18067_Wurst Property_BAR_20170221

February 21, 2017
Mr. Jim Knoles
Spec Con, Inc.
[e-mail]
Report of Soil Testing
810 Lufkin Road
Apex, North Carolina
Our project Number: 121-17-86861
Gentlemen:
TERRATECH
ENGINEERS- I NC
Geotechnical Engineering
Environmental Consulting
Construction Materials Testing
As requested, a representative of TerraTech Engineers, Inc. recently collected soil samples to test for the
presence of soil contaminants in potential imported fill soils. We understand that these soils would be used
to backfill an excavation for a Brownfield site located at 810 Lufkin Road in Apex, North Carolina. We
understand that NC Department of Environmental Quality (NCDEQ) requires potential import soils to be
tested prior to use as structural fill soils. The scope of this investigation is based on our conversations with
you.
Methodoloay Used
We collected a total of six soil samples from two potential soil stock piles. Samples S-1 through S-3 were
collected at selected locations on the soil stockpile located at the Wake Stone Quarry in Moncure, North
Carolina. The soils collected generally consisted of sandy silt and sandy clay with various amounts of
gravel. Samples S-4 through S-6 were collected from a soil stock pile located near the intersection of Jenks
Road and NC Highway 64 in Apex, North Carolina. We observed dump trucks hauling soils to the stockpile
from offsite locations at the time of our sampling. The soils collected generally consisted of silt, sandy silt,
and sandy clay. The soil samples were stored in sealed containers, placed on ice, and transported to Pace
Analytical Laboratories for testing by EPA Method 8260 for Volatile Organic Compounds, EPA Method
8270 for Semi -Volatile Organic Compounds, and EPA Methods 6061 and 7471 for 8 RCRA Metals.
Analytical Test Results
The results of our laboratory testing are provided in the attached documents and summarized in the
following table:
Sample ID:
B-1
I B-2
B-3
B-4
B-5
B-6
Arsenic (mg/kg)
7.1
4.2
5.3
1.9
1.8
2
Barium (mg/kg)
22.7
16
25.8
63.5
57.1
66.6
Cadmium (mg/kg)
ND
ND
ND
ND
ND
ND
Chromium (mg/kg)
6.3
5.7
6.5
4.9
6.2
9.6
Lead (mg/kg)
10.4
10.9
9.9
7.9
7.3
9
Selenium (mg/kg)
3.4
3.5
3.1
ND
ND
ND
Silver (mg/kg)
ND
ND
ND
ND
ND
ND
Mercury (mg/kg)
0.051
0.064
0.033
ND
ND
ND
VOCs (mg/kg)
ND
ND
ND
ND
ND
ND
SVOCs (mg/kg)
ND
ND
ND
ND
ND
ND
TerraTech Engineers, Inc.
NC Engineering Corporation C-1356
4905 Professional Court • Raleigh, North Carolina 27609
Phone: [phone] • Fax: [phone]

Page 2 of 2
TFRP ECH
E N G I N E E R S- I N C
Geotechnical Engineering
Environmental Consulting
Construction Materials Testing
Semi -Volatile Organic Compounds and Volatile Organic Compounds were not detected in any of the soil
samples collected. Various metals including Arsenic, Barium, Chromium, Lead, Selenium, and Mercury
were detected in the soil samples collected at levels below the Industrial/Commercial action levels
established in the NC Maximum Soil Contamination Concentration (MSCC) levels established by the
NCDEQ. A copy of these guidelines are included in the Appendix.
Closure
We appreciate the opportunity to provide these soil testing services. If you have any questions concerning
these test results or if we can be of further service to you, please do not hesitate to contact us.
Sincerely,
TerraTech Engineers, Inc. (C-1356)
William B. Strayhorn
Project Manager
WBS/sk
Enclosures: Pace Analytical Test Report
NCDEQ Table 1
` CAR0f
Q.o
Erwin T. Williams 11I:EAR
Principal Environmental Czsu�gp
2
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/// /N T iW ; \\\\���

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 16, 2017
Will Strayhorn
Terratech Engineers
4905 Professional Court
Raleigh, NC 27609
RE: Project: SOIL SAMPLING
Pace Project No.: 92329914
Dear Will Strayhorn:
Enclosed are the analytical results for sample(s) received by the laboratory on February 13, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, p
Taylor Ezell
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOIL SAMPLING
Pace Project No.: 92329914
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 53

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SOIL SAMPLING
92329914
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92329914001
B-1
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
RES
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92329914002
B-2
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
RES
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92329914003
B-3
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
RES
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92329914004
B-4
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
RES
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92329914005
B-5
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
RES
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92329914006
B-6
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
RES
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-1
Lab ID: 92329914001
Collected: 02/13/17
12:50
Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
7.1
mg/kg
1.0
1
02/15/17 23:00
02/16/17 11:21
7440-38-2 M1
Barium
22.7
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:21
7440-39-3
Cadmium
ND
mg/kg
0.10
1
02/15/17 23:00
02/16/17 11:21
7440-43-9
Chromium
6.3
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:21
7440-47-3
Lead
10.4
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:21
7439-92-1
Selenium
3.4
mg/kg
1.0
1
02/15/17 23:00
02/16/17 11:21
7782-49-2 M1
Silver
ND
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:21
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
0.051
mg/kg
0.0057
1
02/16/17 05:55
02/16/17 10:21
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
83-32-9
Acenaphthylene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
208-96-8
Aniline
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
62-53-3
Anthracene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
120-12-7
Benzo(a)anthracene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
56-55-3
Benzo(a)pyrene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
207-08-9
Benzoic Acid
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
65-85-0
Benzyl alcohol
ND
ug/kg
831
1
02/15/17 08:30
02/15/17 14:58
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
101-55-3
Butylbenzylphthalate
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
831
1
02/15/17 08:30
02/15/17 14:58
59-50-7
4-Chloroaniline
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
111-44-4
2-Chloronaphthalene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
91-58-7
2-Chlorophenol
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
7005-72-3
Chrysene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
53-70-3
Dibenzofuran
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
91-94-1
2,4-Dichlorophenol
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
120-83-2
Diethylphthalate
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
84-66-2
2,4-Dimethylphenol
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
105-67-9
Dimethylphthalate
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
131-11-3
Di-n-butylphthalate
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
831
1
02/15/17 08:30
02/15/17 14:58
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-1
Lab ID: 92329914001 Collected: 02/13/17
12:50
Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
606-20-2
Di-n-octylphthalate
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
117-81-7
Fluoranthene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
206-44-0
Fluorene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
87-68-3
Hexachlorobenzene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
77-47-4
Hexachloroethane
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
193-39-5
Isophorone
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
78-59-1
1-Methylnaphthalene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
90-12-0
2-Methylnaphthalene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
Naphthalene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
91-20-3
2-Nitroaniline
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
88-74-4
3-Nitroaniline
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
99-09-2
4-Nitroaniline
ND
ug/kg
831
1
02/15/17 08:30
02/15/17 14:58
100-01-6
Nitrobenzene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
98-95-3
2-Nitrophenol
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
88-75-5
4-Nitrophenol
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
108-60-1 M1
Pentachlorophenol
ND
ug/kg
2080
1
02/15/17 08:30
02/15/17 14:58
87-86-5
Phenanthrene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
85-01-8
Phenol
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
Pyrene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
415
1
02/15/17 08:30
02/15/17 14:58
88-06-2
Surrogates
Nitrobenzene-d5 (S)
42
%
23-110
1
02/15/17 08:30
02/15/17 14:58
4165-60-0
2-Fluorobiphenyl (S)
64
%
30-110
1
02/15/17 08:30
02/15/17 14:58
321-60-8
Terphenyl-dl4 (S)
80
%
28-110
1
02/15/17 08:30
02/15/17 14:58
1718-51-0
Phenol-d6 (S)
55
%
22-110
1
02/15/17 08:30
02/15/17 14:58
13127-88-3
2-Fluorophenol (S)
56
%
13-110
1
02/15/17 08:30
02/15/17 14:58
367-12-4
2,4,6-Tribromophenol (S)
83
%
27-110
1
02/15/17 08:30
02/15/17 14:58
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND
ug/kg
170
1
02/15/1716:46
67-64-1
Benzene
ND
ug/kg
8.5
1
02/15/1716:46
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-1 Lab ID: 92329914001 Collected: 02/13/17 12:50 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
ug/kg
8.5
1
02/15/17 16:46
108-86-1
Bromochloromethane
ND
ug/kg
8.5
1
02/15/17 16:46
74-97-5
Bromodichloromethane
ND
ug/kg
8.5
1
02/15/17 16:46
75-27-4
Bromoform
ND
ug/kg
8.5
1
02/15/17 16:46
75-25-2
Bromomethane
ND
ug/kg
17.0
1
02/15/17 16:46
74-83-9
2-Butanone (MEK)
ND
ug/kg
170
1
02/15/17 16:46
78-93-3
n-Butylbenzene
ND
ug/kg
8.5
1
02/15/17 16:46
104-51-8
sec-Butylbenzene
ND
ug/kg
8.5
1
02/15/17 16:46
135-98-8
tert-Butyl benzene
ND
ug/kg
8.5
1
02/15/17 16:46
98-06-6
Carbon tetrachloride
ND
ug/kg
8.5
1
02/15/17 16:46
56-23-5
Chlorobenzene
ND
ug/kg
8.5
1
02/15/17 16:46
108-90-7
Chloroethane
ND
ug/kg
17.0
1
02/15/17 16:46
75-00-3
Chloroform
ND
ug/kg
8.5
1
02/15/17 16:46
67-66-3
Chloromethane
ND
ug/kg
17.0
1
02/15/17 16:46
74-87-3
2-Chlorotoluene
ND
ug/kg
8.5
1
02/15/17 16:46
95-49-8
4-Chlorotoluene
ND
ug/kg
8.5
1
02/15/17 16:46
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
8.5
1
02/15/17 16:46
96-12-8
Dibromochloromethane
ND
ug/kg
8.5
1
02/15/17 16:46
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
8.5
1
02/15/17 16:46
106-93-4
Dibromomethane
ND
ug/kg
8.5
1
02/15/17 16:46
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
8.5
1
02/15/17 16:46
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
8.5
1
02/15/17 16:46
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
8.5
1
02/15/17 16:46
106-46-7
Dichlorodifluoromethane
ND
ug/kg
17.0
1
02/15/17 16:46
75-71-8
1,1-Dichloroethane
ND
ug/kg
8.5
1
02/15/17 16:46
75-34-3
1,2-Dichloroethane
ND
ug/kg
8.5
1
02/15/17 16:46
107-06-2
1,1-Dichloroethene
ND
ug/kg
8.5
1
02/15/17 16:46
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
8.5
1
02/15/17 16:46
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
8.5
1
02/15/17 16:46
156-60-5
1,2-Dichloropropane
ND
ug/kg
8.5
1
02/15/17 16:46
78-87-5
1,3-Dichloropropane
ND
ug/kg
8.5
1
02/15/17 16:46
142-28-9
2,2-Dichloropropane
ND
ug/kg
8.5
1
02/15/17 16:46
594-20-7
1,1-Dichloropropene
ND
ug/kg
8.5
1
02/15/17 16:46
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
8.5
1
02/15/17 16:46
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
8.5
1
02/15/17 16:46
10061-02-6
Diisopropyl ether
ND
ug/kg
8.5
1
02/15/17 16:46
108-20-3
Ethylbenzene
ND
ug/kg
8.5
1
02/15/17 16:46
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
8.5
1
02/15/17 16:46
87-68-3
2-Hexanone
ND
ug/kg
84.8
1
02/15/17 16:46
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
8.5
1
02/15/17 16:46
98-82-8
p-Isopropyltoluene
ND
ug/kg
8.5
1
02/15/17 16:46
99-87-6
Methylene Chloride
ND
ug/kg
33.9
1
02/15/17 16:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
84.8
1
02/15/17 16:46
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
8.5
1
02/15/17 16:46
1634-04-4
Naphthalene
ND
ug/kg
8.5
1
02/15/17 16:46
91-20-3
n-Propylbenzene
ND
ug/kg
8.5
1
02/15/17 16:46
103-65-1
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-1 Lab ID: 92329914001 Collected: 02/13/17 12:50 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
ug/kg
8.5
1
02/15/1716:46
100-42-5
ND
ug/kg
8.5
1
02/15/1716:46
630-20-6
ND
ug/kg
8.5
1
02/15/1716:46
79-34-5
ND
ug/kg
8.5
1
02/15/1716:46
127-18-4
ND
ug/kg
8.5
1
02/15/1716:46
108-88-3
ND
ug/kg
8.5
1
02/15/1716:46
87-61-6
ND
ug/kg
8.5
1
02/15/1716:46
120-82-1
ND
ug/kg
8.5
1
02/15/1716:46
71-55-6
ND
ug/kg
8.5
1
02/15/1716:46
79-00-5
ND
ug/kg
8.5
1
02/15/1716:46
79-01-6
ND
ug/kg
8.5
1
02/15/1716:46
75-69-4
ND
ug/kg
8.5
1
02/15/1716:46
96-18-4
ND
ug/kg
8.5
1
02/15/1716:46
95-63-6
ND
ug/kg
8.5
1
02/15/1716:46
108-67-8
ND
ug/kg
84.8
1
02/15/1716:46
108-05-4
ND
ug/kg
17.0
1
02/15/1716:46
75-01-4
ND
ug/kg
17.0
1
02/15/1716:46
1330-20-7
ND
ug/kg
17.0
1
02/15/1716:46
179601-23-1
ND
ug/kg
8.5
1
02/15/1716:46
95-47-6
105
%
70-130
1
02/15/1716:46
2037-26-5
102
%
70-130
1
02/15/1716:46
460-00-4
81
%
70-132
1
02/15/1716:46
17060-07-0
Analytical Method: ASTM D2974-87
20.5 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/15/17 07:07
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 53

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Pace Analytical Services, LLC
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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-2 Lab ID: 92329914002 Collected: 02/13/17 13:00 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
4.2
mg/kg
0.96
1
02/15/17 23:00
02/16/17 11:29
7440-38-2
Barium
16.0
mg/kg
0.48
1
02/15/17 23:00
02/16/17 11:29
7440-39-3
Cadmium
ND
mg/kg
0.096
1
02/15/17 23:00
02/16/17 11:29
7440-43-9
Chromium
5.7
mg/kg
0.48
1
02/15/17 23:00
02/16/17 11:29
7440-47-3
Lead
10.9
mg/kg
0.48
1
02/15/17 23:00
02/16/17 11:29
7439-92-1
Selenium
3.5
mg/kg
0.96
1
02/15/17 23:00
02/16/17 11:29
7782-49-2
Silver
ND
mg/kg
0.48
1
02/15/17 23:00
02/16/17 11:29
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.064
mg/kg
0.0061
1
02/16/17 05:55
02/16/17 10:23
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
83-32-9
Acenaphthylene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
208-96-8
Aniline
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
62-53-3
Anthracene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
120-12-7
Benzo(a)anthracene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
56-55-3
Benzo(a)pyrene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
207-08-9
Benzoic Acid
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
65-85-0
Benzyl alcohol
ND
ug/kg
763
1
02/15/17 08:30
02/16/17 10:37
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
101-55-3
Butylbenzylphthalate
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
763
1
02/15/17 08:30
02/16/17 10:37
59-50-7
4-Chloroaniline
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
111-44-4
2-Chloronaphthalene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
91-58-7
2-Chlorophenol
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
7005-72-3
Chrysene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
53-70-3
Dibenzofuran
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
91-94-1
2,4-Dichlorophenol
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
120-83-2
Diethylphthalate
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
84-66-2
2,4-Dimethylphenol
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
105-67-9
Dimethylphthalate
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
131-11-3
Di-n-butylphthalate
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
763
1
02/15/17 08:30
02/16/17 10:37
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 53

