatics MADEP-EPH- 320 ug/L 18 006 MW-24 Aqueous C9 - C18 Aliphatics MADEP-EPH- 260 ug/L 18 006 MW-24 Aqueous C19 - C36 Aliphatics MADEP-EPH- 190 ug/L 18 006 MW-24 Aqueous C5 - C8 Aliphatics MADEP-VPH- 1900 ug/L 18 006 MW-24 Aqueous C9 - C12 Aliphatics MADEP-VPH- 400 ug/L 18 006 MW-24 Aqueous C9 - C10 Aromatics MADEP-VPH- 520 ug/L 19 007 MW-13 Aqueous Benzene SM 6200B- 48 ug/L 20 007 MW-13 Aqueous Ethylbenzene SM 6200B- 1.6 ug/L 20 007 MW-13 Aqueous Methyl tertiary butyl ether SM 6200B- 2.7 ug/L 20 007 MW-13 Aqueous Toluene SM 6200B- 1.4 ug/L 20 007 MW-13 Aqueous Xylenes (total) SM 6200B- 2.0 ug/L 20 009 DUP21519 Aqueous Benzene SM 6200B- 48 ug/L 22 009 DUP21519 Aqueous Ethylbenzene SM 6200B- 1.6 ug/L 22 009 DUP21519 Aqueous Methyl tertiary butyl ether SM 6200B- 3.0 ug/L 22 009 DUP21519 Aqueous Toluene SM 6200B- 1.3 ug/L 22 009 DUP21519 Aqueous Xylenes (total) SM 6200B- 2.0 ug/L 22 (28 detections) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-001 Description: MW-25D Matrix: Aqueous Date Sampled:02/15/2019 0930 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 02/21/2019 1457 BWS 98301 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 95 70-130 1,2-Dichloroethane-d4 106 70-130 Toluene-d8 96 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 02/24/2019 1805 CMP2 02/20/2019 1632 98194 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 625.1 ND 1.6 0.80 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 1.6 0.80 ug/L 1 Anthracene 120-12-7 625.1 ND 1.6 0.80 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 1.6 0.80 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 1.6 0.80 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 0.80 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 0.80 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 0.80 ug/L 1 Benzyl alcohol 100-51-6 625.1 ND 3.2 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 0.80 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 0.80 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1.6 0.80 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 0.80 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 0.80 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 0.80 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 0.80 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 1.6 0.80 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 0.80 ug/L 1 Chrysene 218-01-9 625.1 ND 1.6 0.80 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 0.80 ug/L 1 Dibenzofuran 132-64-9 625.1 ND 1.6 1.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 1.6 0.80 ug/L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 1.6 0.80 ug/L 1 1,4-Dichlorobenzene 106-46-7 625.1 ND 1.6 0.80 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-001 Description: MW-25D Matrix: Aqueous Date Sampled:02/15/2019 0930 Date Received:02/18/2019 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 02/24/2019 1805 CMP2 02/20/2019 1632 98194 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 0.80 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 0.80 ug/L Diethylphthalate 84-66-2 625.1 ND 1.6 0.80 ug/L Dimethyl phthalate 131-11-3 625.1 ND 1.6 0.80 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 0.80 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 0.81 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 0.80 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 0.80 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 1.6 0.80 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 0.80 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 4.0 ug/L Fluoranthene 206-44-0 625.1 ND 1.6 0.80 ug/L Fluorene 86-73-7 625.1 ND 1.6 0.80 ug/L Hexachlorobenzene 118-74-1 625.1 ND 1.6 0.80 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 1.6 0.80 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 4.0 ug/L Hexachloroethane 67-72-1 625.1 ND 1.6 0.80 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 0.80 ug/L Isophorone 78-59-1 625.1 ND 1.6 0.80 ug/L 1-Methylnaphthalene 90-12-0 625.1 ND 1.6 0.40 ug/L 2-Methylnaphthalene 91-57-6 625.1 ND 1.6 0.40 ug/L 2-Methylphenol 95-48-7 625.1 ND 1.6 0.67 ug/L 3+4-Methylphenol 106-44-5 625.1 ND 1.6 1.5 ug/L Naphthalene 91-20-3 625.1 ND 1.6 0.80 ug/L Nitrobenzene 98-95-3 625.1 ND 1.6 0.80 ug/L 2-Nitrophenol 88-75-5 625.1 ND 3.2 0.80 ug/L 4-Nitrophenol 100-02-7 625.1 ND 8.0 4.0 ug/L N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 0.80 ug/L N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 0.80 ug/L Pentachlorophenol 87-86-5 625.1 ND 8.0 4.0 ug/L Phenanthrene 85-01-8 625.1 ND 1.6 0.80 ug/L Phenol 108-95-2 625.1 ND 1.6 0.80 ug/L Pyrene 129-00-0 625.1 ND 1.6 0.80 ug/L 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 0.80 ug/L 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 0.80 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-001 Description: MW-25D Matrix: Aqueous Date Sampled:02/15/2019 0930 Date Received:02/18/2019 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 54 37-129 2-Fluorophenol 38 24-127 Nitrobenzene-d5 63 38-127 Phenol-d5 50 28-128 Terphenyl-d14 79 10-148 2,4,6-Tribromophenol 65 41-144 MADEP EPH (aliphatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 02/20/2019 1939 CHG 02/20/2019 0934 98139 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND 100 100 ug/L 1 C9 - C18 Aliphatics - Unfractionated MADEP-EPH-04 ND 100 100 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) - Unfractionated 101 40-140 MADEP EPH (aromatics) - Unfractionated Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 02/20/2019 1939 CHG 02/20/2019 0934 98140 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND 100 100 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) - Unfractionated 71 40-140 2-Fluorobiphenyl (fractionation 1) 84 40-140 2-Bromonaphthalene (fractionation 2) 86 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 02/20/20191734 JJG 98319 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-001 Description: MW-25D Matrix: Aqueous Date Sampled:02/15/2019 0930 Date Received:02/18/2019 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 115 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 02/20/20191734 JJG 98317 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 116 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-002 Description: MW-4 Matrix: Aqueous Date Sampled:02/15/2019 1005 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 02/21/2019 1520 BWS 98301 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 96 70-130 1,2-Dichloroethane-d4 104 70-130 Toluene-d8 96 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-003 Description: MW-25 Matrix: Aqueous Date Sampled:02/15/2019 1015 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 02/21/2019 1543 BWS 98301 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 95 70-130 1,2-Dichloroethane-d4 103 70-130 Toluene-d8 96 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 02/27/2019 1916 CMP2 02/20/2019 1632 98194 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 625.1 ND 1.6 0.80 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 1.6 0.80 ug/L 1 Anthracene 120-12-7 625.1 ND 1.6 0.80 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 1.6 0.80 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 1.6 0.80 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 0.80 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 0.80 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 0.80 ug/L 1 Benzyl alcohol 100-51-6 625.1 ND 3.2 2.