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Home My WebLink About13019_Planters Oil Mill_RRPT_20110930Brownfield's Cleanup Report Former Planter's Oil Mill Property Rocky Mount, North Carolina H&H Job No. CRM-008 September 30, 2011 ti Hart & Hickman 3334 Hillsborough Street Raleigh, NC 27607 919-847-4241 2923 South Tryon Street Suite 100 Charlotte, NC 28203 704-586-0007 #C-1269 Engineering #C-245 Geology Brownfield's Cleanup Report Former Planter's Oil Mill Property Rocky Mount, North Carolina H&H Job No. CRM-008 Table of Contents Section Pate No. EXECUTIVESUMMARY...................................................................................................................1 1.0 Introduction and Background.......................................................................................................3 1.1 Site Description.........................................................................................................................3 1.2 Site History................................................................................................................................4 1.3 Previous Environmental Assessments.......................................................................................4 2.0 Pre -Construction Activities...........................................................................................................6 2.1 Contractor Selection................................................................................................................. 6 2.2 Backfill Sampling..................................................................................................................... 6 2.2.1 Chemical Analyses..................................................................................................... 6 2.2.2 Geotechnical Analyses............................................................................................... 7 2.3 Erosion and Sedimentation Control Plan................................................................................. 7 3.0 Cleanup Activities — August/September 2011.............................................................................8 3.1 Installation of Erosion Control Measures................................................................................ 8 3.2 Cap Emplacement, Compaction and Testing.......................................................................... 8 3.3 Site Restoration.........................................................................................................................9 3.4 Topographic Survey of Cap..................................................................................................... 9 4.0 Summary and Conclusions...........................................................................................................10 i Hart & Hickman, PC SAAAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-11 doc List of Figures Figure 1 Site Location Figure 2 Site Layout with Historic Features Figure 3 Area Proposed for Clean Soil Cap Figure 4 Topographic Survey of Placed Fill List of Appendices Appendix A Chemical Laboratory Data for Cap Source Soil Appendix B Geotechnical Data for Cap Source Soil Appendix C Erosion Control Plan and Approval Letter Appendix D Photographs of Cleanup Activities Appendix E Geotechnical Certification of Cap Compaction and Thickness ii Hart & Hickman, PC SA\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 l.doc EXECUTIVE SUMMARY This Brownfield Cleanup Report (BCR) for the Former Planter's Oil Mill Property Site (Site) has been prepared by Hart & Hickman, PC (H&H) under the City of Rocky Mount's (City's) United States Environmental Protection Agency (US EPA) Region IV Brownfield Cleanup Grant (BF- 95414908-0), and documents the capping of impacted media at the Site during August and September of 2011. The capping of shallow soils impacted primarily with polynuclear aromatic hydrocarbon (PAH) compounds and arsenic was undertaken as the recommended cleanup option in accordance with the Analysis of Brownfield Cleanup Alternatives (ABCA) prepared by H&H and submitted to the US EPA Region IV and the North Carolina Department of Environment and Natural Resources (NCDENR) on June 29, 2011. After incorporating comments from the NCDENR Brownfields Program Project Manager, the ABCA was subsequently approved for implementation by both USEPA and NCDENR. Soil impacts at the site are limited to various PAH compounds above Soil Remediation Goals (SRGs) across most of the 7.3 acre site. Additionally, arsenic is present above its SRG in shallow soil at several locations. The approved remedy for soil cleanup includes: • Covering the entire 7.3 acre parcel with one foot of clean compacted fill (demonstrated through sampling) • Covering portions of the site with hardscape and building foundation materials • Any sensitive population use area such as community gardens or playgrounds will include a geotextile barrier over the fill material and in the case of gardens or other landscaping, raised be construction so the 1 foot of clean fill will not be disturbed. The City utilized its remaining Brownfield Grant funds to place a one foot layer of clean compacted fill over approximately 4.5 acres of the subject site. The remaining 2.8 acres of the overall site cannot be capped until additional funds become available which is anticipated to be 1 Hart & Hickman, PC S:\.AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc during the City's fiscal year starting July 1, 2012. This report documents implementation of the approved cleanup remedy of capping for approximately 4.5 acres of the subject property. Groundwater at the site has been impacted by various volatile organic compound (VOC), however, only two VOCs (benzene and 1,2-dichloropropane) are present above applicable standards. Additionally, the impact to groundwater in excess of applicable standards is limited in areal extent. Other groundwater contaminants in excess of applicable standards include arsenic, beryllium, cobalt, lead, manganese, dieldrin and the semivolatile organic compounds naphthalene, 2-methylnaphthalene. The approved remedy for groundwater includes various land use restrictions for both groundwater use and evaluation of potential vapor intrusion, if applicable, based upon future use of the property. The groundwater remedy is not addressed in this report. The City and NCDENR are currently finalizing a Brownfield Agreement (BFA) that will outline parameters associated with implementation of additional cleanup activities such as capping the remaining 2.8 acres and formally establishing land use restrictions in accordance with anticipated future land use. It is anticipated this BFA will be finalized by the end of 2011. 2 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc Brownfield Cleanup Report Former Planter's OR Mill Property Rocky Mount, North Carolina H&H Job No. CRM-008 1.0 Introduction and Background On behalf of the City of Rocky Mount, H&H submits this BCR for the former Planters Oil Mill property. The BCR is based on the selected cleanup alternative in the EPA and NCDENR- approved Analysis of Brownfields Cleanup Alternatives, Former Planters Oil Mill Property, Rocky Mount, North Carolina (Hart & Hickman, June 29, 2011). The soil cleanup alternative selected for the site (covering the parcel with one foot of clean compacted fill) was implemented based on effectiveness, technical feasibility, and cost, under the assumption that future use of the site could include development for multi -unit residential, associated parking, recreational and community gardens and potentially light industrial or other commercial use. Due to budgetary constraints the area capped was limited to approximately 4.5 acres of the 7.3 acre site. The remaining area will be capped as funding allows and will not be redeveloped until it has been capped and approved for redevelopment by the NCDENR Brownfield Program. 1.1 Site Description The subject site is a 7.3 acre parcel located at 1006 Cokey Road in Rocky Mount, Edgecombe County, North Carolina (Figure 1). The address has recently been changed by the City because the 1004 Cokey Road address is actually the address for the former telephone company parcel adjacent to the former Planters Oil Mill Site. The site is bounded along its eastern boundary by Cokey Road; to the north by Short Street and a former Bellsouth Facility (situated at the northeast corner of the property); to the west by Branch Street; and along the entire southern boundary by the CSX Railroad right of way (beyond which runs Norfolk Street). A site map illustrating historical structures and other features is included as Figure 2. The site is currently vacant with no existing structural improvements; all former structures were razed by the City in November 2007. The site is surrounded by an 8 ft chain link fence line along the north, east and western boundaries, and by a 6 ft chain link fence along the southern boundary. There are gated 3 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc entrances to the site along Cokey Road and Branch Street, and a break in the fence along Short Street. 1.2 Site History The property was formerly used to manufacture cottonseed and soybean oils, primarily on the eastern portion of the site. These and other manufacturing processes were reportedly performed on the site as early as 1907. The site was also used for fertilizer manufacturing operations by Kaiser Agricultural Chemical on the western portion of the property beginning in the 1970s extending through 1983, although early site operations included fertilizer production in the eastern portion of the site as well. All site operations ceased in 1983 due to a major fire that resulted in the total loss of several on -site buildings. The fire was believed to have resulted in a release of a significant volume of hexane (used to extract oil from soybeans) to the subsurface in the oil processing area (southeastern area). Following the fire and termination of operation at the facility, one or more outbuildings were leased by the owner for storage or other purposes. Ultimately the site fell into disrepair and was purchased by the City in September 2007. All structures on the site were razed by the City during November 2007. 1.3 Previous Environmental Assessments Reports and project plans developed for the site using funds from the previous US EPA Assessment Grant and the current Cleanup Grant include: • Hart & Hickman, PC, October 10, 2007, Phase I ESA, Planters Oil Mill, • Hart & Hickman, PC, August 27, 2007, Asbestos Survey, Former Planters Oil Mill Facility, • Hart & Hickman, PC, November 18, 2010, Generic QAPP, Former Planters Oil Mill Site, • Hart & Hickman, PC, November 18, 2010, Site -Specific QAPP Addendum, Former Planters Oil Mill Site, • Hart & Hickman, PC, January 7, 2011, Site -Specific QAPP Addendum, Former Planters Oil Mill Site, 4 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc • Hart & Hickman, PC, April 12, 2011, UST Closure Report, Former Planters Oil Mill. • Hart & Hickman, PC, June 29, 2011, Analysis of Brownfields Cleanup Alternatives, Former Planters Oil Mill Additional previous reports prepared under the TBA Grant include: • Oneida Total Integrated Enterprises, T N & Associates, May, 2009, Phase II Environmental Site Assessment Report, Revision 1, Planter's Oil Mill TBA, Rocky Mount, Edgecombe County, NC, • Geo Solutions, Ltd., October 29, 2008, Geophysical Evaluation, Planters Oil Mill Site, Rocky Mount, NC A summary of these previous site assessments is provided in the June 29, 2011 ABCA. 5 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc 2.0 Pre -Construction Activities 2.1 Contractor Selection The City of Rocky Mount prepared bid documents and solicited bids from qualified contractors to complete capping of 4.5 acres of the site as shown on Figure 3. The City received five qualified responses. Upon review of the bids, PLT Construction Co., Inc of Wilson, NC was selected as the winning bidder. The City also subcontracted Geotechnologies, Inc., of Raleigh, NC to perform independent geotechnical testing of the backfill material including: • Sampling proposed backfill material at the Hanson Quarry, located at NC 97 West near Rocky Mount • Compaction testing of the completed cap • Certification of the completed cap thickness 2.2 Backfll Sampling 2.2.1 Chemical Analyses To ensure that backfill materials were not contaminated prior to placement at the site, two representative samples of the backfill material were collected by H&H personnel from the Hanson Quarry and submitted for laboratory analysis for the following parameters: • VOCs — 8260B • SVOCs — 8270 • Pesticides — 8081 • PCBs — 8082 • Priority Pollutant Metals — 6010C The samples, designated BF-1 and BF-2 were collected by H&H on August 9, 2011 and submitted to Test America a NC certified laboratory located in Nashville, TN. The analytical data for these samples indicated the backfill source was "clean" and suitable for use as the cap 6 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc material. No VOCs, SVOCs, pesticides or PCBs were detected in sample BF-1. As expected in native material, low concentrations of arsenic, chromium, copper, lead, nickel and zinc were detected at background concentrations. Sample BF-2 had no SVOCs, pesticides or PCBs detected. Very low concentrations of acetone and bromomethane were detected in sample BF-2 and are believed to be associated with laboratory contamination. Arsenic, chromium, copper, lead, nickel and zinc were also detected at low, background concentrations. The laboratory certificates are included as Appendix A. 2.2.2 Geotechnical Analyses To ensure the backfill material would compact properly, two samples designated S-2 and S-3 were collected and tested by Geotechnologies, Inc. The results indicated the soil would compact to meet the 95% compaction required for the cap. Results of the laboratory compaction tests are included in Appendix B. 2.3 Erosion and Sedimentation Control Plan An erosion and sedimentation control plan was prepared and certified by Mr. Michael Tolson, PE, PLS — Assistant Water Resources Engineer for the City of Rocky Mount on July 7, 2011. The plan required the installation of temporary silt fencing around the entire 4.5 acre area planned for capping; constructing fill for positive drainage and final site restoration to include proper seeding for cap stabilization. The plan was approved by the NCDENR Division of Land Resources Land Quality Section on July 25, 2011. Copies of the plan drawings and the approval letter are included as Appendix C. 7 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc 3.0 Cleanup Activities — August/September 2011 Cleanup activities were completed to install 12-inches of clean, compacted fill material over approximately 4.5 acres of the 7.3 acre site. Capping of these 4.5 acres exhausted the remaining Brownfield Grant funds. It is anticipated the remaining area will be capped when additional funds (either City or Grant monies) become available. If additional grant funds cannot be obtained, the City may be able to fund the additional capping during the fiscal year beginning July 1, 2012. The primary cleanup objective for the site, in the context of a Brownfields redevelopment, is to reduce or prevent potential risk to future site workers engaged in redevelopment efforts, and future users of the site after redevelopment. PLT Construction performed the backfill operations under the daily oversight of City of Rocky Mount inspector Allen Goff and engineer Michael Tolson, PE, PLS. Photographs of the cleanup activities are included in Appendix D. 3.1 Installation of Erosion Control Measures During the week of August 8, 2011, prior to initiation of onsite capping operations, PLT personnel installed silt fencing in accordance with the approved Sediment and Erosion Control Plan. Additionally, a construction entrance was constructed using large stone as illustrated in the Plan drawing. 3.2 Cap Emplacement, Compaction and Testing Hauling, placement and compaction of soil for the cap was initiated on Tuesday August 16 and continued through Friday August 19. During this period, 8,880 cubic yards (cu yds) of fill material was placed on the site, spread with a bull dozer and compacted using a vibratory roller. On Sunday August 21, Rocky Mount received several inches of rain, however, erosion of the cap was minimal and the silt fencing worked as designed to control silt runoff. Due to the heavy 8 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc rain, no material was hauled during the week of August 22. Hurricane Irene hit the area on Friday evening and Saturday August 26 and 27, dumping several inches of rain on the area. Again, the site experienced minimal erosion and the silt fencing and other erosion control measures worked as designed. On Monday, September 19 the independent geotechnical engineering firm, Geotechnologies, Inc. measured the thickness of the cap and determined that additional fill material was necessary to reach the minimum compacted thickness of 12-inches, On Tuesday, September 20 PLT hauled and compacted an additional 806 cu yds of fill material bringing the total volume of fill material to 9,686. On Wednesday, September 21 Geotechnologies, Inc. completed in -place soil density testing and checked the cap thickness. Nine in -place density tests were performed. All tests achieved the required compaction of 95 percent (ASTM D-698). The depth of the in -place material ranged from 12 inches to 13.5 inches. Based upon their results, Geotechnologies, Inc. certified that the material placed meets or exceeds the required compaction depth. The certified testing results are included as Appendix E. 3.3 Site Restoration Site restoration included spreading grass seed using a "hydro seeding" method. Hydro -seeding is an application method by which grass seed, fertilizer, "hydromulch" and water are applied to an area in liquefied form. Application of this material is less labor intensive than hand seeding, and should ensure even coverage across the area of the Site. As of the date of this report an excellent stand of grass had germinated across most of the cap. Minor bare spots will be re -seeded during October 2011 to ensure the entire cap surface has been stabilized. 3.4 Topographic Survey of Cap To document the final elevation of the compacted cap material, a City of Rocky Mount survey crew, overseen by Assistant Water Resources Engineer, Michael Tolson, PE, PLS, completed a topographic survey of the cap which serves as an as -built drawing. This drawing is included as Figure 4. 