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-2 Lab ID: 92329914002 Collected: 02/13/17 13:00 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
606-20-2
Di-n-octylphthalate
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
117-81-7
Fluoranthene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
206-44-0
Fluorene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
87-68-3
Hexachlorobenzene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
77-47-4
Hexachloroethane
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
193-39-5
Isophorone
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
78-59-1
1-Methylnaphthalene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
90-12-0
2-Methylnaphthalene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
Naphthalene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
91-20-3
2-Nitroaniline
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
88-74-4
3-Nitroaniline
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
99-09-2
4-Nitroaniline
ND
ug/kg
763
1
02/15/17 08:30
02/16/17 10:37
100-01-6
Nitrobenzene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
98-95-3
2-Nitrophenol
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
88-75-5
4-Nitrophenol
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
108-60-1
Pentachlorophenol
ND
ug/kg
1910
1
02/15/17 08:30
02/16/17 10:37
87-86-5
Phenanthrene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
85-01-8
Phenol
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
Pyrene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
381
1
02/15/17 08:30
02/16/17 10:37
88-06-2
Surrogates
Nitrobenzene-d5 (S)
54
%
23-110
1
02/15/17 08:30
02/16/17 10:37
4165-60-0
2-Fluorobiphenyl (S)
58
%
30-110
1
02/15/17 08:30
02/16/17 10:37
321-60-8
Terphenyl-dl4 (S)
60
%
28-110
1
02/15/17 08:30
02/16/17 10:37
1718-51-0
Phenol-d6 (S)
51
%
22-110
1
02/15/17 08:30
02/16/17 10:37
13127-88-3
2-Fluorophenol (S)
54
%
13-110
1
02/15/17 08:30
02/16/17 10:37
367-12-4
2,4,6-Tribromophenol (S)
60
%
27-110
1
02/15/17 08:30
02/16/17 10:37
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND
ug/kg
222
1
02/15/1717:06
67-64-1
Benzene
ND
ug/kg
11.1
1
02/15/1717:06
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 53

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-2 Lab ID: 92329914002 Collected: 02/13/17 13:00 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
ug/kg
11.1
1
02/15/17 17:06
108-86-1
Bromochloromethane
ND
ug/kg
11.1
1
02/15/17 17:06
74-97-5
Bromodichloromethane
ND
ug/kg
11.1
1
02/15/17 17:06
75-27-4
Bromoform
ND
ug/kg
11.1
1
02/15/17 17:06
75-25-2
Bromomethane
ND
ug/kg
22.2
1
02/15/17 17:06
74-83-9
2-Butanone (MEK)
ND
ug/kg
222
1
02/15/17 17:06
78-93-3
n-Butylbenzene
ND
ug/kg
11.1
1
02/15/17 17:06
104-51-8
sec-Butylbenzene
ND
ug/kg
11.1
1
02/15/17 17:06
135-98-8
tert-Butyl benzene
ND
ug/kg
11.1
1
02/15/17 17:06
98-06-6
Carbon tetrachloride
ND
ug/kg
11.1
1
02/15/17 17:06
56-23-5
Chlorobenzene
ND
ug/kg
11.1
1
02/15/17 17:06
108-90-7
Chloroethane
ND
ug/kg
22.2
1
02/15/17 17:06
75-00-3
Chloroform
ND
ug/kg
11.1
1
02/15/17 17:06
67-66-3
Chloromethane
ND
ug/kg
22.2
1
02/15/17 17:06
74-87-3
2-Chlorotoluene
ND
ug/kg
11.1
1
02/15/17 17:06
95-49-8
4-Chlorotoluene
ND
ug/kg
11.1
1
02/15/17 17:06
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
11.1
1
02/15/17 17:06
96-12-8
Dibromochloromethane
ND
ug/kg
11.1
1
02/15/17 17:06
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
11.1
1
02/15/17 17:06
106-93-4
Dibromomethane
ND
ug/kg
11.1
1
02/15/17 17:06
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
11.1
1
02/15/17 17:06
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
11.1
1
02/15/17 17:06
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
11.1
1
02/15/17 17:06
106-46-7
Dichlorodifluoromethane
ND
ug/kg
22.2
1
02/15/17 17:06
75-71-8
1,1-Dichloroethane
ND
ug/kg
11.1
1
02/15/17 17:06
75-34-3
1,2-Dichloroethane
ND
ug/kg
11.1
1
02/15/17 17:06
107-06-2
1,1-Dichloroethene
ND
ug/kg
11.1
1
02/15/17 17:06
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
11.1
1
02/15/17 17:06
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
11.1
1
02/15/17 17:06
156-60-5
1,2-Dichloropropane
ND
ug/kg
11.1
1
02/15/17 17:06
78-87-5
1,3-Dichloropropane
ND
ug/kg
11.1
1
02/15/17 17:06
142-28-9
2,2-Dichloropropane
ND
ug/kg
11.1
1
02/15/17 17:06
594-20-7
1,1-Dichloropropene
ND
ug/kg
11.1
1
02/15/17 17:06
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
11.1
1
02/15/17 17:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
11.1
1
02/15/17 17:06
10061-02-6
Diisopropyl ether
ND
ug/kg
11.1
1
02/15/17 17:06
108-20-3
Ethylbenzene
ND
ug/kg
11.1
1
02/15/17 17:06
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
11.1
1
02/15/17 17:06
87-68-3
2-Hexanone
ND
ug/kg
ill
1
02/15/17 17:06
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
11.1
1
02/15/17 17:06
98-82-8
p-Isopropyltoluene
ND
ug/kg
11.1
1
02/15/17 17:06
99-87-6
Methylene Chloride
ND
ug/kg
44.4
1
02/15/17 17:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
ill
1
02/15/17 17:06
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
11.1
1
02/15/17 17:06
1634-04-4
Naphthalene
ND
ug/kg
11.1
1
02/15/17 17:06
91-20-3
n-Propylbenzene
ND
ug/kg
11.1
1
02/15/17 17:06
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-2 Lab ID: 92329914002 Collected: 02/13/17 13:00 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
ug/kg
11.1
1
02/15/1717:06
100-42-5
ND
ug/kg
11.1
1
02/15/1717:06
630-20-6
ND
ug/kg
11.1
1
02/15/1717:06
79-34-5
ND
ug/kg
11.1
1
02/15/1717:06
127-18-4
ND
ug/kg
11.1
1
02/15/1717:06
108-88-3
ND
ug/kg
11.1
1
02/15/1717:06
87-61-6
ND
ug/kg
11.1
1
02/15/1717:06
120-82-1
ND
ug/kg
11.1
1
02/15/1717:06
71-55-6
ND
ug/kg
11.1
1
02/15/1717:06
79-00-5
ND
ug/kg
11.1
1
02/15/1717:06
79-01-6
ND
ug/kg
11.1
1
02/15/1717:06
75-69-4
ND
ug/kg
11.1
1
02/15/1717:06
96-18-4
ND
ug/kg
11.1
1
02/15/1717:06
95-63-6
ND
ug/kg
11.1
1
02/15/1717:06
108-67-8
ND
ug/kg
ill
1
02/15/1717:06
108-05-4
ND
ug/kg
22.2
1
02/15/1717:06
75-01-4
ND
ug/kg
22.2
1
02/15/1717:06
1330-20-7
ND
ug/kg
22.2
1
02/15/1717:06
179601-23-1
ND
ug/kg
11.1
1
02/15/1717:06
95-47-6
106
%
70-130
1
02/15/1717:06
2037-26-5
101
%
70-130
1
02/15/1717:06
460-00-4
82
%
70-132
1
02/15/1717:06
17060-07-0
Analytical Method: ASTM D2974-87
13.4 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/15/17 07:07
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-3 Lab ID: 92329914003 Collected: 02/13/17 13:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
5.3
mg/kg
0.85
1
02/15/17 23:00
02/16/17 11:33
7440-38-2
Barium
25.8
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:33
7440-39-3
Cadmium
ND
mg/kg
0.085
1
02/15/17 23:00
02/16/17 11:33
7440-43-9
Chromium
6.5
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:33
7440-47-3
Lead
9.9
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:33
7439-92-1
Selenium
3.1
mg/kg
0.85
1
02/15/17 23:00
02/16/17 11:33
7782-49-2
Silver
ND
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:33
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.033
mg/kg
0.0031
1
02/16/17 05:55
02/16/17 10:26
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
83-32-9
Acenaphthylene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
208-96-8
Aniline
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
62-53-3
Anthracene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
120-12-7
Benzo(a)anthracene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
56-55-3
Benzo(a)pyrene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
207-08-9
Benzoic Acid
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
65-85-0
Benzyl alcohol
ND
ug/kg
856
1
02/15/17 08:30
02/15/17 16:34
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
101-55-3
Butylbenzylphthalate
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
856
1
02/15/17 08:30
02/15/17 16:34
59-50-7
4-Chloroaniline
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
111-44-4
2-Chloronaphthalene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
91-58-7
2-Chlorophenol
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
7005-72-3
Chrysene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
53-70-3
Dibenzofuran
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
91-94-1
2,4-Dichlorophenol
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
120-83-2
Diethylphthalate
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
84-66-2
2,4-Dimethylphenol
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
105-67-9
Dimethylphthalate
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
131-11-3
Di-n-butylphthalate
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
856
1
02/15/17 08:30
02/15/17 16:34
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 53

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-3 Lab ID: 92329914003 Collected: 02/13/17 13:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
606-20-2
Di-n-octylphthalate
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
117-81-7
Fluoranthene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
206-44-0
Fluorene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
87-68-3
Hexachlorobenzene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
77-47-4
Hexachloroethane
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
193-39-5
Isophorone
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
78-59-1
1-Methylnaphthalene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
90-12-0
2-Methylnaphthalene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
Naphthalene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
91-20-3
2-Nitroaniline
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
88-74-4
3-Nitroaniline
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
99-09-2
4-Nitroaniline
ND
ug/kg
856
1
02/15/17 08:30
02/15/17 16:34
100-01-6
Nitrobenzene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
98-95-3
2-Nitrophenol
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
88-75-5
4-Nitrophenol
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
108-60-1
Pentachlorophenol
ND
ug/kg
2140
1
02/15/17 08:30
02/15/17 16:34
87-86-5
Phenanthrene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
85-01-8
Phenol
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
Pyrene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
428
1
02/15/17 08:30
02/15/17 16:34
88-06-2
Surrogates
Nitrobenzene-d5 (S)
42
%
23-110
1
02/15/17 08:30
02/15/17 16:34
4165-60-0
2-Fluorobiphenyl (S)
52
%
30-110
1
02/15/17 08:30
02/15/17 16:34
321-60-8
Terphenyl-dl4 (S)
68
%
28-110
1
02/15/17 08:30
02/15/17 16:34
1718-51-0
Phenol-d6 (S)
41
%
22-110
1
02/15/17 08:30
02/15/17 16:34
13127-88-3
2-Fluorophenol (S)
48
%
13-110
1
02/15/17 08:30
02/15/17 16:34
367-12-4
2,4,6-Tribromophenol (S)
68
%
27-110
1
02/15/17 08:30
02/15/17 16:34
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND
ug/kg
155
1
02/16/1713:13
67-64-1
Benzene
ND
ug/kg
7.8
1
02/16/1713:13
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 53

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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-3 Lab ID: 92329914003 Collected: 02/13/17 13:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
ug/kg
7.8
1
02/16/17 13:13
108-86-1
Bromochloromethane
ND
ug/kg
7.8
1
02/16/17 13:13
74-97-5
Bromodichloromethane
ND
ug/kg
7.8
1
02/16/17 13:13
75-27-4
Bromoform
ND
ug/kg
7.8
1
02/16/17 13:13
75-25-2
Bromomethane
ND
ug/kg
15.5
1
02/16/17 13:13
74-83-9
2-Butanone (MEK)
ND
ug/kg
155
1
02/16/17 13:13
78-93-3
n-Butylbenzene
ND
ug/kg
7.8
1
02/16/17 13:13
104-51-8
sec-Butylbenzene
ND
ug/kg
7.8
1
02/16/17 13:13
135-98-8
tert-Butyl benzene
ND
ug/kg
7.8
1
02/16/17 13:13
98-06-6
Carbon tetrachloride
ND
ug/kg
7.8
1
02/16/17 13:13
56-23-5
Chlorobenzene
ND
ug/kg
7.8
1
02/16/17 13:13
108-90-7
Chloroethane
ND
ug/kg
15.5
1
02/16/17 13:13
75-00-3
Chloroform
ND
ug/kg
7.8
1
02/16/17 13:13
67-66-3
Chloromethane
ND
ug/kg
15.5
1
02/16/17 13:13
74-87-3
2-Chlorotoluene
ND
ug/kg
7.8
1
02/16/17 13:13
95-49-8
4-Chlorotoluene
ND
ug/kg
7.8
1
02/16/17 13:13
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.8
1
02/16/17 13:13
96-12-8
Dibromochloromethane
ND
ug/kg
7.8
1
02/16/17 13:13
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.8
1
02/16/17 13:13
106-93-4
Dibromomethane
ND
ug/kg
7.8
1
02/16/17 13:13
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.8
1
02/16/17 13:13
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.8
1
02/16/17 13:13
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.8
1
02/16/17 13:13
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.5
1
02/16/17 13:13
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.8
1
02/16/17 13:13
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.8
1
02/16/17 13:13
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.8
1
02/16/17 13:13
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.8
1
02/16/17 13:13
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.8
1
02/16/17 13:13
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.8
1
02/16/17 13:13
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.8
1
02/16/17 13:13
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.8
1
02/16/17 13:13
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.8
1
02/16/17 13:13
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
7.8
1
02/16/17 13:13
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.8
1
02/16/17 13:13
10061-02-6
Diisopropyl ether
ND
ug/kg
7.8
1
02/16/17 13:13
108-20-3
Ethylbenzene
ND
ug/kg
7.8
1
02/16/17 13:13
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
7.8
1
02/16/17 13:13
87-68-3
2-Hexanone
ND
ug/kg
77.7
1
02/16/17 13:13
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.8
1
02/16/17 13:13
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.8
1
02/16/17 13:13
99-87-6
Methylene Chloride
ND
ug/kg
31.1
1
02/16/17 13:13
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
77.7
1
02/16/17 13:13
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.8
1
02/16/17 13:13
1634-04-4
Naphthalene
ND
ug/kg
7.8
1
02/16/17 13:13
91-20-3
n-Propylbenzene
ND
ug/kg
7.8
1
02/16/17 13:13
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-3 Lab ID: 92329914003 Collected: 02/13/17 13:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
ug/kg
7.8
1
02/16/1713:13
100-42-5
ND
ug/kg
7.8
1
02/16/1713:13
630-20-6
ND
ug/kg
7.8
1
02/16/1713:13
79-34-5
ND
ug/kg
7.8
1
02/16/1713:13
127-18-4
ND
ug/kg
7.8
1
02/16/1713:13
108-88-3
ND
ug/kg
7.8
1
02/16/1713:13
87-61-6
ND
ug/kg
7.8
1
02/16/1713:13
120-82-1
ND
ug/kg
7.8
1
02/16/1713:13
71-55-6
ND
ug/kg
7.8
1
02/16/1713:13
79-00-5
ND
ug/kg
7.8
1
02/16/1713:13
79-01-6
ND
ug/kg
7.8
1
02/16/1713:13
75-69-4
ND
ug/kg
7.8
1
02/16/1713:13
96-18-4
ND
ug/kg
7.8
1
02/16/1713:13
95-63-6
ND
ug/kg
7.8
1
02/16/1713:13
108-67-8
ND
ug/kg
77.7
1
02/16/1713:13
108-05-4
ND
ug/kg
15.5
1
02/16/1713:13
75-01-4
ND
ug/kg
15.5
1
02/16/1713:13
1330-20-7
ND
ug/kg
15.5
1
02/16/1713:13
179601-23-1
ND
ug/kg
7.8
1
02/16/1713:13
95-47-6
103
%
70-130
1
02/16/1713:13
2037-26-5
100
%
70-130
1
02/16/1713:13
460-00-4
80
%
70-132
1
02/16/1713:13
17060-07-0
Analytical Method: ASTM D2974-87
22.9 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/15/17 07:08
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-4 Lab ID: 92329914004 Collected: 02/13/17 14:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
1.9
mg/kg
0.90
1
02/15/17 23:00
02/16/17 11:36
7440-38-2
Barium
63.5
mg/kg
0.45
1
02/15/17 23:00
02/16/17 11:36
7440-39-3
Cadmium
ND
mg/kg
0.090
1
02/15/17 23:00
02/16/17 11:36
7440-43-9
Chromium
4.9
mg/kg
0.45
1
02/15/17 23:00
02/16/17 11:36
7440-47-3
Lead
7.9
mg/kg
0.45
1
02/15/17 23:00
02/16/17 11:36
7439-92-1
Selenium
ND
mg/kg
0.90
1
02/15/17 23:00
02/16/17 11:36
7782-49-2
Silver
ND
mg/kg
0.45
1
02/15/17 23:00
02/16/17 11:36
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
ND
mg/kg
0.0044
1
02/16/17 05:55
02/16/17 10:28
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
83-32-9
Acenaphthylene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
208-96-8
Aniline
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
62-53-3
Anthracene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
120-12-7
Benzo(a)anthracene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
56-55-3
Benzo(a)pyrene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
207-08-9
Benzoic Acid
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
65-85-0
Benzyl alcohol
ND
ug/kg
750
1
02/15/17 08:30
02/15/17 17:07
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
101-55-3
Butylbenzylphthalate
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
750
1
02/15/17 08:30
02/15/17 17:07
59-50-7
4-Chloroaniline
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
111-44-4
2-Chloronaphthalene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
91-58-7
2-Chlorophenol
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
7005-72-3
Chrysene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
53-70-3
Dibenzofuran
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
91-94-1
2,4-Dichlorophenol
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
120-83-2
Diethylphthalate
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
84-66-2
2,4-Dimethylphenol
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
105-67-9
Dimethylphthalate
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
131-11-3
Di-n-butylphthalate
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
750
1
02/15/17 08:30
02/15/17 17:07
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 53

