22074_Gathing Motor_ BAR 20190315

BROWNFIELDS ASSESSMENT REPORT
Former Gathings Motor Company
1100 and 1200 South Tryon Street
Charlotte, North Carolina
Brownfields Project Number 22074-18-060
PREPARED FOR:
Tryon Investors, LLC
Care of Spectrum Development Company, LLC
300 South Tryon Street, Ste. 200
Charlotte, North Carolina 28202
PREPARED BY:
Wood Environment & Infrastructure Solutions, Inc.
2801 Yorkmont Road, Suite 100
Charlotte, North Carolina 28208
March 15, 2019
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
1
TABLE OF CONTENTS
1.0 SITE INFORMATION AND HISTORY..................................................................................2
2.0 ASSESSMENT ACTIVITIES ................................................................................................3
2.1 Brownfields Receptor Survey ..................................................................................................................3
2.2 Soil Sampling and Analysis ......................................................................................................................4
2.3 Soil-Gas Sampling and Analysis .......................................................................................5
2.4 Groundwater Assessment ........................................................................................................................5
3.0 RESULTS ............................................................................................................................6
3.1 Soil ..................................................................................................................................................................6
3.2 Soil-Gas ............................................................................................................................9
3.3 Groundwater ................................................................................................................................................6
4.0 CONCLUSIONS...................................................................................................................6
TABLES
FIGURES
APPENDICES LIST OF TABLES
Table 1 Summary of Monitoring Well Construction and Groundwater Elevation Data
Table 2 Summary of Soil Analytical Results
Table 3 Summary of Soil-Gas Analytical Results
Table 4 Summary of Detected Constituents in Groundwater
LIST OF FIGURES
Figure 1 Site Topo
Figure 2 Receptor Survey Map
Figure 3 Soil Sample Locations
Figure 4 Soil-Gas Sample Locations
Figure 5 Groundwater Sample Locations and Elevations
LIST OF APPENDICES
Appendix A Brownfields Receptor Survey Form
Appendix B Subsurface Investigation Permit (SIP), Boring Logs and Well Records
Appendix C Soil-Gas Field Sheets
Appendix D Monitoring Well Sampling Field Data Sheets
Appendix E Laboratory Analytical Reports and Chain-of-Custody Forms
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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1.0 SITE INFORMATION AND HISTORY
Wood recently completed a Phase I Environmental Site Assessment (ESA) report (dated July 30,
2018). The site consists of four parcels totaling approximately 4.9 acres situated at the
intersection of South Tryon Street and West Carson Boulevard (Figure 1).The Phase I ESA
identified recognized environmental conditions (RECs) in connection with the site including the
following:
Based on regulatory status, Former Gathings Motor Company (UST Incident #40680) is
considered a controlled REC in relation to the subject property.
The former presence of a gasoline station (Top Gas & Oil) and various auto repair
businesses on the site is considered a REC.
Based on the historical use as a gasoline station (Top Gas & Oil) from at least 1958 to
1986, documented groundwater contamination, and the open status of this incident (UST
Incident #40460) is considered a current REC.
Based on available assessment data, Wood developed a proposed scope of assessment work
and presented it to Ms. Carolyn Minnich of the NCDEQ Brownfields Program (BFP)in a written
work plan (dated February 15, 2009).The work plan was approved by the BFP on February 20,
2019.The scope of work outlined in the approved work plan was developed to address the
following “data gaps”:
The direction of shallow groundwater flow across the properties;
Current groundwater quality data across the properties;
Current soil-vapor analytical data within the proposed footprints of the proposed
commercial office buildings and retail areas;
Additional soil quality data in the vicinity of the affected area known as the former Top
Gas & Oil; and,
“Background” metals in soil and groundwater at the properties.
The proposed assessment activities will be performed in general accordance with the most
recent Inactive Hazardous Sites Branch (IHSB) Program Guidelines for Assessment and Cleanup
(http://portal.ncdenr.org/web/wm/sf/ihs/ihsguide), dated October 2015 and the most recent
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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versions of the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem
Support Division (SESD) Field Branches Quality System and Technical Procedures guidance.
2.0 ASSESSMENT ACTIVITIES
2.1 Brownfields Receptor Survey
On March 6, 2019, Wood visited the subject property and surrounding area. Based on
information obtained during this reconnaissance and our previous work at the property, Wood
completed a Brownfields Receptor Survey Form (Appendix A).According to the Mecklenburg
County Well database, no private or public water-supply wells are located within a one-mile
radius of the subject property.During the driving tour receptor survey,Wood did not identify
potential receptors within approximately 1,500 feet of the subject property (Figure 2).
2.2 Soil Sampling and Analysis
Prior to mobilization to the property to advance soil borings,Wood contacted the North
Carolina underground utility location service (811) and arranged for our Subsurface Utility
Engineering (SUE) personnel to visit the site and mark buried objects such as pipes, tanks or
underground utility lines. The purpose of this effort was to minimize the potential for probing
into underground utilities, tanks or lines buried at the subject property.
On February 23, 2019, Wood personnel and Innovative Environmental Technologies, Inc. (IET),
our probing subcontractor licensed in the State of North Carolina, mobilized to the subject
property to advance six soil borings as approved by NCDEQ. Locations of the soil borings are
depicted on Figure 3.IET used a direct-push probe rig to penetrate pavement, if present at each
of the boring locations.A MacroCore®or equivalent sampler was driven into the soil to remove
soil cores from the subsurface. To minimize the potential for cross-contamination between
samples, a new PVC sleeve (tube) was inserted into the sampler for each soil sample interval.On
this date,IET and Wood advanced two soil borings (shown as GP-1 and GP-3 on Figure 3)
within the proposed sediment basins to depths of 14 and 12 feet below ground surface (bgs),
respectively. Three additional soil borings (GP-2, GP-4 and GP-5) were advanced using direct-
push equipment to depths ranging from 12 to 14 feet bgs.One “background” soil boring (BG)
was advanced at the location shown on Figure 3 to a depth of 12 feet bgs to assess naturally-
occurring metals concentrations in the soil at the subject property.
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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In each of the soil borings, representative portions of samples collected at 2-foot intervals
between ground surface and the estimated depth to the water table were removed from the
tube sampler,and placed in two re-sealable plastic bags. Visual and olfactory observations
relative to the soil samples were recorded by our field personnel. The soil types encountered in
the borings were recorded to prepare soil boring logs (Appendix B). One plastic bag from each
interval was placed in a cooler on ice and the other plastic bag from each interval was screened
in the field with a photoionization detector (PID).Because the field screening results ranged
from 3.8 to 6.8 parts per million (ppm), a range indicative of “background” organic vapor
concentrations,two soil samples were collected from each soil boring for analysis. The samples
selected for analysis are summarized in Table 2 and included an “upper” soil sample was
selected for analysis (0 to 2), (2 to 4) or (4 to 6)feet below ground surface (bgs) and a “lower”
soil sample was selected for analysis (6 to 8) or (10 to 12)feet bgs.Soil from the corresponding
plastic bags placed on ice were then placed in laboratory-provided containers, placed in a cooler
on ice and delivered by courier under chain-of-custody protocol to Con-Test Analytical
Laboratory (Con-Test) in East Longmeadow, Massachusetts for analysis. Con-Test is certified by
the State of North Carolina for analysis.
The soil samples collected from the proposed sediment basins borings (GP-1 and GP-3) were
analyzed for volatile organic compounds (VOCs) by EPA Method 8260B, semi-volatile organic
compounds (SVOCs) by EPA Method 8270D,Resource Conservation and Recovery Act (RCRA)
Metals (total) by EPA Methods 6020B/7471B and hexavalent chromium (Method 7199). The soil
samples collected from the monitoring well borings (GP-2, GP-4 and GP-5) were analyzed for
VOCs, SVOCs and RCRA metals (total) by the methods described above. The soil samples
collected from the “background” boring (BG) were analyzed for RCRA Metals (total) by EPA
Method 6020B/7471B and hexavalent chromium (Method 7199).
One field duplicate QA/QC sample (DUP-1) was collected from boring GP-2 (6 to 8 feet bgs) and
also analyzed for VOCs, SVOCs and RCRA metals (total) by the methods described above.
Following the completion of the soil sampling activities, the two sediment basin borings (GP-1
and GP-3)and the “background” boring (BG) were backfilled with native soil to the ground
surface.
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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2.3 Soil-Gas Sampling and Analysis
On February 24, 2019, Wood’s subcontractor IET advanced eight borings to a depth of 5 feet
bgs using a direct-push rig. IET and Wood personnel installed soil-gas sampling points in each
of the borings to a depth of 5 bgs.The soil-gas sampling was performed in general accordance
with the NCDEQ, DWM Vapor Intrusion Guidance, dated February 2018
(https://deq.nc.gov/about/divisions/waste-management/waste-management-permit-
guidance/dwm-vapor-intrusion-guidance).The locations of the eight soil-gas sampling points
are shown on Figure 4 and include four points within the footprint of the office building
planned for the northwest corner of the property. Furthermore, since retail tenant space is
planned for the perimeter of the proposed parking deck (southern portion of the property). Four
soil-gas sampling points were installed in this area. Wood proposed to install the two interior
temporary sub-slab soil-gas sampling points through the concrete floor slab of the existing
office building (1100 S. Tryon Street) to a depth of about six inches beneath the base of the slab.
However,due to tenant occupation on the first floor of the office building, installation of these
sample points was not feasible.
For the eight exterior locations, dedicated sampling points were placed in each open borehole
and connected to Teflon™ tubing extending to the ground surface and attached to 6-liter
Summa®canisters. A sand pack of approximately 8 to 10 inches thick was placed around the
sampling points. The remaining annulus of the boreholes was filled with hydrated bentonite to
the ground surface. Prior to sample collection, each sample train was purged of stagnant air and
a leak-check was performed. The Summa®canisters and sample train were surrounded by a
helium-shroud for leak-check detection.The helium-shroud consisted of plastic container placed
over the Summa®canisters and sample tubing and then filled with helium. A leak test was
performed at each soil-gas point. Wood personnel collected the leak test samples using Tedlar®
bags. Each leak test sample was screened in the field for helium using a MGD-2002 Multi-Gas
leak (di-electric) detector. Wood personnel also used the helium detector to monitor the
concentration of helium inside the shrouds. A leak was considered to have occurred when the
helium concentration inside the Tedlar®bag was greater than 10% of the helium concentration
within the shroud.
Following the leak-check, a soil-gas sample was collected into the Summa®canister at an
approximate flow rate of 200 mL/min (30-min sample time). Following collection of the soil-gas
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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samples, the Summa®canisters were shipped via courier to Con-Test for analysis. The soil-gas
samples were analyzed by Con-Test for analysis of VOCs via EPA Method TO-15. The soil-gas
samples were maintained under chain-of-custody protocol. One field duplicate QA/QC soil-gas
sample (Dup-2) was collected from the sample point SG-2 for analysis by Method TO-15.
Following the collection of the soil-gas samples, the soil-gas points were removed and the
boreholes were abandoned by filling with bentonite to grade.
2.3 Groundwater Assessment
Prior to mobilization to the property to install monitoring wells,Wood obtained a Subsurface
Investigation Permit (SIP) from the Mecklenburg County Health Department (Appendix B).In
2007,Wood (as MACTEC Engineering &Consulting, Inc.) installed two monitoring wells (MW-
OWS and MW-Tank 3)in the southern corner of the property (Figure 5).During preparation of
the work plan, Wood confirmed that one of the wells (MW-Tank 3)is presently covered with a
large steel shipping container (presumably used for storage) situated between the two
remaining structures that occupy Tax Parcel 073-073-06. Wood also verified the presence and
accessibility of well MW-OWS.
On February 23, 2019,Wood’s subcontract probing/drilling crew from IET utilized hollow-stem
augers to enlarge and deepen soil boring GP-2,within the proposed footprint of the office
building planned for the northwest corner of the property to install monitoring well MW-1
(Figure 5). The same equipment and procedure was employed to convert soil boring GP-4 into
monitoring well MW-2 (southwestern portion of the property within the footprint of the
proposed parking structure)and soil boring GP-5 into monitoring well MW-3 (eastern edge of
the existing office building). Monitoring well MW-3 was installed near the former location of the
Top Gas & Oil station that occupied the northeastern corner of the property in the past.Based
on the depth to groundwater measured in each of the boreholes on the drilling date, the wells
were installed to a depth of 23 feet bgs. Well MW-1 was installed with a 10-foot screened
interval and wells MW-2 and MW-3 were installed with a 15-foot screened interval. Wood
personnel examined soil cuttings during drilling to assist in preparing boring/well construction
logs (Appendix B).
At the three monitoring well locations,IET personnel installed two-inch diameter PVC well
screens and risers into the approximate 8-inch diameter boreholes. A filter sand pack was placed
around each well screen to at least two feet above the top of the screened interval. A bentonite
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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seal was placed above the sand pack. Portland cement was mixed and placed in the annulus of
the borehole above the bentonite seal to land surface. A concrete pad (approximately 2 feet by
2 feet) was constructed at each well head. Each well was completed with a steel flush-mounted
manhole cover to allow for vehicular traffic.A locking cap and lock was placed on each well.Soil
cuttings and development/purge water generated during these activities were spread on the
ground surface at the property because evidence of significant impacts was not observed during
the field screening of soil samples.The well construction records are included in Appendix B.
IET personnel developed each of the newly-installed wells by pumping to reduce the turbidity of
the groundwater.
On March 1, 2019,Wood personnel used a survey level and stadia rod to establish the top of
casing elevation (Table 1)of each of the three newly-installed wells and well MW-OWS relative
to known datum elevations (base of curb in the paved parking lot and rim of storm drain
manhole (SDMH) along South Tryon Street as shown on Figure 5).Subsequent water level
measurements taken in each well were used to calculate the groundwater elevation. The
groundwater elevation data for each well was used to evaluate the groundwater flow direction
at the subject properties.
Following development,Wood collected samples of groundwater from each well using low-flow
purging techniques in general accordance with the Environmental Protection Agency (EPA)
Region IV Science and Ecosystem Support Division (SESD) Field Branches Quality System and
Technical Procedures guidance.During purging, groundwater field parameters were collected
using an YSI ProPlus water quality meter with commercially-manufactured flow cell and an HFS
MicroTPI turbidity meter. Groundwater field parameters collected through the flow cell included
pH, specific conductivity, dissolved oxygen, temperature and oxidation reduction potential
(ORP).
Turbidity measurements were collected prior to the groundwater entering the flow cell.Field
sampling data sheets are included as Appendix D.Following completion of purging,
groundwater samples were collected from monitoring wells MW-OWS, MW-1, MW-2 and MW-3
and placed in laboratory-provided containers.The groundwater samples were labeled with a
unique ID and placed in an ice-filled sample cooler and delivered to Con-Test for analysis. The
samples were maintained under chain-of-custody protocol. The groundwater samples were
analyzed for VOCs by EPA Method 8260B and SVOCs by EPA Method 8270D.Two of the
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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groundwater samples (MW-2 and MW-3),were also analyzed for RCRA Metals (total) by EPA
Method 6020B/7471B to establish baseline metals concentrations in the groundwater at the
subject property.One field duplicate QA/QC sample (DUP-3)was collected from well MW-2 and
analyzed for VOCs and SVOCs. A trip blank was analyzed for VOCs.
3.0 RESULTS
3.1 Soil
The constituents detected in the soil samples are summarized in Table 2.A copy of the
laboratory report describing these results is included in Appendix E.The results of the analysis
identified the following:
No detectable concentrations of VOCs were identified in the soil samples.
Analysis of soil sample GP-2 (10-12)identified a concentration (0.21 J mg/kg)of
benzo(a)pyrene that exceeded both the NCDEQ IHSB Residential Health Based and
Protection of Groundwater (PoG)Preliminary Soil Remediation Goals PSRGs for
benzo(a)pyrene.However, the concentration was J-flagged indicating the compound was
detected at a concentration below the reporting limit (lowest calibration standard) and is
considered an estimated value.
Concentrations of total chromium (ranging from 5.7 J to 110 mg/kg) were identified in
the soil samples collected from borings GP-1 through GP-5 which exceeded the NCDEQ
IHSB Residential Health Based and PoG PSRGs for total chromium.In addition,11 of the
total chromium concentrations identified exceeded the Industrial/Commercial Health
Based PSRG for total chromium.However, the total chromium concentrations identified
in background samples BG (2-4) and BG (10-12) also exceeded the NCDEQ IHSB
Industrial/Commercial Health Based, Residential Health Based,and PoG PSRGs. This data
suggests that the total chromium concentrations identified in the soil at the subject
properties are within the range of “naturally-occurring”chromium concentrations.In
addition,according to published literature (see Table 2)the concentrations identified are
within the typical “naturally-occurring” chromium levels in soil in the Piedmont of North
Carolina.
Hexavalent chromium was identified in soil sample GP-1 (0-2) at a concentration of 1.2
mg/kg. This concentration exceeded the Residential Health Based PSRG for hexavalent
chromium. However, no other concentrations of hexavalent chromium were identified in
the five other soil samples (GP-1 (6-8), GP-3 (2-4), GP-3 (10-12), BG (2-4), and BG (10-
12)) tested for hexavalent chromium by EPA Method 7199.
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
9
Concentrations of total arsenic (ranging from 1.5 to 2.7 mg/kg)were identified in soil
samples GP-1 (0-2), GP-2 (4-6), GP-4 (0-2), and GP-5 (2-4) that exceeded the NCDEQ
IHSB Residential Health Based PSRG for arsenic. The total arsenic concentrations
identified in background samples BG (2-4) and BG (10-12) also exceeded the NCDEQ
IHSB Residential Health Based PSRG.This data suggests that the total arsenic
concentrations identified in the soil at the subject properties are within the range of
“naturally-occurring”arsenic concentrations. In addition, according to published
literature (see Table 2) the concentrations identified are within the typical “naturally-
occurring”arsenic levels in soil in the Piedmont of North Carolina.
3.2 Soil-Gas
The constituents detected in the soil-gas samples are summarized in Table 3. A copy of the
laboratory report describing these results is included in Appendix E. The results of the analysis
identified detectable concentrations of various VOCs in the soil-gas samples. However, none of
the concentrations exceeded the DWM Non-Residential Soil-Gas Screening Levels (SGSLs).
3.3 Groundwater
Wood’s evaluation of the February 25,and March 8,2019 groundwater elevation measurements
(Table 1)suggested that the shallow groundwater flows across the site from the west toward
the east. This is not consistent with the topography of the site and surrounding properties.For
this reason, a groundwater contour map was not prepared.Figure 5 shows the topographic
contours of the ground surface. A topographic high or small knoll is shown in the area of the
existing office building sloping toward the northwest, west and southeast. If more groundwater
elevation data points were available, it is Wood’s opinion that the shallow groundwater flow
would be toward the northwest, west and southeast.A summary of groundwater elevations is
included in Table 1, and the February 25th groundwater elevations are shown on Figure 5.The
constituents detected in groundwater are summarized in Table 4.A copy of the laboratory
report describing these results is included in Appendix E. The results of the analysis identified
the following:
Concentrations of benzene,1,2-dichloroethane (1,2-DCA), tert-Butyl Alcohol (TBA),
naphthalene, xylenes (total)and 1-Methylnaphthalene were identified in the
groundwater sample collected from well MW-3 that exceeded their respective North
Carolina Administrative Code, Title 15A, Subchapter 2L, Section .0202, Groundwater
Quality Standard (NC 2L Standard)or Interim Maximum Allowable Concentration
(IMACs).In addition, the concentration of 1,2-DCA identified was J-flagged indicating the
compound was detected at a concentration below the reporting limit (lowest calibration
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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standard) and is considered an estimated value.Historically,1,2-dichloroethane (1,2-
DCA)was used as an anti-knock additive in leaded fuels to scavenge lead from cylinders
and valves.
Concentrations of ethylbenzene, naphthalene, 1,2,4-Trimethylbenzene (1,2,4-TMB),1,3,5-
Trimethylbenzene (1,3,5-TMB)and total xylenes were identified in the groundwater
sample from well MW-3 that exceeded the NCDEQ Residential Vapor Intrusion
Groundwater Screening Levels (GWSLs).In addition, the ethylbenzene and total xylenes
concentrations also exceeded the NCDEQ Vapor Intrusion Non-Residential GWSLs.
A concentration of chloroform was identified in the groundwater sample collected from
well MW-1 that exceeded the NCDEQ Residential Vapor Intrusion GWSL for chloroform.
A concentration of total chromium was identified in the groundwater sample from well
MW-3 that exceeded the NC 2L standard.
4.0 Conclusions
Based on the results of the assessment, Wood concludes the following:
The source of the hexavalent chromium in the soil sample GP-1 (0-2) collected from the
area of the proposed sediment basin in the northern corner of the property is unknown.
This area was historically occupied by residences and a used auto sales business (1960s).
These land uses are not typically associated with hexavalent chromium.
No detectable concentrations of VOCs were identified in the soil samples.
The source of the benzo(a)pyrene identified in soil sample GP-2 (10-12) is unknown.In
addition,the concentration was J-flagged indicating the compound was detected at a
concentration below the reporting limit (lowest calibration standard) and is considered
an estimated value.Furthermore,SVOC concentrations above their respective reporting
limits were not identified in the shallow sample collected from boring GP-2.This area
was historically occupied by residences.
The concentrations of total chromium (ranging from 5.7 J to 110 mg/kg) identified in
nine of the 10 soil samples collected are within the range of “naturally-occurring”
chromium concentrations in this region according to published literature.
The concentrations of total arsenic (ranging from 1.5 to 2.7 mg/kg) identified in soil
samples GP-1 (0-2), GP-2 (4-6), GP-4 (0-2), and GP-5 (2-4)are within the range of
“naturally-occurring”arsenic concentrations in this region according to published
literature.
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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The concentrations of constituents identified in the soil-gas samples did not exceed the
DWM Non-Residential SGSLs.
Analysis of the groundwater sample collected from well MW-3 (vicinity of the former Top
Gas & Oil auto filling station)identified concentrations of petroleum-related
hydrocarbons and total chromium which exceeded their respective NC 2L Standards or
IMACs.These results are consistent with previous assessment work in this portion of the
property. The petroleum release(s) associated with the former Top Gas & Oil auto filling
station has affected soil and groundwater in the eastern portion of the subject property.
A concentration of chloroform was identified in the groundwater sample collected from
well MW-1 that exceeded the NCDEQ Residential Vapor Intrusion GWSL for chloroform.
However, chloroform is a known laboratory contaminant and Wood does not consider
the concentration detected to be indicative of a release.
The results indicate that further evaluation of vapor intrusion or vapor mitigation controls is not
warranted as part of site redevelopment. Management of soil with low levels of SVOCs may be
warranted.An assessment to evaluate soil export options is presently underway.
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
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Tables
Well ID Date Installed TOC Elevation
(ft above MSL)
Constructed
Well Depth
(ft bgs)
Date Measured Depth to Water
(ft below TOC)
Groundwater Elevation
(ft above MSL)
2/25/2019 14.19 732.65
3/8/2019 13.88 732.96
2/25/2019 11.15 734.57
3/8/2019 10.81 734.91
2/25/2019 18.43 731.08
3/8/2019 18.11 731.40
MW-Tank 3 4/10/2007 NM 26 NM NM NM
2/25/2019 17.75 733.02
3/8/2019 17.38 733.39
Notes:Prepared By/Date:RPD 3/5/19
1. TOC = Top of Casing.Checked By/Date:AJF 3/5/19
2. ft = Feet.
3. bgs = Below Ground Surface.
4. NM = Not Measured, well was obstructed at time of measurement.
5. MSL = Mean Sea Level.
6. TOC elevations established by Wood personnel relative to the base of the curb in the center of the parking lot and a storm drain manhole along
South Tryon Street, reported at 748.86 and 747.96 ft above MSL, respectively. The referenced elevations were obtained from the Boundary Survey,
prepared by R.B Pharr & Associates, P.A., dated 5-21-18.
MW-3 1/23/2019 749.51 23
MW-OWS 4/10/2007 750.77 26
MW-1 2/23/2019 746.84 23
MW-2 2/23/2019 745.72 23
Table 1 - Summary of Monitoring Well Construction and Groundwater Elevation Data
Well Construction Details Well Gauging Details
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
Constituent GP-1 (0-2)GP-1 (6-8)GP-2 (4-6)GP-2 (10-12)GP-3 (2-4)GP-3 (10-12)GP-4 (0-2)GP-4 (6-8)GP-5 (2-4)GP-5 (10-12)BG (2-4)BG (10-12)DUP-1
Depth Collected 0-2 6-8 4-6 10-12 2-4 10-12 0-2 6-8 2-4 10-12 2-4 10-12 4-6
Metals (Total)Range Mean
Arsenic 1.5 0.58 1.9 0.59 0.33 0.39 1.5 0.43 2.7 0.47 0.95 1.0 1.4 0.68 3.0 5.8 1.0-40*NE
Barium 100 21 16 76 44 220 16 23 14 160 11 13 13 3100 47000 580 50-1000 356
Cadmium <0.42 <0.41 <0.46 <0.44 <0.38 0.048 J <0.46 <0.43 <0.42 <0.47 <0.38 <0.41 <0.42 14 200 3 0.01-7.0*NE
Chromium 88 13 18 11 26 13 51 10 110 5.7 J 19 22 23 0.31 6.5 3.8 7-300 65
Chromium, Hexavalent 1.2 <0.83 NA NA <0.78 <0.85 NA NA NA NA <0.82 <0.80 NA 0.31 6.5 3.8 NE NE
Lead 5.9 9.5 9.8 12 3.6 4.7 9.2 9.9 12 51 6.0 8.8 8.4 400 800 250 2-200*NE
Mercury 0.40 <0.032 0.023 J <0.035 <0.031 <0.032 0.087 <0.035 0.022 J <0.036 0.029 J 0.016 J 0.045 2.3 9.7 1.0 0.03-0.52 0.121
Selenium 0.26 J 0.090 J 0.38 J <0.97 <0.85 <0.93 0.29 J <0.95 0.38 J <1.0 <0.84 <0.90 <0.92 78 1200 2.1 <0.1-0.8 0.42
Silver 0.080 J 0.015 J 0.024 J 0.019 J 0.029 J 0.025 J 0.027 J 0.011 J 0.049 J 0.025 J 0.028 J 0.032 J 0.042 J 78 1200 3.4 NE NE
Semi-Volatile Organic Compounds (SVOCs)
Benzo(a)anthracene <0.23 <0.22 <0.25 0.20 J <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 1.1 21 0.35
Benzo(a)pyrene <0.23 <0.22 <0.25 0.21 J <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 0.11 2.1 0.12
Benzo(b)fluoranthene <0.23 <0.22 <0.25 0.35 <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 1.1 21 1.2
Benzo(g,h,i)perylene <0.23 <0.22 <0.25 0.18 J <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 NE NE 15600
Chrysene <0.23 <0.22 <0.25 0.31 <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 110 2100 36
Fluoranthene <0.23 <0.22 0.15 J 0.78 <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 480 6000 670
Indeno(1,2,3-cd)pyrene <0.23 <0.22 <0.25 0.20 <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 1.1 21 3.9
Phenanthrene <0.23 <0.22 <0.25 0.41 <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 NE NE 134
Pyrene <0.23 <0.22 <0.25 0.57 <0.21 <0.23 <0.25 <0.23 <0.22 <0.25 NA NA <0.22 360 4500 440
Benzene <0.0022 <0.0025 <0.0027 <0.0023 <0.0028 <0.0020 <0.0026 <0.0023 <0.0022 <0.0027 NA NA <0.0022 1.2 5.4 0.01
Tetrachloroethene <0.0022 <0.0025 <0.0027 <0.0023 <0.0028 <0.0020 <0.0026 <0.0023 <0.0022 <0.0027 NA NA <0.0022 17 82 0.0063
Trichloroethene <0.0022 <0.0025 <0.0027 <0.0023 <0.0028 <0.0020 <0.0026 <0.0023 <0.0022 <0.0027 NA NA <0.0022 0.87 4.0 0.021
Notes:
1. Concentrations shown in milligrams per kilograms (mg/kg) relative to the Reporting Limit (RL).Prepared By/Date:RPD 3/7/19
2. Samples collected on February 23, 2019.Checked By/Date:AJF 3/7/19
3. Depths shown in feet below ground surface (bgs).
4. North Carolina Department of Environmental Quality (NCDEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRG) dated February 2018.
5. Only detections above laboratory reporting limits and J-flagged results are shown.
6. J = Indicates that compound was detected at a concentration below the Reporting Limit (Lowest Calibration standard). Therefore, result is an estimated concentration.
7. NA- Not Analyzed.
8. NE- Not established.
9. Bold font indicates identified concentration exceeded Residential PSRG.
11.Underlined value indicates concentration exceeded Industrial/Commercial PSRG.
13. DUP-1 collected from GP-2 (4-6) location/depth.
(1) Range and mean values for "Background Metals for North Carolina Soils" taken from Elements in North American Soils by Dragun and Chekiri, 2005.
*Typical Range of "Native Soil Concentrations of Various Elements" as taken from The Soil Chemistry of Hazardous Materials, Dragun, James, 1988.
12. Bold font and shaded green cell indicates concentration exceeded Industrial/Commercial and Protection of Groundwater (PoG) PSRG, the concentration is below or within the range of "naturally occurring" metals in soil.
Not Applicable
Regional Background Metals in Soil(1)
NCDEQ IHSB
Residential
Health Based
PSRG
NCDEQ IHSB
Industrial/
Commercial
Health Based
PSRG
NCDEQ IHSB
Protection of
Groundwater
PSRG
Volitile Organic Compounds (VOCs)
Not Applicable
Table 2 - Summary of Soil Analytical Results
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
10. Shaded gray cell indicates concentration exceeded Protection of Groundwater (PoG) PSRG.
Constituent SG-1 SG-2 SG-3 SG-4 SG-5 SG-6 SG-7 SG-8 Dup-2
Date Collected 2/24/2019 2/24/2019 2/24/2019 2/24/2019 2/24/2019 2/24/2019 2/24/2019 2/24/2019 2/24/2019
Acetone 15 J 14 J 17 J 13 J 29 20 J 21 31 20 2,700,000
Benzene 14 3.8 9.3 1.2 9.3 7.6 10 16 1.9 1,600
1,3-Butadiene 9.8 8.7 8.5 3.4 7.0 <1.1 15 12 <0.44 180
2-Butanone (MEK)5.6 J 4.8 J 6.6 J 4.0 J 6.6 J 22 J 7.4 J 8.9 J 5.3 J 440,000
Chloroform 27 110 13 26 <0.98 <2.4 <0.98 5.4 140 530
Cyclohexane <0.69 <0.69 <0.69 <0.69 <0.69 47 <0.69 <0.69 <0.69 530,000
Dichlorodifluoromethane (Freon 12)2.0 4.4 <0.99 <0.99 <0.99 <2.5 <0.99 <0.99 <0.99 8,800
Ethanol 13 J 8.0 J 7.5 J 12 J 7.7 J <38 7.5 J <15 6.8 J NSL
Ethylbenzene 15 0.75 J 9.2 <0.87 13 4.5 10 22 <0.87 4,900
4-Ethyltoluene 9.9 <0.98 4.0 <0.98 9.7 <2.5 8.9 20 <0.98 NSL
Heptane 24 3.9 17 <0.82 17 19 16 22 2.4 35,000
Hexane 27 J <1.2 25 J <28 23 J 64 J 27 J 27 J <28 61,000
2-Hexanone (MBK)<0.82 <0.82 5.1 <0.82 <0.82 <2.0 <0.82 <0.82 <0.82 2,600
Isopropanol <20 <20 <20 <20 <20 4.3 J <20 <20 <20 18,000
Methylene Chloride 2.2 J 16 <6.9 <6.9 0.88 J <17 <6.9 1.8 J 18 53,000
4-Methyl-2-pentanone (MIBK)7.6 4.8 8.4 <0.82 6.8 7.3 5.8 6.5 2.8 260,000
m&p-Xylene 51 2.0 30 <1.7 46 14 37 80 1.6 J 8,800
o-Xylene 16 0.76 J 9.3 <0.87 15 7.9 14 27 0.57 J 8,800
Propene <14 <14 85 <14 <14 <34 <14 <14 <14 260,000
Tetrachloroethylene 35 <1.4 24 <1.4 27 110 23 37 <1.4 3,500
Toluene 130 4.6 85 2.2 97 31 75 160 4.6 440,000
Trichlorofluoromethane (Freon 11)3.4 J 1.9 J 1.9 J 3.0 J 1.8 J <11 1.7 J 2.2 J 2.1 J NSL
1,2,4-Trimethylbenzene 8.7 0.9 J 2.8 <0.98 10 <2.5 11 23 <0.98 5,300
1,3,5-Trimethylbenzene 2.8 <0.98 <0.98 <0.98 3.0 <2.5 3.2 6.6 <0.98 5,300
Notes:Prepared By/Date:RPD 3/5/19
1. Concentrations shown in micrograms per meter cubed (µg/m3)Checked By/Date:DRH 3/5/19
2. DWM Non-Residential SGSLs = Division of Waste Management Non-Residential Soil-Gas Screening Levels, dated February 2018
3. NSL = No screening level established
4. J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
5. Samples analyzed for VOCs via EPA Method TO-15
6. Helium used as leak-check and was added to shroud surrounding the sample train prior to collection the sample. Helium was analyzed in the field using a MGD-2002 Multi-Gas leak (di-electric) detector
7. Values shown as less than (<) reference the reporting limits (RLs)
8. Dup-2 collected from SG-2 location
Table 3: Soil-Gas Analytical Results
DWM Non-Residential
SGSLs
Wood Project: 6228-18-0495
Charlotte, North Carolina
Former Gathings Motor Company
Constituent MW-1 MW-2 MW-3 MW-OWS MW-Tank 3 DUP-3 Trip Blank
NC 2L
Standards/
IMACs
Residential
GWSLs
Non-Residential
GWSLs
Benzene <1.0 <1.0 5.5 <1.0 NS <1.0 <1.0 1 16 69
tert-Butyl Alcohol (TBA)<0.50 <0.50 350 <20 NS <20 <20 10 NSL NSL
sec-Butylbenzene <1.0 <1.0 2.2 J <1.0 NS <1.0 <1.0 70 NSL NSL
Chloroform 23 1.6 J <10 <2.0 NS 1.6 J <2.0 70 8.1 36
1,2-Dichloroethane <1.0 <1.0 1.4 J <1.0 NS <1.0 <1.0 0.4 22 98
Ethylbenzene <1.0 <1.0 150 <1.0 NS <1.0 <1.0 600 35 150
Isopropylbenzene (Cumene)<1.0 <1.0 12 <1.0 NS <1.0 <1.0 70 180 750
p-Isopropyltoluene (p-Cymene)<1.0 <1.0 2.2 J <1.0 NS <1.0 <1.0 25 NSL NSL
Methyl tert-Butyl Ether (MTBE)<1.0 <1.0 7.5 <1.0 NS <1.0 <1.0 20 4,500 20,000
Naphthalene <5.0 <5.0 45 <5.0 NS <5.0 <5.0 6 35 150
n-Propylbenzene <1.0 <1.0 30 <1.0 NS <1.0 <1.0 70 490 2,000
Toluene <1.0 <1.0 110 <1.0 NS <1.0 <1.0 600 3,800 16,000
1,2,4-Trimethylbenzene <1.0 <1.0 150 <1.0 NS <1.0 <1.0 400 50 210
1,3,5-Trimethylbenzene <1.0 <1.0 150 <1.0 NS <1.0 <1.0 400 35 150
Xylenes, total <2.0 <2.0 630 <2.0 NS <2.0 <2.0 500 77 320
1-Methylnaphthalene <5.2 <5.2 19 <5.2 NS <5.3 NA 1 NSL NSL
2-Methylnaphthalene <5.2 <5.2 17 <5.2 NS <5.3 NA 30 NSL NSL
Naphthalene <5.2 <5.2 33 <5.2 NS <5.3 NA 6 35 150
Arsenic NA <0.4 0.54 NA NS NA NA 10 NSL NSL
Barium NA 80 400 NA NS NA NA 700 NSL NSL
Cadmium NA <0.50 0.61 NA NS NA NA 2 NSL NSL
Chromium NA 3.1 50 NA NS NA NA 10 NSL NSL
Lead NA <1.0 0.36 J NA NS NA NA 15 NSL NSL
Mercury NA 0.047 J 0.063 J NA NS NA NA 1 0.18 0.75
Selenium NA <5.0 3.8 J NA NS NA NA 20 NSL NSL
Notes:Prepared By/Date:RPD 3/5/19
1. Concentrations shown in micrograms per liter (µg/L).Checked By/Date:AJF 3/5/19
2. Samples collected on February 25, 2019.
3. Samples analyzed for VOCs, SVOCS and Metals via EPA Method 8260 and 8270, only detections above laboratory reporting limits are shown.
4. NC 2L Standards = North Carolina Administrative Code, Title 15A, Subchapter 2L, Section .0202, Groundwater Quality Standards, dated April 2013.
5. GWSLs = NCDEQ Division of Waste Management, Vapor Intrusion Groundwater Screening Levels, dated February 2018.
6. Bold values exceeded NC 2L Standards.
7. Shaded values exceeded Residential GWSLs.
8. Underlined values exceeded Non-Residential GWSLs.
9. NSL = No Standard Listed.
10. DUP-3 collected at MW-2 location.
11. J = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
12. NA = Not Analyzed.
13. NS = Not Sampled, well obstructed at time of sampling.
14. IMACs = North Carolina Administrative Code, Title 15A, Subchapter 2L, Section 0.0202, Interim Maximum Allowable Concentrations, dated April 2018.
Charlotte, North Carolina
Former Gathings Motor Company
Table 4 - Summary of Detected Constituents in Groundwater
Metals
Semi-Volatile Organic Compounds
Volatile Organic Compounds
Wood Project: 6228-18-0495
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
13
Figures
USGS The National Map: National Boundaries Dataset, National ElevationDataset, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; U.S. Census Bureau - TIGER/Line; HERERoad Data. Data Refreshed July, 2017.
PREPARED BY: LM DATE: 3/12/2019 DATE: 3/12/2019CHECKED BY: RCF
Site Boundary
Document Path: F:\AMEC_Projects\2018\6228-18-0495\MXD\Topo.mxd¯
PROJECT NO: 6228-18-0495 FIGURE NO: 1
SITE TOPOFormer Gathings Motor Company1100-1200 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
0 1,000 2,000500Feet
Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and the GIS User Community
PREPARED BY: LMM CHECKED BY: RCFDATE: 3/6/2019 DATE: 3/6/2019 PROJECT NO.:6228-18-0495 FIGURE NO.:2
RECEPTOR SURVEY MAPFormer Gathings Motor Company1100-1200 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
¯
0 500 1,000250Feet
Parcels
Site Boundary
Creeks/Streams
Buffer (500ft)
Buffer (1,000ft)
Buffer (1,500ft)
Roman Catholic Diocese of Charlotte Pastoral College
PPP)B)BP7 4 8
746
7
5
0
744
742
740
738
752736
754756752754750750750
742
746
750752752
750742748750750
750752
7 5 0 746750750750742
7 5 2
BG
GP-1GP-3
GP-2/MW-1
GP-5/MW-3
GP-4/MW-2
Soil Sample LocationsFormer Gathings Motor Company1100-1200 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
PROJECT NO.:FIGURE NO.:6228-18-0495 3
0 60 12030Feet
¯
LEGEND
)B Sediment Basin Soil Boring Location
P Soil Boring and Monitoring Well Location
P BG = "background" metals soil boring location
2017 Contours (feet)
PPPPPPP
PSG-5
SG-1
SG-2SG-3
SG-4
SG-7
SG-6
SG-8
Soil-Gas Sample LocationsFormer Gathings Motor Company1100-1200 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
PROJECT NO.:FIGURE NO.:6228-18-0495 4
0 60 12030Feet
¯
P Soil-Gas Sample Location (collected February 24, 2019)
LEGEND
Proposed Building Footprint
748
746
75
0
744
742
740
738
752736
754756752754750750750742
746
750752752
75074274875075
0
750752750 746750750 750742
752P
P
P
P
MW-1(732.65)
MW-2(734.57)
MW-3(731.08)
MW-OWS(733.02)
Groundwater Sample Locations and ElevationsFormer Gathings Motor Company1100-1200 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
PROJECT NO.:FIGURE NO.:6228-18-0495 5
¯
Groundwater elevations established by Wood personnel relative to the "benchmarks" shown on this figure.The referenced elevations of the points was obtained from the Boundary Survey prepared by R.B. Pharr & Associates, P.A., dated May 21, 2018.
LEGEND
0 60 12030Feet
E
E
P Approximate Groundwater Monitoring Well LocationGroundwater Elevation (feet) as measured on February 25, 2019Groundwater Contour (feet)Estimated Groundwater Flow Direction
(734.57)
E Approximate locations of "benchmarks" used by Wood to establish top of casing elevations for monitoring wells
MW-Tank 3P
2017 Contours (feet)
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
14
Appendix A
Brownfields Receptor Survey Form
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Former Gathings Motor Company
Address:1100 and 1200 South Tryon Street
City:Charlotte
County:Mecklenburg
Brownfields Project 22074-18-060
Property and Building Characteristics
The four-story office building has a heavy slab foundation, a face brick external wall and was built in 1988.
The single story service garage has a commercial slab foundation, face brick external wall and was built in 1946.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
See Above
The remaining portions of the site are occupied by asphalt-paved parking lots, gravel and crushed brick parking and
landscaped areas.
Surface Conditions
Size of Property (acres)
% of property that is wooded/brush
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as
needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings (e.g.
windows, bay doors), and height (number of stories).
% of property that is covered by buildings
4.9
0%
9%
60%
NA
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated by the
DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed Usage
0%
31%
a. Provide occupancy and use information.
The site is occupied by a four-story approximate 64,294 square foot office building (built in 1988).
One approximate 1,320 square foot brick garage building (built in 1946).
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved or gravel
One approximate 252 square foot small brick office building (built in 1960).
The single story brick office building has a commercial slab foundation, face brick external wall and was built in 1960.
Rev. 09/2015 Page 1 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
Not Applicable
Surrounding Property Land Use
North
South
East
West
N
Y
N
Utilities
Is there a septic system on-site? (Y or N) ___N______
Please provide the utility providers for the subject property
a. Natural Gas Piedmont Natural Gas
b. Sewer City of Charlotte
c. Electricity Duke Energy
d. Other No facilities or utilities presently at property.
See Figure 2
Direction
Is there a basement within 1,000 ft of the Property
Distance
(ft)Address
Zoning/Land Use Proposed Usage Current Use/Occupant
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return,
and design considerations (e.g. positive pressure?).
The office building has forced air-ducted. The service garage and retail building have forced air-not ducted.
Same as Current
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding
areas. If specific receptors are present, please provide addresses of the facilities.
Same as Current
Same as Current
Same as Current
Commercial, Multi-family Residential and Parking Lots
Multi-Family Residential and Commercial
Multi-Family Residential and Commercial
Multi and Single-Family Residential
For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction
material, and diameter of the utilities. In addition, please provide the following information on utilty providers. If
additional assessment is required, the public utility locators should be contacted. This information can then be added to a
site map.
Is a school or daycare center within 1,000 ft of the Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Is there a residence within 1,000 ft of the Property?
Rev. 09/2015 Page 2 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
For surrounding properties, please complete the following table with available information.
Y
Y
N
Y
Y
Y
N
Water Supply
What is the potable water supply for the property? Public __X____ Private ______
N
N
N
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the
subject property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a
windshield survey within 1,500 ft of the property boundaries should be completed to determine if water supply or
irrigation wells may be present. Information from applicable databases can and should be utilized; however, should not be
utilized in lieu of the windshield survey. If multiple wells are present within the requested radius, please provide a map of
the well locations. If needed, please attach a separate table to list all wells. Please note, the PM may opt for a more
extensive water supply well survey if needed.
DirectionUtility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Is a storm water pipe within 100 ft of the Property boundary?
Y/N *Distance
(ft)
Is a sanitary sewer within 100 ft of the Property boundary?
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please
include the water providers name.
Distance
(ft)Direction Address
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
See Utility Survey
Rev. 09/2015 Page 3 of 4
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surface Water & Wetlands
Provide Information regarding Surface Water
and Wetlands
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the
vicinity of the Property.
No
Are there surface water features on the
property? (If yes, please complete a. to d.)
Are there any wetlands present on the
property? If no wetlands on-site, are wetlands
suspected on adjoining properties?
a. Is the water body naturally developed or
man-made?
Response/Comments
unnamed Tributary of Little Sugar Creek
No
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Rev. 09/2015 Page 4 of 4
SPECTRUM
SOUTH TRYON
SPECTRUM
1100 S TRYON ST.
CHARLOTTE, NC 28203
1018203
EXISTING CONDITIONS
N/A
G1.04
12/21/2018 1:36 PM SEAN KAUFMAN N:\_2018\1018203\CAD\CONSTRUCTION DOCUMENTS\8203-PLN_EXISTING CONDITIONS.DWG
AS NOTED

KEY MAP
SEAL
SHEET NUMBER
SHEET TITLE
LANDDESIGN PROJ.#
SCALE
PROJECT
NORTH
NO.DESCRIPTION DATE
REVISION / ISSUANCE
ORIGINAL SHEET SIZE: 24" X 36"
VERT:
HORZ:
CHECKED BY:
DRAWN BY:
DESIGNED BY:
223 NORTH GRAHAM STREET
CHARLOTTE, NC 28202
704.333.0325
WWW.LANDDESIGN.COM
NC ENG. FIRM LICENSE # C-0658
TRYON
S
T
SITE
I-2
7
7MOREH
E
A
D

S
T
MINT
S
T
CAR
SO
N

B
L
V
D
SOUT
H BL
V
D
12/21/2018LAND DEVELOPMENT1
NOT TO SCALE
*FOR REFERENCE ONLY*
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
15
Appendix B
Subsurface Investigation Permit (SIP), Boring Logs and Well Records
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________ 
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

Owner
2/14/2019
70002589
Tryon Investors, LLC
Jason Fish
7043383212
300 S Tryon St Suite 200
Charlotte NC 28202
Wood E&IS
Rob Foster
7043575530
2801 Yorkmont Rd
Charlotte NC 28208
South Tryon Development
07307309
NC
BORING #20
PROJECT #
DATE DRILLED
DRILLING SUB-CONTRACTOR DRILL RIG
Page:1
2/23/2019 WEATHER CONDITIONS 40F, Rain
GP-1 BORING DEPTH (ft)NUMBER OF PAGES 1
6228-18-0495
1
IET AMS PowerProbe
DEPTH
(ft bgs)SAMPLE INFOSOIL DESCRIPTION
Sample 6-8 ft
interval @ 10:30
Sample 0-2 ftinterval @ 10:15
PROJECT NAME Former Gathings Motor Co.
Asphalt
PID
(ppm)
5.0
3
2
Tan, Orange, Red Silty Clay
5
4
5.1
4.8
7
6 Tan, orange, red fine grained sandy silt with clay
9
8
4.7
5.1
11
10 Pink, red fine grained sandy silt with clay
13
12
4.6
3.8
15
14 Stopped soil screening at 14 ft
Wet at 15 ft
SOIL BORING LOG
Log Completed By:AJF
20
Boring terminated at 20 ft
17
16
Pink, orange, black fine grained sandy silt with clay
19
18
BORING #20
PROJECT #
DATE DRILLED
DRILLING SUB-CONTRACTOR DRILL RIG
Page:1Log Completed By:AJF
20
Boring terminated at 20 ft
17
16
19
18
Brown, orange fine grained sandy silt with clay
13
12
Wet at 12 ft
Stopped soil screening at 12 ft
3.8
15
14
Light brown silty clay
9
8
4.7
4.2
11
10
5
4
4.8
5.0
7
6
Light tan fine grained sandy silt with clay
Gravel
PID
(ppm)
5.0
3
2 Light tan silty clay
SOIL BORING LOG
Sample 10-12 ft
interval @ 13:15
Sample 2-4 ftinterval @ 13:00
PROJECT NAME Former Gathings Motor Co.