9 Hart & Hickman, PC S:\AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc 4.0 Summary and Conclusions Approximately 4.5 acres of the former Planters Oil Mill site were cleaned up in accordance with the approved ABCA dated June 29, 2011. The site was capped with soils from a source that had been deemed "clean" based upon independent sampling. An independent geotechnical engineering firm has certified the cap meets or exceeds the required 12-inch thickness and 95% compaction. Final site restoration included stabilization by establishing a grass cover. Based on the capping activities completed, H&H concludes that 4.5 acres of the Planters Oil Mill site was cleaned up and meets the requirements of the approved ABCA. 10 Hart & Hickman, PC S:\.AAA-Master Projects\City of Rocky Mount - CRM\CRM-008 POM Cleanup Grant\Final Cleanup Report\CRM-008 POM Cleanup Report -FINAL- 9-30-1 Ldoc FIGURES APPROXIMATE o 2000 4000 4 SCALE /mFEET U.S.G.S.QUADRANGLE MAP ROCKY MOUNT, NC1977 QUADRANGLE 7.5MINUTE SERIES (TT)P0GRAPH|C) FORMER \ GAS STATION (TURNAGE PROPERTY)\ ------ C, P -------L------L cl SHORT STREET (FORMERLY HENNA STREET) FORMER __------------_---- \ OFFICE BUILDING \ \ ----- \ -------- ------ ------ LOCATIONFORMER CONC.�71 MAINTENPNCIt SHOP POLE(CORRUGATED STEEL) \ /, \ FORMER BOILER ROOM / RUCK SCALE FORMER �--- ---_ \ E �CK BUILDING' STODRUM RAGE CONC. PAD FORMER DRUM \ i SCA STORAGE AREA ,/ TRUCK SCALE � CONC. PIERS (FORMER SADDLE / SUMP..:..:::::.::.... PIT\l, CONCRETE PAD TANK SUPPORTS)\ \ -_ SOIL• - -I STOCKPILE PPE CONC. --__----r ----------- FORMER r FORMER FORMER , PAD \---------------__ FORMER 5,000 GAL. —__ r I BULK \ CONCRETE BALE COTTON I I FERTILIZER I FERTILIZER I - LOADING/UNSO�iN�G- #6 FUEL OIL UST CONC. RAMP STORAGE I WAREHOUSE WAREHOUSE I - - I I - - - - - - J - TRANSFORMER PAD � \ 1E�EdQ Jt— — — — — — J FORMER HULL HOUSE I \ \ L------ +� �-I ►� '_1-i' f +I� APPROXIMATE LOCATION ± FORMER RR SPUR I� +I� CONCRETE PIT HEXANE I W TER VALVE/METER BOXES® \ - - - FORMER STRUCTURE LOCATION W/RISER STORAGE TANK COOLING I ®®, �- - \ \ ® EXISTING STRUCTURE APPROXIMATE EDGE FORMER - TOWER - 1 :- .- -.-.- - - 77n- T OF TREEUNE OIL AST - - - - - J BEAN DRYER`J \ 0 EXISTING CONCRETE 1.. ...... ...... ...... ...... .. I - - ® FORMER AST LOCATION I I: CONCRETE DRY -..�.- - SUMP L FORMER I I F I �- F �P EXISTING RAILROAD I I::::::::::::::::::::::'::::::::::::SLAB:::::::: ::::::::::::::::::::::::: STORAGE .::::: :::. -. -.. ":- SOLVENT L -I SEED \ {BUILDIN I SHED 1:::::.;:::::.::::::::::::::::::......................:::::::::::::::::......::::::::::::::. I OFFICE + H ABANDONED RAILROAD G F .. -EXTRACTION I HOUSE 0 OTP .:.....:........ .. RI NT FORMER FERTI " ' I L - J IIZER .. 1 ........... BEAN DRYER FORMER .FERTILIZ ': ::' :::::.::::::::::::::BAG I ....._:::::::::::::::::::::::::::.:::::.::::::::::::::::::::::: MI ER.....Cp GING HOUSE.... ® I ELEVAT R ER NCRETE: ® ® ® FORMER FORMER \ -....................................... ...... .... ...XING.... STORAGE"-%%% ........� I -- _:.:::::. STAB::::::::::::::::::::::::::::::::::::::::® ® ® LINTER I BOILER I ---_ _ J®®® Im ® I I ROOM r FORMER OIL ASTs BASEMENT -f I-I-f 4- 1-4 -I-I-I -- �® I ►� ) SEED \ N I-I'f i�1-} I -I _ I 1 TANK SEED -} 1-I- f APPROXIMATES _ -- - - I } I-f } 1-+ 1-f +-1-f +-1-f -f-I-f +_ _ _ j-�1 SEED TANK i FORMER RR SPUR APPROXIMATE-PPROPER -� L - TANK I'I 7-1'f i-I-I I-I_I 1-I'4 I�I'f I-1'i I i__I' I �SX RIGHT OF W4Y C — - -- C VEYOR \ APPROXIMATE I 1-1 + I-f + NSFORMER PAD _ 0 100 200 I- TRANSFORMER PALEiiiiiiFma SCALE IN FEET L — (PIT) R \ ------------------------------ CSX RAILROAD ---__—__ FORMER OIL � ---- PROCESSING FACILITY HISTORIC SITE LAYOUT -------__—__— — (CRACKING HOUSE) RFOLK STREET -------------__-__ `RIN'EC` FORMER PLANTERS OIL MILL _ 1006 COKEY ROAD W-r---__-_ - _ - ROCKY MOUNT, EDGECOMBE COUNTY, NC W E, ---__— 3334 FIillsborough Street �afi & �C�� Raleigh, North Carolina 27607 �J r ___ A PROFESSIONAL CORPORATION 919-847-4241(p)919-847-4261(� iI WILFAB METALS SITE I x I I U I i DATE: 09/30/11 REVISION NO. 0 JOB NO: CRM-008 FIGURE NO. 2 ------------- 1 - SHORT STREET (FORMERLY HENNA STREET) --- APPROXIMATE PROPERTY LINE 7--cSX RIGHT OF WAY ----- ...... ...... ------...... ...... ...... ...... RAILROAD r------------ - �------------0----------- ------- FOLK STREET I -----------,-------- --------------- ------ W -r----------- ------ i I I o E, I I ------ --- � __-__------------------------- ----- �x ►' iz.,�i i i i ii EXISTING RAILROAD AREA PROPOSED FOR CLEAN SOIL CAP APPROXIMATE 100 200 SCALE IN FEET AREA PROPOSED FOR CLEAN SOIL CAP PROJECT FORMER PLANTERS OIL MILL 1006 COKEY ROAD ROCKY MOUNT, EDGECOMBE COUNTY, NC g ciman 3334 FIillsb Street Raleigh, Northrth Carolina 27607 A PROFESSIONAL CORPORATION 919-847-4241(p)919-847-4261(f Q1i12wow, «•7f�1 JOB NO: CRM-008 FIGURE NO. 3 PROD VICINITY MAP - 5CALE - 1 " = 2000' I 4s I I :z SSMH f = 107.05' ----_ r - 105.45'_ , F 't I1 22 III l� o _ m It � s 4 � I �END OF PIPE i rVOT LOCATED 6' PPE 6" p U) i ;� CB 1 TOP = 715.83' I I INK = 114.20' 515MH ' TOP = 117.42' - INV IN = 107.72' INV OUT = 107.62' \ i N 22W'51 " E 8 TO 31r IPF) �I 1 24" RCP X INV. 112.79' J3`7 I � TOP 716.33' I IINV. IN (EAST) = 709.63' V. IN (SOUTH) INV OUT -� 709.63 jlll � j SS,MH � 1 ! TOP = 114.88' SHORT S T l�E T 1 INV. IN = lOB.38' 2 NV OUT = 108.28' VARfALE��so F� y cac 8" TERRACOTA SANITARY SEVER LINE _ __-_ - HONE I Dp 30" , HEAP E R!C and TF_ - O a f �» E 30.'a'8' 374 t Dqj� b N 86 ` %� _ N 89 4 '4 132. R 6' CHAIN LINK FENCE PF erdtsEtEG `x' FOUND �trt6 CHAIN UNK F NCE/��r� xt74145OXIMATE LOCATION x7P5.35 x71e.47 END OF SEWER = `� tx coxcRE>F x7t4 11..9s xtida OF EXI5T,1t�t.g`;JI.T FENCE LINE NOT FOUND cr, n-' x X114.60 114.77 xtt4.8a 7i -ppi� °) Q ��3 \A � 1 ��O �2Q \� of \ �O -L\ �: ae�� \\h� / \ ! '� �\A u/'A �\ T x114.51 'o T f r X1r4.4r {, � X714.62 XtI4.60 Xtt \ X175.211 XP6 X127 �� /X 115.02 r>) O) 1X� if 715.Ov2 115 / �1+4.ff7 <0 G7� �� \G%• X 3 +\ X7t5.42 Xit&38 \�• jy 1,147/ 9- xlr5.as X174.19 X i73.72 x114.00� 12 o� ..Z 1 \ \{a• xrt4.sr �\ Lo' \�t'i48e-715-\-GJ-- Xt15.S \' X9T7�- \\,L)• X114.57 Co14.35JSX5.PRCXrE �ATIOU G15TINGICTICONSTON _ ENTRAN,(;;ARIT fi f �- ' X114.89 V 2Xf14.62 ( X11422 +t 5.04 a x j �O3 x175.14 \ x114.e4 / xt 944\� a �. \2 p2 115.14 ` (y 5.32 O^ j 'pa o� Xr &ai \tO2 \tO Z\�X174.55 �\�'\ 1 \\ xrr5.De/�\\� \�-1\,`4, + \ �\ + �\ +\ a b WXftX83 X115-08 774.70 X t P5$4 X I15. 8 ' �I X115.76 CITY OF ROCKY MOUNT n4.stx NO Municipal Cor orati: y Cp1 �--'" Xtta36 17 p �a I APPROXIMATE L ' 08 f/ DB 1500, PC4)W07 OCA�bW X11S73 �! \ \\OF EX15TING 51 T FENCE r� y �/ of O� �� 365 A�'a"es X 16.14 X 116 94 �`--��?0��__ \ 3 x 11s/S� /'; \ (pO \ � • + \ +\ t X77535 176---._ X77 Al X }`64. 69 _1 1t5.82 .--""7 5 - �515 / + X7 .4.-1P6 \� =\\'� + Xif423 C .38 (94 ,�` V-XIt4.77 Xtt£37 X114.65 CS \ _ 1_._\ +�115.2s < \ TOP=+5.74' T-x7-/ss xtl4.ra xlr4.rf xt IN OUT (6"' = 114.34' I"' X775.37 �� X 175.23 X 1 t576 x�rS.31 x114.51 X114.40 i LO� \X 11555 X11533 Xtt4.43 n t +", \�' �� \ \ X714.36 X77A22 ' X7 b i33�0 XIPL43 m I 1Pl- n INV = 112.90' PK NAIL SET g18 BAD `83/2007 N- 795,024.979 usft E- 2,357,585.166 usft ELEV- 117.89 usft (SEE NOTE 5) 1 1 566 , IN. �2 I 131 4. X 77 . .30 (X 71( x116.25L'DITCLt x 115.98 R/W 7tI X715.41 NOTE5: I . THE BACKGROUND BOUNDARY AND TOPOGRAPHIC INFORMATION SHOWN IN GRAY ON TH15 PLAN WAS TAKEN FROM A SURVEY PREPARED BY JOYNER KEENY, PLLC PLANNING AND LAND 5URVEYING ENTITLED "BOUNDARY AND TOPOGRAPHIC MAP OF: PLANTERS OIL MILL 51TE ROCKY MOUNT, NC' DATED 04/ 1 5/2010, 2. IT 15 THE PURP05E AND INTENT OF TH15 DRAWING TO 5HOW GROUND ELEVATION5 A5 Of 9-22-201 1 A5 GATHERED BY CITY OF ROCKY MOUNT SURVEYING PERSONNEL. NO OTHER BOUNDARY OR UTILITY RETRACEMENT OR RELOCATION WA5 PERFORMED DURING TH15 FIELD SURVEY. m 1-STORY BRICK BUILDING D'S RENTAL, LLP DB 1515, PG 219 - F 7#17 J?. 7 �774.63 z \3.99 L..-'1 i 4 n3 a2 f �•''� f xtr3.4s X }73.H0 DI TOP = 111.37' ItJV. IN (15) - IN V OUT (2a1 106.72' l� a� END OF PIPE xrts.7,4 �� x173.48 11.5. xl is3Pf�"' NOT LOCATED X113.79--p1. �--- \� \ X71 °.35 Xt74.f4 \ C� GO TOP = 112.21' n474 ✓ / x11346 \y aa5 \ INV IN (15') - 106.71' APPROXIM T LOQCATION OF EXISTI (TE'P FENCE x1r tt �`i3 xt'�NY.) \ �s 17A57�\ \q' X114.24 X114.12 xtfa.35 ,. END OF PIPE o \Gj • +VAS. \U FOUND io\ X I14. 15 X1N30 [K XIILoo \�� \A `XPf4.31 X114.15 „ \ 106 Ss My/ TO 713.&1' ` IrNV. IN = 108.21' INV. OUT = 108.11' yam. 3f4"` L 7PF \ x \5 - 13.14� 1 t X\�t X 11394 \ �Q X713.47 X11zFR \ , Xit348 s Xt7379 XPP465 X 774.77 \\\ 1 Q,. x1P4.4o�, rt367 CONCRETE Vt'ALt x 2• HIGH V1/ WATER _ F o PIPES IN BOTTOM Xt X 113 78 S S ay'-� `a SEAL s L-4789 _> S /7q llttiDlllil Vl 2 V REV1510N5 Idl aF g?p--% ` ROCKY T\ MOUNT NORTH CAROLINA X 114. Z3 Xt7373 \ $SkAI'( ` XIKJI X�-73.sr 0 To = 97335' x1142 �-_ IN V IN = 109.55' INV. OUT 109.45' X 713, 69 X 11A67 "'GAG-- _ X7t4.40 X' pa PLANTER,5 STREET x r1 .10 X7f457 XlM55 X714.56 \ X 1730 S _� X 114.66 Y X714,50 71X38 tx 84 `\ 7t4.0\3'>C 773.20 % a xn4.43 �'\ y X114.64 \\ \ X974.59 X7P4.78 \r tt3.53 r �2 . Oc7 1ssf- ��CIYAIN LINK FEftrCE' 76�_ -115 S� 5 xr16.07 X776.66 _ t 15 114'79 t T LF �� RAILROAD --_-X77535 Ai1t4.PE N 845021" 3✓ TRACK xrt4.Ss i - J7al.g2 (#4 TO78� x114.s3 - �- x 174.46 -114�3- CSX RAILROAD X1P4.33 INV = 109,23' J 130' R+0j R/W _ R/W R/W S.S& TOP INV. \ N \ 1C Tk INV. = 109.11'�.. '- q INV. = 108.82' END OF PIPE - NOT LOCATED RK NAIL SETSET NAD '83f2007 F N- 794,917766 usft E- 2,358,772.259 usft ELEV- 115.53 usft i (SEE NOTE 5) , BEFORE YOU CALL Ffno 5HEET TITLE: PLANTE[� OI L MILL FILL REMEDIATION TOPOGfZAPt11C SURVEY OF PLACED FILL PROJECT #: POCLE CAD FILE: Planter5-5P DATE: 09-23-20 I 1 5URVEYED BY: see notes 1 RLC DESIGNED BY: n/a DRAWN BY: mcit CHECKED BY: mcit 5CALE: I It= 50' DRAWING #: D-541 2 5HEET NUMBER: I OF I FIGURE 4 sa zs o sa :oa as GR FMC 5CALE: 1"= Sa 3NE CALL CE P✓WW. r7Cf7GG. APPENDIX A Chemical Laboratory Data of Cap Source Soil TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Road Nashville, TN 37204 Tel: 800-765-0980 TestAmerica Job ID: NUH1259 Client Project/Site: CRM-008 Client Project Description: City of Rocky Mount - POM For: Hart & Hickman 3334 Hillsborough St Raleigh, NC 27607 Attn: Leonard Moretz Authorized for release by: 0811112011 04:59:38 PM Ken A. Hayes Senior Project Manager ken.hayes@testamericainc.com This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Page 1 of 38 08/11 /2011 Client: Hart & Hickman Project/Site: CRM-008 Table of Contents TestAmerica Job ID: NUH1259 Cover Page .............................................. 1 Table of Contents ......................................... 2 Sample Summary ......................................... 3 Definitions ............................................... 4 Client Sample Results ...................................... 5 QC Sample Results ........................................ 15 QC Association ........................................... 31 Chronicle................................................ 34 Method Summary ......................................... 35 Certification Summary ...................................... 36 Chain of Custody .......................................... 37 TestAmerica Nashville Page 2 of 38 08/11/2011 Client: Hart & Hickman Sample Summary TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Lab Sample ID Client Sample ID Matrix Collected Received NUH1259-01 NUH1259-02 BF-1 BF-2 Soil Soil 08/09/1112:50 08/09/1113:10 08/10/1106:30 08/10/1106:30 TestAmerica Nashville Page 3 of 38 08/11/2011 Client: Hart &Hickman Definitions/Glossary TestAmerica Job ID: NUH1259 Project/Site: CRM-008 wuai flers GCMS Semivolatiles Qualifier Qualifier Description MNR No results were reported for the MS/MSD. The sample used for the MS/MSD required dilution due to the sample matrix. Because of this, the spike compounds were diluted below the detection limit. Pesticides Qualifier Qualifier Description Z2 Surrogate recovery was above the acceptance limits. Data not impacted. Metals Qualifier Qualifier Description M7 The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS). M8 The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS). Glossary Abbreviation These commonly used abbreviations may or may not be present in this report Listed under the "D" column to designate that the result is reported on a dry weight basis. %R Percent Recovery EDL Estimated Detection Limit (Dioxin) EPA United States Environmental Protection Agency MDL Method Detection Limit ML Minimum Level (Dioxin) ND Not detected at the reporting limit (or method detection limit if shown). PQL Practical Quantitation Limit RE, RE1 (etc.) Indicates a Re -extraction or Reanalysis of the sample. RL Reporting Limit RPD Relative Percent Difference, a measure of the relative difference between two points. TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) 0 TestAmerica Nashville Page 4 of 38 08/11/2011 Client: Hart &Hickman Client Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-1 Lab Sample ID: NUH1259-01 Date Collected: 08/09/11 12:50 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.3 Method: SW846 8260E - Volatile Organic Compounds by EPA Method 8260E Analyte Result Qualifier RL MDL unit D Prepared Analyzed Dil Fac Acetone ND 0.0577 mg/kg dry 3:� 08/09/11 12:50 08/10/11 17:12 1.00 Benzene ND 0.00231 mg/kg dry # 08/09/11 12:50 08/10/11 17:12 1.00 Bromobenzene ND 0.00231 mg/kg dry # 08/09/11 12:50 08/10/11 17:12 1.00 Bromochloromethane ND 0.00231 mg/kg dry # 08/09/11 12:50 08/10/11 17:12 1.00 Bromodichloromethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Bromoform ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Bromomethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2-Dibromo-3-chloropropane ND 0.00577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 2-Butanone ND 0.0577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 sec -Butyl benzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 n-Butylbenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 tert-Butylbenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Carbon disulfide ND 0.00577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Carbon Tetrachloride ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Chlorobenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Chlorodibromomethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Chloroethane ND 0.00577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Chloroform ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Chloromethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 2-Chlorotoluene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 4-Chlorotoluene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2-Dibromoethane (EDB) ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Dibromomethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,4-Dichlorobenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,3-Dichlorobenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2-Dichlorobenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Dichlorodifluoromethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,1-Dichloroethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2-Dichloroethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 cis-1,2-Dichloroethene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,1-Dichloroethene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 trans-1,2-Dichloroethene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,3-Dichloropropane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2-Dichloropropane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 2,2-Dichloropropane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 cis-1,3-Dichloropropene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 trans-1,3-Dichloropropene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,1-Dichloropropene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Ethylbenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Hexachlorobutadiene ND 0.00577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 2-Hexanone ND 0.0577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Isopropylbenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 p-Isopropyltoluene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Methyl tert-Butyl Ether ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Methylene Chloride ND 0.0115 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 4-Methyl-2-pentanone ND 0.0577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Naphthalene ND 0.00577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 n-Propylbenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Styrene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,1,1,2-Tetrachloroethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 TestAmerica Nashville Page 5 of 38 08/11 /2011 Client Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-1 Lab Sample ID: NUH1259-01 Date Collected: 08/09/11 12:50 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.3 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2,2-Tetrachloroethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Tetrachloroethene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Toluene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2,3-Trichlorobenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2,4-Trichlorobenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,1,2-Trichloroethane ND 0.00577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,1,1-Trichloroethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Trichloroethene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Trichlorofluoromethane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2,3-Trichloropropane ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,3,5-Trimethylbenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2,4-Trimethylbenzene ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Vinyl chloride ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Xylenes, total ND 0.00577 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Diisopropyl Ether ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 1,2-Dichloroethene (total) ND 0.00231 mg/kg dry 08/09/11 12:50 08/10/11 17:12 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 98 67- 138 08109111 12:50 08110111 17:12 1.00 Dibromofluoromethane 88 75 - 125 08109111 12:50 08110111 17:12 1.00 Toluene-d8 105 76 - 129 08109111 12:50 08110111 17:12 1.00 4-Bromofluorobenzene 108 67 - 147 08109111 12:50 08110111 17:12 1.00 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Acenaphthylene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Anthracene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Benzo (a) anthracene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Benzo (a) pyrene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Benzo (b) fluoranthene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Benzo (g,h,i) perylene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Benzo (k) fluoranthene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 4-Bromophenyl phenyl ether ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Butyl benzyl phthalate ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Carbazole ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 4-Chloro-3-methylphenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 4-Chloroaniline ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Bis(2-chloroethoxy)methane ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Bis(2-chloroethyl)ether ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Bis(2-chloroisopropyl)ether ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2-Chloronaphthalene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2-Chlorophenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 4-Chlorophenyl phenyl ether ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Chrysene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Dibenz (a,h) anthracene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Dibenzofuran ND 0.408 mg/kg dry 357 08/10/11 11:30 08/11/11 14:41 1.00 Di-n-butyl phthalate ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 1,4-Dichlorobenzene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 1,2-Dichlorobenzene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 TestAmerica Nashville Page 6 of 38 08/11 /2011 Client: Hart &Hickman Client Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-1 Lab Sample ID: NUH1259-01 Date Collected: 08/09/11 12:50 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.3 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D (Continued) Analyte Result Qualifier RL MDL unit D Prepared Analyzed Dil Fac 1,3-Dichlorobenzene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 3,3-Dichlorobenzidine ND 0.817 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2,4-Dichlorophenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Diethyl phthalate ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2,4-Dimethyl phenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Dimethyl phthalate ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 4,6-Dinitro-2-methylphenol ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2,4-Dinitrophenol ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2,6-Dinitrotoluene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2,4-Dinitrotoluene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Di-n-octyl phthalate ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Bis(2-ethylhexyl)phthalate ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Fluoranthene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Fluorene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Hexachlorobenzene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Hexachlorobutadiene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Hexachlorocyclopentadiene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Hexachloroethane ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Indeno (1,2,3-cd) pyrene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Isophorone ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2-Methyl naphthalene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2-Methylphenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 3/4-Methylphenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Naphthalene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 3-Nitroaniline ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2-Nitroaniline ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 4-Nitroaniline ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Nitrobenzene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 4-Nitrophenol ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2-Nitrophenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 N-Nitrosodiphenylamine ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 N-Nitrosodi-n-propylamine ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Pentachlorophenol ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Phenanthrene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Phenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Pyrene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 1,2,4-Trichlorobenzene ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 1-Methyl naphthalene ND 0.0820 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2,4,6-Trichlorophenol ND 0.408 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 2,4,5-Trichlorophenol ND 1.02 mg/kg dry 08/10/11 11:30 08/11/11 14:41 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac Terphenyl-d14 80 18- 120 08110111 11:30 08111111 14:41 1.00 2,4,6-Tribromophenol 58 19-120 08110111 11:30 08111111 14:41 1.00 Phenol-d5 58 18 - 120 08110111 11:30 08111111 14:41 1.00 2-Fluorobiphenyl 59 14 - 120 08110111 11:30 08111111 14:41 1.00 2-Fluorophenol 61 17 - 120 08110111 11:30 08111111 14:41 1.00 Nitrobenzene-d5 58 17 - 120 08110111 11:30 08111111 14:41 1.00 TestAmerica Nashville Page 7 of 38 08/11/2011 Client Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-1 Lab Sample ID: NUH1259-01 Date Collected: 08/09/11 12:50 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.3 Method: SW846 8081 B - Organochlorine Pesticides by EPA Method 8081 B Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin ND 0.00205 mg/kg dry 3:� 08/10/11 11:14 08/10/11 19:43 1.00 7- delta-BHC ND 0.00205 mg/kg dry # 08/10/11 11:14 08/10/11 19:43 1.00 alpha-BHC ND 0.00205 mg/kg dry # 08/10/11 11:14 08/10/11 19:43 1.00 beta-BHC ND 0.00398 mg/kg dry # 08/10/11 11:14 08/10/11 19:43 1.00 gamma-BHC (Lindane) ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 alpha -Chlordane ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 F gamma -Chlordane ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Chlordane ND 0.0805 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 F 4,4'-DDD ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 4,4'-DDE ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 4,4'-DDT ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Dieldrin ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Endosulfan I ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Endosulfan 11 ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Endosulfan sulfate ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Endrin ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Endrin aldehyde ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Endrin ketone ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Heptachlor ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Heptachlor epoxide ND 0.00205 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Methoxychlor ND 0.00398 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Toxaphene ND 0.0805 mg/kg dry 08/10/11 11:14 08/10/11 19:43 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro-meta-xylene 92 22 - 150 08110111 11:14 08110111 19:43 1.00 Decachlorobiphenyl 106 25 - 150 08/10/11 11:14 08/10/11 19:43 1.00 Method: SW846 8082A - Polychlorinated Biphenyls by EPA Method 8082A Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac PCB-1016 ND 0.0402 mg/kg dry * 08/10/11 12:05 08/11/11 00:04 1.00 PCB-1221 ND 0.0402 mg/kg dry # 08/10/11 12:05 08/11/11 00:04 1.00 PCB-1232 ND 0.0402 mg/kg dry # 08/10/11 12:05 08/11/11 00:04 1.00 PCB-1242 ND 0.0402 mg/kg dry # 08/10/11 12:05 08/11/11 00:04 1.00 PCB-1248 ND 0.0402 mg/kg dry # 08/10/11 12:05 08/11/11 00:04 1.00 PCB-1254 ND 0.0402 mg/kg dry # 08/10/11 12:05 08/11/11 00:04 1.00 PCB-1260 ND 0.0402 mg/kg dry * 08/10/11 12:05 08/11/11 00:04 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro-meta-xylene 70 19 - 147 08110111 12:05 08111111 00:04 1.00 Decachlorobiphenyl 114 20 - 150 08110111 12:05 08111111 00:04 1.00 Method: SW846 6010C - Total Metals by EPA 6010C Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 11.9 mg/kg dry * 08/10/11 12:00 08/10/11 21:06 1.00 Arsenic 5.80 1.19 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 Beryllium ND 1.19 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 Cadmium ND 1.19 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 Chromium 25.2 1.19 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 Copper 16.1 2.38 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 Lead 14.1 1.19 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 Nickel 10.2 1.19 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 TestAmerica Nashville Page 8 of 38 08/11 /2011 Client Sample Results Client: Hart & Hickman Project/Site: CRM-008 TestAmerica Job ID: NUH1259 Client Sample ID: BF-1 Lab Sample ID: NUH1259-01 Date Collected: 08/09/11 12:50 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.3 Method: SW846 6010C - Total Metals by EPA 6010C (Continued) Analyte Result Qualifier RL Selenium ND 2.38 Silver ND 1.19 Thallium ND 2.38 Zinc 61.4 11.9 Method: SW846 7471 B - Mercury by EPA Method 7471 B Analyte Result Qualifier RL Mercury ND 0.12 Method: SW-846 - General Chemistry Parameters Analyte Result Qualifier RL % Dry Solids 81.3 0.500 MDL Unit D Prepared Analyzed Dil Fac mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 mg/kg dry 08/10/11 12:00 08/10/11 21:06 1.00 F MDL Unit D Prepared Analyzed Dil Fac mg/kg dry 08/11/11 10:00 08/11/11 13:50 1.0 MDL Unit D Prepared Analyzed Dil Fac % 08/10/1114:32 08/11/1110:48 1.00 TestAmerica Nashville Page 9 of 38 08/11/2011 Client: Hart &Hickman Client Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-2 Lab Sample ID: NUH1259-02 Date Collected: 08/09/11 13:10 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.5 Method: SW846 8260E - Volatile Organic Compounds by EPA Method 8260E Analyte Result Qualifier RL MDL unit D Prepared Analyzed Dil Fac Acetone 0.0943 0.0621 mg/kg dry 3:� 08/09/11 13:10 08/10/11 17:44 1.00 Benzene ND 0.00248 mg/kg dry # 08/09/11 13:10 08/10/11 17:44 1.00 Bromobenzene ND 0.00248 mg/kg dry # 08/09/11 13:10 08/10/11 17:44 1.00 Bromochloromethane ND 0.00248 mg/kg dry # 08/09/11 13:10 08/10/11 17:44 1.00 Bromodichloromethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Bromoform ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Bromomethane 0.00267 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2-Dibromo-3-chloropropane ND 0.00621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 2-Butanone ND 0.0621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 sec -Butyl benzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 n-Butylbenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 tert-Butylbenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Carbon disulfide ND 0.00621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Carbon Tetrachloride ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Chlorobenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Chlorodibromomethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Chloroethane ND 0.00621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Chloroform ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Chloromethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 2-Chlorotoluene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 4-Chlorotoluene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2-Dibromoethane (EDB) ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Dibromomethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,4-Dichlorobenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,3-Dichlorobenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2-Dichlorobenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Dichlorodifluoromethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,1-Dichloroethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2-Dichloroethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 cis-1,2-Dichloroethene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,1-Dichloroethene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 trans-1,2-Dichloroethene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,3-Dichloropropane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2-Dichloropropane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 2,2-Dichloropropane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 cis-1,3-Dichloropropene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 trans-1,3-Dichloropropene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,1-Dichloropropene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Ethylbenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Hexachlorobutadiene ND 0.00621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 2-Hexanone ND 0.0621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Isopropylbenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 p-Isopropyltoluene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Methyl tert-Butyl Ether ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Methylene Chloride ND 0.0124 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 4-Methyl-2-pentanone ND 0.0621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Naphthalene ND 0.00621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 n-Propylbenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Styrene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,1,1,2-Tetrachloroethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 TestAmerica Nashville Page 10 of 38 08/11/2011 Client Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-2 Lab Sample ID: NUH1259-02 Date Collected: 08/09/11 13:10 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.5 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,2,2-Tetrachloroethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Tetrachloroethene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Toluene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2,3-Trichlorobenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2,4-Trichlorobenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,1,2-Trichloroethane ND 0.00621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,1,1-Trichloroethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Trichloroethene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Trichlorofluoromethane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2,3-Trichloropropane ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,3,5-Trimethylbenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2,4-Trimethylbenzene ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Vinyl chloride ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Xylenes, total ND 0.00621 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Diisopropyl Ether ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 1,2-Dichloroethene (total) ND 0.00248 mg/kg dry 08/09/11 13:10 08/10/11 17:44 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 96 67- 138 08109111 13:10 08110111 17:44 1.00 Dibromofluoromethane 89 75 - 125 08109111 13:10 08110111 17:44 1.00 Toluene-d8 105 76 - 129 08109111 13:10 08110111 17:44 1.00 4-Bromofluorobenzene 113 67 - 147 08109111 13:10 08110111 17:44 1.00 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Acenaphthylene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Anthracene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Benzo (a) anthracene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Benzo (a) pyrene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Benzo (b) fluoranthene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Benzo (g,h,i) perylene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Benzo (k) fluoranthene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 4-Bromophenyl phenyl ether ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Butyl benzyl phthalate ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Carbazole ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 4-Chloro-3-methylphenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 4-Chloroaniline ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Bis(2-chloroethoxy)methane ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Bis(2-chloroethyl)ether ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Bis(2-chloroisopropyl)ether ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2-Chloronaphthalene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2-Chlorophenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 4-Chlorophenyl phenyl ether ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Chrysene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Dibenz (a,h) anthracene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Dibenzofuran ND 0.401 mg/kg dry 357 08/10/11 11:30 08/11/11 15:04 1.00 Di-n-butyl phthalate ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 1,4-Dichlorobenzene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 1,2-Dichlorobenzene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 TestAmerica Nashville Page 11 of 38 08/11/2011 Client: Hart &Hickman Client Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-2 Lab Sample ID: NUH1259-02 Date Collected: 08/09/11 13:10 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.5 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D (Continued) Analyte Result Qualifier RL MDL unit D Prepared Analyzed Dil Fac 1,3-Dichlorobenzene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 3,3-Dichlorobenzidine ND 0.803 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2,4-Dichlorophenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Diethyl phthalate ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2,4-Dimethyl phenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Dimethyl phthalate ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 4,6-Dinitro-2-methylphenol ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2,4-Dinitrophenol ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2,6-Dinitrotoluene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2,4-Dinitrotoluene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Di-n-octyl phthalate ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Bis(2-ethylhexyl)phthalate ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Fluoranthene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Fluorene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Hexachlorobenzene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Hexachlorobutadiene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Hexachlorocyclopentadiene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Hexachloroethane ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Indeno (1,2,3-cd) pyrene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Isophorone ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2-Methyl