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Pace Analytical Services, LLC
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[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-4 Lab ID: 92329914004 Collected: 02/13/17 14:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
606-20-2
Di-n-octylphthalate
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
117-81-7
Fluoranthene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
206-44-0
Fluorene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
87-68-3
Hexachlorobenzene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
77-47-4
Hexachloroethane
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
193-39-5
Isophorone
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
78-59-1
1-Methylnaphthalene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
90-12-0
2-Methylnaphthalene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
Naphthalene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
91-20-3
2-Nitroaniline
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
88-74-4
3-Nitroaniline
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
99-09-2
4-Nitroaniline
ND
ug/kg
750
1
02/15/17 08:30
02/15/17 17:07
100-01-6
Nitrobenzene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
98-95-3
2-Nitrophenol
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
88-75-5
4-Nitrophenol
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
108-60-1
Pentachlorophenol
ND
ug/kg
1870
1
02/15/17 08:30
02/15/17 17:07
87-86-5
Phenanthrene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
85-01-8
Phenol
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
Pyrene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
375
1
02/15/17 08:30
02/15/17 17:07
88-06-2
Surrogates
Nitrobenzene-d5 (S)
32
%
23-110
1
02/15/17 08:30
02/15/17 17:07
4165-60-0
2-Fluorobiphenyl (S)
43
%
30-110
1
02/15/17 08:30
02/15/17 17:07
321-60-8
Terphenyl-dl4 (S)
52
%
28-110
1
02/15/17 08:30
02/15/17 17:07
1718-51-0
Phenol-d6 (S)
45
%
22-110
1
02/15/17 08:30
02/15/17 17:07
13127-88-3
2-Fluorophenol (S)
50
%
13-110
1
02/15/17 08:30
02/15/17 17:07
367-12-4
2,4,6-Tribromophenol (S)
54
%
27-110
1
02/15/17 08:30
02/15/17 17:07
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND
ug/kg
157
1
02/15/1717:47
67-64-1
Benzene
ND
ug/kg
7.8
1
02/15/1717:47
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 53

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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-4 Lab ID: 92329914004 Collected: 02/13/17 14:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
ug/kg
7.8
1
02/15/17 17:47
108-86-1
Bromochloromethane
ND
ug/kg
7.8
1
02/15/17 17:47
74-97-5
Bromodichloromethane
ND
ug/kg
7.8
1
02/15/17 17:47
75-27-4
Bromoform
ND
ug/kg
7.8
1
02/15/17 17:47
75-25-2
Bromomethane
ND
ug/kg
15.7
1
02/15/17 17:47
74-83-9
2-Butanone (MEK)
ND
ug/kg
157
1
02/15/17 17:47
78-93-3
n-Butylbenzene
ND
ug/kg
7.8
1
02/15/17 17:47
104-51-8
sec-Butylbenzene
ND
ug/kg
7.8
1
02/15/17 17:47
135-98-8
tert-Butyl benzene
ND
ug/kg
7.8
1
02/15/17 17:47
98-06-6
Carbon tetrachloride
ND
ug/kg
7.8
1
02/15/17 17:47
56-23-5
Chlorobenzene
ND
ug/kg
7.8
1
02/15/17 17:47
108-90-7
Chloroethane
ND
ug/kg
15.7
1
02/15/17 17:47
75-00-3
Chloroform
ND
ug/kg
7.8
1
02/15/17 17:47
67-66-3
Chloromethane
ND
ug/kg
15.7
1
02/15/17 17:47
74-87-3
2-Chlorotoluene
ND
ug/kg
7.8
1
02/15/17 17:47
95-49-8
4-Chlorotoluene
ND
ug/kg
7.8
1
02/15/17 17:47
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
7.8
1
02/15/17 17:47
96-12-8
Dibromochloromethane
ND
ug/kg
7.8
1
02/15/17 17:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
7.8
1
02/15/17 17:47
106-93-4
Dibromomethane
ND
ug/kg
7.8
1
02/15/17 17:47
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
7.8
1
02/15/17 17:47
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
7.8
1
02/15/17 17:47
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
7.8
1
02/15/17 17:47
106-46-7
Dichlorodifluoromethane
ND
ug/kg
15.7
1
02/15/17 17:47
75-71-8
1,1-Dichloroethane
ND
ug/kg
7.8
1
02/15/17 17:47
75-34-3
1,2-Dichloroethane
ND
ug/kg
7.8
1
02/15/17 17:47
107-06-2
1,1-Dichloroethene
ND
ug/kg
7.8
1
02/15/17 17:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
7.8
1
02/15/17 17:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
7.8
1
02/15/17 17:47
156-60-5
1,2-Dichloropropane
ND
ug/kg
7.8
1
02/15/17 17:47
78-87-5
1,3-Dichloropropane
ND
ug/kg
7.8
1
02/15/17 17:47
142-28-9
2,2-Dichloropropane
ND
ug/kg
7.8
1
02/15/17 17:47
594-20-7
1,1-Dichloropropene
ND
ug/kg
7.8
1
02/15/17 17:47
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
7.8
1
02/15/17 17:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
7.8
1
02/15/17 17:47
10061-02-6
Diisopropyl ether
ND
ug/kg
7.8
1
02/15/17 17:47
108-20-3
Ethylbenzene
ND
ug/kg
7.8
1
02/15/17 17:47
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
7.8
1
02/15/17 17:47
87-68-3
2-Hexanone
ND
ug/kg
78.5
1
02/15/17 17:47
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
7.8
1
02/15/17 17:47
98-82-8
p-Isopropyltoluene
ND
ug/kg
7.8
1
02/15/17 17:47
99-87-6
Methylene Chloride
ND
ug/kg
31.4
1
02/15/17 17:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
78.5
1
02/15/17 17:47
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
7.8
1
02/15/17 17:47
1634-04-4
Naphthalene
ND
ug/kg
7.8
1
02/15/17 17:47
91-20-3
n-Propylbenzene
ND
ug/kg
7.8
1
02/15/17 17:47
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-4 Lab ID: 92329914004 Collected: 02/13/17 14:05 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
ug/kg
7.8
1
02/15/1717:47
100-42-5
ND
ug/kg
7.8
1
02/15/1717:47
630-20-6
ND
ug/kg
7.8
1
02/15/1717:47
79-34-5
ND
ug/kg
7.8
1
02/15/1717:47
127-18-4
ND
ug/kg
7.8
1
02/15/1717:47
108-88-3
ND
ug/kg
7.8
1
02/15/1717:47
87-61-6
ND
ug/kg
7.8
1
02/15/1717:47
120-82-1
ND
ug/kg
7.8
1
02/15/1717:47
71-55-6
ND
ug/kg
7.8
1
02/15/1717:47
79-00-5
ND
ug/kg
7.8
1
02/15/1717:47
79-01-6
ND
ug/kg
7.8
1
02/15/1717:47
75-69-4
ND
ug/kg
7.8
1
02/15/1717:47
96-18-4
ND
ug/kg
7.8
1
02/15/1717:47
95-63-6
ND
ug/kg
7.8
1
02/15/1717:47
108-67-8
ND
ug/kg
78.5
1
02/15/1717:47
108-05-4
ND
ug/kg
15.7
1
02/15/1717:47
75-01-4
ND
ug/kg
15.7
1
02/15/1717:47
1330-20-7
ND
ug/kg
15.7
1
02/15/1717:47
179601-23-1
ND
ug/kg
7.8
1
02/15/1717:47
95-47-6
104
%
70-130
1
02/15/1717:47
2037-26-5
100
%
70-130
1
02/15/1717:47
460-00-4
86
%
70-132
1
02/15/1717:47
17060-07-0
Analytical Method: ASTM D2974-87
12.0 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/15/17 07:08
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-5 Lab ID: 92329914005 Collected: 02/13/17 14:15 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
1.8
mg/kg
1.0
1
02/15/17 23:00
02/16/17 11:48
7440-38-2
Barium
57.1
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:48
7440-39-3
Cadmium
ND
mg/kg
0.10
1
02/15/17 23:00
02/16/17 11:48
7440-43-9
Chromium
6.2
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:48
7440-47-3
Lead
7.3
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:48
7439-92-1
Selenium
ND
mg/kg
1.0
1
02/15/17 23:00
02/16/17 11:48
7782-49-2
Silver
ND
mg/kg
0.52
1
02/15/17 23:00
02/16/17 11:48
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
ND
mg/kg
0.0034
1
02/16/17 05:55
02/16/17 10:30
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
83-32-9
Acenaphthylene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
208-96-8
Aniline
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
62-53-3
Anthracene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
120-12-7
Benzo(a)anthracene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
56-55-3
Benzo(a)pyrene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
207-08-9
Benzoic Acid
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
65-85-0
Benzyl alcohol
ND
ug/kg
777
1
02/15/17 08:30
02/15/17 17:39
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
101-55-3
Butylbenzylphthalate
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
777
1
02/15/17 08:30
02/15/17 17:39
59-50-7
4-Chloroaniline
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
111-44-4
2-Chloronaphthalene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
91-58-7
2-Chlorophenol
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
7005-72-3
Chrysene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
53-70-3
Dibenzofuran
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
91-94-1
2,4-Dichlorophenol
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
120-83-2
Diethylphthalate
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
84-66-2
2,4-Dimethylphenol
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
105-67-9
Dimethylphthalate
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
131-11-3
Di-n-butylphthalate
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
777
1
02/15/17 08:30
02/15/17 17:39
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 53

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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-5 Lab ID: 92329914005 Collected: 02/13/17 14:15 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
606-20-2
Di-n-octylphthalate
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
117-81-7
Fluoranthene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
206-44-0
Fluorene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
87-68-3
Hexachlorobenzene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
77-47-4
Hexachloroethane
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
193-39-5
Isophorone
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
78-59-1
1-Methylnaphthalene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
90-12-0
2-Methylnaphthalene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
Naphthalene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
91-20-3
2-Nitroaniline
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
88-74-4
3-Nitroaniline
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
99-09-2
4-Nitroaniline
ND
ug/kg
777
1
02/15/17 08:30
02/15/17 17:39
100-01-6
Nitrobenzene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
98-95-3
2-Nitrophenol
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
88-75-5
4-Nitrophenol
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
108-60-1
Pentachlorophenol
ND
ug/kg
1940
1
02/15/17 08:30
02/15/17 17:39
87-86-5
Phenanthrene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
85-01-8
Phenol
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
Pyrene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
389
1
02/15/17 08:30
02/15/17 17:39
88-06-2
Surrogates
Nitrobenzene-d5 (S)
48
%
23-110
1
02/15/17 08:30
02/15/17 17:39
4165-60-0
2-Fluorobiphenyl (S)
58
%
30-110
1
02/15/17 08:30
02/15/17 17:39
321-60-8
Terphenyl-dl4 (S)
81
%
28-110
1
02/15/17 08:30
02/15/17 17:39
1718-51-0
Phenol-d6 (S)
67
%
22-110
1
02/15/17 08:30
02/15/17 17:39
13127-88-3
2-Fluorophenol (S)
66
%
13-110
1
02/15/17 08:30
02/15/17 17:39
367-12-4
2,4,6-Tribromophenol (S)
94
%
27-110
1
02/15/17 08:30
02/15/17 17:39
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND
ug/kg
114
1
02/15/1718:08
67-64-1
Benzene
ND
ug/kg
5.7
1
02/15/1718:08
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 53

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-5 Lab ID: 92329914005 Collected: 02/13/17 14:15 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
ug/kg
5.7
1
02/15/17 18:08
108-86-1
Bromochloromethane
ND
ug/kg
5.7
1
02/15/17 18:08
74-97-5
Bromodichloromethane
ND
ug/kg
5.7
1
02/15/17 18:08
75-27-4
Bromoform
ND
ug/kg
5.7
1
02/15/17 18:08
75-25-2
Bromomethane
ND
ug/kg
11.4
1
02/15/17 18:08
74-83-9
2-Butanone (MEK)
ND
ug/kg
114
1
02/15/17 18:08
78-93-3
n-Butylbenzene
ND
ug/kg
5.7
1
02/15/17 18:08
104-51-8
sec-Butylbenzene
ND
ug/kg
5.7
1
02/15/17 18:08
135-98-8
tert-Butyl benzene
ND
ug/kg
5.7
1
02/15/17 18:08
98-06-6
Carbon tetrachloride
ND
ug/kg
5.7
1
02/15/17 18:08
56-23-5
Chlorobenzene
ND
ug/kg
5.7
1
02/15/17 18:08
108-90-7
Chloroethane
ND
ug/kg
11.4
1
02/15/17 18:08
75-00-3
Chloroform
ND
ug/kg
5.7
1
02/15/17 18:08
67-66-3
Chloromethane
ND
ug/kg
11.4
1
02/15/17 18:08
74-87-3
2-Chlorotoluene
ND
ug/kg
5.7
1
02/15/17 18:08
95-49-8
4-Chlorotoluene
ND
ug/kg
5.7
1
02/15/17 18:08
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.7
1
02/15/17 18:08
96-12-8
Dibromochloromethane
ND
ug/kg
5.7
1
02/15/17 18:08
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.7
1
02/15/17 18:08
106-93-4
Dibromomethane
ND
ug/kg
5.7
1
02/15/17 18:08
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.7
1
02/15/17 18:08
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.7
1
02/15/17 18:08
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.7
1
02/15/17 18:08
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.4
1
02/15/17 18:08
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.7
1
02/15/17 18:08
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.7
1
02/15/17 18:08
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.7
1
02/15/17 18:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.7
1
02/15/17 18:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.7
1
02/15/17 18:08
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.7
1
02/15/17 18:08
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.7
1
02/15/17 18:08
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.7
1
02/15/17 18:08
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.7
1
02/15/17 18:08
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.7
1
02/15/17 18:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.7
1
02/15/17 18:08
10061-02-6
Diisopropyl ether
ND
ug/kg
5.7
1
02/15/17 18:08
108-20-3
Ethylbenzene
ND
ug/kg
5.7
1
02/15/17 18:08
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.7
1
02/15/17 18:08
87-68-3
2-Hexanone
ND
ug/kg
56.8
1
02/15/17 18:08
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.7
1
02/15/17 18:08
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.7
1
02/15/17 18:08
99-87-6
Methylene Chloride
ND
ug/kg
22.7
1
02/15/17 18:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
56.8
1
02/15/17 18:08
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.7
1
02/15/17 18:08
1634-04-4
Naphthalene
ND
ug/kg
5.7
1
02/15/17 18:08
91-20-3
n-Propylbenzene
ND
ug/kg
5.7
1
02/15/17 18:08
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 53

