13019_Planters Oil Mill_RRPT_20110412

UST Closure Report
Former Planters Oil Mill
1004 Cokey Road
Rocky Mount, North Carolina
H&H Job No. CRM-008
April 12, 2011
rtiHarl & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
704-586-0007
3334 Hillsborough Street
Raleigh, NC 27607
919-847-4241
#C-1269 Engineering
#C-245 Geology

Underground Storage Tank Closure Report
A. Site Information
1. Site Identification
Date of Report: April 12, 2011
Facility ID: N/A -Orphan USTs UST Incident Number: N/A
Site Name: Former Planters Oil Mill
Site Street Address: 1004 Cokev Road
City, Town: Rocky Mount Zip Code: 27801 County: Edgecombe
Description of Geographical Data Point: _Top/Midline of UST 001
Location Method: Google Earth
Latitude: 350 55' 45.09" N Longitude: 770 47'22.48" W
2. Information about Contacts Associated with the UST System
UST Owner: City of Rocky Mount, NC
Address: 331 S. Franklin St., Rocky Mount, NC 27802
Tel.: [phone]
UST Operator: Planters Oil Mill (Out of Business)
Address: 1004 Cokey Road, Rocky Mount, NC 27802
Tel.: N/A
Property Owner: City of Rocky Mount, NC
Address: 331 S. Franklin St., Rocky Mount, NC 27802
Tel.: [phone]
Property Occupant Vacant
Address: N/A
Tel.: N/A
Consultant/Contractor: Hart & Hickman, PC
Address: 3334 Hillsborough St., Raleigh, NC 27607
Tel.: [phone]
Analytical Laboratory: Prism Laboratories, Inc.
State Cert. No. 402
Address: 449 Springbrook Road, Charlotte, NC 28224
Tel.: [phone]
3. Information About Release
Date Discovered: 03/11/2011 (Analytical data associated with single sample)
Estimated Quantity of Release: Unknown/Not determined
Cause of Release: Possible overfills or spillage associated with UST 001
Source of Release: 20,000 Gal #6 Fuel Oil UST syste
Sizes and contents of UST system: 1-20,000 Gal. #6 Fuel Oil UST, 1-22,500
Gal. Hexane UST
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4. Certification
I, Leonard Moretz, P.G., a Professional Geologist for Hart & Hickman, PC, do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
•tttuu,
•,.••4�� CARo�
s SEA
L
Hart & Hickman, PC is licensed to practice geology/engineering in North Carolina. The
certification numbers of the company are C-245/C-1269.
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B. Site History and Characterization
1. UST Owner and Operator Information:
UST ID Number
001
Facility ID Number
NA, Unregistered
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/
City of Rocky Mount, NC
N/A — Orphan UST
Street Address
331 S. Franklin St.
city
State
Zip
Telephone Number
Rocky Mount
NC
27802
252-972-1325
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
N/A — Orphan USTs
Mid-1960's to 1983
Street Address
1004 Cokey Road
city
State
Zip
Telephone Number
Rocky Mount
I NC
127801
N/A Closed Facilit
UST ID Number
002
Facility ID Number
NA, Unregistered
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/
City of Rocky Mount, NC
N/A — Orphan UST
Street Address
331 S. Franklin St.
city
State
Zip
Tele hone Number
Rocky Mount
NC
27802
N/A Closed Facility
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
N/A — Orphan USTs
Mid-1960's to 1983
Street Address
1004 Cokey Road
city
State
zip
Telephone Number
Rocky Mount
I NC
127801
1 N/A Closed Facility
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2. UST Information:
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
System?
001
#6 Fuel Oil
#6 Fuel
20,000
Single Wall
31'4" x
NA
Unknown,
Closed /
YES
& Water,
Oil
Steel
10'6" dia.
Pre-1970
Removed
Sludge
002
Water,
Hexane
22,500
Single Wall
34' x
NA
Unknown,
Closed /
NO
Sludge
I
I Steel
10'6" dia.
Pre-1970
i Removed
3. AST Information:
Was
Description
release
of
Date
AST ID
Current/Last
Previous
Capacity
Construction
Tank
Status of
associated
Associated
Tank
Number
Contents
Contents
(gallons)
Details
Dimensions
AST
with the
Piping and
Installed
AST
Pumps
S stem?
None
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4. Historical Release Information:
There are no documented historical UST, non -UST, or off -site releases known to be
associated with the Planters Oil Mill property.
5. Site characteristics:
The site is a currently vacant property located at 1004 Cokey Road in Rocky Mount,
Edgecombe County, North Carolina. The site is surrounded to the west, north and east by
City owned street right of ways, beyond which lie residential areas. The site is bordered
to the south by the CSX Railway right of way. Beyond the right of way are residential
and commercial/retail properties. A topographic site location map is presented as Figure
1, and a site map is presented as Figure 2. UST locations are shown on Figure 3.
The site is located at an elevation of 114 ft above mean sea level. Topography at the site
is generally flat, sloping slightly to the east, towards Cokey Road. Based on topography
surrounding the site, H&H anticipates the groundwater flow direction at the site is to the
east-southeast.
Soils observed during the excavation and removal of the USTs at the site included brown
& tan silty sand to depths of approximately 8 ft. beneath ground surface (bgs), grading to
dark brown fine silty sand to depths of approximately 13 ft. bgs. These soils are believed
to be fill material associated with the installation of the USTs. Groundwater infiltrated
the excavations to depths of approximately 8 ft. bgs.
The site is located within the Coastal Plain Physiographic Province. According to the
Geologic Map of North Carolina dated 1985, the subject property lies within the
Yorktown formation, underlain by the Upper Cape Fear Aquifer. In the site area, the
Geologic Map describes the underlying sediment as fossiliferous clay. "The clay is often
separated with lenses of fine grained sand or shell material." These clays help to provide
a highly competent confining unit above the Upper Cape Fear Aquifer. The major source
of recharge for the Upper Cape Fear Aquifer occurs where the aquifer is in
communication with the surficial aquifer, near the aquifer's westward limit. Yields from
water wells set in the Upper Cape Fear Aquifer are high, averaging 200 to 400 gallons
per minute (gpm), however drawdown of the aquifer can have a significant impact for a
large radius surrounding the drawdown location. According to the NC Division of Water
Resources, Groundwater Management Division, the Upper Cape Fear Aquifer ranges
from 3 to 3892 feet thick, and averages 185 feet thick. The aquifer is composed of very
fine to coarse sands and occasional gravels.
A water supply well survey was not conducted during UST closure activities, however,
the area is served by the City of Rocky Mount municipal water supply system. No
surface waters were identified on the site property or within 1,500 feet of the site.
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C. Closure Procedure
1. Preparations for closure including the steps taken to notify authorities, permits
obtained and the steps taken to clean and purge the tanks:
Prior to removal of the USTs, H&H submitted a GW/UST-3 (Notice of Intent: UST
Permanent Closure or Change in Service) form to the North Carolina Department of
Environment and Natural Resources (NCDENR), Division of Waste Management
(DWM), Underground Storage Tank Section on February 22, 2011. A copy of the form
is presented in Appendix A. The work performed at the site was conducted as part of the
City of Rocky Mounts' US EPA funded Brownfield Cleanup program. A copy of the site
specific Health and Safety Plan, Brownfield Assessment, Revision 1, dated November 18,
2010, is presented in Appendix B.
When originally located, it was believed that the tanks were full of water. H&H arrived
at the site on January 13, 2011 with the intention of sampling the liquids with each tank
for characterization. Upon gauging UST 001, it was found the tank contained #6 fuel oil,
rather than water as originally believed. For this reason, a sample of the material was not
obtained for analysis. A water sample from UST 002 was collected with a disposable
bailer. This sample was submitted for analysis by EPA Methods 8260 (VOCs, plus
hexane) and 1010 (flashpoint). Data for the EPA 8260 analysis indicated the presence of
hexane, toluene and benzene at levels of 8,200, 40 and 41 ug/L. Flashpoint analysis by
EPA Method 1010 showed the flashpoint of the liquid to be greater than 170' F.
Approximately one week prior to UST removals, EVO Corporation (EVO) of Winston
Salem, NC mobilized to the site to remove residual #6 fuel oil from UST 001. Due to it's
viscosity, the product in the tank was heated using a mobile steam distillation unit so the
liquids could be pumped from the tank and removed for recycling. Water contained
within UST 002 (a former hexane UST) was pumped from the UST by the City into the
City's publically owned treatment works (POTW). This water was discharged to the City
POTW based on analytical data for the water sample obtained by H&H. Based on the
low levels of hexane, toluene and benzene present in the water sample from the UST, the
City restricted the flow from the UST to less than 7 gallon per minute (gpm) to ensure
compliance with their discharge limits for the compounds. The pumping of water from
the tank occurred over the course of six days, ending the day prior to UST closure.
To start closure of the USTs on March 7, 2011, the overburden covering the tanks was
removed with a trackhoe, and soils were situated along three sides of each UST
excavated to expose the USTs. Soils removed from the excavations were stockpiled
adjacent to the tank locations pending analytical data for closure samples. These soils did
not exhibit odors or staining normally associated with a release, nor did screening of
samples with a photo ionization detector (PID) indicate a release.
Dry ice (carbon dioxide) was introduced into each of the USTs to displace any explosive
vapors within the tanks. After purging, an oxygen/lower explosion level (02/LEL) meter
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was utilized to determine the potential for explosive atmospheres within the tanks. The
measurement of 02/LEL within each UST was overseen by the City of Rocky Mount Fire
Marshall's Office. At the time of 02/LEL measurements, the levels detected were
acceptable to the Fire Marshall, who approved removal of the tanks.
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2. Closure procedures:
Initially, soil was removed from the top and sides of the USTs with a trackhoe so that the
tanks could be exposed and removed from the subsurface. Soils encountered during the
excavation were evaluated in the field for the presence of odors and staining, as well as
organic vapor readings using a PID. The PID was calibrated prior to its use against an
isobutylene standard. No evidence of a release from either UST was noted during closure
procedures, based both on PID measurements and the absence of staining or odors which
might be indicative of a release. Notably, each of the tanks was secured beneath grade
with steel straps, likely emplaced to prevent the tanks from "floating" on a high water
table. The USTs were subsequently removed from the subsurface using a trackhoe, and
ultimately loaded onto flatbed trailers with a 50 ton hydraulic truck crane.
Following removal, the USTs were cleared of soils adhering to their exteriors, and
inspected for evidence of holes, pitting, and corrosion. The USTs were constructed of
steel and appeared to be in very good condition, with only minor pitting observed on the
exterior of the tanks. No holes resulting from degradation were noted in either tank.
Steel piping associated with the USTs had been cut from the tanks at an earlier date, and
no product lines or piping were removed during closure activities.
After UST removals, closure soil samples were collected in accordance with the DENR
UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and
Abatement for UST Releases, March 1, 2007 Version, Change 3, Effective December 1,
2008 (Guidelines). Because groundwater infiltrated each excavation and stabilized
between 7 and 8 ft. bgs, sampling was performed as per the requirements of Section 5.3D
of the Guidelines (Closure of USTs in Areas with High Water Tables). There were no
field indications of a release based on PID readings of the closure soil samples or random
soil samples obtained for screening, nor were staining or odors indicative of releases from
the UST systems noted.
Following receipt of analytical data for closure samples collected from the excavated
areas, the UST excavations were backfilled with the clean soil that was removed during
closure activities, in addition to processed fill material provided by the City.
After UST closure activities, H&H submitted a Site Investigation Report for Permanent
Closure or Change -in -Service of UST (UST-2 Form) to the DENR — Raleigh Central
Office and Raleigh Regional Office on March 31, 2011 on behalf of the City. A copy of
this form is included in Appendix C.
3. Note the amount of residual material pumped from the tank and describe the
storage, sampling and disposal of the residual material and the disposal of the tank,
pumps and piping:
Approximately one week prior to UST removals, EVO Corporation (EVO) of Winston
Salem, NC mobilized to the site to remove residual #6 fuel oil from UST 001. Product
contained in the tank was heated using a mobile steam distillation unit so the product
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could be pumped from the tank and removed for recycling. Water contained within UST
002 (the hexane UST) was pumped from the UST by the City into the City's publicly
operated treatment works (POTW). This water was discharged to the City POTW based
on analysis of a sample of the water obtained by H&H, analyzed by EPA Method 8260
(plus hexane). Analytical data for this sample is presented in Appendix E. Based on the
low level of hexane present in the water sample from the UST, the City restricted the
flow from the UST to less than 7 gallons per minute (gpm), in order to prevent an
exceedance of their discharge limit for the compound. The pumping of water from the
tank occurred over the course of six days, ending the day prior to UST closure.
A total of approximately 22,500 gallons of water were pumped from the hexane UST
(UST 002) by the City. This water was pumped directly into the City POTW. No
disposal manifest for these residuals was produced.
A total of 9,000 gallons of #6 fuel oil was pumped from UST 001 and transported from
the site for recycling. This material was transported to Triangle Biof eels Industries
located in Wilson NC.
A total of 5,895 gallons of residual contaminated water was removed from UST 001.
This residual water was transported to HOH Corporation in Winston-Salem, NC for
disposal through wastewater treatment.
A combined total of 10,700 gallons of residual sludge material was removed from the
tanks. This sludge material was transported to HOH Corporation in Winston-Salem, NC
for disposal through solidification.
USTs removed from the site were transported to American Metal Transfer in Elizabeth
City, NC for destruction and recycling.
Manifests and disposal certificates for product, water and sludges removed from the
tanks, as well as a certificate of disposal for the tanks are presented in Appendix D. No
pumps associated with the UST systems were identified during the tank removals.
4. Soil Excavation Activities:
As previously stated, there were no field indications of a release based on PID readings of
the closure soil samples collected adjacent to the USTs. Additionally, there were no field
indications of a release based on PID readings of the overburden soils that were
excavated to remove the USTs, nor were odors or staining normally associated with a
release noted. Dimensions of the UST soil excavations were approximately 41 ft by 19 ft
by 12 ft deep (UST 001) and approximately 54 ft by 15 ft by 13 ft deep (UST-002). The
top of the USTs were located approximately 3 ft bgs. Soils observed during the
excavation and removal of the USTs at the site included brown & tan silty sand to depths
of approximately 8 ft. bgs, grading to dark brown fine silty sand to depths of
approximately 13 ft. bgs. These soils were believed to be fill material associated with the
installation of the USTs. Groundwater infiltrated the excavations and stabilized at depths
between 7 and 8 ft. bgs.
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The UST excavations were backfilled with the clean soil that was removed from the
excavations during closure activities, in addition to processed fill material provided by
the City. Neither compaction, nor compaction testing of the backfilled excavations was
performed.
D. Site investigation:
1. Description of field screening:
Field screening of soil samples included the screening of samples collected for closure of
the USTs, in addition to random soil samples originating from the overburden soils.
Screening of samples was performed using a RAE Systems MiniRAE 3000TM PID. The
PID was calibrated prior to use in accordance with manufacturer's specifications. Soil
samples were placed in separate plastic Ziploc® bags and subsequently screened with the
PID. Screening of soil samples associated with the closure of these tanks showed the
presence of volatile vapors as measured with the PID ranging from 0 to 4 ppm, however
the levels did not vary from those measured in background air, and were not thought to
be indicative of a release. No odors or staining which might be indicative of a release
were noted in soil samples screened.
2. Soil Sampling Information:
Following the removal of the USTs, closure soil samples were collected in accordance
with the DENR UST Section Guidelines using the excavator bucket. As groundwater had
infiltrated the excavations to within approximately 8 ft. of surface grade, sampling of the
sidewalls of the excavations at 10 ft. intervals was performed, in accordance with Section
5.3D of the Guidelines (Closure of USTs in Areas with High Water Tables).
Soil samples were collected from the center of the excavator bucket from soil not in
direct contact with the bucket. Samples originating from each excavation were collected
at depths of approximately 6 to 7 ft. bgs, along the sidewalls of the excavated areas,
spaced in approximate 10 ft. intervals.
The locations of soil samples obtained as a part of the UST closure activities are depicted
on Figure 4. Samples T1-S1, T1-S2, T1-S3, T1-S4, T1-S5, T1-S6, T1-S7, T1-S8, T1-S9,
T1-S10, T1-S11 and T1-S12 were collected in association with closure of UST 001, the
20,000 gallon #6 fuel oil UST. These samples were submitted for analysis of total
petroleum hydrocarbons (TPH) as diesel range organics (DRO) and gasoline -range
organics (GRO) by EPA Method 8015B.
Samples T2-S1, T2-S2, T2-S3, T2-S4, T2-S5, T2-S6, T2-S7, T2-S8, T2-S9, T2-S10, T2-
S 11, T2-S 12, T2-S 13 and T2-S 14 were collected in association with closure of UST 002,
the 22,500 gallon hexane UST. These samples were submitted for analysis of volatile
organic compound (VOCs), including hexane, by EPA Method 8260B.
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3. Ground water and surface water sampling information:
No surface water or ground water sampling was conducted at the subject site in
association with UST closures.
4. Quality -control information:
During UST closure activities, soil samples were collected using a nitrile glove -covered
hand and placed into laboratory -supplied sample containers and then labeled as to
content, analyses requested, sample date and time, and sampler's name. Soil samples
collected for GRO and EPA-8260B analyses were collected using a specialized "T
handle" sampling device provided by the laboratory. Samples were placed in an iced
cooler subsequent to collection and were ultimately submitted to Prism Laboratories, Inc.
(NC Certification # 402) under chain -of -custody protocol.
5. Sample results:
With the exception of a single sample, analytical data for samples collected for closure of
UST 001 and analyzed for diesel and gasoline range TPH did not indicate the presence of
detectable TPH. Data for sample T1-S11 indicated the presence of diesel range TPH at a
level of 28 mg/kg. This level exceeds the minimum reportable concentration (RC) of 10
mg/kg for diesel range TPH defined by the NCDENR-DWM.
On March 14, 2011, H&H contacted Ms. Brenda Hafshejani with the UST Corrective
Action Branch of the Raleigh Regional Office of NCDENR-DWM to advise her of these
results. As all other data did not indicate the presence of a release form the UST system,
Ms. Hafshejani advised H&H that she would require the collection of a single additional
sample from the location of sample T 1-S 11, and this sample should be analyzed by the
"risk -based" methods, including VOCs by EPA-8260B, SVOCs by 8270C, and
extractable petroleum hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH)
by the Massachusetts Department of Environmental Protection (MADEP) method.
H&H obtained sample T 1-S 11 A on March 21, 2011 through the use of a Geoprobe® drill
rig, employing a MacroCoreTM sampling device. This sample was retained from the same
location of T1-S11, at a depth of 6.5 ft bgs. The sample was analyzed by the "risk based"
analytical methods including EPA-8260, 8270 and the MADEP-VPH and EPH methods.
Data for this sample did not indicate the presence of targeted compounds by EPA
Methods 8260 or 8270 at levels above the method detection limit(s). Data for the
MADEP EPH method did not reveal targeted aliphatic or aromatic hydrocarbons at levels
above the method detection limit. MADEP VPH data did not indicate the presence of
targeted aliphatic or aromatic hydrocarbons, with the exception of C9-C 12 aliphatic
hydrocarbons at a level of 13 mg/kg. This level does not exceed the Soil to Groundwater,
Residential, or Industrial/Commercial Maximum Soil Contaminant Concentration
(MSCC) for the compound range.
Analytical data for samples T2-S 1 through T2-S 14, collected in association with the
closure of the hexane UST, did not show the presence of targeted compounds by EPA
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Method 8260B. Based on these data, and in the absence of other indications of a release,
it appears there has been no release from UST 002 (the hexane UST).
Soil sample analytical results, analytical methods, and sample depths are summarized in
Table B3. The laboratory analytical data reports and chain -of -custody records are
provided in Appendix E.
E. Conclusions and Recommendations
On March 8, 2011, two USTs, one 20,000 gallon #6 fuel oil tank and one 22,500 gallon
hexane tank were removed from the subject site using industry standard methods. Both
USTs were in good condition, with only minor pitting of the tanks observed. There were
no indications of releases from the UST systems based on PID measurements of soil
samples collected during the closure proceedings, nor were staining or odors noted which
might indicate a release. Groundwater infiltrated each excavation and stabilized between
7 and 8 ft. bgs in the excavations.
Laboratory analytical results for closure samples associated with the closure of UST 001
indicate that no concentrations of TPH DRO or GRO were detected in UST closure soil
samples collected at the site, with the exception of diesel range TPH detected at a level of
28 mg/kg in sample T 1-S 11.
NCDENR UST Section was notified of the results from T1-S11. Ms. Brenda Hafshejani
of the UST Section requested the collection of a single additional sample from the
location of sample T1-S11, and this sample should be analyzed by the "risk -based"
methods, including VOCs by EPA-8260B, SVOCs by 8270C, and extractable petroleum
hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH) by the Massachusetts
Department of Environmental Protection (MADEP) method. A sample was collected on
March 21, 2011 and analyzed for these parameters. All analyzed parameters were below
detection limits, except C9-C 12 aliphatic hydrocarbons, detected at a level of 13 mg/kg.
This level does not exceed the Soil to Groundwater MSCC.
Analytical data for samples T2-S 1 through T2-S 14, collected in association with the
closure of the hexane UST (UST 002), did not show the presence of targeted compounds
by EPA Method 8260B. Based on these data, and in the absence of other indications of a
release, it appears there has been no release from UST 002 (the hexane UST).
Based upon the analytical data and observations made during the closure of the UST
systems at the site, and the additional analysis performed on sample T 1-S 11 A, no further
action should be required for this site in association with the closure of the tanks.
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Tables
Table B3 Summary of Soil Sampling Analytical Results
Figures
Figure 1 Topographic Site Location Map
Figure 2 Site Map
Figure 3 UST Locations
Figure 4 UST Closure Soil Sample Locations
Appendices
Appendix A Notice of Intent: UST Permanent Closure or Change -in -Service Form
(UST-3 Form)
Appendix B Site Specific Health and Safety Plan
Appendix C Site Investigation Report for Permanent Closure or Change -in Service of
UST Form (UST-2 Form)
Appendix D Tank Disposal Certificates, Residuals Manifests, Residuals Certificates of
Disposal
Appendix E Laboratory Analytical Data Reports and Chain -of -Custody Records
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Appendix A
Notice of Intent: UST Permanent Closure or Change -in -Service Form
(UST-3 Form)
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Table B3
Summary of Soil Sampling Results
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Table B- 3 Summary of Soil Sampling Results
Revision Date: 03/23/11 Incident Number and Name: Unassigned, Planters Oil Mill Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260) 4
826
MADEP
MADEP
MADEP-
MADEP
MADEP-
MADEP
8015
8015
0
8270
-VPH
-VPH
VPH
-EPH
EPH
-EPH
Contaminant of Concern 4
•4
a
� '
o
� �
Q.
Qn
Sample
Date
Source
Sample
Incident Phase
ID
Collected
Area (eg.
Depth (ft
(Closure, 20Day,
W
(m/dd/yy)
Tank pit
BGS)
LSA, etc.)
A
N
r?
N
1)
U
o
oho
x
x
H
H
T1-S1
03/08/11
UST1
6.5
Closure
<1.3
<0.55
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
T1-S2
03/08/11
UST1
6.5
Closure
<1.3
<0.56
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
T1-S3
03/08/11
UST1
6.5
Closure
<1.4
<0.56
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
T1-S4
03/08/11
UST1
6.5
Closure
<1.2
<0.77
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
UST1
T1-S5
03/08/11
6.5
Closure
<1.3
<0.69
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
T1-S6
03/08/11
UST1
6.5
Closure
<1.3
<0.69
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
UST1
T1-S7
03/08/11
6.5
Closure
<1.3
<0.56
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
UST1
T1-S8
03/08/11
6.5
Closure
<1.3
<0.62
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
UST1
T1-S9
03/08/11
6.5
Closure
<1.3
<0.61
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
T1-S10
03/08/11
UST1
6.5
Closure
<1.3
<0.71
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
T1-S11
03/08/11
UST1
6.5
Closure
28
<0.64
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
T1-S12
03/08/11
UST1
6.5
Closure
<1.2
<0.45
NA
NA
NA
NA
NA
NA
NA
NA
Excay.
03/21/11
UST1
T1-S11A
6.5
Closure
NA
NA
ND
ND
<1.7
13
<0.49
<0.72
<1.2
<3.1
Excay.
Soil to groundwater MSCC (mg/kg)
N/A
N/A
-
-
68
540
31
540
#
31
Residential MSCC (mg/kg)
N/A
N/A
-
-
939
1500
469
1500
31000
469
Industrial/Commercial MSCC (mg/kg)
N/A
N/A
-
-
24528
40000
12264
40000
810000
12264
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface ND = No compounds detected by method shown
mg/kg =milligrams per kilogram NA = Not Analyzed by method shown # Health Based Level > 100%

Table B- 3 Summary of Soil Sampling Results
Revision Date: 03/23/11 Incident Number and Name: Unassigned, Planters Oil Mill Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260)
8260
Contaminant of Concern 4
0
N
°O
W
i �1
U
O
a
Sample ID
Date Collected
(m/dd/yy)
Source Area
(eg. Tank pit 1)
Sample
Depth (ft
BGS)
Incident
Phase
(Closure,
20Day,
LSA, etc.)
T2-S1
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S2
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S3
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S4
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S5
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S6
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S7
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S8
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S9
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S10
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S11
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S12
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S13
03/08/11
UST2 Excay.
6.5
Closure
ND
T2-S14
03/08/11
UST2 Excay.
6.5
Closure
ND
Soil to groundwater MSCC (mg/kg)
Residential MSCC (mg/kg)
Industrial/Commercial MSCC (mg/kg)
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface Results must be reported in mg/kg.
mg/kg =milligrams per kilogram # Health Based Level > 100% ND = No compounds detected above method detection limits

Figures
Figure 1 Topographic Site Location Map
Figure 2 Site Map
Figure 3 UST Locations
Figure 4 UST Closure Soil Sample Locations

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Appendix A
Notice of Intent: UST Permanent Closure or Change -in -Service Form
(UST-3 Form)
Hart & Hickman, PC

> f f 1 `�' 10 '01 r!
e 1
UST-3 Notice of intent: UST Permanent Closure or Change -in -Service
Return completed form to:
STATE USE ONLY
The DWM Regional Office located in the area where the facility is located. Send a copy to the Central Office in Raleigh so that
t U u
the status of the tank may be changed to "PERMANENTLY CLOSED" and your tank fee account can be closed out.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
fate Received
INSTRUCTIONS (READ THIS FIRST)
Complete and return at least thirty (30) days prior to closure or change -in-service activities. If a Professional Engineer (P.E.) or a Licensed Geologist (L.G.)
provides supervision for closure or change -in-service site assessment activities and signs and seals all closure reports then at least a five (5) working
days notice is acceptable.
Completed UST closure or change-in-servico site assessment reports, along with a copy of the UST-2 form, should be submitted to the appropriate Division
of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be submitted to the Central
Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out.
UST closure and change -in-service site assessments must be completed in accordance with the latest version of the Guidelines for Tank Closure. The
Guidelines for Tank Closure can be obtained at www.wastenotnc.org.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
I aken for disposal. Usually, USTs are cleaned and cut up for scrap metal- This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
1.OWNERSHIP OF TANKS
It. LOCATION
Owner Name -City of Rocky Mount, NG
Facility Name or Company Former Planters Oil Mill
Street Address 331 S. Franklin Street
Facility ID 9 (it known) N/A _ Orphan Tanks
City Rocky Mount County Edgecombe
Street Address 1004 Cokey Road
State North Carolina Zip code 27802
City Rocky Mount GOunEdgecombe p c07802
Phone Number 252-972-1325
Phone Number N/A
III. CONTACT PERSONNEL
Name: Kevin Buchanan
Company Name: Hart & Hickman
Job Title: Sr. Env.Soecialist
,
019-847-4244,
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE -IN SERVICE -='t
i. Contact local fire marshal. S. Provide a sketch locating piping, tanks and a P.E. or L.G-, with _ 4-cl. - site
2. Plan entire closure event, soil sampling locations. assessment reports bearing -.-the signature
3. Conduct Site Soil Assessment. 6. Submit a closure report in the formand seal of the P.E. or L.G. rf,- releaseRlas
at of UST-12 (including the form UST-2) within not occurred, the supervisionsigrCaure or
4. if removing tanks or closing in place, refer to thirty (30) days following the site seal of a P.E. or L.G. is not required.
API Publication 2015 Cleaning Petroleum investigation. 8. Keep closure records for three (3) years.
Storage Tanks and 1604 Removal and If a release from the tanks has occurred, the
St! of Used Underground Petroleum
Storageorage site assessment portion of the tank closure
Tanks.
must be conducted under the supervision of
V. WORK TO BE PERFORMED BY
Contractor Name: Tony Fischer
Contractor Company Name: EVO Corporation
Address: 1703 Var rave St , tA�/inston-Salem
9
State: RlC
Zip Code:
27107
Phone No:
336-725-5844
Primary Consultant Name:
Leonard Moretz
Primary Consultant Company Name:
Hart & Hickman. PC
Consultant Phone No:
919-847-4241
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE -IN-SERVICE
Proposed Activit
Closure
Change -In -Service
Tank ID No.
Size in Gallons
Last Contents
Removal
Abandonment in Place `
New Contents Stored
001
20,000
#6 Fuel Oil
[]
❑
002
20,000
Hexane
0
❑
❑
❑
Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER'S AUTHORIZED REPRESENTATIVE
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title: Kevin B. Buchanan, Senior Environmental Specialist, Hart & Hickman, PC
Signature
Date Signed
SCHEDULED REMOVAL DATE
Notify your DWM Regional Office
i� � sa'. v
02122/`I 1
March 8, 201 1
48 hours before this dateif
scheduled removal date changes
U5 t -3 rtev 1 u12UUs

Appendix B
Site Specific Health and Safety Plan
Hart & Hickman, PC

Health and Safety Plan
Brownfield Assessment
Revision 1
Planters Oil Mill Site
Rocky Mount, North Carolina
Prepared for:
City of Rocky Mount
H&H Job No. CRM-008
November 18, 2010
ti Hart &Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
704-586-0007
3334 Hillsborough Road
Raleigh, NC 27607
919-847-4241

Health and Safety Plan
Brownfield Assessment
November 18, 2010
H&H Job No. CRM-008
Revision 1
Planters Oil Mill Site
Rocky Mount, North Carolina
Table of Contents
Section
Pate No.
1.0 Summary..................................................................................................................................1
1.1 Site History............................................................................................................................1
1.2 Known Site Contaminant Conditions....................................................................................2
1.3 Potential Assessment Worker Exposure Pathways...............................................................2
2.0 Applicability............................................................................................................................4
3.0 Facility Background/Work Plan............................................................................................5
3.1 Purpose and Scope of Work..................................................................................................5
4.0 Responsibilities........................................................................................................................6
4.1 Project Manager (H&H)........................................................................................................6
4.2 Site Safety Officer(H&H).....................................................................................................7
4.3 Manager, Health and Safety(H&H).....................................................................................9
4.4 Project Personnel (H&H)......................................................................................................9
4.5 Subcontractor's Safety Representative................................................................................10
4.6 Subcontractor Personnel......................................................................................................10
5.0 Job Hazard Analysis.............................................................................................................12
5.1 Heat Stress and Cold Stress Recognition and Control........................................................13
5.2 Chemical Hazards................................................................................................................13
5.3 Noise Hazards......................................................................................................................17
5.4 Underground Utilities (Pre -Drilling Protocol)....................................................................18
5.5 Work Area Protection (Traffic Control)..............................................................................18
5.6 Hazard Communication.......................................................................................................18
i u
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art & Hickman, PC

5.7 Heavy Equipment................................................................................................................19
5.8 Electrical Equipment/Lock Out -Tag Out............................................................................20
5.9 Structural Hazards...............................................................................................................21
6.0 Exposure Monitoring Plan...................................................................................................22
6.1 Chemical Exposure Monitoring..........................................................................................22
6.3 Data Logging.......................................................................................................................24
6.4 Dust Control........................................................................................................................24
7.0 Personal Protective Equipment...........................................................................................25
7.1 Limitations of Protective Clothing......................................................................................26
7.2 Duration of Work Tasks......................................................................................................27
8.0 Site Control............................................................................................................................28
8.1 General...............................................................................................................................28
8.2 Work Zones.........................................................................................................................29
9.0 Decontamination Procedures...............................................................................................31
9.1 Sanitation.............................................................................................................................32
9.2 Decontamination -Medical Emergencies.............................................................................32
9.3 Decontamination of Tools...................................................................................................32
10.0 Safe Work Practices............................................................................................................34
10.1 General..............................................................................................................................34
10.2 Sampling Practices............................................................................................................36
10.3 Health and Safety Equipment List.....................................................................................36
10.4 Buddy System....................................................................................................................37
11.0 Emergency Response Plan.................................................................................................38
11.1 Places of Refuge................................................................................................................39
11.2 Fire.....................................................................................................................................39
11.3 Communication.................................................................................................................39
11.4 Safety Eyewash.................................................................................................................40
11.5 Incident Report ..................................................................................................................40
11.6 Operation Shutdown..........................................................................................................40
11.7 Spill or Hazardous Materials Release...............................................................................41
11.8 Emergency Medical Treatment Procedures.......................................................................41
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art & Hickman, PC

11.9 Community Safety.............................................................................................................41
12.0 Training and Medical Surveillance...................................................................................42
13.0 Recordkeeping.....................................................................................................................44
14.0 Toxic Snake and Insect Bites and Plants..........................................................................45
14.1 Poisonous Snakebites........................................................................................................45
14.2 Poisonous Insect Bites.......................................................................................................46
14.3 Tickborne Diseases............................................................................................................48
14.4 Poisonous Plants................................................................................................................50
15.0 Medical Surveillance...........................................................................................................51
16.0 Forms...................................................................................................................................52
List of Appendices
Appendix A Safety Plan Compliance Agreement
Appendix B Hospital Route Map
Appendix C Accident/Exposure Report Form
Appendix D Site Safety Briefing Form
Appendix E Daily Instrument Calibration Check Sheet
ill u
S:\AAA-Master ProjectsVCity of Rocky Mount - CRMVCRM-OOtAPlanters Oil MillAPhase fhQAPP\POM H&SP.doc Hart
art & Hickman, PC

