17047 REEP Additional Waste Disposal Assessment Report 20180507

Via Email
May 7, 2018

NC DEQ – Brownfields Section
1646 Mail Service Center Raleigh, NC 27699-1646 Attn: Mr. Bill Schmithorst, PG
Subject: Additional Waste Disposal Assessment Report
REEP-LRC Project 1
1900 Continental Boulevard Charlotte, North Carolina Brownfields Project No. 17047-13-60
H&H Job No. LRC-006

Dear Bill:
Enclosed is the Additional Waste Disposal Assessment Report for the REEP-LRC Project 1 site
located at 1900 Continental Boulevard in Charlotte North Carolina (Brownfields Project No.
17047-13-60) for your review and approval.
Thank you for your assistance with this project. Should you have any questions or need additional information, please do not hesitate to call us at [phone].

Very truly yours, Hart & Hickman, PC
Matt Bramblett, PE
Principal
Attachment Cc: Ms. Lori Hinnant, K&L Gates (via email) Mr. Michael Cain, Foundry Commercial (via email)
Mr. Jason Oriol, Foundry Commercial (via email)
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Additional Waste Disposal Assessment Report
REEP-LRC Project 1 Site
Charlotte, North Carolina
H&H Job No. LRC-006
Table of Contents
1.0 Introduction ............................................................................................................................ 1
2.0 Waste Removal and Assessment Activities .......................................................................... 2
2.1 Waste Disposal Area ......................................................................................................... 2
2.2 Groundwater Sampling ..................................................................................................... 3
2.3 Asbestos Disposal Areas ................................................................................................... 4
2.4 Quality Assurance/Quality Control................................................................................... 5
3.0 Results ..................................................................................................................................... 7
3.1 Waste Disposal Area Soil Sample Results ........................................................................ 7
3.2 Groundwater Sample Results ............................................................................................ 7
3.3 Asbestos Soil Confirmation Sample Results .................................................................... 8
4.0 Summary and Conclusions.................................................................................................... 9

List of Tables
Table 1 Summary of Waste and Confirmation Soil Sample Analytical Results.
Table 2 Summary of Groundwater Analytical Results
List of Figures
Figure 1 Site Location Map
Figure 2 Soil and Groundwater Sample Location Map
Figure 3 Asbestos Soil Sample Location Map
List of Appendices
Appendix A Photographs
Appendix B Laboratory Analytical Reports
Appendix C Waste Disposal Documentation
Appendix D Well Construction Details
Appendix E Vapor Intrusion Risk Calculator
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Additional Waste Disposal Assessment Report
REEP-LRC Project 1 Site
Charlotte, North Carolina
H&H Job No. LRC-006
1.0 Introduction

On behalf of LRC-Patriot, LLC, Hart & Hickman, PC (H&H) is providing this Additional Waste
Disposal Assessment Report for the REEP-LRC Project 1 site located at 1900 Continental
Boulevard (previously referred to as 1700 Continental Blvd) in Charlotte, Mecklenburg County,
North Carolina (Site or subject Site). A site location map is provided as Figure 1. The Site is
comprised of approximately 27 acres of undeveloped wooded land. Redevelopment plans include
clearing the wooded area, removing concrete foundations and other remnants of former Site
operations, grading the Site; and construction of an approximate 360,000 square foot (sq ft)
warehouse, parking area, and a storm water retention pond.

The site is enrolled in the North Carolina Department of Environmental Quality (DEQ)
Brownfields Program (Brownfields Project ID 17047-13-60). The Brownfields Program requested
that the property owner conduct additional assessment and waste removal activities at the site. The
waste removal and additional assessment activities generally included the removal of waste
materials generated during exploratory excavation in the former waste disposal area, the collection
of soil and groundwater samples, and the collection of confirmation soil samples in the former
asbestos disposal areas. During collection of the confirmation soil sample in the asbestos disposal
area located in the central portion of the site, H&H personnel observed the presence of additional
asbestos material (transite) below the leaf layer and within the topsoil layer. As such, H&H also
conducted additional transite removal from this portion of the site prior to collection of the
confirmation soil sample. Details of the additional transite material removal and disposal are also
included in this report.

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2.0 Waste Removal and Assessment Activities

The waste removal and sampling activities were conducted in accordance with the approved Waste
Disposal Assessment Work Plan (Work Plan) dated February 7, 2018, in accordance with
applicable guidelines, and as described below. The work plan was approved in an email from Mr.
Bill Schmithorst, PG with DEQ dated February 8, 2018.

2.1 Waste Disposal Area

As indicated in H&H’s September 28, 2017 Waste, Drums, and ACM Removal Report, H&H
suspected that at least one drum remained buried following previous excavation activities
conducted in the southern portion of the Site. On February 21, 2018, H&H’s contractor Evo
Corporation (Evo) excavated in the vicinity of the suspected drum to recover and dispose of the
drum (if present) and conducted exploratory excavation activities in the vicinity of a GPR anomaly
identified and discussed in the December 26, 2017 GPR Survey Report.

The result of the excavation activities did not uncover additional drums in the suspected drum
location or in the GPR anomaly area. In the area of the suspected drum, a drum lid and
approximately five 5-gallon metal pails were uncovered. The pails were deteriorated and did not
contain free liquids. The drum lid, pails, and soil overburden (which primarily consisted of
previously identified burned/melted rubber and soil) were direct loaded into a lined front-end
loader and transported to a lined roll-off container staged in a paved area of the Site. Following
excavation activities, H&H collected a sample (Base-2) from below the area of the 5-gallon pails
and drum lid and submitted the sample to Prism Laboratories Inc. (Prism) under standard chain-
of-custody protocol for laboratory analysis of volatile organic compounds (VOCs) by EPA Method
8260, semi-volatile organic compounds (SVOCs) by EPA Method 8270, and Hazardous Substance
List (HSL) metals by EPA Methods 6020/7470/7441. The location of sample Base-2 is shown on
Figure 2 and the results are discussed in Section 3.0. Photographs of the exploratory excavation
are shown in Appendix A.

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In the area of the GPR anomaly, H&H encountered an ash-like material at a depth of approximately
2 ft to 4 ft bgs, which was the approximate depth of the previously identified GPR anomaly. This
ash-material had not been previously identified at the site. As such, H&H collected and submitted
a sample of the ash-like material (ASH-1) to Prism for laboratory analysis of VOCs by EPA
Method 8260, semi-volatile SVOCs by EPA Method 8270, and HSL metals by EPA Methods
6020/7470/7441. H&H continued the excavation in the area of the GPR anomaly to a total depth
of approximately 6 ft, and no other previously unidentified waste material or drums were observed.
A base sample (Base-3) was collected from the bottom of the GPR anomaly excavation and
submitted to Prism for laboratory analysis of VOCs by EPA Method 8260, semi-volatile SVOCs
by EPA Method 8270, and HSL metals by EPA Methods 6020/7470/7441. The locations of
samples Ash-2 and Base-3 are shown on Figure 2 and the laboratory analytical results are discussed
in Section 3.0. The ash-like material and overburden were direct loaded into a lined front-end
loader and transported to a lined roll-off container staged in a paved area of the Site. Photographs
of the GPR anomaly excavation are shown in Appendix A.

Following excavation activities, H&H sampled the roll-off box materials for waste
characterization purposes. The sample (Soil-1) was submitted for laboratory analysis of toxicity
characteristic leaching procedure (TCLP) VOCs, TCLP SVOCs, and TCLP RCRA metals.
Laboratory analytical results of the waste characterization sample did not indicate the presence of
compounds above the characteristically hazardous waste thresholds. As such, the material was
disposed at a permitted facility in accordance with applicable guidelines. A total of approximately
2.4 tons of material was disposed of off-site. The laboratory analytical data for the waste
characterization sample are included in Appendix B, and the waste disposal manifest is included
in Appendix C.

2.2 Groundwater Sampling

On March 14, 2018, H&H collected two groundwater samples in accordance the approved Work
Plan. One groundwater sample (TMW-3) was collected in the vicinity of the southern disposal
area and one groundwater sample (TMW-4) was collected in the vicinity of previous subsurface
soil boring SB-8. The groundwater samples were collected by installing a temporary monitoring
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well at each location using a track mounted direct push technology (DPT) rig. The locations of
temporary monitoring wells are shown on Figure 2.

The temporary monitoring wells were constructed of 1-inch diameter PVC with 10 ft of well
prepack screen set to bracket the water table and 1-inch diameter PVC well casing to the ground
surface. Well construction details are provided in Appendix D. Following installation, the wells
were allowed to equilibrate to static conditions, and the depth to water was measured in each well.
The depths to water in TMW-2 and TMW-3 were measured to be approximately 23 ft. Following
depth to water measurements, the wells were developed by removing a minimum of 3 to 5 well
volumes and until field parameters stabilized (pH ± 0.1 SU and conductivity varies no more than
5%).

After well development, groundwater samples were collected by low flow/low stress purging
techniques using a peristaltic pump and dedicated polyethylene tubing. During purging, H&H
utilized a water quality meter to collect measurements of pH, temperature, dissolved oxygen,
oxidation reduction potential, turbidity, and specific conductivity. Purging was considered
complete when the parameters stabilize (pH ± 0.1 SU and conductivity varies no more than 5%).

Once groundwater parameters stabilized, the groundwater sample was collected directly into
laboratory supplied sample containers using the “soda straw” method. The sample containers were
then labeled with the sample identification, date, and requested analysis, and placed in an iced
laboratory supplied cooler. Samples were submitted to Prism Laboratories under standard chain
of custody protocols for analysis of VOCs by EPA Method 8260B. Groundwater sample results
are discussed in Section 3.0.