naphthalene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2-Methylphenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 3/4-Methylphenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Naphthalene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 3-Nitroaniline ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2-Nitroaniline ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 4-Nitroaniline ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Nitrobenzene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 4-Nitrophenol ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2-Nitrophenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 N-Nitrosodiphenylamine ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 N-Nitrosodi-n-propylamine ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Pentachlorophenol ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Phenanthrene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Phenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Pyrene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 1,2,4-Trichlorobenzene ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 1-Methyl naphthalene ND 0.0807 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2,4,6-Trichlorophenol ND 0.401 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 2,4,5-Trichlorophenol ND 1.00 mg/kg dry 08/10/11 11:30 08/11/11 15:04 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac Terphenyl-d14 93 18- 120 08110111 11:30 08111111 15:04 1.00 2,4,6-Tribromophenol 74 19-120 08110111 11:30 08111111 15:04 1.00 Phenol-d5 74 18 - 120 08110111 11:30 08111111 15:04 1.00 2-Fluorobiphenyl 77 14 - 120 08110111 11:30 08111111 15:04 1.00 2-Fluorophenol 74 17 - 120 08110111 11:30 08111111 15:04 1.00 Nitrobenzene-d5 70 17 - 120 08110111 11:30 08111111 15:04 1.00 TestAmerica Nashville Page 12 of 38 08/11/2011 Client Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-2 Lab Sample ID: NUH1259-02 Date Collected: 08/09/11 13:10 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.5 Method: SW846 8081 B - Organochlorine Pesticides by EPA Method 8081 B Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin ND 0.00206 mg/kg dry 3:� 08/10/11 11:14 08/10/11 19:58 1.00 7- delta-BHC ND 0.00206 mg/kg dry # 08/10/11 11:14 08/10/11 19:58 1.00 alpha-BHC ND 0.00206 mg/kg dry # 08/10/11 11:14 08/10/11 19:58 1.00 beta-BHC ND 0.00400 mg/kg dry # 08/10/11 11:14 08/10/11 19:58 1.00 gamma-BHC (Lindane) ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 alpha -Chlordane ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 F gamma -Chlordane ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Chlordane ND 0.0809 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 F 4,4'-DDD ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 4,4'-DDE ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 4,4'-DDT ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Dieldrin ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Endosulfan I ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Endosulfan 11 ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Endosulfan sulfate ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Endrin ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Endrin aldehyde ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Endrin ketone ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Heptachlor ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Heptachlor epoxide ND 0.00206 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Methoxychlor ND 0.00400 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Toxaphene ND 0.0809 mg/kg dry 08/10/11 11:14 08/10/11 19:58 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro-meta-xylene 76 22 - 150 08110111 11:14 08110111 19:58 1.00 Decachlorobiphenyl 86 25 - 150 08110111 11:14 08110111 19:58 1.00 Method: SW846 8082A - Polychlorinated Biphenyls by EPA Method 8082A Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac PCB-1016 ND 0.0399 mg/kg dry * 08/10/11 12:05 08/11/11 00:25 1.00 PCB-1221 ND 0.0399 mg/kg dry # 08/10/11 12:05 08/11/11 00:25 1.00 PCB-1232 ND 0.0399 mg/kg dry # 08/10/11 12:05 08/11/11 00:25 1.00 PCB-1242 ND 0.0399 mg/kg dry # 08/10/11 12:05 08/11/11 00:25 1.00 PCB-1248 ND 0.0399 mg/kg dry # 08/10/11 12:05 08/11/11 00:25 1.00 PCB-1254 ND 0.0399 mg/kg dry # 08/10/11 12:05 08/11/11 00:25 1.00 PCB-1260 ND 0.0399 mg/kg dry * 08/10/11 12:05 08/11/11 00:25 1.00 Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro-meta-xylene 82 19 - 147 08110111 12:05 08111111 00:25 1.00 Decachlorobiphenyl 166 Z2 20 - 150 08110111 12:05 08111111 00:25 1.00 Method: SW846 6010C - Total Metals by EPA 6010C Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 11.7 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 Arsenic 5.19 1.17 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 Beryllium ND 1.17 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 Cadmium ND 1.17 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 Chromium 20.5 1.17 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 Copper 13.8 2.34 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 Lead 13.4 1.17 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 Nickel 6.59 1.17 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 TestAmerica Nashville Page 13 of 38 08/11/2011 Client Sample Results Client: Hart & Hickman Project/Site: CRM-008 TestAmerica Job ID: NUH1259 Client Sample ID: BF-2 Lab Sample ID: NUH1259-02 Date Collected: 08/09/11 13:10 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.5 Method: SW846 6010C - Total Metals by EPA 6010C (Continued) Analyte Result Qualifier RL Selenium ND 2.34 Silver ND 1.17 Thallium ND 2.34 Zinc 52.4 11.7 Method: SW846 7471 B - Mercury by EPA Method 7471 B Analyte Result Qualifier RL Mercury ND 0.12 Method: SW-846 - General Chemistry Parameters Analyte Result Qualifier RL % Dry Solids 81.5 0.500 MDL Unit D Prepared Analyzed Dil Fac mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 mg/kg dry 08/10/11 12:00 08/10/11 21:10 1.00 F MDL Unit D Prepared Analyzed Dil Fac mg/kg dry 08/11/11 10:00 08/11/11 13:53 1.0 MDL Unit D Prepared Analyzed Dil Fac % 08/10/1114:32 08/11/1110:48 1.00 TestAmerica Nashville Page 14 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B Lab Sample ID: 11 H2752-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11H2752_13 Blank Blank Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acetone ND 0.0500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Benzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Bromobenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Bromochloromethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Bromodichloromethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Bromoform ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Bromomethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2-Dibromo-3-chloropropane ND 0.00500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 2-Butanone ND 0.0500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 sec -Butyl benzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 n-Butylbenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 tert-Butylbenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Carbon disulfide ND 0.00500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Carbon Tetrachloride ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Chlorobenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Chlorodibromomethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Chloroethane ND 0.00500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Chloroform ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Chloromethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 2-Chlorotoluene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 4-Chlorotoluene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2-Dibromoethane (EDB) ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Dibromomethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,4-Dichlorobenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,3-Dichlorobenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2-Dichlorobenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Dichlorodifluoromethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,1-Dichloroethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2-Dichloroethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 cis-1,2-Dichloroethene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,1-Dichloroethene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 trans-1,2-Dichloroethene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,3-Dichloropropane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2-Dichloropropane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 2,2-Dichloropropane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 cis-1,3-Dichloropropene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 trans-1,3-Dichloropropene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,1-Dichloropropene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Ethylbenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Hexachlorobutadiene ND 0.00500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 2-Hexanone ND 0.0500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Isopropylbenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 p-Isopropyltoluene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Methyl tert-Butyl Ether ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Methylene Chloride ND 0.0100 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 4-Methyl-2-pentanone ND 0.0500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Naphthalene ND 0.00500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 n-Propylbenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Styrene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 C 0 TestAmerica Nashville Page 15 of 38 08/11/2011 QC Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 L Project/Site: CRM-008 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Lab Sample ID: 11 H2752-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11 H2752_P Blank Blank Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane ND 0.00200 mg/kg wet 88/10/11 10:23 08/10/11 12:28 1.00 1,1,2,2-Tetrachloroethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Tetrachloroethene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Toluene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2,3-Trichlorobenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2,4-Trichlorobenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,1,2-Trichloroethane ND 0.00500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,1,1-Trichloroethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Trichloroethene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Trichlorofluoromethane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2,3-Trichloropropane ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,3,5-Trimethylbenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2,4-Trimethylbenzene ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Vinyl chloride ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Xylenes, total ND 0.00500 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Diisopropyl Ether ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 1,2-Dichloroethene (total) ND 0.00200 mg/kg wet 08/10/11 10:23 08/10/11 12:28 1.00 Blank Blank Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 96 67- 138 08110111 10:23 08110111 12:28 1.00 Dibromofluoromethane 85 75 - 125 08/10/11 10:23 08/10/11 12:28 1.00 Toluene-d8 104 76 - 129 08/10/11 10:23 08/10/11 12:28 1.00 4-Bromofluorobenzene 117 67 - 147 08110111 10:23 08110111 12:28 1.00 Lab Sample ID: 11 H2752-BSI Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: I I H2752_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D °/u Rec Limits Acetone 250 229 ug/kg 92 60 -150 Benzene 50.0 49.9 ug/kg 100 78 -126 Bromobenzene 50.0 58.5 ug/kg 117 79 -126 Bromochloromethane 50.0 42.8 ug/kg 86 78 - 126 Bromodichloromethane 50.0 45.4 ug/kg 91 75 - 129 Bromoform 50.0 41.9 ug/kg 84 74 -133 Bromomethane 50.0 38.5 ug/kg 77 50 -150 1,2-Dibromo-3-chloropropane 50.0 41.9 ug/kg 84 62 -150 2-Butanone 250 250 ug/kg 100 68 - 149 sec -Butyl benzene 50.0 56.2 ug/kg 112 76 - 135 n-Butylbenzene 50.0 61.4 ug/kg 123 73 -143 tert-Butylbenzene 50.0 52.8 ug/kg 106 80 -129 Carbon disulfide 50.0 48.1 ug/kg 96 80 -132 Carbon Tetrachloride 50.0 45.3 ug/kg 91 70 -138 Chlorobenzene 50.0 50.5 ug/kg 101 80 -123 Chlorodibromomethane 50.0 44.1 ug/kg 88 80 -127 Chloroethane 50.0 46.2 ug/kg 92 55 -150 Chloroform 50.0 45.4 ug/kg 91 70 -127 Chloromethane 50.0 53.5 ug/kg 107 36 -137 2-Chlorotoluene 50.0 56.1 ug/kg 112 80 - 130 TestAmerica Nashville Page 16 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Lab Sample ID: 11H2752-BSI Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11 H2752_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D °/, Rec Limits 4-Chlorotoluene 50.0 57.7 ug/kg 115 77 -132 1,2-Dibromoethane (EDB) 50.0 51.7 ug/kg 103 80 -131 Dibromomethane 50.0 45.2 ug/kg 90 78 -128 1,4-Dichlorobenzene 50.0 52.6 ug/kg 105 80 - 129 1,3-Dichlorobenzene 50.0 52.7 ug/kg 105 80 -131 1,2-Dichlorobenzene 50.0 54.3 ug/kg 109 80 -127 Dichlorodifluoromethane 50.0 55.0 ug/kg 110 30 -150 1,1-Dichloroethane 50.0 49.7 ug/kg 99 71-126 1,2-Dichloroethane 50.0 46.1 ug/kg 92 70 -139 cis-1,2-Dichloroethene 50.0 48.7 ug/kg 97 75 -126 1,1-Dichloroethene 50.0 44.3 ug/kg 89 70-125 trans-1,2-Dichloroethene 50.0 49.1 ug/kg 98 73 -128 1,3-Dichloropropane 50.0 53.6 ug/kg 107 79 -128 1,2-Dichloropropane 50.0 51.7 ug/kg 103 75 -120 2,2-Dichloropropane 50.0 50.7 ug/kg 101 60 -139 cis-1,3-Dichloropropene 50.0 50.3 ug/kg 101 74 -136 trans-1,3-Dichloropropene 50.0 48.9 ug/kg 98 73 -128 1,1-Dichloropropene 50.0 47.8 ug/kg 96 78-125 Ethylbenzene 50.0 53.9 ug/kg 108 79 -130 Hexachlorobutadiene 50.0 50.2 ug/kg 100 75 -150 2-Hexanone 250 315 ug/kg 126 65-150 Isopropylbenzene 50.0 53.4 ug/kg 107 65 -121 p-Isopropyltoluene 50.0 55.9 ug/kg 112 76 -133 Methyl tert-Butyl Ether 50.0 45.9 ug/kg 92 70 -128 Methylene Chloride 50.0 42.4 ug/kg 85 69 -140 4-Methyl-2-pentanone 250 306 ug/kg 123 67 -147 Naphthalene 50.0 53.4 ug/kg 107 72 -150 n-Propylbenzene 50.0 57.4 ug/kg 115 76 -133 Styrene 50.0 53.0 ug/kg 106 80 -140 1,1,1,2-Tetrachloroethane 50.0 48.7 ug/kg 97 80-132 1,1,2,2-Tetrachloroethane 50.0 59.0 ug/kg 118 75-135 Tetrachloroethene 50.0 46.7 ug/kg 93 76 -130 Toluene 50.0 53.0 ug/kg 106 76 -126 1,2,3-Trichlorobenzene 50.0 52.4 ug/kg 105 75 -150 1,2,4-Trichlorobenzene 50.0 52.4 ug/kg 105 64 -150 1,1,2-Trichloroethane 50.0 51.0 ug/kg 102 73-133 1,1,1-Trichloroethane 50.0 46.5 ug/kg 93 70-132 Trichloroethene 50.0 43.9 ug/kg 88 79 -129 Trichlorofluoromethane 50.0 40.2 ug/kg 80 52 -148 1,2,3-Trichloropropane 50.0 58.1 ug/kg 116 70 -125 1,3,5-Trimethylbenzene 50.0 55.5 ug/kg ill 80 -134 1,2,4-Trimethylbenzene 50.0 55.0 ug/kg 110 80 -132 Vinyl chloride 50.0 54.9 ug/kg 110 53 -142 Xylenes, total 150 165 ug/kg 110 80 -130 Diisopropyl Ether 50.0 52.6 ug/kg 105 71 -125 1,2-Dichloroethene (total) 100 97.8 ug/kg 98 74 - 126 LCS LCS Surrogate % Recovery Qualifier Limits 1,2-Dichloroethane-d4 96 67. 138 TestAmerica Nashville Page 17 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Lab Sample ID: 11H2752-BSI Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11 H2752_P LCS LCS Surrogate % Recovery Qualifier Limits Dibromofluoromethane 88 75 - 125 Toluene-d8 102 76 - 129 4-Bromofluorobenzene 107 67. 147 Lab Sample ID: 11H2752-MS1 Client Sample ID: Matrix Spike Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11 H2752_P Sample Sample Spike Matrix Spike Matrix Spike % Rec. Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits Acetone 0.0278 0.203 0.199 mg/kg wet 84 29 . 881 Benzene 0.00143 0.0405 0.0356 mg/kg wet 84 42.141 Bromobenzene ND 0.0405 0.0408 mg/kg wet 101 19.154 Bromochloromethane ND 0.0405 0.0298 mg/kg wet 73 41 _ 146 Bromodichloromethane ND 0.0405 0.0298 mg/kg wet 73 32. 155 Bromoform ND 0.0405 0.0265 mg/kg wet 65 10 -155 Bromomethane ND 0.0405 0.0269 mg/kg wet 66 10 -199 1,2-Dibromo-3-chloropropane ND 0.0405 0.0263 mg/kg wet 65 10 -167 2-Butanone 0.00556 0.203 0.186 mg/kg wet 89 38 -161 sec -Butyl benzene ND 0.0405 0.0395 mg/kg wet 97 10 -170 n-Butylbenzene ND 0.0405 0.0374 mg/kg wet 92 10 -183 tert-Butylbenzene ND 0.0405 0.0384 mg/kg wet 95 11 -165 Carbon disulfide ND 0.0405 0.0349 mg/kg wet 86 50.136 Carbon Tetrachloride ND 0.0405 0.0314 mg/kg wet 77 30.159 Chlorobenzene ND 0.0405 0.0347 mg/kg wet 86 25.151 Chlorodibromomethane ND 0.0405 0.0296 mg/kg wet 73 27.150 Chloroethane ND 0.0405 0.0340 mg/kg wet 84 15.197 Chloroform ND 0.0405 0.0325 mg/kg wet 80 33.148 Chloromethane ND 0.0405 0.0405 mg/kg wet 100 10 -166 2-Chlorotoluene ND 0.0405 0.0401 mg/kg wet 99 25 -166 4-Chlorotoluene ND 0.0405 0.0400 mg/kg wet 99 19.163 1,2-Dibromoethane (EDB) ND 0.0405 0.0355 mg/kg wet 88 30 -155 Dibromomethane ND 0.0405 0.0300 mg/kg wet 74 30 -149 1,4-Dichlorobenzene ND 0.0405 0.0330 mg/kg wet 82 10 -170 1,3-Dichlorobenzene ND 0.0405 0.0344 mg/kg wet 85 10 -173 1,2-Dichlorobenzene ND 0.0405 0.0344 mg/kg wet 85 10 -168 Dichlorodifluoromethane ND 0.0405 0.0304 mg/kg wet 75 10 -188 1,1-Dichloroethane ND 0.0405 0.0354 mg/kg wet 87 51 _135 1,2-Dichloroethane ND 0.0405 0.0318 mg/kg wet 78 32.155 cis-1,2-Dichloroethene ND 0.0405 0.0331 mg/kg wet 82 32.150 1,1-Dichloroethene ND 0.0405 0.0322 mg/kg wet 80 46.141 trans-1,2-Dichloroethene ND 0.0405 0.0339 mg/kg wet 84 41 _146 1,3-Dichloropropane ND 0.0405 0.0379 mg/kg wet 93 35. 148 1,2-Dichloropropane ND 0.0405 0.0363 mg/kg wet 90 34.139 2,2-Dichloropropane ND 0.0405 0.0349 mg/kg wet 86 29 -152 cis-1,3-Dichloropropene ND 0.0405 0.0340 mg/kg wet 84 23 -152 trans-1,3-Dichloropropene ND 0.0405 0.0308 mg/kg wet 76 24 -151 1,1-Dichloropropene ND 0.0405 0.0332 mg/kg wet 82 40 -151 Ethylbenzene 0.00213 0.0405 0.0379 mg/kg wet 88 21 -165 Hexachlorobutadiene ND 0.0405 0.0302 mg/kg wet 75 10 -173 TestAmerica Nashville Page 18 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Lab Sample ID: 11H2752-MS1 Client Sample ID: Matrix Spike Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11 H2752_P Sample Sample Spike Matrix Spike Matrix Spike % Rec. Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits 2-Hexanone ND 0.203 0.217 mg/kg wet 107 13 - 174 Isopropylbenzene ND 0.0405 0.0364 mg/kg wet 90 20 - 139 p-Isopropyltoluene ND 0.0405 0.0386 mg/kg wet 95 10 - 164 Methyl tert-Butyl Ether ND 0.0405 0.0316 mg/kg wet 78 34 - 154 Methylene Chloride ND 0.0405 0.0289 mg/kg wet 71 36 - 163 4-Methyl-2-pentanone ND 0.203 0.228 mg/kg wet 112 19. 