22039 1300 W Morehead St BAR 2019.01.21

Brownfields Assessment Report
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
Brownfields Project No. 22039-18-060
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2923 South Tryon Street, Suite 100 I 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607
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704.586.0007 main 1 919.847.4241 main
www.harthickman.com

Brownfields Assessment Report
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
Brownfields Project No. 22039-18-060
H&H Job No. COP-008
Table of Contents
1.0 Introduction and Background.....................................................................................................1
2.0 Brownfields Assessment Activities..............................................................................................4
3.0 Soil Assessment Activities............................................................................................................5
3.1 Soil Sampling Methodology
3.2 Soil Analytical Results
5
6
4.0 Groundwater Assessment Activities...........................................................................................9
4.1 Groundwater Sampling Methodology
4.2 Groundwater Analytical Results
N
11
5.0 Vapor Intrusion Assessment Activities....................................................................................12
5.1 Sub -Slab Vapor Sampling Methodology...........................................................................12
5.2 Sub -Slab Vapor Analytical Results....................................................................................13
5.3 Indoor Air Sampling Methodology....................................................................................14
5.4 Indoor Air Analytical Results.............................................................................................15
6.0 Receptor Survey Activities........................................................................................................17
7.0 Conclusions and Recommendations.........................................................................................19
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hart hickman
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Table 1 Summary of Soil Analytical Results
Table 2 Summary of Temporary Well Construction and Groundwater Elevation Data
Table 3 Summary of Groundwater Analytical Results
Table 4 Summary of Sub -Slab Vapor Analytical Results
Table 5 Summary of Indoor Air Analytical Results
List of Figures
Figure 1 Site Location Map
Figure 2 Site and Sample Location Map
Figure 3 Groundwater Potentiometric Surface Map
Figure 4 Receptor Survey Map
List of Appendices
Appendix A
Boring Logs
Appendix B
Laboratory Analytical Reports
Appendix C
DEQ Risk Calculator Output
Appendix D
Field Forms
Appendix E
Brownfields Property Receptor Survey Form
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hart hickman
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Brownfields Assessment Report
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
Brownfields Project No. 22039-18-060
H&H Job No. COP-008
1.0 Introduction and Background
Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment Report on behalf of 1300
West Morehead LLC (Prospective Developer or PD) for the commercial property (Brownfields
Project No. 22039-18-060) located at 1300 W. Morehead Street in Charlotte, Mecklenburg County,
North Carolina (Site). A Site location map is provided as Figure 1.
The Site consists of one parcel of land (Parcel Identification Number 07324102) that is an
approximately 0.36 acre. The central and northern portions of the Site are developed with an
approximately 11,700-square foot (sq ft) office/warehouse building that is used as a real estate
management office and for miscellaneous storage by the Site owner. The southern portion of the
Site consists of an asphalt -paved parking lot. A Site map is included as Figure 2.
Based on review of historical records, it appears that the Site was developed prior to 1929 as an
automotive sales and service facility. Subsequently, the facility was utilized as a truck wholesale
facility (1930s until the early 1950s), a training center and armory for the United States Marine
Corps (1950s), a textile machinery warehouse (early 1960s), a truck tire shop (late 1970s), and an
office/warehouse for various businesses (1980s to present).
According to a Phase I Environmental Site Assessment (ESA) dated June 21, 1999 prepared by
EnviroAssessments, PLLC, an adjacent property located west-northwest and topographically
upgradient of the Site (1310 W. Morehead Street) was occupied by a trailer manufacturing company
from 1941 to 1946, a motor equipment service company from the late 1940s to 1960, metal
fabrication facilities in the 1970s and 1980s, and an automotive repair facility in the 1990s.
In September 1999, Phase II ESA groundwater sampling activities were conducted at the
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adjacent property at 1310 W. Morehead Street. Analytical data indicated the presence of
trichloroethene (TCE; 58 µg/L) in a monitoring well (GP-2-W) at a concentration above the
North Carolina 2L Groundwater Standard (2L Standard) of 3.0 µg/L. Bis(2-ethylhexyl)phthalate
(35 µg/L) was also detected in GP-2-W above the 2L Standard of 3.0 µg/L. GP-2-W is located
approximately 30 ft northwest and topographically upgradient of the Site. A Brownfields
Agreement (amended) was filed for the adjacent property at 1310 W. Morehead Street in
March 2002 (Brownfields Property No. 04001-00-060).
During subsequent due diligence related assessment activities performed at 1310 W. Morehead
Street in 2015, TICE was detected at a concentration of 930 µg/L in a groundwater sample
collected adjacent to the southwestern Site boundary. TCE and tetrachloroethene (PCE) were
also detected above the North Carolina Department of Environmental Quality (DEQ) Sub -Slab
and Exterior Soil Gas Screening Levels (SGSLs) during the 2015 due diligence assessment.
The Site received a letter of eligibility for entry into the North Carolina Department of
Environmental Quality (DEQ) Brownfields Program (Brownfields Project No. 22039-18-060) on
July 18, 2018. The PD elected to participate in the Brownfields Program Redevelopment Now
option.
On October 5, 2018, a kick-off/data gap meeting was held with the PD, DEQ Brownfields Program
personnel, and H&H to discuss Site history, previous environmental assessment activities at the
adjacent Brownfields property, proposed redevelopment plans, data gaps, and the proposed schedule
for completing the Brownfields Agreement. To address the data gaps, H&H submitted a
Brownfields Assessment Work Plan (Work Plan) for additional assessment activities on November
5, 2018. DEQ indicated via email correspondence on November 16, 2018 that the Work Plan was
approved pending completion of revisions to the Work Plan as noted by DEQ. H&H submitted a
revised version of the Work Plan on November 16, 2018.
To evaluate the potential for impacts associated with environmental concerns identified during
the previous off -Site Phase II ESA activities at 1310 W. Morehead Street and based on the
October 2018 data gap meeting, H&H proposed to conduct soil, groundwater, soil vapor, and
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indoor air assessment activities at the Site. H&H also conducted a sensitive receptor survey in
the nearby surrounding area of the Site. The Brownfields assessment activities were completed
in accordance with the DEQ-approved Work Plan. The methods and results of the assessment
activities are summarized in the following sections.
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2.0 Brownfields Assessment Activities
In November and December 2018, H&H completed soil, groundwater, sub -slab vapor, and
indoor air assessment activities at the Site to evaluate potential impacts associated with historical
Site and nearby property uses and to assist in the development of an Environmental Management
Plan (EMP) for use during future redevelopment of the Site. Soil, groundwater, soil vapor, and
indoor air sample locations are depicted on Figure 2.
Prior to conducting assessment activities, H&H contacted North Carolina 811, the public utility
locator, to mark subsurface utilities on the Site. H&H also contracted with Probe Utility
Locating, a private utility locator, to screen proposed sample locations for subgrade utilities and to
confirm public utility locator markings. Additionally, boring locations were hand cleared to
approximately 5 ft below the ground surface (bgs) to further screen the boring locations for the
presence of subsurface utilities. In accordance with Mecklenburg County regulations, H&H
obtained a Subsurface Investigation Permit (SIP No. 70002568) from the Mecklenburg County
Land Use and Environmental Services Agency (LUESA) prior to beginning groundwater
assessment activities.
The assessment activities were conducted in general accordance with the DEQ Inactive Hazardous
Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated October 2015, DEQ's Division
of Waste Management (DWM) Vapor Intrusion Guidance dated March 2018, and the most recent
versions of the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem
Support (SESD) Field Branches Quality System and Technical Procedures guidance. The results of
the soil, groundwater, and vapor intrusion assessment are provided in Sections 3.0, 4.0, and 5.0,
respectively; the receptor survey results are provided in Section 6.0; and conclusions and
recommendations based on the results of the assessment activities are provided in Section 7.0.
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3.0 Soil Assessment Activities
3.1 Soil Sampling Methodology
On December 3 and 4, 2018, H&H contracted Carolina Soil Investigations (CSI), a North
Carolina -licensed drilling contractor, to advance five soil borings (SB-1 through SB-5) using a
track -mounted direct push technology (DPT) drill rig and hand auger. Soil boring locations are
described below and are depicted on Figure 2.
• Four soil borings (SB-1 and SB-3 through SB-5) were advanced to 10 ft bgs adjacent to
floor drains in the warehouse.
• One soil boring (SB-2) was advanced to 25 ft bgs adjacent to a sump in the warehouse.
H&H also advanced a background soil boring (BKG-SOIL-1) to 10 ft bgs in the parking area in
the southern portion of the Site to establish Site -specific background concentrations for naturally
occurring metals.
Continuous soil samples were collected from each boring, logged for lithologic description, and
screened for the presence of staining, odors, and volatile organic vapors using a calibrated
photoionization detector (PID). Boring logs are provided in Appendix A.
Based upon field screening results, no obvious indications of potential soil impacts were
observed. Therefore, the soil samples were collected from depth intervals most likely to be
impacted (e.g., depth interval below the floor drains). A soil sample was collected from boring
SB-2 from a depth of 4.0 to 6.0 ft bgs, and soil samples were collected from borings SB-3 and
SB-5 from a depth of 1.0 to 3.0 ft bgs. In accordance with the DEQ-approved Work Plan, no soil
samples were collected from borings SB-1 and SB-4 based on the lack of obvious field evidence
of impacts.
Soil samples selected for laboratory analysis were placed directly into dedicated laboratory -
supplied sample containers; labeled with the sample identification, date, and requested analysis;
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and placed in a laboratory -supplied sample cooler with ice. The samples were delivered to Con -
Test Analytical Laboratory (Con -Test), a North Carolina certified laboratory, under standard chain
of custody protocols for analysis of volatile organic compounds (VOCs) by EPA Method 8260B,
semi-VOCs (SVOCs) by EPA Method 8270D, Resource Conservation and Recovery Act
(RCRA) metals by EPA Methods 602013/7471 B, and hexavalent chromium by EPA Method
7199. The background soil sample was analyzed for RCRA metals by EPA Method 602013/7471B
and hexavalent chromium by EPA Method 7199.
For quality assurance purposes, a duplicate soil sample was collected from the SB-5 parent soil
sample and submitted to Con -Test for analysis of VOCs by EPA Method 8260B, SVOCs by EPA
Method 8270D, RCRA metals by EPA Methods 6020A/7471 B, and hexavalent chromium by EPA
Method 7199.
3.2 Soil Analytical Results
A tabular summary of soil analytical results is presented in Table 1. The laboratory analytical
report and chain of custody record are provided in Appendix B. The soil analytical results were
compared to the DEQ IHSB Unrestricted Use and Industrial/Commercial Preliminary Soil
Remediation Goals (PSRGs) dated February 2018. In addition to the PSRGs, metals data were
compared to Site -specific background levels and published regional background concentrations.
Laboratory analytical results indicate the presence of acetone (0.036 to 0.048 mg/kg) in samples
SB-2 (4-6 ft), SB-3 (1-3 ft), and SB-5 (1-3 ft) at estimated concentrations (i.e., "J flag" values)
below the PSRGs. Acetone is a common laboratory contaminant; therefore, the detection of
trace levels of acetone may not be representative of Site soil conditions. No other VOCs were
detected the soil samples above the laboratory method detection limits (MDLs).
Results of SVOC analysis indicate that bis(2-ethylhexyl)phthalate (0.38 mg/kg) was detected in
sample SB-3 (1-3 ft) at a concentration below the Unrestricted Use PSRG of 39 mg/kg. No other
SVOCs were detected above the MDLs.
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Several metals, including arsenic, barium, cadmium, chromium, lead, mercury, selenium, and
silver, were detected in samples SB-2 (4-6 ft), SB-3 (1-3 ft), and SB-5 (1-3 ft). Arsenic (1.6
mg/kg) was detected in sample SB-3 (1-3 ft) at a concentration above the Unrestricted Use
PSRG of 0.68 mg/kg. However, the detected concentration is below the Site -specific
background concentration of 1.9 mg/kg and the average published background concentration of
4.8 mg/kg for North Carolina soils. Total chromium was detected in samples SB-2 (4-6 ft), SB-3
(1-3 ft), and SB-5 (1-3 ft) at concentrations ranging from 9.5 mg/kg to 66 mg/kg, which are
below the Site -specific background concentration of 96 mg/kg and generally consistent with the
average published background concentration of 65 mg/kg for North Carolina soils. In
accordance with DEQ's request, the background sample was analyzed for hexavalent chromium.
Hexavalent chromium was detected in the background sample at a concentration of 2.3 mg/kg,
which is above the Unrestricted Use PSRG of 0.31 mg/kg. The remaining soil samples were not
analyzed for hexavalent chromium. The detected metals concentrations are likely naturally
occurring.
Analytical data for the duplicate soil sample (DUP-SOIL-1) are generally consistent with the data
for the parent sample (SB-5). This result indicates good quality control with regard to data
repeatability.
DEQ Risk Calculator
As noted above, hexavalent chromium and arsenic were detected in soil at concentrations above
the Unrestricted Use PSRGs. However, the DEQ PSRGs are conservative and based upon
lifetime incremental cancer risk (LICR) for potential carcinogenic risks of 1 x 10"6 and a non -
carcinogenic hazard index (HI) of 0.2 for potential non -carcinogenic risks. The DEQ acceptable
LICR is typically 1 x 10-4, and the acceptable cumulative risk level for non -carcinogenic risks is
an HI equal to or less than 1. Therefore, H&H used DEQ's risk calculator (February 2018) to
calculate potential cumulative risks at the Site using the highest concentrations of VOCs,
SVOCs, and metals detected in the soil samples. H&H utilized the DEQ risk calculator for
residential, non-residential, and construction worker hypothetical land use scenarios. The results
of risk calculations are summarized below and are included in Appendix C.
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Land Use Scenario
Calculated
Calculated
Calculated LICR or
Cumulative LICR
Cumulative Hl
HI Exceeds
Acceptable Risk
Levels?
Residential
1.0 x 10-5
0.09
No
Non -Residential Worker
9.9 x 10-7
0.0087
No
Construction Worker
7.5 x 10"7
0.06
No
As shown in the above table, the results of the risk calculations using combined Site soil data
indicate that the calculated cumulative risks are below acceptable risk levels for the residential, non-
residential worker, and construction worker exposure scenarios.
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4.0 Groundwater Assessment Activities
4.1 Groundwater Sampling Methodology
On December 3 and 4, 2018, CSI installed three temporary monitoring wells (TMW-1 through
TMW-3) using DPT drilling methods. Temporary monitoring well locations are depicted on
Figure 2 and are described as follows:
• One temporary monitoring well (TMW-1) was installed in the southern portion of the Site
and downgradient of documented off -Site chlorinated solvent impacts at the adjacent
property at 1310 W. Morehead Street.
• One temporary monitoring well (TMW-2) was installed adjacent to the on -Site sump and in
the downgradient portion of the warehouse.
• One temporary monitoring well (TMW-3) was installed in the northern (upgradient) portion
of the Site to evaluate potential groundwater impacts from off -Site sources and background
concentrations of naturally occurring metals.
Continuous soil samples were collected from the temporary well borings. H&H field screened the
samples for the presence of staining, odors, and volatile organic vapors using a calibrated PID.
Elevated PID readings were observed during screening of temporary well boring TMW-1 from
depths of approximately 5.0 to 25 ft bgs. The PID readings appear to be related to
moisture/humidity and/or chlorinated solvent -impacted groundwater at this location (see Section
4.2).
The temporary monitoring wells were constructed of 1-inch diameter PVC riser pipe with 10 ft of
pre -packed well screen set to bracket the water table. Additional filter sand was placed in the well
annulus from the base of the borehole to approximately two feet above the well screen. At least 2 ft
of hydrated bentonite was placed above the sand pack of each well. Temporary well boring logs are
provided in Appendix A, and temporary well construction details are provided in Table 2.
Upon completion of temporary monitoring well installation activities, the top of casing elevations
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were surveyed relative to an arbitrary datum of 100 ft, and depth to groundwater measurements
were collected using an electronic water level indicator. On December 5, 2018, depths to the
equilibrated water table ranged from approximately 12.02 ft bgs (TMW-3) in the northern portion of
the Site to 13.22 ft bgs (TMW-1) in the southern portion of the Site. Based on the groundwater
elevation data, groundwater flow at the Site is generally to the south. A groundwater potentiometric
surface map is provided as Figure 3.
Each temporary well was developed until field parameters stabilized (pH f 0.1 SU and conductivity
varied no more than 5%) by removing a minimum of 3 to 5 well volumes. After development, the
temporary monitoring wells were purged using low-flow/low-stress purging techniques using a
peristaltic pump and dedicated polyethylene tubing. The intake point of the pump tubing was
placed in the approximate mid -portion of the screened interval of the well, and groundwater was
removed at a rate no greater than 200 milliliters per minute. H&H utilized a calibrated water quality
meter to collect measurements of pH, temperature, dissolved oxygen, oxidation-reduction potential,
turbidity, and specific conductivity during the purging process. Purging was considered complete
when the parameters had stabilized (pH ± 0.1 SU, conductivity varied no more than 5%, and
turbidity was less than 10 Nephelometric Turbidity Units or NTUs, where practical). Groundwater
sampling forms completed by H&H sampling personnel are provided in Appendix D.
The groundwater samples for VOC analysis were collected directly into laboratory supplied sample
containers using the "soda straw" method to minimize volatile loss through the peristaltic pump
head. The sample containers were labeled with the sample identification, date, and requested
analysis, and placed in an iced laboratory supplied cooler. The samples were delivered to Con -Test
under standard chain of custody protocols for analysis of VOCs by EPA Method 8260B, SVOCs by
EPA Method 8270D, and RCRA metals by EPA Method 602013/7470A.
For quality assurance/quality control purposes, a duplicate groundwater sample was collected
from the TMW-2 and submitted to Con -Test for analysis of VOCs by EPA Method 8260B, SVOCs
by EPA Method 8270D, and RCRA metals by EPA Method 602013/7470A. In addition, a trip
blank sample was analyzed for VOCs by EPA Method 8260B.
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Upon completion of soil and groundwater sampling activities, the soil borings and temporary
monitoring wells were properly abandoned with hydrated bentonite, and the ground surface was
restored to match pre -drilling conditions. After sampling the temporary monitoring wells, the SIP
was closed out by submitting well abandonment records to LUESA.
4.2 Groundwater Analytical Results
A tabular summary of groundwater analytical results is presented in Table 3. The laboratory
analytical report and chain of custody record are provided in Appendix B. Groundwater data were
compared to the 2L Standards and the DEQ DWM Residential and Non -Residential Groundwater
Vapor Intrusion Screening Levels (GWSLs) dated February 2018.
TCE (2,900 µg/L) was detected in sample TMW-1 at a concentration above the 2L Standard of 3.0
µg/L and the Residential and Non -Residential GWSLs of 1.0 µg/L and 4.4 µg/L, respectively. TCE
was also detected in sample TMW-2 at a concentration of 3.7 µg/L, which exceeds the 2L Standard
and Residential GWSL. PCE was detected in sample TMW-2 at a concentration of 1.0 µg/L, which
is above the 2L Standard of 0.7 µg/L but is below the Residential and Non -Residential GWSLs of
12 µg/L and 48 µg/L, respectively. Additional VOCs, including tert-butyl alcohol, chloroform, cis-
1,2-dichloroethene, tetrahydrofuran, and/or toluene, were detected in samples TMW-1, TMW-2,
and TMW-3; however, the detected concentrations are below the 2L Standards.
No SVOCs were detected above the MDLs in samples TMW-1 through TMW-3.
Several metals, including barium, chromium, and mercury, were detected in samples TMW-1
through TMW-3. None of the metals detected in groundwater were present at concentrations
above the respective 2L Standards.
Analytical data for the duplicate groundwater sample (DUP-GW-1) are generally consistent with the
data for the parent sample (TMW-2). No VOCs were detected above the MDLs in the trip blank.
These data indicate good quality control.
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5.0 Vapor Intrusion Assessment Activities
On November 29 and December 5, 2018, H&H collected three co -located sub -slab vapor samples
(SSV-1 through SSV-3) and indoor air samples (IAQ-1 through IAQ-3) within the Site building. hi
addition, one exterior background sample (BKG-IAQ-1) of ambient air was collected northeast of
the Site building, which was upwind of the Site during the indoor air sampling event. Sub -slab
vapor and indoor air sample locations are shown on Figure 2 and described below.
• Sample SSV-1 and IAQ-1 were collected in the southern portion of the warehouse.
• Sample SSV-2 and IAQ-2 were collected in the central portion of the warehouse.
• Sample SSV-3 and IAQ-3 were collected in the northern portion of the warehouse.
5.1 Sub -Slab Vapor Sampling Methodology
H&H installed Cox -Colvin Vapor Pins® (vapor pins) at each sub -slab soil vapor sample location.
For installation of the vapor pins, a hammer drill with a 5/8-inch diameter bit was utilized to
penetrate the concrete slab with a drilled pilot hole. The vapor pin assembly (sampling point and
silicone sleeve) was then placed into the pilot hole and secured using an installation/extraction tool
and a "dead blow" hammer to form an air -tight seal. Once the vapor pin assembly was secured in
the pilot hole, 1/4-inch diameter Teflon® sample tubing was attached to the vapor pin assembly
barbed sample port.
After installation, a leak check was conducted at each sub -slab vapor sample location by
constructing a shroud around the sampling point and flooding the air within the shroud with helium
gas. Helium concentrations inside the shroud were measured using a helium gas detector. Using a
syringe and three-way valve, the Teflon tubing and surrounding sand pack was purged of
approximately three sample volumes. Following purging, a sample was collected from the sample
tubing outside the shroud and analyzed using the helium gas detector to ensure that helium
concentrations were less than 10% of the helium concentrations in the shroud.
Following a successful leak check, a laboratory -supplied 6-liter stainless steel Summa sample
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canister was connected to in -line flow controller with a vacuum gauge and was subsequently
connected to the sample tubing at each sampling point using a brass nut and ferrule assembly to
form an air -tight seal. The flow regulator was pre-set by the laboratory to regulate the vapor intake
rate to approximately 6-liters per hour. Once the sample train was assembled, the intake valve on
the canister was fully opened to begin collection of the sub -slab vapor sample. Vacuum readings on
the Summa canister were recorded prior to and following the one -hour sampling period to ensure
adequate sample volume was collected. Per laboratory standard operating procedures, a vacuum
was maintained within the canisters at the conclusion of the sampling event.
After sample collection, the Summa canister's valves were closed prior to the regulator being
disconnected from the canister and the Summa canisters were then placed in laboratory supplied
shipping containers, properly labeled, and shipped under standard chain -of -custody protocols to
Con -Test for analysis of VOCs by EPA Method TO-15. For quality control purposes, one duplicate
sub -slab vapor sample was collected from SSV-1 and analyzed for VOCs by EPA Method TO-15.
Upon completion of sampling activities, each sub -slab vapor boring was abandoned, and the
surfaces were repaired to match pre -drilling conditions.
5.2 Sub -Slab Vapor Analytical Results
Results of sub -slab soil vapor analyses are summarized in Table 4. The laboratory analytical report
and chain of custody record are provided in Appendix B. Sub -slab vapor analytical results were
compared to the February 2018 DEQ DWM Residential and Non -Residential SGSLs.
Laboratory analytical results indicate the presence of several VOCs, including chlorinated and
petroleum -related compounds, in sub -slab vapor samples SSV-1 through SSV-3. TCE (2,600
µg/m3) was detected in sample SSV-2 (central portion of building) above the Non -Residential
SGSL of 180 µg/m3. No other compounds were detected sub -slab vapor samples at concentrations
exceeding the Residential or Non -Residential SGSLs.
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Analytical data for the duplicate sub -slab vapor sample (DUP-SSV-1) are generally consistent
with the data for the parent sample (SSV-1). These data indicate good quality control.
5.3 Indoor Air Sampling Methodology
Indoor air samples were collected with the windows of the buildings closed and ingress and egress
activities minimized. The samples were collected while the HVAC system was running normally.
The background and indoor air samples were collected using 6-liter stainless steel Summa sample
canisters connected to in -line flow controllers with a vacuum gauge. The flow controllers were set
so that the samples were collected over an approximately 8-hour period. A 3-foot long sampling
cane was connected to the flow controller so that the sample intake point was positioned
approximately 5 ft above grade (typical breathing zone height) when the sample canister is set on its
base.
During the sampling activities, indoor/outdoor air pressure differential was measured near the start,
middle, and end of the 8-hour sampling period using a manometer sensitive to 0.001 inches of
water. In addition, exterior wind speed, exterior wind direction, indoor/outdoor temperature, and
precipitation were recorded near the start, middle, and end of the sampling period. For quality
assurance purposes, H&H personnel monitored the sample canisters to prevent tampering or
damages for the duration of the sampling event. Per laboratory standard operating procedures, a
vacuum was maintained within the canisters at the conclusion of the sampling event.
Prior to and after the indoor and background air samples were collected, vacuum in each of the
canisters was measured using a laboratory -supplied vacuum gauge. These measurements were
recorded on the sample chain -of -custody. The sample canisters were labeled and shipped under
standard chain -of -custody procedures to Con -Test for analysis of VOCs by EPA Method TO-15.
Indoor air sample analysis was placed on hold by the laboratory pending the results of analysis of
the sub -slab vapor samples.
For quality control purposes, one duplicate indoor air sample (DUP-IAQ-1) was collected from the
IAQ-3 sample location and submitted for analysis of VOCs by EPA Method TO-15.
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5.4 Indoor Air Analytical Results
Results of indoor air and background air analyses are summarized in Table 4. The laboratory
analytical report and chain of custody record are provided in Appendix B. Indoor air sample
analytical results were compared to the February 2018 DEQ DWM Indoor Air Screening Levels
(IASLs).
Based on the results of the sub -slab vapor analysis, DEQ Brownfields requested that indoor air
samples IAQ-I and IAQ-2 and background air sample BKG-IAQ-I be analyzed for all VOCs that
were detected above the MDLs in sub -slab vapor samples SSV-1 and SSV-2. Laboratory analytical
results indicate that several VOCs were detected above the MDLs in indoor air samples IAQ-1 and
IAQ-2. Benzene was detected in samples IAQ-1 (13 µg/m3) and IAQ-2 (10 µg/m3) at
concentrations above the Residential IASL of 3.6 µg/m3 but below the Non -Residential IASL of 16
µg/m3. Note that the concentrations of benzene detected in indoor air samples are greater than the
benzene concentrations detected in sub -slab samples. Further, benzene was also detected in the
background air sample BKG-IAQ-I at a concentration of 1.3 µg/m3, and small containers of
gasoline and other potential benzene -containing petroleum products were observed in the
warehouse during the indoor air sampling event. As such, it appears that the benzene detections in
indoor air samples are not representative of vapor intrusion related to subsurface contamination at
the Site.
As noted above, a duplicate indoor air sample was collected concurrently with the parent sample
IAQ-3. Based on the absence of VOC concentrations above SGSLs in sample SSV-3, indoor air
sample IAQ-3 and its duplicate sample were not analyzed by the laboratory.
DEQ Risk Calculator
As noted above, benzene was detected in indoor air samples IAQ-1 and IAQ-2 at concentrations
above the Unrestricted Use PSRGs. However, the DEQ IASLs are conservative and based upon
lifetime incremental cancer risk (LICR) for potential carcinogenic risks of I x 10-5 and a non -
carcinogenic hazard index (HI) of 0.2 for potential non -carcinogenic risks. The DEQ acceptable
LICR is typically 1 x 10-4, and the acceptable cumulative risk level for non -carcinogenic risks is
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SMARTER ENVIRONMENTAL SOLUTIONS

an HI equal to or less than 1. Therefore, H&H used DEQ's risk calculator (February 2018) to
calculate potential cumulative risks at the Site using the highest VOC concentrations detected in
the indoor air samples. H&H utilized the DEQ risk calculator assuming residential and non-
residential worker hypothetical land use scenarios. The results of risk calculations are
summarized below and are included in Appendix C.
Land Use Scenario
Calculated
Calculated
Calculated LICR or
Cumulative LICR
Cumulative HI
HI Exceeds
Acceptable Risk
Levels?
Residential
3.6 x 10-5
0.47
No
Non -Residential Worker
8.3 x 10-6
0.11
No
As shown in the above table, the results of the risk calculations using indoor air data indicate that
the calculated cumulative risks are below acceptable risk levels for the residential and non-
residential worker exposure scenarios.
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6.0 Receptor Survey Activities
On December 12, 2018, H&H performed receptor survey activities at the Site and in the nearby
area. The receptor survey included a pedestrian and vehicular survey to obtain information about
land use, water supply, basements, underground utilities, drains, and surface water bodies located
within a 1,500-foot (ft) radius of the Site in accordance with the DEQ-approved Work Plan. H&H
also utilized the online Mecklenburg County Groundwater & Wastewater Services (GWS) Well
Information System to check for potable water supply wells located within a 1,500-ft radius of the
Site. In addition, H&H identified land use, zoning, underground utilities using other Mecklenburg
County online resources. The Brownfields Property Receptor Survey Form is included as Appendix
E, and a Receptor Survey Map is provided as Figure 4. The results of the receptor survey are
summarized below.
Zoning
The subject Site, an adjacent property to the west-northwest of the Site, and an adjacent property to
the southwest of the Site beyond W. Morehead Street are zoned "business" (B-1). An adjacent
property located east of the Site beyond Calvert Street is zoned "urban residential -commercial"
(UR-C). An adjacent property located south of the Site across W. Morehead Street is zoned "mixed
use development district" (MUDD).
Municipal Water Availability
Municipal water supplied by Charlotte Water is available to the Site and surrounding area. H&H
did not identify sources of public drinking water within 1,500-ft of the Site based on the DEQ
Source Water Assessment Program's geographic information system map. The City of Charlotte
and Mecklenburg County obtain their water from Lake Norman and Mountain Island Lake.
Mountain Island Lake is the closest drinking water source and is located approximately 8.8 miles
northwest of the Site. Additionally, H&H observed municipal water meters for the Site and
surrounding properties.
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Water SpNly Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500-ft radius of the Site
to identify potential water supply wells. No public or private water supply wells were identified
during pedestrian and vehicular survey activities. H&H also utilized the online Mecklenburg
County GWS Well Information System to identify potential potable water supply wells located
within a 1,500-ft radius of the Site. The nearest active water supply well is a private well located
approximately 4.0 miles to the west-northwest of the Site, and a permanently abandoned drinking
water well is located approximately 1.0 mile to the northwest of the Site.
Surface Water Bodies
No surface water bodies were identified on the Site or adjacent properties. Irwin Creek is located
approximately 500 ft southeast of the Site. Based on the DEQ classification system, Irwin Creek is
a Class C surface water body. A Class C surface water body is defined as "waters protected for uses
such as secondary recreation, fishing, wildlife, fish consumption, aquatic life including propagation,
survival and maintenance of biological integrity, and agriculture. Secondary recreation includes
wading, boating, and other uses involving human body contact with water where such activities take
place in an infrequent, unorganized, or incidental manner." Irwin Creek flows southwest and
discharges into Sugar Creek, which is located approximately 3.9 miles southwest of the Site.
Subsurface Structures
H&H conducted a visual reconnaissance in the Site area to identify potential subsurface structures
within 1,000 ft of the subject Site. H&H observed evidence of subsurface utilities, including
sanitary sewer, storm sewer, municipal water, natural gas, communication, and electrical on and
adjacent to the subject Site. The Site's sewer lines connect to the municipal sanitary sewer system
that runs along W. Morehead Street. H&H observed basements at 626 and 700 Walnut Avenue;
513 S. Summit Avenue; and 617, 621, 625, 629, 633, 701, 707, 711, 715, and 719 Grandin Road.
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7.0 Conclusions and Recommendations
H&H has completed Brownfields assessment activities on the 1300 West Morehead Street
Brownfields Property (Brownfields Project No. 22039-18-060) located in Charlotte, Mecklenburg
County, North Carolina. The assessment activities were conducted in accordance with the DEQ-
approved Work Plan and included a receptor survey and soil, groundwater, sub -slab vapor, and
indoor air sampling to evaluate potential environmental risks associated with redevelopment of
the Site. A summary of the assessment results is provided below.
Receptor SurveX
H&H conducted a Brownfields receptor survey for the Site and nearby area. The results of the
receptor survey indicate that municipal water is available to the Site and area within a 1,500-ft
radius of the Site. No sources of public drinking water are within 1,500 ft of the Site. H&H did
not identify water supply wells within the 1,500 ft radius of the Site. No surface water bodies
were identified on the Site or on adjacent properties. H&H observed evidence of subsurface
utilities, including sanitary sewer, storm sewer, municipal water, natural gas, and/or electrical on
the Site and nearby adjacent properties. H&H also observed several structures with crawlspaces
and/or basements within a 1,500-ft radius of the Site.
Soil
H&H collected three soil samples for laboratory analysis from five soil borings to evaluate the
potential for soil impacts adjacent to floor drains (samples SB-3 and SB-5) and a sump (sample
SB-2). In addition, one background soil sample was collected in the southern portion of the Site
to evaluate naturally occurring metals concentrations.
Laboratory analytical results did not indicate the presence of VOCs or SVOCs in soil samples at
concentrations above the Unrestricted Use or Industrial/Commercial PSRGs.
Arsenic (1.6 mg/kg) was detected in sample SB-3 (1-3 ft) at a concentration above the
Unrestricted Use PSRG of 0.68 mg/kg. However, the detected concentration is below the Site -
specific background concentration of 1.9 mg/kg and the average published background
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concentration of 4.8 mg/kg for North Carolina soils. Total chromium was detected in samples
SB-2 (4-6 ft), SB-3 (1-3 ft), and SB-5 (1-3 ft) at concentrations ranging from 9.5 mg/kg to 66
mg/kg, which are below the Site -specific background concentration of 96 mg/kg and generally
consistent with the average published background concentration of 65 mg/kg for North Carolina
soils. In accordance with DEQ's request, the background sample was analyzed for hexavalent
chromium. Hexavalent chromium was detected at a concentration of 2.3 mg/kg in the
background sample, which is above the Unrestricted Use PSRG of 0.31 mg/kg. The metals
concentrations (including hexavalent chromium) are likely naturally occurring.
The results of the risk calculations using combined Site soil data indicate that the calculated
cumulative risks are below acceptable risk levels for the residential, non-residential worker, and
construction worker exposure scenarios.
Groundwater
H&H installed and sampled three temporary groundwater monitoring wells (TMW-1 through
TMW-3) at the Site. TCE (2,900 µg/L) was detected in sample TMW-1 at a concentration above
the 2L Standard of 3.0 µg/L and the Residential and Non -Residential GWSLs of 1.0 µg/L and
4.4 µg/L, respectively. Sample TMW-1 was collected in the southern portion of the Site and
downgradient of an off -Site TCE release. TCE was also detected in sample TMW-2 at a
concentration of 3.7 µg/L, which exceeds the 2L Standard and Residential GWSL. PCE was
detected in sample TMW-2 at a concentration of 1.0 µg/L, which is above the 2L Standard of 0.7
µg/L but is below the Residential and Non -Residential GWSLs of 12 µg/L and 48 µg/L,
respectively. No VOCs, SVOCs, or metals were detected in sample TMW-3 (upgradient portion
of the Site) at concentrations above the 2L Standards.
Sub -Slab Vapor
H&H collected three sub -slab vapor samples (SSV-1 through SSV-3) from the warehouse portion
of the Site building to evaluate vapor intrusion at the Site. Laboratory analytical results indicate the
presence of several VOCs, including chlorinated and petroleum -related compounds, in sub -slab
vapor samples SSV-1 through SSV-3. TCE (2,600 µg/m3) was detected in sample SSV-2 (central
portion of the Site building) above the Non -Residential SGSL of 180 µg/m3. No other compounds
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were detected sub -slab vapor samples at concentrations exceeding the Residential or Non -
Residential SGSLs.
Indoor Air
H&H collected three indoor air samples (IAQ-1 through IAQ-3) to evaluate the potential for sub -
slab vapor intrusion into the Site building. Based on the results of sub -slab vapor analysis, only
samples IAQ-1 and IAQ-2 were submitted for laboratory analysis. Benzene was detected in
indoor air samples IAQ-1 (13 µg/m3) and IAQ-2 (10 µg/m3) at concentrations above the
Residential IASL of 3.6 µg/m3 but below the Non -Residential IASL of 16 µg/m3. Note that the
concentrations of benzene detected in indoor air samples are greater than the benzene
concentrations detected in sub -slab samples. Further, benzene was also detected in the
background air sample at a concentration of 1.3 µg/m3, and small containers of gasoline and
other potential benzene -containing petroleum products were observed in the warehouse during
the indoor air sampling event. As such, it appears that the benzene detections in indoor air
samples are not representative of vapor intrusion related to subsurface contamination at the Site.
The results of the risk calculations using indoor air data (including benzene) indicate that the
calculated cumulative risks are below acceptable risk levels for the residential and non-residential
worker exposure scenarios.
Recommendations
Based on the results of the Brownfields Assessment and the proposed re -use of the existing Site
building, no additional soil, groundwater, or vapor intrusion assessment is recommended. In
addition, vapor intrusion mitigation is not warranted for the Site building based on sub -slab vapor
and indoor air sampling results.
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Table 1
Summary of Soil Analytical Results
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
H&H Job No. COP-008
Sample ID
SB-2
SB-3
SB-5/DUP-SOIL-1
BKG-SB-1
Unrestricted
(1�
Industrial/
Commercial
Regional Background
Metals in Soil (z)
Date
12/4/2018
12/4/2018
12/4/2018 12/4/2018
12/4/2018
Adjacent to
Southern Portion
Sample Location
Adjacent to Floor Drains
Use PSRGs
(1)
Sump
of Site
PSRGs
Depth ft b s
4-6
1-3
1-3
1-3
1-3
Range
Mean
VOCs (8260B)
Acetone
0.043 J
0.038 J
0.048 J
0.036 J
NA
12,000
140,000
--
--
SVOCs (8270D)
Bis(2- Ethyl hexyl)phthalate
<0.16
0.38 J
<0.15
<0.15
NA
39
160
--
--
RCRA Metals (6020B/7471 B/7199)
Arsenic
0.63
1.6
0.30
0.35
1.9
0.68
3.0
1.0 - 18
4.8
Barium
22
150
14
14
68
3,100
47,000
50 - 1,000
356
Cadmium
<0.013
0.053 J
<0.012
<0.014
14
200
1.0 - 10
4.3
Chromium (total)
22
66
10
9.5
96
--
--
7.0 - 300
65
Hexavalent Chromium
NA
NA
NA
2.3
0.31
6.5
NS
NS
Trivalent Chromium
--
--
--
--
93.7
23,000
350,000
NS
NS
Lead
5.3
30
2.6
2.4
12
400
800
ND - 50
16
Mercury
0.0038 J
0.024 J
0.0070 J
0.0076 J
0.16
2.3
9.7
0.03 - 0.52
0.121
Selenium
<0.081
0.16 J
<0.075
0.080 J
0.29 J
78
1,200
<0.1 - 0.8
0.42
Silver
0.022 J
0.053 J
0.018 J
0.018 J
0.073 J
78
1,200
ND - 5.0
NS
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (February 2018).
2) Range and mean values of background metals for North Carolina soils obtained from Elements in North American Soils by Dragun and Chekiri, 2005. Background levels for Southeastern
or Conterminous USA are shown for arsenic, cadmium, and silver.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
For VOCs and SVOCs, only compounds detected are shown.
Compound concentrations are reported to the laboratory method detection limits.
Bold values exceed unrestricted use PSRGs for VOCs and SVOCs and (and above background concentrations for metals)
RCRA = Resource Conservation and Recovery Act; VOCs = volatile organic compounds
SVOCs = semi -volatile organic compounds; ft bgs= feet below ground surface
NA = not analyzed; NS = not specified; -- = not applicable; ND = not detected
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
Table
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Table 2
Summary of Temporary Well Construction and Groundwater Elevation Data
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
H&H Job No. COP-008
Ground
Static Depth to
Groundwater
Well
TOC
Well Depth
Screen Interval
Well ID
Surface
Groundwater
Elevation
Diameter (in)
Elevation (ft)
(ft bgs)
(ft bgs)
Elevation (ft)
(ft below TOC)
(ft)
TMW-1
1
95.85
95.46
20.18
10.18-20.18
13.61
82.24
TMW-2
1
95.06
95.20
19.70
9.70-19.70
12.58
82.48
TMW-3
1
96.86
95.81
18.56
8.56-18.56
13.07
83.79
Notes:
TOC = top of casing; bgs = below ground surface
Depth to groundwater measurements collected on December 5, 2018.
Elevations are approximate and are referenced to an arbitrary datum of 100.00 ft.
Table
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Table 3
Summary of Groundwater Analytical Results
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
H&H Job No. COP-008
Sample ID
TMW-1
TMW-2/DUP-GW-1
TMW-3
NC 2L
DWM Residential
DWM
Date
12/5/2018
12/5/2018
12/5/2018
Groundwater
Groundwater
Non -Residential
Southern Portion of
(11
Groundwater
Adjacent to the Sump and Downgradient
Northern/Upgradient
Standards
VISL(z)
(2)
Sample Location
Site/Downgradient
Portion of the Warehouse
Portion of Site
VISL
of Off -Site Impacts
VOCs (8260B)
tert-Butyl Alcohol (TBA)
<110
9.5 J
<2.2
<2.2
10
NS
NS
Chloroform
<11
0.76 J
0.66 J
<0.22
70
8.1
36
cis-1,2-Dichloroethene
22 J
<0.15
<0.15
<0.15
70
NS
NS
Tetrachloroethene
<14
1.0
0.79 J
<0.27
0.7
12
48
Tetrahydrofuran
<54
<1.1
<1.1
2.0 J
NS
140,000
610,000
Toluene
<8.5
<0.17
<0.17
0.19 J
600
3,800
16,000
Trichloroethene
2,900
3.7
3.5
0.88 J
3.0
1.0
4.4
SVOCs (8270D)
All SVOCs Below Laboratory Detection Limits
--
--
--
RCRA Metals (6020B, 7470A)
Arsenic
<0.72
<0.72
<0.72
<0.72
10
--
--
Barium
35
32
32
39
700
--
Cadmium
<0.14
<0.14
<0.14
<0.14
2.0
--
--
Chromium (total)
1.5 J
2.8
2.7
1.1 J
10
--
--
Lead
<0.48
<0.48
<0.48
<0.48
15
--
--
Mercury
0.076 J
0.068 J
0.069 J
0.059 J
1.0
0.18
0.75
Selenium
<2.8
<2.8
<2.8
<2.8
20
--
--
Silver
<0.15
<0.15
<0.15
<0.15
20
--
--
Notes:
1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (NC 2L Standards) (April 2013).
2) NC DEQ Division of Waste Management (DWM) Groundwater Vapor Intrusion Groundwater Screening Levels (VISLs) (February 2018)
With the exception of metals, only constituents detected in at least one sample are shown.
Concentrations are reported in micrograms per liter (pg/L).
Compound concentrations are reported to the laboratory method detection limits.
Laboratory analytical methods are shown in parentheses.
Bold values exceed NC 2L Standard (April 2013).
Underlined values exceed the DWM Residential GWSL (February 2018).
Highlighted values exceed Non -Residential GWSL (February 2018).
VOCs = volatile organic compounds; SVOCs = semi -volatile organic compounds, RCRA = Resource Conservation and Recovery Act
NA = not analyzed; NS = not specified; -- = not applicable
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
Table
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Table 4
Summary of Sub -Slab Vapor Analytical Results
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
H&H Job No. COP-008
N
r
r
T
N
O
I..L
CO
C
ICU
C
_0O
Y
LU
N
O
E
�i
N
E
O
O
4)
N
O
N
N
N
C
E
O
N
i
C)
J
O
U
OL
O
O
:EO
00
N
O
3
O
O
Q
E
Q
E
Q
E
iv
N
c
N
_
O
O
O
U
L
U
U
N
N
M
ca
C
U
N
m
L
N
N
O
C
C
(n
(n
U)
<
<
CO
C\l
U
-
0
W
F__
H
F
H
H
SSV-1
9.4 J
<0.26
<0.92
<0.36
1.3
2.7
10 J
4.7
<0.39
<0.39
14
1.2 J
Southern Portion of
Warehouse
12/5/2018
DUP-SSV-1
10 J
<0.26
<0.92
<0.36
1.4
2.6
9.4 J
5.0
<0.39
<0.39
14
1.3 J
TO-15
Central Portion of
SSV-2
12/5/2018
22
2.8
2.8 J
3.1
2.0
2.6
21
170
1.7
3.5
2,600
1.5 J
Warehouse
Northern Portion of
SSV-3
12/5/2018
11 J
<0.26
1.8 J
<0.36
6.1
2.7
89
1.8
<0.39
1.2
<0.43
1.4 J
Warehouse
DWM Residential SGSL (1)
220,000
120
35,000
41
NS
700
NS
280
14,000
35,000
14
NS
DWM Non -Residential SGSL (2)
2,700,000
1,600
440,000
530
NS
8,800
NS
3,500
180,000
440,000
180
NS
Notes:
1) North Carolina Department of Environment Quality (DEQ) Division of Waste Management (DWM) Residential Sub -slab and Exterior Soil Gas Screening Levels (SGSLs) (February 2018)
2) North Carlolina DEQ DWM Non -Residential SGSLs (February 2018)
Bold value exceeds the NCDEQ DWM Residential and Non -Residential SGSLs.
Compound concentrations are reported to the laboratory detection limits.
Compound concentrations are reported in micrograms per cubic meter (lag/m3).
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
NS = Not Specified
Table 4
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Table 5
Summary of Indoor Air Analytical Results
1300 West Morehead Street
Brownfields Property
Charlotte, North Carolina
H&H Job No. COP-008
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c
t
a)
O
E
a)
Q
M
L
N
L
O
N
E
L
o
0
0
O
m
ai
0
_Z3
H
0
Q
a)
Q
0-O
0
2
o
o
O
o
0
�,
o
0
E
E
E
c0
a)
C
t
co
c i
c i
in
(n
Cn
Q
Q
00
C\jm
/O\
U
0 —
Lu
H
H
H
Southern Portion of
IAQ-1
11/29/2018
33
13
5.6
<0.073
<0.12
2.6
110
0.63
2.6
47
<0.087
1.9
Warehouse
Central Portion of
IAQ-2
11/29/2018
TO-15
28
10
4.6
<0.064
<0.11
2.8
75
0.43
3.4
37
<0.076
2.0
Warehouse
BKG-IAQ-1
Upwind, Northeast of
11/29/2018
13
1.3
2.4 J
<0.064
<0.11
3.8
15
0.37
<0.069
3.1
<0.076
2.2
Warehouse
DWM Residential IASL (1)
6,500
3.6
1,000
1.2
NS
21
NS
8.3
420
1,000
0.42
NS
DWM Non -Residential IASL (2)
27,000
16
4,400
5.3
NS
88
NS
170
1,800
4,400
1.8
NS
Notes:
1) North Carolina Department of Environment Quality (DEQ) Division of Waste Management (DWM) Residential Indoor Air Screening Limits (IASLs) (February 2018) using Total Cumulative Risk of 1x10'
2) North Carlolina DEQ DWM Non -Residential IASLs (February 2018)
Underlined value exceeds the NCDEQ DWM Residential IASLs.
Compound concentrations are reported to the laboratory detection limits.
Compound concentrations are reported in micrograms per cubic meter (pg/m3).
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
NS = Not Specified
Table 5
s:\AAA-Master Projects\Colliers Properties, Inc. - COP\COP-008 1300 W. Morehead\Brownfields Assessment\Final Figures and Appendices\Data Tables (1-17-19)
1/21/2019 Hart & Hickman, PC

APPROXIMATE
N 0 2000 4000
SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 1991
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)

11
.N, -
O /
40
b� 00 oO�
_ o
Y - �
LEGEND
SITE PROPERTY BOUNDARY
STREAM
1,500 FT BUFFER
SW SUB -GRADE STORM SEWER
OVERHEAD ELECTRICAL
B BASEMENT
a O�O NOTES:
JAG
l�
;t QO 1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS 2018.
O Q . 2. ADDITIONAL UTILITIES, INCLUDING WATER, SANITARY
SEWER, AND COMMUNICATIONS, WERE OBSERVED
ON -SITE. HOWEVER, THE LOCATIONS OF THESE
l� UTILITIES COULD NOT BE CONFIRMED AND / OR CANNOT
BE ACCURATELY DEPICTED DUE TO MAP SCALE.
I� C7
O
APPROXIMATE
0 50 100
EmEmEmmommil
SCALE IN FEET
TITLI
RECEPTOR SURVEY MAP
." PROJECT 1300 WEST MOREHEAD STREET
BROWNFIELDS PROPERTY
CHARLOTTE, NORTH CAROLINA
te 100
hart ` hickman 11a,2923 SouthTryonarolina2823
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(�
SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
DATE: 1-21-19 REVISION NO. 0
JOB NO. COP 008 FIGURE NO. 4

Appendix A
Boring Logs
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

■
Client: 1300 West Morehead LLC
BORING LOG
hart hickman
►
Project: COP-008
Boring No. SB-1
1300 West Morehead Street
5MRRTER E WRONMEWAL 501 lJT 1ON 5
Address:
Charlotte, NC
Page: 1 of 1
Drilling Start Date: 12/4/18
Boring Depth (ft): 10.0
Drilling End Date: 1214118
Boring Diameter (in):
Drilling Company: CSI
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment:
DTW After Drilling (ft):
Driller: Danny Summers
Ground Surface Elev. (ft):
Logged By: Matt Vawter
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
L
....
�
O1>
Jp
z F
E2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
W
W
O2
N
W
O
2
J
Q
°� O
O
E
H
U
3
a�
'o
n
p
m
9
W
0
O
N
d
J
�
m
�
0 0
(0') Concrete
(0.5') Lean CLAY (CL); some silt, medium plasticity, very stiff, dry, reddish -brown & tan
4.3
2.7
3.6
(4.5') As Above: black mottling
5
4.6
5
(6) Silty SAND (SM); medium dense, dry, reddish -brown & tan
(7') Sandy SILT (ML); some clay, medium stiff, dry, brown
6.6
(9') Silty SAND (SM); medium dense, dry, brown & white & gray, saprolite
10
10
(10') Boring terminated
15 15
NOTES: Hole precleared to 5.0' on 12/4/18 by CSI using hand auger.
generated using GroundLogs.online

■
Client: 1300 West Morehead LLC
BORING LOG
hart hickman
►
Project: COP-008
Boring No. SB-3
1300 West Morehead Street
5MRRTER FWRONWNTAL501l1T1ON5
Address:
Charlotte, NC
Page: 1 of 1
Drilling Start Date: 12/04/2018
Boring Depth (ft): 10.0
Drilling End Date: 12/04/2018
Boring Diameter (in):
Drilling Company: CSI
Sampling Method(s): Grab
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment:
DTW After Drilling (ft):
Driller: Danny Summers
Ground Surface Elev. (ft):
Logged By: Matt Vawter
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
O
....
�
O1>
Jp
z F
E2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
W
W
O2
N
W
O
2
J
Q
°� O
E
H
U
3
a�
'o
n
p
m
9
W
0
O
d
J
�
m
�
0 0
(0') Concrete
(0.5') Lean CLAY (CL); some fine sand, some silt, medium plasticity, medium stiff, dry,
3.2
12:00
reddish -brown & tan
23.6
SB-3
(1') Silty SAND (SM); loose, dry, dark brown
(1'4)
(2') Lean CLAY (CL); some silt, medium plasticity, stiff, dry, light brown & tan
4.5
(4.5') SILT (ML); some clay, medium stiff, dry, light brown
5
5.1
5
(55) Sandy SILT (ML); soft, saturated, brown, perched water
4.2
(8') Silty GRAVEL (GM); loose, saturated, brown, perched water
(9') Lean CLAY (CL); some silt, medium plasticity, stiff, moist, brown
10
10
(10') Baring terminated
15 15
NOTES: Hole precleared to 5.0' on 12/04/2018 by CSI using hand auger.
generated using GroundLogs.online

■
Client: 1300 West Morehead LLC
BORING LOG
hart hickman
►
Project: COP-008
Boring No. SB-4
1300 West Morehead Street
5MRRTER FWRONWNTAL501l1T1ON5
Address:
Charlotte, NC
Page: 1 of 1
Drilling Start Date: 12/04/2018
Boring Depth (ft): 10.0
Drilling End Date: 12/04/2018
Boring Diameter (in):
Drilling Company: CSI
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment:
DTW After Drilling (ft):
Driller: Danny Summers
Ground Surface Elev. (ft):
Logged By: Matt Vawter
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
O
....
�
O1>
Jp
z F
E2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
W
W
O2
N
W
O
2
J
Q
°� O
E
H
U
3
a�
'o
n
p
m
9
W
0
O
d
J
�
m
�
0 0
(0') Concrete
(0.5') Lean CLAY (CL); some silt, medium plasticity, stiff, dry, reddish -brown & tan
2.3
4.5
0.7
(4') Silty SAND (SM); medium dense, dry, reddish -brown
5
1.9
5
(6) Sandy SILT (ML); some clay, stiff, dry, reddish -brown & black & tan
2.0
(9') As Above: moist
10
10
(10') Boring terminated
15 15
NOTES: Hole precleared to 5.0' on 12/04/2018 by CSI using hand auger.
generated using GroundLogs.online

■
Client: 1300 West Morehead LLC
BORING LOG
hart hickman
►
Project: COP-008
Boring No. SB-5
1300 West Morehead Street
5MRRTER FWRONWNTAL501l1T1ON5
Address:
Charlotte, NC
Page: 1 of 1
Drilling Start Date: 12/04/2018
Boring Depth (ft): 10.0
Drilling End Date: 12/04/2018
Boring Diameter (in):
Drilling Company: CSI
Sampling Method(s): Grab
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment:
DTW After Drilling (ft):
Driller: Danny Summers
Ground Surface Elev. (ft):
Logged By: Matt Vawter
Location (X,Y):
COLLECT
MEASURE
....
Y
J
W
Z
O
....
�
O1>
Jp
z F
E2
d
H
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
W
W
O2
N
W
O
2
J
Q
°� O
E
H
U
3
a�
'o
n
p
m
9
W
0
O
d
J
0 0
(0') Concrete
(0.5') Poorly graded SAND (SP); loose, moist, dark brawn
1.1
12:30
(1') Lean CLAY (CL); some fine -medium sand, some silt, medium plasticity, medium
2.7
SB-5
(1'-3')
stiff, dry, light brown & red
(2.5') Silty SAND (SM); loose, dry, reddish -brown & tan
4.3
(3.5') Lean CLAY (CL); some silt, medium plasticity, stiff, dry, reddish -brown & tan,
trace black mottling
(4.5') Silty SAND (SM); loose, dry, brown
5
4.3
5
(55) SILT (ML); trace fine -medium sand, some clay, medium stiff, dry, reddish -brown
(7') Silty SAND (SM); loose, dry, tan
3.8
(8.5') Sandy SILT (ML); trace clay, medium stiff, dry, light brown
10
10
(10') Baring terminated
15 15
NOTES: Hole precleared to 5.0' on 12/04/2018 by CSI using hand auger.
generated using GroundLogs.online