2.3 Asbestos Disposal Areas

On February 20, 2018, H&H collected soil samples in the asbestos containing material (ACM)
removal areas located in the two northern portions of the Site (Area-1 and Area-2) to determine if
asbestos impacts were present in soil following removal activities conducted in March 2016. As
noted in Section 1.0, during sampling in the central portion of the site, additional transite was
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observed below the leaf and topsoil layers. As such, a sample was not collected at that time to
allow for removal of the additional transite material prior to sampling. A brief description of the
additional transite removal is included below.

On March 21 through 23, 2018, H&H contracted with Evo, in conjunction with a licensed asbestos
abatement contractor, to remove the additional transite material in the central portion of the site.
The transite and soil mixture was removed via a mini excavator and direct loaded into a lined front-
end loader for transport to a lined roll-off container. Once the roll-offs were filled, they were
wrapped in poly-sheeting and sealed for transportation and disposal at a permitted facility.
Approximately 52 tons of transite and soil mixture were removed from the site. Waste disposal
manifests for the transite and soil mixture are included in Appendix C. Following excavation, a
confirmation soil sample was collected from the central transite disposal area (Area-3) in
accordance with the approved Work Plan and submitted to EMSL Analytical, Inc. (EMSL) for
asbestos analysis in soil by the 400 count EPA 600 Method. The locations of the asbestos
confirmation soil samples (Area-1, Area-2, and Area-3) are shown on Figure 3.

2.4 Quality Assurance/Quality Control

H&H conducted the assessment activities in accordance with the QA/QC procedures described in
the approved work plan and as discussed below. The QA/QC procedures included utilizing field
procedures outlined in the NC DEQ Inactive Hazardous Sites Branch (IHSB) Guidance (October
2015), US EPA Region IV Science and Ecosystem Support Division (SESD) protocols, and the
collection of QA/QC samples. The QA/QC samples included laboratory analysis of a trip blank
sample for VOCs by EPA Method 8260 and collection of one duplicate soil sample and one
duplicate groundwater sample. The duplicate soil sample was submitted for laboratory analysis
of VOCs by EPA Method 8260B, SVOCs by EPA Method 8270D, and HSL metals by EPA
Methods 6020/7470/7441 and the duplicate groundwater sample was submitted for laboratory
analysis of VOCs by EPA Method 8260B. A brief summary of the results of the QA/QC samples
is provided below.

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• The laboratory analytical results of Trip Blank-1 did not indicate the presence of
compounds above laboratory detection limits. This result indicates that additional VOC
mass was not introduced to the samples during sampling activities or in transit to the
laboratory.

• Blind duplicate samples were collected from soil sample Base-3 and TMW-2. The samples
were collected concurrently with their respective parent samples and were submitted to the
laboratory without a time entry to prevent the laboratory from identifying the parent
sample. The laboratory analytical result of duplicate samples did not indicate a significant
deviation in concentrations as compared to the parent samples. These results indicate good
laboratory analytical repeatability.

The laboratory analytical results for the duplicate samples are summarized on Table 1 and Table
2, and the laboratory report is included in Appendix B.

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3.0 Results

3.1 Waste Disposal Area Soil Sample Results

Laboratory analytical results of the soil samples collected from the waste disposal area during the
March 2018 assessment activities did not identify VOCs, SVOCs, or metals above Inactive
Hazardous Sites Branch (IHSB) Industrial Preliminary Soil Remedial Goals (PSRGs) and/or were
within published background ranges except for the concentration of arsenic (13 mg/kg) detected
in sample Ash-1 which was above the IHSB Industrial PSRG of 3.0 mg/kg. Although this
concentration of arsenic is within published background ranges, it appears to be elevated as
compared to other arsenic concentrations detected at the site. The location of the potentially
elevated arsenic is a fill location for the proposed building. A summary of the soil laboratory
analytical data is provided in Table 1. The laboratory report and chain of custody form are provided
in Appendix B.

3.2 Groundwater Sample Results

The laboratory analytical results of the groundwater samples indicate the presence of low levels of
tetrachloroethylene (PCE) in and trichloroethylene (TCE) in TMW-3 (4.2 µg/L and 16 µg/L) and
TMW-4 (2.6 µg/L and 8.3 µg/L) slightly above their North Carolina Administrative Code 15A 2L
Groundwater Standards (2L Standards) of 0.7 µg/L and 3 µg/L. In addition, the concentration of
TCE detected in TMW-3 and TMW-4 was above the Division of Waste Management (DWM)
Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) of 1.0 µg/L.

Other VOCs were detected above laboratory reporting limits in the groundwater samples collected,
but the concentrations detected were below applicable 2L Standards and DWM Non-Residential
GWSLs. The laboratory analytical results for the groundwater samples are included in Table 2.
The laboratory report and chain of custody form are provided in Appendix B.

To evaluate potential vapor intrusion risks associated with the groundwater concentrations
detected in TMW-3 and TMW-4, H&H utilized DEQ’s Vapor Intrusion Risk Calculator (February
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2018) to calculate the Lifetime Incremental Cancer Risk (LICR) and Hazard Quotient (HQ)
associated with the groundwater concentrations detected. The risk calculations indicate that the
groundwater sample concentrations due not exceed the thresholds of a LICR 1 x 10-4 and HQ of
1.0. Copies of the risk calculator results are included as Appendix E.

To further evaluate the potential vapor intrusion risk associated with the site, H&H also utilized
the most recent version of the DEQ Risk Calculator (February 2018) to reevaluate the previous
soil gas concentrations detected in VMP-7 and VMP-8, which were located in the southern portion
of the proposed warehouse building. The prior soil gas concentrations were within acceptable risk
levels as presented in H&H’s Brownfields Assessment Report dated October 27, 2017. Using the
most recent version of the risk calculator, the results for VMP-7 indicate a LICR of 9.1 x 10-7 and
HQ of 0.25. The results of the risk calculation for VMP-8 indicate a LICR of 2.0 x 10-6 and HQ
of 0.58. Consistent with the previous vapor intrusion evaluation, the risk calculation values for
SGP-7 and SGP-8 do not exceed actionable levels as defined by NC DEQ. Copies of the updated
risk calculator results for VMP-7 and VMP-8 are also included in Appendix E.

3.3 Asbestos Soil Confirmation Sample Results

Laboratory analytical results for the asbestos soil confirmation samples from three locations did
not contain detectable levels of asbestos. The laboratory report and chain of custody form are
included in Appendix B. The results indicate the asbestos removal actions were effective in
removing the discarded ACMs.

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4.0 Summary and Conclusions

H&H has conducted additional assessment and waste disposal activities at the REEP-LRC Project-
1 Site (Brownfields Project ID 17047-13-60). The additional assessment and waste disposal
activities were conducted in accordance with the DEQ approved February 7, 2018 Work Plan for
Additional Waste Disposal Assessment. The waste removal and additional assessment activities
generally included the removal of waste materials generated during exploratory excavation in the
former waste disposal area, the collection of soil and groundwater samples, and the collection of
confirmation soil samples in the former asbestos disposal areas. In addition, H&H conducted
removal of additional transite material discovered in the central portion of the site during
confirmation soil sampling activities.

Waste Disposal Area
On February 21, 2018, H&H collected three soil samples from the former waste disposal area. One
soil sample was collected from below the suspected drum location (Base-2); one soil sample was
collected from below the GPR anomaly (Base-3); and one soil sample was collected from an ash-
like material (Ash-1) uncovered during excavation in the GPR anomaly area. No drums or liquids
were observed during the excavation activities. Approximately 2.4 tons of overburden soil and
waste materials (including approximately five deteriorated 5-gallon metal pails, a drum lid, ash-
like material, apparent melted tire rubber, and soil) were sampled for waste characterization
purposes and disposed off-site.

Laboratory analytical results of the soil samples collected from the waste disposal area did not
indicate the presence of VOCs, SVOCs, and metals above IHSB Industrial PSRGs and/or were
within published background ranges except for the concentration of arsenic (13 mg/kg) detected
in Ash-1. This concentration is above the IHSB Industrial PSRG of 3.0 mg/kg. Although this
concentration of arsenic is within published background ranges, it appears to be elevated compared
to other arsenic concentrations detected at the site. The location of the potential elevated arsenic
is a fill location for the proposed warehouse building.

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Groundwater Sampling
On March 14, 2017 H&H installed and sampled two additional temporary monitoring wells at the
site in accordance with the approved Work Plan. One temporary monitoring well was installed
downgradient of the waste disposal area (TMW-3), and one temporary monitoring well (TMW-4)
was installed in the vicinity of former soil gas sample VMP-8.

The laboratory analytical results of the groundwater samples indicated the presence of low levels
of PCE and TCE slightly above 2L Standards and DWM Non-Residential GWSLs. To evaluate
potential vapor intrusion risks associated with the groundwater concentrations detected in TMW-
3 and TMW-4, H&H utilized DEQ’s Vapor Intrusion Risk Calculator (February 2018). The result
of the risk calculation indicated that the LICR for each sample were below 1 x 10-4 and the HQ
for each sample was below 1.0.

To further evaluate the potential vapor intrusion risk associated with the site, H&H also utilized
the most recent version DEQ Risk Calculator to reevaluate the soil gas concentrations previously
detected in SGP-7 and SGP-8 (which were previously reported to be below acceptable risk
thresholds). The results of the risk calculation for VMP-7 indicate a LICR of 9.1 x 10-7 and HQ
of 0.25. The results of the risk calculation for VMP-8 indicate a LICR of 2.0 x 10-6 and HQ of
0.58. Consistent with the previous vapor intrusion evaluation, the risk calculation values for SGP-
7 and SGP-8 do not exceed actionable levels as defined by NC DEQ.