Health and Safety Plan
Brownfield Assessment
November 18, 2010
H&H Job No. CRM-008
Revision 1
Planters Oil Mill Site
Rocky Mount, North Carolina
Contact Numbers
Site Contact Peter Varney
Assistant City manager
City of Rocky Mount
One Government Plaza
PO Box 1180
Rocky Mount, NC 27802
Fire:
Ambulance:
(252)-972-1330
911
911
Hospital: Nash General Hospital
2460 Curtis Ellis Drive
Rocky Mount, NC 27804
[phone]
(Note — See Hospital Route Maps and Directions in Appendix B)
Poison Control: [phone]
Project Manager: Leonard Moretz [phone]
Site Safety Coordinator: Tim Klotz [phone]
Manager Health & Safety: Shannon Cottrill [phone]
Preparation Date: December 10, 2007
Revision Date: November 18, 2010
iii
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Health and Safety Plan
Brownfield Assessment
November 18, 2010
H&H Job No. CRM-008
Revision 1
Planters Oil Mill Site
Rocky Mount, North Carolina
Approvals
Project Director:
OZ'�a,'-te C.. /j10Ail�-
Leonard Moretz, PG
This Health and Safety Plan is valid only for this specific project as described in Section 3.0. It
is not to be used for other projects or subsequent phases of this project without the written
approval of the Manager of Health and Safety.
1v
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00 I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Glossary of Terms, Acronyms, and Abbreviations used in this Plan
ACGIH
American Conference of Governmental Industrial Hygienists
analyzer
refers to the field instrument described in Section 6.1
atm
atmosphere
OC
centigrade
Carcinogen
A substance that can cause cancer
cc
cubic centimeter
CGI
Combustible Gas Indicator
CNS
Central Nervous System
MH&S
Manager, Health & Safety
eV
Electron volts
EPA
U.S. Environmental Protection Agency
OF
Degrees Fahrenheit
GM
General Manager
HSP
Health and Safety Plan
kg
kilogram
LEL
Lower Explosive Limit
Lpm
liter per minute
MSDS
Material Safety Data Sheet
In
meter
mg
milligram
mg/M3
milligram per cubic meter
ml
milliliter
mm
millimeter
ND
Not Detected
NIOSH
National Institute for Occupational Safety and Health
OBZ
Operator's Breathing Zone
OEL
Occupational Exposure Limit
OSC
Office Safety Coordinator
v
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Glossary of Terms, Acronyms, and Abbreviations used in this Plan
OSHA
Occupational Safety and Health Administration
OVA
Organic Vapor Analyzer (Foxboro -Century)
PEL
Permissible Exposure Limit
PID
Photo -ionization Detector
PM
Project Manager
ppb
parts per billion
ppm
parts per million
RFI/RI
RCRA Facility Investigation/Remedial Investigation
REL
Recommended Exposure Limit
SSO
Site Safety Officer
SSR
Subcontractor's Safety Representative
STEL
Short Term Exposure Limit
TLV
Threshold Limit Value
UEL
Upper Explosive Limit
VOC
Volatile Organic Compound
vi
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Health and Safety Plan
Brownfield Assessment
November 18, 2010
H&H Job No. CRM-008
Revision 1
Planters Oil Mill Site
Rocky Mount, North Carolina
1.0 Summary
Hart & Hickman, PC (H&H) is performing Brownfield site assessment activities at the former
Planters Oil Mill Site at 1004 Cokey Road, which includes approximately 7.3 acres of property
bordered to the north by Short Street (formerly Henna Street), to the east by Cokey Road, to the
south by Norfolk Street and to the west by Branch Street in Rocky Mount, North Carolina ("the
subject property"). Assessment activities will include advancement of soil borings, monitor well
installation and sampling, and collection of soil and ground water samples for lithologic and
chemical quality purposes. The objectives of the proposed work are to assess potential
environmental risks to future site users, and to potentially facilitate negotiating a Brownfield
agreement with the North Carolina Department of Environment and Natural Resources (DENR)
for redevelopment of the site.
1.1 Site History
Available historic information indicates that the subject site was developed as early as 1907 as a
vegetable oil processing facility. Raw products have included cottonseed and soybeans.
Fertilizer manufacturing has also occurred onsite. Petroleum products, hexane (solvent used for
oil extraction), pesticides, PCBs, and nitrogen are known or suspected to have been used onsite.
An on -site fire that occurred in January 1983 destroyed the site buildings in the vicinity of the
hexane area including the former Cracking House, Solvent Extraction Tower, and former Hull
House. Commercial operations at the site ceased after the fire.
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1.2 Known Site Contaminant Conditions
An investigation conducted by fire investigators after the January 1983 fire indicated that soil
down to about three feet below ground was saturated with hexane in and around the former Hull
House, which was located adjacent to the hexane use area. Hexane was also stored onsite in an
underground storage tank (UST) near the solvent extraction tower. The status of the hexane
UST and the disposition of the residual hexane in the UST is unknown. There is no
documentation indicating that soil contaminated with hexane was removed from the site.
Two petroleum USTs were reportedly removed from the site in 1991. Other than the fire
investigation and the two UST removals, there are no known records of site contaminants. Other
suspect contaminants include metals and nitrates from fertilizer manufacture and storage,
pesticides from onsite use and storage, and PCBs from former onsite electrical transformers.
1.3 Potential Assessment Worker Exposure Pathways
Potential exposures anticipated from site contaminants are expected to be minimal based on
reported conditions at the site. The level of disturbance posed by proposed sampling and site
work practices is also expected to create minimal exposure hazards.
Skin contact with potentially contaminated soil or water will be minimized by wearing personal
protective clothing (as described in Section 7.0). Inhalation of vapors during assessment
activities will be minimized by air monitoring, engineering controls, and the use of respiratory
protection if action levels (see Section 6.1) are exceeded. Ingestion of contaminated materials
will be minimized by good personal hygiene during decontamination (i.e., thoroughly washing
face and hands with soap and water before eating or drinking).
A Photoionization Detector (PID) will be used to monitor for vapors . The PID will be used on a
regular basis, typically every five to ten minutes, to monitor in the immediate vicinity of the
sampling area. If readings exceed an average of 0.5 ppm above background for more than one
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minute, monitoring in the operator's breathing zone (OBZ) of the person working nearest the
borehole will start immediately, and the procedures described in Section 7.0 will be
implemented. An explosimeter will be used to monitor the ambient air for the Lower Explosive
Limit (LEL) of hexane when working in the former Hexane Use and Storage Area. Additional
exposure monitoring and personal protective equipment criteria are found in Sections 6.0 and
7.0, respectively.
General safety during sampling activities (i.e., heavy equipment, slip -trip -fall hazards, etc.) will
be accomplished through site safety (tailgate) meetings prior to initiation of work activities each
day.
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2.0 Applicability
The purpose of this plan, which was developed specifically for assessment activities at the
former Planters Oil Mill site at 1004 Cokey Road in Rocky Mount, North Carolina, is to assign
responsibilities; establish personal protection standards and safety procedures; and provide for
contingencies that may arise while assessment activities are being conducted at the site. This
plan complies with, but does not replace, Federal Health and Safety Regulations as set forth in
29 CFR 1910 and 1926. This plan is to be used by H&H's personnel as a supplement to such
rules, regulations, and guidance. The provisions of the plan are mandatory for all on -site H&H
employees conducting site activities that may involve health and safety hazards.
Changing and/or unanticipated site conditions may require modification of this site safety plan in
order to maintain a safe and healthful work environment. Proposed changes to this plan should
be reviewed with the H&H Manager of Health and Safety, or his designee, prior to their
implementation. If this is not feasible, the site/project manager may modify the plan and record
changes in the field log book. Under no circumstances will modifications to this plan conflict
with Federal, state, or local health and safety regulations.
H&H will provide a copy of this Health and Safety Plan to site subcontractors in order to fulfill
its obligation under 29 CFR 1910.120(b)(iv) to inform subcontractors of site hazards. Each
H&H subcontractor is to provide their own Health & Safety Plan that addresses the activities of
its employees relative to this project.
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3.0 Facility Background/Work Plan
As mentioned previously in Section 1.0, the subject site has been developed for commercial
purposes since before 1907. Previous uses of the site include vegetable oil processing and
fertilizer manufacturing and storage. Petroleum products, solvents, particularly hexane,
pesticides and nitrogen, potash, and PCBs are anticipated to have been used at the site.
Therefore, VOCs, PAHs, petroleum hydrocarbons, metals, pesticides, PCBs, and nitrates are
potential contaminants of concern at the site.
Aside from limited soil data related to UST removals onsite and qualitative information
pertaining to hexane contamination of soil developed during the 1983 fire investigation, there is
no previously developed quantitative data regarding potential contaminants of concern at the
subject site.
3.1 Purpose and Scope of Work
H&H is performing Brownfield site assessment activities at the site on behalf of the City of
Rocky Mount. The proposed activities will include soil boring advancement, soil sampling,
monitor well installation, and ground water sampling. Details concerning site assessment
activities are included in the Site -Specific Quality Assurance Project Plan Addendum for the
subject site.
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4.0 Responsibilities
Provisions of this HSP are mandatory for H&H employees who are engaged in assessment and
hazardous material management activities at the site. This HSP has been developed under U.S.
Environmental Protection Agency (EPA) guidelines and complies with applicable regulations,
including Occupational Safety and Health Administration (OSHA) standards [29 Code of
Federal Regulations (CFR) 1910 and 1926].
H&H will have site safety and health oversight and coordination responsibilities for H&H
personnel. Each subcontractor will be held accountable for the safe and healthful performance of
work by each of their employees, subcontractor, or support personnel who may enter the site.
H&H subcontractors expected to be present include a, utility locating service, drilling contractor
and land surveyor.
The specific job duties of H&H personnel are provided below.
4.1 Project Manager (H&H)
The Project Manager (PM) shall direct on -site operations. The PM may delegate all or part of
these duties to a properly qualified H&H employee who is designated as the Site Safety Officer
(SSO). At the site, the PM, assisted by the SSO, has primary responsibility for:
1. Seeing that appropriate personal protective equipment and monitoring equipment are
available and properly utilized by on -site H&H personnel;
2. Establishing that H&H personnel are aware of the provisions of this plan, are instructed in
the work practices necessary to ensure safety, and are familiar with planned procedures for
dealing with emergencies;
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3. Establishing that H&H on -site personnel have completed a minimum of 40 hours of health
and safety training and have appropriate medical clearance as required by 29 CFR 1910.120,
and have been fit tested for the appropriate respirators;
4. Seeing that H&H personnel are aware of the potential hazards associated with site
operations;
5. Monitoring the safety performance of all H&H personnel to see that the required work
practices are employed;
6. Correcting H&H work practices or conditions that may result in injury or exposure to
hazardous substances;
7. Preparing accident/incident reports for H&H activities (see Section 13.0);
8. Seeing to the completion of Plan Acceptance forms by H&H personnel (See Appendix A);
9. Halting H&H site operations, if necessary, in the event of an emergency or to correct unsafe
work practices; and
10. Reviewing and approving this project health and safety plan.
4.2 Site Safety Officer (H&H)
The Site Safety Officer's (SSO) duties may be carried out by the PM or other H&H site manager.
The SSO, unless specifically directed by this health & safety plan (HSP), does not mandate
health and safety guidance to any subcontractor unless there is an imminent endangerment to
personnel, in which case guidance is to be directed to the Subcontractor's Safety Representative
(SSR) only. The SSO:
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1. Implements project Health and Safety Plans, and reports any deviations from the anticipated
conditions described in the plan to the PM, and, if necessary, the Manager of Health &
Safety (MH&S).
2. Determines that monitoring equipment is used properly by H&H personnel and is calibrated
in accordance with manufacturer's instructions or other standards, and that results are
properly recorded and filed. (See Appendix F for Daily Calibration Check Sheet).
3. Checks with the MH&S to see that assigned H&H personnel have current Fit -For -Duty
medical and training authorizations.
4. Assumes any other duties as directed by the PM or MH&S.
5. Identifies all H&H personnel with special medical problems (e.g., allergies, perforated
eardrum, etc.).
6. Conducts daily safety meetings and completes the Site Safety Briefing Report (see Appendix
D).
7. Provides ongoing review of the protection level needs as project work is performed, and
informs the PM of the need to upgrade/downgrade protection levels as appropriate.
8. Sees that decontamination procedures listed in Section 9.0 are followed by H&H personnel.
9. Establishes monitoring of H&H personnel and records results of exposure evaluations.
10. Halting H&H site operations, if necessary, in the event of an emergency or to correct unsafe
work practices.
11. Reviews project health and safety plan and signs acceptance form.
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4.3 Manager, Health and Safety (H&H)
The Manager, Health & Safety (MH&S) shall:
1. Determine the need for periodic audits of the operation to evaluate compliance with this plan.
2. Provide health and safety support as requested by the SSO and PM.
4.4 Project Personnel (H&H)
Project personnel involved in on -site investigations and operations are responsible for:
1. Taking reasonable precautions to prevent injury to themselves and to their fellow employees.
2. Performing only those tasks that they believe they can do safely, and immediately reporting
any accidents and/or unsafe conditions to the SSO and/or PM.
3. Implementing the procedures set forth in the Health and Safety Plan, and reporting deviations
from the procedures described in the Plan to the SSO and/or PM for action.
4. Notifying the PM and SSO of any special medical problems (i.e., allergies) and seeing that
on -site H&H personnel are aware of any such problems.
5. Reviews project health and safety plan and signs acceptance form.
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4.5 Subcontractor's Safety Representative
Each subcontractor is required to designate a Subcontractor's Safety Representative (SSR), who
is the subcontractor supervisor. The SSR is responsible for the safe and healthful performance of
work by his work force and subcontractors. During the subcontractor's activities on -site, the
SSR will perform continuing work area inspections, and conduct safety meetings and safety
orientations for all new employees. The SSR will attend periodic safety meetings with the SSO.
The SSR will also investigate accidents and overexposures involving subcontractor personnel.
4.6 Subcontractor Personnel
H&H will insist on the following health and safety requirements from its subcontractors:
• Subcontractor employees must have appropriate training [i.e., either a 40-hour or 24-hour
OSHA -required (29 CFR 1910.120) health and safety course for hazardous waste work, or
certified equivalent training].
• Personnel working at hazardous waste sites must have had an annual physical (or physician's
waiver for biennial physical) and be certified "fit for duty" and "fit for respirator use," if
necessary, by a qualified physician.
• Upon request H&H will obtain proof of both training and a physical before site work may
begin.
• Personnel must have appropriate personal protective equipment (PPE) for the specific job.
At a minimum, personnel should have the following equipment:
— Hard hat
— Safety shoes
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— Gloves
— Goggles/safety glasses
— Hearing protection, if appropriate
— Respiratory protection, if appropriate (with fit test)
— Other equipment as specified by the HSP.
• Drilling equipment and field operations must meet applicable safety standards and satisfy
H&H's field inspection. Unsafe equipment or operations will necessitate shut down of the
job at a cost to the subcontractor.
Before field activities begin, the subcontractor must develop a health and safety plan. H&H will
provide a copy of its health and safety plan, but this is not a substitute for an independent plan by
the subcontractor. If the subcontractor has not developed a site -specific health and safety plan,
H&H will assist the subcontractor in preparing its own separate, site -specific HSP for
implementation by the subcontractor. The subcontractor must agree to comply with at least the
minimum requirements of its own site -specific HSP, be responsible for the health and safety of
its own employees, and sign the Subcontractor Statement of Compliance (see Appendix A of this
Plan) for all on -site employees before site work begins. The subcontractor also must agree that it
will take any additional measures it deems necessary to meet at least minimum applicable health
and safety standards if unforeseen circumstances arise.
The subcontractor will provide at least minimum safety equipment as required by the site -
specific HSP. When respirators are necessary, the subcontractor will provide a respirator fit test
certificate and a physician's "fit for respirator use" declaration upon request.
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5.0 Job Hazard Analysis
The primary environmental hazards anticipated for assessment at the Planters Oil Mill site are
potential exposures to VOCs particularly hexane, SVOCs, pesticides, PCBs, and metals. Other
hazards may include physical hazards due to lifting, use of tools and heavy equipment, use of
drilling equipment and drill rigs, excavation, electrical hazards, traffic hazards, and physical
hazards associated with recent demolition of structures at the site. Based on available data, the
most probable contaminants of concern at the facility include hexane, petroleum
hydrocarbons, metals, pesticides, PCBs, nitrates.
While the exposures anticipated from these materials during assessment and sampling activities
are expected to be minimal, and not all of the above contaminants are necessarily expected to be
encountered at the site, the provisions of this plan are directed toward helping to ensure that
potential exposures are minimized during site activities. When necessary, field sampling
personnel will wear NIOSH-approved air -purifying respirators with combination HEPA and
organic vapor filters as warranted by site conditions and sampling procedures.
Physical hazards at this work site include those associated with:
— heat stress and cold stress;
— slip -trip -fall type of accidents;
— back injuries due to improper lifting;
— being caught in or struck by moving equipment; and
— electrocution or explosion hazards associated with drilling or excavation activities or while
working on equipment.
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5.1 Heat Stress and Cold Stress Recognition and Control
The wearing of Personal Protective Equipment (PPE) can place a hazardous waste worker at
considerable risk of developing heat stress. This can result in health effects ranging from
transient heat fatigue to serious illness or death. Heat stress is caused by a number of interacting
factors, including environmental conditions, clothing, workload, and the individual
characteristics of the worker. Because heat stress is probably one of the most common (and
potentially serious) illnesses at hazardous waste sites, regular monitoring and other preventive
precautions are vital.
Heat stress monitoring should commence when personnel are wearing PPE, including Tyvek-
type coveralls, and the ambient temperature exceeds 70°F. If standard work garments (cotton
coveralls) are worn, monitoring should commence at 85°F.
Protection against cold stress should be initiated when temperatures drop below 45°F.
5.2 Chemical Hazards
From an occupational health standpoint, given that potential exposure to site personnel will be
only for a short period of time (intermittent for several days), the levels of contaminants
expected at the site should not represent a significant concern. Overviews of the hazards
associated with exposure to the major potential compounds of concern are presented below in
terms of the following types of occupational exposure limits:
• PEL - Permissible Exposure Limit
• C - Ceiling
• TLV - Threshold Limit Value
• TLV-STEL - Short Term Exposure Limit
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OSHA Permissible Exposure Limits (PELs), ACGIH Threshold Limit Values (TLVs), and time
weighted averages (TWAs) are defined as concentrations for an 8-hour work day, 40-hour work
week to which almost all workers can be repeatedly exposed without suffering adverse health
effects.
Short Term Exposure Limit (STEL) is defined as the concentration to which workers can be
exposed for short time periods without irritation, tissue damage, or narcosis sufficient to likely
cause impairment of self -rescue or precipitate accidental injury. The STEL is a 15-minute time -
weighted average that should not be exceeded at any time during the work day.
A ceiling value (c) is a concentration that should not be exceeded at any time in any work day.
Air
Air
Compound
TWA (ppm)(,)
STEL
Air
IDLH (ppm)
Ceiling (ppm)
(ppm)
Benzene
0.5
2.5
--
500
Hexane
50
--
--
1,100
Parathion
0.1 mg/m3
--
--
10 mg/ m3
DDT
1 mg/m3
--
--
500 mg/m3
Arsenic and Inorganic
0.010 mg/m 3
--
--
5 mg/m 3
Compounds
Lead and Inorganic
0.05 mg/m 3
--
--
100 mg/m 3
Compounds
Ref NIOSH Pocket Guide and ACGIH TVLs and BEIs
(1) Compounds TWAs with units of mg/m3 are based on dust exposure
(L) Exposure by all routes should be carefully controlled to levels as low as possible
Benzene WAS 71-43-2)
Benzene is a central nervous system depressant. Symptoms include headache, nausea,
remors, and fatigue, but these do not typically occur until exposure concentrations are in
excess of 150 ppm. There is significant evidence that chronic exposures are carcinogenic
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causing a progressively malignant disease of blood -forming organs (leukemia). Benzene
is known to the State of California to cause cancer under the criteria of Proposition 65.
Benzene is poorly absorbed through intact skin, but contact with liquid benzene may
cause blistering and dermatitis. Benzene vapors can cause transient eye irritation. The
mean air odor threshold for benzene is 34 ppm, which yields unsatisfactory warning
properties. Benzene's ionization potential (IP) is 9.25 eV.
Hexane WAS 110-54-3
Hexane is a colorless liquid with a gasoline -like odor. Hexane is highly flammable and
poses an extreme fire and explosion risk. Its flashpoint is -22' C and the range in
explosive limit is 1.1 to 7.5 % volume in air. The vapor generated from hexane is
heavier than air and can migrate along the ground with distant ignition possible. Hexane
can react with strong oxidizers posing a fire and explosion hazard. Hexane inhalation can
cause mild irritation of the eyes, nose, throat and respiratory tract. Inhalation of the
contaminant should be kept below the TWA of 50 ppm. The OSHA PEL is 500 ppm on a
time -weighted average basis. Acute exposure to high concentrations can lead to severe
central nervous system depression, respiratory arrest and death. Hexane can also be
absorbed through the skin and is a strong skin irritant.
Parathion WAS 56-38-2
Parathion is an organophosphorus compound used as an insecticide and an acaricide. It
is a pale yellow to brown liquid with a garlic -like odor. Parathion is absorbed by dermal,
inhalation and ingestion exposure routes. Parathion exposure can lead to headaches,
convulsions, impaired vision, vomiting, abdominal pain and unconsciousness. It is
incompatible with strong oxidizers and alkaline materials.
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DDT WAS 50-29-3
DDT, a pesticide, is either colorless crystals or an off-white powder in its pure form.
DDT has an aromatic odor, and is a known carcinogen. Exposure to DDT can be from
inhalation, absorption, ingestion and contact and impacts the eyes, skin, central nervous
system, kidneys and liver. Symptoms of exposure include irritation to the eyes or skin,
paresthesia to the tongue, lips or face, tremors, anxiety, dizziness, feeling of confusion or
discomfort, headache, weakness or exhaustion, convulsions, partial paralysis of the hands
or vomiting. If large concentration is inhaled, provide fresh air. Provide immediate
medical attention if breathing ever ceases.
Arsenic and Inorganic Compounds WAS 7440-38-2
Arsenic is a naturally occurring element and a known human carcinogen. Breathing high
concentrations of inorganic arsenic can cause sore throat or irritated lungs. Ingestion of
high levels of inorganic arsenic can result in death. Lower levels of arsenic can cause
nausea and vomiting, decreased production of red and white blood cells, abnormal heart
rhythm, damage to blood vessels, and a sensation of "pins and needles" in hands and feet.
Acute exposure by inhalation or ingestion may cause a darkening of the skin and
appearance of small "corns" or "warts" on the palms, soles, and torso. Skin contact with
inorganic arsenic may cause redness and swelling. Several studies have shown that
inorganic arsenic can increase the risk of lung, skin, bladder, liver, kidney, and prostate
cancer.
Lead and Inorganic Compounds WAS 7439-92-1
Acute lead poisoning usually manifests as gastroenteritis. Lead accumulates in the body;
chronic lead poisoning is manifested by anemia, constipation, and abdominal pain.
Accumulation in the peripheral nerves leads to wrist and ankle drop. Lead enters the
body primarily by inhalation. In the respiratory tract, most lead compounds are absorbed
rapidly and stored in nerve tissue so that poisoning can develop from long-term exposure
to low doses. Poisoning can also develop slowly from ingestion via lead -contaminated
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food, drink or tobacco products. Prevention of lead poisoning is almost entirely a matter
of good personal hygiene and housekeeping.
The following potential exposures may exist at the site:
• Skin contact with contaminated materials (soil, water);
• Inhalation of vapors or particulates; and
• Ingestion of contaminated materials; especially if poor personal hygiene is practiced.
Skin contact with potentially contaminated soil or water will be minimized by the use of
personal protective clothing (as described in Section 7.0). Inhalation of vapors or particulates
during the sampling activities will be minimized by air monitoring and the use of engineering
controls and respiratory protection if action levels (see Section 6.1) are exceeded. Ingestion of
contaminated materials will be minimized by the use of appropriate personal hygiene procedures
during decontamination (i.e., thoroughly washing face and hands with soap and water after
leaving the work area and prior to eating or drinking).
5.3 Noise Hazards
The primary noise hazard at this site is from drilling equipment. Previous surveys indicate that
such equipment may produce continuous and impact noise at or above the action level of 85 dba.
All H&H personnel within 25 feet of operating equipment shall wear hearing protective devices
(either muffs or plugs). Personnel will wash their hands with soap and water prior to inserting
ear plugs to avoid initiating ear infections.
5.4 Underground Utilities (Pre -Drilling Protocol)
H&H will locate underground utility locations prior to the commencement of drilling or
excavation activities. H&H will contact the North Carolina One -Call system (800-632-4949) to
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have all public utility services marked. H&H will also work with the City of Rocky Mount, the
current property owner, to aid in identification of underground utilities at the site.
5.5 Work Area Protection (Traffic Control)
The Planters Oil Mill site is in an active traffic area, however work will likely be done at a
distance from the street, therefore the potential for significant on -site traffic concerns is low.
Nevertheless, traffic control may be needed based upon certain site conditions or during specific
tasks to protect site workers. In general, personnel working in areas of traffic concern will
utilize safety vests and cones. Since the site is an open area, traffic cones will be utilized to
increase visibility of the work area.
5.6 Hazard Communication
The H&H Hazard Communication Program complies with the OSHA Hazard Communication
Standard (HCS) found in 29 CFR 1910.1200 and 29 CFR 1926.59, which applies to any
chemical present in the workplace in such a manner that employees may be exposed under
normal conditions of use or in a foreseeable emergency. Although waste materials are excluded
from the OSHA requirement, decontamination chemicals for sampling apparatus or protective
clothing (such as acetone) and calibration standards (such as isobutylene gas) require Material
Safety Data Sheets (MSDSs).
The principle of communicating the hazards of materials used in the workplace to employees
applies broadly to firm -wide activities, from informational programs on the conduct of hazardous
waste activities to the firm's insistence upon adequate safety and health training. It is also
important for personnel to have an awareness of client concern for Hazard Communication due
to Federal, state, and local regulations directly affecting certain client activities.
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In order to comply with Hazard Communication Standard (29 CFR 1910.1200), H&H has
determined that:
• Containers of hazardous chemicals must be appropriately labeled or tagged to identify the
hazard and provide information on effects and appropriate protective measures.
• Labels, tags, or signs must be properly affixed and visible at all times while a hazard is
present and removed promptly when the hazard no longer exists.
• Written information (MSDS) on hazardous chemicals in the workplace must be available to
employees working with the substance.
• Appropriate MSDS will be available to any contractor or subcontractor employees working
in H&H offices or at construction, excavation, or other sites under H&H's control.
• Hazard Communication Training will be provided to H&H employees.
5.7 Heavy Equipment
Operation of heavy equipment in drilling, excavation or other activities presents potential
physical hazards to personnel. The following precautions shall be observed whenever heavy
equipment is in use:
• Personal protective equipment (PPE) such as steel -toed shoes, safety glasses or goggles, and
hard hats shall be worn whenever such equipment is present.
• Personnel should at all times be aware of the location and operation of heavy equipment, and
take precautions to avoid getting in the way of its operation. Never assume that the
equipment operator sees you; make eye contact and use hand signals to inform the operator
of your intent.
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• Never walk directly in back of, or to the side of, heavy equipment without the operator's
knowledge.
• When an equipment operator must operate in tight quarters, the equipment subcontractor
should provide a person to assist in guiding the operator's movements.
• Keep all non -essential personnel out of the work area.
• All heavy equipment that is used in the exclusion zone should remain in that zone until its
task is completed. The equipment subcontractor should decontaminate such equipment in the
designated equipment decontamination area as required.
5.8 Electrical Equipment/Lock Out -Tag Out
It is not anticipated that lock out -tag out procedures will be required for these work activities.
However, maintenance or repair of equipment could potentially involve electrical equipment
such as motors, control panels, motor starters, etc. When working on electrical equipment
appropriate lock out -tag out procedures should be followed to ensure that the equipment is not
energized. This procedure involves de -energizing the system at the control/breaker panel and
then locking or tagging the panel to prevent inadvertently energizing the system during repair
activities.
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5.9 Structural Hazards
Several of the above -grade structures at the Planters Oil Mill site are in poor condition.
However, the City of Rocky Mount is in the process of demolishing these structures, including
the three large -capacity seed tanks. In addition there are several sub -surface sumps or open pit
structures at the site from previous operations. Care will be taken to avoid these structures.
Near the former hexane use area where demolition activities have already occurred, the ground
surface is uneven and riddled with partially filled in holes. Some of the Phase II tasks are
planned in these areas. The area will be reviewed with the subcontractor to confirm site access is
possible in these areas with planned equipment. If not, contingent means of obtaining samples in
these areas will be implemented.
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6.0 Exposure Monitoring Plan
Heat stress, noise, and chemical exposures are site hazards which may require monitoring. Heat
stress monitoring and prevention is addressed in Section 5.0. Noise levels will generally not be
monitored; H&H personnel will wear hearing protection as described in Section 5.3. Chemical
exposure monitoring is discussed below.
6.1 Chemical Exposure Monitoring
Field instrumentation described in this subsection has been selected for the contaminants that
may be reasonably anticipated to be encountered during the course of this project. Selection
factors include anticipated airborne concentrations, potential interferences, ionization potentials,
instrument sensitivity, and occupational exposure limits. The action levels described below are
established with the expectation that these specific instruments will be used. Do not substitute
instruments without the consent of the PM or the MH&S.
An explosimeter will be used to monitor periodically for hexane vapors when working in the
former hexane use and storage area.
A Photoionization Detector (PID) will be used to monitor intermittently for hydrocarbon vapors.
If readings exceed an average of 0.5 ppm above background for more than one minute,
monitoring in the operator's breathing zone (OBZ) of the person working nearest the borehole
will start and personnel will don protective clothing as described in Section 7.0.
An OBZ reading steadily above 0.5 ppm for more than one minute will require the use of full -
face respirators with organic vapor cartridges. If the PID reads more than 20 ppm
instantaneously (>5 seconds) or 10 ppm for more than one minute, work will stop, and workers
will move upwind while the vapors dissipate; if elevated levels remain for more than five
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minutes, the boring and cuttings will be covered with clean soil or plastic sheeting and the
MH&S and/or PM will be contacted for further guidance.
A summary of the response criteria is presented below.
(OBZ - Operator's Breathing Zone)
Analvzer Reading* Location Time Period Action
< 0.5 ppm
Borehole/
----------
Continue periodic
excavation
monitoring.
> 0.5 ppm
Borehole/
>1 minute
Monitor OBZ; don
excavation
protective clothing as
described in 7.0; establish
work zones described in 8.1.
< 0.5 ppm
OBZ
----------
No respirators required.
> 0.5 ppm
OBZ
>1 minute
Full -face respirators with
HEPA/organic vapor
cartridges; establish decon
area as described in 9.0.
> 10 ppm
OBZ
>1 minute
Stop work; move upwind
while vapors dissipate. If
OR
elevated levels remain,
cover boring and cuttings,
> 20 ppm
OBZ
instantaneous
evacuate upwind and notify
MH&S or PM.
* Above background readings
6.2 Background Readings
All direct -reading instrument readings will be evaluated relative to background readings, not
"meter zero". Prior to the start of work at each shift, and whenever there is a significant shift in
wind direction, instrument readings will be obtained upwind of the site work zone in order to
determine the level of "background" readings from local vehicle traffic, emissions from nearby
operations unrelated to the site, etc. Site readings will be evaluated against these background
readings (i.e., if an action level is listed as 20 ppm, it is evaluated as 20 ppm above background).
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6.3 Data Logging
Exposure monitoring data, including background readings, will be logged in the field log book.
The results of daily instrument calibrations can either be logged on the form provided in
Appendix E or in the field log book. Monitoring instruments will be calibrated in accordance
with the manufacturer's instructions. Calibration should also be performed when inconsistent or
erratic readings are obtained.
6.4 Dust Control
Elevated levels of organic contaminants may be present at the site. Airborne exposure could
potentially occur to the organics identified in Section 5.2 of this Plan during excavation or
drilling operations. If excavation or drilling operations generate sustained visible dust, a water
mist may be applied to reduce dust generation. If the mist is not effective in reducing dust
generation or this is impractical, personnel will don respirators (full -face as appropriate for
analyzer readings) with combination organic vapor-HEPA cartridges (such as North's organic
vapor/particulate cartridges).
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7.0 Personal Protective Equipment
Minimum Protective Equipment for Site Personnel:
• Hardhat
• Safety glasses
• Steel -toed boots
Work/Exclusion Zone Requirements:
• Hardhat
• Eye protection (face shield or safety glasses)
• Chemical -resistant steel -toed boots
• Ear protection in vicinity of drilling/remediation equipment
• Cotton coveralls (optional)
• Nitrile/latex/vinyl gloves (as needed for chemical protection)
If the analyzer reading is greater than the action level prescribed in Section 6.1 of this plan in the
work area for more than one minute or if dusty conditions are present, add:
• Tyvek coveralls (use poly -coated Tyvek if significant liquid contact is expected)
If the analyzer reading is greater than the action level prescribed in Section 6.1 of this plan in the
OBZ for more than one minute, add:
• Full -face respirator with combination organic vapor and HEPA cartridges.
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7.1 Limitations of Protective Clothing
The protective equipment ensembles selected for this project are anticipated to provide
protection against the types and concentrations of hazardous materials that may potentially be
encountered during field operations. However, no protective garment, glove or boot is resistant
to all chemicals at any concentration; in fact, chemicals may continue to permeate or degrade a
garment even after the source of contamination is removed.
In order to obtain optimum usage from PPE, the following procedures are to be followed by all
H&H personnel:
• When using disposable coveralls, don a clean, new garment after each rest break or at the
beginning of each shift;
• Inspect all clothing, gloves and boots both prior to and during use for:
— Imperfect seams
— Non -uniform coatings
— Tears
— Poorly functioning closures
• Inspect reusable garments, boots and gloves both prior to and during use for:
— Visible signs of chemical permeation such as swelling, discoloration, stiffness or
brittleness
— Cracks or any signs of puncture or abrasion
• Reusable garments exhibiting such characteristics will be discarded.
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7.2 Duration of Work Tasks
The duration of work tasks in which personnel use PPE ensembles that include chemical
protective clothing (including uncoated Tyvek) will be established by the SSO. Variables to be
considered include ambient temperature and other weather conditions, the capacity of individual
personnel to work in the required level of PPE in heat and cold, and the limitations of specific
PPE ensembles. The minimum rest breaks are as follows:
• Fifteen minutes midway between shift startup and lunch
• Lunch break (30 to 60 minutes)
• Fifteen minutes midway between lunch and shift end
Rest breaks are to be taken in the support zone or other clean area after personnel have
completed the decontamination process, including soap and water wash of hands and face.
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8.0 Site Control
8.1 General
The purpose of site control is to minimize potential contamination of workers, protect the public
from the site's hazards, and prevent vandalism. Site control is especially important in emergency
situations. When necessary, several site control procedures will be implemented to reduce
worker and public exposure to chemical, physical, biological, and safety hazards.
Barricades and barricade tape should be used to delineate a work zone for safety purposes
around the work area. The barriers should be set in a 25-foot radius (as practical) around the
work area to provide sufficient maneuvering space for personnel and equipment. A short piece
of barricade tape can be affixed to a secure upright or drill rig mast to serve as a wind -direction
tell -tale. A five-foot opening in the barricades at the support zone (upwind of the work area) will
serve as the personnel and equipment entry and exit point. The personnel decontamination
station will be established at this point if formal decontamination procedures are required (see
Section 9.0). Entry to and exit from the work area will be made at this opening in order to
control potential sources of contamination and leave contaminated soil and debris in the work
area.
At the end of the shift, all boring/sampling holes and excavations must be covered or otherwise
secured. Cuttings and decontamination fluids are to be handled in accordance with relevant
regulations and instructions from the PM. For this project, soil and ground water will be
containerized in 55-gallon drums.
The PM or SSO will determine an upwind evacuation area prior to each shift, and personnel will
be notified of its location. A horn or other signaling device will be used to signal an evacuation
in the event of an emergency. Three blasts of the horn will be the signal to immediately stop
work and proceed to the evacuation area.
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The SSO will log site visitors in the field log book. The SSO will provide site hazard and
emergency action information to site visitors before they enter the site; this can be done by
providing a copy of this SSP to the visitor.
8.2 Work Zones
If PID readings exceed the first criteria in Section 6.1, requiring the use of chemical protective
equipment, work zones must be established as described below. This criterion is listed in
Section 6.1 of this Plan.
• Exclusion Zone - a 25 ft (as practical) circle around the work area will be defined before
work starts. The encircled area will constitute the 'Exclusion Zone". This zone is where
potentially hazardous contaminants and physical hazards to the workers will be contained.
Full personal protection will be required in this area. Plastic sheeting (visqueen) and/or tarps
may be used as necessary to control cuttings spilled to the ground during drilling or other
operations. The size of the Exclusion Zone may be altered to accommodate site conditions
and to ensure contaminant containment.
• Contamination Reduction Zone (CRZ) - a corridor leading from the Exclusion Zone will be
defined, and will lead from the work area to a break area. Decontamination activities will
occur in the CRZ. A waste container will be placed at the end of the corridor so
contaminated disposal equipment can be placed inside and covered. Surface/soil
contamination in this area should be controlled using plastic sheeting. No H&H personnel
will be permitted into the Contamination Reduction Zone or Exclusion Zone unless they are
in compliance with the requirements of this Plan.
• Support Zone - a Support Zone, the outermost part of the site, must be defined for each field
activity. Support equipment is located in this uncontaminated or clean area. Normal work
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clothes are appropriate within this zone. The location of this zone depends on factors such as
accessibility, wind direction (upwind of work area), and resources (i.e., roads, shelter,
utilities).
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9.0 Decontamination Procedures
The following steps will be followed whenever personnel leave the exclusion zone/work area (as
appropriate):
1. Remove equipment, sample containers, and notes to the CRZ. Using decontamination
solutions decon shovels, auger flights, etc. by brushing them under a water rinse. A high-
pressure steam cleaner may also be used for decon. Waste and spent decon solutions will
be properly contained.
2. Scrub boots and gloves with a stiff bristle brush and water. Washtubs and chairs will be
provided.
3. Remove outer gloves (and boot covers, if used).
4. Remove Tyvek coverall; discard in provided container.
5. Remove hardhat and eye protection.
6. Remove respirator.
7. Remove inner gloves.
8. Wash hands and face.
The decontamination area will be covered with plastic sheeting which will be replaced when torn
or heavily soiled, and at the end of each shift.
Each worker will be responsible for cleaning, sanitizing and storing their own respirator in
accordance with manufacturer's guidance (i.e., washing in warm water and detergent or
sanitizing solution, air drying, and storing in a plastic storage bag; see Attachments). Cartridges
will be changed when breakthrough occurs (detection of organic vapor odor while wearing the
respirator) and at the end of each shift. Respirators will be kept in storage bags or boxes when
not in use.
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All spent decontamination fluids (rinse waters, etc.) shall be handled as directed by the PM and
in accordance with relevant regulations.
9.1 Sanitation
Potable water will be made available at the site, either from a pressurized source or
commercially available bottled water. Drinking cups will be supplied so personnel will neither
drink directly from the source of water nor have to share drinking cups. Sources of non -potable
water shall be clearly labeled as such.
Toilet facilities are not available on site. However, transportation is readily available to
transport personnel to nearby (within five minutes) toilet facilities. Therefore, portable toilet
facilities will not be provided on site.
Washing facilities will be provided on site, and will be located in the decontamination area or the
support area. Soap, clean water, wash basins and single -use towels will be available for
personnel use.
9.2 Decontamination -Medical Emergencies
In the event of physical injury or other serious medical concerns, immediate first -aid is to be
administered in lieu of further decontamination efforts.
9.3 Decontamination of Tools
When all work activities have been completed, contaminated tools used by H&H personnel will
be either completely decontaminated or properly disposed of.
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It is expected that all tools will be constructed of non -porous, non -absorbent materials. This will
aid the decontamination process. Any tool, or part of a tool, which is made of a
porous/absorbent material will be discarded and disposed if it cannot be properly
decontaminated.
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10.0 Safe Work Practices
10.1 General
1. Eating, drinking, chewing gum or tobacco, and smoking are prohibited in the contaminated
or potentially contaminated area or where the possibility for the transfer of contamination
exists.
2. If established, personnel will enter designated work areas only through the contamination
reduction zone (CRZ). All personnel leaving an exclusion/work zone must exit through the
CRZ and pass through the decontamination station as described in 9.0.
3. Personnel will wash their hands and face thoroughly with soap and water prior to eating,
drinking or smoking.
4. Avoid contact with potentially contaminated substances. Do not walk through puddles,
pools, mud, etc. Avoid, whenever possible, kneeling on the ground, leaning or sitting on
equipment or ground. Do not place monitoring equipment on potentially contaminated
surfaces (i.e., ground, etc.).
5. Field crew members should make use of their senses to alert them to potentially dangerous
situations in which they should not become involved (i.e., presence of strong, irritating or
nauseating odors).
6. Only those vehicles and equipment required to complete work tasks should be permitted
within the work zone (drill rigs, excavators, and similar items). Non -essential vehicles
should remain within the support zone.
7. Containers, such as drums, will be moved only with the proper equipment and will be
secured to prevent dropping or loss of control during transport.
8. Field survey instruments (i.e., PID) will be covered with plastic or similar covering to
minimize the potential for contamination.
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9. No matches or lighters will be permitted in the work area/exclusion zone or contamination
reduction zone.
10. Prevent, to the extent possible, spillages. In the event that a spillage occurs, contain liquid if
possible.
11. Prevent splashing of the contaminated materials.
12. Field crew members shall be familiar with the physical characteristics of investigations,
including:
— Wind direction in relation to contaminated area;
— Accessibility to equipment and vehicles;
— Communications;
— Hot zone (areas of known or suspected contamination);
— Site access; and
— Nearest water sources.
13. The number of personnel and equipment in the contaminated area should be minimized but
only to the extent consistent with workforce requirements of safe site operations.
14. Wastes generated during H&H and/or subcontractor activities at the site will be disposed as
directed by the PM.
15. All personal protective equipment will be used as specified and required.
16. The buddy system will be used at all times when performing sampling when the first action
level criteria has been exceeded or when working in remote areas.
17. Personnel are to immediately notify the SSO and/or PM if there are indications of potential
explosions or unusual conditions are observed.
18. No one wearing contact lenses or having a beard will be permitted in the work area if
respirators need to be worn.
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10.2 Sampling Practices
For all sampling activities, the following standard safety procedures shall be employed:
1. Sampling equipment should be cleaned before proceeding to the site.
2. At the sampling site, sampling equipment should be cleaned after each use.
3. Work in "cleaner" areas should be conducted first where practical.
4. All unauthorized personnel will remain outside exclusion zones at all times.
10.3 Health and Safety Equipment List
• Hardhats;
• Safety glasses;
• Ear plugs or muffs;
• Tyvek and polycoated Tyvek coveralls;
• Chemical resistant steel -toed boots;
• Work gloves;
• Nitrile gloves;
• Plastic sheeting (visqueen);
• 55 gal 17-H drums (for contaminated solids) and 17-E drums (for liquids);
• Barricade tape and cones;
• Wash tubs and scrub brushes;
• Decon solution;
• Folding chairs;
• 5 or 10 gallon portable eyewash (if one is not available on -site);
• First Aid kit;
• Drinking water;
• Gatorade or similar drink;
• Type ABC fire extinguishers;
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• Half -face or full -face respirators (NIOSH/MSHA approved);
• Organic vapor cartridges;
• Photoionization Detector (PID) and calibration kit;
• Explosimeter and calibration kit; and
• Tape.
40.4 Buddy System
Workers will conduct hazardous site activities with a buddy who is able to:
1. Provide his or her partner with assistance.
2. Observe his or her partner for signs of chemical or heat exposure.
3. Periodically check the integrity of his or her partner's protective clothing.
4. Notify the site supervisor if emergency help is needed.
5. Prearrange hand signals or other emergency communication signals as prescribed in Section
11.3 of this Plan.
Subcontractor personnel may be used to satisfy the buddy system.
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11.0 Emergency Response Plan
It is H&H's policy to evacuate personnel from areas involved in hazardous material emergencies
and to summon outside assistance from agencies with personnel trained to deal with the specific
emergency. This section outlines the procedures to be followed by H&H personnel in the event
of a site emergency. These procedures are to be reviewed during the on -site safety briefings
conducted by the SSO.
In the event of a fire or medical emergency, the numbers listed at the front of this Plan can be
called for assistance.
Hospital
The nearest public hospital to the Planters Oil Mill site is Nash General Hospital located at 2460
Curtis Ellis Drive in Rocky Mount, NC. The hospital is approximately 15 minutes from the job
site and the direct phone number is [phone]. See the hospital route map in Appendix B
for a map to the hospital.
Paramedics should be summoned to the site at 1004 Cokey Road, using 911 in the event of a
serious injury; they will arrange to transport the victim to the nearest appropriate facility. A first
aid kit will be available at the site for use in case of minor injuries. If anyone receives a splash
or particle in the eye, the portable eyewash will be used to irrigate the eye for 15 minutes. If
direct contact with contaminants occurs, affected skin areas should be washed immediately with
soap and water.
In the event of serious trauma or unknown chemical exposure, the employee should be stabilized
by one group of employees while the emergency phone number list is consulted and an
ambulance immediately requested.
Workers with suspected back or neck injuries are NOT to be moved until professional
emergency assistance arrives.
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11.1 Places of Refuge
In the event of a site emergency requiring evacuation, personnel will evacuate to a pre -
designated area located in the support zone, a safe distance from the work/exclusion zone. The
SSO will designate the assembly area prior to the start of work.
11.2 Fire
Type ABC fire extinguishers will be available on -site to contain and extinguish small fires. The
local fire department should be summoned to the site at the nearest building address using 911 in
the event of any fire on site. If it is safe to do so, site personnel may:
• Use fire -fighting equipment available on -site to control or extinguish the fire.
• Remove or isolate flammable or other hazardous materials that may contribute to the fire.
11.3 Communication
A communication network shall be set up to alert site personnel of emergencies and to summon
outside emergency assistance. Where voice communication is not feasible an alarm system (i.e.,
sirens, horns, etc.) should be set up to alert employees of emergencies. Radio communication
may also be used to communicate with personnel in the exclusion zone. Where phone service is
not readily available, radios or portable phones should be used to communicate with outside
agencies. Site personnel shall be trained on the use of the site emergency communication
network.
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The following hand signals will be used by personnel in the event of an emergency:
Signal
Hands clutching throat
Hands on top of head
Thumbs up
Thumbs down
Arms waving upright
Grip partner's wrist
11.4 Safety Eyewash
Definition
Out of air/can't breathe
Need assistance
OK/I'm all right/I understand
No/negative
Send back support
Exit area immediately
A safety eyewash will be available at the site for the sole purpose of flushing foreign particles or
contaminants out of eyes.
11.5 Incident Report
In the event of an injury or illness, work is to be stopped until the SSO, MH&S, and PM have
determined the cause of the incident and have taken the appropriate action. Any injury or illness,
regardless of severity, is to be reported on the accident report form (see Appendix Q.
11.6 Operation Shutdown
Under certain extreme hazardous situations the on -site personnel, SSO or PM may request that
site operations be temporarily suspended while the underlying hazard is corrected or controlled.
During operation shutdown, all personnel will be required to stand upwind to prevent exposure
to fugitive emissions. The SSO and PM will have ultimate authority for operations shutdown
and restart.
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11.7 Spill or Hazardous Materials Release
Small spills are immediately reported to the SSO and are dealt with according to chemical
manufacturers' recommended procedures. Spills or release of hazardous materials which result
in human exposure or off -site environmental contamination shall be promptly reported by the
PM or SSO to the client and appropriate measures shall be taken to contain and/or collect the
material for approved storage and disposal.
11.8 Emergency Medical Treatment Procedures
Personnel who become ill or injured in the Work/Exclusion Zone must be decontaminated to the
maximum extent possible. If the injury or illness is minor, decontamination should be completed
and first aid administered prior to transport. If the worker's condition is serious, partial
decontamination may be completed if the process would not further endanger the injured
personnel. First aid should be administered while awaiting an ambulance or paramedics. All
injuries and illnesses must be reported immediately to the PM.
Personnel who are transported to a clinic or hospital for treatment shall take with them
information on the chemical(s) they have been exposed to at the site. This information is
included in Section 5.2 of this Plan.
11.9 Community Safety
There is a low potential for migration of chemicals from the site as a result of project activities.
In the unlikely event that significant release of contaminants occur during the course of the field
work appropriate actions, such as contacting local fire/emergency response personnel using 911,
will be taken to protect the public health and mitigate the contaminant release.
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12.0 Training and Medical Surveillance
All H&H field personnel will have met the requirements of 29 CFR 1910.120 (e), including:
• Forty hours or initial off -site training or its recognized equivalent;
• Eight hours of annual refresher training for all personnel;
• Eight hours of supervisor training for personnel serving as Site Safety Officers;
• Three days of work activity under the supervision of a trained and experienced supervisor.
H&H site personnel are participating in medical surveillance programs that meet the
requirements of 29 CFR 1910.120(f). The MH&S will maintain current copies of training
certificates and statements of medical program participation for all site personnel.
In addition, all H&H site personnel will review this HSP and sign a copy of the safety plan
compliance agreement, which is found in the Attachments. The MH&S will maintain these
documents.
Prior to the start of operations at the site, the SSO will conduct a site safety briefing, which will
include all personnel involved in site operations. At this meeting, the SSO will discuss:
• Contents of this HSP;
• Types of hazards at the site and means for minimizing exposure to them;
• The type of monitoring that will be performed;
• Action levels for upgrade and downgrade of personal protective equipment;
• Personal protective equipment that will be used;
• Decontamination protocol;
• Site control measures, including safe operating practices and communication;
• Location and use of emergency equipment; and
• Evacuation signals and procedures.
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Subsequent site safety briefings will be conducted prior to each shift to review pertinent safety
issues, discuss any problems, and outline safety aspects of the shift's tasks.
For each briefing, the SSO will complete a Site Safety Briefing form (see Appendix D) and
maintain them in the project files.
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13.0 Recordkeeping
The PM and SSO are responsible for site recordkeeping. Prior to the start of work, they will
review this plan; if there are no changes to be made, the PM will sign the approval form and
forward a copy to the project file.
H&H personnel will review the HSP and sign the plan acceptance form in Appendix A; copies of
these forms will be maintained in the project file.
The SSO will conduct a Site Safety Briefing in accordance with Section 12.0 prior to each shift
and have all attendees sign the form in Appendix D; copies will be maintained in the project file.
An accident or exposure incident will be investigated and the form in Appendix C will be
completed and forwarded to the PM and MH&S. These will then be maintained in the project
file.
All instrument readings and calibrations, PPE use and changes, health and safety -related issues,
and deviations from this HSP will be recorded in the Field Log or the appropriate form (if
applicable).
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14.0 Toxic Snake and Insect Bites and Plants
14.1 Poisonous Snakebites
Reactions from snakebite are aggravated by acute fear and anxiety. Other factors that affect the
severity of local and general reaction from poisonous snakebite include: the amount of venom
injected and the speed of absorption of venom into the victim's circulation; the size of the victim;
protection from clothing, including shoes and gloves; quick antivenin therapy; and location of
the bite.
First Aid Procedure
The objective of first aid is to reduce the circulation of blood through the bite area, to delay
absorption of venom, to prevent aggravation of the local wound, and to sustain respiration.
The most important step is to get the snakebite victim to the hospital quickly. Meanwhile, take
the following first aid measures:
1. Keep the victim from moving around.
2. Keep the victim as calm as possible and preferably in a lying position.
3. Immobilize the bitten extremity and keep it at or below heart level. If the victim can reach a
hospital within 4 to 5 hours and if no symptoms develop, no further first aid measures need
be applied.
4. If mild -to -moderate symptoms develop, apply a constricting band 2 to 4 inches above the
bite, but not around a joint (the elbow, knee, wrist, or ankle) and not around the head, neck,
or trunk. The band should be 3/4 to 1 1/2 inches wide, not thin like a rubber band. The band
should be snug but loose enough for a finger to be slipped underneath. Watch out for
swelling. Loosen the band if it becomes too tight, but do not remove it. Periodically check
the pulse in the extremity beyond the bite to insure that the blood flow has not stopped.
45
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Several other factors must be considered in cases of snakebite:
• Shock. Keep the victim lying down and comfortable, and maintain his or her body
temperature.
• Breathing and heartbeat. If breathing stops, give mouth-to-mouth resuscitation. If breathing
stops and there is no pulse, perform cardiopulmonary resuscitation (CPR) if you have been
trained to do so.
• Identifying the snake. If you can kill the snake without risk or delay, bring it to the hospital
for identification, but exercise extreme caution in handling the snake.
• Cleaning the bitten area. You may wash the bitten area with soap and water and blot it dry
with sterile gauze. You may apply dressings and bandages, but only for a short period of
time.
• Medicine to relieve pain. Do not give the victim alcohol, sedatives, aspirin, or any medicine
containing aspirin. Some painkillers, however, may be given. Consult a doctor or other
medical personnel for specific medications that may be used.
• Snakebite kits. Keep a kit accessible for all outings in primitive areas or areas known or
suspected to be snake -infested.
It is not recommended that cold compresses, ice, dry ice, chemical ice packs, spray refrigerants,
or other methods of cold therapy be used in the first aid treatment of snakebite.
14.2 Poisonous Insect Bites
Spiders
Spiders in the United States are generally harmless, with two notable exceptions: the Black
Widow spider (Latrodectus Mactans) and the Brown Recluse or violin spider (Lox Osceles
Reclusa).
46
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The symptoms of a Black Widow spider bite are: slight local reaction, severe pain produced by
nerve toxin, profuse sweating, nausea, painful cramps in abdominal muscles, and difficulty in
breathing and speaking. Victims recover in almost all cases, but an occasional death is reported.
Symptoms are relatively similar for bites from the Brown Recluse.
Field personnel should exercise caution when lifting covers off manholes, sumps, etc., since
Black Widow and Brown Recluse spiders can typically be found in these areas.
Scorpions
Scorpions inject venom through a stinger in the tail. In bites from the more dangerous species,
there are marked systemic effects within 1 to 2 hours. Fatalities have been recorded.
The symptoms of a scorpion bite are: excruciating pain at the site of the sting, nausea and
vomiting, abdominal pain, shock, and possible development of convulsions and coma.
General First Aid for Poisonous Insect Bites:
1. Minor Bites and Stings
• Cold applications.
• Soothing lotions, such as calamine.
2. Severe Reactions
• Give artificial respiration if indicated.
• Apply a constricting band above the injection site on the victim's arm or leg (between the
site and the heart). Do not apply tightly. You should be able to slip your index finger
under the band when it is in place.
• Keep the affected part down, below the level of the victim's heart.
• If medical care is readily available, leave the band in place; otherwise, remove it after 30
minutes.
• Apply ice contained in a towel or plastic bag, or cold cloths, to the site of the sting or
bite.
47
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