■
Client: 1300 West Morehead LLC
BORING LOG
hart hickman
►
Project: COP-008
Boring No. BKG-SOIL-1
West Morehead Street
S MARTER F WRONWNTA L SOLITnON 5
Address: Charlotte, NC
Cha
Page: 1 of 1
Drilling Start Date: 12/03/2018
Boring Depth (ft): 10.0
Drilling End Date: 12/03/2018
Boring Diameter (in):
Drilling Company: CSI
Sampling Method(s): Grab
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment:
DTW After Drilling (ft):
Driller: Danny Summers
Ground Surface Elev. (ft):
Logged By: Matt Vawter
Location (X,Y):
COLLECT
MEASURE
}
(3
Lu
W
Z
0
=
O
w
0
ZW
N
a
�
a
p
af
W
ER a
02
H
a
SOIL/ROCK VISUAL DESCRIPTION
n
W
❑
2
J
Q
00p
N
E
U
3
N
0
n
❑
m
�
W
❑
CJ
E
a)a
cn
m
a'
0 0
(0') Asphalt
(0.3') Concrete
11:50
(0.5') Sandy SILT (ML); trace clay, soft, dry, reddish -brown
3.8
BKG-
SOIL-
1
(2') Lean CLAY (CL); trace silt, medium plasticity, very stiff, dry, orange & red
5.1
5
14.6
5
(6.5') Silty SAND (SM); trace clay, medium dense, dry, reddish -brown
36.7
(9') SILT (ML); some clay, medium stiff, moist, brown
10
10
(10') Boring terminated
15 15
NOTES: Hole precleared to 5.0' on 12/03/2018 by CSI using hand auger. Elevated PID readings appear to have been attributed to humidity.
generated using GroundLogs.onllne

■
Client: 1300 West Morehead LLC
WELL LOG
hart hickman
►
Project: COP-008
Well No. TMW-1
West Morehead Street
S MARTER F WRONWNTA L SOLITnON 5
Address: Charlotte, NC
Cha
Page: 1 of 1
Drilling Start Date: 12/3/18
Boring Depth (ft): 25.0
Well Depth (ft): 20.18
Drilling End Date: 12/3/18
Boring Diameter (in):
Well Diameter (in): 1.0
Drilling Company: CSI
Sampling Method(s): Grab
Screen Slot (in):
Drilling Method: Direct Push
DTW During Drilling (ft):
Riser Material: Sch 40 PVC
Drilling Equipment:
DTW After Drilling (ft): 13.6
Screen Material: PVC Prepack
Driller: Danny Summers
Top of Casing Elev. (ft):
Seal Material(s):
Logged By: Matt Vawter
Location (X,Y):
Filter Pack: Sand Pack
COLLECT
MEASURE
_J
Lu
w
z
O
_
w
a
O
p
J
a
N
Q
o
N
SOIL/ROCK VISUAL DESCRIPTION
n
E
a
wo
w
g
��
E
CO)
w
Q
O
U
a
H
m
m
a
m
0 0
(0') Asphalt
2.6
(0.5') Silty GRAVEL (GM); gray, some concrete
(0.6') Lean CLAY (CL); some silt, medium plasticity, soft, dry, orange & red
(2') As Above: stiff
9.2
5
(6) Lean CLAY (CL); trace silt, medium plasticity, very stiff, dry, orange & red
35.7
5
(8.5') SILT (ML); trace clay, medium stiff, dry, reddish -brown
10
(9') Silty SAND (SM); loose, dry, brown
10
(9.5') Sandy SILT (ML); soft, dry, light brown
68.4
_
15
75.1
15
(18.5') Silty SAND (SM); loose, moist, dark brown &white
20
(195) wet encountered
85.0
20
(23') Silty SAND (SM); dense, moist, white & light brown & gray, saprolite
25
25
(26) Boring terminated
30 30
NOTES: Hole precleared to 5.0' on 12/3/18 by CSI using hand auger Elevated PID readings appear to have been attributed to humidity and
groundwater impacts.
generated using GroundLogs.onhne

is
hart hickman
Client: 1300 West Morehead LLC
WELL LOG
Project: COP-008
Well No. TMW-2/SB-2
1300 West Morehead Street
5MRRTFLR FNVIRONMEWASOtUTON5
Address:
Charlotte, NC
Page: 1 of 1
Drilling Start Date: 12/4/18
Boring Depth (ft): 20.0
Well Depth (ft): 19.7
Drilling End Date: 12/04/2018
Boring Diameter (in):
Well Diameter (in):
Drilling Company: CSI
Sampling Method(s):
Screen Slot (in):
Drilling Method: Direct Push
DTW During Drilling (ft):
Riser Material: Sch 40 PVC
Drilling Equipment:
DTW After Drilling (ft): 12.6
Screen Material: PVC Prepack
Driller: Danny Summers
Top of Casing Elev. (ft):
Seal Material(s):
Logged By: Matt Vawter
Location (X,Y):
Filter Pack: Sand Pack
COLLECT
MEASURE
}
J
w
W
z
w
EJp
0
E
JO
w a
4
a)
N
a
$
Z
SOIL/ROCK VISUAL DESCRIPTION
n
E
a
w
=
~
w
�2
m
E
U
a
n
m
w
J
Q
O
�-
0
0
0
V)
0 0
(0') Concrete
2.1
(05) Lean CLAY (CL); some silt, medium plasticity, stiff, dry, orangish-red
2.3
12:50
(4') Sandy SILT (ML); trace clay, soft, dry, light brown
3.8
GR
SB-2
(4 -6)
5
5
9.4
(65) Silty GRAVEL (GM); loose, dry, gray
(7') Sandy SILT (ML); trace clay, medium stiff, dry, light brown
3.6
10
4 7
10
(12') As Above: very moist, white & brown & gray
15
6.0
15
(17') Silty GRAVEL (GM); medium dense, moist, brown & white, saprolite
20
20
(20') Boring terminated
25
25
30 30
NOTES: Hole precleared to 5.0' on 12/4/18 by CSI using hand auger.
generated using GroundLogs.online

■
Client: 1300 West Morehead LLC
WELL LOG
hart hickman
►
Project: COP-008
Well No. TMW-3
1300 West Morehead Street
5MARTER FWRONWNTAL501l1T1ON5
Address:
Charlotte, NC
Page: 1 of 1
Drilling Start Date: 12/04/2018
Boring Depth (ft): 20.0
Well Depth (ft): 18.56
Drilling End Date: 12/04/2018
Boring Diameter (in):
Well Diameter (in): 1.0
Drilling Company: CSI
Sampling Method(s):
Screen Slot (in):
Drilling Method: Direct Push
DTW During Drilling (ft):
Riser Material: Sch 40 PVC
Drilling Equipment:
DTW After Drilling (ft): 13.1
Screen Material: PVC Prepack
Driller: Danny Summers
Top of Casing Elev. (ft):
Seal Material(s):
Logged By: Matt Vawter
Location (X,Y):
Filter Pack: Sand Pack
COLLECT
MEASURE
}
J
w
W
z
w
aJp
0
E
JO
w a
4
a)
N
a
$
Z
SOIL/ROCK VISUAL DESCRIPTION
n
E
a
w
=
~
w
��
m
E
U
a
0
n
m
w
J
Q
O
CJ
�-
0
0
@
m
d
m
0 0
(0') Concrete
1.3
(05) Lean CLAY (CL); some silt, medium plasticity, stiff, dry, reddish -brown
3.1
(3') As Above: hard
5
1.9
5
(8') Silty SAND (SM); loose, dry, light brown
(9') Sandy SILT (ML); trace clay, medium stiff, dry, light brown
10
34
10
(13') Silty SAND (SM); medium dense, moist, white & gray, saprolite
15
1 1
15
(18.5') No Recovery
20
20
(20') Boring terminated
25
25
30 30
NOTES: Hole precleared to 5.0' on 12/04/2018 by CSI using hand auger.
generated using GroundLogs. online

Appendix B
Laboratory Analytical Reports
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
January 7, 2019
Bo Cappleman
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Charlotte, NC
Client Job Number:
Project Number: COP-008
Laboratory Work Order Number: 18L0295
Enclosed are results of analyses for samples received by the laboratory on December 6, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 68

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
18L0295-01
18L0295-02
18L0295-03
18L0295-04
18L0295-05
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/MS
B218864
Semivolatile Organic Compounds by GUMS
B218913
Metals Analyses (Total)
B218953
B219056
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
7
7
13
19
25
28
34
35
35
35
40
40
45
45
46
47
48
54
Page 2 of 68

Table of Contents
40 ,con -testy
ANALYTICAL LABORATORY
39 Spruce StreetEast Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100 REPORT DATE: 1/7/2019
Charlotte, NC 28203 PURCHASE ORDER NUMBER:
ATTN: Bo Cappleman
PROJECT NUMBER: COP-008
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18LO295
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Charlotte, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
SB-2 (4'-6') 18L0295-01 Soil SM 254OG
SW-846 6020B
SW-846 7471B
SW-846 8260B
SW-846 8270D
SB-3 (1'-3') 18L0295-02 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260B
SW-846 8270D
SB-5 (1'-3') 18LO295-03 Soil SM 254OG
SW-846 6020B
SW-846 7471B
SW-846 8260B
SW-846 8270D
BKG-SOIL-1 18LO295-04 Soil NC DW37706, WW12/ FL
NELAPE87627
+Additional
SM 2540G
SW-846 6020B
SW-846 7471B
DUP-SOIL-1 18L0295-05 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8260B
SW-846 8270D
Page 3 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
REVISED REPORT - 1/7/2019 - Hexavalent chromium added to sample -04 per client's request.
For method 6020, all dilutions were performed as per standard operating procedure. Additional dilutions were performed due to high conentration.
Page 4 of 68

Table of Contents
40 ,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
SW-846 8260B
Qualifications:
L-04
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
Chloromethane
18L0295-01[SB-2 (4'-6')1, 18LO295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')1, 18LO295-05[DUP-SOIL-1], B218864-BLKI, B218864-BS1, B218864-BSD1
L-07A
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
outside of control limits. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
Acetone
B218864-BS1
R-05
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
Acetone
18L0295-01[SB-2 (4'-6')], 18LO295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')], 18LO295-05[DUP-SOIL-1], B218864-BLKI, 13218864-13SI, B218864-BSD1
5-17
Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less than the reporting limit and
bias is on the high side.
Analyte & Samples(s) Qualified:
1,2-Dichloroethane-d4
18L0295-01[SB-2 (4'-6')], 18L0295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')], 18L0295-05[DUP-SOIL-1]
SW-846 8270D
Qualifications:
R-05
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
Di-n-octylphthalate
18L0295-01[SB-2 (4'-6')], 18L0295-02[SB-3 (1'-3')], B218913-BLKI, 13218913-13SI, B218913-BSDI
V-04
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
Aniline
18L0295-01[SB-2 (4'-6')], 18LO295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')], 18LO295-05[DUP-SOIL-1], B218913-BLKI, 13218913-13SI, B218913-BSD1
Benzidine
18L0295-01[SB-2 (4'-6')], 18LO295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')], 18LO295-05[DUP-SOIL-1], B218913-BLKI, 13218913-13SI, B218913-BSD1
Page 5 of 68

,con-testo
ANALYTICAL LABORATORY
Table of Contents
V-05
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] ` TEL. [phone]
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
1,2-Diphenylhydrazine/Azobenzem
18L0295-02[SB-3 (1'-3')]
4-Nitrophenol
18L0295-02[SB-3 (1'-3')]
Benzidine
18L0295-01[SB-2 (4'-6')], 18L0295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')], 18L0295-05[DUP-SOIL-1], B218913-BLKI, B218913-BS1, B218913-BSDI
Benzo(g,h,i)perylene
18L0295-01[SB-2 (4'-6')], 18L0295-03[SB-5 (1'-3')], 18L0295-05[DUP-SOIL-1], B218913-BLKI, B218913-BSI, B218913-BSDI
Butylbenzylphthalate
18L0295-02[SB-3 (1'-3')]
Hexachlorocyclopentadiene
18L0295-01[SB-2 (4'-6')], 18L0295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')], 18L0295-05[DUP-SOIL-1], B218913-BLKI, B218913-BSI, B218913-BSDI
Nitrobenzene
18L0295-01[SB-2 (4'-6')], B218913-BLKI, B218913-BS1, B218913-BSDI
N-Nitrosodimethylamine
18L0295-01[SB-2 (4'-6')], 18L0295-02[SB-3 (1'-3')], B218913-BLKI, B218913-BSI, B218913-BSDI
Pyridine
18L0295-01[SB-2 (4'-6')], 18L0295-03[SB-5 (1'-3')], 18L0295-05[DUP-SOIL-1], B218913-BLKI, B218913-BSI, B218913-BSDI
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
4-Chloroaniline
18L0295-01[SB-2 (4'-6')], 18L0295-02[SB-3 (1'-3')], 18L0295-03[SB-5 (1'-3')], 18L0295-05[DUP-SOIL-1], B218913-BLKI, B218913-BS1, B218913-BSD1
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 6 of 68

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-2 (4'-6') Sampled: 12/4/2018 12:50
Sample ID: 18L0295-01
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
0.043
0.11
0.026
mg/Kg dry
1 R-05, J
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Acrylonitrile
ND
0.0066
0.0027
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Benzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Bromobenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Bromochloromethane
ND
0.0022
0.0015
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Bromodichloromethane
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Bromoform
ND
0.0022
0.0015
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Bromomethane
ND
0.011
0.0046
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
2-Butanone (MEK)
ND
0.044
0.019
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
tert-Butyl Alcohol (TBA)
ND
0.044
0.023
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
n-Butylbenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
sec-Butylbenzene
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
tert-Butylbenzene
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0011
0.00066
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Carbon Disulfide
ND
0.0066
0.0047
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Carbon Tetrachloride
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Chlorobenzene
ND
0.0022
0.00077
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Chlorodibromomethane
ND
0.0011
0.00077
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Chloroethane
ND
0.022
0.0016
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Chloroform
ND
0.0044
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Chloromethane
ND
0.011
0.0070
mg/Kg dry
1 L-04
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
2-Chlorotoluene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
4-Chlorotoluene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0022
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2-Dibromoethane (EDB)
ND
0.0011
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Dibromomethane
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2-Dichlorobenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,3-Dichlorobenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,4-Dichlorobenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
trans-1,4-Dichloro-2-butene
ND
0.0044
0.0023
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.022
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,1-Dichloroethane
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2-Dichloroethane
ND
0.0022
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1, 1 -Dichloroethylene
ND
0.0044
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
cis-1,2-Dichloroethylene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
trans-1,2-Dichloroethylene
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2-Dichloropropane
ND
0.0022
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,3-Dichloropropane
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
2,2-Dichloropropane
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1, 1 -Dichloropropene
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
cis-1,3-Dichloropropene
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
trans-1,3-Dichloropropene
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Diethyl Ether
ND
0.022
0.0020
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Page 7 of 68

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ANALYTICAL LABORATORY
Table of Contents
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SB-2 (4'-6')
Sample ID: 18L0295-01
Samnle Matrix: Soil
Analyte
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 12: 5 0
Volatile Organic Compounds by GC/MS
Results RL DL Units Dilution Flag/Qual Method
Work Order: 18L0295
Date Date/Time
Prepared Analyzed Analyst
Diisopropyl Ether (DIPE)
ND
0.0011
0.00066
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,4-Dioxane
ND
0.11
0.063
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Ethylbenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Hexachlorobutadiene
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
2-Hexanone (MBK)
ND
0.022
0.012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Isopropylbenzene (Cumene)
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0044
0.00099
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Methylene Chloride
ND
0.022
0.0078
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.022
0.0084
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Naphthalene
ND
0.0044
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
n-Propylbenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Styrene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0022
0.0020
mg/Kgdry
1
SW-8468260B
12/10/18
12/10/18 12:49
MFF
1,1,2,2-Tetrachloroethane
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Tetrachloroethylene
ND
0.0022
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Tetrahydrofuran
ND
0.011
0.0024
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Toluene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2,3-Trichlorobenzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2,4-Trichlorobenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,3,5-Trichlorobenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,1,1-Trichloroethane
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,1,2-Trichloroethane
ND
0.0022
0.0013
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Trichloroethylene
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Trichlorofluoromethane (Freon 11)
ND
0.011
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,2,3-Trichloropropane
ND
0.0022
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.011
0.00099
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
1,3,5-Trimethylbenzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Vinyl Chloride
ND
0.011
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
m+p Xylene
ND
0.0044
0.0019
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
o-Xylene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 12:49
MFF
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 139 * 70-130
Toluene-d8 101 70-130
4-Bromofluorobenzene 111 70-130
S-17
12/10/18 12:49
12/10/18 12:49
12/10/18 12:49
Page 8 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-2 (4'-6') Sampled: 12/4/2018 12:50
Samnle ID: 18L0295-01
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.21
0.062
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Acenaphthylene
ND
0.21
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Acetophenone
ND
0.41
0.082
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Aniline
ND
0.41
0.12
mg/Kg dry
1 V-04
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Anthracene
ND
0.21
0.060
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Benzidine
ND
0.80
0.52
mg/Kg dry
1 V-04, V-05
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Benzo(a)anthracene
ND
0.21
0.055
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Benzo(a)pyrene
ND
0.21
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Benzo(b)fluoranthene
ND
0.21
0.059
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Benzo(g,h,i)perylene
ND
0.21
0.091
mg/Kg dry
1 V-05
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Benzo(k)fluoranthene
ND
0.21
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Benzoic Acid
ND
1.2
0.22
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Bis(2-chloroethoxy)methane
ND
0.41
0.079
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Bis(2-chloroethyl)ether
ND
0.41
0.082
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Bis(2-chloroisopropyl)ether
ND
0.41
0.089
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.41
0.16
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
4-Bromophenylphenylether
ND
0.41
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Butylbenzylphthalate
ND
0.41
0.099
mg/Kg dry
I
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Carbazole
ND
0.21
0.054
mg/Kg dry
I
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
4-Chloroaniline
ND
0.80
0.095
mg/Kg dry
1 V-34
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
4-Chloro-3-methylphenol
ND
0.80
0.089
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2-Chloronaphthalene
ND
0.41
0.078
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2-Chlorophenol
ND
0.41
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
4-Chlorophenylphenylether
ND
0.41
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Chrysene
ND
0.21
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Dibenz(a,h)anthracene
ND
0.21
0.13
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Dibenzofuran
ND
0.41
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Di-n-butylphthalate
ND
0.41
0.090
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
1,2-Dichlorobenzene
ND
0.41
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
1,3-Dichlorobenzene
ND
0.41
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
1,4-Dichlorobenzene
ND
0.41
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
3,3-Dichlorobenzidine
ND
0.21
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2,4-Dichlorophenol
ND
0.41
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Diethylphthalate
ND
0.41
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2,4-Dimethylphenol
ND
0.41
0.077
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Dimethylphthalate
ND
0.41
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
4,6-Dinitro-2-methylphenol
ND
0.41
0.39
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2,4-Dinitrophenol
ND
0.80
0.24
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2,4-Dinitrotoluene
ND
0.41
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2,6-Dinitrotoluene
ND
0.41
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Di-n-octylphthalate
ND
0.41
0.22
mg/Kg dry
1 R-05
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
0.41
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Fluoranthene
ND
0.21
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Flumene
ND
0.21
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Page 9 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-2 (4'-6') Sampled: 12/4/2018 12:50
Samnle ID: 18L0295-01
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.41
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Hexachlorobutadiene
ND
0.41
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Hexachlorocyclopentadiene
ND
0.41
0.088
mg/Kg dry
1
V-05
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Hexachloroethane
ND
0.41
0.083
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Indeno(1,2,3-cd)pyrene
ND
0.21
0.15
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Isophorone
ND
0.41
0.080
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
1-Methylnaphthalene
ND
0.21
0.079
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2-Methylnaphthalene
ND
0.21
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2-Methylphenol
ND
0.41
0.10
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
3/4-Methylphenol
ND
0.41
0.13
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Naphthalene
ND
0.21
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2-Nitroaniline
ND
0.41
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
3-Nitroaniline
ND
0.41
0.060
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
4-Nitroaniline
ND
0.41
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Nitrobenzene
ND
0.41
0.078
mg/Kg dry
1
V-05
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2-Nitrophenol
ND
0.41
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
4-Nitrophenol
ND
0.80
0.090
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
N-Nitrosodimethylamine
ND
0.41
0.26
mg/Kg dry
1
V-05
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
0.41
0.085
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
N-Nitrosodi-n-propylamine
ND
0.41
0.085
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Pentachloronitrobenzene
ND
0.41
0.099
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Pentachlorophenol
ND
0.41
0.10
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Phenanthrene
ND
0.21
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Phenol
ND
0.41
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Pyrene
ND
0.21
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Pyridine
ND
0.41
0.067
mg/Kg dry
1
V-05
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
1,2,4,5-Texachlorobenzene
ND
0.41
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
1,2,4-Trichlorobenzene
ND
0.41
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2,4,5-Trichlorophenol
ND
0.41
0.094
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
2,4,6-Trichlorophenol
ND
0.41
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/11/18 21:07
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
45.8
30-130
12/11/18 21:07
Phenol-d6
47.5
30-130
12/11/18 21:07
Nitrobenzene-d5
47.7
30-130
12/11/18 21:07
2-Fluorobiphenyl
40.7
30-130
12/11/18 21:07
2,4,6-Tribromophenol
50.7
30-130
12/11/18 21:07
p-Terphenyl-dl4
50.8
30-130
12/11/18 21:07
Page 10 of 68

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SB-2 (4'-6')
Samnle ID: 18L0295-01
Samnle Matrix: Soil
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 12:50
Work Order: 18L0295
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
0.63
0.20
0.033
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:15
MJH
Chromium
22
5.1
0.39
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:15
MJH
Lead
5.3
2.0
0.067
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:15
MJH
Mercury
0.0038
0.030
0.0030
mg/Kg dry
1 J
SW-846 7471B
12/12/18
12/12/18 14:16
AJL
Selenium
ND
0.85
0.081
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:15
MJH
Silver
0.022
0.090
0.0081
mg/Kg dry
5 J
SW-846 6020B
12/11/18
12/12/18 11:15
MJH
Barium
22
10
0.41
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:15
MJH
Cadmium
ND
0.39
0.013
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:15
MJH
Page 11 of 68

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-2 (4'-6') Sampled: 12/4/2018 12:50
Samnle ID: 18L0295-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 82.0 % Wt 1
SM 2540G 12/11/18 12/11/18 18:17 AVF
Page 12 of 68

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-3 (1'-3') Sampled: 12/4/2018 12:00
Sample ID: 18L0295-02
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
0.038
0.10
0.024
mg/Kg dry
1 R-05, J
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Acrylonitrile
ND
0.0060
0.0025
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0010
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Benzene
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Bromobenzene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Bromochloromethane
ND
0.0020
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Bromodichloromethane
ND
0.0020
0.00060
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Bromoform
ND
0.0020
0.0014
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Bromomethane
ND
0.010
0.0042
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
2-Butanone (MEK)
ND
0.040
0.018
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
tert-Butyl Alcohol (TBA)
ND
0.040
0.021
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
n-Butylbenzene
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
sec-Butylbenzene
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
tert-Butylbenzene
ND
0.0020
0.00090
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0010
0.00060
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Carbon Disulfide
ND
0.0060
0.0043
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Carbon Tetrachloride
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Chlorobenzene
ND
0.0020
0.00070
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Chlorodibromomethane
ND
0.0010
0.00070
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Chloroethane
ND
0.020
0.0015
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Chloroform
ND
0.0040
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Chloromethane
ND
0.010
0.0064
mg/Kg dry
1 L-04
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
2-Chlorotoluene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
4-Chlorotoluene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0020
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2-Dibromoethane (EDB)
ND
0.0010
0.0010
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Dibromomethane
ND
0.0020
0.00060
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2-Dichlorobenzene
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,3-Dichlorobenzene
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,4-Dichlorobenzene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
trans-1,4-Dichloro-2-butene
ND
0.0040
0.0021
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.020
0.0013
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,1-Dichloroethane
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2-Dichloroethane
ND
0.0020
0.0013
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1, 1 -Dichloroethylene
ND
0.0040
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
cis-1,2-Dichloroethylene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
trans-1,2-Dichloroethylene
ND
0.0020
0.00090
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2-Dichloropropane
ND
0.0020
0.0013
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,3-Dichloropropane
ND
0.0010
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
2,2-Dichloropropane
ND
0.0020
0.00090
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1, 1 -Dichloropropene
ND
0.0020
0.00090
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
cis-1,3-Dichloropropene
ND
0.0010
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
trans-1,3-Dichloropropene
ND
0.0010
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Diethyl Ether
ND
0.020
0.0018
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Page 13 of 68

icon-te w
ANALYTICAL LABORATORY
Table of Contents
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SB-3 (1'-3')
Sample ID: 18L0295-02
Samnle Matrix: Soil
Analyte
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 12:00
Volatile Organic Compounds by GC/MS
Results RL DL Units Dilution Flag/Qual Method
Work Order: 18L0295
Date Date/Time
Prepared Analyzed Analyst
Diisopropyl Ether (DIPE)
ND
0.0010
0.00060
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,4-Dioxane
ND
0.10
0.058
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Ethylbenzene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Hexachlorobutadiene
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
2-Hexanone (MBK)
ND
0.020
0.011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Isopropylbenzene (Cumene)
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0040
0.00090
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Methylene Chloride
ND
0.020
0.0071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.020
0.0076
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Naphthalene
ND
0.0040
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
n-Propylbenzene
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Styrene
ND
0.0020
0.00060
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0020
0.0018
mg/Kgdry
1
SW-8468260B
12/10/18
12/10/18 14:04
MFF
1,1,2,2-Tetrachloroethane
ND
0.0020
0.00090
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Tetrachloroethylene
ND
0.0020
0.0013
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Tetrahydrofuran
ND
0.010
0.0022
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Toluene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2,3-Trichlorobenzene
ND
0.0020
0.00060
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2,4-Trichlorobenzene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,3,5-Trichlorobenzene
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,1,1-Trichloroethane
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,1,2-Trichloroethane
ND
0.0020
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Trichloroethylene
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Trichlorofluoromethane (Freon 11)
ND
0.010
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,2,3-Trichloropropane
ND
0.0020
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.010
0.00090
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0020
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
1,3,5-Trimethylbenzene
ND
0.0020
0.00060
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Vinyl Chloride
ND
0.010
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
m+p Xylene
ND
0.0040
0.0017
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
o-Xylene
ND
0.0020
0.00070
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 14:04
MFF
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 137 * 70-130
Toluene-d8 98.8 70-130
4-Bromofluorobenzene 106 70-130
S-17
12/10/18 14:04
12/10/18 14:04
12/10/18 14:04
Page 14 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-3 (1'-3') Sampled: 12/4/2018 12:00
Samnle ID: 18L0295-02
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.21
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Acenaphthylene
ND
0.21
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Acetophenone
ND
0.42
0.083
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Aniline
ND
0.42
0.12
mg/Kg dry
1 V-04
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Anthracene
ND
0.21
0.061
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Benzidine
ND
0.82
0.53
mg/Kg dry
1 V-04, V-05
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Benzo(a)anthracene
ND
0.21
0.056
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Benzo(a)pyrene
ND
0.21
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Benzo(b)fluoranthene
ND
0.21
0.059
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Benzo(g,h,i)perylene
ND
0.21
0.093
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Benzo(k)fluoranthene
ND
0.21
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Benzoic Acid
ND
1.2
0.22
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Bis(2-chloroethoxy)methane
ND
0.42
0.080
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Bis(2-chloroethyl)ether
ND
0.42
0.083
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Bis(2-chloroisopropyl)ether
ND
0.42
0.090
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Bis(2-Ethylhexyl)phthalate
0.38
0.42
0.16
mg/Kg dry
1 J
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
4-Bromophenylphenylether
ND
0.42
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Butylbenzylphthalate
ND
0.42
0.10
mg/Kg dry
I V-05
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Carbazole
ND
0.21
0.054
mg/Kg dry
I
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
4-Chloroaniline
ND
0.82
0.097
mg/Kg dry
1 V-34
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
4-Chloro-3-methylphenol
ND
0.82
0.090
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2-Chloronaphthalene
ND
0.42
0.079
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2-Chlorophenol
ND
0.42
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
4-Chlorophenylphenylether
ND
0.42
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Chrysene
ND
0.21
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Dibenz(a,h)anthracene
ND
0.21
0.13
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Dibenzofuran
ND
0.42
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Di-n-butylphthalate
ND
0.42
0.092
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
1,2-Dichlorobenzene
ND
0.42
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
1,3-Dichlorobenzene
ND
0.42
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
1,4-Dichlorobenzene
ND
0.42
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
3,3-Dichlorobenzidine
ND
0.21
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2,4-Dichlorophenol
ND
0.42
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Diethylphthalate
ND
0.42
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2,4-Dimethylphenol
ND
0.42
0.078
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Dimethylphthalate
ND
0.42
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
4,6-Dinitro-2-methylphenol
ND
0.42
0.40
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2,4-Dinitrophenol
ND
0.82
0.24
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2,4-Dinitrotoluene
ND
0.42
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2,6-Dinitrotoluene
ND
0.42
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Di-n-octylphthalate
ND
0.42
0.22
mg/Kg dry
1 R-05
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
1,2-Diphenylhydrazine/Azobenzene
ND
0.42
0.068
mg/Kg dry
I V-05
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Fluoranthene
ND
0.21
0.069
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Flumene
ND
0.21
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Page 15 of 68

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-3 (1'-3') Sampled: 12/4/2018 12:00
Samnle ID: 18L0295-02
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.42
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Hexachlorobutadiene
ND
0.42
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Hexachlorocyclopentadiene
ND
0.42
0.089
mg/Kg dry
1
V-05
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Hexachloroethane
ND
0.42
0.084
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Indeno(1,2,3-cd)pyrene
ND
0.21
0.15
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Isophorone
ND
0.42
0.082
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
1-Methylnaphthalene
ND
0.21
0.080
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2-Methylnaphthalene
ND
0.21
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2-Methylphenol
ND
0.42
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
3/4-Methylphenol
ND
0.42
0.13
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Naphthalene
ND
0.21
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2-Nitroaniline
ND
0.42
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
3-Nitroaniline
ND
0.42
0.061
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
4-Nitroaniline
ND
0.42
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Nitrobenzene
ND
0.42
0.079
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2-Nitrophenol
ND
0.42
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
4-Nitrophenol
ND
0.82
0.092
mg/Kg dry
1
V-05
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
N-Nitrosodimethylamine
ND
0.42
0.27
mg/Kg dry
1
V-05
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
N-Nitrosodiphenylamine/Diphenylamine
ND
0.42
0.087
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
N-Nitrosodi-n-propylamine
ND
0.42
0.087
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Pentachloronitrobenzene
ND
0.42
0.10
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Pentachlorophenol
ND
0.42
0.10
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Phenanthrene
ND
0.21
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Phenol
ND
0.42
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Pyrene
ND
0.21
0.069
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Pyridine
ND
0.42
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
1,2,4,5-Texachlorobenzene
ND
0.42
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
1,2,4-Trichlorobenzene
ND
0.42
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2,4,5-Trichlorophenol
ND
0.42
0.095
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
2,4,6-Trichlorophenol
ND
0.42
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 8:57
CDT
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
48.3
30-130
12/12/18 8:57
Phenol-d6
51.9
30-130
12/12/18 8:57
Nitrobenzene-d5
52.1
30-130
12/12/18 8:57
2-Fluorobiphenyl
46.7
30-130
12/12/18 8:57
2,4,6-Tribromophenol
51.3
30-130
12/12/18 8:57
p-Terphenyl-dl4
53.0
30-130
12/12/18 8:57
Page 16 of 68

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SB-3 (1'-3')
Samnle ID: 18L0295-02
Samnle Matrix: Soil
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 12:00
Work Order: 18L0295
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
1.6
0.21
0.034
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:19
MJH
Chromium
66
5.2
0.40
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:19
MJH
Lead
30
2.1
0.069
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:19
MJH
Mercury
0.024
0.031
0.0031
mg/Kg dry
1
J
SW-846 7471B
12/12/18
12/12/18 14:18
AJL
Selenium
0.16
0.88
0.083
mg/Kg dry
5
J
SW-846 6020B
12/11/18
12/12/18 11:19
MJH
Silver
0.053
0.092
0.0084
mg/Kg dry
5
J
SW-846 6020B
12/11/18
12/12/18 11:19
MJH
Barium
150
42
1.7
mg/Kg dry
20
SW-846 6020B
12/11/18
12/12/18 11:33
WSD
Cadmium
0.053
0.40
0.013
mg/Kg dry
5
J
SW-846 6020B
12/11/18
12/12/18 11:19
MJH
Page 17 of 68

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-3 (1'-3') Sampled: 12/4/2018 12:00
Samnle ID: 18L0295-02
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 79.5 % Wt 1
SM 2540G 12/11/18 12/11/18 18:17 AVF
Page 18 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-5 (1'-3') Sampled: 12/4/2018 12:30
Sample ID: 18L0295-03
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
0.048
0.11
0.025
mg/Kg dry
1 R-05, J
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Acrylonitrile
ND
0.0064
0.0027
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0011
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Benzene
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Bromobenzene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Bromochloromethane
ND
0.0021
0.0015
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Bromodichloromethane
ND
0.0021
0.00064
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Bromoform
ND
0.0021
0.0015
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Bromomethane
ND
0.011
0.0045
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
2-Butanone (MEK)
ND
0.043
0.019
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
tert-Butyl Alcohol (TBA)
ND
0.043
0.022
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
n-Butylbenzene
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
sec-Butylbenzene
ND
0.0021
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
tert-Butylbenzene
ND
0.0021
0.00096
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0011
0.00064
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Carbon Disulfide
ND
0.0064
0.0046
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Carbon Tetrachloride
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Chlorobenzene
ND
0.0021
0.00075
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Chlorodibromomethane
ND
0.0011
0.00075
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Chloroethane
ND
0.021
0.0016
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Chloroform
ND
0.0043
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Chloromethane
ND
0.011
0.0068
mg/Kg dry
1 L-04
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
2-Chlorotoluene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
4-Chlorotoluene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0021
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2-Dibromoethane (EDB)
ND
0.0011
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Dibromomethane
ND
0.0021
0.00064
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2-Dichlorobenzene
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,3-Dichlorobenzene
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,4-Dichlorobenzene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
trans-1,4-Dichloro-2-butene
ND
0.0043
0.0022
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.021
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,1-Dichloroethane
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2-Dichloroethane
ND
0.0021
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1, 1 -Dichloroethylene
ND
0.0043
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
cis-1,2-Dichloroethylene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
trans-1,2-Dichloroethylene
ND
0.0021
0.00096
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2-Dichloropropane
ND
0.0021
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,3-Dichloropropane
ND
0.0011
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
2,2-Dichloropropane
ND
0.0021
0.00096
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1, 1 -Dichloropropene
ND
0.0021
0.00096
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
cis-1,3-Dichloropropene
ND
0.0011
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
trans-1,3-Dichloropropene
ND
0.0011
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Diethyl Ether
ND
0.021
0.0019
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Page 19 of 68

icon-te w
ANALYTICAL LABORATORY
Table of Contents
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SB-5 (1'-3')
Sample ID: 18L0295-03
Samnle Matrix: Soil
Analyte
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 12:3 0
Volatile Organic Compounds by GC/MS
Results RL DL Units Dilution Flag/Qual Method
Work Order: 18L0295
Date Date/Time
Prepared Analyzed Analyst
Diisopropyl Ether (DIPE)
ND
0.0011
0.00064
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,4-Dioxane
ND
0.11
0.061
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Ethylbenzene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Hexachlorobutadiene
ND
0.0021
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
2-Hexanone (MBK)
ND
0.021
0.012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Isopropylbenzene (Cumene)
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0043
0.00096
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Methylene Chloride
ND
0.021
0.0076
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.021
0.0081
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Naphthalene
ND
0.0043
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
n-Propylbenzene
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Styrene
ND
0.0021
0.00064
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0021
0.0019
mg/Kgdry
1
SW-8468260B
12/10/18
12/10/18 13:14
MFF
1,1,2,2-Tetrachloroethane
ND
0.0021
0.00096
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Tetrachloroethylene
ND
0.0021
0.0014
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Tetrahydrofuran
ND
0.011
0.0023
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Toluene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2,3-Trichlorobenzene
ND
0.0021
0.00064
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2,4-Trichlorobenzene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,3,5-Trichlorobenzene
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,1,1-Trichloroethane
ND
0.0021
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,1,2-Trichloroethane
ND
0.0021
0.0013
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Trichloroethylene
ND
0.0021
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Trichlorofluoromethane (Freon 11)
ND
0.011
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,2,3-Trichloropropane
ND
0.0021
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.011
0.00096
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0021
0.00085
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
1,3,5-Trimethylbenzene
ND
0.0021
0.00064
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Vinyl Chloride
ND
0.011
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
m+p Xylene
ND
0.0043
0.0018
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
o-Xylene
ND
0.0021
0.00075
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:14
MFF
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 141 * 70-130
Toluene-d8 102 70-130
4-Bromofluorobenzene 111 70-130
S-17
12/10/18 13:14
12/10/18 13:14
12/10/18 13:14
Page 20 of 68

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-5 (1'-3') Sampled: 12/4/2018 12:30
Samnle ID: 18L0295-03
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.19
0.057
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Acenaphthylene
ND
0.19
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Acetophenone
ND
0.38
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Aniline
ND
0.38
0.11
mg/Kg dry
1 V-04
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Anthracene
ND
0.19
0.055
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Benzidine
ND
0.74
0.47
mg/Kg dry
1 V-04, V-05
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Benzo(a)anthracene
ND
0.19
0.050
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Benzo(a)pyrene
ND
0.19
0.059
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Benzo(b)fluoranthene
ND
0.19
0.053
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Benzo(g,h,i)perylene
ND
0.19
0.084
mg/Kg dry
1 V-05
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Benzo(k)fluoranthene
ND
0.19
0.059
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Benzoic Acid
ND
1.1
0.20
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Bis(2-chloroethoxy)methane
ND
0.38
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Bis(2-chloroethyl)ether
ND
0.38
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Bis(2-chloroisopropyl)ether
ND
0.38
0.081
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.38
0.15
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
4-Bromophenylphenylether
ND
0.38
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Butylbenzylphthalate
ND
0.38
0.090
mg/Kg dry
I
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Carbazole
ND
0.19
0.049
mg/Kg dry
I
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
4-Chloroaniline
ND
0.74
0.087
mg/Kg dry
1 V-34
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
4-Chloro-3-methylphenol
ND
0.74
0.081
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2-Chloronaphthalene
ND
0.38
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2-Chlorophenol
ND
0.38
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
4-Chlorophenylphenylether
ND
0.38
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Chrysene
ND
0.19
0.059
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Dibenz(a,h)anthracene
ND
0.19
0.12
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Dibenzofuran
ND
0.38
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Di-n-butylphthalate
ND
0.38
0.082
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
1,2-Dichlorobenzene
ND
0.38
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
1,3-Dichlorobenzene
ND
0.38
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
1,4-Dichlorobenzene
ND
0.38
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
3,3-Dichlorobenzidine
ND
0.19
0.058
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2,4-Dichlorophenol
ND
0.38
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Diethylphthalate
ND
0.38
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2,4-Dimethylphenol
ND
0.38
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Dimethylphthalate
ND
0.38
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
4,6-Dinitro-2-methylphenol
ND
0.38
0.36
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2,4-Dinitrophenol
ND
0.74
0.22
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2,4-Dinitrotoluene
ND
0.38
0.061
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2,6-Dinitrotoluene
ND
0.38
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Di-n-octylphthalate
ND
0.38
0.20
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
0.38
0.061
mg/Kg dry
I
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Fluoranthene
ND
0.19
0.062
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Flumene
ND
0.19
0.061
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Page 21 of 68

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-5 (1'-3') Sampled: 12/4/2018 12:30
Samnle ID: 18L0295-03
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.38
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Hexachlorobutadiene
ND
0.38
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Hexachlorocyclopentadiene
ND
0.38
0.080
mg/Kg dry
1 V-05
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Hexachloroethane
ND
0.38
0.076
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Indeno(1,2,3-cd)pyrene
ND
0.19
0.14
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Isophorone
ND
0.38
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
1-Methylnaphthalene
ND
0.19
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2-Methylnaphthalene
ND
0.19
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2-Methylphenol
ND
0.38
0.095
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
3/4-Methylphenol
ND
0.38
0.12
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Naphthalene
ND
0.19
0.097
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2-Nitroaniline
ND
0.38
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
3-Nitroaniline
ND
0.38
0.055
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
4-Nitroaniline
ND
0.38
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Nitrobenzene
ND
0.38
0.071
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2-Nitrophenol
ND
0.38
0.10
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
4-Nitrophenol
ND
0.74
0.082
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
N-Nitrosodimethylamine
ND
0.38
0.24
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
0.38
0.078
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
N-Nitrosodi-n-propylamine
ND
0.38
0.078
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Pentachloronitrobenzene
ND
0.38
0.090
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Pentachlorophenol
ND
0.38
0.091
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Phenanthrene
ND
0.19
0.098
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Phenol
ND
0.38
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Pyrene
ND
0.19
0.062
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Pyridine
ND
0.38
0.061
mg/Kg dry
1 V-05
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
1,2,4,5-Texachlorobenzene
ND
0.38
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
1,2,4-Trichlorobenzene
ND
0.38
0.068
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2,4,5-Trichlorophenol
ND
0.38
0.086
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
2,4,6-Trichlorophenol
ND
0.38
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 20:41
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
61.1
30-130
12/12/18 20:41
Phenol-d6
65.2
30-130
12/12/18 20:41
Nitrobenzene-d5
65.4
30-130
12/12/18 20:41
2-Fluorobiphenyl
51.4
30-130
12/12/18 20:41
2,4,6-Tribromophenol
63.0
30-130
12/12/18 20:41
p-Terphenyl-dl4
62.9
30-130
12/12/18 20:41
Page 22 of 68

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SB-5 (1'-3')
Samnle ID: 18L0295-03
Samnle Matrix: Soil
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 12:30
Work Order: 18L0295
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
0.30
0.19
0.031
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:22
MJH
Chromium
10
4.7
0.36
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:22
MJH
Lead
2.6
1.9
0.061
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:22
MJH
Mercury
0.0070
0.028
0.0028
mg/Kg dry
1 J
SW-846 7471B
12/12/18
12/12/18 14:20
AJL
Selenium
ND
0.79
0.075
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:22
MJH
Silver
0.018
0.082
0.0075
mg/Kg dry
5 J
SW-846 6020B
12/11/18
12/12/18 11:22
MJH
Barium
14
9.4
0.38
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:22
MJH
Cadmium
ND
0.36
0.012
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:22
MJH
Page 23 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: SB-5 (1'-3') Sampled: 12/4/2018 12:30
Samnle ID: 18L0295-03
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 88.6 % Wt 1
SM 2540G 12/11/18 12/11/18 18:17 AVF
Page 24 of 68

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: BKG-SOIL-1
Samnle ID: 18LO295-04
Samnle Matrix: Soil
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 11:50
Work Order: 18L0295
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
1.9
0.22
0.035
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:26
MJH
Chromium
96
5.4
0.41
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:26
MJH
Lead
12
2.2
0.071
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:26
MJH
Mercury
0.16
0.030
0.0030
mg/Kg dry
1
SW-846 7471B
12/12/18
12/12/18 14:21
AJL
Selenium
0.29
0.90
0.086
mg/Kg dry
5 J
SW-846 6020B
12/11/18
12/12/18 11:26
MJH
Silver
0.073
0.095
0.0086
mg/Kg dry
5 J
SW-846 6020B
12/11/18
12/12/18 11:26
MJH
Barium
68
11
0.44
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:26
MJH
Cadmium
ND
0.41
0.014
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:26
MJH
Page 25 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: BKG-SOIL-1 Sampled: 12/4/2018 11:50
Samnle ID: 18LO295-04
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 77.1 % Wt 1
SM 2540G 12/11/18 12/11/18 18:17 AVF
Page 26 of 68

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ANALYTICAL LABORATORY
Table of Contents
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: BKG-SOIL-1
Sample ID: 18LO295-04
Samnle Matrix: Soil
Analyte
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description: Work Order: 18L0295
Sampled: 12/4/2018 11: 5 0
Miscellaneous Test
Date Date/Time
Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
See Attached Report Pages Attached Attached mg/Kg 1 7199 1/3/19 2:02 PAL
Page 27 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: DUP-SOIL-1 Sampled: 12/4/2018 00:00
Sample ID: 18LO295-05
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
0.036
0.089
0.021
mg/Kg dry
1 R-05, J
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Acrylonitrile
ND
0.0053
0.0022
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.00089
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Benzene
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Bromobenzene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Bromochloromethane
ND
0.0018
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Bromodichloromethane
ND
0.0018
0.00053
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Bromoform
ND
0.0018
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Bromomethane
ND
0.0089
0.0037
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
2-Butanone (MEK)
ND
0.036
0.016
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
tert-Butyl Alcohol (TBA)
ND
0.036
0.019
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
n-Butylbenzene
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
sec-Butylbenzene
ND
0.0018
0.00089
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
tert-Butylbenzene
ND
0.0018
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.00089
0.00053
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Carbon Disulfide
ND
0.0053
0.0038
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Carbon Tetrachloride
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Chlorobenzene
ND
0.0018
0.00062
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Chlorodibromomethane
ND
0.00089
0.00062
mg/Kg dry
I
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Chloroethane
ND
0.018
0.0013
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Chloroform
ND
0.0036
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Chloromethane
ND
0.0089
0.0057
mg/Kg dry
1 L-04
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
2-Chlorotoluene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
4-Chlorotoluene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0018
0.00098
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2-Dibromoethane (EDB)
ND
0.00089
0.00089
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Dibromomethane
ND
0.0018
0.00053
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2-Dichlorobenzene
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,3-Dichlorobenzene
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,4-Dichlorobenzene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
trans-1,4-Dichloro-2-butene
ND
0.0036
0.0019
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.018
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,1-Dichloroethane
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2-Dichloroethane
ND
0.0018
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1, 1 -Dichloroethylene
ND
0.0036
0.00098
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
cis-1,2-Dichloroethylene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
trans-1,2-Dichloroethylene
ND
0.0018
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2-Dichloropropane
ND
0.0018
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,3-Dichloropropane
ND
0.00089
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
2,2-Dichloropropane
ND
0.0018
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1, 1 -Dichloropropene
ND
0.0018
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
cis-1,3-Dichloropropene
ND
0.00089
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
trans-1,3-Dichloropropene
ND
0.00089
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Diethyl Ether
ND
0.018
0.0016
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Page 28 of 68

icon-te w
ANALYTICAL LABORATORY
Table of Contents
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: DUP-SOIL-1
Sample ID: 18LO295-05
Samnle Matrix: Soil
Analyte
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 00:00
Volatile Organic Compounds by GC/MS
Results RL DL Units Dilution Flag/Qual Method
Work Order: 18L0295
Date Date/Time
Prepared Analyzed Analyst
Diisopropyl Ether (DIPE)
ND
0.00089
0.00053
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,4-Dioxane
ND
0.089
0.051
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Ethylbenzene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Hexachlorobutadiene
ND
0.0018
0.00089
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
2-Hexanone (MBK)
ND
0.018
0.0097
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Isopropylbenzene (Cumene)
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0036
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Methylene Chloride
ND
0.018
0.0063
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.018
0.0068
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Naphthalene
ND
0.0036
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
n-Propylbenzene
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Styrene
ND
0.0018
0.00053
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0018
0.0016
mg/Kgdry
1
SW-8468260B
12/10/18
12/10/18 13:39
MFF
1,1,2,2-Tetrachloroethane
ND
0.0018
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Tetrachloroethylene
ND
0.0018
0.0012
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Tetrahydrofuran
ND
0.0089
0.0020
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Toluene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2,3-Trichlorobenzene
ND
0.0018
0.00053
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2,4-Trichlorobenzene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,3,5-Trichlorobenzene
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,1,1-Trichloroethane
ND
0.0018
0.00089
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,1,2-Trichloroethane
ND
0.0018
0.0011
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Trichloroethylene
ND
0.0018
0.00089
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Trichlorofluoromethane (Freon 11)
ND
0.0089
0.00098
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,2,3-Trichloropropane
ND
0.0018
0.00098
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.0089
0.00080
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0018
0.00071
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
1,3,5-Trimethylbenzene
ND
0.0018
0.00053
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Vinyl Chloride
ND
0.0089
0.00098
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
m+p Xylene
ND
0.0036
0.0015
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
o-Xylene
ND
0.0018
0.00062
mg/Kg dry
1
SW-846 8260B
12/10/18
12/10/18 13:39
MFF
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 139 * 70-130
Toluene-d8 101 70-130
4-Bromofluorobenzene 113 70-130
S-17
12/10/18 13:39
12/10/18 13:39
12/10/18 13:39
Page 29 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: DUP-SOIL-1 Sampled: 12/4/2018 00:00
Samnle ID: 18LO295-05
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.19
0.056
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Acenaphthylene
ND
0.19
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Acetophenone
ND
0.37
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Aniline
ND
0.37
0.11
mg/Kg dry
1 V-04
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Anthracene
ND
0.19
0.054
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Benzidine
ND
0.73
0.47
mg/Kg dry
1 V-04, V-05
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Benzo(a)anthracene
ND
0.19
0.050
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Benzo(a)pyrene
ND
0.19
0.058
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Benzo(b)fluoranthene
ND
0.19
0.053
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Benzo(g,h,i)perylene
ND
0.19
0.083
mg/Kg dry
1 V-05
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Benzo(k)fluoranthene
ND
0.19
0.058
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Benzoic Acid
ND
1.1
0.20
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Bis(2-chloroethoxy)methane
ND
0.37
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Bis(2-chloroethyl)ether
ND
0.37
0.074
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Bis(2-chloroisopropyl)ether
ND
0.37
0.080
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.37
0.15
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
4-Bromophenylphenylether
ND
0.37
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Butylbenzylphthalate
ND
0.37
0.089
mg/Kg dry
I
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Carbazole
ND
0.19
0.048
mg/Kg dry
I
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
4-Chloroaniline
ND
0.73
0.086
mg/Kg dry
1 V-34
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
4-Chloro-3-methylphenol
ND
0.73
0.080
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2-Chloronaphthalene
ND
0.37
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2-Chlorophenol
ND
0.37
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
4-Chlorophenylphenylether
ND
0.37
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Chrysene
ND
0.19
0.058
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Dibenz(a,h)anthracene
ND
0.19
0.11
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Dibenzofuran
ND
0.37
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Di-n-butylphthalate
ND
0.37
0.082
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
1,2-Dichlorobenzene
ND
0.37
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
1,3-Dichlorobenzene
ND
0.37
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
1,4-Dichlorobenzene
ND
0.37
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
3,3-Dichlorobenzidine
ND
0.19
0.057
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2,4-Dichlorophenol
ND
0.37
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Diethylphthalate
ND
0.37
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2,4-Dimethylphenol
ND
0.37
0.069
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Dimethylphthalate
ND
0.37
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
4,6-Dinitro-2-methylphenol
ND
0.37
0.36
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2,4-Dinitrophenol
ND
0.73
0.21
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2,4-Dinitrotoluene
ND
0.37
0.061
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2,6-Dinitrotoluene
ND
0.37
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Di-n-octylphthalate
ND
0.37
0.20
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
0.37
0.061
mg/Kg dry
I
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Fluoranthene
ND
0.19
0.062
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Flumene
ND
0.19
0.061
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Page 30 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: DUP-SOIL-1 Sampled: 12/4/2018 00:00
Samnle ID: 18LO295-05
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.37
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Hexachlorobutadiene
ND
0.37
0.066
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Hexachlorocyclopentadiene
ND
0.37
0.079
mg/Kg dry
1 V-05
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Hexachloroethane
ND
0.37
0.075
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Indeno(1,2,3-cd)pyrene
ND
0.19
0.13
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Isophorone
ND
0.37
0.073
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
1-Methylnaphthalene
ND
0.19
0.072
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2-Methylnaphthalene
ND
0.19
0.065
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2-Methylphenol
ND
0.37
0.094
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
3/4-Methylphenol
ND
0.37
0.12
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Naphthalene
ND
0.19
0.096
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2-Nitroaniline
ND
0.37
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
3-Nitroaniline
ND
0.37
0.054
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
4-Nitroaniline
ND
0.37
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Nitrobenzene
ND
0.37
0.070
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2-Nitrophenol
ND
0.37
0.099
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
4-Nitrophenol
ND
0.73
0.082
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
N-Nitrosodimethylamine
ND
0.37
0.24
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
0.37
0.077
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
N-Nitrosodi-n-propylamine
ND
0.37
0.077
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Pentachloronitrobenzene
ND
0.37
0.089
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Pentachlorophenol
ND
0.37
0.090
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Phenanthrene
ND
0.19
0.097
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Phenol
ND
0.37
0.064
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Pyrene
ND
0.19
0.062
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Pyridine
ND
0.37
0.061
mg/Kg dry
1 V-05
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
1,2,4,5-Texachlorobenzene
ND
0.37
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
1,2,4-Trichlorobenzene
ND
0.37
0.067
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2,4,5-Trichlorophenol
ND
0.37
0.085
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
2,4,6-Trichlorophenol
ND
0.37
0.063
mg/Kg dry
1
SW-846 8270D
12/10/18
12/12/18 21:08
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
44.1
30-130
12/12/18 21:08
Phenol-d6
46.0
30-130
12/12/18 21:08
Nitrobenzene-d5
45.7
30-130
12/12/18 21:08
2-Fluorobiphenyl
37.7
30-130
12/12/18 21:08
2,4,6-Tribromophenol
48.2
30-130
12/12/18 21:08
p-Terphenyl-dl4
47.9
30-130
12/12/18 21:08
Page 31 of 68