Based on the results of the groundwater and soil gas sampling and proposed industrial use of the
site, potential vapor intrusion levels do not pose a vapor intrusion risk beyond acceptable levels as
defined by DEQ. Therefore, additional vapor intrusion sampling and mitigation are not warranted
for the proposed warehouse building.

Former ACM Areas
On February 20, 2018, H&H collected soil samples in ACM removal areas located in the two
northern portions of the Site to determine if asbestos impacts were present in soil following
removal activities conducted in March 2016. During sampling in the central portion of the site,
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additional transite was observed below a layer of leaves and within topsoil. As such, additional
transite material was removed prior to sampling.

On March 21 through 23, 2018, H&H contracted with Evo, in conjunction with a licensed asbestos
abatement contractor, to remove the additional transite material. Approximately 52 tons of transite
and soil mixture were removed from central area of the Site. Following excavation, the
confirmation soil sample was collected.

Laboratory analytical results of the asbestos soil confirmation samples did not contain detectable
levels of asbestos. The results indicate the asbestos removal actions were effective in removing
the discarded ACMs.

Table 1
Summary of Waste and Confirmation Soil Analytical Results
REEP-LRC Project 1
1900 Continental Boulevard
Charlotte, North Carolina
H&H Job No. LRC-006
Sample ID Base-2 Base-3 Dup-1
(Base-3)Ash-1
Sample Depth (ft bgs)
2/21/2018 2/21/2018 2/21/2018 2/21/2018 PSRG Industrial1
VOCs (8260) (mg/kg)1,1-Dichloroethane 0.013 <0.0062 <0.0075 <0.010 17Acetone0.12 <0.025 <0.030 0.084 140,000Benzene0.17 <0.0037 <0.0045 <0.0063 5.4cis-1,2-Dichloroethylene 0.027 <0.0062 <0.0075 <0.010 470Cyclohexane9.0 <0.0062 <0.0075 <0.010 5,800Ethylbenzene4.9 <0.0062 <0.0075 <0.021 27
Isopropylbenzene (cumene)0.0085 J <0.012 <0.015 <0.021 2,100
Methocyclohexane 0.12 <0.0062 <0.0075 <0.010 NE
Methyl Isobutyl Ketone <0.011 <0.012 <0.015 0.013 J 30,000Tetrachloroethylene<0.011 <0.012 <0.15 0.010 J 82Toluene0.092 <0.0062 <0.0075 <0.010 9,700Trichloroethylene<0.0057 <0.0062 <0.0075 0.0056 J 4.0Vinyl chloride 0.0049 J <0.012 <0.015 <0.021 1.7Xylenes, Total 15 <0.019 <0.022 <0.031 530SVOCs (8270) (mg/kg)
N-Nitrosodiphenylamine 0.75 <0.049 <0.053 <0.042 470Pyrene<0.42 <0.049 <0.053 0.21 J 4,500HSL Metals (6020/7441/7490)
(mg/kg)Range
(mg/kg)
Mean
(mg/kg)
Antimony 0.63 B 0.67 B, J 0.56 B, J 0.53 B, J 93 <1.0-8.8 0.76Arsenic1.8 J 1.5 J 1.5 J 13 3.0 1-18 4.8Beryllium1.7 2.8 2.5 0.35 470 ND-2.0 0.11
Cadmium 0.11 J 0.052 J 0.047 J 5.0 200 1.0-10 4.30
Chromium, Total 3.4 B 76 B 65 B 35 B 6.5 7.0-300 65
Copper 41 B 59 B 51 B 18 B 9,300 3.0-100 34
Lead 16 22 18 31 800 ND - 50 16
Manganese 320 900 670 160 5,600 8.0-3,394 594
Mercury <0.025 <0.028 <0.029 0.0079 J 9.7 0.03-0.52 0.121Nickel15 B 69 B 62 B 29 B 4,700 ND-150 23Selenium5.3 4.3 4.0 0.79 J 1,200 <0.1-0.8 0.42
Silver 0.049 J 0.050 J 0.039 J 0.095 J 1,200 ND-5.0 NE
Thallium 0.046 J 0.16 J 0.10 J 0.071 J 2.3 NE NEZinc35014011035,000 70,000 25-124 56
Notes:
1) NC DEQ Inactive Hazardous Sites Branch (IHSB) Industrial Health Based Preliminary
Soil Remediation Goals (PSRGs) - Februrary 2018
Bold concentration indicates exceedance of NC DEQ IHSB Preliminary Soil Remediation Goal (as well as background levels in the case of metals)
J=estimated concentration detected below reporting limit but above method detection limit; B=analyte found in associated blank at grater than 1/2 reporting limit
* = Range and Mean background values for North Carolina or Southeast soils taken from Elements in North American Soils by Dragun and Chekiri, 2005
EPA Method follows parameter in parenthesis; NE = Not established
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; HSL = Hazardous Substance List
Only compounds detected shown
Sample Date
Screening Criteria
Background*
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4/20/2018
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2
Summary of Groundwater Analytical Results
REEP-LRC Project 1
1900 Continental Boulevard
Charlotte, North Carolina
H&H Job No. LRC-006
Sample ID TMW-1 TMW-2 TMW-3 Dup-1 TMW-4 DWM Vapor Intrusion GWSLs
Sample Date 10/20/2016 10/17/2016 3/14/2018 3/14/2018 3/14/2018 Non-Residential(2)
Units µg/L
VOCs (8260B)
1,1-Dichloroethane <1.00 2.79 2.6 2.8 3.3 6 330
1,1,1-Trichloroethane <1.00 <1.00 2.8 2.1 3.2 200 6,200
1,1-Dichloroethylene <1.00 <1.00 2.3 1.0 <1.0 7 160
Acetone <25.0 <25.0 14 18 150 6,000 19,000,000
cis-1,2-Dichloroethylene <1.00 <1.00 3.1 3.4 5.2 70 NS
Tetrachloroethylene <1.00 <1.00 4.1 4.2 2.6 0.7 48
Trichloroethylene <1.00 <1.00 15 16 8.3 3 4.4
Explosives (8330A)All BRL All BRL NA NA NA varies N/A
Notes:
1) North Carolina Department of Environmental Quality (DEQ) 15A North Carolina Administrative Code 02L.0202 Groundwater Quality Standard2) DEQ Division of Waste Management (DWM) Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) (February 2018)
Only those compounds detected in at least one sample shown above
Bold value indicates concentration is above NCAC 2L Groundwater Standard Bold and Underlined value indicates concentration is above DWM Non-Residential GWSL
Compound concentrations are reported in micrograms per liter (μg/L)Method number follows parameter in parenthesis
VOCs = volatile organic compounds; BRL = below laboratory reporting limits; NA = Not Analyzed; N/A = Not Applicable
NCAC 2L
Groundwater
Standard(1)
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Table 2
Hart & Hickman, PC
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE WEST, NORTH CAROLINA 1996
TITLE
PROJECT
SITE LOCATION MAP
REEP-LRC PROJECT 1
1900 CONTINENTAL BOULEVARDCHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
2-7-18 0
1LRC-006
TMW-3
TMW-4
VMP-8VMP-7
ASH-1
BASE-2
BASE-1
JOB NO. LRC-006
REVISION NO. 0DATE: 4-20-18
FIGURE NO. 2
UNDEVELOPED PARCEL
1900 CONTINENTAL BOULEVARD
CHARLOTTE, NORTH CAROLINA
SOIL AND GROUND WATER
SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
LEGEND
SITE PROPERTY BOUNDARY
RAILROAD SPURS
PROPOSED BUILDING FOOTPRINT
PREVIOUS EXCAVATION AREA
SOIL SAMPLE LOCATION
SOIL VAPOR SAMPLE LOCATION
TEMPORARY MONITORING WELLLOCATION
NOTES:
1. BASE MAP OBTAINED FROM MECKLENBURG CO. GIS
(2017).
2. H&H CONDUCTED ASSESSMENT ON ACTIVITIES ONOCTOBER 13, 14, 17, & 20 2016.
APPROXIMATE EXTENT OF SOILDISTURBANCEBASED ON GPR SURVEY
APPROXIMATE LOCATION OF
POTENTIAL REMAINING DRUM
(NO DRUM FOUND)
LOCATION OF GPR
ANOMALY EXCAVATION
(NO DRUM FOUND)S:\AAA-Master Projects\LRC Patriot (LRC)\LRC-006 New Building Waste Assessment\Figures\Excavation Sample Location Map.dwg, FIG 2, 4/20/2018 8:50:40 AM, erichardson
AREA-1(ND)
AREA-2(ND)
AREA-3(ND)
APPROXIMATE AREA OF ASBESTOS TRANSITEDEBRIS (REMOVED)
APPROXIMATE AREA OF ASBESTOS ROOFING
DEBRIS (REMOVED)
JOB NO. LRC-006
REVISION NO. 0DATE: 4-16-18
FIGURE NO. 3
UNDEVELOPED PARCEL
1900 CONTINENTAL BOULEVARD
CHARLOTTE, NORTH CAROLINA
ASBESTOS SOIL SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
LEGEND
SITE PROPERTY BOUNDARY
RAILROAD SPURS
PROPOSED BUILDING FOOTPRINT
ASBESTOS SOIL SAMPLE LOCATION
NOTES:
1. BASE MAP OBTAINED FROM MECKLENBURG CO. GIS
(2017).
2. H&H CONDUCTED ASSESSMENT ON ACTIVITIES ONOCTOBER 13, 14, 17, & 20 2016.
3. ND = NON DETECT
S:\AAA-Master Projects\LRC Patriot (LRC)\LRC-006 New Building Waste Assessment\Figures\Excavation Sample Location Map.dwg, FIG 3, 4/20/2018 8:50:56 AM, erichardson