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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-5 Lab ID: 92329914005 Collected: 02/13/17 14:15 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
ug/kg
5.7
1
02/15/1718:08
100-42-5
ND
ug/kg
5.7
1
02/15/1718:08
630-20-6
ND
ug/kg
5.7
1
02/15/1718:08
79-34-5
ND
ug/kg
5.7
1
02/15/1718:08
127-18-4
ND
ug/kg
5.7
1
02/15/1718:08
108-88-3
ND
ug/kg
5.7
1
02/15/1718:08
87-61-6
ND
ug/kg
5.7
1
02/15/1718:08
120-82-1
ND
ug/kg
5.7
1
02/15/1718:08
71-55-6
ND
ug/kg
5.7
1
02/15/1718:08
79-00-5
ND
ug/kg
5.7
1
02/15/1718:08
79-01-6
ND
ug/kg
5.7
1
02/15/1718:08
75-69-4
ND
ug/kg
5.7
1
02/15/1718:08
96-18-4
ND
ug/kg
5.7
1
02/15/1718:08
95-63-6
ND
ug/kg
5.7
1
02/15/1718:08
108-67-8
ND
ug/kg
56.8
1
02/15/1718:08
108-05-4
ND
ug/kg
11.4
1
02/15/1718:08
75-01-4
ND
ug/kg
11.4
1
02/15/1718:08
1330-20-7
ND
ug/kg
11.4
1
02/15/1718:08
179601-23-1
ND
ug/kg
5.7
1
02/15/1718:08
95-47-6
105
%
70-130
1
02/15/1718:08
2037-26-5
103
%
70-130
1
02/15/1718:08
460-00-4
77
%
70-132
1
02/15/1718:08
17060-07-0
Analytical Method: ASTM D2974-87
15.1 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/15/17 07:08
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 53

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Pace Analytical Services, LLC
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[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-6 Lab ID: 92329914006 Collected: 02/13/17 14:20 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
2.0
mg/kg
0.86
1
02/15/17 23:00
02/16/17 11:51
7440-38-2
Barium
66.6
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:51
7440-39-3
Cadmium
ND
mg/kg
0.086
1
02/15/17 23:00
02/16/17 11:51
7440-43-9
Chromium
9.6
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:51
7440-47-3
Lead
9.0
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:51
7439-92-1
Selenium
ND
mg/kg
0.86
1
02/15/17 23:00
02/16/17 11:51
7782-49-2
Silver
ND
mg/kg
0.43
1
02/15/17 23:00
02/16/17 11:51
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
ND
mg/kg
0.0062
1
02/16/17 05:55
02/16/17 10:33
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
83-32-9
Acenaphthylene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
208-96-8
Aniline
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
62-53-3
Anthracene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
120-12-7
Benzo(a)anthracene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
56-55-3
Benzo(a)pyrene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
207-08-9
Benzoic Acid
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
65-85-0
Benzyl alcohol
ND
ug/kg
770
1
02/15/17 08:30
02/15/17 18:43
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
101-55-3
Butylbenzylphthalate
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
770
1
02/15/17 08:30
02/15/17 18:43
59-50-7
4-Chloroaniline
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
111-44-4
2-Chloronaphthalene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
91-58-7
2-Chlorophenol
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
7005-72-3
Chrysene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
53-70-3
Dibenzofuran
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
91-94-1
2,4-Dichlorophenol
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
120-83-2
Diethylphthalate
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
84-66-2
2,4-Dimethylphenol
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
105-67-9
Dimethylphthalate
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
131-11-3
Di-n-butylphthalate
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
770
1
02/15/17 08:30
02/15/17 18:43
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 53

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-6 Lab ID: 92329914006 Collected: 02/13/17 14:20 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
606-20-2
Di-n-octylphthalate
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
117-81-7
Fluoranthene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
206-44-0
Fluorene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
87-68-3
Hexachlorobenzene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
77-47-4
Hexachloroethane
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
193-39-5
Isophorone
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
78-59-1
1-Methylnaphthalene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
90-12-0
2-Methylnaphthalene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
Naphthalene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
91-20-3
2-Nitroaniline
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
88-74-4
3-Nitroaniline
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
99-09-2
4-Nitroaniline
ND
ug/kg
770
1
02/15/17 08:30
02/15/17 18:43
100-01-6
Nitrobenzene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
98-95-3
2-Nitrophenol
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
88-75-5
4-Nitrophenol
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
108-60-1
Pentachlorophenol
ND
ug/kg
1930
1
02/15/17 08:30
02/15/17 18:43
87-86-5
Phenanthrene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
85-01-8
Phenol
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
Pyrene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
385
1
02/15/17 08:30
02/15/17 18:43
88-06-2
Surrogates
Nitrobenzene-d5 (S)
33
%
23-110
1
02/15/17 08:30
02/15/17 18:43
4165-60-0
2-Fluorobiphenyl (S)
49
%
30-110
1
02/15/17 08:30
02/15/17 18:43
321-60-8
Terphenyl-dl4 (S)
76
%
28-110
1
02/15/17 08:30
02/15/17 18:43
1718-51-0
Phenol-d6 (S)
51
%
22-110
1
02/15/17 08:30
02/15/17 18:43
13127-88-3
2-Fluorophenol (S)
51
%
13-110
1
02/15/17 08:30
02/15/17 18:43
367-12-4
2,4,6-Tribromophenol (S)
72
%
27-110
1
02/15/17 08:30
02/15/17 18:43
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Acetone
ND
ug/kg
122
1
02/15/1718:28
67-64-1
Benzene
ND
ug/kg
6.1
1
02/15/1718:28
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 53

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-6 Lab ID: 92329914006 Collected: 02/13/17 14:20 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
ug/kg
6.1
1
02/15/17 18:28
108-86-1
Bromochloromethane
ND
ug/kg
6.1
1
02/15/17 18:28
74-97-5
Bromodichloromethane
ND
ug/kg
6.1
1
02/15/17 18:28
75-27-4
Bromoform
ND
ug/kg
6.1
1
02/15/17 18:28
75-25-2
Bromomethane
ND
ug/kg
12.2
1
02/15/17 18:28
74-83-9
2-Butanone (MEK)
ND
ug/kg
122
1
02/15/17 18:28
78-93-3
n-Butylbenzene
ND
ug/kg
6.1
1
02/15/17 18:28
104-51-8
sec-Butylbenzene
ND
ug/kg
6.1
1
02/15/17 18:28
135-98-8
tert-Butyl benzene
ND
ug/kg
6.1
1
02/15/17 18:28
98-06-6
Carbon tetrachloride
ND
ug/kg
6.1
1
02/15/17 18:28
56-23-5
Chlorobenzene
ND
ug/kg
6.1
1
02/15/17 18:28
108-90-7
Chloroethane
ND
ug/kg
12.2
1
02/15/17 18:28
75-00-3
Chloroform
ND
ug/kg
6.1
1
02/15/17 18:28
67-66-3
Chloromethane
ND
ug/kg
12.2
1
02/15/17 18:28
74-87-3
2-Chlorotoluene
ND
ug/kg
6.1
1
02/15/17 18:28
95-49-8
4-Chlorotoluene
ND
ug/kg
6.1
1
02/15/17 18:28
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.1
1
02/15/17 18:28
96-12-8
Dibromochloromethane
ND
ug/kg
6.1
1
02/15/17 18:28
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.1
1
02/15/17 18:28
106-93-4
Dibromomethane
ND
ug/kg
6.1
1
02/15/17 18:28
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.1
1
02/15/17 18:28
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.1
1
02/15/17 18:28
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.1
1
02/15/17 18:28
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.2
1
02/15/17 18:28
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.1
1
02/15/17 18:28
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.1
1
02/15/17 18:28
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.1
1
02/15/17 18:28
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.1
1
02/15/17 18:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.1
1
02/15/17 18:28
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.1
1
02/15/17 18:28
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.1
1
02/15/17 18:28
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.1
1
02/15/17 18:28
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.1
1
02/15/17 18:28
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.1
1
02/15/17 18:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.1
1
02/15/17 18:28
10061-02-6
Diisopropyl ether
ND
ug/kg
6.1
1
02/15/17 18:28
108-20-3
Ethylbenzene
ND
ug/kg
6.1
1
02/15/17 18:28
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.1
1
02/15/17 18:28
87-68-3
2-Hexanone
ND
ug/kg
60.9
1
02/15/17 18:28
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
6.1
1
02/15/17 18:28
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.1
1
02/15/17 18:28
99-87-6
Methylene Chloride
ND
ug/kg
24.4
1
02/15/17 18:28
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
60.9
1
02/15/17 18:28
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.1
1
02/15/17 18:28
1634-04-4
Naphthalene
ND
ug/kg
6.1
1
02/15/17 18:28
91-20-3
n-Propylbenzene
ND
ug/kg
6.1
1
02/15/17 18:28
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
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ANALYTICAL RESULTS
Project: SOIL SAMPLING
Pace Project No.: 92329914
Sample: B-6 Lab ID: 92329914006 Collected: 02/13/17 14:20 Received: 02/13/17 15:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
ug/kg
6.1
1
02/15/1718:28
100-42-5
ND
ug/kg
6.1
1
02/15/1718:28
630-20-6
ND
ug/kg
6.1
1
02/15/1718:28
79-34-5
ND
ug/kg
6.1
1
02/15/1718:28
127-18-4
ND
ug/kg
6.1
1
02/15/1718:28
108-88-3
ND
ug/kg
6.1
1
02/15/1718:28
87-61-6
ND
ug/kg
6.1
1
02/15/1718:28
120-82-1
ND
ug/kg
6.1
1
02/15/1718:28
71-55-6
ND
ug/kg
6.1
1
02/15/1718:28
79-00-5
ND
ug/kg
6.1
1
02/15/1718:28
79-01-6
ND
ug/kg
6.1
1
02/15/1718:28
75-69-4
ND
ug/kg
6.1
1
02/15/1718:28
96-18-4
ND
ug/kg
6.1
1
02/15/1718:28
95-63-6
ND
ug/kg
6.1
1
02/15/1718:28
108-67-8
ND
ug/kg
60.9
1
02/15/1718:28
108-05-4
ND
ug/kg
12.2
1
02/15/1718:28
75-01-4
ND
ug/kg
12.2
1
02/15/1718:28
1330-20-7
ND
ug/kg
12.2
1
02/15/1718:28
179601-23-1
ND
ug/kg
6.1
1
02/15/1718:28
95-47-6
104
%
70-130
1
02/15/1718:28
2037-26-5
99
%
70-130
1
02/15/1718:28
460-00-4
85
%
70-132
1
02/15/1718:28
17060-07-0
Analytical Method: ASTM D2974-87
14.3 % 0.10 1
REPORT OF LABORATORY ANALYSIS
02/15/17 07:08
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QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
QC Batch: 348452
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 92329914001, 92329914002,
92329914003, 92329914004, 92329914005, 92329914006
METHOD BLANK: 1933355
Matrix: Solid
Associated Lab Samples: 92329914001, 92329914002,
92329914003, 92329914004, 92329914005, 92329914006
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mercury mg/kg
ND 0.0060 02/16/1710:02
LABORATORY CONTROL SAMPLE: 1933356
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury mg/kg
.083 0.084 101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1933357 1933358
MS MSD
92329087001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.067
.18 .17 0.27 0.19 109 72 75-125 34 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
QC Batch: 348310 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92329914001, 92329914002, 92329914003, 92329914004, 92329914005, 92329914006
METHOD BLANK: 1932372
Matrix:
Solid
Associated Lab Samples:
92329914001, 92329914002,
92329914003, 92329914004, 92329914005,
92329914006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
02/16/1711:11
Barium
mg/kg
ND
0.50
02/16/1711:11
Cadmium
mg/kg
ND
0.10
02/16/1711:11
Chromium
mg/kg
ND
0.50
02/16/1711:11
Lead
mg/kg
ND
0.50
02/16/1711:11
Selenium
mg/kg
ND
1.0
02/16/1711:11
Silver
mg/kg
ND
0.50
02/16/1711:11
LABORATORY CONTROL SAMPLE: 1932373
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
50.6
101
80-120
Barium
mg/kg
50
44.2
88
80-120
Cadmium
mg/kg
50
49.3
99
80-120
Chromium
mg/kg
50
46.5
93
80-120
Lead
mg/kg
50
50.3
101
80-120
Selenium
mg/kg
50
51.5
103
80-120
Silver
mg/kg
25
24.7
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1932374 1932375
MS
MSD
92329914001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
7.1
51.6
45.6
45.1
38.9
74
70
75-125
15 M1
Barium
mg/kg
22.7
51.6
45.6
69.8
62.4
91
87
75-125
11
Cadmium
mg/kg
ND
51.6
45.6
46.6
39.6
90
87
75-125
16
Chromium
mg/kg
6.3
51.6
45.6
50.7
43.9
86
82
75-125
14
Lead
mg/kg
10.4
51.6
45.6
56.0
49.0
88
85
75-125
13
Selenium
mg/kg
3.4
51.6
45.6
43.1
35.4
77
70
75-125
20 M1
Silver
mg/kg
ND
25.8
22.8
23.9
20.5
92
89
75-125
15
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 53