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 0.80 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 0.80 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1.6 0.80 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 0.80 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 0.80 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 0.80 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 0.80 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 1.6 0.80 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 0.80 ug/L 1 Chrysene 218-01-9 625.1 ND 1.6 0.80 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 0.80 ug/L 1 Dibenzofuran 132-64-9 625.1 ND 1.6 1.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 1.6 0.80 ug/L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 1.6 0.80 ug/L 1 1,4-Dichlorobenzene 106-46-7 625.1 ND 1.6 0.80 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-003 Description: MW-25 Matrix: Aqueous Date Sampled:02/15/2019 1015 Date Received:02/18/2019 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 02/27/2019 1916 CMP2 02/20/2019 1632 98194 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 0.80 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 0.80 ug/L Diethylphthalate 84-66-2 625.1 ND 1.6 0.80 ug/L Dimethyl phthalate 131-11-3 625.1 ND 1.6 0.80 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 0.80 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 0.81 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 0.80 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 0.80 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 1.6 0.80 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 0.80 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 4.0 ug/L Fluoranthene 206-44-0 625.1 ND 1.6 0.80 ug/L Fluorene 86-73-7 625.1 ND 1.6 0.80 ug/L Hexachlorobenzene 118-74-1 625.1 ND 1.6 0.80 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 1.6 0.80 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 4.0 ug/L Hexachloroethane 67-72-1 625.1 ND 1.6 0.80 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 0.80 ug/L Isophorone 78-59-1 625.1 ND 1.6 0.80 ug/L 1-Methylnaphthalene 90-12-0 625.1 ND 1.6 0.40 ug/L 2-Methylnaphthalene 91-57-6 625.1 ND 1.6 0.40 ug/L 2-Methylphenol 95-48-7 625.1 ND 1.6 0.67 ug/L 3+4-Methylphenol 106-44-5 625.1 ND 1.6 1.5 ug/L Naphthalene 91-20-3 625.1 ND 1.6 0.80 ug/L Nitrobenzene 98-95-3 625.1 ND 1.6 0.80 ug/L 2-Nitrophenol 88-75-5 625.1 ND 3.2 0.80 ug/L 4-Nitrophenol 100-02-7 625.1 ND 8.0 4.0 ug/L N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 0.80 ug/L N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 0.80 ug/L Pentachlorophenol 87-86-5 625.1 ND 8.0 4.0 ug/L Phenanthrene 85-01-8 625.1 ND 1.6 0.80 ug/L Phenol 108-95-2 625.1 ND 1.6 0.80 ug/L Pyrene 129-00-0 625.1 ND 1.6 0.80 ug/L 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 0.80 ug/L 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 0.80 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-003 Description: MW-25 Matrix: Aqueous Date Sampled:02/15/2019 1015 Date Received:02/18/2019 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 64 37-129 2-Fluorophenol 38 24-127 Nitrobenzene-d5 66 38-127 Phenol-d5 50 28-128 Terphenyl-d14 67 10-148 2,4,6-Tribromophenol 79 41-144 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 02/25/2019 2012 CHG 02/20/2019 0934 98295 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) 73 40-140 2-Fluorobiphenyl (fractionation 1) 87 40-140 2-Bromonaphthalene (fractionation 2) 62 40-140 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 02/25/2019 1745 CHG 02/20/2019 0934 98294 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1 C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) 73 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 02/20/20191802 JJG 98319 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-003 Description: MW-25 Matrix: Aqueous Date Sampled:02/15/2019 1015 Date Received:02/18/2019 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 112 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 02/20/20191802 JJG 98317 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 111 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-004 Description: MW-6 Matrix: Aqueous Date Sampled:02/15/2019 1030 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 02/21/2019 1606 BWS 98301 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 99 70-130 1,2-Dichloroethane-d4 107 70-130 Toluene-d8 97 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 14 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-005 Description: MW-8 Matrix: Aqueous Date Sampled:02/15/2019 1115 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 02/21/2019 1629 BWS 98301 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- 10 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 96 70-130 1,2-Dichloroethane-d4 104 70-130 Toluene-d8 99 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 15 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-006 Description: MW-24 Matrix: Aqueous Date Sampled:02/15/2019 1230 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 SM 620013- SM 620OB-2011 1 02/26/2019 0127 KGT 98643 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 620013- 13 0.50 0.40 ug/L 2 Ethylbenzene 100-41-4 SM 6200113- 14 0.50 0.40 ug/L 2 Toluene 108-88-3 SM 6200113- 3.3 0.50 0.40 ug/L 2 Xylenes (total) 1330-20-7 SM 6200113- 7.4 0.50 0.40 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 97 70-130 1,2-Dichloroethane-d4 99 70-130 Toluene-d8 104 70-130 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 02/27/2019 1940 CMP2 02/20/2019 1632 98194 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acenaphthene 83-32-9 625.1 7.0 3.2 1.6 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 3.2 1.6 ug/L 1 Anthracene 120-12-7 625.1 2.9 J 3.2 1.6 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 3.2 1.6 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 3.2 1.6 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 3.2 1.6 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 3.2 1.6 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 3.2 1.6 ug/L 1 Benzyl alcohol 100-51-6 625.1 ND 6.4 4.0 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 3.2 1.6 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 3.2 1.6 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 3.2 1.6 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 3.2 1.6 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 3.2 1.6 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 3.2 1.6 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 3.2 1.6 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 3.2 1.6 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 3.2 1.6 ug/L 1 Chrysene 218-01-9 625.1 ND 3.2 1.6 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 3.2 1.6 ug/L 1 Dibenzofuran 132-64-9 625.1 ND 3.2 2.