176 Naphthalene ND 0.0405 0.0160 mg/kg wet 40 10 - 160 n-Propylbenzene 0.000763 0.0405 0.0421 mg/kg wet 102 16 - 174 Styrene ND 0.0405 0.0332 mg/kg wet 82 10 - 177 1,1,1,2-Tetrachloroethane ND 0.0405 0.0344 mg/kg wet 85 31 - 150 1,1,2,2-Tetrachloroethane ND 0.0405 0.0444 mg/kg wet 110 27- 163 Tetrachloroethene ND 0.0405 0.0347 mg/kg wet 86 33 - 155 Toluene 0.00542 0.0405 0.0387 mg/kg wet 82 45 - 145 1,2,3-Trichlorobenzene ND 0.0405 0.0220 mg/kg wet 54 10 - 182 1,2,4-Trichlorobenzene ND 0.0405 0.0217 mg/kg wet 53 10 - 175 1,1,2-Trichloroethane ND 0.0405 0.0376 mg/kg wet 93 43- 145 1, 1, 1 -Trichloroethane ND 0.0405 0.0334 mg/kg wet 82 39- 148 Trichloroethene ND 0.0405 0.0307 mg/kg wet 76 39 - 150 Trichlorofluoromethane ND 0.0405 0.0303 mg/kg wet 75 25 - 174 1,2,3-Trichloropropane ND 0.0405 0.0420 mg/kg wet 104 10 - 152 1,3,5-Trimethyl benzene 0.000709 0.0405 0.0394 mg/kg wet 95 38 - 148 1,2,4-Trimethyl benzene 0.00251 0.0405 0.0386 mg/kg wet 89 22 _ 164 Vinyl chloride ND 0.0405 0.0409 mg/kg wet 101 32 _ 163 Xylenes, total 0.00459 0.122 0.114 mg/kg wet 90 31 - 159 Diisopropyl Ether ND 0.0405 0.0376 mg/kg wet 93 44 - 141 1,2-Dichloroethene (total) ND 0.0810 0.0670 mg/kg wet 83 38 - 147 Matrix Spike Matrix Spike Surrogate % Recovery Qualifier Limits 1,2-Dichloroethane-d4 94 67- 138 Dibromofluoromethane 86 75 - 125 Toluene-d8 106 76 - 129 4-Bromofluorobenzene 111 67 - 147 Lab Sample ID: 11H2752-MSD1 Client Sample ID: Matrix Spike Duplicate Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11 H2752_P Sample Sample Spike Oatrix Spike Dup Matrix Spike Dut % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Acetone 0.6278 0.205 0.209 mg/kg wet 89 29 - 181 5 50 Benzene 0.00143 0.0409 0.0387 mg/kg wet 91 42. 141 8 50 Bromobenzene ND 0.0409 0.0342 mg/kg wet 84 19. 154 18 50 Bromochloromethane ND 0.0409 0.0307 mg/kg wet 75 41 - 146 3 50 Bromodichloromethane ND 0.0409 0.0314 mg/kg wet 77 32 - 155 5 50 Bromoform ND 0.0409 0.0234 mg/kg wet 57 10 - 155 12 43 Bromomethane ND 0.0409 0.0301 mg/kg wet 73 10 - 199 11 46 1,2-Dibromo-3-chloropropane ND 0.0409 0.0258 mg/kg wet 63 10 - 167 2 45 2-Butanone 0.00556 0.205 0.202 mg/kg wet 96 38 - 161 8 50 sec-Butylbenzene ND 0.0409 0.0335 mg/kg wet 82 10 - 170 16 50 n-Butylbenzene ND 0.0409 0.0324 mg/kg wet 79 10 - 183 14 50 0 TestAmerica Nashville Page 19 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Lab Sample ID: 11 H2752-MSD1 Client Sample ID: Matrix Spike Duplicate Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11H2752_P Sample Sample Spike Oatrix Spike Dup Matrix Spike Dul % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %u Rec Limits RPD Limit tert-Butylbenzene ND 0.0409 0.0310 mg/kg wet 76 11 -165 21 50 Carbon disulfide ND 0.0409 0.0371 mg/kg wet 91 50 -136 6 48 Carbon Tetrachloride ND 0.0409 0.0339 mg/kg wet 83 30 -159 8 44 Chlorobenzene ND 0.0409 0.0319 mg/kg wet 78 25 -151 8 50 Chlorodibromomethane ND 0.0409 0.0263 mg/kg wet 64 27 -150 12 48 Chloroethane ND 0.0409 0.0367 mg/kg wet 90 15 -197 8 50 Chloroform ND 0.0409 0.0345 mg/kg wet 84 33 -148 6 50 Chloromethane ND 0.0409 0.0451 mg/kg wet 110 10 -166 11 44 2-Chlorotoluene ND 0.0409 0.0335 mg/kg wet 82 25 -166 18 50 4-Chlorotoluene ND 0.0409 0.0343 mg/kg wet 84 19 -163 15 50 1,2-Dibromoethane (EDB) ND 0.0409 0.0317 mg/kg wet 77 30 -155 11 45 Dibromomethane ND 0.0409 0.0313 mg/kg wet 77 30 -149 4 50 1,4-Dichlorobenzene ND 0.0409 0.0286 mg/kg wet 70 10 -170 14 50 1,3-Dichlorobenzene ND 0.0409 0.0293 mg/kg wet 72 10 - 173 16 50 1,2-Dichlorobenzene ND 0.0409 0.0289 mg/kg wet 71 10 - 168 17 50 Dichlorodifluoromethane ND 0.0409 0.0495 mg/kg wet 121 10 -188 48 50 1,1-Dichloroethane ND 0.0409 0.0387 mg/kg wet 95 51 - 135 9 50 1,2-Dichloroethane ND 0.0409 0.0336 mg/kg wet 82 32 - 155 6 50 cis-1,2-Dichloroethene ND 0.0409 0.0363 mg/kg wet 89 32 - 150 9 50 1,1-Dichloroethene ND 0.0409 0.0355 mg/kg wet 87 46 -141 10 50 trans-1,2-Dichloroethene ND 0.0409 0.0372 mg/kg wet 91 41 -146 9 40 1,3-Dichloropropane ND 0.0409 0.0343 mg/kg wet 84 35 -148 10 42 1,2-Dichloropropane ND 0.0409 0.0388 mg/kg wet 95 34 -139 6 50 2,2-Dichloropropane ND 0.0409 0.0389 mg/kg wet 95 29 -152 11 39 cis-1,3-Dichloropropene ND 0.0409 0.0305 mg/kg wet 74 23 -152 11 50 trans-1,3-Dichloropropene ND 0.0409 0.0274 mg/kg wet 67 24 -151 12 48 1,1-Dichloropropene ND 0.0409 0.0369 mg/kg wet 90 40 -151 10 50 Ethylbenzene 0.00213 0.0409 0.0352 mg/kg wet 81 21 -165 7 50 Hexachlorobutadiene ND 0.0409 0.0245 mg/kg wet 60 10 - 173 21 50 2-Hexanone ND 0.205 0.207 mg/kg wet 101 13 - 174 5 50 Isopropylbenzene ND 0.0409 0.0336 mg/kg wet 82 20 -139 8 50 p-Isopropyltoluene ND 0.0409 0.0329 mg/kg wet 80 10 -164 16 50 Methyl tert-Butyl Ether ND 0.0409 0.0345 mg/kg wet 84 34 - 154 9 50 Methylene Chloride ND 0.0409 0.0314 mg/kg wet 77 36 -163 8 50 4-Methyl-2-pentanone ND 0.205 0.211 mg/kg wet 103 19 -176 8 45 Naphthalene ND 0.0409 0.0185 mg/kg wet 45 10 -160 15 50 n-Propylbenzene 0.000763 0.0409 0.0358 mg/kg wet 86 16 -174 16 50 Styrene ND 0.0409 0.0317 mg/kg wet 78 10 -177 4 50 1,1,1,2-Tetrachloroethane ND 0.0409 0.0306 mg/kg wet 75 31 -150 12 50 1,1,2,2-Tetrachloroethane ND 0.0409 0.0357 mg/kg wet 87 27-163 22 45 Tetrachloroethene ND 0.0409 0.0315 mg/kg wet 77 33 -155 10 50 Toluene 0.00542 0.0409 0.0363 mg/kg wet 76 45 -145 6 50 1,2,3-Trichlorobenzene ND 0.0409 0.0191 mg/kg wet 47 10 -182 14 50 1,2,4-Trichlorobenzene ND 0.0409 0.0195 mg/kg wet 48 10 - 175 11 50 1,1,2-Trichloroethane ND 0.0409 0.0334 mg/kg wet 82 43-145 12 50 1,1, 1 -Trichloroethane, ND 0.0409 0.0362 mg/kg wet 88 39-148 8 41 Trichloroethene ND 0.0409 0.0330 mg/kg wet 81 39 -150 7 50 Trichlorofluoromethane ND 0.0409 0.0331 mg/kg wet 81 25 - 174 9 47 1,2,3-Trichloropropane ND 0.0409 0.0344 mg/kg wet 84 10 - 152 20 47 1,3,5-Trimethylbenzene 0.000709 0.0409 0.0337 mg/kg wet 81 38 -148 16 50 0 TestAmerica Nashville Page 20 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8260B - Volatile Organic Compounds by EPA Method 8260B (Continued) Lab Sample ID: 11 H2752-MSD1 Client Sample ID: Matrix Spike Duplicate Matrix: Soil Prep Type: Total Analysis Batch: U014254 Prep Batch: 11H2752_P Sample Sample Spike Oatrix Spike Dup Matrix Spike Dul % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit 1,2,4-Trimethylbenzene 0.00251 0.0409 0.0336 mg/kg wet 76 22 - 164 14 50 Vinyl chloride ND 0.0409 0.0456 mg/kg wet ill 32 - 163 11 39 Xylenes, total 0.00459 0.123 0.106 mg/kg wet 83 31 -159 7 50 Diisopropyl Ether ND 0.0409 0.0400 mg/kg wet 98 44 - 141 6 50 1,2-Dichloroethene (total) ND 0.0818 0.0735 mg/kg wet 90 38 - 147 9 41 Matrix Spike Dup Matrix Spike Dup Surrogate % Recovery Qualifier Limits 1,2-Dichloroethane-d4 108 67-138 Dibromofluoromethane 97 75 - 125 Toluene-d8 103 76 - 129 4-Bromofluorobenzene 99 67 - 147 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D Lab Sample ID: 11 H2345-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: 11 H2345 Prep Batch: 11 H2345_P Blank Blank Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0.0670 mg/kg wet 08/l0/ 11 11.30 08/11/11 13:56 1.00 Acenaphthylene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Anthracene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Benzo (a) anthracene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Benzo (a) pyrene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Benzo (b) fluoranthene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Benzo (g,h,i) perylene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Benzo (k) fluoranthene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 4-Bromophenyl phenyl ether ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Butyl benzyl phthalate ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Carbazole ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 4-Chloro-3-methylphenol ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 4-Chloroaniline ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Bis(2-chloroethoxy)methane ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Bis(2-chloroethyl)ether ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Bis(2-chloroisopropyl)ether ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 2-Chloronaphthalene ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 2-Chlorophenol ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 4-Chlorophenyl phenyl ether ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Chrysene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Dibenz (a,h) anthracene ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Dibenzofuran ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Di-n-butyl phthalate ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 1,4-Dichlorobenzene ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 1,2-Dichlorobenzene ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 1,3-Dichlorobenzene ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 3,3-Dichlorobenzidine ND 0.667 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 2,4-Dichlorophenol ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Diethyl phthalate ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 2,4-Di methyl phenol ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 0 TestAmerica Nashville Page 21 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D (Continued) Lab Sample ID: 11 H2345-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: 11 H2345 Prep Batch: 11 H2345_P Analyte Dimethyl phthalate 4,6-Di n itro-2-methylphenol 2,4-Dinitrophenol 2,6-Dinitrotoluene 2,4-Dinitrotoluene Di-n-octyl phthalate Bis(2-ethyl hexyl )phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexach lorocyclopentadiene Hexachloroethane Indeno (1,2,3-cd) pyrene Isophorone 2-Methyl naphthalene 2-Methylphenol 3/4-Methylphenol Naphthalene 3-Nitroaniline 2-Nitroaniline 4-Nitroaniline Nitrobenzene 4-Nitrophenol 2-Nitrophenol N-N itrosodi phenylami ne N-N itrosodi-n-propylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine 1,2,4-Trichlorobenzene 1-Methyl naphthalene 2,4, 6-Trichlorophenol 2,4, 5-Trichlorophenol Surrogate Terphenyl-d14 2, 4, 6-Tribromophenol Phenol-d5 2-Fluorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Blank Blank Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1_ ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.667 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.0670 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.333 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 ND 0.833 mg/kg wet 08/10/11 11:30 08/11/11 13:56 1.00 Blank Blank Recovery Qualifier Limits Prepared Analyzed Dil Fac 95 18 - 120 08110111 11:30 08111111 13:56 1.00 70 19 - 120 08110111 11:30 08111111 13:56 1.00 77 18 - 120 08110111 11:30 08111111 13:56 1.00 76 14 - 120 08110111 11:30 08111111 13:56 1.00 77 17 - 120 08110111 11:30 08111111 13:56 1.00 75 17 - 120 08110111 11:30 08111111 13:56 1.00 TestAmerica Nashville Page 22 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D (Continued) Lab Sample ID: 11H2345-BS1 Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: 11 H2345 Prep Batch: 11 H2345_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D % Rec Limits Acenaphthene 1.67 1.33 MNR mg/kg wet 80 49. 120 Acenaphthylene 1.67 1.31 MNR mg/kg wet 79 52 _ 120 Anthracene 1.67 1.36 MNR mg/kg wet 81 58 - 120 Benzo (a) anthracene 1.67 1.38 MNR mg/kg wet 83 57 - 120 Benzo (a) pyrene 1.67 1.47 MNR mg/kg wet 88 55 - 120 Benzo (b) fluoranthene 1.67 1.50 MNR mg/kg wet 90 51 - 123 Benzo (g,h,i) perylene 1.67 1.34 MNR mg/kg wet 81 49 - 121 Benzo (k) fluoranthene 1.67 1.27 MNR mg/kg wet 76 42 - 129 4-Bromophenyl phenyl ether 1.67 1.33 MNR mg/kg wet 80 49 - 120 Butyl benzyl phthalate 1.67 1.46 MNR mg/kg wet 87 59 - 124 Carbazole 1.67 1.35 MNR mg/kg wet 81 54 - 120 4-Chloro-3-methyl phenol 1.67 1.24 MNR mg/kg wet 75 49 - 120 4-Chloroaniline 1.67 1.37 MNR mg/kg wet 82 41 - 120 Bis(2-chloroethoxy)methane 1.67 1.14 MNR mg/kg wet 68 37 - 120 Bis(2-chloroethyl)ether 1.67 1.32 MNR mg/kg wet 79 29 - 120 Bis(2-chloroisopropyl)ether 1.67 1.34 MNR mg/kg wet 81 28. 120 2-Chloronaphthalene 1.67 1.06 MNR mg/kg wet 64 45 - 120 2-Chlorophenol 1.67 1.47 MNR mg/kg wet 88 42 _ 120 4-Chlorophenyl phenyl ether 1.67 1.27 MNR mg/kg wet 76 52 - 120 Chrysene 1.67 1.33 MNR mg/kg wet 80 55 - 120 Dibenz (a,h) anthracene 1.67 1.37 MNR mg/kg wet 82 50 - 123 Dibenzofuran 1.67 1.36 MNR mg/kg wet 81 54 - 120 Di-n-butyl phthalate 1.67 1.26 MNR mg/kg wet 75 58 - 120 1,4-Dichlorobenzene 1.67 1.17 MNR mg/kg wet 70 15 - 120 1,2-Dichlorobenzene 1.67 1.24 MNR mg/kg wet 74 17 - 120 1,3-Dichlorobenzene 1.67 1.22 MNR mg/kg wet 73 13 - 120 3,3-Dichlorobenzidine 1.67 1.36 MNR mg/kg wet 82 54 - 120 2,4-Dichlorophenol 1.67 1.23 MNR mg/kg wet 74 43 - 120 Diethyl phthalate 1.67 1.26 MNR mg/kg wet 76 52 - 120 2,4-Dimethylphenol 1.67 1.26 MNR mg/kg wet 76 47 - 120 Dimethyl phthalate 1.67 1.30 MNR mg/kg wet 78 55 - 120 4,6-Dinitro-2-methyl phenol 1.67 1.53 MNR mg/kg wet 92 27. 134 2,4-Dinitrophenol 1.67 1.53 MNR mg/kg wet 92 15 - 145 2,6-Dinitrotoluene 1.67 1.26 MNR mg/kg wet 76 56 - 120 2,4-Dinitrotoluene 1.67 1.26 MNR mg/kg wet 76 55 - 122 Di-n-octyl phthalate 1.67 1.40 MNR mg/kg wet 84 48 - 131 Bis(2-ethylhexyl)phthaIate 1.67 1.36 MNR mg/kg wet 81 51 - 127 Fluoranthene 1.67 1.39 MNR mg/kg wet 83 58 - 120 Fluorene 1.67 1.39 MNR mg/kg wet 84 54 - 120 Hexachlorobenzene 1.67 1.24 MNR mg/kg wet 74 56 - 120 Hexachlorobutadiene 1.67 1.25 MNR mg/kg wet 75 19 - 120 Hexachlorocyclopentadiene 1.67 1.07 MNR mg/kg wet 64 11 - 120 Hexachloroethane 1.67 1.40 MNR mg/kg wet 84 14 - 120 Indeno (1,2,3-cd) pyrene 1.67 1.33 MNR mg/kg wet 80 50 - 122 Isophorone 1.67 1.09 MNR mg/kg wet 65 43 - 120 2-Methyl naphthalene 1.67 1.22 MNR mg/kg wet 73 36 - 120 2-Methylphenol 1.67 1.26 MNR mg/kg wet 76 47 - 120 3/4-Methyl phenol 1.67 1.22 MNR mg/kg wet 73 53 - 135 Naphthalene 1.67 1.28 MNR mg/kg wet 77 28 - 120 0 TestAmerica Nashville Page 23 of 38 08/11/2011 QC Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8270D - Semivolatile Organic Compounds by EPA Method 8270D (Continued) Lab Sample ID: 11H2345-BSI Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: 11 H2345 Prep Batch: 11 H2345_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D °/, Rec Limits 3-Nitroaniline 1.67 1.40 MNR mg/kg wet 84 54 -120 2-Nitroaniline 1.67 1.32 MNR mg/kg wet 79 59 -120 4-Nitroaniline 1.67 1.44 MNR mg/kg wet 86 55 - 121 Nitrobenzene 1.67 0.908 MNR mg/kg wet 54 30 - 120 4-Nitrophenol 1.67 1.33 MNR mg/kg wet 80 44 - 133 2-Nitrophenol 1.67 1.21 MNR mg/kg wet 73 36 -120 N-Nitrosodiphenylamine 1.67 1.46 MNR mg/kg wet 87 56 -120 N-Nitrosodi-n-propylamine 1.67 1.33 MNR mg/kg wet 80 45 -120 Pentachlorophenol 1.67 1.46 MNR mg/kg wet 88 42 -135 Phenanthrene 1.67 1.36 MNR mg/kg wet 82 56 -120 Phenol 1.67 1.36 MNR mg/kg wet 81 45 -120 Pyrene 1.67 1.39 MNR mg/kg wet 83 56 -120 Pyridine 1.67 0.926 MNR mg/kg wet 56 26 -120 1,2,4-Trichlorobenzene 1.67 1.10 MNR mg/kg wet 66 22 -120 1-Methyl naphthalene 1.67 1.02 MNR mg/kg wet 61 36 -120 2,4,6-Trichlorophenol 1.67 1.23 MNR mg/kg wet 74 50 - 120 2,4,5-Trichlorophenol 1.67 1.15 MNR mg/kg wet 69 54 -120 LCS LCS Surrogate % Recovery Qualifier Limits Terphenyl-d14 82 18- 120 Z4,6-Tribromophenol 62 19 - 120 Phenol-d5 69 18 - 120 2-Fluorobiphenyl 63 14 - 120 2-Fluorophenol 74 17 - 120 Nitrobenzene-d5 59 17 - 120 Method: SW846 8081 B - Organochlorine Pesticides by EPA Method 8081 B Lab Sample ID: 11H2333-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: U014169 Prep Batch: 11 H2333_P Blank Blank Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Aldrin ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 delta-BHC ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 alpha-BHC ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 beta-BHC ND 0.00330 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 gamma-BHC (Lindane) ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 alpha -Chlordane ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 gamma -Chlordane ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Chlordane ND 0.0667 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 4,4'-DDD ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 4,4'-DDE ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 4,4'-DDT ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Dieldrin ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Endosulfan I ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Endosulfan 11 ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Endosulfan sulfate ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Endrin ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 TestAmerica Nashville Page 24 of 38 08/11/2011 QC Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8081 B - Organochlorine Pesticides by EPA Method 8081 B (Continued) Lab Sample ID: 11H2333-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: U014169 Prep Batch: 11 H2333_P Blank Blank Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Endrin aldehyde ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Endrin ketone ND 0.00170 mg/kg wet 08/10/11 11:14 • 08/10/11 18:32 1.00 Heptachlor ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Heptachlor epoxide ND 0.00170 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Methoxychlor ND 0.00330 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Toxaphene ND 0.0667 mg/kg wet 08/10/11 11:14 08/10/11 18:32 1.00 Blank Blank Surrogate % Recovery Qualifier Limits Prepared Analyzed Dil Fac Tetrachloro-meta-xylene 110 22 - 150 08110111 11:14 08110111 18:32 1.00 Decachlorobiphenyl 120 25 - 150 08110111 11:14 08110111 18:32 1.00 Lab Sample ID: 11 H2333-BS1 Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: U014169 Prep Batch: 11 H2333_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D % Rec Limits Aldrin 0.0167 0.0153 mg/kg wet 92 43 - 150 delta-BHC 0.0167 0.0147 mg/kg wet 88 34 - 147 alpha-BHC 0.0167 0.0157 mg/kg wet 94 47 - 142 beta-BHC 0.0167 0.0160 mg/kg wet 96 52 - 148 gamma-BHC (Lindane) 0.0167 0.0157 mg/kg wet 94 53 - 142 alpha -Chlordane 0.0167 0.0160 mg/kg wet 96 50 - 148 gamma -Chlordane 0.0167 0.0160 mg/kg wet 96 46 - 150 4,4'-DDD 0.0167 0.0163 mg/kg wet 98 47 - 150 4,4'-DDE 0.0167 0.0160 mg/kg wet 96 42 - 150 4,4'-DDT 0.0167 0.0167 mg/kg wet 100 38 - 150 Dieldrin 0.0167 0.0160 mg/kg wet 96 53 - 142 Endosulfan 1 0.0167 0.0163 mg/kg wet 98 50 - 143 Endosulfan 11 0.0167 0.0160 mg/kg wet 96 51 - 150 Endosulfan sulfate 0.0167 0.0160 mg/kg wet 96 49 - 143 Endrin 0.0167 0.0170 mg/kg wet 102 49 - 150 Endrin aldehyde 0.0167 0.0160 mg/kg wet 96 40 - 150 Endrin ketone 0.0167 0.0173 mg/kg wet 104 55 - 139 Heptachlor 0.0167 0.0157 mg/kg wet 94 49 - 149 Heptachlor epoxide 0.0167 0.0157 mg/kg wet 94 53 - 150 Methoxychlor 0.0167 0.0173 mg/kg wet 104 43 - 144 LCS LCS Surrogate % Recovery Qualifier Limits Tetrachloro-meta-xylene 98 22 - 150 Decachlorobiphenyl 116 25 - 150 Lab Sample ID: 11H2333-BS2 Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: U014169 Prep Batch: 11 H2333_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D % Rec Limits Chlordane 0.167 0.161 mg/kg wet 97 59 - 150 Toxaphene 0.333 0.366 mg/kg wet 110 18 - 150 TestAmerica Nashville Page 25 of 38 08/11/2011 QC Sample Results Client: Hart & Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8081 B - Organochlorine Pesticides by EPA Method 8081 B (Continued) Lab Sample ID: 11H2333-BS2 Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: U014169 Prep Batch: 11 H2333_P LCS LCS Surrogate % Recovery Qualifier Limits Tetrachloro-meta-xylene 94 22 - 150 Decachlorobiphenyl 118 25 - 150 -ab Sample ID: 11 H2333-MS1 Client Sample ID: BF-1 Matrix: Soil Prep Type: Total 4nalysis Batch: U014169 Prep Batch: 11 H2333_P Sample Sample Spike Matrix Spike Matrix Spike % Rec. knalyte Result Qualifier Added Result Qualifier Unit D % Rec Limits aldrin ND 0.0205 0.0168 mg/kg dry 82 34. 