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QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
QC Batch: 348335 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92329914001, 92329914002, 92329914004, 92329914005, 92329914006
METHOD BLANK: 1932522 Matrix: Solid
Associated Lab Samples: 92329914001, 92329914002, 92329914004, 92329914005, 92329914006
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
4.8
02/15/17 12:01
1,1,1-Trichloroethane
ug/kg
ND
4.8
02/15/17 12:01
1,1,2,2-Tetrachloroethane
ug/kg
ND
4.8
02/15/17 12:01
1,1,2-Trichloroethane
ug/kg
ND
4.8
02/15/17 12:01
1,1-Dichloroethane
ug/kg
ND
4.8
02/15/17 12:01
1,1-Dichloroethene
ug/kg
ND
4.8
02/15/17 12:01
1,1-Dichloropropene
ug/kg
ND
4.8
02/15/17 12:01
1,2,3-Trichlorobenzene
ug/kg
ND
4.8
02/15/17 12:01
1,2,3-Trichloropropane
ug/kg
ND
4.8
02/15/17 12:01
1,2,4-Trichlorobenzene
ug/kg
ND
4.8
02/15/17 12:01
1,2,4-Trimethylbenzene
ug/kg
ND
4.8
02/15/17 12:01
1,2-Dibromo-3-chloropropane
ug/kg
ND
4.8
02/15/17 12:01
1,2-Dibromoethane (EDB)
ug/kg
ND
4.8
02/15/17 12:01
1,2-Dichlorobenzene
ug/kg
ND
4.8
02/15/17 12:01
1,2-Dichloroethane
ug/kg
ND
4.8
02/15/17 12:01
1,2-Dichloropropane
ug/kg
ND
4.8
02/15/17 12:01
1,3,5-Trimethylbenzene
ug/kg
ND
4.8
02/15/17 12:01
1,3-Dichlorobenzene
ug/kg
ND
4.8
02/15/17 12:01
1,3-Dichloropropane
ug/kg
ND
4.8
02/15/17 12:01
1,4-Dichlorobenzene
ug/kg
ND
4.8
02/15/17 12:01
2,2-Dichloropropane
ug/kg
ND
4.8
02/15/17 12:01
2-Butanone (MEK)
ug/kg
ND
96.0
02/15/17 12:01
2-Chlorotoluene
ug/kg
ND
4.8
02/15/17 12:01
2-Hexanone
ug/kg
ND
48.0
02/15/17 12:01
4-Chlorotoluene
ug/kg
ND
4.8
02/15/17 12:01
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
48.0
02/15/17 12:01
Acetone
ug/kg
ND
96.0
02/15/17 12:01
Benzene
ug/kg
ND
4.8
02/15/17 12:01
Bromobenzene
ug/kg
ND
4.8
02/15/17 12:01
Bromochloromethane
ug/kg
ND
4.8
02/15/17 12:01
Bromodichloromethane
ug/kg
ND
4.8
02/15/17 12:01
Bromoform
ug/kg
ND
4.8
02/15/17 12:01
Bromomethane
ug/kg
ND
9.6
02/15/17 12:01
Carbon tetrachloride
ug/kg
ND
4.8
02/15/17 12:01
Chlorobenzene
ug/kg
ND
4.8
02/15/17 12:01
Chloroethane
ug/kg
ND
9.6
02/15/17 12:01
Chloroform
ug/kg
ND
4.8
02/15/17 12:01
Chloromethane
ug/kg
ND
9.6
02/15/17 12:01
cis-1,2-Dichloroethene
ug/kg
ND
4.8
02/15/17 12:01
cis-1,3-Dichloropropene
ug/kg
ND
4.8
02/15/17 12:01
Dibromochloromethane
ug/kg
ND
4.8
02/15/17 12:01
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
METHOD BLANK: 1932522 Matrix: Solid
Associated Lab Samples: 92329914001, 92329914002, 92329914004, 92329914005, 92329914006
Blank Reporting
Parameter Units Result Limit Analyzed
Dibromomethane
ug/kg
ND
4.8
02/15/17 12:01
Dichlorodifluoromethane
ug/kg
ND
9.6
02/15/17 12:01
Diisopropyl ether
ug/kg
ND
4.8
02/15/17 12:01
Ethylbenzene
ug/kg
ND
4.8
02/15/17 12:01
Hexachloro-1,3-butadiene
ug/kg
ND
4.8
02/15/17 12:01
Isopropylbenzene (Cumene)
ug/kg
ND
4.8
02/15/17 12:01
m&p-Xylene
ug/kg
ND
9.6
02/15/17 12:01
Methyl-tert-butyl ether
ug/kg
ND
4.8
02/15/17 12:01
Methylene Chloride
ug/kg
ND
19.2
02/15/17 12:01
n-Butylbenzene
ug/kg
ND
4.8
02/15/17 12:01
n-Propylbenzene
ug/kg
ND
4.8
02/15/17 12:01
Naphthalene
ug/kg
ND
4.8
02/15/17 12:01
o-Xylene
ug/kg
ND
4.8
02/15/17 12:01
p-Isopropyltoluene
ug/kg
ND
4.8
02/15/17 12:01
sec-Butylbenzene
ug/kg
ND
4.8
02/15/17 12:01
Styrene
ug/kg
ND
4.8
02/15/17 12:01
tert-Butyl benzene
ug/kg
ND
4.8
02/15/17 12:01
Tetrachloroethene
ug/kg
ND
4.8
02/15/17 12:01
Toluene
ug/kg
ND
4.8
02/15/17 12:01
trans-1,2-Dichloroethene
ug/kg
ND
4.8
02/15/17 12:01
trans- 1,3-Dichloropropene
ug/kg
ND
4.8
02/15/17 12:01
Trichloroethene
ug/kg
ND
4.8
02/15/17 12:01
Trichlorofluoromethane
ug/kg
ND
4.8
02/15/17 12:01
Vinyl acetate
ug/kg
ND
48.0
02/15/17 12:01
Vinyl chloride
ug/kg
ND
9.6
02/15/17 12:01
Xylene (Total)
ug/kg
ND
9.6
02/15/17 12:01
1,2-Dichloroethane-d4 (S)
%
85
70-132
02/15/17 12:01
4-Bromofluorobenzene (S)
%
101
70-130
02/15/17 12:01
Toluene-d8 (S)
%
107
70-130
02/15/17 12:01
Qualifiers
LABORATORY CONTROL SAMPLE:
1932523
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
58.5
50.0
85
74-137
1,1,1-Trichloroethane
ug/kg
58.5
46.9
80
67-140
1,1,2,2-Tetrachloroethane
ug/kg
58.5
44.9
77
72-141
1,1,2-Trichloroethane
ug/kg
58.5
49.4
84
78-138
1,1-Dichloroethane
ug/kg
58.5
52.3
89
69-134
1,1-Dichloroethene
ug/kg
58.5
50.1
86
67-138
1,1-Dichloropropene
ug/kg
58.5
48.7
83
69-139
1,2,3-Trichlorobenzene
ug/kg
58.5
48.4
83
70-146
1,2,3-Trichloropropane
ug/kg
58.5
46.5
79
69-144
1,2,4-Trichlorobenzene
ug/kg
58.5
48.4
83
68-148
1,2,4-Trimethylbenzene
ug/kg
58.5
47.6
81
74-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
LABORATORY CONTROL SAMPLE:
Parameter
1932523
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/kg
58.5
43.2
74
65-140
1,2-Dibromoethane (EDB)
ug/kg
58.5
47.0
80
77-135
1,2-Dichlorobenzene
ug/kg
58.5
49.5
84
77-141
1,2-Dichloroethane
ug/kg
58.5
47.2
81
65-137
1,2-Dichloropropane
ug/kg
58.5
49.2
84
72-136
1,3,5-Trimethylbenzene
ug/kg
58.5
47.1
80
76-133
1,3-Dichlorobenzene
ug/kg
58.5
49.0
84
74-138
1,3-Dichloropropane
ug/kg
58.5
49.6
85
71-139
1,4-Dichlorobenzene
ug/kg
58.5
49.8
85
76-138
2,2-Dichloropropane
ug/kg
58.5
43.9
75
68-137
2-Butanone (MEK)
ug/kg
117
83J
71
58-147
2-Chlorotoluene
ug/kg
58.5
49.0
84
73-139
2-Hexanone
ug/kg
117
76.2
65
62-145
4-Chlorotoluene
ug/kg
58.5
48.4
83
76-141
4-Methyl-2-pentanone (MIBK)
ug/kg
117
86.5
74
64-149
Acetone
ug/kg
117
91.3J
78
53-153
Benzene
ug/kg
58.5
50.1
86
73-135
Bromobenzene
ug/kg
58.5
49.1
84
75-133
Bromochloromethane
ug/kg
58.5
48.6
83
73-134
Bromodichloromethane
ug/kg
58.5
50.4
86
71-135
Bromoform
ug/kg
58.5
45.1
77
66-141
Bromomethane
ug/kg
58.5
53.4
91
53-160
Carbon tetrachloride
ug/kg
58.5
45.1
77
60-145
Chlorobenzene
ug/kg
58.5
50.2
86
78-130
Chloroethane
ug/kg
58.5
62.3
106
64-149
Chloroform
ug/kg
58.5
48.6
83
70-134
Chloromethane
ug/kg
58.5
55.1
94
52-150
cis-1,2-Dichloroethene
ug/kg
58.5
47.4
81
70-133
cis-1,3-Dichloropropene
ug/kg
58.5
51.1
87
68-134
Dibromochloromethane
ug/kg
58.5
51.0
87
71-138
Dibromomethane
ug/kg
58.5
46.6
80
74-130
Dichlorodifluoromethane
ug/kg
58.5
42.9
73
40-160
Diisopropyl ether
ug/kg
58.5
56.0
96
69-141
Ethylbenzene
ug/kg
58.5
47.8
82
75-133
Hexachloro-1,3-butadiene
ug/kg
58.5
47.4
81
68-143
Isopropylbenzene (Cumene)
ug/kg
58.5
48.1
82
76-143
m&p-Xylene
ug/kg
117
96.7
83
75-136
Methyl-tert-butyl ether
ug/kg
58.5
53.7
92
68-144
Methylene Chloride
ug/kg
58.5
49.4
84
45-154
n-Butylbenzene
ug/kg
58.5
45.7
78
72-137
n-Propylbenzene
ug/kg
58.5
48.1
82
76-136
Naphthalene
ug/kg
58.5
46.8
80
68-151
o-Xylene
ug/kg
58.5
49.4
84
76-141
p-Isopropyltoluene
ug/kg
58.5
45.2
77
76-140
sec-Butylbenzene
ug/kg
58.5
47.8
82
79-139
Styrene
ug/kg
58.5
49.7
85
79-137
tert-Butyl benzene
ug/kg
58.5
43.7
75
74-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
LABORATORY CONTROL SAMPLE:
1932523
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Tetrachloroethene
ug/kg
58.5
44.3
76
71-138
Toluene
ug/kg
58.5
48.7
83
74-131
trans-1,2-Dichloroethene
ug/kg
58.5
53.7
92
67-135
trans- 1,3-Dichloropropene
ug/kg
58.5
49.7
85
65-146
Trichloroethene
ug/kg
58.5
51.2
87
67-135
Trichlorofluoromethane
ug/kg
58.5
59.1
101
59-144
Vinyl acetate
ug/kg
117
72.7
62
40-160
Vinyl chloride
ug/kg
58.5
46.3
79
56-141
Xylene (Total)
ug/kg
176
146
83
76-137
1,2-Dichloroethane-d4 (S)
%
96
70-132
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
1933446
92329760001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
22.3
17.3
77
70-130
1,1,1-Trichloroethane
ug/kg
ND
22.3
19.4
87
70-130
1,1,2,2-Tetrachloroethane
ug/kg
ND
22.3
18.2
82
70-130
1,1,2-Trichloroethane
ug/kg
ND
22.3
19.0
85
70-130
1,1-Dichloroethane
ug/kg
ND
22.3
22.0
99
70-130
1,1-Dichloroethene
ug/kg
ND
22.3
22.8
102
49-180
1,1-Dichloropropene
ug/kg
ND
22.3
18.7
84
70-130
1,2,3-Trichlorobenzene
ug/kg
ND
22.3
8.0
36
70-130 M1
1,2,3-Trichloropropane
ug/kg
ND
22.3
19.3
86
70-130
1,2,4-Trichlorobenzene
ug/kg
ND
22.3
7.4
33
70-130 M1
1,2,4-Trimethylbenzene
ug/kg
ND
22.3
15.2
68
70-130 M1
1,2-Dibromo-3-chloropropane
ug/kg
ND
22.3
16.0
71
70-130
1,2-Dibromoethane (EDB)
ug/kg
ND
22.3
17.8
80
70-130
1,2-Dichlorobenzene
ug/kg
ND
22.3
15.7
70
70-130
1,2-Dichloroethane
ug/kg
ND
22.3
19.9
89
70-130
1,2-Dichloropropane
ug/kg
ND
22.3
19.8
89
70-130
1,3,5-Trimethylbenzene
ug/kg
ND
22.3
14.4
64
70-130 M1
1,3-Dichlorobenzene
ug/kg
ND
22.3
14.3
64
70-130 M1
1,3-Dichloropropane
ug/kg
ND
22.3
18.8
84
70-130
1,4-Dichlorobenzene
ug/kg
ND
22.3
14.6
65
70-130 M1
2,2-Dichloropropane
ug/kg
ND
22.3
19.0
85
70-130
2-Butanone (MEK)
ug/kg
ND
44.6
42J
94
70-130
2-Chlorotoluene
ug/kg
ND
22.3
16.9
76
70-130
2-Hexanone
ug/kg
ND
44.6
29.9J
67
70-130 M1
4-Chlorotoluene
ug/kg
ND
22.3
16.3
73
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
44.6
34.6J
78
70-130
Acetone
ug/kg
ND
44.6
79.7J
119
70-130
Benzene
ug/kg
ND
22.3
20.3
91
50-166
Bromobenzene
ug/kg
ND
22.3
18.3
82
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 53

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
MATRIX SPIKE SAMPLE:
1933446
92329760001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/kg
ND
22.3
19.6
88
70-130
Bromodichloromethane
ug/kg
ND
22.3
19.8
89
70-130
Bromoform
ug/kg
ND
22.3
15.4
69
70-130 M1
Bromomethane
ug/kg
ND
22.3
23.0
103
70-130
Carbon tetrachloride
ug/kg
ND
22.3
17.7
79
70-130
Chlorobenzene
ug/kg
ND
22.3
17.9
80
43-169
Chloroethane
ug/kg
ND
22.3
27.5
123
70-130
Chloroform
ug/kg
ND
22.3
19.4
87
70-130
Chloromethane
ug/kg
ND
22.3
28.3
127
70-130
cis-1,2-Dichloroethene
ug/kg
ND
22.3
19.6
88
70-130
cis-1,3-Dichloropropene
ug/kg
ND
22.3
17.9
80
70-130
Dibromochloromethane
ug/kg
ND
22.3
17.3
78
70-130
Dibromomethane
ug/kg
ND
22.3
18.7
84
70-130
Dichlorodifluoromethane
ug/kg
ND
22.3
24.5
110
70-130
Diisopropyl ether
ug/kg
ND
22.3
20.7
93
70-130
Ethylbenzene
ug/kg
ND
22.3
18.3
82
70-130
Hexachloro-1,3-butadiene
ug/kg
ND
22.3
ND
9
70-130 M1
Isopropylbenzene (Cumene)
ug/kg
ND
22.3
16.1
72
70-130
m&p-Xylene
ug/kg
ND
44.6
36.3
81
70-130
Methyl-tert-butyl ether
ug/kg
ND
22.3
20.2
91
70-130
Methylene Chloride
ug/kg
ND
22.3
23.8
107
70-130
n-Butylbenzene
ug/kg
ND
22.3
6.8
30
70-130 M1
n-Propylbenzene
ug/kg
ND
22.3
15.2
68
70-130 M1
Naphthalene
ug/kg
ND
22.3
13.8
62
70-130 M1
o-Xylene
ug/kg
ND
22.3
18.8
84
70-130
p-Isopropyltoluene
ug/kg
ND
22.3
9.6
43
70-130 M1
sec-Butylbenzene
ug/kg
ND
22.3
10.2
46
70-130 M1
Styrene
ug/kg
ND
22.3
17.7
79
70-130
tert-Butyl benzene
ug/kg
ND
22.3
12.0
54
70-130 M1
Tetrachloroethene
ug/kg
ND
22.3
16.1
72
70-130
Toluene
ug/kg
ND
22.3
19.3
85
52-163
trans-1,2-Dichloroethene
ug/kg
ND
22.3
20.6
92
70-130
trans- 1,3-Dichloropropene
ug/kg
ND
22.3
16.2
73
70-130
Trichloroethene
ug/kg
ND
22.3
18.1
81
49-167
Trichlorofluoromethane
ug/kg
ND
22.3
26.0
117
70-130
Vinyl acetate
ug/kg
ND
44.6
22.3J
50
70-130 M1
Vinyl chloride
ug/kg
ND
22.3
21.4
96
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-132
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 1933445
35295057001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane ug/kg 2.2U ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 53