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: DUP-SOIL-1
Samnle ID: 18LO295-05
Samnle Matrix: Soil
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/4/2018 00:00
Work Order: 18L0295
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
0.35
0.18
0.030
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:29
WSD
Chromium
9.5
4.5
0.35
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:29
WSD
Lead
2.4
1.8
0.059
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:29
WSD
Mercury
0.0076
0.027
0.0027
mg/Kg dry
1
J
SW-846 7471B
12/12/18
12/12/18 14:23
AJL
Selenium
0.080
0.76
0.072
mg/Kg dry
5
J
SW-846 6020B
12/11/18
12/12/18 11:29
WSD
Silver
0.018
0.079
0.0072
mg/Kg dry
5
J
SW-846 6020B
12/11/18
12/12/18 11:29
WSD
Barium
14
9.0
0.37
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:29
WSD
Cadmium
ND
0.34
0.012
mg/Kg dry
5
SW-846 6020B
12/11/18
12/12/18 11:29
WSD
Page 32 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0295
Date Received: 12/6/2018
Field Sample #: DUP-SOIL-1 Sampled: 12/4/2018 00:00
Samnle ID: 18LO295-05
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 90.5 % Wt 1
SM 2540G 12/11/18 12/11/18 18:17 AVF
Page 33 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
18L0295-01 [SB-2 (4'-6')]
B218935
12/11/18
18L0295-02 [SB-3 (1'-3')]
B218935
12/11/18
18L0295-03 [SB-5 (1'-3')]
B218935
12/11/18
18L0295-04 [BKG-SOIL-1]
B218935
12/11/18
18L0295-05 [DUP-SOIL-1]
B218935
12/11/18
Prep Method: SW-846 3050B-SW-846 6020B
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18L0295-01 [SB-2 (4'-6')]
B218953
1.50
50.0
12/11/18
18L0295-02 [SB-3 (1'-3')]
B218953
1.50
50.0
12/11/18
18L0295-03 [SB-5 (1'-3')]
B218953
1.51
50.0
12/11/18
18L0295-04 [BKG-SOIL-1]
B218953
1.51
50.0
12/11/18
18L0295-05 [DUP-SOIL-1]
B218953
1.53
50.0
12/11/18
Prep Method: SW-846 7471-SW-846 7471B
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18L0295-01 [SB-2 (4'-6')]
B219056
0.614
50.0
12/12/18
18L0295-02 [SB-3 (1'-3')]
B219056
0.600
50.0
12/12/18
18L0295-03 [SB-5 (1'-3')]
B219056
0.609
50.0
12/12/18
18L0295-04 [BKG-SOIL-1]
B219056
0.638
50.0
12/12/18
18L0295-05 [DUP-SOIL-1]
B219056
0.622
50.0
12/12/18
Prep Method: SW-846 5035-SW-846 8260B
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18L0295-01 [SB-2 (4'-6')]
B218864
5.55
10.0
12/10/18
18L0295-02 [SB-3 (1'-3')]
B218864
6.26
10.0
12/10/18
18L0295-03 [SB-5 (1'-3')]
B218864
5.30
10.0
12/10/18
18L0295-05 [DUP-SOIL-1]
B218864
6.20
10.0
12/10/18
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18L0295-01 [SB-2 (4'-6')]
B218913
30.0
1.00
12/10/18
18L0295-02 [SB-3 (1'-3')]
B218913
30.5
1.00
12/10/18
18L0295-03 [SB-5 (1'-3')]
B218913
30.4
1.00
12/10/18
18L0295-05 [DUP-SOIL-1]
B218913
30.1
1.00
12/10/18
Page 34 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218864 - SW-846 5035
Blank (B218864-BLK1)
Prepared & Analyzed: 12/10/18
Acetone
ND
0.10
mg/Kg wet R-05
Acrylonitrile
ND
0.0060
mg/Kg wet
tert-Amyl Methyl Ether (TAME)
ND
0.0010
mg/Kg wet
Benzene
ND
0.0020
mg/Kg wet
Bromobenzene
ND
0.0020
mg/Kg wet
Bromochloromethane
ND
0.0020
mg/Kg wet
Bromodichloromethane
ND
0.0020
mg/Kg wet
Bromoform
ND
0.0020
mg/Kg wet
Bromomethane
ND
0.010
mg/Kg wet
2-Butanone (MEK)
ND
0.040
mg/Kg wet
tert-Butyl Alcohol (TBA)
ND
0.040
mg/Kg wet
n-Butylbenzene
ND
0.0020
mg/Kg wet
sec-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butyl Ethyl Ether (TBEE)
ND
0.0010
mg/Kg wet
Carbon Disulfide
ND
0.0060
mg/Kg wet
Carbon Tetrachloride
ND
0.0020
mg/Kg wet
Chlorobenzene
ND
0.0020
mg/Kg wet
Chlorodibromomethane
ND
0.0010
mg/Kg wet
Chloroethane
ND
0.020
mg/Kg wet
Chloroform
ND
0.0040
mg/Kg wet
Chloromethane
ND
0.010
mg/Kg wet L-04
2-Chlorotoluene
ND
0.0020
mg/Kg wet
4-Chlorotoluene
ND
0.0020
mg/Kg wet
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0020
mg/Kg wet
1,2-Dibromoethane (EDB)
ND
0.0010
mg/Kg wet
Dibromomethane
ND
0.0020
mg/Kg wet
1,2-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,3-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,4-Dichlorobenzene
ND
0.0020
mg/Kg wet
trans-1,4-Dichloro-2-butene
ND
0.0040
mg/Kg wet
Dichlorodifluoromethane (Freon 12)
ND
0.020
mg/Kg wet
1,1-Dichloroethane
ND
0.0020
mg/Kg wet
1,2-Dichloroethane
ND
0.0020
mg/Kg wet
1,1-Dichloroethylene
ND
0.0040
mg/Kg wet
cis-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
trans-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
1,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,3-Dichloropropane
ND
0.0010
mg/Kg wet
2,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,1-Dichloropropene
ND
0.0020
mg/Kg wet
cis-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
trans-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
Diethyl Ether
ND
0.020
mg/Kg wet
Diisopropyl Ether (RIPE)
ND
0.0010
mg/Kg wet
1,4-Dioxane
ND
0.10
mg/Kg wet
Ethylbenzene
ND
0.0020
mg/Kg wet
Hexachlorobutadiene
ND
0.0020
mg/Kg wet
2-Hexanone (MBK)
ND
0.020
mg/Kg wet
Isopropylbenzene (Cumene)
ND
0.0020
mg/Kg wet
p-Isopropyltoluene (p-Cymene)
ND
0.0020
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.0040
mg/Kg wet
Page 35 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
malyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218864 - SW-846 5035
Blank (B218864-BLK1)
Prepared & Analyzed: 12/10/18
Methylene Chloride
ND
0.020
mg/Kg wet
4-Methyl-2-pentanone (MIBK)
ND
0.020
mg/Kg wet
Naphthalene
ND
0.0040
mg/Kg wet
n-Propylbenzene
ND
0.0020
mg/Kg wet
Styrene
ND
0.0020
mg/Kg wet
1, 1, 1,2-Tetrachloroethane
ND
0.0020
mg/Kg wet
1,1,2,2-Tetrachloroethane
ND
0.0020
mg/Kg wet
Tetrachloroethylene
ND
0.0020
mg/Kg wet
Tetrahydrofuran
ND
0.010
mg/Kg wet
Toluene
ND
0.0020
mg/Kg wet
1,2,3-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,3,5-Trichlorobenzene
ND
0.0020
mg/Kg wet
1, 1, 1 -Trichloroethane
ND
0.0020
mg/Kg wet
1,1,2-Trichloroethane
ND
0.0020
mg/Kg wet
Trichloroethylene
ND
0.0020
mg/Kg wet
Trichlorofluoromethane (Freon 11)
ND
0.010
mg/Kg wet
1,2,3-Trichloropropane
ND
0.0020
mg/Kg wet
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.010
mg/Kg wet
113)
1,2,4-Trimethylbenzene
ND
0.0020
mg/Kg wet
1,3,5-Trimethylbenzene
ND
0.0020
mg/Kg wet
Vinyl Chloride
ND
0.010
mg/Kg wet
m+p Xylene
ND
0.0040
mg/Kg wet
o-Xylene
ND
0.0020
mg/Kg wet
Surrogate: 1,2-Dichloroethane-d4 0.0550 mg/Kg wet 0.0500 110 70-130
Surrogate: Toluene-d8 0.0503 mg/Kg wet 0.0500 101 70-130
Surrogate:4-Bromofluorobenzene 0.0510 mg/Kg wet 0.0500 102 70-130
LCS (B218864-BSI) Prepared & Analyzed: 12/10/18
Acetone
0.425
0.10
mg/Kg wet
0.200
212 *
70-160
Acrylonitrile
0.0168
0.0060
mg(Kgwet
0.0200
84.1
70-130
tert-Amyl Methyl Ether (TAME)
0.0190
0.0010
mg/Kg wet
0.0200
94.8
70-130
Benzene
0.0177
0.0020
mg/Kg wet
0.0200
88.5
70-130
Bromobenzene
0.0179
0.0020
mg/Kgwet
0.0200
89.6
70-130
Bromochloromethane
0.0163
0.0020
mg/Kg wet
0.0200
81.7
70-130
Bromodichloromethane
0.0209
0.0020
mg/Kg wet
0.0200
105
70-130
Bromoform
0.0208
0.0020
mg/Kgwet
0.0200
104
70-130
Bromomethane
0.0124
0.010
mg/Kg wet
0.0200
62.2
40-130
2-Butanone (MEK)
0.265
0.040
mg/Kg wet
0.200
132
70-160
tert-Butyl Alcohol (TBA)
0.180
0.040
mg/Kg wet
0.200
90.0
40-130
n-Butylbenzene
0.0186
0.0020
mg/Kg wet
0,0200
92.9
70-130
sec-Butylbenzene
0.0193
0.0020
mg/Kg wet
0.0200
96.7
70-130
tert-Butylbenzene
0.0199
0.0020
mg/Kgwet
0.0200
99.5
70-160
tert-Butyl Ethyl Ether (TBEE)
0.0188
0.0010
mg/Kg wet
0,0200
93.8
70-130
Carbon Disulfide
0.0198
0.0060
mg/Kg wet
0.0200
99.0
70-130
Carbon Tetrachloride
0.0251
0.0020
mg/Kg wet
0.0200
126
70-130
Chlorobenzene
0.0190
0.0020
mg/Kg wet
0,0200
95.0
70-130
Chlorodibromomethane
0.0225
0.0010
mg/Kg wet
0.0200
113
70-130
Chloroethane
0.0190
0.020
mg/Kg wet
0.0200
95.0
70-130
Chloroform
0.0208
0.0040
mg/Kg wet
0,0200
104
70-130
Chloromethane
0.0124
0.010
mg/Kg wet
0.0200
62.2 *
70-130
2-Chlorotoluene
0.0191
0.0020
mg/Kg wet
0.0200
95.6
70-130
R-05, L-07A t
t
t
t
t
L-04
Page 36 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218864 - SW-846 5035
LCS (B218864-BSI) Prepared & Analyzed: 12/10/18
4-Chlorotoluene
0.0201
0.0020
mg/Kg wet
0.0200
100
70-130
1,2-Dibromo-3-chloropropane (DBCP)
0.0172
0.0020
mg/Kg wet
0.0200
86.2
70-130
1,2-Dibromoethane (EDB)
0.0209
0.0010
mg/Kg wet
0.0200
105
70-130
Dibromomethane
0.0188
0.0020
mg/Kg wet
0.0200
94.2
70-130
1,2-Dichlorobenzene
0.0186
0.0020
mg/Kg wet
0.0200
92.9
70-130
1,3-Dichlorobenzene
0.0192
0.0020
mg/Kg wet
0.0200
96.1
70-130
1,4-Dichlorobenzene
0.0181
0.0020
mg/Kg wet
0.0200
90.5
70-130
trans-1,4-Dichloro-2-butene
0.0182
0.0040
mg/Kg wet
0.0200
90.9
70-130
Dichlorodifluoromethane(Freon 12)
0.0123
0.020
mg/Kg wet
0.0200
61.4
40-160
1,1-Dichloroethane
0.0191
0.0020
mg/Kg wet
0.0200
95.3
70-130
1,2-Dichloroethane
0.0220
0.0020
mg/Kg wet
0.0200
110
70-130
1,1-Dichloroethylene
0.0202
0.0040
mg/Kg wet
0.0200
101
70-130
cis-1,2-Dichloroethylene
0.0193
0.0020
mg/Kg wet
0.0200
96.3
70-130
trans-1,2-Dichloroethylene
0.0187
0.0020
mg/Kg wet
0.0200
93.6
70-130
1,2-Dichloropropane
0.0161
0.0020
mg/Kg wet
0.0200
80.6
70-130
1,3-Dichloropropane
0.0172
0.0010
mg/Kg wet
0.0200
85.8
70-130
2,2-Dichloropropane
0.0252
0.0020
mg/Kg wet
0.0200
126
70-130
1,1-Dichloropropene
0.0209
0.0020
mg/Kg wet
0.0200
105
70-130
cis-1,3-Dichloropropene
0.0187
0.0010
mg/Kg wet
0.0200
93.4
70-130
trans-1,3-Dichloropropene
0.0215
0.0010
mg/Kg wet
0.0200
107
70-130
Diethyl Ether
0.0164
0.020
mg/Kg wet
0.0200
82.0
70-130
Diisopropyl Ether (DIPE)
0.0162
0.0010
mg/Kg wet
0.0200
80.9
70-130
1,4-Dioxane
0.168
0.10
mg/Kg wet
0.200
83.9
40-160
Ethylbenzene
0.0188
0.0020
mg/Kg wet
0.0200
94.0
70-130
Hexachlorobutadiene
0.0200
0.0020
mg/Kg wet
0.0200
99.9
70-160
2-Hexanone (MBK)
0.223
0.020
mg/Kg wet
0.200
ill
70-160
Isopropylbenzene (Cumene)
0.0204
0.0020
mg/Kg wet
0.0200
102
70-130
p-Isopropyltoluene (p-Cymene)
0.0188
0.0020
mg/Kg wet
0.0200
94.0
70-130
Methyl tert-Butyl Ether (MTBE)
0.0213
0.0040
mg/Kg wet
0.0200
107
70-130
Methylene Chloride
0.0165
0.020
mg/Kg wet
0.0200
82.7
40-160
4-Methyl-2-pentanone (MIBK)
0.162
0.020
mg/Kg wet
0.200
81.0
70-160
Naphthalene
0.0175
0.0040
mg/Kg wet
0.0200
87.4
40-130
n-Propylbenzene
0.0191
0.0020
mg/Kg wet
0.0200
95.4
70-130
Styrene
0.0185
0.0020
mg/Kg wet
0.0200
92.5
70-130
1, 1, 1,2-Tetrachloroethane
0.0219
0.0020
mg/Kg wet
0.0200
109
70-130
1,1,2,2-Tetrachloroethane
0.0165
0.0020
mg/Kg wet
0.0200
82.7
70-130
Tetrachloroethylene
0.0193
0.0020
mg/Kg wet
0.0200
96.5
70-130
Tetrahydrofuran
0.0166
0.010
mg/Kg wet
0.0200
83.1
70-130
Toluene
0.0178
0.0020
mg/Kg wet
0.0200
89.2
70-130
1,2,3-Trichlorobenzene
0.0177
0.0020
mg/Kg wet
0.0200
88.3
70-130
1,2,4-Trichlorobenzene
0.0184
0.0020
mg/Kg wet
0.0200
92.0
70-130
1,3,5-Trichlorobenzene
0.0184
0.0020
mg/Kg wet
0.0200
92.2
70-130
1, 1, 1 -Trichloroethane
0.0241
0.0020
mg/Kg wet
0.0200
120
70-130
1,1,2-Trichloroethane
0.0185
0.0020
mg/Kg wet
0.0200
92.3
70-130
Trichloroethylene
0.0195
0.0020
mg/Kg wet
0.0200
97.7
70-130
Trichlorofluoromethane (Freon 11)
0.0210
0.010
mg/Kg wet
0.0200
105
70-130
1,2,3-Trichloropropane
0.0173
0.0020
mg/Kg wet
0.0200
86.3
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0206
0.010
mg/Kg wet
0.0200
103
70-130
113)
1,2,4-Trimethylbenzene
0.0192
0.0020
mg/Kg wet
0.0200
95.8
70-130
1,3,5-Trimethylbenzene
0.0203
0.0020
mg/Kg wet
0.0200
101
70-130
Vinyl Chloride
0.0143
0.010
mg/Kg wet
0,0200
71.4
40-130
J f
J
t
t
J t
t
t
Page 37 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218864 - SW-846 5035
LCS (B218864-BSI)
Prepared & Analyzed: 12/10/18
m+p Xylene
0.0388
0.0040
mg/Kg wet
0.0400
97.0
70-130
o-Xylene
0.0191
0.0020
mg/Kg wet
0.0200
95.6
70-130
Surrogate:l,2-Dichloroethane-d4
0.0558
mg/Kg wet
0.0500
112
70-130
Surrogate: Toluene-d8
0.0484
mg/Kg wet
0.0500
96.7
70-130
Surrogate:4-Bromofluorobenzene
0.0530
mg/Kg wet
0.0500
106
70-130
LCS Dup (B218864-BSD1)
Prepared & Analyzed: 12/10/18
Acetone
0.289
0.10
mg/Kg wet
0.200
144
70-160
38.0
* 25
R-05 t
Acrylonitrile
0.0181
0.0060
mg/Kg wet
0.0200
90.6
70-130
7.49
25
tert-Amyl Methyl Ether (TAME)
0.0193
0.0010
mg/Kg wet
0.0200
96.6
70-130
1.88
25
Benzene
0.0180
0.0020
mg/Kg wet
0.0200
90.0
70-130
1.73
25
Bromobenzene
0.0174
0.0020
mg/Kg wet
0.0200
86.9
70-130
3.01
25
Bromochloromethane
0.0178
0.0020
mg/Kg wet
0.0200
88.9
70-130
8.49
25
Bromodichloromethane
0.0202
0.0020
mg/Kg wet
0.0200
101
70-130
3.49
25
Bromoform
0.0186
0.0020
mg/Kg wet
0.0200
92.8
70-130
11.5
25
Bromomethane
0.0134
0.010
mg/Kg wet
0.0200
66.9
40-130
7.35
25
f
2-Butanone (MEK)
0.214
0.040
mg/Kg wet
0.200
107
70-160
21.1
25
t
tert-Butyl Alcohol (TBA)
0.189
0.040
mg/Kg wet
0.200
94.4
40-130
4.76
25
t
n-Butylbenzene
0.0177
0.0020
mg/Kg wet
0.0200
88.6
70-130
4.64
25
sec-Butylbenzene
0.0184
0.0020
mg/Kg wet
0.0200
92.1
70-130
4.88
25
tert-Butylbenzene
0.0184
0.0020
mg/Kg wet
0.0200
92.2
70-160
7.67
25
t
tert-Butyl Ethyl Ether (TBEE)
0.0191
0.0010
mg/Kg wet
0.0200
95.4
70-130
1.72
25
Carbon Disulfide
0.0186
0.0060
mg/Kg wet
0.0200
92.8
70-130
6.49
25
Carbon Tetrachloride
0.0242
0.0020
mg/Kg wet
0.0200
121
70-130
3.82
25
Chlorobenzene
0.0177
0.0020
mg/Kg wet
0.0200
88.4
70-130
7.16
25
Chlorodibromomethane
0.0224
0.0010
mg/Kg wet
0.0200
112
70-130
0.561
25
Chloroethane
0.0186
0.020
mg/Kg wet
0.0200
92.9
70-130
2.20
25
J
Chloroform
0.0204
0.0040
mg/Kg wet
0.0200
102
70-130
2.37
25
Chloromethane
0.0130
0.010
mg/Kg wet
0.0200
65.1
* 70-130
4.62
25
L-04
2-Chlorotoluene
0.0187
0.0020
mg/Kg wet
0.0200
93.7
70-130
2.07
25
4-Chlorotoluene
0.0200
0.0020
mg/Kg wet
0.0200
100
70-130
0.479
25
1,2-Dibromo-3-chloropropane (DBCP)
0.0195
0.0020
mg/Kg wet
0.0200
97.5
70-130
12.3
25
1,2-Dibromoethane (EDB)
0.0202
0.0010
mg/Kg wet
0.0200
101
70-130
3.62
25
Dibromomethane
0.0198
0.0020
mg/Kg wet
0.0200
99.0
70-130
4.97
25
1,2-Dichlorobenzene
0.0175
0.0020
mg/Kg wet
0.0200
87.6
70-130
5.80
25
1,3-Dichlorobenzene
0.0181
0.0020
mg/Kg wet
0.0200
90.4
70-130
6.12
25
1,4-Dichlorobenzene
0.0174
0.0020
mg/Kg wet
0.0200
87.2
70-130
3.78
25
trans-1,4-Dichloro-2-butene
0.0194
0.0040
mg/Kg wet
0.0200
97.0
70-130
6.49
25
Dichlorodifluoromethane (Freon 12)
0.0120
0.020
mg/Kg wet
0.0200
60.1
40-160
2.27
25
J t
1, 1 -Dichloroethane
0.0189
0.0020
mg/Kg wet
0.0200
94.3
70-130
1.04
25
1,2-Dichloroethane
0.0227
0.0020
mg/Kg wet
0.0200
114
70-130
3.39
25
1,1-Dichloroethylene
0.0198
0.0040
mg/Kg wet
0.0200
99.2
70-130
1.87
25
cis-1,2-Dichloroethylene
0.0200
0.0020
mg/Kg wet
0.0200
100
70-130
3.82
25
trans-1,2-Dichloroethylene
0.0182
0.0020
mg/Kg wet
0.0200
90.8
70-130
3.02
25
1,2-Dichloropropane
0.0156
0.0020
mg/Kg wet
0.0200
78.0
70-130
3.33
25
1,3-Dichloropropane
0.0172
0.0010
mg/Kg wet
0.0200
85.8
70-130
0.105
25
2,2-Dichloropropane
0.0251
0.0020
mg/Kg wet
0.0200
126
70-130
0.0716
25
1,1-Dichloropropene
0.0196
0.0020
mg/Kg wet
0.0200
98.0
70-130
6.62
25
cis-1,3-Dichloropropene
0.0186
0.0010
mg/Kg wet
0.0200
93.1
70-130
0.279
25
trans-1,3-Dichloropropene
0.0215
0.0010
mg/Kg wet
0.0200
107
70-130
0.102
25
Diethyl Ether
0.0166
0.020
mg/Kg wet
0.0200
83.2
70-130
1.40
25
1
Diisopropyl Ether (DIPE)
0.0161
0.0010
mg/Kg wet
0.0200
80.7
70-130
0.235
25
Page 38 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218864 - SW-846 5035
LCS Dup (B218864-BSD1)
Prepared & Analyzed: 12/10/18
1,4-Dioxane
0.170
0.10
mg/Kg wet
0.200
85.2
40-160
1.49
50
f #
Ethylbenzene
0.0177
0.0020
mg/Kg wet
0.0200
88.6
70-130
5.96
25
Hexachlorobutadiene
0.0198
0.0020
mg/Kg wet
0.0200
99.1
70-160
0.754
25
2-Hexanone (MBK)
0.181
0.020
mg/Kg wet
0.200
90.4
70-160
20.7
25
f
Isopropylbenzene (Cumene)
0.0194
0.0020
mg/Kg wet
0.0200
96.9
70-130
5.01
25
p-Isopropyltoluene (p-Cymene)
0.0180
0.0020
mg/Kg wet
0.0200
90.2
70-130
4.20
25
Methyl tert-Butyl Ether (MTBE)
0.0215
0.0040
mg/Kg wet
0.0200
107
70-130
0.785
25
Methylene Chloride
0.0138
0.020
mg/Kg wet
0.0200
69.1
40-160
17.9
25
J t
4-Methyl-2-pentanone (MIBK)
0.162
0.020
mg/Kg wet
0.200
81.1
70-160
0.159
25
t
Naphthalene
0.0170
0.0040
mg/Kg wet
0.0200
84.8
40-130
2.95
25
f
n-Propylbenzene
0.0185
0.0020
mg/Kg wet
0.0200
92.4
70-130
3.19
25
Styrene
0.0174
0.0020
mg/Kg wet
0.0200
86.9
70-130
6.19
25
1, 1, 1,2-Tetrachloroethane
0.0201
0.0020
mg/Kg wet
0.0200
101
70-130
8.31
25
1,1,2,2-Tetrachloroethane
0.0153
0.0020
mg/Kg wet
0.0200
76.6
70-130
7.62
25
Tetrachloroethylene
0.0190
0.0020
mg/Kg wet
0.0200
94.8
70-130
1.72
25
Tetrahydroforan
0.0157
0.010
mg/Kg wet
0.0200
78.3
70-130
6.03
25
Toluene
0.0175
0.0020
mg/Kg wet
0.0200
87.3
70-130
2.09
25
1,2,3-Trichlorobenzene
0.0169
0.0020
mg/Kg wet
0.0200
84.3
70-130
4.66
25
1,2,4-Trichlorobenzene
0.0176
0.0020
mg/Kg wet
0.0200
88.0
70-130
4.37
25
1,3,5-Trichlorobenzene
0.0183
0.0020
mg/Kg wet
0.0200
91.5
70-130
0.719
25
1, 1, 1 -Trichloroethane
0.0237
0.0020
mg/Kg wet
0.0200
119
70-130
1.48
25
1,1,2-Trichloroethane
0.0196
0.0020
mg/Kg wet
0.0200
98.2
70-130
6.18
25
Trichloroethylene
0.0200
0.0020
mg/Kg wet
0.0200
99.8
70-130
2.16
25
Trichlorofluoromethane (Freon 11)
0.0203
0.010
mg/Kg wet
0.0200
101
70-130
3.42
25
1,2,3-Trichloropropane
0.0165
0.0020
mg/Kg wet
0.0200
82.4
70-130
4.67
25
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0201
0.010
mg/Kg wet
0.0200
101
70-130
2.54
25
113)
1,2,4-Trimethylbenzene
0.0182
0.0020
mg/Kg wet
0.0200
91.2
70-130
4.88
25
1,3,5-Trimethylbenzene
0.0199
0.0020
mg/Kg wet
0.0200
99.3
70-130
2.15
25
Vinyl Chloride
0.0140
0.010
mg/Kg wet
0.0200
69.9
40-130
2.12
25
t
m+p Xylene
0.0369
0.0040
mg/Kg wet
0.0400
92.3
70-130
4.98
25
o-Xylene
0.0184
0.0020
mg/Kg wet
0.0200
92.0
70-130
3.89
25
Surrogate:l,2-Dichloroethane-d4
0.0573
mg/Kg wet
0.0500
115
70-130
Surrogate: Toluene-d8
0.0500
mg/Kg wet
0.0500
100
70-130
Surrogate:4-Bromofluorobenzene
0.0537
mg/Kg wet
0.0500
107
70-130
Page 39 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218913 - SW-846 3546
Blank (B218913-BLK1) Prepared: 12/10/18 Analyzed: 12/11/18
Acenaphthene
ND
0.17
mg/Kg wet
Acenaphthylene
ND
0.17
mg/Kg wet
Acetophenone
ND
0.34
mg/Kg wet
Aniline
ND
0.34
mg/Kg wet
Anthracene
ND
0.17
mg/Kg wet
Benzidine
ND
0.66
mg/Kg wet
Benzo(a)anthracene
ND
0.17
mg/Kg wet
Benzo(a)pyrene
ND
0.17
mg/Kg wet
Benzo(b)fluoranthene
ND
0.17
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.17
mg/Kg wet
Benzo(b)fluoranthene
ND
0.17
mg/Kg wet
Benzoic Acid
ND
1.0
mg/Kg wet
Bis(2-chloroethoxy)methane
ND
0.34
mg/Kg wet
Bis(2-chloroethyl)ether
ND
0.34
mg/Kg wet
Bis(2-chloroisopropyl)ether
ND
0.34
mg/Kg wet
Bis(2-Ethylhexyl)phthalate
ND
0.34
mg/Kg wet
4-Bromophenylphenylether
ND
0.34
mg/Kg wet
Butylbenzylphthalate
ND
0.34
mg/Kg wet
Carbazole
ND
0.17
mg/Kg wet
4-Chloroaniline
ND
0.66
mg/Kg wet
4-Chloro-3-methylphenol
ND
0.66
mg/Kg wet
2-Chloronaphthalene
ND
0.34
mg/Kg wet
2-Chlorophenol
ND
0.34
mg/Kg wet
4-Chlorophenylphenylether
ND
0.34
mg/Kg wet
Chrysene
ND
0.17
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.17
mg/Kg wet
Dibenzofuran
ND
0.34
mg/Kg wet
Di-n-butylphthalate
ND
0.34
mg/Kg wet
1,2-Dichlorobenzene
ND
0.34
mg/Kg wet
1,3-Dichlorobenzene
ND
0.34
mg/Kg wet
1,4-Dichlorobenzene
ND
0.34
mg/Kg wet
3,3-Dichlorobenzidine
ND
0.17
mg/Kg wet
2,4-Dichlorophenol
ND
0.34
mg/Kg wet
Diethylphthalate
ND
0.34
mg/Kg wet
2,4-Dimethylphenol
ND
0.34
mg/Kg wet
Dimethylphthalate
ND
0.34
mg/Kg wet
4,6-Dinitro-2-methylphenol
ND
0.34
mg/Kg wet
2,4-Dinitrophenol
ND
0.66
mg/Kg wet
2,4-Dinitrotoluene
ND
0.34
mg/Kg wet
2,6-Dinitrotoluene
ND
0.34
mg/Kg wet
Di-n-octylphthalate
ND
0.34
mg/Kg wet
1,2-Diphenylhydrazine/Azobenzene
ND
0.34
mg/Kg wet
Fluoranthene
ND
0.17
mg/Kg wet
Fluorene
ND
0.17
mg/Kg wet
Hexachlorobenzene
ND
0.34
mg/Kg wet
Hexachlorobutadiene
ND
0.34
mg/Kg wet
Hexachlorocyclopentadiene
ND
0.34
mg/Kg wet
Hexachloroethane
ND
0.34
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.17
mg/Kg wet
Isophorone
ND
0.34
mg/Kg wet
1-Methylnaphthalene
ND
0.17
mg/Kg wet
2-Methylnaphthalene
ND
0.17
mg/Kg wet
V-04
V-05, V-04
V-05
V-34
R-05
V-05
Page 40 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218913 - SW-846 3546
Blank (B218913-BLK1)
Prepared: 12/10/18 Analyzed: 12/11/18
2-Methylphenol
ND
0.34
mg/Kg wet
3/4-Methylphenol
ND
0.34
mg/Kg wet
Naphthalene
ND
0.17
mg/Kg wet
2-Nitroaniline
ND
0.34
mg/Kg wet
3-Nitroaniline
ND
0.34
mg/Kg wet
4-Nitroaniline
ND
0.34
mg/Kg wet
Nitrobenzene
ND
0.34
mg/Kg wet
V-05
2-Nitrophenol
ND
0.34
mg/Kg wet
4-Nitrophenol
ND
0.66
mg/Kg wet
N-Nitrosodimethylamine
ND
0.34
mg/Kg wet
V-05
N-Nitrosodiphenylamine/Diphenylamine
ND
0.34
mg/Kg wet
N-Nitrosodi-n-propylamine
ND
0.34
mg/Kg wet
Pentachloronitrobenzene
ND
0.34
mg/Kg wet
Pentachlorophenol
ND
0.34
mg/Kg wet
Phenanthrene
ND
0.17
mg/Kg wet
Phenol
ND
0.34
mg/Kg wet
Pyrene
ND
0.17
mg/Kg wet
Pyridine
ND
0.34
mg/Kg wet
V-05
1,2,4,5-Tetrachlorobenzene
ND
0.34
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.34
mg/Kg wet
2,4,5-Trichlorophenol
ND
0.34
mg/Kg wet
2,4,6-Trichlorophenol
ND
0.34
mg/Kg wet
Surrogate:2-Fluorophenol
5.44
mg/Kg wet
6.67
81.6
30-130
Surrogate: Phenol-d6
5.71
mg/Kg wet
6.67
85.6
30-130
Surrogate: Nitrobenzene-d5
3.12
mg/Kg wet
3.33
93.5
30-130
Surrogate:2-Fluorobiphenyl
2.37
mg/Kg wet
3.33
71.0
30-130
Surrogate: 2,4,6-Tribromophenol
6.58
mg/Kg wet
6.67
98.7
30-130
Surrogate: p-Terphenyl-dl4
3.01
mg/Kg wet
3.33
90.3
30-130
LCS (B218913-BS1)
Prepared: 12/10/18 Analyzed: 12/11/18
Acenaphthene
1.37
0.17
mg/Kg wet
1.67
82.1
40-140
Acenaphthylene
1.42
0.17
mg/Kg wet
1.67
85.0
40-140
Acetophenone
1.39
0.34
mg/Kg wet
1.67
83.5
40-140
Aniline
1.11
0.34
mg/Kg wet
1.67
66.5
10-140
V-04 t
Anthracene
1.46
0.17
mg/Kg wet
1.67
87.6
40-140
Benzidine
1.29
0.66
mg/Kg wet
1.67
77.4
40-140
V-04,V-05
Benzo(a)anthracene
1.45
0.17
mg/Kg wet
1.67
87.0
40-140
Benzo(a)pyrene
1.53
0.17
mg/Kg wet
1.67
91.8
40-140
Benzo(b)fluoranthene
1.88
0.17
mg/Kg wet
1.67
113
40-140
Benzo(g,h,i)perylene
1.26
0.17
mg/Kg wet
1.67
75.4
40-140
V-05
Benzo(k)fluoranthene
1.80
0.17
mg/Kg wet
1.67
108
40-140
Benzoic Acid
1.49
1.0
mg/Kg wet
1.67
89.3
30-130
Bis(2-chloroethoxy)methane
1.62
0.34
mg/Kg wet
1.67
97.4
40-140
Bis(2-chloroethyl)ether
1.41
0.34
mg/Kg wet
1.67
84.5
40-140
Bis(2-chloroisopropyl)ether
1.74
0.34
mg/Kg wet
1.67
104
40-140
Bis(2-Ethylhexyl)phthalate
1.46
0.34
mg/Kg wet
1.67
87.6
40-140
4-Bromophenylphenylether
1.45
0.34
mg/Kg wet
1.67
87.1
40-140
Butylbenzylphthalate
1.63
0.34
mg/Kg wet
1.67
97.8
40-140
Carbazole
1.42
0.17
mg/Kg wet
1.67
85.0
40-140
4-Chloroaniline
0.933
0.66
mg/Kg wet
1.67
56.0
10-140
V-34
4-Chloro-3-methylphenol
1.53
0.66
mg/Kg wet
1.67
91.6
30-130
2-Chloronaphthalene
1.20
0.34
mg/Kg wet
1.67
72.1
40-140
Page 41 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218913 - SW-846 3546
LCS (B218913-BSI) Prepared: 12/10/18 Analyzed: 12/11/18
2-Chlorophenol
1.34
0.34
mg/Kg wet
1.67
80.3
30-130
4-Chlorophenylphenylether
1.47
0.34
mg/Kg wet
1.67
88.1
40-140
Chrysene
1.30
0.17
mg/Kg wet
1.67
78.2
40-140
Dibenz(a,h)anthracene
1.22
0.17
mg/Kg wet
1.67
73.1
40-140
Dibenzofuran
1.48
0.34
mg/Kg wet
1.67
88.7
40-140
Di-n-butylphthalate
1.43
0.34
mg/Kg wet
1.67
85.9
40-140
1,2-Dichlorobenzene
1.27
0.34
mg/Kg wet
1.67
76.1
40-140
1,3-Dichlorobenzene
1.23
0.34
mg/Kg wet
1.67
73.8
40-140
1,4-Dichlorobenzene
1.25
0.34
mg/Kg wet
1.67
75.0
40-140
3,3-Dichlorobenzidine
1.23
0.17
mg/Kg wet
1.67
73.6
20-140
t
2,4-Dichlorophenol
1.47
0.34
mg/Kg wet
1.67
88.2
30-130
Diethylphthalate
1.45
0.34
mg/Kg wet
1.67
86.8
40-140
2,4-Dimethylphenol
1.41
0.34
mg/Kg wet
1.67
84.6
30-130
Dimethylphthalate
1.43
0.34
mg/Kg wet
1.67
85.9
40-140
4,6-Dinitro-2-methylphenol
1.62
0.34
mg/Kg wet
1.67
97.3
30-130
2,4-Dinitrophenol
1.48
0.66
mg/Kg wet
1.67
88.8
30-130
2,4-Dinitrotoluene
1.67
0.34
mg/Kg wet
1.67
100
40-140
2,6-Dinitrotoluene
1.70
0.34
mg/Kg wet
1.67
102
40-140
Di-n-octylphthalate
2.09
0.34
mg/Kg wet
1.67
125
40-140
R-05
1,2-Diphenylhydrazine/Azobenzene
1.44
0.34
mg/Kg wet
1.67
86.3
40-140
Fluoranthene
1.41
0.17
mg/Kg wet
1.67
84.8
40-140
Fluorene
1.43
0.17
mg/Kg wet
1.67
85.7
40-140
Hexachlorobenzene
1.41
0.34
mg/Kg wet
1.67
84.8
40-140
Hexachlorobutadiene
1.32
0.34
mg/Kg wet
1.67
78.9
40-140
Hexachlorocyclopentadiene
0.793
0.34
mg/Kg wet
1.67
47.6
40-140
V-05
Hexachloroethane
1.26
0.34
mg/Kg wet
1.67
75.4
40-140
Indeno(1,2,3-cd)pyrene
1.32
0.17
mg/Kg wet
1.67
79.3
40-140
Isophorone
1.53
0.34
mg/Kg wet
1.67
91.6
40-140
1-Methylnaphthalene
1.35
0.17
mg/Kg wet
1.67
81.1
40-140
2-Methylnaphthalene
1.53
0.17
mg/Kg wet
1.67
91.6
40-140
2-Methylphenol
1.47
0.34
mg/Kg wet
1.67
87.9
30-130
3/4-Methylphenol
1.44
0.34
mg/Kg wet
1.67
86.7
30-130
Naphthalene
1.35
0.17
mg/Kg wet
1.67
81.1
40-140
2-Nitroaniline
1.60
0.34
mg/Kg wet
1.67
95.7
40-140
3-Nitroaniline
1.35
0.34
mg/Kg wet
1.67
80.8
30-140
t
4-Nitroaniline
1.59
0.34
mg/Kg wet
1.67
95.4
40-140
Nitrobenzene
1.41
0.34
mg/Kg wet
1.67
84.8
40-140
V-05
2-Nitrophenol
1.64
0.34
mg/Kg wet
1.67
98.2
30-130
4-Nitrophenol
1.58
0.66
mg/Kg wet
1.67
94.5
30-130
N-Nitrosodimethylamine
0.784
0.34
mg/Kg wet
1.67
47.0
40-140
V-05
N-Nitrosodiphenylamine/Diphenylamine
1.48
0.34
mg/Kg wet
1.67
88.7
40-140
N-Nitrosodi-n-propylamine
1.36
0.34
mg/Kg wet
1.67
81.6
40-140
Pentachloronitrobenzene
1.60
0.34
mg/Kg wet
1.67
95.7
40-140
Pentachlorophenol
1.31
0.34
mg/Kg wet
1.67
78.4
30-130
Phenanthrene
1.46
0.17
mg/Kg wet
1.67
87.6
40-140
Phenol
1.33
0.34
mg/Kg wet
1.67
80.1
30-130
Pyrene
1.59
0.17
mg/Kg wet
1.67
95.2
40-140
Pyridine
0.587
0.34
mg/Kg wet
1.67
35.2
30-140
V-05
1,2,4,5-Tetrachlorobenzene
1.37
0.34
mg/Kg wet
1.67
82.1
40-140
1,2,4-Trichlorobenzene
1.34
0.34
mg/Kg wet
1.67
80.3
40-140
2,4,5-Trichlorophenol
1.47
0.34
mg/Kg wet
1.67
88.1
30-130
2,4,6-Trichlorophenol
1.48
0.34
mg/Kg wet
1.67
89.0
30-130
Page 42 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218913 - SW-846 3546
LCS (B218913-BSI) Prepared: 12/10/18 Analyzed: 12/11/18
Surrogate:2-Fluorophenol
5.65
mg/Kg wet
6.67
84.7
30-130
Surrogate: Phenol-d6
5.88
mg/Kg wet
6.67
88.2
30-130
Surrogate: Nitrobenzene-d5
3.10
mg/Kg wet
3.33
93.1
30-130
Surrogate:2-Fluorobiphenyl
2.48
mg/Kg wet
3.33
74.4
30-130
Surrogate: 2,4,6-Tribromophenol
6.87
mg/Kg wet
6.67
103
30-130
Surrogate:p-Terphenyl-dl4
3.18
mg/Kg wet
3.33
95.5
30-130
LCS Dup (B218913-BSD1)
Prepared: 12/10/18 Analyzed: 12/11/18
Acenaphthene
1.22
0.17
mg/Kg wet
1.67
72.9
Acenaphthylene
1.53
0.17
mg/Kg wet
1.67
91.6
Acetophenone
1.32
0.34
mg/Kg wet
1.67
79.3
Aniline
0.962
0.34
mg/Kg wet
1.67
57.7
Anthracene
1.43
0.17
mg/Kg wet
1.67
85.7
Benzidine
1.09
0.66
mg/Kg wet
1.67
65.3
Benzo(a)anthracene
1.42
0.17
mg/Kg wet
1.67
85.4
Benzo(a)pyrene
1.50
0.17
mg/Kg wet
1.67
90.0
Benzo(b)fluoranthene
1.40
0.17
mg/Kg wet
1.67
83.9
Benzo(g,h,i)perylene
1.31
0.17
mg/Kg wet
1.67
78.5
Benzo(b)fluoranthene
1.37
0.17
mg/Kg wet
1.67
82.4
Benzoic Acid
1.44
1.0
mg/Kg wet
1.67
86.5
Bis(2-chloroethoxy)methane
1.54
0.34
mg/Kg wet
1.67
92.4
Bis(2-chloroethyl)ether
1.37
0.34
mg/Kg wet
1.67
82.1
Bis(2-chloroisopropyl)ether
1.64
0.34
mg/Kg wet
1.67
98.7
Bis(2-Ethylhexyl)phthalate
1.35
0.34
mg/Kg wet
1.67
80.9
4-Bromophenylphenylether
1.39
0.34
mg/Kg wet
1.67
83.3
Butylbenzylphthalate
1.56
0.34
mg/Kg wet
1.67
93.4
Carbazole
1.35
0.17
mg/Kg wet
1.67
80.9
4-Chloroaniline
0.763
0.66
mg/Kg wet
1.67
45.8
4-Chloro-3-methylphenol
1.43
0.66
mg/Kg wet
1.67
85.9
2-Chloronaphthalene
1.32
0.34
mg/Kg wet
1.67
79.1
2-Chorophenol
1.32
0.34
mg/Kg wet
1.67
79.2
4-Chlorophenylphenylether
1.25
0.34
mg/Kg wet
1.67
74.8
Chrysene
1.32
0.17
mg/Kg wet
1.67
79.1
Dibenz(a,h)anthracene
1.20
0.17
mg/Kg wet
1.67
72.0
Dibenzofuran
1.21
0.34
mg/Kg wet
1.67
72.9
Di-n-butylphthalate
1.37
0.34
mg/Kg wet
1.67
82.4
1,2-Dichlorobenzene
1.23
0.34
mg/Kg wet
1.67
73.8
1,3-Dichlorobenzene
1.20
0.34
mg/Kg wet
1.67
72.0
1,4-Dichlorobenzene
1.21
0.34
mg/Kg wet
1.67
72.5
3,3-Dichlorobenzidine
1.17
0.17
mg/Kg wet
1.67
70.4
2,4-Dichlorophenol
1.45
0.34
mg/Kg wet
1.67
87.1
Diethylphthalate
1.20
0.34
mg/Kg wet
1.67
71.9
2,4-Dimethylphenol
1.39
0.34
mg/Kg wet
1.67
83.1
Dimethylphthalate
1.56
0.34
mg/Kg wet
1.67
93.6
4,6-Dinitro-2-methylphenol
1.59
0.34
mg/Kg wet
1.67
95.6
2,4-Dinitrophenol
1.29
0.66
mg/Kg wet
1.67
77.5
2,4-Dinitrotoluene
1.36
0.34
mg/Kg wet
1.67
81.5
2,6-Dinitrotoluene
1.81
0.34
mg/Kg wet
1.67
109
Di-n-octylphthalate
1.42
0.34
mg/Kg wet
1.67
85.3
1,2-Diphenylhydrazine/Azobenzene
1.35
0.34
mg/Kg wet
1.67
80.9
Fluoranthene
1.37
0.17
mg/Kg wet
1.67
82.0
Fluorene
1.21
0.17
mg/Kg wet
1.67
72.4
40-140
11.8
30
40-140
7.47
30
40-140
5.09
30
10-140
14.2
50
V-04
t #
40-140
2.26
30
40-140
17.0
30
V-04, V-05
40-140
1.86
30
40-140
2.02
30
40-140
29.1
30
40-140
4.06
30
V-05
40-140
27.1
30
30-130
3.19
50
$
40-140
5.31
30
40-140
2.83
30
40-140
5.44
30
40-140
7.88
30
40-140
4.44
30
40-140
4.66
30
40-140
4.92
30
10-140
20.1
30
V-34
t
30-130
6.35
30
40-140
9.18
30
30-130
1.35
30
40-140
16.2
30
40-140
1.17
30
40-140
1.49
30
40-140
19.6
30
40-140
4.16
30
40-140
3.02
30
40-140
2.47
30
40-140
3.42
30
20-140
4.47
50
t #
30-130
1.19
30
40-140
18.8
30
30-130
1.69
30
40-140
8.63
30
30-130
1.74
30
30-130
13.5
30
40-140
20.3
30
40-140
6.31
30
40-140
38.1
* 30
R-05
40-140
6.44
30
40-140
3.40
30
40-140
16.8
30
Page 43 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218913 - SW-846 3546
LCS Dup (B218913-BSD1) Prepared: 12/10/18 Analyzed: 12/11/18
Hexachlorobenzene
1.43
0.34
mg/Kg wet
1.67
85.6
40-140
0.962
30
Hexachlorobutadiene
1.28
0.34
mg/Kg wet
1.67
76.9
40-140
2.62
30
Hexachlorocyclopentadiene
0.888
0.34
mg/Kg wet
1.67
53.3
40-140
11.3
30
V-05
Hexachloroethane
1.23
0.34
mg/Kg wet
1.67
73.6
40-140
2.39
30
Indeno(1,2,3-cd)pyrene
1.34
0.17
mg/Kg wet
1.67
80.4
40-140
1.33
30
Isophorone
1.46
0.34
mg/Kg wet
1.67
87.4
40-140
4.74
30
I-Methylnaphthalene
1.28
0.17
mg/Kg wet
1.67
76.6
40-140
5.81
30
2-Methylnaphthalene
1.43
0.17
mg/Kg wet
1.67
85.6
40-140
6.75
30
2-Methylphenol
1.39
0.34
mg/Kg wet
1.67
83.2
30-130
5.56
30
3/4-Methylphenol
1.34
0.34
mg/Kg wet
1.67
80.5
30-130
7.42
30
Naphthalene
1.34
0.17
mg/Kg wet
1.67
80.3
40-140
0.942
30
2-Nitroanihne
1.74
0.34
mg/Kg wet
1.67
105
40-140
8.94
30
3-Nitroaniline
1.30
0.34
mg/Kg wet
1.67
77.8
30-140
3.76
30
f
4-Nitroaniline
1.31
0.34
mg/Kg wet
1.67
78.4
40-140
19.5
30
Nitrobenzene
1.33
0.34
mg/Kg wet
1.67
79.5
40-140
6.40
30
V-05
2-Nitrophenol
1.59
0.34
mg/Kg wet
1.67
95.3
30-130
2.94
30
4-Nitrophenol
1.31
0.66
mg/Kg wet
1.67
78.8
30-130
18.1
50
$
N-Nitrosodimethylamine
0.947
0.34
mg/Kg wet
1.67
56.8
40-140
18.8
30
V-05
N-Nitrosodiphenylamine/Diphenylamine
1.46
0.34
mg/Kg wet
1.67
87.3
40-140
1.57
30
N-Nitrosodi-n-propylamine
1.30
0.34
mg/Kg wet
1.67
78.2
40-140
4.23
30
Pentachloronitrobenzene
1.62
0.34
mg/Kg wet
1.67
97.0
40-140
1.35
30
Pentachlorophenol
1.26
0.34
mg/Kg wet
1.67
75.5
30-130
3.77
30
Phenanthrene
1.40
0.17
mg/Kg wet
1.67
83.8
40-140
4.48
30
Phenol
1.31
0.34
mg/Kg wet
1.67
78.5
30-130
1.99
30
Pyrene
1.49
0.17
mg/Kg wet
1.67
89.3
40-140
6.35
30
Pyridine
0.651
0.34
mg/Kg wet
1.67
39.1
30-140
10.3
30
V-05 t
1,2,4,5-Tetrachlorobenzene
1.54
0.34
mg/Kg wet
1.67
92.2
40-140
11.5
30
1,2,4-Trichlorobenzene
1.34
0.34
mg/Kg wet
1.67
80.4
40-140
0.124
30
2,4,5-Trichlorophenol
1.98
0.34
mg/Kg wet
1.67
95.0
30-130
7.62
30
2,4,6-Trichlorophenol
1.61
0.34
mg/Kg wet
1.67
96.8
30-130
8.48
30
Surrogate: 2-Fluorophenol
5.56
mg/Kg wet
6.67
83.3
30-130
Surrogate: Phenol-d6
5.70
mg/Kg wet
6.67
85.5
30-130
Surrogate: Nitrobenzene-d5
2.94
mg/Kg wet
3.33
88.2
30-130
Surrogate:2-Fluorobiphenyl
2.71
mg/Kg wet
3.33
81.2
30-130
Surrogate: 2,4,6-Tribromophenol
6.05
mg/Kg wet
6.67
90.7
30-130
Surrogate:p-Terphenyl-dl4
3.01
mg/Kg wet
3.33
90.3
30-130
Page 44 of 68

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218953 - SW-846 3050B
Blank (B218953-BLK1)
Prepared: 12/11/18 Analyzed: 12/12/18
Arsenic
ND
0.17
mg/Kg wet
Chromium
ND
4.2
mg/Kg wet
Lead
ND
1.7
mg/Kg wet
Selenium
ND
0.70
mg/Kg wet
Silver
ND
0.073
mg/Kg wet
Barium
ND
8.3
mg/Kg wet
Cadmium
ND
0.32
mg/Kg wet
LCS (B218953-BS1)
Prepared: 12/11/18 Analyzed: 12/12/18
Arsenic
203
2.0
mg/Kg wet
202 101 82.7-117.3
Chromium
174
50
mg/Kg wet
167 104 81.4-118
Lead
77.5
20
mg/Kg wet
73.8 105 82.9-117.1
Selenium
50.4
8.3
mg/Kg wet
49.9 101 79.2-120.6
Silver
71.9
0.87
mg/Kg wet
71.1 101 79.7-120.1
Barium
277
99
mg/Kg wet
270 102 82.6-117.8
Cadmium
141
3.8
mg/Kg wet
141 99.8 83-117
LCS Dup (B218953-BSD1)
Prepared: 12/11/18 Analyzed: 12/12/18
Arsenic
202
2.0
mg/Kgwet
202 100 82.7-117.3
0.303
30
Chromium
173
49
mg/Kg wet
167 104 81.4-118
0.798
30
Lead
78.2
20
mg/Kg wet
73.8 106 82.9-117.1
0.893
30
Selenium
49.9
8.3
mg/Kg wet
49.9 99.9 79.2-120.6
1.19
30
Silver
72.4
0.87
mg/Kg wet
71.1 102 79.7-120.1
0.671
30
Barium
277
99
mg/Kg wet
270 103 82.6-117.8
0.203
30
Cadmium
139
3.8
mg/Kgwet
141 98.4 83-117
1.42
30
Duplicate (B218953-DUPI)
Source: 18LO295-01
Prepared: 12/11/18 Analyzed: 12/12/18
Arsenic
0.626
0.20
mg/Kg dry
0.630
0.577
35
Chromium
20.2
5.1
mg/Kg dry
21.6
6.85
35
Lead
5.37
2.0
mg/Kg dry
5.35
0.360
35
Selenium
0.0842
0.85
mg/Kg dry
ND
NC
35 J
Silver
0.0208
0.089
mg/Kg dry
0.0216
3.71
35 J
Barium
20.6
10
mg/Kg dry
21.5
4.50
35
Cadmium
ND
0.38
mg/Kg dry
ND
NC
35
Matrix Spike (B218953-MS1)
Source: 18LO295-01
Prepared: 12/11/18 Analyzed: 12/12/18
Arsenic
18.5
0.82
mg/Kg dry
20.4 0.630 87.4 75-125
Chromium
43.8
20
mg/Kg dry
20.4 21.6 108 75-125
Lead
27.0
8.2
mg/Kg dry
20.4 5.35 106 75-125
Selenium
17.3
3.4
mg/Kg dry
20.4 ND 84.6 75-125
Silver
20.1
0.36
mg/Kg dry
20.4 ND 98.5 75-125
Barium
43.4
41
mg/Kg dry
20.4 21.5 107 75-125
Cadmium
20.6
1.6
mg/Kg dry
20.4 ND 101 75-125
Page 45 of 68