Appendix A
Photographs

Photograph 2: View of excavation in GPR anomaly area.LRC-006REEP-LRC PROJECT 1 SITE1900 CONTINENTAL BLVD
CHARLOTTE, NORTH CAROLINA
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
Photograph 1: View of excavation in known potential drum area
5-GALLON PAIL
REMNANT
ASH LAYER
Photograph 4: View of excavated transite soil mixture .LRC-006REEP-LRC PROJECT 1 SITE1900 CONTINENTAL BLVD
CHARLOTTE, NORTH CAROLINA
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
Photograph 3: View of southern excavation area following restoration
LRC-006REEP-LRC PROJECT 1 SITE1900 CONTINENTAL BLVD
CHARLOTTE, NORTH CAROLINA
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
Photograph 5: View of central transite disposal area following excavation

Appendix B
Laboratory Analytical Reports

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
03/05/2018
Hart & Hickman (Charlotte)
John Lopez
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: LRC-006 Continental Tire
Lab Submittal Date: 02/22/2018
Prism Work Order: 8020409
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
Method Detection LimitMDL
Not Detected at the MDLU
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 12
Sample Receipt Summary
03/05/2018
Prism Work Order: 8020409
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
8020409-01 02/21/18Soil-1 02/22/18Solid
Samples were received in good condition at 4.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 12
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8020409
03/05/2018
Summary of Detections
0.070 mg/L8020409-01 Soil-1 Benzene *8260B
0.073 mg/L8020409-01 Soil-1 Trichloroethylene *8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 12
Laboratory Report
03/05/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020409-01
Prism Work Order: 8020409
Time Collected: 02/21/18 15:00
Time Submitted: 02/22/18 16:00
Soil-1
TCLP Extraction by EPA 1311
*1311 P8B047112/27/18 7:15 JABN/ATCLP Extraction Complete
*1311 ZHE P8B050613/2/18 8:00 ANGN/ATCLP Extraction Complete
TCLP Metals
*7470A P8B047410.010 2/27/18 13:45 JABmg/L 0.000030Mercury0.000030 U
*6010D P8B048210.050 2/28/18 20:14 JABmg/L 0.016Arsenic0.016 U
*6010D P8B048215.0 2/28/18 20:14 JABmg/L 0.0040Barium0.0040 U
*6010D P8B048210.025 2/28/18 20:14 JABmg/L 0.00075Cadmium0.00075 U
*6010D P8B048210.25 2/28/18 20:14 JABmg/L 0.0018Chromium0.0018 U
*6010D P8B048210.050 2/28/18 20:14 JABmg/L 0.0040Lead0.0040 U
*6010D P8B048210.10 2/28/18 20:14 JABmg/L 0.028Selenium0.028 U
*6010D P8B048210.25 2/28/18 20:14 JABmg/L 0.0020Silver0.0020 U
TCLP Semivolatile Organic Compounds by GC/MS
*8270D P8C003010.25 2/27/18 14:41 JMVmg/L 0.00162,4,5-Trichlorophenol 0.0016 U
*8270D P8C003010.10 2/27/18 14:41 JMVmg/L 0.00182,4,6-Trichlorophenol 0.0018 U
*8270D P8C003010.050 2/27/18 14:41 JMVmg/L 0.00142,4-Dinitrotoluene 0.0014 U
*8270D P8C003010.050 2/27/18 14:41 JMVmg/L 0.00182-Methylphenol 0.0018 U
*8270D P8C003010.050 2/27/18 14:41 JMVmg/L 0.00153/4-Methylphenol 0.0015 U
*8270D P8C003010.050 2/27/18 14:41 JMVmg/L 0.0013Hexachlorobenzene0.0013 U
*8270D P8C003010.050 2/27/18 14:41 JMVmg/L 0.0021Hexachlorobutadiene0.0021 U
*8270D P8C003010.050 2/27/18 14:41 JMVmg/L 0.0017Hexachloroethane0.0017 U
*8270D P8C003010.050 2/27/18 14:41 JMVmg/L 0.0026Nitrobenzene0.0026 U
*8270D P8C003010.25 2/27/18 14:41 JMVmg/L 0.0012Pentachlorophenol0.0012 U
*8270D P8C003010.25 2/27/18 14:41 JMVmg/L 0.0010Pyridine0.0010 U
Surrogate Recovery Control Limits
43-14084 %2,4,6-Tribromophenol
44-11984 %2-Fluorobiphenyl
19-11956 %2-Fluorophenol
44-12079 %Nitrobenzene-d5
11-5235 %Phenol-d5
50-13491 %Terphenyl-d14
TCLP Volatile Organic Compounds by GC/MS
*8260B P8C003810.035 3/2/18 18:12 KDMmg/L 0.000831,1-Dichloroethylene 0.00083 U
*8260B P8C003810.025 3/2/18 18:12 KDMmg/L 0.000661,2-Dichloroethane 0.00066 U
*8260B P8C003810.38 3/2/18 18:12 KDMmg/L 0.000501,4-Dichlorobenzene 0.00050 U
*8260B P8C003810.025 3/2/18 18:12 KDMmg/L 0.00048Benzene0.070
*8260B P8C003810.025 3/2/18 18:12 KDMmg/L 0.0011Carbon Tetrachloride 0.0011 U
*8260B P8C003815.0 3/2/18 18:12 KDMmg/L 0.00062Chlorobenzene0.00062 U
*8260B P8C003810.30 3/2/18 18:12 KDMmg/L 0.00076Chloroform0.00076 U
*8260B P8C00381103/2/18 18:12 KDMmg/L 0.0024Methyl Ethyl Ketone (2-Butanone)0.0024 U
*8260B P8C003810.035 3/2/18 18:12 KDMmg/L 0.00098Tetrachloroethylene0.00098 U
*8260B P8C003810.025 3/2/18 18:12 KDMmg/L 0.00078Trichloroethylene0.073
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 12
Laboratory Report
03/05/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020409-01
Prism Work Order: 8020409
Time Collected: 02/21/18 15:00
Time Submitted: 02/22/18 16:00
Soil-1
*8260B P8C003810.020 3/2/18 18:12 KDMmg/L 0.00097Vinyl chloride 0.00097 U
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 12
3/5/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020409
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0038 - 5030B
Blank (P8C0038-BLK1)Prepared & Analyzed: 03/02/18
1,1-Dichloroethylene mg/LBRL0.035
1,2-Dichloroethane mg/LBRL0.025
1,4-Dichlorobenzene mg/LBRL0.38
Benzene mg/LBRL0.025
Carbon Tetrachloride mg/LBRL0.025
Chlorobenzene mg/LBRL5.0
Chloroform mg/LBRL0.30
Methyl Ethyl Ketone (2-Butanone)mg/LBRL10
Tetrachloroethylene mg/LBRL0.035
Trichloroethylene mg/LBRL0.025
Vinyl chloride mg/LBRL0.020
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.5
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10251.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.6
LCS (P8C0038-BS1)Prepared & Analyzed: 03/02/18
1,1-Dichloroethylene mg/L0.0201 0.035 0.02000 70-154101
1,2-Dichloroethane mg/L0.0212 0.025 0.02000 68-131106
1,4-Dichlorobenzene mg/L0.0186 0.38 0.02000 75-12693
Benzene mg/L0.0216 0.025 0.02000 77-128108
Carbon Tetrachloride mg/L0.0199 0.025 0.02000 72-14299
Chlorobenzene mg/L0.0199 5.0 0.02000 78-119100
Chloroform mg/L0.0209 0.30 0.02000 77-130104
Methyl Ethyl Ketone (2-Butanone)mg/L0.0196 10 0.02000 71-13498
Tetrachloroethylene mg/L0.0207 0.035 0.02000 80-129104
Trichloroethylene mg/L0.0216 0.025 0.02000 77-133108
Vinyl chloride mg/L0.0198 0.010 0.02000 57-14199
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9547.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10050.0
ug/L 50.00 77-123Surrogate: Toluene-d8 9447.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 12
3/5/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020409
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0038 - 5030B
LCS Dup (P8C0038-BSD1)Prepared & Analyzed: 03/02/18
1,1-Dichloroethylene mg/L0.0194 0.035 0.02000 2070-15497 4
1,2-Dichloroethane mg/L0.0203 0.025 0.02000 2068-131101 4
1,4-Dichlorobenzene mg/L0.0188 0.38 0.02000 2075-12694 1
Benzene mg/L0.0209 0.025 0.02000 2077-128105 3
Carbon Tetrachloride mg/L0.0190 0.025 0.02000 2072-14295 4
Chlorobenzene mg/L0.0196 5.0 0.02000 2078-11998 1
Chloroform mg/L0.0201 0.30 0.02000 2077-130100 4
Methyl Ethyl Ketone (2-Butanone)mg/L0.0197 10 0.02000 2071-13498 0.3
Tetrachloroethylene mg/L0.0204 0.035 0.02000 2080-129102 2
Trichloroethylene mg/L0.0208 0.025 0.02000 2077-133104 4
Vinyl chloride mg/L0.0188 0.010 0.02000 2057-14194 5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9648.1
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9447.0
ug/L 50.00 77-123Surrogate: Toluene-d8 9447.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 12
3/5/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020409
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8C0030 - 3510C MS
Blank (P8C0030-BLK1)Prepared & Analyzed: 02/26/18
2,4,5-Trichlorophenol mg/LBRL0.25
2,4,6-Trichlorophenol mg/LBRL0.10
2,4-Dinitrotoluene mg/LBRL0.050
2-Methylphenol mg/LBRL0.050
3/4-Methylphenol mg/LBRL0.050
Hexachlorobenzene mg/LBRL0.050
Hexachlorobutadiene mg/LBRL0.050
Hexachloroethane mg/LBRL0.050
Nitrobenzene mg/LBRL0.050
Pentachlorophenol mg/LBRL0.25
Pyridine mg/LBRL0.25
mg/L 0.5000 43-140Surrogate: 2,4,6-Tribromophenol 830.414
mg/L 0.2500 44-119Surrogate: 2-Fluorobiphenyl 770.193
mg/L 0.5000 19-119Surrogate: 2-Fluorophenol 510.257
mg/L 0.2500 44-120Surrogate: Nitrobenzene-d5 720.181
mg/L 0.5000 11-52Surrogate: Phenol-d5 310.155
mg/L 0.2500 50-134Surrogate: Terphenyl-d14 900.226
LCS (P8C0030-BS1)Prepared & Analyzed: 02/26/18
2,4,5-Trichlorophenol mg/L0.193 0.25 0.2500 53-12377
2,4,6-Trichlorophenol mg/L0.188 0.10 0.2500 50-12575
2,4-Dinitrotoluene mg/L0.182 0.050 0.2500 57-12873
2-Methylphenol mg/L0.173 0.050 0.2500 30-11769
3/4-Methylphenol mg/L0.132 0.050 0.2500 29-11053
Hexachlorobenzene mg/L0.190 0.050 0.2500 53-12576
Hexachlorobutadiene mg/L0.156 0.050 0.2500 22-12462
Hexachloroethane mg/L0.141 0.050 0.2500 21-11556
Nitrobenzene mg/L0.154 0.050 0.2500 45-12162
Pentachlorophenol mg/L0.216 0.25 0.2500 35-13886
Pyridine mg/L0.104 0.25 0.2500 10-5342
mg/L 0.5000 43-140Surrogate: 2,4,6-Tribromophenol 830.414
mg/L 0.2500 44-119Surrogate: 2-Fluorobiphenyl 790.197
mg/L 0.5000 19-119Surrogate: 2-Fluorophenol 520.260
mg/L 0.2500 44-120Surrogate: Nitrobenzene-d5 700.175
mg/L 0.5000 11-52Surrogate: Phenol-d5 310.157
mg/L 0.2500 50-134Surrogate: Terphenyl-d14 850.213
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 12
3/5/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020409
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8C0030 - 3510C MS
LCS Dup (P8C0030-BSD1)Prepared & Analyzed: 02/26/18
2,4,5-Trichlorophenol mg/L0.190 0.25 0.2500 2053-12376 2
2,4,6-Trichlorophenol mg/L0.180 0.10 0.2500 2050-12572 4
2,4-Dinitrotoluene mg/L0.173 0.050 0.2500 2057-12869 5
2-Methylphenol mg/L0.164 0.050 0.2500 2030-11766 5
3/4-Methylphenol mg/L0.130 0.050 0.2500 2029-11052 2
Hexachlorobenzene mg/L0.182 0.050 0.2500 2053-12573 4
Hexachlorobutadiene mg/L0.153 0.050 0.2500 2022-12461 2
Hexachloroethane mg/L0.138 0.050 0.2500 2021-11555 2
Nitrobenzene mg/L0.152 0.050 0.2500 2045-12161 2
Pentachlorophenol mg/L0.215 0.25 0.2500 2035-13886 0.1
Pyridine mg/L0.0858 0.25 0.2500 2010-5334 20
mg/L 0.5000 43-140Surrogate: 2,4,6-Tribromophenol 820.408
mg/L 0.2500 44-119Surrogate: 2-Fluorobiphenyl 760.191
mg/L 0.5000 19-119Surrogate: 2-Fluorophenol 500.252
mg/L 0.2500 44-120Surrogate: Nitrobenzene-d5 680.171
mg/L 0.5000 11-52Surrogate: Phenol-d5 310.156
mg/L 0.2500 50-134Surrogate: Terphenyl-d14 810.204
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 12
3/5/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020409
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP Metals - Quality Control
Batch P8B0474 - 7470A
Blank (P8B0474-BLK1)Prepared & Analyzed: 02/27/18