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 3.2 1.6 ug/L 1 1,3-Dichlorobenzene 541-73-1 625.1 ND 3.2 1.6 ug/L 1 1,4-Dichlorobenzene 106-46-7 625.1 ND 3.2 1.6 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 16 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-006 Description: MW-24 Matrix: Aqueous Date Sampled:02/15/2019 1230 Date Received:02/18/2019 Semivolatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 2 02/27/2019 1940 CMP2 02/20/2019 1632 98194 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 16 1.6 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 3.2 1.6 ug/L Diethylphthalate 84-66-2 625.1 ND 3.2 1.6 ug/L Dimethyl phthalate 131-11-3 625.1 ND 3.2 1.6 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 3.2 1.6 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 3.2 1.6 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 16 1.6 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 16 1.6 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 3.2 1.6 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 3.2 1.6 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 16 8.0 ug/L Fluoranthene 206-44-0 625.1 7.9 3.2 1.6 ug/L Fluorene 86-73-7 625.1 ND 3.2 1.6 ug/L Hexachlorobenzene 118-74-1 625.1 ND 3.2 1.6 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 3.2 1.6 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 16 8.0 ug/L Hexachloroethane 67-72-1 625.1 ND 3.2 1.6 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 3.2 1.6 ug/L Isophorone 78-59-1 625.1 ND 3.2 1.6 ug/L 1-Methylnaphthalene 90-12-0 625.1 4.1 3.2 0.80 ug/L 2-Methylnaphthalene 91-57-6 625.1 ND 3.2 0.80 ug/L 2-Methylphenol 95-48-7 625.1 ND 3.2 1.3 ug/L 3+4-Methylphenol 106-44-5 625.1 ND 3.2 3.0 ug/L Naphthalene 91-20-3 625.1 4.5 3.2 1.6 ug/L Nitrobenzene 98-95-3 625.1 ND 3.2 1.6 ug/L 2-Nitrophenol 88-75-5 625.1 ND 6.4 1.6 ug/L 4-Nitrophenol 100-02-7 625.1 ND 16 8.0 ug/L N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 3.2 1.6 ug/L N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 3.2 1.6 ug/L Pentachlorophenol 87-86-5 625.1 ND 16 8.0 ug/L Phenanthrene 85-01-8 625.1 2.3 J 3.2 1.6 ug/L Phenol 108-95-2 625.1 ND 3.2 1.6 ug/L Pyrene 129-00-0 625.1 6.2 3.2 1.6 ug/L 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 3.2 1.6 ug/L 2,4,6-Trichlorophenol 88-06-2 625.1 ND 3.2 1.6 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 17 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-006 Description: MW-24 Matrix: Aqueous Date Sampled:02/15/2019 1230 Date Received:02/18/2019 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 55 37-129 2-Fluorophenol 29 24-127 Nitrobenzene-d5 53 38-127 Phenol-d5 42 28-128 Terphenyl-d14 64 10-148 2,4,6-Tribromophenol 88 41-144 MADEP EPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 02/25/2019 2041 CHG 02/20/2019 0934 98295 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C11 - C22 Aromatics MADEP-EPH- 320 100 100 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits o - Terphenyl (aromatic) 66 40-140 2-Fluorobiphenyl (fractionation 1) 80 40-140 2-Bromonaphthalene (fractionation 2) 49 40-140 MADEP EPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 MADEP-EPH- MADEP-EPH-04 1 02/25/2019 1815 CHG 02/20/2019 0934 98294 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C18 Aliphatics MADEP-EPH- 260 100 100 ug/L 1 C19 - C36 Aliphatics MADEP-EPH- 190 100 100 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 1-Chloro-octadecane (aliphatic) 65 40-140 MADEP VPH (aliphatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 VPH MADEP-VPH-18-2.1 5 02/21/20191631 JJG 98425 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C5 - C8 Aliphatics MADEP-VPH- 1900 380 75 ug/L 2 C9 - C12 Aliphatics MADEP-VPH- 400 380 75 ug/L 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 18 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-006 Description: MW-24 Matrix: Aqueous Date Sampled:02/15/2019 1230 Date Received:02/18/2019 Run 2 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (FID) 108 70-130 MADEP VPH (aromatics) Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 VPH MADEP-VPH-18-2.1 1 02/20/20191831 JJG 98317 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run C9 - C10 Aromatics MADEP-VPH- 520 25 5.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2,5-Dibromotoluene (PID) 100 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 19 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-007 Description: MW-13 Matrix: Aqueous Date Sampled:02/15/2019 1235 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 SM 620013- SM 620OB-2011 1 02/26/2019 0150 KGT 98643 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- 48 0.50 0.40 ug/L 2 Ethylbenzene 100-41-4 SM 6200B- 1.6 0.50 0.40 ug/L 2 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- 2.7 0.50 0.40 ug/L 2 Toluene 108-88-3 SM 6200B- 1.4 0.50 0.40 ug/L 2 Xylenes (total) 1330-20-7 SM 6200B- 2.0 0.50 0.40 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 102 70-130 1,2-Dichloroethane-d4 100 70-130 Toluene-d8 105 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 20 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-008 Description: EB-1 Matrix: Aqueous Date Sampled:02/15/2019 1030 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 02/21/2019 1154 BWS 98301 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 98 70-130 1,2-Dichloroethane-d4 106 70-130 Toluene-d8 97 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 21 of 62 Client:Apex Companies, LLC Laboratory ID: UB18028-009 Description: DUP21519 Matrix: Aqueous Date Sampled:02/15/2019 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 SM 620013- SM 620OB-2011 1 02/26/2019 0214 KGT 98643 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 620013- 48 0.50 0.40 ug/L 2 Ethylbenzene 100-41-4 SM 6200B- 1.6 0.50 0.40 ug/L 2 