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B219056 - SW-846 7471
Blank (B219056-BLK1) Prepared & Analyzed: 12/12/18
Mercury ND 0.025 mg/Kg wet
LCS (B219056-BS1) Prepared & Analyzed: 12/12/18
Mercury 4.27 0.39 mg/Kgwet 3.71 115 65-135
LCS Dup (B219056-BSD1) Prepared & Analyzed: 12/12/18
Mercury 3.29 0.38 mg/Kg wet 3.71 88.6 65-135 25.9 30
Page 46 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
fi Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-07A Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for
this compound.
R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
5-17 Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less
than the reporting limit and bias is on the high side.
V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound.
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
Page 47 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 6020B in Soil
Arsenic
NY,VA,NH,NC,ME
Chromium
NY,NC,ME
Lead
NY,NC,ME
Selenium
NY,VA,NH,NC,ME
Silver
NY,NC,ME
Barium
NY,NC
Cadmium
NY,NC,ME
SW-846 7470A in Water
Mercury
CT,NH,NY,NC,ME,VA
SW-846 7471B in Soil
Mercury
CT,NH,NY,NC,ME,VA
SW-846 8260B in Soil
Acetone
NC
Acrylonitrile
NC
tert-Amyl Methyl Ether (TAME)
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Bromoform
NC
Bromomethane
NC
2-Butanone (MEK)
NC
tert-Butyl Alcohol (TBA)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
tert-Butyl Ethyl Ether (TBEE)
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromo-3-chloropropane (DBCP)
NC
1,2-Dibromoethane (EDB)
NC
Dibromomethane
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
trans-1,4-Dichloro-2-butene
NC
Dichlorodifluoromethane (Freon 12)
NC
1,1-Dichloroethane
NC
1,2-Dichloroethane
NC
Page 48 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
SW-846 8260B in Soil
1,1-Dichloroethylene
cis-1,2-Dichloroethylene
trans- l,2-Dichloro ethylene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3 -Dichloropropene
trans- 1, 3 -Dichloropropene
Diethyl Ether
Diisopropyl Ether (DIPE)
1,4-Dioxane
Ethylbenzene
Hexachlorobutadiene
2-Hexanone (MBK)
Isopropylbenzene (Cumene)
p-Isopropyltoluene (p-Cymene)
Methyl tert-Butyl Ether (MTBE)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethylene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethylene
Trichlorofluoromethane (Freon 11)
1,2,3-Trichloropropane
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Chloride
m+p Xylene
o-Xylene
SW-846 8270D in Soil
Acenaphthene
Acenaphthylene
Acetophenone
Certifications
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
NY,NH,ME,NC,VA
Page 49 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Soil
Aniline
NY,NH,ME,NC,VA
Anthracene
CT,NY,NH,ME,NC,VA
Benzidine
CT,NY,NH,ME,NC,VA
Benzo(a)anthracene
CT,NY,NH,ME,NC,VA
Benzo(a)pyrene
CT,NY,NH,ME,NC,VA
Benzo(b)fluoranthene
CT,NY,NH,ME,NC,VA
Benzo(g,h,i)perylene
CT,NY,NH,ME,NC,VA
Benzo(k)fluoranthene
CT,NY,NH,ME,NC,VA
Benzoic Acid
NY,NH,ME,NC,VA
Bis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VA
Bis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VA
Bis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VA
Bis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA
4-Bromophenylphenylether
CT,NY,NH,ME,NC,VA
Butylbenzylphthalate
CT,NY,NH,ME,NC,VA
Carbazole
NC
4-Chloroaniline
CT,NY,NH,ME,NC,VA
4-Chloro-3-methylphenol
CT,NY,NH,ME,NC,VA
2-Chloronaphthalene
CT,NY,NH,NC,VA
2-Chlorophenol
CT,NY,NH,ME,NC,VA
4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VA
Chrysene
CT,NY,NH,ME,NC,VA
Dibenz(a,h)anthracene
CT,NY,NH,ME,NC,VA
Dibenzofuran
CT,NY,NH,ME,NC,VA
Di-n-butylphthalate
CT,NY,NH,ME,NC,VA
1,2-Dichlorobenzene
NY,NH,ME,NC,VA
1,3-Dichlorobenzene
NY,NH,ME,NC,VA
1,4-Dichlorobenzene
NY,NH,ME,NC,VA
3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA
2,4-Dichlorophenol
CT,NY,NH,ME,NC,VA
Diethylphthalate
CT,NY,NH,ME,NC,VA
2,4-Dimethylphenol
CT,NY,NH,ME,NC,VA
Dimethylphthalate
CT,NY,NH,ME,NC,VA
4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA
2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VA
Di-n-octylphthalate
CT,NY,NH,ME,NC,VA
1,2-Diphenylhydrazine/Azobenzene
NY,NH,ME,NC, VA
Fluoranthene
CT,NY,NH,ME,NC,VA
Fluorene
NY,NH,ME,NC,VA
Hexachlorobenzene
CT,NY,NH,ME,NC,VA
Hexachlorobutadiene
CT,NY,NH,ME,NC,VA
Hexachlorocyclopentadiene
CT,NY,NH,ME,NC,VA
Hexachloroethane
CT,NY,NH,ME,NC,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA
Isophorone
CT,NY,NH,ME,NC,VA
Page 50 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Soil
I -Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NH,ME,NC,VA
2-Methylphenol
CT,NY,NH,ME,NC,VA
3/4-Methylphenol
CT,NY,NH,ME,NC,VA
Naphthalene
CT,NY,NH,ME,NC,VA
2-Nitroaniline
CT,NY,NH,ME,NC,VA
3-Nitroaniline
CT,NY,NH,ME,NC,VA
4-Nitroaniline
CT,NY,NH,ME,NC,VA
Nitrobenzene
CT,NY,NH,ME,NC,VA
2-Nitrophenol
CT,NY,NH,ME,NC,VA
4-Nitrophenol
CT,NY,NH,ME,NC,VA
N-Nitrosodimethylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodi-n-propylamine
CT,NY,NH,ME,NC,VA
Pentachloronitrobenzene
NY,NC
Pentachlorophenol
CT,NY,NH,ME,NC,VA
Phenanthrene
CT,NY,NH,ME,NC,VA
Phenol
CT,NY,NH,ME,NC,VA
Pyrene
CT,NY,NH,ME,NC,VA
Pyridine
CT,NY,NH,ME,NC,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA
2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA
2,4,6-Trichlorophenol
CT,NY,NH,ME,NC,VA
2-Fluorophenol
NC
SW-846 8270D in Water
Acenaphthene
CT,NY,NC,ME,NH,VA
Acenaphthylene
CT,NY,NC,ME,NH,VA
Acetophenone
NY,NC
Aniline
CT,NY,NC,ME,VA
Anthracene
CT,NY,NC,ME,NH,VA
Benzidine
CT,NY,NC,ME,NH,VA
Benzo(a)anthracene
CT,NY NC,ME,NH,VA
Benzo(a)pyrene
CT,NY,NC,ME,NH,VA
Benzo(b)fluoranthene
CT,NY,NC,ME,NH,VA
Benzo(g,h,i)perylene
CT,NY,NC,ME,NH,VA
Benzo(k)fluoranthene
CT,NY,NC,ME,NH,VA
Benzoic Acid
NY,NC,ME,NH,VA
Bis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VA
Bis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA
4-Bromophenylphenylether
CT,NY,NC,ME,NH,VA
Butylbenzylphthalate
CT,NY,NC,ME,NH,VA
Carbazole
NC
4-Chloroaniline
CT,NY,NC,ME,NH,VA
4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA
Page 51 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Water
2-Chloronaphthalene
CT,NY,NC,ME,NH,VA
2-Chlorophenol
CT,NY NC,ME,NH,VA
4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VA
Chrysene
CT,NY,NC,ME,NH,VA
Dibenz(a,h)anthracene
CT,NY,NC,ME,NH,VA
Dibenzofuran
CT,NY,NC,ME,NH,VA
Di-n-butylphthalate
CT,NY,NC,ME,NH,VA
1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA
3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA
2,4-Dichlorophenol
CT,NY,NC,ME,NH,VA
Diethylphthalate
CT,NY,NC,ME,NH,VA
2,4-Dimethylphenol
CT,NY,NC,ME,NH,VA
Dimethylphthalate
CT,NY,NC,ME,NH,VA
4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA
2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VA
Di-n-octylphthalate
CT,NY,NC,ME,NH,VA
1,2-Diphenylhydrazine/Azobenzene
NY,NC
Fluoranthene
CT,NY,NC,ME,NH,VA
Fluorene
NY,NC,ME,NH,VA
Hexachlorobenzene
CT,NY,NC,ME,NH,VA
Hexachlorobutadiene
CT,NY,NC,ME,NH,VA
Hexachlorocyclopentadiene
CT,NY,NC,ME,NH,VA
Hexachloroethane
CT,NY,NC,ME,NH,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VA
Isophorone
CT,NY,NC,ME,NH,VA
I -Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NC,ME,NH,VA
2-Methylphenol
CT,NY,NC,NH,VA
3/4-Methylphenol
CT,NY,NC,NH,VA
Naphthalene
CT,NY,NC,ME,NH,VA
2-Nitroaniline
CT,NY,NC,ME,NH,VA
3-Nitroaniline
CT,NY,NC,ME,NH,VA
4-Nitroaniline
CT,NY,NC,ME,NH,VA
Nitrobenzene
CT,NY,NC,ME,NH,VA
2-Nitrophenol
CT,NY,NC,ME,NH,VA
4-Nitrophenol
CT,NY,NC,ME,NH,VA
N-Nitrosodimethylamine
CT,NY,NC,ME,NH,VA
N-Nitrosodi-n-propylamine
CT,NY,NC,ME,NH,VA
Pentachloronitrobenzene
NC
Pentachlorophenol
CT,NY,NC,ME,NH,VA
Phenanthrene
CT,NY,NC,ME,NH,VA
Phenol
CT,NY,NC,ME,NH,VA
Pyrene
CT,NY,NC,ME,NH,VA
Page 52 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8270D in Water
Pyridine CT,NY,NC,ME,NH,VA
1,2,4,5-Tetrachlorobenzene NY,NC
1,2,4-Trichlorobenzene CT,NY,NC,ME,NH,VA
2,4,5-Trichlorophenol CT,NY,NC,ME,NH,VA
2,4,6-Trichlorophenol CT,NY,NC,ME,NH,VA
2-Fluorophenol NC
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description
Number
Expires
AIHA AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA Massachusetts DEP
M-MAI00
06/30/2019
CT Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY New York State Department of Health
10899 NELAP
04/1/2019
NH-S New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI Rhode Island Department of Health
LA000112
12/30/2019
NC North Carolina Div. of Water Quality
652
12/31/2019
NJ New Jersey DEP
MA007 NELAP
06/30/2019
FL Florida Department of Health
E871027 NELAP
06/30/2019
VT Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME State of Maine
2011028
06/9/2019
VA Commonwealth of Virginia
460217
12/14/2019
NH-P New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW North Carolina Department of Health
25703
07/31/2019
Page 53 of 68

Table of Contents
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Table of Contents
Delivered
Friday 12/07/2018 at 9.50 am
FROM
Charlotte, NC US
Multiple -piece Shipment
DELIVERED
Signed for by B.BBCCA
GET STATUS UPDATES
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3 Piece shipment
TO
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a
TRACKING NUMBER SHIPPER CITY, STATE . ' SHIP DATE STATUS DELIVERY DATE DESTINATIONIRECIPIENT
CITY, STATE
7%3903660982 CHARIOT 1 NC 12/06/2018 12/07/2018 FAST LONG,MI AIJOW, MA
(o�tastEer j
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773903661371 CHARLOTTE, NC 12/D6/2018
Shipment Facts
TRACKING NUMBER SERVICE
173903b60982 t edFx Sta icard Overnight
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TOTAL PIECES
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PACKAGING
SPECIAL HANDLING SECTION
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MASTER TRACKING NUMBER
77390366098?
DELIVERED TO
SniRping/Receiving
TERMS
ThFrd Party
STANDARD TRANSIT
12/07; 7018 by 3 00 Em
EAST LONGMEAE)OK MA
EAST LONGMEADOW, MA
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Table of Contents
I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Relinquishing
Af�lALYTICAL LABORATORY
Over Samples
Doc .277 Rev 5 2017
Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client JA-0 r � 1 0-1 �,"Jvl n
Received By
How were the samples
received?
Were samples within
Temperature? 2-WC
Date
In Cooler i No Cooler
Direct from Sampling
Was Custody Seal Intact?
By Gun #
By Blank #
Was COG Reknquished . D---_
Are there broken/leaking/loose caps on any samples?
Time
On Ice
Ambient
Actual Temp - 7 , �-
61 �-u
No Ice
Melted Ice
Actual Temp -
Were Samples Tampered with?
Does Chain Agree With Samples? fi
C
Is COC in ink/ Legible? 4 Were samples received within holding time? -T
Did COC include all Client
"r
pertinent Information? Project
-�
Are Sample labels filled out and legible?
-F-
Are there Lab to Filters?
Are there Rushes?
Are there Short Holds?
Is there enough Volume?
Is there Headspace where applicable?
Proper Media/Containers Used?
Were trip blanks received?
Do all samples have the proper pH?'s
Analysis 1 Sampler Name �-
ID's T Collection Dates/Times
Who was notified?
Who was notified?
Who was notified?
MS/MSD?
Is splitting samples required?4
_
On COC?
Acid Base
:m r
Unp-
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Am /Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz /Clear
Bisulfate-
Flashpoint
Col./Bacteria
2oz Am Cle
DI-
Other Glass
Other Plastic
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Sulfuric-
Perchlorate
Ziplock
Room
Unp-
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
4oz AmbIClear
Bisulfate-
Col./Bacteria
Flashpoint
2oz Amb/Clear
Dl-
Other Plastic
Other Glass
Encore
Thiosulfate-
SOC Kit
Plastic BagFrozen:
Sulfuric-
Perchlorate
Ziplock
Comments:

aceAnalytical
—pacelabs.com
Pace Table of Contents
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 03, 2019
Laurie Kopyscinski
Con -Test Analytical Laboratory
39 Spruce Street
East Longmeadow, MA 01028
RE: Project: 18L029512/21
Pace Project No.: 92411904
Dear Laurie Kopyscinski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 21, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
[phone]
Project Manager
Enclosures
cc: Kerry McGee, Con -Test Analytical Laboratory
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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CERTIFICATIONS
Project: 18 L 0295 12/21
Pace Project No.: 92411904
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Nebraska Certification: NE-OS-28-14
Alabama Certification #: 41320
New Hampshire Certification #: 2958
Colorado Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
Connecticut Certification M PH-0216
New York Certification #: 11608
Florida Certification #: E83079
North Carolina Environmental Certificate #: 667
Georgia Certification #: 955
North Carolina Certification #: 12710
Guam Certification: FL NELAC Reciprocity
North Dakota Certification #: R-216
Hawaii Certification: FL NELAC Reciprocity
Oklahoma Certification #: D9947
Illinois Certification #: 200068
Pennsylvania Certification #: 68-00547
Indiana Certification: FL NELAC Reciprocity
Puerto Rico Certification #: FLO1264
Kansas Certification #: E-10383
South Carolina Certification: #96042001
Kentucky Certification #: 90050
Tennessee Certification #: TN02974
Louisiana Certification #: FL NELAC Reciprocity
Texas Certification: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
US Virgin Islands Certification: FL NELAC Reciprocity
Maryland Certification: #346
Virginia Environmental Certification #: 460165
Michigan Certification #: 9911
West Virginia Certification #: 9962C
Mississippi Certification: FL NELAC Reciprocity
Wisconsin Certification #: 399079670
Missouri Certification #: 236
Wyoming (EPA Region 8): FL NELAC Reciprocity
Montana Certification #: Cert 0074
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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SAMPLE SUMMARY
Project: 18 L 0295 12/21
Pace Project No.: 92411904
Lab ID Sample ID Matrix Date Collected Date Received
92411904001 18L0295-04 Solid 12/04/1811:50 12/21/1812:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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SAMPLE ANALYTE COUNT
Project: 18 L 0295 12/21
Pace Project No.: 92411904
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92411904001 18L0295-04 ASTM D2974-87 NMP 1 PASI-0
EPA 7199 ALD 1 PASI-O
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: 18 L 0295 12/21
Pace Project No.: 92411904
Sample: 18L0295-04 Lab ID: 92411904001 Collected: 12/04/18 11:50 Received: 12/21/18 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 29.9 % 0.10 0.10 1 01/02/19 13:33
7199 Hexavalent Chromium Soil Analytical Method: EPA 7199 Preparation Method: EPA 3060
Chromium, Hexavalent 2.3 mg/kg 0.93 0.39 1 12/27/18 10:47 01/03/19 02:02 18540-29-9
Date: 01/03/2019 05:50 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: 18 L 0295 12/21
Pace Project No.: 92411904
QC Batch: 505243
Analysis Method:
ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description:
Dry Weight/Percent Moisture
Associated Lab Samples: 92411904001
SAMPLE DUPLICATE: 2728415
35437468050
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
2.2
2.3 6
5 D6
SAMPLE DUPLICATE: 2728416
35439514004
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
9.6
10.4 8
5 D6
SAMPLE DUPLICATE: 2728417
35439528002
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
3.3
2.9 13
5 D6
SAMPLE DUPLICATE: 2728418
35439537002
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
25.3
26.4 4
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /03/2019 05:50 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: 18 L 0295 12/21
Pace Project No.: 92411904
QC Batch: 504009
Analysis Method:
EPA 7199
QC Batch Method: EPA 3060
Analysis Description:
7199 Hexavelent Chromium Soil
Associated Lab Samples: 92411904001
METHOD BLANK: 2723288
Matrix: Solid
Associated Lab Samples: 92411904001
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Chromium, Hexavalent
mg/kg
<0.26 0.62 0.26
01/02/19 23:26
LABORATORY CONTROL SAMPLE: 2723289
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Chromium, Hexavalent
mg/kg
39.1 40.4
103
80-120
MATRIX SPIKE SAMPLE: 2723291
92411878001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Chromium, Hexavalent
mg/kg
0.54J 66.7
37.7
56
75-125 M1
SAMPLE DUPLICATE: 2723290
92411878001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Chromium, Hexavalent
mg/kg
0.54J <0.46
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /03/2019 05:50 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: 18 L 0295 12/21
Pace Project No.: 92411904
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /03/2019 05:50 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 18 L 0295 12/21
Pace Project No.: 92411904
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92411904001 18L0295-04 ASTM D2974-87 505243
92411904001 18L0295-04 EPA 3060 504009 EPA 7199 505523
Date: 01/03/2019 05:50 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 65 of 68

Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
Table of Contents
i(SCUR} Pa e 1 of 2
Issuing�ALOWW'ItYr�:�Pace Carolin
Huntersville Raleigh❑ Mechanicsville❑
CgentName: project#: WO# 92411904
Courier: ad Ex ❑UPS Cl ❑USP5 - ❑Chen
❑ Commerdal ❑Pace �, ❑other: 92411904
ss�tad tal Pr�s•ait� ❑Yes — Lyrvo 5dais lntaet7 --[]Yes / — — t 111 j(� y1i I �V
Dole/pale/Initials Person Examining Cortt•ntsI —
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Thersta6mete�"ver: Type of icc: 41❑Blue
r-
t_UR tun to; 92T O46
CoolairTetnp rC}: gqCorrection Factor. Add/Subtract ('C) p,Q
Cooler Temp. Corrected S'CJ: �.�i----
USDA Regulated Soil {❑ N/A, watersampfe}'
Did samples arigr' n a quaranilne zone within the United States: CA, ICY, or SC{Check maps
Flv. n
Chain ofCustedyAresent?
es
ONo
N/A
Samples Arrived Lmthln HaIdTrrie?
❑No
❑N/A
Short Hold A neAfte(ysss t[72 hr.)?
es
❑No
❑ A
Rush Turn Around Time Requested?
Oyu
❑
❑NIA
SufficlentValvme?
es
❑No
❑N/A
Correct Containers Used?
-Pace Containers Used?
es No
No
❑NIA
❑hI/A
Containers Intact?
es
❑No
`NIA.
Dissolved anal sis: Samples Field Faltered?
❑Yes
❑No
/A
Sample Ubds Match COC?
AncludezDate/Trne/11]/Analysis Matrix:
es
❑No
❑N/A
Headspaa is VOA Vials >5-fimmi?
❑Yes
Duo
Trip Blankprezent"?
Trip SlankCustodySeals Present?
❑Yes
❑Yes
❑No
No
/A
!A
COMMENTS/SAMPLE DISCREPANCY
Biological Tissue Fr ?.
[]Yes []NO /A
❑NGO
Temp should be above freeringto6% - .
05a Inples out of temp cdterEa. Samples an Ice, cooling process
hasbEun
Lot lD nfs lit coata[ners:
CLIENT NOTIFICATIOtv/Re OLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager 5RF Review:
Field Deta Required? ❑Yes ❑No
DateJtrne;
Date: 2
J
Date'
srrzr�> . aFp�

f' 4.-e
Condition Upon Receipt(SCUR) ra n A ur A Table of Contents
Dorument No.:. Issuing Authority:
FCAR-(S-433-Rev.06 Paco Carolinas Qua C1f$ce
`Check mark top half of box If pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptlons: VOA, Colirarm, Toc, Via rid Grease, DW/8015 {water} 00C, LLH9
"Bottom half of box is to list number of bottle .
Project# WO# : 92411904
PM: C131 Due Date: 12/27/18
CLIENT: 92-Con-Test
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PH Adjustment Log for Preserved Sanples
SamplelD Type of Preservative pH upon receipt 1wepreservation adjusted. -rime presuvation Amountofpreservative Lot
adjus'd added
!Vote: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this force win le sent to the North Carolina DHi [R CertratiQn Office {i.e.
Out of hold, incorrectpreservative, cut of temp, incorrect containers.
Miami• • •i

Table of Contents
SUBCONTRACT ORDER
Con -Test Analytical Laboratory
18LO295
SENDING LABORATORY: RECEIVING LABORAIORY:
Con -Test Analytical Laboratory Pace Analytical Services - NC
39 Spruce Street r 9800 Kincey Avenue, Suite 100
East Longmeadow, MAO1028 Huntersville, NC 28078
Phone: [phone] Phone :[phone]
—Fax: [phone] —
Project Manager: Kerry K. McGee
Analysis Due Expires Laboratory ID Comments
Sample ID: 18L0295-04 SDII Sampled: 12/04/18 11:50 6l tLA � 1 _I U (-� - U 0 1
Miscellaneous 2 01/02/1915:00 12/18/18 11:50 hexavalmt chromium by method 7199. Report to
MDL
Containers Supplied-
4 oz amber glass jar (B)
Released By Date Received By Date
Page 1 of 1
Page 68 of 68

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
December 13, 2018
Bo Cappleman
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Charlotte, NC
Client Job Number:
Project Number: COP-008
Laboratory Work Order Number: 18L0322
Enclosed are results of analyses for samples received by the laboratory on December 6, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 54

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
18L0322-01
18L0322-02
18L0322-03
18L0322-04
18L0322-05
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/MS
B218882
Semivolatile Organic Compounds by GUMS
B218940
B219039
Metals Analyses (Total)
B218876
B219057
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
7
7
12
17
22
27
29
30
30
30
35
35
39
45
45
46
47
48
52
Page 2 of 54

Table of Contents
40 ,con -testy
ANALYTICAL LABORATORY
39 Spruce StreetEast Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100 REPORT DATE: 12/13/2018
Charlotte, NC 28203 PURCHASE ORDER NUMBER:
ATTN: Bo Cappleman
PROJECT NUMBER: COP-008
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18LO322
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Charlotte, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
TMW-1 18L0322-01 Ground Water SW-846 6020B
SW-846 7470A
SW-846 8260B
SW-846 8270D
TMW-2 18LO322-02 Ground Water SW-846 6020B
SW-846 7470A
SW-846 8260B
SW-846 8270D
TMW-3 18L0322-03 Ground Water SW-846 6020B
SW-846 7470A
SW-846 8260B
SW-846 8270D
DUP-GW-1 18L0322-04 Ground Water SW-846 6020B
SW-846 7470A
SW-846 8260B
SW-846 8270D
Trip Blank-1 18LO322-05 Trip Blank Water SW-846 8260B
Page 3 of 54

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6020, all dilutions for water were performed as per standard operating procedure.
For method 8260B elevated reporting limits for sample 18L0322-01 due to high concentrations of target compounds.
Page 4 of 54

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
SW-846 8260B
Qualifications
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
Acetone
B218882-BSDI
RL-11
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
18L0322-01[TMW-1]
SW-846 8270D
Qualifications:
L-04
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
Benzidine
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI
N-Nitrosodimethylamine
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI
MS-23
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
outside of the method specified criteria. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
Benzidine
B219039-BSD1
R-05
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
1-Methylnaphthalene
18L0322-03[TMW-3], B219039-BLKI, B219039-BSI, B219039-BSDI
2-Methylnaphthalene
18L0322-03[TMW-3], B219039-BLKI, B219039-BSI, B219039-BSDI
4-Chloro-3-methylphenol
18L0322-03[TMW-3], B219039-BLKI, B219039-BS1, B219039-BSD1
Benzidine
18L0322-01[TMW-1], 18LO322-02[TMW-2], 18L0322-03[TMW-3], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BSI
Butylbenzylphthalate
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18LO322-03[TMW-3], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BS1,B219039-BSD1
Pyrene
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18L0322-03[TMW-3], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSD1, B219039-BLKI,
B219039-BSI,B219039-BSDI
V-04
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
Aniline
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18LO322-03[TMW-3], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BS1,B219039-BSD1
Benzidine
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18L0322-03[TMW-3], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BSI,B219039-BSDI
Page 5 of 54

,con-testo
ANALYTICAL LABORATORY
Table of Contents
V-05
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] ` TEL. [phone]
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
Benzidine
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18L0322-03[TMW-3], 18LO322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BS1,B219039-BSD1
Benzo(g,h,i)perylene
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18L0322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI
Hexachlorocyclopentadiene
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18LO322-03[TMW-3], 18LO322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BS1,B219039-BSD1
Pyridine
18L0322-01[TMW-1], 18L0322-02[TMW-2], 18LO322-03[TMW-3], 18LO322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BSI,B219039-BSDI
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
4-Chloroaniline
18L0322-0I[TMW-1], 18L0322-02[TMW-2], 18LO322-03[TMW-3], 18LO322-04[DUP-GW-1], B218940-BLKI, B218940-BSI, B218940-BSDI, B219039-BLKI,
B219039-BS1,B219039-BSD1
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Director of Operations
Page 6 of 54

Table of Contents
icon-te w
ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: TMW-1
Sample ID: 18L0322-01
Samnle Matrix: Ground Water
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/5/2018 10:05
Work Order: 18L0322
Sample Flags: RL-11
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
2500
480
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Acrylonitrile
ND
250
29
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
tert-Amyl Methyl Ether (TAME)
ND
25
5.3
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Benzene
ND
50
6.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Bromobenzene
ND
50
7.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Bromochloromethane
ND
50
11
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Bromodichloromethane
ND
25
15
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Bromoform
ND
100
10
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Bromomethane
ND
100
47
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
2-Butanone (MEK)
ND
1000
120
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
tert-Butyl Alcohol (TBA)
ND
1000
110
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
n-Butylbenzene
ND
50
7.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
sec-Butylbenzene
ND
50
6.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
tert-Butylbenzene
ND
50
6.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
tert-Butyl Ethyl Ether (TBEE)
ND
25
4.8
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Carbon Disulfide
ND
200
51
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Carbon Tetrachloride
ND
250
12
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Chlorobenzene
ND
50
8.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Chlorodibromomethane
ND
25
5.2
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Chloroethane
ND
100
14
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Chloroform
ND
100
11
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Chloromethane
ND
100
28
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
2-Chlorotoluene
ND
50
6.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
4-Chlorotoluene
ND
50
7.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2-Dibromo-3-chloropropane (DBCP)
ND
250
18
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2-Dibromoethane (EDB)
ND
25
7.4
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Dibromomethane
ND
50
8.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2-Dichlorobenzene
ND
50
8.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,3-Dichlorobenzene
ND
50
8.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,4-Dichlorobenzene
ND
50
7.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
trans-1,4-Dichloro-2-butene
ND
100
16
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Dichlorodifluoromethane (Freon 12)
ND
100
14
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,1-Dichloroethane
ND
50
7.9
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2-Dichloroethane
ND
50
9.7
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1, 1 -Dichloroethylene
ND
50
10
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
cis-1,2-Dichloroethylene
22
50
7.4
µg/L
50 J
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
trans-1,2-Dichloroethylene
ND
50
7.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2-Dichloropropane
ND
50
6.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,3-Dichloropropane
ND
25
6.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
2,2-Dichloropropane
ND
50
11
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1, 1 -Dichloropropene
ND
100
6.4
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
cis-1,3-Dichloropropene
ND
25
6.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
trans-1,3-Dichloropropene
ND
25
5.6
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Diethyl Ether
ND
100
11
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Page 7 of 54

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-1 Sampled: 12/5/2018 10:05
Sample ID: 18L0322-01
Samnle Matrix: Ground Water
Sample Flags: RL-11 Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
25
9.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,4-Dioxane
ND
2500
1300
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Ethylbenzene
ND
50
6.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Hexachlorobutadiene
ND
30
29
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
2-Hexanone (MBK)
ND
500
76
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Isopropylbenzene (Cumene)
ND
50
6.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
p-Isopropyltoluene (p-Cymene)
ND
50
7.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Methyl tert-Butyl Ether (MTBE)
ND
50
4.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Methylene Chloride
ND
250
160
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
4-Methyl-2-pentanone (MIBK)
ND
500
73
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Naphthalene
ND
100
6.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
n-Propylbenzene
ND
50
6.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Styrene
ND
50
7.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1, 1, 1,2-Tetrachloroethane
ND
50
6.0
µg/L
50
SW-8468260B
12/10/18
12/13/18 3:24
EEH
1,1,2,2-Tetrachloroethane
ND
25
8.0
µg/L
50
SW-8468260B
12/10/18
12/13/18 3:24
EEH
Tetrachloroethylene
ND
50
14
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Tetrahydrofuran
ND
500
54
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Toluene
ND
50
8.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2,3-Trichlorobenzene
ND
250
7.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2,4-Trichlorobenzene
ND
50
9.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,3,5-Trichlorobenzene
ND
50
8.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1, 1, 1 -Trichloroethane
ND
50
6.6
µg/L
50
SW-8468260B
12/10/18
12/13/18 3:24
EEH
1,1,2-Trichloroethane
ND
50
12
µg/L
50
SW-8468260B
12/10/18
12/13/18 3:24
EEH
Trichloroethylene
2900
50
10
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Trichlorofluoromethane (Freon 11)
ND
100
7.4
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,2,3-Trichloropropane
ND
100
11
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
50
9.8
µg/L
50
SW-8468260B
12/10/18
12/13/18 3:24
EEH
(Freon 113)
1,2,4-Trimethylbenzene
ND
50
9.0
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
1,3,5-Trimethylbenzene
ND
50
6.5
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Vinyl Chloride
ND
100
6.6
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
m+p Xylene
ND
100
13
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
o-Xylene
ND
50
6.6
µg/L
50
SW-846 8260B
12/10/18
12/13/18 3:24
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
85.3
70-130
12/13/18 3:24
Toluene-d8
96.4
70-130
12/13/18 3:24
4-Bromofluorobenzene
97.0
70-130
12/13/18 3:24
Page 8 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-1 Sampled: 12/5/2018 10:05
Samnle ID: 18L0322-01
Samnle Matrix: Ground Water
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
5.6
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Acenaphthylene
ND
5.6
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Acetophenone
ND
11
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Aniline
ND
5.6
2.8
µg/L
1
V-04
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Anthracene
ND
5.6
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Benzidine
ND
22
11
µg/L
1
L-04, R-05, V-04,
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
V-05
Benzo(a)anthracene
ND
5.6
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Benzo(a)pyrene
ND
5.6
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Benzo(b)fluoranthene
ND
5.6
1.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Benzo(g,h,i)perylene
ND
5.6
2.5
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Benzo(k)fluoranthene
ND
5.6
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Benzoic Acid
ND
11
2.2
µg/L
I
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Bis(2-chloroethoxy)methane
ND
11
2.0
µg/L
I
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Bis(2-chloroethyl)ether
ND
11
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Bis(2-chloroisopropyl)ether
ND
11
2.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Bis(2-Ethylhexyl)phthalate
ND
11
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
4-Bromophenylphenylether
ND
11
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Butylbenzylphthalate
ND
11
2.2
µg/L
1
R-05
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Carbazole
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
4-Chloroaniline
ND
11
1.7
µg/L
1
V-34
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
4-Chloro-3-methylphenol
ND
11
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2-Chloronaphthalene
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2-Chlorophenol
ND
11
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
4-Chlorophenylphenylether
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Chrysene
ND
5.6
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Dibenz(a,h)anthracene
ND
5.6
2.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Dibenzofman
ND
5.6
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Di-n-butylphthalate
ND
11
2.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
1,2-Dichlorobenzene
ND
5.6
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
1,3-Dichlorobenzene
ND
5.6
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
1,4-Dichlorobenzene
ND
5.6
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
3,3-Dichlorobenzidine
ND
11
2.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2,4-Dichlorophenol
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Diethylphthalate
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2,4-Dimethylphenol
ND
11
4.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Dimethylphthalate
ND
11
1.7
µg/L
I
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
4,6-Dinitro-2-methylphenol
ND
11
2.2
µg/L
I
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2,4-Dinitrophenol
ND
11
3.7
µg/L
I
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2,4-Dinitrotoluene
ND
11
2.0
µg/L
I
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2,6-Dinitrotoluene
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Di-n-octylphthalate
ND
11
2.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
11
2.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Fluoranthene
ND
5.6
2.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Page 9 of 54

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-1 Sampled: 12/5/2018 10:05
Sample ID: 18L0322-01
Samnle Matrix: Ground Water
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Flumene
ND
5.6
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Hexachlorobenzene
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Hexachlorobutadiene
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Hexachlorocyclopentadiene
ND
11
2.1
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Hexachloroethane
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Indeno(1,2,3-cd)pyrene
ND
5.6
2.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Isophorone
ND
11
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
1-Methylnaphthalene
ND
5.6
2.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2-Methylnaphthalene
ND
5.6
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2-Methylphenol
ND
11
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
3/4-Methylphenol
ND
11
1.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Naphthalene
ND
5.6
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2-Nitroaniline
ND
11
2.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
3-Nitroaniline
ND
11
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
4-Nitroaniline
ND
11
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Nitrobenzene
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2-Nitrophenol
ND
11
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
4-Nitrophenol
ND
11
1.2
µg/L
I
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
N-Nitrosodimethylamine
ND
11
1.7
µg/L
I
L-04
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
11
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
N-Nitrosodi-n-propylamine
ND
11
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Pentachloronitrobenzene
ND
11
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Pentachlorophenol
ND
11
1.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Phenanthrene
ND
5.6
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Phenol
ND
11
1.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Pyrene
ND
5.6
1.7
µg/L
1
R-05
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Pyridine
ND
5.6
2.4
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
1,2,4,5-Tetrachlorobenzene
ND
11
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
1,2,4-Trichlorobenzene
ND
5.6
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2,4,5-Trichlorophenol
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
2,4,6-Trichlorophenol
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 18:53
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
48.3
15-110
12/12/18 18:53
Phenol-d6
36.6
15-110
12/12/18 18:53
Nitrobenzene-d5
77.9
30-130
12/12/18 18:53
2-Fluorobiphenyl
64.9
30-130
12/12/18 18:53
2,4,6-Tribromophenol
78.4
15-110
12/12/18 18:53
p-Terphenyl-dl4
77.9
30-130
12/12/18 18:53
Page 10 of 54

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: TMW-1
Samnle ID: 18L0322-01
Samnle Matrix: Ground Water
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/5/2018 10:05
Work Order: 18L0322
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
ND
0.80
0.72
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:23
WSD
Barium
35
20
11
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:23
WSD
Cadmium
ND
1.0
0.14
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:23
WSD
Chromium
1.5
2.0
0.86
µg/L
2 J
SW-846 6020B
12/10/18
12/11/18 13:23
WSD
Lead
ND
2.0
0.48
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:23
WSD
Mercury
0.000076 0.00010
0.000034
mg/L
1 J
SW-846 7470A
12/12/18
12/13/18 11:33
AJL
Selenium
ND
10
2.8
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:23
WSD
Silver
ND
1.0
0.15
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:23
WSD
Page 11 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-2 Sampled: 12/5/2018 14:40
Sample ID: 18L0322-02
Samnle Matrix: Ground Water
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
50
9.7
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Acrylonitrile
ND
5.0
0.58
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
tert-Amyl Methyl Ether (TAME)
ND
0.50
0.11
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Benzene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Bromobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Bromochloromethane
ND
1.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Bromodichloromethane
ND
0.50
0.30
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Bromoform
ND
2.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Bromomethane
ND
2.0
0.94
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
2-Butanone (MEK)
ND
20
2.4
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
tert-Butyl Alcohol (TBA)
9.5
20
2.2
µg/L
1 J
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
n-Butylbenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
sec-Butylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
tert-Butylbenzene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
tert-Butyl Ethyl Ether (TBEE)
ND
0.50
0.095
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Carbon Disulfide
ND
4.0
1.0
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Carbon Tetrachloride
ND
5.0
0.25
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Chlorobenzene
ND
1.0
0.16
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Chlorodibromomethane
ND
0.50
0.10
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Chloroethane
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Chloroform
0.76
2.0
0.22
µg/L
1 J
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Chloromethane
ND
2.0
0.55
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
2-Chlomtoluene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
4-Chlorotoluene
ND
1.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2-Dibromo-3-chloropropane (DBCP)
ND
5.0
0.37
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2-Dibromoethane (EDB)
ND
0.50
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Dibromomethane
ND
1.0
0.16
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,3-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,4-Dichlorobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
trans-1,4-Dichloro-2-butene
ND
2.0
0.31
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Dichlorodifluoromethane (Freon 12)
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,1-Dichloroethane
ND
1.0
0.16
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2-Dichloroethane
ND
1.0
0.19
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1, 1 -Dichloroethylene
ND
1.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
cis-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
trans-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2-Dichloropropane
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,3-Dichloropropane
ND
0.50
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
2,2-Dichloropropane
ND
1.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1, 1 -Dichloropropene
ND
2.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
cis-1,3-Dichloropropene
ND
0.50
0.12
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
trans-1,3-Dichloropropene
ND
0.50
0.11
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Diethyl Ether
ND
2.0
0.22
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Page 12 of 54

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-2 Sampled: 12/5/2018 14:40
Samnle ID: 18L0322-02
Samnle Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.50
0.18
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,4-Dioxane
ND
50
26
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Ethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Hexachlorobutadiene
ND
0.60
0.59
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
2-Hexanone (MBK)
ND
10
1.5
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Isopropylbenzene (Cumene)
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
p-Isopropyltoluene (p-Cymene)
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Methyl tert-Butyl Ether (MTBE)
ND
1.0
0.090
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Methylene Chloride
ND
5.0
3.2
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
4-Methyl-2-pentanone (MIBK)
ND
t0
1.5
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Naphthalene
ND
2.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
n-Propylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Styrene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1, 1, 1,2-Tetrachloroethane
ND
1.0
0.12
µg/L
1
SW-8468260B
12/10/18
12/12/18 23:52
EEH
1,1,2,2-Tetrachloroethane
ND
0.50
0.16
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Tetrachloroethylene
1.0
1.0
0.27
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Tetrahydrofuran
ND
10
1.1
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Toluene
ND
1.0
0.17
µg/L
I
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2,3-Trichlorobenzene
ND
5.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2,4-Trichlorobenzene
ND
1.0
0.19
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,3,5-Trichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1, 1, 1 -Trichloroethane
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,1,2-Trichloroethane
ND
1.0
0.24
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Trichloroethylene
3.7
1.0
0.20
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Trichlorofluoromethane (Freon 11)
ND
2.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,2,3-Trichloropropane
ND
2.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.20
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
(Freon 113)
1,2,4-Trimethylbenzene
ND
1.0
0.18
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
1,3,5-Trimethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Vinyl Chloride
ND
2.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
m+p Xylene
ND
2.0
0.26
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
o-Xylene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 23:52
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
86.7
70-130
12/12/18 23:52
Toluene-d8
95.4
70-130
12/12/18 23:52
4-Bromofluorobenzene
97.1
70-130
12/12/18 23:52
Page 13 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-2 Sampled: 12/5/2018 14:40
Samnle ID: 18L0322-02
Samnle Matrix: Ground Water
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
5.2
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Acenaphthylene
ND
5.2
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Acetophenone
ND
10
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Aniline
ND
5.2
2.6
µg/L
1
V-04
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Anthracene
ND
5.2
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Benzidine
ND
21
10
µg/L
1
L-04, R-05, V-04,
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
V-05
Benzo(a)anthracene
ND
5.2
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Benzo(a)pyrene
ND
5.2
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Benzo(b)fluoranthene
ND
5.2
1.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Benzo(g,h,i)perylene
ND
5.2
2.3
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Benzo(k)fluoranthene
ND
5.2
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Benzoic Acid
ND
10
2.1
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Bis(2-chloroethoxy)methane
ND
10
1.8
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Bis(2-chloroethyl)ether
ND
10
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Bis(2-chloroisopropyl)ether
ND
10
2.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Bis(2-Ethylhexyl)phthalate
ND
10
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
4-Bromophenylphenylether
ND
10
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Butylbenzylphthalate
ND
10
2.0
µg/L
1
R-05
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Carbazole
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
4-Chloroaniline
ND
10
1.6
µg/L
1
V-34
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
4-Chloro-3-methylphenol
ND
10
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2-Chloronaphthalene
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2-Chlorophenol
ND
10
1.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
4-Chlorophenylphenylether
ND
10
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Chrysene
ND
5.2
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Dibenz(a,h)anthracene
ND
5.2
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Dibenzofman
ND
5.2
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Di-n-butylphthalate
ND
10
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
1,2-Dichlorobenzene
ND
5.2
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
1,3-Dichlorobenzene
ND
5.2
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
1,4-Dichlorobenzene
ND
5.2
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
3,3-Dichlorobenzidine
ND
10
2.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2,4-Dichlorophenol
ND
10
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Diethylphthalate
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2,4-Dimethylphenol
ND
10
3.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Dimethylphthalate
ND
10
1.6
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
4,6-Dinitro-2-methylphenol
ND
10
2.1
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2,4-Dinitrophenol
ND
10
3.5
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2,4-Dinitrotoluene
ND
10
1.9
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2,6-Dinitrotoluene
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Di-n-octylphthalate
ND
10
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
10
2.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Fluoranthene
ND
5.2
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Page 14 of 54

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-2 Sampled: 12/5/2018 14:40
Sample ID: 18L0322-02
Samnle Matrix: Ground Water
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Flumene
ND
5.2
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Hexachlorobenzene
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Hexachlorobutadiene
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Hexachlorocyclopentadiene
ND
t0
2.0
µg/L
1
V-05
SW-8468270D
12/11/18
12/12/18 19:20
BGL
Hexachloroethane
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Indeno(1,2,3-cd)pyrene
ND
5.2
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Isophorone
ND
t0
2.0
µg/L
1
SW-8468270D
12/11/18
12/12/18 19:20
BGL
1-Methylnaphthalene
ND
5.2
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2-Methylnaphthalene
ND
5.2
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2-Methylphenol
ND
10
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
3/4-Methylphenol
ND
t0
1.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Naphthalene
ND
5.2
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2-Nitroaniline
ND
10
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
3-Nitroaniline
ND
10
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
4-Nitroaniline
ND
10
2.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Nitrobenzene
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2-Nitrophenol
ND
10
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
4-Nitrophenol
ND
10
1.1
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
N-Nitrosodimethylamine
ND
10
1.6
µg/L
I
L-04
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
10
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
N-Nitrosodi-n-propylamine
ND
10
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Pentachloronitrobenzene
ND
10
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Pentachlorophenol
ND
10
1.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Phenanthrene
ND
5.2
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Phenol
ND
10
1.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Pyrene
ND
5.2
1.6
µg/L
1
R-05
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Pyridine
ND
5.2
2.2
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
1,2,4,5-Tetrachlorobenzene
ND
t0
1.7
µg/L
1
SW-8468270D
12/11/18
12/12/18 19:20
BGL
1,2,4-Trichlorobenzene
ND
5.2
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
2,4,5-Trichlorophenol
ND
t0
1.6
µg/L
1
SW-8468270D
12/11/18
12/12/18 19:20
BGL
2,4,6-Trichlorophenol
ND
10
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:20
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
45.8
15-110
12/12/18 19:20
Phenol-d6
34.1
15-110
12/12/18 19:20
Nitrobenzene-d5
73.7
30-130
12/12/18 19:20
2-Fluorobiphenyl
60.6
30-130
12/12/18 19:20
2,4,6-Tribromophenol
74.5
15-110
12/12/18 19:20
p-Terphenyl-dl4
73.4
30-130
12/12/18 19:20
Page 15 of 54

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: TMW-2
Samnle ID: 18L0322-02
Samnle Matrix: Ground Water
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/5/2018 14:40
Work Order: 18L0322
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
ND
0.80
0.72
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:27
WSD
Barium
32
20
11
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:27
WSD
Cadmium
ND
1.0
0.14
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:27
WSD
Chromium
2.8
2.0
0.86
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:27
WSD
Lead
ND
2.0
0.48
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:27
WSD
Mercury
0.000068 0.00010
0.000034
mg/L
1 J
SW-846 7470A
12/12/18
12/13/18 11:34
AJL
Selenium
ND
10
2.8
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:27
WSD
Silver
ND
1.0
0.15
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:27
WSD
Page 16 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-3 Sampled: 12/5/2018 15:15
Sample ID: 18L0322-03
Samnle Matrix: Ground Water
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
50
9.7
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Acrylonitrile
ND
5.0
0.58
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
tert-Amyl Methyl Ether (TAME)
ND
0.50
0.11
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Benzene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Bromobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Bromochloromethane
ND
1.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Bromodichloromethane
ND
0.50
0.30
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Bromoform
ND
2.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Bromomethane
ND
2.0
0.94
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
2-Butanone (MEK)
ND
20
2.4
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
tert-Butyl Alcohol (TBA)
ND
20
2.2
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
n-Butylbenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
sec-Butylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
tert-Butylbenzene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
tert-Butyl Ethyl Ether (TBEE)
ND
0.50
0.095
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Carbon Disulfide
ND
4.0
1.0
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Carbon Tetrachloride
ND
5.0
0.25
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Chlorobenzene
ND
1.0
0.16
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Chlorodibromomethane
ND
0.50
0.10
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Chloroethane
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Chloroform
ND
2.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Chloromethane
ND
2.0
0.55
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
2-Chlomtoluene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
4-Chlomtoluene
ND
1.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,2-Dibromo-3-chloropropane (DBCP)
ND
5.0
0.37
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,2-Dibromoethane (EDB)
ND
0.50
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Dibromomethane
ND
1.0
0.16
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,2-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,3-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,4-Dichlorobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
trans-1,4-Dichloro-2-butene
ND
2.0
0.31
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Dichlorodifluoromethane (Freon 12)
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,1-Dichloroethane
ND
1.0
0.16
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:19
EEH
1,2-Dichloroethane
ND
1.0
0.19
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1, 1 -Dichloroethylene
ND
1.0
0.21
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:19
EEH
cis-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
trans-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,2-Dichloropropane
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,3-Dichloropropane
ND
0.50
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
2,2-Dichloropropane
ND
1.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1, 1 -Dichloropropene
ND
2.0
0.13
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:19
EEH
cis-1,3-Dichloropropene
ND
0.50
0.12
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
trans-1,3-Dichloropropene
ND
0.50
0.11
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Diethyl Ether
ND
2.0
0.22
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Page 17 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-3 Sampled: 12/5/2018 15:15
Samnle ID: 18L0322-03
Samnle Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.50
0.18
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,4-Dioxane
ND
50
26
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Ethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Hexachlorobutadiene
ND
0.60
0.59
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
2-Hexanone (MBK)
ND
10
1.5
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Isopropylbenzene (Cumene)
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
p-Isopropyltoluene (p-Cymene)
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Methyl tert-Butyl Ether (MTBE)
ND
1.0
0.090
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Methylene Chloride
ND
5.0
3.2
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
4-Methyl-2-pentanone (MIBK)
ND
10
1.5
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Naphthalene
ND
2.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
n-Propylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Styrene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1, 1, 1,2-Tetrachloroethane
ND
1.0
0.12
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:19
EEH
1,1,2,2-Tetrachloroethane
ND
0.50
0.16
µg/L
I
SW-8468260B
12/10/18
12/13/18 0:19
EEH
Tetrachloroethylene
ND
1.0
0.27
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Tetrahydrofuran
2.0
10
1.1
µg/L
I
J
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Toluene
0.19
1.0
0.17
µg/L
I
J
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,2,3-Trichlorobenzene
ND
5.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,2,4-Trichlorobenzene
ND
1.0
0.19
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,3,5-Trichlorobenzene
ND
1.0
0.17
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1, 1, 1 -Trichloroethane
ND
1.0
0.13
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:19
EEH
1,1,2-Trichloroethane
ND
1.0
0.24
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:19
EEH
Trichloroethylene
0.88
1.0
0.20
µg/L
1
J
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Trichlorofluoromethane (Freon 11)
ND
2.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,2,3-Trichloropropane
ND
2.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.20
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:19
EEH
(Freon 113)
1,2,4-Trimethylbenzene
ND
1.0
0.18
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
1,3,5-Trimethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Vinyl Chloride
ND
2.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
m+p Xylene
ND
2.0
0.26
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
o-Xylene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:19
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
86.7
70-130
12/13/18 0:19
Toluene-d8
95.1
70-130
12/13/18 0:19
4-Bromofluorobenzene
95.2
70-130
12/13/18 0:19
Page 18 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-3 Sampled: 12/5/2018 15:15
Samnle ID: 18L0322-03
Samnle Matrix: Ground Water
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
5.1
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Acenaphthylene
ND
5.1
1.4
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Acetophenone
ND
10
1.7
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Aniline
ND
5.1
2.5
µg/L
1 V-04
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Anthracene
ND
5.1
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Benzidine
ND
20
9.9
µg/L
1 R-05, V-04, V-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Benzo(a)anthracene
ND
5.1
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Benzo(a)pyrene
ND
5.1
1.6
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Benzo(b)fluoranthene
ND
5.1
1.2
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Benzo(g,h,i)perylene
ND
5.1
2.3
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Benzo(k)fluoranthene
ND
5.1
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Benzoic Acid
ND
10
2.0
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Bis(2-chloroethoxy)methane
ND
10
1.8
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Bis(2-chloroethyl)ether
ND
10
1.7
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Bis(2-chloroisopropyl)ether
ND
10
2.3
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Bis(2-Ethylhexyl)phthalate
ND
10
2.0
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
4-Bromophenylphenylether
ND
10
1.4
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Butylbenzylphthalate
ND
10
2.0
µg/L
I R-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Carbazole
ND
10
1.6
µg/L
I
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
4-Chloroaniline
ND
10
1.5
µg/L
1 V-34
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
4-Chloro-3-methylphenol
ND
10
1.4
µg/L
1 R-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2-Chloronaphthalene
ND
10
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2-Chlorophenol
ND
10
1.3
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
4-Chlorophenylphenylether
ND
10
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Chrysene
ND
5.1
1.4
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Dibenz(a,h)anthracene
ND
5.1
2.1
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Dibenzofuran
ND
5.1
1.4
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Di-n-butylphthalate
ND
10
1.8
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
1,2-Dichlorobenzene
ND
5.1
1.3
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
1,3-Dichlorobenzene
ND
5.1
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
1,4-Dichlorobenzene
ND
5.1
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
3,3-Dichlorobenzidine
ND
10
2.3
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2,4-Dichlorophenol
ND
10
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Diethylphthalate
ND
t0
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2,4-Dimethylphenol
ND
10
3.8
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Dimethylphthalate
ND
10
1.6
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
4,6-Dinitro-2-methylphenol
ND
10
2.0
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2,4-Dinitrophenol
ND
10
3.4
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2,4-Dinitrotoluene
ND
10
1.8
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2,6-Dinitrotoluene
ND
10
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Di-n-octylphthalate
ND
10
2.2
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
10
2.6
µg/L
I
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Fluoranthene
ND
5.1
1.8
µg/L
I
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Flumene
ND
5.1
1.5
µg/L
I
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Page 19 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: TMW-3 Sampled: 12/5/2018 15:15
Samnle ID: 18L0322-03
Samnle Matrix: Ground Water
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
10
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Hexachlorobutadiene
ND
10
1.6
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Hexachlorocyclopentadiene
ND
10
2.0
µg/L
1
V-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Hexachloroethane
ND
10
1.6
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Indeno(1,2,3-cd)pyrene
ND
5.1
2.1
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Isophorone
ND
10
1.9
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
1-Methylnaphthalene
ND
5.1
1.8
µg/L
1
R-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2-Methylnaphthalene
ND
5.1
1.7
µg/L
1
R-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2-Methylphenol
ND
t0
1.4
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
3/4-Methylphenol
ND
10
1.2
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Naphthalene
ND
5.1
1.7
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2-Nitroaniline
ND
10
2.2
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
3-Nitroaniline
ND
10
2.0
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
4-Nitroaniline
ND
10
2.0
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Nitrobenzene
ND
10
1.6
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2-Nitrophenol
ND
10
1.6
µg/L
I
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
4-Nitrophenol
ND
10
1.1
µg/L
I
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
N-Nitrosodimethylamine
ND
10
1.6
µg/L
I
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
10
1.9
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
N-Nitrosodi-n-propylamine
ND
10
1.7
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Pentachloronitrobenzene
ND
10
1.7
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Pentachlorophenol
ND
10
1.1
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Phenanthrene
ND
5.1
1.4
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Phenol
ND
10
1.0
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Pyrene
ND
5.1
1.6
µg/L
1
R-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Pyridine
ND
5.1
2.2
µg/L
1
V-05
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
1,2,4,5-Tetrachlorobenzene
ND
10
1.7
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
1,2,4-Trichlorobenzene
ND
5.1
1.6
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2,4,5-Trichlorophenol
ND
10
1.6
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
2,4,6-Trichlorophenol
ND
10
1.5
µg/L
1
SW-846 8270D
12/12/18
12/13/18 10:48
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
72.0
15-110
12/13/18 10:48
Phenol-d6
58.6
15-110
12/13/18 10:48
Nitrobenzene-d5
73.0
30-130
12/13/18 10:48
2-Fluorobiphenyl
58.0
30-130
12/13/18 10:48
2,4,6-Tribromophenol
68.4
15-110
12/13/18 10:48
p-Terphenyl-dl4
71.1
30-130
12/13/18 10:48
Page 20 of 54