2/23/2019 WEATHER CONDITIONS 40F, Rain
GP-3 BORING DEPTH (ft)NUMBER OF PAGES 1
6228-18-0495
1
IET AMS PowerProbe
DEPTH
(ft bgs)SAMPLE INFOSOIL DESCRIPTION
BORING #20
PROJECT #
DATE DRILLED
DRILLING SUB-CONTRACTOR DRILL RIG
Page:1Log Completed By:AJF
20
Boring terminated at 20 ft
Dup-1 collected from GP-2 (4-6)
17
16
19
18
Tan, orange silty clay
13
12
4.2
5.1
15
14 Stopped soil screening at 14 ft
Wet at 15 ft
9
8
4.3
4.9
11
10 Tan, dark red/purple fine grained sandy silt with clay
5
4
5.4
4.5
7
6
Asphalt
PID
(ppm)
5.3
3
2
Tan, red fine grained sandy silt with clay
SOIL BORING LOG
Sample 10-12 ft
interval @ 11:15
Sample 4-6 ft
interval @11:00
PROJECT NAME Former Gathings Motor Co.
2/23/2019 WEATHER CONDITIONS 40F, Rain
GP-2 BORING DEPTH (ft)NUMBER OF PAGES 1
6228-18-0495
1
IET AMS PowerProbe
DEPTH
(ft bgs)SAMPLE INFOSOIL DESCRIPTION
BORING #20
PROJECT #
DATE DRILLED
DRILLING SUB-CONTRACTOR DRILL RIG
Page:1Log Completed By:AJF
20
Boring terminated at 20 ft
17
16
19
18
13
12
Stopped soil screening at 12 ft
Red silty clay6.1
15
14
9
8
Wet at 9 ft4.8
6.3
11
10
5
4
6.0
4.2
7
6
PID
(ppm)
6.0
3
2
Red, orange silty clay
SOIL BORING LOG
Sample 6-8 ft
interval @ 14:00
Sample 0-2 ftinterval @13:45
PROJECT NAME Former Gathings Motor Co.
2/23/2019 WEATHER CONDITIONS 40F, Rain
GP-4 BORING DEPTH (ft)NUMBER OF PAGES 1
6228-18-0495
1
IET AMS PowerProbe
DEPTH
(ft bgs)SAMPLE INFOSOIL DESCRIPTION
BORING #20
PROJECT #
DATE DRILLED
DRILLING SUB-CONTRACTOR DRILL RIG
Page:1Log Completed By:AJF
20
Boring terminated at 20 ft
17
16
19
18 Tan, white, orange fine grained sandy silt
13
12
Wet at 13 ft
6.8
15
14 Pink, white sandy silt
9
8
6.2
5.9
11
10
Red, tan fine grained sandy silt
5
4
Red silty clay6.0
6.1
7
6
Tan, red silty clay
PID
(ppm)
5.9
3
2
SOIL BORING LOG
Sample 10-12 ft
interval 14:45
Sample 2-4 ftinterval @ 14:30
PROJECT NAME Former Gathings Motor Co.
2/23/2019 WEATHER CONDITIONS 40F, Rain
GP-5 BORING DEPTH (ft)NUMBER OF PAGES 1
6228-18-0495
1
IET AMS PowerProbe
DEPTH
(ft bgs)SAMPLE INFOSOIL DESCRIPTION
BORING #12
PROJECT #
DATE DRILLED
DRILLING SUB-CONTRACTOR DRILL RIG
Page:1Log Completed By:AJF
13
12
5.0
14
9
8
White/tan sandy silt
5.0
4.9
11
10
5
4
4.6
5.1
7
6
Red/orange silty clay
PID
(ppm)
4.8
3
2
Sample 10-12 ft
interval @ 15:15
Sample 2-4 ftinterval @ 15:00
SOIL BORING PID SCREENING WORKSHEET
PROJECT NAME Former Gathings Motor Co.
2/23/2019 WEATHER CONDITIONS 40F, Rain
BG BORING DEPTH (ft)NUMBER OF PAGES 1
6228-18-0495
1
IET AMS PowerProbe
DEPTH
(ft bgs)SAMPLE INFOSOIL DESCRIPTION
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): □Permanent or □Temporary
7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
SIP # 70002589
2/23/19 MW-1
Spectrum Properties
Winnifred & W. Catherine Sts, Charlotte
Mecklenburg
35 13 11.215 80 51 13.147
23
14
8.5
auger
2/27/19
15 23 silty sand
0 13 2 Sch 40 PVC
13 23 2 0.010 Sch 40 PVC
0
11
3
11
23
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Print Form
pour through augers
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): □Permanent or □Temporary
7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
SIP # 70002589
2/23/19 MW-2
Spectrum Properties
Winnifred & W. Catherine Sts, Charlotte
Mecklenburg
35 13 10.441 80 51 10.613
23
11
8.5
auger
2/27/19
11 23 silty sand
0 8 2 Sch 40 PVC
8 23 2 0.010 Sch 40 PVC
0
3
6
3
6
23
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Print Form
pour through augers
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): □Permanent or □Temporary
7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)
10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:
14. WATER ZONES
FROM TO DESCRIPTION
ft.ft.
ft.ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft.ft.in.
ft.ft.in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft.ft.
ft.ft.
ft.ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft.ft.
ft.ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21. REMARKS
22. Certification:
Signature of Certified Well Contractor Date
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
SIP # 70002589
2/23/19 MW-3
Spectrum Properties
Winnifred & W. Catherine Sts, Charlotte
Mecklenburg
35 13 8.375 80 51 16.056
23
18
8.5
auger
2/27/19
18 23 silty sand
0 8 2 Sch 40 PVC
8 23 2 0.010 Sch 40 PVC
0
3
6
3
6
23
concrete
bentonite
#2 silica sand pour through augers
pour
See Report
Print Form
pour through augers
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
16
Appendix C
Soil-Gas Field Sheets
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
17
Appendix D
Monitoring Well Sampling Field Data Sheets
Brownfields Assessment Report March 15, 2019
Former Gathings Motor Company
Charlotte, North Carolina
Wood Project: 6228-18-0495
18
Appendix E
Laboratory Analytical Reports and Chain-of-Custody Forms
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 5, 2019
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228-18-0485.03
Laboratory Work Order Number: 19B1097
Enclosed are results of analyses for samples received by the laboratory on February 25, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 52
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 8
19B1097-01 8
19B1097-02 12
19B1097-03 17
19B1097-04 22
19B1097-05 26
19B1097-06 30
Sample Preparation Information 32
QC Data 33
Volatile Organic Compounds by GC/MS 33
B224603 33
Semivolatile Organic Compounds by GC/MS 38
B224592 38
Metals Analyses (Total) 43
B224641 43
B224682 43
B224896 43
Flag/Qualifier Summary 45
Certifications 46
Chain of Custody/Sample Receipt 50
Page 2 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/5/2019
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0485.03
19B1097
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
MW-1 19B1097-01 Ground Water SW-846 8260D
SW-846 8270D
MW2 19B1097-02 Ground Water SW-846 6020B
SW-846 7470A
SW-846 8260D
SW-846 8270D
MW-3 19B1097-03 Ground Water SW-846 6020B
SW-846 7470A
SW-846 8260D
SW-846 8270D
TANK OWS 19B1097-04 Ground Water SW-846 8260D
SW-846 8270D
DUP-3 19B1097-05 Ground Water SW-846 8260D
SW-846 8270D
Trip Blank 19B1097-06 Trip Blank Water SW-846 8260D
[TOC_1]Sample Summary[TOC]
Page 3 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 8260D, elevated reporting limits for sample(s) 18B1097-03 due to a high concentration of target compounds.
[TOC_1]Case Narrative[TOC]
Page 4 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 6020B
Qualifications:
Analyte is found in the associated laboratory blank as well as in the sample.
Analyte & Samples(s) Qualified:
B
Chromium
19B1097-02RE1[MW2], B224896-BLK1
Data is not affected by elevated level in laboratory blank since sample result is >10x level found in the blank.
Analyte & Samples(s) Qualified:
B-07
Chromium
19B1097-03RE1[MW-3]
SW-846 7470A
Qualifications:
Analyte is found in the associated laboratory blank as well as in the sample.
Analyte & Samples(s) Qualified:
B
Mercury
19B1097-02[MW2], 19B1097-03[MW-3], B224641-BLK1
SW-846 8260D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Acetone
B224603-BS1, B224603-BSD1
Bromochloromethane
B224603-BS1, B224603-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Bromomethane
19B1097-01[MW-1], 19B1097-02[MW2], 19B1097-03[MW-3], 19B1097-04[TANK OWS], 19B1097-05[DUP-3], 19B1097-06[Trip Blank], B224603-BLK1, B224603-BS1,
B224603-BSD1, S033004-CCV1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19B1097-03[MW-3]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
1,2-Dibromo-3-chloropropane (DBCP)
19B1097-01[MW-1], 19B1097-02[MW2], 19B1097-03[MW-3], 19B1097-04[TANK OWS], 19B1097-05[DUP-3], 19B1097-06[Trip Blank], B224603-BLK1, B224603-BS1,
B224603-BSD1, S033004-CCV1
Naphthalene
19B1097-01[MW-1], 19B1097-02[MW2], 19B1097-03[MW-3], 19B1097-04[TANK OWS], 19B1097-05[DUP-3], 19B1097-06[Trip Blank], B224603-BLK1, B224603-BS1,
B224603-BSD1, S033004-CCV1
Page 5 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
1,1,2-Trichloro-1,2,2-trifluoroethane (F
B224603-BS1, B224603-BSD1, S033004-CCV1
1,1-Dichloropropene
B224603-BS1, B224603-BSD1, S033004-CCV1
Bromochloromethane
B224603-BS1, B224603-BSD1, S033004-CCV1
Carbon Tetrachloride
B224603-BS1, B224603-BSD1, S033004-CCV1
Dichlorodifluoromethane (Freon 12)
B224603-BS1, B224603-BSD1, S033004-CCV1
Trichlorofluoromethane (Freon 11)
B224603-BS1, B224603-BSD1, S033004-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-36
Carbon Disulfide
B224603-BS1, B224603-BSD1, S033004-CCV1
SW-846 8270D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Benzidine
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Benzidine
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
V-04
Benzidine
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1, S033061-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
2,4-Dimethylphenol
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1, S032965-CCV1, S033061-CCV1
2,4-Dinitrophenol
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1, S033061-CCV1
4-Nitroaniline
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1, S032965-CCV1, S033061-CCV1
Benzidine
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1, S032965-CCV1, S033061-CCV1
Hexachlorocyclopentadiene
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1, S033061-CCV1
Page 6 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
S032965-CCV1
3-Nitroaniline
S032965-CCV1
4-Chloroaniline
19B1097-01RE1[MW-1], 19B1097-02RE1[MW2], 19B1097-03RE1[MW-3], 19B1097-04RE1[TANK OWS], 19B1097-05RE1[DUP-3], B224592-BLK1, B224592-BS1,
B224592-BSD1, S032965-CCV1, S033061-CCV1
Aniline
S032965-CCV1
Benzidine
S032965-CCV1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 7 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/25/2019 10:50
[TOC_2]19B1097-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/1/19 2:09 LBDg/L9.7 2/28/19SW-846 8260D1Acetone
ND 5.0 3/1/19 2:09 LBDg/L0.58 2/28/19SW-846 8260D1Acrylonitrile
ND 0.50 3/1/19 2:09 LBDg/L0.11 2/28/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 1.0 3/1/19 2:09 LBDg/L0.12 2/28/19SW-846 8260D1Benzene
ND 1.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D1Bromobenzene
ND 1.0 3/1/19 2:09 LBDg/L0.22 2/28/19SW-846 8260D1Bromochloromethane
ND 0.50 3/1/19 2:09 LBDg/L0.30 2/28/19SW-846 8260D1Bromodichloromethane
ND 1.0 3/1/19 2:09 LBDg/L0.21 2/28/19SW-846 8260D1Bromoform
ND 2.0 3/1/19 2:09 LBDg/L0.94 2/28/19SW-846 8260D1R-05Bromomethane
ND 20 3/1/19 2:09 LBDg/L2.4 2/28/19SW-846 8260D12-Butanone (MEK)
ND 20 3/1/19 2:09 LBDg/L2.2 2/28/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 1.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D1n-Butylbenzene
ND 1.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D1sec-Butylbenzene
ND 1.0 3/1/19 2:09 LBDg/L0.12 2/28/19SW-846 8260D1tert-Butylbenzene
ND 0.50 3/1/19 2:09 LBDg/L0.095 2/28/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 4.0 3/1/19 2:09 LBDg/L1.0 2/28/19SW-846 8260D1Carbon Disulfide
ND 5.0 3/1/19 2:09 LBDg/L0.25 2/28/19SW-846 8260D1Carbon Tetrachloride
ND 1.0 3/1/19 2:09 LBDg/L0.16 2/28/19SW-846 8260D1Chlorobenzene
ND 0.50 3/1/19 2:09 LBDg/L0.10 2/28/19SW-846 8260D1Chlorodibromomethane
ND 2.0 3/1/19 2:09 LBDg/L0.28 2/28/19SW-846 8260D1Chloroethane
23 2.0 3/1/19 2:09 LBDg/L0.22 2/28/19SW-846 8260D1Chloroform
ND 2.0 3/1/19 2:09 LBDg/L0.55 2/28/19SW-846 8260D1Chloromethane
ND 1.0 3/1/19 2:09 LBDg/L0.12 2/28/19SW-846 8260D12-Chlorotoluene
ND 1.0 3/1/19 2:09 LBDg/L0.14 2/28/19SW-846 8260D14-Chlorotoluene
ND 5.0 3/1/19 2:09 LBDg/L0.37 2/28/19SW-846 8260D1V-051,2-Dibromo-3-chloropropane (DBCP)
ND 0.50 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 1.0 3/1/19 2:09 LBDg/L0.16 2/28/19SW-846 8260D1Dibromomethane
ND 1.0 3/1/19 2:09 LBDg/L0.17 2/28/19SW-846 8260D11,2-Dichlorobenzene
ND 1.0 3/1/19 2:09 LBDg/L0.17 2/28/19SW-846 8260D11,3-Dichlorobenzene
ND 1.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D11,4-Dichlorobenzene
ND 2.0 3/1/19 2:09 LBDg/L0.31 2/28/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 2.0 3/1/19 2:09 LBDg/L0.28 2/28/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/1/19 2:09 LBDg/L0.16 2/28/19SW-846 8260D11,1-Dichloroethane
ND 1.0 3/1/19 2:09 LBDg/L0.19 2/28/19SW-846 8260D11,2-Dichloroethane
ND 1.0 3/1/19 2:09 LBDg/L0.21 2/28/19SW-846 8260D11,1-Dichloroethylene
ND 1.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 1.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 1.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D11,2-Dichloropropane
ND 0.50 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D11,3-Dichloropropane
ND 1.0 3/1/19 2:09 LBDg/L0.21 2/28/19SW-846 8260D12,2-Dichloropropane
ND 2.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D11,1-Dichloropropene
ND 0.50 3/1/19 2:09 LBDg/L0.12 2/28/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.50 3/1/19 2:09 LBDg/L0.11 2/28/19SW-846 8260D1trans-1,3-Dichloropropene
ND 2.0 3/1/19 2:09 LBDg/L0.22 2/28/19SW-846 8260D1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 8 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/25/2019 10:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/1/19 2:09 LBDg/L0.18 2/28/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 50 3/1/19 2:09 LBDg/L26 2/28/19SW-846 8260D11,4-Dioxane
ND 1.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D1Ethylbenzene
ND 1.0 3/1/19 2:09 LBDg/L0.59 2/28/19SW-846 8260D1Hexachlorobutadiene
ND 10 3/1/19 2:09 LBDg/L1.5 2/28/19SW-846 8260D12-Hexanone (MBK)
ND 1.0 3/1/19 2:09 LBDg/L0.12 2/28/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 1.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 1.0 3/1/19 2:09 LBDg/L0.090 2/28/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/1/19 2:09 LBDg/L3.2 2/28/19SW-846 8260D1Methylene Chloride
ND 10 3/1/19 2:09 LBDg/L1.5 2/28/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 5.0 3/1/19 2:09 LBDg/L0.12 2/28/19SW-846 8260D1V-05Naphthalene
ND 1.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D1n-Propylbenzene
ND 1.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D1Styrene
ND 1.0 3/1/19 2:09 LBDg/L0.12 2/28/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.50 3/1/19 2:09 LBDg/L0.16 2/28/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 1.0 3/1/19 2:09 LBDg/L0.27 2/28/19SW-846 8260D1Tetrachloroethylene
ND 10 3/1/19 2:09 LBDg/L1.1 2/28/19SW-846 8260D1Tetrahydrofuran
ND 1.0 3/1/19 2:09 LBDg/L0.17 2/28/19SW-846 8260D1Toluene
ND 5.0 3/1/19 2:09 LBDg/L0.14 2/28/19SW-846 8260D11,2,3-Trichlorobenzene
ND 1.0 3/1/19 2:09 LBDg/L0.19 2/28/19SW-846 8260D11,2,4-Trichlorobenzene
ND 1.0 3/1/19 2:09 LBDg/L0.17 2/28/19SW-846 8260D11,3,5-Trichlorobenzene
ND 1.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D11,1,1-Trichloroethane
ND 1.0 3/1/19 2:09 LBDg/L0.24 2/28/19SW-846 8260D11,1,2-Trichloroethane
ND 1.0 3/1/19 2:09 LBDg/L0.20 2/28/19SW-846 8260D1Trichloroethylene
ND 2.0 3/1/19 2:09 LBDg/L0.15 2/28/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 2.0 3/1/19 2:09 LBDg/L0.22 2/28/19SW-846 8260D11,2,3-Trichloropropane
ND 1.0 3/1/19 2:09 LBDg/L0.20 2/28/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 1.0 3/1/19 2:09 LBDg/L0.18 2/28/19SW-846 8260D11,2,4-Trimethylbenzene
ND 1.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D11,3,5-Trimethylbenzene
ND 2.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D1Vinyl Chloride
ND 2.0 3/1/19 2:09 LBDg/L0.26 2/28/19SW-846 8260D1m+p Xylene
ND 1.0 3/1/19 2:09 LBDg/L0.13 2/28/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.7 3/1/19 2:0970-130
Toluene-d8 101 3/1/19 2:0970-130
4-Bromofluorobenzene 103 3/1/19 2:0970-130
Page 9 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/25/2019 10:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 15:58 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthene
ND 5.2 3/2/19 15:58 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthylene
ND 10 3/2/19 15:58 BGLg/L3.1 2/28/19SW-846 8270D1Acetophenone
ND 5.2 3/2/19 15:58 BGLg/L3.8 2/28/19SW-846 8270D1Aniline
ND 5.2 3/2/19 15:58 BGLg/L2.8 2/28/19SW-846 8270D1Anthracene
ND 21 3/2/19 15:58 BGLg/L12 2/28/19SW-846 8270D1L-04, R-05, V-04,
V-05
Benzidine
ND 5.2 3/2/19 15:58 BGLg/L2.4 2/28/19SW-846 8270D1Benzo(a)anthracene
ND 5.2 3/2/19 15:58 BGLg/L2.5 2/28/19SW-846 8270D1Benzo(a)pyrene
ND 5.2 3/2/19 15:58 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(b)fluoranthene
ND 5.2 3/2/19 15:58 BGLg/L3.5 2/28/19SW-846 8270D1Benzo(g,h,i)perylene
ND 5.2 3/2/19 15:58 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(k)fluoranthene
ND 10 3/2/19 15:58 BGLg/L9.1 2/28/19SW-846 8270D1Benzoic Acid
ND 10 3/2/19 15:58 BGLg/L2.6 2/28/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 10 3/2/19 15:58 BGLg/L3.2 2/28/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 10 3/2/19 15:58 BGLg/L2.7 2/28/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 10 3/2/19 15:58 BGLg/L1.9 2/28/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 10 3/2/19 15:58 BGLg/L3.5 2/28/19SW-846 8270D14-Bromophenylphenylether
ND 10 3/2/19 15:58 BGLg/L2.3 2/28/19SW-846 8270D1Butylbenzylphthalate
ND 10 3/2/19 15:58 BGLg/L2.8 2/28/19SW-846 8270D1Carbazole
ND 10 3/2/19 15:58 BGLg/L2.3 2/28/19SW-846 8270D1V-344-Chloroaniline
ND 10 3/2/19 15:58 BGLg/L1.6 2/28/19SW-846 8270D14-Chloro-3-methylphenol
ND 10 3/2/19 15:58 BGLg/L2.9 2/28/19SW-846 8270D12-Chloronaphthalene
ND 10 3/2/19 15:58 BGLg/L2.1 2/28/19SW-846 8270D12-Chlorophenol
ND 10 3/2/19 15:58 BGLg/L2.5 2/28/19SW-846 8270D14-Chlorophenylphenylether
ND 5.2 3/2/19 15:58 BGLg/L2.5 2/28/19SW-846 8270D1Chrysene
ND 5.2 3/2/19 15:58 BGLg/L3.2 2/28/19SW-846 8270D1Dibenz(a,h)anthracene
ND 5.2 3/2/19 15:58 BGLg/L2.6 2/28/19SW-846 8270D1Dibenzofuran
ND 10 3/2/19 15:58 BGLg/L2.2 2/28/19SW-846 8270D1Di-n-butylphthalate
ND 5.2 3/2/19 15:58 BGLg/L1.9 2/28/19SW-846 8270D11,2-Dichlorobenzene
ND 5.2 3/2/19 15:58 BGLg/L1.9 2/28/19SW-846 8270D11,3-Dichlorobenzene
ND 5.2 3/2/19 15:58 BGLg/L2.1 2/28/19SW-846 8270D11,4-Dichlorobenzene
ND 10 3/2/19 15:58 BGLg/L3.6 2/28/19SW-846 8270D13,3-Dichlorobenzidine
ND 10 3/2/19 15:58 BGLg/L2.0 2/28/19SW-846 8270D12,4-Dichlorophenol
ND 10 3/2/19 15:58 BGLg/L1.8 2/28/19SW-846 8270D1Diethylphthalate
ND 10 3/2/19 15:58 BGLg/L3.6 2/28/19SW-846 8270D1V-052,4-Dimethylphenol
ND 10 3/2/19 15:58 BGLg/L1.8 2/28/19SW-846 8270D1Dimethylphthalate
ND 10 3/2/19 15:58 BGLg/L7.9 2/28/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 10 3/2/19 15:58 BGLg/L8.1 2/28/19SW-846 8270D1V-052,4-Dinitrophenol
ND 10 3/2/19 15:58 BGLg/L1.8 2/28/19SW-846 8270D12,4-Dinitrotoluene
ND 10 3/2/19 15:58 BGLg/L1.8 2/28/19SW-846 8270D12,6-Dinitrotoluene
ND 10 3/2/19 15:58 BGLg/L3.0 2/28/19SW-846 8270D1Di-n-octylphthalate
ND 10 3/2/19 15:58 BGLg/L5.4 2/28/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 5.2 3/2/19 15:58 BGLg/L2.4 2/28/19SW-846 8270D1Fluoranthene
Page 10 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-01
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 2/25/2019 10:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 15:58 BGLg/L2.5 2/28/19SW-846 8270D1Fluorene
ND 10 3/2/19 15:58 BGLg/L3.1 2/28/19SW-846 8270D1Hexachlorobenzene
ND 10 3/2/19 15:58 BGLg/L1.8 2/28/19SW-846 8270D1Hexachlorobutadiene
ND 10 3/2/19 15:58 BGLg/L8.4 2/28/19SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 10 3/2/19 15:58 BGLg/L1.9 2/28/19SW-846 8270D1Hexachloroethane
ND 5.2 3/2/19 15:58 BGLg/L3.8 2/28/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 10 3/2/19 15:58 BGLg/L2.2 2/28/19SW-846 8270D1Isophorone
ND 5.2 3/2/19 15:58 BGLg/L3.0 2/28/19SW-846 8270D11-Methylnaphthalene
ND 5.2 3/2/19 15:58 BGLg/L2.7 2/28/19SW-846 8270D12-Methylnaphthalene
ND 10 3/2/19 15:58 BGLg/L2.2 2/28/19SW-846 8270D12-Methylphenol
ND 10 3/2/19 15:58 BGLg/L2.2 2/28/19SW-846 8270D13/4-Methylphenol
ND 5.2 3/2/19 15:58 BGLg/L2.7 2/28/19SW-846 8270D1Naphthalene
ND 10 3/2/19 15:58 BGLg/L3.7 2/28/19SW-846 8270D12-Nitroaniline
ND 10 3/2/19 15:58 BGLg/L1.7 2/28/19SW-846 8270D13-Nitroaniline
ND 10 3/2/19 15:58 BGLg/L1.7 2/28/19SW-846 8270D1V-054-Nitroaniline
ND 10 3/2/19 15:58 BGLg/L2.2 2/28/19SW-846 8270D1Nitrobenzene
ND 10 3/2/19 15:58 BGLg/L2.1 2/28/19SW-846 8270D12-Nitrophenol
ND 10 3/2/19 15:58 BGLg/L3.9 2/28/19SW-846 8270D14-Nitrophenol
ND 10 3/2/19 15:58 BGLg/L3.3 2/28/19SW-846 8270D1N-Nitrosodimethylamine
ND 10 3/2/19 15:58 BGLg/L6.4 2/28/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 10 3/2/19 15:58 BGLg/L3.1 2/28/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 10 3/2/19 15:58 BGLg/L5.2 2/28/19SW-846 8270D1Pentachloronitrobenzene
ND 10 3/2/19 15:58 BGLg/L8.3 2/28/19SW-846 8270D1Pentachlorophenol
ND 5.2 3/2/19 15:58 BGLg/L2.8 2/28/19SW-846 8270D1Phenanthrene
ND 10 3/2/19 15:58 BGLg/L3.2 2/28/19SW-846 8270D1Phenol
ND 5.2 3/2/19 15:58 BGLg/L3.6 2/28/19SW-846 8270D1Pyrene
ND 5.2 3/2/19 15:58 BGLg/L3.3 2/28/19SW-846 8270D1Pyridine
ND 10 3/2/19 15:58 BGLg/L2.2 2/28/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 5.2 3/2/19 15:58 BGLg/L2.0 2/28/19SW-846 8270D11,2,4-Trichlorobenzene
ND 10 3/2/19 15:58 BGLg/L1.9 2/28/19SW-846 8270D12,4,5-Trichlorophenol
ND 10 3/2/19 15:58 BGLg/L2.1 2/28/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 35.9 3/2/19 15:5815-110
Phenol-d6 27.0 3/2/19 15:5815-110
Nitrobenzene-d5 54.9 3/2/19 15:5830-130
2-Fluorobiphenyl 60.3 3/2/19 15:5830-130
2,4,6-Tribromophenol 78.3 3/2/19 15:5815-110
p-Terphenyl-d14 88.0 3/2/19 15:5830-130
Page 11 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-02
Field Sample #: MW2
Sample Matrix: Ground Water
Sampled: 2/25/2019 14:30
[TOC_2]19B1097-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/1/19 2:40 LBDg/L9.7 2/28/19SW-846 8260D1Acetone
ND 5.0 3/1/19 2:40 LBDg/L0.58 2/28/19SW-846 8260D1Acrylonitrile
ND 0.50 3/1/19 2:40 LBDg/L0.11 2/28/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 1.0 3/1/19 2:40 LBDg/L0.12 2/28/19SW-846 8260D1Benzene
ND 1.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D1Bromobenzene
ND 1.0 3/1/19 2:40 LBDg/L0.22 2/28/19SW-846 8260D1Bromochloromethane
ND 0.50 3/1/19 2:40 LBDg/L0.30 2/28/19SW-846 8260D1Bromodichloromethane
ND 1.0 3/1/19 2:40 LBDg/L0.21 2/28/19SW-846 8260D1Bromoform
ND 2.0 3/1/19 2:40 LBDg/L0.94 2/28/19SW-846 8260D1R-05Bromomethane
ND 20 3/1/19 2:40 LBDg/L2.4 2/28/19SW-846 8260D12-Butanone (MEK)
ND 20 3/1/19 2:40 LBDg/L2.2 2/28/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 1.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D1n-Butylbenzene
ND 1.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D1sec-Butylbenzene
ND 1.0 3/1/19 2:40 LBDg/L0.12 2/28/19SW-846 8260D1tert-Butylbenzene
ND 0.50 3/1/19 2:40 LBDg/L0.095 2/28/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 4.0 3/1/19 2:40 LBDg/L1.0 2/28/19SW-846 8260D1Carbon Disulfide
ND 5.0 3/1/19 2:40 LBDg/L0.25 2/28/19SW-846 8260D1Carbon Tetrachloride
ND 1.0 3/1/19 2:40 LBDg/L0.16 2/28/19SW-846 8260D1Chlorobenzene
ND 0.50 3/1/19 2:40 LBDg/L0.10 2/28/19SW-846 8260D1Chlorodibromomethane
ND 2.0 3/1/19 2:40 LBDg/L0.28 2/28/19SW-846 8260D1Chloroethane
1.6 2.0 3/1/19 2:40 LBDg/L0.22 2/28/19SW-846 8260D1JChloroform
ND 2.0 3/1/19 2:40 LBDg/L0.55 2/28/19SW-846 8260D1Chloromethane
ND 1.0 3/1/19 2:40 LBDg/L0.12 2/28/19SW-846 8260D12-Chlorotoluene
ND 1.0 3/1/19 2:40 LBDg/L0.14 2/28/19SW-846 8260D14-Chlorotoluene
ND 5.0 3/1/19 2:40 LBDg/L0.37 2/28/19SW-846 8260D1V-051,2-Dibromo-3-chloropropane (DBCP)
ND 0.50 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 1.0 3/1/19 2:40 LBDg/L0.16 2/28/19SW-846 8260D1Dibromomethane
ND 1.0 3/1/19 2:40 LBDg/L0.17 2/28/19SW-846 8260D11,2-Dichlorobenzene
ND 1.0 3/1/19 2:40 LBDg/L0.17 2/28/19SW-846 8260D11,3-Dichlorobenzene
ND 1.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D11,4-Dichlorobenzene
ND 2.0 3/1/19 2:40 LBDg/L0.31 2/28/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 2.0 3/1/19 2:40 LBDg/L0.28 2/28/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/1/19 2:40 LBDg/L0.16 2/28/19SW-846 8260D11,1-Dichloroethane
ND 1.0 3/1/19 2:40 LBDg/L0.19 2/28/19SW-846 8260D11,2-Dichloroethane
ND 1.0 3/1/19 2:40 LBDg/L0.21 2/28/19SW-846 8260D11,1-Dichloroethylene
ND 1.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 1.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 1.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D11,2-Dichloropropane
ND 0.50 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D11,3-Dichloropropane
ND 1.0 3/1/19 2:40 LBDg/L0.21 2/28/19SW-846 8260D12,2-Dichloropropane
ND 2.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D11,1-Dichloropropene
ND 0.50 3/1/19 2:40 LBDg/L0.12 2/28/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.50 3/1/19 2:40 LBDg/L0.11 2/28/19SW-846 8260D1trans-1,3-Dichloropropene
ND 2.0 3/1/19 2:40 LBDg/L0.22 2/28/19SW-846 8260D1Diethyl Ether
Page 12 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-02
Field Sample #: MW2
Sample Matrix: Ground Water
Sampled: 2/25/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/1/19 2:40 LBDg/L0.18 2/28/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 50 3/1/19 2:40 LBDg/L26 2/28/19SW-846 8260D11,4-Dioxane
ND 1.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D1Ethylbenzene
ND 1.0 3/1/19 2:40 LBDg/L0.59 2/28/19SW-846 8260D1Hexachlorobutadiene
ND 10 3/1/19 2:40 LBDg/L1.5 2/28/19SW-846 8260D12-Hexanone (MBK)
ND 1.0 3/1/19 2:40 LBDg/L0.12 2/28/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 1.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 1.0 3/1/19 2:40 LBDg/L0.090 2/28/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/1/19 2:40 LBDg/L3.2 2/28/19SW-846 8260D1Methylene Chloride
ND 10 3/1/19 2:40 LBDg/L1.5 2/28/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 5.0 3/1/19 2:40 LBDg/L0.12 2/28/19SW-846 8260D1V-05Naphthalene
ND 1.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D1n-Propylbenzene
ND 1.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D1Styrene
ND 1.0 3/1/19 2:40 LBDg/L0.12 2/28/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.50 3/1/19 2:40 LBDg/L0.16 2/28/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 1.0 3/1/19 2:40 LBDg/L0.27 2/28/19SW-846 8260D1Tetrachloroethylene
ND 10 3/1/19 2:40 LBDg/L1.1 2/28/19SW-846 8260D1Tetrahydrofuran
ND 1.0 3/1/19 2:40 LBDg/L0.17 2/28/19SW-846 8260D1Toluene
ND 5.0 3/1/19 2:40 LBDg/L0.14 2/28/19SW-846 8260D11,2,3-Trichlorobenzene
ND 1.0 3/1/19 2:40 LBDg/L0.19 2/28/19SW-846 8260D11,2,4-Trichlorobenzene
ND 1.0 3/1/19 2:40 LBDg/L0.17 2/28/19SW-846 8260D11,3,5-Trichlorobenzene
ND 1.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D11,1,1-Trichloroethane
ND 1.0 3/1/19 2:40 LBDg/L0.24 2/28/19SW-846 8260D11,1,2-Trichloroethane
ND 1.0 3/1/19 2:40 LBDg/L0.20 2/28/19SW-846 8260D1Trichloroethylene
ND 2.0 3/1/19 2:40 LBDg/L0.15 2/28/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 2.0 3/1/19 2:40 LBDg/L0.22 2/28/19SW-846 8260D11,2,3-Trichloropropane
ND 1.0 3/1/19 2:40 LBDg/L0.20 2/28/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 1.0 3/1/19 2:40 LBDg/L0.18 2/28/19SW-846 8260D11,2,4-Trimethylbenzene
ND 1.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D11,3,5-Trimethylbenzene
ND 2.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D1Vinyl Chloride
ND 2.0 3/1/19 2:40 LBDg/L0.26 2/28/19SW-846 8260D1m+p Xylene
ND 1.0 3/1/19 2:40 LBDg/L0.13 2/28/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.0 3/1/19 2:4070-130
Toluene-d8 101 3/1/19 2:4070-130
4-Bromofluorobenzene 104 3/1/19 2:4070-130
Page 13 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-02
Field Sample #: MW2
Sample Matrix: Ground Water
Sampled: 2/25/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 16:24 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthene
ND 5.2 3/2/19 16:24 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthylene
ND 10 3/2/19 16:24 BGLg/L3.1 2/28/19SW-846 8270D1Acetophenone
ND 5.2 3/2/19 16:24 BGLg/L3.8 2/28/19SW-846 8270D1Aniline
ND 5.2 3/2/19 16:24 BGLg/L2.8 2/28/19SW-846 8270D1Anthracene
ND 21 3/2/19 16:24 BGLg/L12 2/28/19SW-846 8270D1L-04, R-05, V-04,
V-05
Benzidine
ND 5.2 3/2/19 16:24 BGLg/L2.4 2/28/19SW-846 8270D1Benzo(a)anthracene
ND 5.2 3/2/19 16:24 BGLg/L2.5 2/28/19SW-846 8270D1Benzo(a)pyrene
ND 5.2 3/2/19 16:24 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(b)fluoranthene
ND 5.2 3/2/19 16:24 BGLg/L3.5 2/28/19SW-846 8270D1Benzo(g,h,i)perylene
ND 5.2 3/2/19 16:24 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(k)fluoranthene
ND 10 3/2/19 16:24 BGLg/L9.1 2/28/19SW-846 8270D1Benzoic Acid
ND 10 3/2/19 16:24 BGLg/L2.6 2/28/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 10 3/2/19 16:24 BGLg/L3.2 2/28/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 10 3/2/19 16:24 BGLg/L2.7 2/28/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 10 3/2/19 16:24 BGLg/L1.9 2/28/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 10 3/2/19 16:24 BGLg/L3.5 2/28/19SW-846 8270D14-Bromophenylphenylether
ND 10 3/2/19 16:24 BGLg/L2.3 2/28/19SW-846 8270D1Butylbenzylphthalate
ND 10 3/2/19 16:24 BGLg/L2.8 2/28/19SW-846 8270D1Carbazole
ND 10 3/2/19 16:24 BGLg/L2.3 2/28/19SW-846 8270D1V-344-Chloroaniline
ND 10 3/2/19 16:24 BGLg/L1.6 2/28/19SW-846 8270D14-Chloro-3-methylphenol
ND 10 3/2/19 16:24 BGLg/L2.9 2/28/19SW-846 8270D12-Chloronaphthalene
ND 10 3/2/19 16:24 BGLg/L2.1 2/28/19SW-846 8270D12-Chlorophenol
ND 10 3/2/19 16:24 BGLg/L2.5 2/28/19SW-846 8270D14-Chlorophenylphenylether
ND 5.2 3/2/19 16:24 BGLg/L2.5 2/28/19SW-846 8270D1Chrysene
ND 5.2 3/2/19 16:24 BGLg/L3.2 2/28/19SW-846 8270D1Dibenz(a,h)anthracene
ND 5.2 3/2/19 16:24 BGLg/L2.6 2/28/19SW-846 8270D1Dibenzofuran
ND 10 3/2/19 16:24 BGLg/L2.2 2/28/19SW-846 8270D1Di-n-butylphthalate
ND 5.2 3/2/19 16:24 BGLg/L1.9 2/28/19SW-846 8270D11,2-Dichlorobenzene
ND 5.2 3/2/19 16:24 BGLg/L1.9 2/28/19SW-846 8270D11,3-Dichlorobenzene
ND 5.2 3/2/19 16:24 BGLg/L2.1 2/28/19SW-846 8270D11,4-Dichlorobenzene
ND 10 3/2/19 16:24 BGLg/L3.6 2/28/19SW-846 8270D13,3-Dichlorobenzidine
ND 10 3/2/19 16:24 BGLg/L2.0 2/28/19SW-846 8270D12,4-Dichlorophenol
ND 10 3/2/19 16:24 BGLg/L1.8 2/28/19SW-846 8270D1Diethylphthalate
ND 10 3/2/19 16:24 BGLg/L3.6 2/28/19SW-846 8270D1V-052,4-Dimethylphenol
ND 10 3/2/19 16:24 BGLg/L1.8 2/28/19SW-846 8270D1Dimethylphthalate
ND 10 3/2/19 16:24 BGLg/L7.9 2/28/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 10 3/2/19 16:24 BGLg/L8.1 2/28/19SW-846 8270D1V-052,4-Dinitrophenol
ND 10 3/2/19 16:24 BGLg/L1.8 2/28/19SW-846 8270D12,4-Dinitrotoluene
ND 10 3/2/19 16:24 BGLg/L1.8 2/28/19SW-846 8270D12,6-Dinitrotoluene
ND 10 3/2/19 16:24 BGLg/L3.0 2/28/19SW-846 8270D1Di-n-octylphthalate
ND 10 3/2/19 16:24 BGLg/L5.4 2/28/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 5.2 3/2/19 16:24 BGLg/L2.4 2/28/19SW-846 8270D1Fluoranthene
Page 14 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-02
Field Sample #: MW2
Sample Matrix: Ground Water
Sampled: 2/25/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 16:24 BGLg/L2.5 2/28/19SW-846 8270D1Fluorene
ND 10 3/2/19 16:24 BGLg/L3.1 2/28/19SW-846 8270D1Hexachlorobenzene
ND 10 3/2/19 16:24 BGLg/L1.8 2/28/19SW-846 8270D1Hexachlorobutadiene
ND 10 3/2/19 16:24 BGLg/L8.4 2/28/19SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 10 3/2/19 16:24 BGLg/L1.9 2/28/19SW-846 8270D1Hexachloroethane
ND 5.2 3/2/19 16:24 BGLg/L3.8 2/28/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 10 3/2/19 16:24 BGLg/L2.2 2/28/19SW-846 8270D1Isophorone
ND 5.2 3/2/19 16:24 BGLg/L3.0 2/28/19SW-846 8270D11-Methylnaphthalene
ND 5.2 3/2/19 16:24 BGLg/L2.7 2/28/19SW-846 8270D12-Methylnaphthalene
ND 10 3/2/19 16:24 BGLg/L2.2 2/28/19SW-846 8270D12-Methylphenol
ND 10 3/2/19 16:24 BGLg/L2.2 2/28/19SW-846 8270D13/4-Methylphenol
ND 5.2 3/2/19 16:24 BGLg/L2.7 2/28/19SW-846 8270D1Naphthalene
ND 10 3/2/19 16:24 BGLg/L3.7 2/28/19SW-846 8270D12-Nitroaniline
ND 10 3/2/19 16:24 BGLg/L1.7 2/28/19SW-846 8270D13-Nitroaniline
ND 10 3/2/19 16:24 BGLg/L1.7 2/28/19SW-846 8270D1V-054-Nitroaniline
ND 10 3/2/19 16:24 BGLg/L2.2 2/28/19SW-846 8270D1Nitrobenzene
ND 10 3/2/19 16:24 BGLg/L2.1 2/28/19SW-846 8270D12-Nitrophenol
ND 10 3/2/19 16:24 BGLg/L3.9 2/28/19SW-846 8270D14-Nitrophenol
ND 10 3/2/19 16:24 BGLg/L3.3 2/28/19SW-846 8270D1N-Nitrosodimethylamine
ND 10 3/2/19 16:24 BGLg/L6.4 2/28/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 10 3/2/19 16:24 BGLg/L3.1 2/28/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 10 3/2/19 16:24 BGLg/L5.2 2/28/19SW-846 8270D1Pentachloronitrobenzene
ND 10 3/2/19 16:24 BGLg/L8.3 2/28/19SW-846 8270D1Pentachlorophenol
ND 5.2 3/2/19 16:24 BGLg/L2.8 2/28/19SW-846 8270D1Phenanthrene
ND 10 3/2/19 16:24 BGLg/L3.2 2/28/19SW-846 8270D1Phenol
ND 5.2 3/2/19 16:24 BGLg/L3.6 2/28/19SW-846 8270D1Pyrene
ND 5.2 3/2/19 16:24 BGLg/L3.3 2/28/19SW-846 8270D1Pyridine
ND 10 3/2/19 16:24 BGLg/L2.2 2/28/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 5.2 3/2/19 16:24 BGLg/L2.0 2/28/19SW-846 8270D11,2,4-Trichlorobenzene
ND 10 3/2/19 16:24 BGLg/L1.9 2/28/19SW-846 8270D12,4,5-Trichlorophenol
ND 10 3/2/19 16:24 BGLg/L2.1 2/28/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 33.2 3/2/19 16:2415-110
Phenol-d6 24.6 3/2/19 16:2415-110
Nitrobenzene-d5 54.5 3/2/19 16:2430-130
2-Fluorobiphenyl 61.2 3/2/19 16:2430-130
2,4,6-Tribromophenol 72.9 3/2/19 16:2415-110
p-Terphenyl-d14 78.1 3/2/19 16:2430-130
Page 15 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-02
Field Sample #: MW2
Sample Matrix: Ground Water
Sampled: 2/25/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
ND 0.40 3/4/19 10:10 MJHg/L0.36 2/28/19SW-846 6020B1Arsenic
80 10 3/4/19 10:10 MJHg/L5.3 2/28/19SW-846 6020B1Barium
ND 0.50 3/4/19 10:10 MJHg/L0.068 2/28/19SW-846 6020B1Cadmium
3.1 1.0 3/5/19 9:32 MJHg/L0.43 3/4/19SW-846 6020B1BChromium
ND 1.0 3/4/19 10:10 MJHg/L0.24 2/28/19SW-846 6020B1Lead
0.000047 0.00010 3/1/19 8:51 TBCmg/L0.000034 2/28/19SW-846 7470A1B, JMercury
ND 5.0 3/4/19 10:10 MJHg/L1.4 2/28/19SW-846 6020B1Selenium
ND 0.50 3/4/19 10:10 MJHg/L0.075 2/28/19SW-846 6020B1Silver
Page 16 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 16:00
[TOC_2]19B1097-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 250 3/1/19 7:20 LBDg/L48 2/28/19SW-846 8260D5Acetone
ND 25 3/1/19 7:20 LBDg/L2.9 2/28/19SW-846 8260D5Acrylonitrile
ND 2.5 3/1/19 7:20 LBDg/L0.53 2/28/19SW-846 8260D5tert-Amyl Methyl Ether (TAME)
5.5 5.0 3/1/19 7:20 LBDg/L0.60 2/28/19SW-846 8260D5Benzene
ND 5.0 3/1/19 7:20 LBDg/L0.75 2/28/19SW-846 8260D5Bromobenzene
ND 5.0 3/1/19 7:20 LBDg/L1.1 2/28/19SW-846 8260D5Bromochloromethane
ND 2.5 3/1/19 7:20 LBDg/L1.5 2/28/19SW-846 8260D5Bromodichloromethane
ND 5.0 3/1/19 7:20 LBDg/L1.0 2/28/19SW-846 8260D5Bromoform
ND 10 3/1/19 7:20 LBDg/L4.7 2/28/19SW-846 8260D5R-05Bromomethane
ND 100 3/1/19 7:20 LBDg/L12 2/28/19SW-846 8260D52-Butanone (MEK)
350 100 3/1/19 7:20 LBDg/L11 2/28/19SW-846 8260D5tert-Butyl Alcohol (TBA)
ND 5.0 3/1/19 7:20 LBDg/L0.75 2/28/19SW-846 8260D5n-Butylbenzene
2.2 5.0 3/1/19 7:20 LBDg/L0.65 2/28/19SW-846 8260D5Jsec-Butylbenzene
ND 5.0 3/1/19 7:20 LBDg/L0.60 2/28/19SW-846 8260D5tert-Butylbenzene
ND 2.5 3/1/19 7:20 LBDg/L0.48 2/28/19SW-846 8260D5tert-Butyl Ethyl Ether (TBEE)
ND 20 3/1/19 7:20 LBDg/L5.1 2/28/19SW-846 8260D5Carbon Disulfide
ND 25 3/1/19 7:20 LBDg/L1.2 2/28/19SW-846 8260D5Carbon Tetrachloride
ND 5.0 3/1/19 7:20 LBDg/L0.80 2/28/19SW-846 8260D5Chlorobenzene