• Give home medicine, such as aspirin, for pain.
• If the victim has a history of allergic reactions to insect bites or is subject to attacks of
hay fever or asthma, or if he or she is not promptly relieved of symptoms, call a physician
or take the victim immediately to the nearest location where medical treatment is
available. In a highly sensitive person, do not wait for symptoms to appear, since delay
can be fatal.
• In case of a bee sting, remove and discard the stinging apparatus and venom sac.
14.3 Tickborne Diseases
Lyme Disease
Lyme disease is an illness caused by a bacterium which may be transmitted by the bite of a tick
(Ixodes Dammini), commonly referred to as the "Deer Tick". The tick is about the size of a
sesame seed, as distinguished from the Dog Tick, which is significantly larger. The Deer Tick is
principally found along the Atlantic coast, living in grassy and wooded areas, and feeds on
mammals such as mice, shrews, birds, raccoons, opossums, deer, and humans. Not all ticks are
infected with the bacterium, however. When an infected tick bites, the bacterium is passed into
the bloodstream of the host, where it multiplies. The various stages and symptoms of the disease
are well recognized and, if detected early, can be treated with antibiotics.
Removal of ticks is best accomplished using small tweezers. Do not squeeze the tick's body.
Grasp it where the mouth parts enter the skin and tug gently, but not firmly, until it releases its
hold on the skin. Save the tick in a jar labeled with the date, body location of the bite, and the
place where it may have been acquired. Wipe the bite thoroughly with an antiseptic and seek
medical attention as soon as possible.
The illness typically occurs in the summer and is characterized by a slowly expanding red rash,
which develops a few days to a few weeks after the bite of an infected tick. This may be
accompanied by flu -like symptoms along with headache, stiff neck, fever, muscle aches, and/or
48
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

general malaise. At this stage treatment by a physician is usually effective; but, if left alone,
these early symptoms may disappear and more serious problems may follow. The most common
late symptom of the untreated disease is arthritis. Other problems which may occur include
meningitis and neurological and cardiac abnormalities. It is important to note that some people
do not get the characteristic rash but progress directly to the later manifestations. Treatment of
later symptoms is more difficult than early symptoms and is not always successful.
When in an area suspected of harboring ticks (grassy, bushy, or woodland area) the following
precautions can minimize the changes of being bitten by a tick:
1. Wear long pants and long-sleeved shirts that fit tightly at the ankles and wrists.
2. Wear light colored clothing so ticks can be easily spotted.
3. Wearing tick repellents may be useful.
4. Inspect clothing frequently while in tick habitat.
5. Inspect your head and body thoroughly when you return from the field.
6. Remove any attached ticks by tugging with tweezers where the tick's mouth parts enter the
skin. Do not squeeze or crush it.
Rocky Mountain Spotted Fever
In the eastern and southern United States this tickborne disease is transmitted by the infected
Dog Tick (Dermacentor Variabilis). It is important to note that the Dog Tick is significantly
larger than the Deer Tick. Nearly all cases of infection occur in the spring and summer,
generally several days after exposure to infected ticks. The onset of illness is abrupt and often
accompanied by high fever, headache, chills, and severe weakness. After the fourth day of fever,
victims develop a spotted pink rash that usually starts on the hands and feet and gradually
extends to most of the body. As with Lyme disease, early detection and treatment significantly
reduces the severity of illness. The disease responds to antibiotic therapy with tetracycline or
chloramphenicol.
49
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Other Tickbome Diseases
Ticks transmit several other diseases, most of which are rare and occur only in specific areas.
Babesiosis occurs mainly in the Cape Cod area and eastern Long Island. Colorado tick fever is
similarly regional and occurs only among those who live or work at altitudes above 4,000 feet.
14.4 Poisonous Plants
Characteristic Reactions
The majority of skin reactions following contact with offending plants are allergic in nature and
are characterized by general symptoms of headache and fever, itching, redness, and a rash.
Some of the most common and most severe allergic reactions result from contact with plants of
the Poison Ivy group including Poison Oak and Poison Sumac. The most distinctive features of
poison ivy and Poison Oak are their leaves, which are composed of three leaflets each. Both
plants also have greenish -white flowers and berries that grow in clusters. Such plants produce a
severe rash characterized by redness, blisters, swelling, and intense burning and itching. The
victim can also develop a high fever and become very ill. Ordinarily, the rash begins within a
few hours after exposure, but it may be delayed for 24 to 48 hours.
First Aid Procedure
1. Remove contaminated clothing.
2. Wash all exposed areas thoroughly with soap and water, followed by rubbing alcohol.
3. Apply calamine or other soothing skin lotion if the rash is mild.
4. Seek medical advice if a severe reaction occurs, or if there is a known history of previous
sensitivity.
50
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

15.0 Medical Surveillance
29 CFR 1910.120 requires employers to institute a medical surveillance program for employees
who are or may be exposed to hazardous substances at or above occupational exposure limits for
more than 30 days per year. Since it is not feasible to monitor every employee at every
potentially hazardous work site, H&H requires all employees whose work includes potential
exposure to hazardous substances to participate in its medical surveillance program.
H&H has in effect a Medical Surveillance Program that allows the Medical Review Officer
(MRO) to:
• Certify individuals to work at H&H sites as required by OSHA regulations;
• Establish a baseline against which any future changes in health or physical well being can be
evaluated;
• Identify underlying illnesses or conditions which might be aggravated by certain exposures
or job activities; and
• Recognize any abnormalities, toxic reactions, or other changes at the earliest opportunity so
that corrective measures may be taken.
No individual shall participate in H&H site activities in which a potential exposure or injury
could occur unless the MRO has determined that the individual is medically qualified to perform
field activities with potential for exposure to hazardous substances activities and medically
qualified to use respiratory protection.
51
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

16.0 Forms
The following forms will be provided to the SSO during final preparations for departure to the
job site:
• Daily Instrument Calibration Checksheet
• Plan Acceptance Form
• Accident/Exposure Report Form
• Site Safety Briefing Form.
All completed forms should be returned to the office for retention in project files.
52
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Appendix A
Safety Plan Compliance Agreement
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Appendix A
Safety Plan Compliance Agreement
for
Health and Safety Plan
Brownfield Assessments
Planters Oil Mill Site
Rocky Mount, North Carolina
I, , have received a copy of the Health and
Safety Plan for the Project. I have reviewed the plan, understand it, and agree to comply with all
of its provisions. I understand that I could be prohibited from working on the project for
violating any of the health and safety requirements specified in the plan.
Signed:
(Signature) (Date)
Firm: Hart & Hickman, PC
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Subcontractor
Statement of Compliance
This is to confirm that the employees listed below are qualified by virtue of training and
experience to engage in field activities at the Planters Oil Mill site in connection with
Contract/Subcontract Agreement between Hart & Hickman, PC and
, dated , 20 . Further, all said employees have been determined to
be properly trained and medically fit to perform those activities prescribed by said contract and
to use the respiratory protective equipment necessary to perform the job safely in accordance
with 29 CFR 1910 and 1926 and any other Federal, State, or local requirements.
1.
2.
3.
9
5.
Employee Names
6.
7.
8.
9.
10.
Authorized Subcontractor Representative
Printed Name
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Appendix B
Hospital Route Map
S:WAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

1004 Cokey lid Rocky Mt, N C '37801 to 2460 Curtis Ellis Dr_ Roely twit, IBC 27804 - Go--- Page 1 of 1
�� .]:art 1004 Cokey Rd fart �xing<, .1�}�, fl,}�{rilf (111f5M1.'
Rocky Mt, NC 27807
M'-p7 End 2460 Curtis Ellis Dr is '
Rocky Mt, NC 27804
Travel -6,9 mi — about 15 mins, up to 25 rains
in traffic
1004 Cokey Rd
Rocky MI, NC 27801
Drive: 6.9 mi — about 15 mins, up to 25 mins in traffic
1_ Head northwest on Cokey Rd toward Planters St
+- 2_ Turn left at Hill St
43. Turn right at NC-97
4 4_ Turn right to merge onto US-64 W
S. Take the Winstead Ave Ext exit
♦ 6_ Turn right at N Winstead Ave
+17_ Turn left at Curtis Ellis Dr
2460 Curtis Ellis Dr
Rocky Mt, NC 27804
N2T997M
0.7 mi a•7 0 4
2 rnlra �d
Orr
0.3 mi iuu
2 rnln F
1.5 mi {
4.0 mi
E rnlns Staff
0.2 mi '
O 1 ran
_ —
_ 611tr
;A i IOr
'ter l
These direct on s are for planniig purposes only_ You may find ghat conshWian project k ,
traffic, or othereuenis may pause rcad condffKmto differ horn the map resd[s.
Map data QMDT NAVTE0„
End
Map data d7 NAUTEQn`
http:r' niaps.goa,Frle.earn•'maps?f h1=en&geocode=434933544ISM103292,35.9760W--7... 1714l2007
S:WAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Appendix C
Accident/Exposure Report Form
S:WAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Hart & Hickman, PC
Accident/Exposure Report
EMPLOYEE NAME DATE OF BIRTH
HOME ADDRESS PHONE NO.
SEX: MALE FEMALE JOB TITLE SOC. SEC. NO.
OFFICE NO. _ OFFICE LOCATION DATE OF HIRE
HOURS USUALLY WORKED: HOURS PER DAY HOURS PER WEEK
TOTAL HOURS WEEKLY
WHERE DID ACCIDENT OR EXPOSURE OCCUR? (INCLUDE ADDRESS)
COUNTY ON EMPLOYER'S PREMISES? YES NO
WHAT WAS EMPLOYEE DOING WHEN INJURED? BE SPECIFIC)
HOW DID THE ACCIDENT OR EXPOSURE OCCUR? (DESCRIBE FULLY)
WHAT STEPS COULD BE TAKEN TO PREVENT SUCH AN OCCURRENCE?
OBJECT OR SUBSTANCE THAT DIRECTLY INJURED EMPLOYEE
DESCRIBE THE INJURY OR ILLNESS
PART OF BODY AFFECTED
S:WAA-Master Projects\City of Rocky Mount - CRWCRM-00 I Tlanters Oil Mill\Phase H\QAPP\POM H&SP.doc marr & trackman, ,vu

NAME AND ADDRESS OF PHYSICIAN
IF HOSPITALIZED, NAME AND ADDRESS OF HOSPITAL
DATE OF INJURY/ILLNESS TIME OF DAY
LOSS OF ONE OR MORE DAY OR WORK? YES/NO
IF YES, DATE LAST WORKED
HAS EMPLOYEE RETURNED TO WORK? IF YES, DATE RETURNED
DID EMPLOYEE DIE? IF YES, DATE
COMPLETED BY (PRINT)
SIGNATURE
TITLE DATE
AN ACCIDENT/EXPOSURE REPORT MUST BE COMPLETED BY THE PROJECT
MANAGER OR SITE SAFETY OFFICER IMMEDIATELY UPON LEARNING OF THE
INCIDENT. THE COMPLETED REPORT MUST BE IMMEDIATELY TRANSMITTED TO
THE MANAGER HEALTH & SAFETY.
S:WAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Appendix D
Site Safety Briefings
S:WAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Hart & Hickman, PC
SITE SAFETY BRIEFING
JOB NAME NUMBER
DATE START TIME COMPLETED
SITE LOCATION
TYPE OF WORK (GENERAL)
SAFETY ISSUES
TASK (THIS SHIFT)
PROTECTIVE CLOTHING/EQUIPMENT
CHEMICAL HAZARDS
PHYSICAL HAZARDS
CONTROL METHODS
SPECIAL EQUIPMENT/TECHNIQUES
NEAREST PHONE
HOSPITAL NAME/ADDRESS
SPECIAL TOPICS (INCIDENTS, ACTIONS TAKEN, ETC.)
S:WAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

ATTENDEES
PRINT NAME SIGN NAME
MEETING CONDUCTED BY:
S:WAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Appendix E
Daily Instrument Calibration Check Sheet
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Hart & Hickman, PC
Daily Instrument Calibration Check Sheet
PROJECT NAME:
PROJECT NUMBER:
INSTRUMENT(S):
SERIAL NO(S):
Date
Pure Air
(Y/N)
Calibration
Gas (PPM)
Battery Check
(Good/Bad)
Calibrated By:
Remarks
PROPER CALIBRATION OF INSTRUMENTS SHALL BE CONDUCTED IMMEDIATELY
PRIOR TO SITE ACTIVITIES. USING FELT TIP PENS/MARKERS OR SIMILAR ITEMS IS
NOT CONSIDERED PROPER CALIBRATION AND IS NOT ACCEPTABLE
S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-00I Tlanters Oil Mill\Phase II\QAPP\POM H&SP.doc Hart & Hickman, PC

Appendix C
Site Investigation Report for Permanent Closure or Change -in Service of UST Form
(UST-2 Form)
Hart & Hickman, PC

UST-2 Site Investigation Report for Permanent Closure or Change -in -Service of UST
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Send a copy to the Central Office in Raleigh so that
the status of the tank may be changed to "PERMANENTLY CLOSED" and your tank fee account can be closed out.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY:
I.D. #
Date Received
INSTRUCTIONS READ THIS FIRST
For more than five UST systems you may attach additional forms as needed.
Permanent closure - For permanent closure, complete all sections of this form.
Change -in-service - For change -in-service where UST systems will be converted from containing a regulated substance to storing a non -regulated
substance, complete sections I, ll, III, IV, and VIII
Effective February 1, 1995, all UST closure/change-in-service reports must be submitted in the format provided in the UST-12 form. UST closure and
change -in -services must be completed in accordance with the latest version of the Guidelines for Tank Closure. A copy of the UST-12 form and the
Guidelines for Tank Closure can be obtained at www-wastenotnc.org.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, LISTS are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
NOTE: If a release from the tank(s) has occurred, the site assessment portion of the tank closure must be conducted under the supervision of a P.E. or
L.G., with all closure site assessment reports bearing the signature and seal of the P.E. or L.G.
I. OWNERSHIP OF TANKS
II. LOCATION OF TANKS
Owner Name ( City of Rocky Rocky Mount,"NC Facility
Name or Company
Former Planters C€1 INA.11
Strees3iess �. S Franklin SSt Facility
ID # (If known) N/A _ Orphan LISTS
City Rocky Mount County EdgeCombe Street
Address 1004 COkey Rd
State North Carolina Zip Code 27802�-11YO City
Rocky Mount EdgeCOrnbe Zip Cod
e27801
Phone Number 252-972-1325 Phone
Number N/A _ Closed Facility
III. CONTACT PERSONNEL
Contact for Facility: Peter Varney
P
Job Title: Assistant City Manager
hone. No:S-? -/3ZS'
Closure Contractor Name:
7 _01 1 EQ
Closure Contractor Company:
E►/a ea,QOOA44770,41
Address: /7a3 ArP6•Z9r`e ,S"r, Phone.
Ale eon
No:
3 - ,
Primary Consultant Name:
G c owW,eiD /!1aW&-7 -Z
Primary Consultant Company:
41,41inr 14(11icx s0,4A1 �G
Address: 333.ENiLe-r1?0 VAOFT. Phone.
o1544E i ,t/c z 7lod 7
No:
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
I V. EXCAVATION CONDITION
Tank
ID No.
Size in
Gallons
Tank
Dimensions
Last
Contents
Last Use
Date
Permanent
Close Date
Change -in-
Service
Date
water in
excavation
Free
oduct
Notable odor or visible
soil contamination
Yes
No
Yes
No
Yes
No
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
1 ❑
❑
❑
❑
❑ I
❑
I ❑
❑
VI. UST INFORMATION
FOR UNREGISTERED UST SYSTEMS
VIE. EXCAVATION CONDITION
Tank
ID No.
Size in
Gallons
Tank
Dimensions
Last
Contents
Last Use
Date
Permanent Tank Owner
Close Date Name'
water in
excavation
Free
oduct
Notable odor or visible
soil contamination
Yes
No
Yes
No
Yes
No
001
20,000
gyp' '°x3l `4"
#6 F.0.
1983
03/08/11
✓❑ "
❑
❑
Rr
❑
C'
002
22,500
1,WjeS4'
Hexane
1983
03/08/11
in
❑
❑
CB,-"
❑
EEr
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
If the tank owner address is different from the one listed in Section I., then enter the street address, city, state, zip code and telephone no. below:
USTs ARE ORPHAN TANKS DISCOVERED ON THE PROPERTY
Vlll. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and
complete.
Print name and official title of owner or owner's authorized representative
Peter Varney, Assistant City Manager :1
Sign atu
Date Signed
3 yg . ll
UST-2 Rev 11/2006

Appendix D
Tank Disposal Certificate
Residuals Manifests
Residuals Certificates of Disposal
Hart & Hickman, PC

ENVIRONMENTAL AND INDUSTRIAL RESOURCES
1703 Vargrave Street
Winston-Salem, NC 27107
ph 336-725-5844
fax [phone]
-isgitir � 1 1
Tank Owner: City of Rocky Mount
Site Address: 1004 Cokey Road
Rocky Mount, NC
Description of Tanks:
Tank Number Size of Tank Contents
1 20,000 Gallons #6 Fuel Oil
2 20,000 Gallons Hexane
Transporter: Edwards Crane Service
EC Project #: 021110
Disposal Certification.
Evo Corporation does hereby certify that the above named storage tanks were
transported to American Metal Transfer in Elizabeth City, NC for proper disposal
and recycling.
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evocorp.netTHE NEXT LEVEL.

GNVERONMENIAL AND INDUS'I RIALRFSOURCES
'1703 vargrave Sireet
W 1ston-Salem, NO 27107
ph 336-725-5844
fax [phone]
Evo Corporation does hereby certify that 9,000 gallons of product received on
03/01 /2011 and 03/02/2011 from:
Generator: City of Rocky Mount
Originating at: 1004 Cokey Road
Rocky Mount, NC
EC Waste ID #: 021110
has been disposed of by Evo Corporation in a manner approved by the North
Carolina Department of Environment and Natural Resources.
Signature
Thomas W. Hammett
CEO
Eva Corporation
www.euocorp.netT L NEXT LEVEL.

--_...
NON-HAZAI?DOUS 9 S Y I g Nunber
WASTE MANIFEST 1. Generator lit Number 2. Pa e 1 of 3. Fmer ano Response # hono 4. Wasse'rracl;in
5. Generator's Name Mailing Address j'
and l (�( / ! , �)!
Generators 5idress (d different than mailing address)
Generator s Phone:
6. Transporter 1 Co Name
I lr`1� ,�,J[!'� IJ�.,�n !
�� EPA
anj
U.S. 19.14umber
7, Transporter 2 Company N rn
U.S. EPA ID Number
8. Designated Facility Name and Site Address j �,%
IM
�;���'
U.S, EPA ID Number
EE I oil,
Facilly s how 1). 1.�
9. Waste Shipping Name and Description
10. Containers
11. Totaf
12. Unit
No.
Type
Quantity
WLNOI,
/f//JTY�fY,
W'
(.jam' y11
3 iy 13� 9 u"Stl
I'G
1✓
W y
2.sfti�a5
r
3
4.
13. Special Handling Instructions and Additional Information
V
14. GENERATOR'S CERTIFICATION: I cedily the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste.
GeneratoyslOHeTor's
Printedffyped Name
Signature Month Day Year
H
15. In ernational Shipments
❑ Import to U.S. ❑ Export from U.S. Port of entry/exit:
z
Transporter Signature for exports only):
Date leaving U.S.:
W
W
18. Transporter Acknowledgment of Receipt of Materials
aTransporter
1 Printed/Typed Name /
Signature Month Day Year
a
Transporter 2 Printed/Pyped Name
Signature Month Day as
r
s
17, Discrepancy
17a. Discrepancy Indication Space
❑ Quantity _ El Type
❑Residue El Partial Rejection ❑ FuEI Rejection
Manifest Reference Number:
17b. Alternate Facility (or Generator)
U.S. EPA ID Number
U
ua.
Faci€itysPhone:
m
17c. Signature of Alternate Faci€ity (or Generator)
Month Day Year
a
z
''` - i isy3u�J', i ���� �� s' _� r^.- '.,,<1n '^'� r
6'�.a.: s, v"�',- ✓ �� �c'�y�}- � i���ry� ���SFr�} �2y� y��y i'�.a���"-,c,,Cq��f�'' �+Ff�N'` 3 j
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18. Designated Facility Owner or Operator: Certification of receipt of materials oovered by the manliest except as noted in Item 17a--
PrintedfTyped Name
Signature Month Day Year
169-BLC-0 5 11977 (Rev. 8/06) :: GENERATOR'S/SHIPPER'S INITIAL COPY

NON-HAZARbOUS 1' Generator ID Number 2. Pa e 1 of 3. f.mor enc ties �onse Phone 4. Waste 7racicin Number
11 tt
E k 1 4
WASTE MANIFEST
5. Generator's�Name and Mailing Address :. yy % ' i ��y
Generator's Site Addre S (€f d[Uereol than nailing address)
_ ,�/�
f
Phone: Zcn z, (
1 /
Generators
�
&..�nr sporter 1 C mpanyfN�a'�m/e,
U.S. EPA ID Number
7. Transporter 2 Company hame
j U.S. EPA ID Number
8. Designated Facility Name and Site Ad ess --
U.S. EPA lD Number
Fac€I€t 's Phone:
d. Waste Shipping Name and Description
10. Containers
11, Total
Quantity
12. Unit
Wt.Nol.
No.
Type
f••
aft`'
�.
!
(yam
�}C..•�1...�i✓'
�
'� Y jY;5
5
1
S
3.
r �'a
o�
4.
13. Spec#al Handling Instructions and Additional Information
f/1tJ 6 r 1Jj( 0
14. GENERATOR'S CERTIFICATION: I certify the materials described above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste.
Gen
tors/Ofteror s Prin dlTyped Name
Signature J ]] Month Day Year
jr
.j
j.,
15. International Shipments
❑ Import to U.S. Export from U.S. Port of enirylexil:
z
Transporter Signature Ifor exports on!
Date leaving U.S.:
cc
16. Transporter Acknowledgment of Receipt of Materials
h
Transporter 1 Printe ped Name
Signature / `Month Day Ylear
? I / I
QTranspoffor
-17�ti
2 Pr'rnted/Typed Name
Signature ' Month Day Year
nc
17. Discrepancy
17a, Discrepancy Indication Space
❑ Quantity ❑Type
❑Residue El Partial Rejection ❑ Full Rejection
Manilest Reference Number:
17b. Alternate Facility (or Generator)
U.S. EPA ID Number
�-t
rat
Facility's Phone:
w
17c. Signature of Alternate Facility (or Generator)
Month Day Year
a
(�
v '. g 1 3 _y. /:-3a'b'Xn:4,'t%`A'a`" =5� �
t !S - S ! h f lih� ��lr � �
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9'r'l.. Rt:&' .L=1��`E .,.i tit_'s,��;C,''S�=*-: 'Y' e"'a�t I �` 7fq <e' ��',�,.,"4� osy;.�•.vd�
t`G 'v4� -� ✓`;��L`'u'.J �' h3 L � LA i =i r �'i i-t �`%.,`` L:
r
18, Designated Facility Owner or Operator: Certification of receipt of materials covered by the manifest except as noted in Item 178
Printed)Typed Name
Signature Month Day Year
]]
169-BLC-0 6 11977 (Rev. 8/06). GENERATOR'S/SHIPPER'S INMAL COPY.—

NON-HAZARD0U5 1. Geneator ID Number
WASTE MANIFEST
k. Waste Tracking Number
2. Paye 1 0l 3. Emergency Respopnse Phoneiont
C q �
_l a f-�
-5Generator's
Name and Mailing Address Generators Site Address (ll dEfie111�al mailiirg�address)
Generators Phone: .
G. Transporter 1 Company Name
S. GP I umber
7. raWs. 2 4pq�y�.e
U.S. EPA ID Number
B. Designated Facility Name and Site Address
e1 I t # ,
_ U.S. EPA ID Number
TV Uf 4e,1S,
Facilit 's Phone:
9. Waste Shipping Name and Description
10. Containers
11. Total
Quantity
12. Unit
Wt.Nol.
No.
Type
1•
f s �` X'
w`
�
2.
C7
ply=�:'
��'i"F.$'e<i•�� . vS,;L.�
3.
13.. Special•Handling lostructions and Additional Information
14. GENERATOR'S CERTIFICATION: I cortify the materials doscdbed above on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste.
GeneratorsfOfferor`s Printed Typed Name
Signature Month Day Year
i
15. International Shipm nts
❑ Import to U.S. ❑, Export from U.S- Port of entry/exit:
—
Transporter Signature for exports on! :
Data leaving U.S.:
cc
16:'Transporter Acknowledgment of Receipt of Materials
LU
a
Transporter 1 PfintediTyped Name
Signature w _ Month Day Year
a
aTransporter
2 Printedfryped Name
Signature / Month Clay Year
GC
h
17. Discrepancy
17a, Discrepancy Indication Space
❑ Quantity El Type
El Residue ❑Partial Rejection El Full Rejection
Manifest Reference Number:
17b, Alternate Facility (or Generator)
U.S. EPA ID Number
.a
O
tat
Facility's Phone:
c2
17c. Signature of Alternate Facility (or Generator)
Month Day Year
a
z
ni
�
-Lry i��r• �f� ,,ci,,} v /try.
l � � f �'��•}�. � �p n CAR 5�.
at
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e �,e`' �����i�a..�F��,',��^F:. 3»,r��.r`�� m?•a.t}3i V3,'�?..,;,,� 'r �'�3�_t.,.<;.
16. Designated Facility Owner or Operator: Certification of receipt of materials covered by the manifest except as noted in Item 17a
Printedfryped Name
Signature Month Day Year
169-BLC-0 5 11977 (Rev. 8106) GENE RATOR'SISHI PPER'S INITIAL COPY `

4
I'M1110NMEN'IAL AND INDUMIAL RGSCURCCS
1703 uargrave Strout
Winston-Salem, NO 27107
ph 336-7215-5844
fax [phone]
Evo Corporation. does hereby certify that 5,895 gallons of non -hazardous
contaminated sludge received on 03/03/2011, 03/04/2011, 03/08/2011,
03/09/2011 and 03/22/201.1. from:
Generator: City of Rocky Mount
Originating at: 1004 Cokey Road
Rocky Mount, NC
EC Waste ID #: 021110
has been disposed of by Evo Corporation. in a mariner approved by the North
Carolina Department of Environment and Natural Resources.
Signature
Thomas W. Hammett
CEO
Evo Corporation
www.evocorp.net HE NEXT LEVEL.

1701 Vag rave St. r
Winston-Salem, NC 27107 www.hohco,l.p.com
NON -HAZARDOUS WASTE MAFMIFES
1�"
Generator:/._.....— �' r` Date: ✓ t _ -
Address:
— bon _ P e #: � / �
EPA ID#. a
Contati: Ito,
Process,wh:i.ch generatedwaste: I certify that the materials -,described below are:properly described, classified, packaged; marred acid
labeled, and are' m,prope.r"condition:to be transported in:commerce under the applicable regulations of the State; the EnvironMental:
Protection Agencyan'd the Depa ent of.Transportation. I:certify that the waste described belovu is non-hazardaiis ,.I.cerk{fy-that the
specific waste:was delivered to: he c tier amed below for legal. treatment,storage,'•or.disposal. at the site indicated:
Signature: Date
NAM E.-AIND/OR DESCRIPTION OF WASTE . ;QUANTITY . CIRCLE UNITS TVPE..1.RLSTYE .
(i e. 5 gaI pail '30 gal:
drum, '$5gal. drum,
i' 85 gal, over pack)
Lbs. Gallons / Drums/ -Totes / Tons / Cu. Yd: Bags
Lbs../ Gallons / .13rums / bites:%Tans /.'Cti Yd. fags -
%L Gallons /, Drums /Totes / Tiyns /,Cu. Yd Bags
1ps '/ Gallaris / Drrt s /.Totes / 7bns !:Cu- Yd. Bags
Lbs. / Gallons / pruiits /Totes /Tons / cu Yd. Sags
kbs. / Gallons :/ Drums /'Totes /'Tons / Cu.,Yd. Bags
Trar3spor#er: �3 77
Phone #:
EPA ID#:.
J. ,
ce thal• tll specWed senl %e / OH CorpnrO' and was accepted,
Ri U lver'i ` atGce to fDeliver' ;rive tore pate
- - F
(DO NOT WRITE BELOUN"THIS LINE),
Facility: MOH Corporations r:. CWT Permit #: 199W EPA ID#. NCR000012260 .
1701 Va rgrave" St:. ,
Winstow-Salem, NC 27107
FIA.NDLI6C`M`PTN0D. Q WAgrRWATER r•RfArXENT SDLi"L�ll GR�'xQN l.lISED;D LRECYCLING y' x
© PACKAGED1)WTdgNEC :GbOUS GRXNDIA,G • ' [ WA. 5T�-TD-EN f�GY.: OTHER. c
•"•I certify•that=thy*' Transparaer"ab.ove".delivered the specified material •to this facility -and was accepted and propedy:handled-in the�above
manner.
Signature: Date:
WHITE COPY-MON YELL:OW.COPYRETURN TGQ GENERATOR PINK COPY -TRANSPORTER; GOLDENROD COPY -GENERATOR.

336,727-4644'.
336 727-8940. finx
www.hohcorp,cam
1-cerfifyAhAf dej,50ibeM bailaWi,aM ly-,described,.t
qmMercewider
I cor e o1wis-nan
prdt AOA�L�ardous. Iry. *pt the
."q
I t th. or.. d P.0�6('A trcarhy d 'I f iega ttjjent.,,L_Stdra9 vr I --the,
spe�ff�c %4Aftd� :.'s� deliv.4 -.0z y. nar I tfea e �jbff.A"dicated.
....... ..... .. .. ........ . ..........
ONTAIftk
TITY
btk RMY104,6P WMU Q!JAN TS
50hipav, 30 gel
-opt, oh*
85
To Lbs -yd'jW1 tot Tons
gs
:
LK /i�s7
,I
L -b Yd:�
tatidn fags
;fo S:
7
j .
ranspor.
S%
EPA, Its. #
. . . . . . . . . . . . . .
60"d)., toC W-4s' xO#fod
o
Pit
IV
'260, A R000012
Tacility, Mtr#� 40.
01 N iogeavtj St..
Wi alift, NO 271
D WA$.r A-r-k
4 4 4"
nawrrutrNa'o��,r4rr�
CbrtYf
A0
-fh,�.wp, ftbtay.
d
IC
thatilhe
Tra
io ove delleted the .
. . . . . . . . . . . . . . . . .
4�
-4,
141TE Copv� kOn V_awwtov t �R-E Cj"
w

HOH COR[,,IORA'TXON
1701 Vargrave St.
Winston-Saiem, NC 27107
CQ116ct,
2 7 2 2 336- 727--4VM-.
336 727-8849; fax:
www.hohcorpxom
generated wa9te, A, ce . rtify..OM the-n . �atOrIalsAescri4od,4elaw are p�.bperly doscribed,-classifiel., packaqfed; :mavked .and
-ati'd 4- d
i�d ' he applicable regulations of the StAte: thd EnvOopmentaV
rej proper condition to be Ir.&,spoited'l. atnfnerce� under t. .
libbled,
the-Dbpartrftent of TreAnj4p
-.
Jo.'nP. . described. --I.L.I
..
shn"
n-haizarddus.I certify •that,the
po ier 'o"forl iWrpye,orjisos61atteMWtclicA6&
S!0Latwm
DO
CONTAT
AiW -AN
-F ,
1),'/OR Dt9CRWTION OFWAST-E,v QUANtl�, Y "PBr SIZE,
5#41 waft, -mok
dram, 55 ya1 divo,: .
pack .95 gA dyer
all6ft f6ri4i; f4as /Tofis Cu. Yd.,-Bags %� ; . r: Z4
Lbs.., af.[Ojns JJW44s j tk,69,1 Tons 7 Cu.,Y.d. bags
Lbs!-Jjjj;s) f flags
-7—GQ66s. Pro

HOH CORPORATION
1701 Vargrave St.
Winston-Salem, NC 27107
Generator:
Address:
Contact:
02./Ifs
336 727-3840 fax
vvvvw.hohcorp.com
D.
phollp
"` XD ll
,- a .� .d
Process, which generated. waste: I e that the, materials described below, are properly described, classified, packaged,: marked and
labeled, and are irr proper -condition o be: ansported in commerce under the applicable regulations of the the Environmental .
Protection Agency..and the D me of T nsportation.•.I,certify that the.. waste.dascribed,below is. non-hazardoius. I certify that:the
speciflaymsttwal delivered t th arri n med below for legal treatment; storage, r d"sposai.at.the:site=indicated.
Signature: _ Date:
CONTAINERS
NAME AND./OR DESCRIPTI N OF WASTE
QUANTITY
CIRCLE -UNITS .
:TYPE:& SIZE
(i e. 5 gal pail, 30 gal,
drum, 55 98/. drum,
85gal over/pack)
s,
:Lb,- ons Drums / Totes / Tons / Cu..Yd. Bags
_.
tabs: ] Gallons /Drams /Totes./ Tons /•,Cu..Yd..Bags:
Lbs. / Gallons. /Drums /Totes /Tans ] Cu. Yd.' "ags. .
Lbs. / Gallons / brums /: Totes,/ Tons / .Cu. Yd. Bags
Lbs. y Gallons] Drums / Totes / Tons, / Cu. Yd. Bag"s
Lbs. / Gallons / Drums /To tes / Tons / Cu. Yd. Bags
Transporter;
a�a�..`'
/ . Phone #:
Lr
} ERA ID#-
r erft that the-speciFedwaste was: [ransferredin a registered (licensed) .ehfc/e io HOH Corporation and was accepted.
Pickup Driver ignature Dat , .: Delivering Drivers Signature'
(DO NOT Wft TE BELOW THT9,LmCU
Facility: HOH Corporation-. CWT Permit #:.1998 EPA ID#: NGR000012260
1701 Vargrave St.
Winston-Salem, NC 27107 "
HANDLING METHOD: ❑ WAaTEl9/A:TER TREATMENT :pLIDIFICA7�TON . ❑ .USED UIf :RECYCL tNG
❑:PACKAGED1RErURNED000D54GRXNDrNG ❑ WAui- M ENERGY OTHER.
I.certifY that the ransporterabavo elivered the specified material to this facility and was accepted and<propedy handled in the above .
manner.
Signature: Date•
NSPORTER
WHITE COPY H YELLaW:C4i�Y-RETURN"TD.GEiVE12ATOR PINK CaPY'�TIiAiLDENROD CQPY-GENERAifbR

-HO"-CORPO RATION
1701 Vargrave St.
Winston-Salem, NC 27107
12702 336 727-4644
336 727-8840 fax
www.hohcorp.c6m
f
NO HAZARDG'US WASTM IFEST
- — - ko
Date:. ,L—
Generator:. .
Add s:-' - - Phnne#• 't
ERA ID#:
Contact:
.Process W.Hich �eneratdd-watte - ` ylth!et�.thd Fhaterlals descri,� d }}�ow--v pr erly y lescri6 , classifled; package t_mar[red And
lab¢led, and are in proper cn�riiirtioh. 'b tram ported`-fn' commerce'under`the applies le regulations of the 5tatk* the Environmental
PfoteCtjoq i g ncy:and ;the.D. ` en f.: ansportation: I cerki thai t ie waste descrilwA below:is non -hazardous. -I certify that the:
speclficwvastea+v S. delivered~ the: " rri med:below'fnl legal°txeattner�t;•stare e, nr ewposal.at the site indicated, '
S��natNre Date:
' CONTAINER
NAME ANb/lOWDESCRIP1 O 'F-WASTE QUA{�1TITY C R61:E-'IiNIrS' TYPE &SIZE
- _(i.e. Sga�pai1, 30gal
"" �,,; '� � • ""' drwr� 3`'Sga1:-drum,
85.ga1. over pack)
Lhs. 1 allon. '/ vi'ui m-/: T-qb sk /`Tons
,. C6s /. Gallons .% Drums % Totes / Tons / eu Y&bays
Lbs /Gallons / ed s /Totes / ,Tons / Cu 1(d. Bags .S
J.
Lbs. / Gallons / Drunis / Totes / Tons/"Cu. Yd. $ags`
A ,
`4 L6s../ Lallans T'Drrrhis: / Tgt~es.;j Tons
r Lbs. J a;all+9hs / p}rums / Totes [Tons / Cu. Yd. Baoo. `'
l .. Phone #u:�A
Iiiet tlt+e aF ed:wait&o wvs wfisle►Ted A* a` registered (/icensedJ'vehicle;-90 Hb �v1 poraboe:Pfi was. accepted,.
pid[up D Ver s 5lghatuire« • :Date . tsleliv g a]rive 's Signature x Date-
� o Nort v r 041r, s: r.114E)
Facility: HOW 'Corporation CVl1'i Perthit #: 1998 '� ,. EPA ID#: NCR00001226t} z
1701 Yargrave S't.
Winit+ n-Salem, HC 27107
k A6iEWATER tREATME141T n�raKyLliJrl bi47ION © USED 0r4.P"YC"#1G
HANI)1 LNG, ME C Jy
[3:PACKAGM11RE'1dME040OD5.GPJN)PMG ' ro �ItASTiE' I' E.. 1Tf1ER:
'I icertify.that the Transport+erabtrlie deliv�Xed the specified mat eniN ws aclhty:aintl vra�s ac epted anti properly Kan a abovia
manner.
_ �.. "�► �'
.Sigriature:
.WHITE COPY=HOH: YELLOWrC{3PY-R TURN.TO.GENERATOR.. ':PINK.COPY4-RANSRORTER -- 60Iat�Nft[3!`��
=td4i``.�'b s43.. ks•."si�,�-,

Winston-Salem, NC 27107 w wa o Corp -co
NON -HAZARDOUS ATMANIFEST
Generator: MIA& Dat ._mm
- --
Ad ss:.__. Phoned#:.
Y�X /I /f.Ell ll..1. :. 1 i EPA ID*: ! V
Confect: /" U;If to: V)
Pra.cess. which ,generated waste. . Icertify that the, materials described below.. are properly described,: classified, packaged, marked: and
labeled, .,a are .in.iiroper con n to:be ansported in cotr►merce under the applicable regulaiiorss of theState, the Environmental
Protection Agency and the be fitof". "- nsNbrtatiom I certify that :the •waste described below is non -hazardous. I certify that.the
specific waste was, delivered to t6 c Her. n d below for legal tireatme�ity:storage, or disposat at//the.site indicated:
Signature; _ Date:6 f l
CONTAINER
WANE AND/OR DES.CitIPTX N OF WASTE:, QUANTITY CIRCLE UNITS TYPE $e SIZE
(i e. 5gal pail, 30 ga%
drum, 55gal drum,
$Sgal, over'pack) .
Lbs. /, allons / Drums / Totes / Tons / Cu, Yd. Bags
Lbs: / Gallons % Drums / Totes /Tons / Cu Ydt Sags
Llis. % Gailnns Totes /.Tops.:/•Cer:
Lbs /" Gallons / ar0his / Totes / Tons / Cu Yd".,gags
Leis.'/Gallons /`Drum$ / Totes' / Tons / Cu..Yd. Bags:
Lbs. /Gallons / Drums /. I otes / Tons /'Cu. Yd. Bags
Transporter:.
Phone #:
�s4--
EPA Ii3#: _
I cefMy that the specified waste was transferred in a rtegistered. (licensed) .vehide".to : it Corporation and was accepted,
Pickup wer's Sign turec Date- • DeUv ringrDrive s;Signature :: - Date
t
(00'NOT WRITE BELOW THIS LINE) .
Facility: HOH Corporation. _ CWTPermit #:, 199 :: El7A iID ., NCRQO.dB12260
1701..Vargrave St;.
Winston-Salem, Nar.27107 . ,
HANDLING METHOD..:: C7 WAS7-4-iNATEf2 TREATMENT SOLFJ.ZF ATION : 0 U.SED:OIL Rl:'CYMrNG:
A'.
El PACKAG,ED/RErtiRNED..G000s,GRrNif3ING f JVASTE-TO-mC'RGY.., Qi'Hm
3 certify that the Frans oiterabove delivered tixe specifired:material to. this:facility,and was;accepted'and:properly"handled in the above:
manner: f
g —
Si nature• � Date,_
WHITE COPY-HOH YELL"O.WCUPY•-(RETURN TO.GENERATOP, PINK COPY -TRANSPORTER GOLDENROD COPY -GENERATOR

B
NN
ENVIRONMENTAL AND iNOUS1 RIAL RLSOURCES
1703 Vargrave Street
Winston-Salen1, NC 2710%
ph 336- 725-.5844
fax [phone]
OF I
Evo Corporation does hereby certify that 10,700 gallons of non -hazardous
contaminated Water received on 03/03/2011 and 03/04/201.1 from:
Generator: City of Rocky Mount
Originating at: 1004 Cokey Road
Rocky Mount, NC
EC Waste ID #: 031110
has been disposed of by Evo Corporation in a manner approved by the North
'Carolina Department of Environment and Natural Resources.
Signature
Thomas W. Hammett
CEO
Eva Corporation
www.evoeorp.netT HE NEXT LEVEL

NC 2,7107
33.6 727-4,644
-s 727-8840 fax
mimm,bahcorp M,
Generator:
NON -HAZARDOUS WASTE M.N.F
Date:
.Pbo..ne #:
EPA.ID#:
13
process mhi rhgeheratodwastq;-, I Certify thatthe maMriPl9'des;Cr.jbe0ibp_l.QWp mproperly'.desCribe0-.Class; ' ItPetl; PICK,49(?il, k!jarlPZoid
are_prope, r' 9-ndI it"l9fi'..46 b'. e' #'#'n&PG.rted in cAm")Ce:�do.rtin he applkablezrOgulati.Oh-.0f.the:Sitate, the Efivironm6ntW
"?iP6f,n­A00ficy-anti tIi Iepp!w L,cefifyribed:40loJ -* Aazkropms tc
wi t"the
d. t
s®r6or
6 We f Honied -66loW fdv:1ePJA're'atm0rk,'�, 'Pt.t.be.smej di
r a�Me
Oats"
a t�-. -
t'"AWANP/0R,6ESCR4PTM3N 0F:,WA9TF QUAUTITY U I :'t-, TYPE -
CIRC )NIT'S.
drum,
ay _04 0 Pk)
Lbs.7- thilan.. .1 Drum f Tons /_Cu� Yfl�'.
3
j
Rail
i i, S:'rTotes .; ylo:h6."Jtm W_134(0s'-
b0irin' s lbio&s Yr *&�s J_. ad'
1 T444'
-Y
ths. Wigh J:0idjil t 1 'ro'ns
phone
EPAAb,*:
fret ofy Me.the VIFgw to wav frqqsfqrre(f in R myj*O�resY ap�qp*4.,-.'
PV (,ice
Pickup D4"tii'jgj: tune Deli
D HIS (CSC}, NOT WAUE ' POO'
EL T
IDA: ACRO.OQ01,7260
1791 Vargrave. St.
v0lstqw'�;04ii6i; MC 27107
00i AtwAmR mtwr iWA 1S01U1MFj4CA#0)V
HANP41NP �ETH USED
4g)ffD1REM)?jVEV;'G00DS JgjU'VDj)VG. WAS'rr-j6rv6�
jjjL' A` 0. 0,... el!P" rjed the... b
the - M 0.
'g .speci above
torag
5ijrf
a
D a
a
ropy-R Em 0 Rr _0111TER QOLDFNRODLCOPY-�GENERATOW,
W NERAT �P

Y NON-HAZARDO� S WASTEF T
Generator:mate ---
j
Aiiifr ss.. ! �— Phone
Contact:_ Bill tns(J
Process which. generated,waste: I certify that.the-materials described be2w are properly described, classi€ied;:packaged, merited and
labeled, and are.in proper condition:to he transported iri commerce under the applicable regulations of the State, the Environmental
Protection Agency and the Department of Transportation. •I• certify -that the wa9te-described below is non.=hazardous:'-.I certify thatthe
specific waste -was delive the carrier namid .below fort"al'treatment, storage, or disposal at the site indicated:
Signature: Date; — Cl
CONTAINER
NAME AND/OR liE erlt ` €on 'o wA �r M` „ f� �a tT�r `" Tiro sY i
2.
(i,e, 5 gal pail, 30 gal.
drum, 55 gal, drum,
85ga1, owrpack)
l bs. allons/ Drums / Totes./ Tons / Cu. Yd: Bags
kbs.. /'Gallons / Drums / Totes / Tons /'Cu. Yd: Bags
His-] Gallons / Drums / Totes] Tons / Cu. Yd. Bags
Lbs Qallans / Ctrtrm %-Totes / Tons./.:Cu. Yd.liags
t bs / Ga€Ions %r rurins ./ Totes / T6,p, % Cu Yd. lia0s '
Lbs. / Gallon$./ Drums Totes j Tons /'Cu.,Yd. Bags
Transporter: c UV,V6,Vxh41
._
—��
EPA.ID#: n1.'
i Celfl.. at_hP.sP, oe#G (edi t ard� ti �15 l 1r�•a FWIka1 " Irfe /rpnr�lion:an , rues acCe fed.: .
-
�ek w s 6 re Da e . D ring G3 er's -Signature Date ;
(DO NOT WRITE BELOW THIS LINE)

at t CORP0RATION
1701 Vargrave St.
winston-Salem, NC 27107
12702 336 727-4f 44 .
336 727-8840 fax
www.hohcorp.c0M rf
r
NQ HAZiARDO`US wASTrfK A. VEST
6e
t Date: Generator.
Addre S• Phone #• p4
EPA ID#:
Contact: Bill to, r. .
Process wHicll-generated waste c ixj/ that the materials descr11 dilb ovirare prgperly de$crib�d, classified,`packaged marked and
labeled, and are in proper cgediiion . trdnported in'tomntrce undefihe applicayle rcgulations'of.th State; the Envi%onmanial "
PtotecrAon Agency and the=D en f ansportation i ceri �f�r that t ie waste described" below: s non,lraxardous. - I certify "that the:
specific;' taw sAlelivered t rrre med.:below far leaatteeatment;•stora et or disposal at the site indicated:
Signature
Date:
-- _ CONTAINER
NAME g11q]OR DESCIIFPT>,OF WASTE QUANTITY CIRCLS UNITS TYP .F,:k $IZE -
Y(drv4 :53Tgd1, drum,
1 M yal. overpack)
Drums:/.Totes 1 Cons./ Cu. Yd-.Bags s:
Lbs. / (;all6hs / Drums Totes /Tons / Cu. Yd eds ;
Q .
L6s /Gallons / Druips /fTotes / Toffs (C Yd. Bags s 71
A
}
- Lbs. Gallons / Drums / Totes / Tons /^ -
/U. Yd. Bags`
�R Llis. J :Gallonsboos / [tu. YiE. Bags
Lbs../ Gallons ./ Drums / Totes / Tons Cu. Yd. Bags
i 4 t
Tranaporte f' -,: 3h'
„ EPA.ID*: 74,
F,.
I � tJra6 the, Fed:waate was transferred in -1 registered rlicensed). vehicle "m:H4 Corporatran.ancl was aecepterl.'.
Pickup D " Ver's Sign Lure. -Date -" I.),e!hF9fiAg Drive s Signature Date
_ ado NOT WRITE �7rH!S UK)
Facility:. HOH Corporation CWi Permit #: 1998 .,L EPA:ID#: NCROOD012260
1701 `Vargrave 5t.
Winston-Salem, NC 27107
HANDLING MEN - J'--%rL1kWATeRMEATI ANT .. " QLrVrFI AMON - © USED OIL::RFCXaING
Q_AAC'KtIGED/REIdRNEDGQODS"GRI/Y.DING C7.VASTL T F +lTfE1tc .
w
I'rert fy.tfratt a .Transporterabo�re"deliy�Xed the specified materia ih�sfacifity and w0s•accepb60`M �rraperiyhan �e above'
manner.
-- .� "a '
Dam:
Sigdsltlre —
l
-WHITE, ' MELLOW COPY-RETURN'.�'0 G15NER'ATOR. PINK. COPYsTRANSPORTER GOt2jli L3IOl3 v
` ;'T - ,..- . "- _ . r m,-a!-'�.:�+.. _��t Y�.'.•�iA��aa'�:k+'-!'�1+:o�ib�.,ua��Qt;}/$�. � ,.. --. ,. "" fit. .