Mercury mg/LBRL0.010
LCS (P8B0474-BS1)Prepared & Analyzed: 02/27/18
Mercury mg/L0.00925 0.010 0.009375 80-12099
Matrix Spike (P8B0474-MS1)Prepared & Analyzed: 02/27/18 Source: 8020409-01
Mercury mg/L0.00954 0.010 0.009375 BRL 80-120102
Matrix Spike Dup (P8B0474-MSD1)Prepared & Analyzed: 02/27/18 Source: 8020409-01
Mercury mg/L0.00945 0.010 0.009375 BRL 2080-120101 0.9
Batch P8B0482 - 3010A
Blank (P8B0482-BLK1)Prepared: 02/27/18 Analyzed: 02/28/18
Arsenic mg/LBRL0.050
Barium mg/LBRL5.0
Cadmium mg/LBRL0.025
Chromium mg/LBRL0.25
Lead mg/LBRL0.050
Selenium mg/LBRL0.10
Silver mg/LBRL0.25
LCS (P8B0482-BS1)Prepared: 02/27/18 Analyzed: 02/28/18
Arsenic mg/L2.48 0.050 2.500 80-12099
Barium mg/L2.51 5.0 2.500 80-120100
Cadmium mg/L2.51 0.025 2.500 80-120100
Chromium mg/L2.47 0.25 2.500 80-12099
Lead mg/L2.47 0.050 2.500 80-12099
Selenium mg/L2.48 0.10 2.500 80-12099
Silver mg/L1.00 0.25 1.000 80-120100
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 12
Sample Extraction Data
Prep Method: 1311
Lab Number Batch Date/TimeInitialFinal
P8B05068020409-01 03/01/18 15:0012.5 250g mL
P8B04718020409-01 02/26/18 14:501002000gmL
Prep Method: 3010A
Lab Number Batch Date/TimeInitialFinal
P8B04828020409-01 02/27/18 9:451050mLmL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P8B04748020409-01 02/27/18 8:052030mLmL
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P8C00308020409-01 02/27/18 9:202001mLmL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P8C00388020409-01 03/02/18 9:41110mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 12
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
03/28/2018
Hart & Hickman (Charlotte)
John Lopez
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: LRC-006 Continental Tire
Lab Submittal Date: 02/22/2018
Prism Work Order: 8020408
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 36
Data Qualifiers Key Reference:
A Analyte is found in the blank at a concentration >1/2 RL.
Aa Re-analysis due to high surr. recovery resulted in similar recoveries. Matrix interference suspected. Initial result
reported.
Ab Surrogate recovery below range due to sample matrix.
B Analyte is found in the associated blank at a concentration >1/2 RL.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
D RPD value outside of the control limits.
ISR Internal standard response outside the QC limits. Analysis repeated without improvement. Initial result reported.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 36
Sample Receipt Summary
03/28/2018
Prism Work Order: 8020408
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
8020408-01 02/21/18Base-2 02/22/18Solid
8020408-02 02/21/18Base-3 02/22/18Solid
8020408-03 02/21/18Ash-1 02/22/18Solid
8020408-04 02/21/18Dup-1 02/22/18Solid
Samples were received in good condition at 4.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-01
Prism Work Order: 8020408
Time Collected: 02/21/18 11:15
Time Submitted: 02/22/18 16:00
Base-2
General Chemistry Parameters
SM2540 G P8B045810.100 2/23/18 15:13 BJC% by
Weight
0.100% Solids 78.7
Semivolatile Organic Compounds by GC/MS
8270D P8B048410.42 2/28/18 16:00 JMVmg/kg dry 0.0351,1’-Biphenyl <0.42
8270D P8B048410.42 2/28/18 16:00 JMVmg/kg dry 0.0652,3,4,6-Tetrachlorophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0792,4,5-Trichlorophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0792,4,6-Trichlorophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0812,4-Dichlorophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0642,4-Dimethylphenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0592,4-Dinitrophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0512,4-Dinitrotoluene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0562,6-Dinitrotoluene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0612-Chloronaphthalene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0592-Chlorophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0672-Methylnaphthalene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0542-Methylphenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0762-Nitroaniline <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0762-Nitrophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0833,3’-Dichlorobenzidine <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0523/4-Methylphenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0723-Nitroaniline <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0634,6-Dinitro-2-methylphenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0724-Bromophenyl phenyl ether <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0594-Chloro-3-methylphenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0504-Chloroaniline <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0764-Nitroaniline <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.0654-Nitrophenol <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.057Acenaphthene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.061Acenaphthylene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.070Acetophenone<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.068Anthracene<0.42
8270D P8B048410.42 2/28/18 16:00 JMVmg/kg dry 0.065Atrazine<0.42
8270D P8B048410.42 2/28/18 16:00 JMVmg/kg dry 0.037Benzaldehyde<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.055Benzo(a)anthracene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.045Benzo(a)pyrene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.049Benzo(b)fluoranthene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.046Benzo(g,h,i)perylene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.055Benzo(k)fluoranthene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.059Bis(2-Chloroethyl)ether <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether <0.42
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-01
Prism Work Order: 8020408
Time Collected: 02/21/18 11:15
Time Submitted: 02/22/18 16:00
Base-2
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.062Bis(2-Ethylhexyl)phthalate <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.060Butyl benzyl phthalate <0.42
8270D P8B048410.42 2/28/18 16:00 JMVmg/kg dry 0.063Caprolactam<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.064Carbazole<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.053Chrysene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.064Dibenzofuran<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.058Diethyl phthalate <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.055Dimethyl phthalate <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.060Di-n-butyl phthalate <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.052Di-n-octyl phthalate <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.053Fluoranthene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.060Fluorene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.067Hexachlorobenzene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.075Hexachlorobutadiene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.075Hexachlorocyclopentadiene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.070Hexachloroethane<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.057Isophorone<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.067Naphthalene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.060Nitrobenzene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.066N-Nitroso-di-n-propylamine <0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.064N-Nitrosodiphenylamine 0.75
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.050Pentachlorophenol<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.054Phenanthrene<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.062Phenol<0.42
8270D P8B048410.42 2/27/18 22:14 JMVmg/kg dry 0.056Pyrene<0.42
Surrogate Recovery Control Limits
37-13168 %2,4,6-Tribromophenol
47-13065 %2-Fluorobiphenyl
44-11763 %2-Fluorophenol
45-12153 %Nitrobenzene-d5
37-12759 %Phenol-d5
38-13565 %Terphenyl-d14
Total Metals
7471B P8B049610.025 2/28/18 11:18 JABmg/kg dry 0.0023Mercury<0.025
6020B P8B0445100.63 3/1/18 15:45 PJFBmg/kg dry 0.033Antimony0.63
6020B P8B0445101.9 3/1/18 15:45 PJFJmg/kg dry 0.17Arsenic1.8
6020B P8B0445100.32 3/1/18 15:45 PJFmg/kg dry 0.054Beryllium1.7
6020B P8B0445100.32 3/1/18 15:45 PJFJmg/kg dry 0.024Cadmium0.11
6020B P8B0445100.63 3/1/18 15:45 PJFBmg/kg dry 0.035Chromium3.4
6020B P8B0445100.63 3/1/18 15:45 PJFBmg/kg dry 0.051Copper41
6020B P8B0445100.32 3/1/18 15:45 PJFmg/kg dry 0.072Lead16
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-01
Prism Work Order: 8020408
Time Collected: 02/21/18 11:15
Time Submitted: 02/22/18 16:00
Base-2
6020B P8B0445103.2 3/1/18 15:45 PJFmg/kg dry 0.089Manganese320
6020B P8B0445100.32 3/1/18 15:45 PJFBmg/kg dry 0.046Nickel15
6020B P8B0445101.3 3/1/18 15:45 PJFmg/kg dry 0.26Selenium5.3
6020B P8B0445100.32 3/1/18 15:45 PJFJmg/kg dry 0.024Silver0.049
6020B P8B0445100.32 3/1/18 15:45 PJFJmg/kg dry 0.025Thallium0.046
6020B P8B044510253/1/18 15:45 PJFmg/kg dry 0.77Zinc350
Volatile Organic Compounds by GC/MS
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000281,1,1-Trichloroethane <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000381,1,2,2-Tetrachloroethane <0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.000421,1,2-Trichloro-1,2,2-trifluoroethane <0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000501,1,2-Trichloroethane <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000161,1-Dichloroethane 0.013
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000251,1-Dichloroethylene <0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene <0.011
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.000421,2,4-Trichlorobenzene <0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000421,2-Dibromo-3-chloropropane <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000231,2-Dibromoethane <0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.000271,2-Dichlorobenzene <0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000341,2-Dichloroethane <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.000351,2-Dichloropropane <0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.000381,3-Dichlorobenzene <0.011
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.000221,4-Dichlorobenzene <0.011
8260B P8B046010.11 2/26/18 17:00 ANGmg/kg dry 0.0121,4-Dioxane <0.11
8260B P8B046010.023 2/26/18 17:00 ANGmg/kg dry 0.0014Acetone0.12
8260B P8B046010.0034 2/26/18 17:00 ANGmg/kg dry 0.00033Benzene0.17