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
SAMPLE DUPLICATE: 1933445
Parameter
Units
35295057001
Result
Dup
Result
1,1,1-Trichloroethane
ug/kg
1.8U
ND
1,1,2,2-Tetrachloroethane
ug/kg
2.OU
ND
1,1,2-Trichloroethane
ug/kg
2.2U
ND
1,1-Dichloroethane
ug/kg
1.5U
ND
1,1-Dichloroethene
ug/kg
1.8U
ND
1,1-Dichloropropene
ug/kg
1.5U
ND
1,2,3-Trichlorobenzene
ug/kg
2.3U
ND
1,2,3-Trichloropropane
ug/kg
1.6U
ND
1,2,4-Trichlorobenzene
ug/kg
1.6U
ND
1,2,4-Trimethylbenzene
ug/kg
2.8J
ND
1,2-Dibromo-3-chloropropane
ug/kg
3.7U
ND
1,2-Dibromoethane (EDB)
ug/kg
1.8U
ND
1,2-Dichlorobenzene
ug/kg
2.OU
ND
1,2-Dichloroethane
ug/kg
2.3U
ND
1,2-Dichloropropane
ug/kg
1.7U
ND
1,3,5-Trimethylbenzene
ug/kg
1.8U
ND
1,3-Dichlorobenzene
ug/kg
2.1U
ND
1,3-Dichloropropane
ug/kg
2.OU
ND
1,4-Dichlorobenzene
ug/kg
1.7U
ND
2,2-Dichloropropane
ug/kg
1.7U
ND
2-Butanone (MEK)
ug/kg
3.OU
ND
2-Chlorotoluene
ug/kg
1.7U
ND
2-Hexanone
ug/kg
4.OU
ND
4-Chlorotoluene
ug/kg
1.8U
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
3.8U
ND
Acetone
ug/kg
66.5J
22.2J
Benzene
ug/kg
1.6U
ND
Bromobenzene
ug/kg
2.1U
ND
Bromochloromethane
ug/kg
1.7U
ND
Bromodichloromethane
ug/kg
2.OU
ND
Bromoform
ug/kg
2AU
ND
Bromomethane
ug/kg
2.6U
ND
Carbon tetrachloride
ug/kg
2.7U
ND
Chlorobenzene
ug/kg
2.OU
ND
Chloroethane
ug/kg
2.5U
ND
Chloroform
ug/kg
1.6U
ND
Chloromethane
ug/kg
2.5U
ND
cis-1,2-Dichloroethene
ug/kg
1.4U
ND
cis-1,3-Dichloropropene
ug/kg
1.8U
ND
Dibromochloromethane
ug/kg
1.8U
ND
Dibromomethane
ug/kg
2.6U
ND
Dichlorodifluoromethane
ug/kg
3.7U
ND
Diisopropyl ether
ug/kg
1.7U
ND
Ethylbenzene
ug/kg
1.8U
ND
Hexachloro-1,3-butadiene
ug/kg
2.1U
ND
Isopropylbenzene (Cumene)
ug/kg
2.OU
ND
m&p-Xylene
ug/kg
3.7U
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 53

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
SAMPLE DUPLICATE: 1933445
Parameter
Units
35295057001
Result
Dup
Result
Methyl-tert-butyl ether
ug/kg
1.5U
ND
Methylene Chloride
ug/kg
3.1U
ND
n-Butylbenzene
ug/kg
1.8U
ND
n-Propylbenzene
ug/kg
1.7U
ND
Naphthalene
ug/kg
2.6J
ND
o-Xylene
ug/kg
2.OU
ND
p-Isopropyltoluene
ug/kg
1.7U
ND
sec-Butylbenzene
ug/kg
1.6U
ND
Styrene
ug/kg
1.8U
ND
tert-Butyl benzene
ug/kg
2.1U
ND
Tetrachloroethene
ug/kg
1.7U
ND
Toluene
ug/kg
3AJ
ND
trans-1,2-Dichloroethene
ug/kg
2.OU
ND
trans- 1,3-Dichloropropene
ug/kg
1.5U
ND
Trichloroethene
ug/kg
2.2U
ND
Trichlorofluoromethane
ug/kg
2.3U
ND
Vinyl acetate
ug/kg
9.OU
ND
Vinyl chloride
ug/kg
1.8U
ND
Xylene (Total)
ug/kg
3.7U
ND
1,2-Dichloroethane-d4 (S)
%
133
83
4-Bromofluorobenzene (S)
%
103
94
Toluene-d8 (S)
%
120
103
RPD Qualifiers
48
10
17
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 53

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
QC Batch: 348542 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92329914003
METHOD BLANK: 1933726
Associated Lab Samples: 92329914003
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.7
02/16/17 11:32
1,1,1-Trichloroethane
ug/kg
ND
5.7
02/16/17 11:32
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.7
02/16/17 11:32
1,1,2-Trichloroethane
ug/kg
ND
5.7
02/16/17 11:32
1,1-Dichloroethane
ug/kg
ND
5.7
02/16/17 11:32
1,1-Dichloroethene
ug/kg
ND
5.7
02/16/17 11:32
1,1-Dichloropropene
ug/kg
ND
5.7
02/16/17 11:32
1,2,3-Trichlorobenzene
ug/kg
ND
5.7
02/16/17 11:32
1,2,3-Trichloropropane
ug/kg
ND
5.7
02/16/17 11:32
1,2,4-Trichlorobenzene
ug/kg
ND
5.7
02/16/17 11:32
1,2,4-Trimethylbenzene
ug/kg
ND
5.7
02/16/17 11:32
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.7
02/16/17 11:32
1,2-Dibromoethane (EDB)
ug/kg
ND
5.7
02/16/17 11:32
1,2-Dichlorobenzene
ug/kg
ND
5.7
02/16/17 11:32
1,2-Dichloroethane
ug/kg
ND
5.7
02/16/17 11:32
1,2-Dichloropropane
ug/kg
ND
5.7
02/16/17 11:32
1,3,5-Trimethylbenzene
ug/kg
ND
5.7
02/16/17 11:32
1,3-Dichlorobenzene
ug/kg
ND
5.7
02/16/17 11:32
1,3-Dichloropropane
ug/kg
ND
5.7
02/16/17 11:32
1,4-Dichlorobenzene
ug/kg
ND
5.7
02/16/17 11:32
2,2-Dichloropropane
ug/kg
ND
5.7
02/16/17 11:32
2-Butanone (MEK)
ug/kg
ND
114
02/16/17 11:32
2-Chlorotoluene
ug/kg
ND
5.7
02/16/17 11:32
2-Hexanone
ug/kg
ND
57.2
02/16/17 11:32
4-Chlorotoluene
ug/kg
ND
5.7
02/16/17 11:32
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
57.2
02/16/17 11:32
Acetone
ug/kg
ND
114
02/16/17 11:32
Benzene
ug/kg
ND
5.7
02/16/17 11:32
Bromobenzene
ug/kg
ND
5.7
02/16/17 11:32
Bromochloromethane
ug/kg
ND
5.7
02/16/17 11:32
Bromodichloromethane
ug/kg
ND
5.7
02/16/17 11:32
Bromoform
ug/kg
ND
5.7
02/16/17 11:32
Bromomethane
ug/kg
ND
11.4
02/16/17 11:32
Carbon tetrachloride
ug/kg
ND
5.7
02/16/17 11:32
Chlorobenzene
ug/kg
ND
5.7
02/16/17 11:32
Chloroethane
ug/kg
ND
11.4
02/16/17 11:32
Chloroform
ug/kg
ND
5.7
02/16/17 11:32
Chloromethane
ug/kg
ND
11.4
02/16/17 11:32
cis-1,2-Dichloroethene
ug/kg
ND
5.7
02/16/17 11:32
cis-1,3-Dichloropropene
ug/kg
ND
5.7
02/16/17 11:32
Dibromochloromethane
ug/kg
ND
5.7
02/16/17 11:32
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
METHOD BLANK: 1933726
Associated Lab Samples: 92329914003
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Dibromomethane
ug/kg
ND
5.7
02/16/17 11:32
Dichlorodifluoromethane
ug/kg
ND
11.4
02/16/17 11:32
Diisopropyl ether
ug/kg
ND
5.7
02/16/17 11:32
Ethylbenzene
ug/kg
ND
5.7
02/16/17 11:32
Hexachloro-1,3-butadiene
ug/kg
ND
5.7
02/16/17 11:32
Isopropylbenzene (Cumene)
ug/kg
ND
5.7
02/16/17 11:32
m&p-Xylene
ug/kg
ND
11.4
02/16/17 11:32
Methyl-tert-butyl ether
ug/kg
ND
5.7
02/16/17 11:32
Methylene Chloride
ug/kg
ND
22.9
02/16/17 11:32
n-Butylbenzene
ug/kg
ND
5.7
02/16/17 11:32
n-Propylbenzene
ug/kg
ND
5.7
02/16/17 11:32
Naphthalene
ug/kg
ND
5.7
02/16/17 11:32
o-Xylene
ug/kg
ND
5.7
02/16/17 11:32
p-Isopropyltoluene
ug/kg
ND
5.7
02/16/17 11:32
sec-Butylbenzene
ug/kg
ND
5.7
02/16/17 11:32
Styrene
ug/kg
ND
5.7
02/16/17 11:32
tert-Butyl benzene
ug/kg
ND
5.7
02/16/17 11:32
Tetrachloroethene
ug/kg
ND
5.7
02/16/17 11:32
Toluene
ug/kg
ND
5.7
02/16/17 11:32
trans-1,2-Dichloroethene
ug/kg
ND
5.7
02/16/17 11:32
trans- 1,3-Dichloropropene
ug/kg
ND
5.7
02/16/17 11:32
Trichloroethene
ug/kg
ND
5.7
02/16/17 11:32
Trichlorofluoromethane
ug/kg
ND
5.7
02/16/17 11:32
Vinyl acetate
ug/kg
ND
57.2
02/16/17 11:32
Vinyl chloride
ug/kg
ND
11.4
02/16/17 11:32
Xylene (Total)
ug/kg
ND
11.4
02/16/17 11:32
1,2-Dichloroethane-d4 (S)
%
89
70-132
02/16/17 11:32
4-Bromofluorobenzene (S)
%
103
70-130
02/16/17 11:32
Toluene-d8 (S)
%
104
70-130
02/16/17 11:32
Qualifiers
LABORATORY CONTROL SAMPLE:
1933727
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
69.1
66.2
96
74-137
1,1,1-Trichloroethane
ug/kg
69.1
57.5
83
67-140
1,1,2,2-Tetrachloroethane
ug/kg
69.1
67.3
97
72-141
1,1,2-Trichloroethane
ug/kg
69.1
64.3
93
78-138
1,1-Dichloroethane
ug/kg
69.1
62.7
91
69-134
1,1-Dichloroethene
ug/kg
69.1
68.8
100
67-138
1,1-Dichloropropene
ug/kg
69.1
60.4
87
69-139
1,2,3-Trichlorobenzene
ug/kg
69.1
70.9
103
70-146
1,2,3-Trichloropropane
ug/kg
69.1
71.1
103
69-144
1,2,4-Trichlorobenzene
ug/kg
69.1
72.8
105
68-148
1,2,4-Trimethylbenzene
ug/kg
69.1
66.2
96
74-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
LABORATORY CONTROL SAMPLE:
Parameter
1933727
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/kg
69.1
63.5
92
65-140
1,2-Dibromoethane (EDB)
ug/kg
69.1
60.4
87
77-135
1,2-Dichlorobenzene
ug/kg
69.1
70.3
102
77-141
1,2-Dichloroethane
ug/kg
69.1
59.4
86
65-137
1,2-Dichloropropane
ug/kg
69.1
60.1
87
72-136
1,3,5-Trimethylbenzene
ug/kg
69.1
64.4
93
76-133
1,3-Dichlorobenzene
ug/kg
69.1
69.7
101
74-138
1,3-Dichloropropane
ug/kg
69.1
66.2
96
71-139
1,4-Dichlorobenzene
ug/kg
69.1
70.4
102
76-138
2,2-Dichloropropane
ug/kg
69.1
56.6
82
68-137
2-Butanone (MEK)
ug/kg
138
113J
82
58-147
2-Chlorotoluene
ug/kg
69.1
66.0
96
73-139
2-Hexanone
ug/kg
138
110
79
62-145
4-Chlorotoluene
ug/kg
69.1
68.9
100
76-141
4-Methyl-2-pentanone (MIBK)
ug/kg
138
120
87
64-149
Acetone
ug/kg
138
127J
92
53-153
Benzene
ug/kg
69.1
60.9
88
73-135
Bromobenzene
ug/kg
69.1
66.9
97
75-133
Bromochloromethane
ug/kg
69.1
58.8
85
73-134
Bromodichloromethane
ug/kg
69.1
65.3
95
71-135
Bromoform
ug/kg
69.1
65.1
94
66-141
Bromomethane
ug/kg
69.1
73.3
106
53-160
Carbon tetrachloride
ug/kg
69.1
54.4
79
60-145
Chlorobenzene
ug/kg
69.1
64.3
93
78-130
Chloroethane
ug/kg
69.1
80.8
117
64-149
Chloroform
ug/kg
69.1
59.5
86
70-134
Chloromethane
ug/kg
69.1
74.5
108
52-150
cis-1,2-Dichloroethene
ug/kg
69.1
57.9
84
70-133
cis-1,3-Dichloropropene
ug/kg
69.1
63.0
91
68-134
Dibromochloromethane
ug/kg
69.1
66.9
97
71-138
Dibromomethane
ug/kg
69.1
59.0
85
74-130
Dichlorodifluoromethane
ug/kg
69.1
72.8
105
40-160
Diisopropyl ether
ug/kg
69.1
68.1
99
69-141
Ethylbenzene
ug/kg
69.1
62.2
90
75-133
Hexachloro-1,3-butadiene
ug/kg
69.1
68.8
100
68-143
Isopropylbenzene (Cumene)
ug/kg
69.1
63.8
92
76-143
m&p-Xylene
ug/kg
138
126
91
75-136
Methyl-tert-butyl ether
ug/kg
69.1
67.0
97
68-144
Methylene Chloride
ug/kg
69.1
61.7
89
45-154
n-Butylbenzene
ug/kg
69.1
66.3
96
72-137
n-Propylbenzene
ug/kg
69.1
65.0
94
76-136
Naphthalene
ug/kg
69.1
70.5
102
68-151
o-Xylene
ug/kg
69.1
63.9
93
76-141
p-Isopropyltoluene
ug/kg
69.1
61.9
90
76-140
sec-Butylbenzene
ug/kg
69.1
66.0
96
79-139
Styrene
ug/kg
69.1
67.3
97
79-137
tert-Butyl benzene
ug/kg
69.1
58.9
85
74-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 53

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
LABORATORY CONTROL SAMPLE:
Parameter
1933727
Units
Spike
Conc.
LCS LCS
Result % Rec
Tetrachloroethene
ug/kg
69.1
56.0
Toluene
ug/kg
69.1
59.2
trans-1,2-Dichloroethene
ug/kg
69.1
61.4
trans- 1,3-Dichloropropene
ug/kg
69.1
63.0
Trichloroethene
ug/kg
69.1
63.2
Trichlorofluoromethane
ug/kg
69.1
75.9
Vinyl acetate
ug/kg
138
107
Vinyl chloride
ug/kg
69.1
62.7
Xylene (Total)
ug/kg
207
190
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
% Rec
Limits
81 71-138
86 74-131
89 67-135
91 65-146
92 67-135
110 59-144
77 40-160
91 56-141
92 76-137
95 70-132
101 70-130
99 70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 53