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: TMW-3
Samnle ID: 18L0322-03
Samnle Matrix: Ground Water
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/5/2018 15:15
Work Order: 18L0322
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
ND
0.80
0.72
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:30
WSD
Barium
39
20
11
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:30
WSD
Cadmium
ND
1.0
0.14
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:30
WSD
Chromium
1.1
2.0
0.86
µg/L
2 J
SW-846 6020B
12/10/18
12/11/18 13:30
WSD
Lead
ND
2.0
0.48
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:30
WSD
Mercury
0.000059 0.00010
0.000034
mg/L
1 J
SW-846 7470A
12/12/18
12/13/18 11:36
AJL
Selenium
ND
10
2.8
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:30
WSD
Silver
ND
1.0
0.15
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:30
WSD
Page 21 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: DUP-GW-1 Sampled: 12/5/2018 00:00
Sample ID: 18L0322-04
Samnle Matrix: Ground Water
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
50
9.7
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Acrylonitrile
ND
5.0
0.58
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
tert-Amyl Methyl Ether (TAME)
ND
0.50
0.11
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Benzene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Bromobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Bromochloromethane
ND
1.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Bromodichloromethane
ND
0.50
0.30
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Bromoform
ND
2.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Bromomethane
ND
2.0
0.94
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
2-Butanone (MEK)
ND
20
2.4
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
tert-Butyl Alcohol (TBA)
ND
20
2.2
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
n-Butylbenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
sec-Butylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
tert-Butylbenzene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
tert-Butyl Ethyl Ether (TBEE)
ND
0.50
0.095
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Carbon Disulfide
ND
4.0
1.0
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Carbon Tetrachloride
ND
5.0
0.25
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Chlorobenzene
ND
1.0
0.16
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Chlorodibromomethane
ND
0.50
0.10
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Chloroethane
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Chloroform
0.66
2.0
0.22
µg/L
1 J
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Chloromethane
ND
2.0
0.55
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
2-Chlomtoluene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
4-Chlomtoluene
ND
1.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,2-Dibromo-3-chloropropane (DBCP)
ND
5.0
0.37
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,2-Dibromoethane (EDB)
ND
0.50
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Dibromomethane
ND
1.0
0.16
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,2-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,3-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,4-Dichlorobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
trans-1,4-Dichloro-2-butene
ND
2.0
0.31
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Dichlorodifluoromethane (Freon 12)
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,1-Dichloroethane
ND
1.0
0.16
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:45
EEH
1,2-Dichloroethane
ND
1.0
0.19
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1, 1 -Dichloroethylene
ND
1.0
0.21
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:45
EEH
cis-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
trans-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,2-Dichloropropane
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,3-Dichloropropane
ND
0.50
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
2,2-Dichloropropane
ND
1.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1, 1 -Dichloropropene
ND
2.0
0.13
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:45
EEH
cis-1,3-Dichloropropene
ND
0.50
0.12
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
trans-1,3-Dichloropropene
ND
0.50
0.11
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Diethyl Ether
ND
2.0
0.22
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Page 22 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: DUP-GW-1 Sampled: 12/5/2018 00:00
Samnle ID: 18L0322-04
Samnle Matrix: Ground Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.50
0.18
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,4-Dioxane
ND
50
26
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Ethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Hexachlorobutadiene
ND
0.60
0.59
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
2-Hexanone (MBK)
ND
10
1.5
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Isopropylbenzene (Cumene)
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
p-Isopropyltoluene (p-Cymene)
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Methyl tert-Butyl Ether (MTBE)
ND
1.0
0.090
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Methylene Chloride
ND
5.0
3.2
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
4-Methyl-2-pentanone (MIBK)
ND
10
1.5
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Naphthalene
ND
2.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
n-Propylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Styrene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1, 1, 1,2-Tetrachloroethane
ND
1.0
0.12
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:45
EEH
1,1,2,2-Tetrachloroethane
ND
0.50
0.16
µg/L
I
SW-8468260B
12/10/18
12/13/18 0:45
EEH
Tetrachloroethylene
0.79
1.0
0.27
µg/L
I J
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Tetrahydrofuran
ND
10
1.1
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Toluene
ND
1.0
0.17
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,2,3-Trichlorobenzene
ND
5.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,2,4-Trichlorobenzene
ND
1.0
0.19
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,3,5-Trichlorobenzene
ND
1.0
0.17
µg/L
I
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1, 1, 1 -Trichloroethane
ND
1.0
0.13
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:45
EEH
1,1,2-Trichloroethane
ND
1.0
0.24
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:45
EEH
Trichloroethylene
3.5
1.0
0.20
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Trichlorofluoromethane (Freon 11)
ND
2.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,2,3-Trichloropropane
ND
2.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.20
µg/L
1
SW-8468260B
12/10/18
12/13/18 0:45
EEH
(Freon 113)
1,2,4-Trimethylbenzene
ND
1.0
0.18
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
1,3,5-Trimethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Vinyl Chloride
ND
2.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
m+p Xylene
ND
2.0
0.26
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
o-Xylene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/13/18 0:45
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
85.4
70-130
12/13/18 0:45
Toluene-d8
95.6
70-130
12/13/18 0:45
4-Bromofluorobenzene
97.4
70-130
12/13/18 0:45
Page 23 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: DUP-GW-1 Sampled: 12/5/2018 00:00
Samnle ID: 18L0322-04
Samnle Matrix: Ground Water
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Acenaphthylene
ND
5.5
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Acetophenone
ND
11
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Aniline
ND
5.5
2.7
µg/L
1
V-04
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Anthracene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Benzidine
ND
22
11
µg/L
1
L-04, R-05, V-04,
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
V-05
Benzo(a)anthracene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Benzo(a)pyrene
ND
5.5
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Benzo(b)fluoranthene
ND
5.5
1.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Benzo(g,h,i)perylene
ND
5.5
2.4
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Benzo(k)fluoranthene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Benzoic Acid
ND
11
2.2
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Bis(2-chloroethoxy)methane
ND
11
1.9
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Bis(2-chloroethyl)ether
ND
11
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Bis(2-chloroisopropyl)ether
ND
11
2.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Bis(2-Ethylhexyl)phthalate
ND
11
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
4-Bromophenylphenylether
ND
11
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Butylbenzylphthalate
ND
11
2.1
µg/L
1
R-05
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Carbazole
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
4-Chloroaniline
ND
11
1.7
µg/L
1
V-34
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
4-Chloro-3-methylphenol
ND
11
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2-Chloronaphthalene
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2-Chlorophenol
ND
11
1.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
4-Chlorophenylphenylether
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Chrysene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Dibenz(a,h)anthracene
ND
5.5
2.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Dibenzofman
ND
5.5
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Di-n-butylphthalate
ND
11
2.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
1,2-Dichlorobenzene
ND
5.5
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
1,3-Dichlorobenzene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
1,4-Dichlorobenzene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
3,3-Dichlorobenzidine
ND
11
2.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2,4-Dichlorophenol
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Diethylphthalate
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2,4-Dimethylphenol
ND
11
4.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Dimethylphthalate
ND
11
1.7
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
4,6-Dinitro-2-methylphenol
ND
11
2.2
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2,4-Dinitrophenol
ND
11
3.7
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2,4-Dinitrotoluene
ND
11
2.0
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2,6-Dinitrotoluene
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Di-n-octylphthalate
ND
11
2.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
1,2-Diphenylhydrazine/Azobenzene
ND
11
2.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Fluoranthene
ND
5.5
2.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Page 24 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: DUP-GW-1 Sampled: 12/5/2018 00:00
Sample ID: 18L0322-04
Samnle Matrix: Ground Water
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Flumene
ND
5.5
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Hexachlorobenzene
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Hexachlorobutadiene
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Hexachlorocyclopentadiene
ND
11
2.1
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Hexachloroethane
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Indeno(1,2,3-cd)pyrene
ND
5.5
2.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Isophorone
ND
11
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
1-Methylnaphthalene
ND
5.5
2.0
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2-Methylnaphthalene
ND
5.5
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2-Methylphenol
ND
11
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
3/4-Methylphenol
ND
11
1.3
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Naphthalene
ND
5.5
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2-Nitroaniline
ND
11
2.4
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
3-Nitroaniline
ND
11
2.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
4-Nitroaniline
ND
11
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Nitrobenzene
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2-Nitrophenol
ND
11
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
4-Nitrophenol
ND
11
1.2
µg/L
I
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
N-Nitrosodimethylamine
ND
11
1.7
µg/L
I
L-04
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
N-Nitrosodiphenylamine/Diphenylamine
ND
11
2.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
N-Nitrosodi-n-propylamine
ND
11
1.9
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Pentachloronitrobenzene
ND
11
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Pentachlorophenol
ND
11
1.2
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Phenanthrene
ND
5.5
1.5
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Phenol
ND
11
1.1
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Pyrene
ND
5.5
1.7
µg/L
1
R-05
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Pyridine
ND
5.5
2.3
µg/L
1
V-05
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
1,2,4,5-Texachlorobenzene
ND
11
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
1,2,4-Trichlorobenzene
ND
5.5
1.8
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2,4,5-Trichlorophenol
ND
11
1.7
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
2,4,6-Trichlorophenol
ND
11
1.6
µg/L
1
SW-846 8270D
12/11/18
12/12/18 19:47
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
48.8
15-110
12/12/18 19:47
Phenol-d6
37.0
15-110
12/12/18 19:47
Nitrobenzene-d5
69.7
30-130
12/12/18 19:47
2-Fluorobiphenyl
57.6
30-130
12/12/18 19:47
2,4,6-Tribromophenol
72.2
15-110
12/12/18 19:47
p-Terphenyl-dl4
74.6
30-130
12/12/18 19:47
Page 25 of 54

Table of Contents
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ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: DUP-GW-1
Samnle ID: 18L0322-04
Samnle Matrix: Ground Water
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Description:
Sampled: 12/5/2018 00:00
Work Order: 18L0322
Metals Analyses (Total)
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
ND
0.80
0.72
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:41
WSD
Barium
32
20
11
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:41
WSD
Cadmium
ND
1.0
0.14
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:41
WSD
Chromium
2.7
2.0
0.86
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:41
WSD
Lead
ND
2.0
0.48
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:41
WSD
Mercury
0.000069 0.00010
0.000034
mg/L
1 J
SW-846 7470A
12/12/18
12/13/18 11:37
AJL
Selenium
ND
10
2.8
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:41
WSD
Silver
ND
1.0
0.15
µg/L
2
SW-846 6020B
12/10/18
12/11/18 13:41
WSD
Page 26 of 54

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: Trip Blank-1 Sampled: 12/5/2018 00:00
Sample ID: 18L0322-05
Samnle Matrix: Trin Blank Water
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
50
9.7
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Acrylonitrile
ND
5.0
0.58
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
tert-Amyl Methyl Ether (TAME)
ND
0.50
0.11
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Benzene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Bromobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Bromochloromethane
ND
1.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Bromodichloromethane
ND
0.50
0.30
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Bromoform
ND
2.0
0.21
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Bromomethane
ND
2.0
0.94
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
2-Butanone (MEK)
ND
20
2.4
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
tert-Butyl Alcohol (TBA)
ND
20
2.2
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
n-Butylbenzene
ND
1.0
0.15
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
sec-Butylbenzene
ND
1.0
0.13
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
tert-Butylbenzene
ND
1.0
0.12
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
tert-Butyl Ethyl Ether (TBEE)
ND
0.50
0.095
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Carbon Disulfide
ND
4.0
1.0
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Carbon Tetrachloride
ND
5.0
0.25
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Chlorobenzene
ND
1.0
0.16
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Chlorodibromomethane
ND
0.50
0.10
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Chloroethane
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Chloroform
ND
2.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Chloromethane
ND
2.0
0.55
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
2-Chlomtoluene
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
4-Chlomtoluene
ND
1.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2-Dibromo-3-chloropropane (DBCP)
ND
5.0
0.37
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2-Dibromoethane (EDB)
ND
0.50
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Dibromomethane
ND
1.0
0.16
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,3-Dichlorobenzene
ND
1.0
0.17
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,4-Dichlorobenzene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
trans-1,4-Dichloro-2-butene
ND
2.0
0.31
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Dichlorodifluoromethane (Freon 12)
ND
2.0
0.28
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,1-Dichloroethane
ND
1.0
0.16
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2-Dichloroethane
ND
1.0
0.19
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1, 1 -Dichloroethylene
ND
1.0
0.21
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
cis-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
trans-1,2-Dichloroethylene
ND
1.0
0.15
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2-Dichloropropane
ND
1.0
0.13
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,3-Dichloropropane
ND
0.50
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
2,2-Dichloropropane
ND
1.0
0.21
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1, 1 -Dichloropropene
ND
2.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
cis-1,3-Dichloropropene
ND
0.50
0.12
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
trans-1,3-Dichloropropene
ND
0.50
0.11
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Diethyl Ether
ND
2.0
0.22
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Page 27 of 54

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Project Location: Charlotte, NC Sample Description: Work Order: 18L0322
Date Received: 12/6/2018
Field Sample #: Trip Blank-1 Sampled: 12/5/2018 00:00
Samnle ID: 18L0322-05
Samnle Matrix: Trin Blank Water
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (RIPE)
ND
0.50
0.18
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,4-Dioxane
ND
50
26
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Ethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Hexachlorobutadiene
ND
0.60
0.59
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
2-Hexanone (MBK)
ND
10
1.5
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Isopropylbenzene (Cumene)
ND
1.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
p-Isopropyltoluene (p-Cymene)
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Methyl tert-Butyl Ether (MTBE)
ND
1.0
0.090
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Methylene Chloride
ND
5.0
3.2
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
4-Methyl-2-pentanone (MIBK)
ND
t0
1.5
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Naphthalene
ND
2.0
0.12
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
n-Propylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Styrene
ND
1.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1, 1, 1,2-Tetrachloroethane
ND
1.0
0.12
µg/L
1
SW-8468260B
12/10/18
12/12/18 21:14
EEH
1,1,2,2-Tetrachloroethane
ND
0.50
0.16
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Tetrachloroethylene
ND
1.0
0.27
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Tetrahydrofuran
ND
10
1.1
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Toluene
ND
1.0
0.17
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2,3-Trichlorobenzene
ND
5.0
0.14
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2,4-Trichlorobenzene
ND
1.0
0.19
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,3,5-Trichlorobenzene
ND
1.0
0.17
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1, 1, 1 -Trichloroethane
ND
1.0
0.13
µg/L
I
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,1,2-Trichloroethane
ND
1.0
0.24
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Trichloroethylene
ND
1.0
0.20
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Trichlorofluoromethane (Freon 11)
ND
2.0
0.15
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,2,3-Trichloropropane
ND
2.0
0.22
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.0
0.20
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
(Freon 113)
1,2,4-Trimethylbenzene
ND
1.0
0.18
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
1,3,5-Trimethylbenzene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Vinyl Chloride
ND
2.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
m+p Xylene
ND
2.0
0.26
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
o-Xylene
ND
1.0
0.13
µg/L
1
SW-846 8260B
12/10/18
12/12/18 21:14
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
86.4
70-130
12/12/18 21:14
Toluene-d8
95.0
70-130
12/12/18 21:14
4-Bromofluorobenzene
99.8
70-130
12/12/18 21:14
Page 28 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3005A-SW-846 6020B
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
18L0322-01 [TMW-1]
B218876
50.0
50.0
12/10/18
18L0322-02 [TMW-2]
B218876
50.0
50.0
12/10/18
18L0322-03 [TMW-3]
B218876
50.0
50.0
12/10/18
18L0322-04 [DUP-GW-1]
B218876
50.0
50.0
12/10/18
Prep Method: SW-846 7470A Prep-SW-846 7470A
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
18L0322-01 [TMW-1]
B219057
6.00
6.00
12/12/18
18L0322-02 [TMW-2]
B219057
6.00
6.00
12/12/18
18L0322-03 [TMW-3]
B219057
6.00
6.00
12/12/18
18L0322-04 [DUP-GW-1]
B219057
6.00
6.00
12/12/18
Prep Method: SW-846 5030B-SW-846 8260B
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
18L0322-01 [TMW-1]
B218882
0.1
5.00
12/10/18
18L0322-02 [TMW-2]
B218882
5
5.00
12/10/18
18L0322-03 [TMW-3]
B218882
5
5.00
12/10/18
18L0322-04 [DUP-GW-1]
B218882
5
5.00
12/10/18
18L0322-05[Trip Blank-1]
B218882
5
5.00
12/10/18
Prep Method: SW-846 3510C-SW-846 8270D
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
18L0322-01 [TMW-1]
B218940
900
1.00
12/11/18
18L0322-02 [TMW-2]
B218940
960
1.00
12/11/18
18L0322-04 [DUP-GW-1]
B218940
910
1.00
12/11/18
Prep Method: SW-846 3510C-SW-846 8270D
Lab Number [Field ID]
Batch
Initial ImLl
Final [mL]
Date
18L0322-03 [TMW-3]
B219039
980
1.00
12/12/18
Page 29 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218882 - SW-846 5030B
Blank (B218882-BLK1) Prepared: 12/10/18 Analyzed: 12/12/18
Acetone
ND
50
µg/L
Acrylonitrile
ND
5.0
µg/L
tert-Amyl Methyl Ether (TAME)
ND
0.50
µg/L
Benzene
ND
1.0
µg/L
Bromobenzene
ND
1.0
µg/L
Bromochloromethane
ND
1.0
µg/L
Bromodichloromethane
ND
0.50
µg/L
Bromoform
ND
1.0
µg/L
Bromomethane
ND
2.0
µg/L
2-Butanone (MEK)
ND
20
µg/L
tert-Butyl Alcohol (TBA)
ND
20
µg/L
n-Butylbenzene
ND
1.0
µg/L
sec-Butylbenzene
ND
1.0
µg/L
tert-Butylbenzene
ND
1.0
µg/L
tert-Butyl Ethyl Ether (TBEE)
ND
0.50
µg/L
Carbon Disulfide
ND
4.0
µg/L
Carbon Tetrachloride
ND
5.0
µg/L
Chlorobenzene
ND
1.0
µg/L
Chlorodibromomethane
ND
0.50
µg/L
Chloroethane
ND
2.0
µg/L
Chloroform
ND
2.0
µg/L
Chloromethane
ND
2.0
µg/L
2-Chlorotoluene
ND
1.0
µg/L
4-Chlorotoluene
ND
1.0
µg/L
1,2-Dibromo-3-chloropropane (DBCP)
ND
5.0
µg/L
1,2-Dibromoethane (EDB)
ND
0.50
µg/L
Dibromomethane
ND
1.0
µg/L
1,2-Dichlorobenzene
ND
1.0
µg/L
1,3-Dichlorobenzene
ND
1.0
µg/L
1,4-Dichlorobenzene
ND
1.0
µg/L
trans-1,4-Dichloro-2-butene
ND
2.0
µg/L
Dichlorodifluoromethane (Freon 12)
ND
2.0
µg/L
1,1-Dichloroethane
ND
1.0
µg/L
1,2-Dichloroethane
ND
1.0
µg/L
1,1-Dichloroethylene
ND
1.0
µg/L
cis-1,2-Dichloroethylene
ND
1.0
µg/L
trans-1,2-Dichloroethylene
ND
1.0
µg/L
1,2-Dichloropropane
ND
1.0
µg/L
1,3-Dichloropropane
ND
0.50
µg/L
2,2-Dichloropropane
ND
1.0
µg/L
1,1-Dichloropropene
ND
2.0
µg/L
cis-1,3-Dichloropropene
ND
0.50
µg/L
trans- 1, 3 -Dichloropropene
ND
0.50
µg/L
Diethyl Ether
ND
2.0
µg/L
Diisopropyl Ether (RIPE)
ND
0.50
µg/L
1,4-Dioxane
ND
50
µg/L
Ethylbenzene
ND
1.0
µg/L
Hexachlorobutadiene
ND
0.60
µg/L
2-Hexanone (MBK)
ND
10
µg/L
Isopropylbenzene (Cumene)
ND
1.0
µg/L
p-Isopropyltoluene (p-Cymene)
ND
1.0
µg/L
Methyl tert-Butyl Ether (MTBE)
ND
1.0
µg/L
Page 30 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218882 - SW-846 5030B
Blank (B218882-BLK1)
Prepared: 12/10/18 Analyzed: 12/12/18
Methylene Chloride
ND
5.0
µg/L
4-Methyl-2-pentanone (MIBK)
ND
10
µg/L
Naphthalene
ND
2.0
µg/L
n-Propylbenzene
ND
1.0
µg/L
Styrene
ND
1.0
µg/L
1, 1, 1,2-Tetrachloroethane
ND
1.0
µg/L
1,1,2,2-Tetrachloroethane
ND
0.50
µg/L
Tetrachloroethylene
ND
1.0
µg/L
Tetrahydrofuran
ND
10
µg/L
Toluene
ND
1.0
µg/L
1,2,3-Trichlorobenzene
ND
5.0
µg/L
1,2,4-Trichlorobenzene
ND
1.0
µg/L
1,3,5-Trichlorobenzene
ND
1.0
µg/L
1, 1, 1 -Trichloroethane
ND
1.0
µg/L
1,1,2-Trichloroethane
ND
1.0
µg/L
Trichloroethylene
ND
1.0
µg/L
Trichlorofluoromethane (Freon 11)
ND
2.0
µg/L
1,2,3-Trichloropropane
ND
2.0
µg/L
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
1.0
µg/L
113)
1,2,4-Trimethylbenzene
ND
1.0
µg/L
1,3,5-Trimethylbenzene
ND
1.0
µg/L
Vinyl Chloride
ND
2.0
µg/L
m+p Xylene
ND
2.0
µg/L
o-Xylene
ND
1.0
µg/L
Surrogate:l,2-Dichloroethane-d4
21.2
µg/L
25.0
84.7
70-130
Surrogate: Toluene-d8
23.9
µg/L
25.0
95.8
70-130
Surrogate:4-Bromofluorobenzene
24.5
µg/L
25.0
97.8
70-130
LCS (B218882-BS1)
Prepared: 12/10/18 Analyzed: 12/12/18
Acetone
76.9
50
µg/L
100
76.9
70-160
t
Acrylonitrile
8.39
5.0
µg/L
10.0
83.9
70-130
tert-Amyl Methyl Ether (TAME)
8.98
0.50
µg/L
10.0
89.8
70-130
Benzene
8.93
1.0
µg/L
10.0
89.3
70-130
Bromobenzene
10.1
1.0
µg/L
10.0
101
70-130
Bromochloromethane
9.11
1.0
µg/L
10.0
91.1
70-130
Bromodichloromethane
9.55
0.50
µg/L
10.0
95.5
70-130
Bromoform
10.2
1.0
µg/L
10.0
102
70-130
Bromomethane
8.39
2.0
µg/L
10.0
85.9
40-160
t
2-Butanone (MEK)
77.1
20
µg/L
100
77.1
40-160
t
tert-Butyl Alcohol(TBA)
86.0
20
µg/L
100
86.0
40-160
t
n-Butylbenzene
10.0
1.0
µg/L
10.0
100
70-130
sec-Butylbenzene
10.6
1.0
µg/L
10.0
106
70-130
tert-Butylbenzene
10.9
1.0
µg/L
10.0
105
70-130
tert-Butyl Ethyl Ether (TBEE)
8.36
0.50
µg/L
10.0
83.6
70-130
Carbon Disulfide
9.54
4.0
µg/L
10.0
95.4
70-130
Carbon Tetrachloride
8.63
5.0
µg/L
10.0
86.3
70-130
Chlorobenzene
10.8
1.0
µg/L
10.0
108
70-130
Chlorodibromomethane
10.1
0.50
µg/L
10.0
101
70-130
Chloroethane
8.39
2.0
µg/L
10.0
83.5
70-130
Chloroform
9.32
2.0
µg/L
10.0
93.2
70-130
Chloromethane
6.34
2.0
µg/L
10.0
63.4
40-160
2-Chlorotoluene
10.1
1.0
µg/L
10.0
101
70-130
Page 31 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218882 - SW-846 5030B
LCS (B218882-BSI) Prepared: 12/10/18 Analyzed: 12/12/18
4-Chlorotoluene
10.1
1.0
µg/L
10.0
101
70-130
1,2-Dibromo-3-chloropropane(DBCP)
8.99
5.0
µg/L
10.0
89.9
70-130
1,2-Dibromoethane (EDB)
10.0
0.50
µg/L
10.0
100
70-130
Dibromomethane
10.2
1.0
µg/L
10.0
102
70-130
1,2-Dichlorobenzene
10.6
1.0
µg/L
10.0
106
70-130
1,3-Dichlorobenzene
11.0
1.0
µg/L
10.0
110
70-130
1,4-Dichlorobenzene
10.4
1.0
µg/L
10.0
104
70-130
trans-1,4-Dichloro-2-butene
9.70
2.0
µg/L
10.0
97.0
70-130
Dichlorodifluoromethane(Freon 12)
6.11
2.0
µg/L
10.0
61.1
40-160
1,1-Dichloroethane
8.98
1.0
µg/L
10.0
89.8
70-130
1,2-Dichloroethane
8.98
1.0
µg/L
10.0
89.8
70-130
1,1-Dichloroethylene
8.48
1.0
µg/L
10.0
84.8
70-130
cis-1,2-Dichloroethylene
8.38
1.0
µg/L
10.0
83.8
70-130
trans-1,2-Dichloroethylene
8.33
1.0
µg/L
10.0
83.3
70-130
1,2-Dichloropropane
9.48
1.0
µg/L
10.0
94.8
70-130
1,3-Dichloropropane
9.03
0.50
µg/L
10.0
90.3
70-130
2,2-Dichloropropane
8.69
1.0
µg/L
10.0
86.9
40-130
1,1-Dichloropropene
8.36
2.0
µg/L
10.0
83.6
70-130
cis- 1,3 -Dichloropropene
9.24
0.50
µg/L
10.0
92.4
70-130
trans- 1, 3 -Dichloropropene
9.34
0.50
µg/L
10.0
93.4
70-130
Diethyl Ether
8.62
2.0
µg/L
10.0
86.2
70-130
Diisopropyl Ether(DIPE)
8.26
0.50
µg/L
10.0
82.6
70-130
1,4-Dioxane
105
50
µg/L
100
105
40-130
Ethylbenzene
10.9
1.0
µg/L
10.0
109
70-130
Hexachlorobutadiene
11.7
0.60
µg/L
10.0
117
70-130
2-Hexanone (MBK)
82.7
10
µg/L
100
82.7
70-160
Isopropylbenzene(Cumene)
11.2
1.0
µg/L
10.0
112
70-130
p-Isopropyltoluene(p-Cymene)
10.5
1.0
µg/L
10.0
105
70-130
Methyl tert-Butyl Ether (MTBE)
8.62
1.0
µg/L
10.0
86.2
70-130
Methylene Chloride
7.34
5.0
µg/L
10.0
73.4
70-130
4-Methyl-2-pentanone (MIBK)
84.3
10
µg/L
100
84.3
70-160
Naphthalene
9.92
2.0
µg/L
10.0
99.2
40-130
n-Propylbenzene
10.0
1.0
µg/L
10.0
100
70-130
Styrene
10.7
1.0
µg/L
10.0
107
70-130
1, 1, 1,2-Tetrachloroethane
11.5
1.0
µg/L
10.0
115
70-130
1,1,2,2-Tetrachloroethane
11.2
0.50
µg/L
10.0
112
70-130
Tetrachloroethylene
11.2
1.0
µg/L
10.0
112
70-130
Tetrahydrofuran
8.62
10
µg/L
10.0
86.2
70-130
Toluene
9.76
1.0
µg/L
10.0
97.6
70-130
1,2,3-Trichlorobenzene
10.2
5.0
µg/L
10.0
102
70-130
1,2,4-Trichlorobenzene
10.4
1.0
µg/L
10.0
104
70-130
1,3,5-Trichlorobenzene
10.8
1.0
µg/L
10.0
108
70-130
1, 1, 1 -Trichloroethane
9.22
1.0
µg/L
10.0
92.2
70-130
1,1,2-Trichloroethane
10.2
1.0
µg/L
10.0
102
70-130
Trichloroethylene
9.90
1.0
µg/L
10.0
99.0
70-130
Trichlorofluoromethane (Freon 11)
8.25
2.0
µg/L
10.0
82.5
70-130
1,2,3-Trichloropropane
10.6
2.0
µg/L
10.0
106
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
10.2
1.0
µg/L
10.0
102
70-130
113)
1,2,4-Trimethylbenzene
9.54
1.0
µg/L
10.0
95.4
70-130
1,3,5-Trimethylbenzene
10.2
1.0
µg/L
10.0
102
70-130
Vinyl Chloride
7.29
2.0
µg/L
10.0
72.9
40-160
f
t
t
t
t
t
J
Page 32 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218882 - SW-846 5030B
LCS (B218882-BSI)
Prepared: 12/10/18 Analyzed: 12/12/18
m+p Xylene
21.0
2.0
µg/L
20.0
105
70-130
o-Xylene
10.4
1.0
µg/L
10.0
104
70-130
Surrogate:l,2-Dichloroethane-d4
21.1
µg/L
25.0
84.6
70-130
Surrogate: Toluene-d8
24.5
µg/L
25.0
98.0
70-130
Surrogate:4-Bromofluorobenzene
24.6
µg/L
25.0
98.6
70-130
LCS Dup (B218882-BSDI)
Prepared: 12/10/18 Analyzed: 12/12/18
Acetone
68.4
50
µg/L
100
68.4 *
70-160
11.7
25
L-07 t
Acrylonitrile
7.51
5.0
µg/L
10.0
75.1
70-130
11.1
25
tert-Amyl Methyl Ether (TAME)
8.81
0.50
µg/L
10.0
88.1
70-130
1.91
25
Benzene
9.03
1.0
µg/L
10.0
90.3
70-130
1.11
25
Bromobenzene
10.6
1.0
µg/L
10.0
106
70-130
4.16
25
Bromochloromethane
9.55
1.0
µg/L
10.0
95.5
70-130
4.72
25
Bromodichloromethane
9.41
0.50
µg/L
10.0
94.1
70-130
1.48
25
Bromoform
10.5
1.0
µg/L
10.0
105
70-130
2.22
25
Bromomethane
10.8
2.0
µg/L
10.0
108
40-160
22.8
25
f
2-Butanone(MEK)
83.4
20
µg/L
100
83.4
40-160
7.87
25
t
tert-Butyl Alcohol (TBA)
72.8
20
µg/L
100
72.8
40-160
16.6
25
t
n-Butylbenzene
10.4
1.0
µg/L
10.0
104
70-130
3.81
25
sec-Butylbenzene
10.8
1.0
µg/L
10.0
108
70-130
1.86
25
tert-Butylbenzene
10.9
1.0
µg/L
10.0
109
70-130
4.02
25
tert-Butyl Ethyl Ether (TBEE)
8.24
0.50
µg/L
10.0
82.4
70-130
1.45
25
Carbon Disulfide
9.15
4.0
µg/L
10.0
91.5
70-130
4.17
25
Carbon Tetrachloride
8.88
5.0
µg/L
10.0
88.8
70-130
2.86
25
Chlorobenzene
11.3
1.0
µg/L
10.0
113
70-130
3.89
25
Chlorodibromomethane
10.1
0.50
µg/L
10.0
101
70-130
0.396
25
Chloroethane
9.19
2.0
µg/L
10.0
91.9
70-130
9.58
25
Chloroform
9.27
2.0
µg/L
10.0
92.7
70-130
0.538
25
Chloromethane
6.74
2.0
µg/L
10.0
67.4
40-160
6.12
25
t
2-Chlorotoluene
10.9
1.0
µg/L
10.0
109
70-130
7.41
25
4-Chlorotoluene
10.5
1.0
µg/L
10.0
105
70-130
4.18
25
1,2-Dibromo-3-chloropropane (DBCP)
8.24
5.0
µg/L
10.0
82.4
70-130
8.71
25
1,2-Dibromoethane (EDB)
10.1
0.50
µg/L
10.0
101
70-130
1.19
25
Dibromomethane
9.84
1.0
µg/L
10.0
98.4
70-130
3.30
25
1,2-Dichlorobenzene
11.0
1.0
µg/L
10.0
110
70-130
3.89
25
1,3-Dichlorobenzene
11.3
1.0
µg/L
10.0
113
70-130
2.33
25
1,4-Dichlorobenzene
10.7
1.0
µg/L
10.0
107
70-130
2.75
25
trans-1,4-Dichloro-2-butene
8.77
2.0
µg/L
10.0
87.7
70-130
10.1
25
Dichlorodifluoromethane (Freon 12)
6.37
2.0
µg/L
10.0
63.7
40-160
4.17
25
t
1, 1 -Dichloroethane
9.19
1.0
µg/L
10.0
91.9
70-130
2.31
25
1,2-Dichloroethane
8.97
1.0
µg/L
10.0
89.7
70-130
0.111
25
1,1-Dichloroethylene
8.67
1.0
µg/L
10.0
86.7
70-130
2.22
25
cis-1,2-Dichloroethylene
8.60
1.0
µg/L
10.0
86.0
70-130
2.59
25
trans-1,2-Dichloroethylene
8.67
1.0
µg/L
10.0
86.7
70-130
4.00
25
1,2-Dichloropropane
9.68
1.0
µg/L
10.0
96.8
70-130
2.09
25
1,3-Dichloropropane
8.96
0.50
µg/L
10.0
89.6
70-130
0.778
25
2,2-Dichloropropane
8.78
1.0
µg/L
10.0
87.8
40-130
1.03
25
t
1,1-Dichloropropene
8.77
2.0
µg/L
10.0
87.7
70-130
4.79
25
cis- 1,3 -Dichloropropene
9.33
0.50
µg/L
10.0
93.3
70-130
0.969
25
trans- l,3-Dichloropropene
9.61
0.50
µg/L
10.0
96.1
70-130
2.85
25
Diethyl Ether
8.77
2.0
µg/L
10.0
87.7
70-130
1.73
25
Diisopropyl Ether(DIPE)
8.25
0.50
µg/L
10.0
82.5
70-130
0.121
25
Page 33 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218882 - SW-846 5030B
LCS Dup (B218882-BSD1) Prepared: 12/10/18 Analyzed: 12/12/18
1,4-Dioxane
86.8
50
µg/L
100
86.8
40-130
19.1
50
f #
Ethylbenzene
112
1.0
µg/L
10.0
112
70-130
2.45
25
Hexachlorobutadiene
12.3
0.60
µg/L
10.0
123
70-130
4.82
25
2-Hexanone (MBK)
72.5
10
µg/L
100
72.5
70-160
13.2
25
f
Isopropylbenzene(Cumene)
11.6
1.0
µg/L
10.0
116
70-130
3.60
25
p-Isopropyltoluene(p-Cymene)
10.7
1.0
µg/L
10.0
107
70-130
2.07
25
Methyl tert-Butyl Ether (MTBE)
8.67
1.0
µg/L
10.0
86.7
70-130
0.578
25
Methylene Chloride
7.56
5.0
µg/L
10.0
75.6
70-130
2.95
25
4-Methyl-2-pentanone (MIBK)
75.7
10
µg/L
100
75.7
70-160
10.8
25
t
Naphthalene
8.78
2.0
µg/L
10.0
87.8
40-130
12.2
25
f
n-Propylbenzene
10.4
1.0
µg/L
10.0
104
70-130
4.21
25
Styrene
11.0
1.0
µg/L
10.0
110
70-130
2.94
25
1, 1, 1,2-Tetrachloroethane
11.8
1.0
µg/L
10.0
118
70-130
3.35
25
1,1,2,2-Tetrachloroethane
10.6
0.50
µg/L
10.0
106
70-130
5.33
25
Tetrachloroethylene
11.3
1.0
µg/L
10.0
113
70-130
0.712
25
Tetrahydroforan
8.16
10
µg/L
10.0
81.6
70-130
5.48
25
J
Toluene
10.1
1.0
µg/L
10.0
101
70-130
3.03
25
1,2,3-Trichlorobenzene
10.0
5.0
µg/L
10.0
100
70-130
1.39
25
1,2,4-Trichlorobenzene
10.1
1.0
µg/L
10.0
101
70-130
3.12
25
1,3,5-Trichlorobenzene
11.1
1.0
µg/L
10.0
ill
70-130
3.38
25
1, 1, 1 -Trichloroethane
9.43
1.0
µg/L
10.0
94.3
70-130
2.25
25
1,1,2-Trichloroethane
10.2
1.0
µg/L
10.0
102
70-130
0.980
25
Trichloroethylene
10.3
1.0
µg/L
10.0
103
70-130
4.25
25
Trichlorofluoromethane (Freon 11)
8.27
2.0
µg/L
10.0
82.7
70-130
0.242
25
1,2,3-Trichloropropane
9.36
2.0
µg/L
10.0
93.6
70-130
12.8
25
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
10.4
1.0
µg/L
10.0
104
70-130
2.72
25
113)
1,2,4-Trimethylbenzene
9.93
1.0
µg/L
10.0
99.3
70-130
4.01
25
1,3,5-Trimethylbenzene
10.5
1.0
µg/L
10.0
105
70-130
2.70
25
Vinyl Chloride
7.58
2.0
µg/L
10.0
75.8
40-160
3.90
25
t
m+p Xylene
21.7
2.0
µg/L
20.0
109
70-130
3.56
25
o-Xylene
10.6
1.0
µg/L
10.0
106
70-130
1.71
25
Surrogate:l,2-Dichloroethane-d4
21.1
µg/L
25.0
84.7
70-130
Surrogate: Toluene-d8
24.2
µg/L
25.0
96.8
70-130
Surrogate:4-Bromofluorobenzene
25.0
µg/L
25.0
100
70-130
Page 34 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218940 - SW-846 3510C
Blank (B218940-BLK1) Prepared: 12/11/18 Analyzed: 12/12/18
Acenaphthene
ND
5.0
µg/L
Acenaphthylene
ND
5.0
µg/L
Acetophenone
ND
10
µg/L
Aniline
ND
5.0
µg/L
Anthracene
ND
5.0
µg/L
Benzidine
ND
20
µg/L
Benzo(a)anthracene
ND
5.0
µg/L
Benzo(a)pyrene
ND
5.0
µg/L
Benzo(b)fluoranthene
ND
5.0
µg/L
Benzo(g,h,i)perylene
ND
5.0
µg/L
Benzo(k)fluoranthene
ND
5.0
µg/L
Benzoic Acid
ND
10
µg/L
Bis(2-chloroethoxy)methane
ND
10
µg/L
Bis(2-chloroethyl)ether
ND
10
µg/L
Bis(2-chloroisopropyl)ether
ND
10
µg/L
Bis(2-Ethylhexyl)phthalate
ND
10
µg/L
4-Bromophenylphenylether
ND
10
µg/L
Butylbenzylphthalate
ND
10
µg/L
Carbazole
ND
10
µg/L
4-Chloroaniline
ND
10
µg/L
4-Chloro-3-methylphenol
ND
10
µg/L
2-Chloronaphthalene
ND
10
µg/L
2-Chlorophenol
ND
10
µg/L
4-Chlorophenylphenylether
ND
10
µg/L
Chrysene
ND
5.0
µg/L
Dibenz(a,h)anthracene
ND
5.0
µg/L
Dibenzofuran
ND
5.0
µg/L
Di-n-butylphthalate
ND
10
µg/L
1,2-Dichlorobenzene
ND
5.0
µg/L
1,3-Dichlorobenzene
ND
5.0
µg/L
1,4-Dichlorobenzene
ND
5.0
µg/L
3,3-Dichlorobenzidine
ND
10
µg/L
2,4-Dichlorophenol
ND
10
µg/L
Diethylphthalate
ND
10
µg/L
2,4-Dimethylphenol
ND
10
µg/L
Dimethylphthalate
ND
10
µg/L
4,6-Dinitro-2-methylphenol
ND
10
µg/L
2,4-Dinitrophenol
ND
10
µg/L
2,4-Dinitrotoluene
ND
10
µg/L
2,6-Dinitrotoluene
ND
10
µg/L
Di-n-octylphthalate
ND
10
µg/L
1,2-Diphenylhydrazine/Azobenzene
ND
10
µg/L
Fluoranthene
ND
5.0
µg/L
Fluorene
ND
5.0
µg/L
Hexachlorobenzene
ND
10
µg/L
Hexachlorobutadiene
ND
10
µg/L
Hexachlorocyclopentadiene
ND
10
µg/L
Hexachloroethane
ND
10
µg/L
Indeno(1,2,3-cd)pyrene
ND
5.0
µg/L
Isophorone
ND
10
µg/L
1-Methylnaphthalene
ND
5.0
µg/L
2-Methylnaphthalene
ND
5.0
µg/L
V-04
L-04, R-05, V-04,
V-05
V-05
R-05
V-34
V-05
Page 35 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218940 - SW-846 3510C
Blank (B218940-BLK1) Prepared: 12/11/18 Analyzed: 12/12/18
2-Methylphenol
ND
10
µg/L
3/4-Methylphenol
ND
10
µg/L
Naphthalene
ND
5.0
µg/L
2-Nitroaniline
ND
10
µg/L
3-Nitroaniline
ND
10
µg/L
4-Nitroaniline
ND
10
µg/L
Nitrobenzene
ND
10
µg/L
2-Nitrophenol
ND
10
µg/L
4-Nitrophenol
ND
10
µg/L
N-Nitrosodimethylamine
ND
10
µg/L
L-04
N-Nitrosodiphenylamine/Diphenylamine
ND
10
µg/L
N-Nitrosodi-n-propylamine
ND
10
µg/L
Pentachloronitrobenzene
ND
10
µg/L
Pentachlorophenol
ND
10
µg/L
Phenanthrene
ND
5.0
µg/L
Phenol
ND
10
µg/L
Pyrene
ND
5.0
µg/L
R-05
Pyridine
ND
5.0
µg/L
V-05
1,2,4,5-Tetrachlorobenzene
ND
10
µg/L
1,2,4-Trichlorobenzene
ND
5.0
µg/L
2,4,5-Trichlorophenol
ND
10
µg/L
2,4,6-Trichlorophenol
ND
10
µg/L
Surrogate:2-Fluorophenol
82.6
µg/L
200
41.3
15-110
Surrogate: Phenol-d6
61.2
µg/L
200
30.6
15-110
Surrogate: Nitrobenzene-d5
74.0
µg/L
100
74.0
30-130
Surrogate:2-Fluorobiphenyl
60.7
µg/L
100
60.7
30-130
Surrogate: 2,4,6-Tribromophenol
162
µg/L
200
80.9
15-110
Surrogate:p-Terphenyl-dl4
78.4
µg/L
100
78.4
30-130
LCS (B218940-BSI)
Prepared: 12/11/18 Analyzed: 12/12/18
Acenaphthene
35.2
5.0
µg/L
50.0
70.4
40-140
Acenaphthylene
35.5
5.0
µg/L
50.0
71.1
40-140
Acetophenone
36.6
10
µg/L
50.0
73.2
40-140
Aniline
25.0
5.0
µg/L
50.0
50.0
40-140
Anthracene
37.5
5.0
µg/L
50.0
75.1
40-140
Benzidine
14.3
20
µg/L
50.0
28.7 *
40-140
Benzo(a)anthracene
38.2
5.0
µg/L
50.0
76.5
40-140
Benzo(a)pyrene
40.0
5.0
µg/L
50.0
80.1
40-140
Benzo(b)fluoranthene
38.2
5.0
µg/L
50.0
76.4
40-140
Benzo(g,h,i)perylene
31.9
5.0
µg/L
50.0
63.8
40-140
Benzo(k)fluoranthene
37.9
5.0
µg/L
50.0
75.8
40-140
Benzoic Acid
23.3
10
µg/L
50.0
46.6
10-130
Bis(2-chloroethoxy)methane
42.1
10
µg/L
50.0
84.3
40-140
Bis(2-chloroethyl)ether
37.5
10
µg/L
50.0
75.1
40-140
Bis(2-chloroisopropyl)ether
46.8
10
µg/L
50.0
93.7
40-140
Bis(2-Ethylhexyl)phthalate
39.5
10
µg/L
50.0
79.1
40-140
4-Bromophenylphenylether
37.1
10
µg/L
50.0
74.2
40-140
Butylbenzylphthalate
56.9
10
µg/L
50.0
114
40-140
Carbazole
37.3
10
µg/L
50.0
74.7
40-140
4-Chloroaniline
25.3
10
µg/L
50.0
50.7
40-140
4-Chloro-3-methylphenol
38.2
10
µg/L
50.0
76.4
30-130
2-Chloronaphthalene
32.2
10
µg/L
50.0
64.5
40-140
V-04
L-04, R-05, V-04,
V-05,J
V-05
t
R-05
V-34
Page 36 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218940 - SW-846 3510C
LCS (B218940-BSI) Prepared: 12/11/18 Analyzed: 12/12/18
2-Chlorophenol
32.5
10
µg/L
50.0
65.1
30-130
4-Chlorophenylphenylether
37.0
10
µg/L
50.0
74.0
40-140
Chrysene
35.4
5.0
µg/L
50.0
70.8
40-140
Dibenz(a,h)anthracene
31.2
5.0
µg/L
50.0
62.4
40-140
Dibenzofuran
36.6
5.0
µg/L
50.0
73.1
40-140
Di-n-butylphthalate
39.9
10
µg/L
50.0
79.8
40-140
1,2-Dichlorobenzene
32.7
5.0
µg/L
50.0
65.4
40-140
1,3-Dichlorobenzene
31.6
5.0
µg/L
50.0
63.2
40-140
1,4-Dichlorobenzene
31.4
5.0
µg/L
50.0
62.8
40-140
3,3-Dichlorobenzidine
39.2
10
µg/L
50.0
78.3
40-140
2,4-Dichlorophenol
36.3
10
µg/L
50.0
72.6
30-130
Diethylphthalate
37.3
10
µg/L
50.0
74.6
40-140
2,4-Dimethylphenol
32.2
10
µg/L
50.0
64.5
30-130
Dimethylphthalate
36.5
10
µg/L
50.0
73.0
40-140
4,6-Dinitro-2-methylphenol
42.8
10
µg/L
50.0
85.6
30-130
2,4-Dinitrophenol
43.6
10
µg/L
50.0
87.1
30-130
2,4-Dinitrotoluene
41.8
10
µg/L
50.0
83.5
40-140
2,6-Dinitrotoluene
43.1
10
µg/L
50.0
86.2
40-140
Di-n-octylphthalate
43.1
10
µg/L
50.0
86.1
40-140
1,2-Diphenylhydrazine/Azobenzene
38.4
10
µg/L
50.0
76.8
40-140
Fluoranthene
37.2
5.0
µg/L
50.0
74.4
40-140
Fluorene
36.8
5.0
µg/L
50.0
73.6
40-140
Hexachlorobenzene
35.8
10
µg/L
50.0
71.7
40-140
Hexachlorobutadiene
33.7
10
µg/L
50.0
67.4
40-140
Hexachlorocyclopentadiene
19.9
10
µg/L
50.0
39.9
30-140
V-05 t
Hexachloroethane
31.5
10
µg/L
50.0
63.0
40-140
Indeno(1,2,3-cd)pyrene
33.3
5.0
µg/L
50.0
66.5
40-140
Isophorone
39.1
10
µg/L
50.0
78.2
40-140
1-Methylnaphthalene
34.6
5.0
µg/L
50.0
69.2
40-140
2-Methylnaphthalene
37.9
5.0
µg/L
50.0
75.8
40-140
2-Methylphenol
32.8
10
µg/L
50.0
65.5
30-130
3/4-Methylphenol
29.7
10
µg/L
50.0
59.5
30-130
Naphthalene
34.9
5.0
µg/L
50.0
69.8
40-140
2-Nitroaniline
40.5
10
µg/L
50.0
81.1
40-140
3-Nitroaniline
33.6
10
µg/L
50.0
67.3
40-140
4-Nitroaniline
40.6
10
µg/L
50.0
81.3
40-140
Nitrobenzene
35.7
10
µg/L
50.0
71.5
40-140
2-Nitrophenol
40.8
10
µg/L
50.0
81.6
30-130
4-Nitrophenol
19.0
10
µg/L
50.0
38.0
10-130
t
N-Nitrosodimethylamine
18.4
10
µg/L
50.0
36.8
* 40-140
L-04
N-Nitrosodiphenylamine/Diphenylamine
37.9
10
µg/L
50.0
75.8
40-140
N-Nitrosodi-n-propylamine
36.1
10
µg/L
50.0
72.2
40-140
Pentachloronitrobenzene
40.2
10
µg/L
50.0
80.4
40-140
Pentachlorophenol
31.8
10
µg/L
50.0
63.7
30-130
Phenanthrene
36.7
5.0
µg/L
50.0
73.3
40-140
Phenol
15.8
10
µg/L
50.0
31.5
20-130
Pyrene
53.2
5.0
µg/L
50.0
106
40-140
R-05
Pyridine
11.8
5.0
µg/L
50.0
23.6
10-140
V-05
1,2,4,5-Tetrachlorobenzene
34.0
10
µg/L
50.0
68.0
40-140
1,2,4-Trichlorobenzene
33.5
5.0
µg/L
50.0
66.9
40-140
2,4,5-Trichlorophenol
35.6
10
µg/L
50.0
71.1
30-130
2,4,6-Trichlorophenol
35.6
10
µg/L
50.0
71.2
30-130
Page 37 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218940 - SW-846 3510C
LCS (B218940-BSI) Prepared: 12/11/18 Analyzed: 12/12/18
Surrogate:2-Fluorophenol
88.3
µg/L
200 44.2
15-110
Surrogate: Phenol-d6
66.8
µg/L
200 33.4
15-110
Surrogate: Nitrobenzene-d5
78.3
µg/L
100 78.3
30-130
Surrogate:2-Fluorobiphenyl
62.4
µg/L
100 62.4
30-130
Surrogate: 2,4,6-Tribromophenol
177
µg/L
200 88.3
15-110
Surrogate:p-Terphenyl-dl4
106
µg/L
100 106
30-130
LCS Dup (B218940-BSD1)
Prepared: 12/11/18 Analyzed: 12/12/18
Acenaphthene
35.9
5.0
µg/L
50.0
Acenaphthylene
36.1
5.0
µg/L
50.0
Acetophenone
36.6
10
µg/L
50.0
Aniline
26.6
5.0
µg/L
50.0
Anthracene
36.9
5.0
µg/L
50.0
Benzidine
9.25
20
µg/L
50.0
Benzo(a)anthracene
37.9
5.0
µg/L
50.0
Benzo(a)pyrene
40.1
5.0
µg/L
50.0
Benzo(b)fluoranthene
38.9
5.0
µg/L
50.0
Benzo(g,h,i)perylene
33.2
5.0
µg/L
50.0
Benzo(k)fluoranthene
38.4
5.0
µg/L
50.0
Benzoic Acid
23.0
10
µg/L
50.0
Bis(2-chloroethoxy)methane
43.0
10
µg/L
50.0
Bis(2-chloroethyl)ether
37.2
10
µg/L
50.0
Bis(2-chloroisopropyl)ether
46.5
10
µg/L
50.0
Bis(2-Ethylhexyl)phthalate
39.1
10
µg/L
50.0
4-Bromophenylphenylether
36.7
10
µg/L
50.0
Butylbenzylphthalate
42.0
10
µg/L
50.0
Carbazole
36.4
10
µg/L
50.0
4-Chloroaniline
24.5
10
µg/L
50.0
4-Chloro-3-methylphenol
37.2
10
µg/L
50.0
2-Chloronaphthalene
32.6
10
µg/L
50.0
2-Chorophenol
31.7
10
µg/L
50.0
4-Chlorophenylphenylether
36.9
10
µg/L
50.0
Chrysene
34.6
5.0
µg/L
50.0
Dibenz(a,h)anthracene
32.6
5.0
µg/L
50.0
Dibenzofuran
37.1
5.0
µg/L
50.0
Di-n-butylphthalate
38.9
10
µg/L
50.0
1,2-Dichlorobenzene
32.5
5.0
µg/L
50.0
1,3-Dichlorobenzene
30.4
5.0
µg/L
50.0
1,4-Dichlorobenzene
30.7
5.0
µg/L
50.0
3,3-Dichlorobenzidine
38.8
10
µg/L
50.0
2,4-Dichlorophenol
36.4
10
µg/L
50.0
Diethylphthalate
38.3
10
µg/L
50.0
2,4-Dimethylphenol
32.1
10
µg/L
50.0
Dimethylphthalate
36.3
10
µg/L
50.0
4,6-Dinitro-2-methylphenol
43.6
10
µg/L
50.0
2,4-Dinitrophenol
40.7
10
µg/L
50.0
2,4-Dinitrotoluene
42.3
10
µg/L
50.0
2,6-Dinitrotoluene
42.7
10
µg/L
50.0
Di-n-octylphthalate
44.4
10
µg/L
50.0
1,2-Diphenylhydrazine/Azobenzene
38.2
10
µg/L
50.0
Fluoranthene
36.8
5.0
µg/L
50.0
Fluorene
37.8
5.0
µg/L
50.0
71.7
40-140
1.89
20
72.3
40-140
1.67
20
73.3
40-140
0.109
20
53.3
40-140
6.23
50
V-04
$
73.8
40-140
1.67
20
18.5
* 40-140
43.1
* 20
V-04, V-05, L-04,
R-05, J
75.7
40-140
0.972
20
80.2
40-140
0.200
20
77.7
40-140
1.74
20
66.5
40-140
4.18
20
V-05
76.8
40-140
1.34
20
45.9
10-130
1.56
50
t 1
86.1
40-140
2.16
20
74.3
40-140
1.04
20
93.1
40-140
0.621
20
78.2
40-140
1.12
20
73.4
40-140
1.11
20
83.9
40-140
30.2
* 20
R-05
72.9
40-140
2.47
20
49.0
40-140
3.37
20
V-34
74.5
30-130
2.55
20
65.3
40-140
1.23
20
63.4
30-130
2.68
20
73.8
40-140
0.298
20
69.2
40-140
2.37
20
65.1
40-140
4.23
20
74.1
40-140
1.33
20
77.9
40-140
2.46
20
65.0
40-140
0.583
20
60.9
40-140
3.77
20
61.4
40-140
2.22
20
77.5
40-140
1.00
20
72.8
30-130
0.330
20
76.6
40-140
2.70
20
64.2
30-130
0.466
20
72.5
40-140
0.660
50
$
87.1
30-130
1.74
50
$
81.4
30-130
6.79
50
$
84.7
40-140
1.38
20
85.4
40-140
0.979
20
88.8
40-140
3.04
20
76.5
40-140
0.392
20
73.7
40-140
0.946
20
75.6
40-140
2.65
20
Page 38 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218940 - SW-846 3510C
LCS Dup (B218940-BSD1)
Prepared: 12/11/18 Analyzed: 12/12/18
Hexachlorobenzene
35.8
10
µg/L
50.0
71.7
40-140
0.0279
20
Hexachlorobutadiene
32.9
10
µg/L
50.0
65.8
40-140
2.46
20
Hexachlorocyclopentadiene
20.2
10
µg/L
50.0
40.5
30-140
1.49
50
V-05 t $
Hexachloroethane
32.4
10
µg/L
50.0
64.9
40-140
2.91
50
$
Indeno(1,2,3-cd)pyrene
35.3
5.0
µg/L
50.0
70.5
40-140
5.87
50
$
Isophorone
39.0
10
µg/L
50.0
78.0
40-140
0.256
20
I-Methylnaphthalene
35.0
5.0
µg/L
50.0
70.0
40-140
1.12
20
2-Methylnaphthalene
39.0
5.0
µg/L
50.0
78.1
40-140
2.96
20
2-Methylphenol
31.2
10
µg/L
50.0
62.4
30-130
4.82
20
3/4-Methylphenol
29.0
10
µg/L
50.0
58.0
30-130
2.45
20
Naphthalene
34.7
5.0
µg/L
50.0
69.5
40-140
0.488
20
2-Nitroanihne
40.7
10
µg/L
50.0
81.4
40-140
0.369
20
3-Nitroaniline
34.1
10
µg/L
50.0
68.3
40-140
1.51
20
4-Nitroaniline
41.3
10
µg/L
50.0
82.7
40-140
1.68
20
Nitrobenzene
36.2
10
µg/L
50.0
72.4
40-140
1.28
20
2-Nitrophenol
40.4
10
µg/L
50.0
80.8
30-130
1.01
20
4-Nitrophenol
19.0
10
µg/L
50.0
38.1
10-130
0.210
50
t #
N-Nitrosodimethylamine
17.6
10
µg/L
50.0
35.3 *
40-140
4.16
20
L-04
N-Nitrosodiphenylamine/Diphenylamine
37.4
10
µg/L
50.0
74.7
40-140
1.36
20
N-Nitrosodi-n-propylamine
35.9
10
µg/L
50.0
71.8
40-140
0.555
20
Pentachloronitrobenzene
40.4
10
µg/L
50.0
80.7
40-140
0.422
20
Pentachlorophenol
30.0
10
µg/L
50.0
60.0
30-130
6.02
50
$
Phenanthrene
36.9
5.0
µg/L
50.0
73.7
40-140
0.544
20
Phenol
15.4
10
µg/L
50.0
30.9
20-130
2.05
20
t
Pyrene
39.6
5.0
µg/L
50.0
79.2
40-140
29.3
* 20
R-05
Pyridine
11.6
5.0
µg/L
50.0
23.1
10-140
2.14
50
V-05 t #
1,2,4,5-Tetrachlorobenzene
35.2
10
µg/L
50.0
70.5
40-140
3.55
20
1,2,4-Trichlorobenzene
33.5
5.0
µg/L
50.0
67.0
40-140
0.0896
20
2,4,5-Trichlorophenol
36.4
10
µg/L
50.0
72.9
30-130
2.42
20
2,4,6-Trichlorophenol
36.6
10
µg/L
50.0
73.1
30-130
2.66
50
$
Surrogate:2-Fluorophenol
89.1
µg/L
200
44.6
15-110
Surrogate: Phenol-d6
66.6
µg/L
200
33.3
15-110
Surrogate: Nitrobenzene-d5
77.0
µg/L
100
77.0
30-130
Surrogate:2-Fluorobiphenyl
64.0
µg/L
100
64.0
30-130
Surrogate: 2,4,6-Tribromophenol
176
µg/L
200
88.1
15-110
Surrogate:p-Terphenyl-dl4
78.3
µg/L
100
78.3
30-130
Batch B219039 - SW-846 3510C
Blank (B219039-BLK1)
Prepared: 12/12/18 Analyzed: 12/13/18
Acenaphthene
ND
5.0
µg/L
Acenaphthylene
ND
5.0
µg/L
Acetophenone
ND
10
µg/L
Aniline
ND
5.0
µg/L
V-04
Anthracene
ND
5.0
µg/L
Benzidine
ND
20
µg/L
V-04, V-05, R-05
Benzo(a)anthracene
ND
5.0
µg/L
Benzo(a)pyrene
ND
5.0
µg/L
Benzo(b)fluoranthene
ND
5.0
µg/L
Benzo(g,h,i)perylene
ND
5.0
µg/L
Benzo(k)fluoranthene
ND
5.0
µg/L
Benzoic Acid
ND
10
µg/L
Bis(2-chloroethoxy)methane
ND
10
µg/L
Page 39 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B219039 - SW-846 3510C
Blank (B219039-BLK1) Prepared: 12/12/18 Analyzed: 12/13/18
Bis(2-chloroethyl)ether
ND
10
µg/L
Bis(2-chloroisopropyl)ether
ND
10
µg/L
Bis(2-Ethylhexyl)phthalate
ND
10
µg/L
4-Bromophenylphenylether
ND
10
µg/L
Butylbenzylphthalate
ND
10
µg/L
Carbazole
ND
10
µg/L
4-Chloroaniline
ND
10
µg/L
4-Chloro-3-methylphenol
ND
10
µg/L
2-Chloronaphthalene
ND
10
µg/L
2-Chlorophenol
ND
10
µg/L
4-Chlorophenylphenylether
ND
10
µg/L
Chrysene
ND
5.0
µg/L
Dibenz(a,h)anthracene
ND
5.0
µg/L
Dibenzofuran
ND
5.0
µg/L
Di-n-butylphthalate
ND
10
µg/L
1,2-Dichlorobenzene
ND
5.0
µg/L
1,3-Dichlorobenzene
ND
5.0
µg/L
1,4-Dichlorobenzene
ND
5.0
µg/L
3,3-Dichlorobenzidine
ND
10
µg/L
2,4-Dichlorophenol
ND
10
µg/L
Diethylphthalate
ND
10
µg/L
2,4-Dimethylphenol
ND
10
µg/L
Dimethylphthalate
ND
10
µg/L
4,6-Dinitro-2-methylphenol
ND
10
µg/L
2,4-Dinitrophenol
ND
10
µg/L
2,4-Dinitrotoluene
ND
10
µg/L
2,6-Dinitrotoluene
ND
10
µg/L
Di-n-octylphthalate
ND
10
µg/L
1,2-Diphenylhydrazine/Azobenzene
ND
10
µg/L
Fluoranthene
ND
5.0
µg/L
Fluorene
ND
5.0
µg/L
Hexachlorobenzene
ND
10
µg/L
Hexachlorobutadiene
ND
10
µg/L
Hexachlorocyclopentadiene
ND
10
µg/L
Hexachloroethane
ND
10
µg/L
Indeno(1,2,3-cd)pyrene
ND
5.0
µg/L
Isophorone
ND
10
µg/L
1-Methylnaphthalene
ND
5.0
µg/L
2-Methylnaphthalene
ND
5.0
µg/L
2-Methylphenol
ND
10
µg/L
3/4-Methylphenol
ND
10
µg/L
Naphthalene
ND
5.0
µg/L
2-Nitroaniline
ND
10
µg/L
3-Nitroaniline
ND
10
µg/L
4-Nitroaniline
ND
10
µg/L
Nitrobenzene
ND
10
µg/L
2-Nitrophenol
ND
10
µg/L
4-Nitrophenol
ND
10
µg/L
N-Nitrosodimethylamine
ND
10
µg/L
N-Nitrosodiphenylamine/Diphenylamine
ND
10
µg/L
N-Nitrosodi-n-propylamine
ND
10
µg/L
Pentachloronitrobenzene
ND
10
µg/L
R-05
V-34
R-05
V-05
R-05
R-05
Page 40 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B219039 - SW-846 3510C
Blank (B219039-BLK1)
Prepared: 12/12/18 Analyzed: 12/13/18
Pentachlorophenol
ND
10
µg/L
Phenanthrene
ND
5.0
µg/L
Phenol
ND
10
µg/L
Pyrene
ND
5.0
µg/L
R-05
Pyridine
ND
5.0
µg/L
V-05
1,2,4,5-Tetrachlorobenzene
ND
10
µg/L
1,2,4-Trichlorobenzene
ND
5.0
µg/L
2,4,5-Trichlorophenol
ND
10
µg/L
2,4,6-Trichlorophenol
ND
10
µg/L
Surrogate:2-Fluorophenol
114
µg/L
200
56.9
15-110
Surrogate: Phenol-d6
81.0
µg/L
200
40.5
15-110
Surrogate: Nitrobenzene-d5
92.8
µg/L
100
92.8
30-130
Surrogate:2-Fluorobiphenyl
75.2
µg/L
100
75.2
30-130
Surrogate: 2,4,6-Tribromophenol
188
µg/L
200
94.1
15-110
Surrogate:p-Terphenyl-dl4
91.6
µg/L
100
91.6
30-130
LCS (B219039-BSI)
Prepared: 12/12/18 Analyzed: 12/13/18
Acenaphthene
32.5
5.0
µg/L
50.0
65.0
40-140
Acenaphthylene
32.5
5.0
µg/L
50.0
65.0
40-140
Acetophenone
34.8
10
µg/L
50.0
69.6
40-140
Aniline
28.9
5.0
µg/L
50.0
57.9
40-140
V-04
Anthracene
34.3
5.0
µg/L
50.0
68.6
40-140
Benzidine
22.9
20
µg/L
50.0
45.8
40-140
R-05, V-04, V-05
Benzo(a)anthracene
34.3
5.0
µg/L
50.0
68.7
40-140
Benzo(a)pyrene
35.6
5.0
µg/L
50.0
71.2
40-140
Benzo(b)fluoranthene
33.9
5.0
µg/L
50.0
67.9
40-140
Benzo(g,h,i)perylene
35.1
5.0
µg/L
50.0
70.2
40-140
Benzo(k)fluoranthene
33.6
5.0
µg/L
50.0
67.1
40-140
Benzoic Acid
21.7
10
µg/L
50.0
43.4
10-130
t
Bis(2-chloroethoxy)methane
39.0
10
µg/L
50.0
77.9
40-140
Bis(2-chloroethyl)ether
37.4
10
µg/L
50.0
74.8
40-140
Bis(2-chloroisopropyl)ether
45.3
10
µg/L
50.0
90.6
40-140
Bis(2-Ethylhexyl)phthalate
35.7
10
µg/L
50.0
71.4
40-140
4-Bromophenylphenylether
34.7
10
µg/L
50.0
69.4
40-140
Butylbenzylphthalate
49.9
10
µg/L
50.0
99.8
40-140
R-05
Carbazole
34.0
10
µg/L
50.0
68.0
40-140
4-Chloroaniline
26.0
10
µg/L
50.0
51.9
40-140
V-34
4-Chloro-3-methylphenol
34.6
10
µg/L
50.0
69.1
30-130
R-05
2-Chloronaphthalene
28.6
10
µg/L
50.0
57.2
40-140
2-Chorophenol
32.8
10
µg/L
50.0
65.6
30-130
4-Chlorophenylphenylether
33.4
10
µg/L
50.0
66.8
40-140
Chrysene
32.8
5.0
µg/L
50.0
65.6
40-140
Dibenz(a,h)anthracene
31.5
5.0
µg/L
50.0
63.0
40-140
Dibenzofuran
33.8
5.0
µg/L
50.0
67.5
40-140
Di-n-butylphthalate
34.7
10
µg/L
50.0
69.3
40-140
1,2-Dichlorobenzene
32.3
5.0
µg/L
50.0
64.5
40-140
1,3-Dichlorobenzene
31.7
5.0
µg/L
50.0
63.4
40-140
1,4-Dichlorobenzene
32.1
5.0
µg/L
50.0
64.3
40-140
3,3-Dichlorobenzidine
34.7
10
µg/L
50.0
69.3
40-140
2,4-Dichlorophenol
33.5
10
µg/L
50.0
67.0
30-130
Diethylphthalate
33.4
10
µg/L
50.0
66.8
40-140
2,4-Dimethylphenol
32.3
10
µg/L
50.0
64.6
30-130
Page 41 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B219039 - SW-846 3510C
LCS (B219039-BSI) Prepared: 12/12/18 Analyzed: 12/13/18
Dimethylphthalate
33.2
10
µg/L
50.0
66.4
40-140
4,6-Dinitro-2-methylphenol
40.0
10
µg/L
50.0
80.0
30-130
2,4-Dinitrophenol
36.9
10
µg/L
50.0
73.8
30-130
2,4-Dinitrotoluene
37.2
10
µg/L
50.0
74.5
40-140
2,6-Dinitrotoluene
39.0
10
µg/L
50.0
77.9
40-140
Di-n-octylphthalate
36.2
10
µg/L
50.0
72.4
40-140
1,2-Diphenylhydrazine/Azobenzene
37.1
10
µg/L
50.0
74.2
40-140
Fluoranthene
33.2
5.0
µg/L
50.0
66.4
40-140
Fluorene
33.3
5.0
µg/L
50.0
66.7
40-140
Hexachlorobenzene
34.3
10
µg/L
50.0
68.6
40-140
Hexachlorobutadiene
31.3
10
µg/L
50.0
62.5
40-140
Hexachlorocyclopentadiene
20.3
10
µg/L
50.0
40.6
30-140
V-05 t
Hexachloroethane
32.3
10
µg/L
50.0
64.7
40-140
Indeno(1,2,3-cd)pyrene
33.7
5.0
µg/L
50.0
67.4
40-140
Isophorone
36.2
10
µg/L
50.0
72.4
40-140
I-Methylnaphthalene
32.0
5.0
µg/L
50.0
63.9
40-140
R-05
2-Methylnaphthalene
34.6
5.0
µg/L
50.0
69.2
40-140
R-05
2-Methylphenol
32.4
10
µg/L
50.0
64.8
30-130
3/4-Methylphenol
29.4
10
µg/L
50.0
58.8
30-130
Naphthalene
32.8
5.0
µg/L
50.0
65.7
40-140
2-Nitroaniline
36.1
10
µg/L
50.0
72.2
40-140
3-Nitroaniline
36.0
10
µg/L
50.0
71.9
40-140
4-Nitroaniline
37.0
10
µg/L
50.0
73.9
40-140
Nitrobenzene
33.4
10
µg/L
50.0
66.8
40-140
2-Nitrophenol
38.7
10
µg/L
50.0
77.4
30-130
4-Nitrophenol
17.8
10
µg/L
50.0
35.6
10-130
t
N-Nitrosodimethylamine
23.0
10
µg/L
50.0
46.1
40-140
N-Nitrosodiphenylamine/Diphenylamine
35.5
10
µg/L
50.0
71.0
40-140
N-Nitrosodi-n-propylamine
34.2
10
µg/L
50.0
68.5
40-140
Pentachloronitrobenzene
36.7
10
µg/L
50.0
73.4
40-140
Pentachlorophenol
29.0
10
µg/L
50.0
58.1
30-130
Phenanthrene
34.6
5.0
µg/L
50.0
69.1
40-140
Phenol
16.1
10
µg/L
50.0
32.3
20-130
t
Pyrene
47.2
5.0
µg/L
50.0
94.4
40-140
R-05
Pyridine
16.1
5.0
µg/L
50.0
32.3
10-140
V-05 f
1,2,4,5-Tetrachlorobenzene
32.5
10
µg/L
50.0
64.9
40-140
1,2,4-Trichlorobenzene
32.3
5.0
µg/L
50.0
64.6
40-140
2,4,5-Trichlorophenol
33.4
10
µg/L
50.0
66.9
30-130
2,4,6-Trichlorophenol
34.0
10
µg/L
50.0
67.9
30-130
Surrogate:2-Fluorophenol
101
µg/L
200
50.3
15-110
Surrogate: Phenol-d6
70.7
µg/L
200
35.4
15-110
Surrogate: Nitrobenzene-d5
74.4
µg/L
100
74.4
30-130
Surrogate:2-Fluorobiphenyl
59.3
µg/L
100
59.3
30-130
Surrogate: 2,4,6-Tribromophenol
155
µg/L
200
77.5
15-110
Surrogate:p-Terphenyl-dl4
96.3
µg/L
100
96.3
30-130
Page 42 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B219039 - SW-846 3510C
LCS Dup (B219039-BSD1) Prepared: 12/12/18 Analyzed: 12/13/18
Acenaphthene
32.1
5.0
µg/L
50.0
Acenaphthylene
31.5
5.0
µg/L
50.0
Acetophenone
33.4
10
µg/L
50.0
Aniline
27.1
5.0
µg/L
50.0
Anthracene
33.7
5.0
µg/L
50.0
Benzidine
11.2
20
µg/L
50.0
Benzo(a)anthracene
33.7
5.0
µg/L
50.0
Benzo(a)pyrene
36.2
5.0
µg/L
50.0
Benzo(b)fluoranthene
34.0
5.0
µg/L
50.0
Benzo(g,h,i)perylene
33.3
5.0
µg/L
50.0
Benzo(k)fluoranthene
33.7
5.0
µg/L
50.0
Benzoic Acid
21.7
10
µg/L
50.0
Bis(2-chloroethoxy)methane
36.0
10
µg/L
50.0
Bis(2-chloroethyl)ether
35.6
10
µg/L
50.0
Bis(2-chloroisopropyl)ether
42.8
10
µg/L
50.0
Bis(2-Ethylhexyl)phthalate
35.7
10
µg/L
50.0
4-Bromophenylphenylether
31.5
10
µg/L
50.0
Butylbenzylphthalate
37.3
10
µg/L
50.0
Carbazole
33.3
10
µg/L
50.0
4-Chloroaniline
23.8
10
µg/L
50.0
4-Chloro-3-methylphenol
25.8
10
µg/L
50.0
2-Chloronaphthalene
29.7
10
µg/L
50.0
2-Chlorophenol
31.3
10
µg/L
50.0
4-Chlorophenylphenylether
34.5
10
µg/L
50.0
Chrysene
31.8
5.0
µg/L
50.0
Dibenz(a,h)anthracene
30.5
5.0
µg/L
50.0
Dibenzofuran
33.7
5.0
µg/L
50.0
Di-n-butylphthalate
35.1
10
µg/L
50.0
1,2-Dichlorobenzene
32.6
5.0
µg/L
50.0
1,3-Dichlorobenzene
32.3
5.0
µg/L
50.0
1,4-Dichlorobenzene
30.9
5.0
µg/L
50.0
3,3-Dichlorobenzidine
34.4
10
µg/L
50.0
2,4-Dichlorophenol
32.9
10
µg/L
50.0
Diethylphthalate
35.0
10
µg/L
50.0
2,4-Dimethylphenol
29.9
10
µg/L
50.0
Dimethylphthalate
34.2
10
µg/L
50.0
4,6-Dinitro-2-methylphenol
40.5
10
µg/L
50.0
2,4-Dinitrophenol
41.2
10
µg/L
50.0
2,4-Dinitrotoluene
41.4
10
µg/L
50.0
2,6-Dinitrotoluene
39.2
10
µg/L
50.0
Di-n-octylphthalate
37.7
10
µg/L
50.0
1,2-Diphenylhydrazine/Azobenzene
31.9
10
µg/L
50.0
Fluoranthene
33.8
5.0
µg/L
50.0
Fluorene
34.0
5.0
µg/L
50.0
Hexachlorobenzene
32.0
10
µg/L
50.0
Hexachlorobutadiene
28.7
10
µg/L
50.0
Hexachlorocyclopentadiene
19.5
10
µg/L
50.0
Hexachloroethane
32.9
10
µg/L
50.0
Indeno(1,2,3-cd)pyrene
33.1
5.0
µg/L
50.0
Isophorone
33.8
10
µg/L
50.0
1-Methylnaphthalene
24.1
5.0
µg/L
50.0
2-Methylnaphthalene
26.2
5.0
µg/L
50.0
64.2
40-140
1.15
20
63.0
40-140
3.15
20
66.8
40-140
4.11
20
54.2
40-140
6.61
50
V-04
$
67.5
40-140
1.70
20
22.4
* 40-140
68.6 *
20
MS-23, V-04,
V-05,J
67.4
40-140
1.88
20
72.4
40-140
1.73
20
67.9
40-140
0.0295
20
66.6
40-140
5.21
20
67.4
40-140
0.357
20
43.5
10-130
0.184
50
t 1
72.0
40-140
7.87
20
71.1
40-140
5.10
20
85.5
40-140
5.75
20
71.4
40-140
0.0840
20
63.0
40-140
9.61
20
74.5
40-140
29.0 *
20
R-05
66.7
40-140
1.96
20
47.7
40-140
8.56
20
V-34
51.5
30-130
29.2 *
20
R-05
59.5
40-140
3.84
20
62.5
30-130
4.75
20
69.0
40-140
3.24
20
63.6
40-140
3.06
20
61.0
40-140
3.16
20
67.4
40-140
0.208
20
70.2
40-140
1.20
20
65.2
40-140
1.02
20
64.6
40-140
1.91
20
61.8
40-140
4.00
20
68.8
40-140
0.724
20
65.8
30-130
1.84
20
69.9
40-140
4.48
20
59.8
30-130
7.75
20
68.3
40-140
2.76
50
$
81.1
30-130
1.37
50
$
82.4
30-130
11.0
50
$
82.8
40-140
10.6
20
78.5
40-140
0.691
20
75.4
40-140
4.09
20
63.8
40-140
15.1
20
67.6
40-140
1.73
20
67.9
40-140
1.87
20
64.1
40-140
6.76
20
57.5
40-140
8.40
20
39.0
30-140
3.97
50
V-05
$
65.8
40-140
1.81
50
66.3
40-140
1.77
50
67.7
40-140
6.74
20
48.2
40-140
28.1 *
20
R-05
52.4
40-140
27.8 *
20
R-05
Page 43 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B219039 - SW-846 3510C
LCS Dup (B219039-BSD1) Prepared: 12/12/18 Analyzed: 12/13/18
2-Methylphenol
29.3
10
µg/L
50.0
58.6
30-130
10.0
20
3/4-Methylphenol
28.3
10
µg/L
50.0
56.6
30-130
3.74
20
Naphthalene
31.0
5.0
µg/L
50.0
62.1
40-140
5.63
20
2-Nitroaniline
35.7
10
µg/L
50.0
71.5
40-140
1.09
20
3-Nitroaniline
33.6
10
µg/L
50.0
67.3
40-140
6.66
20
4-Nitroaniline
39.8
10
µg/L
50.0
79.5
40-140
7.27
20
Nitrobenzene
30.2
10
µg/L
50.0
60.4
40-140
10.0
20
2-Nitrophenol
36.6
10
µg/L
50.0
73.2
30-130
5.55
20
4-Nitrophenol
19.4
10
µg/L
50.0
38.7
10-130
8.51
50
t $
N-Nitrosodimethylamine
24.1
10
µg/L
50.0
48.2
40-140
4.46
20
N-Nitrosodiphenylamine/Diphenylamine
33.2
10
µg/L
50.0
66.4
40-140
6.70
20
N-Nitrosodi-n-propylamine
33.0
10
µg/L
50.0
66.0
40-140
3.72
20
Pentachloronitrobenzene
38.2
10
µg/L
50.0
76.4
40-140
4.01
20
Pentachlorophenol
28.1
10
µg/L
50.0
56.3
30-130
3.18
50
$
Phenanthrene
33.7
5.0
µg/L
50.0
67.5
40-140
2.43
20
Phenol
15.6
10
µg/L
50.0
31.1
20-130
3.60
20
f
Pyrene
33.9
5.0
µg/L
50.0
67.8
40-140
32.8
* 20
R-05
Pyridine
15.7
5.0
µg/L
50.0
31.5
10-140
2.51
50
V-05 t $
1,2,4,5-Tetrachlorobenzene
32.4
10
µg/L
50.0
64.8
40-140
0.247
20
1,2,4-Trichlorobenzene
31.3
5.0
µg/L
50.0
62.6
40-140
3.11
20
2,4,5-Trichlorophenol
32.8
10
µg/L
50.0
65.6
30-130
1.96
20
2,4,6-Trichlorophenol
32.9
10
µg/L
50.0
65.8
30-130
3.20
50
$
Surrogate:2-Fluorophenol
98.7
µg/L
200
49.4
15-110
Surrogate: Phenol-d6
65.6
µg/L
200
32.8
15-110
Surrogate: Nitrobenzene-d5
68.2
µg/L
100
68.2
30-130
Surrogate:2-Fluorobiphenyl
57.4
µg/L
100
57.4
30-130
Surrogate: 2,4,6-Tribromophenol
170
µg/L
200
85.1
15-110
Surrogate:p-Terphenyl-d14
68.5
µg/L
100
68.5
30-130
Page 44 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B218876 - SW-846 3005A
Blank (B218876-BLK1)
Prepared: 12/10/18 Analyzed: 12/11/18
Arsenic
ND
0.80
µg/L
Barium
ND
20
µg/L
Cadmium
ND
1.0
µg/L
Chromium
ND
2.0
µg/L
Lead
ND
2.0
µg/L
Selenium
ND
10
µg/L
Silver
ND
1.0
µg/L
LCS (B218876-BS1)
Prepared: 12/10/18 Analyzed: 12/11/18
Arsenic
437
4.0
µg/L
500 107
80-120
Barium
525
100
µg/L
500 105
80-120
Cadmium
937
5.0
µg/L
500 107
80-120
Chromium
546
10
µg/L
500 109
80-120
Lead
535
10
µg/L
500 107
80-120
Selenium
948
50
µg/L
500 110
80-120
Silver
527
5.0
µg/L
500 105
80-120
LCS Dup (B218876-BSD1)
Prepared: 12/10/18 Analyzed: 12/11/18
Arsenic
527
4.0
µg/L
500 105
80-120
1.80
20
Barium
511
100
µg/L
500 102
80-120
2.62
20
Cadmium
520
5.0
µg/L
500 104
80-120
3.09
20
Chromium
532
10
µg/L
500 106
80-120
2.58
20
Lead
523
10
µg/L
500 105
80-120
2.30
20
Selenium
534
50
µg/L
500 107
80-120
2.51
20
Silver
512
5.0
µg/L
500 102
80-120
3.02
20
Duplicate (B218876-DUP1)
Source: 18LO322-01
Prepared: 12/10/18 Analyzed: 12/11/18
Arsenic
ND
0.80
µg/L
ND
NC
20
Barium
34.8
20
µg/L
35.0
0.579
20
Cadmium
ND
1.0
µg/L
ND
NC
20
Chromium
1.47
2.0
µg/L
1.50
2.30
20 J
Lead
ND
2.0
µg/L
ND
NC
20
Selenium
ND
10
µg/L
ND
NC
20
Silver
ND
1.0
µg/L
ND
NC
20
Matrix Spike (B218876-MS1)
Source: 18LO322-01
Prepared: 12/10/18 Analyzed: 12/11/18
Arsenic
530
4.0
µg/L
500 ND 106
75-125
Barium
547
100
µg/L
500 ND 109
75-125
Cadmium
524
5.0
µg/L
500 ND 105
75-125
Chromium
531
10
µg/L
500 ND 106
75-125
Lead
521
10
µg/L
500 ND 104
75-125
Selenium
537
50
µg/L
500 ND 107
75-125
Silver
442
5.0
µg/L
500 ND 88.5
75-125
Page 45 of 54