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00031Bromochloromethane<0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00032Bromodichloromethane<0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00065Bromoform<0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00070Bromomethane<0.011
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00028Carbon disulfide <0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00028Carbon Tetrachloride <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00030Chlorobenzene<0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00047Chloroethane<0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00041Chloroform<0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00038Chloromethane<0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene 0.027
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00037CyclohexaneSee 8260ML
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00023Dibromochloromethane<0.0057
8260B P8B046010.011 2/26/18 17:00 ANGCCVmg/kg dry 0.00026Dichlorodifluoromethane<0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00022EthylbenzeneSee 8260ML
8260B P8B046010.011 2/26/18 17:00 ANGJmg/kg dry 0.00034Isopropylbenzene (Cumene)0.0085
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00053m,p-Xylenes See 8260ML
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-01
Prism Work Order: 8020408
Time Collected: 02/21/18 11:15
Time Submitted: 02/22/18 16:00
Base-2
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00086Methyl Acetate <0.0057
8260B P8B046010.057 2/26/18 17:00 ANGmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)<0.057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00049Methylcyclohexane0.12
8260B P8B046010.023 2/26/18 17:00 ANGmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)<0.023
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00049Methyl Isobutyl Ketone <0.011
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00032Methylene Chloride <0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00023o-Xylene See 8260ML
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00034Styrene<0.0057
8260B P8B046010.011 2/26/18 17:00 ANGmg/kg dry 0.00027Tetrachloroethylene<0.011
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00033Toluene0.092
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene <0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00037Trichloroethylene<0.0057
8260B P8B046010.0057 2/26/18 17:00 ANGmg/kg dry 0.00037Trichlorofluoromethane<0.0057
8260B P8B046010.011 2/26/18 17:00 ANGJmg/kg dry 0.00028Vinyl chloride 0.0049
8260B P8B046010.017 2/26/18 17:00 ANGmg/kg dry 0.0011Xylenes, total See 8260ML
Surrogate Recovery Control Limits
70-130105 %4-Bromofluorobenzene
84-12394 %Dibromofluoromethane
76-129111 %Toluene-d8
Volatile Organic Compounds by GC/MS (Medium Level)
8260B P8C0010500.29 2/28/18 17:10 ANGmg/kg dry 0.068Cyclohexane9.0
8260B P8C0010500.29 2/28/18 17:10 ANGmg/kg dry 0.066Ethylbenzene4.9
8260B P8C0010500.58 2/28/18 17:10 ANGmg/kg dry 0.14m,p-Xylenes 12
8260B P8C0010500.29 2/28/18 17:10 ANGmg/kg dry 0.064o-Xylene 2.4
8260B P8C0010500.87 2/28/18 17:10 ANGmg/kg dry 0.20Xylenes, total 15
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-13096 %Dibromofluoromethane
70-130110 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-02
Prism Work Order: 8020408
Time Collected: 02/21/18 13:30
Time Submitted: 02/22/18 16:00
Base-3
General Chemistry Parameters
SM2540 G P8B045810.100 2/23/18 15:13 BJC% by
Weight
0.100% Solids 67.2
Semivolatile Organic Compounds by GC/MS
8270D P8B048410.49 2/28/18 14:51 JMVmg/kg dry 0.0411,1’-Biphenyl <0.49
8270D P8B048410.49 2/28/18 14:51 JMVmg/kg dry 0.0762,3,4,6-Tetrachlorophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0922,4,5-Trichlorophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0922,4,6-Trichlorophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0952,4-Dichlorophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0752,4-Dimethylphenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0692,4-Dinitrophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0602,4-Dinitrotoluene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0652,6-Dinitrotoluene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0712-Chloronaphthalene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0702-Chlorophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0782-Methylnaphthalene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0632-Methylphenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0892-Nitroaniline <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0892-Nitrophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0973,3’-Dichlorobenzidine <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0603/4-Methylphenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0843-Nitroaniline <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0744,6-Dinitro-2-methylphenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0844-Bromophenyl phenyl ether <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0694-Chloro-3-methylphenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0594-Chloroaniline <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0644-Chlorophenyl phenyl ether <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0894-Nitroaniline <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.0764-Nitrophenol <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.067Acenaphthene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.071Acenaphthylene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.082Acetophenone<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.079Anthracene<0.49
8270D P8B048410.49 2/28/18 14:51 JMVmg/kg dry 0.076Atrazine<0.49
8270D P8B048410.49 2/28/18 14:51 JMVmg/kg dry 0.043Benzaldehyde<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.064Benzo(a)anthracene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.053Benzo(a)pyrene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.057Benzo(b)fluoranthene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.054Benzo(g,h,i)perylene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.064Benzo(k)fluoranthene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.085bis(2-Chloroethoxy)methane <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.069Bis(2-Chloroethyl)ether <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.084Bis(2-chloroisopropyl)ether <0.49
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-02
Prism Work Order: 8020408
Time Collected: 02/21/18 13:30
Time Submitted: 02/22/18 16:00
Base-3
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.073Bis(2-Ethylhexyl)phthalate <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.070Butyl benzyl phthalate <0.49
8270D P8B048410.49 2/28/18 14:51 JMVmg/kg dry 0.074Caprolactam<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.075Carbazole<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.062Chrysene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.060Dibenzo(a,h)anthracene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.075Dibenzofuran<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.068Diethyl phthalate <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.065Dimethyl phthalate <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.070Di-n-butyl phthalate <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.060Di-n-octyl phthalate <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.063Fluoranthene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.070Fluorene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.078Hexachlorobenzene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.088Hexachlorobutadiene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.088Hexachlorocyclopentadiene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.082Hexachloroethane<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.056Indeno(1,2,3-cd)pyrene <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.066Isophorone<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.079Naphthalene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.070Nitrobenzene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.077N-Nitroso-di-n-propylamine <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.075N-Nitrosodiphenylamine <0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.058Pentachlorophenol<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.064Phenanthrene<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.072Phenol<0.49
8270D P8B048410.49 2/27/18 17:42 JMVmg/kg dry 0.065Pyrene<0.49
Surrogate Recovery Control Limits
37-13168 %2,4,6-Tribromophenol
47-13068 %2-Fluorobiphenyl
44-11768 %2-Fluorophenol
45-12158 %Nitrobenzene-d5
37-12764 %Phenol-d5
38-13572 %Terphenyl-d14
Total Metals
7471B P8B049610.028 2/28/18 11:32 JABmg/kg dry 0.0027Mercury<0.028
6020B P8B0445100.74 3/1/18 16:08 PJFB, J mg/kg dry 0.038Antimony0.67
6020B P8B0445102.2 3/1/18 16:08 PJFJmg/kg dry 0.20Arsenic1.5
6020B P8B0445100.37 3/1/18 16:08 PJFmg/kg dry 0.063Beryllium2.8
6020B P8B0445100.37 3/1/18 16:08 PJFJmg/kg dry 0.028Cadmium0.052
6020B P8B0445100.74 3/1/18 16:08 PJFBmg/kg dry 0.041Chromium76
6020B P8B0445100.74 3/1/18 16:08 PJFBmg/kg dry 0.059Copper59
6020B P8B0445100.37 3/1/18 16:08 PJFmg/kg dry 0.084Lead22
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-02
Prism Work Order: 8020408
Time Collected: 02/21/18 13:30
Time Submitted: 02/22/18 16:00
Base-3
6020B P8B0445103.7 3/1/18 16:08 PJFmg/kg dry 0.10Manganese900
6020B P8B0445100.37 3/1/18 16:08 PJFBmg/kg dry 0.053Nickel69
6020B P8B0445101.5 3/1/18 16:08 PJFmg/kg dry 0.30Selenium4.3
6020B P8B0445100.37 3/1/18 16:08 PJFJmg/kg dry 0.028Silver0.050
6020B P8B0445100.37 3/1/18 16:08 PJFJmg/kg dry 0.029Thallium0.16
6020B P8B044510293/1/18 16:08 PJFmg/kg dry 0.89Zinc140
Volatile Organic Compounds by GC/MS
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000301,1,1-Trichloroethane <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000421,1,2,2-Tetrachloroethane <0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.000461,1,2-Trichloro-1,2,2-trifluoroethane <0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000551,1,2-Trichloroethane <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000171,1-Dichloroethane <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000271,1-Dichloroethylene <0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.000351,2,3-Trichlorobenzene <0.012