ND 2.5 3/1/19 7:20 LBDg/L0.52 2/28/19SW-846 8260D5Chlorodibromomethane
ND 10 3/1/19 7:20 LBDg/L1.4 2/28/19SW-846 8260D5Chloroethane
ND 10 3/1/19 7:20 LBDg/L1.1 2/28/19SW-846 8260D5Chloroform
ND 10 3/1/19 7:20 LBDg/L2.8 2/28/19SW-846 8260D5Chloromethane
ND 5.0 3/1/19 7:20 LBDg/L0.60 2/28/19SW-846 8260D52-Chlorotoluene
ND 5.0 3/1/19 7:20 LBDg/L0.70 2/28/19SW-846 8260D54-Chlorotoluene
ND 25 3/1/19 7:20 LBDg/L1.8 2/28/19SW-846 8260D5V-051,2-Dibromo-3-chloropropane (DBCP)
ND 2.5 3/1/19 7:20 LBDg/L0.74 2/28/19SW-846 8260D51,2-Dibromoethane (EDB)
ND 5.0 3/1/19 7:20 LBDg/L0.80 2/28/19SW-846 8260D5Dibromomethane
ND 5.0 3/1/19 7:20 LBDg/L0.85 2/28/19SW-846 8260D51,2-Dichlorobenzene
ND 5.0 3/1/19 7:20 LBDg/L0.85 2/28/19SW-846 8260D51,3-Dichlorobenzene
ND 5.0 3/1/19 7:20 LBDg/L0.75 2/28/19SW-846 8260D51,4-Dichlorobenzene
ND 10 3/1/19 7:20 LBDg/L1.6 2/28/19SW-846 8260D5trans-1,4-Dichloro-2-butene
ND 10 3/1/19 7:20 LBDg/L1.4 2/28/19SW-846 8260D5Dichlorodifluoromethane (Freon 12)
ND 5.0 3/1/19 7:20 LBDg/L0.79 2/28/19SW-846 8260D51,1-Dichloroethane
1.4 5.0 3/1/19 7:20 LBDg/L0.97 2/28/19SW-846 8260D5J1,2-Dichloroethane
ND 5.0 3/1/19 7:20 LBDg/L1.0 2/28/19SW-846 8260D51,1-Dichloroethylene
ND 5.0 3/1/19 7:20 LBDg/L0.74 2/28/19SW-846 8260D5cis-1,2-Dichloroethylene
ND 5.0 3/1/19 7:20 LBDg/L0.75 2/28/19SW-846 8260D5trans-1,2-Dichloroethylene
ND 5.0 3/1/19 7:20 LBDg/L0.65 2/28/19SW-846 8260D51,2-Dichloropropane
ND 2.5 3/1/19 7:20 LBDg/L0.65 2/28/19SW-846 8260D51,3-Dichloropropane
ND 5.0 3/1/19 7:20 LBDg/L1.1 2/28/19SW-846 8260D52,2-Dichloropropane
ND 10 3/1/19 7:20 LBDg/L0.64 2/28/19SW-846 8260D51,1-Dichloropropene
ND 2.5 3/1/19 7:20 LBDg/L0.60 2/28/19SW-846 8260D5cis-1,3-Dichloropropene
ND 2.5 3/1/19 7:20 LBDg/L0.56 2/28/19SW-846 8260D5trans-1,3-Dichloropropene
ND 10 3/1/19 7:20 LBDg/L1.1 2/28/19SW-846 8260D5Diethyl Ether
Page 17 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 2.5 3/1/19 7:20 LBDg/L0.90 2/28/19SW-846 8260D5Diisopropyl Ether (DIPE)
ND 250 3/1/19 7:20 LBDg/L130 2/28/19SW-846 8260D51,4-Dioxane
150 5.0 3/1/19 7:20 LBDg/L0.65 2/28/19SW-846 8260D5Ethylbenzene
ND 5.0 3/1/19 7:20 LBDg/L2.9 2/28/19SW-846 8260D5Hexachlorobutadiene
ND 50 3/1/19 7:20 LBDg/L7.6 2/28/19SW-846 8260D52-Hexanone (MBK)
12 5.0 3/1/19 7:20 LBDg/L0.60 2/28/19SW-846 8260D5Isopropylbenzene (Cumene)
2.2 5.0 3/1/19 7:20 LBDg/L0.75 2/28/19SW-846 8260D5Jp-Isopropyltoluene (p-Cymene)
7.5 5.0 3/1/19 7:20 LBDg/L0.45 2/28/19SW-846 8260D5Methyl tert-Butyl Ether (MTBE)
ND 25 3/1/19 7:20 LBDg/L16 2/28/19SW-846 8260D5Methylene Chloride
ND 50 3/1/19 7:20 LBDg/L7.3 2/28/19SW-846 8260D54-Methyl-2-pentanone (MIBK)
45 25 3/1/19 7:20 LBDg/L0.60 2/28/19SW-846 8260D5V-05Naphthalene
30 5.0 3/1/19 7:20 LBDg/L0.65 2/28/19SW-846 8260D5n-Propylbenzene
ND 5.0 3/1/19 7:20 LBDg/L0.75 2/28/19SW-846 8260D5Styrene
ND 5.0 3/1/19 7:20 LBDg/L0.60 2/28/19SW-846 8260D51,1,1,2-Tetrachloroethane
ND 2.5 3/1/19 7:20 LBDg/L0.80 2/28/19SW-846 8260D51,1,2,2-Tetrachloroethane
ND 5.0 3/1/19 7:20 LBDg/L1.4 2/28/19SW-846 8260D5Tetrachloroethylene
ND 50 3/1/19 7:20 LBDg/L5.4 2/28/19SW-846 8260D5Tetrahydrofuran
110 5.0 3/1/19 7:20 LBDg/L0.85 2/28/19SW-846 8260D5Toluene
ND 25 3/1/19 7:20 LBDg/L0.70 2/28/19SW-846 8260D51,2,3-Trichlorobenzene
ND 5.0 3/1/19 7:20 LBDg/L0.95 2/28/19SW-846 8260D51,2,4-Trichlorobenzene
ND 5.0 3/1/19 7:20 LBDg/L0.85 2/28/19SW-846 8260D51,3,5-Trichlorobenzene
ND 5.0 3/1/19 7:20 LBDg/L0.66 2/28/19SW-846 8260D51,1,1-Trichloroethane
ND 5.0 3/1/19 7:20 LBDg/L1.2 2/28/19SW-846 8260D51,1,2-Trichloroethane
ND 5.0 3/1/19 7:20 LBDg/L1.0 2/28/19SW-846 8260D5Trichloroethylene
ND 10 3/1/19 7:20 LBDg/L0.74 2/28/19SW-846 8260D5Trichlorofluoromethane (Freon 11)
ND 10 3/1/19 7:20 LBDg/L1.1 2/28/19SW-846 8260D51,2,3-Trichloropropane
ND 5.0 3/1/19 7:20 LBDg/L0.98 2/28/19SW-846 8260D51,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
150 5.0 3/1/19 7:20 LBDg/L0.90 2/28/19SW-846 8260D51,2,4-Trimethylbenzene
150 5.0 3/1/19 7:20 LBDg/L0.65 2/28/19SW-846 8260D51,3,5-Trimethylbenzene
ND 10 3/1/19 7:20 LBDg/L0.66 2/28/19SW-846 8260D5Vinyl Chloride
440 10 3/1/19 7:20 LBDg/L1.3 2/28/19SW-846 8260D5m+p Xylene
190 5.0 3/1/19 7:20 LBDg/L0.66 2/28/19SW-846 8260D5o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.7 3/1/19 7:2070-130
Toluene-d8 103 3/1/19 7:2070-130
4-Bromofluorobenzene 105 3/1/19 7:2070-130
Page 18 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 16:52 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthene
ND 5.2 3/2/19 16:52 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthylene
ND 10 3/2/19 16:52 BGLg/L3.1 2/28/19SW-846 8270D1Acetophenone
ND 5.2 3/2/19 16:52 BGLg/L3.8 2/28/19SW-846 8270D1Aniline
ND 5.2 3/2/19 16:52 BGLg/L2.8 2/28/19SW-846 8270D1Anthracene
ND 21 3/2/19 16:52 BGLg/L12 2/28/19SW-846 8270D1L-04, R-05, V-04,
V-05
Benzidine
ND 5.2 3/2/19 16:52 BGLg/L2.4 2/28/19SW-846 8270D1Benzo(a)anthracene
ND 5.2 3/2/19 16:52 BGLg/L2.5 2/28/19SW-846 8270D1Benzo(a)pyrene
ND 5.2 3/2/19 16:52 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(b)fluoranthene
ND 5.2 3/2/19 16:52 BGLg/L3.5 2/28/19SW-846 8270D1Benzo(g,h,i)perylene
ND 5.2 3/2/19 16:52 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(k)fluoranthene
ND 10 3/2/19 16:52 BGLg/L9.1 2/28/19SW-846 8270D1Benzoic Acid
ND 10 3/2/19 16:52 BGLg/L2.6 2/28/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 10 3/2/19 16:52 BGLg/L3.2 2/28/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 10 3/2/19 16:52 BGLg/L2.7 2/28/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 10 3/2/19 16:52 BGLg/L1.9 2/28/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 10 3/2/19 16:52 BGLg/L3.5 2/28/19SW-846 8270D14-Bromophenylphenylether
ND 10 3/2/19 16:52 BGLg/L2.3 2/28/19SW-846 8270D1Butylbenzylphthalate
ND 10 3/2/19 16:52 BGLg/L2.8 2/28/19SW-846 8270D1Carbazole
ND 10 3/2/19 16:52 BGLg/L2.3 2/28/19SW-846 8270D1V-344-Chloroaniline
ND 10 3/2/19 16:52 BGLg/L1.6 2/28/19SW-846 8270D14-Chloro-3-methylphenol
ND 10 3/2/19 16:52 BGLg/L2.9 2/28/19SW-846 8270D12-Chloronaphthalene
ND 10 3/2/19 16:52 BGLg/L2.1 2/28/19SW-846 8270D12-Chlorophenol
ND 10 3/2/19 16:52 BGLg/L2.5 2/28/19SW-846 8270D14-Chlorophenylphenylether
ND 5.2 3/2/19 16:52 BGLg/L2.5 2/28/19SW-846 8270D1Chrysene
ND 5.2 3/2/19 16:52 BGLg/L3.2 2/28/19SW-846 8270D1Dibenz(a,h)anthracene
ND 5.2 3/2/19 16:52 BGLg/L2.6 2/28/19SW-846 8270D1Dibenzofuran
ND 10 3/2/19 16:52 BGLg/L2.2 2/28/19SW-846 8270D1Di-n-butylphthalate
ND 5.2 3/2/19 16:52 BGLg/L1.9 2/28/19SW-846 8270D11,2-Dichlorobenzene
ND 5.2 3/2/19 16:52 BGLg/L1.9 2/28/19SW-846 8270D11,3-Dichlorobenzene
ND 5.2 3/2/19 16:52 BGLg/L2.1 2/28/19SW-846 8270D11,4-Dichlorobenzene
ND 10 3/2/19 16:52 BGLg/L3.6 2/28/19SW-846 8270D13,3-Dichlorobenzidine
ND 10 3/2/19 16:52 BGLg/L2.0 2/28/19SW-846 8270D12,4-Dichlorophenol
ND 10 3/2/19 16:52 BGLg/L1.8 2/28/19SW-846 8270D1Diethylphthalate
ND 10 3/2/19 16:52 BGLg/L3.6 2/28/19SW-846 8270D1V-052,4-Dimethylphenol
ND 10 3/2/19 16:52 BGLg/L1.8 2/28/19SW-846 8270D1Dimethylphthalate
ND 10 3/2/19 16:52 BGLg/L7.9 2/28/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 10 3/2/19 16:52 BGLg/L8.1 2/28/19SW-846 8270D1V-052,4-Dinitrophenol
ND 10 3/2/19 16:52 BGLg/L1.8 2/28/19SW-846 8270D12,4-Dinitrotoluene
ND 10 3/2/19 16:52 BGLg/L1.8 2/28/19SW-846 8270D12,6-Dinitrotoluene
ND 10 3/2/19 16:52 BGLg/L3.0 2/28/19SW-846 8270D1Di-n-octylphthalate
ND 10 3/2/19 16:52 BGLg/L5.4 2/28/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 5.2 3/2/19 16:52 BGLg/L2.4 2/28/19SW-846 8270D1Fluoranthene
Page 19 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 16:52 BGLg/L2.5 2/28/19SW-846 8270D1Fluorene
ND 10 3/2/19 16:52 BGLg/L3.1 2/28/19SW-846 8270D1Hexachlorobenzene
ND 10 3/2/19 16:52 BGLg/L1.8 2/28/19SW-846 8270D1Hexachlorobutadiene
ND 10 3/2/19 16:52 BGLg/L8.4 2/28/19SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 10 3/2/19 16:52 BGLg/L1.9 2/28/19SW-846 8270D1Hexachloroethane
ND 5.2 3/2/19 16:52 BGLg/L3.8 2/28/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 10 3/2/19 16:52 BGLg/L2.2 2/28/19SW-846 8270D1Isophorone
19 5.2 3/2/19 16:52 BGLg/L3.0 2/28/19SW-846 8270D11-Methylnaphthalene
17 5.2 3/2/19 16:52 BGLg/L2.7 2/28/19SW-846 8270D12-Methylnaphthalene
ND 10 3/2/19 16:52 BGLg/L2.2 2/28/19SW-846 8270D12-Methylphenol
ND 10 3/2/19 16:52 BGLg/L2.2 2/28/19SW-846 8270D13/4-Methylphenol
33 5.2 3/2/19 16:52 BGLg/L2.7 2/28/19SW-846 8270D1Naphthalene
ND 10 3/2/19 16:52 BGLg/L3.7 2/28/19SW-846 8270D12-Nitroaniline
ND 10 3/2/19 16:52 BGLg/L1.7 2/28/19SW-846 8270D13-Nitroaniline
ND 10 3/2/19 16:52 BGLg/L1.7 2/28/19SW-846 8270D1V-054-Nitroaniline
ND 10 3/2/19 16:52 BGLg/L2.2 2/28/19SW-846 8270D1Nitrobenzene
ND 10 3/2/19 16:52 BGLg/L2.1 2/28/19SW-846 8270D12-Nitrophenol
ND 10 3/2/19 16:52 BGLg/L3.9 2/28/19SW-846 8270D14-Nitrophenol
ND 10 3/2/19 16:52 BGLg/L3.3 2/28/19SW-846 8270D1N-Nitrosodimethylamine
ND 10 3/2/19 16:52 BGLg/L6.4 2/28/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 10 3/2/19 16:52 BGLg/L3.1 2/28/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 10 3/2/19 16:52 BGLg/L5.2 2/28/19SW-846 8270D1Pentachloronitrobenzene
ND 10 3/2/19 16:52 BGLg/L8.3 2/28/19SW-846 8270D1Pentachlorophenol
ND 5.2 3/2/19 16:52 BGLg/L2.8 2/28/19SW-846 8270D1Phenanthrene
ND 10 3/2/19 16:52 BGLg/L3.2 2/28/19SW-846 8270D1Phenol
ND 5.2 3/2/19 16:52 BGLg/L3.6 2/28/19SW-846 8270D1Pyrene
ND 5.2 3/2/19 16:52 BGLg/L3.3 2/28/19SW-846 8270D1Pyridine
ND 10 3/2/19 16:52 BGLg/L2.2 2/28/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 5.2 3/2/19 16:52 BGLg/L2.0 2/28/19SW-846 8270D11,2,4-Trichlorobenzene
ND 10 3/2/19 16:52 BGLg/L1.9 2/28/19SW-846 8270D12,4,5-Trichlorophenol
ND 10 3/2/19 16:52 BGLg/L2.1 2/28/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 36.3 3/2/19 16:5215-110
Phenol-d6 28.5 3/2/19 16:5215-110
Nitrobenzene-d5 58.6 3/2/19 16:5230-130
2-Fluorobiphenyl 58.1 3/2/19 16:5230-130
2,4,6-Tribromophenol 69.5 3/2/19 16:5215-110
p-Terphenyl-d14 71.7 3/2/19 16:5230-130
Page 20 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-03
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 16:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.54 0.40 3/4/19 10:14 MJHg/L0.36 2/28/19SW-846 6020B1Arsenic
400 10 3/4/19 10:14 MJHg/L5.3 2/28/19SW-846 6020B1Barium
0.61 0.50 3/4/19 10:14 MJHg/L0.068 2/28/19SW-846 6020B1Cadmium
50 1.0 3/5/19 9:36 MJHg/L0.43 3/4/19SW-846 6020B1B-07Chromium
0.36 1.0 3/4/19 10:14 MJHg/L0.24 2/28/19SW-846 6020B1JLead
0.000063 0.00010 3/1/19 8:53 TBCmg/L0.000034 2/28/19SW-846 7470A1B, JMercury
3.8 5.0 3/4/19 10:14 MJHg/L1.4 2/28/19SW-846 6020B1JSelenium
ND 0.50 3/4/19 10:14 MJHg/L0.075 2/28/19SW-846 6020B1Silver
Page 21 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-04
Field Sample #: TANK OWS
Sample Matrix: Ground Water
Sampled: 2/25/2019 12:50
[TOC_2]19B1097-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/1/19 3:11 LBDg/L9.7 2/28/19SW-846 8260D1Acetone
ND 5.0 3/1/19 3:11 LBDg/L0.58 2/28/19SW-846 8260D1Acrylonitrile
ND 0.50 3/1/19 3:11 LBDg/L0.11 2/28/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 1.0 3/1/19 3:11 LBDg/L0.12 2/28/19SW-846 8260D1Benzene
ND 1.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D1Bromobenzene
ND 1.0 3/1/19 3:11 LBDg/L0.22 2/28/19SW-846 8260D1Bromochloromethane
ND 0.50 3/1/19 3:11 LBDg/L0.30 2/28/19SW-846 8260D1Bromodichloromethane
ND 1.0 3/1/19 3:11 LBDg/L0.21 2/28/19SW-846 8260D1Bromoform
ND 2.0 3/1/19 3:11 LBDg/L0.94 2/28/19SW-846 8260D1R-05Bromomethane
ND 20 3/1/19 3:11 LBDg/L2.4 2/28/19SW-846 8260D12-Butanone (MEK)
ND 20 3/1/19 3:11 LBDg/L2.2 2/28/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 1.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D1n-Butylbenzene
ND 1.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D1sec-Butylbenzene
ND 1.0 3/1/19 3:11 LBDg/L0.12 2/28/19SW-846 8260D1tert-Butylbenzene
ND 0.50 3/1/19 3:11 LBDg/L0.095 2/28/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 4.0 3/1/19 3:11 LBDg/L1.0 2/28/19SW-846 8260D1Carbon Disulfide
ND 5.0 3/1/19 3:11 LBDg/L0.25 2/28/19SW-846 8260D1Carbon Tetrachloride
ND 1.0 3/1/19 3:11 LBDg/L0.16 2/28/19SW-846 8260D1Chlorobenzene
ND 0.50 3/1/19 3:11 LBDg/L0.10 2/28/19SW-846 8260D1Chlorodibromomethane
ND 2.0 3/1/19 3:11 LBDg/L0.28 2/28/19SW-846 8260D1Chloroethane
ND 2.0 3/1/19 3:11 LBDg/L0.22 2/28/19SW-846 8260D1Chloroform
ND 2.0 3/1/19 3:11 LBDg/L0.55 2/28/19SW-846 8260D1Chloromethane
ND 1.0 3/1/19 3:11 LBDg/L0.12 2/28/19SW-846 8260D12-Chlorotoluene
ND 1.0 3/1/19 3:11 LBDg/L0.14 2/28/19SW-846 8260D14-Chlorotoluene
ND 5.0 3/1/19 3:11 LBDg/L0.37 2/28/19SW-846 8260D1V-051,2-Dibromo-3-chloropropane (DBCP)
ND 0.50 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 1.0 3/1/19 3:11 LBDg/L0.16 2/28/19SW-846 8260D1Dibromomethane
ND 1.0 3/1/19 3:11 LBDg/L0.17 2/28/19SW-846 8260D11,2-Dichlorobenzene
ND 1.0 3/1/19 3:11 LBDg/L0.17 2/28/19SW-846 8260D11,3-Dichlorobenzene
ND 1.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D11,4-Dichlorobenzene
ND 2.0 3/1/19 3:11 LBDg/L0.31 2/28/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 2.0 3/1/19 3:11 LBDg/L0.28 2/28/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/1/19 3:11 LBDg/L0.16 2/28/19SW-846 8260D11,1-Dichloroethane
ND 1.0 3/1/19 3:11 LBDg/L0.19 2/28/19SW-846 8260D11,2-Dichloroethane
ND 1.0 3/1/19 3:11 LBDg/L0.21 2/28/19SW-846 8260D11,1-Dichloroethylene
ND 1.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 1.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 1.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D11,2-Dichloropropane
ND 0.50 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D11,3-Dichloropropane
ND 1.0 3/1/19 3:11 LBDg/L0.21 2/28/19SW-846 8260D12,2-Dichloropropane
ND 2.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D11,1-Dichloropropene
ND 0.50 3/1/19 3:11 LBDg/L0.12 2/28/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.50 3/1/19 3:11 LBDg/L0.11 2/28/19SW-846 8260D1trans-1,3-Dichloropropene
ND 2.0 3/1/19 3:11 LBDg/L0.22 2/28/19SW-846 8260D1Diethyl Ether
Page 22 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-04
Field Sample #: TANK OWS
Sample Matrix: Ground Water
Sampled: 2/25/2019 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/1/19 3:11 LBDg/L0.18 2/28/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 50 3/1/19 3:11 LBDg/L26 2/28/19SW-846 8260D11,4-Dioxane
ND 1.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D1Ethylbenzene
ND 1.0 3/1/19 3:11 LBDg/L0.59 2/28/19SW-846 8260D1Hexachlorobutadiene
ND 10 3/1/19 3:11 LBDg/L1.5 2/28/19SW-846 8260D12-Hexanone (MBK)
ND 1.0 3/1/19 3:11 LBDg/L0.12 2/28/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 1.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 1.0 3/1/19 3:11 LBDg/L0.090 2/28/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/1/19 3:11 LBDg/L3.2 2/28/19SW-846 8260D1Methylene Chloride
ND 10 3/1/19 3:11 LBDg/L1.5 2/28/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 5.0 3/1/19 3:11 LBDg/L0.12 2/28/19SW-846 8260D1V-05Naphthalene
ND 1.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D1n-Propylbenzene
ND 1.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D1Styrene
ND 1.0 3/1/19 3:11 LBDg/L0.12 2/28/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.50 3/1/19 3:11 LBDg/L0.16 2/28/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 1.0 3/1/19 3:11 LBDg/L0.27 2/28/19SW-846 8260D1Tetrachloroethylene
ND 10 3/1/19 3:11 LBDg/L1.1 2/28/19SW-846 8260D1Tetrahydrofuran
ND 1.0 3/1/19 3:11 LBDg/L0.17 2/28/19SW-846 8260D1Toluene
ND 5.0 3/1/19 3:11 LBDg/L0.14 2/28/19SW-846 8260D11,2,3-Trichlorobenzene
ND 1.0 3/1/19 3:11 LBDg/L0.19 2/28/19SW-846 8260D11,2,4-Trichlorobenzene
ND 1.0 3/1/19 3:11 LBDg/L0.17 2/28/19SW-846 8260D11,3,5-Trichlorobenzene
ND 1.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D11,1,1-Trichloroethane
ND 1.0 3/1/19 3:11 LBDg/L0.24 2/28/19SW-846 8260D11,1,2-Trichloroethane
ND 1.0 3/1/19 3:11 LBDg/L0.20 2/28/19SW-846 8260D1Trichloroethylene
ND 2.0 3/1/19 3:11 LBDg/L0.15 2/28/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 2.0 3/1/19 3:11 LBDg/L0.22 2/28/19SW-846 8260D11,2,3-Trichloropropane
ND 1.0 3/1/19 3:11 LBDg/L0.20 2/28/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 1.0 3/1/19 3:11 LBDg/L0.18 2/28/19SW-846 8260D11,2,4-Trimethylbenzene
ND 1.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D11,3,5-Trimethylbenzene
ND 2.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D1Vinyl Chloride
ND 2.0 3/1/19 3:11 LBDg/L0.26 2/28/19SW-846 8260D1m+p Xylene
ND 1.0 3/1/19 3:11 LBDg/L0.13 2/28/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 100 3/1/19 3:1170-130
Toluene-d8 101 3/1/19 3:1170-130
4-Bromofluorobenzene 106 3/1/19 3:1170-130
Page 23 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-04
Field Sample #: TANK OWS
Sample Matrix: Ground Water
Sampled: 2/25/2019 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 17:19 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthene
ND 5.2 3/2/19 17:19 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthylene
ND 10 3/2/19 17:19 BGLg/L3.2 2/28/19SW-846 8270D1Acetophenone
ND 5.2 3/2/19 17:19 BGLg/L3.9 2/28/19SW-846 8270D1Aniline
ND 5.2 3/2/19 17:19 BGLg/L2.8 2/28/19SW-846 8270D1Anthracene
ND 21 3/2/19 17:19 BGLg/L12 2/28/19SW-846 8270D1L-04, R-05, V-04,
V-05
Benzidine
ND 5.2 3/2/19 17:19 BGLg/L2.4 2/28/19SW-846 8270D1Benzo(a)anthracene
ND 5.2 3/2/19 17:19 BGLg/L2.5 2/28/19SW-846 8270D1Benzo(a)pyrene
ND 5.2 3/2/19 17:19 BGLg/L2.9 2/28/19SW-846 8270D1Benzo(b)fluoranthene
ND 5.2 3/2/19 17:19 BGLg/L3.5 2/28/19SW-846 8270D1Benzo(g,h,i)perylene
ND 5.2 3/2/19 17:19 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(k)fluoranthene
ND 10 3/2/19 17:19 BGLg/L9.2 2/28/19SW-846 8270D1Benzoic Acid
ND 10 3/2/19 17:19 BGLg/L2.7 2/28/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 10 3/2/19 17:19 BGLg/L3.2 2/28/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 10 3/2/19 17:19 BGLg/L2.7 2/28/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 10 3/2/19 17:19 BGLg/L1.9 2/28/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 10 3/2/19 17:19 BGLg/L3.5 2/28/19SW-846 8270D14-Bromophenylphenylether
ND 10 3/2/19 17:19 BGLg/L2.3 2/28/19SW-846 8270D1Butylbenzylphthalate
ND 10 3/2/19 17:19 BGLg/L2.8 2/28/19SW-846 8270D1Carbazole
ND 10 3/2/19 17:19 BGLg/L2.3 2/28/19SW-846 8270D1V-344-Chloroaniline
ND 10 3/2/19 17:19 BGLg/L1.6 2/28/19SW-846 8270D14-Chloro-3-methylphenol
ND 10 3/2/19 17:19 BGLg/L3.0 2/28/19SW-846 8270D12-Chloronaphthalene
ND 10 3/2/19 17:19 BGLg/L2.2 2/28/19SW-846 8270D12-Chlorophenol
ND 10 3/2/19 17:19 BGLg/L2.5 2/28/19SW-846 8270D14-Chlorophenylphenylether
ND 5.2 3/2/19 17:19 BGLg/L2.6 2/28/19SW-846 8270D1Chrysene
ND 5.2 3/2/19 17:19 BGLg/L3.2 2/28/19SW-846 8270D1Dibenz(a,h)anthracene
ND 5.2 3/2/19 17:19 BGLg/L2.6 2/28/19SW-846 8270D1Dibenzofuran
ND 10 3/2/19 17:19 BGLg/L2.2 2/28/19SW-846 8270D1Di-n-butylphthalate
ND 5.2 3/2/19 17:19 BGLg/L1.9 2/28/19SW-846 8270D11,2-Dichlorobenzene
ND 5.2 3/2/19 17:19 BGLg/L1.9 2/28/19SW-846 8270D11,3-Dichlorobenzene
ND 5.2 3/2/19 17:19 BGLg/L2.2 2/28/19SW-846 8270D11,4-Dichlorobenzene
ND 10 3/2/19 17:19 BGLg/L3.6 2/28/19SW-846 8270D13,3-Dichlorobenzidine
ND 10 3/2/19 17:19 BGLg/L2.0 2/28/19SW-846 8270D12,4-Dichlorophenol
ND 10 3/2/19 17:19 BGLg/L1.8 2/28/19SW-846 8270D1Diethylphthalate
ND 10 3/2/19 17:19 BGLg/L3.7 2/28/19SW-846 8270D1V-052,4-Dimethylphenol
ND 10 3/2/19 17:19 BGLg/L1.9 2/28/19SW-846 8270D1Dimethylphthalate
ND 10 3/2/19 17:19 BGLg/L8.0 2/28/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 10 3/2/19 17:19 BGLg/L8.1 2/28/19SW-846 8270D1V-052,4-Dinitrophenol
ND 10 3/2/19 17:19 BGLg/L1.8 2/28/19SW-846 8270D12,4-Dinitrotoluene
ND 10 3/2/19 17:19 BGLg/L1.8 2/28/19SW-846 8270D12,6-Dinitrotoluene
ND 10 3/2/19 17:19 BGLg/L3.0 2/28/19SW-846 8270D1Di-n-octylphthalate
ND 10 3/2/19 17:19 BGLg/L5.5 2/28/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 5.2 3/2/19 17:19 BGLg/L2.4 2/28/19SW-846 8270D1Fluoranthene
Page 24 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-04
Field Sample #: TANK OWS
Sample Matrix: Ground Water
Sampled: 2/25/2019 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.2 3/2/19 17:19 BGLg/L2.6 2/28/19SW-846 8270D1Fluorene
ND 10 3/2/19 17:19 BGLg/L3.1 2/28/19SW-846 8270D1Hexachlorobenzene
ND 10 3/2/19 17:19 BGLg/L1.8 2/28/19SW-846 8270D1Hexachlorobutadiene
ND 10 3/2/19 17:19 BGLg/L8.5 2/28/19SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 10 3/2/19 17:19 BGLg/L1.9 2/28/19SW-846 8270D1Hexachloroethane
ND 5.2 3/2/19 17:19 BGLg/L3.9 2/28/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 10 3/2/19 17:19 BGLg/L2.2 2/28/19SW-846 8270D1Isophorone
ND 5.2 3/2/19 17:19 BGLg/L3.1 2/28/19SW-846 8270D11-Methylnaphthalene
ND 5.2 3/2/19 17:19 BGLg/L2.8 2/28/19SW-846 8270D12-Methylnaphthalene
ND 10 3/2/19 17:19 BGLg/L2.2 2/28/19SW-846 8270D12-Methylphenol
ND 10 3/2/19 17:19 BGLg/L2.2 2/28/19SW-846 8270D13/4-Methylphenol
ND 5.2 3/2/19 17:19 BGLg/L2.8 2/28/19SW-846 8270D1Naphthalene
ND 10 3/2/19 17:19 BGLg/L3.8 2/28/19SW-846 8270D12-Nitroaniline
ND 10 3/2/19 17:19 BGLg/L1.7 2/28/19SW-846 8270D13-Nitroaniline
ND 10 3/2/19 17:19 BGLg/L1.7 2/28/19SW-846 8270D1V-054-Nitroaniline
ND 10 3/2/19 17:19 BGLg/L2.3 2/28/19SW-846 8270D1Nitrobenzene
ND 10 3/2/19 17:19 BGLg/L2.1 2/28/19SW-846 8270D12-Nitrophenol
ND 10 3/2/19 17:19 BGLg/L3.9 2/28/19SW-846 8270D14-Nitrophenol
ND 10 3/2/19 17:19 BGLg/L3.3 2/28/19SW-846 8270D1N-Nitrosodimethylamine
ND 10 3/2/19 17:19 BGLg/L6.4 2/28/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 10 3/2/19 17:19 BGLg/L3.2 2/28/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 10 3/2/19 17:19 BGLg/L5.3 2/28/19SW-846 8270D1Pentachloronitrobenzene
ND 10 3/2/19 17:19 BGLg/L8.4 2/28/19SW-846 8270D1Pentachlorophenol
ND 5.2 3/2/19 17:19 BGLg/L2.9 2/28/19SW-846 8270D1Phenanthrene
ND 10 3/2/19 17:19 BGLg/L3.2 2/28/19SW-846 8270D1Phenol
ND 5.2 3/2/19 17:19 BGLg/L3.7 2/28/19SW-846 8270D1Pyrene
ND 5.2 3/2/19 17:19 BGLg/L3.3 2/28/19SW-846 8270D1Pyridine
ND 10 3/2/19 17:19 BGLg/L2.3 2/28/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 5.2 3/2/19 17:19 BGLg/L2.0 2/28/19SW-846 8270D11,2,4-Trichlorobenzene
ND 10 3/2/19 17:19 BGLg/L1.9 2/28/19SW-846 8270D12,4,5-Trichlorophenol
ND 10 3/2/19 17:19 BGLg/L2.1 2/28/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 39.6 3/2/19 17:1915-110
Phenol-d6 28.8 3/2/19 17:1915-110
Nitrobenzene-d5 61.6 3/2/19 17:1930-130
2-Fluorobiphenyl 60.6 3/2/19 17:1930-130
2,4,6-Tribromophenol 65.1 3/2/19 17:1915-110
p-Terphenyl-d14 70.8 3/2/19 17:1930-130
Page 25 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-05
Field Sample #: DUP-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 00:00
[TOC_2]19B1097-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/1/19 3:42 LBDg/L9.7 2/28/19SW-846 8260D1Acetone
ND 5.0 3/1/19 3:42 LBDg/L0.58 2/28/19SW-846 8260D1Acrylonitrile
ND 0.50 3/1/19 3:42 LBDg/L0.11 2/28/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 1.0 3/1/19 3:42 LBDg/L0.12 2/28/19SW-846 8260D1Benzene
ND 1.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D1Bromobenzene
ND 1.0 3/1/19 3:42 LBDg/L0.22 2/28/19SW-846 8260D1Bromochloromethane
ND 0.50 3/1/19 3:42 LBDg/L0.30 2/28/19SW-846 8260D1Bromodichloromethane
ND 1.0 3/1/19 3:42 LBDg/L0.21 2/28/19SW-846 8260D1Bromoform
ND 2.0 3/1/19 3:42 LBDg/L0.94 2/28/19SW-846 8260D1R-05Bromomethane
ND 20 3/1/19 3:42 LBDg/L2.4 2/28/19SW-846 8260D12-Butanone (MEK)
ND 20 3/1/19 3:42 LBDg/L2.2 2/28/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 1.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D1n-Butylbenzene
ND 1.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D1sec-Butylbenzene
ND 1.0 3/1/19 3:42 LBDg/L0.12 2/28/19SW-846 8260D1tert-Butylbenzene
ND 0.50 3/1/19 3:42 LBDg/L0.095 2/28/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 4.0 3/1/19 3:42 LBDg/L1.0 2/28/19SW-846 8260D1Carbon Disulfide
ND 5.0 3/1/19 3:42 LBDg/L0.25 2/28/19SW-846 8260D1Carbon Tetrachloride
ND 1.0 3/1/19 3:42 LBDg/L0.16 2/28/19SW-846 8260D1Chlorobenzene
ND 0.50 3/1/19 3:42 LBDg/L0.10 2/28/19SW-846 8260D1Chlorodibromomethane
ND 2.0 3/1/19 3:42 LBDg/L0.28 2/28/19SW-846 8260D1Chloroethane
1.6 2.0 3/1/19 3:42 LBDg/L0.22 2/28/19SW-846 8260D1JChloroform
ND 2.0 3/1/19 3:42 LBDg/L0.55 2/28/19SW-846 8260D1Chloromethane
ND 1.0 3/1/19 3:42 LBDg/L0.12 2/28/19SW-846 8260D12-Chlorotoluene
ND 1.0 3/1/19 3:42 LBDg/L0.14 2/28/19SW-846 8260D14-Chlorotoluene
ND 5.0 3/1/19 3:42 LBDg/L0.37 2/28/19SW-846 8260D1V-051,2-Dibromo-3-chloropropane (DBCP)
ND 0.50 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 1.0 3/1/19 3:42 LBDg/L0.16 2/28/19SW-846 8260D1Dibromomethane
ND 1.0 3/1/19 3:42 LBDg/L0.17 2/28/19SW-846 8260D11,2-Dichlorobenzene
ND 1.0 3/1/19 3:42 LBDg/L0.17 2/28/19SW-846 8260D11,3-Dichlorobenzene
ND 1.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D11,4-Dichlorobenzene
ND 2.0 3/1/19 3:42 LBDg/L0.31 2/28/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 2.0 3/1/19 3:42 LBDg/L0.28 2/28/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/1/19 3:42 LBDg/L0.16 2/28/19SW-846 8260D11,1-Dichloroethane
ND 1.0 3/1/19 3:42 LBDg/L0.19 2/28/19SW-846 8260D11,2-Dichloroethane
ND 1.0 3/1/19 3:42 LBDg/L0.21 2/28/19SW-846 8260D11,1-Dichloroethylene
ND 1.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 1.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 1.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D11,2-Dichloropropane
ND 0.50 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D11,3-Dichloropropane
ND 1.0 3/1/19 3:42 LBDg/L0.21 2/28/19SW-846 8260D12,2-Dichloropropane
ND 2.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D11,1-Dichloropropene
ND 0.50 3/1/19 3:42 LBDg/L0.12 2/28/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.50 3/1/19 3:42 LBDg/L0.11 2/28/19SW-846 8260D1trans-1,3-Dichloropropene
ND 2.0 3/1/19 3:42 LBDg/L0.22 2/28/19SW-846 8260D1Diethyl Ether
Page 26 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-05
Field Sample #: DUP-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/1/19 3:42 LBDg/L0.18 2/28/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 50 3/1/19 3:42 LBDg/L26 2/28/19SW-846 8260D11,4-Dioxane
ND 1.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D1Ethylbenzene
ND 1.0 3/1/19 3:42 LBDg/L0.59 2/28/19SW-846 8260D1Hexachlorobutadiene
ND 10 3/1/19 3:42 LBDg/L1.5 2/28/19SW-846 8260D12-Hexanone (MBK)
ND 1.0 3/1/19 3:42 LBDg/L0.12 2/28/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 1.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 1.0 3/1/19 3:42 LBDg/L0.090 2/28/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/1/19 3:42 LBDg/L3.2 2/28/19SW-846 8260D1Methylene Chloride
ND 10 3/1/19 3:42 LBDg/L1.5 2/28/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 5.0 3/1/19 3:42 LBDg/L0.12 2/28/19SW-846 8260D1V-05Naphthalene
ND 1.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D1n-Propylbenzene
ND 1.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D1Styrene
ND 1.0 3/1/19 3:42 LBDg/L0.12 2/28/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.50 3/1/19 3:42 LBDg/L0.16 2/28/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 1.0 3/1/19 3:42 LBDg/L0.27 2/28/19SW-846 8260D1Tetrachloroethylene
ND 10 3/1/19 3:42 LBDg/L1.1 2/28/19SW-846 8260D1Tetrahydrofuran
ND 1.0 3/1/19 3:42 LBDg/L0.17 2/28/19SW-846 8260D1Toluene
ND 5.0 3/1/19 3:42 LBDg/L0.14 2/28/19SW-846 8260D11,2,3-Trichlorobenzene
ND 1.0 3/1/19 3:42 LBDg/L0.19 2/28/19SW-846 8260D11,2,4-Trichlorobenzene
ND 1.0 3/1/19 3:42 LBDg/L0.17 2/28/19SW-846 8260D11,3,5-Trichlorobenzene
ND 1.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D11,1,1-Trichloroethane
ND 1.0 3/1/19 3:42 LBDg/L0.24 2/28/19SW-846 8260D11,1,2-Trichloroethane
ND 1.0 3/1/19 3:42 LBDg/L0.20 2/28/19SW-846 8260D1Trichloroethylene
ND 2.0 3/1/19 3:42 LBDg/L0.15 2/28/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 2.0 3/1/19 3:42 LBDg/L0.22 2/28/19SW-846 8260D11,2,3-Trichloropropane
ND 1.0 3/1/19 3:42 LBDg/L0.20 2/28/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 1.0 3/1/19 3:42 LBDg/L0.18 2/28/19SW-846 8260D11,2,4-Trimethylbenzene
ND 1.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D11,3,5-Trimethylbenzene
ND 2.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D1Vinyl Chloride
ND 2.0 3/1/19 3:42 LBDg/L0.26 2/28/19SW-846 8260D1m+p Xylene
ND 1.0 3/1/19 3:42 LBDg/L0.13 2/28/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.8 3/1/19 3:4270-130
Toluene-d8 102 3/1/19 3:4270-130
4-Bromofluorobenzene 105 3/1/19 3:4270-130
Page 27 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-05
Field Sample #: DUP-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.3 3/2/19 17:47 BGLg/L2.6 2/28/19SW-846 8270D1Acenaphthene
ND 5.3 3/2/19 17:47 BGLg/L2.5 2/28/19SW-846 8270D1Acenaphthylene
ND 11 3/2/19 17:47 BGLg/L3.2 2/28/19SW-846 8270D1Acetophenone
ND 5.3 3/2/19 17:47 BGLg/L3.9 2/28/19SW-846 8270D1Aniline
ND 5.3 3/2/19 17:47 BGLg/L2.9 2/28/19SW-846 8270D1Anthracene
ND 21 3/2/19 17:47 BGLg/L12 2/28/19SW-846 8270D1L-04, R-05, V-04,
V-05
Benzidine
ND 5.3 3/2/19 17:47 BGLg/L2.5 2/28/19SW-846 8270D1Benzo(a)anthracene
ND 5.3 3/2/19 17:47 BGLg/L2.5 2/28/19SW-846 8270D1Benzo(a)pyrene
ND 5.3 3/2/19 17:47 BGLg/L2.9 2/28/19SW-846 8270D1Benzo(b)fluoranthene
ND 5.3 3/2/19 17:47 BGLg/L3.5 2/28/19SW-846 8270D1Benzo(g,h,i)perylene
ND 5.3 3/2/19 17:47 BGLg/L2.8 2/28/19SW-846 8270D1Benzo(k)fluoranthene
ND 11 3/2/19 17:47 BGLg/L9.3 2/28/19SW-846 8270D1Benzoic Acid
ND 11 3/2/19 17:47 BGLg/L2.7 2/28/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 11 3/2/19 17:47 BGLg/L3.2 2/28/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 11 3/2/19 17:47 BGLg/L2.8 2/28/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 11 3/2/19 17:47 BGLg/L2.0 2/28/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 11 3/2/19 17:47 BGLg/L3.5 2/28/19SW-846 8270D14-Bromophenylphenylether
ND 11 3/2/19 17:47 BGLg/L2.3 2/28/19SW-846 8270D1Butylbenzylphthalate
ND 11 3/2/19 17:47 BGLg/L2.8 2/28/19SW-846 8270D1Carbazole
ND 11 3/2/19 17:47 BGLg/L2.3 2/28/19SW-846 8270D1V-344-Chloroaniline
ND 11 3/2/19 17:47 BGLg/L1.7 2/28/19SW-846 8270D14-Chloro-3-methylphenol
ND 11 3/2/19 17:47 BGLg/L3.0 2/28/19SW-846 8270D12-Chloronaphthalene
ND 11 3/2/19 17:47 BGLg/L2.2 2/28/19SW-846 8270D12-Chlorophenol
ND 11 3/2/19 17:47 BGLg/L2.6 2/28/19SW-846 8270D14-Chlorophenylphenylether
ND 5.3 3/2/19 17:47 BGLg/L2.6 2/28/19SW-846 8270D1Chrysene
ND 5.3 3/2/19 17:47 BGLg/L3.3 2/28/19SW-846 8270D1Dibenz(a,h)anthracene
ND 5.3 3/2/19 17:47 BGLg/L2.6 2/28/19SW-846 8270D1Dibenzofuran
ND 11 3/2/19 17:47 BGLg/L2.2 2/28/19SW-846 8270D1Di-n-butylphthalate
ND 5.3 3/2/19 17:47 BGLg/L1.9 2/28/19SW-846 8270D11,2-Dichlorobenzene
ND 5.3 3/2/19 17:47 BGLg/L1.9 2/28/19SW-846 8270D11,3-Dichlorobenzene
ND 5.3 3/2/19 17:47 BGLg/L2.2 2/28/19SW-846 8270D11,4-Dichlorobenzene
ND 11 3/2/19 17:47 BGLg/L3.7 2/28/19SW-846 8270D13,3-Dichlorobenzidine
ND 11 3/2/19 17:47 BGLg/L2.1 2/28/19SW-846 8270D12,4-Dichlorophenol
ND 11 3/2/19 17:47 BGLg/L1.8 2/28/19SW-846 8270D1Diethylphthalate
ND 11 3/2/19 17:47 BGLg/L3.7 2/28/19SW-846 8270D1V-052,4-Dimethylphenol
ND 11 3/2/19 17:47 BGLg/L1.9 2/28/19SW-846 8270D1Dimethylphthalate
ND 11 3/2/19 17:47 BGLg/L8.1 2/28/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 11 3/2/19 17:47 BGLg/L8.2 2/28/19SW-846 8270D1V-052,4-Dinitrophenol
ND 11 3/2/19 17:47 BGLg/L1.9 2/28/19SW-846 8270D12,4-Dinitrotoluene
ND 11 3/2/19 17:47 BGLg/L1.8 2/28/19SW-846 8270D12,6-Dinitrotoluene
ND 11 3/2/19 17:47 BGLg/L3.1 2/28/19SW-846 8270D1Di-n-octylphthalate
ND 11 3/2/19 17:47 BGLg/L5.6 2/28/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 5.3 3/2/19 17:47 BGLg/L2.5 2/28/19SW-846 8270D1Fluoranthene
Page 28 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-05
Field Sample #: DUP-3
Sample Matrix: Ground Water
Sampled: 2/25/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 5.3 3/2/19 17:47 BGLg/L2.6 2/28/19SW-846 8270D1Fluorene
ND 11 3/2/19 17:47 BGLg/L3.1 2/28/19SW-846 8270D1Hexachlorobenzene
ND 11 3/2/19 17:47 BGLg/L1.8 2/28/19SW-846 8270D1Hexachlorobutadiene
ND 11 3/2/19 17:47 BGLg/L8.6 2/28/19SW-846 8270D1V-05Hexachlorocyclopentadiene
ND 11 3/2/19 17:47 BGLg/L1.9 2/28/19SW-846 8270D1Hexachloroethane
ND 5.3 3/2/19 17:47 BGLg/L3.9 2/28/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 11 3/2/19 17:47 BGLg/L2.3 2/28/19SW-846 8270D1Isophorone
ND 5.3 3/2/19 17:47 BGLg/L3.1 2/28/19SW-846 8270D11-Methylnaphthalene
ND 5.3 3/2/19 17:47 BGLg/L2.8 2/28/19SW-846 8270D12-Methylnaphthalene
ND 11 3/2/19 17:47 BGLg/L2.2 2/28/19SW-846 8270D12-Methylphenol
ND 11 3/2/19 17:47 BGLg/L2.2 2/28/19SW-846 8270D13/4-Methylphenol
ND 5.3 3/2/19 17:47 BGLg/L2.8 2/28/19SW-846 8270D1Naphthalene
ND 11 3/2/19 17:47 BGLg/L3.8 2/28/19SW-846 8270D12-Nitroaniline
ND 11 3/2/19 17:47 BGLg/L1.7 2/28/19SW-846 8270D13-Nitroaniline
ND 11 3/2/19 17:47 BGLg/L1.7 2/28/19SW-846 8270D1V-054-Nitroaniline
ND 11 3/2/19 17:47 BGLg/L2.3 2/28/19SW-846 8270D1Nitrobenzene
ND 11 3/2/19 17:47 BGLg/L2.2 2/28/19SW-846 8270D12-Nitrophenol
ND 11 3/2/19 17:47 BGLg/L4.0 2/28/19SW-846 8270D14-Nitrophenol
ND 11 3/2/19 17:47 BGLg/L3.3 2/28/19SW-846 8270D1N-Nitrosodimethylamine
ND 11 3/2/19 17:47 BGLg/L6.5 2/28/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 11 3/2/19 17:47 BGLg/L3.2 2/28/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 11 3/2/19 17:47 BGLg/L5.4 2/28/19SW-846 8270D1Pentachloronitrobenzene
ND 11 3/2/19 17:47 BGLg/L8.5 2/28/19SW-846 8270D1Pentachlorophenol
ND 5.3 3/2/19 17:47 BGLg/L2.9 2/28/19SW-846 8270D1Phenanthrene
ND 11 3/2/19 17:47 BGLg/L3.3 2/28/19SW-846 8270D1Phenol
ND 5.3 3/2/19 17:47 BGLg/L3.7 2/28/19SW-846 8270D1Pyrene
ND 5.3 3/2/19 17:47 BGLg/L3.4 2/28/19SW-846 8270D1Pyridine
ND 11 3/2/19 17:47 BGLg/L2.3 2/28/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 5.3 3/2/19 17:47 BGLg/L2.0 2/28/19SW-846 8270D11,2,4-Trichlorobenzene
ND 11 3/2/19 17:47 BGLg/L1.9 2/28/19SW-846 8270D12,4,5-Trichlorophenol
ND 11 3/2/19 17:47 BGLg/L2.1 2/28/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 40.5 3/2/19 17:4715-110
Phenol-d6 28.5 3/2/19 17:4715-110
Nitrobenzene-d5 66.2 3/2/19 17:4730-130
2-Fluorobiphenyl 65.9 3/2/19 17:4730-130
2,4,6-Tribromophenol 72.3 3/2/19 17:4715-110
p-Terphenyl-d14 79.5 3/2/19 17:4730-130
Page 29 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-06
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 2/25/2019 00:00
[TOC_2]19B1097-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/1/19 0:36 LBDg/L9.7 2/28/19SW-846 8260D1Acetone
ND 5.0 3/1/19 0:36 LBDg/L0.58 2/28/19SW-846 8260D1Acrylonitrile
ND 0.50 3/1/19 0:36 LBDg/L0.11 2/28/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 1.0 3/1/19 0:36 LBDg/L0.12 2/28/19SW-846 8260D1Benzene
ND 1.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D1Bromobenzene
ND 1.0 3/1/19 0:36 LBDg/L0.22 2/28/19SW-846 8260D1Bromochloromethane
ND 0.50 3/1/19 0:36 LBDg/L0.30 2/28/19SW-846 8260D1Bromodichloromethane
ND 1.0 3/1/19 0:36 LBDg/L0.21 2/28/19SW-846 8260D1Bromoform
ND 2.0 3/1/19 0:36 LBDg/L0.94 2/28/19SW-846 8260D1R-05Bromomethane
ND 20 3/1/19 0:36 LBDg/L2.4 2/28/19SW-846 8260D12-Butanone (MEK)