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Metals Analyses (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B219057 - SW-846 7470A Prep
Blank (B219057-BLK1) Prepared: 12/12/18 Analyzed: 12/13/18
Mercury 0.000077 0.00010 mg/L J
LCS (B219057-BS1) Prepared: 12/12/18 Analyzed: 12/13/18
Mercury 0.00204 0.00010 mg/L 0.00200 102 80-120
LCS Dup (B219057-BSD1) Prepared: 12/12/18 Analyzed: 12/13/18
Mercury 0.00209 0.00010 mg/L 0.00200 105 80-120 2.41 20
Page 46 of 54

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
fi
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
MS-23 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is outside of the method specified criteria. Reduced precision anticipated for any reported
result for this compound.
R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
RL-11 Elevated reporting limit due to high concentration of target compounds.
V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound.
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
Page 47 of 54

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 6020B in Water
Arsenic
CT,NH,NY,ME,VA,NC
Barium
CT,NH,NY,ME,VA,NC
Cadmium
CT,NH,NY,RI,ME,VA,NC
Chromium
CT,NH,NY,ME,VA,NC
Lead
CT,NH,NY,ME,VA,NC
Selenium
CT,NH,NY,ME,VA,NC
Silver
CT,NH,NY,ME,VA,NC
SW-846 7470A in Water
Mercury
CT,NH,NY,NC,ME,VA
SW-846 8260B in Water
Acetone
NC
Acrylonitrile
NC
tert-Amyl Methyl Ether (TAME)
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Bromoform
NC
Bromomethane
NC
2-Butanone (MEK)
NC
tert-Butyl Alcohol (TBA)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
tert-Butyl Ethyl Ether (TBEE)
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromo-3-chloropropane (DBCP)
NC
1,2-Dibromoethane (EDB)
NC
Dibromomethane
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
trans-1,4-Dichloro-2-butene
NC
Dichlorodifluoromethane (Freon 12)
NC
1,1-Dichloroethane
NC
1,2-Dichloroethane
NC
1,1-Dichloroethylene
NC
cis-1,2-Dichloroethylene
NC
Page 48 of 54

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
SW-846 8260B in Water
trans- l,2-Dichloro ethylene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis- 1,3 -Dichloropropene
trans- 1, 3 -Dichloropropene
Diethyl Ether
Diisopropyl Ether (DIPE)
1,4-Dioxane
Ethylbenzene
Hexachlorobutadiene
2-Hexanone (MBK)
Isopropylbenzene (Cumene)
p-Isopropyltoluene (p-Cymene)
Methyl tert-Butyl Ether (MTBE)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethylene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethylene
Trichlorofluoromethane (Freon 11)
1,2,3-Trichloropropane
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Chloride
m+p Xylene
o-Xylene
SW-846 8270D in Water
Acenaphthene
Acenaphthylene
Acetophenone
Aniline
Anthracene
Certifications
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
CT,NY,NC,ME,NH,VA
CT,NY,NC,ME,NH,VA
NY,NC
CT,NY,NC,ME,VA
CT,NY,NC,ME,NH,VA
Page 49 of 54

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Water
Benzidine
CT,NY,NC,ME,NH,VA
Benzo(a)anthracene
CT,NY NC,ME,NH,VA
Benzo(a)pyrene
CT,NY,NC,ME,NH,VA
Benzo(b)fluoranthene
CT,NY,NC,ME,NH,VA
Benzo(g,h,i)perylene
CT,NY,NC,ME,NH,VA
Benzo(k)fluoranthene
CT,NY,NC,ME,NH,VA
Benzoic Acid
NY,NC,ME,NH,VA
Bis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VA
Bis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-Ethy1hexy1)phtha1ate
CT,NY,NC,ME,NH,VA
4-Bromophenylphenylether
CT,NY,NC,ME,NH,VA
Butylbenzylphthalate
CT,NY,NC,ME,NH,VA
Carbazole
NC
4-Chloroaniline
CT,NY,NC,ME,NH,VA
4-Chloro-3-methylphenot
CT,NY,NC,ME,NH,VA
2-Chloronaphthalene
CT,NY,NC,ME,NH,VA
2-Chlorophenol
CT,NY,NC,ME,NH,VA
4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VA
Chrysene
CT,NY,NC,ME,NH,VA
Dibenz(a,h)anthracene
CT,NY NC,ME,NH,VA
Dibenzofuran
CT,NY,NC,ME,NH,VA
Di-n-butylphthalate
CT,NY,NC,ME,NH,VA
1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA
3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA
2,4-Dichlorophenol
CT,NY,NC,ME,NH,VA
Diethylphthalate
CT,NY,NC,ME,NH,VA
2,4-Dimethylphenol
CT,NY,NC,ME,NH,VA
Dimethylphthalate
CT,NY,NC,ME,NH,VA
4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA
2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VA
Di-n-octylphthalate
CT,NY,NC,ME,NH,VA
1,2-Diphenylhydrazine/Azobenzene
NY,NC
Fluoranthene
CT,NY,NC,ME,NH,VA
Fluorene
NY,NC,ME,NH,VA
Hexachlorobenzene
CT,NY,NC,ME,NH,VA
Hexachlorobutadiene
CT,NY,NC,ME,NH,VA
Hexachlorocyclopentadiene
CT,NY,NC,ME,NH,VA
Hexachloroethane
CT,NY,NC,ME,NH,VA
Indeno(1,2,3-cd)pyrene
CT,NY NC,ME,NH,VA
Isophorone
CT,NY,NC,ME,NH,VA
I -Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NC,ME,NH,VA
Page 50 of 54

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8270D in Water
2-Methylphenol
CT,NY,NC,NH,VA
3/4-Methylphenol
CT,NY,NC,NH,VA
Naphthalene
CT,NY,NC,ME,NH,VA
2-Nitroaniline
CT,NY,NC,ME,NH,VA
3-Nitroaniline
CT,NY,NC,ME,NH,VA
4-Nitroaniline
CT,NY,NC,ME,NH,VA
Nitrobenzene
CT,NY,NC,ME,NH,VA
2-Nitrophenol
CT,NY,NC,ME,NH,VA
4-Nitrophenol
CT,NY,NC,ME,NH,VA
N-Nitrosodimethylamine
CT,NY,NC,ME,NH,VA
N-Nitrosodi-n-propylamine
CT,NY,NC,ME,NH,VA
Pentachloronitrobenzene
NC
Pentachlorophenol
CT,NY,NC,ME,NH,VA
Phenanthrene
CT,NY,NC,ME,NH,VA
Phenol
CT,NY,NC,ME,NH,VA
Pyrene
CT,NY,NC,ME,NH,VA
Pyridine
CT,NY,NC,ME,NH,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA
2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA
2,4,6-Trichlorophenol
CT,NY,NC,ME,NH,VA
2-Fluorophenol
NC
The CON -TEST Environmental Laboratory operates under the
following certifications and accreditations:
Code Description
Number
Expires
AIHA AIHA-LAP, LLC - ISO17025:2005
100033
03/1/2020
MA Massachusetts DEP
M-MA100
06/30/2019
CT Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY New York State Department of Health
10899 NELAP
04/1/2019
NH-S New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI Rhode Island Department of Health
LA000112
12/30/2018
NC North Carolina Div. of Water Quality
652
12/31/2019
NJ New Jersey DEP
MA007 NELAP
06/30/2019
FL Florida Department of Health
E871027 NELAP
06/30/2019
VT Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME State of Maine
2011028
06/9/2019
VA Commonwealth of Virginia
460217
12/14/2018
NH-P New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW North Carolina Department of Health
25703
07/31/2019
Page 51 of 54

Table of Contents
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Delivered
Friday 12/07/201 S at 9:50 am
DELIVERED
Signed for by B.BECCA
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
FROM TO
Charioltr, NO US EAST L0NGPr1EAD<7'%N, MA US
Multiple -piece Shipment
3 Piece shipment
Table of Contents
TRACKING NUMBER SHIPPER CITY, STATE SHIP DATE STATUS DELIVERY DATE DLSTMATION/RECIPIENT
CITY, STATE
773903660982 CHARLOTTE, NC 12/06/2018 1210112018 EAST LON('�ME.ADOVV,, MA
Jllaster
773903b6'073 CHARLOTTE, N!, 12/06/2018 21D7!2018 EAST I ONGMEADOVd, NvA
77390366137 CHARLOTTE, INC 12/06/2018 1210711I2015 CAST LONG�,,1CAEi04 MA
Shipment Facts
TRACKING NUMBER
SERVICE
MASTER TRACKING NUMBER
7''908660982.
FodFxstaridard0,-c=rr,iglt
7739n.�66o��2
WEIGHT
DIMENSIONS
DELIVERED TO
0 ills 14 54 krr;
24x 14x €4 el_
Shii)pirrg/Pc-cew�r�g
TOTAL PIECES
TOTAL SHIPMENT WEIGHT
TERMS
30 Ilas / 13 61 kg ,
T Nrd Party
PACKAGING
SPECIAL HANDLING SECTION
STANDARD TRANSIT
You! Packaging
IX4ver Weekdav
210712f118 by,; 00 pm
https://www.fedex.com/apps/fedextrack/?action=track&tracknumbets=773903660982&locale=en_US&cntry_code=u
s
Page 53 of 54

Table of Contents
I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Relin uishin
� g �! � � ` ANALYTICAL LA60RATORY
Over Samples
Qoc# 2�7 ReW 5 217
Login Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client ij i, A ti 0-� t, v y11 � /-\
Received By
Date
How were the samples In Cooler No Cooler
received? Direct from Sampling
B G # 1
o- Time 0 SZU
On Ice 7— No Ice
Ambient Melted Ice
Actual Tem ( i i
Were samples within
y un
p
Temperature? 2-6°C
By Blank #
Actual Temp -
Was Custody Seal Intact?
f
Were Samples Tampered with?
Was COC Relinquished ?
Does Chain Agree With Samples? r
Are there broken/leaking/loose caps on any samples? i
Is COC in ink/ Legible?
Were samples received within holding time?�
Did COC include all Client
��
Analysis T Sampler Name ,—
pertinent Information? Project
i
ID's -r Collection Dates/Times T
Are Sample labels filled out and legible?
Are there Lab to Filters?
Who was notified?
Are there Rushes?
Who was notified?
Are there Short Holds?
Who was notified?
Is there enough Volume?
T
Is there Headspace where applicable?
MSIMSD?
Proper Media/Containers Used?
i
Is splitting samples required?
Were trip blanks received?
On COC? `F
Do all samples have the proper pH?
Acid L_L Base
Unp-
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz Amb/Clear
Meoh-
250 mL Amb.
250 mL Plastic
' (
4oz AmblClear
Bisulfate-
Flashpoint
Col./Bacteria
2oz Amb/Clear
DI-
Other Glass
Other Plastic
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Sulfuric-
I
Perchlorate
Ziplock
Unp-
1 Liter Amb.
1 Liter Plastic
16 oz Amb.
HCL-
500 mL Amb.
500 mL Plastic
8oz AmblClear
Meoh-
250 mL Amb.
250 mL Plastic
4oz Amb/Clear
Bisulfate-
Cal./Bacteria
Flash oint
2oz Amb/Clear
DI-
Other Plastic
Other Glass
Encore
Thiosulfate-
SOC Kit
Plastic Bag
Frozen:
Sulfuric-
I
Perchlorate
Ziplock

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
December 13, 2018
Bo Cappleman
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Charlotte, NC
Client Job Number:
Project Number: COP-008
Laboratory Work Order Number: 18LO293
Enclosed are results of analyses for samples received by the laboratory on December 6, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
�11 �. A��
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Hart & Hickman - Charlotte, NC REPORT DATE: 12/13/2018
2923 South Tryon Street, Suite 100
Charlotte, NC 28203 PURCHASE ORDER NUMBER: COP-008
ATTN: Bo Cappleman
PROJECT NUMBER: COP-008
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18LO293
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Charlotte, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
SSV-1
18L0293-01
Sub Slab
EPA TO-15
SSV-2
18L0293-02
Sub Slab
EPA TO-15
SSV-3
18LO293-03
Sub Slab
EPA TO-15
DUP-SSV
18L0293-04
Sub Slab
EPA TO-15
Page 2 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not affected since all results are
"not detected" for all samples in this batch for this compound and bias is on the high side.
Analyte & Samples(s) Qualified:
Carbon Disulfide
B219146-BSI
Continuing calibration did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene, Hexachlorobutadiene
S030250-CC V 1
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene, Hexachlorobutadiene
S030210-CCV 1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
Carbon Disulfide
B219146-BS1, S030210-CCV1
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in
house limits of 50-150%.
Analyte & Samples(s) Qualified:
Ethanol, Hexachlorobutadiene
B219031-BS1,B219146-BSI
Page 3 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 4 of 34

,con -testy
ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SSV-1
Sample ID: 18L0293-01
Sample Matrix: Sub Slab
Sampled: 12/5/2018 14:54
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location: Work Order: 18L0293
Sub Description/Location: Initial Vacuum(in Hg): -28.9
Canister ID: 1110 Final Vacuum(in Hg): -5
Canister Size: 6 liter Receipt Vacuum(in Hg): -5.1
Flow Controller ID: 4173 Flow Controller Type: Fixed -Orifice
Sample Type: 1 hr Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv
ug/m3
Date/Time
Analyte
Results
RL
MDL Flag/Qual
Results
ILL
MDL
Dilution
Analyzed
Analyst
Acetone
4.0
8.0
2.8 J
9.4
19
6.6
4
12/12/18 14:38
BRF
Benzene
ND
0.20
0.082
ND
0.64
0.26
4
12/12/18 14:38
BRF
Benzyl chloride
ND
0.20
0.044
ND
1.0
0.23
4
12/12/18 14:38
BRF
Bromodichloromethane
ND
0.20
0.074
ND
1.3
0.49
4
12/12/18 14:38
BRF
Bromoform
ND
0.20
0.090
ND
2.1
0.93
4
12/12/18 14:38
BRF
Bromomethane
ND
0.20
0.14
ND
0.78
0.53
4
12/12/18 14:38
BRF
1,3-Butadiene
ND
0.20
0.13
ND
0.44
0.28
4
12/12/18 14:38
BRF
2-Butanone (MEK)
ND
8.0
0.31
ND
24
0.92
4
12/12/18 14:38
BRF
Carbon Disulfide
ND
2.0
0.14
ND
6.2
0.43
4
12/12/18 14:38
BRF
Carbon Tetrachloride
ND
0.20
0.065
ND
1.3
0.41
4
12/12/18 14:38
BRF
Chlorobenzene
ND
0.20
0.098
ND
0.92
0.45
4
12/12/18 14:38
BRF
Chloroethane
ND
0.40
0.12
ND
1.1
0.32
4
12/12/18 14:38
BRF
Chloroform
ND
0.20
0.074
ND
0.98
0.36
4
12/12/18 14:38
BRF
Chloromethane
ND
0.40
0.14
ND
0.83
0.28
4
12/12/18 14:38
BRF
Cyclohexane
ND
0.20
0.14
ND
0.69
0.49
4
12/12/18 14:38
BRF
Dibromochloromethane
ND
0.20
0.066
ND
1.7
0.57
4
12/12/18 14:38
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.078
ND
1.5
0.60
4
12/12/18 14:38
BRF
1,2-Dichlorobenzene
ND
0.20
0.096
ND
1.2
0.58
4
12/12/18 14:38
BRF
1,3-Dichlorobenzene
0.21
0.20
0.10
1.3
1.2
0.62
4
12/12/18 14:38
BRF
1,4-Dichlorobenzene
ND
0.20
0.12
ND
1.2
0.73
4
12/12/18 14:38
BRF
Dichlorodifluoromethane (Freon 12)
0.54
0.20
0.087
2.7
0.99
0.43
4
12/12/18 14:38
BRF
1, 1 -Dichloroethane
ND
0.20
0.061
ND
0.81
0.25
4
12/12/18 14:38
BRF
1,2-Dichloroethane
ND
0.20
0.076
ND
0.81
0.31
4
12/12/18 14:38
BRF
1, 1 -Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 14:38
BRF
cis-1,2-Dichloroethylene
ND
0.20
0.082
ND
0.79
0.32
4
12/12/18 14:38
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 14:38
BRF
1,2-Dichloropropane
ND
0.20
0.071
ND
0.92
0.33
4
12/12/18 14:38
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.070
ND
0.91
0.32
4
12/12/18 14:38
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.073
ND
0.91
0.33
4
12/12/18 14:38
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND
0.20
0.10
ND
1.4
0.70
4
12/12/18 14:38
BRF
1,4-Dioxane
ND
2.0
1.3
ND
7.2
4.6
4
12/12/18 14:38
BRF
Ethanol
5.3
8.0
3.6 J
10
15
6.7
4
12/12/18 14:38
BRF
Ethyl Acetate
ND
0.40
0.15
ND
1.4
0.54
4
12/12/18 14:38
BRF
Ethylbenzene
ND
0.20
0.12
ND
0.87
0.50
4
12/12/18 14:38
BRF
4-Ethyltoluene
ND
0.20
0.12
ND
0.98
0.60
4
12/12/18 14:38
BRF
Heptane
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 14:38
BRF
Hexachlorobutadiene
ND
0.20
0.092
ND
2.1
0.98
4
12/12/18 14:38
BRF
Hexane
ND
8.0
0.35
ND
28
1.2
4
12/12/18 14:38
BRF
2-Hexanone (MBK)
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 14:38
BRF
Isopropanol
ND
8.0
0.25
ND
20
0.60
4
12/12/18 14:38
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.10
ND
0.72
0.36
4
12/12/18 14:38
BRF
Methylene Chloride
ND
2.0
0.24
ND
6.9
0.84
4
12/12/18 14:38
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.096
ND
0.82
0.39
4
12/12/18 14:38
BRF
Naphthalene
ND
0.20
0.15
ND
1.0
0.80
4
12/12/18 14:38
BRF
Propene
ND
8.0
0.20
ND
14
0.34
4
12/12/18 14:38
BRF
Styrene
ND
0.20
0.12
ND
0.85
0.53
4
12/12/18 14:38
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.089
ND
1.4
0.61
4
12/12/18 14:38
BRF
Page 5 of 34

,con -testy
ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SSV-1
Sample ID: 18L0293-01
Sample Matrix: Sub Slab
Sampled: 12/5/2018 14:54
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 1110
Canister Size: 6 liter
Flow Controller ID: 4173
Sample Type: 1 hr
Work Order: 18L0293
Initial Vacuum(in Hg): -28.9
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.1
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst
Tetrachloroethylene
0.70
0.20
0.11
4.7
1.4
0.75
4
12/12/18 14:38
BRF
Tetrahydrofuran
ND
0.20
0.13
ND
0.59
0.39
4
12/12/18 14:38
BRF
Toluene
ND
0.20
0.10
ND
0.75
0.39
4
12/12/18 14:38
BRF
1,2,4-Trichlorobenzene
ND
0.20
0.14
ND
1.5
1.0
4
12/12/18 14:38
BRF
1, 1, 1 -Trichloroethane
ND
0.20
0.075
ND
1.1
0.41
4
12/12/18 14:38
BRF
1,1,2-Trichloroethane
ND
0.20
0.082
ND
1.1
0.45
4
12/12/18 14:38
BRF
Trichloroethylene
2.5
0.20
0.081
14
1.1
0.43
4
12/12/18 14:38
BRF
Trichlorofluoromethane (Freon 11)
0.22
0.80
0.12
J 1.2
4.5
0.65
4
12/12/18 14:38
BRF
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
ND
0.80
0.12
ND
6.1
0.93
4
12/12/18 14:38
BRF
1,2,4-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.63
4
12/12/18 14:38
BRF
1,3,5-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.62
4
12/12/18 14:38
BRF
Vinyl Acetate
ND
4.0
0.095
ND
14
0.34
4
12/12/18 14:38
BRF
Vinyl Chloride
ND
0.20
0.13
ND
0.51
0.32
4
12/12/18 14:38
BRF
m&p-Xylene
ND
0.40
0.23
ND
1.7
1.00
4
12/12/18 14:38
BRF
o-Xylene
ND
0.20
0.12
ND
0.87
0.54
4
12/12/18 14:38
BRF
Surrogates
4-Bromofluorobenzene (1)
% Recovery
102
% REC Limits
70-130
12/12/18 14:38
Page 6 of 34

,con -testy
ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SSV-2
Sample ID: 18L0293-02
Sample Matrix: Sub Slab
Sampled: 12/5/2018 14:44
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location: Work Order: 18L0293
Sub Description/Location: Initial Vacuum(in Hg): -29.9
Canister ID: 1854 Final Vacuum(in Hg): -5
Canister Size: 6 liter Receipt Vacuum(in Hg): -5.5
Flow Controller ID: 4254 Flow Controller Type: Fixed -Orifice
Sample Type: 1 hr Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv
ug/m3
Date/Time
Analyte
Results
RL
MDL Flag/Qual
Results
RL
MDL
Dilution
Analyzed
Analyst
Acetone
9.1
8.0
2.8
22
19
6.6
4
12/12/18 15:35
BRF
Benzene
0.89
0.20
0.082
2.8
0.64
0.26
4
12/12/18 15:35
BRF
Benzyl chloride
ND
0.20
0.044
ND
1.0
0.23
4
12/12/18 15:35
BRF
Bromodichloromethane
ND
0.20
0.074
ND
1.3
0.49
4
12/12/18 15:35
BRF
Bromoform
ND
0.20
0.090
ND
2.1
0.93
4
12/12/18 15:35
BRF
Bromomethane
ND
0.20
0.14
ND
0.78
0.53
4
12/12/18 15:35
BRF
1,3-Butadiene
ND
0.20
0.13
ND
0.44
0.28
4
12/12/18 15:35
BRF
2-Butanone (MEK)
0.96
8.0
0.31 J
2.8
24
0.92
4
12/12/18 15:35
BRF
Carbon Disulfide
ND
2.0
0.14
ND
6.2
0.43
4
12/12/18 15:35
BRF
Carbon Tetrachloride
ND
0.20
0.065
ND
1.3
0.41
4
12/12/18 15:35
BRF
Chlorobenzene
ND
0.20
0.098
ND
0.92
0.45
4
12/12/18 15:35
BRF
Chloroethane
ND
0.40
0.12
ND
1.1
0.32
4
12/12/18 15:35
BRF
Chloroform
0.64
0.20
0.074
3.1
0.98
0.36
4
12/12/18 15:35
BRF
Chloromethane
ND
0.40
0.14
ND
0.83
0.28
4
12/12/18 15:35
BRF
Cyclohexane
ND
0.20
0.14
ND
0.69
0.49
4
12/12/18 15:35
BRF
Dibromochloromethane
ND
0.20
0.066
ND
1.7
0.57
4
12/12/18 15:35
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.078
ND
1.5
0.60
4
12/12/18 15:35
BRF
1,2-Dichlorobenzene
ND
0.20
0.096
ND
1.2
0.58
4
12/12/18 15:35
BRF
1,3-Dichlorobenzene
0.34
0.20
0.10
2.0
1.2
0.62
4
12/12/18 15:35
BRF
1,4-Dichlorobenzene
ND
0.20
0.12
ND
1.2
0.73
4
12/12/18 15:35
BRF
Dichlorodifluoromethane (Freon 12)
0.52
0.20
0.087
2.6
0.99
0.43
4
12/12/18 15:35
BRF
1,1-Dichloroethane
ND
0.20
0.061
ND
0.81
0.25
4
12/12/18 15:35
BRF
1,2-Dichloroethane
ND
0.20
0.076
ND
0.81
0.31
4
12/12/18 15:35
BRF
1,1-Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 15:35
BRF
cis-1,2-Dichloroethylene
ND
0.20
0.082
ND
0.79
0.32
4
12/12/18 15:35
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 15:35
BRF
1,2-Dichloropropane
ND
0.20
0.071
ND
0.92
0.33
4
12/12/18 15:35
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.070
ND
0.91
0.32
4
12/12/18 15:35
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.073
ND
0.91
0.33
4
12/12/18 15:35
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND
0.20
0.10
ND
1.4
0.70
4
12/12/18 15:35
BRF
1,4-Dioxane
ND
2.0
1.3
ND
7.2
4.6
4
12/12/18 15:35
BRF
Ethanol
11
8.0
3.6
21
15
6.7
4
12/12/18 15:35
BRF
Ethyl Acetate
ND
0.40
0.15
ND
1.4
0.54
4
12/12/18 15:35
BRF
Ethylbenzene
ND
0.20
0.12
ND
0.87
0.50
4
12/12/18 15:35
BRF
4-Ethyltoluene
ND
0.20
0.12
ND
0.98
0.60
4
12/12/18 15:35
BRF
Heptane
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 15:35
BRF
Hexachlorobutadiene
ND
0.20
0.092
ND
2.1
0.98
4
12/12/18 15:35
BRF
Hexane
ND
8.0
0.35
ND
28
1.2
4
12/12/18 15:35
BRF
2-Hexanone (MBK)
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 15:35
BRF
Isopropanol
ND
8.0
0.25
ND
20
0.60
4
12/12/18 15:35
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.10
ND
0.72
0.36
4
12/12/18 15:35
BRF
Methylene Chloride
ND
2.0
0.24
ND
6.9
0.84
4
12/12/18 15:35
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.096
ND
0.82
0.39
4
12/12/18 15:35
BRF
Naphthalene
ND
0.20
0.15
ND
1.0
0.80
4
12/12/18 15:35
BRF
Propene
ND
8.0
0.20
ND
14
0.34
4
12/12/18 15:35
BRF
Styrene
ND
0.20
0.12
ND
0.85
0.53
4
12/12/18 15:35
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.089
ND
1.4
0.61
4
12/12/18 15:35
BRF
Page 7 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Sample Description/Location:
Work Order: 18L0293
Date Received: 12/6/2018
Sub Description/Location:
Initial Vacuum(in Hg): -29.9
Field Sample #: SSV-2
Canister ID: 1854
Final Vacuum(in Hg): -5
Sample ID: 18L0293-02
Canister Size: 6 liter
Receipt Vacuum(in Hg): -5.5
Sample Matrix: Sub Slab
Flow Controller ID: 4254
Flow Controller Type: Fixed -Orifice
Sampled: 12/5/2018 14:44
Sample Type: 1 hr
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv
ug/m3
Date/Time
Analyte
Results
RL
MDL
Flag/Qual Results
RL
MDL
Dilution
Analyzed
Analyst
Tetrachloroethylene
25
0.20
0.11
170
1.4
0.75
4
12/12/18 15:35
BRF
Tetrahydrofuran
0.59
0.20
0.13
1.7
0.59
0.39
4
12/12/18 15:35
BRF
Toluene
0.92
0.20
0.10
3.5
0.75
0.39
4
12/12/18 15:35
BRF
1,2,4-Trichlorobenzene
ND
0.20
0.14
ND
1.5
1.0
4
12/12/18 15:35
BRF
1, 1, 1 -Trichloroethane
ND
0.20
0.075
ND
1.1
0.41
4
12/12/18 15:35
BRF
1,1,2-Trichloroethane
ND
0.20
0.082
ND
1.1
0.45
4
12/12/18 15:35
BRF
Trichloroethylene
480
2.0
0.81
2600
11
4.3
40
12/11/18 16:07
BRF
Trichlorofluoromethane (Freon 11)
0.27
0.80
0.12
J 1.5
4.5
0.65
4
12/12/18 15:35
BRF
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
ND
0.80
0.12
ND
6.1
0.93
4
12/12/18 15:35
BRF
1,2,4-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.63
4
12/12/18 15:35
BRF
1,3,5-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.62
4
12/12/18 15:35
BRF
Vinyl Acetate
ND
4.0
0.095
ND
14
0.34
4
12/12/18 15:35
BRF
Vinyl Chloride
ND
0.20
0.13
ND
0.51
0.32
4
12/12/18 15:35
BRF
m&p-Xylene
ND
0.40
0.23
ND
1.7
1.00
4
12/12/18 15:35
BRF
o-Xylene
ND
0.20
0.12
ND
0.87
0.54
4
12/12/18 15:35
BRF
Surrogates
% Recovery
% REC Limits
4-Bromofluorobenzene(1)
102
70-130
12/11/18 16:07
4-Bromofluorobenzene (1)
101
70-130
12/12/18 15:35
Page 8 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Sample Description/Location:
Work Order: 18L0293
Date Received: 12/6/2018
Sub Description/Location:
Initial Vacuum(in Hg): -29.3
Field Sample #: SSV-3
Canister ID: 1507
Final Vacuum(in Hg): -5
Sample ID: 18L0293-03
Canister Size: 6 liter
Receipt Vacuum(in Hg): -5.7
Sample Matrix: Sub Slab
Flow Controller ID: 4247
Flow Controller Type: Fixed -Orifice
Sampled: 12/5/2018 14:45
Sample Type: 1 hr
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
4.7
8.0
2.8
J 11
19
6.6
4
12/12/18 16:03
BRF
Benzene
ND
0.20
0.082
ND
0.64
0.26
4
12/12/18 16:03
BRF
Benzyl chloride
ND
0.20
0.044
ND
1.0
0.23
4
12/12/18 16:03
BRF
Bromodichloromethane
ND
0.20
0.074
ND
1.3
0.49
4
12/12/18 16:03
BRF
Bromoform
ND
0.20
0.090
ND
2.1
0.93
4
12/12/18 16:03
BRF
Bromomethane
ND
0.20
0.14
ND
0.78
0.53
4
12/12/18 16:03
BRF
1,3-Butadiene
ND
0.20
0.13
ND
0.44
0.28
4
12/12/18 16:03
BRF
2-Butanone (MEK)
0.60
8.0
0.31
J 1.8
24
0.92
4
12/12/18 16:03
BRF
Carbon Disulfide
ND
2.0
0.14
ND
6.2
0.43
4
12/12/18 16:03
BRF
Carbon Tetrachloride
ND
0.20
0.065
ND
1.3
0.41
4
12/12/18 16:03
BRF
Chlorobenzene
ND
0.20
0.098
ND
0.92
0.45
4
12/12/18 16:03
BRF
Chloroethane
ND
0.40
0.12
ND
1.1
0.32
4
12/12/18 16:03
BRF
Chloroform
ND
0.20
0.074
ND
0.98
0.36
4
12/12/18 16:03
BRF
Chloromethane
ND
0.40
0.14
ND
0.83
0.28
4
12/12/18 16:03
BRF
Cyclohexane
ND
0.20
0.14
ND
0.69
0.49
4
12/12/18 16:03
BRF
Dibromochloromethane
ND
0.20
0.066
ND
1.7
0.57
4
12/12/18 16:03
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.078
ND
1.5
0.60
4
12/12/18 16:03
BRF
1,2-Dichlorobenzene
ND
0.20
0.096
ND
1.2
0.58
4
12/12/18 16:03
BRF
1,3-Dichlorobenzene
1.0
0.20
0.10
6.1
1.2
0.62
4
12/12/18 16:03
BRF
1,4-Dichlorobenzene
ND
0.20
0.12
ND
1.2
0.73
4
12/12/18 16:03
BRF
Dichlorodifluoromethane (Freon 12)
0.55
0.20
0.087
2.7
0.99
0.43
4
12/12/18 16:03
BRF
1,1-Dichloroethane
ND
0.20
0.061
ND
0.81
0.25
4
12/12/18 16:03
BRF
1,2-Dichloroethane
ND
0.20
0.076
ND
0.81
0.31
4
12/12/18 16:03
BRF
1,1-Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 16:03
BRF
cis-1,2-Dichloroethylene
ND
0.20
0.082
ND
0.79
0.32
4
12/12/18 16:03
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 16:03
BRF
1,2-Dichloropropane
ND
0.20
0.071
ND
0.92
0.33
4
12/12/18 16:03
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.070
ND
0.91
0.32
4
12/12/18 16:03
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.073
ND
0.91
0.33
4
12/12/18 16:03
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
ND
0.20
0.10
ND
1.4
0.70
4
12/12/18 16:03
BRF
1,4-Dioxane
ND
2.0
1.3
ND
7.2
4.6
4
12/12/18 16:03
BRF
Ethanol
47
8.0
3.6
89
15
6.7
4
12/12/18 16:03
BRF
Ethyl Acetate
ND
0.40
0.15
ND
1.4
0.54
4
12/12/18 16:03
BRF
Ethylbenzene
ND
0.20
0.12
ND
0.87
0.50
4
12/12/18 16:03
BRF
4-Ethyltoluene
ND
0.20
0.12
ND
0.98
0.60
4
12/12/18 16:03
BRF
Heptane
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 16:03
BRF
Hexachlorobutadiene
ND
0.20
0.092
ND
2.1
0.98
4
12/12/18 16:03
BRF
Hexane
ND
8.0
0.35
ND
28
1.2
4
12/12/18 16:03
BRF
2-Hexanone (MBK)
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 16:03
BRF
Isopropanol
ND
8.0
0.25
ND
20
0.60
4
12/12/18 16:03
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.10
ND
0.72
0.36
4
12/12/18 16:03
BRF
Methylene Chloride
ND
2.0
0.24
ND
6.9
0.84
4
12/12/18 16:03
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.096
ND
0.82
0.39
4
12/12/18 16:03
BRF
Naphthalene
ND
0.20
0.15
ND
1.0
0.80
4
12/12/18 16:03
BRF
Propene
ND
8.0
0.20
ND
14
0.34
4
12/12/18 16:03
BRF
Styrene
ND
0.20
0.12
ND
0.85
0.53
4
12/12/18 16:03
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.089
ND
1.4
0.61
4
12/12/18 16:03
BRF
Page 9 of 34