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.000461,2,4-Trichlorobenzene <0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000461,2-Dibromo-3-chloropropane <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000251,2-Dibromoethane <0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.000291,2-Dichlorobenzene <0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000371,2-Dichloroethane <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.000381,2-Dichloropropane <0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.000411,3-Dichlorobenzene <0.012
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.000241,4-Dichlorobenzene <0.012
8260B P8B046010.12 2/26/18 17:28 ANGmg/kg dry 0.0121,4-Dioxane <0.12
8260B P8B046010.025 2/26/18 17:28 ANGmg/kg dry 0.0015Acetone<0.025
8260B P8B046010.0037 2/26/18 17:28 ANGmg/kg dry 0.00036Benzene<0.0037
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00034Bromochloromethane<0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00034Bromodichloromethane<0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00070Bromoform<0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00076Bromomethane<0.012
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00030Carbon disulfide <0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00031Carbon Tetrachloride <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00033Chlorobenzene<0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00052Chloroethane<0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00045Chloroform<0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00042Chloromethane<0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00040Cyclohexane<0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00025Dibromochloromethane<0.0062
8260B P8B046010.012 2/26/18 17:28 ANGCCVmg/kg dry 0.00028Dichlorodifluoromethane<0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00024Ethylbenzene<0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00037Isopropylbenzene (Cumene)<0.012
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00057m,p-Xylenes <0.012
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-02
Prism Work Order: 8020408
Time Collected: 02/21/18 13:30
Time Submitted: 02/22/18 16:00
Base-3
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00093Methyl Acetate <0.0062
8260B P8B046010.062 2/26/18 17:28 ANGmg/kg dry 0.00056Methyl Butyl Ketone (2-Hexanone)<0.062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00053Methylcyclohexane<0.0062
8260B P8B046010.025 2/26/18 17:28 ANGmg/kg dry 0.00056Methyl Ethyl Ketone (2-Butanone)<0.025
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00053Methyl Isobutyl Ketone <0.012
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00035Methylene Chloride <0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00025o-Xylene <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00037Styrene<0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00029Tetrachloroethylene<0.012
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00035Toluene<0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00037trans-1,2-Dichloroethylene <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00033trans-1,3-Dichloropropylene <0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00040Trichloroethylene<0.0062
8260B P8B046010.0062 2/26/18 17:28 ANGmg/kg dry 0.00040Trichlorofluoromethane<0.0062
8260B P8B046010.012 2/26/18 17:28 ANGmg/kg dry 0.00030Vinyl chloride <0.012
8260B P8B046010.019 2/26/18 17:28 ANGmg/kg dry 0.0012Xylenes, total <0.019
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
84-123100 %Dibromofluoromethane
76-129106 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-03
Prism Work Order: 8020408
Time Collected: 02/21/18 14:00
Time Submitted: 02/22/18 16:00
Ash-1
General Chemistry Parameters
SM2540 G P8B045810.100 2/23/18 15:13 BJC% by
Weight
0.100% Solids 78.7
Semivolatile Organic Compounds by GC/MS
8270D P8B048410.42 2/28/18 15:14 JMVmg/kg dry 0.0351,1’-Biphenyl <0.42
8270D P8B048410.42 2/28/18 15:14 JMVmg/kg dry 0.0652,3,4,6-Tetrachlorophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0792,4,5-Trichlorophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0792,4,6-Trichlorophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0812,4-Dichlorophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0642,4-Dimethylphenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0592,4-Dinitrophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0512,4-Dinitrotoluene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0562,6-Dinitrotoluene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0612-Chloronaphthalene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0592-Chlorophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0672-Methylnaphthalene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0542-Methylphenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0762-Nitroaniline <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0762-Nitrophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0833,3’-Dichlorobenzidine <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0523/4-Methylphenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0723-Nitroaniline <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0634,6-Dinitro-2-methylphenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0724-Bromophenyl phenyl ether <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0594-Chloro-3-methylphenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0504-Chloroaniline <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0764-Nitroaniline <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.0654-Nitrophenol <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.057Acenaphthene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.061Acenaphthylene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.070Acetophenone<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.068Anthracene<0.42
8270D P8B048410.42 2/28/18 15:14 JMVmg/kg dry 0.065Atrazine<0.42
8270D P8B048410.42 2/28/18 15:14 JMVmg/kg dry 0.037Benzaldehyde<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.055Benzo(a)anthracene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.045Benzo(a)pyrene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.049Benzo(b)fluoranthene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.046Benzo(g,h,i)perylene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.055Benzo(k)fluoranthene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.059Bis(2-Chloroethyl)ether <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether <0.42
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-03
Prism Work Order: 8020408
Time Collected: 02/21/18 14:00
Time Submitted: 02/22/18 16:00
Ash-1
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.062Bis(2-Ethylhexyl)phthalate <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.060Butyl benzyl phthalate <0.42
8270D P8B048410.42 2/28/18 15:14 JMVmg/kg dry 0.063Caprolactam<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.064Carbazole<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.053Chrysene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.064Dibenzofuran<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.058Diethyl phthalate <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.055Dimethyl phthalate <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.060Di-n-butyl phthalate <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.052Di-n-octyl phthalate <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.053Fluoranthene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.060Fluorene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.067Hexachlorobenzene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.075Hexachlorobutadiene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.075Hexachlorocyclopentadiene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.070Hexachloroethane<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.057Isophorone<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.067Naphthalene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.060Nitrobenzene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.066N-Nitroso-di-n-propylamine <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.064N-Nitrosodiphenylamine <0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.050Pentachlorophenol<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.054Phenanthrene<0.42
8270D P8B048410.42 2/27/18 18:05 JMVmg/kg dry 0.062Phenol<0.42
8270D P8B048410.42 2/27/18 18:05 JMVJmg/kg dry 0.055Pyrene0.21
Surrogate Recovery Control Limits
37-1315 %2,4,6-Tribromophenol Ab
47-1305 %2-Fluorobiphenyl Ab
44-1175 %2-Fluorophenol Ab
45-1214 %Nitrobenzene-d5 Ab
37-1275 %Phenol-d5 Ab
38-1355 %Terphenyl-d14 Ab
Total Metals
7471B P8B049610.028 2/28/18 11:36 JABJmg/kg dry 0.0026Mercury0.0079
6020B P8B0445100.63 3/1/18 16:16 PJFB, J mg/kg dry 0.033Antimony0.53
6020B P8B0445101.9 3/1/18 16:16 PJFmg/kg dry 0.17Arsenic13
6020B P8B0445100.32 3/1/18 16:16 PJFmg/kg dry 0.054Beryllium0.35
6020B P8B0445100.32 3/1/18 16:16 PJFmg/kg dry 0.024Cadmium5.0
6020B P8B0445100.63 3/1/18 16:16 PJFBmg/kg dry 0.035Chromium35
6020B P8B0445100.63 3/1/18 16:16 PJFBmg/kg dry 0.051Copper18
6020B P8B0445100.32 3/1/18 16:16 PJFmg/kg dry 0.072Lead31
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-03
Prism Work Order: 8020408
Time Collected: 02/21/18 14:00
Time Submitted: 02/22/18 16:00
Ash-1
6020B P8B0445103.2 3/1/18 16:16 PJFmg/kg dry 0.089Manganese160
6020B P8B0445100.32 3/1/18 16:16 PJFBmg/kg dry 0.046Nickel29
6020B P8B0445101.3 3/1/18 16:16 PJFJmg/kg dry 0.26Selenium0.79
6020B P8B0445100.32 3/1/18 16:16 PJFJmg/kg dry 0.024Silver0.095
6020B P8B0445100.32 3/1/18 16:16 PJFJmg/kg dry 0.025Thallium0.071
6020B P8B044540010003/1/18 17:10 PJFmg/kg dry 31Zinc35000
Volatile Organic Compounds by GC/MS
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.000511,1,1-Trichloroethane <0.010
8260B P8B046010.010 2/26/18 17:56 ANGISRmg/kg dry 0.000711,1,2,2-Tetrachloroethane <0.010
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.000781,1,2-Trichloro-1,2,2-trifluoroethane <0.021
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.000931,1,2-Trichloroethane <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.000291,1-Dichloroethane <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.000461,1-Dichloroethylene <0.010
8260B P8B046010.021 2/26/18 17:56 ANGISRmg/kg dry 0.000591,2,3-Trichlorobenzene <0.021