ND 20 3/1/19 0:36 LBDg/L2.2 2/28/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 1.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D1n-Butylbenzene
ND 1.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D1sec-Butylbenzene
ND 1.0 3/1/19 0:36 LBDg/L0.12 2/28/19SW-846 8260D1tert-Butylbenzene
ND 0.50 3/1/19 0:36 LBDg/L0.095 2/28/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 4.0 3/1/19 0:36 LBDg/L1.0 2/28/19SW-846 8260D1Carbon Disulfide
ND 5.0 3/1/19 0:36 LBDg/L0.25 2/28/19SW-846 8260D1Carbon Tetrachloride
ND 1.0 3/1/19 0:36 LBDg/L0.16 2/28/19SW-846 8260D1Chlorobenzene
ND 0.50 3/1/19 0:36 LBDg/L0.10 2/28/19SW-846 8260D1Chlorodibromomethane
ND 2.0 3/1/19 0:36 LBDg/L0.28 2/28/19SW-846 8260D1Chloroethane
ND 2.0 3/1/19 0:36 LBDg/L0.22 2/28/19SW-846 8260D1Chloroform
ND 2.0 3/1/19 0:36 LBDg/L0.55 2/28/19SW-846 8260D1Chloromethane
ND 1.0 3/1/19 0:36 LBDg/L0.12 2/28/19SW-846 8260D12-Chlorotoluene
ND 1.0 3/1/19 0:36 LBDg/L0.14 2/28/19SW-846 8260D14-Chlorotoluene
ND 5.0 3/1/19 0:36 LBDg/L0.37 2/28/19SW-846 8260D1V-051,2-Dibromo-3-chloropropane (DBCP)
ND 0.50 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 1.0 3/1/19 0:36 LBDg/L0.16 2/28/19SW-846 8260D1Dibromomethane
ND 1.0 3/1/19 0:36 LBDg/L0.17 2/28/19SW-846 8260D11,2-Dichlorobenzene
ND 1.0 3/1/19 0:36 LBDg/L0.17 2/28/19SW-846 8260D11,3-Dichlorobenzene
ND 1.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D11,4-Dichlorobenzene
ND 2.0 3/1/19 0:36 LBDg/L0.31 2/28/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 2.0 3/1/19 0:36 LBDg/L0.28 2/28/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 1.0 3/1/19 0:36 LBDg/L0.16 2/28/19SW-846 8260D11,1-Dichloroethane
ND 1.0 3/1/19 0:36 LBDg/L0.19 2/28/19SW-846 8260D11,2-Dichloroethane
ND 1.0 3/1/19 0:36 LBDg/L0.21 2/28/19SW-846 8260D11,1-Dichloroethylene
ND 1.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 1.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 1.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D11,2-Dichloropropane
ND 0.50 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D11,3-Dichloropropane
ND 1.0 3/1/19 0:36 LBDg/L0.21 2/28/19SW-846 8260D12,2-Dichloropropane
ND 2.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D11,1-Dichloropropene
ND 0.50 3/1/19 0:36 LBDg/L0.12 2/28/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.50 3/1/19 0:36 LBDg/L0.11 2/28/19SW-846 8260D1trans-1,3-Dichloropropene
ND 2.0 3/1/19 0:36 LBDg/L0.22 2/28/19SW-846 8260D1Diethyl Ether
Page 30 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1097Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1097-06
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 2/25/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/1/19 0:36 LBDg/L0.18 2/28/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 50 3/1/19 0:36 LBDg/L26 2/28/19SW-846 8260D11,4-Dioxane
ND 1.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D1Ethylbenzene
ND 1.0 3/1/19 0:36 LBDg/L0.59 2/28/19SW-846 8260D1Hexachlorobutadiene
ND 10 3/1/19 0:36 LBDg/L1.5 2/28/19SW-846 8260D12-Hexanone (MBK)
ND 1.0 3/1/19 0:36 LBDg/L0.12 2/28/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 1.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 1.0 3/1/19 0:36 LBDg/L0.090 2/28/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/1/19 0:36 LBDg/L3.2 2/28/19SW-846 8260D1Methylene Chloride
ND 10 3/1/19 0:36 LBDg/L1.5 2/28/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 5.0 3/1/19 0:36 LBDg/L0.12 2/28/19SW-846 8260D1V-05Naphthalene
ND 1.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D1n-Propylbenzene
ND 1.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D1Styrene
ND 1.0 3/1/19 0:36 LBDg/L0.12 2/28/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.50 3/1/19 0:36 LBDg/L0.16 2/28/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 1.0 3/1/19 0:36 LBDg/L0.27 2/28/19SW-846 8260D1Tetrachloroethylene
ND 10 3/1/19 0:36 LBDg/L1.1 2/28/19SW-846 8260D1Tetrahydrofuran
ND 1.0 3/1/19 0:36 LBDg/L0.17 2/28/19SW-846 8260D1Toluene
ND 5.0 3/1/19 0:36 LBDg/L0.14 2/28/19SW-846 8260D11,2,3-Trichlorobenzene
ND 1.0 3/1/19 0:36 LBDg/L0.19 2/28/19SW-846 8260D11,2,4-Trichlorobenzene
ND 1.0 3/1/19 0:36 LBDg/L0.17 2/28/19SW-846 8260D11,3,5-Trichlorobenzene
ND 1.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D11,1,1-Trichloroethane
ND 1.0 3/1/19 0:36 LBDg/L0.24 2/28/19SW-846 8260D11,1,2-Trichloroethane
ND 1.0 3/1/19 0:36 LBDg/L0.20 2/28/19SW-846 8260D1Trichloroethylene
ND 2.0 3/1/19 0:36 LBDg/L0.15 2/28/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 2.0 3/1/19 0:36 LBDg/L0.22 2/28/19SW-846 8260D11,2,3-Trichloropropane
ND 1.0 3/1/19 0:36 LBDg/L0.20 2/28/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 1.0 3/1/19 0:36 LBDg/L0.18 2/28/19SW-846 8260D11,2,4-Trimethylbenzene
ND 1.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D11,3,5-Trimethylbenzene
ND 2.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D1Vinyl Chloride
ND 2.0 3/1/19 0:36 LBDg/L0.26 2/28/19SW-846 8260D1m+p Xylene
ND 1.0 3/1/19 0:36 LBDg/L0.13 2/28/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.3 3/1/19 0:3670-130
Toluene-d8 99.4 3/1/19 0:3670-130
4-Bromofluorobenzene 104 3/1/19 0:3670-130
Page 31 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3005A-SW-846 6020B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B224682 02/28/1950.0 50.019B1097-02 [MW2]
B224682 02/28/1950.0 50.019B1097-03 [MW-3]
Prep Method: SW-846 3005A-SW-846 6020B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B224896 03/04/1950.0 50.019B1097-02RE1 [MW2]
B224896 03/04/1950.0 50.019B1097-03RE1 [MW-3]
Prep Method: SW-846 7470A Prep-SW-846 7470A
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B224641 02/28/196.00 6.0019B1097-02 [MW2]
B224641 02/28/196.00 6.0019B1097-03 [MW-3]
Prep Method: SW-846 5030B-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B224603 02/28/195 5.0019B1097-01 [MW-1]
B224603 02/28/195 5.0019B1097-02 [MW2]
B224603 02/28/191 5.0019B1097-03 [MW-3]
B224603 02/28/195 5.0019B1097-04 [TANK OWS]
B224603 02/28/195 5.0019B1097-05 [DUP-3]
B224603 02/28/195 5.0019B1097-06 [Trip Blank]
Prep Method: SW-846 3510C-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B224592 02/28/19970 1.0019B1097-01RE1 [MW-1]
B224592 02/28/19970 1.0019B1097-02RE1 [MW2]
B224592 02/28/19970 1.0019B1097-03RE1 [MW-3]
B224592 02/28/19960 1.0019B1097-04RE1 [TANK OWS]
B224592 02/28/19950 1.0019B1097-05RE1 [DUP-3]
[TOC_1]Sample Preparation Information[TOC]
Page 32 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B224603 - SW-846 5030B
[TOC_3]B224603[TOC]
Blank (B224603-BLK1) Prepared & Analyzed: 02/28/19
Acetone g/L50ND
Acrylonitrile g/L5.0ND
tert-Amyl Methyl Ether (TAME)g/L0.50ND
Benzene g/L1.0ND
Bromobenzene g/L1.0ND
Bromochloromethane g/L1.0ND
Bromodichloromethane g/L0.50ND
Bromoform g/L1.0ND
Bromomethane g/L2.0 R-05ND
2-Butanone (MEK)g/L20ND
tert-Butyl Alcohol (TBA)g/L20ND
n-Butylbenzene g/L1.0ND
sec-Butylbenzene g/L1.0ND
tert-Butylbenzene g/L1.0ND
tert-Butyl Ethyl Ether (TBEE)g/L0.50ND
Carbon Disulfide g/L4.0ND
Carbon Tetrachloride g/L5.0ND
Chlorobenzene g/L1.0ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L2.0ND
Chloroform g/L2.0ND
Chloromethane g/L2.0ND
2-Chlorotoluene g/L1.0ND
4-Chlorotoluene g/L1.0ND
1,2-Dibromo-3-chloropropane (DBCP)g/L5.0 V-05ND
1,2-Dibromoethane (EDB)g/L0.50ND
Dibromomethane g/L1.0ND
1,2-Dichlorobenzene g/L1.0ND
1,3-Dichlorobenzene g/L1.0ND
1,4-Dichlorobenzene g/L1.0ND
trans-1,4-Dichloro-2-butene g/L2.0ND
Dichlorodifluoromethane (Freon 12)g/L2.0ND
1,1-Dichloroethane g/L1.0ND
1,2-Dichloroethane g/L1.0ND
1,1-Dichloroethylene g/L1.0ND
cis-1,2-Dichloroethylene g/L1.0ND
trans-1,2-Dichloroethylene g/L1.0ND
1,2-Dichloropropane g/L1.0ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L1.0ND
1,1-Dichloropropene g/L2.0ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diethyl Ether g/L2.0ND
Diisopropyl Ether (DIPE)g/L0.50ND
1,4-Dioxane g/L50ND
Ethylbenzene g/L1.0ND
Hexachlorobutadiene g/L0.60ND
2-Hexanone (MBK)g/L10ND
Isopropylbenzene (Cumene)g/L1.0ND
p-Isopropyltoluene (p-Cymene)g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
[TOC_1]QC Data[TOC]
Page 33 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224603 - SW-846 5030B
Blank (B224603-BLK1) Prepared & Analyzed: 02/28/19
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L10ND
Naphthalene g/L2.0 V-05ND
n-Propylbenzene g/L1.0ND
Styrene g/L1.0ND
1,1,1,2-Tetrachloroethane g/L1.0ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L1.0ND
Tetrahydrofuran g/L10ND
Toluene g/L1.0ND
1,2,3-Trichlorobenzene g/L5.0ND
1,2,4-Trichlorobenzene g/L1.0ND
1,3,5-Trichlorobenzene g/L1.0ND
1,1,1-Trichloroethane g/L1.0ND
1,1,2-Trichloroethane g/L1.0ND
Trichloroethylene g/L1.0ND
Trichlorofluoromethane (Freon 11)g/L2.0ND
1,2,3-Trichloropropane g/L2.0ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
1,3,5-Trimethylbenzene g/L1.0ND
Vinyl Chloride g/L2.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 98.824.7
g/L 25.0 70-130Surrogate: Toluene-d8 99.925.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.2
LCS (B224603-BS1) Prepared & Analyzed: 02/28/19
Acetone g/L50 100 L-0270-160189*189
Acrylonitrile g/L5.0 10.0 70-13010910.9
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 70-13011311.3
Benzene g/L1.0 10.0 70-13011011.0
Bromobenzene g/L1.0 10.0 70-13097.49.74
Bromochloromethane g/L1.0 10.0 V-20, L-0270-130134*13.4
Bromodichloromethane g/L0.50 10.0 70-13011011.0
Bromoform g/L1.0 10.0 70-13010110.1
Bromomethane g/L2.0 10.0 R-0540-16055.15.51
2-Butanone (MEK)g/L20 100 40-160129129
tert-Butyl Alcohol (TBA)g/L20 100 40-160116116
n-Butylbenzene g/L1.0 10.0 70-13082.98.29
sec-Butylbenzene g/L1.0 10.0 70-13087.38.73
tert-Butylbenzene g/L1.0 10.0 70-13087.28.72
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 70-13010510.5
Carbon Disulfide g/L4.0 10.0 V-3670-13011911.9
Carbon Tetrachloride g/L5.0 10.0 V-2070-13011611.6
Chlorobenzene g/L1.0 10.0 70-13010010.0
Chlorodibromomethane g/L0.50 10.0 70-13011511.5
Chloroethane g/L2.0 10.0 70-13010010.0
Chloroform g/L2.0 10.0 70-13011011.0
Chloromethane g/L2.0 10.0 40-16078.27.82
2-Chlorotoluene g/L1.0 10.0 70-13098.49.84
Page 34 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224603 - SW-846 5030B
LCS (B224603-BS1) Prepared & Analyzed: 02/28/19
4-Chlorotoluene g/L1.0 10.0 70-13098.29.82
1,2-Dibromo-3-chloropropane (DBCP)g/L5.0 10.0 V-0570-13081.58.15
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13011211.2
Dibromomethane g/L1.0 10.0 70-13011711.7
1,2-Dichlorobenzene g/L1.0 10.0 70-13091.29.12
1,3-Dichlorobenzene g/L1.0 10.0 70-13093.49.34
1,4-Dichlorobenzene g/L1.0 10.0 70-13090.49.04
trans-1,4-Dichloro-2-butene g/L2.0 10.0 70-13091.49.14
Dichlorodifluoromethane (Freon 12)g/L2.0 10.0 V-2040-16087.18.71
1,1-Dichloroethane g/L1.0 10.0 70-13010910.9
1,2-Dichloroethane g/L1.0 10.0 70-13010610.6
1,1-Dichloroethylene g/L1.0 10.0 70-13010810.8
cis-1,2-Dichloroethylene g/L1.0 10.0 70-13011111.1
trans-1,2-Dichloroethylene g/L1.0 10.0 70-13011311.3
1,2-Dichloropropane g/L1.0 10.0 70-13010310.3
1,3-Dichloropropane g/L0.50 10.0 70-13010610.6
2,2-Dichloropropane g/L1.0 10.0 40-13010410.4
1,1-Dichloropropene g/L2.0 10.0 V-2070-13011311.3
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010110.1
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010310.3
Diethyl Ether g/L2.0 10.0 70-13010910.9
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13097.99.79
1,4-Dioxane g/L50 100 40-130100100
Ethylbenzene g/L1.0 10.0 70-13095.79.57
Hexachlorobutadiene g/L0.60 10.0 70-13089.58.95
2-Hexanone (MBK)g/L10 100 70-160113113
Isopropylbenzene (Cumene)g/L1.0 10.0 70-13010010.0
p-Isopropyltoluene (p-Cymene)g/L1.0 10.0 70-13087.68.76
Methyl tert-Butyl Ether (MTBE)g/L1.0 10.0 70-13011511.5
Methylene Chloride g/L5.0 10.0 70-13099.39.93
4-Methyl-2-pentanone (MIBK)g/L10 100 70-16099.199.1
Naphthalene g/L2.0 10.0 V-0540-13082.88.28
n-Propylbenzene g/L1.0 10.0 70-13099.19.91
Styrene g/L1.0 10.0 70-13098.69.86
1,1,1,2-Tetrachloroethane g/L1.0 10.0 70-13010410.4
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010010.0
Tetrachloroethylene g/L1.0 10.0 70-13011811.8
Tetrahydrofuran g/L10 10.0 70-13010610.6
Toluene g/L1.0 10.0 70-13010710.7
1,2,3-Trichlorobenzene g/L5.0 10.0 70-13093.39.33
1,2,4-Trichlorobenzene g/L1.0 10.0 70-13091.59.15
1,3,5-Trichlorobenzene g/L1.0 10.0 70-13091.69.16
1,1,1-Trichloroethane g/L1.0 10.0 70-13011511.5
1,1,2-Trichloroethane g/L1.0 10.0 70-13011311.3
Trichloroethylene g/L1.0 10.0 70-13011611.6
Trichlorofluoromethane (Freon 11)g/L2.0 10.0 V-2070-13010110.1
1,2,3-Trichloropropane g/L2.0 10.0 70-13010510.5
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
g/L1.0 10.0 V-2070-13011211.2
1,2,4-Trimethylbenzene g/L1.0 10.0 70-13083.38.33
1,3,5-Trimethylbenzene g/L1.0 10.0 70-13096.89.68
Vinyl Chloride g/L2.0 10.0 40-16094.09.40
Page 35 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224603 - SW-846 5030B
LCS (B224603-BS1) Prepared & Analyzed: 02/28/19
m+p Xylene g/L2.0 20.0 70-13097.019.4
o-Xylene g/L1.0 10.0 70-13096.59.65
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 96.524.1
g/L 25.0 70-130Surrogate: Toluene-d8 99.624.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.3
LCS Dup (B224603-BSD1) Prepared & Analyzed: 02/28/19
Acetone g/L50 100 25 L-0270-160189 0.0529*189
Acrylonitrile g/L5.0 10.0 2570-130111 1.7311.1
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 2570-130117 3.2211.7
Benzene g/L1.0 10.0 2570-130117 5.9911.7
Bromobenzene g/L1.0 10.0 2570-130100 3.0310.0
Bromochloromethane g/L1.0 10.0 25 L-02, V-2070-130133 0.673*13.3
Bromodichloromethane g/L0.50 10.0 2570-130114 4.2911.4
Bromoform g/L1.0 10.0 2570-130102 1.5710.2
Bromomethane g/L2.0 10.0 25 R-0540-16075.3 31.0 *7.53
2-Butanone (MEK)g/L20 100 2540-160128 0.265128
tert-Butyl Alcohol (TBA)g/L20 100 2540-160110 5.47110
n-Butylbenzene g/L1.0 10.0 2570-13088.4 6.428.84
sec-Butylbenzene g/L1.0 10.0 2570-13091.1 4.269.11
tert-Butylbenzene g/L1.0 10.0 2570-13091.2 4.489.12
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 2570-130108 2.4410.8
Carbon Disulfide g/L4.0 10.0 25 V-3670-130124 4.2812.4
Carbon Tetrachloride g/L5.0 10.0 25 V-2070-130122 5.6212.2
Chlorobenzene g/L1.0 10.0 2570-130103 2.6610.3
Chlorodibromomethane g/L0.50 10.0 2570-130118 2.7511.8
Chloroethane g/L2.0 10.0 2570-130110 9.2211.0
Chloroform g/L2.0 10.0 2570-130116 5.4111.6
Chloromethane g/L2.0 10.0 2540-16082.8 5.718.28
2-Chlorotoluene g/L1.0 10.0 2570-130104 5.4410.4
4-Chlorotoluene g/L1.0 10.0 2570-130102 3.9910.2
1,2-Dibromo-3-chloropropane (DBCP)g/L5.0 10.0 25 V-0570-13082.0 0.6128.20
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130117 4.1011.7
Dibromomethane g/L1.0 10.0 2570-130114 2.3411.4
1,2-Dichlorobenzene g/L1.0 10.0 2570-13093.6 2.609.36
1,3-Dichlorobenzene g/L1.0 10.0 2570-13096.5 3.269.65
1,4-Dichlorobenzene g/L1.0 10.0 2570-13092.4 2.199.24
trans-1,4-Dichloro-2-butene g/L2.0 10.0 2570-13089.3 2.328.93
Dichlorodifluoromethane (Freon 12)g/L2.0 10.0 25 V-2040-16090.6 3.949.06
1,1-Dichloroethane g/L1.0 10.0 2570-130116 5.7711.6
1,2-Dichloroethane g/L1.0 10.0 2570-130107 1.6910.7
1,1-Dichloroethylene g/L1.0 10.0 2570-130116 6.5311.6
cis-1,2-Dichloroethylene g/L1.0 10.0 2570-130115 3.5511.5
trans-1,2-Dichloroethylene g/L1.0 10.0 2570-130121 6.8612.1
1,2-Dichloropropane g/L1.0 10.0 2570-130106 2.8810.6
1,3-Dichloropropane g/L0.50 10.0 2570-130110 3.7911.0
2,2-Dichloropropane g/L1.0 10.0 2540-130107 3.4210.7
1,1-Dichloropropene g/L2.0 10.0 25 V-2070-130121 6.8412.1
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130106 5.0010.6
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130104 0.77410.4
Diethyl Ether g/L2.0 10.0 2570-130113 3.4211.3
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130101 3.2210.1
Page 36 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224603 - SW-846 5030B
LCS Dup (B224603-BSD1) Prepared & Analyzed: 02/28/19
1,4-Dioxane g/L50 100 5040-130106 5.58106
Ethylbenzene g/L1.0 10.0 2570-13098.9 3.299.89
Hexachlorobutadiene g/L0.60 10.0 2570-13094.2 5.129.42
2-Hexanone (MBK)g/L10 100 2570-160112 1.25112
Isopropylbenzene (Cumene)g/L1.0 10.0 2570-130103 2.4610.3
p-Isopropyltoluene (p-Cymene)g/L1.0 10.0 2570-13090.5 3.269.05
Methyl tert-Butyl Ether (MTBE)g/L1.0 10.0 2570-130120 4.6012.0
Methylene Chloride g/L5.0 10.0 2570-130103 3.8510.3
4-Methyl-2-pentanone (MIBK)g/L10 100 2570-16098.5 0.67898.5
Naphthalene g/L2.0 10.0 25 V-0540-13081.8 1.228.18
n-Propylbenzene g/L1.0 10.0 2570-130102 3.2810.2
Styrene g/L1.0 10.0 2570-130102 3.5910.2
1,1,1,2-Tetrachloroethane g/L1.0 10.0 2570-130105 0.67010.5
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130101 1.2910.1
Tetrachloroethylene g/L1.0 10.0 2570-130126 6.3312.6
Tetrahydrofuran g/L10 10.0 2570-130107 1.2210.7
Toluene g/L1.0 10.0 2570-130112 4.8411.2
1,2,3-Trichlorobenzene g/L5.0 10.0 2570-13094.2 0.9609.42
1,2,4-Trichlorobenzene g/L1.0 10.0 2570-13093.6 2.279.36
1,3,5-Trichlorobenzene g/L1.0 10.0 2570-13096.1 4.799.61
1,1,1-Trichloroethane g/L1.0 10.0 2570-130124 6.9512.4
1,1,2-Trichloroethane g/L1.0 10.0 2570-130118 3.9811.8
Trichloroethylene g/L1.0 10.0 2570-130119 2.2111.9
Trichlorofluoromethane (Freon 11)g/L2.0 10.0 25 V-2070-130108 6.4910.8
1,2,3-Trichloropropane g/L2.0 10.0 2570-130105 0.47610.5
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
g/L1.0 10.0 25 V-2070-130117 4.3811.7
1,2,4-Trimethylbenzene g/L1.0 10.0 2570-13085.9 3.078.59
1,3,5-Trimethylbenzene g/L1.0 10.0 2570-130101 4.2510.1
Vinyl Chloride g/L2.0 10.0 2540-16098.5 4.689.85
m+p Xylene g/L2.0 20.0 2570-130101 4.1920.2
o-Xylene g/L1.0 10.0 2570-130102 5.2510.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.624.4
g/L 25.0 70-130Surrogate: Toluene-d8 10225.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.8
Page 37 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B224592 - SW-846 3510C
[TOC_3]B224592[TOC]
Blank (B224592-BLK1) Prepared: 02/28/19 Analyzed: 03/02/19
Acenaphthene g/L5.0ND
Acenaphthylene g/L5.0ND
Acetophenone g/L10ND
Aniline g/L5.0ND
Anthracene g/L5.0ND
Benzidine g/L20 L-04, R-05, V-04,
V-05
ND
Benzo(a)anthracene g/L5.0ND
Benzo(a)pyrene g/L5.0ND
Benzo(b)fluoranthene g/L5.0ND
Benzo(g,h,i)perylene g/L5.0ND
Benzo(k)fluoranthene g/L5.0ND
Benzoic Acid g/L10ND
Bis(2-chloroethoxy)methane g/L10ND
Bis(2-chloroethyl)ether g/L10ND
Bis(2-chloroisopropyl)ether g/L10ND
Bis(2-Ethylhexyl)phthalate g/L10ND
4-Bromophenylphenylether g/L10ND
Butylbenzylphthalate g/L10ND
Carbazole g/L10ND
4-Chloroaniline g/L10 V-34ND
4-Chloro-3-methylphenol g/L10ND
2-Chloronaphthalene g/L10ND
2-Chlorophenol g/L10ND
4-Chlorophenylphenylether g/L10ND
Chrysene g/L5.0ND
Dibenz(a,h)anthracene g/L5.0ND
Dibenzofuran g/L5.0ND
Di-n-butylphthalate g/L10ND
1,2-Dichlorobenzene g/L5.0ND
1,3-Dichlorobenzene g/L5.0ND
1,4-Dichlorobenzene g/L5.0ND
3,3-Dichlorobenzidine g/L10ND
2,4-Dichlorophenol g/L10ND
Diethylphthalate g/L10ND
2,4-Dimethylphenol g/L10 V-05ND
Dimethylphthalate g/L10ND
4,6-Dinitro-2-methylphenol g/L10ND
2,4-Dinitrophenol g/L10 V-05ND
2,4-Dinitrotoluene g/L10ND
2,6-Dinitrotoluene g/L10ND
Di-n-octylphthalate g/L10ND
1,2-Diphenylhydrazine/Azobenzene g/L10ND
Fluoranthene g/L5.0ND
Fluorene g/L5.0ND
Hexachlorobenzene g/L10ND
Hexachlorobutadiene g/L10ND
Hexachlorocyclopentadiene g/L10 V-05ND
Hexachloroethane g/L10ND
Indeno(1,2,3-cd)pyrene g/L5.0ND
Isophorone g/L10ND
1-Methylnaphthalene g/L5.0ND
2-Methylnaphthalene g/L5.0ND
Page 38 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224592 - SW-846 3510C
Blank (B224592-BLK1) Prepared: 02/28/19 Analyzed: 03/02/19
2-Methylphenol g/L10ND
3/4-Methylphenol g/L10ND
Naphthalene g/L5.0ND
2-Nitroaniline g/L10ND
3-Nitroaniline g/L10ND
4-Nitroaniline g/L10 V-05ND
Nitrobenzene g/L10ND
2-Nitrophenol g/L10ND
4-Nitrophenol g/L10ND
N-Nitrosodimethylamine g/L10ND
N-Nitrosodiphenylamine/Diphenylamine g/L10ND
N-Nitrosodi-n-propylamine g/L10ND
Pentachloronitrobenzene g/L10ND
Pentachlorophenol g/L10ND
Phenanthrene g/L5.0ND
Phenol g/L10ND
Pyrene g/L5.0ND
Pyridine g/L5.0ND
1,2,4,5-Tetrachlorobenzene g/L10ND
1,2,4-Trichlorobenzene g/L5.0ND
2,4,5-Trichlorophenol g/L10ND
2,4,6-Trichlorophenol g/L10ND
g/L 200 15-110Surrogate: 2-Fluorophenol 39.178.3
g/L 200 15-110Surrogate: Phenol-d6 28.456.9
g/L 100 30-130Surrogate: Nitrobenzene-d5 62.762.7
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 62.762.7
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 72.6145
g/L 100 30-130Surrogate: p-Terphenyl-d14 85.285.2
LCS (B224592-BS1) Prepared: 02/28/19 Analyzed: 03/02/19
Acenaphthene g/L5.0 50.0 40-14060.430.2
Acenaphthylene g/L5.0 50.0 40-14064.232.1
Acetophenone g/L10 50.0 40-14071.235.6
Aniline g/L5.0 50.0 40-14054.227.1
Anthracene g/L5.0 50.0 40-14076.638.3
Benzidine g/L20 50.0 L-04, R-05, V-04,
V-05, J
40-14032.2 *16.1
Benzo(a)anthracene g/L5.0 50.0 40-14074.137.1
Benzo(a)pyrene g/L5.0 50.0 40-14078.239.1
Benzo(b)fluoranthene g/L5.0 50.0 40-14074.837.4
Benzo(g,h,i)perylene g/L5.0 50.0 40-14076.838.4
Benzo(k)fluoranthene g/L5.0 50.0 40-14074.937.4
Benzoic Acid g/L10 50.0 10-13043.721.9
Bis(2-chloroethoxy)methane g/L10 50.0 40-14078.239.1
Bis(2-chloroethyl)ether g/L10 50.0 40-14068.634.3
Bis(2-chloroisopropyl)ether g/L10 50.0 40-14077.939.0
Bis(2-Ethylhexyl)phthalate g/L10 50.0 40-14093.746.8
4-Bromophenylphenylether g/L10 50.0 40-14078.539.2
Butylbenzylphthalate g/L10 50.0 40-14083.541.7
Carbazole g/L10 50.0 40-14073.236.6
4-Chloroaniline g/L10 50.0 V-3440-14062.131.1
4-Chloro-3-methylphenol g/L10 50.0 30-13080.940.4
2-Chloronaphthalene g/L10 50.0 40-14061.430.7
Page 39 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224592 - SW-846 3510C
LCS (B224592-BS1) Prepared: 02/28/19 Analyzed: 03/02/19
2-Chlorophenol g/L10 50.0 30-13069.434.7
4-Chlorophenylphenylether g/L10 50.0 40-14072.736.4
Chrysene g/L5.0 50.0 40-14072.636.3
Dibenz(a,h)anthracene g/L5.0 50.0 40-14076.338.2
Dibenzofuran g/L5.0 50.0 40-14067.333.6
Di-n-butylphthalate g/L10 50.0 40-14084.542.3
1,2-Dichlorobenzene g/L5.0 50.0 40-14065.232.6
1,3-Dichlorobenzene g/L5.0 50.0 40-14063.631.8
1,4-Dichlorobenzene g/L5.0 50.0 40-14063.231.6
3,3-Dichlorobenzidine g/L10 50.0 40-14086.343.2
2,4-Dichlorophenol g/L10 50.0 30-13074.037.0
Diethylphthalate g/L10 50.0 40-14074.337.1
2,4-Dimethylphenol g/L10 50.0 V-0530-13067.133.6
Dimethylphthalate g/L10 50.0 40-14073.036.5
4,6-Dinitro-2-methylphenol g/L10 50.0 30-13067.633.8
2,4-Dinitrophenol g/L10 50.0 V-0530-13063.531.8
2,4-Dinitrotoluene g/L10 50.0 40-14073.536.8
2,6-Dinitrotoluene g/L10 50.0 40-14072.436.2
Di-n-octylphthalate g/L10 50.0 40-14089.744.9
1,2-Diphenylhydrazine/Azobenzene g/L10 50.0 40-14075.037.5
Fluoranthene g/L5.0 50.0 40-14076.938.4
Fluorene g/L5.0 50.0 40-14069.634.8
Hexachlorobenzene g/L10 50.0 40-14085.042.5
Hexachlorobutadiene g/L10 50.0 40-14070.035.0
Hexachlorocyclopentadiene g/L10 50.0 V-0530-14052.426.2
Hexachloroethane g/L10 50.0 40-14063.631.8
Indeno(1,2,3-cd)pyrene g/L5.0 50.0 40-14076.038.0
Isophorone g/L10 50.0 40-14077.939.0
1-Methylnaphthalene g/L5.0 50.0 40-14069.134.6
2-Methylnaphthalene g/L5.0 50.0 40-14076.738.3
2-Methylphenol g/L10 50.0 30-13061.530.7
3/4-Methylphenol g/L10 50.0 30-13060.930.4
Naphthalene g/L5.0 50.0 40-14066.833.4
2-Nitroaniline g/L10 50.0 40-14070.335.1
3-Nitroaniline g/L10 50.0 40-14064.632.3
4-Nitroaniline g/L10 50.0 V-0540-14063.531.7
Nitrobenzene g/L10 50.0 40-14068.034.0
2-Nitrophenol g/L10 50.0 30-13070.835.4
4-Nitrophenol g/L10 50.0 10-13043.621.8
N-Nitrosodimethylamine g/L10 50.0 40-14046.823.4
N-Nitrosodiphenylamine/Diphenylamine g/L10 50.0 40-14079.339.6
N-Nitrosodi-n-propylamine g/L10 50.0 40-14072.336.2
Pentachloronitrobenzene g/L10 50.0 40-14086.143.0
Pentachlorophenol g/L10 50.0 30-13070.235.1
Phenanthrene g/L5.0 50.0 40-14076.638.3
Phenol g/L10 50.0 20-13033.516.8
Pyrene g/L5.0 50.0 40-14073.836.9
Pyridine g/L5.0 50.0 10-14029.314.6
1,2,4,5-Tetrachlorobenzene g/L10 50.0 40-14065.032.5
1,2,4-Trichlorobenzene g/L5.0 50.0 40-14068.934.4
2,4,5-Trichlorophenol g/L10 50.0 30-13068.434.2
2,4,6-Trichlorophenol g/L10 50.0 30-13068.034.0
Page 40 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224592 - SW-846 3510C
LCS (B224592-BS1) Prepared: 02/28/19 Analyzed: 03/02/19
g/L 200 15-110Surrogate: 2-Fluorophenol 46.893.5
g/L 200 15-110Surrogate: Phenol-d6 35.671.3
g/L 100 30-130Surrogate: Nitrobenzene-d5 71.471.4
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 71.471.4
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 93.5187
g/L 100 30-130Surrogate: p-Terphenyl-d14 92.092.0
LCS Dup (B224592-BSD1) Prepared: 02/28/19 Analyzed: 03/02/19
Acenaphthene g/L5.0 50.0 2040-14060.0 0.63130.0
Acenaphthylene g/L5.0 50.0 2040-14062.8 2.2131.4
Acetophenone g/L10 50.0 2040-14071.8 0.83935.9
Aniline g/L5.0 50.0 5040-14054.6 0.66227.3
Anthracene g/L5.0 50.0 2040-14074.3 3.0837.1
Benzidine g/L20 50.0 20 V-04, V-05, L-04,
R-05, J
40-14025.9 21.5**13.0
Benzo(a)anthracene g/L5.0 50.0 2040-14068.9 7.3034.4
Benzo(a)pyrene g/L5.0 50.0 2040-14074.1 5.3837.1
Benzo(b)fluoranthene g/L5.0 50.0 2040-14070.4 5.9535.2
Benzo(g,h,i)perylene g/L5.0 50.0 2040-14073.7 4.0436.9
Benzo(k)fluoranthene g/L5.0 50.0 2040-14071.3 4.8235.7
Benzoic Acid g/L10 50.0 5010-13035.9 19.618.0
Bis(2-chloroethoxy)methane g/L10 50.0 2040-14076.8 1.7538.4
Bis(2-chloroethyl)ether g/L10 50.0 2040-14068.2 0.58534.1
Bis(2-chloroisopropyl)ether g/L10 50.0 2040-14075.8 2.7337.9
Bis(2-Ethylhexyl)phthalate g/L10 50.0 2040-14083.2 11.841.6
4-Bromophenylphenylether g/L10 50.0 2040-14078.2 0.38339.1
Butylbenzylphthalate g/L10 50.0 2040-14080.1 4.1140.1
Carbazole g/L10 50.0 2040-14069.0 5.7934.5
4-Chloroaniline g/L10 50.0 20 V-3440-14058.7 5.6629.4
4-Chloro-3-methylphenol g/L10 50.0 2030-13079.7 1.4939.8
2-Chloronaphthalene g/L10 50.0 2040-14061.3 0.16330.6
2-Chlorophenol g/L10 50.0 2030-13067.8 2.2733.9
4-Chlorophenylphenylether g/L10 50.0 2040-14070.1 3.6735.0
Chrysene g/L5.0 50.0 2040-14068.7 5.4934.4
Dibenz(a,h)anthracene g/L5.0 50.0 2040-14071.5 6.5035.8
Dibenzofuran g/L5.0 50.0 2040-14065.9 2.0732.9
Di-n-butylphthalate g/L10 50.0 2040-14080.4 5.0740.2
1,2-Dichlorobenzene g/L5.0 50.0 2040-14062.6 3.9431.3
1,3-Dichlorobenzene g/L5.0 50.0 2040-14059.3 6.9329.7
1,4-Dichlorobenzene g/L5.0 50.0 2040-14060.6 4.2330.3
3,3-Dichlorobenzidine g/L10 50.0 2040-14078.2 9.8539.1
2,4-Dichlorophenol g/L10 50.0 2030-13074.0 0.027037.0
Diethylphthalate g/L10 50.0 2040-14068.5 8.0434.3
2,4-Dimethylphenol g/L10 50.0 20 V-0530-13065.8 1.9932.9
Dimethylphthalate g/L10 50.0 5040-14068.5 6.3634.3
4,6-Dinitro-2-methylphenol g/L10 50.0 5030-13065.4 3.3732.7
2,4-Dinitrophenol g/L10 50.0 50 V-0530-13059.0 7.3829.5
2,4-Dinitrotoluene g/L10 50.0 2040-14067.7 8.2733.8
2,6-Dinitrotoluene g/L10 50.0 2040-14070.6 2.4635.3
Di-n-octylphthalate g/L10 50.0 2040-14085.3 5.0742.6
1,2-Diphenylhydrazine/Azobenzene g/L10 50.0 2040-14073.0 2.7036.5
Fluoranthene g/L5.0 50.0 2040-14073.3 4.7136.7
Fluorene g/L5.0 50.0 2040-14064.7 7.3032.4
Page 41 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224592 - SW-846 3510C
LCS Dup (B224592-BSD1) Prepared: 02/28/19 Analyzed: 03/02/19
Hexachlorobenzene g/L10 50.0 2040-14081.1 4.6240.6
Hexachlorobutadiene g/L10 50.0 2040-14070.1 0.25735.1
Hexachlorocyclopentadiene g/L10 50.0 50 V-0530-14051.1 2.4725.6
Hexachloroethane g/L10 50.0 5040-14060.4 5.2330.2
Indeno(1,2,3-cd)pyrene g/L5.0 50.0 5040-14072.0 5.4636.0
Isophorone g/L10 50.0 2040-14076.7 1.5838.4
1-Methylnaphthalene g/L5.0 50.0 2040-14068.8 0.40634.4
2-Methylnaphthalene g/L5.0 50.0 2040-14077.1 0.49438.5
2-Methylphenol g/L10 50.0 2030-13061.8 0.45430.9
3/4-Methylphenol g/L10 50.0 2030-13059.8 1.7629.9
Naphthalene g/L5.0 50.0 2040-14065.7 1.6632.9
2-Nitroaniline g/L10 50.0 2040-14066.4 5.6533.2
3-Nitroaniline g/L10 50.0 2040-14060.5 6.5530.2
4-Nitroaniline g/L10 50.0 20 V-0540-14059.3 6.7829.7
Nitrobenzene g/L10 50.0 2040-14065.7 3.4732.8
2-Nitrophenol g/L10 50.0 2030-13071.5 0.98335.8
4-Nitrophenol g/L10 50.0 5010-13041.2 5.7020.6
N-Nitrosodimethylamine g/L10 50.0 2040-14043.3 7.7321.6
N-Nitrosodiphenylamine/Diphenylamine g/L10 50.0 2040-14074.1 6.7337.1
N-Nitrosodi-n-propylamine g/L10 50.0 2040-14070.9 1.9835.4
Pentachloronitrobenzene g/L10 50.0 2040-14078.8 8.8839.4
Pentachlorophenol g/L10 50.0 5030-13064.3 8.8132.1
Phenanthrene g/L5.0 50.0 2040-14073.9 3.6736.9
Phenol g/L10 50.0 2020-13032.7 2.4816.4
Pyrene g/L5.0 50.0 2040-14070.0 5.3435.0
Pyridine g/L5.0 50.0 5010-14029.4 0.40914.7
1,2,4,5-Tetrachlorobenzene g/L10 50.0 2040-14064.8 0.30832.4
1,2,4-Trichlorobenzene g/L5.0 50.0 2040-14068.1 1.1434.1
2,4,5-Trichlorophenol g/L10 50.0 2030-13064.3 6.1532.1
2,4,6-Trichlorophenol g/L10 50.0 5030-13065.6 3.5032.8
g/L 200 15-110Surrogate: 2-Fluorophenol 46.593.0
g/L 200 15-110Surrogate: Phenol-d6 34.969.9
g/L 100 30-130Surrogate: Nitrobenzene-d5 72.672.6
g/L 100 30-130Surrogate: 2-Fluorobiphenyl 72.772.7
g/L 200 15-110Surrogate: 2,4,6-Tribromophenol 86.3173
g/L 100 30-130Surrogate: p-Terphenyl-d14 86.686.6
Page 42 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B224641 - SW-846 7470A Prep
[TOC_3]B224641[TOC]
Blank (B224641-BLK1) Prepared: 02/28/19 Analyzed: 03/01/19
Mercury mg/L0.00010 B, J0.000054
LCS (B224641-BS1) Prepared: 02/28/19 Analyzed: 03/01/19
Mercury mg/L0.00010 0.00400 80-1201010.00403
LCS Dup (B224641-BSD1) Prepared: 02/28/19 Analyzed: 03/01/19
Mercury mg/L0.00010 0.00400 2080-12097.4 3.280.00390
Duplicate (B224641-DUP1) Prepared: 02/28/19 Analyzed: 03/01/19 Source: 19B1097-02
Mercury mg/L0.00010 20 J7.080.0000502 0.0000468
Matrix Spike (B224641-MS1) Prepared: 02/28/19 Analyzed: 03/01/19 Source: 19B1097-02
Mercury mg/L0.00010 0.00400 75-12597.10.00393 0.0000468
Batch B224682 - SW-846 3005A
[TOC_3]B224682[TOC]
Blank (B224682-BLK1) Prepared: 02/28/19 Analyzed: 03/04/19
Arsenic g/L0.40ND
Barium g/L10ND
Cadmium g/L0.50ND
Lead g/L1.0ND
Selenium g/L5.0ND
Silver g/L0.50ND
LCS (B224682-BS1) Prepared: 02/28/19 Analyzed: 03/01/19
Arsenic g/L4.0 500 80-120104521
Barium g/L100 500 80-120105523
Cadmium g/L5.0 500 80-120106530
Lead g/L10 500 80-120105525
Selenium g/L50 500 80-120100502
Silver g/L5.0 500 80-120104518
LCS Dup (B224682-BSD1) Prepared: 02/28/19 Analyzed: 03/01/19
Arsenic g/L4.0 500 2080-120105 0.438524
Barium g/L100 500 2080-120104 0.194522
Cadmium g/L5.0 500 2080-120106 0.0114530
Lead g/L10 500 2080-120105 0.290527
Selenium g/L50 500 2080-120103 2.19513
Silver g/L5.0 500 2080-120104 0.0476518
Batch B224896 - SW-846 3005A
[TOC_3]B224896[TOC]
Blank (B224896-BLK1) Prepared: 03/04/19 Analyzed: 03/05/19
Chromium g/L1.0 B, J0.76
Page 43 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
Batch B224896 - SW-846 3005A
LCS (B224896-BS1) Prepared: 03/04/19 Analyzed: 03/05/19
Chromium g/L10 500 80-120103514
LCS Dup (B224896-BSD1) Prepared: 03/04/19 Analyzed: 03/05/19
Chromium g/L10 500 2080-120104 1.41522
Page 44 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Analyte is found in the associated laboratory blank as well as in the sample.B
Data is not affected by elevated level in laboratory blank since sample result is >10x level found in the blank.B-07
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Elevated reporting limit due to high concentration of target compounds.RL-11
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-04
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
V-36
[TOC_1]Flag/Qualifier Summary[TOC]
Page 45 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 6020B in Water
CT,NH,NY,ME,VA,NCArsenic
CT,NH,NY,ME,VA,NCBarium
CT,NH,NY,RI,ME,VA,NCCadmium
CT,NH,NY,ME,VA,NCChromium
CT,NH,NY,ME,VA,NCLead
CT,NH,NY,ME,VA,NCSelenium
CT,NH,NY,ME,VA,NCSilver
SW-846 7470A in Water
CT,NH,NY,NC,ME,VAMercury
SW-846 8260D in Water
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
[TOC_1]Certifications[TOC]
Page 46 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Water
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D in Water
CT,NY,NC,ME,NH,VAAcenaphthene
CT,NY,NC,ME,NH,VAAcenaphthylene
NY,NCAcetophenone
CT,NY,NC,ME,VAAniline
CT,NY,NC,ME,NH,VAAnthracene
Page 47 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Water
CT,NY,NC,ME,NH,VABenzidine
CT,NY,NC,ME,NH,VABenzo(a)anthracene
CT,NY,NC,ME,NH,VABenzo(a)pyrene
CT,NY,NC,ME,NH,VABenzo(b)fluoranthene
CT,NY,NC,ME,NH,VABenzo(g,h,i)perylene
CT,NY,NC,ME,NH,VABenzo(k)fluoranthene
NY,NC,ME,NH,VABenzoic Acid
CT,NY,NC,ME,NH,VABis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VABis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VABis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VABis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA4-Bromophenylphenylether
CT,NY,NC,ME,NH,VAButylbenzylphthalate
NCCarbazole
CT,NY,NC,ME,NH,VA4-Chloroaniline
CT,NY,NC,ME,NH,VA4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA2-Chloronaphthalene
CT,NY,NC,ME,NH,VA2-Chlorophenol
CT,NY,NC,ME,NH,VA4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VAChrysene
CT,NY,NC,ME,NH,VADibenz(a,h)anthracene
CT,NY,NC,ME,NH,VADibenzofuran
CT,NY,NC,ME,NH,VADi-n-butylphthalate
CT,NY,NC,ME,NH,VA1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA2,4-Dichlorophenol
CT,NY,NC,ME,NH,VADiethylphthalate
CT,NY,NC,ME,NH,VA2,4-Dimethylphenol
CT,NY,NC,ME,NH,VADimethylphthalate
CT,NY,NC,ME,NH,VA4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VADi-n-octylphthalate
NY,NC1,2-Diphenylhydrazine/Azobenzene
CT,NY,NC,ME,NH,VAFluoranthene
NY,NC,ME,NH,VAFluorene
CT,NY,NC,ME,NH,VAHexachlorobenzene
CT,NY,NC,ME,NH,VAHexachlorobutadiene
CT,NY,NC,ME,NH,VAHexachlorocyclopentadiene
CT,NY,NC,ME,NH,VAHexachloroethane
CT,NY,NC,ME,NH,VAIndeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NC,ME,NH,VA2-Methylnaphthalene
Page 48 of 52
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Water
CT,NY,NC,NH,VA2-Methylphenol
CT,NY,NC,NH,VA3/4-Methylphenol
CT,NY,NC,ME,NH,VANaphthalene
CT,NY,NC,ME,NH,VA2-Nitroaniline
CT,NY,NC,ME,NH,VA3-Nitroaniline
CT,NY,NC,ME,NH,VA4-Nitroaniline
CT,NY,NC,ME,NH,VANitrobenzene
CT,NY,NC,ME,NH,VA2-Nitrophenol
CT,NY,NC,ME,NH,VA4-Nitrophenol
CT,NY,NC,ME,NH,VAN-Nitrosodimethylamine
CT,NY,NC,ME,NH,VAN-Nitrosodi-n-propylamine
NCPentachloronitrobenzene
CT,NY,NC,ME,NH,VAPentachlorophenol
CT,NY,NC,ME,NH,VAPhenanthrene
CT,NY,NC,ME,NH,VAPhenol
CT,NY,NC,ME,NH,VAPyrene
CT,NY,NC,ME,NH,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NC,ME,NH,VA1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
Page 49 of 52
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 4, 2019
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228-18-0495.03
Laboratory Work Order Number: 19B1092
Enclosed are results of analyses for samples received by the laboratory on February 25, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/4/2019Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0495.03
19B1092
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
SG-1 19B1092-01 Soil Gas EPA TO-15
SG-2 19B1092-02 Soil Gas EPA TO-15
SG-3 19B1092-03 Soil Gas EPA TO-15
SG-4 19B1092-04 Soil Gas EPA TO-15
SG-5 19B1092-05 Soil Gas EPA TO-15
SG-6 19B1092-06 Soil Gas EPA TO-15
SG-7 19B1092-07 Soil Gas EPA TO-15
SG-8 19B1092-08 Soil Gas EPA TO-15
Dup-2 19B1092-09 Soil Gas EPA TO-15
Page 2 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Elevated reporting limit due to matrix interference.