Appendix E
Laboratory Analytical Data Reports and Chain -of -Custody Records
Hexane Liquid Characterization
UST Closure Samples
Hart & Hickman, PC

Appendix E
Laboratory Analytical Data Reports and Chain -of -Custody Records
Hexane Liquid Characterization
UST Closure Samples
Hart & Hickman, PC

Hexane Liquid Characterization — UST 002
Hart & Hickman, PC

LP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Hart & Hickman (Raleigh)
Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
NC Certification No. 402 Case Narrative
SC Certification No. 99012
NC Drinking Water Cert No. 37735 01 /27/2011
Project: City of Rocky Mount (Planters Oil Mill)
Project No.: CRM-008
Lab Submittal Date: 01/14/2011
Prism Work Order: 1010261
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Flashpoint analysis was subcontracted to GCAL. Laboratory report is attached.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 18

Sample Receipt Summary
fflyaR I S M Full -Service Analytical R 01 /27/2011
Environmental Solutions
LABORATORIES, INC.
Prism Work Order: 1010261
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
Hexane Liquid 1010261-01 Water 01/13/11 01/14/11
Samples received in good condition at 3.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 18

%j6P R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
Laboratory Report
01/27/2011
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount (Planters
Oil Mill)
Project No.: CRM-008
Sample Matrix: Water
Client Sample ID: Hexane Liquid
Prism Sample ID: 1010261-01
Prism Work Order: 1010261
Time Collected: 01/13/11 10:55
Time Submitted: 01/14/11 13:10
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1,1,1,2-Tetrachloroethane
BRL
ug/L
40
5.9
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,1,1-Trichloroethane
BRL
ug/L
40
2.5
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,1,2,2-Tetrachloroethane
BRL
ug/L
40
2.9
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,1,2-Trichloroethane
BRL
ug/L
40
6.6
40
`8260B
1/19/11
0:36
LMW
PlA0273
1,1-Dichloroethane
BRL
ug/L
40
3.8
40
`8260B
1/19/11
0:36
LMW
PlA0273
1,1-Dichloroethylene
BRL
ug/L
40
3.1
40
`8260B
1/19/11
0:36
LMW
PlA0273
1,1-Dichloropropylene
BRL
ug/L
40
2.5
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,2,3-Trichlorobenzene
BRL
ug/L
80
8.0
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,2,3-Trichloropropane
BRL
ug/L
40
3.2
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,2,4-Trichlorobenzene
BRL
ug/L
40
4.1
40
"8260B
1/19/11
0:36
LMW
PlA0273
1,2,4-Trimethyl benzene
BRL
ug/L
40
1.9
40
"8260B
1/19/11
0:36
LMW
PlA0273
1,2-Dibromo-3-chloropropane
BRL
ug/L
80
24
40
"8260B
1/19/11
0:36
LMW
PlA0273
1,2-Dibromoethane
BRL
ug/L
40
5.5
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,2-Dichlorobenzene
BRL
ug/L
40
3.1
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,2-Dichloroethane
BRL
ug/L
40
5.6
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,2-Dichloropropane
BRL
ug/L
40
5.1
40
`8260B
1/19/11
0:36
LMW
PlA0273
1,3,5-Trimethyl benzene
BRL
ug/L
40
2.3
40
`8260B
1/19/11
0:36
LMW
PlA0273
1,3-Dichlorobenzene
BRL
ug/L
40
3.0
40
`8260B
1/19/11
0:36
LMW
PlA0273
1,3-Dichloropropane
BRL
ug/L
40
4.4
40
'8260B
1/19/11
0:36
LMW
PlA0273
1,4-Dichlorobenzene
BRL
ug/L
40
2.7
40
'8260B
1/19/11
0:36
LMW
PlA0273
2,2-Dichloropropane
BRL
ug/L
80
4.6
40
'8260B
1/19/11
0:36
LMW
PlA0273
2-Chloroethyl Vinyl Ether
BRL
ug/L
80
9.0
40
"8260B
1/19/11
0:36
LMW
PlA0273
2-Chlorotoluene
BRL
ug/L
40
1.5
40
"8260B
1/19/11
0:36
LMW
PlA0273
4-Chlorotoluene
BRL
ug/L
40
2.1
40
"8260B
1/19/11
0:36
LMW
PlA0273
4-Isopropyltoluene
BRL
ug/L
40
2.6
40
'8260B
1/19/11
0:36
LMW
PlA0273
Acetone
BRL
ug/L
400
25
40
'8260B
1/19/11
0:36
LMW
PlA0273
Acrolein
BRL
ug/L
4000
44
40
'8260B
1/19/11
0:36
LMW
PlA0273
Acrylonitrile
BRL
ug/L
4000
34
40
`8260B
1/19/11
0:36
LMW
PlA0273
Benzene
41
ug/L
40
2.9
40
"826013
1/19/11
0:36
LMW
PlA0273
Bromobenzene
BRL
ug/L
40
2.6
40
'8260B
1/19/11
0:36
LMW
PlA0273
Bromochloromethane
BRL
ug/L
40
5.0
40
'8260B
1/19/11
0:36
LMW
PlA0273
Bromodichloromethane
BRL
ug/L
40
2.5
40
`8260B
1/19/11
0:36
LMW
PlA0273
Bromoform
BRL
ug/L
40
11
40
`8260B
1/19/11
0:36
LMW
PlA0273
Bromomethane
BRL
ug/L
120
19
40
`8260B
1/19/11
0:36
LMW
PlA0273
Carbon disulfide
BRL
ug/L
200
55
40
'8260B
1/19/11
0:36
LMW
PlA0273
Carbon Tetrachloride
BRL
ug/L
80
4.7
40
'8260B
1/19/11
0:36
LMW
PlA0273
Chlorobenzene
BRL
ug/L
40
2.5
40
'8260B
1/19/11
0:36
LMW
PlA0273
Chloroethane
BRL
ug/L
200
5.1
40
"8260B
1/19/11
0:36
LMW
PlA0273
Chloroform
BRL
ug/L
40
3.5
40
"8260B
1/19/11
0:36
LMW
PlA0273
Chloromethane
BRL
ug/L
80
4.4
40
"8260B
1/19/11
0:36
LMW
PlA0273
cis-1,2-Dichloroethylene
BRL
ug/L
40
3.0
40
'8260B
1/19/11
0:36
LMW
PlA0273
cis-1,3-Dichloropropylene
BRL
ug/L
40
4.2
40
'8260B
1/19/11
0:36
LMW
PlA0273
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 18

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 01/27/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (Planters Client Sample ID: Hexane Liquid
Attn: Kevin Buchanan Oil Mill) Prism Sample ID: 1010261-01
3334 Hillsborough St. Project No.: CRM-008 Prism Work Order: 1010261
Raleigh, NC 27607 Sample Matrix: Water Time Collected: 01/13/11 10:55
Time Submitted: 01/14/11 13:10
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Dibromochloromethane
BRL
ug/L
40
12
40
*8260B
1/19/11
0:36
LMW
PlA0273
Dibromomethane
BRL
ug/L
40
5.2
40
*8260B
1/19/11
0:36
LMW
PlA0273
Dichlorodifluoromethane
BRL
ug/L
80
4.3
40
*8260B
1/19/11
0:36
LMW
PlA0273
Ethylbenzene
BRL
ug/L
40
2.7
40
*8260B
1/19/11
0:36
LMW
PlA0273
Hexachlorobutadiene
BRL
ug/L
80
15
40
*8260B
1/19/11
0:36
LMW
PlA0273
Hexane
8200
ug/L
4000
1500
400
*8260B
1/19/11
10:56
LMW
PlA0273
Isopropyl Ether
BRL
ug/L
40
1.7
40
*8260B
1/19/11
0:36
LMW
PlA0273
Isopropylbenzene (Cumene)
BRL
ug/L
40
2.9
40
*8260B
1/19/11
0:36
LMW
PlA0273
m,p-Xylenes
BRL
ug/L
80
3.2
40
*8260B
1/19/11
0:36
LMW
PlA0273
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/L
200
7.6
40
*8260B
1/19/11
0:36
LMW
PlA0273
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/L
200
36
40
*8260B
1/19/11
0:36
LMW
PlA0273
Methyl Isobutyl Ketone
BRL
ug/L
200
5.0
40
*8260B
1/19/11
0:36
LMW
PlA0273
Methylene Chloride
BRL
ug/L
80
18
40
*8260B
1/19/11
0:36
LMW
PlA0273
Methyl-tert-Butyl Ether
BRL
ug/L
40
2.8
40
*8260B
1/19/11
0:36
LMW
PlA0273
Naphthalene
BRL
ug/L
40
3.9
40
*8260B
1/19/11
0:36
LMW
PlA0273
n-Butylbenzene
BRL
ug/L
40
4.5
40
*8260B
1/19/11
0:36
LMW
PlA0273
n-Propylbenzene
BRL
ug/L
40
2.4
40
*8260B
1/19/11
0:36
LMW
PlA0273
o-Xylene
BRL
ug/L
40
1.8
40
*8260B
1/19/11
0:36
LMW
PlA0273
sec-Butylbenzene
BRL
ug/L
40
3.5
40
*8260B
1/19/11
0:36
LMW
PlA0273
Styrene
BRL
ug/L
40
1.9
40
*8260B
1/19/11
0:36
LMW
PlA0273
tert-Butylbenzene
BRL
ug/L
40
3.2
40
*8260B
1/19/11
0:36
LMW
PlA0273
Tetrachloroethylene
BRL
ug/L
40
2.8
40
*8260B
1/19/11
0:36
LMW
PlA0273
Toluene
40
ug/L
40
1.7
40
*8260B
1/19/11
0:36
LMW
PlA0273
trans-1,2-Dichloroethylene
BRL
ug/L
80
4.6
40
*8260B
1/19/11
0:36
LMW
PlA0273
trans-1,3-Dichloropropylene
BRL
ug/L
40
1.7
40
*8260B
1/19/11
0:36
LMW
PlA0273
Trichloroethylene
BRL
ug/L
80
2.2
40
*8260B
1/19/11
0:36
LMW
PlA0273
Trichlorofluoromethane
BRL
ug/L
80
3.5
40
*8260B
1/19/11
0:36
LMW
PlA0273
Vinyl acetate
BRL
ug/L
800
4.0
40
*8260B
1/19/11
0:36
LMW
PlA0273
Vinyl chloride
BRL
ug/L
80
6.2
40
*8260B
1/19/11
0:36
LMW
PlA0273
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
105 %
80-124
Dibromofluoromethane
102 %
75-129
Toluene-d8
100 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 18

P R I IS M EService Analytical
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
1127111
Hart & Hickman (Raleigh) Project: City of Rocky Mount (Planters
Attn: Kevin Buchanan Oil Mill)
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 1010261
Time Submitted: 1/14/11 1:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1A0273 - 5030B
Blank (PlA0273-BLK1)
Prepared & Analyzed: 01/18/11
1,1,1,2-Tetrachloroethane
BRL
1.0
ug/L
1,1,1-Trichloroethane
BRL
1.0
ug/L
1,1,2,2-Tetrachloroethane
BRL
1.0
ug/L
1,1,2-Trichloroethane
BRL
1.0
ug/L
1,1-Dichloroethane
BRL
1.0
ug/L
1,1-Dichloroethylene
BRL
1.0
ug/L
1,1-Dichloropropylene
BRL
1.0
ug/L
1,2,3-Trichlorobenzene
BRL
2.0
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
BRL
1.0
ug/L
1,2,4-Trimethyl benzene
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
1.0
ug/L
1,2-Dichlorobenzene
BRL
1.0
ug/L
1,2-Dichloroethane
BRL
1.0
ug/L
1,2-Dichloropropane
BRL
1.0
ug/L
1,3,5-Trimethyl benzene
BRL
1.0
ug/L
1,3-Dichlorobenzene
BRL
1.0
ug/L
1,3-Dichloropropane
BRL
1.0
ug/L
1,4-Dichlorobenzene
BRL
1.0
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
2-Chloroethyl Vinyl Ether
BRL
2.0
ug/L
2-Chlorotoluene
BRL
1.0
ug/L
4-Chlorotoluene
BRL
1.0
ug/L
4-Isopropyltoluene
BRL
1.0
ug/L
Acetone
BRL
10
ug/L
Acrolein
BRL
100
ug/L
Acrylonitrile
BRL
100
ug/L
Benzene
BRL
1.0
ug/L
Bromobenzene
BRL
1.0
ug/L
Bromochloromethane
BRL
1.0
ug/L
Bromodichloromethane
BRL
1.0
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
3.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
1.0
ug/L
Chloroethane
BRL
5.0
ug/L
Chloroform
BRL
1.0
ug/L
Chloromethane
BRL
2.0
ug/L
cis-1,2-Dichloroethylene
BRL
1.0
ug/L
cis-1,3-Dichloropropylene
BRL
1.0
ug/L
Dibromochloromethane
BRL
1.0
ug/L
Dibromomethane
BRL
1.0
ug/L
Dichlorodifluoromethane
BRL
2.0
ug/L
Ethylbenzene
BRL
1.0
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 18

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (Planters
Attn: Kevin Buchanan Oil Mill)
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
1 /27/11
Prism Work Order: 1010261
Time Submitted: 1/14/11 1:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1A0273 - 5030B
Blank (PlA0273-BLK1)
Prepared & Analyzed: 01/18/11
Hexachlorobutadiene
BRL
2.0
ug/L
Hexane
BRL
10
ug/L
Isopropyl Ether
BRL
1.0
ug/L
Isopropylbenzene (Cumene)
BRL
1.0
ug/L
m,p-Xylenes
BRL
2.0
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methylene Chloride
BRL
2.0
ug/L
Methyl-tert-Butyl Ether
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
n-Butylbenzene
BRL
1.0
ug/L
n-Propylbenzene
BRL
1.0
ug/L
o-Xylene
BRL
1.0
ug/L
sec-Butylbenzene
BRL
1.0
ug/L
Styrene
BRL
1.0
ug/L
tert-Butylbenzene
BRL
1.0
ug/L
Tetrachloroethylene
BRL
1.0
ug/L
Toluene
BRL
1.0
ug/L
trans-1,2-Dichloroethylene
BRL
2.0
ug/L
trans-1,3-Dichloropropylene
BRL
1.0
ug/L
Trichloroethylene
BRL
2.0
ug/L
Trichlorofluoromethane
BRL
2.0
ug/L
Vinyl acetate
BRL
20
ug/L
Vinyl chloride
BRL
2.0
ug/L
Surrogate:4-Bromofluorobenzene
25.9
ug/L
25.0 104 80-124
Surrogate: Dibromofluoromethane
25.3
ug/L
25.0 101 75-129
Surrogate: Toluene-d8
25.1
ug/L
25.0 100 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 6 of 18

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (Planters
Attn: Kevin Buchanan Oil Mill)
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
1 /27/11
Prism Work Order: 1010261
Time Submitted: 1/14/11 1:10:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch PlA0273 - 5030B
LCS (PlA0273-BSI)
Prepared & Analyzed: 01/18/11
1,1-Dichloroethylene
56.2
1.0
ug/L
50.0
112
70-154
Benzene
50.4
1.0
ug/L
50.0
101
77-128
Chlorobenzene
51.2
1.0
ug/L
50.0
102
78-119
Hexane
57.9
10
ug/L
50.0
116
70-130
Toluene
49.9
1.0
ug/L
50.0
100
76-131
Trichloroethylene
50.5
2.0
ug/L
50.0
101
77-133
Surrogate:4-Bromofluorobenzene
25.6
ug/L
25.0
102
80-124
Surrogate: Dibromofluoromethane
25.6
ug/L
25.0
102
75-129
Surrogate: Toluene-d8
25.6
ug/L
25.0
102
77-123
LCS Dup (P1A0273-BSD1)
Prepared & Analyzed: 01/18/11
1,1-Dichloroethylene
52.2
1.0
ug/L
50.0
104
70-154
7
Benzene
47.8
1.0
ug/L
50.0
96
77-128
5
Chlorobenzene
48.3
1.0
ug/L
50.0
97
78-119
6
Hexane
53.4
10
ug/L
50.0
107
70-130
8
Toluene
47.1
1.0
ug/L
50.0
94
76-131
6
Trichloroethylene
46.9
2.0
ug/L
50.0
94
77-133
7
Surrogate:4-Bromofluorobenzene
25.1
ug/L
25.0
101
80-124
Surrogate: Dibromofluoromethane
25.2
ug/L
25.0
101
75-129
Surrogate: Toluene-d8
25.3
ug/L
25.0
101
77-123
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch
Initial
Final
Date
1010261-01 PlA0273 10 mL 10 mL 01/18/11
1010261-01 PlA0273 10 mL 10 mL 01/18/11
Subcontracted Analyses
The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc.
Lab Number Analysis
1010261-01
Flash Point (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 18

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Aces
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
1010261
LABORATORY REPORT NUMBER
211012526
DATE
01 /26/2011
Primary Data Review By
Curtis Ekker
Data Validation Manager, GCAL
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
aarnick@ac(;essanalyticalinc.com
- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979 GSRI
Avenue, Baton Rouge, LA 70820.
- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955, NELAP
certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of
GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access
Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Page 9 of 18

NELAP CERTIFICATE NUMBER 01955
DOD FLAP CERTIFICATE NUMBER ADE - 1482
ANALYTICAL RESULTS
PERFORMED BY
GULF COAST ANALYTICAL LABORATORIES, INC.
7979 GSRI Avenue
Baton Rouge, LA 70820
Report Date 01 /26/2011
GCAL Report 211012526II
Deliver To Prism Laboratories Inc.
PO BOX 240543
Charlotte, NC. 28224
706-529-6364
Attn Robbi Jones
Project 1010261
Page 10 of 18

CASE NARRATIVE
Client: Prism Laboratories, Inc. Report: 211012526
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the sample cross-reference page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Page 11 of 18

Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the
Environmental Protection Agency or other recognized agencies. The samples and their corresponding
extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention
period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.
Common Abbreviations Utilized in this Report
ND Indicates the result was Not Detected at the specified RDL
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLO Indicates the analysis was performed in the Field
PQL Practical Quantitation Limit
MDL Method Detection Limit
RDL Reporting Detection Limit
00:00 Reported as a time equivalent to 12:00 AM
Reporting Flags Utilized in this Report
J Indicates an estimated value
U Indicates the compound was analyzed for but not detected
B (ORGANICS) Indicates the analyte was detected in the associated Method Blank
B (INORGANICS) Indicates the result is between the RDL and MDL
Sample receipt at GCAL is documented through the attached chain of custody. In accordance with
NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results
contained within this report relate only to the samples reported. The documented results are presented
within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as
a permanent record thereof. The results contained within this report are intended for the use of the client.
Any unauthorized use of the information contained in this report is prohibited.
certify that this data package is in compliance with the NELAC standard and terms and conditions of the
contract and Statement of Work both technically and for completeness, for other than the conditions in the
case narrative. Release of the data contained in this hardcopy data package and in the
computer -readable data submitted has been authorized by the Quality Assurance Manager or his/her
designee, as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the
DOD QSM as specified in the contract if applicable.
�nte�� *,,Sign
Robyn Migues
Technical Director
GCAL REPORT 211012526
THIS REPORT CONTAINSlnt!4S'PRGES.
Page 12 of 18

GCAL ID Client ID
21101252601 HEXANE LIQUID
GCAL Report 211012526
Report Sample Summary
Matrix Collect Date/Time Receive Date/Time
Water 01/13/201110:55 01/25/201109:30
Page 13 of 18

Summary of Compounds Detected
There were no detects
GCAL Report 211012526
Page 14 of 18

5v
-o4t7 -lu,lu rtasnpolni
'rep Date Prep Batch Prep Method Dilution Analyzed By Analytical Batch
1 01/251201116:20 AEL 449604
CAS# Parameter
000000-01-3 FlashPoint
GCAL Report 211012526
Result RDL MDL
>170 50 50
Units
Deg F
Page 15 of 18

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Page 16 of 18

LIAAPWLABORATORIES,
Fula-Service Analytical &SM Environmental Solutions
WG
SUBCONTRACT ORDER
Certification: NELAC_ CJSACE
Prism Laboratories, Inc.
SC_ Other N G
1010261
N/A
SENDING LABORATORY:
RECEiVI1VG LABORATORY:
Prism Laboratories, Inc.
Gulf Coast Analytical Labs, Inc.
P. O. Box 240543
7979 GSR1 Avenue
Charlotte, NC 28224-0543
Baton Rouge, LA 70820
Phone: [phone]
Phone :[phone]
Fax: [phone]
Fax: [phone]
Project Manager: Rabbi A. Tones
Analysis Due Expires Laboratory ID Comments
Sample ID: 1010261-01 Water Sampled:01/13/11 10:55
Flash Point (Sub) �t�6 01127/1 1 10:55
Containers Supplied. „*W�rWakw+--a
�50 mi ��,--
'4.1
//ay r/el
C4 L_
1/Z?
Released By Date Received By Date
Released By Date Received By Date
Page 1 of 1
Page 17 of 18 1

SAMPLE RECEIVING CHECKLIST
Workorder: 211012526 Client: Access Analytical
Received by: Rabom, Michelle Received Datef lme: 1/25/2011 9:30:00 AM
Samples Received via: FEDEX Number of Coolers Received: }
Cooler tracking numbers(s): I q 6 G V7 4 3 oa6
Cooler temperatures): 4.1
Were all coolers received at a temperature of 0 - 6° C?
i es i
No
N/A
Were all custody -seats intact?
l---7e-s s
No
NIA
Were all samples recevied in proper containers?
I Yes
No
NIA
Were all samples properly preserved?
�+' fifes s
No
NIA
Was preservative added to any container at the lab?
Yes
No
NIA
Were all containers received in good condition?
Yes
No
NIA
Were all VOA vials received with no head space?
i Yes
No
��tlA
Do all sample labels match the Chain of Custody?
i es
No
NIA
Was the client notified about any discrepancies?
Yes
No
NIA
Notes/Comments:
Page 18 of 18

UST Closure Samples
Hart & Hickman, PC

LP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Hart & Hickman (Raleigh)
Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Project: City of Rocky Mount (CRM-008)
Lab Submittal Date: 03/09/2011
Prism Work Order: 1030182
Case Narrative
03/14/2011
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
IS Internal standard area outside the QC limits. No compounds found or reported under this internal standard.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 59

&P R I IS M Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
Sample Receipt Summary
03/14/2011
Prism Work Order: 1030182
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
T1-S1
1030182-01
Solid
03/08/11
03/09/11
T1-S2
1030182-02
Solid
03/08/11
03/09/11
T1-S3
1030182-03
Solid
03/08/11
03/09/11
T1-S4
1030182-04
Solid
03/08/11
03/09/11
T1-S5
1030182-05
Solid
03/08/11
03/09/11
T1-S6
1030182-06
Solid
03/08/11
03/09/11
T1-S7
1030182-07
Solid
03/08/11
03/09/11
T1-S8
1030182-08
Solid
03/08/11
03/09/11
T1-S9
1030182-09
Solid
03/08/11
03/09/11
T1-S10
1030182-10
Solid
03/08/11
03/09/11
T1-S11
1030182-11
Solid
03/08/11
03/09/11
T1-S12
1030182-12
Solid
03/08/11
03/09/11
T2-S1
1030182-13
Solid
03/08/11
03/09/11
T2-S2
1030182-14
Solid
03/08/11
03/09/11
T2-S3
1030182-15
Solid
03/08/11
03/09/11
T2-S4
1030182-16
Solid
03/08/11
03/09/11
T2-S5
1030182-17
Solid
03/08/11
03/09/11
T2-S6
1030182-18
Solid
03/08/11
03/09/11
T2-S7
1030182-19
Solid
03/08/11
03/09/11
T2-S8
1030182-20
Solid
03/08/11
03/09/11
T2-S9
1030182-21
Solid
03/08/11
03/09/11
T2-S10
1030182-22
Solid
03/08/11
03/09/11
T2-S11
1030182-23
Solid
03/08/11
03/09/11
T2-S12
1030182-24
Solid
03/08/11
03/09/11
T2-S13
1030182-25
Solid
03/08/11
03/09/11
T2-S14
1030182-26
Solid
03/08/11
03/09/11
Samples received in good condition at 3.5 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 59

%j6P R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T1-S1
Prism Sample ID: 1030182-01
Prism Work Order: 1030182
Time Collected: 03/08/11 15:45
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 7.9 1.3 1 *8015C 3/10/11 12:08 JMV P1CO214
Surrogate Recovery Control Limits
o-Terphenyl 78 % 49-124
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 4.3 0.55 50 *8015C 3/10/11 0:53 CGP P1CO233
Surrogate
Recovery Control Limits
a,a,a-Trifluorotoluene 61 % 55-129
General Chemistry Parameters
% Solids 88.4 % by 0.100 0.100 1 *SM2540 G 3/9/11 15:45 JAB PICO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S2
Prism Sample ID: 1030182-02
Prism Work Order: 1030182
Time Collected: 03/08/11 15:55
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 8.1 1.3 1 *8015C 3/10/11 12:43 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 4.3 0.56 50 *8015C 3/10/11 1:24 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 85.6 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S3
Prism Sample ID: 1030182-03
Prism Work Order: 1030182
Time Collected: 03/08/11 15:50
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 8.4 1.4 1 *8015C 3/10/11 13:18 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 4.3 0.56 50 *8015C 3/10/11 1:55 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 83.5 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S4
Prism Sample ID: 1030182-04
Prism Work Order: 1030182
Time Collected: 03/08/11 15:00
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 7.7 1.2 1 *8015C 3/10/11 13:54 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 5.9 0.77 50 *8015C 3/10/11 3:28 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 91.0 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S5
Prism Sample ID: 1030182-05
Prism Work Order: 1030182
Time Collected: 03/08/11 15:05
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 8.0 1.3 1 *8015C 3/10/11 14:29 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 5.3 0.69 50 *8015C 3/10/11 4:00 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 86.4 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S6
Prism Sample ID: 1030182-06
Prism Work Order: 1030182
Time Collected: 03/08/11 15:10
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 7.9 1.3 1 *8015C 3/10/11 15:05 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 5.3 0.69 50 *8015C 3/10/11 4:31 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 88.3 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S7
Prism Sample ID: 1030182-07
Prism Work Order: 1030182
Time Collected: 03/08/11 15:15
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 7.9 1.3 1 *8015C 3/10/11 15:41 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 4.3 0.56 50 *8015C 3/10/11 4:31 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 87.5 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S8
Prism Sample ID: 1030182-08
Prism Work Order: 1030182
Time Collected: 03/08/11 15:20
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 7.9 1.3 1 *8015C 3/10/11 16:16 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 4.7 0.62 50 *8015C 3/10/11 5:33 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 87.3 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S9
Prism Sample ID: 1030182-09
Prism Work Order: 1030182
Time Collected: 03/08/11 15:25
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 8.0 1.3 1 *8015C 3/10/11 16:52 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 4.7 0.61 50 *8015C 3/10/11 6:04 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 87.1 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S10
Prism Sample ID: 1030182-10
Prism Work Order: 1030182
Time Collected: 03/08/11 15:30
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 7.8 1.3 1 *8015C 3/10/11 17:27 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 5.5 0.71 50 *8015C 3/10/11 6:36 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 89.5 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 59

�Full-Service Analytical
P R I S M
Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T1-S11
Prism Sample ID: 1030182-11
Prism Work Order: 1030182
Time Collected: 03/08/11 15:35
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics 28 mg/kg dry 7.5 1.2 1 *8015C 3/11/11 8:50 JMV P1CO214
Surrogate Recovery Control Limits
o-Terphenyl 102 % 49-124
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 4.9 0.64 50 *8015C 3/10/11 7:07 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 92.2 % by 0.100 0.100 1 *SM2540 G 3/9/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 59

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/14/2011
Hart & Hickman (Raleigh) Project: City of Rocky Mount
Attn: Kevin Buchanan (CRM-008)
3334 Hillsborough St.
Raleigh, NC 27607 Sample Matrix: Solid
Client Sample ID: T1-S12
Prism Sample ID: 1030182-12
Prism Work Order: 1030182
Time Collected: 03/08/11 15:40
Time Submitted: 03/09/11 16:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Diesel Range Organics by GC/FID
Diesel Range Organics BRL mg/kg dry 7.7 1.2 1 *8015C 3/10/11 18:37 JMV P1CO214
Surrogate
Recovery Control Limits
Gasoline Range Organics by GC/FID
Gasoline Range Organics BRL mg/kg dry 3.5 0.45 50 *8015C 3/10/11 7:38 CGP P1CO233
Surrogate
Recovery Control Limits
General Chemistry Parameters
% Solids 90.3 % by 0.100 0.100 1 *SM2540 G 319/11 15:45 JAB P1CO208
Weight
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S1
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-13
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 13:55
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
88.7
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.2
0.56
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,1,1-Trichloroethane
BRL
ug/kg dry
4.2
0.60
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.2
0.54
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,1,2-Trichloroethane
BRL
ug/kg dry
4.2
0.51
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,1-Dichloroethane
BRL
ug/kg dry
4.2
0.40
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,1-Dichloroethylene
BRL
ug/kg dry
4.2
0.43
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,1-Dichloropropylene
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2,3-Trichlorobenzene
BRL
ug/kg dry
8.4
0.81
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2,3-Trichloropropane
BRL
ug/kg dry
4.2
0.46
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2,4-Trichlorobenzene
BRL
ug/kg dry
8.4
0.89
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2,4-Trimethyl benzene
BRL
ug/kg dry
8.4
0.83
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.2
0.56
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2-Dibromoethane
BRL
ug/kg dry
4.2
0.54
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2-Dichlorobenzene
BRL
ug/kg dry
8.4
0.65
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2-Dichloroethane
BRL
ug/kg dry
4.2
0.42
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,2-Dichloropropane
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,3,5-Trimethyl benzene
BRL
ug/kg dry
8.4
0.64
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,3-Dichlorobenzene
BRL
ug/kg dry
8.4
0.73
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,3-Dichloropropane
BRL
ug/kg dry
4.2
0.41
1
*8260B
3/10/11 19:04
KLA
PlCO235
1,4-Dichlorobenzene
BRL
ug/kg dry
8.4
0.71
1
*8260B
3/10/11 19:04
KLA
PlCO235
2,2-Dichloropropane
BRL
ug/kg dry
4.2
0.71
1
*8260B
3/10/11 19:04
KLA
PlCO235
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
8.4
0.48
1
*8260B
3/10/11 19:04
KLA
PlCO235
2-Chlorotoluene
BRL
ug/kg dry
8.4
0.62
1
*8260B
3/10/11 19:04
KLA
PlCO235
4-Chlorotoluene
BRL
ug/kg dry
8.4
0.74
1
*8260B
3/10/11 19:04
KLA
PlCO235
4-Isopropyltoluene
BRL
ug/kg dry
13
0.82
1
*8260B
3/10/11 19:04
KLA
PlCO235
Acetone
BRL
ug/kg dry
17
6.3
1
*8260B
3/10/11 19:04
KLA
PlCO235
Acrolein
BRL
ug/kg dry
84
0.66
1
*8260B
3/10/11 19:04
KLA
PlCO235
Acrylonitrile
BRL
ug/kg dry
84
1.1
1
*8260B
3/10/11 19:04
KLA
PlCO235
Benzene
BRL
ug/kg dry
2.5
0.41
1
*8260B
3/10/11 19:04
KLA
PlCO235
Bromobenzene
BRL
ug/kg dry
4.2
0.60
1
*8260B
3/10/11 19:04
KLA
PlCO235
Bromochloromethane
BRL
ug/kg dry
4.2
0.39
1
*8260B
3/10/11 19:04
KLA
PlCO235
Bromodichloromethane
BRL
ug/kg dry
4.2
0.41
1
*8260B
3/10/11 19:04
KLA
PlCO235
Bromoform
BRL
ug/kg dry
4.2
0.43
1
*8260B
3/10/11 19:04
KLA
PlCO235
Bromomethane
BRL
ug/kg dry
8.4
0.53
1
*8260B
3/10/11 19:04
KLA
PlCO235
Carbon disulfide
BRL
ug/kg dry
8.4
0.54
1
*8260B
3/10/11 19:04
KLA
PlCO235
Carbon Tetrachloride
BRL
ug/kg dry
4.2
0.42
1
*8260B
3/10/11 19:04
KLA
PlCO235
Chlorobenzene
BRL
ug/kg dry
4.2
0.61
1
*8260B
3/10/11 19:04
KLA
PlCO235
Chloroethane
BRL
ug/kg dry
8.4
0.53
1
*8260B
3/10/11 19:04
KLA
PlCO235
Chloroform
BRL
ug/kg dry
4.2
0.51
1
*8260B
3/10/11 19:04
KLA
PlCO235
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 15 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S1
Prism Sample ID: 1030182-13
Prism Work Order: 1030182
Time Collected: 03/08/11 13:55
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
8.4
0.44
1
*8260B
3/10/11 19:04
KLA
PlCO235
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11 19:04
KLA
PlCO235
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11 19:04
KLA
PlCO235
Dibromochloromethane
BRL
ug/kg dry
4.2
0.46
1
*8260B
3/10/11 19:04
KLA
PlCO235
Dibromomethane
BRL
ug/kg dry
4.2
0.41
1
*8260B
3/10/11 19:04
KLA
PlCO235
Dichlorodifluoromethane
BRL
ug/kg dry
8.4
0.49
1
*8260B
3/10/11 19:04
KLA
PlCO235
Ethylbenzene
BRL
ug/kg dry
4.2
0.60
1
*8260B
3/10/11 19:04
KLA
PlCO235
Hexachlorobutadiene
BRL
ug/kg dry
13
0.81
1
*8260B
3/10/11 19:04
KLA
PlCO235
Hexane
BRL
ug/kg dry
8.4
0.51
1
*8260B
3/10/11 19:04
KLA
PlCO235
Isopropyl Ether
BRL
ug/kg dry
4.2
0.40
1
*8260B
3/10/11 19:04
KLA
PlCO235
Isopropylbenzene (Cumene)
BRL
ug/kg dry
8.4
0.64
1
*8260B
3/10/11 19:04
KLA
PlCO235
m,p-Xylenes
BRL
ug/kg dry
8.4
1.2
1
*8260B
3/10/11 19:04
KLA
PlCO235
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
42
2.4
1
*8260B
3/10/11 19:04
KLA
PlCO235
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
17
4.0
1
*8260B
3/10/11 19:04
KLA
PlCO235
Methyl Isobutyl Ketone
BRL
ug/kg dry
8.4
0.81
1
*8260B
3/10/11 19:04
KLA
PlCO235
Methylene Chloride
BRL
ug/kg dry
8.4
0.35
1
*8260B
3/10/11 19:04
KLA
PlCO235
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.2
0.29
1
*8260B
3/10/11 19:04
KLA
PlCO235
Naphthalene
BRL
ug/kg dry
4.2
0.81
1
*8260B
3/10/11 19:04
KLA
PlCO235
n-Butylbenzene
BRL
ug/kg dry
13
0.75
1
*8260B
3/10/11 19:04
KLA
PlCO235
n-Propylbenzene
BRL
ug/kg dry
8.4
0.68
1
*8260B
3/10/11 19:04
KLA
PlCO235
o-Xylene
BRL
ug/kg dry
4.2
0.57
1
*8260B
3/10/11 19:04
KLA
PlCO235
sec-Butylbenzene
BRL
ug/kg dry
13
0.80
1
*8260B
3/10/11 19:04
KLA
PlCO235
Styrene
BRL
ug/kg dry
4.2
0.67
1
*8260B
3/10/11 19:04
KLA
PlCO235
tert-Butylbenzene
BRL
ug/kg dry
17
0.68
1
*8260B
3/10/11 19:04
KLA
PlCO235
Tetrachloroethylene
BRL
ug/kg dry
8.4
0.61
1
*8260B
3/10/11 19:04
KLA
PlCO235
Toluene
BRL
ug/kg dry
4.2
0.54
1
*8260B
3/10/11 19:04
KLA
PlCO235
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.2
0.62
1
*8260B
3/10/11 19:04
KLA
PlCO235
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11 19:04
KLA
PlCO235
Trichloroethylene
BRL
ug/kg dry
4.2
0.43
1
*8260B
3/10/11 19:04
KLA
PlCO235
Trichlorofluoromethane
BRL
ug/kg dry
4.2
0.47
1
*8260B
3/10/11 19:04
KLA
PlCO235
Vinyl acetate
BRL
ug/kg dry
8.4
0.62
1
*8260B
3/10/11 19:04
KLA
PlCO235
Vinyl chloride
BRL
ug/kg dry
8.4
0.48
1
*8260B
3/10/11 19:04
KLA
PlCO235
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
103 %
70-130
Dibromofluoromethane
107
%
84-123
Toluene-d8
100 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 59

Laboratory Report
Full -Service Analytical
P R S M
&
Environmental Solutions
LABORATORIES INC.
03/14/2011
Hart & Hickman (Raleigh)
Project: City of Rocky
Mount
Client
Sample ID:
T2-S2
Attn: Kevin Buchanan
(CRM-008)
Prism
Sample ID:
1030182-14
3334 Hillsborough St.
Prism
Work Order: 1030182
Raleigh, NC 27607
Sample Matrix: Solid
Time Collected: 03/08/11 13:50
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
89.6
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.3
0.58
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,1,1-Trichloroethane
BRL
ug/kg dry
4.3
0.61
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.3
0.55
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,1,2-Trichloroethane
BRL
ug/kg dry
4.3
0.53
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,1-Dichloroethane
BRL
ug/kg dry
4.3
0.41
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,1-Dichloroethylene
BRL
ug/kg dry
4.3
0.44
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,1-Dichloropropylene
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2,3-Trichlorobenzene
BRL
ug/kg dry
8.7
0.83
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2,3-Trichloropropane
BRL
ug/kg dry
4.3
0.47
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2,4-Trichlorobenzene
BRL
ug/kg dry
8.7
0.92
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2,4-Trimethyl benzene
BRL
ug/kg dry
8.7
0.85
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.3
0.57
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2-Dibromoethane
BRL
ug/kg dry
4.3
0.55
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2-Dichlorobenzene
BRL
ug/kg dry
8.7
0.67
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2-Dichloroethane
BRL
ug/kg dry
4.3
0.43
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,2-Dichloropropane
BRL
ug/kg dry
4.3
0.46
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,3,5-Trimethyl benzene
BRL
ug/kg dry
8.7
0.66
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,3-Dichlorobenzene
BRL
ug/kg dry
8.7
0.76
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,3-Dichloropropane
BRL
ug/kg dry
4.3
0.42
1
*8260B
3/11/11 17:43
KLA
PlCO270
1,4-Dichlorobenzene
BRL
ug/kg dry
8.7
0.73
1
*8260B
3/11/11 17:43
KLA
PlCO270
2,2-Dichloropropane
BRL
ug/kg dry
4.3
0.73
1
*8260B
3/11/11 17:43
KLA
PlCO270
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
8.7
0.50
1
*8260B
3/11/11 17:43
KLA
PlCO270
2-Chlorotoluene
BRL
ug/kg dry
8.7
0.64
1
*8260B
3/11/11 17:43
KLA
PlCO270
4-Chlorotoluene
BRL
ug/kg dry
8.7
0.76
1
*8260B
3/11/11 17:43
KLA
PlCO270
4-Isopropyltoluene
BRL
ug/kg dry
13
0.85
1
*8260B
3/11/11 17:43
KLA
PlCO270
Acetone
BRL
ug/kg dry
17
6.5
1
*8260B
3/11/11 17:43
KLA
PlCO270
Acrolein
BRL
ug/kg dry
87
0.68
1
*8260B
3/11/11 17:43
KLA
PlCO270
Acrylonitrile
BRL
ug/kg dry
87
1.1
1
*8260B
3/11/11 17:43
KLA
PlCO270
Benzene
BRL
ug/kg dry
2.6
0.42
1
*8260B
3/11/11 17:43
KLA
PlCO270
Bromobenzene
BRL
ug/kg dry
4.3
0.62
1
*8260B
3/11/11 17:43
KLA
PlCO270
Bromochloromethane
BRL
ug/kg dry
4.3
0.40
1
*8260B
3/11/11 17:43
KLA
PlCO270
Bromodichloromethane
BRL
ug/kg dry
4.3
0.43
1
*8260B
3/11/11 17:43
KLA
PlCO270
Bromoform
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/11/11 17:43
KLA
PlCO270
Bromomethane
BRL
ug/kg dry
8.7
0.54
1
*8260B
3/11/11 17:43
KLA
PlCO270
Carbon disulfide
BRL
ug/kg dry
8.7
0.55
1
*8260B
3/11/11 17:43
KLA
PlCO270
Carbon Tetrachloride
BRL
ug/kg dry
4.3
0.43
1
*8260B
3/11/11 17:43
KLA
PlCO270
Chlorobenzene
BRL
ug/kg dry
4.3
0.63
1
*8260B
3/11/11 17:43
KLA
PlCO270
Chloroethane
BRL
ug/kg dry
8.7
0.54
1
*8260B
3/11/11 17:43
KLA
PlCO270
Chloroform
BRL
ug/kg dry
4.3
0.52
1
*8260B
3/11/11 17:43
KLA
PlCO270
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S2
Prism Sample ID: 1030182-14
Prism Work Order: 1030182
Time Collected: 03/08/11 13:50
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
8.7
0.46
1
*8260B
3/11/11 17:43
KLA
PlCO270
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.3
0.46
1
*8260B
3/11/11 17:43
KLA
PlCO270
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/11/11 17:43
KLA
PlCO270
Dibromochloromethane
BRL
ug/kg dry
4.3
0.47
1
*8260B
3/11/11 17:43
KLA
PlCO270
Dibromomethane
BRL
ug/kg dry
4.3
0.42
1
*8260B
3/11/11 17:43
KLA
PlCO270
Dichlorodifluoromethane
BRL
ug/kg dry
8.7
0.51
1
*8260B
3/11/11 17:43
KLA
PlCO270
Ethylbenzene
BRL
ug/kg dry
4.3
0.61
1
*8260B
3/11/11 17:43
KLA
PlCO270
Hexachlorobutadiene
BRL
ug/kg dry
13
0.83
1
*8260B
3/11/11 17:43
KLA
PlCO270
Hexane
BRL
ug/kg dry
8.7
0.53
1
*8260B
3/11/11 17:43
KLA
PlCO270
Isopropyl Ether
BRL
ug/kg dry
4.3
0.41
1
*8260B
3/11/11 17:43
KLA
PlCO270
Isopropylbenzene (Cumene)
BRL
ug/kg dry
8.7
0.66
1
*8260B
3/11/11 17:43
KLA
PlCO270
m,p-Xylenes
BRL
ug/kg dry
8.7
1.2
1
*8260B
3/11/11 17:43
KLA
PlCO270
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
43
2.5
1
*8260B
3/11/11 17:43
KLA
PlCO270
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
17
4.1
1
*8260B
3/11/11 17:43
KLA
PlCO270
Methyl Isobutyl Ketone
BRL
ug/kg dry
8.7
0.83
1
*8260B
3/11/11 17:43
KLA
PlCO270
Methylene Chloride
BRL
ug/kg dry
8.7
0.36
1
*8260B
3/11/11 17:43
KLA
PlCO270
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.3
0.30
1
*8260B
3/11/11 17:43
KLA
PlCO270
Naphthalene
BRL
ug/kg dry
4.3
0.83
1
*8260B
3/11/11 17:43
KLA
PlCO270
n-Butylbenzene
BRL
ug/kg dry
13
0.77
1
*8260B
3/11/11 17:43
KLA
PlCO270
n-Propylbenzene
BRL
ug/kg dry
8.7
0.70
1
*8260B
3/11/11 17:43
KLA
PlCO270
o-Xylene
BRL
ug/kg dry
4.3
0.58
1
*8260B
3/11/11 17:43
KLA
PlCO270
sec-Butylbenzene
BRL
ug/kg dry
13
0.83
1
*8260B
3/11/11 17:43
KLA
PlCO270
Styrene
BRL
ug/kg dry
4.3
0.69
1
*8260B
3/11/11 17:43
KLA
PlCO270
tert-Butylbenzene
BRL
ug/kg dry
17
0.70
1
*8260B
3/11/11 17:43
KLA
PlCO270
Tetrachloroethylene
BRL
ug/kg dry
8.7
0.63
1
*8260B
3/11/11 17:43
KLA
PlCO270
Toluene
BRL
ug/kg dry
4.3
0.55
1
*8260B
3/11/11 17:43
KLA
PlCO270
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.3
0.64
1
*8260B
3/11/11 17:43
KLA
PlCO270
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/11/11 17:43
KLA
PlCO270
Trichloroethylene
BRL
ug/kg dry
4.3
0.44
1
*8260B
3/11/11 17:43
KLA
PlCO270
Trichlorofluoromethane
BRL
ug/kg dry
4.3
0.49
1
*8260B
3/11/11 17:43
KLA
PlCO270
Vinyl acetate
BRL
ug/kg dry
8.7
0.63
1
*8260B
3/11/11 17:43
KLA
PlCO270
Vinyl chloride
BRL
ug/kg dry
8.7
0.50
1
*8260B
3/11/11 17:43
KLA
PlCO270
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
70-130
Dibromofluoromethane
107
%
84-123
Toluene-d8
100 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 59