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
QC Batch: 348297 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92329914001, 92329914002, 92329914003, 92329914004, 92329914005, 92329914006
METHOD BLANK: 1932283 Matrix: Solid
Associated Lab Samples: 92329914001, 92329914002, 92329914003, 92329914004, 92329914005, 92329914006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
330
02/15/17 11:41
1,2-Dichlorobenzene
ug/kg
ND
330
02/15/17 11:41
1,3-Dichlorobenzene
ug/kg
ND
330
02/15/17 11:41
1,4-Dichlorobenzene
ug/kg
ND
330
02/15/17 11:41
1-Methylnaphthalene
ug/kg
ND
330
02/15/17 11:41
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
330
02/15/17 11:41
2,4,5-Trichlorophenol
ug/kg
ND
330
02/15/17 11:41
2,4,6-Trichlorophenol
ug/kg
ND
330
02/15/17 11:41
2,4-Dichlorophenol
ug/kg
ND
330
02/15/17 11:41
2,4-Dimethylphenol
ug/kg
ND
330
02/15/17 11:41
2,4-Dinitrophenol
ug/kg
ND
1650
02/15/17 11:41
2,4-Dinitrotoluene
ug/kg
ND
330
02/15/17 11:41
2,6-Dinitrotoluene
ug/kg
ND
330
02/15/17 11:41
2-Chloronaphthalene
ug/kg
ND
330
02/15/17 11:41
2-Chlorophenol
ug/kg
ND
330
02/15/17 11:41
2-Methylnaphthalene
ug/kg
ND
330
02/15/17 11:41
2-Methylphenol(o-Cresol)
ug/kg
ND
330
02/15/17 11:41
2-Nitroaniline
ug/kg
ND
1650
02/15/17 11:41
2-Nitrophenol
ug/kg
ND
330
02/15/17 11:41
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
330
02/15/17 11:41
3,3'-Dichlorobenzidine
ug/kg
ND
1650
02/15/17 11:41
3-Nitroaniline
ug/kg
ND
1650
02/15/17 11:41
4,6-Dinitro-2-methyl phenol
ug/kg
ND
660
02/15/17 11:41
4-Bromophenylphenyl ether
ug/kg
ND
330
02/15/17 11:41
4-ChIoro-3-methyl phenol
ug/kg
ND
660
02/15/17 11:41
4-Chloroaniline
ug/kg
ND
1650
02/15/17 11:41
4-Chlorophenylphenyl ether
ug/kg
ND
330
02/15/17 11:41
4-Nitroaniline
ug/kg
ND
660
02/15/17 11:41
4-Nitrophenol
ug/kg
ND
1650
02/15/17 11:41
Acenaphthene
ug/kg
ND
330
02/15/17 11:41
Acenaphthylene
ug/kg
ND
330
02/15/17 11:41
Aniline
ug/kg
ND
330
02/15/17 11:41
Anthracene
ug/kg
ND
330
02/15/17 11:41
Benzo(a)anthracene
ug/kg
ND
330
02/15/17 11:41
Benzo(a)pyrene
ug/kg
ND
330
02/15/17 11:41
Benzo(b)fluoranthene
ug/kg
ND
330
02/15/17 11:41
Benzo(g,h,i)perylene
ug/kg
ND
330
02/15/17 11:41
Benzo(k)fluoranthene
ug/kg
ND
330
02/15/17 11:41
Benzoic Acid
ug/kg
ND
1650
02/15/17 11:41
Benzyl alcohol
ug/kg
ND
660
02/15/17 11:41
bis(2-Chloroethoxy)methane
ug/kg
ND
330
02/15/17 11:41
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 53

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
METHOD BLANK: 1932283 Matrix: Solid
Associated Lab Samples: 92329914001, 92329914002, 92329914003, 92329914004, 92329914005, 92329914006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
bis(2-Chloroethyl) ether
ug/kg
ND
330
02/15/17 11:41
bis(2-Ethylhexyl)phthalate
ug/kg
ND
330
02/15/17 11:41
Butylbenzylphthalate
ug/kg
ND
330
02/15/17 11:41
Chrysene
ug/kg
ND
330
02/15/17 11:41
Di-n-butylphthalate
ug/kg
ND
330
02/15/17 11:41
Di-n-octylphthalate
ug/kg
ND
330
02/15/17 11:41
Dibenz(a,h)anthracene
ug/kg
ND
330
02/15/17 11:41
Dibenzofuran
ug/kg
ND
330
02/15/17 11:41
Diethylphthalate
ug/kg
ND
330
02/15/17 11:41
Dimethylphthalate
ug/kg
ND
330
02/15/17 11:41
Fluoranthene
ug/kg
ND
330
02/15/17 11:41
Fluorene
ug/kg
ND
330
02/15/17 11:41
Hexachloro-1,3-butadiene
ug/kg
ND
330
02/15/17 11:41
Hexachlorobenzene
ug/kg
ND
330
02/15/17 11:41
Hexachlorocyclopentadiene
ug/kg
ND
330
02/15/17 11:41
Hexachloroethane
ug/kg
ND
330
02/15/17 11:41
Indeno(1,2,3-cd)pyrene
ug/kg
ND
330
02/15/17 11:41
Isophorone
ug/kg
ND
330
02/15/17 11:41
N-Nitroso-di-n-propylamine
ug/kg
ND
330
02/15/17 11:41
N-Nitrosodimethylamine
ug/kg
ND
330
02/15/17 11:41
N-Nitrosodiphenylamine
ug/kg
ND
330
02/15/17 11:41
Naphthalene
ug/kg
ND
330
02/15/17 11:41
Nitrobenzene
ug/kg
ND
330
02/15/17 11:41
Pentachlorophenol
ug/kg
ND
1650
02/15/17 11:41
Phenanthrene
ug/kg
ND
330
02/15/17 11:41
Phenol
ug/kg
ND
330
02/15/17 11:41
Pyrene
ug/kg
ND
330
02/15/17 11:41
2,4,6-Tribromophenol (S)
%
110
27-110
02/15/17 11:41
2-Fluorobiphenyl (S)
%
78
30-110
02/15/17 11:41
2-Fluorophenol (S)
%
77
13-110
02/15/17 11:41
Nitrobenzene-d5 (S)
%
54
23-110
02/15/17 11:41
Phenol-d6 (S)
%
82
22-110
02/15/17 11:41
Terphenyl-d14 (S)
%
90
28-110
02/15/17 11:41
LABORATORY CONTROL SAMPLE:
1932284
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1670
1230
74
36-120
1,2-Dichlorobenzene
ug/kg
1670
1170
70
41-120
1,3-Dichlorobenzene
ug/kg
1670
1120
67
66-120
1,4-Dichlorobenzene
ug/kg
1670
1120
67
42-120
1-Methylnaphthalene
ug/kg
1670
1370
82
40-120
2,2'-Oxybis(1-chloropropane)
ug/kg
1670
941
56
17-120
2,4,5-Trichlorophenol
ug/kg
1670
1260
76
37-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 53

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
LABORATORY CONTROL SAMPLE:
Parameter
1932284
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,6-TrichIorophenol
ug/kg
1670
1300
78
40-120
2,4-DichIorophenol
ug/kg
1670
1340
80
33-120
2,4-Dimethylphenol
ug/kg
1670
1280
77
36-120
2,4-Dinitrophenol
ug/kg
8330
6030
72
22-121
2,4-Dinitrotoluene
ug/kg
1670
1580
95
60-120
2,6-Dinitrotoluene
ug/kg
1670
1570
94
54-120
2-Chloronaphthalene
ug/kg
1670
1210
73
41-120
2-Chlorophenol
ug/kg
1670
1280
77
39-120
2-Methylnaphthalene
ug/kg
1670
1410
85
26-120
2-Methylphenol(o-Cresol)
ug/kg
1670
1140
68
41-120
2-Nitroaniline
ug/kg
3330
1950
59
45-120
2-Nitrophenol
ug/kg
1670
1210
73
35-120
3&4-Methyl phenol (m&p Cresol)
ug/kg
1670
1130
68
35-120
3,3'-Dichlorobenzidine
ug/kg
3330
2670
80
16-125
3-Nitroaniline
ug/kg
3330
2740
82
45-120
4,6-Dinitro-2-methyl phenol
ug/kg
3330
2740
82
46-120
4-Bromophenylphenyl ether
ug/kg
1670
1330
80
36-120
4-Chloro-3-methylphenol
ug/kg
3330
2610
78
37-120
4-Chloroaniline
ug/kg
3330
2610
78
35-120
4-Chlorophenylphenyl ether
ug/kg
1670
1230
74
30-120
4-Nitroaniline
ug/kg
3330
2850
86
48-120
4-Nitrophenol
ug/kg
8330
5150
62
43-120
Acenaphthene
ug/kg
1670
1290
77
46-120
Acenaphthylene
ug/kg
1670
1340
80
46-120
Aniline
ug/kg
1670
883
53
33-120
Anthracene
ug/kg
1670
1400
84
63-120
Benzo(a)anthracene
ug/kg
1670
1380
83
61-120
Benzo(a)pyrene
ug/kg
1670
1470
88
59-120
Benzo(b)fluoranthene
ug/kg
1670
1200
72
55-120
Benzo(g,h,i)perylene
ug/kg
1670
1340
81
57-120
Benzo(k)fluoranthene
ug/kg
1670
1340
80
56-120
Benzoic Acid
ug/kg
8330
4270
51
13-120
Benzyl alcohol
ug/kg
3330
2300
69
34-120
bis(2-Chloroethoxy)methane
ug/kg
1670
1070
64
21-120
bis(2-Chloroethyl) ether
ug/kg
1670
1030
62
25-120
bis(2-Ethylhexyl)phthalate
ug/kg
1670
1430
86
56-123
Butylbenzylphthalate
ug/kg
1670
1360
82
57-120
Chrysene
ug/kg
1670
1360
81
64-120
Di-n-butylphthalate
ug/kg
1670
1600
96
58-120
Di-n-octylphthalate
ug/kg
1670
1480
89
47-121
Dibenz(a,h)anthracene
ug/kg
1670
1360
82
56-120
Dibenzofuran
ug/kg
1670
1310
78
43-120
Diethylphthalate
ug/kg
1670
1410
84
55-120
Dimethylphthalate
ug/kg
1670
1420
85
54-120
Fluoranthene
ug/kg
1670
1550
93
61-120
Fluorene
ug/kg
1670
1330
80
51-120
Hexachloro-1,3-butadiene
ug/kg
1670
1100
66
22-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 53

aceAnalytical
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[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
LABORATORY CONTROL SAMPLE:
1932284
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Hexachlorobenzene
ug/kg
1670
1470
88
53-120
Hexachlorocyclopentadiene
ug/kg
1670
856
51
18-150
Hexachloroethane
ug/kg
1670
1020
61
39-120
Indeno(1,2,3-cd)pyrene
ug/kg
1670
1390
84
58-120
Isophorone
ug/kg
1670
1230
74
38-120
N-Nitroso-di-n-propylamine
ug/kg
1670
1050
63
30-120
N-Nitrosodimethylamine
ug/kg
1670
849
51
32-120
N-Nitrosodiphenylamine
ug/kg
1670
1300
78
50-120
Naphthalene
ug/kg
1670
1270
76
38-120
Nitrobenzene
ug/kg
1670
1010
60
37-120
Pentachlorophenol
ug/kg
3330
3220
97
10-120
Phenanthrene
ug/kg
1670
1370
82
62-120
Phenol
ug/kg
1670
1160
70
37-120
Pyrene
ug/kg
1670
1250
75
63-120
2,4,6-Tribromophenol (S)
%
110
27-110
2-Fluorobiphenyl (S)
%
71
30-110
2-Fluorophenol(S)
%
64
13-110
Nitrobenzene-d5 (S)
%
56
23-110
Phenol-d6 (S)
%
69
22-110
Terphenyl-d14 (S)
%
81
28-110
MATRIX SPIKE SAMPLE:
1932285
92329914001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
2100
1380
66
18-119
1,2-Dichlorobenzene
ug/kg
ND
2100
1260
60
50-110
1,3-Dichlorobenzene
ug/kg
ND
2100
1230
58
27-110
1,4-Dichlorobenzene
ug/kg
ND
2100
1260
60
28-110
1-Methylnaphthalene
ug/kg
ND
2100
1470
70
24-116
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
2100
998
48
50-150 M1
2,4,5-Trichlorophenol
ug/kg
ND
2100
1390
66
28-110
2,4,6-Trichlorophenol
ug/kg
ND
2100
1390
66
17-117
2,4-Dichlorophenol
ug/kg
ND
2100
1400
67
21-128
2,4-Dimethylphenol
ug/kg
ND
2100
1370
65
10-120
2,4-Dinitrophenol
ug/kg
ND
10500
6690
64
10-107
2,4-Dinitrotoluene
ug/kg
ND
2100
1690
80
36-109
2,6-Dinitrotoluene
ug/kg
ND
2100
1650
79
32-110
2-Chloronaphthalene
ug/kg
ND
2100
1360
65
30-107
2-Chlorophenol
ug/kg
ND
2100
1370
65
14-106
2-Methylnaphthalene
ug/kg
ND
2100
1500
72
10-135
2-Methylphenol(o-Cresol)
ug/kg
ND
2100
1100
52
10-124
2-Nitroaniline
ug/kg
ND
4190
2150
51
26-116
2-Nitrophenol
ug/kg
ND
2100
1370
66
28-103
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
2100
1090
52
10-109
3,3'-Dichlorobenzidine
ug/kg
ND
4190
2810
67
10-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 53