Analyte & Samples(s) Qualified:
19B1092-06[SG-6]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
19B1092-01[SG-1], 19B1092-02[SG-2], 19B1092-03[SG-3], 19B1092-04[SG-4], 19B1092-05[SG-5], 19B1092-06[SG-6], 19B1092-07[SG-7], 19B1092-08[SG-8],
19B1092-09[Dup-2], S033069-CCV1
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in
house limits of 50-150%.
Analyte & Samples(s) Qualified:
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
19B1092-01[SG-1], 19B1092-02[SG-2], 19B1092-03[SG-3], 19B1092-04[SG-4], 19B1092-05[SG-5], 19B1092-06[SG-6], 19B1092-07[SG-7], 19B1092-08[SG-8],
19B1092-09[Dup-2], B224871-BS1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 3 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19B1092-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 2/24/2019 11:15
Canister ID: 1209
Flow Controller ID: 4068
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 6.2 8.0 3/1/19 20:31 BRFJ15 4192.8 6.6
Benzene 4.5 0.20 3/1/19 20:31 BRF14 40.640.082 0.26
Benzyl chloride ND 0.20 3/1/19 20:31 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/1/19 20:31 BRFND41.30.074 0.49
Bromoform ND 0.20 3/1/19 20:31 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/1/19 20:31 BRFND40.780.14 0.53
1,3-Butadiene 4.4 0.20 3/1/19 20:31 BRF9.8 40.440.13 0.28
2-Butanone (MEK)1.9 8.0 3/1/19 20:31 BRFJ5.6 4240.31 0.92
Carbon Disulfide ND 2.0 3/1/19 20:31 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/1/19 20:31 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/1/19 20:31 BRFND40.920.098 0.45
Chloroethane ND 0.40 3/1/19 20:31 BRFND41.10.12 0.32
Chloroform 5.6 0.20 3/1/19 20:31 BRF27 40.980.074 0.36
Chloromethane ND 0.40 3/1/19 20:31 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/1/19 20:31 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/1/19 20:31 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/1/19 20:31 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/1/19 20:31 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/1/19 20:31 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/1/19 20:31 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.40 0.20 3/1/19 20:31 BRF2.0 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/1/19 20:31 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/1/19 20:31 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/1/19 20:31 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/1/19 20:31 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/1/19 20:31 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/1/19 20:31 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/1/19 20:31 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/1/19 20:31 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/1/19 20:31 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/1/19 20:31 BRFND47.21.3 4.6
Ethanol 6.7 8.0 3/1/19 20:31 BRFJ13 4153.6 6.7
Ethyl Acetate ND 0.40 3/1/19 20:31 BRFND41.40.15 0.54
Ethylbenzene 3.4 0.20 3/1/19 20:31 BRF15 40.870.12 0.50
4-Ethyltoluene 2.0 0.20 3/1/19 20:31 BRF9.9 40.980.12 0.60
Heptane 5.9 0.20 3/1/19 20:31 BRF24 40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/1/19 20:31 BRFND44.30.092 0.98
Hexane 7.8 8.0 3/1/19 20:31 BRFJ27 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/1/19 20:31 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/1/19 20:31 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/1/19 20:31 BRFND40.720.10 0.36
Methylene Chloride 0.62 2.0 3/1/19 20:31 BRFJ2.2 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)1.8 0.20 3/1/19 20:31 BRF7.6 40.820.096 0.39
Naphthalene ND 0.20 3/1/19 20:31 BRFND41.00.15 0.80
Propene ND 8.0 3/1/19 20:31 BRFND4140.20 0.34
Styrene ND 0.20 3/1/19 20:31 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/1/19 20:31 BRFND41.40.089 0.61
Page 4 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19B1092-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 2/24/2019 11:15
Canister ID: 1209
Flow Controller ID: 4068
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 5.1 0.20 3/1/19 20:31 BRF35 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/1/19 20:31 BRFND40.590.13 0.39
Toluene 35 0.20 3/1/19 20:31 BRF130 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/1/19 20:31 BRFND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/1/19 20:31 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/1/19 20:31 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/1/19 20:31 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.60 0.80 3/1/19 20:31 BRFJ3.4 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/1/19 20:31 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 1.8 0.20 3/1/19 20:31 BRF8.7 40.980.13 0.63
1,3,5-Trimethylbenzene 0.56 0.20 3/1/19 20:31 BRF2.8 40.980.13 0.62
Vinyl Acetate ND 4.0 3/1/19 20:31 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/1/19 20:31 BRFND40.510.13 0.32
m&p-Xylene 12 0.40 3/1/19 20:31 BRF51 41.70.23 1.00
o-Xylene 3.7 0.20 3/1/19 20:31 BRF16 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)105 3/1/19 20:3170-130
Page 5 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19B1092-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 2/24/2019 11:34
Canister ID: 1616
Flow Controller ID: 4103
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 5.7 8.0 3/1/19 21:28 BRFJ14 4192.8 6.6
Benzene 1.2 0.20 3/1/19 21:28 BRF3.8 40.640.082 0.26
Benzyl chloride ND 0.20 3/1/19 21:28 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/1/19 21:28 BRFND41.30.074 0.49
Bromoform ND 0.20 3/1/19 21:28 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/1/19 21:28 BRFND40.780.14 0.53
1,3-Butadiene 3.9 0.20 3/1/19 21:28 BRF8.7 40.440.13 0.28
2-Butanone (MEK)1.6 8.0 3/1/19 21:28 BRFJ4.8 4240.31 0.92
Carbon Disulfide ND 2.0 3/1/19 21:28 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/1/19 21:28 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/1/19 21:28 BRFND40.920.098 0.45
Chloroethane ND 0.40 3/1/19 21:28 BRFND41.10.12 0.32
Chloroform 23 0.20 3/1/19 21:28 BRF110 40.980.074 0.36
Chloromethane ND 0.40 3/1/19 21:28 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/1/19 21:28 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/1/19 21:28 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/1/19 21:28 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/1/19 21:28 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/1/19 21:28 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/1/19 21:28 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.88 0.20 3/1/19 21:28 BRF4.4 40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/1/19 21:28 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/1/19 21:28 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/1/19 21:28 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/1/19 21:28 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/1/19 21:28 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/1/19 21:28 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/1/19 21:28 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/1/19 21:28 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/1/19 21:28 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/1/19 21:28 BRFND47.21.3 4.6
Ethanol 4.3 8.0 3/1/19 21:28 BRFJ8.0 4153.6 6.7
Ethyl Acetate ND 0.40 3/1/19 21:28 BRFND41.40.15 0.54
Ethylbenzene 0.17 0.20 3/1/19 21:28 BRFJ0.75 40.870.12 0.50
4-Ethyltoluene ND 0.20 3/1/19 21:28 BRFND40.980.12 0.60
Heptane 0.95 0.20 3/1/19 21:28 BRF3.9 40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/1/19 21:28 BRFND44.30.092 0.98
Hexane ND 8.0 3/1/19 21:28 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/1/19 21:28 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/1/19 21:28 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/1/19 21:28 BRFND40.720.10 0.36
Methylene Chloride 4.7 2.0 3/1/19 21:28 BRF16 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)1.2 0.20 3/1/19 21:28 BRF4.8 40.820.096 0.39
Naphthalene ND 0.20 3/1/19 21:28 BRFND41.00.15 0.80
Propene ND 8.0 3/1/19 21:28 BRFND4140.20 0.34
Styrene ND 0.20 3/1/19 21:28 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/1/19 21:28 BRFND41.40.089 0.61
Page 6 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19B1092-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.7
Sampled: 2/24/2019 11:34
Canister ID: 1616
Flow Controller ID: 4103
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 3/1/19 21:28 BRFND41.40.11 0.75
Tetrahydrofuran ND 0.20 3/1/19 21:28 BRFND40.590.13 0.39
Toluene 1.2 0.20 3/1/19 21:28 BRF4.6 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/1/19 21:28 BRFND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/1/19 21:28 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/1/19 21:28 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/1/19 21:28 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.33 0.80 3/1/19 21:28 BRFJ1.9 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/1/19 21:28 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 0.18 0.20 3/1/19 21:28 BRFJ0.90 40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/1/19 21:28 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/1/19 21:28 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/1/19 21:28 BRFND40.510.13 0.32
m&p-Xylene 0.46 0.40 3/1/19 21:28 BRF2.0 41.70.23 1.00
o-Xylene 0.18 0.20 3/1/19 21:28 BRFJ0.76 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)103 3/1/19 21:2870-130
Page 7 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-3
Sample ID: 19B1092-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -3
Receipt Vacuum(in Hg): -5.4
Sampled: 2/24/2019 11:38
Canister ID: 1020
Flow Controller ID: 4293
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 7.3 8.0 3/1/19 21:56 BRFJ17 4192.8 6.6
Benzene 2.9 0.20 3/1/19 21:56 BRF9.3 40.640.082 0.26
Benzyl chloride ND 0.20 3/1/19 21:56 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/1/19 21:56 BRFND41.30.074 0.49
Bromoform ND 0.20 3/1/19 21:56 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/1/19 21:56 BRFND40.780.14 0.53
1,3-Butadiene 3.9 0.20 3/1/19 21:56 BRF8.5 40.440.13 0.28
2-Butanone (MEK)2.2 8.0 3/1/19 21:56 BRFJ6.6 4240.31 0.92
Carbon Disulfide ND 2.0 3/1/19 21:56 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/1/19 21:56 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/1/19 21:56 BRFND40.920.098 0.45
Chloroethane ND 0.40 3/1/19 21:56 BRFND41.10.12 0.32
Chloroform 2.6 0.20 3/1/19 21:56 BRF13 40.980.074 0.36
Chloromethane ND 0.40 3/1/19 21:56 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/1/19 21:56 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/1/19 21:56 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/1/19 21:56 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/1/19 21:56 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/1/19 21:56 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/1/19 21:56 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/1/19 21:56 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/1/19 21:56 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/1/19 21:56 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/1/19 21:56 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/1/19 21:56 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/1/19 21:56 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/1/19 21:56 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/1/19 21:56 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/1/19 21:56 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/1/19 21:56 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/1/19 21:56 BRFND47.21.3 4.6
Ethanol 4.0 8.0 3/1/19 21:56 BRFJ7.5 4153.6 6.7
Ethyl Acetate ND 0.40 3/1/19 21:56 BRFND41.40.15 0.54
Ethylbenzene 2.1 0.20 3/1/19 21:56 BRF9.2 40.870.12 0.50
4-Ethyltoluene 0.82 0.20 3/1/19 21:56 BRF4.0 40.980.12 0.60
Heptane 4.2 0.20 3/1/19 21:56 BRF17 40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/1/19 21:56 BRFND44.30.092 0.98
Hexane 7.0 8.0 3/1/19 21:56 BRFJ25 4280.35 1.2
2-Hexanone (MBK)1.3 0.20 3/1/19 21:56 BRF5.1 40.820.12 0.48
Isopropanol ND 8.0 3/1/19 21:56 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/1/19 21:56 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/1/19 21:56 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)2.0 0.20 3/1/19 21:56 BRF8.4 40.820.096 0.39
Naphthalene ND 0.20 3/1/19 21:56 BRFND41.00.15 0.80
Propene 49 8.0 3/1/19 21:56 BRF85 4140.20 0.34
Styrene ND 0.20 3/1/19 21:56 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/1/19 21:56 BRFND41.40.089 0.61
Page 8 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-3
Sample ID: 19B1092-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -3
Receipt Vacuum(in Hg): -5.4
Sampled: 2/24/2019 11:38
Canister ID: 1020
Flow Controller ID: 4293
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 3.5 0.20 3/1/19 21:56 BRF24 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/1/19 21:56 BRFND40.590.13 0.39
Toluene 23 0.20 3/1/19 21:56 BRF85 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/1/19 21:56 BRFND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/1/19 21:56 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/1/19 21:56 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/1/19 21:56 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.34 0.80 3/1/19 21:56 BRFJ1.9 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/1/19 21:56 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 0.57 0.20 3/1/19 21:56 BRF2.8 40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/1/19 21:56 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/1/19 21:56 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/1/19 21:56 BRFND40.510.13 0.32
m&p-Xylene 6.9 0.40 3/1/19 21:56 BRF30 41.70.23 1.00
o-Xylene 2.1 0.20 3/1/19 21:56 BRF9.3 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 3/1/19 21:5670-130
Page 9 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-4
Sample ID: 19B1092-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -6.9
Sampled: 2/24/2019 11:48
Canister ID: 1247
Flow Controller ID: 4292
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 5.4 8.0 3/1/19 22:25 BRFJ13 4192.8 6.6
Benzene 0.38 0.20 3/1/19 22:25 BRF1.2 40.640.082 0.26
Benzyl chloride ND 0.20 3/1/19 22:25 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/1/19 22:25 BRFND41.30.074 0.49
Bromoform ND 0.20 3/1/19 22:25 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/1/19 22:25 BRFND40.780.14 0.53
1,3-Butadiene 1.5 0.20 3/1/19 22:25 BRF3.4 40.440.13 0.28
2-Butanone (MEK)1.4 8.0 3/1/19 22:25 BRFJ4.0 4240.31 0.92
Carbon Disulfide ND 2.0 3/1/19 22:25 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/1/19 22:25 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/1/19 22:25 BRFND40.920.098 0.45
Chloroethane ND 0.40 3/1/19 22:25 BRFND41.10.12 0.32
Chloroform 5.3 0.20 3/1/19 22:25 BRF26 40.980.074 0.36
Chloromethane ND 0.40 3/1/19 22:25 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/1/19 22:25 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/1/19 22:25 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/1/19 22:25 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/1/19 22:25 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/1/19 22:25 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/1/19 22:25 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/1/19 22:25 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/1/19 22:25 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/1/19 22:25 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/1/19 22:25 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/1/19 22:25 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/1/19 22:25 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/1/19 22:25 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/1/19 22:25 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/1/19 22:25 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/1/19 22:25 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/1/19 22:25 BRFND47.21.3 4.6
Ethanol 6.5 8.0 3/1/19 22:25 BRFJ12 4153.6 6.7
Ethyl Acetate ND 0.40 3/1/19 22:25 BRFND41.40.15 0.54
Ethylbenzene ND 0.20 3/1/19 22:25 BRFND40.870.12 0.50
4-Ethyltoluene ND 0.20 3/1/19 22:25 BRFND40.980.12 0.60
Heptane ND 0.20 3/1/19 22:25 BRFND40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/1/19 22:25 BRFND44.30.092 0.98
Hexane ND 8.0 3/1/19 22:25 BRFND4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/1/19 22:25 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/1/19 22:25 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/1/19 22:25 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/1/19 22:25 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)ND 0.20 3/1/19 22:25 BRFND40.820.096 0.39
Naphthalene ND 0.20 3/1/19 22:25 BRFND41.00.15 0.80
Propene ND 8.0 3/1/19 22:25 BRFND4140.20 0.34
Styrene ND 0.20 3/1/19 22:25 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/1/19 22:25 BRFND41.40.089 0.61
Page 10 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-4
Sample ID: 19B1092-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -6.9
Sampled: 2/24/2019 11:48
Canister ID: 1247
Flow Controller ID: 4292
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 3/1/19 22:25 BRFND41.40.11 0.75
Tetrahydrofuran ND 0.20 3/1/19 22:25 BRFND40.590.13 0.39
Toluene 0.58 0.20 3/1/19 22:25 BRF2.2 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/1/19 22:25 BRFND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/1/19 22:25 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/1/19 22:25 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/1/19 22:25 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.54 0.80 3/1/19 22:25 BRFJ3.0 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/1/19 22:25 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 3/1/19 22:25 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/1/19 22:25 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 3/1/19 22:25 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/1/19 22:25 BRFND40.510.13 0.32
m&p-Xylene ND 0.40 3/1/19 22:25 BRFND41.70.23 1.00
o-Xylene ND 0.20 3/1/19 22:25 BRFND40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)104 3/1/19 22:2570-130
Page 11 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-5
Sample ID: 19B1092-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -7
Sampled: 2/24/2019 13:00
Canister ID: 1077
Flow Controller ID: 4312
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 12 8.0 3/1/19 22:54 BRF29 4192.8 6.6
Benzene 2.9 0.20 3/1/19 22:54 BRF9.3 40.640.082 0.26
Benzyl chloride ND 0.20 3/1/19 22:54 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/1/19 22:54 BRFND41.30.074 0.49
Bromoform ND 0.20 3/1/19 22:54 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/1/19 22:54 BRFND40.780.14 0.53
1,3-Butadiene 3.2 0.20 3/1/19 22:54 BRF7.0 40.440.13 0.28
2-Butanone (MEK)2.3 8.0 3/1/19 22:54 BRFJ6.6 4240.31 0.92
Carbon Disulfide ND 2.0 3/1/19 22:54 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/1/19 22:54 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/1/19 22:54 BRFND40.920.098 0.45
Chloroethane ND 0.40 3/1/19 22:54 BRFND41.10.12 0.32
Chloroform ND 0.20 3/1/19 22:54 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/1/19 22:54 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/1/19 22:54 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/1/19 22:54 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/1/19 22:54 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/1/19 22:54 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/1/19 22:54 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/1/19 22:54 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/1/19 22:54 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/1/19 22:54 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/1/19 22:54 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/1/19 22:54 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/1/19 22:54 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/1/19 22:54 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/1/19 22:54 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/1/19 22:54 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/1/19 22:54 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/1/19 22:54 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/1/19 22:54 BRFND47.21.3 4.6
Ethanol 4.1 8.0 3/1/19 22:54 BRFJ7.7 4153.6 6.7
Ethyl Acetate ND 0.40 3/1/19 22:54 BRFND41.40.15 0.54
Ethylbenzene 2.9 0.20 3/1/19 22:54 BRF13 40.870.12 0.50
4-Ethyltoluene 2.0 0.20 3/1/19 22:54 BRF9.7 40.980.12 0.60
Heptane 4.2 0.20 3/1/19 22:54 BRF17 40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/1/19 22:54 BRFND44.30.092 0.98
Hexane 6.5 8.0 3/1/19 22:54 BRFJ23 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/1/19 22:54 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/1/19 22:54 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/1/19 22:54 BRFND40.720.10 0.36
Methylene Chloride 0.25 2.0 3/1/19 22:54 BRFJ0.88 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)1.7 0.20 3/1/19 22:54 BRF6.8 40.820.096 0.39
Naphthalene ND 0.20 3/1/19 22:54 BRFND41.00.15 0.80
Propene ND 8.0 3/1/19 22:54 BRFND4140.20 0.34
Styrene ND 0.20 3/1/19 22:54 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/1/19 22:54 BRFND41.40.089 0.61
Page 12 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-5
Sample ID: 19B1092-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -4
Receipt Vacuum(in Hg): -7
Sampled: 2/24/2019 13:00
Canister ID: 1077
Flow Controller ID: 4312
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 3.9 0.20 3/1/19 22:54 BRF27 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/1/19 22:54 BRFND40.590.13 0.39
Toluene 26 0.20 3/1/19 22:54 BRF97 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/1/19 22:54 BRFND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/1/19 22:54 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/1/19 22:54 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/1/19 22:54 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.32 0.80 3/1/19 22:54 BRFJ1.8 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/1/19 22:54 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 2.0 0.20 3/1/19 22:54 BRF10.0 40.980.13 0.63
1,3,5-Trimethylbenzene 0.60 0.20 3/1/19 22:54 BRF3.0 40.980.13 0.62
Vinyl Acetate ND 4.0 3/1/19 22:54 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/1/19 22:54 BRFND40.510.13 0.32
m&p-Xylene 11 0.40 3/1/19 22:54 BRF46 41.70.23 1.00
o-Xylene 3.5 0.20 3/1/19 22:54 BRF15 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 3/1/19 22:5470-130
Page 13 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-6
Sample ID: 19B1092-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -24
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -7.7
Sampled: 2/24/2019 12:50
Canister ID: 1081
Flow Controller ID: 4183
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
Sample Flags: RL-12
MDL MDL
Acetone 8.2 20 3/1/19 23:21 BRFJ20 10486.9 16
Benzene 2.4 0.50 3/1/19 23:21 BRF7.6 101.60.21 0.66
Benzyl chloride ND 0.50 3/1/19 23:21 BRFND102.60.11 0.57
Bromodichloromethane ND 0.50 3/1/19 23:21 BRFND103.40.18 1.2
Bromoform ND 0.50 3/1/19 23:21 BRFND105.20.22 2.3
Bromomethane ND 0.50 3/1/19 23:21 BRFND101.90.34 1.3
1,3-Butadiene ND 0.50 3/1/19 23:21 BRFND101.10.32 0.70
2-Butanone (MEK)7.5 20 3/1/19 23:21 BRFJ22 10590.78 2.3
Carbon Disulfide ND 5.0 3/1/19 23:21 BRFND10160.34 1.1
Carbon Tetrachloride ND 0.50 3/1/19 23:21 BRFND103.10.16 1.0
Chlorobenzene ND 0.50 3/1/19 23:21 BRFND102.30.24 1.1
Chloroethane ND 1.0 3/1/19 23:21 BRFND102.60.30 0.80
Chloroform ND 0.50 3/1/19 23:21 BRFND102.40.19 0.91
Chloromethane ND 1.0 3/1/19 23:21 BRFND102.10.34 0.70
Cyclohexane 14 0.50 3/1/19 23:21 BRF47 101.70.36 1.2
Dibromochloromethane ND 0.50 3/1/19 23:21 BRFND104.30.17 1.4
1,2-Dibromoethane (EDB)ND 0.50 3/1/19 23:21 BRFND103.80.20 1.5
1,2-Dichlorobenzene ND 0.50 3/1/19 23:21 BRFND103.00.24 1.4
1,3-Dichlorobenzene ND 0.50 3/1/19 23:21 BRFND103.00.26 1.6
1,4-Dichlorobenzene ND 0.50 3/1/19 23:21 BRFND103.00.30 1.8
Dichlorodifluoromethane (Freon 12)ND 0.50 3/1/19 23:21 BRFND102.50.22 1.1
1,1-Dichloroethane ND 0.50 3/1/19 23:21 BRFND102.00.15 0.62
1,2-Dichloroethane ND 0.50 3/1/19 23:21 BRFND102.00.19 0.77
1,1-Dichloroethylene ND 0.50 3/1/19 23:21 BRFND102.00.20 0.80
cis-1,2-Dichloroethylene ND 0.50 3/1/19 23:21 BRFND102.00.20 0.81
trans-1,2-Dichloroethylene ND 0.50 3/1/19 23:21 BRFND102.00.20 0.80
1,2-Dichloropropane ND 0.50 3/1/19 23:21 BRFND102.30.18 0.82
cis-1,3-Dichloropropene ND 0.50 3/1/19 23:21 BRFND102.30.18 0.79
trans-1,3-Dichloropropene ND 0.50 3/1/19 23:21 BRFND102.30.18 0.83
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.50 3/1/19 23:21 BRFV-05, Z-01 ND 103.50.25 1.7
1,4-Dioxane ND 5.0 3/1/19 23:21 BRFND10183.2 12
Ethanol ND 20 3/1/19 23:21 BRFND10388.9 17
Ethyl Acetate ND 1.0 3/1/19 23:21 BRFND103.60.37 1.3
Ethylbenzene 1.0 0.50 3/1/19 23:21 BRF4.5 102.20.29 1.3
4-Ethyltoluene ND 0.50 3/1/19 23:21 BRFND102.50.30 1.5
Heptane 4.6 0.50 3/1/19 23:21 BRF19 102.00.29 1.2
Hexachlorobutadiene ND 1.0 3/1/19 23:21 BRFND10110.23 2.5
Hexane 18 20 3/1/19 23:21 BRFJ64 10700.88 3.1
2-Hexanone (MBK)ND 0.50 3/1/19 23:21 BRFND102.00.30 1.2
Isopropanol 1.8 20 3/1/19 23:21 BRFJ4.3 10490.61 1.5
Methyl tert-Butyl Ether (MTBE)ND 0.50 3/1/19 23:21 BRFND101.80.25 0.90
Methylene Chloride ND 5.0 3/1/19 23:21 BRFND10170.61 2.1
4-Methyl-2-pentanone (MIBK)1.8 0.50 3/1/19 23:21 BRF7.3 102.00.24 0.99
Naphthalene ND 0.50 3/1/19 23:21 BRFND102.60.38 2.0
Propene ND 20 3/1/19 23:21 BRFND10340.50 0.85
Styrene ND 0.50 3/1/19 23:21 BRFND102.10.31 1.3
1,1,2,2-Tetrachloroethane ND 0.50 3/1/19 23:21 BRFND103.40.22 1.5
Page 14 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-6
Sample ID: 19B1092-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -24
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -7.7
Sampled: 2/24/2019 12:50
Canister ID: 1081
Flow Controller ID: 4183
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
Sample Flags: RL-12
MDL MDL
Tetrachloroethylene 16 0.50 3/1/19 23:21 BRF110 103.40.28 1.9
Tetrahydrofuran ND 0.50 3/1/19 23:21 BRFND101.50.33 0.98
Toluene 8.1 0.50 3/1/19 23:21 BRF31 101.90.26 0.97
1,2,4-Trichlorobenzene ND 1.0 3/1/19 23:21 BRFND107.40.34 2.6
1,1,1-Trichloroethane ND 0.50 3/1/19 23:21 BRFND102.70.19 1.0
1,1,2-Trichloroethane ND 0.50 3/1/19 23:21 BRFND102.70.21 1.1
Trichloroethylene ND 0.50 3/1/19 23:21 BRFND102.70.20 1.1
Trichlorofluoromethane (Freon 11)ND 2.0 3/1/19 23:21 BRFND10110.29 1.6
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 2.0 3/1/19 23:21 BRFND10150.30 2.3
1,2,4-Trimethylbenzene ND 0.50 3/1/19 23:21 BRFND102.50.32 1.6
1,3,5-Trimethylbenzene ND 0.50 3/1/19 23:21 BRFND102.50.31 1.5
Vinyl Acetate ND 10 3/1/19 23:21 BRFND10350.24 0.84
Vinyl Chloride ND 0.50 3/1/19 23:21 BRFND101.30.32 0.81
m&p-Xylene 3.2 1.0 3/1/19 23:21 BRF14 104.30.58 2.5
o-Xylene 1.8 0.50 3/1/19 23:21 BRF7.9 102.20.31 1.4
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)104 3/1/19 23:2170-130
Page 15 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-7
Sample ID: 19B1092-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -1
Receipt Vacuum(in Hg): -3.7
Sampled: 2/24/2019 12:45
Canister ID: 1076
Flow Controller ID: 4182
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 9.0 8.0 3/1/19 23:50 BRF21 4192.8 6.6
Benzene 3.2 0.20 3/1/19 23:50 BRF10 40.640.082 0.26
Benzyl chloride ND 0.20 3/1/19 23:50 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/1/19 23:50 BRFND41.30.074 0.49
Bromoform ND 0.20 3/1/19 23:50 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/1/19 23:50 BRFND40.780.14 0.53
1,3-Butadiene 6.7 0.20 3/1/19 23:50 BRF15 40.440.13 0.28
2-Butanone (MEK)2.5 8.0 3/1/19 23:50 BRFJ7.4 4240.31 0.92
Carbon Disulfide ND 2.0 3/1/19 23:50 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/1/19 23:50 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/1/19 23:50 BRFND40.920.098 0.45
Chloroethane ND 0.40 3/1/19 23:50 BRFND41.10.12 0.32
Chloroform ND 0.20 3/1/19 23:50 BRFND40.980.074 0.36
Chloromethane ND 0.40 3/1/19 23:50 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/1/19 23:50 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/1/19 23:50 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/1/19 23:50 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/1/19 23:50 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/1/19 23:50 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/1/19 23:50 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/1/19 23:50 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/1/19 23:50 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/1/19 23:50 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/1/19 23:50 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/1/19 23:50 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/1/19 23:50 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/1/19 23:50 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/1/19 23:50 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/1/19 23:50 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/1/19 23:50 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/1/19 23:50 BRFND47.21.3 4.6
Ethanol 4.0 8.0 3/1/19 23:50 BRFJ7.5 4153.6 6.7
Ethyl Acetate ND 0.40 3/1/19 23:50 BRFND41.40.15 0.54
Ethylbenzene 2.4 0.20 3/1/19 23:50 BRF10 40.870.12 0.50
4-Ethyltoluene 1.8 0.20 3/1/19 23:50 BRF8.9 40.980.12 0.60
Heptane 4.0 0.20 3/1/19 23:50 BRF16 40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/1/19 23:50 BRFND44.30.092 0.98
Hexane 7.6 8.0 3/1/19 23:50 BRFJ27 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/1/19 23:50 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/1/19 23:50 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/1/19 23:50 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 3/1/19 23:50 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)1.4 0.20 3/1/19 23:50 BRF5.8 40.820.096 0.39
Naphthalene ND 0.20 3/1/19 23:50 BRFND41.00.15 0.80
Propene ND 8.0 3/1/19 23:50 BRFND4140.20 0.34
Styrene ND 0.20 3/1/19 23:50 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/1/19 23:50 BRFND41.40.089 0.61
Page 16 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-7
Sample ID: 19B1092-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -1
Receipt Vacuum(in Hg): -3.7
Sampled: 2/24/2019 12:45
Canister ID: 1076
Flow Controller ID: 4182
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 3.3 0.20 3/1/19 23:50 BRF23 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/1/19 23:50 BRFND40.590.13 0.39
Toluene 20 0.20 3/1/19 23:50 BRF75 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/1/19 23:50 BRFND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/1/19 23:50 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/1/19 23:50 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/1/19 23:50 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.30 0.80 3/1/19 23:50 BRFJ1.7 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/1/19 23:50 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 2.2 0.20 3/1/19 23:50 BRF11 40.980.13 0.63
1,3,5-Trimethylbenzene 0.64 0.20 3/1/19 23:50 BRF3.2 40.980.13 0.62
Vinyl Acetate ND 4.0 3/1/19 23:50 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/1/19 23:50 BRFND40.510.13 0.32
m&p-Xylene 8.5 0.40 3/1/19 23:50 BRF37 41.70.23 1.00
o-Xylene 3.1 0.20 3/1/19 23:50 BRF14 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 3/1/19 23:5070-130
Page 17 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-8
Sample ID: 19B1092-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -6.8
Sampled: 2/24/2019 13:46
Canister ID: 1315
Flow Controller ID: 4313
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 13 8.0 3/2/19 0:18 BRF31 4192.8 6.6
Benzene 4.9 0.20 3/2/19 0:18 BRF16 40.640.082 0.26
Benzyl chloride ND 0.20 3/2/19 0:18 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 3/2/19 0:18 BRFND41.30.074 0.49
Bromoform ND 0.20 3/2/19 0:18 BRFND42.10.090 0.93
Bromomethane ND 0.20 3/2/19 0:18 BRFND40.780.14 0.53
1,3-Butadiene 5.5 0.20 3/2/19 0:18 BRF12 40.440.13 0.28
2-Butanone (MEK)3.0 8.0 3/2/19 0:18 BRFJ8.9 4240.31 0.92
Carbon Disulfide ND 2.0 3/2/19 0:18 BRFND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/2/19 0:18 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 3/2/19 0:18 BRFND40.920.098 0.45
Chloroethane ND 0.40 3/2/19 0:18 BRFND41.10.12 0.32
Chloroform 1.1 0.20 3/2/19 0:18 BRF5.4 40.980.074 0.36
Chloromethane ND 0.40 3/2/19 0:18 BRFND40.830.14 0.28
Cyclohexane ND 0.20 3/2/19 0:18 BRFND40.690.14 0.49
Dibromochloromethane ND 0.20 3/2/19 0:18 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/2/19 0:18 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/2/19 0:18 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/2/19 0:18 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/2/19 0:18 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/2/19 0:18 BRFND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/2/19 0:18 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/2/19 0:18 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/2/19 0:18 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/2/19 0:18 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/2/19 0:18 BRFND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/2/19 0:18 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/2/19 0:18 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/2/19 0:18 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/2/19 0:18 BRFV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/2/19 0:18 BRFND47.21.3 4.6
Ethanol ND 8.0 3/2/19 0:18 BRFND4153.6 6.7
Ethyl Acetate ND 0.40 3/2/19 0:18 BRFND41.40.15 0.54
Ethylbenzene 5.1 0.20 3/2/19 0:18 BRF22 40.870.12 0.50
4-Ethyltoluene 4.0 0.20 3/2/19 0:18 BRF20 40.980.12 0.60
Heptane 5.3 0.20 3/2/19 0:18 BRF22 40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/2/19 0:18 BRFND44.30.092 0.98
Hexane 7.7 8.0 3/2/19 0:18 BRFJ27 4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/2/19 0:18 BRFND40.820.12 0.48
Isopropanol ND 8.0 3/2/19 0:18 BRFND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/2/19 0:18 BRFND40.720.10 0.36
Methylene Chloride 0.52 2.0 3/2/19 0:18 BRFJ1.8 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)1.6 0.20 3/2/19 0:18 BRF6.5 40.820.096 0.39
Naphthalene ND 0.20 3/2/19 0:18 BRFND41.00.15 0.80
Propene ND 8.0 3/2/19 0:18 BRFND4140.20 0.34
Styrene ND 0.20 3/2/19 0:18 BRFND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/2/19 0:18 BRFND41.40.089 0.61
Page 18 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: SG-8
Sample ID: 19B1092-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -6.8
Sampled: 2/24/2019 13:46
Canister ID: 1315
Flow Controller ID: 4313
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 5.5 0.20 3/2/19 0:18 BRF37 41.40.11 0.75
Tetrahydrofuran ND 0.20 3/2/19 0:18 BRFND40.590.13 0.39
Toluene 41 0.20 3/2/19 0:18 BRF160 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/2/19 0:18 BRFND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/2/19 0:18 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/2/19 0:18 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 3/2/19 0:18 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.39 0.80 3/2/19 0:18 BRFJ2.2 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/2/19 0:18 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene 4.6 0.20 3/2/19 0:18 BRF23 40.980.13 0.63
1,3,5-Trimethylbenzene 1.3 0.20 3/2/19 0:18 BRF6.6 40.980.13 0.62
Vinyl Acetate ND 4.0 3/2/19 0:18 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 3/2/19 0:18 BRFND40.510.13 0.32
m&p-Xylene 18 0.40 3/2/19 0:18 BRF80 41.70.23 1.00
o-Xylene 6.3 0.20 3/2/19 0:18 BRF27 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)108 3/2/19 0:1870-130
Page 19 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: Dup-2
Sample ID: 19B1092-09
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.2
Sampled: 2/24/2019 00:00
Canister ID: 1865
Flow Controller ID: 4104
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 8.5 8.0 3/2/19 10:56 TPH20 4192.8 6.6
Benzene 0.59 0.20 3/2/19 10:56 TPH1.9 40.640.082 0.26
Benzyl chloride ND 0.20 3/2/19 10:56 TPHND41.00.044 0.23
Bromodichloromethane ND 0.20 3/2/19 10:56 TPHND41.30.074 0.49
Bromoform ND 0.20 3/2/19 10:56 TPHND42.10.090 0.93
Bromomethane ND 0.20 3/2/19 10:56 TPHND40.780.14 0.53
1,3-Butadiene ND 0.20 3/2/19 10:56 TPHND40.440.13 0.28
2-Butanone (MEK)1.8 8.0 3/2/19 10:56 TPHJ5.3 4240.31 0.92
Carbon Disulfide ND 2.0 3/2/19 10:56 TPHND46.20.14 0.43
Carbon Tetrachloride ND 0.20 3/2/19 10:56 TPHND41.30.065 0.41
Chlorobenzene ND 0.20 3/2/19 10:56 TPHND40.920.098 0.45
Chloroethane ND 0.40 3/2/19 10:56 TPHND41.10.12 0.32
Chloroform 28 0.20 3/2/19 10:56 TPH140 40.980.074 0.36
Chloromethane ND 0.40 3/2/19 10:56 TPHND40.830.14 0.28
Cyclohexane ND 0.20 3/2/19 10:56 TPHND40.690.14 0.49
Dibromochloromethane ND 0.20 3/2/19 10:56 TPHND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/2/19 10:56 TPHND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 3/2/19 10:56 TPHND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 3/2/19 10:56 TPHND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 3/2/19 10:56 TPHND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)ND 0.20 3/2/19 10:56 TPHND40.990.087 0.43
1,1-Dichloroethane ND 0.20 3/2/19 10:56 TPHND40.810.061 0.25
1,2-Dichloroethane ND 0.20 3/2/19 10:56 TPHND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 3/2/19 10:56 TPHND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 3/2/19 10:56 TPHND40.790.082 0.32
trans-1,2-Dichloroethylene ND 0.20 3/2/19 10:56 TPHND40.790.081 0.32
1,2-Dichloropropane ND 0.20 3/2/19 10:56 TPHND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 3/2/19 10:56 TPHND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 3/2/19 10:56 TPHND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/2/19 10:56 TPHV-05, Z-01 ND 41.40.10 0.70
1,4-Dioxane ND 2.0 3/2/19 10:56 TPHND47.21.3 4.6
Ethanol 3.6 8.0 3/2/19 10:56 TPHJ6.8 4153.6 6.7
Ethyl Acetate ND 0.40 3/2/19 10:56 TPHND41.40.15 0.54
Ethylbenzene ND 0.20 3/2/19 10:56 TPHND40.870.12 0.50
4-Ethyltoluene ND 0.20 3/2/19 10:56 TPHND40.980.12 0.60
Heptane 0.59 0.20 3/2/19 10:56 TPH2.4 40.820.12 0.48
Hexachlorobutadiene ND 0.40 3/2/19 10:56 TPHND44.30.092 0.98
Hexane ND 8.0 3/2/19 10:56 TPHND4280.35 1.2
2-Hexanone (MBK)ND 0.20 3/2/19 10:56 TPHND40.820.12 0.48
Isopropanol ND 8.0 3/2/19 10:56 TPHND4200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/2/19 10:56 TPHND40.720.10 0.36
Methylene Chloride 5.3 2.0 3/2/19 10:56 TPH18 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)0.68 0.20 3/2/19 10:56 TPH2.8 40.820.096 0.39
Naphthalene ND 0.20 3/2/19 10:56 TPHND41.00.15 0.80
Propene ND 8.0 3/2/19 10:56 TPHND4140.20 0.34
Styrene ND 0.20 3/2/19 10:56 TPHND40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 3/2/19 10:56 TPHND41.40.089 0.61
Page 20 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 2/25/2019
Work Order: 19B1092Sample Description/Location:
Field Sample #: Dup-2
Sample ID: 19B1092-09
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.2
Sampled: 2/24/2019 00:00
Canister ID: 1865
Flow Controller ID: 4104
Sub Description/Location:
Canister Size: 6 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 30 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 3/2/19 10:56 TPHND41.40.11 0.75
Tetrahydrofuran ND 0.20 3/2/19 10:56 TPHND40.590.13 0.39
Toluene 1.2 0.20 3/2/19 10:56 TPH4.6 40.750.10 0.39
1,2,4-Trichlorobenzene ND 0.40 3/2/19 10:56 TPHND43.00.14 1.0
1,1,1-Trichloroethane ND 0.20 3/2/19 10:56 TPHND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 3/2/19 10:56 TPHND41.10.082 0.45
Trichloroethylene ND 0.20 3/2/19 10:56 TPHND41.10.081 0.43
Trichlorofluoromethane (Freon 11)0.37 0.80 3/2/19 10:56 TPHJ2.1 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/2/19 10:56 TPHND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 3/2/19 10:56 TPHND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 3/2/19 10:56 TPHND40.980.13 0.62
Vinyl Acetate ND 4.0 3/2/19 10:56 TPHND4140.095 0.34
Vinyl Chloride ND 0.20 3/2/19 10:56 TPHND40.510.13 0.32
m&p-Xylene 0.36 0.40 3/2/19 10:56 TPHJ1.6 41.70.23 1.00
o-Xylene 0.13 0.20 3/2/19 10:56 TPHJ0.57 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)106 3/2/19 10:5670-130
Page 21 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
19B1092-01 [SG-1]B224871 1.5 1 N/A 1000 400 150 03/01/19
19B1092-02 [SG-2]B224871 1.5 1 N/A 1000 400 150 03/01/19
19B1092-03 [SG-3]B224871 1.5 1 N/A 1000 400 150 03/01/19
19B1092-04 [SG-4]B224871 1.5 1 N/A 1000 400 150 03/01/19
19B1092-05 [SG-5]B224871 1.5 1 N/A 1000 400 150 03/01/19
19B1092-06 [SG-6]B224871 1.5 1 N/A 1000 400 60 03/01/19
19B1092-07 [SG-7]B224871 1.5 1 N/A 1000 400 150 03/01/19
19B1092-08 [SG-8]B224871 1.5 1 N/A 1000 400 150 03/01/19
19B1092-09 [Dup-2]B224871 1.5 1 N/A 1000 400 150 03/01/19
Page 22 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B224871 - TO-15 Prep
Blank (B224871-BLK1)Prepared & Analyzed: 03/01/19
1.4NDAcetone
0.035NDBenzene
0.035NDBenzyl chloride
0.035NDBromodichloromethane
0.035NDBromoform
0.035NDBromomethane
0.035ND1,3-Butadiene
1.4ND2-Butanone (MEK)
0.35NDCarbon Disulfide
0.035NDCarbon Tetrachloride
0.035NDChlorobenzene
0.035NDChloroethane
0.035NDChloroform
0.070NDChloromethane
0.035NDCyclohexane
0.035NDDibromochloromethane
0.035ND1,2-Dibromoethane (EDB)
0.035ND1,2-Dichlorobenzene
0.035ND1,3-Dichlorobenzene
0.035ND1,4-Dichlorobenzene
0.035NDDichlorodifluoromethane (Freon 12)
0.035ND1,1-Dichloroethane
0.035ND1,2-Dichloroethane
0.035ND1,1-Dichloroethylene
0.035NDcis-1,2-Dichloroethylene
0.035NDtrans-1,2-Dichloroethylene
0.035ND1,2-Dichloropropane
0.035NDcis-1,3-Dichloropropene
0.035NDtrans-1,3-Dichloropropene
0.035ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.35ND1,4-Dioxane
1.4NDEthanol
0.035NDEthyl Acetate
0.035NDEthylbenzene
0.035ND4-Ethyltoluene
0.035NDHeptane
0.035NDHexachlorobutadiene
1.4NDHexane
0.035ND2-Hexanone (MBK)
1.4NDIsopropanol
0.035NDMethyl tert-Butyl Ether (MTBE)
0.35NDMethylene Chloride
0.035ND4-Methyl-2-pentanone (MIBK)
0.035NDNaphthalene
1.4NDPropene
0.035NDStyrene
Page 23 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B224871 - TO-15 Prep
Blank (B224871-BLK1)Prepared & Analyzed: 03/01/19
0.035ND1,1,2,2-Tetrachloroethane
0.035NDTetrachloroethylene
0.035NDTetrahydrofuran
0.035NDToluene
0.035ND1,2,4-Trichlorobenzene
0.035ND1,1,1-Trichloroethane
0.035ND1,1,2-Trichloroethane
0.035NDTrichloroethylene
0.14NDTrichlorofluoromethane (Freon 11)
0.14ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.035ND1,2,4-Trimethylbenzene
0.035ND1,3,5-Trimethylbenzene
0.70NDVinyl Acetate
0.035NDVinyl Chloride
0.070NDm&p-Xylene
0.035NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1028.13
LCS (B224871-BS1)Prepared & Analyzed: 03/01/19
5.00 70-13082.84.14Acetone
5.00 70-13078.33.92Benzene
5.00 70-13082.74.13Benzyl chloride
5.00 70-13079.93.99Bromodichloromethane
5.00 70-13095.54.78Bromoform
5.00 70-13075.23.76Bromomethane
5.00 70-13089.04.451,3-Butadiene
5.00 70-13079.53.972-Butanone (MEK)
5.00 70-1301105.50Carbon Disulfide
5.00 70-13083.44.17Carbon Tetrachloride
5.00 70-13076.93.85Chlorobenzene
5.00 70-13088.54.42Chloroethane
5.00 70-13077.53.88Chloroform
5.00 70-13081.64.08Chloromethane
5.00 70-13087.84.39Cyclohexane
5.00 70-13079.94.00Dibromochloromethane
5.00 70-13081.64.081,2-Dibromoethane (EDB)
5.00 70-13099.84.991,2-Dichlorobenzene
5.00 70-13093.94.701,3-Dichlorobenzene
5.00 70-13096.14.811,4-Dichlorobenzene
5.00 70-13073.73.69Dichlorodifluoromethane (Freon 12)
5.00 70-13075.03.751,1-Dichloroethane
5.00 70-13075.93.801,2-Dichloroethane
5.00 70-13086.94.351,1-Dichloroethylene
5.00 70-13076.73.83cis-1,2-Dichloroethylene
5.00 70-13087.34.37trans-1,2-Dichloroethylene
5.00 70-13080.34.021,2-Dichloropropane
Page 24 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B224871 - TO-15 Prep
LCS (B224871-BS1)Prepared & Analyzed: 03/01/19
5.00 70-13081.44.07cis-1,3-Dichloropropene
5.00 70-13085.04.25trans-1,3-Dichloropropene
5.00 Z-0170-13065.63.281,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
*
5.00 70-1301015.051,4-Dioxane
5.00 70-1301055.27Ethanol
5.00 70-13086.64.33Ethyl Acetate
5.00 70-13083.64.18Ethylbenzene
5.00 70-13089.44.474-Ethyltoluene
5.00 70-13085.44.27Heptane
5.00 70-1301025.08Hexachlorobutadiene
5.00 70-13086.34.32Hexane
5.00 70-13080.24.012-Hexanone (MBK)
5.00 70-13072.93.65Isopropanol
5.00 70-13075.93.80Methyl tert-Butyl Ether (MTBE)
5.00 70-13077.73.89Methylene Chloride
5.00 70-13085.54.284-Methyl-2-pentanone (MIBK)
5.00 70-1301085.42Naphthalene
5.00 70-13087.54.38Propene
5.00 70-13094.94.74Styrene
5.00 70-13082.34.121,1,2,2-Tetrachloroethane
5.00 70-13090.14.51Tetrachloroethylene
5.00 70-13078.43.92Tetrahydrofuran
5.00 70-13082.04.10Toluene
5.00 70-1301055.231,2,4-Trichlorobenzene
5.00 70-13074.53.731,1,1-Trichloroethane
5.00 70-13087.24.361,1,2-Trichloroethane
5.00 70-13084.44.22Trichloroethylene
5.00 70-13079.73.99Trichlorofluoromethane (Freon 11)
5.00 70-13086.44.321,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13092.74.641,2,4-Trimethylbenzene
5.00 70-13092.34.611,3,5-Trimethylbenzene
5.00 70-13075.93.79Vinyl Acetate
5.00 70-13075.73.78Vinyl Chloride
10.0 70-13086.68.66m&p-Xylene
5.00 70-13085.14.26o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1078.53
Page 25 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B224871 - TO-15 Prep
Duplicate (B224871-DUP1)Prepared & Analyzed: 03/01/19 Source: 19B1092-01
8.0 6.2 25 J6.855.8Acetone 1914
0.20 4.5 257.764.2Benzene 0.6413
0.20 ND 25NDBenzyl chloride 1.0ND
0.20 ND 25NDBromodichloromethane1.3ND
0.20 ND 25NDBromoform2.1ND
0.20 ND 25NDBromomethane0.78ND
0.20 4.4 255.874.21,3-Butadiene 0.449.2
8.0 1.9 25 J2.761.92-Butanone (MEK)245.5
2.0 ND 25NDCarbon Disulfide 6.2ND
0.20 ND 25NDCarbon Tetrachloride 1.3ND
0.20 ND 25NDChlorobenzene0.92ND
0.20 ND 25NDChloroethane0.53ND
0.20 5.6 250.6475.5Chloroform 0.9827
0.40 ND 25NDChloromethane0.83ND
0.20 ND 25NDCyclohexane0.69ND
0.20 ND 25NDDibromochloromethane1.7ND
0.20 ND 25ND1,2-Dibromoethane (EDB)1.5ND
0.20 ND 25ND1,2-Dichlorobenzene 1.2ND
0.20 ND 25ND1,3-Dichlorobenzene 1.2ND
0.20 ND 25ND1,4-Dichlorobenzene 1.2ND
0.20 0.40 252.000.40Dichlorodifluoromethane (Freon 12)0.992.0
0.20 ND 25ND1,1-Dichloroethane 0.81ND
0.20 ND 25ND1,2-Dichloroethane 0.81ND
0.20 ND 25ND1,1-Dichloroethylene 0.79ND
0.20 ND 25NDcis-1,2-Dichloroethylene 0.79ND
0.20 ND 25NDtrans-1,2-Dichloroethylene 0.79ND
0.20 ND 25ND1,2-Dichloropropane 0.92ND
0.20 ND 25NDcis-1,3-Dichloropropene 0.91ND
0.20 ND 25NDtrans-1,3-Dichloropropene 0.91ND
0.20 ND 25ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
1.4ND
2.0 ND 25ND1,4-Dioxane 7.2ND
8.0 6.7 25 J15.95.7Ethanol 1511
0.20 ND 25NDEthyl Acetate 0.72ND
0.20 3.4 252.363.4Ethylbenzene 0.8715
0.20 2.0 252.402.04-Ethyltoluene 0.989.7
0.20 5.9 2510.85.3Heptane 0.8222
0.20 ND 25NDHexachlorobutadiene2.1ND
8.0 7.8 25 J4.907.4Hexane 2826
0.20 ND 25ND2-Hexanone (MBK)0.82ND
8.0 ND 25NDIsopropanol20ND
0.20 ND 25NDMethyl tert-Butyl Ether (MTBE)0.72ND
2.0 0.62 25 J1.950.61Methylene Chloride 6.92.1
0.20 1.8 258.581.74-Methyl-2-pentanone (MIBK)0.826.9
0.20 ND 25NDNaphthalene1.0ND
8.0 ND 25NDPropene14ND
0.20 ND 25NDStyrene0.85ND
Page 26 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B224871 - TO-15 Prep
Duplicate (B224871-DUP1)Prepared & Analyzed: 03/01/19 Source: 19B1092-01
0.20 ND 25ND1,1,2,2-Tetrachloroethane 1.4ND
0.20 5.1 250.2355.1Tetrachloroethylene 1.435
0.20 ND 25NDTetrahydrofuran0.59ND
0.20 35 254.9833Toluene0.75120
0.20 ND 25ND1,2,4-Trichlorobenzene 1.5ND
0.20 ND 25ND1,1,1-Trichloroethane 1.1ND
0.20 ND 25ND1,1,2-Trichloroethane 1.1ND
0.20 ND 25NDTrichloroethylene1.1ND
0.80 0.60 25 J9.000.55Trichlorofluoromethane (Freon 11)4.53.1
0.80 ND 25ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
6.1ND
0.20 1.8 252.061.71,2,4-Trimethylbenzene 0.988.5
0.20 0.56 250.7070.571,3,5-Trimethylbenzene 0.982.8
4.0 ND 25NDVinyl Acetate 14ND
0.20 ND 25NDVinyl Chloride 0.51ND
0.40 12 254.1111m&p-Xylene 1.749
0.20 3.7 252.443.6o-Xylene 0.8715
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1088.67
Page 27 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Elevated reporting limit due to matrix interference.RL-12
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult
compound and passes the in house limits of 50-150%.