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- 3.0 0.50 0.40 ug/L 2 Toluene 108-88-3 SM 6200B- 1.3 0.50 0.40 ug/L 2 Xylenes (total) 1330-20-7 SM 6200B- 2.0 0.50 0.40 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 102 70-130 1,2-Dichloroethane-d4 102 70-130 Toluene-d8 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 22 of 62 Client:Apex Companies, LLC Laboratory ID:UB18028-010 Description: TB Matrix: Aqueous Date Sampled:02/15/2019 Date Received:02/18/2019 Volatile Organic Compounds by GC/MS Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 SM 620013- SM 620OB-2011 1 02/21/2019 1217 BWS 98301 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Benzene 71-43-2 SM 6200B- ND 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 SM 6200B- ND 0.50 0.40 ug/L 1 Methyl tertiary butyl ether (MTBE) 1634-04-4 SM 6200B- ND 0.50 0.40 ug/L 1 Toluene 108-88-3 SM 6200B- ND 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 SM 6200B- ND 0.50 0.40 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 95 70-130 1,2-Dichloroethane-d4 108 70-130 Toluene-d8 95 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 23 of 62 QC Summary Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 24 of 62 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ98301-001 Matrix: Aqueous Batch: 98301 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Parameter Result Q Dil LOQ DL Units Analysis Date Benzene ND 1 0.50 0.40 ug/L 02/21/2019 1052 Ethylbenzene ND 1 0.50 0.40 ug/L 02/21/2019 1052 Methyl tertiary butyl ether (MTBE) ND 1 0.50 0.40 ug/L 02/21/2019 1052 Toluene ND 1 0.50 0.40 ug/L 02/21/2019 1052 Xylenes (total) ND 1 0.50 0.40 ug/L 02/21/2019 1052 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 93 70-130 1,2-Dichloroethane-d4 110 70-130 Toluene-d8 95 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 25 of 62 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ98301-002 Matrix: Aqueous Batch: 98301 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Benzene 50 49 1 98 70-130 02/21/2019 0916 Ethylbenzene 50 47 1 94 70-130 02/21/2019 0916 Methyl tertiary butyl ether (MTBE) 50 52 1 104 70-130 02/21/2019 0916 Toluene 50 47 1 94 70-130 02/21/2019 0916 Xylenes (total) 100 92 1 92 70-130 02/21/2019 0916 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 94 70-130 1,2-Dichloroethane-d4 103 70-130 Toluene-d8 94 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 26 of 62 Volatile Organic Compounds by GC/MS - MS Sample ID: UB18028-006MS Matrix: Aqueous Batch: 98301 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Benzene ND 2500 2700 50 109 70-130 02/21/20191910 Ethylbenzene ND 2500 2700 50 110 70-130 02/21/20191910 Toluene ND 2500 2700 50 108 70-130 02/21/20191910 Xylenes (total) ND 5000 5400 50 108 70-130 02/21/2019 1910 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 103 70-130 1,2-Dichloroethane-d4 103 70-130 Toluene-d8 100 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 27 of 62 Volatile Organic Compounds by GC/MS - MSD Sample ID: UB18028-006MD Matrix: Aqueous Batch: 98301 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Benzene ND 2500 2600 50 105 3.7 70-130 20 02/21/20191933 Ethylbenzene ND 2500 2800 50 113 2.7 70-130 20 02/21/20191933 Toluene ND 2500 2700 50 109 0.67 70-130 20 02/21/20191933 Xylenes (total) ND 5000 5600 50 111 2.5 70-130 20 02/21/2019 1933 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 104 70-130 1,2-Dichloroethane-d4 97 70-130 Toluene-d8 101 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 28 of 62 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ98643-001 Matrix: Aqueous Batch: 98643 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Parameter Result Q Dil LOQ DL Units Analysis Date Benzene ND 1 0.50 0.40 ug/L 02/25/2019 1757 Ethylbenzene ND 1 0.50 0.40 ug/L 02/25/2019 1757 Methyl tertiary butyl ether (MTBE) ND 1 0.50 0.40 ug/L 02/25/2019 1757 Toluene ND 1 0.50 0.40 ug/L 02/25/2019 1757 Xylenes (total) ND 1 0.50 0.40 ug/L 02/25/2019 1757 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 100 70-130 1,2-Dichloroethane-d4 101 70-130 Toluene-d8 102 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 29 of 62 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ98643-002 Matrix: Aqueous Batch: 98643 Prep Method: SM 620OB-2011 Analytical Method: SM 620OB-2011 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Benzene 50 52 1 104 70-130 02/25/2019 1648 Ethylbenzene 50 52 1 103 70-130 02/25/2019 1648 Methyl tertiary butyl ether (MTBE) 50 50 1 99 70-130 02/25/2019 1648 Toluene 50 52 1 103 70-130 02/25/2019 1648 Xylenes (total) 100 100 1 103 70-130 02/25/2019 1648 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 94 70-130 1,2-Dichloroethane-d4 97 70-130 Toluene-d8 99 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 30 of 62 Semivolatile Organic Compounds by GC/MS - MB Sample ID: UQ98194-001 Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Parameter Result Q Dil LOQ DL Units Analysis Date Acenaphthene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Acenaphthylene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Anthracene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Benzo(a)anthracene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Benzo(a)pyrene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Benzo(b)fluoranthene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Benzo(g,h,i)perylene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Benzo(k)fluoranthene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Benzyl alcohol ND 1 3.2 2.0 ug/L 02/24/2019 1717 4-Bromophenyl phenyl ether ND 1 1.6 0.80 ug/L 02/24/2019 1717 Butyl benzyl phthalate ND 1 1.6 0.80 ug/L 02/24/2019 1717 bis (2-Chloro-1-methylethyl) ether ND 1 1.6 0.80 ug/L 02/24/2019 1717 4-Chloro-3-methyl phenol ND 1 1.6 0.80 ug/L 02/24/2019 1717 bis(2-Chloroethoxy)methane ND 1 1.6 0.80 ug/L 02/24/2019 1717 bis(2-Chloroethyl)ether ND 1 1.6 0.80 ug/L 02/24/2019 1717 2-Chloronaphthalene ND 1 1.6 0.80 ug/L 02/24/2019 1717 2-Chlorophenol ND 1 1.6 0.80 ug/L 02/24/2019 1717 4-Chlorophenyl phenyl ether ND 1 1.6 0.80 ug/L 02/24/2019 1717 Chrysene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Dibenzo(a,h)anth race ne ND 1 1.6 0.80 ug/L 02/24/2019 1717 Dibenzofuran ND 1 1.6 1.0 ug/L 02/24/2019 1717 1,2-Dichlorobenzene ND 1 1.6 0.80 ug/L 02/24/2019 1717 1,3-Dichlorobenzene ND 1 1.6 0.80 ug/L 02/24/2019 1717 1,4-Dichlorobenzene ND 1 1.6 0.80 ug/L 02/24/2019 1717 3,3'-Dichlorobenzidine ND 1 8.0 0.80 ug/L 02/24/2019 1717 2,4-Dichlorophenol ND 1 1.6 0.80 ug/L 02/24/2019 1717 Diethylphthalate ND 1 1.6 0.80 ug/L 02/24/2019 1717 Dimethyl phthalate ND 1 1.6 0.80 ug/L 02/24/2019 1717 2,4-Dimethylphenol ND 1 1.6 0.80 ug/L 02/24/2019 1717 Di-n-butyl phthalate ND 1 1.6 0.81 ug/L 02/24/2019 1717 4,6-Dinitro-2-methyl