aceAnalytical
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
MATRIX SPIKE SAMPLE:
1932285
92329914001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
3-Nitroaniline
ug/kg
ND
4190
2970
71
22-110
4,6-Dinitro-2-methyl phenol
ug/kg
ND
4190
2910
69
13-121
4-Bromophenylphenyl ether
ug/kg
ND
2100
1420
68
31-109
4-Chloro-3-methylphenol
ug/kg
ND
4190
2680
64
13-128
4-Chloroaniline
ug/kg
ND
4190
2700
64
18-102
4-Chlorophenylphenyl ether
ug/kg
ND
2100
1340
64
29-112
4-Nitroaniline
ug/kg
ND
4190
3070
73
16-111
4-Nitrophenol
ug/kg
ND
10500
5100
49
14-135
Acenaphthene
ug/kg
ND
2100
1380
66
26-114
Acenaphthylene
ug/kg
ND
2100
1460
69
32-108
Aniline
ug/kg
ND
2100
618
29
10-107
Anthracene
ug/kg
ND
2100
1630
78
32-111
Benzo(a)anthracene
ug/kg
ND
2100
1420
68
25-117
Benzo(a)pyrene
ug/kg
ND
2100
1620
77
25-106
Benzo(b)fluoranthene
ug/kg
ND
2100
1430
68
24-110
Benzo(g,h,i)perylene
ug/kg
ND
2100
1460
70
19-112
Benzo(k)fluoranthene
ug/kg
ND
2100
1670
80
24-114
Benzoic Acid
ug/kg
ND
10500
1670J
16
10-110
Benzyl alcohol
ug/kg
ND
4190
2120
51
24-106
bis(2-Chloroethoxy)methane
ug/kg
ND
2100
1100
52
13-119
bis(2-Chloroethyl) ether
ug/kg
ND
2100
1120
53
10-134
bis(2-Ethylhexyl)phthalate
ug/kg
ND
2100
1480
71
10-125
Butylbenzylphthalate
ug/kg
ND
2100
1410
67
18-110
Chrysene
ug/kg
ND
2100
1510
72
30-110
Di-n-butylphthalate
ug/kg
ND
2100
1620
77
19-112
Di-n-octylphthalate
ug/kg
ND
2100
1470
70
17-105
Dibenz(a,h)anthracene
ug/kg
ND
2100
1470
70
23-111
Dibenzofuran
ug/kg
ND
2100
1400
67
35-103
Diethylphthalate
ug/kg
ND
2100
1480
71
27-113
Dimethylphthalate
ug/kg
ND
2100
1550
74
26-111
Fluoranthene
ug/kg
ND
2100
1740
83
33-109
Fluorene
ug/kg
ND
2100
1420
67
32-113
Hexachloro-1,3-butadiene
ug/kg
ND
2100
1280
61
16-116
Hexachlorobenzene
ug/kg
ND
2100
1570
75
27-120
Hexachlorocyclopentadiene
ug/kg
ND
2100
953
45
10-108
Hexachloroethane
ug/kg
ND
2100
1130
54
10-117
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2100
1510
72
10-122
Isophorone
ug/kg
ND
2100
1290
62
28-114
N-Nitroso-di-n-propylamine
ug/kg
ND
2100
993
47
27-113
N-Nitrosodimethylamine
ug/kg
ND
2100
806
38
10-109
N-Nitrosodiphenylamine
ug/kg
ND
2100
1320
63
10-128
Naphthalene
ug/kg
ND
2100
1420
68
25-110
Nitrobenzene
ug/kg
ND
2100
1170
56
18-114
Pentachlorophenol
ug/kg
ND
4190
3250
78
10-122
Phenanthrene
ug/kg
ND
2100
1490
71
30-114
Phenol
ug/kg
ND
2100
1130
54
11-102
Pyrene
ug/kg
ND
2100
1210
58
25-116
Results presented on this
page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SOIL SAMPLING
Pace Project No.: 92329914
MATRIX SPIKE SAMPLE:
Parameter
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
1932285
Units
92329914001 Spike MS MS
Result Conc. Result % Rec
% Rec
Limits
%
91
27-110
%
63
30-110
%
54
13-110
%
48
23-110
%
54
22-110
%
61
28-110
SAMPLE DUPLICATE: 1932286
Parameter
Units
92329914005
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
1-Methylnaphthalene
ug/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
2,4,5-Trichlorophenol
ug/kg
ND
ND
2,4,6-Trichlorophenol
ug/kg
ND
ND
2,4-Dichlorophenol
ug/kg
ND
ND
2,4-Dimethylphenol
ug/kg
ND
ND
2,4-Dinitrophenol
ug/kg
ND
ND
2,4-Dinitrotoluene
ug/kg
ND
ND
2,6-Dinitrotoluene
ug/kg
ND
ND
2-Chloronaphthalene
ug/kg
ND
ND
2-Chlorophenol
ug/kg
ND
ND
2-Methylnaphthalene
ug/kg
ND
ND
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
2-Nitroaniline
ug/kg
ND
ND
2-Nitrophenol
ug/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
3,3'-Dichlorobenzidine
ug/kg
ND
ND
3-Nitroaniline
ug/kg
ND
ND
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
4-Bromophenylphenyl ether
ug/kg
ND
ND
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
4-Chloroaniline
ug/kg
ND
ND
4-Chlorophenylphenyl ether
ug/kg
ND
ND
4-Nitroaniline
ug/kg
ND
ND
4-Nitrophenol
ug/kg
ND
ND
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
Aniline
ug/kg
ND
ND
Anthracene
ug/kg
ND
ND
Benzo(a)anthracene
ug/kg
ND
ND
Benzo(a)pyrene
ug/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
SAMPLE DUPLICATE: 1932286
Parameter
Units
92329914005
Result
Dup
Result
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
94
80
2-Fluorobiphenyl (S)
%
58
52
2-Fluorophenol(S)
%
66
54
Nitrobenzene-d5 (S)
%
48
42
Phenol-d6 (S)
%
67
53
Terphenyl-d14 (S)
%
81
71
RPD Qualifiers
16
11
19
14
24
13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SOIL SAMPLING
Pace Project No.: 92329914
QC Batch: 348197 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92329914001, 92329914002, 92329914003, 92329914004, 92329914005, 92329914006
SAMPLE DUPLICATE: 1932003
92329914001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 20.5 23.1 12
SAMPLE DUPLICATE: 1932004
92329912012 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 17.2 17.7 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: SOIL SAMPLING
Pace Project No.: 92329914
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/16/2017 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 53

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SOIL SAMPLING
92329914
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92329914001
B-1
EPA 3050
348310
EPA 6010
348441
92329914002
B-2
EPA 3050
348310
EPA 6010
348441
92329914003
B-3
EPA 3050
348310
EPA 6010
348441
92329914004
B-4
EPA 3050
348310
EPA 6010
348441
92329914005
B-5
EPA 3050
348310
EPA 6010
348441
92329914006
B-6
EPA 3050
348310
EPA 6010
348441
92329914001
B-1
EPA 7471
348452
EPA 7471
348469
92329914002
B-2
EPA 7471
348452
EPA 7471
348469
92329914003
B-3
EPA 7471
348452
EPA 7471
348469
92329914004
B-4
EPA 7471
348452
EPA 7471
348469
92329914005
B-5
EPA 7471
348452
EPA 7471
348469
92329914006
B-6
EPA 7471
348452
EPA 7471
348469
92329914001
B-1
EPA 3546
348297
EPA 8270
348379
92329914002
B-2
EPA 3546
348297
EPA 8270
348379
92329914003
B-3
EPA 3546
348297
EPA 8270
348379
92329914004
B-4
EPA 3546
348297
EPA 8270
348379
92329914005
B-5
EPA 3546
348297
EPA 8270
348379
92329914006
B-6
EPA 3546
348297
EPA 8270
348379
92329914001
B-1
EPA 8260
348335
92329914002
B-2
EPA 8260
348335
92329914003
B-3
EPA 8260
348542
92329914004
B-4
EPA 8260
348335
92329914005
B-5
EPA 8260
348335
92329914006
B-6
EPA 8260
348335
92329914001
B-1
ASTM D2974-87
348197
92329914002
B-2
ASTM D2974-87
348197
92329914003
B-3
ASTM D2974-87
348197
92329914004
B-4
ASTM D2974-87
348197
92329914005
B-5
ASTM D2974-87
348197
92329914006
B-6
ASTM D2974-87
348197
Date: 02/16/2017 03:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 50 of 53

i--c - acNL. cA' cvi�
/715ceAnavicaI Sample Condition Upon Receipt(SCUR) Page 1 of 2
r
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville.�] Raleigh❑ MechanicsvilleF�
WO#:92329914
Sample p ■ Client Name:
- r Project #:U II l III l llllll l lllll Ill
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client 92329914
❑ Commercial ❑Pace ❑Other:
Custody Seal Present? Des QNO Seals Intact? ❑Yes C}No
Packing Material: ❑Bubble Wrap `�bble Bags ❑None Mother: Date/Initials Person Examining Contents:
Thermometer:
�IR Gun ID: Type o Ic Wet ❑Blue ❑None Samples on ice, cooling process has begun
Correction Factor. Confer Temp Corrected {°C): r �� Biological Tissue Frozen? ❑Yes No ❑N/A
Temp should be above reezing to 6°C
USDA Regulated Soil (qN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check
❑Yes [!We
maps)?
Did samples originate from a foreign source (intetnationally,
including Hawaii and Puerto Rico)? ❑Yes [i Np
Comments/Discrepancy:
Chain of Custody Present?
415
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
[]No
[_—]N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
QN0
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
Yes
❑No
❑N/A
5.
Correct Containers Used?
1Yes
[:]No
❑N/A
6.
-Pace Containers Used?
Yes
❑No
❑N/A
Containers Intact?
C es
[:]No
❑N/A
7.
Samples Field Filtered?
[]Yes
❑No
N/A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
UQyes
❑No
❑N/A
4.
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
N%A
10.
Trip Blank Present?
❑Yes
❑No
/A
11.
Trip Blank Custody Seals Present?
LJYes
[]No
N/
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes ❑No
Person Contacted:
Comments/Sample
Discrepancy:
Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out or temp, incorrect containers)
Page 51 of 53

Document Name: Document Revised: Sept. 21, 2016
Sample Condition Upon Receipt(5CUR) Page 2 of 2
,/-'aceAna lyfICal Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Office
*Check mark top half of box if pal and/or dechlorination
is verified and within the acceptance range for
preservation samples.
**Bottom half of box is to list number of bottles
Project # I
W4#:92329914
pM: PTE Due Date: 02/20/17
CLIENT: 92—TERRATECH
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Lot #
Page 52 of 53

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Page 53 of 53

Tables
Non -UST Releases of Petroleum
Table 1 Maximum Soil Contaminant Concentrations (MSCCs)
(See http://Portal.ncdenr.org/web/wm/ust/guidance#OTHRCAB for current version)
Constituent
CAS#
Soil -to -Water
Maximum
Contaminant
Concentration
(Soil mg/kg)
Residential
Soil
Cleanup
Levels
(mg/kg)
Industrial/
Commercial
Soil
Cleanup
Levels
(mg/kg)
Acena hthene
83-32-9
8.2
940
24000
Acena hth lene
208-96-8
11
469
12264
Acetone
67-64-1
24
14000
360000
Ali hatics, C5-C8
N/A
68
939
24528
Ali hatics, C9-C18
N/A
540
1500
40000
Ali hatics, C19-C36
N/A
#
31000
810000
tert-Am I alcohol TAA
75-85-4
0.1
tert-Am I methyl ether TAME
994-05-8
0.52
1960
51100
Anthracene
120-12-7
940
4600
122000
Aromatics, C9-C22
N/A
31
469
12264
Barium
7440-39-3
290
3100
81000
Benzene
71-43-2
0.0056
18
164
Benzo a anthracene benz a anthracene
56-55-3
0.35
0.88
8
Benzo b fluoranthene
205-99-2
1.2
0.88
8
Benzo ,h,i er lene
191-24-2
6400
469
12264
Benzo k fluoranthene
207-08-9
12
9
78
Benzoic acid
65-85-0
120
62571
1635200
Benzo a rene
50-32-8
0.096
0.088
0.78
Benz I alcohol
100-51-6
2
1000
40000
Bis chloroeth I ether BCEE
111-44-4
0.00016
0.58
5.2
Bis 2-eth lhex I hthalate DEHP
117-81-7
6.6
46
410
Bromoform tribromomethane
75-25-2
0.026
81
724
Bromomethane meth (bromide
74-83-9
0.4
22
570
Butanol
71-36-3
2
1000
40000
tert-But l alcohol (TBA) (tert-butanol
75-65-0
0.04
213
1910
n-But (benzene
104-51-8
4.3
626
16350
sec -But lbenzene
135-98-8
3.3
626
16350
tert-But (benzene
98-06-6
3.4
626
16350
tert-But I formate (TBF)
762-75-4
0.1
Carbon disulfide
75-15-0
4.3
1564
40880
Chlorobenzene
108-90-7
0.44
312
8176
Chloroform trichloromethane
67-66-3
0.37
20
180
Chloromethane (methyl chloride
74-87-3
0.02
49
440
4-Chlorotoluene-chlorotoluene
106-43-4
0.1
1000
20000
Chromium Total
7440-50-8
5.4
47
1226
Chromium III
16065-83-1
4200
23460
613200
Chromium VI
18540-29-9
5.4
47
1226
44

Tables
Non -UST Releases of Petroleum
Constituent
CAS#
Soil -to -Water
Maximum
Contaminant
Concentration
(Soil mg/kg)
Residential
Soil
Cleanup
Levels
(mg/kg)
Industrial/
Commercial
Soil
Cleanup
Levels
(mg/kg)
Chrysene
218-01-9
39
88
780
Dibenz a,h anthracene
53-70-3
0.17
0.088
0.78
Dibenzofuran
132-64-9
4.7
62
1635
Dibromochloromethane
124-48-1
0.0021
7
68
1,2-Dichlorobenzene
orthodichlorobenzene
95-50-1
0.23
1400
36000
1,3-Dichlorobenzene
metadichlorobenzene
541-73-1
7.6
460
12000
1,4-Dichlorobenzene
aradichlorobenzene
106-46-7
0.099
110
1000
Dichlorodifluoromethane Freon-12; halon
75-71-8
210
3129
81760
1,1-Dichloroethane
75-34-3
0.032
110
1000
1,2-Dichloroethane (ethylene dichloride
107-06-2
0.0019
7
63
1,2-Dichloroethene cis
156-59-2
0.35
156
4000
1,2-Dichloroethene trans
156-60-5
0.54
310
8200
1,2-Dichloroethene cis and trans
540-59-0
0.35
100
3000
1,1-Dichloroeth lene vin lidene chloride
75-35-4
0.045
780
20000
2,4-Dichloro henol
120-83-2
0.0034
40
1000
1,2-Dichloro ro ane
78-87-5
0.003
10
92
1,3-Dichloropropene (cis and trans
isomers
542-75-6
0.001
5
57
2,4-Dimeth I henol 2,4-x lenol
105-67-9
0.64
312
8176
Ethanol
64-17-5
16
7000
200000
Ethyl acetate
141-78-6
12
14078
367920
Eth (benzene
100-41-4
4.9
1560
40000
Ethylene dibromide 1,2-dibromoethane
106-93-4
0.000098
0.31
2.8
Ethylene glycol
107-21-1
40
31290
817600
Ethyl tert-but I ether
63-79-23
0.2
Fluoranthene
206-44-0
290
620
16400
Fluorene
86-73-7
47
620
16400
Hexachlorobutadiene
87-68-3
0.23
4.6
73
2-Hexanone (methyl n-but I ketone, MBK
591-78-6
0.1
70
2000
lndeno 1,2,3-cd rene
193-39-5
3.4
0.88
8
Isopropyl benzene cumene
98-82-8
1.7
1564
40880
Isopropyl ether diiso ro I ether
108-20-3
0.37
156
4088
4-Isopropyltoluene (p-isopropyltoluene, p-
c mene
99-87-6
0.12
100
4000
Lead
7439-92-1
270
400
400
Methanol
67561
16
7821
204400
Methyl ethyl ketone 2-butanone; MEK
78-93-3
16
9385
245280
Methyl tert-but l ether MTBE
1634-04-4
0.091
350
3100
Methylene chloride
75-09-2
0.02
85
763
45

Tables
Non -UST Releases of Petroleum
Constituent
CAS#
Soil -to -Water
Maximum
Contaminant
Concentration
(Soil mg/kg)
Residential
Soil
Cleanup
Levels
(mg/kg)
Industrial/
Commercial
Soil
Cleanup
Levels
(mg/kg)
Methyl isobut l ketone MIBK
108-10-1
0.4
1200
32000
1-Meth Ina hthalene
90-12-0
0.004
20
100
2-Methyl nahthalene
91-57-6
3.6
63
1635
2-Meth I henol
95-48-7
1
700
20000
Naphthalene
91-20-3
0.16
313
8176
Pentachloro henol
87-86-5
0.0065
5
48
Phenanthrene
85-01-8
56
469
12264
Phenol
108-95-2
0.17
4693
122600
n-Pro (benzene
103-65-1
1.7
626
16350
P rene
129-00-0
270
469
12264
Silver
7440-22-4
0.25
78.2
2044
Styrene ethen (benzene
100-42-5
1.5
3128
81760
1, 1, 1,2-Tetrachloroethane
360-20-6
0.004
20
200
1,1,2,2-Tetrachloroethane
79-34-5
0.001
0.78
20
Tetrachloroethylene (perchloroethylene;
PCE
127-18-4
0.0074
1.1
10
Toluene
108-88-3
4.3
1200
32000
1,2,4-Trichlorobenzene
120-82-1
2.6
156
4088
1,1,1-Trichloroethane (methyl chloroform
71-55-6
1.6
31000
810000
1,1,2-Trichloroethane
79-00-5
0.002
10
100
Trichloroeth Iene TCE
79-01-6
0.019
4.6
120
Trichlorofluoromethane
75-69-4
29
4692
122640
1,2,4-Trimeth (benzene
95-63-6
8.5
782
20440
1,3,5-Trimeth lbenzene
108-67-8
8.3
782
20440
2,4,6-Trichloro henol
88-06-2
0.01
10
400
Vinyl acetate
108-05-4
0.36
10000
400000
Vinyl chloride
75-01-4
0.00018
0.46
4.1
X lenes o-, m-, and -; mixed
1330-20-7
4.6
3129
81760
# Health based level > 100%
## considered immobile
46
Rev.
4/16/2012