,con -testy
ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: SSV-3
Sample ID: 18L0293-03
Sample Matrix: Sub Slab
Sampled: 12/5/2018 14:45
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 1507
Canister Size: 6 liter
Flow Controller ID: 4247
Sample Type: 1 hr
Work Order: 18L0293
Initial Vacuum(in Hg): -29.3
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.7
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst
Tetrachloroethylene
0.27
0.20
0.11
1.8
1.4
0.75
4
12/12/18 16:03
BRF
Tetrahydrofuran
ND
0.20
0.13
ND
0.59
0.39
4
12/12/18 16:03
BRF
Toluene
0.31
0.20
0.10
1.2
0.75
0.39
4
12/12/18 16:03
BRF
1,2,4-Trichlorobenzene
ND
0.20
0.14
ND
1.5
1.0
4
12/12/18 16:03
BRF
1, 1, 1 -Trichloroethane
ND
0.20
0.075
ND
1.1
0.41
4
12/12/18 16:03
BRF
1,1,2-Trichloroethane
ND
0.20
0.082
ND
1.1
0.45
4
12/12/18 16:03
BRF
Trichloroethylene
ND
0.20
0.081
ND
1.1
0.43
4
12/12/18 16:03
BRF
Trichlorofluoromethane (Freon 11)
0.24
0.80
0.12
J 1.4
4.5
0.65
4
12/12/18 16:03
BRF
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
ND
0.80
0.12
ND
6.1
0.93
4
12/12/18 16:03
BRF
1,2,4-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.63
4
12/12/18 16:03
BRF
1,3,5-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.62
4
12/12/18 16:03
BRF
Vinyl Acetate
ND
4.0
0.095
ND
14
0.34
4
12/12/18 16:03
BRF
Vinyl Chloride
ND
0.20
0.13
ND
0.51
0.32
4
12/12/18 16:03
BRF
m&p-Xylene
ND
0.40
0.23
ND
1.7
1.00
4
12/12/18 16:03
BRF
o-Xylene
ND
0.20
0.12
ND
0.87
0.54
4
12/12/18 16:03
BRF
Surrogates
4-Bromofluorobenzene (1)
% Recovery
101
% REC Limits
70-130
12/12/18 16:03
Page 10 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Sample Description/Location:
Work Order: 18L0293
Date Received: 12/6/2018
Sub Description/Location:
Initial Vacuum(in Hg): -28.9
Field Sample #: DUP-SSV
Canister ID: 1721
Final Vacuum(in Hg): -5
Sample ID: 18L0293-04
Canister Size: 6 liter
Receipt Vacuum(in Hg): -5.1
Sample Matrix: Sub Slab
Flow Controller ID:
Flow Controller Type: Fixed -Orifice
Sampled: 12/5/2018 00:00
Sample Type: 1 hr
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual Results
ug/m3
RL
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
4.3
8.0
2.8
J 10
19
6.6
4
12/12/18 16:31
BRF
Benzene
ND
0.20
0.082
ND
0.64
0.26
4
12/12/18 16:31
BRF
Benzyl chloride
ND
0.20
0.044
ND
1.0
0.23
4
12/12/18 16:31
BRF
Bromodichloromethane
ND
0.20
0.074
ND
1.3
0.49
4
12/12/18 16:31
BRF
Bromoform
ND
0.20
0.090
ND
2.1
0.93
4
12/12/18 16:31
BRF
Bromomethane
ND
0.20
0.14
ND
0.78
0.53
4
12/12/18 16:31
BRF
1,3-Butadiene
ND
0.20
0.13
ND
0.44
0.28
4
12/12/18 16:31
BRF
2-Butanone (MEK)
ND
8.0
0.31
ND
24
0.92
4
12/12/18 16:31
BRF
Carbon Disulfide
ND
2.0
0.14
ND
6.2
0.43
4
12/12/18 16:31
BRF
Carbon Tetrachloride
ND
0.20
0.065
ND
1.3
0.41
4
12/12/18 16:31
BRF
Chlorobenzene
ND
0.20
0.098
ND
0.92
0.45
4
12/12/18 16:31
BRF
Chloroethane
ND
0.40
0.12
ND
1.1
0.32
4
12/12/18 16:31
BRF
Chloroform
ND
0.20
0.074
ND
0.98
0.36
4
12/12/18 16:31
BRF
Chloromethane
ND
0.40
0.14
ND
0.83
0.28
4
12/12/18 16:31
BRF
Cyclohexane
ND
0.20
0.14
ND
0.69
0.49
4
12/12/18 16:31
BRF
Dibromochloromethane
ND
0.20
0.066
ND
1.7
0.57
4
12/12/18 16:31
BRF
1,2-Dibromoethane (EDB)
ND
0.20
0.078
ND
1.5
0.60
4
12/12/18 16:31
BRF
1,2-Dichlorobenzene
ND
0.20
0.096
ND
1.2
0.58
4
12/12/18 16:31
BRF
1,3-Dichlorobenzene
0.24
0.20
0.10
1.4
1.2
0.62
4
12/12/18 16:31
BRF
1,4-Dichlorobenzene
ND
0.20
0.12
ND
1.2
0.73
4
12/12/18 16:31
BRF
Dichlorodifluoromethane (Freon 12)
0.52
0.20
0.087
2.6
0.99
0.43
4
12/12/18 16:31
BRF
1,1-Dichloroethane
ND
0.20
0.061
ND
0.81
0.25
4
12/12/18 16:31
BRF
1,2-Dichloroethane
ND
0.20
0.076
ND
0.81
0.31
4
12/12/18 16:31
BRF
1,1-Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 16:31
BRF
cis-1,2-Dichloroethylene
ND
0.20
0.082
ND
0.79
0.32
4
12/12/18 16:31
BRF
trans-1,2-Dichloroethylene
ND
0.20
0.081
ND
0.79
0.32
4
12/12/18 16:31
BRF
1,2-Dichloropropane
ND
0.20
0.071
ND
0.92
0.33
4
12/12/18 16:31
BRF
cis- 1,3 -Dichloropropene
ND
0.20
0.070
ND
0.91
0.32
4
12/12/18 16:31
BRF
trans- 1, 3 -Dichloropropene
ND
0.20
0.073
ND
0.91
0.33
4
12/12/18 16:31
BRF
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
ND
0.20
0.10
ND
1.4
0.70
4
12/12/18 16:31
BRF
1,4-Dioxane
ND
2.0
1.3
ND
7.2
4.6
4
12/12/18 16:31
BRF
Ethanol
5.0
8.0
3.6
J 9.4
15
6.7
4
12/12/18 16:31
BRF
Ethyl Acetate
ND
0.40
0.15
ND
1.4
0.54
4
12/12/18 16:31
BRF
Ethylbenzene
ND
0.20
0.12
ND
0.87
0.50
4
12/12/18 16:31
BRF
4-Ethyltoluene
ND
0.20
0.12
ND
0.98
0.60
4
12/12/18 16:31
BRF
Heptane
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 16:31
BRF
Hexachlorobutadiene
ND
0.20
0.092
ND
2.1
0.98
4
12/12/18 16:31
BRF
Hexane
ND
8.0
0.35
ND
28
1.2
4
12/12/18 16:31
BRF
2-Hexanone (MBK)
ND
0.20
0.12
ND
0.82
0.48
4
12/12/18 16:31
BRF
Isopropanol
ND
8.0
0.25
ND
20
0.60
4
12/12/18 16:31
BRF
Methyl tert-Butyl Ether (MTBE)
ND
0.20
0.10
ND
0.72
0.36
4
12/12/18 16:31
BRF
Methylene Chloride
ND
2.0
0.24
ND
6.9
0.84
4
12/12/18 16:31
BRF
4-Methyl-2-pentanone (MIBK)
ND
0.20
0.096
ND
0.82
0.39
4
12/12/18 16:31
BRF
Naphthalene
ND
0.20
0.15
ND
1.0
0.80
4
12/12/18 16:31
BRF
Propene
ND
8.0
0.20
ND
14
0.34
4
12/12/18 16:31
BRF
Styrene
ND
0.20
0.12
ND
0.85
0.53
4
12/12/18 16:31
BRF
1,1,2,2-Tetrachloroethane
ND
0.20
0.089
ND
1.4
0.61
4
12/12/18 16:31
BRF
Page 11 of 34

,con -testy
ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 12/6/2018
Field Sample #: DUP-SSV
Sample ID: 18L0293-04
Sample Matrix: Sub Slab
Sampled: 12/5/2018 00:00
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 1721
Canister Size: 6 liter
Flow Controller ID:
Sample Type: 1 hr
Work Order: 18L0293
Initial Vacuum(in Hg): -28.9
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -5.1
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst
Tetrachloroethylene
0.74
0.20
0.11
5.0
1.4
0.75
4
12/12/18 16:31
BRF
Tetrahydrofuran
ND
0.20
0.13
ND
0.59
0.39
4
12/12/18 16:31
BRF
Toluene
ND
0.20
0.10
ND
0.75
0.39
4
12/12/18 16:31
BRF
1,2,4-Trichlorobenzene
ND
0.20
0.14
ND
1.5
1.0
4
12/12/18 16:31
BRF
1, 1, 1 -Trichloroethane
ND
0.20
0.075
ND
1.1
0.41
4
12/12/18 16:31
BRF
1,1,2-Trichloroethane
ND
0.20
0.082
ND
1.1
0.45
4
12/12/18 16:31
BRF
Trichloroethylene
2.7
0.20
0.081
14
1.1
0.43
4
12/12/18 16:31
BRF
Trichlorofluoromethane (Freon 11)
0.24
0.80
0.12
J 1.3
4.5
0.65
4
12/12/18 16:31
BRF
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
ND
0.80
0.12
ND
6.1
0.93
4
12/12/18 16:31
BRF
1,2,4-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.63
4
12/12/18 16:31
BRF
1,3,5-Trimethylbenzene
ND
0.20
0.13
ND
0.98
0.62
4
12/12/18 16:31
BRF
Vinyl Acetate
ND
4.0
0.095
ND
14
0.34
4
12/12/18 16:31
BRF
Vinyl Chloride
ND
0.20
0.13
ND
0.51
0.32
4
12/12/18 16:31
BRF
m&p-Xylene
ND
0.40
0.23
ND
1.7
1.00
4
12/12/18 16:31
BRF
o-Xylene
ND
0.20
0.12
ND
0.87
0.54
4
12/12/18 16:31
BRF
Surrogates
4-Bromofluorobenzene (1)
% Recovery
102
% REC Limits
70-130
12/12/18 16:31
Page 12 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction
Data
Prep Method: TO-15 Prep -EPA TO-15
Pre-Dil
Pre-Dil
Default
Actual
Pressure
Pre
Initial
Final
Injection
Injection
Lab Number [Field ID]
Batch
Dilution
Dilution
mL
mL
mL
mL
Date
18L0293-02RE1 [SSV-2]
B219031
1.5
1
N/A
1000
400
15
12/11/18
Prep Method: TO-15 Prep -EPA TO-15
Pre-Dil
Pre-Dil
Default
Actual
Pressure
Pre
Initial
Final
Injection
Injection
Lab Number [Field ID]
Batch
Dilution
Dilution
mL
mL
mL
mL
Date
18LO293-01 [SSV-1]
B219146
1.5
1
N/A
1000
400
150
12/12/18
18L0293-02 [SSV-2]
B219146
1.5
1
N/A
1000
400
150
12/12/18
18L0293-03 [SSV-3]
B219146
1.5
1
N/A
1000
400
150
12/12/18
18L0293-04 [DUP-SSV]
B219146
1.5
1
N/A
1000
400
150
12/12/18
Page 13 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua
Batch B219031 - TO-15 Prep
Blank (B219031-BLK1)
Prepared & Analyzed: 12/11/18
Acetone
0.62
1.4
J
Benzene
ND
0.035
Benzyl chloride
ND
0.035
Bromodichloromethane
ND
0.035
Bromoform
ND
0.035
Bromomethane
ND
0.035
1,3-Butadiene
ND
0.035
2-Butanone (MEK)
ND
1.4
Carbon Disulfide
ND
0.35
Carbon Tetrachloride
ND
0.035
Chlorobenzene
ND
0.035
Chloroethane
ND
0.035
Chloroform
ND
0.035
Chloromethane
ND
0.070
Cyclohexane
ND
0.035
Dibromochloromethane
ND
0.035
1,2-Dibromoethane (EDB)
ND
0.035
1,2-Dichlorobenzene
ND
0.035
1,3-Dichlorobenzene
ND
0.035
1,4-Dichlorobenzene
ND
0.035
Dichlorodifluoromethane (Freon 12)
ND
0.035
1,1-Dichloroethane
ND
0.035
1,2-Dichloroethane
ND
0.035
1,1-Dichloroethylene
ND
0.035
cis-1,2-Dichloroethylene
ND
0.035
trans-1,2-Dichloroethylene
ND
0.035
1,2-Dichloropropane
ND
0.035
cis- 1,3 -Dichloropropene
ND
0.035
trans- l,3-Dichloropropene
ND
0.035
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane
ND
0.035
(Freon 114)
1,4-Dioxane
ND
0.35
Ethanol
ND
1.4
Ethyl Acetate
ND
0.035
Ethylbenzene
ND
0.035
4-Ethyltoluene
ND
0.035
Heptane
ND
0.035
Hexachlorobutadiene
ND
0.035
Hexane
ND
1.4
2-Hexanone (MBK)
ND
0.035
Isopropanol
ND
1.4
Methyl tert-Butyl Ether (MTBE)
ND
0.035
Methylene Chloride
ND
0.35
4-Methyl-2-pentanone (MIBK)
ND
0.035
Naphthalene
ND
0.035
Propene
ND
1.4
Styrene
ND
0.035
Page 14 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
knalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua]
Batch B219031 - TO-15 Prep
Blank (B219031-BLKI)
Prepared & Analyzed: 12/11/18
1,1,2,2-Tetrachloroethane
ND
0.035
Tetrachloroethylene
ND
0.035
Tetrahydrofuran
ND
0.035
Toluene
ND
0.035
1,2,4-Trichlorobenzene
ND
0.035
1, 1, 1 -Trichloroethane
ND
0.035
1,1,2-Trichloroethane
ND
0.035
Trichloroethylene
ND
0.035
Trichlorofluoromethane (Freon 11)
ND
0.14
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.14
113)
1,2,4-Trimethylbenzene
ND
0.035
1,3,5-Trimethylbenzene
ND
0.035
Vinyl Acetate
ND
0.70
Vinyl Chloride
ND
0.035
m&p-Xylene
ND
0.070
o-Xylene
ND
0.035
Surrogate: 4-Bromofluorobenzene (1)
LCS (B219031-BSI)
8.16
8.00 102
Prepared & Analyzed: 12/11/18
70-130
Acetone
5.36
5.00
107
70-130
Benzene
4.82
5.00
96.3
70-130
Benzyl chloride
4.95
5.00
98.9
70-130
Bromodichloromethane
5.03
5.00
101
70-130
Bromoform
5.77
5.00
115
70-130
Bromomethane
4.71
5.00
94.2
70-130
1,3-Butadiene
5.37
5.00
107
70-130
2-Butanone (MEK)
4.88
5.00
97.7
70-130
Carbon Disulfide
6.39
5.00
128
70-130
Carbon Tetrachloride
5.62
5.00
112
70-130
Chlorobenzene
4.94
5.00
98.7
70-130
Chloroethane
4.65
5.00
93.0
70-130
Chloroform
5.92
5.00
118
70-130
Chloromethane
5.03
5.00
101
70-130
Cyclohexane
5.42
5.00
108
70-130
Dibromochloromethane
5.36
5.00
107
70-130
1,2-Dibromoethane (EDB)
5.47
5.00
109
70-130
1,2-Dichlorobenzene
5.81
5.00
116
70-130
1,3-Dichlorobenzene
5.64
5.00
113
70-130
1,4-Dichlorobenzene
5.83
5.00
117
70-130
Dichlorodifluoromethane (Freon 12)
5.66
5.00
113
70-130
1,1-Dichloroethane
5.75
5.00
115
70-130
1,2-Dichloroethane
5.60
5.00
112
70-130
1,1-Dichloroethylene
4.87
5.00
97.3
70-130
cis-1,2-Dichloroethylene
5.64
5.00
113
70-130
trans-1,2-Dichloroethylene
6.06
5.00
121
70-130
1,2-Dichloropropane
5.00
5.00
100
70-130
Page 15 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua
Batch B219031 - TO-15 Prep
LCS (B219031-BSI)
Prepared & Analyzed: 12/11/18
cis-1,3-Dichloropropene
5.19
5.00
104
70-130
trans-1,3-Dichloropropene
5.32
5.00
106
70-130
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane
5.22
5.00
104
70-130
(Freon 114)
1,4-Dioxane
4.87
5.00
97.4
70-130
Ethanol
3.34
5.00
66.8 *
70-130 Z-01
Ethyl Acetate
5.69
5.00
114
70-130
Ethylbenzene
4.84
5.00
96.8
70-130
4-Ethyltoluene
5.17
5.00
103
70-130
Heptane
4.81
5.00
96.3
70-130
Hexachlorobutadiene
6.57
5.00
131 *
70-130 Z-01
Hexane
6.01
5.00
120
70-130
2-Hexanone (MBK)
4.18
5.00
83.6
70-130
Isopropanol
4.11
5.00
82.1
70-130
Methyl tert-Butyl Ether (MTBE)
5.81
5.00
116
70-130
Methylene Chloride
4.70
5.00
94.1
70-130
4-Methyl-2-pentanone (MIBK)
4.33
5.00
86.7
70-130
Naphthalene
4.96
5.00
99.1
70-130
Propene
4.74
5.00
94.7
70-130
Styrene
5.40
5.00
108
70-130
1,1,2,2-Tetrachloroethane
4.80
5.00
96.0
70-130
Tetrachloroethylene
5.67
5.00
113
70-130
Tetrahydrofuran
5.58
5.00
112
70-130
Toluene
5.14
5.00
103
70-130
1,2,4-Trichlorobenzene
6.09
5.00
122
70-130
1, 1, 1 -Trichloroethane
4.97
5.00
99.4
70-130
1,1,2-Trichloroethane
5.22
5.00
104
70-130
Trichloroethylene
5.42
5.00
108
70-130
Trichlorofluoromethane (Freon 11)
5.64
5.00
113
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
5.53
5.00
ill
70-130
113)
1,2,4-Trimethylbenzene
5.30
5.00
106
70-130
1,3,5-Trimethylbenzene
5.31
5.00
106
70-130
Vinyl Acetate
4.66
5.00
93.3
70-130
Vinyl Chloride
5.28
5.00
106
70-130
m&p-Xylene
10.3
10.0
103
70-130
o-Xylene
5.21
5.00
104
70-130
Surrogate: 4-Bromofluorobenzene (1) 8.59 8.00 107 70-130
Page 16 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
.nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua
Batch B219146 - TO-15 Prep
Blank (B219146-BLKI)
Prepared & Analyzed: 12/12/18
Acetone
ND
1.4
Benzene
ND
0.035
Benzyl chloride
ND
0.035
Bromodichloromethane
ND
0.035
Bromoform
ND
0.035
Bromomethane
ND
0.035
1,3-Butadiene
ND
0.035
2-Butanone (MEK)
ND
1.4
Carbon Disulfide
ND
0.35
Carbon Tetrachloride
ND
0.035
Chlorobenzene
ND
0.035
Chloroethane
ND
0.035
Chloroform
ND
0.035
Chloromethane
ND
0.070
Cyclohexane
ND
0.035
Dibromochloromethane
ND
0.035
1,2-Dibromoethane (EDB)
ND
0.035
1,2-Dichlorobenzene
ND
0.035
1,3-Dichlorobenzene
ND
0.035
1,4-Dichlorobenzene
ND
0.035
Dichlorodifluoromethane (Freon 12)
ND
0.035
1,1-Dichloroethane
ND
0.035
1,2-Dichloroethane
ND
0.035
1,1-Dichloroethylene
ND
0.035
cis-1,2-Dichloroethylene
ND
0.035
trans-1,2-Dichloroethylene
ND
0.035
1,2-Dichloropropane
ND
0.035
cis-1,3-Dichloropropene
ND
0.035
trans- 1, 3 -Dichloropropene
ND
0.035
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane
ND
0.035
(Freon 114)
1,4-Dioxane
ND
0.35
Ethanol
ND
1.4
Ethyl Acetate
ND
0.035
Ethylbenzene
ND
0.035
4-Ethyltoluene
ND
0.035
Heptane
ND
0.035
Hexachlorobutadiene
ND
0.035
Hexane
ND
1.4
2-Hexanone (MBK)
ND
0.035
Isopropanol
ND
1.4
Methyl tert-Butyl Ether (MTBE)
ND
0.035
Methylene Chloride
ND
0.35
4-Methyl-2-pentanone (MIBK)
ND
0.035
Naphthalene
ND
0.035
Propene
ND
1.4
Styrene
ND
0.035
Page 17 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
knalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua]
Batch B219146 - TO-15 Prep
Blank (B219146-BLKI)
Prepared & Analyzed: 12/12/18
1,1,2,2-Tetrachloroethane
ND
0.035
Tetrachloroethylene
ND
0.035
Tetrahydrofuran
ND
0.035
Toluene
ND
0.035
1,2,4-Trichlorobenzene
ND
0.035
1, 1, 1 -Trichloroethane
ND
0.035
1,1,2-Trichloroethane
ND
0.035
Trichloroethylene
ND
0.035
Trichlorofluoromethane (Freon 11)
ND
0.14
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.14
113)
1,2,4-Trimethylbenzene
ND
0.035
1,3,5-Trimethylbenzene
ND
0.035
Vinyl Acetate
ND
0.70
Vinyl Chloride
ND
0.035
m&p-Xylene
ND
0.070
o-Xylene
ND
0.035
Surrogate: 4-Bromofluorobenzene (1)
LCS (B219146-BSI)
8.14
8.00 102
Prepared & Analyzed: 12/12/18
70-130
Acetone
5.65
5.00
113
70-130
Benzene
4.97
5.00
99.4
70-130
Benzyl chloride
5.13
5.00
103
70-130
Bromodichloromethane
5.21
5.00
104
70-130
Bromoform
5.85
5.00
117
70-130
Bromomethane
5.03
5.00
101
70-130
1,3-Butadiene
5.62
5.00
112
70-130
2-Butanone (MEK)
5.05
5.00
101
70-130
Carbon Disulfide
6.63
5.00
133
* 70-130 L-01, V-36
Carbon Tetrachloride
5.82
5.00
116
70-130
Chlorobenzene
5.01
5.00
100
70-130
Chloroethane
4.88
5.00
97.5
70-130
Chloroform
6.30
5.00
126
70-130
Chloromethane
5.25
5.00
105
70-130
Cyclohexane
5.60
5.00
112
70-130
Dibromochloromethane
5.54
5.00
ill
70-130
1,2-Dibromoethane (EDB)
5.64
5.00
113
70-130
1,2-Dichlorobenzene
5.98
5.00
120
70-130
1,3-Dichlorobenzene
5.82
5.00
116
70-130
1,4-Dichlorobenzene
6.00
5.00
120
70-130
Dichlorodifluoromethane (Freon 12)
5.90
5.00
118
70-130
1,1-Dichloroethane
6.21
5.00
124
70-130
1,2-Dichloroethane
5.96
5.00
119
70-130
1,1-Dichloroethylene
5.26
5.00
105
70-130
cis-1,2-Dichloroethylene
6.09
5.00
122
70-130
trans-1,2-Dichloroethylene
6.48
5.00
130
70-130
1,2-Dichloropropane
5.08
5.00
102
70-130
Page 18 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua
Batch B219146 - TO-15 Prep
LCS (B219146-BSI)
Prepared & Analyzed: 12/12/18
cis-1,3-Dichloropropene
5.38
5.00
108
70-130
trans-1,3-Dichloropropene
5.51
5.00
110
70-130
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane
5.59
5.00
112
70-130
(Freon 114)
1,4-Dioxane
4.86
5.00
97.2
70-130
Ethanol
3.44
5.00
68.8 *
70-130 Z-01
Ethyl Acetate
6.03
5.00
121
70-130
Ethylbenzene
4.94
5.00
98.8
70-130
4-Ethyltoluene
5.29
5.00
106
70-130
Heptane
4.91
5.00
98.3
70-130
Hexachlorobutadiene
6.90
5.00
138 *
70-130 Z-01
Hexane
6.37
5.00
127
70-130
2-Hexanone (MBK)
4.12
5.00
82.5
70-130
Isopropanol
4.34
5.00
86.8
70-130
Methyl tert-Butyl Ether (MTBE)
6.28
5.00
126
70-130
Methylene Chloride
4.92
5.00
98.5
70-130
4-Methyl-2-pentanone (MIBK)
4.31
5.00
86.2
70-130
Naphthalene
5.38
5.00
108
70-130
Propene
4.84
5.00
96.9
70-130
Styrene
5.47
5.00
109
70-130
1,1,2,2-Tetrachloroethane
4.88
5.00
97.5
70-130
Tetrachloroethylene
5.96
5.00
119
70-130
Tetrahydrofuran
5.89
5.00
118
70-130
Toluene
5.29
5.00
106
70-130
1,2,4-Trichlorobenzene
6.24
5.00
125
70-130
1, 1, 1 -Trichloroethane
5.07
5.00
101
70-130
1,1,2-Trichloroethane
5.40
5.00
108
70-130
Trichloroethylene
5.61
5.00
112
70-130
Trichlorofluoromethane (Freon 11)
6.10
5.00
122
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
5.87
5.00
117
70-130
113)
1,2,4-Trimethylbenzene
5.41
5.00
108
70-130
1,3,5-Trimethylbenzene
5.38
5.00
108
70-130
Vinyl Acetate
4.94
5.00
98.8
70-130
Vinyl Chloride
5.49
5.00
110
70-130
m&p-Xylene
10.4
10.0
104
70-130
o-Xylene
5.33
5.00
107
70-130
Surrogate: 4-Bromofluorobenzene (1) 8.58 8.00 107 70-130
Page 19 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
knalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua]
Batch B219146 - TO-15 Prep
Duplicate (B219146-DUPI)
Source: 18LO293-01
Prepared & Analyzed: 12/12/18
Acetone
3.9
8.0
9.1
19
4.0
2.87 25 1
Benzene
ND
0.20
ND
0.64
ND
25
Benzyl chloride
ND
0.20
ND
1.0
ND
25
Bromodichloromethane
ND
0.20
ND
1.3
ND
25
Bromoform
ND
0.20
ND
2.1
ND
25
Bromomethane
ND
0.20
ND
0.78
ND
25
1,3-Butadiene
ND
0.20
ND
0.44
ND
25
2-Butanone (MEK)
ND
8.0
ND
24
ND
25
Carbon Disulfide
ND
2.0
ND
6.2
ND
25
Carbon Tetrachloride
ND
0.20
ND
1.3
ND
25
Chlorobenzene
ND
0.20
ND
0.92
ND
25
Chloroethane
ND
0.20
ND
0.53
ND
25
Chloroform
ND
0.20
ND
0.98
ND
25
Chloromethane
ND
0.40
ND
0.83
ND
25
Cyclohexane
ND
0.20
ND
0.69
ND
25
Dibromochloromethane
ND
0.20
ND
1.7
ND
25
1,2-Dibromoethane (EDB)
ND
0.20
ND
1.5
ND
25
1,2-Dichlorobenzene
ND
0.20
ND
1.2
ND
25
1,3-Dichlorobenzene
0.22
0.20
1.3
1.2
0.21
5.50 25
1,4-Dichlorobenzene
ND
0.20
ND
1.2
ND
25
Dichlorodifluoromethane (Freon 12)
0.54
0.20
2.7
0.99
0.54
0.00 25
1,1-Dichloroethane
ND
0.20
ND
0.81
ND
25
1,2-Dichloroethane
ND
0.20
ND
0.81
ND
25
1,1-Dichloroethylene
ND
0.20
ND
0.79
ND
25
cis-1,2-Dichloroethylene
ND
0.20
ND
0.79
ND
25
trans-1,2-Dichloroethylene
ND
0.20
ND
0.79
ND
25
1,2-Dichloropropane
ND
0.20
ND
0.92
ND
25
cis-1,3-Dichloropropene
ND
0.20
ND
0.91
ND
25
trans- 1, 3 -Dichloropropene
ND
0.20
ND
0.91
ND
25
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane
ND
0.20
ND
1.4
ND
25
(Freon 114)
1,4-Dioxane
ND
2.0
ND
7.2
ND
25
Ethanol
5.3
8.0
9.9
15
5.3
1.51 25 1
Ethyl Acetate
ND
0.20
ND
0.72
ND
25
Ethylbenzene
ND
0.20
ND
0.87
ND
25
4-Ethyltoluene
ND
0.20
ND
0.98
ND
25
Heptane
ND
0.20
ND
0.82
ND
25
Hexachlorobutadiene
ND
0.20
ND
2.1
ND
25
Hexane
ND
8.0
ND
28
ND
25
2-Hexanone (MBK)
ND
0.20
ND
0.82
ND
25
Isopropanol
ND
8.0
ND
20
ND
25
Methyl tert-Butyl Ether (MTBE)
ND
0.20
ND
0.72
ND
25
Methylene Chloride
ND
2.0
ND
6.9
ND
25
4-Methyl-2-pentanone (MIBK)
ND
0.20
ND
0.82
ND
25
Naphthalene
ND
0.20
ND
1.0
ND
25
Propene
ND
8.0
ND
14
ND
25
Styrene
ND
0.20
ND
0.85
ND
25
Page 20 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual
Batch B219146 - TO-15 Prep
Duplicate (B219146-DUPI)
Source: 18LO293-01
Prepared & Analyzed: 12/12/18
1,1,2,2-Tetrachloroethane
ND
0.20
ND
1.4
ND
25
Tetrachloroethylene
0.74
0.20
5.0
1.4
0.70
6.67 25
Tetrahydrofuran
ND
0.20
ND
0.59
ND
25
Toluene
ND
0.20
ND
0.75
ND
25
1,2,4-Trichlorobenzene
ND
0.20
ND
1.5
ND
25
1, 1, 1 -Trichloroethane
ND
0.20
ND
1.1
ND
25
1,1,2-Trichloroethane
ND
0.20
ND
1.1
ND
25
Trichloroethylene
2.6
0.20
14
1.1
2.5
3.44 25
Trichlorofluoromethane (Freon 11)
0.26
0.80
1.5
4.5
0.22
18.2 25 J
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.80
ND
6.1
ND
25
113)
1,2,4-Trimethylbenzene
ND
0.20
ND
0.98
ND
25
1,3,5-Trimethylbenzene
ND
0.20
ND
0.98
ND
25
Vinyl Acetate
ND
4.0
ND
14
ND
25
Vinyl Chloride
ND
0.20
ND
0.51
ND
25
m&p-Xylene
ND
0.40
ND
1.7
ND
25
o-Xylene
ND
0.20
ND
0.87
ND
25
Surrogate: 4-Bromofluorobenzene (1) 8.08 8.00 101 70-130
Page 21 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
t
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
RL
Reporting Limit
MDL
Method Detection Limit
RPD
Relative Percent Difference
LCS
Laboratory Control Sample
LCS Dup
Duplicate Laboratory Control Sample
MS
Matrix Spike Sample
MS Dup
Duplicate Matrix Spike Sample
REC
Recovery
QC
Quality Control
ppbv
Parts per billion volume
EPA
United States Environmental Protection Agency
% REC
Percent Recovery
ND
Not Detected
N/A
Not Applicable
DL
Detection Limit
NC Not Calculated
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation -Reduction Potential
wet Not dry weight corrected
% wt Percent weight
Kg Kilogram
g Gram
mg Milligram
µg Microgram
ng Nanogram
L Liter
mL Milliliter
µL Microliter
m3 Cubic Meter
EPH Extractable Petroleum Hydrocarbons
VPH Volatile Petroleum Hydrocarbons
APH Air Petroleum Hydrocarbons
FID Flame Ionization Detector
PID Photo Ionization Detector
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-01 Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not
affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high
side.
V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound.
V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
V-36 Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
Z-01 Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult
compound and passes the in house limits of 50-150%.
Page 22 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYST
RLF Rebecca Faust
RAP Raisa A. Petraitis
KKM Kerry K. McGee
BRF Brittany R. Fisk
Page 23 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] ` TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area o/
Limits
RT Diff
RT Diff
Limit
Q
Initial Cal Check (S029991-ICV1) Lab File ID: B120417.D Analyzed: 12/04/18 22:13
Bromochloromethane (1)
80510
5.072
82524
5.077
98
60 - 140
-0.0050
+/-0.50
1,4-Difluorobenzene (1)
180031
6.292
183364
6.291
98
60 - 140
0.0010
+/-0.50
Chlorobenzene-d5(1)
157522
9.891
164139
9.89
96
60-140
0.0010
+/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area o/
Limits
RT Diff
RT Diff
Limit
Q
Calibration Check (S030210-CCV1) Lab File ID: 13121104.1) Analyzed: 12/11/18 10:10
Bromochloromethane (1)
80580
5.073
82524
5.077
98
60 - 140
-0.0040
+/-0.50
1,4-Difluorobenzene (1)
198654
6.292
183364
6.291
108
60 - 140
0.0010
+/-0.50
Chlorobenzene-d5(1)
177968
9.892
164139
9.89
108
60-140
0.0020
+/-0.50
LCS (B219031-BS1 ) Lab File ID: B121105.D Analyzed: 12/11/18 10:38
Bromochloromethane (1)
78305
5.071
80580
5.073
97
60 - 140
-0.0020
+/-0.50
1,4-Difluorobenzene (1)
192472
6.297
198654
6.292
97
60 - 140
0.0050
+/-0.50
Chlorobenzene-d5(1)
172160
9.89
177968
9.892
97
60-140
-0.0020
+/-0.50
Blank (B219031-BLK1) Lab File ID: B121107.D Analyzed: 12/11/18 11:39
Bromochloromethane (1)
80889
5.073
80580
5.073
100
60 - 140
0.0000
+/-0.50
1,4-Difluorobenzene (1)
199242
6.293
198654
6.292
100
60 - 140
0.0010
+/-0.50
Chlorobenzene-d5(1)
181433
9.892
177968
9.892
102
60-140
0.0000
+/-0.50
SSV-2 (18L0293-02RE1) Lab File ID: B121112.D Analyzed: 12/11/18 16:07
Bromochloromethane (1)
78488
5.077
80580
5.073
97
60 - 140
0.0040
+/-0.50
1,4-Difluorobenzene (1)
197038
6.297
198654
6.292
99
60 - 140
0.0050
+/-0.50
Chlorobenzene-d5(1)
176130
9.89
177968
9.892
99
60-140
-0.0020
+/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area %
Limits
RT Diff
RT Diff
Limit
Q
Calibration Check (S030250-CCV1) Lab File ID: B121204.D Analyzed: 12/12/18 10:26
Bromochloromethane (1)
75997
5.078
82524
5.077
92
60 - 140
0.0010
+/-0.50
1,4-Difluorobenzene (1)
193987
6.298
183364
6.291
106
60 - 140
0.0070
+/-0.50
Chlorobenzene-d5(1)
175616
9.891
164139
9.89
107
60-140
0.0010
+/-0.50
LCS (B219146-BS1 ) Lab File ID: B121205.D Analyzed: 12/12/18 10:54
Bromochloromethane (1)
74877
5.072
75997
5.078
99
60 - 140
-0.0060
+/-0.50
1,4-Difluorobenzene (1)
195233
6.292
193987
6.298
101
60 - 140
-0.0060
+/-0.50
Chlorobenzene-d5(1)
175233
9.891
175616
9.891
100
60-140
0.0000
+/-0.50
Page 24 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] ` TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area %
Limits
RT Diff
RT Diff
Limit
Q
Blank (B219146-BLK1 Lab File ID: B121208.D Analyzed: 12/12/18 12:27
Bromochloromethane (1)
74543
5.073
75997
5.078
98
60 - 140
-0.0050
+/-0.50
1,4-Difluorobenzene (1)
188897
6.293
193987
6.298
97
60 - 140
-0.0050
+/-0.50
Chlorobenzene-d5 (1)
171195
9.892
175616
9.891
97
60-140
0.0010
+/-0.50
SSV-1 (18L0293-01 ) Lab File ID: B121211.13 Analyzed: 12/12/18 14:38
Bromochloromethane (1)
76330
5.073
75997
5.078
100
60 - 140
-0.0050
+/-0.50
1,4-Difluorobenzene (1)
191322
6.292
193987
6.298
99
60 - 140
-0.0060
+/-0.50
Chlorobenzene-d5 (1)
167152
9.892
175616
9.891
95
60-140
0.0010
+/-0.50
Duplicate (B219146-DUP1) Lab File ID: B121212.D Analyzed: 12/12/18 15:06
Bromochloromethane (1)
74377
5.071
75997
5.078
98
60 - 140
-0.0070
+/-0.50
1,4-Difluorobenzene (1)
185146
6.291
193987
6.298
95
60 - 140
-0.0070
+/-0.50
Chlorobenzene-d5(1)
163995
9.89
175616
9.891
93
60-140
-0.0010
+/-0.50
SSV-2 (181,0293-02 ) Lab File ID: B121213.D Analyzed: 12/12/18 15:35
Bromochloromethane (1)
77026
5.072
75997
5.078
101
60 - 140
-0.0060
+/-0.50
1,4-Difluorobenzene (1)
198984
6.292
193987
6.298
103
60 - 140
-0.0060
+/-0.50
Chlorobenzene-d5(1)
168593
9.891
175616
9.891
96
60-140
0.0000
+/-0.50
SSV-3 (181,0293-03 ) Lab File ID: B121214.D Analyzed: 12/12/18 16:03
Bromochloromethane (1)
74724
5.075
75997
5.078
98
60 - 140
-0.0030
+/-0.50
1,4-Difluorobenzene (1)
188275
6.295
193987
6.298
97
60 - 140
-0.0030
+/-0.50
Chlorobenzene-d5(1)
167194
9.888
175616
9.891
95
60-140
-0.0030
+/-0.50
DUP-SSV (181,0293-04) Lab File ID: 13121215.13 Analyzed: 12/12/18 16:31
Bromochloromethane (1)
75983
5.075
75997
5.078
100
60 - 140
-0.0030
+/-0.50
1,4-Difluorobenzene (1)
194422
6.295
193987
6.298
100
60 - 140
-0.0030
+/-0.50
Chlorobenzene-d5(1)
171575
9.888
175616
9.891
98
60-140
-0.0030
+/-0.50
Page 25 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S030210-CCV1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
Acetone
A
5.00
4.77
0.9623388
0.8230529
-4.6
30
Benzene
A
5.00
4.78
0.6955533
0.6649551
-4.4
30
Benzyl chloride
A
5.00
5.46
0.8474379
0.9255686
9.2
30
Bromodichloromethane
A
5.00
5.13
0.4967154
0.5100084
2.7
30
Bromofonn
A
5.00
6.00
0.4996463
0.6000539
20.1
30
Bromomethane
A
5.00
4.59
0.4888406
0.4483693
-8.3
30
1,3-Butadiene
A
5.00
5.20
0.3561068
0.3699777
3.9
30
2-Butanone (MEK)
A
5.00
4.73
1.336089
1.263162
-5.5
30
Carbon Disulfide
L
5.00
4.55
1.040696
0.9103202
-9.0
30
Carbon Tetrachloride
A
5.00
5.58
0.3685789
0.4115296
11.7
30
Chlorobenzene
A
5.00
5.00
0.6427787
0.6425515
-0.04
30
Chloroethane
A
5.00
4.53
0.2552372
0.2314023
-9.3
30
Chloroform
A
5.00
5.84
0.9890879
1.154768
16.8
30
Chloromethane
A
5.00
5.27
0.5680116
0.5991561
5.5
30
Cyclohexane
A
5.00
5.22
0.280792
0.2931247
4.4
30
Dibromochloromethane
A
5.00
5.53
0.5163955
0.5713566
10.6
30
1,2-Dibromoethane(EDB)
A
5.00
5.56
0.416186
0.4629057
11.2
30
1,2-Dichlorobenzene
A
5.00
5.99
0.5675353
0.6797896
19.8
30
1,3-Dichlorobenzene
A
5.00
5.89
0.6177324
0.7274836
17.8
30
1,4-Dichlorobenzene
A
5.00
6.05
0.6137396
0.7424616
21.0
30
Dichlorodifluoromethane (Freon 12)
A
5.00
5.42
1.322997
1.434142
8.4
30
1,1-Dichloroethane
A
5.00
5.56
0.8504494
0.9453264
11.2
30
1,2-Dichloroethane
A
5.00
5.51
0.6491051
0.7148771
10.1
30
1,1-Dichloroethylene
A
5.00
4.72
0.722363
0.6824125
-5.5
30
cis-1,2-Dichloroethylene
A
5.00
5.53
0.6369715
0.7043137
10.6
30
trans-1,2-Dichloroethylene
L
5.00
5.09
0.5990668
0.6460164
1.8
30
1,2-Dichloropropane
A
5.00
4.95
0.243713
0.2413523
-1.0
30
cis- 1,3 -Dichloropropene
A
5.00
5.22
0.3954339
0.4130841
4.5
30
trans- l,3-Dichloropropene
A
5.00
5.40
0.3529045
0.3814149
8.1
30
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1
A
5.00
5.39
1.469019
1.582308
7.7
30
1,4-Dioxane
A
5.00
5.10
0.1530093
0.1559133
1.9
30
Ethanol
A
5.00
3.79
0.181169
0.1373641
-24.2
30
Ethyl Acetate
A
5.00
5.47
0.1810735
0.1981633
9.4
30
Ethylbenzene
A
5.00
4.93
1.068258
1.052378
-1.5
30
4-Ethyltoluene
A
5.00
5.33
1.04842
1.117675
6.6
30
Heptane
A
5.00
4.85
0.2034395
0.197328
-3.0
30
Hexachlorobutadiene
A
5.00
6.61
0.3567604
0.4716893
32.2
30
Hexane
A
5.00
5.49
0.3085741
0.3388632
9.8
30
Page 26 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S030210-CCV1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
2-Hexanone (MBK)
A
5.00
4.41
0.729345
0.6426324
-11.9
30
Isopropanol
A
5.00
4.66
1.083093
1.009759
-6.8
30
Methyl tert-Butyl Ether (MTBE)
A
5.00
5.39
1.315446
1.417404
7.8
30
Methylene Chloride
A
5.00
4.58
0.691259
0.6329312
-8.4
30
4-Methyl-2-pentanone (MI13K)
A
5.00
4.49
0.6784377
0.6095422
-10.2
30
Naphthalene
A
5.00
5.59
0.9853207
1.10089
11.7
30
Propene
A
5.00
4.75
0.4844323
0.4605808
-4.9
30
Styrene
A
5.00
5.59
0.5493248
0.6143936
11.8
30
1,1,2,2-Tetrachloroethane
A
5.00
5.04
0.7259972
0.7322395
0.9
30
Tetrachloroethylene
A
5.00
5.77
0.3710352
0.4279421
15.3
30
Tetrahydrofuran
A
5.00
5.71
0.6749896
0.7710896
14.2
30
Toluene
A
5.00
5.02
0.7672716
0.7697204
0.3
30
1,2,4-Trichlorobenzene
A
5.00
6.51
0.397651
0.5179808
30.3
30
1, 1, 1 -Trichloroethane
A
5.00
5.37
0.375154
0.4032418
7.5
30
1,1,2-Trichloroethane
A
5.00
5.22
0.2748379
0.2868471
4.4
30
Trichloroethylene
A
5.00
5.43
0.2710247
0.2943168
8.6
30
Trichlorofluoromethane (Freon 11)
A
5.00
5.40
1.077722
1.163663
8.0
30
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 11
A
5.00
5.33
0.8187388
0.8723554
6.5
30
1,2,4-Trimethylbenzene
A
5.00
5.53
0.7969344
0.8819923
10.7
30
1,3,5-Trimethylbenzene
A
5.00
5.53
0.7967432
0.8806887
10.5
30
Vinyl Acetate
A
5.00
4.81
1.677035
1.613403
-3.8
30
Vinyl Chloride
A
5.00
5.22
0.5200947
0.5427252
4.4
30
m&p-Xylene
A
10.0
10.3
0.7722412
0.7985256
3.4
30
o-Xylene
A
5.00
5.30
0.7523287
0.7970152
5.9
30
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
* Values outside of QC limits
Page 27 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S030250-CCV 1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
Acetone
A
5.00
5.14
0.9623388
0.8872771
2.9
30
Benzene
A
5.00
5.12
0.6955533
0.712856
2.5
30
Benzyl chloride
A
5.00
5.66
0.8474379
0.9592292
13.2
30
Bromodichloromethane
A
5.00
5.50
0.4967154
0.5463789
10.0
30
Bromofonn
A
5.00
6.35
0.4996463
0.634539
27.0
30
Bromomethane
A
5.00
4.96
0.4888406
0.4849455
-0.8
30
1,3-Butadiene
A
5.00
5.49
0.3561068
0.3907102
9.7
30
2-Butanone (MEK)
A
5.00
5.04
1.336089
1.346243
0.8
30
Carbon Disulfide
L
5.00
6.00
1.040696
1.195016
20.1
30
Carbon Tetrachloride
A
5.00
5.99
0.3685789
0.4415306
19.8
30
Chlorobenzene
A
5.00
5.28
0.6427787
0.6792365
5.7
30
Chloroethane
A
5.00
4.86
0.2552372
0.248094
-2.8
30
Chloroform
A
5.00
6.48
0.9890879
1.281335
29.5
30
Chloromethane
A
5.00
5.63
0.5680116
0.6391621
12.5
30
Cyclohexane
A
5.00
5.59
0.280792
0.3139509
11.8
30
Dibromochloromethane
A
5.00
5.92
0.5163955
0.6118076
18.5
30
1,2-Dibromoethane(EDB)
A
5.00
5.86
0.416186
0.4879829
17.3
30
1,2-Dichlorobenzene
A
5.00
6.30
0.5675353
0.7144953
25.9
30
1,3-Dichlorobenzene
A
5.00
6.20
0.6177324
0.7656614
23.9
30
1,4-Dichlorobenzene
A
5.00
6.30
0.6137396
0.7734785
26.0
30
Dichlorodifluoromethane (Freon 12)
A
5.00
5.93
1.322997
1.568315
18.5
30
1,1-Dichloroethane
A
5.00
6.11
0.8504494
1.039388
22.2
30
1,2-Dichloroethane
A
5.00
6.08
0.6491051
0.7889154
21.5
30
1,1-Dichloroethylene
A
5.00
5.46
0.722363
0.7895259
9.3
30
cis-1,2-Dichloroethylene
A
5.00
6.08
0.6369715
0.7743464
21.6
30
trans-1,2-Dichloroethylene
L
5.00
5.67
0.5990668
0.72026
13.4
30
1,2-Dichloropropane
A
5.00
5.30
0.243713
0.2581039
5.9
30
cis- 1,3 -Dichloropropene
A
5.00
5.58
0.3954339
0.44111
11.6
30
trans- l,3-Dichloropropene
A
5.00
5.76
0.3529045
0.4061715
15.1
30
1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1
A
5.00
5.83
1.469019
1.713752
16.7
30
1,4-Dioxane
A
5.00
5.49
0.1530093
0.1680195
9.8
30
Ethanol
A
5.00
4.17
0.181169
0.1509744
-16.7
30
Ethyl Acetate
A
5.00
5.84
0.1810735
0.2116926
16.9
30
Ethylbenzene
A
5.00
5.17
1.068258
1.103799
3.3
30
4-Ethyltoluene
A
5.00
5.57
1.04842
1.16854
11.5
30
Heptane
A
5.00
5.13
0.2034395
0.2085748
2.5
30
Hexachlorobutadiene
A
5.00
7.01
0.3567604
0.5001367
40.2
30
Hexane
A
5.00
5.89
0.3085741
0.3635301
17.8
30
Page 28 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S030250-CCV 1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
2-Hexanone (MBK)
A
5.00
4.55
0.729345
0.6640306
-9.0
30
Isopropanol
A
5.00
5.04
1.083093
1.090969
0.7
30
Methyl tert-Butyl Ether (MTBE)
A
5.00
5.96
1.315446
1.567262
19.1
30
Methylene Chloride
A
5.00
4.85
0.691259
0.6705317
-3.0
30
4-Methyl-2-pentanone (MI13K)
A
5.00
4.67
0.6784377
0.6342363
-6.5
30
Naphthalene
A
5.00
5.76
0.9853207
1.13545
15.2
30
Propene
A
5.00
4.96
0.4844323
0.4803348
-0.8
30
Styrene
A
5.00
5.74
0.5493248
0.6310131
14.9
30
1,1,2,2-Tetrachloroethane
A
5.00
5.27
0.7259972
0.7655066
5.4
30
Tetrachloroethylene
A
5.00
6.15
0.3710352
0.456496
23.0
30
Tetrahydrofuran
A
5.00
6.10
0.6749896
0.8227693
21.9
30
Toluene
A
5.00
5.37
0.7672716
0.8245353
7.5
30
1,2,4-Trichlorobenzene
A
5.00
6.74
0.397651
0.5358145
34.7
30
1, 1, 1 -Trichloroethane
A
5.00
5.79
0.375154
0.4341652
15.7
30
1,1,2-Trichloroethane
A
5.00
5.52
0.2748379
0.303617
10.5
30
Trichloroethylene
A
5.00
5.94
0.2710247
0.3218855
18.8
30
Trichlorofluoromethane (Freon 11)
A
5.00
5.98
1.077722
1.288409
19.5
30
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 11
A
5.00
6.38
0.8187388
1.045052
27.6
30
1,2,4-Trimethylbenzene
A
5.00
5.77
0.7969344
0.9200164
15.4
30
1,3,5-Trimethylbenzene
A
5.00
5.77
0.7967432
0.9200346
15.5
30
Vinyl Acetate
A
5.00
5.19
1.677035
1.741227
3.8
30
Vinyl Chloride
A
5.00
5.65
0.5200947
0.5876021
13.0
30
m&p-Xylene
A
10.0
10.8
0.7722412
0.8365297
8.3
30
o-Xylene
A
5.00
5.54
0.7523287
0.8330904
10.7
30
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
* Values outside of QC limits
Page 29 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
EPA TO-15 in Air
Acetone
Benzene
Benzyl chloride
Bromodichloromethane
Bromoform
Bromomethane
1,3-Butadiene
2-Butanone (MEK)
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Cyclohexane
Dibromochloromethane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane (Freon 12)
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethylene
cis-1,2-Dichloroethylene
trans- l,2-Dichloro ethylene
1,2-Dichloropropane
cis- 1,3 -Dichloropropene
trans- 1, 3 -Dichloropropene
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
1,4-Dioxane
Ethanol
Ethyl Acetate
Ethylbenzene
4-Ethyltoluene
Heptane
Hexachlorobutadiene
Hexane
2-Hexanone (MBK)
Isopropanol
Methyl tart -Butyl Ether (MTBE)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Naphthalene
Propene
Styrene
1,1,2,2-Tetrachloroethane
Certifications
AIHA,NY,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,NJ,NY,VA,ME
AIHA,NJ,NY,VA,ME
AIHA,FL,NJ,NY,ME
AIHA,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,NJ,NY,VA,ME
AIHA,NY,ME
AIHA,NJ,NY,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,NJ,NY,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,NY,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NY,VA,ME
AIHA,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,NY,ME
AIHA,NJ,NY,VA,ME
AIHA,NJ,NY,VA,ME
AIHA
AIHA
AIHA,FL,NJ,NY,VA,ME
AIHA,NJ
AIHA,NJ,NY,VA,ME
AIHA,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA
AIHA,NY,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,ME
NY,ME
AIHA
AIHA,FL,NJ,NY,VA,ME
AIHA,FL,NJ,NY,VA,ME
Page 30 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
EPA TO-15 in Air
Tetrachloroethylene
AIHA,FL,NJ,NY,VA,ME
Tetrahydrofuran
AIHA
Toluene
AIHA,FL,NJ,NY,VA,ME
1,2,4-Trichlorobenzene
AIHA,NJ,NY,VA,ME
1, 1, 1 -Trichloroethane
AIHA,FL,NJ,NY,VA,ME
1,1,2-Trichloroethane
AIHA,FL,NJ,NY,VA,ME
Trichloroethylene
AIHA,FL,NJ,NY,VA,ME
Trichlorofluoromethane (Freon 11)
AIHA,NY,ME
1,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
AIHA,NJ,NY,VA,ME
1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME
1,3,5-Trimethylbenzene
AIHA,NJ,NY,ME
Vinyl Acetate
AIHA,FLNJ,NY,VA,ME
Vinyl Chloride
AIHA,FLNJ,NY,VA,ME
m&p-Xylene
AIHA,FL,NJ,NY,VA,ME
o-Xylene
AIHA,FL,NJ,NY,VA,ME
The CON -TEST Environmental
Laboratory operates under the
following certifications and accreditation:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA
Massachusetts DEP
M-MA100
06/30/2019
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2019
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI
Rhode Island Department of Health
LA000112
12/30/2018
NC
North Carolina Div. of Water Quality
652
12/31/2019
NJ
New Jersey DEP
MA007 NELAP
06/30/2019
FL
Florida Department of Health
E871027 NELAP
06/30/2019
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME
State of Maine
2011028
06/9/2019
VA
Commonwealth of Virginia
460217
12/14/2018
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW
North Carolina Department of Health
25703
07/31/2019
Page 31 of 34