Laboratory Report
Full -Service Analytical
P R S M
&
Environmental Solutions
LABORATORIES INC.
03/14/2011
Hart & Hickman (Raleigh)
Project: City of Rocky
Mount
Client
Sample ID:
T2-S3
Attn: Kevin Buchanan
(CRM-008)
Prism
Sample ID:
1030182-15
3334 Hillsborough St.
Prism
Work Order: 1030182
Raleigh, NC 27607
Sample Matrix: Solid
Time Collected: 03/08/11 13:45
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
89.2
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.3
0.57
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,1,1-Trichloroethane
BRL
ug/kg dry
4.3
0.61
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.3
0.55
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,1,2-Trichloroethane
BRL
ug/kg dry
4.3
0.52
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,1-Dichloroethane
BRL
ug/kg dry
4.3
0.40
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,1-Dichloroethylene
BRL
ug/kg dry
4.3
0.44
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,1-Dichloropropylene
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2,3-Trichlorobenzene
BRL
ug/kg dry
8.6
0.82
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2,3-Trichloropropane
BRL
ug/kg dry
4.3
0.47
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2,4-Trichlorobenzene
BRL
ug/kg dry
8.6
0.91
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2,4-Trimethyl benzene
BRL
ug/kg dry
8.6
0.85
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.3
0.57
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2-Dibromoethane
BRL
ug/kg dry
4.3
0.55
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2-Dichlorobenzene
BRL
ug/kg dry
8.6
0.66
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2-Dichloroethane
BRL
ug/kg dry
4.3
0.43
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,2-Dichloropropane
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,3,5-Trimethyl benzene
BRL
ug/kg dry
8.6
0.65
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,3-Dichlorobenzene
BRL
ug/kg dry
8.6
0.75
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,3-Dichloropropane
BRL
ug/kg dry
4.3
0.41
1
*8260B
3/10/11 20:10
KLA
PlCO235
1,4-Dichlorobenzene
BRL
ug/kg dry
8.6
0.73
1
*8260B
3/10/11 20:10
KLA
PlCO235
2,2-Dichloropropane
BRL
ug/kg dry
4.3
0.73
1
*8260B
3/10/11 20:10
KLA
PlCO235
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
8.6
0.49
1
*8260B
3/10/11 20:10
KLA
PlCO235
2-Chlorotoluene
BRL
ug/kg dry
8.6
0.64
1
*8260B
3/10/11 20:10
KLA
PlCO235
4-Chlorotoluene
BRL
ug/kg dry
8.6
0.76
1
*8260B
3/10/11 20:10
KLA
PlCO235
4-Isopropyltoluene
BRL
ug/kg dry
13
0.84
1
*8260B
3/10/11 20:10
KLA
PlCO235
Acetone
BRL
ug/kg dry
17
6.4
1
*8260B
3/10/11 20:10
KLA
PlCO235
Acrolein
BRL
ug/kg dry
86
0.68
1
*8260B
3/10/11 20:10
KLA
PlCO235
Acrylonitrile
BRL
ug/kg dry
86
1.1
1
*8260B
3/10/11 20:10
KLA
PlCO235
Benzene
BRL
ug/kg dry
2.6
0.42
1
*8260B
3/10/11 20:10
KLA
PlCO235
Bromobenzene
BRL
ug/kg dry
4.3
0.62
1
*8260B
3/10/11 20:10
KLA
PlCO235
Bromochloromethane
BRL
ug/kg dry
4.3
0.40
1
*8260B
3/10/11 20:10
KLA
PlCO235
Bromodichloromethane
BRL
ug/kg dry
4.3
0.42
1
*8260B
3/10/11 20:10
KLA
PlCO235
Bromoform
BRL
ug/kg dry
4.3
0.44
1
*8260B
3/10/11 20:10
KLA
PlCO235
Bromomethane
BRL
ug/kg dry
8.6
0.54
1
*8260B
3/10/11 20:10
KLA
PlCO235
Carbon disulfide
BRL
ug/kg dry
8.6
0.55
1
*8260B
3/10/11 20:10
KLA
PlCO235
Carbon Tetrachloride
BRL
ug/kg dry
4.3
0.43
1
*8260B
3/10/11 20:10
KLA
PlCO235
Chlorobenzene
BRL
ug/kg dry
4.3
0.63
1
*8260B
3/10/11 20:10
KLA
PlCO235
Chloroethane
BRL
ug/kg dry
8.6
0.54
1
*8260B
3/10/11 20:10
KLA
PlCO235
Chloroform
BRL
ug/kg dry
4.3
0.52
1
*8260B
3/10/11 20:10
KLA
PlCO235
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S3
Prism Sample ID: 1030182-15
Prism Work Order: 1030182
Time Collected: 03/08/11 13:45
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
8.6
0.45
1
*8260B
3/10/11 20:10
KLA
PlCO235
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/10/11 20:10
KLA
PlCO235
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/10/11 20:10
KLA
PlCO235
Dibromochloromethane
BRL
ug/kg dry
4.3
0.47
1
*8260B
3/10/11 20:10
KLA
PlCO235
Dibromomethane
BRL
ug/kg dry
4.3
0.42
1
*8260B
3/10/11 20:10
KLA
PlCO235
Dichlorodifluoromethane
BRL
ug/kg dry
8.6
0.50
1
*8260B
3/10/11 20:10
KLA
PlCO235
Ethylbenzene
BRL
ug/kg dry
4.3
0.61
1
*8260B
3/10/11 20:10
KLA
PlCO235
Hexachlorobutadiene
BRL
ug/kg dry
13
0.83
1
*8260B
3/10/11 20:10
KLA
PlCO235
Hexane
BRL
ug/kg dry
8.6
0.52
1
*8260B
3/10/11 20:10
KLA
PlCO235
Isopropyl Ether
BRL
ug/kg dry
4.3
0.41
1
*8260B
3/10/11 20:10
KLA
PlCO235
Isopropylbenzene (Cumene)
BRL
ug/kg dry
8.6
0.65
1
*8260B
3/10/11 20:10
KLA
PlCO235
m,p-Xylenes
BRL
ug/kg dry
8.6
1.2
1
*8260B
3/10/11 20:10
KLA
PlCO235
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
43
2.5
1
*8260B
3/10/11 20:10
KLA
PlCO235
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
17
4.1
1
*8260B
3/10/11 20:10
KLA
PlCO235
Methyl Isobutyl Ketone
BRL
ug/kg dry
8.6
0.83
1
*8260B
3/10/11 20:10
KLA
PlCO235
Methylene Chloride
BRL
ug/kg dry
8.6
0.36
1
*8260B
3/10/11 20:10
KLA
PlCO235
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.3
0.29
1
*8260B
3/10/11 20:10
KLA
PlCO235
Naphthalene
BRL
ug/kg dry
4.3
0.83
1
*8260B
3/10/11 20:10
KLA
PlCO235
n-Butylbenzene
BRL
ug/kg dry
13
0.76
1
*8260B
3/10/11 20:10
KLA
PlCO235
n-Propylbenzene
BRL
ug/kg dry
8.6
0.69
1
*8260B
3/10/11 20:10
KLA
PlCO235
o-Xylene
BRL
ug/kg dry
4.3
0.58
1
*8260B
3/10/11 20:10
KLA
PlCO235
sec-Butylbenzene
BRL
ug/kg dry
13
0.82
1
*8260B
3/10/11 20:10
KLA
PlCO235
Styrene
BRL
ug/kg dry
4.3
0.69
1
*8260B
3/10/11 20:10
KLA
PlCO235
tert-Butylbenzene
BRL
ug/kg dry
17
0.70
1
*8260B
3/10/11 20:10
KLA
PlCO235
Tetrachloroethylene
BRL
ug/kg dry
8.6
0.62
1
*8260B
3/10/11 20:10
KLA
PlCO235
Toluene
BRL
ug/kg dry
4.3
0.55
1
*8260B
3/10/11 20:10
KLA
PlCO235
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.3
0.63
1
*8260B
3/10/11 20:10
KLA
PlCO235
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.3
0.45
1
*8260B
3/10/11 20:10
KLA
PlCO235
Trichloroethylene
BRL
ug/kg dry
4.3
0.44
1
*8260B
3/10/11 20:10
KLA
PlCO235
Trichlorofluoromethane
BRL
ug/kg dry
4.3
0.48
1
*8260B
3/10/11 20:10
KLA
PlCO235
Vinyl acetate
BRL
ug/kg dry
8.6
0.63
1
*8260B
3/10/11 20:10
KLA
PlCO235
Vinyl chloride
BRL
ug/kg dry
8.6
0.49
1
*8260B
3/10/11 20:10
KLA
PlCO235
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
103 %
70-130
Dibromofluoromethane
107
%
84-123
Toluene-d8
98 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S4
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-16
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 13:40
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
88.8
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.5
0.61
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,1,1-Trichloroethane
BRL
ug/kg dry
4.5
0.64
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.5
0.58
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,1,2-Trichloroethane
BRL
ug/kg dry
4.5
0.55
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,1-Dichloroethane
BRL
ug/kg dry
4.5
0.43
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,1-Dichloroethylene
BRL
ug/kg dry
4.5
0.46
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,1-Dichloropropylene
BRL
ug/kg dry
4.5
0.48
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2,3-Trichlorobenzene
BRL
ug/kg dry
9.1
0.87
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2,3-Trichloropropane
BRL
ug/kg dry
4.5
0.50
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2,4-Trichlorobenzene
BRL
ug/kg dry
9.1
0.96
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2,4-Trimethyl benzene
BRL
ug/kg dry
9.1
0.89
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.5
0.60
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2-Dibromoethane
BRL
ug/kg dry
4.5
0.58
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2-Dichlorobenzene
BRL
ug/kg dry
9.1
0.70
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2-Dichloroethane
BRL
ug/kg dry
4.5
0.46
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,2-Dichloropropane
BRL
ug/kg dry
4.5
0.48
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,3,5-Trimethyl benzene
BRL
ug/kg dry
9.1
0.69
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,3-Dichlorobenzene
BRL
ug/kg dry
9.1
0.79
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,3-Dichloropropane
BRL
ug/kg dry
4.5
0.44
1
*8260B
3/10/11 20:43
KLA
PlCO235
1,4-Dichlorobenzene
BRL
ug/kg dry
9.1
0.77
1
*8260B
3/10/11 20:43
KLA
PlCO235
2,2-Dichloropropane
BRL
ug/kg dry
4.5
0.77
1
*8260B
3/10/11 20:43
KLA
PlCO235
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
9.1
0.52
1
*8260B
3/10/11 20:43
KLA
PlCO235
2-Chlorotoluene
BRL
ug/kg dry
9.1
0.67
1
*8260B
3/10/11 20:43
KLA
PlCO235
4-Chlorotoluene
BRL
ug/kg dry
9.1
0.80
1
*8260B
3/10/11 20:43
KLA
PlCO235
4-Isopropyltoluene
BRL
ug/kg dry
14
0.89
1
*8260B
3/10/11 20:43
KLA
PlCO235
Acetone
BRL
ug/kg dry
18
6.8
1
*8260B
3/10/11 20:43
KLA
PlCO235
Acrolein
BRL
ug/kg dry
91
0.71
1
*8260B
3/10/11 20:43
KLA
PlCO235
Acrylonitrile
BRL
ug/kg dry
91
1.2
1
*8260B
3/10/11 20:43
KLA
PlCO235
Benzene
BRL
ug/kg dry
2.7
0.44
1
*8260B
3/10/11 20:43
KLA
PlCO235
Bromobenzene
BRL
ug/kg dry
4.5
0.65
1
*8260B
3/10/11 20:43
KLA
PlCO235
Bromochloromethane
BRL
ug/kg dry
4.5
0.42
1
*8260B
3/10/11 20:43
KLA
PlCO235
Bromodichloromethane
BRL
ug/kg dry
4.5
0.45
1
*8260B
3/10/11 20:43
KLA
PlCO235
Bromoform
BRL
ug/kg dry
4.5
0.47
1
*8260B
3/10/11 20:43
KLA
PlCO235
Bromomethane
BRL
ug/kg dry
9.1
0.57
1
*8260B
3/10/11 20:43
KLA
PlCO235
Carbon disulfide
BRL
ug/kg dry
9.1
0.58
1
*8260B
3/10/11 20:43
KLA
PlCO235
Carbon Tetrachloride
BRL
ug/kg dry
4.5
0.45
1
*8260B
3/10/11 20:43
KLA
PlCO235
Chlorobenzene
BRL
ug/kg dry
4.5
0.66
1
*8260B
3/10/11 20:43
KLA
PlCO235
Chloroethane
BRL
ug/kg dry
9.1
0.57
1
*8260B
3/10/11 20:43
KLA
PlCO235
Chloroform
BRL
ug/kg dry
4.5
0.55
1
*8260B
3/10/11 20:43
KLA
PlCO235
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 21 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S4
Prism Sample ID: 1030182-16
Prism Work Order: 1030182
Time Collected: 03/08/11 13:40
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
9.1
0.48
1
*8260B
3/10/11 20:43
KLA
PlCO235
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.5
0.48
1
*8260B
3/10/11 20:43
KLA
PlCO235
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.5
0.47
1
*8260B
3/10/11 20:43
KLA
PlCO235
Dibromochloromethane
BRL
ug/kg dry
4.5
0.49
1
*8260B
3/10/11 20:43
KLA
PlCO235
Dibromomethane
BRL
ug/kg dry
4.5
0.44
1
*8260B
3/10/11 20:43
KLA
PlCO235
Dichlorodifluoromethane
BRL
ug/kg dry
9.1
0.53
1
*8260B
3/10/11 20:43
KLA
PlCO235
Ethylbenzene
BRL
ug/kg dry
4.5
0.64
1
*8260B
3/10/11 20:43
KLA
PlCO235
Hexachlorobutadiene
BRL
ug/kg dry
14
0.87
1
*8260B
3/10/11 20:43
KLA
PlCO235
Hexane
BRL
ug/kg dry
9.1
0.55
1
*8260B
3/10/11 20:43
KLA
PlCO235
Isopropyl Ether
BRL
ug/kg dry
4.5
0.43
1
*8260B
3/10/11 20:43
KLA
PlCO235
Isopropylbenzene (Cumene)
BRL
ug/kg dry
9.1
0.69
1
*8260B
3/10/11 20:43
KLA
PlCO235
m,p-Xylenes
BRL
ug/kg dry
9.1
1.2
1
*8260B
3/10/11 20:43
KLA
PlCO235
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
45
2.6
1
*8260B
3/10/11 20:43
KLA
PlCO235
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
18
4.3
1
*8260B
3/10/11 20:43
KLA
PlCO235
Methyl Isobutyl Ketone
BRL
ug/kg dry
9.1
0.87
1
*8260B
3/10/11 20:43
KLA
PlCO235
Methylene Chloride
BRL
ug/kg dry
9.1
0.38
1
*8260B
3/10/11 20:43
KLA
PlCO235
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.5
0.31
1
*8260B
3/10/11 20:43
KLA
PlCO235
Naphthalene
BRL
ug/kg dry
4.5
0.87
1
*8260B
3/10/11 20:43
KLA
PlCO235
n-Butylbenzene
BRL
ug/kg dry
14
0.81
1
*8260B
3/10/11 20:43
KLA
PlCO235
n-Propylbenzene
BRL
ug/kg dry
9.1
0.73
1
*8260B
3/10/11 20:43
KLA
PlCO235
o-Xylene
BRL
ug/kg dry
4.5
0.61
1
*8260B
3/10/11 20:43
KLA
PlCO235
sec-Butylbenzene
BRL
ug/kg dry
14
0.87
1
*8260B
3/10/11 20:43
KLA
PlCO235
Styrene
BRL
ug/kg dry
4.5
0.73
1
*8260B
3/10/11 20:43
KLA
PlCO235
tert-Butylbenzene
BRL
ug/kg dry
18
0.74
1
*8260B
3/10/11 20:43
KLA
PlCO235
Tetrachloroethylene
BRL
ug/kg dry
9.1
0.66
1
*8260B
3/10/11 20:43
KLA
PlCO235
Toluene
BRL
ug/kg dry
4.5
0.58
1
*8260B
3/10/11 20:43
KLA
PlCO235
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.5
0.67
1
*8260B
3/10/11 20:43
KLA
PlCO235
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.5
0.47
1
*8260B
3/10/11 20:43
KLA
PlCO235
Trichloroethylene
BRL
ug/kg dry
4.5
0.46
1
*8260B
3/10/11 20:43
KLA
PlCO235
Trichlorofluoromethane
BRL
ug/kg dry
4.5
0.51
1
*8260B
3/10/11 20:43
KLA
PlCO235
Vinyl acetate
BRL
ug/kg dry
9.1
0.66
1
*8260B
3/10/11 20:43
KLA
PlCO235
Vinyl chloride
BRL
ug/kg dry
9.1
0.52
1
*8260B
3/10/11 20:43
KLA
PlCO235
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101
%
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
99 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S5
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-17
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 12:10
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
89.7
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.5
0.60
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,1,1-Trichloroethane
BRL
ug/kg dry
4.5
0.64
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.5
0.58
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,1,2-Trichloroethane
BRL
ug/kg dry
4.5
0.55
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,1-Dichloroethane
BRL
ug/kg dry
4.5
0.43
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,1-Dichloroethylene
BRL
ug/kg dry
4.5
0.46
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,1-Dichloropropylene
BRL
ug/kg dry
4.5
0.47
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2,3-Trichlorobenzene
BRL
ug/kg dry
9.0
0.87
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2,3-Trichloropropane
BRL
ug/kg dry
4.5
0.50
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2,4-Trichlorobenzene
BRL
ug/kg dry
9.0
0.96
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2,4-Trimethyl benzene
BRL
ug/kg dry
9.0
0.89
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.5
0.60
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2-Dibromoethane
BRL
ug/kg dry
4.5
0.58
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2-Dichlorobenzene
BRL
ug/kg dry
9.0
0.70
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2-Dichloroethane
BRL
ug/kg dry
4.5
0.45
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,2-Dichloropropane
BRL
ug/kg dry
4.5
0.48
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,3,5-Trimethyl benzene
BRL
ug/kg dry
9.0
0.68
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,3-Dichlorobenzene
BRL
ug/kg dry
9.0
0.79
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,3-Dichloropropane
BRL
ug/kg dry
4.5
0.44
1
*8260B
3/10/11 21:16
KLA
PlCO235
1,4-Dichlorobenzene
BRL
ug/kg dry
9.0
0.76
1
*8260B
3/10/11 21:16
KLA
PlCO235
2,2-Dichloropropane
BRL
ug/kg dry
4.5
0.77
1
*8260B
3/10/11 21:16
KLA
PlCO235
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
9.0
0.52
1
*8260B
3/10/11 21:16
KLA
PlCO235
2-Chlorotoluene
BRL
ug/kg dry
9.0
0.67
1
*8260B
3/10/11 21:16
KLA
PlCO235
4-Chlorotoluene
BRL
ug/kg dry
9.0
0.80
1
*8260B
3/10/11 21:16
KLA
PlCO235
4-Isopropyltoluene
BRL
ug/kg dry
14
0.89
1
*8260B
3/10/11 21:16
KLA
PlCO235
Acetone
BRL
ug/kg dry
18
6.7
1
*8260B
3/10/11 21:16
KLA
PlCO235
Acrolein
BRL
ug/kg dry
90
0.71
1
*8260B
3/10/11 21:16
KLA
PlCO235
Acrylonitrile
BRL
ug/kg dry
90
1.2
1
*8260B
3/10/11 21:16
KLA
PlCO235
Benzene
BRL
ug/kg dry
2.7
0.44
1
*8260B
3/10/11 21:16
KLA
PlCO235
Bromobenzene
BRL
ug/kg dry
4.5
0.65
1
*8260B
3/10/11 21:16
KLA
PlCO235
Bromochloromethane
BRL
ug/kg dry
4.5
0.42
1
*8260B
3/10/11 21:16
KLA
PlCO235
Bromodichloromethane
BRL
ug/kg dry
4.5
0.45
1
*8260B
3/10/11 21:16
KLA
PlCO235
Bromoform
BRL
ug/kg dry
4.5
0.47
1
*8260B
3/10/11 21:16
KLA
PlCO235
Bromomethane
BRL
ug/kg dry
9.0
0.57
1
*8260B
3/10/11 21:16
KLA
PlCO235
Carbon disulfide
BRL
ug/kg dry
9.0
0.58
1
*8260B
3/10/11 21:16
KLA
PlCO235
Carbon Tetrachloride
BRL
ug/kg dry
4.5
0.45
1
*8260B
3/10/11 21:16
KLA
PlCO235
Chlorobenzene
BRL
ug/kg dry
4.5
0.66
1
*8260B
3/10/11 21:16
KLA
PlCO235
Chloroethane
BRL
ug/kg dry
9.0
0.57
1
*8260B
3/10/11 21:16
KLA
PlCO235
Chloroform
BRL
ug/kg dry
4.5
0.55
1
*8260B
3/10/11 21:16
KLA
PlCO235
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 23 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S5
Prism Sample ID: 1030182-17
Prism Work Order: 1030182
Time Collected: 03/08/11 12:10
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
9.0
0.48
1
*8260B
3/10/11 21:16
KLA
PlCO235
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.5
0.48
1
*8260B
3/10/11 21:16
KLA
PlCO235
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.5
0.47
1
*8260B
3/10/11 21:16
KLA
PlCO235
Dibromochloromethane
BRL
ug/kg dry
4.5
0.49
1
*8260B
3/10/11 21:16
KLA
PlCO235
Dibromomethane
BRL
ug/kg dry
4.5
0.44
1
*8260B
3/10/11 21:16
KLA
PlCO235
Dichlorodifluoromethane
BRL
ug/kg dry
9.0
0.53
1
*8260B
3/10/11 21:16
KLA
PlCO235
Ethylbenzene
BRL
ug/kg dry
4.5
0.64
1
*8260B
3/10/11 21:16
KLA
PlCO235
Hexachlorobutadiene
BRL
ug/kg dry
14
0.87
1
*8260B
3/10/11 21:16
KLA
PlCO235
Hexane
BRL
ug/kg dry
9.0
0.55
1
*8260B
3/10/11 21:16
KLA
PlCO235
Isopropyl Ether
BRL
ug/kg dry
4.5
0.43
1
*8260B
3/10/11 21:16
KLA
PlCO235
Isopropylbenzene (Cumene)
BRL
ug/kg dry
9.0
0.68
1
*8260B
3/10/11 21:16
KLA
PlCO235
m,p-Xylenes
BRL
ug/kg dry
9.0
1.2
1
*8260B
3/10/11 21:16
KLA
PlCO235
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
45
2.6
1
*8260B
3/10/11 21:16
KLA
PlCO235
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
18
4.3
1
*8260B
3/10/11 21:16
KLA
PlCO235
Methyl Isobutyl Ketone
BRL
ug/kg dry
9.0
0.87
1
*8260B
3/10/11 21:16
KLA
PlCO235
Methylene Chloride
BRL
ug/kg dry
9.0
0.38
1
*8260B
3/10/11 21:16
KLA
PlCO235
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.5
0.31
1
*8260B
3/10/11 21:16
KLA
PlCO235
Naphthalene
BRL
ug/kg dry
4.5
0.87
1
*8260B
3/10/11 21:16
KLA
PlCO235
n-Butylbenzene
BRL
ug/kg dry
14
0.80
1
*8260B
3/10/11 21:16
KLA
PlCO235
n-Propylbenzene
BRL
ug/kg dry
9.0
0.73
1
*8260B
3/10/11 21:16
KLA
PlCO235
o-Xylene
BRL
ug/kg dry
4.5
0.61
1
*8260B
3/10/11 21:16
KLA
PlCO235
sec-Butylbenzene
BRL
ug/kg dry
14
0.87
1
*8260B
3/10/11 21:16
KLA
PlCO235
Styrene
BRL
ug/kg dry
4.5
0.72
1
*8260B
3/10/11 21:16
KLA
PlCO235
tert-Butylbenzene
BRL
ug/kg dry
18
0.73
1
*8260B
3/10/11 21:16
KLA
PlCO235
Tetrachloroethylene
BRL
ug/kg dry
9.0
0.66
1
*8260B
3/10/11 21:16
KLA
PlCO235
Toluene
BRL
ug/kg dry
4.5
0.58
1
*8260B
3/10/11 21:16
KLA
PlCO235
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.5
0.67
1
*8260B
3/10/11 21:16
KLA
PlCO235
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.5
0.47
1
*8260B
3/10/11 21:16
KLA
PlCO235
Trichloroethylene
BRL
ug/kg dry
4.5
0.46
1
*8260B
3/10/11 21:16
KLA
PlCO235
Trichlorofluoromethane
BRL
ug/kg dry
4.5
0.51
1
*8260B
3/10/11 21:16
KLA
PlCO235
Vinyl acetate
BRL
ug/kg dry
9.0
0.66
1
*8260B
3/10/11 21:16
KLA
PlCO235
Vinyl chloride
BRL
ug/kg dry
9.0
0.52
1
*8260B
3/10/11 21:16
KLA
PlCO235
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
100 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S6
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-18
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 12:15
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
91.4
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
PlCO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.6
0.61
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
4.6
0.65
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.6
0.59
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
4.6
0.56
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
4.6
0.43
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
4.6
0.47
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
4.6
0.48
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
9.2
0.88
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
4.6
0.50
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
9.2
0.97
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
9.2
0.90
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.6
0.61
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
4.6
0.59
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
9.2
0.71
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
4.6
0.46
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
4.6
0.48
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
9.2
0.69
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
9.2
0.80
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
4.6
0.44
1
*8260B
3/10/11 13:44
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
9.2
0.77
1
*8260B
3/10/11 13:44
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
4.6
0.78
1
*8260B
3/10/11 13:44
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
9.2
0.53
1
*8260B
3/10/11 13:44
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
9.2
0.68
1
*8260B
3/10/11 13:44
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
9.2
0.81
1
*8260B
3/10/11 13:44
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
14
0.90
1
*8260B
3/10/11 13:44
KLA
PlCO210
Acetone
BRL
ug/kg dry
18
6.8
1
*8260B
3/10/11 13:44
KLA
PlCO210
Acrolein
BRL
ug/kg dry
92
0.72
1
*8260B
3/10/11 13:44
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
92
1.2
1
*8260B
3/10/11 13:44
KLA
PlCO210
Benzene
BRL
ug/kg dry
2.8
0.44
1
*8260B
3/10/11 13:44
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
4.6
0.66
1
*8260B
3/10/11 13:44
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
4.6
0.43
1
*8260B
3/10/11 13:44
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
4.6
0.45
1
*8260B
3/10/11 13:44
KLA
PlCO210
Bromoform
BRL
ug/kg dry
4.6
0.47
1
*8260B
3/10/11 13:44
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
9.2
0.58
1
*8260B
3/10/11 13:44
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
9.2
0.58
1
*8260B
3/10/11 13:44
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
4.6
0.46
1
*8260B
3/10/11 13:44
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
4.6
0.67
1
*8260B
3/10/11 13:44
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
9.2
0.58
1
*8260B
3/10/11 13:44
KLA
PlCO210
Chloroform
BRL
ug/kg dry
4.6
0.56
1
*8260B
3/10/11 13:44
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 25 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S6
Prism Sample ID: 1030182-18
Prism Work Order: 1030182
Time Collected: 03/08/11 12:15
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
9.2
0.48
1
*8260B
3/10/11 13:44
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.6
0.48
1
*8260B
3/10/11 13:44
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.6
0.48
1
*8260B
3/10/11 13:44
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
4.6
0.50
1
*8260B
3/10/11 13:44
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
4.6
0.45
1
*8260B
3/10/11 13:44
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
9.2
0.54
1
*8260B
3/10/11 13:44
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
4.6
0.65
1
*8260B
3/10/11 13:44
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
14
0.88
1
*8260B
3/10/11 13:44
KLA
PlCO210
Hexane
BRL
ug/kg dry
9.2
0.56
1
*8260B
3/10/11 13:44
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
4.6
0.44
1
*8260B
3/10/11 13:44
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
9.2
0.69
1
*8260B
3/10/11 13:44
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
9.2
1.3
1
*8260B
3/10/11 13:44
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
46
2.7
1
*8260B
3/10/11 13:44
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
18
4.3
1
*8260B
3/10/11 13:44
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
9.2
0.88
1
*8260B
3/10/11 13:44
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
9.2
0.38
1
*8260B
3/10/11 13:44
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.6
0.31
1
*8260B
3/10/11 13:44
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
4.6
0.88
1
*8260B
3/10/11 13:44
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
14
0.81
1
*8260B
3/10/11 13:44
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
9.2
0.74
1
*8260B
3/10/11 13:44
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
4.6
0.62
1
*8260B
3/10/11 13:44
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
14
0.88
1
*8260B
3/10/11 13:44
KLA
PlCO210
Styrene
BRL
ug/kg dry
4.6
0.73
1
*8260B
3/10/11 13:44
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
18
0.75
1
*8260B
3/10/11 13:44
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
9.2
0.67
1
*8260B
3/10/11 13:44
KLA
PlCO210
Toluene
BRL
ug/kg dry
4.6
0.59
1
*8260B
3/10/11 13:44
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.6
0.68
1
*8260B
3/10/11 13:44
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.6
0.48
1
*8260B
3/10/11 13:44
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
4.6
0.47
1
*8260B
3/10/11 13:44
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
4.6
0.52
1
*8260B
3/10/11 13:44
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
9.2
0.67
1
*8260B
3/10/11 13:44
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
9.2
0.53
1
*8260B
3/10/11 13:44
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
104 %
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
99 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S7
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-19
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 12:20
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
91.3
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
5.0
0.66
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
5.0
0.70
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
5.0
0.63
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
5.0
0.61
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
5.0
0.47
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
5.0
0.50
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
5.0
0.52
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
9.9
0.95
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
5.0
0.54
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
9.9
1.1
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
9.9
0.98
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
5.0
0.66
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
5.0
0.63
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
9.9
0.76
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
5.0
0.50
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
5.0
0.52
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
9.9
0.75
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
9.9
0.87
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
5.0
0.48
1
*8260B
3/10/11 13:11
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
9.9
0.84
1
*8260B
3/10/11 13:11
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
5.0
0.84
1
*8260B
3/10/11 13:11
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
9.9
0.57
1
*8260B
3/10/11 13:11
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
9.9
0.73
1
*8260B
3/10/11 13:11
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
9.9
0.88
1
*8260B
3/10/11 13:11
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
15
0.97
1
*8260B
3/10/11 13:11
KLA
PlCO210
Acetone
BRL
ug/kg dry
20
7.4
1
*8260B
3/10/11 13:11
KLA
PlCO210
Acrolein
BRL
ug/kg dry
99
0.78
1
*8260B
3/10/11 13:11
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
99
1.3
1
*8260B
3/10/11 13:11
KLA
PlCO210
Benzene
BRL
ug/kg dry
3.0
0.48
1
*8260B
3/10/11 13:11
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
5.0
0.71
1
*8260B
3/10/11 13:11
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
5.0
0.46
1
*8260B
3/10/11 13:11
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
5.0
0.49
1
*8260B
3/10/11 13:11
KLA
PlCO210
Bromoform
BRL
ug/kg dry
5.0
0.51
1
*8260B
3/10/11 13:11
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
9.9
0.62
1
*8260B
3/10/11 13:11
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
9.9
0.63
1
*8260B
3/10/11 13:11
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
5.0
0.50
1
*8260B
3/10/11 13:11
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
5.0
0.72
1
*8260B
3/10/11 13:11
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
9.9
0.62
1
*8260B
3/10/11 13:11
KLA
PlCO210
Chloroform
BRL
ug/kg dry
5.0
0.60
1
*8260B
3/10/11 13:11
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 27 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S7
Prism Sample ID: 1030182-19
Prism Work Order: 1030182
Time Collected: 03/08/11 12:20
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
9.9
0.52
1
*8260B
3/10/11 13:11
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
5.0
0.52
1
*8260B
3/10/11 13:11
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
5.0
0.52
1
*8260B
3/10/11 13:11
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
5.0
0.54
1
*8260B
3/10/11 13:11
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
5.0
0.48
1
*8260B
3/10/11 13:11
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
9.9
0.58
1
*8260B
3/10/11 13:11
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
5.0
0.70
1
*8260B
3/10/11 13:11
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
15
0.96
1
*8260B
3/10/11 13:11
KLA
PlCO210
Hexane
BRL
ug/kg dry
9.9
0.61
1
*8260B
3/10/11 13:11
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
5.0
0.47
1
*8260B
3/10/11 13:11
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
9.9
0.75
1
*8260B
3/10/11 13:11
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
9.9
1.4
1
*8260B
3/10/11 13:11
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
50
2.9
1
*8260B
3/10/11 13:11
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
20
4.7
1
*8260B
3/10/11 13:11
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
9.9
0.95
1
*8260B
3/10/11 13:11
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
9.9
0.41
1
*8260B
3/10/11 13:11
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
5.0
0.34
1
*8260B
3/10/11 13:11
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
5.0
0.95
1
*8260B
3/10/11 13:11
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
15
0.88
1
*8260B
3/10/11 13:11
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
9.9
0.80
1
*8260B
3/10/11 13:11
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
5.0
0.67
1
*8260B
3/10/11 13:11
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
15
0.95
1
*8260B
3/10/11 13:11
KLA
PlCO210
Styrene
BRL
ug/kg dry
5.0
0.79
1
*8260B
3/10/11 13:11
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
20
0.81
1
*8260B
3/10/11 13:11
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
9.9
0.72
1
*8260B
3/10/11 13:11
KLA
PlCO210
Toluene
BRL
ug/kg dry
5.0
0.63
1
*8260B
3/10/11 13:11
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
5.0
0.73
1
*8260B
3/10/11 13:11
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
5.0
0.52
1
*8260B
3/10/11 13:11
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
5.0
0.50
1
*8260B
3/10/11 13:11
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
5.0
0.56
1
*8260B
3/10/11 13:11
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
9.9
0.73
1
*8260B
3/10/11 13:11
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
9.9
0.57
1
*8260B
3/10/11 13:11
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
100 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S8
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-20
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 12:25
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
89.1
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.7
0.63
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,1,1-Trichloroethane
BRL
ug/kg dry
4.7
0.67
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.7
0.60
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,1,2-Trichloroethane
BRL
ug/kg dry
4.7
0.58
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,1-Dichloroethane
BRL
ug/kg dry
4.7
0.44
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,1-Dichloroethylene
BRL
ug/kg dry
4.7
0.48
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,1-Dichloropropylene
BRL
ug/kg dry
4.7
0.50
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2,3-Trichlorobenzene
BRL
ug/kg dry
9.4
0.91
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2,3-Trichloropropane
BRL
ug/kg dry
4.7
0.52
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2,4-Trichlorobenzene
BRL
ug/kg dry
9.4
1.0
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2,4-Trimethyl benzene
BRL
ug/kg dry
9.4
0.93
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.7
0.63
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2-Dibromoethane
BRL
ug/kg dry
4.7
0.60
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2-Dichlorobenzene
BRL
ug/kg dry
9.4
0.73
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2-Dichloroethane
BRL
ug/kg dry
4.7
0.47
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,2-Dichloropropane
BRL
ug/kg dry
4.7
0.50
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,3,5-Trimethyl benzene
BRL
ug/kg dry
9.4
0.71
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,3-Dichlorobenzene
BRL
ug/kg dry
9.4
0.82
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,3-Dichloropropane
BRL
ug/kg dry
4.7
0.46
1
*8260B
3/10/11 18:31
KLA
PlCO235
1,4-Dichlorobenzene
BRL
ug/kg dry
9.4
0.80
1
*8260B
3/10/11 18:31
KLA
PlCO235
2,2-Dichloropropane
BRL
ug/kg dry
4.7
0.80
1
*8260B
3/10/11 18:31
KLA
PlCO235
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
9.4
0.54
1
*8260B
3/10/11 18:31
KLA
PlCO235
2-Chlorotoluene
BRL
ug/kg dry
9.4
0.70
1
*8260B
3/10/11 18:31
KLA
PlCO235
4-Chlorotoluene
BRL
ug/kg dry
9.4
0.83
1
*8260B
3/10/11 18:31
KLA
PlCO235
4-Isopropyltoluene
BRL
ug/kg dry
14
0.92
1
*8260B
3/10/11 18:31
KLA
PlCO235
Acetone
BRL
ug/kg dry
19
7.0
1
*8260B
3/10/11 18:31
KLA
PlCO235
Acrolein
BRL
ug/kg dry
94
0.74
1
*8260B
3/10/11 18:31
KLA
PlCO235
Acrylonitrile
BRL
ug/kg dry
94
1.2
1
*8260B
3/10/11 18:31
KLA
PlCO235
Benzene
BRL
ug/kg dry
2.8
0.46
1
*8260B
3/10/11 18:31
KLA
PlCO235
Bromobenzene
BRL
ug/kg dry
4.7
0.68
1
*8260B
3/10/11 18:31
KLA
PlCO235
Bromochloromethane
BRL
ug/kg dry
4.7
0.44
1
*8260B
3/10/11 18:31
KLA
PlCO235
Bromodichloromethane
BRL
ug/kg dry
4.7
0.46
1
*8260B
3/10/11 18:31
KLA
PlCO235
Bromoform
BRL
ug/kg dry
4.7
0.49
1
*8260B
3/10/11 18:31
KLA
PlCO235
Bromomethane
BRL
ug/kg dry
9.4
0.59
1
*8260B
3/10/11 18:31
KLA
PlCO235
Carbon disulfide
BRL
ug/kg dry
9.4
0.60
1
*8260B
3/10/11 18:31
KLA
PlCO235
Carbon Tetrachloride
BRL
ug/kg dry
4.7
0.47
1
*8260B
3/10/11 18:31
KLA
PlCO235
Chlorobenzene
BRL
ug/kg dry
4.7
0.69
1
*8260B
3/10/11 18:31
KLA
PlCO235
Chloroethane
BRL
ug/kg dry
9.4
0.59
1
*8260B
3/10/11 18:31
KLA
PlCO235
Chloroform
BRL
ug/kg dry
4.7
0.57
1
*8260B
3/10/11 18:31
KLA
PlCO235
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 29 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S8
Prism Sample ID: 1030182-20
Prism Work Order: 1030182
Time Collected: 03/08/11 12:25
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
9.4
0.50
1
*8260B
3/10/11 18:31
KLA
PlCO235
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.7
0.50
1
*8260B
3/10/11 18:31
KLA
PlCO235
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.7
0.49
1
*8260B
3/10/11 18:31
KLA
PlCO235
Dibromochloromethane
BRL
ug/kg dry
4.7
0.51
1
*8260B
3/10/11 18:31
KLA
PlCO235
Dibromomethane
BRL
ug/kg dry
4.7
0.46
1
*8260B
3/10/11 18:31
KLA
PlCO235
Dichlorodifluoromethane
BRL
ug/kg dry
9.4
0.55
1
*8260B
3/10/11 18:31
KLA
PlCO235
Ethylbenzene
BRL
ug/kg dry
4.7
0.67
1
*8260B
3/10/11 18:31
KLA
PlCO235
Hexachlorobutadiene
BRL
ug/kg dry
14
0.91
1
*8260B
3/10/11 18:31
KLA
PlCO235
Hexane
BRL
ug/kg dry
9.4
0.58
1
*8260B
3/10/11 18:31
KLA
PlCO235
Isopropyl Ether
BRL
ug/kg dry
4.7
0.45
1
*8260B
3/10/11 18:31
KLA
PlCO235
Isopropylbenzene (Cumene)
BRL
ug/kg dry
9.4
0.71
1
*8260B
3/10/11 18:31
KLA
PlCO235
m,p-Xylenes
BRL
ug/kg dry
9.4
1.3
1
*8260B
3/10/11 18:31
KLA
PlCO235
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
47
2.7
1
*8260B
3/10/11 18:31
KLA
PlCO235
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
19
4.5
1
*8260B
3/10/11 18:31
KLA
PlCO235
Methyl Isobutyl Ketone
BRL
ug/kg dry
9.4
0.91
1
*8260B
3/10/11 18:31
KLA
PlCO235
Methylene Chloride
BRL
ug/kg dry
9.4
0.39
1
*8260B
3/10/11 18:31
KLA
PlCO235
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.7
0.32
1
*8260B
3/10/11 18:31
KLA
PlCO235
Naphthalene
BRL
ug/kg dry
4.7
0.91
1
*8260B
3/10/11 18:31
KLA
PlCO235
n-Butylbenzene
BRL
ug/kg dry
14
0.84
1
*8260B
3/10/11 18:31
KLA
PlCO235
n-Propylbenzene
BRL
ug/kg dry
9.4
0.76
1
*8260B
3/10/11 18:31
KLA
PlCO235
o-Xylene
BRL
ug/kg dry
4.7
0.64
1
*8260B
3/10/11 18:31
KLA
PlCO235
sec-Butylbenzene
BRL
ug/kg dry
14
0.90
1
*8260B
3/10/11 18:31
KLA
PlCO235
Styrene
BRL
ug/kg dry
4.7
0.75
1
*8260B
3/10/11 18:31
KLA
PlCO235
tert-Butylbenzene
BRL
ug/kg dry
19
0.77
1
*8260B
3/10/11 18:31
KLA
PlCO235
Tetrachloroethylene
BRL
ug/kg dry
9.4
0.69
1
*8260B
3/10/11 18:31
KLA
PlCO235
Toluene
BRL
ug/kg dry
4.7
0.60
1
*8260B
3/10/11 18:31
KLA
PlCO235
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.7
0.70
1
*8260B
3/10/11 18:31
KLA
PlCO235
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.7
0.49
1
*8260B
3/10/11 18:31
KLA
PlCO235
Trichloroethylene
BRL
ug/kg dry
4.7
0.48
1
*8260B
3/10/11 18:31
KLA
PlCO235
Trichlorofluoromethane
BRL
ug/kg dry
4.7
0.53
1
*8260B
3/10/11 18:31
KLA
PlCO235
Vinyl acetate
BRL
ug/kg dry
9.4
0.69
1
*8260B
3/10/11 18:31
KLA
PlCO235
Vinyl chloride
BRL
ug/kg dry
9.4
0.54
1
*8260B
3/10/11 18:31
KLA
PlCO235
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101
%
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
99 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S9
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-21
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 12:30
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
93.8
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
5.1
0.68
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
5.1
0.72
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
5.1
0.65
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
5.1
0.62
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
5.1
0.48
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
5.1
0.52
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
5.1
0.53
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
10
0.98
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
5.1
0.56
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
10
1.1
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
10
1.0
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
5.1
0.67
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
5.1
0.65
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
10
0.78
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
5.1
0.51
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
5.1
0.54
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
10
0.77
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
10
0.89
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
5.1
0.49
1
*8260B
3/10/11 12:05
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
10
0.86
1
*8260B
3/10/11 12:05
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
5.1
0.86
1
*8260B
3/10/11 12:05
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
10
0.58
1
*8260B
3/10/11 12:05
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
10
0.75
1
*8260B
3/10/11 12:05
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
10
0.90
1
*8260B
3/10/11 12:05
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
15
1.0
1
*8260B
3/10/11 12:05
KLA
PlCO210
Acetone
BRL
ug/kg dry
20
7.6
1
*8260B
3/10/11 12:05
KLA
PlCO210
Acrolein
BRL
ug/kg dry
100
0.80
1
*8260B
3/10/11 12:05
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
100
1.3
1
*8260B
3/10/11 12:05
KLA
PlCO210
Benzene
BRL
ug/kg dry
3.1
0.49
1
*8260B
3/10/11 12:05
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
5.1
0.73
1
*8260B
3/10/11 12:05
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
5.1
0.47
1
*8260B
3/10/11 12:05
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
5.1
0.50
1
*8260B
3/10/11 12:05
KLA
PlCO210
Bromoform
BRL
ug/kg dry
5.1
0.53
1
*8260B
3/10/11 12:05
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
10
0.64
1
*8260B
3/10/11 12:05
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
10
0.65
1
*8260B
3/10/11 12:05
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
5.1
0.51
1
*8260B
3/10/11 12:05
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
5.1
0.74
1
*8260B
3/10/11 12:05
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
10
0.64
1
*8260B
3/10/11 12:05
KLA
PlCO210
Chloroform
BRL
ug/kg dry
5.1
0.62
1
*8260B
3/10/11 12:05
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 31 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S9
Prism Sample ID: 1030182-21
Prism Work Order: 1030182
Time Collected: 03/08/11 12:30
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
10
0.54
1
*8260B
3/10/11 12:05
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
5.1
0.54
1
*8260B
3/10/11 12:05
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
5.1
0.53
1
*8260B
3/10/11 12:05
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
5.1
0.55
1
*8260B
3/10/11 12:05
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
5.1
0.50
1
*8260B
3/10/11 12:05
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
10
0.59
1
*8260B
3/10/11 12:05
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
5.1
0.72
1
*8260B
3/10/11 12:05
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
15
0.98
1
*8260B
3/10/11 12:05
KLA
PlCO210
Hexane
BRL
ug/kg dry
10
0.62
1
*8260B
3/10/11 12:05
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
5.1
0.48
1
*8260B
3/10/11 12:05
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
10
0.77
1
*8260B
3/10/11 12:05
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
10
1.4
1
*8260B
3/10/11 12:05
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
51
2.9
1
*8260B
3/10/11 12:05
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
20
4.8
1
*8260B
3/10/11 12:05
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
10
0.98
1
*8260B
3/10/11 12:05
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
10
0.42
1
*8260B
3/10/11 12:05
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
5.1
0.35
1
*8260B
3/10/11 12:05
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
5.1
0.98
1
*8260B
3/10/11 12:05
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
15
0.90
1
*8260B
3/10/11 12:05
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
10
0.82
1
*8260B
3/10/11 12:05
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
5.1
0.68
1
*8260B
3/10/11 12:05
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
15
0.97
1
*8260B
3/10/11 12:05
KLA
PlCO210
Styrene
BRL
ug/kg dry
5.1
0.81
1
*8260B
3/10/11 12:05
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
20
0.83
1
*8260B
3/10/11 12:05
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
10
0.74
1
*8260B
3/10/11 12:05
KLA
PlCO210
Toluene
BRL
ug/kg dry
5.1
0.65
1
*8260B
3/10/11 12:05
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
5.1
0.75
1
*8260B
3/10/11 12:05
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
5.1
0.53
1
*8260B
3/10/11 12:05
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
5.1
0.52
1
*8260B
3/10/11 12:05
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
5.1
0.57
1
*8260B
3/10/11 12:05
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
10
0.74
1
*8260B
3/10/11 12:05
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
10
0.58
1
*8260B
3/10/11 12:05
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101
%
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
99 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S10
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-22
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 14:05
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
89.5
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.8
0.64
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
4.8
0.68
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.8
0.61
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
4.8
0.58
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
4.8
0.45
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
4.8
0.49
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
9.6
0.92
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
4.8
0.53
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
9.6
1.0
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
9.6
0.94
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.8
0.64
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
4.8
0.61
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
9.6
0.74
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
4.8
0.48
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
9.6
0.72
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
9.6
0.84
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
4.8
0.46
1
*8260B
3/10/11 11:32
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
9.6
0.81
1
*8260B
3/10/11 11:32
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
4.8
0.81
1
*8260B
3/10/11 11:32
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
9.6
0.55
1
*8260B
3/10/11 11:32
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
9.6
0.71
1
*8260B
3/10/11 11:32
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
9.6
0.85
1
*8260B
3/10/11 11:32
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
14
0.94
1
*8260B
3/10/11 11:32
KLA
PlCO210
Acetone
BRL
ug/kg dry
19
7.1
1
*8260B
3/10/11 11:32
KLA
PlCO210
Acrolein
BRL
ug/kg dry
96
0.75
1
*8260B
3/10/11 11:32
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
96
1.2
1
*8260B
3/10/11 11:32
KLA
PlCO210
Benzene
BRL
ug/kg dry
2.9
0.46
1
*8260B
3/10/11 11:32
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
4.8
0.69
1
*8260B
3/10/11 11:32
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
4.8
0.45
1
*8260B
3/10/11 11:32
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
4.8
0.47
1
*8260B
3/10/11 11:32
KLA
PlCO210
Bromoform
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11 11:32
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
9.6
0.60
1
*8260B
3/10/11 11:32
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
9.6
0.61
1
*8260B
3/10/11 11:32
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
4.8
0.48
1
*8260B
3/10/11 11:32
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
4.8
0.70
1
*8260B
3/10/11 11:32
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
9.6
0.60
1
*8260B
3/10/11 11:32
KLA
PlCO210
Chloroform
BRL
ug/kg dry
4.8
0.58
1
*8260B
3/10/11 11:32
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 33 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S10
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-22
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 14:05
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Chloromethane
BRL
ug/kg dry
9.6
0.51
1
*8260B
3/10/11 11:32
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11 11:32
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11 11:32
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
4.8
0.52
1
*8260B
3/10/11 11:32
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
4.8
0.47
1
*8260B
3/10/11 11:32
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
9.6
0.56
1
*8260B
3/10/11 11:32
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
4.8
0.68
1
*8260B
3/10/11 11:32
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
14
0.92
1
*8260B
3/10/11 11:32
KLA
PlCO210
Hexane
BRL
ug/kg dry
9.6
0.58
1
*8260B
3/10/11 11:32
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
4.8
0.45
1
*8260B
3/10/11 11:32
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
9.6
0.72
1
*8260B
3/10/11 11:32
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
9.6
1.3
1
*8260B
3/10/11 11:32
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
48
2.8
1
*8260B
3/10/11 11:32
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
19
4.5
1
*8260B
3/10/11 11:32
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
9.6
0.92
1
*8260B
3/10/11 11:32
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
9.6
0.40
1
*8260B
3/10/11 11:32
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.8
0.33
1
*8260B
3/10/11 11:32
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
4.8
0.92
1
*8260B
3/10/11 11:32
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
14
0.85
1
*8260B
3/10/11 11:32
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
9.6
0.77
1
*8260B
3/10/11 11:32
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
4.8
0.64
1
*8260B
3/10/11 11:32
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
14
0.92
1
*8260B
3/10/11 11:32
KLA
PlCO210
Styrene
BRL
ug/kg dry
4.8
0.77
1
*8260B
3/10/11 11:32
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
19
0.78
1
*8260B
3/10/11 11:32
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
9.6
0.70
1
*8260B
3/10/11 11:32
KLA
PlCO210
Toluene
BRL
ug/kg dry
4.8
0.61
1
*8260B
3/10/11 11:32
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.8
0.71
1
*8260B
3/10/11 11:32
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11 11:32
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
4.8
0.49
1
*8260B
3/10/11 11:32
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
4.8
0.54
1
*8260B
3/10/11 11:32
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
9.6
0.70
1
*8260B
3/10/11 11:32
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
9.6
0.55
1
*8260B
3/10/11 11:32
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
104 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
101 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S11
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-23
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 14:15
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
88.7
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.0
0.53
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
4.0
0.57
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.0
0.51
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
4.0
0.49
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
4.0
0.38
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
4.0
0.40
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
4.0
0.42
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
8.0
0.77
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
4.0
0.44
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
8.0
0.85
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
8.0
0.78
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.0
0.53
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
4.0
0.51
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
8.0
0.61
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
4.0
0.40
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
4.0
0.42
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
8.0
0.60
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
8.0
0.70
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
4.0
0.38
1
*8260B
3/10/11 11:00
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
8.0
0.67
1
*8260B
3/10/11 11:00
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
4.0
0.68
1
*8260B
3/10/11 11:00
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
8.0
0.46
1
*8260B
3/10/11 11:00
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
8.0
0.59
1
*8260B
3/10/11 11:00
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
8.0
0.70
1
*8260B
3/10/11 11:00
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
12
0.78
1
*8260B
3/10/11 11:00
KLA
PlCO210
Acetone
BRL
ug/kg dry
16
5.9
1
*8260B
3/10/11 11:00
KLA
PlCO210
Acrolein
BRL
ug/kg dry
80
0.63
1
*8260B
3/10/11 11:00
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
80
1.0
1
*8260B
3/10/11 11:00
KLA
PlCO210
Benzene
BRL
ug/kg dry
2.4
0.39
1
*8260B
3/10/11 11:00
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
4.0
0.57
1
*8260B
3/10/11 11:00
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
4.0
0.37
1
*8260B
3/10/11 11:00
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
4.0
0.39
1
*8260B
3/10/11 11:00
KLA
PlCO210
Bromoform
BRL
ug/kg dry
4.0
0.41
1
*8260B
3/10/11 11:00
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
8.0
0.50
1
*8260B
3/10/11 11:00
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
8.0
0.51
1
*8260B
3/10/11 11:00
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
4.0
0.40
1
*8260B
3/10/11 11:00
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
4.0
0.58
1
*8260B
3/10/11 11:00
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
8.0
0.50
1
*8260B
3/10/11 11:00
KLA
PlCO210
Chloroform
BRL
ug/kg dry
4.0
0.48
1
*8260B
3/10/11 11:00
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 35 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S11
Prism Sample ID: 1030182-23
Prism Work Order: 1030182
Time Collected: 03/08/11 14:15
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
8.0
0.42
1
*8260B
3/10/11 11:00
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.0
0.42
1
*8260B
3/10/11 11:00
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.0
0.42
1
*8260B
3/10/11 11:00
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
4.0
0.43
1
*8260B
3/10/11 11:00
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
4.0
0.39
1
*8260B
3/10/11 11:00
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
8.0
0.47
1
*8260B
3/10/11 11:00
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
4.0
0.57
1
*8260B
3/10/11 11:00
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
12
0.77
1
*8260B
3/10/11 11:00
KLA
PlCO210
Hexane
BRL
ug/kg dry
8.0
0.49
1
*8260B
3/10/11 11:00
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
4.0
0.38
1
*8260B
3/10/11 11:00
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
8.0
0.60
1
*8260B
3/10/11 11:00
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
8.0
1.1
1
*8260B
3/10/11 11:00
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
40
2.3
1
*8260B
3/10/11 11:00
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
16
3.8
1
*8260B
3/10/11 11:00
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
8.0
0.77
1
*8260B
3/10/11 11:00
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
8.0
0.33
1
*8260B
3/10/11 11:00
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.0
0.27
1
*8260B
3/10/11 11:00
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
4.0
0.77
1
*8260B
3/10/11 11:00
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
12
0.71
1
*8260B
3/10/11 11:00
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
8.0
0.65
1
*8260B
3/10/11 11:00
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
4.0
0.54
1
*8260B
3/10/11 11:00
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
12
0.76
1
*8260B
3/10/11 11:00
KLA
PlCO210
Styrene
BRL
ug/kg dry
4.0
0.64
1
*8260B
3/10/11 11:00
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
16
0.65
1
*8260B
3/10/11 11:00
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
8.0
0.58
1
*8260B
3/10/11 11:00
KLA
PlCO210
Toluene
BRL
ug/kg dry
4.0
0.51
1
*8260B
3/10/11 11:00
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.0
0.59
1
*8260B
3/10/11 11:00
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.0
0.42
1
*8260B
3/10/11 11:00
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
4.0
0.41
1
*8260B
3/10/11 11:00
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
4.0
0.45
1
*8260B
3/10/11 11:00
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
8.0
0.58
1
*8260B
3/10/11 11:00
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
8.0
0.46
1
*8260B
3/10/11 11:00
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101
%
70-130
Dibromofluoromethane
104 %
84-123
Toluene-d8
98 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S12
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-24
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 14:00
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
91.4
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
PlCO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.4
0.58
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
4.4
0.62
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.4
0.56
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
4.4
0.53
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
4.4
0.41
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
4.4
0.44
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
4.4
0.46
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
8.8
0.84
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
4.4
0.48
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
8.8
0.93
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
8.8
0.86
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.4
0.58
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
4.4
0.56
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
8.8
0.67
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
4.4
0.44
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
4.4
0.46
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
8.8
0.66
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
8.8
0.76
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
4.4
0.42
1
*8260B
3/10/11 10:27
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
8.8
0.74
1
*8260B
3/10/11 10:27
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
4.4
0.74
1
*8260B
3/10/11 10:27
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
8.8
0.50
1
*8260B
3/10/11 10:27
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
8.8
0.65
1
*8260B
3/10/11 10:27
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
8.8
0.77
1
*8260B
3/10/11 10:27
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
13
0.86
1
*8260B
3/10/11 10:27
KLA
PlCO210
Acetone
BRL
ug/kg dry
18
6.5
1
*8260B
3/10/11 10:27
KLA
PlCO210
Acrolein
BRL
ug/kg dry
88
0.69
1
*8260B
3/10/11 10:27
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
88
1.1
1
*8260B
3/10/11 10:27
KLA
PlCO210
Benzene
BRL
ug/kg dry
2.6
0.42
1
*8260B
3/10/11 10:27
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
4.4
0.63
1
*8260B
3/10/11 10:27
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
4.4
0.41
1
*8260B
3/10/11 10:27
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
4.4
0.43
1
*8260B
3/10/11 10:27
KLA
PlCO210
Bromoform
BRL
ug/kg dry
4.4
0.45
1
*8260B
3/10/11 10:27
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
8.8
0.55
1
*8260B
3/10/11 10:27
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
8.8
0.56
1
*8260B
3/10/11 10:27
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
4.4
0.44
1
*8260B
3/10/11 10:27
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
4.4
0.64
1
*8260B
3/10/11 10:27
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
8.8
0.55
1
*8260B
3/10/11 10:27
KLA
PlCO210
Chloroform
BRL
ug/kg dry
4.4
0.53
1
*8260B
3/10/11 10:27
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 37 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S12
Prism Sample ID: 1030182-24
Prism Work Order: 1030182
Time Collected: 03/08/11 14:00
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
8.8
0.46
1
*8260B
3/10/11 10:27
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.4
0.46
1
*8260B
3/10/11 10:27
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.4
0.46
1
*8260B
3/10/11 10:27
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
4.4
0.47
1
*8260B
3/10/11 10:27
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
4.4
0.43
1
*8260B
3/10/11 10:27
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
8.8
0.51
1
*8260B
3/10/11 10:27
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
4.4
0.62
1
*8260B
3/10/11 10:27
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
13
0.84
1
*8260B
3/10/11 10:27
KLA
PlCO210
Hexane
BRL
ug/kg dry
8.8
0.53
1
*8260B
3/10/11 10:27
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
4.4
0.41
1
*8260B
3/10/11 10:27
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
8.8
0.66
1
*8260B
3/10/11 10:27
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
8.8
1.2
1
*8260B
3/10/11 10:27
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
44
2.5
1
*8260B
3/10/11 10:27
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
18
4.1
1
*8260B
3/10/11 10:27
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
8.8
0.84
1
*8260B
3/10/11 10:27
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
8.8
0.36
1
*8260B
3/10/11 10:27
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.4
0.30
1
*8260B
3/10/11 10:27
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
4.4
0.84
1
*8260B
3/10/11 10:27
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
13
0.78
1
*8260B
3/10/11 10:27
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
8.8
0.71
1
*8260B
3/10/11 10:27
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
4.4
0.59
1
*8260B
3/10/11 10:27
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
13
0.84
1
*8260B
3/10/11 10:27
KLA
PlCO210
Styrene
BRL
ug/kg dry
4.4
0.70
1
*8260B
3/10/11 10:27
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
18
0.71
1
*8260B
3/10/11 10:27
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
8.8
0.64
1
*8260B
3/10/11 10:27
KLA
PlCO210
Toluene
BRL
ug/kg dry
4.4
0.56
1
*8260B
3/10/11 10:27
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.4
0.65
1
*8260B
3/10/11 10:27
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.4
0.46
1
*8260B
3/10/11 10:27
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
4.4
0.45
1
*8260B
3/10/11 10:27
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
4.4
0.49
1
*8260B
3/10/11 10:27
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
8.8
0.64
1
*8260B
3/10/11 10:27
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
8.8
0.50
1
*8260B
3/10/11 10:27
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
106 %
84-123
Toluene-d8
100 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S13
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-25
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 14:10
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
92.3
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
PlCO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.2
0.57
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
4.2
0.60
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.2
0.54
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
4.2
0.52
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
4.2
0.40
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
4.2
0.43
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
8.5
0.81
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
4.2
0.46
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
8.5
0.90
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
8.5
0.83
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.2
0.56
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
4.2
0.54
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
8.5
0.65
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
4.2
0.43
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
4.2
0.45
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
8.5
0.64
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
8.5
0.74
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
4.2
0.41
1
*8260B
3/10/11
9:54
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
8.5
0.72
1
*8260B
3/10/11
9:54
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
4.2
0.72
1
*8260B
3/10/11
9:54
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
8.5
0.48
1
*8260B
3/10/11
9:54
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
8.5
0.63
1
*8260B
3/10/11
9:54
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
8.5
0.75
1
*8260B
3/10/11
9:54
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
13
0.83
1
*8260B
3/10/11
9:54
KLA
PlCO210
Acetone
BRL
ug/kg dry
17
6.3
1
*8260B
3/10/11
9:54
KLA
PlCO210
Acrolein
BRL
ug/kg dry
85
0.67
1
*8260B
3/10/11
9:54
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
85
1.1
1
*8260B
3/10/11
9:54
KLA
PlCO210
Benzene
BRL
ug/kg dry
2.5
0.41
1
*8260B
3/10/11
9:54
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
4.2
0.61
1
*8260B
3/10/11
9:54
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
4.2
0.40
1
*8260B
3/10/11
9:54
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
4.2
0.42
1
*8260B
3/10/11
9:54
KLA
PlCO210
Bromoform
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11
9:54
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
8.5
0.53
1
*8260B
3/10/11
9:54
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
8.5
0.54
1
*8260B
3/10/11
9:54
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
4.2
0.42
1
*8260B
3/10/11
9:54
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
4.2
0.62
1
*8260B
3/10/11
9:54
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
8.5
0.53
1
*8260B
3/10/11
9:54
KLA
PlCO210
Chloroform
BRL
ug/kg dry
4.2
0.51
1
*8260B
3/10/11
9:54
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 39 of 59