550 ielta-BHC ND 0.0205 0.0160 mg/kg dry 78 15. 147 alpha-BHC ND 0.0205 0.0172 mg/kg dry 84 35. 143 )eta-BHC ND 0.0205 0.0176 mg/kg dry 86 21 _ 175 iamma-BHC (Lindane) ND 0.0205 0.0176 mg/kg dry 86 36. 147 alpha -Chlordane ND 0.0205 0.0172 mg/kg dry 84 36. 148 Gamma -Chlordane ND 0.0205 0.0168 mg/kg dry 82 31 _ 150 1,4'-DDD ND 0.0205 0.0180 mg/kg dry 88 27. 166 1,4'-DDE ND 0.0205 0.0172 mg/kg dry 84 32 _ 150 1,4'-DDT ND 0.0205 0.0176 mg/kg dry 86 36. 150 )ieldrin ND 0.0205 0.0172 mg/kg dry 84 26. 157 ndosulfan I ND 0.0205 0.0176 mg/kg dry 86 28 - 151 ndosulfan II ND 0.0205 0.0176 mg/kg dry 86 28 - 166 ndosulfan sulfate ND 0.0205 0.0172 mg/kg dry 84 34 - 149 =ndrin ND 0.0205 0.0184 mg/kg dry 90 24 - 173 =ndrin aldehyde ND 0.0205 0.0172 mg/kg dry 84 26. 166 =ndrin ketone ND 0.0205 0.0188 mg/kg dry 92 44. 152 ieptachlor ND 0.0205 0.0176 mg/kg dry 86 33. 160 ieptachlor epoxide ND 0.0205 0.0172 mg/kg dry 84 38. 150 dethoxychlor ND 0.0205 0.0188 mg/kg dry 92 10. 175 Matrix Spike Matrix Spike surrogate % Recovery Qualifier Limits retrachloro-meta-xylene 92 22. 150 )ecachlorobiphenyl 102 25 - 150 -ab Sample ID: 11H2333-MSD1 Client Sample ID: BF-1 Matrix: Soil Prep Type: Total 4nalysis Batch: U014169 Prep Batch: 11 H2333_P Sample Sample Spike Matrix Spike Dup Matrix Spike Du{ % Rec. RPD knalyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit aldrin ND 0.0204 0.0167 mg/kg dry 82 34. 150 0.3 36 lelta-BHC ND 0.0204 0.0159 mg/kg dry 78 15. 147 0.3 40 alpha-BHC ND 0.0204 0.0167 mg/kg dry 82 35. 143 3 38 )eta-BHC ND 0.0204 0.0171 mg/kg dry 84 21 _ 175 3 50 iamma-BHC (Lindane) ND 0.0204 0.0171 mg/kg dry 84 36. 147 3 39 alpha -Chlordane ND 0.0204 0.0171 mg/kg dry 84 36. 148 0.3 37 iamma-Chlordane ND 0.0204 0.0171 mg/kg dry 84 31 _ 150 2 39 1,4'-DDD ND 0.0204 0.0175 mg/kg dry 86 27. 166 3 43 1,4'-DDE ND 0.0204 0.0171 mg/kg dry 84 32 _ 150 0.3 37 1,4'-DDT ND 0.0204 0.0175 mg/kg dry 86 36. 150 0.3 45 )ieldrin ND 0.0204 0.0171 mg/kg dry 84 26. 157 0.3 39 TestAmerica Nashville Page 26 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8081 B - Organochlorine Pesticides by EPA Method 8081 B (Continued) Lab Sample ID: 11H2333-MSD1 Client Sample ID: BF-1 Matrix: Soil Prep Type: Total Analysis Batch: U014169 Prep Batch: 11 H2333_P Sample Sample Spike Matrix Spike Dup Matrix Spike Dul % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Endosulfan I ND 0.0204 0.0175 mg/kg dry 3:� 86 28 - 151 0.3 39 Endosulfan 11 ND 0.0204 0.0171 mg/kg dry 84 28 - 166 3 44 Endosulfan sulfate ND 0.0204 0.0171 mg/kg dry 84 34 - 149 0.3 40 Endrin ND 0.0204 0.0183 mg/kg dry 90 24 - 173 0.3 48 Endrin aldehyde ND 0.0204 0.0171 mg/kg dry 84 26 - 166 0.3 46 Endrin ketone ND 0.0204 0.0188 mg/kg dry 92 44 - 152 0.3 44 Heptachlor ND 0.0204 0.0171 mg/kg dry 84 33 - 160 3 38 Heptachlor epoxide ND 0.0204 0.0171 mg/kg dry 84 38 - 150 0.3 34 Methoxychlor ND 0.0204 0.0183 mg/kg dry 90 10 - 175 3 50 Matrix Spike Dup, Matrix Spike Dup Surrogate % Recovery Qualifier Limits Tetrachloro-meta-xylene 88 22 - 150 Decachlorobiphenyl 98 25 - 150 Method: SW846 8082A - Po Lab Sample ID: 11 H2343-BLK1 Matrix: Soil Analysis Batch: U014151 Analyte PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260 Surrogate Tetrachl oro-meta-xylene Decachlorobiphenyl Lab Sample ID: 11 H2343-BS1 Matrix: Soil Analysis Batch: U014151 Analyte PCB-1016 PCB-1260 lorinated Biph Blank Blank Result Qualifier ND ND ND ND ND ND ND Blank Blank % Recovery Qualifier 84 124 EPA Method 8082A Client Sample ID: Method Blank Prep Type: Total Prep Batch: 11 H2343_P RL MDL Unit D Prepared Analyzed Dil Fac 0.0333 mg/kg wet 08/10/11 12:05 08/10/11 22:15 1.00 0.0333 mg/kg wet 08/10/11 12:05 08/10/11 22:15 1.00 0.0333 mg/kg wet 08/10/11 12:05 08/10/11 22:15 1.00 0.0333 mg/kg wet 08/10/11 12:05 08/10/11 22:15 1.00 0.0333 mg/kg wet 08/10/11 12:05 08/10/11 22:15 1.00 0.0333 mg/kg wet 08/10/11 12:05 08/10/11 22:15 1.00 0.0333 mg/kg wet 08/10/11 12:05 08/10/11 22:15 1.00 Limits 19-147 20-150 Prepared Analyzed Dil Fac 0811011112:05 0811011122:15 1.00 0811011112:05 0811011122:15 1.00 Client Sample ID: Lab Control Sample Prep Type: Total Prep Batch: 11 H2343_P Spike LCS LCS % Rec. Added Result Qualifier Unit D % Rec Limits 0.167 0.159 mg/kg wet 96 64 - 122 0.167 0.163 mg/kg wet 98 56 - 150 LCS LCS Surrogate % Recovery Qualifier Limits Tetrachloro-meta-xylene 92 19 - 147 Decachlorobiphenyl 124 20 - 150 u Page 27 of 38 TestAmerica Nashville 08/11 /2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 8082A - Polychlorinated Biphenyls by EPA Method 8082A (Continued) Lab Sample ID: 11 H2343-MS1 Client Sample ID: BF-2 Matrix: Soil Prep Type: Total Analysis Batch: U014151 Prep Batch: 11 H2343_P Sample Sample Spike Matrix Spike Matrix Spike °% Rec. Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits PCB-1016 ND 0.212 0.197 mg/kg dry 93 20 - 175 PCB-1260 ND 0.212 0.206 mg/kg dry 97 51 _ 159 Matrix Spike Matrix Spike Surrogate % Recovery Qualifier Limits Tetrachloro-meta-xylene 80 19 - 147 Decachlorobiphenyl 110 20 - 150 Lab Sample ID: 11 H2343-MSD1 Client Sample ID: BF-2 Matrix: Soil Prep Type: Total Analysis Batch: U014151 Prep Batch: 11 H2343_P Sample Sample Spike Matrix Spike Dup Matrix Spike Dul % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit PCB-1016 ND 0.200 0.181 mg/kg dry 91 20 - 175 8 50 PCB-1260 ND 0.200 0.213 mg/kg dry 106 51 - 159 3 36 Matrix Spike Dup Matrix Spike Dup Surrogate % Recovery Qualifier Limits Tetrachloro-meta-xylene 82 19 - 147 Decachlorobiphenyl 128 20 - 150 Method: SW846 6010C - Total Metals by EPA 6010C Lab Sample ID: 11 H2347-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: 11 H2347 Prep Batch: 11 H2347_P Blank Blank Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony ND 10.1 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Arsenic ND 1.01 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Beryllium ND 1.01 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Cadmium ND 1.01 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Chromium ND 1.01 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Copper ND 2.02 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Lead ND 1.01 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Nickel ND 1.01 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Selenium ND 2.02 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Silver ND 1.01 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Thallium ND 2.02 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Zinc ND 10.1 mg/kg wet 08/10/11 12:00 08/10/11 20:18 1.00 Lab Sample ID: 11 H2347-BS1 Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: 11 H2347 Prep Batch: 11 H2347_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D % Rec Limits Antimony 38.1 38.5 mg/kg wet 101 80 - 120 Arsenic 19.0 18.5 mg/kg wet 97 80 - 120 Beryllium 19.0 18.3 mg/kg wet 96 80 - 120 Cadmium 19.0 18.6 mg/kg wet 98 80 - 120 Chromium 76.2 74.1 mg/kg wet 97 80 - 120 0 TestAmerica Nashville Page 28 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 6010C - Total Metals by EPA 6010C (Continued) Lab Sample ID: 11H2347-BS1 Matrix: Soil Analysis Batch: 11 H2347 Spike LCS Analyte Added Result LCS Qualifier Client Sample ID: Lab Control Sample Prep Type: Total Prep Batch: 11 H2347_P % Rec. Unit D % Rec Limits Copper 95.2 90.7 mg/kg wet 95 80 - 120 Lead 19.0 19.1 mg/kg wet 100 80 - 120 Nickel 190 192 mg/kg wet 101 80 - 120 Selenium 19.0 18.6 mg/kg wet 98 80 - 120 Silver 19.0 18.6 mg/kg wet 98 75 - 125 Thallium 19.0 19.1 mg/kg wet 100 80 - 120 Zinc 190 179 mg/kg wet 94 80 - 120 Lab Sample ID: 11 H2347-BSD1 Client Sample ID: Lab Control Sample Dup Matrix: Soil Prep Type: Total Analysis Batch: 11 H2347 Prep Batch: 11 H2347_P Spike LCS Dup LCS Dup % Rec. RPD Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit Antimony 39.9 40.4 mg/kg wet 101 80 - 120 5 20 Arsenic 20.0 19.1 mg/kg wet 96 80 - 120 3 20 Beryllium 20.0 19.2 mg/kg wet 96 80 - 120 5 20 Cadmium 20.0 19.4 mg/kg wet 97 80 - 120 4 20 Chromium 79.8 77.6 mg/kg wet 97 80 - 120 5 20 Copper 99.8 95.1 mg/kg wet 95 80 - 120 5 20 Lead 20.0 20.1 mg/kg wet 101 80 - 120 5 20 Nickel 200 201 mg/kg wet 101 80 - 120 5 20 Selenium 20.0 19.9 mg/kg wet 100 80 - 120 6 20 Silver 20.0 19.4 mg/kg wet 97 75 - 125 4 20 Thallium 20.0 20.0 mg/kg wet 100 80 - 120 5 20 Zinc 200 187 mg/kg wet 94 80 - 120 4 20 Lab Sample ID: 11 H2347-MS1 Matrix: Soil Analysis Batch: 11 H2347 Analyte Sample Sample Result Qualifier Spike Added Matrix Spike Result Matrix Spike Qualifier Unit D Client Sample ID: Matrix Spike Prep Type: Total Prep Batch: 11 H2347_P % Rec. % Rec Limits Antimony 0.915 41.1 37.3 mg/kg dry 88 75 - 125 Arsenic 0.855 20.6 22.5 mg/kg dry 105 75 - 125 Beryllium 0.139 20.6 19.2 mg/kg dry 93 75 - 125 Cadmium ND 20.6 17.6 mg/kg dry 86 75 - 125 Chromium 5.91 82.3 104 mg/kg dry 120 75 - 125 Copper 5.01 103 135 M7 mg/kg dry 126 75 - 125 Lead 10.8 20.6 40.4 M7 mg/kg dry 144 75 - 125 Nickel 1.83 206 218 mg/kg dry 105 75 - 125 Selenium ND 20.6 13.9 M8 mg/kg dry 67 75 - 125 Silver ND 20.6 18.5 mg/kg dry 90 75 - 125 Thallium ND 20.6 20.5 mg/kg dry 100 75 - 125 Zinc 43.8 206 236 mg/kg dry 93 75 - 125 Lab Sample ID: 11 H2347-MSD1 Client Sample ID: Matrix Spike Duplicate Matrix: Soil Prep Type: Total Analysis Batch: 11 H2347 Prep Batch: 11 H2347_P Sample Sample Spike Matrix Spike Dup Matrix Spike Dul % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Antimony 0.915 41.4 36.8 mg/kg dry # 87 75 - 125 1 20 0 TestAmerica Nashville Page 29 of 38 08/11/2011 Client: Hart & Hickman QC Sample Results TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Method: SW846 6010C - Total Metals by EPA 6010C (Continued) Lab Sample ID: 11H2347-MSD1 Matrix: Soil Analysis Batch: 11H2347 Client Sample ID: Matrix Spike Duplicate Prep Type: Total Prep Batch: 11 H2347_P Sample Sample Spike Matrix Spike Dup Matrix Spike Dui % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Arsenic 0.855 20.7 22.7 mg/kg dry 3:� 106 75. 125 0.9 20 Beryllium 0.139 20.7 19.1 mg/kg dry 3:� 92 75. 125 0.3 20 u Cadmium ND 20.7 17.8 mg/kg dry 86 75. 125 0.8 20 Chromium 5.91 82.8 103 mg/kg dry 118 75. 125 1 20 Copper 5.01 103 141 M7 mg/kg dry 132 75. 125 5 20 Lead 10.8 20.7 45.9 M7 mg/kg dry 170 75 - 125 13 20 Nickel 1.83 207 220 mg/kg dry 105 75 - 125 0.5 20 Selenium ND 20.7 13.5 M8 mg/kg dry 65 75 - 125 2 20 Silver ND 20.7 18.3 mg/kg dry 88 75. 125 1 20 Thallium ND 20.7 21.1 mg/kg dry 102 75. 125 3 20 Zinc 43.8 207 243 mg/kg dry 96 75. 125 3 20 Method: SW846 7471 B - Mercury by EPA Method 7471 B Lab Sample ID: 11 H2O33-BLK1 Client Sample ID: Method Blank Matrix: Soil Prep Type: Total Analysis Batch: 11 H2O33 Prep Batch: 11 H2O33_P Blank Blank Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury ND 0.10 mg/kg wet 08/11/11 10:00 08/11/11 13:18 1.0 Lab Sample ID: 11 H2O33-BS1 Client Sample ID: Lab Control Sample Matrix: Soil Prep Type: Total Analysis Batch: 11 H2O33 Prep Batch: 11 H2O33_P Spike LCS LCS % Rec. Analyte Added Result Qualifier Unit D % Rec Limits Mercury 0.165 0.18 mg/kg wet 107 80. 120 Lab Sample ID: 11 H2O33-MS1 Client Sample ID: Matrix Spike Matrix: Soil Prep Type: Total Analysis Batch: 11 H2O33 Prep Batch: 11 H2O33_P Sample Sample Spike Matrix Spike Matrix Spike % Rec. Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits Mercury ND 0.163 0.19 mg/kg wet 116 80 - 120 Lab Sample ID: 11H2033-MSD1 Client Sample ID: Matrix Spike Duplicate Matrix: Soil Prep Type: Total Analysis Batch: 11 H2O33 Prep Batch: 11 H2O33_P Sample Sample Spike Matrix Spike Dup Matrix Spike Du{ % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Mercury ND 0.160 0.19 mg/kg wet 118 80. 120 0.09 20 Method: SW-846 - General Chemistry Parameters Lab Sample ID: 11H2394-DUP1 Client Sample ID: Duplicate Matrix: Soil Prep Type: Total Analysis Batch: 11 H2394 Prep Batch: 11 H2394_P Sample Sample Duplicate Duplicate RPD Analyte Result Qualifier Result Qualifier Unit D RPD Limit % Dry Solids 81.1 76.2 % 6 20 TestAmerica Nashville Page 30 of 38 08/11/2011 QC Association Summary Client: Hart &Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 GCMS Volatiles Analysis Batch: U014254 Lab Sample ID Client Sample ID Prep Type Matrix Method 11 H2752-BS1 Lab Control Sample Total Soil SW846 82606 11 H2752-BLK1 Method Blank Total Soil SW846 8260E NUH1259-01 BF-1 Total Soil SW846 8260B NUH1259-02 BF-2 Total Soil SW846 8260B 11 H2752-MS1 Matrix Spike Total Soil SW846 8260B 11 H2752-MSD1 Matrix Spike Duplicate Total Soil SW846 8260B Prep Batch: 11 H2752_P Lab Sample ID Client Sample ID Prep Type Matrix Method 11 H2752-BS1 Lab Control Sample Total Soil EPA 5035 11 H2752-BLK1 Method Blank Total Soil EPA 5035 NUH1259-01 BF-1 Total Soil EPA 5035 NUH1259-02 BF-2 Total Soil EPA 5035 11 H2752-MS1 Matrix Spike Total Soil EPA 5035 11 H2752-MSD1 Matrix Spike Duplicate Total Soil EPA 5035 GCMS Semivolatiles Analysis Batch: 11 H2345 Lab Sample ID Client Sample ID Prep Type Matrix Method 11 H2345-BLK1 Method Blank Total Soil SW846 8270D 11 H2345-BS1 Lab Control Sample Total Soil SW846 8270D NUH1259-01 BF-1 Total Soil SW846 8270D NUH1259-02 BF-2 Total Soil SW846 8270D Prep Batch: 11 H2345_P Lab Sample ID Client Sample ID Prep Type Matrix Method 11 H2345-BLK1 Method Blank Total Soil EPA 3550C 11 H2345-BS1 Lab Control Sample Total Soil EPA 3550C NUH1259-01 BF-1 Total Soil EPA 3550C NUH1259-02 BF-2 Total Soil EPA 3550C Pesticides Analysis Batch: U014151 FLab Sample ID 11H2343-BLK1 11H2343-BS1 11 H2343-MS1 11 H2343-MSD1 NUH1259-01 NUH1259-02 Analysis Batch: U014169 Prep Batch 11H2752=P 11 H2752P 11H2752_P 11 H2752P 11H2752_P 11H2752_P Prep Batch Prep Batch 11H2345_P 11H2345_P 11H2345_P 11H2345_P Prep Batch Client Sample ID Prep Type Matrix Method Prep Batch Method Blank Total Soil SW846 8082A 11 H2343 P Lab Control Sample Total Soil SW846 8082A 11 H2343_P BF-2 Total Soil SW846 8082A 11 H2343P BF-2 Total Soil SW846 8082A 11 H2343P BF-1 Total Soil SW846 8082A 11 H2343P BF-2 Total Soil SW846 8082A 11 H2343P Lab Sample ID Client Sample ID 11 H2333-BLK1 Method Blank 11 H2333-BS1 Lab Control Sample 11 H2333-BS2 Lab Control Sample 11 H2333-MS1 BF-1 11 H2333-MSD1 BF-1 NUH 1259-01 BF-1 NUH 1259-02 BF-2 Prep Type Matrix Method Prep Batch Total Soil SW846 8081 B 11 H2333 P Total Soil SW846 8081 B 11 H2333_P Total Soil SW846 8081 B 11 H2333_P Total Soil SW846 8081 B 11 H2333 P Total Soil SW846 8081 B 11 H2333 P Total Soil SW846 8081 B 11 H2333_P Total Soil SW846 8081 B 11 H2333 P TestAmerica Nashville Page 31 of 38 08/11/2011 QC Association Summary Client: Hart &Hickman TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Pesticides (Continued) Prep Batch: 11 H2333_P Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 11 H2333-BLK1 Method Blank Total Soil EPA 3550C 11 H2333-BSI Lab Control Sample Total Soil EPA 3550C 11 H2333-BS2 Lab Control Sample Total Soil EPA 3550C 11 H2333-MS1 BF-1 Total Soil EPA 3550C 11 H2333-MSD1 BF-1 Total Soil EPA 3550C NUH1259-01 BF-1 Total Soil EPA 3550C NUH1259-02 BF-2 Total Soil EPA 3550C Prep Batch: 11 H2343_P Lab Sample ID Client Sample ID 11 H2343-BLK1 Method Blank 11 H2343-BS1 Lab Control Sample 11 H2343-MS1 BF-2 11 H2343-MSD1 BF-2 NUH1259-01 BF-1 NUH1259-02 BF-2 Metals Prep Type Matrix Method Prep Batch F Total Soil EPA 3550C/3665A Total Soil EPA 3550C/3665A Total Soil EPA 3550C/3665A Total Soil EPA 3550C/3665A Total Soil EPA 3550C/3665A Total Soil EPA 3550C/3665A Analysis Batch: 11 H2O33 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 11 H2O33-BLK1 Method Blank Total Soil SW846 7471 B 11 H2033 P 11 H2O33-BS1 Lab Control Sample Total Soil SW846 7471 B 11 H2O33_P 11 H2O33-MS1 Matrix Spike Total Soil SW846 7471 B 11 H2O33_P 11 H2O33-MSD1 Matrix Spike Duplicate Total Soil SW846 7471 B 11 H2O33_P NUH1259-01 BF-1 Total Soil SW8467471B 11H2033 P NUH1259-02 BF-2 Total Soil SW8467471B 11H2033 P Analysis Batch: 11 H2347 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 11 H2347-BLK1 Method Blank Total Soil SW846 6010C 11 H2347_P 11 H2347-BS1 Lab Control Sample Total Soil SW846 6010C 11 H2347_P 11 H2347-BSD1 Lab Control Sample Dup Total Soil SW846 6010C 11 H2347_P 11 H2347-MS1 Matrix Spike Total Soil SW846 6010C 11 H2347_P 11 H2347-MSD1 Matrix Spike Duplicate Total Soil SW846 6010C 11 H2347_P NUH1259-01 BF-1 Total Soil SW8466010C 11 H2347P NUH1259-02 BF-2 Total Soil SW8466010C 11 H2347P Prep Batch: 11 H2O33_P Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 11 H2O33-BLK1 Method Blank Total Soil EPA 7471 11 H2O33-BS1 Lab Control Sample Total Soil EPA 7471 11 H2O33-MS1 Matrix Spike Total Soil EPA 7471 11 H2O33-MSD1 Matrix Spike Duplicate Total Soil EPA 7471 NUH1259-01 BF-1 Total Soil EPA 7471 NUH1259-02 BF-2 Total Soil EPA 7471 TestAmerica Nashville Page 32 of 38 08/11/2011 QC Association Summary Client: Hart & Hickman TestAmerica Job ID: NUH1259 L Project/Site: CRM-008 Metals (Continued) Prep Batch: 11 H2347_P Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 11 H2347-BLK1 Method Blank Total Soil EPA 3051 A/6010 11 H2347-BS1 Lab Control Sample Total Soil EPA 3051 A/6010 11 H2347-BSD1 Lab Control Sample Dup Total Soil EPA 3051 A/6010 11 H2347-MS1 Matrix Spike Total Soil EPA 3051 A/6010 11 H2347-MSD1 Matrix Spike Duplicate Total Soil EPA 3051 A/6010 NUH1259-01 BF-1 Total Soil EPA 3051 A/6010 NUH1259-02 BF-2 Total Soil EPA 3051 A/6010 Extractions Analysis Batch: 11 H2394 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 11 H2394-DUP1 Duplicate Total Soil SW-846 11 H2394_P NUH1259-01 BF-1 Total Soil SW-846 11 H2394P NUH1259-02 BF-2 Total Soil SW-846 11 H2394P Prep Batch: 11 H2394_P Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 11 H2394-DUP1 Duplicate Total Soil % Solids NUH1259-01 BF-1 Total Soil % Solids NUH1259-02 BF-2 Total Soil % Solids TestAmerica Nashville Page 33 of 38 08/11/2011 Client: Hart & Hickman Lab Chronicle TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Client Sample ID: BF-1 Lab Sample ID: NUH1259-01 Date Collected: 08/09/11 12:50 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.3 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Or Analyzed Analyst Lab Total