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Page 32 of 34

12/10/2018 Track your package or shipment with FedEx TrackingN&C
Ai
M4239430766
Delivered
Monday 12/10/2018 at 1209 pm
FROM
EAST LONGMEADOb°J. MA US
Shipment Facts
TRACKING NUMBER
784239430766
DIMENSIONS
22x19x14 in
PACKAGING
P@ckage
ACTUAL DELIVERY
Fvlori 12/10/2018 12.09 p it
Travel History
DELIVERED
Signed for by: HBECKY
GET STATUS UPDATES
OBTAIN PROF OF DELIVERY
SERVICE
I=edEx Ground
TOTAL PIECES
1
ISST�ANDARD TRANSIT
C'
12110/2018
TO
East Longmeadow, MA US
WEIGHT
28.E ibs / 12 88 kgs
TERMS
Third Party
SHIP DATE
C)
Thu12/06/2018
Monday, 1211C;2018
12:C9 pm
East Longmeadow, MA
Delivered
2:09 am
SOUTH WINDSOR, CT
On FedEx vehicle for delivery
Saturday, 12/6Bl2018
4 51 am
SOUTH WINDSOR, CT
On FedEx vehicle for delivery
4.42 am
SOUTH WINDSOR, CT
At local FedEx facility
3.15 am
WILLWGTON, CT
Departed FedEx location
https://www.fedex.com/a pps/fed
extrack/?action=track&tracking n u mb er=784239430766&cntry_cOde=us &locale=en—US
Local Scan Time V
Page 33 of 34

Received By '_ Date
How were the samples In Cooler
received? In Box
Were samples within Temperature By Gun
Compliance? 2-60C By Blan
Was Custody Seal Intact?.
Was COC Relinquished ? A
Are there any loose caps/valves on any samples?
Is COC in ink/ Legible? —�
Did COC Include all Client �C
Pertinent Information? Project
Are Sample Labels filled out and legible?
Are there Rushes? V7
Samples are received within holding time?
Proper Media Used?
Are there Trip Blanks?
----� Time
On Ice No Ice
Ambient "Melted Ice
# Actual Temp -
k # Actual Temp -
Were Samples Tampered with?
Does Chain Agree With Samples?
E
Analysis _�l Sampler Name T
ID's 7 Collection Dates/Times g
Who was notified?
Individually Certified Cans? F
Is there enough Volume? 1
Summa Cans Q4 Nut/Ferrule IC Train
Tedlar Baqs Tubing
TO-17 Tubes T-Connector
Radiello Syrin e
Pufs/TO-11 s Tedlar
nts:
�Gv �� sou pCe -f�J - ��s�/ C►�ii��
Page 34 of 34

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
December 19, 2018
Bo Cappleman
Hart & Hickman - Charlotte, NC
2923 South Tryon Street, Suite 100
Charlotte, NC 28203
Project Location: Charlotte, NC
Client Job Number:
Project Number: COP-008
Laboratory Work Order Number: 18L0001
Enclosed are results of analyses for samples received by the laboratory on November 30, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
�11 �. A��
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Hart & Hickman - Charlotte, NC REPORT DATE: 12/19/2018
2923 South Tryon Street, Suite 100
Charlotte, NC 28203 PURCHASE ORDER NUMBER: COP-008
ATTN: Bo Cappleman
PROJECT NUMBER: COP-008
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18L0001
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: Charlotte, NC
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
IAQ-1 18L0001-01 Indoor air EPA TO-15
IAQ-2 18L0001-02 Indoor air EPA TO-15
BKG-IAQ-1 18L0001-04 Indoor air EPA TO-15
Page 2 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 3 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Sample Description/Location:
Date Received: 11/30/2018
Sub Description/Location:
Field Sample #: IAQ-1
Canister ID: 2156
Sample ID: 18L0001-01
Canister Size: 6 liter
Sample Matrix: Indoor air
Flow Controller ID: 3125
Sampled: 11/29/2018 17:33
Sample Type: 8 hr
Work Order: 18L0001
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -9.5
Receipt Vacuum(in Hg): -9.7
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual Results
ug/m3
ILL
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
14
1.6
0.56
33
3.8
1.3
0.8
12/14/18 2:25
BRF
Benzene
4.0
0.040
0.016
13
0.13
0.053
0.8
12/14/18 2:25
BRF
2-Butanone (MEK)
1.9
1.6
0.062
5.6
4.7
0.18
0.8
12/14/18 2:25
BRF
Chloroform
ND
0.040
0.015
ND
0.20
0.073
0.8
12/14/18 2:25
BRF
1,3-Dichlorobenzene
ND
0.040
0.021
ND
0.24
0.12
0.8
12/14/18 2:25
BRF
Dichlorodifluoromethane (Freon 12)
0.53
0.040
0.017
2.6
0.20
0.086
0.8
12/14/18 2:25
BRF
Ethanol
57
40
18
110
75
34
20
12/14/18 1:48
BRF
Tetrachloroethylene
0.093
0.040
0.022
0.63
0.27
0.15
0.8
12/14/18 2:25
BRF
Tetrahydrofuran
0.89
0.040
0.027
2.6
0.12
0.078
0.8
12/14/18 2:25
BRF
Toluene
13
0.040
0.021
47
0.15
0.078
0.8
12/14/18 2:25
BRF
Trichloroethylene
ND
0.040
0.016
ND
0.21
0.087
0.8
12/14/18 2:25
BRF
Trichlorofluoromethane (Freon 11)
0.34
0.16
0.023
1.9
0.90
0.13
0.8
12/14/18 2:25
BRF
Surrogates
4-Bromofluorobenzene (1)
4-Bromofluorobenzene (1)
% Recovery
103
106
% REC Limits
70-130
70-130
12/14/18 1:48
12/14/18 2:25
Page 4 of 18

,con -testy
ANALYTICAL LABORATORY
Project Location: Charlotte, NC
Date Received: 11/30/2018
Field Sample #: IAQ-2
Sample ID: 18L0001-02
Sample Matrix: Indoor air
Sampled: 11 /29/2018 16:45
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Sample Description/Location:
Sub Description/Location:
Canister ID: 2003
Canister Size: 6 liter
Flow Controller ID: 3209
Sample Type: 8 hr
Work Order: 18L0001
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): 46
Receipt Vacuum(in Hg): -5.3
Flow Controller Type: Fixed -Orifice
Flow Controller Calibration
RPD Pre and Post -Sampling:
EPA TO-15
ppbv ug/m3 Date/Time
Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst
Acetone
12
1.4
0.49
28
3.3
1.2
0.702
12/14/18 3:01
BRF
Benzene
3.2
0.035
0.014
10
0.11
0.046
0.702
12/14/18 3:01
BRF
2-Butanone (MEK)
1.5
1.4
0.055
4.6
4.1
0.16
0.702
12/14/18 3:01
BRF
Chloroform
ND
0.035
0.013
ND
0.17
0.064
0.702
12/14/18 3:01
BRF
1,3-Dichlorobenzene
ND
0.035
0.018
ND
0.21
0.11
0.702
12/14/18 3:01
BRF
Dichlorodifluoromethane (Freon 12)
0.56
0.035
0.015
2.8
0.17
0.075
0.702
12/14/18 3:01
BRF
Ethanol
40
1.4
0.63
75
2.6
1.2
0.702
12/14/18 3:01
BRF
Ethanol
34
20
8.9
65
38
17
10
12/19/18 7:18
BRF
Tetrachloroethylene
0.064
0.035
0.020
0.43
0.24
0.13
0.702
12/14/18 3:01
BRF
Tetrahydrofuran
1.1
0.035
0.023
3.4
0.10
0.069
0.702
12/14/18 3:01
BRF
Toluene
9.7
0.035
0.018
37
0.13
0.068
0.702
12/14/18 3:01
BRF
Trichloroethylene
ND
0.035
0.014
ND
0.19
0.076
0.702
12/14/18 3:01
BRF
Trichlorofluoromethane (Freon 11)
0.36
0.14
0.020
2.0
0.79
0.11
0.702
12/14/18 3:01
BRF
Surrogates
4-Bromofluorobenzene (1)
4-Bromofluorobenzene (1)
% Recovery
106
114
% REC Limits
70-130
70-130
12/14/18 3:01
12/19/18 7:18
Page 5 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Sample Description/Location:
Work Order: 18L0001
Date Received: 11/30/2018
Sub Description/Location:
Initial Vacuum(in Hg): -29
Field Sample #: BKG-IAQ-1
Canister ID: 1505
Final Vacuum(in Hg): -5.0
Sample ID: 18L0001-04
Canister Size: 6 liter
Receipt Vacuum(in Hg): -3.9
Sample Matrix: Indoor air
Flow Controller ID: 3586
Flow Controller Type: Fixed -Orifice
Sampled: 11/29/2018 17:38
Sample Type: 8 hr
Flow Controller Calibration
RPD Pre and Post -Sampling:
Analyte
Results
ppbv
RL
EPA TO-15
MDL
Flag/Qual Results
ug/m3
RI
MDL
Dilution
Date/Time
Analyzed
Analyst
Acetone
5.5
1.4
0.49
13
3.3
1.2
0.702
12/14/18 4:12
BRF
Benzene
0.41
0.035
0.014
1.3
0.11
0.046
0.702
12/14/18 4:12
BRF
2-Butanone (MEK)
0.80
1.4
0.055
J 2.4
4.1
0.16
0.702
12/14/18 4:12
BRF
Chloroform
ND
0.035
0.013
ND
0.17
0.064
0.702
12/14/18 4:12
BRF
1,3-Dichlorobenzene
ND
0.035
0.018
ND
0.21
0.11
0.702
12/14/18 4:12
BRF
Dichlorodifluoromethane (Freon 12)
0.76
0.035
0.015
3.8
0.17
0.075
0.702
12/14/18 4:12
BRF
Ethanol
8.0
1.4
0.63
15
2.6
1.2
0.702
12/14/18 4:12
BRF
Tetrachloroethylene
0.055
0.035
0.020
0.37
0.24
0.13
0.702
12/14/18 4:12
BRF
Tetrahydrofuran
ND
0.035
0.023
ND
0.10
0.069
0.702
12/14/18 4:12
BRF
Toluene
0.83
0.035
0.018
3.1
0.13
0.068
0.702
12/14/18 4:12
BRF
Trichloroethylene
ND
0.035
0.014
ND
0.19
0.076
0.702
12/14/18 4:12
BRF
Trichlorofluoromethane (Freon 11)
0.39
0.14
0.020
2.2
0.79
0.11
0.702
12/14/18 4:12
BRF
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene(1) 109 70-130 12/14/18 4:12
Page 6 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction
Data
Prep Method: TO-15 Prep -EPA TO-15
Pre-Dil
Pre-Dil
Default
Actual
Pressure
Pre
Initial
Final
Injection
Injection
Lab Number [Field ID]
Batch
Dilution
Dilution
mL
mL
mL
mL
Date
18L0001-01 [IAQ-11
B219368
2
1
N/A
1000
400
1000
12/13/18
18L0001-01RE1 [IAQ-1]
B219368
2
1
N/A
1000
400
40
12/13/18
18L0001-02 [IAQ-2]
B219368
1.5
1
N/A
1000
400
855
12/13/18
18L0001-04 [BKG-IAQ-1]
B219368
1.5
1
N/A
1000
400
855
12/13/18
Prep Method: TO-15 Prep -EPA TO-15
Pre-Dil
Pre-Dil
Default
Actual
Pressure
Pre
Initial
Final
Injection
Injection
Lab Number [Field ID]
Batch
Dilution
Dilution
mL
mL
mL
mL
Date
18L0001-02RE1 [IAQ-2]
B219577
1.5
1
N/A
1000
400
60
12/18/18
Page 7 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua
Batch B219368 - TO-15 Prep
Blank (B219368-BLK1)
Prepared & Analyzed: 12/13/18
Acetone
ND
1.4
Benzene
ND
0.035
2-Butanone (MEK)
ND
1.4
Chloroform
ND
0.035
1,3-Dichlorobenzene
ND
0.035
Dichlorodifluoromethane (Freon 12)
ND
0.035
Ethanol
ND
1.4
Tetrachloroethylene
ND
0.035
Tetrahydrofuran
ND
0.035
Toluene
ND
0.035
Trichloroethylene
ND
0.035
Trichlorofluoromethane (Freon 11)
ND
0.14
Surrogate: 4-Bromofluorobenzene (1)
LCS (B219368-BS1)
8.30
8.00
Prepared & Analyzed:
104
12/13/18
70-130
Acetone
5.62
5.00
112
70-130
Benzene
4.86
5.00
97.3
70-130
2-Butanone (MEK)
5.13
5.00
103
70-130
Chloroform
6.49
5.00
130
70-130
1,3-Dichlorobenzene
5.89
5.00
118
70-130
Dichlorodifluoromethane(Freon 12)
6.08
5.00
122
70-130
Ethanol
3.76
5.00
75.2
70-130
Tetrachloroethylene
6.22
5.00
124
70-130
Tetrahydroforan
5.86
5.00
117
70-130
Toluene
5.37
5.00
107
70-130
Trichloroethylene
5.69
5.00
114
70-130
Trichlorofluoromethane (Freon 11)
6.20
5.00
124
70-130
Surrogate: 4-Bromofluorobenzene (1) 8.55 8.00 107 70-130
Page 8 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Air Toxics by EPA Compendium Methods - Quality Control
ppbv ug/m3 Spike Level Source %REC RPD
Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual
Batch B219577 - TO-15 Prep
Blank (B219577-BLKI)
Prepared: 12/18/18 Analyzed: 12/19/18
Acetone
ND
1.4
Benzene
ND
0.035
2-Butanone (MEK)
ND
1.4
Chloroform
ND
0.035
1,3-Dichlorobenzene
ND
0.035
Dichlorodifluoromethane (Freon 12)
ND
0.035
Ethanol
ND
1.4
Tetrachloroethylene
ND
0.035
Tetrahydrofuran
ND
0.035
Toluene
ND
0.035
Trichloroethylene
ND
0.035
Trichlorofluoromethane (Freon 11)
ND
0.14
Surrogate: 4-Bromofluorobenzene (1)
8.94
8.00 112
70-130
LCS (B219577-BSI)
Prepared: 12/18/18 Analyzed: 12/19/18
Acetone
5.28
5.00 106
70-130
Benzene
4.50
5.00 90.1
70-130
2-Butanone (MEK)
4.82
5.00 96.4
70-130
Chloroform
7.00
5.00 140 *
70-130
1,3-Dichlorobenzene
5.85
5.00 117
70-130
Dichlorodifluoromethane(Freon 12)
6.30
5.00 126
70-130
Ethanol
4.03
5.00 80.6
70-130
Tetrachloroethylene
6.41
5.00 128
70-130
Tetrahydrofuran
5.56
5.00 ill
70-130
Toluene
4.99
5.00 99.7
70-130
Trichloroethylene
5.79
5.00 116
70-130
Trichlorofluoromethane (Freon 11)
6.82
5.00 136 *
70-130
Surrogate: 4-Bromofluorobenzene (1) 9.22 8.00 115 70-130
Page 9 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
t
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
RL
Reporting Limit
MDL
Method Detection Limit
RPD
Relative Percent Difference
LCS
Laboratory Control Sample
LCS Dup
Duplicate Laboratory Control Sample
MS
Matrix Spike Sample
MS Dup
Duplicate Matrix Spike Sample
REC
Recovery
QC
Quality Control
ppbv
Parts per billion volume
EPA
United States Environmental Protection Agency
% REC Percent Recovery
ND Not Detected
N/A Not Applicable
DL Detection Limit
NC Not Calculated
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation -Reduction Potential
wet Not dry weight corrected
% wt Percent weight
Kg Kilogram
g Gram
mg Milligram
µg Microgram
ng Nanogram
L Liter
mL Milliliter
µL Microliter
m3 Cubic Meter
EPH Extractable Petroleum Hydrocarbons
VPH Volatile Petroleum Hydrocarbons
APH Air Petroleum Hydrocarbons
FID Flame Ionization Detector
PID Photo Ionization Detector
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
ANALYST
RAP Raisa A. Petraitis
PEB Paula E. Blakeborough
KKM Kerry K. McGee
BRF Brittany R. Fisk
Page 10 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] ` TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area o/
Limits
RT Diff
RT Diff
Limit
Q
Initial Cal Check (S029991-ICV1) Lab File ID: B120417.D Analyzed: 12/04/18 22:13
Bromochloromethane (1)
80510
5.072
82524
5.077
98
60 - 140
-0.0050
+/-0.50
1,4-Difluorobenzene (1)
180031
6.292
183364
6.291
98
60 - 140
0.0010
+/-0.50
Chlorobenzene-d5(1)
157522
9.891
164139
9.89
96
60-140
0.0010
+/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area o/
Limits
RT Diff
RT Diff
Limit
Q
Calibration Check (S030352-CCV1) Lab File ID: 13121304.1) Analyzed: 12/13/18 11:52
Bromochloromethane (1)
71727
5.078
82524
5.077
87
60 - 140
0.0010
+/-0.50
1,4-Difluorobenzene (1)
191232
6.292
183364
6.291
104
60 - 140
0.0010
+/-0.50
Chlorobenzene-d5(1)
167360
9.891
164139
9.89
102
60-140
0.0010
+/-0.50
LCS (B219368-BS1 ) Lab File ID: B121305.D Analyzed: 12/13/18 12:21
Bromochloromethane (1)
69733
5.073
71727
5.078
97
60 - 140
-0.0050
+/-0.50
1,4-Difluorobenzene (1)
187548
6.293
191232
6.292
98
60 - 140
0.0010
+/-0.50
Chlorobenzene-d5(1)
164187
9.892
167360
9.891
98
60-140
0.0010
+/-0.50
Blank (B219368-BLK1) Lab File ID: B121309.D Analyzed: 12/13/18 14:20
Bromochloromethane (1)
70372
5.078
71727
5.078
98
60 - 140
0.0000
+/-0.50
1,4-Difluorobenzene (1)
185962
6.298
191232
6.292
97
60 - 140
0.0060
+/-0.50
Chlorobenzene-d5(1)
166934
9.891
167360
9.891
100
60-140
0.0000
+/-0.50
IAQ-1 (18L0001-01RE1) Lab File ID: B121330.D Analyzed: 12/14/18 01:48
Bromochloromethane (1)
61172
5.072
71727
5.078
85
60 - 140
-0.0060
+/-0.50
1,4-Difluorobenzene (1)
165162
6.292
191232
6.292
86
60 - 140
0.0000
+/-0.50
Chlorobenzene-d5(1)
147108
9.891
167360
9.891
88
60-140
0.0000
+/-0.50
IAQ-1 (18L0001-01 ) Lab File ID: B121331.13 Analyzed: 12/14/18 02:25
Bromochloromethane (1)
62370
5.073
71727
5.078
87
60 - 140
-0.0050
+/-0.50
1,4-Difluorobenzene (1)
166920
6.292
191232
6.292
87
60 - 140
0.0000
+/-0.50
Chlorobenzene-d5(1)
149841
9.892
167360
9.891
90
60-140
0.0010
+/-0.50
IAQ-2 (18L0001-02) Lab File ID: B121332.D Analyzed: 12/14/18 03:01
Bromochloromethane (1)
61529
5.073
71727
5.078
86
60 - 140
-0.0050
+/-0.50
1,4-Difluorobenzene (1)
167576
6.293
191232
6.292
88
60 - 140
0.0010
+/-0.50
Chlorobenzene-d5(1)
151419
9.892
167360
9.891
90
60-140
0.0010
+/-0.50
BKG-IAQ-1 (181,0001-04) Lab File ID: B121334.1) Analyzed: 12/14/18 04:12
Bromochloromethane (1)
61509
5.071
71727
5.078
86
60 - 140
-0.0070
+/-0.50
1,4-Difluorobenzene (1)
177693
6.291
191232
6.292
93
60 - 140
-0.0010
+/-0.50
Chlorobenzene-d5(1)
158544
9.89
167360
9.891
95
60-140
-0.0010
+/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Page 11 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] ` TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Internal Standard
Response
RT
Reference
Response
Reference
RT
Area %
Area o/
Limits
RT Diff
RT Diff
Limit
Q
Calibration Check (S030467-CCV1) Lab File ID: B121804.D Analyzed: 12/18/18 10:41
Bromochloromethane (1)
71821
5.086
82524
5.077
87
60 - 140
0.0090
+/-0.50
1,4-Difluorobenzene (1)
203503
6.3
183364
6.291
111
60 - 140
0.0090
+/-0.50
Chlorobenzene-d5(1)
174589
9.893
164139
9.89
106
60-140
0.0030
+/-0.50
LCS (B219577-BS1 ) Lab File ID: B121829.D Analyzed: 12/19/18 01:29
Bromochloromethane (1)
55437
5.072
71821
5.086
77
60 - 140
-0.0140
+/-0.50
1,4-Difluorobenzene (1)
163226
6.292
203503
6.3
80
60 - 140
-0.0080
+/-0.50
Chlorobenzene-d5 (1)
147713
9.891
174589
9.893
85
60-140
-0.0020
+/-0.50
Blank (B219577-BLK1) Lab File ID: B121831.13 Analyzed: 12/19/18 02:35
Bromochloromethane (1)
57249
5.074
71821
5.086
80
60 - 140
-0.0120
+/-0.50
1,4-Difluorobenzene (1)
165069
6.294
203503
6.3
81
60 - 140
-0.0060
+/-0.50
Chlorobenzene-d5(1)
143062
9.887
174589
9.893
82
60-140
-0.0060
+/-0.50
IAQ-2 (18L0001-02RE1) Lab File ID: B121841.D Analyzed: 12/19/18 07:18
Bromochloromethane (1)
85302
5.072
71821
5.086
119
60 - 140
-0.0140
+/-0.50
1,4-Difluorobenzene (1)
267968
6.292
203503
6.3
132
60 - 140
-0.0080
+/-0.50
Chlorobenzene-d5(1)
236816
9.891
174589
9.893
136
60-140
-0.0020
+/-0.50
Page 12 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S030352-CCV 1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD
CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
Acetone
A
5.00
5.18
0.8623388
0.8924728
3.5
30
Benzene
A
5.00
4.84
0.6955533
0.6731258
-3.2
30
2-Butanone (MEK)
A
5.00
4.99
1.336089
1.333746
-0.2
30
Chloroform
A
5.00
6.32
0.9890879
1.251255
26.5
30
1,3-Dichlorobenzene
A
5.00
6.13
0.6177324
0.7568834
22.5
30
Dichlorodifluoromethane (Freon 12)
A
5.00
5.79
1.322997
1.531005
15.7
30
Ethanol
A
5.00
4.12
0.181169
0.149411
-17.5
30
Tetrachloroethylene
A
5.00
6.24
0.3710352
0.4630784
24.8
30
Tetrahydrofuran
A
5.00
5.88
0.6749896
0.7932299
17.5
30
Toluene
A
5.00
5.29
0.7672716
0.811673
5.8
30
Trichloroethylene
A
5.00
5.77
0.2710247
0.31291
15.5
30
Trichlorofluoromethane (Freon 11)
A
5.00
6.01
1.077722
1.294709
20.1
30
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
* Values outside of QC limits
Page 13 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S030467-CCV 1
COMPOUND
TYPE
CONC. (ppbv)
RESPONSE FACTOR
% DIFF / DRIFT
STD CCV
ICAL
CCV
MIN (#)
CCV
LIMIT (#)
Ethanol
A
5.00 4.08
0.181169
0.1476783
-18.5
30
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
* Values outside of QC limits
Page 14 of 18

,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
EPA TO-15 in Air
Acetone
NY,ME
Benzene
AIHA,FL,NJ,NY,VA,ME
2-Butanone (MEK)
AIHA,FL,NJ,NY,VA,ME
Chloroform
AIHA,FL,NJ,NY,VA,ME
1,3-Dichlorobenzene
AIHA,NJ,NY,ME
Dichlorodifluoromethane (Freon 12)
NY,ME
Tetrachlomethylene
AIHA,FL,NJ,NY,VA,ME
Tetrahydrofuran
VA
Toluene
AIHA,FL,NJ,NY,VA,ME
Trichloroethylene
AIHA,FL,NJ,NY,VA,ME
Trichlorofluoromethane (Freon 11)
NY,ME
The CON -TEST Environmental
Laboratory operates under the
following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA
Massachusetts DEP
M-MA100
06/30/2019
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2019
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI
Rhode Island Department of Health
LA000112
12/30/2019
NC
North Carolina Div. of Water Quality
652
12/31/2019
NJ
New Jersey DEP
MA007 NELAP
06/30/2019
FL
Florida Department of Health
E871027 NELAP
06/30/2019
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME
State of Maine
2011028
06/9/2019
VA
Commonwealth of Virginia
460217
12/14/2019
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW
North Carolina Department of Health
25703
07/31/2019
Page 15 of 18

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Page 16 of 18

121412018 Track your package or shipment with FedEx Tracking
773852156628
Delivered
Monday 12/03/201 S at 1.54 pm
FROM
Charlotte, NC US
Multiple -piece Shipment
DELIVERED
Signed for by: PBLAG
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
3 Piece shipment
TO
East Longmeadow, MA US
tt.
TRACKING NUMBER SHIPPER CITY, STATE SHIP DATE STATUS DELIVERY DATE DESTINATIONIRECIPI.EMT
CITY, STATE
773852156580 CHARLOTTE, INC 11/30/2018 12/03/2018 EASI LONGMEADOW, MA
(master j
773852156135 CHARLDTTF NC 11/30/2018
12/03,12018 EAST LONGMEADOW, MA
773852156628 CHARLOTTE, NC
11/30/2018
12/03;2018 EAST LONGMEADOW, MA
Shipment Facts
TRACKING NUMBER
SERVICE
MASTER TRACKING NUMBER
773852156628
FedEx Ground
773852156580
WEIGHT
DIMENSIONS
TOTAL PIECES
10 Ibs / 4.54 kgs
18x10x10 in
3
TOTAL SHIPMENT WEIGHT
TERMS
PACKAGING
30 Ibs / 13.61 kgs
Third Party
Package
STANDARD TRANSIT
SHIP DATE
ACTUAL DELIVERY
U
Mon 12/03/2018 1:54 pm
12/04/2018
Fri11/30/2018
hops:l/www.fedex.comlappslfedextrackl?action=track&tracknumbers=773852166628&locale=en_US&entry_code=us Page 17 of 18

Received By RE) Date
How were the samples In Cooler On Ice
received? In Box Ambient
Were samples within Temperature By Gun;; - Actual Temp _
Compliance? 2-6°C t_)pk By Blank # Actual Temp -
Was Custody Seal Intact?
Was COC Relinquished ? _ __ t E
Are there any loose caps/valves on any samples?
Is COC in ink/ Legible?
Time C�
No Ice
Melted Ice
Were Samples Tampered with?
Does Chain Agree With Samples?
1=
Did COC Include all Client T• Analysis Sampler Name
Pertinent Information? Project _T" ID's T' Collection Dates/Times T
Are Sample Labels filled out and legible? `F
Are there Rushes? F Who was notified?
Samples are received within holding time? L
Proper Media Used? -T--_ Individually Certified Cans?
Are there Trip Blanks? F= Is there enough Volume? T
Summa Cans
't; =
Nut/Ferrule
IC Train
Tedlar Batts
Tubing
TO-17 Tubee
T-Connector
Radiello
Syringe
�—Pufs/TO-11,s
Tedlar
Page 18 of 18 1

Appendix C
DEQ Risk Calculator Output
hart hickman
SMARTER ENVIRONMENTAL SOW71ONS

Point Concentrations
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID: Soil Combined
Exposure Unit ID:
Surface Soil Exposure Point Concentration Table
Exposure Point
Concentration
(mg/kg)
Justification for Exposure
Point Concentration
CAS Number
Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection Limits
Concentration
Used for
Screenin
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
( Y/N)
Rationale for
Selection or
Deletion
0.048
67-64-1
Acetone
mg/kg
1.9
7440-38-2
Arsenic, Inorganic
mg/kg
150
7440-39-3
Barium
mg/kg
0.053
7440-43-9
Cadmium (Diet)
mg/kg
93.7
16065-83-1
Chromium(III), Insoluble Salts
mg/kg
2.3
18540-29-9
Chromium(VI)
mg/kg
30
7439-92-1
Lead and Compounds
mg/kg
0.16
7439-97-6
Mercury (elemental)
mg/kg
0.38
117-81-7
—Bis(2-ethylhexyl)phthalate
mg/kg
0.29
7782-49-2
Selenium
mg/kg
0.073
7440-22-4
Silver
mg/kg
North Carolina DEQ Risk Calculator

Summary of Risk Assessment Output
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID: Soil Combined
Exposure Unit ID:
PRIMARY CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Soil Combined Pathways
1.0E-05
9.0E-02
NO
Groundwater Combined Pathways*
NC
NC
NC
Non -Residential Worker
Soil Combined Pathways
9.9E-07
8.7E-03
NO
Groundwater Combined Pathways*
NC
NC
NC
Construction Worker
Soil Combined Pathways
7.5E-07
6.0E-02
NO
User Defined
Soil Combined Pathways
NC
NC
NC
Surface Water Combined Pathways*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
Carcinogenic
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
NC
NC
NC
Soil Gas to Indoor Air
NC
NC
NC
Indoor Air
NC
NC
NC
Non -Residential Worker
Groundwater to Indoor Air
NC
NC
NC
Soil Gas to Indoor Air
NC
NC
NC
Indoor Air
NC
NC
NC
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target POE Concentrations Exceeded?
Protection of Groundwater Use
Source Soil
Exceedence of 2L at POE?
NM
Source Groundwater
Exceedence of 2L at POE?
NC
Protection of Surface Water
Source Soil
Exceedence of 2B at POE?
NM
Source Groundwater
Exceedence of 2B at POE?
NC
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for
lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed
the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a
risk -based closure.
North Carolina DEQ Risk Calculator

xposure Point Concentrations
ersion Date: February 2018
(Basis: November 2017 EPA RSL Table
Site ID: IAQ Combined
Exposure Unit ID:
Indoor Air Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Risks are calculated for these chemicals if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion.
Exposure Point
Minimum
Maximum
Location of
Range of
Concentration
Screening
Potential
Potential
Rationale for
Concentration
Justification for Exposure Point
CAS Number
Chemical
Concentration
Concentration
Units
Maximum
Detection
Detection
Used for
Background
Toxicity Value
ARAR/TBC
ARAR/TBC
COPC Flag
Selection or
3
(ug/m)
Concentration
(Qualifier)
(Qualifier)
Concentration
Frequency
Limits
Screening
Value
(Screening
Value
Source
(Y/N)
Deletion
Level) (n/c)
33
67-64-1
Acetone
ug/m3
13
71-43-2
Benzene
ug/m3
2.8
75-71-8
Dichlorodifluoromethane
ug/m3
3.4
109-99-9
—Tetrahydrofuran
ug/m3
5.6
78-93-3
Methyl Ethyl Ketone (2-Butanone)
ug/m3
0.63
127-18-4
Tetrachloroethylene
ug/m3
47
108-88-3
Toluene
ug/m3
2
75-69-4
Trichlorofluoromethane
ug/m3
North Carolina DEQ Risk Calculator

Summary of Risk Assessment Output
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID: IAQ Combined
Exposure Unit ID:
PRIMARY CALCULATORS
Receptor
Pathway
CarcinogenicRisk
Hazard Index
Risk exceeded?
Resident
Soil Combined Pathways
NC
NC
NC
Groundwater Combined Pathways*
NC
NC
NC
Non -Residential Worker
Soil Combined Pathways
NC
NC
NC
Groundwater Combined Pathways*
NC
NC
NC
Construction Worker
Soil Combined Pathways
NC
NC
NC
User Defined
Soil Combined Pathways
NC
NC
NC
Surface Water Combined Pathways*
NC
NC
NC
VAPOR INTRUSION CALCULATORS
Receptor
Pathway
Carcinogenic
Hazard Index
Risk exceeded?
Resident
Groundwater to Indoor Air
NC
NC
NC
Soil Gas to Indoor Air
NC
NC
NC
Indoor Air
3.6E-05
4.7E-01
NO
Non -Residential Worker
Groundwater to Indoor Air
NC
NC
NC
Soil Gas to Indoor Air
NC
NC
NC
Indoor Air
8.3E-06
1.1E-01
NO
CONTAMINANT MIGRATION CALCULATORS
Pathway
Source
Target POE Concentrations Exceeded?
Protection of Groundwater Use
Source Soil
Exceedence of 2L at POE?
NC
Source Groundwater
Exceedence of 2L at POE?
NC
Protection of Surface Water
Source Soil
Exceedence of 2B at POE?
NC
Source Groundwater
Exceedence of 2B at POE?
NC
Notes:
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for
lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed
the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a
risk -based closure.
North Carolina DEQ Risk Calculator

Appendix D
Field Forms
Is
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS
LOW -FLOW GROUNDWATER
SAMPLING RECORD
Job No: COP-008
Well ID: TMW-1
Well Location: Charlotte, NC
Facility Name: 1300 West Morehead Street Date: 12/5/18
Top of Casing Elevation (ft msl): Casing Material: PVC Volume of Water Per Well Volume: NA
Total Well Depth (ft): 20.18 Depth to Water (ft): 13.61 Well Diameter: 1-inch
Sampling Personnel: MRV I Screen Interval (ft bgs): 10.18 - 20.18
Type of Pump: Peristaltic Tubing Material: Polyethylene Pump/Tubing set at: 17.5
Weather Conditions: 40 F, partly cloudy NOTES: Had to keep lowering tubing due to drawdown
Ran dry at 09:45 & 10:00.
ft.
GROUNDWATER SAMPLING PARAMETERS
Water
Volume
Pumping
DO
Temp.
S. Cond.
pH
ORP
Turbidity
Time
Level
Pumped
Rate
m /I
S/cm
mV
NTU
09:14
15.62
0.4 L
100 mL/min
4.42
17.8
158.6
6.01
138.6
8.20
09:18
16.53
0.8
100
4.68
19.4
154.4
6.28
88.6
9.70
09:22
17.02
1.0
50
4.59
18.9
164.2
6.42
72.2
21.70
09:26
17.80
1.2
50
4.60
18.6
167.3
6.44
42.5
30.70
09:30
18.52
1.6
50
4.53
18.4
157.8
6.37
29.9
30.80
09:35
19.12
1.9
50
4.13
18.3
141.2
6.28
14.5
37.20
09:40
19.80
2.2
50
4.90
18.4
144.0
6.37
-56.0
17.90
09:45
20.00
2.5
50
4.92
17.8
138.9
6.26
-7.7
22.80
09:50
19.72
2.8
50
3.92
16.7
133.8
6.26
-46.8
30.20
09:55
19.77
3.1
50
4.52
16.3
134.8
6.23
-44.8
10.20
10:00
19.84
3.4
50
4.23
16.6
131.8
6.19
-38.6
7.80
Other Sample Parameters: Turbidity at 3.58 when collected metals sample
Sampled at: 10:05 Parameters taken with: YSI Pro Plus & HACH Turbidity Meter
Sample Delivered to: Con -Test by at
Field Filtration: ®Yes O No If yes, which sample parameters were field filtered:
Sample Parameter Containers (Types, Number of Containers, Preservatives):
VOCs (x3 40mL VOAs w/ HCI), SVOCs (x1 1 L amber), RCRA metals (x1 250mL plastic)
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record Stabilization criteria guidelines from the EPA SESD Operating
Date:11/5/2018 Procedure for Groundwater Sampling, dated April 26, 2017.

halt '�! hickman
Stabilization Criteria
Primary: Secondary:
pH +/- 0.1 unit DO +/- 0.2 mg/I
Job No: COP-008
SMARTER ENVIRONMENTAL SOLUTIONS
S. Cond. +/- 5% ORP +/- 20 mV
LOW -FLOW GROUNDWATER
Well ID: TMW-2 & DUP-GW-1
Turb. +/- 10% (<10 NTUs for metals)
SAMPLING RECORD
Well Location: Charlotte, NC
Facility Name: 1300 West Morehead Street
Date: 12/5/18
Top of Casing Elevation (ft msl):
Casing Material: PVC Volume of Water Per Well Volume:
NA
Total Well Depth (ft): 19.70
Depth to Water (ft): 12.58
Well Diameter:
1-inch
Sampling Personnel: MRV
I
Screen Interval (ft bgs): 9.70
-
19.70
Type of Pump: Peristaltic
Tubing Material: Polyethylene
Pump/Tubing set at:
17 ft.
Weather Conditions: 46 F, partly cloudy
NOTES: Initial issues with turbidity, so purged about 3 L
letting turbdity drop before collecting parameters
GROUNDWATER SAMPLING PARAMETERS
Water Volume
Pumping DO Temp.
S. Cond. pH
ORP
Turbidity
Time Level Pumped
Rate m /I (
S/cm
mV
NTU
13:34 13.54 0.0 L
100 mL/min 5.13 20.2
109.5 6.34
88.2
43.40
13:38 13.98 0.4
100 4.69 20.9
111.5 6.24
88.3
180.00
13:42 14.12 0.8
100 5.09 21.0
110.3 6.11
94.1
63.70
13:46 14.17 1.2
100 5.20 21.1
108.5 5.97
100.0
74.50
13:50 14.18 1.6
100 4.98 21.1
109.1 5.98
101.3
51.00
13:55 14.21 2.0
100 4.70 21.0
108.5 5.97
99.7
35.50
14:05 14.21 2.4
100 4.86 21.0
107.9 5.94
101.2
36.90
14:15 14.27 2.8
100 4.60 21.0
107.5 5.89
104.9
37.00
14:25 14.32 3.2
100 4.78 21.1
107.3 5.89
108.7
39.00
14:35 14.33 3.6
100 4.90 21.0
107.4 5.90
108.9
37.30
Other Sample Parameters: Turbidity down to
16.83 when collected metals sample.
Sampled at: 14:40
Parameters taken with:
YSI Pro Plus & HACH Turbidity
Meter
Sample Delivered to: Con -Test
by
at
Field Filtration: ®Yes O No If yes, which sample parameters were field filtered:
Sample Parameter Containers (Types, Number of Containers, Preservatives):
VOCs (x3 40mL VOAs w/ HCI), SVOCs (x1 1
L amber), RCRA metals (x1 250mL plastic)
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record Stabilization criteria guidelines from the EPA SESD Operating
Date:11/5/2018 Procedure for Groundwater Sampling, dated April 26, 2017.

halt '�! hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Stabilization Criteria
Primary: Secondary:
pH +/- 0.1 unit DO +/- 0.2 mg/I
S. Cond. +/- 5% ORP +/- 20 mV
Job No: COP-008
LOW -FLOW GROUNDWATER
Turb. +/- 10% (<10 NTUs for metals)
Well ID: TMW-3
SAMPLING RECORD
Well Location: Charlotte, NC
Facility Name: 1300 West Morehead Street
Date: 12/5/18
Top of Casing Elevation (ft msl):
Casing Material: PVC Volume of Water Per Well Volume:
NA
Total Well Depth (ft): 18.56
Depth to Water (ft): 13.07
Well Diameter:
1-inch
Sampling Personnel: MRV
I
Screen Interval (ft bgs): 8.56
- 18.56
Type of Pump: Peristaltic
Tubing Material: Polyethylene
Pump/Tubing set at:
17.5 ft.
Weather Conditions: 46 F, partly cloudy
NOTES: Initial pumping had high turbidity, so pumped dry
twice, then let recharge before collecting parameters.
GROUNDWATER SAMPLING PARAMETERS
Water Volume
Pumping DO Temp.
S. Cond. pH
ORP Turbidity
Time Level Pumped
Rate m /I (
S/cm
mV NTU
14:56 17.04 1.4 L
50 ml-min 4.40 18.8
175.5 6.44
63.4 28.90
15:00 17.04 1.6
50 5.22 18.7
176.5 6.43
2.3 144.00
15:04 16.63 1.8
50 6.74 18.7
173.0 6.46
0.5 32.00
15:08 16.68 2.0
50 7.07 18.6
172.5 6.41
1.3 9.29
15:12 16.70 2.2
50 7.49 18.7
170.1 6.37
12.6 5.16
Other Sample Parameters:
Sampled at: 15:15
Parameters taken with:
YSI Pro Plus & HACH Turbidity
Meter
Sample Delivered to: Con -Test
by
at
Field Filtration: ®Yes O No If yes, which sample parameters were field filtered:
Sample Parameter Containers (Types, Number of Containers, Preservatives):
VOCs (x3 40mL VOAs w/ HCI), SVOCs (x1 1
L amber), RCRA metals (x1 250mL plastic)
File: S:\AAA-Master Templates\Forms-Groundwater\Low Flow Groundwater Sampling Record Stabilization criteria guidelines from the EPA SESD Operating
Date:11/5/2018 Procedure for Groundwater Sampling, dated April 26, 2017.

Sub -Slab / Soil Gas Vapor QA/QC Field Form
Project No.: COP-008
Canister /
Vapor Monitoring Point Construction
Helium Leak Test
Regulator
ID Numbers
Sample /
Shut-in Test
Type
Ground Surface
Depth of
Date &Time
Ambient
Purge Method
Purge Vol
Helium Conc.
Helium Conc.
Leak Test
passed
Screen
Temp.
Shroud
Purge
Passed
Canister /
perm.
concrete, wood,
thickness
mm/dd/yy
syringe, peristaltic,
% or ppm
Yes / No
Regulator
Yes / No
SS, SG
temp.
asphalt, grass, soil,
p
inches
ft b s
g
24-hour clock
of
etc.
Liters
o
/o
(indicate units
(see note)
gravel etc.
(if appl.)
below)
S: SSV-1
O Yes
12/5/18
0.0
O Yes
C: 1110
Temp.
Concret
6.0
48.0
Syringe
1.2
86.5
O ppm
0 No
R: 4173
O No
13:10
O %
S: SSV-2
O Yes
12/5/18
0.0
O Yes
C: 1854
O No
Temp.
Concret
6.0
48.0
Syringe
1.2
85.2
O ppm
0 No
R: 4254
13:15
O
S: SSV-3
O Yes
12/5/18
0�0
O Yes
C: 1507
O No
Temp.
Concret
6.0
48 .0
Syringe
1.2
81.7
O ppm
O No
R: 4247
13:15
O %
S: DUP-SSV-1
�
O Yes
O Yes
C: 1721
O No
Temp.
O ppm
O No
R: 4173
O %
5= sample; G/K = canister/regulator-, 55 = sub -slab-, 56 = soil gas; perm = permanent; temp = temporary
-49
hart
Sampler(s):
Weather:
Notes:
40's F, sunny
Duplicate sample taken on SSV-1
hickman
SMARTER ENVIRONMENTAL SOLUTIONS
SABBB Master Templates\Forms -Soil Gas\Sub-slab & Soil Gas QA_QC Field Form
Sub -Slab / Soil Gas Sampling Vapor QA/QC Field Form
Hart & Hickman, PC

INDOOR AIR BUILDING SURVEY
and SAMPLING FORM
Site Name: 1300 West Morehead Street
Preparer's name:
Preparer's affiliation:
Part I - Occupants
Building Address: _
Property Contact:
Matt Vawter
Hart & Hickman, PC
DSCAID#: Not Applicable
Date: 11 /29/18
Phone #: [phone]
1300 West Morehed Street, Charlotte , NC
Lawrence Shaw
Owner / Renter / other: Buyer
Contact's Phone: home P007j work ( ) cell ( )
# of Building occupants: Children under age 13 0 Children age 13-18 0 Adults 4
Part II — Building Characteristics
Building type: residential / multi -family residential / office / strip mall / commercial / industrial
Describe building: Garage/warehouse Year constructed: 1929
Sensitive population: day care / nursing home / hospital / school / other (specify): _
Number of floors below grade: 0 (full basement / crawl space / slab on grade)
Number of floors at or above grade: 1
Depth of basement below grade surface: ft. Basement size: ft2
None
Basement floor construction: concrete / dirt / floating / stone / other (specify):
Foundation walls: poured concrete / cinder blocks / stone / other (specify) brick
Basement sump present? Yes No Sump pump? Yes / No Water in sump? Yes / No
Type of heating system (circle all that apply):
hot air circulation hot air radiation wood steam radiation
heat pump hot water radiation kerosene heater electric baseboard
other (specify): unknown
Type of ventilations stem (circle all that apply):
central air conditionin mechanical fans hroom ventilation f
individual air conditioning units kitchen range hood fan outside air intake
other (specify):
Type of fuel utilized (circle all that apply):
atural electric fuel oil / wood / coal / solar / kerosene
Are the basement walls or floor sealed with waterproof paint or epoxy coatings? Yes / No

Is there a whole house fan? Yes / No
Septic system? Yes / Yes (but not used) / No
Irrigation/private well? Yes / Yes (but not used) No
Type of ground cover outside of building: grass concrete asphalt other (specify)
Existing subsurface depressurization (radon) system in place? Yes / No
Sub -slab vapor/moisture barrier in place? Yes / No
Type of barrier:
Part III - Outside Contaminant Sources
Other stationary sources nearby (gas stations, emission stacks, etc.):
Unknown
active /passive
Heavy vehicular traffic nearby (or other mobile sources): Yes, roads south &east, parking north
Part IV — Indoor Contaminant Sources
Identify all potential indoor sources found in the building (including attached garages), the location of the
source (floor and room), and whether the item was removed from the building 48 hours prior to indoor air
sampling event. Any ventilation implemented after removal of the items should be completed at least 24
hours prior to the commencement of the indoor air sampling event.
Potential Sources
Location(s)
Removed
(Yes / No / NA)
Gasoline storage cans
North annex, x2
No
Gas -powered equipment
Cars, x5
No
Kerosene storage cans
No
Paints / thinners / strippers
household latex/oil-based paints
Yes
Cleaning solvents
Oven cleaners
Carpet / upholstery cleaners
Other house cleaning products
household cleaners
Yes
Moth balls
Polishes / waxes
Insecticides
Furniture / floor polish
Nail polish / polish remover
Hairspray
Cologne / perfume
Air fresheners
Fuel tank (inside building)
NA
Wood stove or fireplace
NA
New furniture / upholstery
New carpeting / flooring
NA
Hobbies - glues, paints, etc.

Part V — Miscellaneous Items
Do any occupants of the building smoke? (Yes )/ No How often? Daily
Last time someone smoked in the building? 12-24 hours / days ago
Does the building have an attached garage directly connected to living space? Yes No
If so, is a car usually parked in the garage? Yes / No
Are gas -powered equipment or cans of gasoline/fuels stored in the garage? Yes / No
Do the occupants of the building have their clothes dry cleaned? Yes No
If yes, how often? weekly / monthly / 3-4 times a year
Do any of the occupants use solvents in work? Yes No
If yes, what types of solvents are used?
If yes, are their clothes washed at work? Yes / No
Have any pesticides/herbicides been applied around the building or in the yard?
If so, when and which chemicals?
Has there ever been a fire in the building? Yes No If yes, when?
Has painting or staining been done in the building in the last 6 months?
If yes, when
Part VI — Sampling Information
Sample Technician: Matt Vawter
and where?
Yes /(So)
Yes / No
Phone number: (704) 586 - 0007
Sample Source:(indoor Air / Crawlspace Air /<iEla / Near Slab Soil Gas / Exterior Soil Gas
Sampler Type: Tedlar bag / Sorbent tainless Steel Canist / Other (specify):
Analytical Method: O-1 / TO-17 / other: Cert. Laboratory,
Con -Test
Sample locations (floor, room):
Field ID # IAQ-1 - Southern warehouse Field ID # IAQ-3 - northern warehouse
Field ID # IAQ-2 Central warehouse
Were "Instructions for Occupants" followed?
If not, describe modifications:
Field ID # -

Provide Drawing of Sample Location(s) in Building
See Figure 2.
Part VII - Meteorological Conditions
Was there significant precipitation within 12 hours prior to (or during) the sampling event? Yes / No
Describe the general weather conditions: 30's F in morning, up to low 50's F in afternoon
slight wind, no precipitation
Part VIII — General Observations
Provide any information that may be pertinent to the sampling event and may assist in the data
interpretation process (e.g., observed that drycleaner operated with door or windows propped open for
ventilation).
Door to office space opened periodically. Couple small holes in windows of garage.
Garage bay doors not flush to wall (gaps at edges)
HVAC system running as normal
(Adapted from the NJDEP Vapor Intrusion Guidance, October 2005)

Appendix E
Brownfields Property Receptor Survey Form
is
hart hickman
SMARTER ENVIRONMENTAL SOLUTIONS

North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information
requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield's
Project Manager (PM).
Site: 1300 West Morehead Street Brownfields Property
Address: 1300 West Morehead Street
City:
County:
Brownfields Project Number:
Charlotte
Mecklenburg
22039-18-060
Property and Building Characteristics
Surface Conditions
Current Usage
Proposed Usage
Size of Property (acres)
0.36
% of property that is wooded/brush
0
% of property that is grassed areas (unpaved)
% of property that is agricultural crops
0
% of property that is paved
25
% of property that is covered by buildings
75
If an existing building is on -site, please respond to the following. Information can be provided on additional sheets as needed. If
numerous buildings are on -site, consult with your PM as only information on specific buildings may be needed.
a. Provide occupancy and use information.
A small portion of the building on -site is actively used by a commerical real estate buisness of about 5 people.
The remaining is a garage that is used for storage by the property owner.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings (e.g. windows,
bay doors), and height (number of stories).
The one-story building has brick exterior walls with a rubber membrane roof and concrete slab foundation. The office
portion of the building is finished with carpet and tile flooring and drywall. The warehouse is composed of brick interior
wall and a concrete floor. Two bay doors and large windows are present along the eastern wall of the warehouse.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
Concrete slab -on -grade with bare concrete, carpet, and tile interior finishes.
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design
considerations (e.g. positive pressure?).
The office and warehouse portions of the building are equipped with a natural gas or electric HVAC system.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
No sub -slab ventilation systems or moisture barriers are currently in place beneath the Site building.
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North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If
specific receptors are present, please provide addresses of the facilities.
Zoning/Land Use
Current Use/Occupant
Proposed Usage
Northeast
Vacant (park nlot)
Unknown
East
Office
Unknown
South/Southwest
Office and multi -family residential
Unknown
West/Northwest
Commercial
Unknown
Specific Land Uses of Interest
YA
Distance atance
Direction
Address
Is a school or daycare center within 1,000 ft of the Property?
N
--
--
--
Is there a residence within 1,000 ft of the Property?
Y
50
NW
701/703 S. Summit
Avenue
Is there a basement within 1,000 ft of the Property
Y
500
NW
719 Grandin Road
Utilities
For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction material, and
diameter of the utilities. In addition, please provide the following information on utilty providers. If additional assessment is
required, the public utility locators should be contacted. This information can then be added to a site map.
Is there a septic system on -site? (Y or N) No
Please provide the utility providers for the subject property
a. Natural Gas Piedmont Natural Gas (underground)
b. Sewer/ Water Charlotte Water (underground)
c. Electricity Duke Energy (underground)
und)
d. Other fiber optics/communication (under & aboveground)
For surrounding properties, please complete the following table with available information.
Utility/Potential Receptor
Y/N
nce Dista
sta
Direction
Is a storm water pipe within 100 ft of the Property boundary?
Y
<50 ft
east/south/
north
Is a sanitary sewer within 100 ft of the Property boundary?
Y
on -site
Is a septic system leach field within 500 ft of the Property boundary?
N
Is a water line main within 100 ft of Property boundary?
Y
on -site
Is a natural gas line main within 100 ft of the Property boundary?
Y
on -site
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Y
on -site
Is a buried electrical cable main within 100 ft of Property boundary?
N
on -site
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject
property.
Rev. 09/2015 Page 2 of 3

North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
What is the potable water supply for the property? Public X Private
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the
water providers name.
Charlotte Water
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield
survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be
present. Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the
windshield survey. If multiple wells are present within the requested radius, please provide a map of the well locations. If needed,
lease attach a se arate table to hst all wells. Please note, the PM may Op t for a more extensive water supp1y
well sur ey if needed.
Water Supply Wells
Y/N
Distance
Direction
Address
Is a public water supply well within 1 mile of the Property boundary?
N
Is a private water supply well within 1,500 ft of the Property boundary?
N
Is an irrigation well within 1,500 ft of the Property boundary?
N
Surface Water & Wetlands
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the
Property.
Provide Information regarding Surface Water and Wetlands
Response/Comments
Are there surface water features on the property? (If yes,
please complete a. to d.)
No
a. Is the water body naturally developed or man-made?
NA
b. List the uses of the water body.
NA
c. What is the source of the water for the water body?
NA
d. What is the nature of the bottom of the water body
(e.g., rocky or concrete bottom, drainage ways or
NA
impoundments)
If no on -site surface water features, what is the nearest
surface water body?
Irwin Creek (500 ft southeast)
Are there any wetlands present on the property? If no
wetlands on -site, are wetlands suspected on adjoining
No
properties?
Rev. 09/2015 Page 3 of 3