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Sample Matrix: Solid
Laboratory Report
03/14/2011
Client Sample ID: T2-S13
Prism Sample ID: 1030182-25
Prism Work Order: 1030182
Time Collected: 03/08/11 14:10
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
BRL
ug/kg dry
8.5
0.45
1
*8260B
3/10/11
9:54
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.2
0.45
1
*8260B
3/10/11
9:54
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11
9:54
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
4.2
0.46
1
*8260B
3/10/11
9:54
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
4.2
0.41
1
*8260B
3/10/11
9:54
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
8.5
0.50
1
*8260B
3/10/11
9:54
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
4.2
0.60
1
*8260B
3/10/11
9:54
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
13
0.82
1
*8260B
3/10/11
9:54
KLA
PlCO210
Hexane
BRL
ug/kg dry
8.5
0.52
1
*8260B
3/10/11
9:54
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
4.2
0.40
1
*8260B
3/10/11
9:54
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
8.5
0.64
1
*8260B
3/10/11
9:54
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
8.5
1.2
1
*8260B
3/10/11
9:54
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
42
2.4
1
*8260B
3/10/11
9:54
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
17
4.0
1
*8260B
3/10/11
9:54
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
8.5
0.81
1
*8260B
3/10/11
9:54
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
8.5
0.35
1
*8260B
3/10/11
9:54
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.2
0.29
1
*8260B
3/10/11
9:54
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
4.2
0.81
1
*8260B
3/10/11
9:54
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
13
0.75
1
*8260B
3/10/11
9:54
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
8.5
0.68
1
*8260B
3/10/11
9:54
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
4.2
0.57
1
*8260B
3/10/11
9:54
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
13
0.81
1
*8260B
3/10/11
9:54
KLA
PlCO210
Styrene
BRL
ug/kg dry
4.2
0.68
1
*8260B
3/10/11
9:54
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
17
0.69
1
*8260B
3/10/11
9:54
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
8.5
0.62
1
*8260B
3/10/11
9:54
KLA
PlCO210
Toluene
BRL
ug/kg dry
4.2
0.54
1
*8260B
3/10/11
9:54
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.2
0.63
1
*8260B
3/10/11
9:54
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.2
0.44
1
*8260B
3/10/11
9:54
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
4.2
0.43
1
*8260B
3/10/11
9:54
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
4.2
0.48
1
*8260B
3/10/11
9:54
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
8.5
0.62
1
*8260B
3/10/11
9:54
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
8.5
0.49
1
*8260B
3/10/11
9:54
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
70-130
Dibromofluoromethane
106 %
84-123
Toluene-d8
100 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S14
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-26
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 14:20
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
% Solids
88.6
% by
0.100
0.100
1
*SM2540 G
319/11 15:45
JAB
P1CO208
Weight
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
ug/kg dry
4.8
0.65
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,1,1-Trichloroethane
BRL
ug/kg dry
4.8
0.68
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,1,2,2-Tetrachloroethane
BRL
ug/kg dry
4.8
0.62
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,1,2-Trichloroethane
BRL
ug/kg dry
4.8
0.59
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,1-Dichloroethane
BRL
ug/kg dry
4.8
0.45
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,1-Dichloroethylene
BRL
ug/kg dry
4.8
0.49
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,1-Dichloropropylene
BRL
ug/kg dry
4.8
0.51
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2,3-Trichlorobenzene
BRL
ug/kg dry
9.7
0.93
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2,3-Trichloropropane
BRL
ug/kg dry
4.8
0.53
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2,4-Trichlorobenzene
BRL
ug/kg dry
9.7
1.0
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2,4-Trimethyl benzene
BRL
ug/kg dry
9.7
0.95
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2-Dibromo-3-chloropropane
BRL
ug/kg dry
4.8
0.64
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2-Dibromoethane
BRL
ug/kg dry
4.8
0.62
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2-Dichlorobenzene
BRL
ug/kg dry
9.7
0.74
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2-Dichloroethane
BRL
ug/kg dry
4.8
0.49
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,2-Dichloropropane
BRL
ug/kg dry
4.8
0.51
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,3,5-Trimethyl benzene
BRL
ug/kg dry
9.7
0.73
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,3-Dichlorobenzene
BRL
ug/kg dry
9.7
0.84
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,3-Dichloropropane
BRL
ug/kg dry
4.8
0.47
1
*8260B
3/10/11
9:21
KLA
PlCO210
1,4-Dichlorobenzene
BRL
ug/kg dry
9.7
0.82
1
*8260B
3/10/11
9:21
KLA
PlCO210
2,2-Dichloropropane
BRL
ug/kg dry
4.8
0.82
1
*8260B
3/10/11
9:21
KLA
PlCO210
2-Chloroethyl Vinyl Ether
BRL
ug/kg dry
9.7
0.55
1
*8260B
3/10/11
9:21
KLA
PlCO210
2-Chlorotoluene
BRL
ug/kg dry
9.7
0.72
1
*8260B
3/10/11
9:21
KLA
PlCO210
4-Chlorotoluene
BRL
ug/kg dry
9.7
0.85
1
*8260B
3/10/11
9:21
KLA
PlCO210
4-Isopropyltoluene
BRL
ug/kg dry
14
0.95
1
*8260B
3/10/11
9:21
KLA
PlCO210
Acetone
BRL
ug/kg dry
19
7.2
1
*8260B
3/10/11
9:21
KLA
PlCO210
Acrolein
BRL
ug/kg dry
97
0.76
1
*8260B
3/10/11
9:21
KLA
PlCO210
Acrylonitrile
BRL
ug/kg dry
97
1.2
1
*8260B
3/10/11
9:21
KLA
PlCO210
Benzene
BRL
ug/kg dry
2.9
0.47
1
*8260B
3/10/11
9:21
KLA
PlCO210
Bromobenzene
BRL
ug/kg dry
4.8
0.69
1
*8260B
3/10/11
9:21
KLA
PlCO210
Bromochloromethane
BRL
ug/kg dry
4.8
0.45
1
*8260B
3/10/11
9:21
KLA
PlCO210
Bromodichloromethane
BRL
ug/kg dry
4.8
0.48
1
*8260B
3/10/11
9:21
KLA
PlCO210
Bromoform
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11
9:21
KLA
PlCO210
Bromomethane
BRL
ug/kg dry
9.7
0.61
1
*8260B
3/10/11
9:21
KLA
PlCO210
Carbon disulfide
BRL
ug/kg dry
9.7
0.62
1
*8260B
3/10/11
9:21
KLA
PlCO210
Carbon Tetrachloride
BRL
ug/kg dry
4.8
0.48
1
*8260B
3/10/11
9:21
KLA
PlCO210
Chlorobenzene
BRL
ug/kg dry
4.8
0.70
1
*8260B
3/10/11
9:21
KLA
PlCO210
Chloroethane
BRL
ug/kg dry
9.7
0.61
1
*8260B
3/10/11
9:21
KLA
PlCO210
Chloroform
BRL
ug/kg dry
4.8
0.58
1
*8260B
3/10/11
9:21
KLA
PlCO210
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 41 of 59

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 03/14/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T2-S14
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030182-26
3334 Hillsborough St. Prism Work Order: 1030182
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/08/11 14:20
Time Submitted: 03/09/11 16:25
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Chloromethane
BRL
ug/kg dry
9.7
0.51
1
*8260B
3/10/11
9:21
KLA
PlCO210
cis-1,2-Dichloroethylene
BRL
ug/kg dry
4.8
0.51
1
*8260B
3/10/11
9:21
KLA
PlCO210
cis-1,3-Dichloropropylene
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11
9:21
KLA
PlCO210
Dibromochloromethane
BRL
ug/kg dry
4.8
0.52
1
*8260B
3/10/11
9:21
KLA
PlCO210
Dibromomethane
BRL
ug/kg dry
4.8
0.47
1
*8260B
3/10/11
9:21
KLA
PlCO210
Dichlorodifluoromethane
BRL
ug/kg dry
9.7
0.56
1
*8260B
3/10/11
9:21
KLA
PlCO210
Ethylbenzene
BRL
ug/kg dry
4.8
0.69
1
*8260B
3/10/11
9:21
KLA
PlCO210
Hexachlorobutadiene
BRL
ug/kg dry
14
0.93
1
*8260B
3/10/11
9:21
KLA
PlCO210
Hexane
BRL
ug/kg dry
9.7
0.59
1
*8260B
3/10/11
9:21
KLA
PlCO210
Isopropyl Ether
BRL
ug/kg dry
4.8
0.46
1
*8260B
3/10/11
9:21
KLA
PlCO210
Isopropylbenzene (Cumene)
BRL
ug/kg dry
9.7
0.73
1
*8260B
3/10/11
9:21
KLA
PlCO210
m,p-Xylenes
BRL
ug/kg dry
9.7
1.3
1
*8260B
3/10/11
9:21
KLA
PlCO210
Methyl Butyl Ketone (2-Hexanone)
BRL
ug/kg dry
48
2.8
1
*8260B
3/10/11
9:21
KLA
PlCO210
Methyl Ethyl Ketone (2-Butanone)
BRL
ug/kg dry
19
4.6
1
*8260B
3/10/11
9:21
KLA
PlCO210
Methyl Isobutyl Ketone
BRL
ug/kg dry
9.7
0.93
1
*8260B
3/10/11
9:21
KLA
PlCO210
Methylene Chloride
BRL
ug/kg dry
9.7
0.40
1
*8260B
3/10/11
9:21
KLA
PlCO210
Methyl-tert-Butyl Ether
BRL
ug/kg dry
4.8
0.33
1
*8260B
3/10/11
9:21
KLA
PlCO210
Naphthalene
BRL
ug/kg dry
4.8
0.93
1
*8260B
3/10/11
9:21
KLA
PlCO210
n-Butylbenzene
BRL
ug/kg dry
14
0.86
1
*8260B
3/10/11
9:21
KLA
PlCO210
n-Propylbenzene
BRL
ug/kg dry
9.7
0.78
1
*8260B
3/10/11
9:21
KLA
PlCO210
o-Xylene
BRL
ug/kg dry
4.8
0.65
1
*8260B
3/10/11
9:21
KLA
PlCO210
sec-Butylbenzene
BRL
ug/kg dry
14
0.92
1
*8260B
3/10/11
9:21
KLA
PlCO210
Styrene
BRL
ug/kg dry
4.8
0.77
1
*8260B
3/10/11
9:21
KLA
PlCO210
tert-Butylbenzene
BRL
ug/kg dry
19
0.78
1
*8260B
3/10/11
9:21
KLA
PlCO210
Tetrachloroethylene
BRL
ug/kg dry
9.7
0.70
1
*8260B
3/10/11
9:21
KLA
PlCO210
Toluene
BRL
ug/kg dry
4.8
0.62
1
*8260B
3/10/11
9:21
KLA
PlCO210
trans-1,2-Dichloroethylene
BRL
ug/kg dry
4.8
0.71
1
*8260B
3/10/11
9:21
KLA
PlCO210
trans-1,3-Dichloropropylene
BRL
ug/kg dry
4.8
0.50
1
*8260B
3/10/11
9:21
KLA
PlCO210
Trichloroethylene
BRL
ug/kg dry
4.8
0.49
1
*8260B
3/10/11
9:21
KLA
PlCO210
Trichlorofluoromethane
BRL
ug/kg dry
4.8
0.55
1
*8260B
3/10/11
9:21
KLA
PlCO210
Vinyl acetate
BRL
ug/kg dry
9.7
0.71
1
*8260B
3/10/11
9:21
KLA
PlCO210
Vinyl chloride
BRL
ug/kg dry
9.7
0.55
1
*8260B
3/10/11
9:21
KLA
PlCO210
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
102 %
70-130
Dibromofluoromethane
105 %
84-123
Toluene-d8
101 %
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 59

P R I IS M EService Analytical s
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/14/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030182
Attn: Kevin Buchanan Time Submitted: 3/9/11 4:25:OOPM
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO210 - 5035
Blank (PlCO210-BLK1)
Prepared: 03/09/11 Analyzed: 03/10/11
1,1,1,2-Tetrachloroethane
BRL
5.0
ug/kg wet
1,1,1-Trichloroethane
BRL
5.0
ug/kg wet
1,1,2,2-Tetrachloroethane
BRL
5.0
ug/kg wet
1,1,2-Trichloroethane
BRL
5.0
ug/kg wet
1,1-Dichloroethane
BRL
5.0
ug/kg wet
1,1-Dichloroethylene
BRL
5.0
ug/kg wet
1,1-Dichloropropylene
BRL
5.0
ug/kg wet
1,2,3-Trichlorobenzene
BRL
10
ug/kg wet
1,2,3-Trichloropropane
BRL
5.0
ug/kg wet
1,2,4-Trichlorobenzene
BRL
10
ug/kg wet
1,2,4-Trimethyl benzene
BRL
10
ug/kg wet
1,2-Dibromo-3-chloropropane
BRL
5.0
ug/kg wet
1,2-Dibromoethane
BRL
5.0
ug/kg wet
1,2-Dichlorobenzene
BRL
10
ug/kg wet
1,2-Dichloroethane
BRL
5.0
ug/kg wet
1,2-Dichloropropane
BRL
5.0
ug/kg wet
1,3,5-Trimethyl benzene
BRL
10
ug/kg wet
1,3-Dichlorobenzene
BRL
10
ug/kg wet
1,3-Dichloropropane
BRL
5.0
ug/kg wet
1,4-Dichlorobenzene
BRL
10
ug/kg wet
2,2-Dichloropropane
BRL
5.0
ug/kg wet
2-Chloroethyl Vinyl Ether
BRL
10
ug/kg wet
2-Chlorotoluene
BRL
10
ug/kg wet
4-Chlorotoluene
BRL
10
ug/kg wet
4-Isopropyltoluene
BRL
15
ug/kg wet
Acetone
BRL
20
ug/kg wet
Acrolein
BRL
100
ug/kg wet
Acrylonitrile
BRL
100
ug/kg wet
Benzene
BRL
3.0
ug/kg wet
Bromobenzene
BRL
5.0
ug/kg wet
Bromochloromethane
BRL
5.0
ug/kg wet
Bromodichloromethane
BRL
5.0
ug/kg wet
Bromoform
BRL
5.0
ug/kg wet
Bromomethane
BRL
10
ug/kg wet
Carbon disulfide
BRL
10
ug/kg wet
Carbon Tetrachloride
BRL
5.0
ug/kg wet
Chlorobenzene
BRL
5.0
ug/kg wet
Chloroethane
BRL
10
ug/kg wet
Chloroform
BRL
5.0
ug/kg wet
Chloromethane
BRL
10
ug/kg wet
cis-1,2-Dichloroethylene
BRL
5.0
ug/kg wet
cis-1,3-Dichloropropylene
BRL
5.0
ug/kg wet
Dibromochloromethane
BRL
5.0
ug/kg wet
Dibromomethane
BRL
5.0
ug/kg wet
Dichlorodifluoromethane
BRL
10
ug/kg wet
Ethylbenzene
BRL
5.0
ug/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
3/14/11
Prism Work Order: 1030182
Time Submitted: 3/9/11 4:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO210 - 5035
Blank (P1CO210-BLK1)
Prepared: 03/09/11 Analyzed: 03/10/11
Hexachlorobutadiene
BRL
15
ug/kg wet
Hexane
BRL
10
ug/kg wet
Isopropyl Ether
BRL
5.0
ug/kg wet
Isopropylbenzene (Cumene)
BRL
10
ug/kg wet
m,p-Xylenes
BRL
10
ug/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
50
ug/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
20
ug/kg wet
Methyl Isobutyl Ketone
BRL
10
ug/kg wet
Methylene Chloride
BRL
10
ug/kg wet
Methyl-tert-Butyl Ether
BRL
5.0
ug/kg wet
Naphthalene
BRL
5.0
ug/kg wet
n-Butylbenzene
BRL
15
ug/kg wet
n-Propylbenzene
BRL
10
ug/kg wet
o-Xylene
BRL
5.0
ug/kg wet
sec-Butylbenzene
BRL
15
ug/kg wet
Styrene
BRL
5.0
ug/kg wet
tert-Butylbenzene
BRL
20
ug/kg wet
Tetrachloroethylene
BRL
10
ug/kg wet
Toluene
BRL
5.0
ug/kg wet
trans-1,2-Dichloroethylene
BRL
5.0
ug/kg wet
trans-1,3-Dichloropropylene
BRL
5.0
ug/kg wet
Trichloroethylene
BRL
5.0
ug/kg wet
Trichlorofluoromethane
BRL
5.0
ug/kg wet
Vinyl acetate
BRL
10
ug/kg wet
Vinyl chloride
BRL
10
ug/kg wet
Surrogate:4-Bromofluorobenzene
50.8
ug/L
50.0 102 70-130
Surrogate: Dibromofluoromethane
50.9
ug/L
50.0 102 84-123
Surrogate: Toluene-d8
51.1
ug/L
50.0 102 76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 44 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
3/14/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030182
Attn: Kevin Buchanan Time Submitted: 3/9/11 4:25:OOPM
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO210 - 5035
LCS (PlCO210-BSI)
Prepared: 03/09/11 Analyzed: 03/10/11
1,1-Dichloroethylene
49.8
5.0
ug/kg wet
50.0
100
67-149
Benzene
42.6
3.0
ug/kg wet
50.0
85
74-127
Chlorobenzene
42.2
5.0
ug/kg wet
50.0
84
74-118
Toluene
42.8
5.0
ug/kg wet
50.0
86
71-129
Trichloroethylene
43.7
5.0
ug/kg wet
50.0
87
75-133
Surrogate:4-Bromofluorobenzene
50.7
ug/L
50.0
101
70-130
Surrogate: Dibromofluoromethane
49.7
ug/L
50.0
99
84-123
Surrogate: Toluene-d8
50.0
ug/L
50.0
100
76-129
LCS Dup (PlCO210-BSD1)
Prepared: 03/09/11
Analyzed: 03/10/11
1,1-Dichloroethylene
50.5
5.0
ug/kg wet
50.0
101
67-149
1
Benzene
42.7
3.0
ug/kg wet
50.0
85
74-127
0.4
Chlorobenzene
42.0
5.0
ug/kg wet
50.0
84
74-118
0.5
Toluene
42.6
5.0
ug/kg wet
50.0
85
71-129
0.4
Trichloroethylene
43.6
5.0
ug/kg wet
50.0
87
75-133
0.2
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.0
101
70-130
Surrogate: Dibromofluoromethane
50.2
ug/L
50.0
100
84-123
Surrogate: Toluene-d8
50.1
ug/L
50.0
100
76-129
Matrix Spike (P1CO210-MS1)
Source: 1030182-26
Prepared: 03/09/11
Analyzed: 03/10/11
1,1-Dichloroethylene
63.1
5.6
ug/kg dry
56.4 BRL
112
54-162
22
Benzene
53.3
3.4
ug/kg dry
56.4 BRL
94
60-135
20
Chlorobenzene
51.6
5.6
ug/kg dry
56.4 BRL
92
57-125
14
Toluene
53.2
5.6
ug/kg dry
56.4 BRL
94
57-135
22
Trichloroethylene
54.8
5.6
ug/kg dry
56.4 BRL
97
38-164
18
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.0
100
70-130
Surrogate: Dibromofluoromethane
49.6
ug/L
50.0
99
84-123
Surrogate: Toluene-d8
50.4
ug/L
50.0
101
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
3/14/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030182
Attn: Kevin Buchanan Time Submitted: 3/9/11 4:25:OOPM
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO210 - 5035
Matrix Spike Dup (PlCO210-MSD1)
Source: 1030182-26
Prepared: 03/09/11 Analyzed: 03/10/11
1,1-Dichloroethylene
60.2
5.6
ug/kg dry
56.4
BRL
107
54-162
5
22
Benzene
52.2
3.4
ug/kg dry
56.4
BRL
92
60-135
2
20
Chlorobenzene
48.8
5.6
ug/kg dry
56.4
BRL
86
57-125
6
14
Toluene
50.5
5.6
ug/kg dry
56.4
BRL
90
57-135
5
22
Trichloroethylene
51.2
5.6
ug/kg dry
56.4
BRL
91
38-164
7
18
Surrogate:4-Bromofluorobenzene
50.6
ug/L
50.0
101
70-130
Surrogate: Dibromofluoromethane
50.3
ug/L
50.0
101
84-123
Surrogate: Toluene-d8
49.1
ug/L
50.0
98
76-129
Batch P1 CO235 - 5035
Blank (PlCO235-BLK1)
Prepared & Analyzed: 03/10/11
1,1,1,2-Tetrachloroethane
BRL
5.0
ug/kg wet
1,1,1-Trichloroethane
BRL
5.0
ug/kg wet
1,1,2,2-Tetrachloroethane
BRL
5.0
ug/kg wet
1,1,2-Trichloroethane
BRL
5.0
ug/kg wet
1,1-Dichloroethane
BRL
5.0
ug/kg wet
1,1-Dichloroethylene
BRL
5.0
ug/kg wet
1,1-Dichloropropylene
BRL
5.0
ug/kg wet
1,2,3-Trichlorobenzene
BRL
10
ug/kg wet
1,2,3-Trichloropropane
BRL
5.0
ug/kg wet
1,2,4-Trichlorobenzene
BRL
10
ug/kg wet
1,2,4-Trimethyl benzene
BRL
10
ug/kg wet
1,2-Dibromo-3-chloropropane
BRL
5.0
ug/kg wet
1,2-Dibromoethane
BRL
5.0
ug/kg wet
1,2-Dichlorobenzene
BRL
10
ug/kg wet
1,2-Dichloroethane
BRL
5.0
ug/kg wet
1,2-Dichloropropane
BRL
5.0
ug/kg wet
1,3,5-Trimethyl benzene
BRL
10
ug/kg wet
1,3-Dichlorobenzene
BRL
10
ug/kg wet
1,3-Dichloropropane
BRL
5.0
ug/kg wet
1,4-Dichlorobenzene
BRL
10
ug/kg wet
2,2-Dichloropropane
BRL
5.0
ug/kg wet
2-Chloroethyl Vinyl Ether
BRL
10
ug/kg wet
2-Chlorotoluene
BRL
10
ug/kg wet
4-Chlorotoluene
BRL
10
ug/kg wet
4-Isopropyltoluene
BRL
15
ug/kg wet
Acetone
BRL
20
ug/kg wet
Acrolein
BRL
100
ug/kg wet
Acrylonitrile
BRL
100
ug/kg wet
Benzene
BRL
3.0
ug/kg wet
Bromobenzene
BRL
5.0
ug/kg wet
Bromochloromethane
BRL
5.0
ug/kg wet
Bromodichloromethane
BRL
5.0
ug/kg wet
Bromoform
BRL
5.0
ug/kg wet
Bromomethane
BRL
10
ug/kg wet
Carbon disulfide
BRL
10
ug/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
3/14/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030182
Attn: Kevin Buchanan Time Submitted: 3/9/11 4:25:OOPM
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO235 - 5035
Blank (PlCO235-BLK1)
Prepared & Analyzed: 03/10/11
Carbon Tetrachloride
BRL
5.0
ug/kg wet
Chlorobenzene
BRL
5.0
ug/kg wet
Chloroethane
BRL
10
ug/kg wet
Chloroform
BRL
5.0
ug/kg wet
Chloromethane
BRL
10
ug/kg wet
cis-1,2-Dichloroethylene
BRL
5.0
ug/kg wet
cis-1,3-Dichloropropylene
BRL
5.0
ug/kg wet
Dibromochloromethane
BRL
5.0
ug/kg wet
Dibromomethane
BRL
5.0
ug/kg wet
Dichlorodifluoromethane
BRL
10
ug/kg wet
Ethylbenzene
BRL
5.0
ug/kg wet
Hexachlorobutadiene
BRL
15
ug/kg wet
Hexane
BRL
10
ug/kg wet
Isopropyl Ether
BRL
5.0
ug/kg wet
Isopropylbenzene (Cumene)
BRL
10
ug/kg wet
m,p-Xylenes
BRL
10
ug/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
50
ug/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
20
ug/kg wet
Methyl Isobutyl Ketone
BRL
10
ug/kg wet
Methylene Chloride
BRL
10
ug/kg wet
Methyl-tert-Butyl Ether
BRL
5.0
ug/kg wet
Naphthalene
BRL
5.0
ug/kg wet
n-Butylbenzene
BRL
15
ug/kg wet
n-Propylbenzene
BRL
10
ug/kg wet
o-Xylene
BRL
5.0
ug/kg wet
sec-Butylbenzene
BRL
15
ug/kg wet
Styrene
BRL
5.0
ug/kg wet
tert-Butylbenzene
BRL
20
ug/kg wet
Tetrachloroethylene
BRL
10
ug/kg wet
Toluene
BRL
5.0
ug/kg wet
trans-1,2-Dichloroethylene
BRL
5.0
ug/kg wet
trans-1,3-Dichloropropylene
BRL
5.0
ug/kg wet
Trichloroethylene
BRL
5.0
ug/kg wet
Trichlorofluoromethane
BRL
5.0
ug/kg wet
Vinyl acetate
BRL
10
ug/kg wet
Vinyl chloride
BRL
10
ug/kg wet
Surrogate:4-Bromofluorobenzene
51.1
ug/L
50.0 102 70-130
Surrogate: Dibromofluoromethane
52.2
ug/L
50.0 104 84-123
Surrogate: Toluene-d8
49.8
ug/L
50.0 100 76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
3/14/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030182
Attn: Kevin Buchanan Time Submitted: 3/9/11 4:25:OOPM
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO235 - 5035
LCS (PlCO235-BSI)
Prepared & Analyzed: 03/10/11
1,1-Dichloroethylene
58.7
5.0
ug/kg wet
50.0
117
67-149
Benzene
47.2
3.0
ug/kg wet
50.0
94
74-127
Chlorobenzene
47.8
5.0
ug/kg wet
50.0
96
74-118
Toluene
47.7
5.0
ug/kg wet
50.0
95
71-129
Trichloroethylene
49.2
5.0
ug/kg wet
50.0
98
75-133
Surrogate:4-Bromofluorobenzene
50.5
ug/L
50.0
101
70-130
Surrogate: Dibromofluoromethane
50.1
ug/L
50.0
100
84-123
Surrogate: Toluene-d8
49.5
ug/L
50.0
99
76-129
LCS Dup (P1CO235-13SD1)
Prepared & Analyzed:
03/10/11
1,1-Dichloroethylene
56.4
5.0
ug/kg wet
50.0
113
67-149
4
Benzene
46.5
3.0
ug/kg wet
50.0
93
74-127
2
Chlorobenzene
46.6
5.0
ug/kg wet
50.0
93
74-118
3
Toluene
47.0
5.0
ug/kg wet
50.0
94
71-129
2
Trichloroethylene
48.6
5.0
ug/kg wet
50.0
97
75-133
1
Surrogate:4-Bromofluorobenzene
49.7
ug/L
50.0
99
70-130
Surrogate: Dibromofluoromethane
49.9
ug/L
50.0
100
84-123
Surrogate: Toluene-d8
48.9
ug/L
50.0
98
76-129
Matrix Spike (PlCO235-MS1)
Source: 1030182-13
Prepared & Analyzed:
03/10/11
1,1-Dichloroethylene
57.8
5.6
ug/kg dry
56.4 BRL
103
54-162
22
Benzene
46.8
3.4
ug/kg dry
56.4 BRL
83
60-135
20
Chlorobenzene
47.4
5.6
ug/kg dry
56.4 BRL
84
57-125
14
Toluene
47.5
5.6
ug/kg dry
56.4 BRL
84
57-135
22
Trichloroethylene
47.5
5.6
ug/kg dry
56.4 BRL
84
38-164
18
Surrogate:4-Bromofluorobenzene
49.2
ug/L
50.0
98
70-130
Surrogate: Dibromofluoromethane
49.9
ug/L
50.0
100
84-123
Surrogate: Toluene-d8
50.1
ug/L
50.0
100
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
3/14/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030182
Attn: Kevin Buchanan Time Submitted: 3/9/11 4:25:OOPM
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO235 - 5035
Matrix Spike Dup (P1CO235-MSD1)
Source: 1030182-13
Prepared & Analyzed: 03/10/11
1,1-Dichloroethylene
55.1
5.6
ug/kg dry
56.4
BRL
98
54-162
5
22
Benzene
44.9
3.4
ug/kg dry
56.4
BRL
80
60-135
4
20
Chlorobenzene
43.1
5.6
ug/kg dry
56.4
BRL
77
57-125
9
14
Toluene
45.1
5.6
ug/kg dry
56.4
BRL
80
57-135
5
22
Trichloroethylene
44.9
5.6
ug/kg dry
56.4
BRL
80
38-164
6
18
Surrogate:4-Bromofluorobenzene
50.8
ug/L
50.0
102
70-130
Surrogate: Dibromofluoromethane
51.1
ug/L
50.0
102
84-123
Surrogate: Toluene-d8
49.7
ug/L
50.0
99
76-129
Batch P1 CO270 - 5035
Blank (PlCO270-BLK1)
Prepared & Analyzed: 03/11/11
1,1,1,2-Tetrachloroethane
BRL
5.0
ug/kg wet
1,1,1-Trichloroethane
BRL
5.0
ug/kg wet
1,1,2,2-Tetrachloroethane
BRL
5.0
ug/kg wet
1,1,2-Trichloroethane
BRL
5.0
ug/kg wet
1,1-Dichloroethane
BRL
5.0
ug/kg wet
1,1-Dichloroethylene
BRL
5.0
ug/kg wet
1,1-Dichloropropylene
BRL
5.0
ug/kg wet
1,2,3-Trichlorobenzene
BRL
10
ug/kg wet
1,2,3-Trichloropropane
BRL
5.0
ug/kg wet
1,2,4-Trichlorobenzene
BRL
10
ug/kg wet
1,2,4-Trimethyl benzene
BRL
10
ug/kg wet
1,2-Dibromo-3-chloropropane
BRL
5.0
ug/kg wet
1,2-Dibromoethane
BRL
5.0
ug/kg wet
1,2-Dichlorobenzene
BRL
10
ug/kg wet
1,2-Dichloroethane
BRL
5.0
ug/kg wet
1,2-Dichloropropane
BRL
5.0
ug/kg wet
1,3,5-Trimethyl benzene
BRL
10
ug/kg wet
1,3-Dichlorobenzene
BRL
10
ug/kg wet
1,3-Dichloropropane
BRL
5.0
ug/kg wet
1,4-Dichlorobenzene
BRL
10
ug/kg wet
2,2-Dichloropropane
BRL
5.0
ug/kg wet
2-Chloroethyl Vinyl Ether
BRL
10
ug/kg wet
2-Chlorotoluene
BRL
10
ug/kg wet
4-Chlorotoluene
BRL
10
ug/kg wet
4-Isopropyltoluene
BRL
15
ug/kg wet
Acetone
BRL
20
ug/kg wet
Acrolein
BRL
100
ug/kg wet
Acrylonitrile
BRL
100
ug/kg wet
Benzene
BRL
3.0
ug/kg wet
Bromobenzene
BRL
5.0
ug/kg wet
Bromochloromethane
BRL
5.0
ug/kg wet
Bromodichloromethane
BRL
5.0
ug/kg wet
Bromoform
BRL
5.0
ug/kg wet
Bromomethane
BRL
10
ug/kg wet
Carbon disulfide
BRL
10
ug/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
3/14/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030182
Attn: Kevin Buchanan Time Submitted: 3/9/11 4:25:OOPM
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO270 - 5035
Blank (PlCO270-BLK1)
Prepared & Analyzed: 03/11/11
Carbon Tetrachloride
BRL
5.0
ug/kg wet
Chlorobenzene
BRL
5.0
ug/kg wet
Chloroethane
BRL
10
ug/kg wet
Chloroform
BRL
5.0
ug/kg wet
Chloromethane
BRL
10
ug/kg wet
cis-1,2-Dichloroethylene
BRL
5.0
ug/kg wet
cis-1,3-Dichloropropylene
BRL
5.0
ug/kg wet
Dibromochloromethane
BRL
5.0
ug/kg wet
Dibromomethane
BRL
5.0
ug/kg wet
Dichlorodifluoromethane
BRL
10
ug/kg wet
Ethylbenzene
BRL
5.0
ug/kg wet
Hexachlorobutadiene
BRL
15
ug/kg wet
Hexane
BRL
10
ug/kg wet
Isopropyl Ether
BRL
5.0
ug/kg wet
Isopropylbenzene (Cumene)
BRL
10
ug/kg wet
m,p-Xylenes
BRL
10
ug/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
50
ug/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
20
ug/kg wet
Methyl Isobutyl Ketone
BRL
10
ug/kg wet
Methylene Chloride
BRL
10
ug/kg wet
Methyl-tert-Butyl Ether
BRL
5.0
ug/kg wet
Naphthalene
BRL
5.0
ug/kg wet
n-Butylbenzene
BRL
15
ug/kg wet
n-Propylbenzene
BRL
10
ug/kg wet
o-Xylene
BRL
5.0
ug/kg wet
sec-Butylbenzene
BRL
15
ug/kg wet
Styrene
BRL
5.0
ug/kg wet
tert-Butylbenzene
BRL
20
ug/kg wet
Tetrachloroethylene
BRL
10
ug/kg wet
Toluene
BRL
5.0
ug/kg wet
trans-1,2-Dichloroethylene
BRL
5.0
ug/kg wet
trans-1,3-Dichloropropylene
BRL
5.0
ug/kg wet
Trichloroethylene
BRL
5.0
ug/kg wet
Trichlorofluoromethane
BRL
5.0
ug/kg wet
Vinyl acetate
BRL
10
ug/kg wet
Vinyl chloride
BRL
10
ug/kg wet
Surrogate:4-Bromofluorobenzene
52.2
ug/L
50.0 104 70-130
Surrogate: Dibromofluoromethane
52.3
ug/L
50.0 105 84-123
Surrogate: Toluene-d8
51.2
ug/L
50.0 102 76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report
3/14/11
Prism Work Order: 1030182
Time Submitted: 3/9/11 4:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO270 - 5035
LCS (PlCO270-BSI)
Prepared & Analyzed: 03/11/11
1,1-Dichloroethylene
53.6
5.0
ug/kg wet
50.0
107
67-149
Benzene
43.2
3.0
ug/kg wet
50.0
86
74-127
Chlorobenzene
42.5
5.0
ug/kg wet
50.0
85
74-118
Hexane
41.0
10
ug/kg wet
50.0
82
70-130
Toluene
43.6
5.0
ug/kg wet
50.0
87
71-129
Trichloroethylene
43.6
5.0
ug/kg wet
50.0
87
75-133
Surrogate:4-Bromofluorobenzene
50.9
ug/L
50.0
102
70-130
Surrogate: Dibromofluoromethane
50.7
ug/L
50.0
101
84-123
Surrogate: Toluene-d8
49.8
ug/L
50.0
100
76-129
LCS Dup (PlCO270-BSD1)
Prepared & Analyzed: 03/11/11
1,1-Dichloroethylene
56.3
5.0
ug/kg wet
50.0
113
67-149
5
Benzene
44.7
3.0
ug/kg wet
50.0
89
74-127
3
Chlorobenzene
44.0
5.0
ug/kg wet
50.0
88
74-118
3
Hexane
41.6
10
ug/kg wet
50.0
83
70-130
2
Toluene
45.3
5.0
ug/kg wet
50.0
91
71-129
4
Trichloroethylene
46.2
5.0
ug/kg wet
50.0
92
75-133
6
Surrogate:4-Bromofluorobenzene
51.0
ug/L
50.0
102
70-130
Surrogate: Dibromofluoromethane
50.2
ug/L
50.0
100
84-123
Surrogate: Toluene-d8
49.5
ug/L
50.0
99
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 51 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Gasoline Range Organics by GC/FID - Quality Control
Level II QC Report
3/14/11
Prism Work Order: 1030182
Time Submitted: 3/9/11 4:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO233 - 5035
Blank (PlCO233-BLK1)
Prepared: 03/09/11 Analyzed: 03/10/11
Gasoline Range Organics
BRL
5.0
mg/kg wet
Surrogate: a,a,a-Trifluorotoluene
0.0980
mg/kg wet
0.100 98
55-129
LCS (PlCO233-BSI)
Prepared & Analyzed: 03/09/11
Gasoline Range Organics
0.955
0.10
mg/kg wet
1.00 96
67-116
Surrogate: a,a,a-Trifluorotoluene
0.110
mg/kg wet
0.100 110
55-129
LCS Dup (P1CO233-BSD1)
Prepared & Analyzed: 03/09/11
Gasoline Range Organics
1.01
0.10
mg/kg wet
1.00 101
67-116 5 200
Surrogate: a,a,a-Trifluorotoluene
0.112
mg/kg wet
0.100 112
55-129
Matrix Spike (PlCO233-MSI)
Source: 1030182-01
Prepared & Analyzed: 03/09/11
Gasoline Range Organics
1.12
0.11
mg/kg dry
1.13 BRL 99
57-113
Surrogate: a,a,a-Trifluorotoluene
0.130
mg/kg dry
0.226 58
55-129
Matrix Spike Dup (PlCO233-MSD1)
Source: 1030182-01
Prepared & Analyzed: 03/09/11
Gasoline Range Organics
1.05
0.11
mg/kg dry
1.11 BRL 94
57-113 7 23
Surrogate: a,a,a-Trifluorotoluene
0.129
mg/kg dry
0.222 58
55-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 52 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Diesel Range Organics by GC/FID - Quality Control
Level II QC Report
3/14/11
Prism Work Order: 1030182
Time Submitted: 3/9/11 4:25:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO214 - 3545A
Blank (PlCO214-BLK1)
Prepared: 03/09/11 Analyzed: 03/10/11
Diesel Range Organics
BRL
7.0
mg/kg wet
Surrogate: o-Terphenyl
1.15
mg/kg wet
1.60 72 49-124
LCS (PlCO214-BSI)
Prepared: 03/09/11 Analyzed: 03/10/11
Diesel Range Organics
52.7
7.0
mg/kg wet
79.9 66 55-109
Surrogate: o-Terphenyl
1.06
mg/kg wet
1.60 66 49-124
LCS Dup (PlCO214-BSD1)
Prepared: 03/09/11 Analyzed: 03/10/11
Diesel Range Organics
54.4
7.0
mg/kg wet
79.8 68 55-109 3 200
Surrogate: o-Terphenyl
1.11
mg/kg wet
1.60 69 49-124
Matrix Spike (PlCO214-MSI)
Source: 1030182-01
Prepared: 03/09/11 Analyzed: 03/10/11
Diesel Range Organics
65.0
7.9
mg/kg dry
89.7 BRL 72 50-117
Surrogate: o-Terphenyl
1.33
mg/kg dry
1.79 74 49-124
Matrix Spike Dup (PlCO214-MSD1)
Source: 1030182-01
Prepared: 03/09/11 Analyzed: 03/10/11
Diesel Range Organics
67.4
7.8
mg/kg dry
89.7 BRL 75 50-117 4 24
Surrogate: o-Terphenyl
1.31
mg/kg dry
1.79 73 49-124
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 53 of 59