Prep EPA 5035 0.938 11 H2752_P 08/09/11 12:50 AAN TAL NSH Total Analysis SW846 8260B 1.00 U014254 08/10/11 17:12 MJH TAL NSH Total Prep EPA 3550C 0.996 11 H2345_P 08/10/11 11:30 JJR TAL NSH Total Analysis SW846 8270D 1.00 11 H2345 08/11/11 14:41 KJP TAL NSH Total Prep EPA 3550C 0.982 11 H2333_P 08/10/11 11:14 AMS TAL NSH Total Analysis SW846 8081 B 1.00 U014169 08/10/11 19:43 WAM TAL NSH Total Prep EPA 3550C/3665A 0.981 11 H2343_P 08/10/11 12:05 AMS TAL NSH Total Analysis SW846 8082A 1.00 U014151 08/11/11 00:04 RMC TAL NSH Total Prep EPA 3051A/6010 0.967 11 H2347_P 08/10/11 12:00 AU TAL NSH Total Analysis SW846 6010C 1.00 11 H2347 08/10/11 21:06 AVR TAL NSH Total Prep EPA 7471 0.96 11 H2033_P 08/11/11 10:00 MB TAL NSH Total Analysis SW8467471B 1.0 11H2O33 08/11/1113:50 MB TAL NSH Total Prep % Solids 1.00 11 H2394_P 08/10/11 14:32 RRS TAL NSH Total Analysis SW-846 1.00 11H2394 08/11/1110:48 RRS TAL NSH Client Sample ID: BF-2 Lab Sample ID: NUH1259-02 Date Collected: 08/09/11 13:10 Matrix: Soil Date Received: 08/10/11 06:30 Percent Solids: 81.5 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number Or Analyzed Analyst Lab Total Prep EPA 5035 1.01 11 H2752_P 08/09/11 13:10 AAN TAL NSH Total Analysis SW846 8260B 1.00 U014254 08/10/11 17:44 MJH TAL NSH Total Prep EPA 3550C 0.982 11 H2345_P 08/10/11 11:30 JJR TAL NSH Total Analysis SW846 8270D 1.00 11 H2345 08/11/11 15:04 KJP TAL NSH Total Prep EPA 3550C 0.989 11 H2333_P 08/10/11 11:14 AMS TAL NSH Total Analysis SW846 8081 B 1.00 U014169 08/10/11 19:58 WAM TAL NSH Total Prep EPA 3550C/3665A 0.976 11 H2343_P 08/10/11 12:05 AMS TAL NSH Total Analysis SW846 8082A 1.00 U014151 08/11/11 00:25 RMC TAL NSH Total Prep EPA 3051A/6010 0.952 11 H2347_P 08/10/11 12:00 AU TAL NSH Total Analysis SW846 6010C 1.00 11 H2347 08/10/11 21:10 AVR TAL NSH Total Prep EPA 7471 1.0 11 H2033_P 08/11/11 10:00 MB TAL NSH Total Analysis SW8467471B 1.0 11H2O33 08/11/1113:53 MB TAL NSH Total Prep % Solids 1.00 11 H2394_P 08/10/11 14:32 RRS TAL NSH Total Analysis SW-846 1.00 11H2394 08/11/1110:48 RRS TAL NSH Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Road, Nashville, TN 37204, TEL 800-765-0980 0 TestAmerica Nashville Page 34 of 38 08/11/2011 Method Summary Client: Hart & Hickman TestAmerica Job ID: NUH1259 L Project/Site: CRM-008 Method Method Description Protocol Laboratory SW-846 General Chemistry Parameters TAIL NSH SW846 8260E Volatile Organic Compounds by EPA Method 8260B TAIL NSH SW846 8270D Semivolatile Organic Compounds by EPA Method 8270D TAIL NSH SW846 8081 B Organochlorine Pesticides by EPA Method 8081 B TAIL NSH SW846 8082A Polychlorinated Biphenyls by EPA Method 8082A TAIL NSH SW846 6010C Total Metals by EPA 6010C TAIL NSH SW846 7471 B Mercury by EPA Method 7471 B TAIL NSH Protocol References: Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Road, Nashville, TN 37204, TEL 800-765-0980 0 TestAmerica Nashville Page 35 of 38 08/11/2011 Client: Hart &Hickman Certification Summary TestAmerica Job ID: NUH1259 Project/Site: CRM-008 Laboratory Authority Program EPA Region Certification ID TestAmerica Nashville A21-A ISO/IEC 17025 0453.07 TestAmerica Nashville A21-A WY UST 453.07 TestAmerica Nashville AIHA IHLAP 100790 TestAmerica Nashville Alabama State Program 4 41150 TestAmerica Nashville Alaska Alaska UST 10 UST-087 TestAmerica Nashville Arizona State Program 9 AZ0473 TestAmerica Nashville Arkansas State Program 6 88-0737 TestAmerica Nashville CALA CALA 3744 TestAmerica Nashville California NELAC 9 1168CA TestAmerica Nashville Colorado State Program 8 N/A TestAmerica Nashville Connecticut State Program 1 PH-0220 TestAmerica Nashville Florida NELAC 4 E87358 TestAmerica Nashville Illinois NELAC 5 200010 TestAmerica Nashville Iowa State Program 7 131 TestAmerica Nashville Kansas NELAC 7 E-10229 TestAmerica Nashville Kentucky Kentucky UST 4 19 TestAmerica Nashville Kentucky State Program 4 90038 TestAmerica Nashville Louisiana NELAC 6 LA100011 TestAmerica Nashville Louisiana NELAC 6 30613 TestAmerica Nashville Maryland State Program 3 316 TestAmerica Nashville Massachusetts State Program 1 M-TN032 TestAmerica Nashville Minnesota NELAC 5 047-999-345 TestAmerica Nashville Mississippi State Program 4 N/A TestAmerica Nashville Montana MT DEQ UST 8 NA TestAmerica Nashville Nevada State Program 9 TN00032 TestAmerica Nashville New Hampshire NELAC 1 2963 TestAmerica Nashville New Jersey NELAC 2 TN965 TestAmerica Nashville New York NELAC 2 11342 TestAmerica Nashville North Carolina North Carolina DENR 4 387 TestAmerica Nashville North Dakota State Program 8 R-146 TestAmerica Nashville Ohio OVAP 5 CL0033 TestAmerica Nashville Oklahoma State Program 6 9412 TestAmerica Nashville Oregon NELAC 10 TN200001 TestAmerica Nashville Pennsylvania NELAC 3 68-00585 TestAmerica Nashville Rhode Island State Program 1 LA000268 TestAmerica Nashville South Carolina State Program 4 84009 TestAmerica Nashville South Carolina State Program 4 84009 TestAmerica Nashville Tennessee State Program 4 2008 TestAmerica Nashville Texas NELAC 6 T104704077-09-TX TestAmerica Nashville USDA USDA S-48469 TestAmerica Nashville Utah NELAC 8 TAN TestAmerica Nashville Virginia NELAC Secondary AB 3 460152 TestAmerica Nashville Virginia State Program 3 00323 TestAmerica Nashville Washington State Program 10 C789 TestAmerica Nashville West Virginia West Virginia DEP 3 219 TestAmerica Nashville Wisconsin State Program 5 998020430 Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory's current list of certified methods and analytes. TestAmerica Nashville Page 36 of 38 08/11/2011 r Nashville, TN COOLER RECEI r Cooler Received/Opened On $•10.11 Q. 060b 1. Tracking #_�%(pz•(p��y $/]/ (last 4 digits, FedEx) Courier: _r� IR Gun ID 94660220 2. Temperature of rep. sample or temp blank when opened:_.il Degrees Celsius NUH1259 3. If Item #2 temperature is 0°C or less, was the representative sample or temp blank frozen? YES NO.(14D 4. Were custody seals on outside of cooler? _ ES).NO...NA If yes, how many and where: 5. Were the seals intact, signed, and dated correctly? <j5)..N0...NA 6. Were custody papers inside cooler? e �E..NO...NA I certify that 1 opened the cooler and answered questions 1 6 (intial) 7. Were custody seals on containers: YES? and Intact YES ... NO. ^Co Were these signed and dated correctly? YES ... NO..tUD 8. Packing mat'] used? 6iDPlastic bag Peanuts Vermiculite am Inse Paper Other None 9. Cooling process: � Ice -pack Ice (direct contact) Dry ice Other None 10. Did all Containers arrive in good condition (unbroken)? E�%.NO...NA 11. Were all container labels complete (#, date, signed, pres., etc)? '�M..NO... NA 12. Did all container labels and tags agree with custody papers? <ZED..NO... fVA 13a. Were VOA vials received? �..NO...NA b. Was there any observable headspace present in any VOA vial? YES ... NO.41M 14. Was there a Trip Blank in this cooler? YES ... NO. If multiple coolers, sequence # I_certify that I unloaded the cooler and answered uestions 7-14 (intial 15a. On pres'd bottles, did pH test strips suggest preservation reached the correct pH level? YES..NO(0► ti- rJid the brttf- !,hers indicate that pisypc rer�re nce•V _..._. C31D ...NA 16. Was residual chlorine present? YES ... NO..,4VV I_certifv that I checked for chlorine and pH as per SOP and answered auestions 15-16 fintiall 17. Were custody properly filled out (ink, signed, etc)? 1j ?..NO...NA M Did you sign the custody papers in the appropriate place? 4EM..NONA 19. Were correct containers used for the analysis requested? ... �,$ ..NO...NA 20. Was sufficient amount of sample sent in each container? �S...NO...NA I certify that I entered this Droiect into LtMS and answered questions 17-20 intial I certify that P attached a label with the unioue LIMS number to each container intial 21. Were there Non -Conformance issues at login? YES.. O as a PIPE generated? YESio. BIS = Broken in shipment Cooler Receipt F'orm.doc LF- I End 1%ge 37 of 38 Revised 6!24,'M 08/11/2011 mm LL C m m m m m CCvFFi �1 O m c O m - OOz o = ai m cl z b C a m - !n c (13 rC/) zt m OD c w rw m 0 zz O Z D C > D' m m a m m D v\ n m X) 70 D n m m U) m v ao = , D m m m Cp" (ems t7 O r `.1.+' c vUJz zN z D Cam: r'r�`O = m D a/.) T -i v -� Z < W o f w m W m O Z w D O m m� r C C v Z 0 7pm Dm o Ln umi m' =' m �♦ _i vx m z W tii t"7 m ¢ Gl T ,J ! S > Dy' m Z CEO to C7� m cn ) t - 03 m rn 2 z D�.�..� 1/ r Q m �T,� r.... m y v n `° �'7 "u D Co =� m O f7 w --i � c mom> z C z D !.J m D o Z C7 _ � m z o 1 m En m A �� X Z }' o Z Z+ COMPOSITE (C) OR GRAB (G) INDICATE m AQUEOUS WATER 0 X SOLID OR SEMISOLID m AIR x _ NONAQUEOUS LIQUID OIL, SOLVENT,... x r$z 31 X XVDCS - N 1 _ r ` CA x m X � �ceC��Z� �m � 7 A Z CD x X. 3 � D�a�5 A 0 z,' D v N � --cn crn oo uo �. a> C O cr T 1 -n 'p y S (D _ k 6 1 N ! 4 CJi .N. -t me �'m>mc vtn a row am F + ...1 aim v n�m v �z m m m °>� a' m Dm �D mm v ��o v �o co m c. m m m m m A o w z co 0 0 o m P`eUof38 08/11 /2011 APPENDIX B Geotechnical Data for Cap Source Soil o1 0 1 I GcoTechnologies, Inc. - - mom ► • - • • 1 ■��. • . IL illiq ■■■■■■■■■,,, ■■■■■■■■■1\\■► ■■■■■■' I■■■■■■■\`OM ■■■■■I,■■■■■■■SAW11 ■■■■■r i■■■■■■■■■V�� ■■■■■M■■■■■■■■ ■■■■■■■■■■■■■■■■■mm ■■■■■■■■■■■■■■■■■m�� ■■■■■■■■■■■■■■■■■■,,,, ■■■■■■■■■■■■■■■■■■„■■, ■■■■■■■■■■■■■■■■■■■Mm ■■■■■■■■■■■■■■■■■■■■■■■■■■■LI■E\ ■■■■■■■■■■■■■■■■■■■■■■■■■■■■■■■MM■�. 1 1 1 1 1 I 1 130 125 120 z 105 w 0 o: 0 100 95 80 0 Job No: 1-11-0488-CA Date: 8/12111 Job Name: Planters Oil Mill Job Location: Rocky Mount NC Boring No: Sample No: S-3 Depth: TEST RESULTS Method of Test: ASTM D 698 Maximum Dry Density: 99.0 PCF Optimum Moisture Content: 22•5% Natural Moisture Content: % Atterberg Limits: LL PI Soil Description: Brown Sandy Silt Date Recieved: 9/9/2011 Dates Tested: 8/10/2011 CURVES OF 100% SATURATION FOR SPECIFIC GRAVITY EQUAL TO: 5 10 15 20 25 30 WATER CONTENT (Percent Dry Weight) MOISTURE -DENSITY RELATIONSHIP 3200 Wellington Court, Suite 108 Raleigh, NC 27615 2.80 2.70 2.60 40 45 APPENDIX C Erosion Control Plan and Approval Letter WCDENK North Carolina Department of Environment and Natural Resources Division of Land Resources Land Quality Section James D. Simons, PG, PE Beverly Eaves Perdue, Governor Director and State Geologist Dee Freeman, Secretary July 25, 2011 LETTER OF APPROVAL City of Rocky Mount ATTN : Charles Penny, City Manager PO Box 1180 Rocky Mount, NC 27802 RE: Project Name: Planters Oil Mill Fill Remediation Project ID: EDGEC-2012-001 Acres Approved: 4.50 County: Edgecombe, Cokey Road and Short Road, Rocky Mount River Basin: Tar -Pamlico Stream Classification: Other Submitted By: Michael Tolson, City of Rocky Mount Date Received by LQS: July 25, 2011 Plan Type: New Dear Sir or Madam: This office has reviewed the subject erosion and sedimentation control plan. We find the plan to be acceptable and hereby issue this Letter of Approval. The enclosed Certificate of Approval must be posted at the job site. This plan approval shall expire three (3) years following the date of approval, if no land -disturbing activity has been undertaken, as is required by Title 15A NCAC 4B .0129. Title 15A NCAC 4B .0118(a) requires that a copy of the approved erosion control plan be on file at the job site. Also, this letter gives the notice required by G.S. 113A-b1.1(a) of our right of periodic inspection to insure compliance with the approved plan. North Carolina's Sedimentation Pollution Control Act is performance -oriented, requiring protection of existing natural resources and adjoining properties. If, following the commencement of this project, the erosion and sedimentation control plan is inadequate to meet the requirements of the Sedimentation Pollution Control Act of 1973 (North Carolina General Statute I I3A-51 through 66), this office may require revisions to the plan and implementation of the revisions to insure compliance with the Act. Acceptance and approval of this plan is conditioned upon your compliance with Federal and State water quality laws, regulations, and rules. In addition, local city or county ordinances or rules may Raleigh Regional Office 1628 Mail Service Center, Raleigh, North Carolina 27699 Phone. (919) 7914200 l Fax: (919) 571-4718 Letter of Approval Project: Planters Oil Mill Fill Remediation July 25, 2011 Page 2 of 2 also apply to this land -disturbing activity. This approval does not supersede any other permit or approval. Please be aware that your project will be covered by the enclosed NPDES General Stormwater Permit NCGO10000 (Construction Activities). You should first become familiar with all of the requirements for compliance with the enclosed general permit. Due to the location of this project, it should be noted that a rule to protect and maintain existing buffers along watercourses in the Tar -Pamlico River Basin became effective on January 1, 2000. _-The Tar -Pamlico River Riparian Area Protection andMaintenance Rule (15A NCAC 2B .0259) applies to all perennial and intermittent streams, lakes, ponds and estuaries in the Tar -Pamlico River Basin with existing vegetation on the adjacent land or "riparian area". In riparian areas with existing vegetation in the first 30 feet directly adjacent to the stream, the rule prohibits land disturbance or new development within the first 30 feet of land next to the water (the remaining 20 feet of the total buffer must be revegetated upon completion of any proposed land -disturbing activity). In riparian areas with existing vegetation that is less than 30 feet wide, the rule prohibits land disturbance or new development within the area that contains the existing vegetation (but not the entire 50 foot riparian area). For more information about this riparian area rule, please contact the Division of Water Quality's Wetland/401 Unit at 919-733-1786, or a Division of Water Quality representative at this regional office. Please note that this approval is based in part on the accuracy of the information provided in the Financial Responsibility Form, which you provided. You are requested to file an amended form if there is any change in the information included on the form. In addition, it would be helpful if you notify this office of the proposed starting date for this project. Please notify us if you plan to have a preconstruction conference. Your cooperation is appreciated. Sincerely, aryn'Pageau�IT, CPESC Assistant Regional Engineer Land Quality Section Enclosures: Certificate of Approval NPDES Permit cc: Michael Tolson, PE, City of Rocky Mount, PO Box 1180, Rocky Mount, NC 27802 Danny Smith, DWQ — SWP Supervisor, Raleigh Regional Office Construction Plans for: PLANTERS OIL MILL FILL RfMfOlA TION CRM PROJECT # POCLf CRM BlD # 7605 / CV COVER 51-1EET GP SEDIMENTATION, EROSION CONTROL GRADING PLAN plans prepared by: CITY OF ROCKY MOUNT DEPARTMENT OF ENGINEERING 33 1 5. FRAN KLI N STREET PO BOX 1 180 ROCKY MOUNT, NC 27802 TEL (252) 972- 1 1 2 1 fAX (252) 972- 1 1 76 VICINITY MAP - SCALE - I" = 2000' SCOPE OF WORK - + ..• ,. ! ----JL __�� AL;:-� w� � Y am { l (-'� � 1 �j i THIS PROJECT INVOLVES THE PLACEMENT OF APPROXIMATELY (5,500 CY OF CLEAN FILL OVER APPROXIMATELY 4.5 ACRES OF A 7.35 '-- n ,sk>ri [� 4f3 �l—J�'-�—� ,-q 3 Lam.- � ,u 8 � � �i�`' `'�a �,y. '1 a o .� / ACRE SITE LOCATED AT THE INTERSECTION OF PLANTERS STREET AND COKPY ROAD. THIS SITE IS SUBJECT TO A BROWNSFIELD �s Sys'" E '� 9yQ """c/ AGREEMENT AND WILL BE INSPECTED DURING CONSTRUCTION TO VERIFY THICKNESS OF FILL AND FOR OVERALL POSITIVE DRAINAGE. 8uvn � 64.. �� THIS PROJECT ALSO INVOLVES THE REMOVAL OF APPROXIMATELY 1500 LF EXISTING PERIMETER CHAIN LINK FENCE AND GATE STRUCTURES WITHOUT DISTURBING THE EXISTING GROUND. EJ �rZ�-�Fr--�r-��i1lnnc,�t''` LQ/U�� a % •�� \�e w I. ,r 0 2 • THE CONTRACTOR SHALL MAKE HI5 OWN PRE BID FIELD DETERMINATION OF ALL EXISTING UTILITIES, STORM DRAINAGE, AND OTHER BURIED OR CONCEALED FACILITIES. THE LOCATION SHOWN ON THE DRAWINGS OF EXISTING UTILITIES, STORM DRAINAGE, AND OTHER BURIED AND OR CONCEALED FACILITIES ARE NOT GUARANTEED AND SHALL BE VERIFIED BY THE CONTRACTOR TO HIS SATISFACTION PRIOR TO START OF WORK. THE DRAWING5 DO NOT SHOW ALL EXISTING UTILITIES, STORM DRAINAGE, AND OTHER BURIED AND OR CONCEALED FACILITIES. • THE CONTRACTOR SHALL CONTACT NC ONE -CALL CENTER AT 51 1 AT LEAST FORTY-EIGHT (48) HOURS PRIOR TO DIGGING. • IN THE EVENT OF CONFLICTS WITH EXISTING UTILITIES, OR IF FURTHER VERIFICATION OF BURIED AND OR CONCEALED UTILITIES, OR TEMPORARY DISRUPTION OF SERVICE 15 NECESSARY, THE CONTRACTOR SHALL CONTACT THE APPROPRIATE UTILITY COMPANY AND SHALL FULLY COORDINATE ANY NECESSARY MODIFICATIONS OF THE WORK WITH THE ENGINEER AND THE APPROPRIATE UTILITY. KNOWN UTILITIES WITHIN THE PROJECT AREA AND THEIR RESPECTIVE CONTRACTS ARE AS FOLLOWS: PR r A. CITY WATER AND SEWER ED JOYNER 972-1 3 17 oO® 5. CITY STREETS AND STORM SEWER [ED WHITE 972-1 2941 C. CITY ELECTRICITY [DARRYL STROTHER 972-1 2721 E �i ^•' Oa a • a D. CITY GAS [LLOYD TURNER 972- 1 2791 �( iqN E. NCDOT STREETS AND STORM SEWER [DAVID REYNOLDS 459-21 251 f. r _ ®®�(- S ��/\ G. CEDNTDENUNK UR INK [WPAD ALABASTER AM OWENS 3�4-446zO51 1 vcsr twuvr ss•" a i tunjs �,_ l • ALL QUANTITIES AND MEASUREMENTS SHOWN ON THE DRAWINGS FOR THE WORK ARE APPROXIMATE AND ARE FOR BIDDING PURPOSES ONLY. THE BA515 OF PAYMENT FOR THE WORK SHALL BE MADE FOR THE ACTUAL FIELD MEASURED QUANTITIES OF ITEMS WHICH HAVE BEEN INSTALLED AND APPROVED BY THE ENGINEER. THE CONTRACTOR SHALL CONTACT NCDOT DIVISION 4, DISTRICT I OFFICE OR DISTRICT 2 OFFICE, A5 APPROPRIATE, PRIOR TO PERFORMING ANY WORK WITHIN NCDOT RIGHT-OF-WAY. A COPY OF ALL APPROVED ENCROACHMENT AGREEMENTS WILL BE FURNISHED BY THE CITY TO THE CONTRACTOR AND SHALL BE KEPT ON -SITE DURING ALL CONSTRUCTION WORK. THE CONTRACTOR IS PROHIBITED FROM STORAGE OF CONSTRUCTION EQUIPMENT AND OR MATERIALS ON NCDOT Po E No MAINTAINED PAVED ROADWAYS AND IS PROHIBITED FROM STOCKPILING OF TRENCH EXCAVATION OR SPOIL MATERIAL �� • � fi ON NCDOT MAINTAINED PAVED ROADWAYS. THE COST OF HAULING AND OFF -SITE STOCKPILING OF THIS CLA55 OF EXCAVATED MATERIALS SHALL BE INCLUDED BY THE CONTRACTOR IN HIS UNIT PRICE BID FOR THE PIPE INSTALLATION. NOTES I . TOPOGRAPHICAL INFORMATION AND LOCATION INFORMATION TAKEN FROM A SURVEY PERFOMED BY JOYNER KEENY, PLLC PLANNING AND LAND SURVEYING ENTITLED "BOUNDARY AND TOPOGRAPHIC MAP OF PLANTERS OIL MILL SITE, ROCKY MOUNT, NC" DATED 04/ 1 5/201 0. 2. THIS PROJECT IS NOT LOCATED WITHIN A SPECIAL FLOOD HAZARD ZONE PER FEMA MAP NUMBER 3720375900,1 EFFECTIVE DATE NOVEMBER 3, 2004. 3. PROJECT DISTURBANCE 15 GREATER THAN I ACRE; THEREFORE, AN EROSION CONTROL PERMIT FROM NCDENR WILL BE REQUIRED. NO WORK SHALL BEGIN UNTIL EROSION CONTROL MEASURES ARE IN PLACE. 