phenol ND 1 8.0 0.80 ug/L 02/24/2019 1717 2,4-Dinitrophenol ND 1 8.0 0.80 ug/L 02/24/2019 1717 Di-n-octylphthalate ND 1 1.6 0.80 ug/L 02/24/2019 1717 1,2-Diphenylhydrazine(as azobenzene) ND 1 1.6 0.80 ug/L 02/24/2019 1717 bis(2-Ethylhexyl)phthalate ND 1 8.0 4.0 ug/L 02/24/2019 1717 Fluoranthene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Fluorene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Hexachlorobenzene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Hexachlorobutadiene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Hexachlorocyclopentadiene ND 1 8.0 4.0 ug/L 02/24/2019 1717 Hexachloroethane ND 1 1.6 0.80 ug/L 02/24/2019 1717 Indeno(1,2,3-c,d)pyrene ND 1 1.6 0.80 ug/L 02/24/2019 1717 Isophorone ND 1 1.6 0.80 ug/L 02/24/2019 1717 1-Methyl naphthalene ND 1 1.6 0.40 ug/L 02/24/2019 1717 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 31 of 62 Semivolatile Organic Compounds by GC/MS - MB Sample ID: UQ98194-001 Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Parameter Result Q Dil LOQ DL Units Analysis Date 2-Methyl naphthalene ND 1 1.6 0.40 ug/L 02/24/20191717 2-Methylphenol ND 1 1.6 0.67 ug/L 02/24/20191717 3+4-Methylphenol ND 1 1.6 1.5 ug/L 02/24/20191717 Naphthalene ND 1 1.6 0.80 ug/L 02/24/20191717 Nitrobenzene ND 1 1.6 0.80 ug/L 02/24/20191717 2-Nitrophenol ND 1 3.2 0.80 ug/L 02/24/20191717 4-Nitrophenol ND 1 8.0 4.0 ug/L 02/24/20191717 N-Nitrosodi-n-propylamine ND 1 1.6 0.80 ug/L 02/24/20191717 N-Nitrosodiphenylamine (Diphenylamine) ND 1 1.6 0.80 ug/L 02/24/2019 1717 Pentachlorophenol ND 1 8.0 4.0 ug/L 02/24/20191717 Phenanthrene ND 1 1.6 0.80 ug/L 02/24/20191717 Phenol ND 1 1.6 0.80 ug/L 02/24/20191717 Pyrene ND 1 1.6 0.80 ug/L 02/24/20191717 1,2,4-Trichlorobenzene ND 1 1.6 0.80 ug/L 02/24/20191717 2,4,6-Trichlorophenol ND 1 1.6 0.80 ug/L 02/24/20191717 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 54 37-129 2-Fluorophenol 54 24-127 Nitrobenzene-d5 63 38-127 Phenol-d5 45 28-128 Terphenyl-d 14 86 10-148 2,4,6-Tribromophenol 65 41-144 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 32 of 62 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: UQ98194-002 Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Acenaphthene 20 13 1 65 47-145 02/25/2019 1113 Acenaphthylene 20 14 1 69 33-145 02/25/2019 1113 Anthracene 20 17 1 83 27-133 02/25/2019 1113 Benzo(a)anthracene 20 19 1 94 33-143 02/25/2019 1113 Benzo(a)pyrene 20 18 1 88 17-163 02/25/2019 1113 Benzo(b)fluoranthene 20 19 1 95 24-159 02/25/2019 1113 Benzo(g,h,i)perylene 20 21 1 103 1-219 02/25/2019 1113 Benzo(k)fluoranthene 20 20 1 98 11-162 02/25/2019 1113 Benzyl alcohol 20 12 1 60 30-130 02/25/2019 1113 4-Bromophenyl phenyl ether 20 15 1 74 53-127 02/25/2019 1113 Butyl benzyl phthalate 20 19 1 97 1-152 02/25/2019 1113 bis (2-Chloro-1-methylethyl) ether 20 12 1 61 36-166 02/25/2019 1113 4-Chloro-3-methyl phenol 20 15 1 74 22-147 02/25/2019 1113 bis(2-Chloroethoxy)methane 20 13 1 65 33-184 02/25/2019 1113 bis(2-Chloroethyl)ether 20 13 1 66 12-158 02/25/2019 1113 2-Chloronaphthalene 20 13 1 64 60-120 02/25/2019 1113 2-Chlorophenol 20 12 1 59 23-134 02/25/2019 1113 4-Chlorophenyl phenyl ether 20 13 1 67 25-158 02/25/2019 1113 Chrysene 20 20 1 101 17-168 02/25/2019 1113 Dibenzo(a,h)anth race ne 20 19 1 97 1-227 02/25/2019 1113 Dibenzofuran 20 13 1 66 48-118 02/25/2019 1113 1,2-Dichlorobenzene 20 12 1 59 32-129 02/25/2019 1113 1,3-Dichlorobenzene 20 12 1 59 1-172 02/25/2019 1113 1,4-Dichlorobenzene 20 12 1 58 20-124 02/25/2019 1113 3,3'-Dichlorobenzidine 20 15 1 77 1-262 02/25/2019 1113 2,4-Dichlorophenol 20 14 1 71 39-135 02/25/2019 1113 Diethylphthalate 20 16 1 79 1-120 02/25/2019 1113 Dimethyl phthalate 20 15 1 73 1-120 02/25/2019 1113 2,4-Dimethylphenol 20 13 1 65 32-120 02/25/2019 1113 Di-n-butyl phthalate 20 19 1 97 1-120 02/25/2019 1113 4,6-Dinitro-2-methyl phenol 20 17 1 85 1-181 02/25/2019 1113 2,4-Dinitrophenol 40 22 1 55 1-191 02/25/2019 1113 Di-n-octylphthalate 20 17 1 85 4-146 02/25/2019 1113 1,2-Diphenylhydrazine(as azobenzene) 20 13 1 65 1-150 02/25/2019 1113 bis(2-Ethylhexyl)phthalate 20 20 1 101 8-158 02/25/2019 1113 Fluoranthene 20 19 1 93 26-137 02/25/2019 1113 Fluorene 20 14 1 68 59-121 02/25/2019 1113 Hexachlorobenzene 20 15 1 76 1-152 02/25/2019 1113 Hexachlorobutadiene 20 12 1 58 24-120 02/25/2019 1113 Hexachlorocyclopentadiene 100 34 1 34 1-150 02/25/2019 1113 Hexachloroethane 20 11 1 55 40-120 02/25/2019 1113 Indeno(1,2,3-c,d)pyrene 20 19 1 95 1-171 02/25/2019 1113 Isophorone 20 14 1 68 21-196 02/25/2019 1113 1-Methyl naphthalene 20 14 1 71 42-126 02/25/2019 1113 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 33 of 62 Semivolatile Organic Compounds by GC/MS - LCS Sample ID: UQ98194-002 Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 2-Methyl naphthalene 20 14 1 72 40-132 02/25/20191113 2-Methylphenol 20 16 1 78 30-130 02/25/20191113 3+4-Methylphenol 20 16 1 81 30-130 02/25/20191113 Naphthalene 20 14 1 71 21-133 02/25/20191113 Nitrobenzene 20 13 1 65 35-180 02/25/20191113 2-Nitrophenol 20 14 1 71 29-182 02/25/20191113 4-Nitrophenol 40 32 1 81 1-132 02/25/20191113 N-Nitrosodi-n-propylamine 20 14 1 72 1-230 02/25/20191113 N-Nitrosodiphenylamine (Diphenylamine) 20 16 1 78 1-150 02/25/2019 1113 Pentachlorophenol 40 32 1 79 14-176 02/25/20191113 Phenanthrene 20 16 1 81 54-120 02/25/20191113 Phenol 20 11 1 53 5-120 02/25/20191113 Pyrene 20 19 1 95 52-120 02/25/20191113 1,2,4-Trichlorobenzene 20 12 1 62 44-142 02/25/20191113 2,4,6-Trichlorophenol 20 13 1 67 37-144 02/25/20191113 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 65 37-129 2-Fluorophenol 35 24-127 Nitrobenzene-d5 66 38-127 Phenol-d5 51 28-128 Terphenyl-d 14 111 10-148 2,4,6-Tribromophenol 70 41-144 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 34 of 62 Semivolatile Organic Compounds by GC/MS - MS Sample ID: UB18028-001 MS Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Acenaphthene ND 40 21 1 52 47-145 02/24/2019 1830 Acenaphthylene ND 40 20 1 50 33-145 02/24/2019 1830 Anthracene ND 40 26 1 64 27-133 02/24/2019 1830 Benzo(a)anthracene ND 40 31 1 79 33-143 02/24/2019 1830 Benzo(a)pyrene ND 40 30 1 75 17-163 02/24/2019 1830 Benzo(b)fluoranthene ND 40 34 1 85 24-159 02/24/2019 1830 Benzo(g,h,i)perylene ND 40 35 1 88 1-219 02/24/2019 1830 Benzo(k)fluoranthene ND 40 32 1 81 11-162 02/24/2019 1830 Benzyl alcohol ND 40 24 1 59 30-130 02/24/2019 1830 4-Bromophenyl phenyl ether ND 40 24 1 59 53-127 02/24/2019 1830 Butyl benzyl phthalate ND 40 30 1 75 1-152 02/24/2019 1830 bis (2-Chloro-1-methylethyl) ether ND 40 22 1 56 36-166 02/24/2019 1830 4-Chloro-3-methyl phenol ND 40 23 1 58 22-147 02/24/2019 1830 bis(2-Chloroethoxy)methane ND 40 25 1 63 33-184 02/24/2019 1830 bis(2-Chloroethyl)ether ND 40 25 1 62 12-158 02/24/2019 1830 