Z-01
Page 28 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYST
Thomas P. HniteckiTPH
Rebecca FaustRLF
PDF Management StationSTATION
Paula E. BlakeboroughPEB
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 29 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S032661-ICV1 )Lab File ID: B021945.D Analyzed: 02/20/19 09:26
Bromochloromethane (1)92871 5.068 89821 5.064 60 - 140103 0.0040 +/-0.50
1,4-Difluorobenzene (1)178650 6.282 169716 6.283 60 - 140105 -0.0010 +/-0.50
Chlorobenzene-d5 (1)166175 9.881 158958 9.883 60 - 140105 -0.0020 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S033069-CCV1 )Lab File ID: B030106.D Analyzed: 03/01/19 15:07
Bromochloromethane (1)66695 5.061 89821 5.064 60 - 14074 -0.0030 +/-0.50
1,4-Difluorobenzene (1)120870 6.28 169716 6.283 60 - 14071 -0.0030 +/-0.50
Chlorobenzene-d5 (1)114434 9.874 158958 9.883 60 - 14072 -0.0090 +/-0.50
LCS (B224871-BS1 )Lab File ID: B030107.D Analyzed: 03/01/19 15:36
Bromochloromethane (1)65581 5.064 66695 5.061 60 - 14098 0.0030 +/-0.50
1,4-Difluorobenzene (1)116654 6.284 120870 6.28 60 - 14097 0.0040 +/-0.50
Chlorobenzene-d5 (1)109134 9.877 114434 9.874 60 - 14095 0.0030 +/-0.50
Blank (B224871-BLK1 )Lab File ID: B030111.D Analyzed: 03/01/19 17:37
Bromochloromethane (1)63139 5.058 66695 5.061 60 - 14095 -0.0030 +/-0.50
1,4-Difluorobenzene (1)113939 6.278 120870 6.28 60 - 14094 -0.0020 +/-0.50
Chlorobenzene-d5 (1)101804 9.877 114434 9.874 60 - 14089 0.0030 +/-0.50
SG-1 (19B1092-01 )Lab File ID: B030117.D Analyzed: 03/01/19 20:31
Bromochloromethane (1)57046 5.062 66695 5.061 60 - 14086 0.0010 +/-0.50
1,4-Difluorobenzene (1)102104 6.282 120870 6.28 60 - 14084 0.0020 +/-0.50
Chlorobenzene-d5 (1)94902 9.876 114434 9.874 60 - 14083 0.0020 +/-0.50
Duplicate (B224871-DUP1 )Lab File ID: B030118.D Analyzed: 03/01/19 20:59
Bromochloromethane (1)64129 5.063 66695 5.061 60 - 14096 0.0020 +/-0.50
1,4-Difluorobenzene (1)124199 6.283 120870 6.28 60 - 140103 0.0030 +/-0.50
Chlorobenzene-d5 (1)112439 9.876 114434 9.874 60 - 14098 0.0020 +/-0.50
SG-2 (19B1092-02 )Lab File ID: B030119.D Analyzed: 03/01/19 21:28
Bromochloromethane (1)67118 5.063 66695 5.061 60 - 140101 0.0020 +/-0.50
1,4-Difluorobenzene (1)129918 6.283 120870 6.28 60 - 140107 0.0030 +/-0.50
Chlorobenzene-d5 (1)113475 9.876 114434 9.874 60 - 14099 0.0020 +/-0.50
SG-3 (19B1092-03 )Lab File ID: B030120.D Analyzed: 03/01/19 21:56
Bromochloromethane (1)68322 5.065 66695 5.061 60 - 140102 0.0040 +/-0.50
1,4-Difluorobenzene (1)133880 6.285 120870 6.28 60 - 140111 0.0050 +/-0.50
Chlorobenzene-d5 (1)119107 9.872 114434 9.874 60 - 140104 -0.0020 +/-0.50
Page 30 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SG-4 (19B1092-04 )Lab File ID: B030121.D Analyzed: 03/01/19 22:25
Bromochloromethane (1)67327 5.062 66695 5.061 60 - 140101 0.0010 +/-0.50
1,4-Difluorobenzene (1)129096 6.282 120870 6.28 60 - 140107 0.0020 +/-0.50
Chlorobenzene-d5 (1)113114 9.875 114434 9.874 60 - 14099 0.0010 +/-0.50
SG-5 (19B1092-05 )Lab File ID: B030122.D Analyzed: 03/01/19 22:54
Bromochloromethane (1)63797 5.062 66695 5.061 60 - 14096 0.0010 +/-0.50
1,4-Difluorobenzene (1)122115 6.281 120870 6.28 60 - 140101 0.0010 +/-0.50
Chlorobenzene-d5 (1)112283 9.875 114434 9.874 60 - 14098 0.0010 +/-0.50
SG-6 (19B1092-06 )Lab File ID: B030123.D Analyzed: 03/01/19 23:21
Bromochloromethane (1)69161 5.058 66695 5.061 60 - 140104 -0.0030 +/-0.50
1,4-Difluorobenzene (1)137429 6.278 120870 6.28 60 - 140114 -0.0020 +/-0.50
Chlorobenzene-d5 (1)119332 9.877 114434 9.874 60 - 140104 0.0030 +/-0.50
SG-7 (19B1092-07 )Lab File ID: B030124.D Analyzed: 03/01/19 23:50
Bromochloromethane (1)68671 5.063 66695 5.061 60 - 140103 0.0020 +/-0.50
1,4-Difluorobenzene (1)137247 6.283 120870 6.28 60 - 140114 0.0030 +/-0.50
Chlorobenzene-d5 (1)123382 9.876 114434 9.874 60 - 140108 0.0020 +/-0.50
SG-8 (19B1092-08 )Lab File ID: B030125.D Analyzed: 03/02/19 00:18
Bromochloromethane (1)71865 5.061 66695 5.061 60 - 140108 0.0000 +/-0.50
1,4-Difluorobenzene (1)153793 6.281 120870 6.28 60 - 140127 0.0010 +/-0.50
Chlorobenzene-d5 (1)136508 9.874 114434 9.874 60 - 140119 0.0000 +/-0.50
Dup-2 (19B1092-09 )Lab File ID: B030134.D Analyzed: 03/02/19 10:56
Bromochloromethane (1)77208 5.058 66695 5.061 60 - 140116 -0.0030 +/-0.50
1,4-Difluorobenzene (1)159412 6.278 120870 6.28 60 - 140132 -0.0020 +/-0.50
Chlorobenzene-d5 (1)138885 9.871 114434 9.874 60 - 140121 -0.0030 +/-0.50
Page 31 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S033069-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.8695824A -23.5 303.82 1.1374465.00Acetone
0.8342583A -23.1 303.84 1.0853035.00Benzene
0.9515773A -20.7 303.97 1.1992935.00Benzyl chloride
0.5808555A -20.3 303.98 0.7292025.00Bromodichloromethane
0.5978922A -5.6 304.72 0.63321235.00Bromoform
0.5362441A -25.4 303.73 0.71876075.00Bromomethane
0.4183822A -14.4 304.28 0.48900045.001,3-Butadiene
1.315049A -23.5 303.82 1.7201115.002-Butanone (MEK)
1.054064A -21.1 303.95 1.3352775.00Carbon Disulfide
0.3952279A -17.9 304.11 0.48129035.00Carbon Tetrachloride
0.7116207A -24.0 303.80 0.9359395.00Chlorobenzene
0.2898448A -11.7 304.41 0.32831495.00Chloroethane
0.985861A -23.1 303.84 1.2826685.00Chloroform
0.5975141A -24.5 303.77 0.7919085.00Chloromethane
0.3554232A -16.6 304.17 0.42595235.00Cyclohexane
0.5389307A -19.3 304.04 0.66760865.00Dibromochloromethane
0.4828355A -19.4 304.03 0.59868755.001,2-Dibromoethane (EDB)
0.6236608A -10.0 304.50 0.69290245.001,2-Dichlorobenzene
0.6706818A -12.6 304.37 0.76721865.001,3-Dichlorobenzene
0.6754356A -12.0 304.40 0.76770885.001,4-Dichlorobenzene
1.272251A -28.1 303.59 1.7704925.00Dichlorodifluoromethane (Freon 12)
0.8945798A -26.9 303.65 1.2243725.001,1-Dichloroethane
0.6167299A -23.5 303.82 0.80666525.001,2-Dichloroethane
0.7457231A -14.5 304.27 0.87236655.001,1-Dichloroethylene
0.6788395A -22.9 303.86 0.88007475.00cis-1,2-Dichloroethylene
0.6137552A -26.0 303.70 0.8292585.00trans-1,2-Dichloroethylene
0.3212443A -19.6 304.02 0.39937115.001,2-Dichloropropane
0.5005444A -19.1 304.05 0.61838285.00cis-1,3-Dichloropropene
0.4632018A -16.2 304.19 0.55306265.00trans-1,3-Dichloropropene
1.472878A -31.2 *303.44 2.1418545.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1889501A -2.9 304.86 0.19449895.001,4-Dioxane
0.1566054A 8.6 305.43 0.14416395.00Ethanol
0.2104626A -15.7 304.22 0.24967725.00Ethyl Acetate
1.234724A -17.5 304.12 1.4968515.00Ethylbenzene
1.201699A -14.2 304.29 1.4009135.004-Ethyltoluene
0.2710747A -15.8 304.21 0.3219415.00Heptane
0.3213031A -24.0 303.80 0.34715465.00Hexachlorobutadiene
0.3565845A -20.4 303.98 0.44774075.00Hexane
Page 32 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S033069-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.8582624A -21.3 303.93 1.0907445.002-Hexanone (MBK)
1.053176A -21.9 303.91 1.3481195.00Isopropanol
1.224104A -29.2 303.54 1.7293545.00Methyl tert-Butyl Ether (MTBE)
0.6534583A -23.9 303.81 0.85830445.00Methylene Chloride
0.886665A -13.9 304.31 1.0293155.004-Methyl-2-pentanone (MIBK)
0.8157436A -26.7 303.67 1.1122215.00Naphthalene
0.5184197A -11.8 304.41 0.5880635.00Propene
0.709803A -8.4 304.58 0.77480215.00Styrene
0.8683293A -19.4 304.03 1.0775175.001,1,2,2-Tetrachloroethane
0.3944842A -14.2 304.29 0.45956315.00Tetrachloroethylene
0.8246495A -20.3 303.98 1.0351895.00Tetrahydrofuran
0.8866316A -21.9 303.90 1.1359545.00Toluene
0.3830051A -27.8 303.61 0.42344465.001,2,4-Trichlorobenzene
0.4265608A -19.4 304.03 0.52925725.001,1,1-Trichloroethane
0.3186046A -15.9 304.21 0.37867675.001,1,2-Trichloroethane
0.2859932A -16.0 304.20 0.34045245.00Trichloroethylene
1.043652A -21.2 303.94 1.3250715.00Trichlorofluoromethane (Freon 11)
0.927134A -16.6 304.17 1.1122045.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.9237534A -11.2 304.44 1.039945.001,2,4-Trimethylbenzene
0.9406435A -10.8 304.46 1.0544335.001,3,5-Trimethylbenzene
1.730768A -21.3 303.94 2.1983085.00Vinyl Acetate
0.6122918A -24.1 303.80 0.80659545.00Vinyl Chloride
0.927927A -15.3 308.47 1.09574410.0m&p-Xylene
0.8944055A -17.1 304.14 1.0789915.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 33 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 34 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
Page 35 of 38
Page 36 of 38
Page 37 of 38
Page 38 of 38
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 8, 2019
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228-18-0485.03
Laboratory Work Order Number: 19B1096
Enclosed are results of analyses for samples received by the laboratory on February 25, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 132
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 6
Sample Results 10
19B1096-01 10
19B1096-02 17
19B1096-03 24
19B1096-04 30
19B1096-05 36
19B1096-06 43
19B1096-07 50
19B1096-08 56
19B1096-09 62
19B1096-10 68
19B1096-11 74
19B1096-12 77
19B1096-13 80
Sample Preparation Information 86
QC Data 88
Volatile Organic Compounds by GC/MS 88
B224530 88
Semivolatile Organic Compounds by GC/MS 93
B224460 93
Metals Analyses (Total) 101
B224478 101
B224531 102
Page 2 of 132
Table of Contents
Table of Contents (continued)
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 103
B224604 103
Flag/Qualifier Summary 104
Certifications 105
Chain of Custody/Sample Receipt 111
Page 3 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/8/2019
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0485.03
19B1096
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
GP-1 (0-2)19B1096-01 Soil -NC DW37706, WW12/ FL
NELAPE87627
+Additional
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-1 (6-8)19B1096-02 Soil -NC DW37706, WW12/ FL
NELAPE87627
+Additional
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-2 (4-6)19B1096-03 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-2 (10-12)19B1096-04 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-3 (2-4)19B1096-05 Soil -NC DW37706, WW12/ FL
NELAPE87627
+Additional
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-3 (10-12)19B1096-06 Soil -NC DW37706, WW12/ FL
NELAPE87627
+Additional
SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
[TOC_1]Sample Summary[TOC]
Page 4 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/8/2019
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0485.03
19B1096
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
GP-4 (0-2)19B1096-07 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-4 (6-8)19B1096-08 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-5 (2-4)19B1096-09 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
GP-5 (10-12)19B1096-10 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
BG (2-4)19B1096-11 Soil -NC DW37706, WW12/ FL
NELAPE87627
+Additional
SM 2540G
SW-846 6020B
SW-846 7471B
BG (10-12)19B1096-12 Soil -NC DW37706, WW12/ FL
NELAPE87627
+Additional
SM 2540G
SW-846 6020B
SW-846 7471B
DUP-1 19B1096-13 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260D
SW-846 8270D
Page 5 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6020, all dilutions were performed as per standard operating procedure.
[TOC_1]Case Narrative[TOC]
Page 6 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 6020B
Qualifications:
Matrix spike recovery outside of control limits. Possibility of sample matrix effects that lead to a low bias for reported result or
non-homogeneous sample aliquots cannot be eliminated.
Analyte & Samples(s) Qualified:
MS-08
Lead
19B1096-10[GP-5 (10-12)], B224478-MS1
Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in the sample. Appropriate or
meaningful recoveries cannot be calculated.Analyte & Samples(s) Qualified:
MS-19
Barium
19B1096-10[GP-5 (10-12)], B224478-MS1
Duplicate RPD is outside of control limits. Outlier can be attributed to sample non-homogeneity encountered during sample prep.
Analyte & Samples(s) Qualified:
R-02
Barium
19B1096-10[GP-5 (10-12)], B224478-DUP1
Lead
19B1096-10[GP-5 (10-12)], B224478-DUP1
Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that are <5 times the reporting
limit (RL).
Analyte & Samples(s) Qualified:
R-04
Silver
19B1096-10[GP-5 (10-12)], B224478-DUP1
SW-846 8260D
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
2-Butanone (MEK)
B224530-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Acetone
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224530-BLK1, B224530-BS1,
B224530-BSD1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
1,2,4-Trimethylbenzene
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224530-BLK1, B224530-BS1,
B224530-BSD1, S032940-CCV1
Dichlorodifluoromethane (Freon 12)
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224530-BLK1, B224530-BS1,
B224530-BSD1, S032940-CCV1
Hexachlorobutadiene
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224530-BLK1, B224530-BS1,
B224530-BSD1, S032940-CCV1
Page 7 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
2-Butanone (MEK)
B224530-BS1, B224530-BSD1, S032940-CCV1
Benzene
B224530-BS1, B224530-BSD1, S032940-CCV1
Tetrahydrofuran
B224530-BS1, B224530-BSD1, S032940-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.Analyte & Samples(s) Qualified:
V-34
Bromomethane
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224530-BLK1, B224530-BS1,
B224530-BSD1, S032940-CCV1
SW-846 8270D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Benzidine
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224460-BLK1, B224460-BS1,
B224460-BSD1, B224460-MS1, B224460-MSD1
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample matrix effects that lead to a low
bias for reported result or non-homogeneous sample aliquots cannot be eliminated.
Analyte & Samples(s) Qualified:
MS-09
4-Chloroaniline
19B1096-01[GP-1 (0-2)], B224460-MS1, B224460-MSD1
Aniline
19B1096-01[GP-1 (0-2)], B224460-MS1, B224460-MSD1
Benzidine
19B1096-01[GP-1 (0-2)], B224460-MS1, B224460-MSD1
Pyridine
19B1096-01[GP-1 (0-2)], B224460-MS1, B224460-MSD1
Matrix spike duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result for this compound in this sample.
Analyte & Samples(s) Qualified:
R-06
Benzidine
19B1096-01[GP-1 (0-2)], B224460-MS1, B224460-MSD1
Pyridine
19B1096-01[GP-1 (0-2)], B224460-MS1, B224460-MSD1
Page 8 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
3,3-Dichlorobenzidine
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224460-BLK1, B224460-BS1,
B224460-BSD1, B224460-MS1, B224460-MSD1, S032956-CCV1
3-Nitroaniline
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224460-BLK1, B224460-BS1,
B224460-BSD1, B224460-MS1, B224460-MSD1, S032956-CCV1
4-Chloroaniline
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224460-BLK1, B224460-BS1,
B224460-BSD1, B224460-MS1, B224460-MSD1, S032956-CCV1
Aniline
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224460-BLK1, B224460-BS1,
B224460-BSD1, B224460-MS1, B224460-MSD1, S032956-CCV1
Benzidine
19B1096-01[GP-1 (0-2)], 19B1096-02[GP-1 (6-8)], 19B1096-03[GP-2 (4-6)], 19B1096-04[GP-2 (10-12)], 19B1096-05[GP-3 (2-4)], 19B1096-06[GP-3 (10-12)],
19B1096-07[GP-4 (0-2)], 19B1096-08[GP-4 (6-8)], 19B1096-09[GP-5 (2-4)], 19B1096-10[GP-5 (10-12)], 19B1096-13[DUP-1], B224460-BLK1, B224460-BS1,
B224460-BSD1, B224460-MS1, B224460-MSD1, S032956-CCV1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 9 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-01
Field Sample #: GP-1 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 10:15
[TOC_2]19B1096-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.11 2/27/19 8:06 MFFmg/Kg dry0.026 2/27/19SW-846 8260D1R-05Acetone
ND 0.0066 2/27/19 8:06 MFFmg/Kg dry0.0028 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Benzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D1Bromobenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Bromoform
ND 0.011 2/27/19 8:06 MFFmg/Kg dry0.0046 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.044 2/27/19 8:06 MFFmg/Kg dry0.019 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.044 2/27/19 8:06 MFFmg/Kg dry0.023 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0066 2/27/19 8:06 MFFmg/Kg dry0.0048 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.022 2/27/19 8:06 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Chloroethane
ND 0.0044 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Chloroform
ND 0.011 2/27/19 8:06 MFFmg/Kg dry0.0071 2/27/19SW-846 8260D1Chloromethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Dibromomethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0044 2/27/19 8:06 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.022 2/27/19 8:06 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0044 2/27/19 8:06 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.022 2/27/19 8:06 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 10 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-01
Field Sample #: GP-1 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.11 2/27/19 8:06 MFFmg/Kg dry0.064 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.022 2/27/19 8:06 MFFmg/Kg dry0.012 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0044 2/27/19 8:06 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.022 2/27/19 8:06 MFFmg/Kg dry0.0079 2/27/19SW-846 8260D1Methylene Chloride
ND 0.022 2/27/19 8:06 MFFmg/Kg dry0.0084 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0044 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Naphthalene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Styrene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0011 2/27/19 8:06 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.011 2/27/19 8:06 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D1Toluene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Trichloroethylene
ND 0.011 2/27/19 8:06 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.011 2/27/19 8:06 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00089 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.011 2/27/19 8:06 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0044 2/27/19 8:06 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1m+p Xylene
ND 0.0022 2/27/19 8:06 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.4 2/27/19 8:0670-130
Toluene-d8 91.4 2/27/19 8:0670-130
4-Bromofluorobenzene 106 2/27/19 8:0670-130
Page 11 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-01
Field Sample #: GP-1 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Acenaphthene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Acenaphthylene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Acetophenone
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1MS-09, V-34Aniline
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Anthracene
ND 0.88 2/27/19 15:08 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1L-04, MS-09, R-06,
V-34
Benzidine
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.3 2/27/19 15:08 IMRmg/Kg dry0.78 2/26/19SW-846 8270D1Benzoic Acid
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.23 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Carbazole
ND 0.88 2/27/19 15:08 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1MS-09, V-344-Chloroaniline
ND 0.88 2/27/19 15:08 IMRmg/Kg dry0.19 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Chlorophenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Chrysene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dibenzofuran
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Diethylphthalate
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.40 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.88 2/27/19 15:08 IMRmg/Kg dry0.61 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Fluoranthene
Page 12 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-01
Field Sample #: GP-1 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Fluorene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.37 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Hexachloroethane
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Isophorone
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12-Methylphenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Naphthalene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.27 2/26/19SW-846 8270D12-Nitroaniline
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.17 2/26/19SW-846 8270D14-Nitroaniline
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Nitrobenzene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12-Nitrophenol
ND 0.88 2/27/19 15:08 IMRmg/Kg dry0.32 2/26/19SW-846 8270D14-Nitrophenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Phenanthrene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Phenol
ND 0.23 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyrene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1MS-09, R-06Pyridine
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.17 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.45 2/27/19 15:08 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 54.8 2/27/19 15:0830-130
Phenol-d6 55.6 2/27/19 15:0830-130
Nitrobenzene-d5 53.6 2/27/19 15:0830-130
2-Fluorobiphenyl 59.8 2/27/19 15:0830-130
2,4,6-Tribromophenol 58.7 2/27/19 15:0830-130
p-Terphenyl-d14 62.1 2/27/19 15:0830-130
Page 13 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-01
Field Sample #: GP-1 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.5 0.22 3/1/19 10:58 MJHmg/Kg dry0.037 2/26/19SW-846 6020B5Arsenic
88 5.6 3/1/19 10:58 MJHmg/Kg dry0.43 2/26/19SW-846 6020B5Chromium
5.9 2.2 3/1/19 10:58 MJHmg/Kg dry0.073 2/26/19SW-846 6020B5Lead
0.40 0.032 2/28/19 9:37 EJBmg/Kg dry0.0097 2/27/19SW-846 7471B1Mercury
0.26 0.94 3/1/19 10:58 MJHmg/Kg dry0.089 2/26/19SW-846 6020B5JSelenium
0.080 0.098 3/1/19 10:58 MJHmg/Kg dry0.0089 2/26/19SW-846 6020B5JSilver
100 11 3/1/19 10:58 MJHmg/Kg dry0.45 2/26/19SW-846 6020B5Barium
ND 0.42 3/1/19 10:58 MJHmg/Kg dry0.014 2/26/19SW-846 6020B5Cadmium
Page 14 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-01
Field Sample #: GP-1 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
75.0 3/1/19 7:43 AVF% Wt 2/28/19SM 2540G1% Solids
Page 15 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-01
Field Sample #: GP-1 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
EPA 7199
Attached Attached 3/5/19 17:48 PALmg/KgAttached 7199 Hexavalent
Chromium Soil
17199 Hexavalent Chromium Soil
Page 16 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-02
Field Sample #: GP-1 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 10:30
[TOC_2]19B1096-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.12 2/27/19 8:31 MFFmg/Kg dry0.029 2/27/19SW-846 8260D1R-05Acetone
ND 0.0075 2/27/19 8:31 MFFmg/Kg dry0.0031 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Benzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1Bromobenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00075 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Bromoform
ND 0.012 2/27/19 8:31 MFFmg/Kg dry0.0052 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.050 2/27/19 8:31 MFFmg/Kg dry0.022 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.050 2/27/19 8:31 MFFmg/Kg dry0.026 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.00075 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0075 2/27/19 8:31 MFFmg/Kg dry0.0053 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.025 2/27/19 8:31 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1Chloroethane
ND 0.0050 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Chloroform
ND 0.012 2/27/19 8:31 MFFmg/Kg dry0.0080 2/27/19SW-846 8260D1Chloromethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00075 2/27/19SW-846 8260D1Dibromomethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0050 2/27/19 8:31 MFFmg/Kg dry0.0026 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.025 2/27/19 8:31 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0050 2/27/19 8:31 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.025 2/27/19 8:31 MFFmg/Kg dry0.0022 2/27/19SW-846 8260D1Diethyl Ether
Page 17 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-02
Field Sample #: GP-1 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 10:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.00075 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.12 2/27/19 8:31 MFFmg/Kg dry0.072 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.025 2/27/19 8:31 MFFmg/Kg dry0.014 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0050 2/27/19 8:31 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.025 2/27/19 8:31 MFFmg/Kg dry0.0088 2/27/19SW-846 8260D1Methylene Chloride
ND 0.025 2/27/19 8:31 MFFmg/Kg dry0.0094 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0050 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Naphthalene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00075 2/27/19SW-846 8260D1Styrene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0022 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0012 2/27/19 8:31 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.012 2/27/19 8:31 MFFmg/Kg dry0.0027 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1Toluene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00075 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Trichloroethylene
ND 0.012 2/27/19 8:31 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.012 2/27/19 8:31 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00075 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.012 2/27/19 8:31 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0050 2/27/19 8:31 MFFmg/Kg dry0.0021 2/27/19SW-846 8260D1m+p Xylene
ND 0.0025 2/27/19 8:31 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.8 2/27/19 8:3170-130
Toluene-d8 93.5 2/27/19 8:3170-130
4-Bromofluorobenzene 121 2/27/19 8:3170-130
Page 18 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-02
Field Sample #: GP-1 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 10:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Acenaphthene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Acenaphthylene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Acetophenone
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1V-34Aniline
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Anthracene
ND 0.87 2/27/19 15:36 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.3 2/27/19 15:36 IMRmg/Kg dry0.78 2/26/19SW-846 8270D1Benzoic Acid
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.30 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Carbazole
ND 0.87 2/27/19 15:36 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.87 2/27/19 15:36 IMRmg/Kg dry0.18 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Chlorophenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Chrysene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dibenzofuran
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Diethylphthalate
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.40 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.87 2/27/19 15:36 IMRmg/Kg dry0.61 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Fluoranthene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Fluorene
Page 19 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-02
Field Sample #: GP-1 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 10:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.37 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Hexachloroethane
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Isophorone
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12-Methylphenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Naphthalene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.26 2/26/19SW-846 8270D12-Nitroaniline
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.17 2/26/19SW-846 8270D14-Nitroaniline
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Nitrobenzene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12-Nitrophenol
ND 0.87 2/27/19 15:36 IMRmg/Kg dry0.32 2/26/19SW-846 8270D14-Nitrophenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.30 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Phenanthrene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Phenol
ND 0.22 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyrene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Pyridine
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.17 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.45 2/27/19 15:36 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 63.1 2/27/19 15:3630-130
Phenol-d6 61.6 2/27/19 15:3630-130
Nitrobenzene-d5 60.4 2/27/19 15:3630-130
2-Fluorobiphenyl 66.6 2/27/19 15:3630-130
2,4,6-Tribromophenol 65.6 2/27/19 15:3630-130
p-Terphenyl-d14 68.7 2/27/19 15:3630-130
Page 20 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-02
Field Sample #: GP-1 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 10:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.58 0.22 3/1/19 11:01 MJHmg/Kg dry0.036 2/26/19SW-846 6020B5Arsenic
13 5.4 3/1/19 11:01 MJHmg/Kg dry0.42 2/26/19SW-846 6020B5Chromium
9.5 2.2 3/1/19 11:01 MJHmg/Kg dry0.071 2/26/19SW-846 6020B5Lead
ND 0.032 2/28/19 9:39 EJBmg/Kg dry0.0097 2/27/19SW-846 7471B1Mercury
0.090 0.91 3/1/19 11:01 MJHmg/Kg dry0.087 2/26/19SW-846 6020B5JSelenium
0.015 0.096 3/1/19 11:01 MJHmg/Kg dry0.0087 2/26/19SW-846 6020B5JSilver
21 11 3/1/19 11:01 MJHmg/Kg dry0.44 2/26/19SW-846 6020B5Barium
ND 0.41 3/1/19 11:01 MJHmg/Kg dry0.014 2/26/19SW-846 6020B5Cadmium
Page 21 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-02
Field Sample #: GP-1 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 10:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.8 3/1/19 7:43 AVF% Wt 2/28/19SM 2540G1% Solids
Page 22 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-02
Field Sample #: GP-1 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 10:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
EPA 7199
Attached Attached 3/5/19 18:01 PALmg/KgAttached 7199 Hexavalent
Chromium Soil
17199 Hexavalent Chromium Soil
Page 23 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-03
Field Sample #: GP-2 (4-6)
Sample Matrix: Soil
Sampled: 2/23/2019 11:00
[TOC_2]19B1096-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 2/27/19 8:56 MFFmg/Kg dry0.031 2/27/19SW-846 8260D1R-05Acetone
ND 0.0080 2/27/19 8:56 MFFmg/Kg dry0.0033 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1Benzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Bromobenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1Bromoform
ND 0.013 2/27/19 8:56 MFFmg/Kg dry0.0056 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.054 2/27/19 8:56 MFFmg/Kg dry0.023 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.054 2/27/19 8:56 MFFmg/Kg dry0.028 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0080 2/27/19 8:56 MFFmg/Kg dry0.0058 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.027 2/27/19 8:56 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1Chloroethane
ND 0.0054 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1Chloroform
ND 0.013 2/27/19 8:56 MFFmg/Kg dry0.0086 2/27/19SW-846 8260D1Chloromethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Dibromomethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0054 2/27/19 8:56 MFFmg/Kg dry0.0028 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.027 2/27/19 8:56 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0054 2/27/19 8:56 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.027 2/27/19 8:56 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1Diethyl Ether
Page 24 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-03
Field Sample #: GP-2 (4-6)
Sample Matrix: Soil
Sampled: 2/23/2019 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 2/27/19 8:56 MFFmg/Kg dry0.077 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.027 2/27/19 8:56 MFFmg/Kg dry0.015 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0054 2/27/19 8:56 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.027 2/27/19 8:56 MFFmg/Kg dry0.0095 2/27/19SW-846 8260D1Methylene Chloride
ND 0.027 2/27/19 8:56 MFFmg/Kg dry0.010 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0054 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1Naphthalene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Styrene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 2/27/19 8:56 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.013 2/27/19 8:56 MFFmg/Kg dry0.0029 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Toluene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Trichloroethylene
ND 0.013 2/27/19 8:56 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.013 2/27/19 8:56 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 2/27/19 8:56 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0054 2/27/19 8:56 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D1m+p Xylene
ND 0.0027 2/27/19 8:56 MFFmg/Kg dry0.00094 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.9 2/27/19 8:5670-130
Toluene-d8 89.4 2/27/19 8:5670-130
4-Bromofluorobenzene 108 2/27/19 8:5670-130
Page 25 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-03
Field Sample #: GP-2 (4-6)
Sample Matrix: Soil
Sampled: 2/23/2019 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Acenaphthene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Acenaphthylene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Acetophenone
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1V-34Aniline
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Anthracene
ND 0.96 2/27/19 16:04 IMRmg/Kg dry0.26 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.5 2/27/19 16:04 IMRmg/Kg dry0.86 2/26/19SW-846 8270D1Benzoic Acid
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.25 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.33 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Carbazole
ND 0.96 2/27/19 16:04 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.96 2/27/19 16:04 IMRmg/Kg dry0.20 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12-Chlorophenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Chrysene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Dibenzofuran
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Diethylphthalate
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.44 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.96 2/27/19 16:04 IMRmg/Kg dry0.67 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.23 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.23 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
0.15 0.25 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1JFluoranthene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Fluorene
Page 26 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-03
Field Sample #: GP-2 (4-6)
Sample Matrix: Soil
Sampled: 2/23/2019 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.41 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Hexachloroethane
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Isophorone
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12-Methylphenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Naphthalene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.29 2/26/19SW-846 8270D12-Nitroaniline
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.19 2/26/19SW-846 8270D14-Nitroaniline
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Nitrobenzene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.20 2/26/19SW-846 8270D12-Nitrophenol
ND 0.96 2/27/19 16:04 IMRmg/Kg dry0.35 2/26/19SW-846 8270D14-Nitrophenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.26 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.33 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Phenanthrene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Phenol
ND 0.25 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pyrene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyridine
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.19 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.16 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.49 2/27/19 16:04 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 67.2 2/27/19 16:0430-130
Phenol-d6 68.5 2/27/19 16:0430-130
Nitrobenzene-d5 64.5 2/27/19 16:0430-130
2-Fluorobiphenyl 72.6 2/27/19 16:0430-130
2,4,6-Tribromophenol 77.2 2/27/19 16:0430-130
p-Terphenyl-d14 78.7 2/27/19 16:0430-130
Page 27 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-03
Field Sample #: GP-2 (4-6)
Sample Matrix: Soil
Sampled: 2/23/2019 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.9 0.24 3/1/19 11:05 MJHmg/Kg dry0.040 2/26/19SW-846 6020B5Arsenic
18 6.0 3/1/19 11:05 MJHmg/Kg dry0.47 2/26/19SW-846 6020B5Chromium
9.8 2.4 3/1/19 11:05 MJHmg/Kg dry0.079 2/26/19SW-846 6020B5Lead
0.023 0.036 2/28/19 9:40 EJBmg/Kg dry0.011 2/27/19SW-846 7471B1JMercury
0.38 1.0 3/1/19 11:05 MJHmg/Kg dry0.096 2/26/19SW-846 6020B5JSelenium
0.024 0.11 3/1/19 11:05 MJHmg/Kg dry0.0097 2/26/19SW-846 6020B5JSilver
16 12 3/1/19 11:05 MJHmg/Kg dry0.49 2/26/19SW-846 6020B5Barium
ND 0.46 3/1/19 11:05 MJHmg/Kg dry0.015 2/26/19SW-846 6020B5Cadmium
Page 28 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-03
Field Sample #: GP-2 (4-6)
Sample Matrix: Soil
Sampled: 2/23/2019 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
68.7 3/1/19 7:43 AVF% Wt 2/28/19SM 2540G1% Solids
Page 29 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-04
Field Sample #: GP-2 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 11:15
[TOC_2]19B1096-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.12 2/27/19 9:21 MFFmg/Kg dry0.027 2/27/19SW-846 8260D1R-05Acetone
ND 0.0070 2/27/19 9:21 MFFmg/Kg dry0.0029 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Benzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Bromobenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00070 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1Bromoform
ND 0.012 2/27/19 9:21 MFFmg/Kg dry0.0049 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.047 2/27/19 9:21 MFFmg/Kg dry0.020 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.047 2/27/19 9:21 MFFmg/Kg dry0.024 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.00070 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0070 2/27/19 9:21 MFFmg/Kg dry0.0050 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.023 2/27/19 9:21 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Chloroethane
ND 0.0047 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Chloroform
ND 0.012 2/27/19 9:21 MFFmg/Kg dry0.0075 2/27/19SW-846 8260D1Chloromethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00070 2/27/19SW-846 8260D1Dibromomethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0047 2/27/19 9:21 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.023 2/27/19 9:21 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0047 2/27/19 9:21 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.023 2/27/19 9:21 MFFmg/Kg dry0.0021 2/27/19SW-846 8260D1Diethyl Ether
Page 30 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-04
Field Sample #: GP-2 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.00070 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.12 2/27/19 9:21 MFFmg/Kg dry0.067 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.023 2/27/19 9:21 MFFmg/Kg dry0.013 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0047 2/27/19 9:21 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.023 2/27/19 9:21 MFFmg/Kg dry0.0083 2/27/19SW-846 8260D1Methylene Chloride
ND 0.023 2/27/19 9:21 MFFmg/Kg dry0.0088 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0047 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Naphthalene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00070 2/27/19SW-846 8260D1Styrene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0021 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0012 2/27/19 9:21 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.012 2/27/19 9:21 MFFmg/Kg dry0.0026 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Toluene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00070 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Trichloroethylene
ND 0.012 2/27/19 9:21 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.012 2/27/19 9:21 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00070 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.012 2/27/19 9:21 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0047 2/27/19 9:21 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1m+p Xylene
ND 0.0023 2/27/19 9:21 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.4 2/27/19 9:2170-130
Toluene-d8 95.4 2/27/19 9:2170-130
4-Bromofluorobenzene 107 2/27/19 9:2170-130
Page 31 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-04
Field Sample #: GP-2 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Acenaphthene
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Acenaphthylene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Acetophenone
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1V-34Aniline
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Anthracene
ND 0.90 2/27/19 16:31 IMRmg/Kg dry0.25 2/26/19SW-846 8270D1L-04, V-34Benzidine
0.20 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1JBenzo(a)anthracene
0.21 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1JBenzo(a)pyrene
0.35 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(b)fluoranthene
0.18 0.23 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1JBenzo(g,h,i)perylene
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.4 2/27/19 16:31 IMRmg/Kg dry0.81 2/26/19SW-846 8270D1Benzoic Acid
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.23 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Carbazole
ND 0.90 2/27/19 16:31 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.90 2/27/19 16:31 IMRmg/Kg dry0.19 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Chlorophenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Chlorophenylphenylether
0.31 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Chrysene
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dibenzofuran
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Diethylphthalate
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.41 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.90 2/27/19 16:31 IMRmg/Kg dry0.63 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.22 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.22 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
0.78 0.23 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Fluoranthene
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Fluorene
Page 32 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-04
Field Sample #: GP-2 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.38 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Hexachloroethane
0.20 0.23 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1JIndeno(1,2,3-cd)pyrene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Isophorone
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12-Methylphenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Naphthalene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.27 2/26/19SW-846 8270D12-Nitroaniline
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.18 2/26/19SW-846 8270D14-Nitroaniline
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Nitrobenzene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12-Nitrophenol
ND 0.90 2/27/19 16:31 IMRmg/Kg dry0.33 2/26/19SW-846 8270D14-Nitrophenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.25 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Pentachlorophenol
0.41 0.23 2/27/19 16:31 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Phenanthrene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Phenol
0.57 0.23 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyrene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Pyridine
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.18 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.46 2/27/19 16:31 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 78.3 2/27/19 16:3130-130
Phenol-d6 76.6 2/27/19 16:3130-130
Nitrobenzene-d5 74.3 2/27/19 16:3130-130
2-Fluorobiphenyl 81.0 2/27/19 16:3130-130
2,4,6-Tribromophenol 79.3 2/27/19 16:3130-130
p-Terphenyl-d14 82.4 2/27/19 16:3130-130
Page 33 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-04
Field Sample #: GP-2 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.59 0.23 3/1/19 11:08 MJHmg/Kg dry0.038 2/26/19SW-846 6020B5Arsenic
11 5.8 3/1/19 11:08 MJHmg/Kg dry0.45 2/26/19SW-846 6020B5Chromium
12 2.3 3/1/19 11:08 MJHmg/Kg dry0.076 2/26/19SW-846 6020B5Lead
ND 0.035 2/28/19 9:42 EJBmg/Kg dry0.010 2/27/19SW-846 7471B1Mercury
ND 0.97 3/1/19 11:08 MJHmg/Kg dry0.092 2/26/19SW-846 6020B5Selenium
0.019 0.10 3/1/19 11:08 MJHmg/Kg dry0.0093 2/26/19SW-846 6020B5JSilver
76 12 3/1/19 11:08 MJHmg/Kg dry0.47 2/26/19SW-846 6020B5Barium
ND 0.44 3/1/19 11:08 MJHmg/Kg dry0.015 2/26/19SW-846 6020B5Cadmium
Page 34 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-04
Field Sample #: GP-2 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
72.4 3/1/19 7:44 AVF% Wt 2/28/19SM 2540G1% Solids
Page 35 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-05
Field Sample #: GP-3 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 13:00
[TOC_2]19B1096-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.14 2/27/19 9:45 MFFmg/Kg dry0.033 2/27/19SW-846 8260D1R-05Acetone
ND 0.0084 2/27/19 9:45 MFFmg/Kg dry0.0035 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1Benzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Bromobenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00084 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1Bromoform
ND 0.014 2/27/19 9:45 MFFmg/Kg dry0.0059 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.056 2/27/19 9:45 MFFmg/Kg dry0.024 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.056 2/27/19 9:45 MFFmg/Kg dry0.029 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.00084 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0084 2/27/19 9:45 MFFmg/Kg dry0.0060 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.028 2/27/19 9:45 MFFmg/Kg dry0.0021 2/27/19SW-846 8260D1Chloroethane
ND 0.0056 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1Chloroform
ND 0.014 2/27/19 9:45 MFFmg/Kg dry0.0089 2/27/19SW-846 8260D1Chloromethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00084 2/27/19SW-846 8260D1Dibromomethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0056 2/27/19 9:45 MFFmg/Kg dry0.0029 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.028 2/27/19 9:45 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0056 2/27/19 9:45 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.028 2/27/19 9:45 MFFmg/Kg dry0.0025 2/27/19SW-846 8260D1Diethyl Ether
Page 36 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-05
Field Sample #: GP-3 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.00084 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.14 2/27/19 9:45 MFFmg/Kg dry0.080 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.028 2/27/19 9:45 MFFmg/Kg dry0.015 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0056 2/27/19 9:45 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.028 2/27/19 9:45 MFFmg/Kg dry0.0099 2/27/19SW-846 8260D1Methylene Chloride
ND 0.028 2/27/19 9:45 MFFmg/Kg dry0.011 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0056 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1Naphthalene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00084 2/27/19SW-846 8260D1Styrene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0025 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0014 2/27/19 9:45 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.014 2/27/19 9:45 MFFmg/Kg dry0.0031 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Toluene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00084 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Trichloroethylene
ND 0.014 2/27/19 9:45 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.014 2/27/19 9:45 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00084 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.014 2/27/19 9:45 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0056 2/27/19 9:45 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1m+p Xylene
ND 0.0028 2/27/19 9:45 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 92.9 2/27/19 9:4570-130
Toluene-d8 95.6 2/27/19 9:4570-130
4-Bromofluorobenzene 98.8 2/27/19 9:4570-130
Page 37 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-05
Field Sample #: GP-3 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1Acenaphthene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Acenaphthylene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Acetophenone
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.097 2/26/19SW-846 8270D1V-34Aniline
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1Anthracene
ND 0.80 2/27/19 16:58 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 2/27/19 16:58 IMRmg/Kg dry0.71 2/26/19SW-846 8270D1Benzoic Acid
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.28 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1Carbazole
ND 0.80 2/27/19 16:58 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.80 2/27/19 16:58 IMRmg/Kg dry0.17 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12-Chlorophenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Chrysene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Dibenzofuran
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.11 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Diethylphthalate
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.36 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.80 2/27/19 16:58 IMRmg/Kg dry0.56 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Fluoranthene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Fluorene
Page 38 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-05
Field Sample #: GP-3 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.34 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Hexachloroethane
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Isophorone
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.11 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Methylphenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Naphthalene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.24 2/26/19SW-846 8270D12-Nitroaniline
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Nitroaniline
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Nitrobenzene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12-Nitrophenol
ND 0.80 2/27/19 16:58 IMRmg/Kg dry0.29 2/26/19SW-846 8270D14-Nitrophenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.28 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1Phenanthrene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Phenol
ND 0.21 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Pyrene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Pyridine
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.16 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.41 2/27/19 16:58 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 75.3 2/27/19 16:5830-130
Phenol-d6 73.3 2/27/19 16:5830-130
Nitrobenzene-d5 72.9 2/27/19 16:5830-130
2-Fluorobiphenyl 77.5 2/27/19 16:5830-130
2,4,6-Tribromophenol 78.0 2/27/19 16:5830-130
p-Terphenyl-d14 79.5 2/27/19 16:5830-130
Page 39 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-05
Field Sample #: GP-3 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.33 0.20 3/1/19 11:12 MJHmg/Kg dry0.033 2/26/19SW-846 6020B5Arsenic
26 5.1 3/1/19 11:12 MJHmg/Kg dry0.39 2/26/19SW-846 6020B5Chromium
3.6 2.0 3/1/19 11:12 MJHmg/Kg dry0.066 2/26/19SW-846 6020B5Lead
ND 0.031 2/28/19 9:43 EJBmg/Kg dry0.0092 2/27/19SW-846 7471B1Mercury
ND 0.85 3/1/19 11:12 MJHmg/Kg dry0.081 2/26/19SW-846 6020B5Selenium
0.029 0.089 3/1/19 11:12 MJHmg/Kg dry0.0081 2/26/19SW-846 6020B5JSilver
44 10 3/1/19 11:12 MJHmg/Kg dry0.41 2/26/19SW-846 6020B5Barium
ND 0.38 3/1/19 11:12 MJHmg/Kg dry0.013 2/26/19SW-846 6020B5Cadmium
Page 40 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-05