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
General Chemistry Parameters - Quality Control
Analyte
Batch P1CO208 - NO PREP
Project: City of Rocky Mount (CRM-008)
Level II QC Report
3/14/11
Prism Work Order: 1030182
Time Submitted: 3/9/11 4:25:OOPM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (PlCO208-BLK1) Prepared & Analyzed: 03/09/11
% Solids 100 0.100 % by Weight
Duplicate (PlCO208-DUP2) Source: 1030182-11 Prepared & Analyzed: 03/09/11
% Solids 92.4 0.100 % by Weight 92.2 0.2 20
Duplicate (PlCO208-DUP3) Source: 1030182-24 Prepared & Analyzed: 03/09/11
% Solids 91.6 0.100 % by Weight 91.4 0.2 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 54 of 59

Sample Extraction Data
Prep Method: 3545A
Lab Number Batch Initial Final Date
1030182-01
P1CO214
25.18
g 1 mL
03/09/11
1030182-02
P1CO214
25.12
g 1 mL
03/09/11
1030182-03
P1CO214
25.01
g 1 mL
03/09/11
1030182-04
P1CO214
25
g 1 mL
03/09/11
1030182-05
P1CO214
25.26
g 1 mL
03/09/11
1030182-06
P1CO214
25.22
g 1 mL
03/09/11
1030182-07
P1CO214
25.25
g 1 mL
03/09/11
1030182-08
P1CO214
25.28
g 1 mL
03/09/11
1030182-09
P1CO214
25.04
g 1 mL
03/09/11
1030182-10
P1CO214
25.1
g 1 mL
03/09/11
1030182-11
P1CO214
25.25
g 1 mL
03/09/11
1030182-12
P1CO214
25.25
g 1 mL
03/09/11
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date
1030182-01
P1CO233
6.64
g 5 mL
03/09/11
1030182-02
P1CO233
6.84
g 5 mL
03/09/11
1030182-03
P1CO233
6.9
g 5 mL
03/09/11
1030182-04
P1CO233
4.64
g 5 mL
03/09/11
1030182-05
PlCO233
5.45
g 5 mL
03/09/11
1030182-06
P1CO233
5.3
g 5 mL
03/09/11
1030182-07
P1CO233
6.61
g 5 mL
03/09/11
1030182-08
P1CO233
6.05
g 5 mL
03/09/11
1030182-09
P1CO233
6.15
g 5 mL
03/09/11
1030182-10
P1CO233
5.11
g 5 mL
03/09/11
1030182-11
P1CO233
5.52
g 5 mL
03/09/11
1030182-12
P1CO233
7.93
g 5 mL
03/09/11
NO PREP
Lab Number
Batch
Initial
Final
Date
1030182-01
P1CO208
30
g 30 mL
03/09/11
1030182-02
P1CO208
30
g 30 mL
03/09/11
1030182-03
P1CO208
30
g 30 mL
03/09/11
1030182-04
P1CO208
30
g 30 mL
03/09/11
1030182-05
PlCO208
30
g 30 mL
03/09/11
1030182-06
P1CO208
30
g 30 mL
03/09/11
1030182-07
P1CO208
30
g 30 mL
03/09/11
1030182-08
P1CO208
30
g 30 mL
03/09/11
1030182-09
P1CO208
30
g 30 mL
03/09/11
1030182-10
P1CO208
30
g 30 mL
03/09/11
1030182-11
P1CO208
30
g 30 mL
03/09/11
1030182-12
P1CO208
30
g 30 mL
03/09/11
1030182-13
PlCO208
30
g 30 mL
03/09/11
1030182-14
P1CO208
30
g 30 mL
03/09/11
1030182-15
P1CO208
30
g 30 mL
03/09/11
1030182-16
P1CO208
30
g 30 mL
03/09/11
1030182-17
P1CO208
30
g 30 mL
03/09/11
1030182-18
P1CO208
30
g 30 mL
03/09/11
1030182-19
P1CO208
30
g 30 mL
03/09/11
1030182-20
P1CO208
30
g 30 mL
03/09/11
1030182-21
PlCO208
30
g 30 mL
03/09/11
1030182-22
P1CO208
30
g 30 mL
03/09/11
1030182-23
P1CO208
30
g 30 mL
03/09/11
1030182-24
P1CO208
30
g 30 mL
03/09/11
1030182-25
P1CO208
30
g 30 mL
03/09/11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 59

Sample Extraction Data
NO PREP
Lab Number Batch Initial Final Date
1030182-26 P1CO208 30 g 30 mL 03/09/11
Prep Method: 5035
Lab Number Batch Initial Final Date
1030182-13
P1CO235
6.7
g 5 mL
03/10/11
1030182-14
P1CO270
6.44
g 5 mL
03/11/11
1030182-15
P1CO235
6.52
g 5 mL
03/10/11
1030182-16
P1CO235
6.2
g 5 mL
03/10/11
1030182-17
P1CO235
6.16
g 5 mL
03/10/11
1030182-18
P1CO210
5.96
g 5 mL
03/09/11
1030182-19
P1CO210
5.52
g 5 mL
03/09/11
1030182-20
PlCO235
5.94
g 5 mL
03/10/11
1030182-21
P1CO210
5.24
g 5 mL
03/09/11
1030182-22
P1CO210
5.83
g 5 mL
03/09/11
1030182-23
P1CO210
7.06
g 5 mL
03/09/11
1030182-24
P1CO210
6.25
g 5 mL
03/09/11
1030182-25
P1CO210
6.39
g 5 mL
03/09/11
1030182-26
P1CO210
5.84
g 5 mL
03/09/11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 Of 59

Full -Service Analytical & CHAIN OF CUSTODY RECORD
&R. ISM I Environmental Solutions PAGE -/ OF 3 QUOTE # TO ENSURE PROPER BILLING:
LABORATORIES ING G/ !/� d�/NT- �t'i¢-�✓jZ�7ZS O/G/�ij,
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543 project Name:
Phone: [phone] • Fax: [phone] Short Hold Analysis: (Yes) to . UST Project: (Yi3p (No)
Client Company Name: !>fi1.��G.rtii�.✓,/�� "Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
Y_IAIZIIG1,A'1 V provisions and/or QC Requirements
Report To/Contact Name: Zf
Reporting Addressi �l/ ��Q_l-, ,fT Invoice To: 1��/� GI/P%�S
�U���� NG 27tvO"j Address:
n i p n i rs J am/ i—
Phone: 7'17 �=y / Fax (Yes) (No):
Email (Yes) (No) Email Address %�.�riG�Nl�i✓
EDD Type: PDF Excel Other
Site Location Name:TL��foi�����
Site Location Physical Address: /OO¢ 4Ltl�
(C /
Purchase Order No./Billing Reference �' DOS -__
Requested Due Date ❑ 1 Day afDa ❑ 3 Days ❑ 4 Days ❑ 5 Days
"Working Days" ❑ 6-9 Days ❑ Standard 10 day S ork Mus
re -Approved
Samples received after 15:00 wilf be processed next buss
Turnaround time is based on business days, excluding weekends and holidays.
(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES, INC. TO CLIENT)
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: NELAC USACE FL NC
SC OTHER NIA
Water Chlorinated: YES— NO
Sample Iced Upon Collection: YES --`NO
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA_
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ANALYSES REQUESTED
REMARKS
PRISM
LAB
ID NO
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Sampled By (Print Name)
Affiliation
Upon relinq ishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must
subrnittfdA writing t9_tJie Prism Project Manager. There will be charges for any changes after analyses have been initialized.
be
Relinquis By: (Slgnatur Received ey: ( 1
c�%
Relinquish d By: (Sign I elved By: (S na ure)
R uished`By: (Si ure) ei d For Pris Labor s By:
Melho6dl Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUI WITH UST DY SEALS FOR TRANSPORTATION TO THE LABORATORY.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINSIf5POUNTIL RECEIVED AT THE LABORATORY.
❑ Fed Ex ❑ ups ❑ Hand -delivered r sm Field Service ❑ Other
ate % Military/Hours Additiomments:
DAdditional C
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NPDES: GR�TfNDWATER: DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑ NC ❑ S l ClC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC Q NC Q SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC Page 57 of 59
*CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

Full -Service Analytical &
P I S M Environmental Solutions
LABORATORIES Ir1G
449 Springbrook Road • P.O. Box 240543 • Charlotte, NC 28224-0543
Phone:[phone] • Fax:[phone]
Client Company Name:f�///G� �G -
ReportTo/ContactName: ZLL-YYi�/��/G�An/LIr✓
Reporting Address: 3334 fii//SG�IJv�i��r` -
�c,�i��YG z7�o7
Phone- &fW-7 AZel Fax (Yes) (No):
Email (Yes) (No) Email Address /-- 6�G11
EDD Type: PDF_ Excel ____Other
Site Location Name:
Site Location Physical Addr9ps: /OOP e:�f `
TIME
MATRIX
CLIENT
DATE
COLLECTED
(SOIL,
SAMPLE DESCRIPTION
COLLECTED
MILITARY
WATER OR
HOURS
SLUDGE)
CHAIN OF CUSTODY RECORD
PAGE Z OF J QUOTE # TO ENSURE PROPER BILLING:
Project Name:e em&
Short Hold Analysis: (Yes) (No) LIST Project: (Yes) (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 11 111 IV)
provisions and/or QC Requirements
Invoice To: _ �1i✓T/i� !�/G�lf
Address:
Purchase Order No./Billing ce t!�iPY►'G�� TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Requested Due Date ❑ 1 Day Da ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC USACE FL NC-k
"Working Days" ❑ 6 9 Days ❑Standard 10 day s or t Be
rAe Approved SC OTHER N/A
Samples received after 15:00 will be processed next b
Turnaround time is based on business days, excluding weekends and holidays. Water Chlorinated: YES _ NO _
(SEE REVERSE FOR TERMS R CONDITIONS REGARDING SERVICES Sample Iced Upon Collection: YES !/ NO
RENDERED BY PRISM LABORATORIES, INC. TO CLIENTi p -
SAMPLE CONTAINER ANALYSES qEQUESTED PRISM
PRE5ERVA- IDLAB
NO.
'TYPE TIVES REMARKS
SEE BELOW NO. SIZE
Z -S/
T Z _-.SZ
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Sampler's Signature
Sampled By (Print Name) d� v�
Affiliation
Upon refl qufshing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
subroltWU In writing he rism Project Manager. There will be charges for ppy changes after analyses Pave been initialized.
Reli ' hed BY: (Sig nat
Received By: (Sig at ) j
7`'
3
3% /r
Military/Hours
OYis3.�
Additional Comments_
elinq }shed By: (Signat re
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Date
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SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINIiCC UNTIL RECEIVED AT THE LABORATORY.
� d j 0LB
❑ Fed Ex ❑ UPS ❑ Hand -delivered rism FMd Service ❑ Other
NPDES: j T GR UNDWATER: I DRINKING WATER: SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
❑NC ❑SC L]SC ❑NC ❑SC i UNC USC ❑NC DSC ❑NC ❑SC ❑NC ❑SC i❑NC ❑SC� Li NC Li SC
Ll
"CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
19
ZD
Page 58 of 59

Pam! RISMI
LABORATORIES, ING
Full -Service Analytical &
Environmental Solutions
449 Springbrook Road @ P.O. Box 240543 + Charlotte, NC 28224-0543
Phone:[phone] • Fax:704J525-0409/,
Client Company Name:
Report To/Contact Name: /��111 �yGs%il/
Reporting Address: 3 ¢ h�rllreo" ST.
� -74 ti25 7_74�4,7
CHAIN OF CUSTODY RECORD
PAGE - -ZOF_-,F-- QUOTE # TO ENSURE PROPER BILLING:
Project Name:icrl__'f-,� ^YexfOre- /Wy
Short Hold Analysis: (Yes) (No) UST Project: CQ (No)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV}
provisions and/or QC Requirements
Invoice To: Ci(/T/1/;4 W,;,/l� -
Address:
Phone: y�711 ?7011 Fax (Yes) (No): - fiO�
�5v Purchase Order No./Billing Reference
Email (Yes) (No) Email Address �`% Requested Due Date ❑ I Day r 2 r ❑ 3 Days ❑ 4 Days 0 5 Days
EDD Type: PDF Excel _Other "Working Days" ❑ 6-9 Days ❑ Standard 10 days or us
Site Location Name: �, 47/� ��u Pre -Approved
�, � / Samples received after 15:00 will be processed next bustn
Site Location Physical A dress: OOI 4r Turnaround tsme is based an business days, excluding weekends and holidays.
&ALA* Z?k±2/7' A4 (SEE REVERSE FOR TERMS iR CONDITIONS REGARDING SERVICES
� 1 - RENDERED 6Y PRISM LABORATORIES, INC. TO CLIENT)
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: NELAC USAGE FL NC
SCOTHER N/A
Water Chlorinated: YES_ NO
Sample Iced Upon Collection: YES a�NO
P �
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
MATRIX
(SOIL,
WATER OR
SLUDGE)
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
s
p� pyC1
REMARKS
+� Y�////Z
(�
PRISM
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Sampler's SignatureC4
Sampled By (Print Name)
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SlteArnYaETlrr#e �.,
Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
submitted in writoig to the Prism Project Manager. There will be charges for any changes after analyses have been Initialized.
Relinquished B . (S ature)
Received By: (Signature
Date
MilitaryMms pu
Additional Comments:
Sdq DBparttY,e Ttme
Relinquish By: Sign l
Rscei d By: (SignaTu
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to f
-✓�� �l
%
Mileage
od of Shipment NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED S UT WIT CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAI ST C UNTIL RECEIVED AT THE LABORATORY.
0 Fed Ex ❑ UPS ❑ Hand -delivered rism Field Service ❑ Other
C C up No.
L V D t
N❑PDES: I GROUNDWATER: DRINKING WATER: I SOLID WASTE: RCRA: CERCLA LANDFILL OTHER:
SC i ❑ RC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC :INC ❑ SC Ll NC ❑ SC ❑ NC ClSC ❑ NC ElSC Page 59 of 59
'CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)

Confirmatory Sample T1-S11A
(Risk -Based Analyses)
Hart & Hickman, PC

Case Narrative
PRI S M Full -Service Analytical &
JI I Environmental Solutions
LABORATORIES, INC.
Hart & Hickman (Raleigh)
Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Project: City of Rocky Mount (CRM-008)
Project No.: CRM-008
Lab Submittal Date: 03/22/2011
Prism Work Order: 1030539
04/04/2011
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By
D RPD value outside of the control limits.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
M Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 23

Sample Receipt Summary
fflyaR I S M Full -Service Analytical R 04/04/2011
Environmental Solutions
LABORATORIES, INC.
Prism Work Order: 1030539
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
T1-S11A 1030539-01 Solid 03/21/11 03/22/11
Samples received in good condition at 6.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 23

�P R I S M Summary of Detections
�,, Full -Service Analytical &
Environmental Solutions 04/04/2011
LABORATORIES, INC.
Prism Work Order: 1030539
Prism ID Client ID Parameter Method Result Units
1030539-01 T1-S11A C9-C12 Aliphatics 'MADEP VPH 13 mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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%j6P R I S M Fun -Service Analytical
Environmental Solutions
LABORATORIES, INC.
Laboratory Report
04/04/2011
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Project No.: CRM-008
Sample Matrix: Solid
Client Sample ID: T1-S11A
Prism Sample ID: 1030539-01
Prism Work Order: 1030539
Time Collected: 03/21/11 15:40
Time Submitted: 03/22/11 14:45
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-Cl8 Aliphatics BRL mg/kg dry 11 0.72 1 *MADEP EPH 3/30/11 3:50 GRR P1C0559
C19-C36 Aliphatics BRL mg/kg dry 11 1.2 1 *MADEP EPH 3/30/11 3:50 GRR P1C0559
C11-C22 Aromatics BRL mg/kg dry 11 3.1 1 *MADEP EPH 3/30/11 4:41 GRR P1C0559
Surrogate Recovery Control Limits
1-Chlorooctadecane
55 %
40-140
o-Terphenyl
73 %
40-140
2-Fluorobiphenyl
59 %
40-140
2-Bromonaphthalene
82 %
40-140
General Chemistry Parameters
% Solids
88.0
% by
0.100
0.100
1
*SM2540 G
3124/11 15:00
JAB
PlC0546
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
1,2-Dichlorobenzene
BRL
mg/kg dry
0.38
0.12
1
*8270D
3/28/11 16:07
KC
PlC0533
1,3-Dichlorobenzene
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.12
1
*8270D
3/28/11 16:07
KC
PlC0533
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
2,4-Dichlorophenol
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
2,4-Dimethylphenol
BRL
mg/kg dry
0.38
0.16
1
*8270D
3/28/11 16:07
KC
PlC0533
2,4-Dinitrophenol
BRL
mg/kg dry
0.38
0.059
1
*8270D
3/28/11 16:07
KC
PlC0533
2,4-Dinitrotoluene
BRL
mg/kg dry
0.38
0.064
1
*8270D
3/28/11 16:07
KC
PlC0533
2,6-Dinitrotoluene
BRL
mg/kg dry
0.38
0.057
1
*8270D
3/28/11 16:07
KC
PlC0533
2-Chloronaphthalene
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
2-Chlorophenol
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
2-Methyl naphthalene
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
2-Methylphenol
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
2-Nitrophenol
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.38
0.063
1
*8270D
3/28/11 16:07
KC
PlC0533
3/4-Methyl phenol
BRL
mg/kg dry
0.38
0.10
1
*8270D
3/28/11 16:07
KC
PlC0533
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.38
0.041
1
*8270D
3/28/11 16:07
KC
PlC0533
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.38
0.084
1
*8270D
3/28/11 16:07
KC
PlC0533
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
4-Chloroaniline
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.38
0.11
1
*8270D
3/28/11 16:07
KC
PlC0533
4-Nitrophenol
BRL
mg/kg dry
0.38
0.047
1
*8270D
3/28/11 16:07
KC
PlC0533
Acenaphthene
BRL
mg/kg dry
0.38
0.12
1
*8270D
3/28/11 16:07
KC
PlC0533
Acenaphthylene
BRL
mg/kg dry
0.38
0.12
1
*8270D
3/28/11 16:07
KC
PlC0533
Anthracene
BRL
mg/kg dry
0.38
0.074
1
*8270D
3/28/11 16:07
KC
PlC0533
Azobenzene
BRL
mg/kg dry
0.38
0.087
1
*8270D
3/28/11 16:07
KC
PlC0533
Benzo(a)anthracene
BRL
mg/kg dry
0.38
0.077
1
*8270D
3/28/11 16:07
KC
PlC0533
Benzo(a)pyrene
BRL
mg/kg dry
0.38
0.070
1
*8270D
3/28/11 16:07
KC
PlC0533
Benzo(b)fluoranthene
BRL
mg/kg dry
0.38
0.052
1
*8270D
3/28/11 16:07
KC
PlC0533
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 23

Laboratory Report
Full -Service Analytical
P R S M
&
Environmental Solutions
LABORATORIES INC.
04/04/2011
Hart & Hickman (Raleigh)
Project: City of Rocky
Mount
Client Sample ID:
T1-S11A
Attn: Kevin Buchanan
(CRM-008)
Prism Sample ID:
1030539-01
3334 Hillsborough St.
Project No.: CRM-008
Prism Work Order: 1030539
Raleigh, NC 27607
Sample Matrix: Solid
Time Collected: 03/21/11 15:40
Time Submitted: 03/22/11 14:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.38
0.12
1
*8270D
3/28/11 16:07
KC
PlC0533
Benzo(k)fluoranthene
BRL
mg/kg dry
0.38
0.11
1
*8270D
3/28/11 16:07
KC
PlC0533
Benzoic Acid
BRL
mg/kg dry
0.38
0.050
1
*8270D
3/28/11 16:07
KC
PlC0533
Benzyl alcohol
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.38
0.19
1
*8270D
3/28/11 16:07
KC
PlC0533
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.15
1
*8270D
3/28/11 16:07
KC
PlC0533
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.38
0.073
1
*8270D
3/28/11 16:07
KC
PlC0533
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.084
1
*8270D
3/28/11 16:07
KC
PlC0533
Chrysene
BRL
mg/kg dry
0.38
0.084
1
*8270D
3/28/11 16:07
KC
PlC0533
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.38
0.12
1
*8270D
3/28/11 16:07
KC
PlC0533
Dibenzofuran
BRL
mg/kg dry
0.38
0.11
1
*8270D
3/28/11 16:07
KC
PlC0533
Diethyl phthalate
BRL
mg/kg dry
0.38
0.068
1
*8270D
3/28/11 16:07
KC
PlC0533
Dimethyl phthalate
BRL
mg/kg dry
0.38
0.070
1
*8270D
3/28/11 16:07
KC
PlC0533
Di-n-butyl phthalate
BRL
mg/kg dry
0.38
0.089
1
*8270D
3/28/11 16:07
KC
PlC0533
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.083
1
*8270D
3/28/11 16:07
KC
PlC0533
Fluoranthene
BRL
mg/kg dry
0.38
0.079
1
*8270D
3/28/11 16:07
KC
PlC0533
Fluorene
BRL
mg/kg dry
0.38
0.088
1
*8270D
3/28/11 16:07
KC
PlC0533
Hexachlorobenzene
BRL
mg/kg dry
0.38
0.063
1
*8270D
3/28/11 16:07
KC
PlC0533
Hexachlorobutadiene
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.38
0.11
1
*8270D
3/28/11 16:07
KC
PlC0533
Hexachloroethane
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.38
0.10
1
*8270D
3/28/11 16:07
KC
PlC0533
Isophorone
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
Naphthalene
BRL
mg/kg dry
0.38
0.15
1
*8270D
3/28/11 16:07
KC
PlC0533
Nitrobenzene
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.38
0.13
1
*8270D
3/28/11 16:07
KC
PlC0533
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.38
0.076
1
*8270D
3/28/11 16:07
KC
PlC0533
Pentachlorophenol
BRL
mg/kg dry
0.38
0.031
1
*8270D
3/28/11 16:07
KC
PlC0533
Phenanthrene
BRL
mg/kg dry
0.38
0.067
1
*8270D
3/28/11 16:07
KC
PlC0533
Phenol
BRL
mg/kg dry
0.38
0.14
1
*8270D
3/28/11 16:07
KC
PlC0533
Pyrene
BRL
mg/kg dry
0.38
0.10
1
*8270D
3/28/11 16:07
KC
PlC0533
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
61 %
34-134
2-Fluorobiphenyl
122 %
17-122
2-Fluorophenol
97 %
13-108
Nitrobenzene-d5
94 %
11-118
Phenol-d5
87 %
23-109
Terphenyl-d14
85 %
41-156
Volatile Organic Compounds by GUMS
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0062
0.00020
1
*8260B
3/24/11 13:06
KC
PlC0557
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0062
0.0010
1
*8260B
3/24/11 13:06
KC
PlC0557
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0062
0.00052
1
*8260B
3/24/11 13:06
KC
PlC0557
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 23

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Hart & Hickman (Raleigh)
Attn: Kevin Buchanan
3334 Hillsborough St.
Raleigh, NC 27607
Project: City of Rocky Mount
(CRM-008)
Project No.: CRM-008
Sample Matrix: Solid
Laboratory Report
04/04/2011
Client Sample ID: T1-S11A
Prism Sample ID: 1030539-01
Prism Work Order: 1030539
Time Collected: 03/21/11 15:40
Time Submitted: 03/22/11 14:45
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1-Dichloroethane
BRL
mg/kg dry
0.0062
0.00052
1
*8260B
3/24/11 13:06
KC
PlC0557
1,1-Dichloroethylene
BRL
mg/kg dry
0.0062
0.00038
1
*8260B
3/24/11 13:06
KC
PlC0557
1,1-Dichloropropylene
BRL
mg/kg dry
0.0062
0.00065
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0062
0.00046
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0062
0.00093
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0062
0.00036
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0062
0.0012
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2-Dibromoethane
BRL
mg/kg dry
0.0062
0.00071
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0062
0.00028
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2-Dichloroethane
BRL
mg/kg dry
0.0062
0.0010
1
*8260B
3/24/11 13:06
KC
PlC0557
1,2-Dichloropropane
BRL
mg/kg dry
0.0062
0.00039
1
*8260B
3/24/11 13:06
KC
PlC0557
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0062
0.00030
1
*8260B
3/24/11 13:06
KC
PlC0557
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0062
0.000085
1
*8260B
3/24/11 13:06
KC
PlC0557
1,3-Dichloropropane
BRL
mg/kg dry
0.0062
0.00067
1
*8260B
3/24/11 13:06
KC
PlC0557
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0062
0.00045
1
*8260B
3/24/11 13:06
KC
PlC0557
2,2-Dichloropropane
BRL
mg/kg dry
0.0062
0.00039
1
*8260B
3/24/11 13:06
KC
PlC0557
2-Chlorotoluene
BRL
mg/kg dry
0.0062
0.00038
1
*8260B
3/24/11 13:06
KC
PlC0557
4-Chlorotoluene
BRL
mg/kg dry
0.0062
0.00029
1
*8260B
3/24/11 13:06
KC
PlC0557
4-Isopropyltoluene
BRL
mg/kg dry
0.0062
0.00039
1
*8260B
3/24/11 13:06
KC
PlC0557
Acetone
BRL
mg/kg dry
0.062
0.0033
1
*8260B
3/24/11 13:06
KC
PlC0557
Benzene
BRL
mg/kg dry
0.0037
0.00038
1
*8260B
3/24/11 13:06
KC
PlC0557
Bromobenzene
BRL
mg/kg dry
0.0062
0.00026
1
*8260B
3/24/11 13:06
KC
PlC0557
Bromochloromethane
BRL
mg/kg dry
0.0062
0.00090
1
*8260B
3/24/11 13:06
KC
PlC0557
Bromodichloromethane
BRL
mg/kg dry
0.0062
0.00028
1
*8260B
3/24/11 13:06
KC
PlC0557
Bromoform
BRL
mg/kg dry
0.0062
0.0011
1
*8260B
3/24/11 13:06
KC
PlC0557
Bromomethane
BRL
mg/kg dry
0.012
0.0017
1
*8260B
3/24/11 13:06
KC
PlC0557
Carbon Tetrachloride
BRL
mg/kg dry
0.0062
0.00034
1
*8260B
3/24/11 13:06
KC
PlC0557
Chlorobenzene
BRL
mg/kg dry
0.0062
0.00029
1
*8260B
3/24/11 13:06
KC
PlC0557
Chloroethane
BRL
mg/kg dry
0.012
0.0047
1
*8260B
3/24/11 13:06
KC
PlC0557
Chloroform
BRL
mg/kg dry
0.0062
0.00026
1
*8260B
3/24/11 13:06
KC
PlC0557
Chloromethane
BRL
mg/kg dry
0.0062
0.0031
1
*8260B
3/24/11 13:06
KC
PlC0557
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0062
0.00050
1
*8260B
3/24/11 13:06
KC
PlC0557
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0062
0.00031
1
*8260B
3/24/11 13:06
KC
PlC0557
Dibromochloromethane
BRL
mg/kg dry
0.0062
0.00042
1
*8260B
3/24/11 13:06
KC
PlC0557
Dichlorodifluoromethane
BRL
mg/kg dry
0.0062
0.00066
1
*8260B
3/24/11 13:06
KC
PlC0557
Ethylbenzene
BRL
mg/kg dry
0.0062
0.00040
1
*8260B
3/24/11 13:06
KC
PlC0557
Isopropyl Ether
BRL
mg/kg dry
0.0062
0.00026
1
*8260B
3/24/11 13:06
KC
PlC0557
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0062
0.00031
1
*8260B
3/24/11 13:06
KC
PlC0557
m,p-Xylenes
BRL
mg/kg dry
0.012
0.00080
1
*8260B
3/24/11 13:06
KC
PlC0557
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.062
0.0013
1
*8260B
3/24/11 13:06
KC
PlC0557
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.12
0.0022
1
*8260B
3/24/11 13:06
KC
PlC0557
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.062
0.0016
1
*8260B
3/24/11 13:06
KC
PlC0557
Methylene Chloride
BRL
mg/kg dry
0.0062
0.00045
1
*8260B
3/24/11 13:06
KC
PlC0557
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 23