2-Chloronaphthalene ND 40 20 N 1 51 60-120 02/24/2019 1830 2-Chlorophenol ND 40 19 1 48 23-134 02/24/2019 1830 4-Chlorophenyl phenyl ether ND 40 23 1 57 25-158 02/24/2019 1830 Chrysene ND 40 33 1 82 17-168 02/24/2019 1830 Dibenzo(a,h)anth race ne ND 40 33 1 82 1-227 02/24/2019 1830 Dibenzofuran ND 40 21 1 52 30-130 02/24/2019 1830 1,2-Dichlorobenzene ND 40 20 1 49 32-129 02/24/2019 1830 1,3-Dichlorobenzene ND 40 19 1 48 1-172 02/24/2019 1830 1,4-Dichlorobenzene ND 40 19 1 48 20-124 02/24/2019 1830 3,3'-Dichlorobenzidine ND 40 29 1 72 1-262 02/24/2019 1830 2,4-Dichlorophenol ND 40 22 1 54 39-135 02/24/2019 1830 Diethylphthalate ND 40 23 1 58 1-120 02/24/2019 1830 Dimethyl phthalate ND 40 21 1 54 1-120 02/24/2019 1830 2,4-Dimethylphenol ND 40 22 1 54 32-120 02/24/2019 1830 Di-n-butyl phthalate ND 40 31 1 76 1-120 02/24/2019 1830 4,6-Dinitro-2-methyl phenol ND 40 41 1 101 1-181 02/24/2019 1830 2,4-Dinitrophenol ND 80 71 1 88 1-191 02/24/2019 1830 Di-n-octylphthalate ND 40 29 1 72 4-146 02/24/2019 1830 1,2-Diphenylhydrazine(as azobenzene) ND 40 21 1 53 1-150 02/24/2019 1830 bis(2-Ethylhexyl)phthalate ND 40 31 1 76 8-158 02/24/2019 1830 Fluoranthene ND 40 32 1 81 26-137 02/24/2019 1830 Fluorene ND 40 21 N 1 51 59-121 02/24/2019 1830 Hexachlorobenzene ND 40 23 1 57 1-152 02/24/2019 1830 Hexachlorobutadiene ND 40 23 1 58 24-120 02/24/2019 1830 Hexachlorocyclopentadiene ND 200 69 1 34 1-150 02/24/2019 1830 Hexachloroethane ND 40 20 1 49 40-120 02/24/2019 1830 Indeno(1,2,3-c,d)pyrene ND 40 32 1 81 1-171 02/24/2019 1830 Isophorone ND 40 25 1 62 21-196 02/24/2019 1830 1-Methyl naphthalene ND 40 23 1 57 42-126 02/24/2019 1830 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 35 of 62 Semivolatile Organic Compounds by GC/MS - MS Sample ID: UB18028-001 MS Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 2-Methyl naphthalene ND 40 23 1 57 40-132 02/24/20191830 2-Methylphenol ND 40 21 1 52 30-130 02/24/20191830 3+4-Methylphenol ND 40 21 1 53 30-130 02/24/20191830 Naphthalene ND 40 23 1 58 21-133 02/24/20191830 Nitrobenzene ND 40 25 1 61 35-180 02/24/20191830 2-Nitrophenol ND 40 27 1 68 29-182 02/24/20191830 4-Nitrophenol ND 80 51 1 64 1-132 02/24/20191830 N-Nitrosodi-n-propylamine ND 40 25 1 61 1-230 02/24/20191830 N-Nitrosodiphenylamine (Diphenylamine) ND 40 23 1 59 1-150 02/24/2019 1830 Pentachlorophenol ND 80 77 1 96 14-176 02/24/20191830 Phenanthrene ND 40 26 1 64 54-120 02/24/20191830 Phenol ND 40 18 1 45 5-120 02/24/20191830 Pyrene ND 40 32 1 80 52-120 02/24/20191830 1,2,4-Trichlorobenzene ND 40 22 1 56 44-142 02/24/20191830 2,4,6-Trichlorophenol ND 40 23 1 57 37-144 02/24/20191830 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 52 37-129 2-Fluorophenol 47 24-127 Nitrobenzene-d5 62 38-127 Phenol-d5 44 28-128 Terphenyl-d 14 84 10-148 2,4,6-Tribromophenol 69 41-144 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 36 of 62 Semivolatile Organic Compounds by GC/MS - MSD Sample ID: UB18028-001 MD Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Acenaphthene ND 40 21 1 52 0.61 47-145 48 02/24/2019 1854 Acenaphthylene ND 40 20 1 51 1.8 33-145 74 02/24/2019 1854 Anthracene ND 40 25 1 61 4.1 27-133 66 02/24/2019 1854 Benzo(a)anthracene ND 40 29 1 73 7.8 33-143 53 02/24/2019 1854 Benzo(a)pyrene ND 40 28 1 70 6.9 17-163 72 02/24/2019 1854 Benzo(b)fluoranthene ND 40 22 1 55 43 24-159 71 02/24/2019 1854 Benzo(g,h,i)perylene ND 40 24 1 59 39 1-219 97 02/24/2019 1854 Benzo(k)fluoranthene ND 40 24 1 59 31 11-162 63 02/24/2019 1854 Benzyl alcohol ND 40 25 1 63 5.4 30-130 40 02/24/2019 1854 4-Bromophenyl phenyl ether ND 40 24 1 60 1.2 53-127 43 02/24/2019 1854 Butyl benzyl phthalate ND 40 26 1 66 13 1-152 60 02/24/2019 1854 bis (2-Chloro-1-methylethyl) ether ND 40 25 1 62 9.4 36-166 76 02/24/2019 1854 4-Chloro-3-methyl phenol ND 40 24 1 59 2.8 22-147 73 02/24/2019 1854 bis(2-Chloroethoxy)methane ND 40 25 1 62 1.4 33-184 54 02/24/2019 1854 bis(2-Chloroethyl)ether ND 40 27 1 67 7.5 12-158 108 02/24/2019 1854 2-Chloronaphthalene ND 40 21 N 1 51 1.2 60-120 24 02/24/2019 1854 2-Chlorophenol ND 40 20 1 51 5.5 23-134 61 02/24/2019 1854 4-Chlorophenyl phenyl ether ND 40 23 1 57 0.67 25-158 61 02/24/2019 1854 Chrysene ND 40 30 1 75 8.8 17-168 87 02/24/2019 1854 Dibenzo(a,h)anth race ne ND 40 23 1 57 36 1-227 126 02/24/2019 1854 Dibenzofuran ND 40 21 1 54 2.1 30-130 40 02/24/2019 1854 1,2-Dichlorobenzene ND 40 20 1 51 3.4 32-129 31 02/24/2019 1854 1,3-Dichlorobenzene ND 40 19 1 49 1.4 1-172 42 02/24/2019 1854 1,4-Dichlorobenzene ND 40 20 1 50 3.8 20-124 32 02/24/2019 1854 3,3'-Dichlorobenzidine ND 40 26 1 66 9.1 1-262 108 02/24/2019 1854 2,4-Dichlorophenol ND 40 22 1 55 1.4 39-135 50 02/24/2019 1854 Diethylphthalate ND 40 22 1 56 5.2 1-120 100 02/24/2019 1854 Dimethyl phthalate ND 40 21 1 53 2.0 1-120 183 02/24/2019 1854 2,4-Dimethylphenol ND 40 23 1 57 4.3 32-120 58 02/24/2019 1854 Di-n-butyl phthalate ND 40 27 1 67 13 1-120 47 02/24/2019 1854 4,6-Dinitro-2-methyl phenol ND 40 39 1 98 2.9 1-181 203 02/24/2019 1854 2,4-Dinitrophenol ND 80 66 1 83 6.9 1-191 132 02/24/2019 1854 Di-n-octylphthalate ND 40 19 1 47 42 4-146 69 02/24/2019 1854 1,2-Diphenylhydrazine(as azobenzene) ND 40 21 1 53 0.48 1-150 40 02/24/2019 1854 bis(2-Ethylhexyl)phthalate ND 40 26 1 65 16 8-158 82 02/24/2019 1854 Fluoranthene ND 40 30 1 75 7.7 26-137 66 02/24/2019 1854 Fluorene ND 40 21 N 1 52 0.91 59-121 38 02/24/2019 1854 Hexachlorobenzene ND 40 22 1 56 2.1 1-152 55 02/24/2019 1854 Hexachlorobutadiene ND 40 23 1 58 1.4 24-120 62 02/24/2019 1854 Hexachlorocyclopentadiene ND 200 72 1 36 5.5 1-150 40 02/24/2019 1854 Hexachloroethane ND 40 20 1 49 0.69 40-120 52 02/24/2019 1854 Indeno(1,2,3-c,d)pyrene ND 40 22 1 56 37 1-171 99 02/24/2019 1854 Isophorone ND 40 25 1 62 1.4 21-196 93 02/24/2019 1854 1-Methyl naphthalene ND 40 23 1 58 2.2 42-126 40 02/24/2019 1854 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 37 of 62 Semivolatile Organic Compounds by GC/MS - MSD Sample ID: UB18028-001 MD Matrix: Aqueous Batch: 98194 Prep Method: 625.1 Analytical Method: 625.1 Prep Date: 02/20/2019 1632 Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date 2-Methyl naphthalene ND 40 23 1 58 1.7 40-132 40 02/24/20191854 2-Methylphenol ND 40 22 1 55 4.0 30-130 40 02/24/20191854 3+4-Methylphenol ND 40 22 1 56 4.5 30-130 40 02/24/20191854 Naphthalene ND 40 24 1 59 2.0 21-133 65 02/24/20191854 Nitrobenzene ND 40 25 1 63 2.3 35-180 62 02/24/20191854 2-Nitrophenol ND 40 28 1 69 1.7 29-182 55 02/24/20191854 4-Nitrophenol ND 80 48 1 60 6.4 1-132 131 02/24/20191854 N-Nitrosodi-n-propylamine ND 40 26 1 66 6.8 1-230 87 02/24/20191854 N-Nitrosodiphenylamine (Diphenylamine) ND 40 23 1 57 2.5 1-150 40 02/24/2019 1854 Pentachlorophenol ND 80 75 1 93 2.5 14-176 86 02/24/20191854 Phenanthrene ND 40 