Field Sample #: GP-3 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.9 3/1/19 7:44 AVF% Wt 2/28/19SM 2540G1% Solids
Page 41 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-05
Field Sample #: GP-3 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
EPA 7199
Attached Attached 3/5/19 18:14 PALmg/KgAttached 7199 Hexavalent
Chromium Soil
17199 Hexavalent Chromium Soil
Page 42 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-06
Field Sample #: GP-3 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 13:15
[TOC_2]19B1096-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.10 2/27/19 10:10 MFFmg/Kg dry0.024 2/27/19SW-846 8260D1R-05Acetone
ND 0.0061 2/27/19 10:10 MFFmg/Kg dry0.0026 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1Benzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D1Bromobenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00061 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Bromoform
ND 0.010 2/27/19 10:10 MFFmg/Kg dry0.0043 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.041 2/27/19 10:10 MFFmg/Kg dry0.018 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.041 2/27/19 10:10 MFFmg/Kg dry0.021 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00092 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00061 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0061 2/27/19 10:10 MFFmg/Kg dry0.0044 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.020 2/27/19 10:10 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Chloroethane
ND 0.0041 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1Chloroform
ND 0.010 2/27/19 10:10 MFFmg/Kg dry0.0065 2/27/19SW-846 8260D1Chloromethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00061 2/27/19SW-846 8260D1Dibromomethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0041 2/27/19 10:10 MFFmg/Kg dry0.0021 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.020 2/27/19 10:10 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0041 2/27/19 10:10 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00092 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00092 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00092 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.020 2/27/19 10:10 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D1Diethyl Ether
Page 43 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-06
Field Sample #: GP-3 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00061 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.10 2/27/19 10:10 MFFmg/Kg dry0.059 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.020 2/27/19 10:10 MFFmg/Kg dry0.011 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0041 2/27/19 10:10 MFFmg/Kg dry0.00092 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.020 2/27/19 10:10 MFFmg/Kg dry0.0073 2/27/19SW-846 8260D1Methylene Chloride
ND 0.020 2/27/19 10:10 MFFmg/Kg dry0.0078 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0041 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1Naphthalene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00061 2/27/19SW-846 8260D1Styrene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0010 2/27/19 10:10 MFFmg/Kg dry0.00092 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.010 2/27/19 10:10 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D1Toluene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00061 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Trichloroethylene
ND 0.010 2/27/19 10:10 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.010 2/27/19 10:10 MFFmg/Kg dry0.00092 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00082 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00061 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.010 2/27/19 10:10 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0041 2/27/19 10:10 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1m+p Xylene
ND 0.0020 2/27/19 10:10 MFFmg/Kg dry0.00072 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.3 2/27/19 10:1070-130
Toluene-d8 92.8 2/27/19 10:1070-130
4-Bromofluorobenzene 106 2/27/19 10:1070-130
Page 44 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-06
Field Sample #: GP-3 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Acenaphthene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Acenaphthylene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Acetophenone
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1V-34Aniline
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Anthracene
ND 0.89 2/27/19 17:25 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.3 2/27/19 17:25 IMRmg/Kg dry0.80 2/26/19SW-846 8270D1Benzoic Acid
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.23 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Carbazole
ND 0.89 2/27/19 17:25 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.89 2/27/19 17:25 IMRmg/Kg dry0.19 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Chlorophenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Chrysene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dibenzofuran
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Diethylphthalate
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.40 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.89 2/27/19 17:25 IMRmg/Kg dry0.62 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.22 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.22 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Fluoranthene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Fluorene
Page 45 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-06
Field Sample #: GP-3 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.38 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Hexachloroethane
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Isophorone
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12-Methylphenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Naphthalene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.27 2/26/19SW-846 8270D12-Nitroaniline
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.18 2/26/19SW-846 8270D14-Nitroaniline
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Nitrobenzene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12-Nitrophenol
ND 0.89 2/27/19 17:25 IMRmg/Kg dry0.32 2/26/19SW-846 8270D14-Nitrophenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Phenanthrene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Phenol
ND 0.23 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyrene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Pyridine
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.18 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.46 2/27/19 17:25 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 70.8 2/27/19 17:2530-130
Phenol-d6 69.1 2/27/19 17:2530-130
Nitrobenzene-d5 67.4 2/27/19 17:2530-130
2-Fluorobiphenyl 71.4 2/27/19 17:2530-130
2,4,6-Tribromophenol 71.7 2/27/19 17:2530-130
p-Terphenyl-d14 76.1 2/27/19 17:2530-130
Page 46 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-06
Field Sample #: GP-3 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.39 0.22 3/1/19 11:15 MJHmg/Kg dry0.036 2/26/19SW-846 6020B5Arsenic
13 5.5 3/1/19 11:15 MJHmg/Kg dry0.43 2/26/19SW-846 6020B5Chromium
4.7 2.2 3/1/19 11:15 MJHmg/Kg dry0.073 2/26/19SW-846 6020B5Lead
ND 0.032 2/28/19 9:49 EJBmg/Kg dry0.0097 2/27/19SW-846 7471B1Mercury
ND 0.93 3/1/19 11:15 MJHmg/Kg dry0.088 2/26/19SW-846 6020B5Selenium
0.025 0.097 3/1/19 11:15 MJHmg/Kg dry0.0088 2/26/19SW-846 6020B5JSilver
220 11 3/1/19 11:15 MJHmg/Kg dry0.45 2/26/19SW-846 6020B5Barium
0.048 0.42 3/1/19 11:15 MJHmg/Kg dry0.014 2/26/19SW-846 6020B5JCadmium
Page 47 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-06
Field Sample #: GP-3 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
73.5 3/1/19 7:44 AVF% Wt 2/28/19SM 2540G1% Solids
Page 48 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-06
Field Sample #: GP-3 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
EPA 7199
Attached Attached 3/5/19 18:27 PALmg/KgAttached 7199 Hexavalent
Chromium Soil
17199 Hexavalent Chromium Soil
Page 49 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-07
Field Sample #: GP-4 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 13:45
[TOC_2]19B1096-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 2/27/19 10:34 MFFmg/Kg dry0.030 2/27/19SW-846 8260D1R-05Acetone
ND 0.0077 2/27/19 10:34 MFFmg/Kg dry0.0032 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1Benzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Bromobenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D1Bromoform
ND 0.013 2/27/19 10:34 MFFmg/Kg dry0.0054 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.052 2/27/19 10:34 MFFmg/Kg dry0.023 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.052 2/27/19 10:34 MFFmg/Kg dry0.027 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0077 2/27/19 10:34 MFFmg/Kg dry0.0055 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.026 2/27/19 10:34 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1Chloroethane
ND 0.0052 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1Chloroform
ND 0.013 2/27/19 10:34 MFFmg/Kg dry0.0083 2/27/19SW-846 8260D1Chloromethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Dibromomethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0052 2/27/19 10:34 MFFmg/Kg dry0.0027 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.026 2/27/19 10:34 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0052 2/27/19 10:34 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.026 2/27/19 10:34 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D1Diethyl Ether
Page 50 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-07
Field Sample #: GP-4 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 2/27/19 10:34 MFFmg/Kg dry0.074 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.026 2/27/19 10:34 MFFmg/Kg dry0.014 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0052 2/27/19 10:34 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.026 2/27/19 10:34 MFFmg/Kg dry0.0092 2/27/19SW-846 8260D1Methylene Chloride
ND 0.026 2/27/19 10:34 MFFmg/Kg dry0.0098 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0052 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1Naphthalene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Styrene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 2/27/19 10:34 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.013 2/27/19 10:34 MFFmg/Kg dry0.0028 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Toluene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Trichloroethylene
ND 0.013 2/27/19 10:34 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.013 2/27/19 10:34 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 2/27/19 10:34 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0052 2/27/19 10:34 MFFmg/Kg dry0.0022 2/27/19SW-846 8260D1m+p Xylene
ND 0.0026 2/27/19 10:34 MFFmg/Kg dry0.00090 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.0 2/27/19 10:3470-130
Toluene-d8 89.1 2/27/19 10:3470-130
4-Bromofluorobenzene 105 2/27/19 10:3470-130
Page 51 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-07
Field Sample #: GP-4 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Acenaphthene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Acenaphthylene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Acetophenone
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1V-34Aniline
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Anthracene
ND 0.99 2/27/19 17:52 IMRmg/Kg dry0.27 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.5 2/27/19 17:52 IMRmg/Kg dry0.88 2/26/19SW-846 8270D1Benzoic Acid
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.25 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.34 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Carbazole
ND 0.99 2/27/19 17:52 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.99 2/27/19 17:52 IMRmg/Kg dry0.21 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12-Chlorophenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Chrysene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Dibenzofuran
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1Diethylphthalate
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.45 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.99 2/27/19 17:52 IMRmg/Kg dry0.69 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.24 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.24 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Fluoranthene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Fluorene
Page 52 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-07
Field Sample #: GP-4 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.42 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Hexachloroethane
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Isophorone
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12-Methylphenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Naphthalene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.30 2/26/19SW-846 8270D12-Nitroaniline
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.19 2/26/19SW-846 8270D14-Nitroaniline
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.21 2/26/19SW-846 8270D1Nitrobenzene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12-Nitrophenol
ND 0.99 2/27/19 17:52 IMRmg/Kg dry0.36 2/26/19SW-846 8270D14-Nitrophenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.27 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.34 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Phenanthrene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Phenol
ND 0.25 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pyrene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyridine
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.19 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.16 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.51 2/27/19 17:52 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 68.6 2/27/19 17:5230-130
Phenol-d6 69.9 2/27/19 17:5230-130
Nitrobenzene-d5 63.3 2/27/19 17:5230-130
2-Fluorobiphenyl 58.3 2/27/19 17:5230-130
2,4,6-Tribromophenol 61.6 2/27/19 17:5230-130
p-Terphenyl-d14 66.0 2/27/19 17:5230-130
Page 53 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-07
Field Sample #: GP-4 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.5 0.24 3/1/19 11:19 MJHmg/Kg dry0.040 2/26/19SW-846 6020B5Arsenic
51 6.1 3/1/19 11:19 MJHmg/Kg dry0.47 2/26/19SW-846 6020B5Chromium
9.2 2.4 3/1/19 11:19 MJHmg/Kg dry0.080 2/26/19SW-846 6020B5Lead
0.087 0.039 2/28/19 9:51 EJBmg/Kg dry0.012 2/27/19SW-846 7471B1Mercury
0.29 1.0 3/1/19 11:19 MJHmg/Kg dry0.097 2/26/19SW-846 6020B5JSelenium
0.027 0.11 3/1/19 11:19 MJHmg/Kg dry0.0097 2/26/19SW-846 6020B5JSilver
16 12 3/1/19 11:19 MJHmg/Kg dry0.49 2/26/19SW-846 6020B5Barium
ND 0.46 3/1/19 11:19 MJHmg/Kg dry0.016 2/26/19SW-846 6020B5Cadmium
Page 54 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-07
Field Sample #: GP-4 (0-2)
Sample Matrix: Soil
Sampled: 2/23/2019 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
66.5 3/1/19 7:44 AVF% Wt 2/28/19SM 2540G1% Solids
Page 55 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-08
Field Sample #: GP-4 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 14:00
[TOC_2]19B1096-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.12 2/27/19 10:59 MFFmg/Kg dry0.027 2/27/19SW-846 8260D1R-05Acetone
ND 0.0069 2/27/19 10:59 MFFmg/Kg dry0.0029 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Benzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Bromobenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00069 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1Bromoform
ND 0.012 2/27/19 10:59 MFFmg/Kg dry0.0049 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.046 2/27/19 10:59 MFFmg/Kg dry0.020 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.046 2/27/19 10:59 MFFmg/Kg dry0.024 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.00069 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0069 2/27/19 10:59 MFFmg/Kg dry0.0050 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.023 2/27/19 10:59 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Chloroethane
ND 0.0046 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Chloroform
ND 0.012 2/27/19 10:59 MFFmg/Kg dry0.0074 2/27/19SW-846 8260D1Chloromethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00069 2/27/19SW-846 8260D1Dibromomethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0046 2/27/19 10:59 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.023 2/27/19 10:59 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0046 2/27/19 10:59 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.023 2/27/19 10:59 MFFmg/Kg dry0.0021 2/27/19SW-846 8260D1Diethyl Ether
Page 56 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-08
Field Sample #: GP-4 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.00069 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.12 2/27/19 10:59 MFFmg/Kg dry0.067 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.023 2/27/19 10:59 MFFmg/Kg dry0.013 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0046 2/27/19 10:59 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.023 2/27/19 10:59 MFFmg/Kg dry0.0082 2/27/19SW-846 8260D1Methylene Chloride
ND 0.023 2/27/19 10:59 MFFmg/Kg dry0.0088 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0046 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1Naphthalene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00069 2/27/19SW-846 8260D1Styrene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0021 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0012 2/27/19 10:59 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.012 2/27/19 10:59 MFFmg/Kg dry0.0025 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Toluene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00069 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Trichloroethylene
ND 0.012 2/27/19 10:59 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.012 2/27/19 10:59 MFFmg/Kg dry0.0010 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00069 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.012 2/27/19 10:59 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0046 2/27/19 10:59 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1m+p Xylene
ND 0.0023 2/27/19 10:59 MFFmg/Kg dry0.00081 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.7 2/27/19 10:5970-130
Toluene-d8 93.5 2/27/19 10:5970-130
4-Bromofluorobenzene 110 2/27/19 10:5970-130
Page 57 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-08
Field Sample #: GP-4 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Acenaphthene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Acenaphthylene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Acetophenone
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1V-34Aniline
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Anthracene
ND 0.88 2/27/19 18:20 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.3 2/27/19 18:20 IMRmg/Kg dry0.79 2/26/19SW-846 8270D1Benzoic Acid
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.23 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Carbazole
ND 0.88 2/27/19 18:20 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.88 2/27/19 18:20 IMRmg/Kg dry0.19 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Chlorophenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Chrysene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dibenzofuran
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Diethylphthalate
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.40 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.88 2/27/19 18:20 IMRmg/Kg dry0.61 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Fluoranthene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Fluorene
Page 58 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-08
Field Sample #: GP-4 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.37 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Hexachloroethane
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Isophorone
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12-Methylphenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Naphthalene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.27 2/26/19SW-846 8270D12-Nitroaniline
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.17 2/26/19SW-846 8270D14-Nitroaniline
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Nitrobenzene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12-Nitrophenol
ND 0.88 2/27/19 18:20 IMRmg/Kg dry0.32 2/26/19SW-846 8270D14-Nitrophenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.31 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Phenanthrene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Phenol
ND 0.23 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyrene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Pyridine
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.17 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.45 2/27/19 18:20 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 82.5 2/27/19 18:2030-130
Phenol-d6 81.7 2/27/19 18:2030-130
Nitrobenzene-d5 80.7 2/27/19 18:2030-130
2-Fluorobiphenyl 78.1 2/27/19 18:2030-130
2,4,6-Tribromophenol 83.6 2/27/19 18:2030-130
p-Terphenyl-d14 85.8 2/27/19 18:2030-130
Page 59 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-08
Field Sample #: GP-4 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.43 0.23 3/1/19 11:22 MJHmg/Kg dry0.037 2/26/19SW-846 6020B5Arsenic
10 5.7 3/1/19 11:22 MJHmg/Kg dry0.44 2/26/19SW-846 6020B5Chromium
9.9 2.3 3/1/19 11:22 MJHmg/Kg dry0.074 2/26/19SW-846 6020B5Lead
ND 0.035 2/28/19 9:52 EJBmg/Kg dry0.011 2/27/19SW-846 7471B1Mercury
ND 0.95 3/1/19 11:22 MJHmg/Kg dry0.090 2/26/19SW-846 6020B5Selenium
0.011 0.099 3/1/19 11:22 MJHmg/Kg dry0.0090 2/26/19SW-846 6020B5JSilver
23 11 3/1/19 11:22 MJHmg/Kg dry0.46 2/26/19SW-846 6020B5Barium
ND 0.43 3/1/19 11:22 MJHmg/Kg dry0.014 2/26/19SW-846 6020B5Cadmium
Page 60 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-08
Field Sample #: GP-4 (6-8)
Sample Matrix: Soil
Sampled: 2/23/2019 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.0 3/1/19 7:45 AVF% Wt 2/28/19SM 2540G1% Solids
Page 61 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-09
Field Sample #: GP-5 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 14:30
[TOC_2]19B1096-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.11 2/27/19 11:23 MFFmg/Kg dry0.025 2/27/19SW-846 8260D1R-05Acetone
ND 0.0065 2/27/19 11:23 MFFmg/Kg dry0.0027 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1Benzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Bromobenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00065 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Bromoform
ND 0.011 2/27/19 11:23 MFFmg/Kg dry0.0046 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.043 2/27/19 11:23 MFFmg/Kg dry0.019 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.043 2/27/19 11:23 MFFmg/Kg dry0.023 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00065 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0065 2/27/19 11:23 MFFmg/Kg dry0.0047 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.022 2/27/19 11:23 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1Chloroethane
ND 0.0043 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1Chloroform
ND 0.011 2/27/19 11:23 MFFmg/Kg dry0.0069 2/27/19SW-846 8260D1Chloromethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00065 2/27/19SW-846 8260D1Dibromomethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0043 2/27/19 11:23 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.022 2/27/19 11:23 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0043 2/27/19 11:23 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.022 2/27/19 11:23 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1Diethyl Ether
Page 62 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-09
Field Sample #: GP-5 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00065 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.11 2/27/19 11:23 MFFmg/Kg dry0.062 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.022 2/27/19 11:23 MFFmg/Kg dry0.012 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0043 2/27/19 11:23 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.022 2/27/19 11:23 MFFmg/Kg dry0.0077 2/27/19SW-846 8260D1Methylene Chloride
ND 0.022 2/27/19 11:23 MFFmg/Kg dry0.0082 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0043 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1Naphthalene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00065 2/27/19SW-846 8260D1Styrene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0011 2/27/19 11:23 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.011 2/27/19 11:23 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1Toluene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00065 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Trichloroethylene
ND 0.011 2/27/19 11:23 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.011 2/27/19 11:23 MFFmg/Kg dry0.00098 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00087 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00065 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.011 2/27/19 11:23 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0043 2/27/19 11:23 MFFmg/Kg dry0.0018 2/27/19SW-846 8260D1m+p Xylene
ND 0.0022 2/27/19 11:23 MFFmg/Kg dry0.00076 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 95.4 2/27/19 11:2370-130
Toluene-d8 104 2/27/19 11:2370-130
4-Bromofluorobenzene 98.4 2/27/19 11:2370-130
Page 63 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-09
Field Sample #: GP-5 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Acenaphthene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Acenaphthylene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Acetophenone
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.11 2/26/19SW-846 8270D1V-34Aniline
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Anthracene
ND 0.87 2/27/19 18:47 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.3 2/27/19 18:47 IMRmg/Kg dry0.78 2/26/19SW-846 8270D1Benzoic Acid
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.30 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Carbazole
ND 0.87 2/27/19 18:47 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.87 2/27/19 18:47 IMRmg/Kg dry0.18 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Chlorophenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Chrysene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dibenzofuran
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Diethylphthalate
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.39 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.87 2/27/19 18:47 IMRmg/Kg dry0.61 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Fluoranthene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Fluorene
Page 64 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-09
Field Sample #: GP-5 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.37 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Hexachloroethane
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Isophorone
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12-Methylphenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Naphthalene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.26 2/26/19SW-846 8270D12-Nitroaniline
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.17 2/26/19SW-846 8270D14-Nitroaniline
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Nitrobenzene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12-Nitrophenol
ND 0.87 2/27/19 18:47 IMRmg/Kg dry0.32 2/26/19SW-846 8270D14-Nitrophenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.24 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.30 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Phenanthrene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Phenol
ND 0.22 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Pyrene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Pyridine
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.17 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.14 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.45 2/27/19 18:47 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 82.3 2/27/19 18:4730-130
Phenol-d6 81.0 2/27/19 18:4730-130
Nitrobenzene-d5 81.2 2/27/19 18:4730-130
2-Fluorobiphenyl 79.1 2/27/19 18:4730-130
2,4,6-Tribromophenol 82.7 2/27/19 18:4730-130
p-Terphenyl-d14 83.6 2/27/19 18:4730-130
Page 65 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-09
Field Sample #: GP-5 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
2.7 0.22 3/1/19 15:28 MJHmg/Kg dry0.036 2/26/19SW-846 6020B5Arsenic
110 11 3/4/19 10:21 MJHmg/Kg dry0.84 2/26/19SW-846 6020B10Chromium
12 2.2 3/1/19 15:28 MJHmg/Kg dry0.072 2/26/19SW-846 6020B5Lead
0.022 0.033 2/28/19 9:54 EJBmg/Kg dry0.0098 2/27/19SW-846 7471B1JMercury
0.38 0.92 3/1/19 15:28 MJHmg/Kg dry0.087 2/26/19SW-846 6020B5JSelenium
0.049 0.096 3/1/19 15:28 MJHmg/Kg dry0.0088 2/26/19SW-846 6020B5JSilver
14 11 3/1/19 15:28 MJHmg/Kg dry0.45 2/26/19SW-846 6020B5Barium
ND 0.42 3/1/19 15:28 MJHmg/Kg dry0.014 2/26/19SW-846 6020B5Cadmium
Page 66 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-09
Field Sample #: GP-5 (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
74.8 3/1/19 7:45 AVF% Wt 2/28/19SM 2540G1% Solids
Page 67 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-10
Field Sample #: GP-5 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 14:45
[TOC_2]19B1096-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 2/27/19 11:48 MFFmg/Kg dry0.031 2/27/19SW-846 8260D1R-05Acetone
ND 0.0080 2/27/19 11:48 MFFmg/Kg dry0.0033 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Benzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Bromobenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1Bromoform
ND 0.013 2/27/19 11:48 MFFmg/Kg dry0.0056 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.053 2/27/19 11:48 MFFmg/Kg dry0.023 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.053 2/27/19 11:48 MFFmg/Kg dry0.028 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0080 2/27/19 11:48 MFFmg/Kg dry0.0057 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.027 2/27/19 11:48 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1Chloroethane
ND 0.0053 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Chloroform
ND 0.013 2/27/19 11:48 MFFmg/Kg dry0.0085 2/27/19SW-846 8260D1Chloromethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Dibromomethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0053 2/27/19 11:48 MFFmg/Kg dry0.0028 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.027 2/27/19 11:48 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0053 2/27/19 11:48 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.027 2/27/19 11:48 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1Diethyl Ether
Page 68 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-10
Field Sample #: GP-5 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.13 2/27/19 11:48 MFFmg/Kg dry0.076 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.027 2/27/19 11:48 MFFmg/Kg dry0.014 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0053 2/27/19 11:48 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.027 2/27/19 11:48 MFFmg/Kg dry0.0094 2/27/19SW-846 8260D1Methylene Chloride
ND 0.027 2/27/19 11:48 MFFmg/Kg dry0.010 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0053 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1Naphthalene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D1Styrene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0013 2/27/19 11:48 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0017 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.013 2/27/19 11:48 MFFmg/Kg dry0.0029 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Toluene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D1Trichloroethylene
ND 0.013 2/27/19 11:48 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.013 2/27/19 11:48 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00080 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.013 2/27/19 11:48 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0053 2/27/19 11:48 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D1m+p Xylene
ND 0.0027 2/27/19 11:48 MFFmg/Kg dry0.00093 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.6 2/27/19 11:4870-130
Toluene-d8 103 2/27/19 11:4870-130
4-Bromofluorobenzene 115 2/27/19 11:4870-130
Page 69 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-10
Field Sample #: GP-5 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Acenaphthene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Acenaphthylene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Acetophenone
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1V-34Aniline
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Anthracene
ND 0.96 2/27/19 19:14 IMRmg/Kg dry0.26 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.5 2/27/19 19:14 IMRmg/Kg dry0.86 2/26/19SW-846 8270D1Benzoic Acid
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.25 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.34 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Carbazole
ND 0.96 2/27/19 19:14 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.96 2/27/19 19:14 IMRmg/Kg dry0.20 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12-Chlorophenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Chrysene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Dibenzofuran
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Diethylphthalate
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.44 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.96 2/27/19 19:14 IMRmg/Kg dry0.67 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.23 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.23 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Fluoranthene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Fluorene
Page 70 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-10
Field Sample #: GP-5 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.19 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.41 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Hexachloroethane
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Isophorone
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.19 2/26/19SW-846 8270D12-Methylphenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Naphthalene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.29 2/26/19SW-846 8270D12-Nitroaniline
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.19 2/26/19SW-846 8270D14-Nitroaniline
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Nitrobenzene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.20 2/26/19SW-846 8270D12-Nitrophenol
ND 0.96 2/27/19 19:14 IMRmg/Kg dry0.35 2/26/19SW-846 8270D14-Nitrophenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.26 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.34 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Phenanthrene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Phenol
ND 0.25 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pyrene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.15 2/26/19SW-846 8270D1Pyridine
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.19 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.16 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.50 2/27/19 19:14 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 76.9 2/27/19 19:1430-130
Phenol-d6 77.5 2/27/19 19:1430-130
Nitrobenzene-d5 76.3 2/27/19 19:1430-130
2-Fluorobiphenyl 75.3 2/27/19 19:1430-130
2,4,6-Tribromophenol 80.3 2/27/19 19:1430-130
p-Terphenyl-d14 76.1 2/27/19 19:1430-130
Page 71 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-10
Field Sample #: GP-5 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.47 0.25 3/1/19 10:37 MJHmg/Kg dry0.040 2/26/19SW-846 6020B5Arsenic
5.7 6.2 3/1/19 10:37 MJHmg/Kg dry0.48 2/26/19SW-846 6020B5JChromium
51 2.5 3/1/19 10:37 MJHmg/Kg dry0.081 2/26/19SW-846 6020B5MS-08, R-02Lead
ND 0.036 2/28/19 9:56 EJBmg/Kg dry0.011 2/27/19SW-846 7471B1Mercury
ND 1.0 3/1/19 10:37 MJHmg/Kg dry0.098 2/26/19SW-846 6020B5Selenium
0.025 0.11 3/1/19 10:37 MJHmg/Kg dry0.0099 2/26/19SW-846 6020B5R-04, JSilver
160 12 3/1/19 10:37 MJHmg/Kg dry0.50 2/26/19SW-846 6020B5MS-19, R-02Barium
ND 0.47 3/1/19 10:37 MJHmg/Kg dry0.016 2/26/19SW-846 6020B5Cadmium
Page 72 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-10
Field Sample #: GP-5 (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
67.8 3/1/19 7:45 AVF% Wt 2/28/19SM 2540G1% Solids
Page 73 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-11
Field Sample #: BG (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 15:00
[TOC_2]19B1096-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.95 0.20 3/1/19 15:32 MJHmg/Kg dry0.033 2/26/19SW-846 6020B5Arsenic
19 5.0 3/1/19 15:32 MJHmg/Kg dry0.38 2/26/19SW-846 6020B5Chromium
6.0 2.0 3/1/19 15:32 MJHmg/Kg dry0.065 2/26/19SW-846 6020B5Lead
0.029 0.030 2/28/19 9:57 EJBmg/Kg dry0.0090 2/27/19SW-846 7471B1JMercury
ND 0.84 3/1/19 15:32 MJHmg/Kg dry0.079 2/26/19SW-846 6020B5Selenium
0.028 0.088 3/1/19 15:32 MJHmg/Kg dry0.0080 2/26/19SW-846 6020B5JSilver
11 10 3/1/19 15:32 MJHmg/Kg dry0.41 2/26/19SW-846 6020B5Barium
ND 0.38 3/1/19 15:32 MJHmg/Kg dry0.013 2/26/19SW-846 6020B5Cadmium
Page 74 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-11
Field Sample #: BG (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
81.7 3/1/19 7:45 AVF% Wt 2/28/19SM 2540G1% Solids
Page 75 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-11
Field Sample #: BG (2-4)
Sample Matrix: Soil
Sampled: 2/23/2019 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
EPA 7199
Attached Attached 3/5/19 18:40 PALmg/KgAttached 7199 Hexavalent
Chromium Soil
17199 Hexavalent Chromium Soil
Page 76 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-12
Field Sample #: BG (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 15:15
[TOC_2]19B1096-12[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.0 0.22 3/1/19 15:35 MJHmg/Kg dry0.035 2/26/19SW-846 6020B5Arsenic
22 5.4 3/1/19 15:35 MJHmg/Kg dry0.41 2/26/19SW-846 6020B5Chromium
8.8 2.2 3/1/19 15:35 MJHmg/Kg dry0.071 2/26/19SW-846 6020B5Lead
0.016 0.033 2/28/19 9:59 EJBmg/Kg dry0.0098 2/27/19SW-846 7471B1JMercury
ND 0.90 3/1/19 15:35 MJHmg/Kg dry0.086 2/26/19SW-846 6020B5Selenium
0.032 0.095 3/1/19 15:35 MJHmg/Kg dry0.0086 2/26/19SW-846 6020B5JSilver
13 11 3/1/19 15:35 MJHmg/Kg dry0.44 2/26/19SW-846 6020B5Barium
ND 0.41 3/1/19 15:35 MJHmg/Kg dry0.014 2/26/19SW-846 6020B5Cadmium
Page 77 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-12
Field Sample #: BG (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 15:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
77.0 3/1/19 7:45 AVF% Wt 2/28/19SM 2540G1% Solids
Page 78 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-12
Field Sample #: BG (10-12)
Sample Matrix: Soil
Sampled: 2/23/2019 15:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
EPA 7199
Attached Attached 3/5/19 18:53 PALmg/KgAttached 7199 Hexavalent
Chromium Soil
17199 Hexavalent Chromium Soil
Page 79 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-13
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 2/23/2019 00:00
[TOC_2]19B1096-13[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.11 2/27/19 12:13 MFFmg/Kg dry0.026 2/27/19SW-846 8260D1R-05Acetone
ND 0.0066 2/27/19 12:13 MFFmg/Kg dry0.0027 2/27/19SW-846 8260D1Acrylonitrile
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Benzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D1Bromobenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Bromochloromethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Bromodichloromethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0015 2/27/19SW-846 8260D1Bromoform
ND 0.011 2/27/19 12:13 MFFmg/Kg dry0.0046 2/27/19SW-846 8260D1V-34Bromomethane
ND 0.044 2/27/19 12:13 MFFmg/Kg dry0.019 2/27/19SW-846 8260D12-Butanone (MEK)
ND 0.044 2/27/19 12:13 MFFmg/Kg dry0.023 2/27/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1n-Butylbenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1sec-Butylbenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1tert-Butylbenzene
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0066 2/27/19 12:13 MFFmg/Kg dry0.0047 2/27/19SW-846 8260D1Carbon Disulfide
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D1Carbon Tetrachloride
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Chlorobenzene
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Chlorodibromomethane
ND 0.022 2/27/19 12:13 MFFmg/Kg dry0.0016 2/27/19SW-846 8260D1Chloroethane
ND 0.0044 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Chloroform
ND 0.011 2/27/19 12:13 MFFmg/Kg dry0.0070 2/27/19SW-846 8260D1Chloromethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D12-Chlorotoluene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D14-Chlorotoluene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Dibromomethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0044 2/27/19 12:13 MFFmg/Kg dry0.0023 2/27/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.022 2/27/19 12:13 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1V-05Dichlorodifluoromethane (Freon 12)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,1-Dichloroethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dichloroethane
ND 0.0044 2/27/19 12:13 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,1-Dichloroethylene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D11,2-Dichloropropane
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,3-Dichloropropane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D12,2-Dichloropropane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D11,1-Dichloropropene
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.022 2/27/19 12:13 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D1Diethyl Ether
Page 80 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-13
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 2/23/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.11 2/27/19 12:13 MFFmg/Kg dry0.063 2/27/19SW-846 8260D11,4-Dioxane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D1Ethylbenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1V-05Hexachlorobutadiene
ND 0.022 2/27/19 12:13 MFFmg/Kg dry0.012 2/27/19SW-846 8260D12-Hexanone (MBK)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0044 2/27/19 12:13 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.022 2/27/19 12:13 MFFmg/Kg dry0.0078 2/27/19SW-846 8260D1Methylene Chloride
ND 0.022 2/27/19 12:13 MFFmg/Kg dry0.0084 2/27/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0044 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1Naphthalene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1n-Propylbenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D1Styrene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0020 2/27/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.0011 2/27/19 12:13 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0014 2/27/19SW-846 8260D1Tetrachloroethylene
ND 0.011 2/27/19 12:13 MFFmg/Kg dry0.0024 2/27/19SW-846 8260D1Tetrahydrofuran
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D1Toluene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0013 2/27/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0011 2/27/19SW-846 8260D1Trichloroethylene
ND 0.011 2/27/19 12:13 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D11,2,3-Trichloropropane
ND 0.011 2/27/19 12:13 MFFmg/Kg dry0.00099 2/27/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00088 2/27/19SW-846 8260D1V-051,2,4-Trimethylbenzene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00066 2/27/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.011 2/27/19 12:13 MFFmg/Kg dry0.0012 2/27/19SW-846 8260D1Vinyl Chloride
ND 0.0044 2/27/19 12:13 MFFmg/Kg dry0.0019 2/27/19SW-846 8260D1m+p Xylene
ND 0.0022 2/27/19 12:13 MFFmg/Kg dry0.00077 2/27/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.3 2/27/19 12:1370-130
Toluene-d8 104 2/27/19 12:1370-130
4-Bromofluorobenzene 105 2/27/19 12:1370-130
Page 81 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-13
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 2/23/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Acenaphthene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Acenaphthylene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Acetophenone
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.10 2/26/19SW-846 8270D1V-34Aniline
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Anthracene
ND 0.86 2/27/19 19:41 IMRmg/Kg dry0.23 2/26/19SW-846 8270D1L-04, V-34Benzidine
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(a)anthracene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(a)pyrene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(b)fluoranthene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Benzo(g,h,i)perylene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Benzo(k)fluoranthene
ND 1.3 2/27/19 19:41 IMRmg/Kg dry0.77 2/26/19SW-846 8270D1Benzoic Acid
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.22 2/26/19SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.30 2/26/19SW-846 8270D1Bis(2-chloroisopropyl)ether
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Bis(2-Ethylhexyl)phthalate
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D14-Bromophenylphenylether
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Butylbenzylphthalate
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Carbazole
ND 0.86 2/27/19 19:41 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-344-Chloroaniline
ND 0.86 2/27/19 19:41 IMRmg/Kg dry0.18 2/26/19SW-846 8270D14-Chloro-3-methylphenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12-Chloronaphthalene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12-Chlorophenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D14-Chlorophenylphenylether
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Chrysene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Dibenz(a,h)anthracene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Dibenzofuran
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Di-n-butylphthalate
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Dichlorobenzene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,3-Dichlorobenzene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11,4-Dichlorobenzene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1V-343,3-Dichlorobenzidine
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D12,4-Dichlorophenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Diethylphthalate
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4-Dimethylphenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Dimethylphthalate
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.39 2/26/19SW-846 8270D14,6-Dinitro-2-methylphenol
ND 0.86 2/27/19 19:41 IMRmg/Kg dry0.60 2/26/19SW-846 8270D12,4-Dinitrophenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,4-Dinitrotoluene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.21 2/26/19SW-846 8270D12,6-Dinitrotoluene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1Di-n-octylphthalate
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D11,2-Diphenylhydrazine/Azobenzene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Fluoranthene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Fluorene
Page 82 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-13
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 2/23/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Hexachlorobenzene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.17 2/26/19SW-846 8270D1Hexachlorobutadiene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.36 2/26/19SW-846 8270D1Hexachlorocyclopentadiene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Hexachloroethane
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Isophorone
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.12 2/26/19SW-846 8270D11-Methylnaphthalene
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D12-Methylnaphthalene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.17 2/26/19SW-846 8270D12-Methylphenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D13/4-Methylphenol
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Naphthalene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.26 2/26/19SW-846 8270D12-Nitroaniline
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1V-343-Nitroaniline
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.17 2/26/19SW-846 8270D14-Nitroaniline
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.18 2/26/19SW-846 8270D1Nitrobenzene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.18 2/26/19SW-846 8270D12-Nitrophenol
ND 0.86 2/27/19 19:41 IMRmg/Kg dry0.31 2/26/19SW-846 8270D14-Nitrophenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.23 2/26/19SW-846 8270D1N-Nitrosodimethylamine
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1N-Nitrosodiphenylamine/Diphenylamine
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.20 2/26/19SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Pentachloronitrobenzene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.30 2/26/19SW-846 8270D1Pentachlorophenol
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.12 2/26/19SW-846 8270D1Phenanthrene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D1Phenol
ND 0.22 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D1Pyrene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.13 2/26/19SW-846 8270D1Pyridine
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.17 2/26/19SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.14 2/26/19SW-846 8270D11,2,4-Trichlorobenzene
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,5-Trichlorophenol
ND 0.44 2/27/19 19:41 IMRmg/Kg dry0.16 2/26/19SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 83.0 2/27/19 19:4130-130
Phenol-d6 83.2 2/27/19 19:4130-130
Nitrobenzene-d5 81.9 2/27/19 19:4130-130
2-Fluorobiphenyl 83.9 2/27/19 19:4130-130
2,4,6-Tribromophenol 83.8 2/27/19 19:4130-130
p-Terphenyl-d14 88.3 2/27/19 19:4130-130
Page 83 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-13
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 2/23/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.4 0.22 3/1/19 15:39 MJHmg/Kg dry0.036 2/26/19SW-846 6020B5Arsenic
23 5.5 3/1/19 15:39 MJHmg/Kg dry0.42 2/26/19SW-846 6020B5Chromium
8.4 2.2 3/1/19 15:39 MJHmg/Kg dry0.072 2/26/19SW-846 6020B5Lead
0.045 0.033 2/28/19 10:00 EJBmg/Kg dry0.0098 2/27/19SW-846 7471B1Mercury
ND 0.92 3/1/19 15:39 MJHmg/Kg dry0.087 2/26/19SW-846 6020B5Selenium
0.042 0.096 3/1/19 15:39 MJHmg/Kg dry0.0088 2/26/19SW-846 6020B5JSilver
13 11 3/1/19 15:39 MJHmg/Kg dry0.45 2/26/19SW-846 6020B5Barium
ND 0.42 3/1/19 15:39 MJHmg/Kg dry0.014 2/26/19SW-846 6020B5Cadmium
Page 84 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/25/2019
Work Order: 19B1096Sample Description:Project Location: Charlotte, NC
Sample ID: 19B1096-13
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 2/23/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
75.6 3/1/19 7:46 AVF% Wt 2/28/19SM 2540G1% Solids
Page 85 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B224604 02/28/1919B1096-01 [GP-1 (0-2)]
B224604 02/28/1919B1096-02 [GP-1 (6-8)]
B224604 02/28/1919B1096-03 [GP-2 (4-6)]
B224604 02/28/1919B1096-04 [GP-2 (10-12)]
B224604 02/28/1919B1096-05 [GP-3 (2-4)]
B224604 02/28/1919B1096-06 [GP-3 (10-12)]
B224604 02/28/1919B1096-07 [GP-4 (0-2)]
B224604 02/28/1919B1096-08 [GP-4 (6-8)]
B224604 02/28/1919B1096-09 [GP-5 (2-4)]
B224604 02/28/1919B1096-10 [GP-5 (10-12)]