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 04/04/2011
LABORATORIES INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount Client Sample ID: T1-S11A
Attn: Kevin Buchanan (CRM-008) Prism Sample ID: 1030539-01
3334 Hillsborough St. Project No.: CRM-008 Prism Work Order: 1030539
Raleigh, NC 27607 Sample Matrix: Solid Time Collected: 03/21/11 15:40
Time Submitted: 03/22/11 14:45
Parameter
Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.012
0.00048
1
*8260B 3/24/11 13:06
KC
PlC0557
Naphthalene
BRL
mg/kg dry
0.012
0.00045
1
*8260B 3/24/11 13:06
KC
PlC0557
n-Butylbenzene
BRL
mg/kg dry
0.0062
0.00027
1
*8260B 3/24/11 13:06
KC
PlC0557
n-Propylbenzene
BRL
mg/kg dry
0.0062
0.00035
1
*8260B 3/24/11 13:06
KC
PlC0557
o-Xylene
BRL
mg/kg dry
0.0062
0.00039
1
*8260B 3/24/11 13:06
KC
PlC0557
sec-Butylbenzene
BRL
mg/kg dry
0.0062
0.00025
1
*8260B 3/24/11 13:06
KC
PlC0557
Styrene
BRL
mg/kg dry
0.0062
0.00027
1
*8260B 3/24/11 13:06
KC
PlC0557
tert-Butylbenzene
BRL
mg/kg dry
0.0062
0.00032
1
*8260B 3/24/11 13:06
KC
PlC0557
Tetrachloroethylene
BRL
mg/kg dry
0.0062
0.00043
1
*8260B 3/24/11 13:06
KC
PlC0557
Toluene
BRL
mg/kg dry
0.0062
0.00037
1
*8260B 3/24/11 13:06
KC
PlC0557
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0062
0.00072
1
*8260B 3/24/11 13:06
KC
PlC0557
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0062
0.00030
1
*8260B 3/24/11 13:06
KC
PlC0557
Trichloroethylene
BRL
mg/kg dry
0.0062
0.00057
1
*8260B 3/24/11 13:06
KC
PlC0557
Trichlorofluoromethane
BRL
mg/kg dry
0.0062
0.00050
1
*8260B 3/24/11 13:06
KC
PlC0557
Vinyl acetate
BRL
mg/kg dry
0.031
0.0018
1
*8260B 3/24/11 13:06
KC
PlC0557
Vinyl chloride
BRL
mg/kg dry
0.0062
0.00080
1
*8260B 3/24/11 13:06
KC
PlC0557
Xylenes, total
BRL
mg/kg dry
0.019
0.0012
1
*8260B 3/24/11 13:06
KC
PlC0557
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
114 %
70-130
Dibromofluoromethane
108 %
84-123
Toluene-d8
105 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
4.7
1.7
100
*MADEP VPH 3/31/11 1:49
CGP
P1C0654
C9-C12 Aliphatics
13
mg/kg dry
4.7
1.7
100
*MADEP VPH 3131/11 1:49
CGP
PlC0654
C9-Cl0 Aromatics
BRL
mg/kg dry
4.7
0.49
100
*MADEP VPH 3/31/11 1:49
CGP
P1C0654
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
113 %
70-130
2,5-Dibromotoluene (FID)
111 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 CO557 - 5035
Blank (P1C0557-BLK1)
Prepared & Analyzed: 03/24/11
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.0050
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.0050
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.050
mg/kg wet
Benzene
BRL
0.0030
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.0050
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.0050
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.050
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.10
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.050
mg/kg wet
Methylene Chloride
BRL
0.0050
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0557 - 5035
Blank (PlC0557-BLK1)
Prepared & Analyzed: 03/24/11
Methyl-tert-Butyl Ether
BRL
0.010
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butylbenzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.0050
mg/kg wet
Vinyl acetate
BRL
0.025
mg/kg wet
Vinyl chloride
BRL
0.0050
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
55.4
ug/L
50.0
111
70-130
Surrogate: Dibromofluoromethane
51.9
ug/L
50.0
104
84-123
Surrogate: Toluene-d8
51.9
ug/L
50.0
104
76-129
LCS (P1C0557-BSI)
Prepared & Analyzed: 03/24/11
1,1-Dichloroethylene
0.0499
0.0050
mg/kg wet
0.0500
100
67-149
Benzene
0.0436
0.0030
mg/kg wet
0.0500
87
74-127
Chlorobenzene
0.0408
0.0050
mg/kg wet
0.0500
82
74-118
Toluene
0.0415
0.0050
mg/kg wet
0.0500
83
71-129
Trichloroethylene
0.0430
0.0050
mg/kg wet
0.0500
86
75-133
Surrogate:4-Bromofluorobenzene
55.2
ug/L
50.0
110
70-130
Surrogate: Dibromofluoromethane
51.4
ug/L
50.0
103
84-123
Surrogate: Toluene-d8
50.5
ug/L
50.0
101
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 9 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0557 - 5035
LCS Dup (PlC0557-BSD1)
Prepared & Analyzed: 03/24/11
1,1-Dichloroethylene
0.0546
0.0050
mg/kg wet
0.0500
109
67-149
9
200
Benzene
0.0459
0.0030
mg/kg wet
0.0500
92
74-127
5
200
Chlorobenzene
0.0434
0.0050
mg/kg wet
0.0500
87
74-118
6
200
Toluene
0.0438
0.0050
mg/kg wet
0.0500
88
71-129
5
200
Trichloroethylene
0.0454
0.0050
mg/kg wet
0.0500
91
75-133
5
200
Surrogate:4-Bromofluorobenzene
55.5
ug/L
50.0
111
70-130
Surrogate: Dibromofluoromethane
51.5
ug/L
50.0
103
84-123
Surrogate: Toluene-d8
51.7
ug/L
50.0
103
76-129
Matrix Spike (P1C0557-MS1)
Source: 1030539-01
Prepared & Analyzed:
03/24/11
1,1-Dichloroethylene
0.0571
0.0057
mg/kg dry
0.0568
BRL
100
54-162
Benzene
0.0492
0.0034
mg/kg dry
0.0568
BRL
87
60-135
Chlorobenzene
0.0425
0.0057
mg/kg dry
0.0568
BRL
75
57-125
Toluene
0.0445
0.0057
mg/kg dry
0.0568
BRL
78
57-135
Trichloroethylene
0.0455
0.0057
mg/kg dry
0.0568
BRL
80
38-164
Surrogate:4-Bromofluorobenzene
56.1
ug/L
50.0
112
70-130
Surrogate: Dibromofluoromethane
50.7
ug/L
50.0
101
84-123
Surrogate: Toluene-d8
51.8
ug/L
50.0
104
76-129
Matrix Spike Dup (PlC0557-MSD1)
Source: 1030539-01
Prepared & Analyzed:
03/24/11
1,1-Dichloroethylene
0.0568
0.0057
mg/kg dry
0.0568
BRL
100
54-162
0.4
22
Benzene
0.0490
0.0034
mg/kg dry
0.0568
BRL
86
60-135
0.4
20
Chlorobenzene
0.0428
0.0057
mg/kg dry
0.0568
BRL
75
57-125
0.6
14
Toluene
0.0450
0.0057
mg/kg dry
0.0568
BRL
79
57-135
1
22
Trichloroethylene
0.0461
0.0057
mg/kg dry
0.0568
BRL
81
38-164
1
18
Surrogate:4-Bromofluorobenzene
56.5
ug/L
50.0
113
70-130
Surrogate: Dibromofluoromethane
51.4
ug/L
50.0
103
84-123
Surrogate: Toluene-d8
51.2
ug/L
50.0
102
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
Blank (PlC0533-BLK1)
Prepared: 03/24/11 Analyzed: 03/28/11
1,2,4-Trichlorobenzene
BRL
0.33
mg/kg wet
1,2-Dichlorobenzene
BRL
0.33
mg/kg wet
1,3-Dichlorobenzene
BRL
0.33
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.33
mg/kg wet
2,4-Dichlorophenol
BRL
0.33
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
0.33
mg/kg wet
2,4-Dinitrotoluene
BRL
0.33
mg/kg wet
2,6-Dinitrotoluene
BRL
0.33
mg/kg wet
2-Chloronaphthalene
BRL
0.33
mg/kg wet
2-Chlorophenol
BRL
0.33
mg/kg wet
2-Methyl naphthalene
BRL
0.33
mg/kg wet
2-Methylphenol
BRL
0.33
mg/kg wet
2-Nitrophenol
BRL
0.33
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.33
mg/kg wet
3/4-Methyl phenol
BRL
0.33
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
0.33
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.33
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Nitrophenol
BRL
0.33
mg/kg wet
Acenaphthene
BRL
0.33
mg/kg wet
Acenaphthylene
BRL
0.33
mg/kg wet
Anthracene
BRL
0.33
mg/kg wet
Azobenzene
BRL
0.33
mg/kg wet
Benzo(a)anthracene
BRL
0.33
mg/kg wet
Benzo(a)pyrene
BRL
0.33
mg/kg wet
Benzo(b)fluoranthene
BRL
0.33
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.33
mg/kg wet
Benzo(k)fluoranthene
BRL
0.33
mg/kg wet
Benzoic Acid
BRL
0.33
mg/kg wet
Benzyl alcohol
BRL
0.33
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.33
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.33
mg/kg wet
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.33
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.33
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.33
mg/kg wet
Dibenzofuran
BRL
0.33
mg/kg wet
Diethyl phthalate
BRL
0.33
mg/kg wet
Dimethyl phthalate
BRL
0.33
mg/kg wet
Di-n-butyl phthalate
BRL
0.33
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
Blank (PlC0533-BLK1)
Prepared: 03/24/11 Analyzed: 03/28/11
Fluoranthene
BRL
0.33
mg/kg wet
Fluorene
BRL
0.33
mg/kg wet
Hexachlorobenzene
BRL
0.33
mg/kg wet
Hexachlorobutadiene
BRL
0.33
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.33
mg/kg wet
Hexachloroethane
BRL
0.33
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.33
mg/kg wet
Isophorone
BRL
0.33
mg/kg wet
Naphthalene
BRL
0.33
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.33
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.33
mg/kg wet
Pentachlorophenol
BRL
0.33
mg/kg wet
Phenanthrene
BRL
0.33
mg/kg wet
Phenol
BRL
0.33
mg/kg wet
Pyrene
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
2.77
mg/kg wet
3.31
84
34-134
Surrogate: 2-Fluorobiphenyl
1.61
mg/kg wet
1.65
97
17-122
Surrogate: 2-Fluorophenol
3.16
mg/kg wet
3.31
96
13-108
Surrogate: Nitrobenzene-d5
1.33
mg/kg wet
1.65
81
11-118
Surrogate: Phenol-d5
3.00
mg/kg wet
3.31
91
23-109
Surrogate: Terphenyl-d14
1.24
mg/kg wet
1.65
75
41-156
LCS (P1C0533-113SI)
Prepared: 03/24/11 Analyzed: 03/28/11
1,2,4-Trichlorobenzene
1.41
0.33
mg/kg wet
1.68
84
35-95
1,2-Dichlorobenzene
1.46
0.33
mg/kg wet
1.68
86
34-94
1,3-Dichlorobenzene
1.43
0.33
mg/kg wet
1.68
85
31-92
1,4-Dichlorobenzene
1.44
0.33
mg/kg wet
1.68
86
33-92
2,4,6-Trichlorophenol
1.58
0.33
mg/kg wet
1.68
94
43-110
2,4-Dichlorophenol
1.41
0.33
mg/kg wet
1.68
84
37-103
2,4-Dimethylphenol
1.48
0.33
mg/kg wet
1.68
88
39-105
2,4-Dinitrophenol
1.54
0.33
mg/kg wet
1.68
91
28-129
2,4-Dinitrotoluene
1.90
0.33
mg/kg wet
1.68
113
59-115
2,6-Dinitrotoluene
1.84
0.33
mg/kg wet
1.68
109
52-120
2-Chloronaphthalene
1.81
0.33
mg/kg wet
1.68
107
41-104 LH
2-Chlorophenol
1.38
0.33
mg/kg wet
1.68
82
35-98
2-Methyl naphthalene
1.46
0.33
mg/kg wet
1.68
87
31-106
2-Methylphenol
1.44
0.33
mg/kg wet
1.68
86
32-108
2-Nitrophenol
1.41
0.33
mg/kg wet
1.68
84
35-100
3,3'-Dichlorobenzidine
1.84
0.33
mg/kg wet
1.68
109
10-200
3/4-Methyl phenol
1.55
0.33
mg/kg wet
1.68
92
36-103
4,6-Dinitro-2-methylphenol
1.87
0.33
mg/kg wet
1.68
ill
44-124
4-Bromophenyl phenyl ether
1.56
0.33
mg/kg wet
1.68
93
44-119
4-Chloro-3-methylphenol
1.42
0.33
mg/kg wet
1.68
85
48-106
4-Chloroaniline
1.42
0.33
mg/kg wet
1.68
84
45-103
4-Chlorophenyl phenyl ether
1.52
0.33
mg/kg wet
1.68
90
53-109
4-Nitrophenol
1.73
0.33
mg/kg wet
1.68
103
40-124
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
LCS (PlC0533-BSI)
Prepared: 03/24/11 Analyzed: 03/28/11
Acenaphthene
1.59
0.33
mg/kg wet
1.68
95
47-106
Acenaphthylene
1.59
0.33
mg/kg wet
1.68
95
47-113
Anthracene
1.71
0.33
mg/kg wet
1.68
101
57-121
Azobenzene
1.70
0.33
mg/kg wet
1.68
101
49-117
Benzo(a)anthracene
1.74
0.33
mg/kg wet
1.68
103
55-123
Benzo(a)pyrene
1.74
0.33
mg/kg wet
1.68
103
61-120
Benzo(b)fluoranthene
1.61
0.33
mg/kg wet
1.68
96
52-126
Benzo(g,h,i)perylene
1.99
0.33
mg/kg wet
1.68
118
53-121
Benzo(k)fluoranthene
1.79
0.33
mg/kg wet
1.68
106
50-131
Benzoic Acid
0.491
0.33
mg/kg wet
1.68
29
10-75
Benzyl alcohol
1.52
0.33
mg/kg wet
1.68
91
35-101
bis(2-Chloroethoxy)methane
1.36
0.33
mg/kg wet
1.68
81
37-106
Bis(2-Chloroethyl)ether
1.49
0.33
mg/kg wet
1.68
89
33-99
Bis(2-chloroisopropyl)ether
1.40
0.33
mg/kg wet
1.68
83
26-106
Bis(2-Ethylhexyl)phthalate
2.10
0.33
mg/kg wet
1.68
125
50-142
Butyl benzyl phthalate
1.62
0.33
mg/kg wet
1.68
96
49-143
Chrysene
1.76
0.33
mg/kg wet
1.68
105
53-126
Dibenzo(a,h)anthracene
1.99
0.33
mg/kg wet
1.68
118
53-124
Dibenzofuran
1.54
0.33
mg/kg wet
1.68
92
48-109
Diethyl phthalate
1.62
0.33
mg/kg wet
1.68
96
59-118
Dimethyl phthalate
1.54
0.33
mg/kg wet
1.68
92
58-113
Di-n-butyl phthalate
1.77
0.33
mg/kg wet
1.68
105
51-129
Di-n-octyl phthalate
1.73
0.33
mg/kg wet
1.68
102
49-140
Fluoranthene
1.92
0.33
mg/kg wet
1.68
114
52-122
Fluorene
1.58
0.33
mg/kg wet
1.68
94
52-110
Hexachlorobenzene
1.58
0.33
mg/kg wet
1.68
94
52-117
Hexachlorobutadiene
1.37
0.33
mg/kg wet
1.68
82
35-101
Hexachlorocyclopentadiene
1.55
0.33
mg/kg wet
1.68
92
31-111
Hexachloroethane
1.50
0.33
mg/kg wet
1.68
89
30-93
Indeno(1,2,3-cd)pyrene
2.02
0.33
mg/kg wet
1.68
120
40-133
Isophorone
1.56
0.33
mg/kg wet
1.68
93
41-103
Naphthalene
1.51
0.33
mg/kg wet
1.68
89
38-98
Nitrobenzene
1.62
0.33
mg/kg wet
1.68
96
28-110
N-Nitroso-di-n-propylamine
1.64
0.33
mg/kg wet
1.68
97
36-104
N-Nitrosodiphenylamine
1.93
0.33
mg/kg wet
1.68
115
57-134
Pentachlorophenol
1.68
0.33
mg/kg wet
1.68
100
48-136
Phenanthrene
1.67
0.33
mg/kg wet
1.68
99
57-118
Phenol
1.32
0.33
mg/kg wet
1.68
78
27-107
Pyrene
1.42
0.33
mg/kg wet
1.68
84
48-132
Surrogate: 2,4,6-Tribromophenol
3.24
mg/kg wet
3.37
96
34-134
Surrogate: 2-Fluorobiphenyl
1.58
mg/kg wet
1.68
94
17-122
Surrogate: 2-Fluorophenol
3.06
mg/kg wet
3.37
91
13-108
Surrogate: Nitrobenzene-d5
1.48
mg/kg wet
1.68
88
11-118
Surrogate: Phenol-d5
2.98
mg/kg wet
3.37
88
23-109
Surrogate: Terphenyl-d14
1.46
mg/kg wet
1.68
87
41-156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
LCS Dup (P1C0533-BSD1)
Prepared: 03/24/11 Analyzed: 03/28/11
1,2,4-Trichlorobenzene
1.44
0.33
mg/kg wet
1.68
85
35-95
2
200
1,2-Dichlorobenzene
1.47
0.33
mg/kg wet
1.68
88
34-94
1
200
1,3-Dichlorobenzene
1.43
0.33
mg/kg wet
1.68
85
31-92
0.06
200
1,4-Dichlorobenzene
1.44
0.33
mg/kg wet
1.68
86
33-92
0.5
200
2,4,6-Trichlorophenol
1.66
0.33
mg/kg wet
1.68
99
43-110
5
200
2,4-Dichlorophenol
1.48
0.33
mg/kg wet
1.68
88
37-103
4
200
2,4-Dimethylphenol
1.50
0.33
mg/kg wet
1.68
89
39-105
1
200
2,4-Dinitrophenol
1.30
0.33
mg/kg wet
1.68
77
28-129
17
200
2,4-Dinitrotoluene
1.85
0.33
mg/kg wet
1.68
110
59-115
2
200
2,6-Dinitrotoluene
1.86
0.33
mg/kg wet
1.68
111
52-120
1
200
2-Chloronaphthalene
1.83
0.33
mg/kg wet
1.68
109
41-104
1
200 LH
2-Chlorophenol
1.44
0.33
mg/kg wet
1.68
86
35-98
4
200
2-Methyl naphthalene
1.53
0.33
mg/kg wet
1.68
91
31-106
5
200
2-Methylphenol
1.44
0.33
mg/kg wet
1.68
86
32-108
0.2
200
2-Nitrophenol
1.40
0.33
mg/kg wet
1.68
83
35-100
0.8
200
3,3'-Dichlorobenzidine
1.77
0.33
mg/kg wet
1.68
106
10-200
4
200
3/4-Methyl phenol
1.52
0.33
mg/kg wet
1.68
91
36-103
2
200
4,6-Dinitro-2-methylphenol
1.72
0.33
mg/kg wet
1.68
102
44-124
8
200
4-Bromophenyl phenyl ether
1.56
0.33
mg/kg wet
1.68
93
44-119
0.3
200
4-Chloro-3-methylphenol
1.55
0.33
mg/kg wet
1.68
93
48-106
9
200
4-Chloroaniline
1.50
0.33
mg/kg wet
1.68
89
45-103
5
200
4-Chlorophenyl phenyl ether
1.57
0.33
mg/kg wet
1.68
93
53-109
3
200
4-Nitrophenol
1.67
0.33
mg/kg wet
1.68
100
40-124
3
200
Acenaphthene
1.62
0.33
mg/kg wet
1.68
97
47-106
2
200
Acenaphthylene
1.63
0.33
mg/kg wet
1.68
97
47-113
3
200
Anthracene
1.65
0.33
mg/kg wet
1.68
98
57-121
3
200
Azobenzene
1.75
0.33
mg/kg wet
1.68
104
49-117
3
200
Benzo(a)anthracene
1.68
0.33
mg/kg wet
1.68
100
55-123
4
200
Benzo(a)pyrene
1.68
0.33
mg/kg wet
1.68
100
61-120
3
200
Benzo(b)fluoranthene
1.77
0.33
mg/kg wet
1.68
106
52-126
10
200
Benzo(g,h,i)perylene
1.75
0.33
mg/kg wet
1.68
104
53-121
13
200
Benzo(k)fluoranthene
1.74
0.33
mg/kg wet
1.68
104
50-131
2
200
Benzoic Acid
0.482
0.33
mg/kg wet
1.68
29
10-75
2
200
Benzyl alcohol
1.51
0.33
mg/kg wet
1.68
90
35-101
0.7
200
bis(2-Chloroethoxy)methane
1.35
0.33
mg/kg wet
1.68
80
37-106
1
200
Bis(2-Chloroethyl)ether
1.48
0.33
mg/kg wet
1.68
88
33-99
0.8
200
Bis(2-chloroisopropyl)ether
1.37
0.33
mg/kg wet
1.68
82
26-106
2
200
Bis(2-Ethylhexyl)phthalate
1.71
0.33
mg/kg wet
1.68
102
50-142
21
200
Butyl benzyl phthalate
1.71
0.33
mg/kg wet
1.68
102
49-143
5
200
Chrysene
1.74
0.33
mg/kg wet
1.68
103
53-126
1
200
Dibenzo(a,h)anthracene
1.71
0.33
mg/kg wet
1.68
102
53-124
15
200
Dibenzofuran
1.61
0.33
mg/kg wet
1.68
96
48-109
5
200
Diethyl phthalate
1.62
0.33
mg/kg wet
1.68
96
59-118
0.1
200
Dimethyl phthalate
1.57
0.33
mg/kg wet
1.68
93
58-113
1
200
Di-n-butyl phthalate
1.69
0.33
mg/kg wet
1.68
100
51-129
5
200
Di-n-octyl phthalate
1.94
0.33
mg/kg wet
1.68
115
49-140
12
200
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
LCS Dup (P1C0533-BSD1)
Prepared: 03/24/11 Analyzed: 03/28/11
Fluoranthene
1.74
0.33
mg/kg wet
1.68
103
52-122
10
200
Fluorene
1.62
0.33
mg/kg wet
1.68
97
52-110
3
200
Hexachlorobenzene
1.59
0.33
mg/kg wet
1.68
95
52-117
0.7
200
Hexachlorobutadiene
1.41
0.33
mg/kg wet
1.68
84
35-101
2
200
Hexachlorocyclopentadiene
1.64
0.33
mg/kg wet
1.68
98
31-111
6
200
Hexachloroethane
1.46
0.33
mg/kg wet
1.68
87
30-93
2
200
Indeno(1,2,3-cd)pyrene
1.63
0.33
mg/kg wet
1.68
97
40-133
21
200
Isophorone
1.64
0.33
mg/kg wet
1.68
98
41-103
5
200
Naphthalene
1.52
0.33
mg/kg wet
1.68
90
38-98
0.8
200
Nitrobenzene
1.55
0.33
mg/kg wet
1.68
93
28-110
4
200
N-Nitroso-di-n-propylamine
1.61
0.33
mg/kg wet
1.68
96
36-104
2
200
N-Nitrosodiphenylamine
1.93
0.33
mg/kg wet
1.68
115
57-134
0.3
200
Pentachlorophenol
1.67
0.33
mg/kg wet
1.68
100
48-136
0.6
200
Phenanthrene
1.67
0.33
mg/kg wet
1.68
100
57-118
0.2
200
Phenol
1.46
0.33
mg/kg wet
1.68
87
27-107
10
200
Pyrene
1.57
0.33
mg/kg wet
1.68
93
48-132
10
200
Surrogate: 2,4,6-Tribromophenol
3.33
mg/kg wet
3.36
99
34-134
Surrogate: 2-Fluorobiphenyl
1.68
mg/kg wet
1.68
100
17-122
Surrogate: 2-Fluorophenol
3.18
mg/kg wet
3.36
95
13-108
Surrogate: Nitrobenzene-d5
1.50
mg/kg wet
1.68
89
11-118
Surrogate: Phenol-d5
3.04
mg/kg wet
3.36
91
23-109
Surrogate: Terphenyl-d14
1.59
mg/kg wet
1.68
95
41-156
Matrix Spike (PlC0533-MS1)
Source: 1030539-01
Prepared:
03/24/11
Analyzed: 03/28/11
1,2,4-Trichlorobenzene
1.70
0.38
mg/kg dry
1.90
BRL
90
25-104
1,2-Dichlorobenzene
1.73
0.38
mg/kg dry
1.90
BRL
91
22-103
1,3-Dichlorobenzene
1.67
0.38
mg/kg dry
1.90
BRL
88
18-101
1,4-Dichlorobenzene
1.63
0.38
mg/kg dry
1.90
BRL
86
14-108
2,4,6-Trichlorophenol
2.11
0.38
mg/kg dry
1.90
BRL
ill
44-115
2,4-Dichlorophenol
1.84
0.38
mg/kg dry
1.90
BRL
97
26-120
2,4-Dimethylphenol
1.79
0.38
mg/kg dry
1.90
BRL
94
33-113
2,4-Dinitrophenol
0.764
0.38
mg/kg dry
1.90
BRL
40
14-148
2,4-Dinitrotoluene
1.76
0.38
mg/kg dry
1.90
BRL
93
49-134
2,6-Dinitrotoluene
2.21
0.38
mg/kg dry
1.90
BRL
117
44-131
2-Chloronaphthalene
2.47
0.38
mg/kg dry
1.90
BRL
130
38-112
M
2-Chlorophenol
1.75
0.38
mg/kg dry
1.90
BRL
92
26-108
2-Methyl naphthalene
1.83
0.38
mg/kg dry
1.90
BRL
97
12-128
2-Methylphenol
1.90
0.38
mg/kg dry
1.90
BRL
100
26-116
2-Nitrophenol
1.65
0.38
mg/kg dry
1.90
BRL
87
20-119
3,3'-Dichlorobenzidine
1.21
0.38
mg/kg dry
1.90
BRL
64
10-191
3/4-Methyl phenol
1.93
0.38
mg/kg dry
1.90
BRL
102
28-116
4,6-Dinitro-2-methylphenol
1.50
0.38
mg/kg dry
1.90
BRL
79
30-148
4-Bromophenyl phenyl ether
2.46
0.38
mg/kg dry
1.90
BRL
130
43-126
M
4-Chloro-3-methylphenol
1.64
0.38
mg/kg dry
1.90
BRL
87
41-120
4-Chloroaniline
1.31
0.38
mg/kg dry
1.90
BRL
69
35-115
4-Chlorophenyl phenyl ether
1.78
0.38
mg/kg dry
1.90
BRL
94
45-123
4-Nitrophenol
0.837
0.38
mg/kg dry
1.90
BRL
44
33-136
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
Matrix Spike (PlC0533-MS1)
Source: 1030539-01
Prepared: 03/24/11 Analyzed: 03/28/11
Acenaphthene
1.98
0.38
mg/kg dry
1.90
BRL
104
46-115
Acenaphthylene
2.00
0.38
mg/kg dry
1.90
BRL
105
40-125
Anthracene
1.99
0.38
mg/kg dry
1.90
BRL
105
56-127
Azobenzene
2.96
0.38
mg/kg dry
1.90
BRL
156
49-123
Benzo(a)anthracene
2.48
0.38
mg/kg dry
1.90
BRL
131
50-134
Benzo(a)pyrene
2.33
0.38
mg/kg dry
1.90
BRL
123
59-129
Benzo(b)fluoranthene
2.49
0.38
mg/kg dry
1.90
BRL
131
46-141
Benzo(g,h,i)perylene
2.53
0.38
mg/kg dry
1.90
BRL
134
47-136
Benzo(k)fluoranthene
2.24
0.38
mg/kg dry
1.90
BRL
118
36-151
Benzoic Acid
1.30
0.38
mg/kg dry
1.90
BRL
69
10-122
Benzyl alcohol
1.90
0.38
mg/kg dry
1.90
BRL
100
29-112
bis(2-Chloroethoxy)methane
1.65
0.38
mg/kg dry
1.90
BRL
87
31-119
Bis(2-Chloroethyl)ether
1.72
0.38
mg/kg dry
1.90
BRL
91
23-111
Bis(2-chloroisopropyl)ether
1.73
0.38
mg/kg dry
1.90
BRL
91
22-109
Bis(2-Ethylhexyl)phthalate
2.54
0.38
mg/kg dry
1.90
BRL
134
45-153
Butyl benzyl phthalate
2.39
0.38
mg/kg dry
1.90
BRL
126
43-156
Chrysene
2.45
0.38
mg/kg dry
1.90
BRL
129
46-140
Dibenzo(a,h)anthracene
2.58
0.38
mg/kg dry
1.90
BRL
136
43-141
Dibenzofuran
1.89
0.38
mg/kg dry
1.90
BRL
99
45-121
Diethyl phthalate
1.84
0.38
mg/kg dry
1.90
BRL
97
53-128
Dimethyl phthalate
1.95
0.38
mg/kg dry
1.90
BRL
103
54-123
Di-n-butyl phthalate
2.07
0.38
mg/kg dry
1.90
0.109
103
44-137
Di-n-octyl phthalate
2.76
0.38
mg/kg dry
1.90
BRL
146
45-151
Fluoranthene
1.93
0.38
mg/kg dry
1.90
BRL
102
37-140
Fluorene
1.74
0.38
mg/kg dry
1.90
BRL
92
49-119
Hexachlorobenzene
2.20
0.38
mg/kg dry
1.90
BRL
116
47-128
Hexachlorobutadiene
1.65
0.38
mg/kg dry
1.90
BRL
87
24-107
Hexachlorocyclopentadiene
1.69
0.38
mg/kg dry
1.90
BRL
89
20-121
Hexachloroethane
1.70
0.38
mg/kg dry
1.90
BRL
90
17-102
Indeno(1,2,3-cd)pyrene
2.63
0.38
mg/kg dry
1.90
BRL
139
27-156
Isophorone
2.04
0.38
mg/kg dry
1.90
BRL
108
22-130
Naphthalene
1.81
0.38
mg/kg dry
1.90
BRL
95
27-111
Nitrobenzene
1.93
0.38
mg/kg dry
1.90
BRL
102
23-120
N-Nitroso-di-n-propylamine
2.01
0.38
mg/kg dry
1.90
BRL
106
27-120
N-Nitrosodiphenylamine
3.07
0.38
mg/kg dry
1.90
BRL
162
46-153
Pentachlorophenol
1.38
0.38
mg/kg dry
1.90
BRL
73
36-155
Phenanthrene
2.51
0.38
mg/kg dry
1.90
BRL
133
48-137
Phenol
1.70
0.38
mg/kg dry
1.90
BRL
90
23-115
Pyrene
2.51
0.38
mg/kg dry
1.90
BRL
132
43-146
Surrogate: 2,4,6-Tribromophenol
2.51
mg/kg dry
3.79
66
34-134
Surrogate: 2-Fluorobiphenyl
2.20
mg/kg dry
1.90
116
17-122
Surrogate: 2-Fluorophenol
3.71
mg/kg dry
3.79
98
13-108
Surrogate: Nitrobenzene-d5
1.72
mg/kg dry
1.90
91
11-118
Surrogate: Phenol-d5
3.57
mg/kg dry
3.79
94
23-109
Surrogate: Terphenyl-d14
2.05
mg/kg dry
1.90
108
41-156
M
A
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
Matrix Spike Dup (P1C0533-11VISD1)
Source: 1030539-01
Prepared: 03/24/11 Analyzed: 03/28/11
1,2,4-Trichlorobenzene
1.55
0.37
mg/kg dry
1.89
BRL
82
25-104
9
46
1,2-Dichlorobenzene
1.55
0.37
mg/kg dry
1.89
BRL
82
22-103
11
49
1,3-Dichlorobenzene
1.51
0.37
mg/kg dry
1.89
BRL
80
18-101
10
55
1,4-Dichlorobenzene
1.51
0.37
mg/kg dry
1.89
BRL
80
14-108
7
50
2,4,6-Trichlorophenol
1.86
0.37
mg/kg dry
1.89
BRL
98
44-115
12
35
2,4-Dichlorophenol
1.68
0.37
mg/kg dry
1.89
BRL
89
26-120
9
45
2,4-Dimethylphenol
1.67
0.37
mg/kg dry
1.89
BRL
88
33-113
7
47
2,4-Dinitrophenol
0.575
0.37
mg/kg dry
1.89
BRL
30
14-148
28
39
2,4-Dinitrotoluene
1.59
0.37
mg/kg dry
1.89
BRL
84
49-134
10
28
2,6-Dinitrotoluene
1.95
0.37
mg/kg dry
1.89
BRL
103
44-131
13
31
2-Chloronaphthalene
2.19
0.37
mg/kg dry
1.89
BRL
115
38-112
12
37
2-Chlorophenol
1.55
0.37
mg/kg dry
1.89
BRL
82
26-108
12
51
2-Methyl naphthalene
1.66
0.37
mg/kg dry
1.89
BRL
87
12-128
10
48
2-Methylphenol
1.69
0.37
mg/kg dry
1.89
BRL
89
26-116
12
48
2-Nitrophenol
1.43
0.37
mg/kg dry
1.89
BRL
76
20-119
14
44
3,3'-Dichlorobenzidine
1.34
0.37
mg/kg dry
1.89
BRL
71
10-191
10
35
3/4-Methyl phenol
1.71
0.37
mg/kg dry
1.89
BRL
90
28-116
12
45
4,6-Dinitro-2-methylphenol
1.20
0.37
mg/kg dry
1.89
BRL
63
30-148
22
27
4-Bromophenyl phenyl ether
2.22
0.37
mg/kg dry
1.89
BRL
117
43-126
10
26
4-Chloro-3-methylphenol
1.57
0.37
mg/kg dry
1.89
BRL
83
41-120
4
35
4-Chloroaniline
1.15
0.37
mg/kg dry
1.89
BRL
61
35-115
13
41
4-Chlorophenyl phenyl ether
1.64
0.37
mg/kg dry
1.89
BRL
86
45-123
9
30
4-Nitrophenol
0.772
0.37
mg/kg dry
1.89
BRL
41
33-136
8
31
Acenaphthene
1.77
0.37
mg/kg dry
1.89
BRL
93
46-115
11
35
Acenaphthylene
1.86
0.37
mg/kg dry
1.89
BRL
98
40-125
7
35
Anthracene
1.78
0.37
mg/kg dry
1.89
BRL
94
56-127
12
26
Azobenzene
2.86
0.37
mg/kg dry
1.89
BRL
151
49-123
3
30
Benzo(a)anthracene
1.96
0.37
mg/kg dry
1.89
BRL
104
50-134
23
25
Benzo(a)pyrene
1.84
0.37
mg/kg dry
1.89
BRL
97
59-129
24
22
Benzo(b)fluoranthene
2.06
0.37
mg/kg dry
1.89
BRL
109
46-141
19
33
Benzo(g,h,i)perylene
2.38
0.37
mg/kg dry
1.89
BRL
126
47-136
6
26
Benzo(k)fluoranthene
1.62
0.37
mg/kg dry
1.89
BRL
86
36-151
32
38
Benzoic Acid
1.20
0.37
mg/kg dry
1.89
BRL
63
10-122
8
60
Benzyl alcohol
1.74
0.37
mg/kg dry
1.89
BRL
92
29-112
8
43
bis(2-Chloroethoxy)methane
1.45
0.37
mg/kg dry
1.89
BRL
77
31-119
13
46
Bis(2-Chloroethyl)ether
1.52
0.37
mg/kg dry
1.89
BRL
80
23-111
13
54
Bis(2-chloroisopropyl)ether
1.52
0.37
mg/kg dry
1.89
BRL
81
22-109
13
50
Bis(2-Ethylhexyl)phthalate
2.33
0.37
mg/kg dry
1.89
BRL
123
45-153
9
26
Butyl benzyl phthalate
2.17
0.37
mg/kg dry
1.89
BRL
115
43-156
10
22
Chrysene
1.98
0.37
mg/kg dry
1.89
BRL
105
46-140
21
32
Dibenzo(a,h)anthracene
2.42
0.37
mg/kg dry
1.89
BRL
128
43-141
6
25
Dibenzofuran
1.70
0.37
mg/kg dry
1.89
BRL
90
45-121
10
36
Diethyl phthalate
1.70
0.37
mg/kg dry
1.89
BRL
90
53-128
8
20
Dimethyl phthalate
1.87
0.37
mg/kg dry
1.89
BRL
99
54-123
4
24
Di-n-butyl phthalate
2.16
0.37
mg/kg dry
1.89
0.109
108
44-137
4
33
Di-n-octyl phthalate
2.26
0.37
mg/kg dry
1.89
BRL
119
45-151
20
25
M
M
0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008)
Attn: Kevin Buchanan
3334 Hillsborough St. Project No: CRM-008
Prism Work Order: 1030539
Time Submitted: 3/22/11 2:45:OOPM
Raleigh, NC 27607
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1 C0533 - 3550C MS
Matrix Spike Dup (PlIC0533-11VISD1)
Source: 1030539-01
Prepared: 03/24/11 Analyzed: 03/28/11
Fluoranthene
1.41
0.37
mg/kg dry
1.89
BRL
75
37-140
31
35
Fluorene
1.55
0.37
mg/kg dry
1.89
BRL
82
49-119
11
31
Hexachlorobenzene
1.97
0.37
mg/kg dry
1.89
BRL
104
47-128
11
23
Hexachlorobutadiene
1.48
0.37
mg/kg dry
1.89
BRL
78
24-107
11
50
Hexachlorocyclopentadiene
1.37
0.37
mg/kg dry
1.89
BRL
72
20-121
21
50
Hexachloroethane
1.53
0.37
mg/kg dry
1.89
BRL
81
17-102
10
50
Indeno(1,2,3-cd)pyrene
2.47
0.37
mg/kg dry
1.89
BRL
130
27-156
6
35
Isophorone
1.89
0.37
mg/kg dry
1.89
BRL
100
22-130
8
37
Naphthalene
1.65
0.37
mg/kg dry
1.89
BRL
87
27-111
9
51
Nitrobenzene
1.72
0.37
mg/kg dry
1.89
BRL
91
23-120
11
43
N-Nitroso-di-n-propylamine
1.80
0.37
mg/kg dry
1.89
BRL
95
27-120
11
47
N-Nitrosodiphenylamine
2.91
0.37
mg/kg dry
1.89
BRL
154
46-153
5
29 M
Pentachlorophenol
1.26
0.37
mg/kg dry
1.89
BRL
67
36-155
9
31
Phenanthrene
1.89
0.37
mg/kg dry
1.89
BRL
100
48-137
28
32
Phenol
1.58
0.37
mg/kg dry
1.89
BRL
84
23-115
7
56
Pyrene
1.77
0.37
mg/kg dry
1.89
BRL
93
43-146
35
31 D
Surrogate: 2,4,6-Tribromophenol
2.18
mg/kg dry
3.79
58
34-134
Surrogate: 2-Fluorobiphenyl
1.99
mg/kg dry
1.89
105
17-122
Surrogate: 2-Fluorophenol
3.25
mg/kg dry
3.79
86
13-108
Surrogate: Nitrobenzene-d5
1.55
mg/kg dry
1.89
82
11-118
Surrogate: Phenol-d5
3.32
mg/kg dry
3.79
88
23-109
Surrogate: Terphenyl-d14
1.72
mg/kg dry
1.89
91
41-156
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 18 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1C0654 - MADEP VPH (S)
Blank (PlC0654-BLK1)
Prepared & Analyzed: 03/30/11
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl2 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
7.60
mg/kg wet
10.0 76
70-130
Surrogate: 2,5-Dibromotoluene (FID)
8.20
mg/kg wet
10.0 82
70-130
LCS (P1C0654-13SI)
Prepared & Analyzed: 03/30/11
C5-C8 Aliphatics
31.0
5.0
mg/kg wet
32.0 97
70-130
C9-Cl0 Aromatics
10.5
5.0
mg/kg wet
10.7 99
70-130
C9-Cl2 Aliphatic
31.1
5.0
mg/kg wet
32.0 97
70-130
Surrogate: 2,5-Dibromotoluene (PID)
9.74
mg/kg wet
10.0 97
70-130
Surrogate: 2,5-Dibromotoluene (FID)
9.92
mg/kg wet
10.0 99
70-130
LCS Dup (PlC0654-BSD1)
Prepared: 03/30/11 Analyzed: 03/31/11
C5-C8 Aliphatics
32.9
5.0
mg/kg wet
32.0 103
70-130 6 200
C9-Cl0 Aromatics
11.4
5.0
mg/kg wet
10.7 106
70-130 7 200
C9-Cl2 Aliphatic
34.5
5.0
mg/kg wet
32.0 108
70-130 10 200
Surrogate: 2,5-Dibromotoluene (PID)
12.7
mg/kg wet
10.0 127
70-130
Surrogate: 2,5-Dibromotoluene (FID)
12.3
mg/kg wet
10.0 123
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 19 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1C0559 - MADEP EPH (S
Blank (PlC0559-BLK1)
Prepared: 03/25/11 Analyzed: 03/29/11
C9-Cl8 Aliphatics
BRL
9.7
mg/kg wet
C19-C36 Aliphatics
BRL
9.7
mg/kg wet
C11-C22 Aromatics
BRL
9.7
mg/kg wet
Surrogate: 1-Chlorooctadecane
0.841
mg/kg wet
1.94
43
40-140
Surrogate: o-Terphenyl
1.26
mg/kg wet
1.94
65
40-140
Surrogate: 2-Fluorobiphenyl
2.21
mg/kg wet
3.88
57
40-140
Surrogate: 2-Bromonaphthalene
3.12
mg/kg wet
3.88
80
40-140
LCS (PlC0559-BSI)
Prepared: 03/25/11
Analyzed: 03/29/11
C9-Cl8 Aliphatics
25.7
9.7
mg/kg wet
58.5
44
40-140
C19-C36 Aliphatics
46.4
9.7
mg/kg wet
78.0
59
40-140
C11-C22 Aromatics
107
9.7
mg/kg wet
166
65
40-140
Surrogate: 1-Chlorooctadecane
0.799
mg/kg wet
1.95
41
40-140
Surrogate: o-Terphenyl
1.29
mg/kg wet
1.95
66
40-140
Surrogate: 2-Fluorobiphenyl
2.14
mg/kg wet
3.90
55
40-140
Surrogate: 2-Bromonaphthalene
2.96
mg/kg wet
3.90
76
40-140
LCS Dup (P1C0559-BSD1)
Prepared: 03/25/11
Analyzed: 03/29/11
C9-Cl8 Aliphatics
27.5
9.7
mg/kg wet
58.4
47
40-140 7 50
C19-C36 Aliphatics
49.6
9.7
mg/kg wet
77.8
64
40-140 7 50
C11-C22 Aromatics
104
9.7
mg/kg wet
165
63
40-140 3 50
Surrogate: 1-Chlorooctadecane
0.844
mg/kg wet
1.95
43
40-140
Surrogate: o-Terphenyl
1.27
mg/kg wet
1.95
65
40-140
Surrogate: 2-Fluorobiphenyl
2.30
mg/kg wet
3.89
59
40-140
Surrogate: 2-Bromonaphthalene
3.20
mg/kg wet
3.89
82
40-140
Matrix Spike (P1C0559-MS1)
Source: 1030539-01
Prepared: 03/25/11
Analyzed: 03/30/11
C9-Cl8 Aliphatics
32.1
11
mg/kg dry
66.4 BRL
48
40-140
C19-C36 Aliphatics
55.2
11
mg/kg dry
88.5 BRL
62
40-140
C11-C22 Aromatics
134
11
mg/kg dry
188 BRL
71
40-140
Surrogate: 1-Chlorooctadecane
0.972
mg/kg dry
2.21
44
40-140
Surrogate: o-Terphenyl
1.46
mg/kg dry
2.21
66
40-140
Surrogate: 2-Fluorobiphenyl
2.54
mg/kg dry
4.43
57
40-140
Surrogate: 2-Bromonaphthalene
3.51
mg/kg dry
4.43
79
40-140
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 23

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
4/4/11
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008)
Attn: Kevin Buchanan
3334 Hillsborough St. Project No: CRM-008
Prism Work Order: 1030539
Time Submitted: 3/22/11 2:45:OOPM
Raleigh, NC 27607
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1C0559 - MADEP EPH (S)
Matrix Spike Dup (PlIC0559-11VISD1)
Source: 1030539-01
Prepared: 03/25/11
Analyzed: 03/30/11
C9-Cl8 Aliphatics
39.0
11 mg/kg dry
67.2 BRL
58
40-140 19 50
C19-C36 Aliphatics
65.9
11 mg/kg dry
89.6 BRL
74
40-140 18 50
C11-C22 Aromatics
135
11 mg/kg dry
190 BRL
71
40-140 0.4 50
Surrogate: 1-Chlorooctadecane
1.14
mg/kg dry
2.24
51
40-140
Surrogate: o-Terphenyl
1.52
mg/kg dry
2.24
68
40-140
Surrogate: 2-Fluorobiphenyl
2.46
mg/kg dry
4.48
55
40-140
Surrogate: 2-Bromonaphthalene
3.44
mg/kg dry
4.48
77
40-140
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 21 of 23

Level II QC Report
P R I S M Full -Service Analytical 4/4/11
Environmental Solutions
. LABORATORIES, INC.
Hart & Hickman (Raleigh) Project: City of Rocky Mount (CRM-008) Prism Work Order: 1030539
Attn: Kevin Buchanan Time Submitted: 3/22/11 2:45:OOPM
3334 Hillsborough St. Project No: CRM-008
Raleigh, NC 27607
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P1C0546 - NO PREP
Blank (PlC0546-BLK1)
Prepared & Analyzed: 03/24/11
% Solids
100
0.100 % by Weight
Sample Extraction Data
Prep Method: MADEP EPH
(S)
Lab Number
Batch
Initial
Final
Date
1030539-01
PlC0559
10.15 g
2 mL
03/25/11
1030539-01
P1CO559
10.15 g
2 mL
03/25/11
Prep Method: 3550C MS
Lab Number
Batch
Initial
Final
Date
1030539-01 P1C0533 29.81 g 1 mL 03/24/11
Prep Method: 5035
Lab Number Batch Initial Final Date
1030539-01 P1CO557 4.59 g 5 mL 03/24/11
Prep Method: MADEP VPH (S)
Lab Number Batch Initial Final Date
1030539-01 P1C0654 6.85 g 6 mL 03/30/11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 23

} Ism
LABORATORIES, IPtC.
Full -Service Analytical &
Environmental Solutions
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Phone:[phone] • Fax: [phone]
Client Company Name:i4>Gi �/77Gllit/I�fr/
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Reporting Ad*ess: A17&.QfA"P "!LJ4
CHAIN/ OF CUSTODY RECORD
PAGE _t OF _3_-._ QU TIE # TO ENSURE PROPER BILLING:
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"Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
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(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
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TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: NELAC USACE FL NC
SC OTHER N/A
Water Chlorinated: YES_ NO _. s
Sle Iced U Collection: YES ✓ No
Sample on on:
p p
CLIENT
SAMPLE DESCRIPTION
DATE
Ti COLLECTED
!
TIME
COLLECTED
MILITARY
MATRIX
(SOIL,
WATER OR
SLUDGE}
SAMPLE CONTAINER
PRESERVA-
TIVES
ANALYSES REQUESTED
//t,u nn� t� �� REMARKS
1/ V
PRISM
LAB
ID NO.
*TYPE
SEE BELOW
NO.
SIZE
G----8G��s_�,¢��s
��
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EPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name:
Hart & Hickman (Raleigh)
Laboratory Name:
Prism Laboratories, Inc.
Project Name:
City of Rocky Mount (CRM-008)
NC Certification # (Lab):
402
Site Location:
1004 Coiley Rd., Rocky Mountain, NC
Sample Matrix:
Soil
Sample Information and Analytical Results
Method for Ranges: MADEP EPH
EPH Surrogate Standards: Aliphatic
EPH Fractionation Surrogates: #1 -
Sample Identification:
Date Collected:
Date Received:
Date Extracted:
Date Analyzed:
% Dry Solids:
Dilution Factor:
Hydrocarbon Ranges in mg/kg:
C9-Cl8 Aliphatics
C19-C36 Aliphatics
C11-C22 Aromatics
Blank: C9-C18 Aliphatics
C19-C36 Aliphatics
C11-C22 Aromatics
RL Cg-C18 Aliphatics
C19-C36 Aliphatics
C11-C22 Aromatics
MDL: C9-C18 Aliphatics
C19-C36 Aliphatics
C11-C22 Aromatics
Aliphatic Surrogate % Rec.:
Aromatic Surroqate % Rec.:
Frac. Surrogate #1 % Rec.:
Frac. Surrogate #2 % Rec.:
- 1-Chloro-octadecane / Aromatic - o-T
2-Bromonaphthalene / #2 - Fluorobiphe
T1-S11A
_
3/21/2011
- y
3/22/2011
3/26/2011
- _
3/30/2011
88.0
1
Sample Results
<11
<11
<11
<9.7
<9.7
.._...:.___..._..�:v
<9.7
11
11
11
0.72
1.2
........-Blank
3.1
40-140 %
43
55
65
73
Blank
40-140 %
80
82
57
59
MDL = Method Detection Limit RL = Reporting Limit Blank = Laboratory Method Blank
Were all performance/acceptance standards for required QA/QC
procedures achieved?
Was blank correction applied as a significant modification of the method?
Were any significant modifications to the EPH method made?
Comments:
1030539
YES JNo - Details Attached
Yes I NO
NO JYes - Details Attached
Page 1 of 1 EPH Soil

VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name: Hart & Hickman (Raleigh) Laboratory Name:
Project Name: City of Rocky Mount (CRM-008) NC Certification # (Lab):
Site Location: 1004 Coiley Rd., Rocky Mountain, NC Sample Matrix:
Prism Laboratories, Inc.
402
c�ii
Sample Information and Analytical Results
Method for Ranges: MADEP VPH
VPH Surrogate Standards: Aliphatic - 2,5-Dibromotoluene / Aromatic - 2,5-Dibromotoluene
Sample Identification:
T1-S11A
Collection Option (for soil'):
n .--_=
1
Date Collected:
-_
3/21/2011
Date Received:
,.�..,m_r
3/22/2011
Date Extracted:
,._..,u;;;,;�,
3/30/2011
Date Analyzed:
3/31/2011
% Dry Solids:
_ =
88.0
Dilution Factor:
-
100
Hydrocarbon Ranges in mg/kg:
sample Results
C5-C8 Aliphatics
<4.7
C9-C12 Aliphatics
13
C9-C10 Aromatics
-
<4.7
Blank:
CS -CS Aliphatics
=_ -
<5.0
C9-C12 Aliphatics
C9-C10Aromatics
<5.0
RL
C5-C8 Aliphatics
--
4.7
C9-C12 Aliphatics
- =
4.7
C9-C10 Aromatics
4.7
MDL:
C5-C8 Aliphatics
1.7
C9-C12 Aliphatics
1.7
C9-Cl0 Aromatics
0.49
Surrogate Acceptance Range:
Blank
70-130 %
Aliphatic Surrogate % Rec. - FID:
82
111
Aromatic Surrogate % Rec. - PID:
76
113
• Option 1 = Established fill line on vial
. Option 2 = Sampling device (indicate brand, e.g., Encore TM)
' Option 3 = Field weight of soil
MDL = Method Detection Limit
Blank = Laboratory Method Blank or Trip Blank
(whichever is higher - indicate type)
Were all performance/acceptance standards for required QA/QC
procedures achieved?
Were any significant modifications to the VPH method made?
Comments: VPH trip blank was not submitted to the laboratory.
RL = Reporting Limit
No - Details Attached
Yes - Details Attached
1030539 Page 1 of 1 VPH Soil