24 1 61 4.1 54-120 39 02/24/20191854 Phenol ND 40 20 1 49 7.6 5-120 64 02/24/20191854 Pyrene ND 40 29 1 72 11 52-120 49 02/24/20191854 1,2,4-Trichlorobenzene ND 40 23 1 57 2.5 44-142 50 02/24/20191854 2,4,6-Trichlorophenol ND 40 23 1 57 0.69 37-144 58 02/24/20191854 Surrogate Q % Rec Acceptance Limit 2-Fluorobiphenyl 52 37-129 2-Fluorophenol 43 24-127 Nitrobenzene-d5 61 38-127 Phenol-d5 47 28-128 Terphenyl-d 14 76 10-148 2,4,6-Tribromophenol 67 41-144 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 38 of 62 MADEP EPH (aliphatics) - Unfractionated - MB Sample ID: UQ98139-001 Matrix: Aqueous Batch: 98139 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Parameter Result Q Dil LOQ DL Units Analysis Date C19 - C36 Aliphatics - Unfractionated ND 1 100 100 ug/L 02/20/2019 1740 C9 - C18 Aliphatics - Unfractionated ND 1 100 100 ug/L 02/20/2019 1740 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) - Unfractionated 98 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 39 of 62 MADEP EPH (aliphatics) - Unfractionated - LCS Sample ID: UQ98139-002 Matrix: Aqueous Batch: 98139 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C19 - C36 Aliphatics - Unfractionated 900 890 1 99 40-140 02/20/2019 1810 C9 - C18 Aliphatics - Unfractionated 650 510 1 78 40-140 02/20/2019 1810 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) - Unfractionated 95 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 40 of 62 MADEP EPH (aliphatics) - Unfractionated - LCSD Sample ID: UQ98139-003 Matrix: Aqueous Batch: 98139 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C19 - C36 Aliphatics - Unfractionated 900 910 1 101 2.3 40-140 25 02/20/2019 1839 C9 - C18 Aliphatics - Unfractionated 650 530 1 81 3.8 40-140 25 02/20/2019 1839 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) - Unfractionated 97 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 41 of 62 MADEP EPH (aromatics) - Unfractionated - MB Sample ID: UQ98140-001 Matrix: Aqueous Batch: 98140 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Parameter Result Q Dil LOQ DL Units Analysis Date C11 - C22 Aromatics - Unfractionated ND 1 100 100 ug/L 02/20/2019 1740 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) - Unfractionated 68 40-140 2-Fluorobiphenyl (fractionation 1) 79 40-140 2-Bromonaphthalene (fractionation 2) 81 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 42 of 62 MADEP EPH (aromatics) - Unfractionated - LCS Sample ID: UQ98140-002 Matrix: Aqueous Batch: 98140 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C11 - C22 Aromatics - Unfractionated 1400 960 1 68 40-140 02/20/2019 1810 Surrogate Q % Rec Acceptance Limit o - Terphenyl (aromatic) - Unfractionated 70 40-140 2-Fluorobiphenyl (fractionation 1) 82 40-140 2-Bromonaphthalene (fractionation 2) 84 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 43 of 62 MADEP EPH (aromatics) - Unfractionated - LCSD Sample ID: UQ98140-003 Matrix: Aqueous Batch: 98140 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C11 - C22 Aromatics - Unfractionated 1400 980 1 70 2.7 40-140 25 02/20/2019 1839 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) - Unfractionated 72 40-140 2-Fluorobiphenyl (fractionation 1) 86 40-140 2-Bromonaphthalene (fractionation 2) 88 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 44 of 62 MADEP EPH (aliphatics) - MB Sample ID: UQ98294-001 Matrix: Aqueous Batch: 98294 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Parameter Result Q Dil LOQ DL Units Analysis Date C9 - C18 Aliphatics ND 1 100 100 ug/L 02/25/2019 1618 C19 - C36 Aliphatics ND 1 100 100 ug/L 02/25/2019 1618 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) 80 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 45 of 62 MADEP EPH (aliphatics) - LCS Sample ID: UQ98294-002 Matrix: Aqueous Batch: 98294 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C9 - C18 Aliphatics 300 200 1 67 40-140 02/25/2019 1647 C19 - C36 Aliphatics 400 300 1 75 40-140 02/25/2019 1647 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) 83 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 46 of 62 MADEP EPH (aliphatics) - LCSD Sample ID: UQ98294-003 Matrix: Aqueous Batch: 98294 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C9 - C18 Aliphatics 300 200 1 65 1.9 40-140 25 02/25/2019 1716 C19 - C36 Aliphatics 400 300 1 76 0.24 40-140 25 02/25/2019 1716 Surrogate Acceptance Q % Rec Limit 1-Chloro-octadecane (aliphatic) 82 40-140 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 47 of 62 MADEP EPH (aromatics) - MB Sample ID: UQ98295-001 Matrix: Aqueous Batch: 98295 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Parameter Result Q Dil LOQ DL Units Analysis Date C11 - C22 Aromatics ND 1 100 100 ug/L 02/25/2019 1844 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) 74 40-140 2-Fluorobiphenyl (fractionation 1) 84 40-140 2-Bromonaphthalene (fractionation 2) 48 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 48 of 62 MADEP EPH (aromatics) - LCS Sample ID: UQ98295-002 Matrix: Aqueous Batch: 98295 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C11 - C22 Aromatics 850 660 1 78 40-140 02/25/2019 1913 Surrogate Q % Rec Acceptance Limit o - Terphenyl (aromatic) 78 40-140 2-Fluorobiphenyl (fractionation 1) 89 40-140 2-Bromonaphthalene (fractionation 2) 68 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 49 of 62 MADEP EPH (aromatics) - LCSD Sample ID: UQ98295-003 Matrix: Aqueous Batch: 98295 Prep Method: MADEP-EPH-04 Analytical Method: MADEP-EPH-04 Prep Date: 02/20/2019 934 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C11 - C22 Aromatics 850 670 1 79 1.4 40-140 25 02/25/2019 1942 Acceptance Surrogate Q % Rec Limit o - Terphenyl (aromatic) 78 40-140 2-Fluorobiphenyl (fractionation 1) 91 40-140 2-Bromonaphthalene (fractionation 2) 64 40-140 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 50 of 62 MADEP VPH (aromatics) - MB Sample ID: UQ98317-001 Matrix: Aqueous Batch: 98317 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C9 - C10 Aromatics ND 1 25 5.0 ug/L 02/20/2019 1551 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 112 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 51 of 62 MADEP VPH (aromatics) - LCS Sample ID: UQ98317-002 Matrix: Aqueous Batch: 98317 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C9 - C10 Aromatics 25 30 1 121 70-130 02/20/2019 1454 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 109 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 52 of 62 MADEP VPH (aromatics) - LCSD Sample ID: UQ98317-003 Matrix: Aqueous Batch: 98317 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C9 - C10 Aromatics 25 28 1 110 9.0 70-130 25 02/20/2019 1523 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (PID) 105 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 