B224604 02/28/1919B1096-11 [BG (2-4)]
B224604 02/28/1919B1096-12 [BG (10-12)]
B224604 02/28/1919B1096-13 [DUP-1]
Prep Method: SW-846 3050B-SW-846 6020B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B224478 02/26/191.49 50.019B1096-01 [GP-1 (0-2)]
B224478 02/26/191.54 50.019B1096-02 [GP-1 (6-8)]
B224478 02/26/191.51 50.019B1096-03 [GP-2 (4-6)]
B224478 02/26/191.49 50.019B1096-04 [GP-2 (10-12)]
B224478 02/26/191.53 50.019B1096-05 [GP-3 (2-4)]
B224478 02/26/191.54 50.019B1096-06 [GP-3 (10-12)]
B224478 02/26/191.55 50.019B1096-07 [GP-4 (0-2)]
B224478 02/26/191.49 50.019B1096-08 [GP-4 (6-8)]
B224478 02/26/191.53 50.019B1096-09 [GP-5 (2-4)]
B224478 02/26/191.50 50.019B1096-10 [GP-5 (10-12)]
B224478 02/26/191.53 50.019B1096-11 [BG (2-4)]
B224478 02/26/191.51 50.019B1096-12 [BG (10-12)]
B224478 02/26/191.51 50.019B1096-13 [DUP-1]
Prep Method: SW-846 7471-SW-846 7471B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B224531 02/27/190.616 50.019B1096-01 [GP-1 (0-2)]
B224531 02/27/190.622 50.019B1096-02 [GP-1 (6-8)]
B224531 02/27/190.612 50.019B1096-03 [GP-2 (4-6)]
B224531 02/27/190.594 50.019B1096-04 [GP-2 (10-12)]
B224531 02/27/190.603 50.019B1096-05 [GP-3 (2-4)]
B224531 02/27/190.631 50.019B1096-06 [GP-3 (10-12)]
B224531 02/27/190.580 50.019B1096-07 [GP-4 (0-2)]
B224531 02/27/190.577 50.019B1096-08 [GP-4 (6-8)]
B224531 02/27/190.612 50.019B1096-09 [GP-5 (2-4)]
B224531 02/27/190.608 50.019B1096-10 [GP-5 (10-12)]
B224531 02/27/190.611 50.019B1096-11 [BG (2-4)]
B224531 02/27/190.596 50.019B1096-12 [BG (10-12)]
B224531 02/27/190.606 50.019B1096-13 [DUP-1]
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
[TOC_1]Sample Preparation Information[TOC]
Page 86 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B224530 02/27/196.03 10.019B1096-01 [GP-1 (0-2)]
B224530 02/27/195.38 10.019B1096-02 [GP-1 (6-8)]
B224530 02/27/195.44 10.019B1096-03 [GP-2 (4-6)]
B224530 02/27/195.93 10.019B1096-04 [GP-2 (10-12)]
B224530 02/27/194.43 10.019B1096-05 [GP-3 (2-4)]
B224530 02/27/196.65 10.019B1096-06 [GP-3 (10-12)]
B224530 02/27/195.83 10.019B1096-07 [GP-4 (0-2)]
B224530 02/27/195.84 10.019B1096-08 [GP-4 (6-8)]
B224530 02/27/196.17 10.019B1096-09 [GP-5 (2-4)]
B224530 02/27/195.56 10.019B1096-10 [GP-5 (10-12)]
B224530 02/27/196.02 10.019B1096-13 [DUP-1]
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B224460 02/26/1930.1 1.0019B1096-01 [GP-1 (0-2)]
B224460 02/26/1930.4 1.0019B1096-02 [GP-1 (6-8)]
B224460 02/26/1930.0 1.0019B1096-03 [GP-2 (4-6)]
B224460 02/26/1930.3 1.0019B1096-04 [GP-2 (10-12)]
B224460 02/26/1930.7 1.0019B1096-05 [GP-3 (2-4)]
B224460 02/26/1930.3 1.0019B1096-06 [GP-3 (10-12)]
B224460 02/26/1930.2 1.0019B1096-07 [GP-4 (0-2)]
B224460 02/26/1930.4 1.0019B1096-08 [GP-4 (6-8)]
B224460 02/26/1930.5 1.0019B1096-09 [GP-5 (2-4)]
B224460 02/26/1930.3 1.0019B1096-10 [GP-5 (10-12)]
B224460 02/26/1930.5 1.0019B1096-13 [DUP-1]
Page 87 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B224530 - SW-846 5035
[TOC_3]B224530[TOC]
Blank (B224530-BLK1) Prepared & Analyzed: 02/27/19
Acetone mg/Kg wet0.10 R-05ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010 V-34ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 V-05ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020 V-05ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
[TOC_1]QC Data[TOC]
Page 88 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224530 - SW-846 5035
Blank (B224530-BLK1) Prepared & Analyzed: 02/27/19
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020 V-05ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 92.30.0462
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 91.30.0457
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1070.0537
LCS (B224530-BS1) Prepared & Analyzed: 02/27/19
Acetone mg/Kg wet0.10 0.200 R-0570-1601040.207
Acrylonitrile mg/Kg wet0.0060 0.0200 70-1301040.0208
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-1301170.0234
Benzene mg/Kg wet0.0020 0.0200 V-2070-1301210.0243
Bromobenzene mg/Kg wet0.0020 0.0200 70-1301020.0203
Bromochloromethane mg/Kg wet0.0020 0.0200 70-1301240.0249
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-13099.20.0198
Bromoform mg/Kg wet0.0020 0.0200 70-13098.30.0197
Bromomethane mg/Kg wet0.010 0.0200 V-3440-13073.00.0146
2-Butanone (MEK)mg/Kg wet0.040 0.200 V-2070-1601490.298
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 40-13080.10.160
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-13086.80.0174
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-13090.60.0181
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-16085.30.0171
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-1301070.0214
Carbon Disulfide mg/Kg wet0.0060 0.0200 70-13088.70.0177
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-13095.30.0191
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301050.0210
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301040.0208
Chloroethane mg/Kg wet0.020 0.0200 70-1301170.0235
Chloroform mg/Kg wet0.0040 0.0200 70-1301090.0218
Chloromethane mg/Kg wet0.010 0.0200 70-13094.00.0188
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13099.20.0198
Page 89 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224530 - SW-846 5035
LCS (B224530-BS1) Prepared & Analyzed: 02/27/19
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-1301010.0202
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-13073.80.0148
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-1301100.0220
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301060.0212
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13097.90.0196
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13093.90.0188
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13092.20.0184
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-13097.60.0195
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 V-05, J40-16065.00.0130
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301150.0230
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-13096.40.0193
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-13079.90.0160
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301100.0220
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301120.0224
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301140.0228
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-1301040.0207
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13086.50.0173
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-1301120.0223
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13099.30.0199
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-1301000.0200
Diethyl Ether mg/Kg wet0.020 0.0200 70-1301130.0225
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-1301160.0231
1,4-Dioxane mg/Kg wet0.10 0.200 40-1601250.250
Ethylbenzene mg/Kg wet0.0020 0.0200 70-1301010.0201
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 V-0570-16079.40.0159
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-1601120.224
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301040.0209
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-13085.90.0172
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 70-13098.60.0197
Methylene Chloride mg/Kg wet0.020 0.0200 J40-16098.50.0197
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-1601120.223
Naphthalene mg/Kg wet0.0040 0.0200 40-13082.00.0164
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-1301030.0206
Styrene mg/Kg wet0.0020 0.0200 70-1301010.0203
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-13095.70.0191
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-1301070.0213
Tetrachloroethylene mg/Kg wet0.0020 0.0200 70-1301030.0206
Tetrahydrofuran mg/Kg wet0.010 0.0200 V-2070-1301270.0254
Toluene mg/Kg wet0.0020 0.0200 70-13094.40.0189
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13092.40.0185
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13081.00.0162
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13080.60.0161
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-1301010.0202
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-1301060.0211
Trichloroethylene mg/Kg wet0.0020 0.0200 70-1301050.0210
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-13084.30.0169
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-1301110.0221
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 70-13084.70.0169
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 V-0570-13084.20.0168
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13099.00.0198
Vinyl Chloride mg/Kg wet0.010 0.0200 40-1301010.0202
Page 90 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224530 - SW-846 5035
LCS (B224530-BS1) Prepared & Analyzed: 02/27/19
m+p Xylene mg/Kg wet0.0040 0.0400 70-13096.60.0386
o-Xylene mg/Kg wet0.0020 0.0200 70-13098.40.0197
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 90.50.0452
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 93.40.0467
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1090.0546
LCS Dup (B224530-BSD1) Prepared & Analyzed: 02/27/19
Acetone mg/Kg wet0.10 0.200 25 R-0570-160137 27.8 *0.274
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-130122 16.10.0244
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-130122 3.980.0243
Benzene mg/Kg wet0.0020 0.0200 25 V-2070-130125 2.720.0249
Bromobenzene mg/Kg wet0.0020 0.0200 2570-13096.0 5.630.0192
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-130129 3.400.0258
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-13093.6 5.770.0187
Bromoform mg/Kg wet0.0020 0.0200 2570-13091.9 6.740.0184
Bromomethane mg/Kg wet0.010 0.0200 25 V-3440-13081.8 11.40.0164
2-Butanone (MEK)mg/Kg wet0.040 0.200 25 L-07, V-2070-160162 8.27*0.324
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 2540-13088.4 9.760.177
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13083.3 4.060.0167
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13092.5 2.130.0185
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-16083.3 2.350.0167
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-130109 1.630.0218
Carbon Disulfide mg/Kg wet0.0060 0.0200 2570-13095.3 7.160.0191
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-130101 5.530.0201
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130100 4.780.0200
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130112 7.600.0224
Chloroethane mg/Kg wet0.020 0.0200 2570-130103 13.40.0205
Chloroform mg/Kg wet0.0040 0.0200 2570-130113 3.090.0225
Chloromethane mg/Kg wet0.010 0.0200 2570-13098.3 4.440.0197
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13092.9 6.600.0186
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13094.5 6.620.0189
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-13087.2 16.60.0174
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130121 9.690.0242
Dibromomethane mg/Kg wet0.0020 0.0200 2570-13097.1 8.930.0194
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13093.9 4.180.0188
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13088.9 5.470.0178
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13085.3 7.790.0171
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-13094.0 3.720.0188
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 V-05, J40-16067.1 3.210.0134
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130118 2.460.0236
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130102 5.220.0203
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-13084.8 6.000.0170
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130115 4.110.0230
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130112 0.2950.0223
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-130103 10.20.0206
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-130116 11.20.0232
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13091.3 5.330.0183
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-130118 5.480.0236
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13097.5 1.820.0195
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-130115 13.60.0229
Diethyl Ether mg/Kg wet0.020 0.0200 2570-130116 3.130.0233
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-130118 2.430.0237
Page 91 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224530 - SW-846 5035
LCS Dup (B224530-BSD1) Prepared & Analyzed: 02/27/19
1,4-Dioxane mg/Kg wet0.10 0.200 5040-160110 12.90.220
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-13095.8 4.960.0192
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 25 V-0570-16092.0 14.60.0184
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-160128 13.50.256
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-13098.2 6.100.0196
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-13082.5 4.050.0165
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 2570-130103 4.620.0206
Methylene Chloride mg/Kg wet0.020 0.0200 2540-160102 3.380.0204
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-160112 0.6900.225
Naphthalene mg/Kg wet0.0040 0.0200 2540-13099.3 19.00.0199
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-13098.5 4.480.0197
Styrene mg/Kg wet0.0020 0.0200 2570-13095.8 5.530.0192
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-13092.3 3.670.0185
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-13098.3 8.020.0197
Tetrachloroethylene mg/Kg wet0.0020 0.0200 2570-130119 14.50.0238
Tetrahydrofuran mg/Kg wet0.010 0.0200 25 V-2070-130128 1.120.0257
Toluene mg/Kg wet0.0020 0.0200 2570-130112 17.10.0224
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13097.9 5.770.0196
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13094.1 15.00.0188
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13093.6 15.00.0187
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130103 2.350.0207
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130123 14.80.0245
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-13097.8 7.130.0196
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-13086.0 2.000.0172
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-130104 6.030.0208
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 2570-13086.6 2.230.0173
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 25 V-0570-13080.6 4.470.0161
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13092.9 6.290.0186
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-130103 2.200.0206
m+p Xylene mg/Kg wet0.0040 0.0400 2570-13092.6 4.140.0371
o-Xylene mg/Kg wet0.0020 0.0200 2570-13094.9 3.630.0190
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 90.20.0451
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 1000.0502
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1080.0541
Page 92 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B224460 - SW-846 3546
[TOC_3]B224460[TOC]
Blank (B224460-BLK1) Prepared: 02/26/19 Analyzed: 02/27/19
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34 V-34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-34, L-04ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66 V-34ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17 V-34ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 93 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224460 - SW-846 3546
Blank (B224460-BLK1) Prepared: 02/26/19 Analyzed: 02/27/19
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34 V-34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 77.55.17
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 78.05.20
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 74.62.49
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 83.12.77
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 99.06.60
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 97.23.24
LCS (B224460-BS1) Prepared: 02/26/19 Analyzed: 02/27/19
Acenaphthene mg/Kg wet0.17 1.67 40-14080.41.34
Acenaphthylene mg/Kg wet0.17 1.67 40-14080.41.34
Acetophenone mg/Kg wet0.34 1.67 40-14068.91.15
Aniline mg/Kg wet0.34 1.67 V-3410-14027.50.458
Anthracene mg/Kg wet0.17 1.67 40-14086.21.44
Benzidine mg/Kg wet 1.67 L-04, V-3440-14035.9 *0.598
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14079.71.33
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14087.31.46
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14083.21.39
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14087.91.46
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14086.11.43
Benzoic Acid mg/Kg wet1.0 1.67 30-13067.11.12
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14090.01.50
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14073.81.23
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14082.01.37
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14084.41.41
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14090.51.51
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14085.01.42
Carbazole mg/Kg wet0.17 1.67 40-14082.41.37
4-Chloroaniline mg/Kg wet 1.67 V-3410-14027.80.463
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13083.91.40
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14069.61.16
Page 94 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224460 - SW-846 3546
LCS (B224460-BS1) Prepared: 02/26/19 Analyzed: 02/27/19
2-Chlorophenol mg/Kg wet0.34 1.67 30-13077.51.29
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14086.31.44
Chrysene mg/Kg wet0.17 1.67 40-14082.11.37
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14081.21.35
Dibenzofuran mg/Kg wet0.34 1.67 40-14082.81.38
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14086.71.45
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14062.71.04
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14061.41.02
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14061.81.03
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 V-3420-14042.20.704
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13086.71.44
Diethylphthalate mg/Kg wet0.34 1.67 40-14086.51.44
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13085.11.42
Dimethylphthalate mg/Kg wet0.34 1.67 40-14087.31.45
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13077.31.29
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13072.41.21
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-14082.11.37
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14085.41.42
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14085.21.42
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 40-14085.31.42
Fluoranthene mg/Kg wet0.17 1.67 40-14082.61.38
Fluorene mg/Kg wet0.17 1.67 40-14082.41.37
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14084.31.40
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14069.31.15
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 40-14066.21.10
Hexachloroethane mg/Kg wet0.34 1.67 40-14059.90.998
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14081.61.36
Isophorone mg/Kg wet0.34 1.67 40-14079.71.33
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14069.71.16
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14080.91.35
2-Methylphenol mg/Kg wet0.34 1.67 30-13077.41.29
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13075.81.26
Naphthalene mg/Kg wet0.17 1.67 40-14074.51.24
2-Nitroaniline mg/Kg wet0.34 1.67 40-14080.91.35
3-Nitroaniline mg/Kg wet0.34 1.67 V-3430-14058.10.968
4-Nitroaniline mg/Kg wet0.34 1.67 40-14082.01.37
Nitrobenzene mg/Kg wet0.34 1.67 40-14070.61.18
2-Nitrophenol mg/Kg wet0.34 1.67 30-13078.21.30
4-Nitrophenol mg/Kg wet0.66 1.67 30-13080.01.33
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14062.01.03
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 40-14091.61.53
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14071.71.20
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14082.71.38
Pentachlorophenol mg/Kg wet0.34 1.67 30-13080.21.34
Phenanthrene mg/Kg wet0.17 1.67 40-14085.51.42
Phenol mg/Kg wet0.34 1.67 30-13081.01.35
Pyrene mg/Kg wet0.17 1.67 40-14082.11.37
Pyridine mg/Kg wet0.34 1.67 30-14046.70.779
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14077.31.29
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14070.91.18
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13081.31.36
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13085.01.42
Page 95 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224460 - SW-846 3546
LCS (B224460-BS1) Prepared: 02/26/19 Analyzed: 02/27/19
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 77.55.17
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 81.75.44
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 75.22.50
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 86.72.89
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 94.86.32
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 88.62.95
LCS Dup (B224460-BSD1) Prepared: 02/26/19 Analyzed: 02/27/19
Acenaphthene mg/Kg wet0.17 1.67 3040-14079.0 1.781.32
Acenaphthylene mg/Kg wet0.17 1.67 3040-14079.2 1.501.32
Acetophenone mg/Kg wet0.34 1.67 3040-14071.7 4.011.19
Aniline mg/Kg wet0.34 1.67 50 V-3410-14032.7 17.50.546
Anthracene mg/Kg wet0.17 1.67 3040-14081.5 5.561.36
Benzidine mg/Kg wet 1.67 30 L-04, V-3440-14038.4 6.89*0.641
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14076.9 3.551.28
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14083.8 4.071.40
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14078.9 5.331.31
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14082.6 6.271.38
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14081.1 6.011.35
Benzoic Acid mg/Kg wet1.0 1.67 5030-13064.0 4.731.07
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14091.4 1.521.52
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14079.2 7.011.32
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14086.2 5.061.44
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14080.7 4.461.35
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14086.8 4.221.45
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14082.5 2.911.38
Carbazole mg/Kg wet0.17 1.67 3040-14077.3 6.361.29
4-Chloroaniline mg/Kg wet 1.67 30 V-3410-14030.0 7.890.501
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13081.7 2.631.36
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14069.6 0.05741.16
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13081.6 5.101.36
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14085.4 1.091.42
Chrysene mg/Kg wet0.17 1.67 3040-14079.0 3.871.32
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14075.8 6.861.26
Dibenzofuran mg/Kg wet0.34 1.67 3040-14080.3 3.021.34
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14079.9 8.261.33
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14067.6 7.581.13
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14066.7 8.241.11
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14066.0 6.451.10
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 50 V-3420-14043.3 2.430.721
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13085.3 1.581.42
Diethylphthalate mg/Kg wet0.34 1.67 3040-14083.0 4.061.38
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13086.8 1.951.45
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14084.7 3.051.41
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13072.6 6.191.21
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13071.0 1.981.18
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14079.1 3.751.32
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14083.5 2.231.39
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14079.8 6.501.33
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 3040-14078.2 8.691.30
Fluoranthene mg/Kg wet0.17 1.67 3040-14077.7 6.161.29
Fluorene mg/Kg wet0.17 1.67 3040-14080.4 2.461.34
Page 96 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224460 - SW-846 3546
LCS Dup (B224460-BSD1) Prepared: 02/26/19 Analyzed: 02/27/19
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14080.8 4.291.35
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14073.8 6.291.23
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 3040-14070.5 6.231.18
Hexachloroethane mg/Kg wet0.34 1.67 3040-14064.2 7.061.07
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14079.6 2.561.33
Isophorone mg/Kg wet0.34 1.67 3040-14080.3 0.8251.34
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14070.4 0.9711.17
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14081.7 0.9841.36
2-Methylphenol mg/Kg wet0.34 1.67 3030-13078.9 1.941.32
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13076.2 0.5271.27
Naphthalene mg/Kg wet0.17 1.67 3040-14076.9 3.221.28
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14078.2 3.341.30
3-Nitroaniline mg/Kg wet0.34 1.67 30 V-3430-14060.6 4.251.01
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14080.8 1.451.35
Nitrobenzene mg/Kg wet0.34 1.67 3040-14074.7 5.731.25
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13081.4 4.011.36
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13077.6 3.051.29
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14066.4 6.951.11
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 3040-14083.6 9.041.39
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14074.3 3.561.24
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14080.0 3.391.33
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13075.9 5.541.26
Phenanthrene mg/Kg wet0.17 1.67 3040-14080.8 5.701.35
Phenol mg/Kg wet0.34 1.67 3030-13082.1 1.451.37
Pyrene mg/Kg wet0.17 1.67 3040-14082.6 0.6561.38
Pyridine mg/Kg wet0.34 1.67 3030-14049.7 6.180.829
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14078.2 1.161.30
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14074.3 4.651.24
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13079.0 2.941.32
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13082.6 2.821.38
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 82.45.49
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 83.85.59
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 80.62.69
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 87.32.91
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 91.16.07
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 90.23.00
Matrix Spike (B224460-MS1) Prepared: 02/26/19 Analyzed: 02/27/19 Source: 19B1096-01
Acenaphthene mg/Kg dry0.22 2.18 40-14067.01.46 ND
Acenaphthylene mg/Kg dry0.22 2.18 40-14066.91.46 ND
Acetophenone mg/Kg dry0.44 2.18 40-14059.01.29 ND
Aniline mg/Kg dry0.44 2.18 MS-09, V-3440-14031.2 *0.679 ND
Anthracene mg/Kg dry0.22 2.18 40-14068.11.48 ND
Benzidine mg/Kg dry 2.18 L-04, MS-09,
R-06, V-34
40-14017.7 *0.387 ND
Benzo(a)anthracene mg/Kg dry0.22 2.18 40-14066.61.45 ND
Benzo(a)pyrene mg/Kg dry0.22 2.18 40-14072.41.58 ND
Benzo(b)fluoranthene mg/Kg dry0.22 2.18 40-14068.91.50 ND
Benzo(g,h,i)perylene mg/Kg dry0.22 2.18 40-14076.91.68 ND
Benzo(k)fluoranthene mg/Kg dry0.22 2.18 40-14070.61.54 ND
Benzoic Acid mg/Kg dry1.3 2.18 40-14065.91.44 ND
Bis(2-chloroethoxy)methane mg/Kg dry0.44 2.18 40-14077.71.69 ND
Bis(2-chloroethyl)ether mg/Kg dry0.44 2.18 40-14066.71.45 ND
Page 97 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224460 - SW-846 3546
Matrix Spike (B224460-MS1) Prepared: 02/26/19 Analyzed: 02/27/19 Source: 19B1096-01
Bis(2-chloroisopropyl)ether mg/Kg dry0.44 2.18 40-14073.31.60 ND
Bis(2-Ethylhexyl)phthalate mg/Kg dry0.44 2.18 40-14071.61.56 ND
4-Bromophenylphenylether mg/Kg dry0.44 2.18 40-14072.21.57 ND
Butylbenzylphthalate mg/Kg dry0.44 2.18 40-14073.61.60 ND
Carbazole mg/Kg dry0.22 2.18 40-14064.91.42 ND
4-Chloroaniline mg/Kg dry 2.18 MS-09, V-3440-14032.1 *0.700 ND
4-Chloro-3-methylphenol mg/Kg dry0.86 2.18 30-13066.31.45 ND
2-Chloronaphthalene mg/Kg dry0.44 2.18 40-14058.61.28 ND
2-Chlorophenol mg/Kg dry0.44 2.18 30-13067.11.46 ND
4-Chlorophenylphenylether mg/Kg dry0.44 2.18 40-14070.51.54 ND
Chrysene mg/Kg dry0.22 2.18 40-14067.81.48 ND
Dibenz(a,h)anthracene mg/Kg dry0.22 2.18 40-14069.11.51 ND
Dibenzofuran mg/Kg dry0.44 2.18 40-14068.41.49 ND
Di-n-butylphthalate mg/Kg dry0.44 2.18 40-14069.01.50 ND
1,2-Dichlorobenzene mg/Kg dry0.44 2.18 40-14058.01.26 ND
1,3-Dichlorobenzene mg/Kg dry0.44 2.18 40-14056.61.23 ND
1,4-Dichlorobenzene mg/Kg dry0.44 2.18 40-14056.21.23 ND
3,3-Dichlorobenzidine mg/Kg dry0.22 2.18 V-3440-14055.01.20 ND
2,4-Dichlorophenol mg/Kg dry0.44 2.18 30-13069.21.51 ND
Diethylphthalate mg/Kg dry0.44 2.18 40-14070.01.53 ND
2,4-Dimethylphenol mg/Kg dry0.44 2.18 30-13072.91.59 ND
Dimethylphthalate mg/Kg dry0.44 2.18 40-14072.01.57 ND
4,6-Dinitro-2-methylphenol mg/Kg dry0.44 2.18 30-13061.61.34 ND
2,4-Dinitrophenol mg/Kg dry0.86 2.18 30-13066.51.45 ND
2,4-Dinitrotoluene mg/Kg dry0.44 2.18 40-14066.71.45 ND
2,6-Dinitrotoluene mg/Kg dry0.44 2.18 40-14070.41.54 ND
Di-n-octylphthalate mg/Kg dry0.44 2.18 40-14083.51.82 ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg dry0.44 2.18 40-14069.31.51 ND
Fluoranthene mg/Kg dry0.22 2.18 40-14068.91.50 ND
Fluorene mg/Kg dry0.22 2.18 40-14068.31.49 ND
Hexachlorobenzene mg/Kg dry0.44 2.18 40-14067.11.46 ND
Hexachlorobutadiene mg/Kg dry0.44 2.18 40-14062.21.36 ND
Hexachlorocyclopentadiene mg/Kg dry0.44 2.18 30-13055.61.21 ND
Hexachloroethane mg/Kg dry0.44 2.18 40-14056.11.22 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.22 2.18 40-14072.21.57 ND
Isophorone mg/Kg dry0.44 2.18 40-14067.81.48 ND
1-Methylnaphthalene mg/Kg dry0.22 2.18 40-14058.61.28 ND
2-Methylnaphthalene mg/Kg dry0.22 2.18 40-14067.91.48 ND
2-Methylphenol mg/Kg dry0.44 2.18 30-13065.11.42 ND
3/4-Methylphenol mg/Kg dry0.44 2.18 30-13061.81.35 ND
Naphthalene mg/Kg dry0.22 2.18 40-14064.01.40 ND
2-Nitroaniline mg/Kg dry0.44 2.18 40-14066.91.46 ND
3-Nitroaniline mg/Kg dry0.44 2.18 V-3440-14055.71.21 ND
4-Nitroaniline mg/Kg dry0.44 2.18 40-14064.71.41 ND
Nitrobenzene mg/Kg dry0.44 2.18 40-14062.11.35 ND
2-Nitrophenol mg/Kg dry0.44 2.18 30-13067.31.47 ND
4-Nitrophenol mg/Kg dry0.86 2.18 30-13064.51.41 ND
N-Nitrosodimethylamine mg/Kg dry0.44 2.18 40-14056.81.24 ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg dry0.44 2.18 40-14073.01.59 ND
N-Nitrosodi-n-propylamine mg/Kg dry0.44 2.18 40-14061.51.34 ND
Pentachloronitrobenzene mg/Kg dry0.44 2.18 40-14066.21.44 ND
Pentachlorophenol mg/Kg dry0.44 2.18 30-13065.01.42 ND
Page 98 of 132
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224460 - SW-846 3546
Matrix Spike (B224460-MS1) Prepared: 02/26/19 Analyzed: 02/27/19 Source: 19B1096-01
Phenanthrene mg/Kg dry0.22 2.18 40-14068.81.50 ND
Phenol mg/Kg dry0.44 2.18 30-13066.51.45 ND
Pyrene mg/Kg dry0.22 2.18 40-14069.81.52 ND
Pyridine mg/Kg dry 2.18 MS-09, R-0640-14013.0 *0.284 ND
1,2,4,5-Tetrachlorobenzene mg/Kg dry0.44 2.18 40-14067.41.47 ND
1,2,4-Trichlorobenzene mg/Kg dry0.44 2.18 40-14061.81.35 ND
2,4,5-Trichlorophenol mg/Kg dry0.44 2.18 30-13066.01.44 ND
2,4,6-Trichlorophenol mg/Kg dry0.44 2.18 30-13069.71.52 ND
mg/Kg dry 8.72 30-130Surrogate: 2-Fluorophenol 66.85.82
mg/Kg dry 8.72 30-130Surrogate: Phenol-d6 67.25.86
mg/Kg dry 4.36 30-130Surrogate: Nitrobenzene-d5 66.52.90
mg/Kg dry 4.36 30-130Surrogate: 2-Fluorobiphenyl 72.73.17
mg/Kg dry 8.72 30-130Surrogate: 2,4,6-Tribromophenol 75.86.61
mg/Kg dry 4.36 30-130Surrogate: p-Terphenyl-d14 72.23.15
Matrix Spike Dup (B224460-MSD1) Prepared: 02/26/19 Analyzed: 02/27/19 Source: 19B1096-01
Acenaphthene mg/Kg dry0.23 2.22 3040-14069.9 5.971.55 ND
Acenaphthylene mg/Kg dry0.23 2.22 3040-14071.1 7.761.58 ND
Acetophenone mg/Kg dry0.45 2.22 3040-14063.2 8.491.40 ND
Aniline mg/Kg dry0.45 2.22 30 MS-09, V-3440-14035.6 14.9*0.789 ND
Anthracene mg/Kg dry0.23 2.22 3040-14074.4 10.51.65 ND
Benzidine mg/Kg dry 2.22 30 L-04, MS-09,
R-06, V-34
40-14031.2 56.5**0.691 ND
Benzo(a)anthracene mg/Kg dry0.23 2.22 3040-14071.2 8.291.58 ND
Benzo(a)pyrene mg/Kg dry0.23 2.22 3040-14080.2 11.81.78 ND
Benzo(b)fluoranthene mg/Kg dry0.23 2.22 3040-14079.1 15.41.75 ND
Benzo(g,h,i)perylene mg/Kg dry0.23 2.22 3040-14080.4 6.071.78 ND
Benzo(k)fluoranthene mg/Kg dry0.23 2.22 3040-14081.5 16.01.81 ND
Benzoic Acid mg/Kg dry1.3 2.22 3040-14073.3 12.41.62 ND
Bis(2-chloroethoxy)methane mg/Kg dry0.45 2.22 3040-14082.9 8.121.84 ND
Bis(2-chloroethyl)ether mg/Kg dry0.45 2.22 3040-14069.2 5.361.53 ND
Bis(2-chloroisopropyl)ether mg/Kg dry0.45 2.22 3040-14078.4 8.471.74 ND
Bis(2-Ethylhexyl)phthalate mg/Kg dry0.45 2.22 3040-14078.2 10.41.73 ND
4-Bromophenylphenylether mg/Kg dry0.45 2.22 3040-14080.5 12.51.78 ND
Butylbenzylphthalate mg/Kg dry0.45 2.22 3040-14079.7 9.601.77 ND
Carbazole mg/Kg dry0.23 2.22 3040-14071.0 10.61.57 ND
4-Chloroaniline mg/Kg dry 2.22 30 MS-09, V-3440-14033.6 6.09*0.744 ND
4-Chloro-3-methylphenol mg/Kg dry0.88 2.22 3030-13073.7 12.21.63 ND
2-Chloronaphthalene mg/Kg dry0.45 2.22 3040-14063.7 9.961.41 ND
2-Chlorophenol mg/Kg dry0.45 2.22 3030-13071.7 8.281.59 ND
4-Chlorophenylphenylether mg/Kg dry0.45 2.22 3040-14075.3 8.151.67 ND
Chrysene mg/Kg dry0.23 2.22 3040-14074.2 10.61.64 ND
Dibenz(a,h)anthracene mg/Kg dry0.23 2.22 3040-14076.0 11.31.69 ND
Dibenzofuran mg/Kg dry0.45 2.22 3040-14072.3 7.251.60 ND
Di-n-butylphthalate mg/Kg dry0.45 2.22 3040-14073.9 8.481.64 ND
1,2-Dichlorobenzene mg/Kg dry0.45 2.22 3040-14058.9 3.191.30 ND
1,3-Dichlorobenzene mg/Kg dry0.45 2.22 3040-14057.2 2.631.27 ND
1,4-Dichlorobenzene mg/Kg dry0.45 2.22 3040-14057.4 3.691.27 ND
3,3-Dichlorobenzidine mg/Kg dry0.23 2.22 30 V-3440-14052.6 2.821.17 ND
2,4-Dichlorophenol mg/Kg dry0.45 2.22 3030-13076.3 11.51.69 ND
Diethylphthalate mg/Kg dry0.45 2.22 3040-14074.9 8.381.66 ND
2,4-Dimethylphenol mg/Kg dry0.45 2.22 3030-13077.6 7.861.72 ND
Dimethylphthalate mg/Kg dry0.45 2.22 3040-14076.3 7.471.69 ND
Page 99 of 132
Table of Contents
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B224460 - SW-846 3546
Matrix Spike Dup (B224460-MSD1) Prepared: 02/26/19 Analyzed: 02/27/19 Source: 19B1096-01
4,6-Dinitro-2-methylphenol mg/Kg dry0.45 2.22 3030-13066.8 9.651.48 ND
2,4-Dinitrophenol mg/Kg dry0.88 2.22 3030-13071.5 8.901.58 ND
2,4-Dinitrotoluene mg/Kg dry0.45 2.22 3040-14071.2 8.231.58 ND
2,6-Dinitrotoluene mg/Kg dry0.45 2.22 3040-14074.3 7.031.65 ND
Di-n-octylphthalate mg/Kg dry0.45 2.22 3040-14091.2 10.42.02 ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg dry0.45 2.22 3040-14077.1 12.31.71 ND
Fluoranthene mg/Kg dry0.23 2.22 3040-14073.5 8.111.63 ND
Fluorene mg/Kg dry0.23 2.22 3040-14073.1 8.441.62 ND
Hexachlorobenzene mg/Kg dry0.45 2.22 3040-14073.7 11.11.63 ND
Hexachlorobutadiene mg/Kg dry0.45 2.22 3040-14064.6 5.471.43 ND
Hexachlorocyclopentadiene mg/Kg dry0.45 2.22 3030-13059.5 8.391.32 ND
Hexachloroethane mg/Kg dry0.45 2.22 3040-14056.0 1.361.24 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.23 2.22 3040-14078.6 10.21.74 ND
Isophorone mg/Kg dry0.45 2.22 3040-14072.2 7.961.60 ND
1-Methylnaphthalene mg/Kg dry0.23 2.22 3040-14063.0 8.851.40 ND
2-Methylnaphthalene mg/Kg dry0.23 2.22 3040-14073.1 8.961.62 ND
2-Methylphenol mg/Kg dry0.45 2.22 3030-13073.5 13.91.63 ND
3/4-Methylphenol mg/Kg dry0.45 2.22 3030-13066.4 8.791.47 ND
Naphthalene mg/Kg dry0.23 2.22 3040-14068.4 8.291.52 ND
2-Nitroaniline mg/Kg dry0.45 2.22 3040-14070.8 7.311.57 ND
3-Nitroaniline mg/Kg dry0.45 2.22 30 V-3440-14059.5 8.211.32 ND
4-Nitroaniline mg/Kg dry0.45 2.22 3040-14069.3 8.421.53 ND
Nitrobenzene mg/Kg dry0.45 2.22 3040-14066.2 7.981.47 ND
2-Nitrophenol mg/Kg dry0.45 2.22 3030-13072.5 9.091.61 ND
4-Nitrophenol mg/Kg dry0.88 2.22 3030-13067.4 6.101.49 ND
N-Nitrosodimethylamine mg/Kg dry0.45 2.22 3040-14060.3 7.621.34 ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg dry0.45 2.22 3040-14081.2 12.21.80 ND
N-Nitrosodi-n-propylamine mg/Kg dry0.45 2.22 3040-14065.8 8.401.46 ND
Pentachloronitrobenzene mg/Kg dry0.45 2.22 3040-14072.8 11.01.61 ND
Pentachlorophenol mg/Kg dry0.45 2.22 3030-13071.7 11.51.59 ND
Phenanthrene mg/Kg dry0.23 2.22 3040-14076.1 11.71.69 ND
Phenol mg/Kg dry0.45 2.22 3030-13072.8 10.71.61 ND
Pyrene mg/Kg dry0.23 2.22 3040-14080.9 16.31.79 ND
Pyridine mg/Kg dry 2.22 30 MS-09, R-0640-14026.2 68.6**0.581 ND
1,2,4,5-Tetrachlorobenzene mg/Kg dry0.45 2.22 3040-14071.9 8.081.59 ND
1,2,4-Trichlorobenzene mg/Kg dry0.45 2.22 3040-14065.9 7.971.46 ND
2,4,5-Trichlorophenol mg/Kg dry0.45 2.22 3030-13074.0 13.11.64 ND
2,4,6-Trichlorophenol mg/Kg dry0.45 2.22 3030-13076.2 10.71.69 ND
mg/Kg dry 8.86 30-130Surrogate: 2-Fluorophenol 71.36.32
mg/Kg dry 8.86 30-130Surrogate: Phenol-d6 72.46.42
mg/Kg dry 4.43 30-130Surrogate: Nitrobenzene-d5 70.53.13
mg/Kg dry 4.43 30-130Surrogate: 2-Fluorobiphenyl 78.33.47
mg/Kg dry 8.86 30-130Surrogate: 2,4,6-Tribromophenol 79.17.01
mg/Kg dry 4.43 30-130Surrogate: p-Terphenyl-d14 83.43.70
Page 100 of 132
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B224478 - SW-846 3050B
[TOC_3]B224478[TOC]
Blank (B224478-BLK1) Prepared: 02/26/19 Analyzed: 03/01/19
Arsenic mg/Kg wet0.17ND
Chromium mg/Kg wet4.2ND
Lead mg/Kg wet1.7ND
Selenium mg/Kg wet0.70ND
Silver mg/Kg wet0.073ND
Barium mg/Kg wet8.3ND
Cadmium mg/Kg wet0.32ND
LCS (B224478-BS1) Prepared: 02/26/19 Analyzed: 03/01/19
Arsenic mg/Kg wet1.9 202 82.7-117.399.2200
Chromium mg/Kg wet48 167 81.4-118104174
Lead mg/Kg wet19 73.8 82.9-117.110477.1
Selenium mg/Kg wet8.1 49.9 79.2-120.610150.6
Silver mg/Kg wet0.85 71.1 79.7-120.196.968.9
Barium mg/Kg wet97 270 82.6-117.8105283
Cadmium mg/Kg wet3.7 141 83-117105148
LCS Dup (B224478-BSD1) Prepared: 02/26/19 Analyzed: 03/01/19
Arsenic mg/Kg wet2.0 202 3082.7-117.3101 1.89204
Chromium mg/Kg wet51 167 3081.4-118106 2.07178
Lead mg/Kg wet20 73.8 3082.9-117.1105 0.55277.5
Selenium mg/Kg wet8.5 49.9 3079.2-120.6105 3.3952.3
Silver mg/Kg wet0.89 71.1 3079.7-120.197.7 0.81369.5
Barium mg/Kg wet100 270 3082.6-117.8106 1.57287
Cadmium mg/Kg wet3.8 141 3083-117107 2.00151
Duplicate (B224478-DUP1) Prepared: 02/26/19 Analyzed: 03/01/19 Source: 19B1096-10
Arsenic mg/Kg dry0.25 3519.20.389 0.471
Chromium mg/Kg dry6.2 35 J14.14.91 5.66
Lead mg/Kg dry2.5 35 R-0296.9 *17.7 50.9
Selenium mg/Kg dry1.0 35NCNDND
Silver mg/Kg dry0.11 35 R-04, J53.7 *0.0145 0.0251
Barium mg/Kg dry12 35 R-02108*46.8 157
Cadmium mg/Kg dry0.47 35NCNDND
Matrix Spike (B224478-MS1) Prepared: 02/26/19 Analyzed: 03/01/19 Source: 19B1096-10
Arsenic mg/Kg dry0.97 24.1 75-12595.323.5 0.471
Chromium mg/Kg dry24 24.1 75-12511232.7 5.66
Lead mg/Kg dry9.7 24.1 MS-0875-125-36.2 *42.2 50.9
Selenium mg/Kg dry4.1 24.1 75-12595.223.0 ND
Silver mg/Kg dry0.42 24.1 75-12510324.8 ND
Barium mg/Kg dry48 24.1 MS-1975-125-364 *69.5 157
Cadmium mg/Kg dry1.8 24.1 75-12510625.7 ND
Page 101 of 132
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
Batch B224531 - SW-846 7471
[TOC_3]B224531[TOC]
Blank (B224531-BLK1) Prepared: 02/27/19 Analyzed: 02/28/19
Mercury mg/Kg wet0.025ND
LCS (B224531-BS1) Prepared: 02/27/19 Analyzed: 02/28/19
Mercury mg/Kg wet0.38 3.71 65-1351043.87
LCS Dup (B224531-BSD1) Prepared: 02/27/19 Analyzed: 02/28/19
Mercury mg/Kg wet0.37 3.71 3065-13588.9 16.13.30
Duplicate (B224531-DUP1) Prepared: 02/27/19 Analyzed: 02/28/19 Source: 19B1096-01
Mercury mg/Kg dry0.032 352.820.408 0.397
Matrix Spike (B224531-MS1) Prepared: 02/27/19 Analyzed: 02/28/19 Source: 19B1096-01
Mercury mg/Kg dry0.032 0.426 75-1251050.845 0.397
Page 102 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B224604 - % Solids
[TOC_3]B224604[TOC]
Duplicate (B224604-DUP1) Prepared: 02/28/19 Analyzed: 03/01/19 Source: 19B1096-03
% Solids % Wt 200.35968.4 68.7
Duplicate (B224604-DUP2) Prepared: 02/28/19 Analyzed: 03/01/19 Source: 19B1096-11
% Solids % Wt 200.28082.0 81.7
Page 103 of 132
Table of Contents
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Matrix spike recovery outside of control limits. Possibility of sample matrix effects that lead to a low bias for
reported result or non-homogeneous sample aliquots cannot be eliminated.
MS-08
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample
matrix effects that lead to a low bias for reported result or non-homogeneous sample aliquots cannot be
eliminated.
MS-09
Sample to spike ratio is greater than or equal to 4:1. Spiked amount is not representative of the native amount in
the sample. Appropriate or meaningful recoveries cannot be calculated.
MS-19
Duplicate RPD is outside of control limits. Outlier can be attributed to sample non-homogeneity encountered
during sample prep.
R-02
Duplicate relative percent difference (RPD) is a less useful indicator of sample precision for sample results that
are <5 times the reporting limit (RL).
R-04
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Matrix spike duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result for
this compound in this sample.
R-06
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
[TOC_1]Flag/Qualifier Summary[TOC]
Page 104 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 6020B in Soil
NY,VA,NH,NC,MEArsenic
NY,NC,MEChromium
NY,NC,MELead
NY,VA,NH,NC,MESelenium
NY,NC,MESilver
NY,NCBarium
NY,NC,MECadmium
SW-846 7471B in Soil
CT,NH,NY,NC,ME,VAMercury
SW-846 8260D in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
[TOC_1]Certifications[TOC]
Page 105 of 132
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
Page 106 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine/Azobenzene
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
Page 107 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
SW-846 8270D in Water
CT,NY,NC,ME,NH,VAAcenaphthene
CT,NY,NC,ME,NH,VAAcenaphthylene
NY,NCAcetophenone
CT,NY,NC,ME,VAAniline
CT,NY,NC,ME,NH,VAAnthracene
CT,NY,NC,ME,NH,VABenzidine
CT,NY,NC,ME,NH,VABenzo(a)anthracene
CT,NY,NC,ME,NH,VABenzo(a)pyrene
CT,NY,NC,ME,NH,VABenzo(b)fluoranthene
CT,NY,NC,ME,NH,VABenzo(g,h,i)perylene
CT,NY,NC,ME,NH,VABenzo(k)fluoranthene
NY,NC,ME,NH,VABenzoic Acid
CT,NY,NC,ME,NH,VABis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VABis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VABis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VABis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA4-Bromophenylphenylether
CT,NY,NC,ME,NH,VAButylbenzylphthalate
NCCarbazole
CT,NY,NC,ME,NH,VA4-Chloroaniline
CT,NY,NC,ME,NH,VA4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA2-Chloronaphthalene
CT,NY,NC,ME,NH,VA2-Chlorophenol
Page 108 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Water
CT,NY,NC,ME,NH,VA4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VAChrysene
CT,NY,NC,ME,NH,VADibenz(a,h)anthracene
CT,NY,NC,ME,NH,VADibenzofuran
CT,NY,NC,ME,NH,VADi-n-butylphthalate
CT,NY,NC,ME,NH,VA1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA2,4-Dichlorophenol
CT,NY,NC,ME,NH,VADiethylphthalate
CT,NY,NC,ME,NH,VA2,4-Dimethylphenol
CT,NY,NC,ME,NH,VADimethylphthalate
CT,NY,NC,ME,NH,VA4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VADi-n-octylphthalate
NY,NC1,2-Diphenylhydrazine/Azobenzene
CT,NY,NC,ME,NH,VAFluoranthene
NY,NC,ME,NH,VAFluorene
CT,NY,NC,ME,NH,VAHexachlorobenzene
CT,NY,NC,ME,NH,VAHexachlorobutadiene
CT,NY,NC,ME,NH,VAHexachlorocyclopentadiene
CT,NY,NC,ME,NH,VAHexachloroethane
CT,NY,NC,ME,NH,VAIndeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NC,ME,NH,VA2-Methylnaphthalene
CT,NY,NC,NH,VA2-Methylphenol
CT,NY,NC,NH,VA3/4-Methylphenol
CT,NY,NC,ME,NH,VANaphthalene
CT,NY,NC,ME,NH,VA2-Nitroaniline
CT,NY,NC,ME,NH,VA3-Nitroaniline
CT,NY,NC,ME,NH,VA4-Nitroaniline
CT,NY,NC,ME,NH,VANitrobenzene
CT,NY,NC,ME,NH,VA2-Nitrophenol
CT,NY,NC,ME,NH,VA4-Nitrophenol
CT,NY,NC,ME,NH,VAN-Nitrosodimethylamine
CT,NY,NC,ME,NH,VAN-Nitrosodi-n-propylamine
NCPentachloronitrobenzene
CT,NY,NC,ME,NH,VAPentachlorophenol
CT,NY,NC,ME,NH,VAPhenanthrene
CT,NY,NC,ME,NH,VAPhenol
CT,NY,NC,ME,NH,VAPyrene
CT,NY,NC,ME,NH,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
Page 109 of 132
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Water
CT,NY,NC,ME,NH,VA1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2005AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2019
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2019
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2019
E871027 NELAPFlorida Department of HealthFL 06/30/2019
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2019
2011028State of MaineME 06/9/2019
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2019
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2019
25703North Carolina Department of HealthNC-DW 07/31/2019
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#=CL#
March 06, 2019
LIMS USE: FR - LAURIE
LIMS OBJECT ID: 92419620
92419620
Project:
Pace Project No.:
RE:
Laurie Kopyscinski
Con-Test Analytical Laboratory
39 Spruce Street
East Longmeadow, MA 01028
19B1096 2/23
Dear Laurie Kopyscinski:
Enclosed are the analytical results for sample(s) received by the laboratory on February 28, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
[phone]
Enclosures
cc:Kerry McGee, Con-Test Analytical Laboratory
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 18Page 115 of 132
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#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92419620
19B1096 2/23
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 18Page 116 of 132
Table of Contents
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92419620
19B1096 2/23
Lab ID Sample ID Matrix Date Collected Date Received
92419620001 19B1096-01 Solid 02/23/19 10:15 02/28/19 18:40
92419620002 19B1096-02 Solid 02/23/19 10:30 02/28/19 18:40
92419620003 19B1096-05 Solid 02/23/19 13:00 02/28/19 18:40
92419620004 19B1096-06 Solid 02/23/19 13:15 02/28/19 18:40
92419620005 19B1096-11 Solid 02/23/19 15:00 02/28/19 18:40
92419620006 19B1096-12 Solid 02/23/19 15:15 02/28/19 18:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 18Page 117 of 132
Table of Contents
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92419620
19B1096 2/23
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92419620001 19B1096-01 ASTM D2974-87 1 PASI-OCLT
EPA 7199 1 PASI-OALD
92419620002 19B1096-02 ASTM D2974-87 1 PASI-OCLT
EPA 7199 1 PASI-OALD
92419620003 19B1096-05 ASTM D2974-87 1 PASI-OCLT
EPA 7199 1 PASI-OALD
92419620004 19B1096-06 ASTM D2974-87 1 PASI-OCLT
EPA 7199 1 PASI-OALD
92419620005 19B1096-11 ASTM D2974-87 1 PASI-OCLT
EPA 7199 1 PASI-OALD
92419620006 19B1096-12 ASTM D2974-87 1 PASI-OCLT
EPA 7199 1 PASI-OALD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 18Page 118 of 132
Table of Contents
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92419620
19B1096 2/23
Sample:19B1096-01 Lab ID:92419620001 Collected:02/23/19 10:15 Received:02/28/19 18:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.5 %03/05/19 08:530.10 0.10 1
Analytical Method: EPA 7199 Preparation Method: EPA 30607199 Hexavalent Chromium Soil
Chromium, Hexavalent 1.2 mg/kg 03/05/19 17:48 18540-29-903/04/19 12:050.85 0.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 18Page 119 of 132
Table of Contents
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92419620
19B1096 2/23
Sample:19B1096-02 Lab ID:92419620002 Collected:02/23/19 10:30 Received:02/28/19 18:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.1 %03/05/19 08:530.10 0.10 1
Analytical Method: EPA 7199 Preparation Method: EPA 30607199 Hexavalent Chromium Soil
Chromium, Hexavalent <0.35 mg/kg 03/05/19 18:01 18540-29-903/04/19 12:050.83 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 18Page 120 of 132
Table of Contents
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92419620
19B1096 2/23
Sample:19B1096-05 Lab ID:92419620003 Collected:02/23/19 13:00 Received:02/28/19 18:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.3 %03/05/19 08:530.10 0.10 1
Analytical Method: EPA 7199 Preparation Method: EPA 30607199 Hexavalent Chromium Soil
Chromium, Hexavalent <0.33 mg/kg 03/05/19 18:14 18540-29-903/04/19 12:050.78 0.33 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 18Page 121 of 132
Table of Contents
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92419620
19B1096 2/23
Sample:19B1096-06 Lab ID:92419620004 Collected:02/23/19 13:15 Received:02/28/19 18:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.3 %03/05/19 08:530.10 0.10 1
Analytical Method: EPA 7199 Preparation Method: EPA 30607199 Hexavalent Chromium Soil
Chromium, Hexavalent <0.36 mg/kg 03/05/19 18:27 18540-29-903/04/19 12:050.85 0.36 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 8 of 18Page 122 of 132
Table of Contents
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92419620
19B1096 2/23
Sample:19B1096-11 Lab ID:92419620005 Collected:02/23/19 15:00 Received:02/28/19 18:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.9 %03/05/19 08:530.10 0.10 1
Analytical Method: EPA 7199 Preparation Method: EPA 30607199 Hexavalent Chromium Soil
Chromium, Hexavalent <0.34 mg/kg 03/05/19 18:40 18540-29-903/04/19 12:050.82 0.34 1
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 9 of 18Page 123 of 132
Table of Contents
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92419620
19B1096 2/23
Sample:19B1096-12 Lab ID:92419620006 Collected:02/23/19 15:15 Received:02/28/19 18:40 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.6 %03/05/19 08:530.10 0.10 1
Analytical Method: EPA 7199 Preparation Method: EPA 30607199 Hexavalent Chromium Soil
Chromium, Hexavalent <0.33 mg/kg 03/05/19 18:53 18540-29-903/04/19 12:050.80 0.33 1
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 10 of 18Page 124 of 132
Table of Contents
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92419620
19B1096 2/23
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
520440
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92419620001, 92419620002, 92419620003, 92419620004, 92419620005, 92419620006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
35451429006
2810251SAMPLE DUPLICATE:
Percent Moisture %24.7 6 1023.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
35451491005
2810252SAMPLE DUPLICATE:
Percent Moisture %6.3 7 105.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
35451418001
2810253SAMPLE DUPLICATE:
Percent Moisture %8.3 4 108.0
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
35451522003
2810254SAMPLE DUPLICATE:
Percent Moisture %8.1 6 107.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 18Page 125 of 132
Table of Contents
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92419620
19B1096 2/23
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
519403
EPA 3060
EPA 7199
7199 Hexavelent Chromium Soil
Associated Lab Samples:92419620001, 92419620002, 92419620003, 92419620004, 92419620005, 92419620006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2804549
Associated Lab Samples:92419620001, 92419620002, 92419620003, 92419620004, 92419620005, 92419620006
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg <0.26 0.63 03/05/19 12:590.26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2804550LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 41.340.7 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2804552MATRIX SPIKE SAMPLE:
MSSpike
Result
35450378001
Chromium, Hexavalent mg/kg <0.27 M140 0 75-1250.28U
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
35450378001
2804551SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg <0.27 H3200.28U
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 18Page 126 of 132
Table of Contents
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92419620
19B1096 2/23
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Sample was received or analysis requested beyond the recognized method holding time.H3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 18Page 127 of 132
Table of Contents
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92419620
19B1096 2/23
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92419620001 52044019B1096-01 ASTM D2974-87
92419620002 52044019B1096-02 ASTM D2974-87
92419620003 52044019B1096-05 ASTM D2974-87
92419620004 52044019B1096-06 ASTM D2974-87
92419620005 52044019B1096-11 ASTM D2974-87
92419620006 52044019B1096-12 ASTM D2974-87
92419620001 519403 52063319B1096-01 EPA 3060 EPA 7199
92419620002 519403 52063319B1096-02 EPA 3060 EPA 7199
92419620003 519403 52063319B1096-05 EPA 3060 EPA 7199
92419620004 519403 52063319B1096-06 EPA 3060 EPA 7199
92419620005 519403 52063319B1096-11 EPA 3060 EPA 7199
92419620006 519403 52063319B1096-12 EPA 3060 EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/06/2019 12:46 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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