4. BOUNDARY INFORMATION 15 FOR REFERENCE ONLY. 5. CONTRACTOR 15 TO LOCATE ALL EXISTING UTILITIES IN PROJECT VICINITY PRIOR TO BEGINNING WORK. G. CONTRACTOR IS TO COORDINATE WITH ENGINEER IN THE EVENT OF UNFORESEEN ISSUES/CONFLICTS. NOTES • THE CONTRACTOR IS RESPONSIBLE FOR PROVIDING, INSTALLING, MAINTAINING AND REMOVING SIGNS, BARRICADES, LIGHTS, ETC., IN ACCORDANCE WITH THE MANUAL OF UNIFORM TRAFFIC CONTROL DEVICES, LATEST EDITION, FOR LANE CLOSURES OR DETOURS ON CITY STREETS. CONTACT THE CITY TRAFFIC ENGINEER AT 252-972-I 123 FOR APPROVAL OF APPROPRIATE INSTALLATION. FOR LANE CLOSURES OR DETOURS ON NCDOT ROADWAYS, CONTACT THE DISTRICT ENGINEER AT 252-459-21 2G. CONSTRUCTION SIGNING SHALL BE CONSIDERED INCIDENTAL TO PIPE LINE CONSTRUCTION AND THE CONTRACTOR SHALL INCLUDE THE COST OF SUCH WORK IN THE UNIT PRICE BID FOR PIPE INSTALLATION. • THE CONTRACTOR SHALL BE RESPONSIBLE FOR AND SHALL CORRECT ANY AND ALL DAMAGES TO PROPERTY, BOTH PUBLIC AND PRIVATE, CAUSED BY HIM DURING THE EXECUTION OF HIS WORK. THE C05T OF REPLACING OR REPAIRING SUCH DAMAGED PROPERTY TO THE ORIGINAL CONDITION SHALL BE INCLUDED BY THE CONTRACTOR IN HI5 UNIT PRICE BID FOR THE PIPE INSTALLATION. • THE CONTRACTOR SHALL BE RESPONSIBLE FOR AND SHALL CORRECT ANY AND ALL DAMAGES TO EXISTING UTILITIES, STORM DRAINAGE AND OTHER FACILITIES CAUSED BY HIM DURING THE EXECUTION OF H15 WORK WHETHER5UCH ITEMS ARE SHOWN ON THE DRAWINGS OR NOT. THE COST OF REPLACING OR REPAIRING SUCH DAMAGED EXISTING UTILITIES, STORM DRAINAGE AND OTHER FACILITIES TO THE SATISFACTION OF THE ENGINEER SHALL BE INCLUDED BYTHE CONTRACTOR IN HIS UNIT PRICE BID FOR THE PIPE INSTALLATION. • FENCES DAMAGED DURING CONSTRUCTION OPERATIONS SHALL BE REPAIRED BY THE CONTRACTOR. THE CONTRACTOR SHALL INSTALL TEMPORARY FENCING TO PREVENT ESCAPE OF LIVESTOCK. • THE CONTRACTOR SHALL BE RESPONSIBLE FOR ANY DAMAGE CAUSED BY HS CONSTRUCTION OPERATIONS TO EXISTING USGS, NCG5, NCDOT AND OR CITY OF ROCKY MOUNT MONUMENTS. THE CONTRACTOR SHALL, AT HIS COST, REPAIR, REPLACE OR RESET ANY MONUMENTS 50 DISTURBED BY HIM AS DETERMINED BY THE ENGINEER. THIS WORK SHALL BE DONE BY A REGISTERED LAND SURVEYOR. • THE CONTRACTOR SHALL TAKE PRECAUTIONS NOT TO DISTURB EXISTING PROPERTY CORNERS. IF THE WORK REQUIRES THE REMOVAL AND RE5ET OF PROPERTY IRONS, THIS WORK SHALL BE DONE BY A REGISTERED LAND SURVEYOR. • THE CONTRACTOR 5HALL GRADE, SHAPE, AND SEED THE RIGHT-OF-WAY AND ALL DISTURBED AREA5 AFTER CONSTRUCTION OPERATIONS ARE COMPLETED IN A PROPER MANNER TO AVOID PONDING OF WATER. THE CONTRACTOR SHALL RESEED AND MULCH ALL DISTURBED AREAS OUTSIDE OF PAVEMENT. SEEDING AND MULCHING SHALL BE DONE WITHIN 14 DAYS OF COMPLETION OF BACKFILL. • THE CONTRACTOR SHALL IMMEDIATELY RESTORE ALL MAIL BOXES, ROADWAY SIGNS, ETC., A5 SOON AS POSSIBLE. AT A MINIMUM THESE ITEMS SHALL BE REPLACED PRIOR TO COMPLETION OF THE WORK. WHEN THE ENGINEER DETERMINES THAT IT IS NECESSARY TO TEMPORARILY REMOVE A STOP SIGN, HE SHALL DIRECT THAT EITHER: (1) A TEMPORARY STOP BE INSTALLED; OR (2) THAT A FLAGMAN SHALL BE USED INSTEAD UNTIL THE PERMANENT STOP SIGN CAN BE REPLACED AT ITS ORIGINAL LOCATION. TI SEAL 9 r 028911 REV1510N5 �c Iry ov ROCKY ' CUNT R SHEET TITLE: PLANTERS OIL MILL FILL REMEDIATION COVER SHEET PROJECT #: POCLE CAD FILE: Planters-SP DATE: 07-07-201 1 SURVEYED BY: SEE NOTES DESIGNED BY: MDT DRAWN BY: mdt CHECKED BY: mdt SCALE: 1 " = 50' DRAWING #: D-541 2 SHEET NUMBER: I OF 2 SHEET CV NOTES: I . BOUNDARY AND TOPOGRAPHIC INFORMATION ON THIS PLAN TAKEN FROM A SURVEY PREPARED BY JOYNER KEENY, PLLC PLANNING AND LAND SURVEYING ENTITLED "BOUNDARY AND TOPOGRAPHIC MAP OF: PLANTERS OIL MILL SITE ROCKY MOUNT, NC" DATED 04/15/2010. 2. ALL CONSTRUCTION TO CONFORM AND COMPLY WITH CITY OF ROCKY MOUNT STANDARDS SPECIFICATIONS. 3. TOTAL DISTURBED AREA = 4.25 ACRES 4. CONSTRUCTION STAKING TO BE PROVIDED BY CITY FORCES. 5. CONTRACTOR SHALL PROVIDE SOURCE OF FILL MATERIAL TO OWNER WITH BID DOCUMENTS. SOURCE OF FILL MUST BE APPROVED PRIOR TO USE. APPROVAL WILL INVOLVE ANALYTICAL TESTING AT THE DISCRETION AND C05T OF THE CITY. G. FILL TO BE PLACED IN 12" LIFTS AND COMPACTED U51NG VIBRATORY DRUM ROLLER AS PRESCRIBED BY APPROVED 13ROWN5FIELD AGREEMENT. 7. TESTING OF COMPACTION AND FILL TH ICKNE55 WILL BE PER THE GUIDELINES OF THE BROWN5FIELD AGREEMENT AND WILL BE PAID FOR BY THE CITY. 8. VEGETATION TO BE ESTABLISHED BY HYDROSEED APPLICATION 9. FUTURE REMOVAL OF TEMPORARY SEDIMENTATION AND EROSION CONTROL MEASURES IS THE RESPONSIBILITY OF THE CONTRACTOR, THE C05T OF REMOVAL OF THESE MEASURES IS CONSIDERED INCIDENTAL TO THE COST OF THE MEASURE. CONSTRUCTION SEQUENCE JULY 201 1 OBTAIN SEDIMENTATION 4 EROSION CONTROL PERMIT AUGUST 201 1 REMOVE CHAIN UNK FENCING PER APPROVED REMOVAL METHOD LISTED IN BROWN51'IELD AGREEMENT INSTALL CONSTRUCTION ENTRANCE / EXIT, SILT FENCE AND ALL OTHER EROSION CONTROL DEVICES PER APPROVED SEDIMENTATION i EROSION CONTROL PLAN BEGIN GRADING OPERATIONS MAINTAIN EROSION CONTROL MEASURES DURING OPERATIONS TO ENSURE PROPER PERFORMANCE SEPTEMBER 2011 PREPARE SEEDBED FOR APPLICATION OF SEED BY HYDRAULIC SEEDING SEED ENTIRE LIMITS OF DISTURBANCE REMOVE SEDIMENT AND EROSION CONTROL MEA5URF5 AFTER VEGETATION HAS BEEN ESTABLISHED AND SITE HAS BEEN APPROVED BY NCDENR REPRESENTATIVE. SSMH TOP = 114.65' INV. IN (EAST) _ 107.05' INV. IN (SOUTH) = 106.45' INV. OUT 106,45' i ag Lo `0 83 s n z I ' a I � I(n I I � � 1 END OF PIPE j NOT LOCATED) 6^ pt E t 6° PIPE U) 0 CB TOP = 115.83, INV. = 114.20' SSMH ' TOP = 117.42' - INV. IN = 107.72' INV. OUT = 107.62' N 22°4651" E 68,15' TIE (1118 TO 3/4» 1PF) 24' RCP I X INV 112.79' PERMANENT AND TEMPORARY SEEDING SCHEDULE: FOR PERMANENT SEEDING: Outside Riparian Buffers Date 5eedTie Planting Rate Inside Riparian Buffers Seed Type Plantiing Pate Sept I - Oct 3) Tall Fescue 240 Ibs / acres 5witchgrass plus 15 Ibs / acre Rye Gram 40 Ibs / acre Nov I - Feb 28 Tall Fescue plus P 240 Ib acre s/ Switch rass plus 9 P 1 5 (Its acre / Winter Rye 50 Ill / acre Rye Grain 40 Its, / acre Mar I -May 31 Tall Fescue 240 IIns / acre 5witchgra55 plus 15 Ibs / acre German Millet 10Ill /acre June I -Aug 31 Tall Fescue plus 120 Ibs / acre 5witchgra5s plus 15 Ill / acre Browntop Millet or 35 Ill / acre German Millet 10 Ibs / acre Sorghum - Sudan Hybrid 25 Its / acre FOR TEMPORARY SEEDING: Outside Riparian Buffers Inside Riparian Buffers Date Seed Tyne Planting Rate Seed Type Planting Rate Sept I -Oct 31 German Millet 40 Its I acres 5witchgrass plus 15 Ibs / acre Rye Grain 40 Its, / acre Nov I - Feb 28 Rye Gram 120 Ibs / acre 5witchgras5 plus 15 Ibs / acre Rye Grain 40 Ibs / acre Mar I -May 31 Annual Lespedeza plus 50 Ibs / acre 5witchgra55 plus 15 Its I acre Rye Gram 120 Ibs / acre German Millet 10 Its / acre June I - Aug 31 German Millet 40 Ibs / acre 5witchgras5 plus 15 Its / acre German Millet 10 Ibis, / acre L� I _J ll�V IN (SOUTH) - 109.83' V. I lNOUT 109.63' I SSMH TOP = 114.88' T 11b° INV. IN - 708.38SHORT STREE' 2� INV. OUT = 108,28' VARIABLE L 7�:WIDTH R/-_-_W 8" TERRACOTA SANITARY SEINER LINE --� - _- ----- - 3D" VEHHEAD ELECTRIC and TELE HC E 394.58 _ r HAY BALES ARE NOT AN ACCEPTABLE ALTERNATIVE TO SILT FENCING. TOP AND BOTTOM STRAND SHALL BE 10 GAUGE MIN. NOTES: WIRE SHALL BE A MINIMUM OF 321 IN WIDTH AND SHALL HAVE A MINIMUM OF G LINE WIRE5 WITH 12" STAY SPACING. FILTER FABRIC SHALL BE A MINIMUM OF 3G" IN WIDTH, SHALL MEET THE REQUIREMENTS OF NCDOT 55R5 SECTION 105G FOR TYPE 3, CLA55 A FILTER FABRIC, AND SHALL BE FASTENED ADEQUATELY TO THE WIRE AS DIRECTED BY THE ENGINEER. STEEL POSTS SHALL BE 5'-0" IN HEIGHT AND BE OF THE SELF -FASTENER ANGLE STEEL TYPE. WOOD P05T5 ARE NOT ALLOWED FOR SILT FENCE SUPPORTS. ROCKY' r' - MIDDLE AND VERTICAL WIRES SHALL BE 12 1/2 GAUGE IMIN I O MAX. WITH WIRE I I MAX. WITHOUT WIRE) II 'M K-F FILTER FABRIC FILTER FABRIC COMPACTED FILL SYMBOL MOUNT TEMPORARY SEDIMENT (SILT) FENCE NMRTH `DEPARTMENTOF I ,� Al� G 6' CHAINLINK FENCE AROUND TER AND WITHIN PROPERTY LIMITS TO I -STORY BRICK BUILDING D4 N 8624 �i9 mr a �N 89 43'43" E 132.90' �0 6 6 nC47 (jXNCE PF Q ,,EXISTING FENCE ALONG D'S RENTAL, LLP 42 ^"" ED 'X' FOUND Nl 6' CHAIN LINK FENCE/ ,� xrrs!as '\ xrr53s END OF SE R ADJOINERTO REMAIN ^. t DB 1516, PG 219 CONCRETE xn4. i s SILT( FENCE INSTALLED APP OXIMATELY �' D Cn' -•� ,! -;r ' i• 7 xa4so I G a 0.5' INSIDE PROPERTLY LINE ALONG AREAS-115"� N C, WHERE FENCE 15 TO BE REMOVED (TYP) _ (Z' }.._ r`:::., :a ..• ,per . __.. •. x',y EXISTING G' CHAINLINK FENCE AROUND '� i'='"''r.�•'`7(r''r'''•;�3/4". xn4sr PERIMETER AND WITHIN PROPERTY LIMBS TO " F4 586°32'S3"W'' PF •;:. BE REMOVED. CUT PO5T5 AT EXISTING X114.41 I I G x11 x GROUND LEVEL FOR REMOVAL. EXISTING x114.B2 xir4so �i 'n4az 97.07' 1i4s9 i 1rX , GROUND NOT TO BE DISTURBED. X115.02 / x7r4.74� x7/366 .i X115.21 X7 B6 3' �l/ a '15.02 /// 774.53X 115 / X114.61 SILT FENCE INSTALLED APPROXIMATELY 1139s 20 IW OE X 50' LONG X G" THICK TEMPORARY / 0.5' INSIDE EXISTING FENCE ALONG x'� & 71l 342 J , a 1o` GRAVEL CONSTRUCTION ENTRANCE / EXIT. AREAS WHERE FENCE 15 TO REMAIN C r) p V X1r349 yq.gg CONTRACTOR TO ENTRANCE DURING OPERATIONS / 11:f x71390 113.86 SO_ 1'OI" 4 EXTEN51ON OF FABRIC AND WIRE INTO FABRIC \� MH / J Tor=1 INV. IN = 108.21' INV. OUT = 108.11' s` o 'P � �� j% � � �a -7 / J VG FENCE ALONG �ER x0 REMAIN .; .473.19 �\ '16 '777- _. o. l�tJl..i� JL MOUNT DEPARTMENT OF 0/ TOP = 711.37' INV. 1N (15') - 06.47' INV. OUT (2 = 106.72' 01 �� GO END OF PIPE NOT LOCATED x r3 s X}1348 X713.B6 \ ,.� " %p TO ENSURE PERFORMANCE OF MEASURE. �� 774\ � x77373 f7d29 3%4� � �Q 4540 -' - X X14.1s 1PF 117 U X114.19 G -Xfi3.72 x114.08 774-„` Xf13.71xj�, 5 x114.14 B x114.61 xr14.8B-115-x198 I , j�-- .._\ TOP = 112.21' XIi4.57 X11346 001. INV IN (15') = 106, 71'C8 xX7 X194.35 X114. 74 x115B5xr16.38 .63 CONTRACTOR TO LEAVE EXISTING GROUND UNDISTURBED AND INSTALL A MINIMUM OF 7S� X114.03 v"Ne ra 'fd'"i%„�X (�'�� V. 0II7('T5") =-70-2 f' r a12" OF CLEAN MATERIAL ACROSS ENTIRE SITE. THE PROPOSED CONTOURS ON THIS x114.89 a 82 �\ x7f5 _GRADING PLAN ARE TO BE USED AS GUIDELINES TO ESTABLISH POSITIVE DRAINAGE X115.14 ACROSS THE SITE. ON51TE INSPECTION WILL BE PROVIDED BY THE OWNER TO VERIFY X 115.14 AND CONFIRM THE MINIMUM THICKNESS OF THE FILL LAYER AND OVERALL DRAINAGE y x/ 6.3E 1, BEHAVIOR OF THE GRADED SITE. FIELD ADJUSTMENTS ARE TO BE APPROVED BY THE x114.55 rn `s'ENGINEER IN ACCORDANCE WITH THE BROWN5PIELD AGREEMENT FOR THI5 SITE. X 114.83 \ X77508 \J 115.08 \ if .73 --I i xr15.84 `2 /TY OF ROCKY \1 SILT FENCE INSTALLED APPROXIMATELY 0.5' x775. 8 -AIDEPROPERTLYLINEALONGAREAS ,� '��-•� xn53s 71 ix NC Municipal Cc WHERE FENCE IS TO BE REMOVED CfYP\ � ydtid-08 X11513 pB 1500, PC i xn .zi \ 5/ 7.365 Act XV76.14 X7 6.24 j��-- --� � 3 X11537 1 7 X7fS3r 176^-- X776.57 X116.59 X115.82 ---�'115- X715�75 xti 44 _. -Q 16 _ xi14.23 X7 6.38 CB x71549 X71529 /'--'X774.77 X114.37 X114.65 TOP 115.74' 1B �'Xtt395 X914.18 XH4.14 INV 0 T (6') = 114.34' C X17531 NZ i EXISTING G' CHAINLINK FENCE AROUND x115.16 s.PERIMETERAND WITHIN PROPERTY LIMITS TO �I17 \ X114.51 x1/4.40 BE REMOVED. CUT P05T5 AT EXISTING AAII��LLLL�� GROUND LEVEL FOR REMOVAL. EXISTING QI5' NS DE16((STV APPRO IMATAREAS x114.43 GROUND NOT TO BE DISTURBED. + WHERE FENCE 15 TO REMAIN CTYfY,. X114. y' 16�4815> .,,e- 2"-3" COARSE AGGREGRATE - 50' MIN. -M•�` �:?,�- � ,r. ,� ,.may 1,.. ` ` x 17f3 J , �p'� �• ''�'a 20' MIN. MIN. GRAVEL CONSTRUCTION ENTRANCE X 113.94 ' X17Z47 uri¢ea CONSTRUCTION SPECIFICATIONS I. Clear the entrance and exit area of all vegetation, roots, and other objectionable material and properly grade it. 2. Place the gravel to the specific grade and dimensions shown on the plans, and smooth it. 3. Provide drainage to carry water to a sediment trap or other suitable outlet. 4. Use 3eotextile fabric to Improve stability of the foundation in locations subject to seepage or high water table. MAINTENANCE Maintain the gravel pad in a condition to prevent mu or sediment from leaven the construction site. d g This may require periodic top dressing with 2-inch stone. After each rainfall, inspect any structure used to trap sediment and clean It out as necessary. Immediately remove all objectionable materials spilled, washed, or tracked onto public roadways. WASHING If conditions at the site are such that most of the mud and sediment are not removed by vehicles traveling over the gravel, the tires should be washed. Washing should be done on an area stabilized with crushed stone that drains into a sediment trap or other suitable disposal area. A wash rack may also be used to make washing more convenient and effective. DATE: JUNE 201 1 1 STANDARD #: 3.17 (mod; 4s7 xn4.24 xr1a.12 xu4.3s END OF PIPE \NOT FOUND \ x7t3.48 \ r JNT, SILT FENCE WILL BE IN5TALLED AT THE LIMITS DISTURBANCE AND jw Xr1a79 \ x114165 7.. 4,� 7Fat% REPRESENTS A TOTAL DISTURBED AREA EN x114.71 \ 07 x 1 .4< OF 4.25 ACRES xtr44o _ i, / 713.67 CONCRETE WALL �xr tx x x 2' HIGH W/ WATER "� < PIPES 80TTOM xt t.s3 IN X774.23 X713.911373 / X1137B �o SSMH C ?� \ TOP = 1I3.35' x714. x114.31 ._.._-- �_ INV. IN = 709.55' X114.29 Xt1369 INV.. OUT = 109.45' --ram.-- Xf14.4o XI D4 PLANTERS STREET X114.30 EXISTING G' CHAINLINK FENCE AROUND PERIMETER AND WITHIN PROPERTY LIMITS TO X114..51 xr74.55 BE REMOVED. CUT P05T5 AT EX15TING LEVEL REMOVAL. EXISTING X114.5s GROUND FOR ir3.'40 xrr4.2z GROUND NOT TO BE DISTURBED. y2 xrr4 ss �,6` X//4,43 X114.50 17X•X11384 9 3/4' _0 6' CHA/A`oLyp FENCE 1 114.03 113zo "px. %PF xi 1rrr�� EXISTING FENCE ALONG s � I t .sB X714.35 RAILROAD TO REMAIN X714.00 /--' \ xt74.43 Xf14.64 \ X714.3/ x11 . Xll .40 �S X X114.78 \` 916.30 - 114.31 X 114.15 / \ X fIA59 `�10.51 Z o _� -atert6 ss - x t . W 1086.08' 1h_ ' x sz R� 198 x716.25 �16---\a I \ .----.-"------. x776.14�11 -'-,- =__ �-----.� ='_--�-'-_ -_".-- � --'-7 X116.35 6 X715.98 - Li3� _ -- 6``<CHAIN LINK FENC£ xft6.o�_ x116.66 76 '' 716- \ _..--�715 lNV. = 112.9D' Xn541 \ 15. 7jSX7rs 1 --- --- .1 v ------._'•176 776----_. -14.79 1" - '^71SX1gg,"--CAL -.-___ _-..-- X915.35 115.03)t� 4.671PF s -CAL RAILROAD TRACK � � ~� N 845027" W 119J. xr14.Bs - PK NAIL SET #18 92 (#4 TO X714.s3 NAD795,02� 979 usft CST #J8) X114.46 E- 2, 357,585166 usft 07 R/W /i RAILROAD Q X114.33 INV. = 109.23' - ELEV- 11789 usft ' (SEE NOTE 5) R/W - �`3� R/�/ R/W INV. = 109.11' U R/W INV. = 108.82' END OF PIPE a NOT LOCATED - PK NAIL SET #4 NAD '8312007 N- 794,91Z766 usft E- 2,358,772.259 usft ELEV- 11553 usft (SEE NOTE 5) I � i 8 N CID z SSMH TOP = 114.12' iNV. OUT = 110.02' N 47 33'03" W I07i i' TIE (14 TO 1 " IPF) 50 25' 0 50 1Do 150 GRAPHIC SCALE: 1"= 50 BEFORE YOU DIG, CALL NORTH CAROLINA 7NE CALL CENTER www.ncocc.org € - SEAL a ' 028911 - a - 3 A �4�y�KNGINEE�AaS i777'� ...... IIII 1' I I REVISIONS C ITV OF ROCKY I MOUNT NORTH CAROLINA SHEET TITLE: PLANTERS OIL MILL FILL REMEDIATION SEDIMENTATION, EROSION CONTROL AND GRADING PLAN PROJECT #: POCLE CAD FILE: Planters-SP DATE: 07-07-201 1 SURVEYED BY: SEE NOTES DESIGNED BY: MDT DRAWN BY: milt CHECKED BY: milt SCALE: III= 50' DRAWING #: D-541 2 SHEET NUMBER: 2 OF 2 SHEET GP APPENDIX D Photographs of Cleanup Activities Photograph 1: Pre -Cap Site Conditions Photograph 2: Dumping & Spreading Cap Soil I 4%� Aad Q Hickman 3334 Hillsborough Street I Planter's Oil Mill I A Pao�aao �lolRhlll�[n16II Raleigh, North Carolina 27607 1006 Cokey Road, Rocky Mount Photograph 3: Spreading Cap Soil Photograph 4: Spreading Cap Soil IAa�{ Q Hickman 3334 Hillsborough Street I Planter's Oil Mill I A Pao�aao �lolRhlll�[n16Raleigh, North Carolina 27607 1006 Cokey Road, Rocky Mount Photograph 5: Cap Soil Partially Placed and Compacted Photograph 6: Cap Soil Partially Placed and Compacted IAa�{ Q u1r]�mai1 3334 Hillsborough Street I Planter's Oil Mill I A Pao�aueo111�1o1Rv��1�[n16llN Raleigh, North Carolina 27607 1006 Cokey Road, Rocky Mount Photograph 7: Geotechnical Testing Photograph 8: Site Conditions After Seeding 124%,501IR l Q uickm 3334 Hillsborough Street Planter's Oil Mill A Pao�aao YR11all�T o^ Raleigh, North Carolina 27607 1006 Cokey Road, Rocky Mount APPENDIX E Geotechnical Certification of Cap Compaction and Thickness Geotechnical and Construction Materials Testing Services September 21, City of Rocky Mount Department of Engineering PO Box 1180 Rocky Mount, North Carolina 27802 Attention: Mr. Michael Tolson Reference: Summary of Testing Services Planters Oil Mill Rocky Mount, North Carolina GeoTechnologies Project No.: 1-11-0488-CA Mr. Tolson: GeoTechnologies, Inc. has completed the construction testing services on the Planters Oil Mill project located in Rocky Mount, North Carolina. It's our understanding the project requirements included placing 12 inches of soil material across the entire site. Our services included performing in -place soil density testing and depth checks. Nine in -place density tests were performed. All tests achieved the required compaction of 95 percent (ASTM D-698). The depth of the in -place material ranged from 12 inches to 13.5 inches. Based on our results, the material placed meets or exceeds the required compaction and depth. Attached are the compaction results of our testing and a location sketch showing approximate test and depth locations. GeoTechnologies appreciates the opportunity to have provided you with our services on this project. Please contact us if you should have questions regarding this report or if we may be of further assistance. Very Truly Yours, GeoTechnologies, Inc. Michael K. Morton Construction Services Manager Edward B. Hearn, P.E. NC Registration No: 9520 3200 Wellington Ct., Ste. 108 m Raleigh, NC 27615 m Phone 919-954-1514 o Fax 919-954-1428 ^ www.geotechpa.com - License No. C-0894 z z o 0 o IL O7 c U z c i s wo c O U O J 0 0 0 0 0 0 aci aCLi aci 0 uc) ac) Q Q Q a) E a) E N iT (L) li. a) E ) E O O O O O O a) a) a) a) a) a) w OO O U a)O U t t t O — O n 00 O) CD O{ (IO) O O) a a) - O O O) T T O U a as a O c U 20 ' rn rn rn rn rn rn rn rn rn a C- -o E a) E� a) 0 co co m rn rn rn V) W) `m _ w c �� v v v 4 v v c Q'o 0 pgU m (n ❑ rn rn rn rn rn rn rn 0 0 ❑ o 0 0 U c a) w N w w O 00 w O O w w :3 w LO n r- O O N O) N y M V V � W L6 � O a0 a ` )) g U H T O a7 O N O a) ❑ Z' ❑ a) O O O O 00 M N a) ❑ U a3 O m m m m m Q m N m N m N m N N N N N N O N N N N N N N N ❑ a) 0 0 � 0 z- co 0 zz 0 0 0 � 0 0 co 0 O Z i W o 0) yU Z) > U) o o� a) .N a 0 C w � 0 a o � U � U o m rw� O N O) Q� N E � o •o U g� o� = o O U � N N J � N U M N= U cl c L U a) E O o �U a) 0 � m m Z o U) m Q U J 00 a.=_o c a� —o U o) � oQ� t _ r O)CO a) 'O a) cU •c � .o 'o �U)U) ca o Fn Zi O c c — 0019 � N N N ❑ N a) 3 F- F N O Lo m� N co O6LLOO 0 H cl a) U c O Q An O 2 5. Q to 0 Q a� U U a) H a) E m Z M r r a) 0) a3 a 61 0 U 6 z a) N C m V J LO CD ti N 3200 Wellington Court, Suite 108 Raleigh, North Carolina 27615 Phone 919-954-1514 OIL MILL -- LOCATION JOB NO. m.�. Nt- i- tl-o�l�S3- cA DATE OWNER TTME TEMP PRESENT AT SITE TO e Ca l;!'QX , Q Q ( 0 -U � THE FOLLOWING WAS NOTED: f J 3 6� U O O n o COPIES TO FIELD REPORT - ATTACHMENT SIGNED