53 of 62 MADEP VPH (aliphatics) - MB Sample ID: UQ98319-001 Matrix: Aqueous Batch: 98319 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C5 - C8 Aliphatics ND 1 75 15 ug/L 02/20/2019 1551 C9 - C12 Aliphatics ND 1 75 15 ug/L 02/20/2019 1551 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 112 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 54 of 62 MADEP VPH (aliphatics) - LCS Sample ID: UQ98319-002 Matrix: Aqueous Batch: 98319 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C5 - C8 Aliphatics 150 170 1 113 70-130 02/20/2019 1454 C9 - C12 Aliphatics 180 190 1 108 70-130 02/20/2019 1454 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID) 107 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 55 of 62 MADEP VPH (aliphatics) - LCSD Sample ID: UQ98319-003 Matrix: Aqueous Batch: 98319 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C5 - C8 Aliphatics 150 160 1 107 5.5 70-130 25 02/20/2019 1523 C9 - C12 Aliphatics 180 180 1 104 4.0 70-130 25 02/20/2019 1523 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 105 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 56 of 62 MADEP VPH (aliphatics) - MB Sample ID: UQ98425-001 Matrix: Aqueous Batch: 98425 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Parameter Result Q Dil LOQ DL Units Analysis Date C5 - C8 Aliphatics ND 1 75 15 ug/L 02/21/2019 1506 C9 - C12 Aliphatics ND 1 75 15 ug/L 02/21/2019 1506 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 107 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 57 of 62 MADEP VPH (aliphatics) - LCS Sample ID: UQ98425-002 Matrix: Aqueous Batch: 98425 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date C5 - C8 Aliphatics 150 160 1 107 70-130 02/21/2019 1409 C9 - C12 Aliphatics 180 180 1 103 70-130 02/21/2019 1409 Surrogate Q % Rec Acceptance Limit 2,5-Dibromotoluene (FID) 104 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 58 of 62 MADEP VPH (aliphatics) - LCSD Sample ID: UQ98425-003 Matrix: Aqueous Batch: 98425 Prep Method: VPH Analytical Method: MADEP-VPH-18-2.1 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date C5 - C8 Aliphatics 150 160 1 104 2.5 70-130 25 02/21/2019 1437 C9 - C12 Aliphatics 180 180 1 101 1.5 70-130 25 02/21/2019 1437 Acceptance Surrogate Q % Rec Limit 2,5-Dibromotoluene (FID) 106 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection ND = Not detected at or above the DL Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 59 of 62 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 60 of 62 SHEALY ENVIRONMENTAL SERVICES, INC. Ili al _ Y L 1 r z . zr V t L4 � V V R 31r' r XX 4 � x _ LZ I yq irai' I amx�4r• - I Lo 4 107 z p F� �I 2 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 61 of 62 SHEALY ENVIRONMENTAL SERVICES, INC. Shkd* I9rrv_im m iaidk S:-Lviccs, Inc. nm-.uro MNurnb•r MEW lsc-14 Page 1 n: l E:reul.iva VatL- @flw1 a Sample I eeeipt Checklist (SRC) climit {miler Ins cctcd b Idellp,' 1V f ' 11 r � .57. Pu e:jns ofrec opt: RSi j] Clival ups ji fedrx ❑ other: . LJ Yms -Iff'No I: M+ tody:wal3 present on the cooler? Yes ❑ No A 2, if cugWy seals went preseA were they ji1mcl u11d unbroken? PH 80-ip [ D.. - Chlorine Ship ID: Tesied by AJ r final temperaturc upon Fv ipt? Derived (Con tad) temperatur yp, D rweipt: %Solid snap -Cap [D' '{_ II P�� Mcabod= }-Tent:, raturc i lo-,rtk ❑A.Uainst Bottles [R Curs ID' _ TR C3un Carraction 1 actt�r' °C 4etiiod of -oolIce ❑ lce Packs Q Dry lee ❑ None — ❑ Yas Era Yes — 9'8 El' NC i A 3- If 1CmperMUTI-- OFCu1V Cooler m eded 60'c, war, Prujea hla nagff Alctifkv P was Notifiad byphrmi-- 1 email) fait to-iltce (Circle onc). 4, Is tlu r;urrui7ercial eouritrl,8 packing slip attached to this fonn? es ❑ No 5. Wcrc proper Custody procedures (relinquished?melved) followed? 4S es No El So 6, Wcm sunplo IDs iist�d on the o C7 7. Wcrc smmpin [Ds Iived on a! I samlrle mnllainm? ❑ No 9. Was colimAion d0.#e & time listed of the Lyjc'? N 9. Was collcL ioik dak & tiInc Iiated on all sample container-.;? Y-cs ❑ lwlo 14. 1?ill all container label inforrtation (ID, date, tiwvj agree with the COC? Yes ❑ No I'll. Won tests to be perfarmad Iisl.cd on the COO Yes ❑ No 12 Did n I I samples arrive in Lhc p apex containers for each test arAror in good Condition (unbroken, lids on, ere.)': _ .— Yes ❑flu 113. was x1equate sample volurrry available? 13 Yes a 114. Were all sample.'. received within 'A thrr holding thue or,18 hour, whichcvcr cunitz first'.' e3 ❑ No 15. WcrC anw smuples containers missin gxcL ui illcic onelsanVies Not lister# on COC? D YCS C l I N.+l 16. For V4 mid R I -l75 samples, were u files prescnl >-`pe2t-size" (!/Vor 6mm in diameter) in any ofthe VOA vials:` ElYes No A 17, Were all f}ROIiineWshiva[enl5awplti rec�eivc,l at a H a7f-� 2? I—J y ❑ No A 1 S- Were all cvauidc smuples received at $ fT > 1 ? and sulfdc samples reoe ivai ai a pIT > 9? ,.,I Yes ❑ No A 19. Wuru till iipplic a N HyqKN!gyan[dt'p ens VUrb (<-0.5m L) samples free ofresr ua Clllori ne'7 ❑ym ❑ND t1 '0, wJk'cm client mmarbftcquesu (i.e,. re€lucsicd dilrr6ipriA, A'lS!MSD des ignation3, etc...) correctly tmiscribtri Jtw the COC into the ;Omrmert section in LIM,,3 }' sy 21- was the quote number lisled on the. container laihel7 if }gas, Quote 4 'ample P-eaer'r'AtiOri (LMLrl lae Cr,:,tpieicd for ally sample(s) incornxdy presf;vved or with htade:pace-) Salmple(s) .k WCrC rC1MjV J irworree-0y pre5crycd and wem adiu5torl }11,:Luwdi119.1 ' in sample receiving vvith A mL of circle nne; H2SC)4, [fNQ3. HCI- NROH using big # ime of presarwatian . If more than one preservative is ncakd, phase ILCte in the cumiriertts boo}w. Sample!») f° were received with bubbles -;�6 mm in diameter. Bamplm(x) l4 were received with TRC > 0-5 rgVL (Ird 19 is no )rind were justed acoardlugly In simple racaidnU with:iodiulta thlosulfate fNa2S303)wvirh Shealy ID: bam4x'u IOmis q)plied by; Gimmenlfi' V �' V f•QC- Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 62 of 62 APPENDIX C CONCENTRATION TIME TREND SERIES GRAPH - MW-13 ``i APEX 200 180 160 140 120 Ell 40 20 L MW-13 I� W W M M O O -1 rj N N m m 'It -Zt Ln M l0 lD Il r� w w m m O O r-I r-I N m m lzt -�t Ln Ln m lD lD I- n w w m rn m rn m m 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0r-I .4 .- ����r-4 r ������r-I rn m\ m m 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 c-I c-I m -i c i N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N N O N Ii Ql n lD M l0 N N -i 00 Q1 Il M Il N -i O L!1 N W c-I O � N -i 00 M � N -i N M 00 lD Ql I- L!1 c-I l0 LI1 N N c-I c-I �--� c-I N .--I N N c-I rl �--I c-I N .--I N c-I N �--I N N c-I N \ c-I c-I \ c-I \ N .--I N N N \ \ N \ N \ \ O N 00 N 00 N CO N 00 N 00 N 00 N CO N 00 N 00 N 00 N CO N 00 00 N N 00 N 00 N 00 rl N W W W N rl Benzene Linear (Benzene)