8260B P8B046010.021 2/26/18 17:56 ANGISRmg/kg dry 0.000781,2,4-Trichlorobenzene <0.021
8260B P8B046010.010 2/26/18 17:56 ANGISRmg/kg dry 0.000771,2-Dibromo-3-chloropropane <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.000421,2-Dibromoethane <0.010
8260B P8B046010.021 2/26/18 17:56 ANGISRmg/kg dry 0.000491,2-Dichlorobenzene <0.021
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.000621,2-Dichloroethane <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.000651,2-Dichloropropane <0.010
8260B P8B046010.021 2/26/18 17:56 ANGISRmg/kg dry 0.000691,3-Dichlorobenzene <0.021
8260B P8B046010.021 2/26/18 17:56 ANGISRmg/kg dry 0.000411,4-Dichlorobenzene <0.021
8260B P8B046010.21 2/26/18 17:56 ANGmg/kg dry 0.0211,4-Dioxane <0.21
8260B P8B046010.042 2/26/18 17:56 ANGmg/kg dry 0.0025Acetone0.084
8260B P8B046010.0063 2/26/18 17:56 ANGmg/kg dry 0.00061Benzene<0.0063
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00057Bromochloromethane<0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00058Bromodichloromethane<0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.0012Bromoform<0.010
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.0013Bromomethane<0.021
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.00051Carbon disulfide <0.021
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00052Carbon Tetrachloride <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00055Chlorobenzene<0.010
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.00087Chloroethane<0.021
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00075Chloroform<0.010
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.00070Chloromethane<0.021
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00045cis-1,2-Dichloroethylene <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00035cis-1,3-Dichloropropylene <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00068Cyclohexane<0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00043Dibromochloromethane<0.010
8260B P8B046010.021 2/26/18 17:56 ANGCCVmg/kg dry 0.00047Dichlorodifluoromethane<0.021
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00040Ethylbenzene<0.010
8260B P8B046010.021 2/26/18 17:56 ANGISRmg/kg dry 0.00062Isopropylbenzene (Cumene)<0.021
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.00096m,p-Xylenes <0.021
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-03
Prism Work Order: 8020408
Time Collected: 02/21/18 14:00
Time Submitted: 02/22/18 16:00
Ash-1
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.0016Methyl Acetate <0.010
8260B P8B046010.10 2/26/18 17:56 ANGmg/kg dry 0.00094Methyl Butyl Ketone (2-Hexanone)<0.10
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00089Methylcyclohexane<0.010
8260B P8B046010.042 2/26/18 17:56 ANGmg/kg dry 0.00094Methyl Ethyl Ketone (2-Butanone)<0.042
8260B P8B046010.021 2/26/18 17:56 ANGJmg/kg dry 0.00089Methyl Isobutyl Ketone 0.013
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.00059Methylene Chloride <0.021
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00033Methyl-tert-Butyl Ether <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00043o-Xylene <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00063Styrene<0.010
8260B P8B046010.021 2/26/18 17:56 ANGJmg/kg dry 0.00050Tetrachloroethylene0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00060Toluene<0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00062trans-1,2-Dichloroethylene <0.010
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00055trans-1,3-Dichloropropylene <0.010
8260B P8B046010.010 2/26/18 17:56 ANGJmg/kg dry 0.00068Trichloroethylene0.0056
8260B P8B046010.010 2/26/18 17:56 ANGmg/kg dry 0.00068Trichlorofluoromethane<0.010
8260B P8B046010.021 2/26/18 17:56 ANGmg/kg dry 0.00051Vinyl chloride <0.021
8260B P8B046010.031 2/26/18 17:56 ANGmg/kg dry 0.0020Xylenes, total <0.031
Surrogate Recovery Control Limits
70-130158 %4-Bromofluorobenzene Aa, ISR
84-123103 %Dibromofluoromethane
76-129126 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-04
Prism Work Order: 8020408
Time Collected: 02/21/18 00:00
Time Submitted: 02/22/18 16:00
Dup-1
General Chemistry Parameters
SM2540 G P8B045810.100 2/23/18 15:13 BJC% by
Weight
0.100% Solids 62.7
Semivolatile Organic Compounds by GC/MS
8270D P8B048410.53 2/28/18 15:37 JMVmg/kg dry 0.0441,1’-Biphenyl <0.53
8270D P8B048410.53 2/28/18 15:37 JMVmg/kg dry 0.0812,3,4,6-Tetrachlorophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0992,4,5-Trichlorophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0992,4,6-Trichlorophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.102,4-Dichlorophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0812,4-Dimethylphenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0742,4-Dinitrophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0642,4-Dinitrotoluene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0702,6-Dinitrotoluene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0762-Chloronaphthalene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0752-Chlorophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0842-Methylnaphthalene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0672-Methylphenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0952-Nitroaniline <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0962-Nitrophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.103,3’-Dichlorobenzidine <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0653/4-Methylphenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0913-Nitroaniline <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0794,6-Dinitro-2-methylphenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0904-Bromophenyl phenyl ether <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0744-Chloro-3-methylphenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0634-Chloroaniline <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0684-Chlorophenyl phenyl ether <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0964-Nitroaniline <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.0814-Nitrophenol <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.072Acenaphthene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.076Acenaphthylene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.088Acetophenone<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.085Anthracene<0.53
8270D P8B048410.53 2/28/18 15:37 JMVmg/kg dry 0.082Atrazine<0.53
8270D P8B048410.53 2/28/18 15:37 JMVmg/kg dry 0.046Benzaldehyde<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.069Benzo(a)anthracene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.057Benzo(a)pyrene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.061Benzo(b)fluoranthene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.058Benzo(g,h,i)perylene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.069Benzo(k)fluoranthene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.091bis(2-Chloroethoxy)methane <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.074Bis(2-Chloroethyl)ether <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.090Bis(2-chloroisopropyl)ether <0.53
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-04
Prism Work Order: 8020408
Time Collected: 02/21/18 00:00
Time Submitted: 02/22/18 16:00
Dup-1
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.078Bis(2-Ethylhexyl)phthalate <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.075Butyl benzyl phthalate <0.53
8270D P8B048410.53 2/28/18 15:37 JMVmg/kg dry 0.080Caprolactam<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.081Carbazole<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.066Chrysene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.064Dibenzo(a,h)anthracene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.080Dibenzofuran<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.073Diethyl phthalate <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.070Dimethyl phthalate <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.075Di-n-butyl phthalate <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.065Di-n-octyl phthalate <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.067Fluoranthene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.076Fluorene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.084Hexachlorobenzene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.095Hexachlorobutadiene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.094Hexachlorocyclopentadiene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.088Hexachloroethane<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.060Indeno(1,2,3-cd)pyrene <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.071Isophorone<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.085Naphthalene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.075Nitrobenzene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.083N-Nitroso-di-n-propylamine <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.080N-Nitrosodiphenylamine <0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.062Pentachlorophenol<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.068Phenanthrene<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.078Phenol<0.53
8270D P8B048410.53 2/27/18 18:28 JMVmg/kg dry 0.070Pyrene<0.53
Surrogate Recovery Control Limits
37-13168 %2,4,6-Tribromophenol
47-13068 %2-Fluorobiphenyl
44-11771 %2-Fluorophenol
45-12161 %Nitrobenzene-d5
37-12767 %Phenol-d5
38-13574 %Terphenyl-d14
Total Metals
7471B P8B049610.029 2/28/18 11:41 JABmg/kg dry 0.0028Mercury<0.029
6020B P8B0445100.79 3/1/18 16:24 PJFB, J mg/kg dry 0.041Antimony0.56
6020B P8B0445102.4 3/1/18 16:24 PJFJmg/kg dry 0.22Arsenic1.5
6020B P8B0445100.40 3/1/18 16:24 PJFmg/kg dry 0.068Beryllium2.5
6020B P8B0445100.40 3/1/18 16:24 PJFJmg/kg dry 0.030Cadmium0.047
6020B P8B0445100.79 3/1/18 16:24 PJFBmg/kg dry 0.044Chromium65
6020B P8B0445100.79 3/1/18 16:24 PJFBmg/kg dry 0.063Copper51
6020B P8B0445100.40 3/1/18 16:24 PJFmg/kg dry 0.090Lead18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-04
Prism Work Order: 8020408
Time Collected: 02/21/18 00:00
Time Submitted: 02/22/18 16:00
Dup-1
6020B P8B0445104.0 3/1/18 16:24 PJFmg/kg dry 0.11Manganese670
6020B P8B0445100.40 3/1/18 16:24 PJFBmg/kg dry 0.057Nickel62
6020B P8B0445101.6 3/1/18 16:24 PJFmg/kg dry 0.33Selenium4.0
6020B P8B0445100.40 3/1/18 16:24 PJFJmg/kg dry 0.030Silver0.039
6020B P8B0445100.40 3/1/18 16:24 PJFJmg/kg dry 0.032Thallium0.10
6020B P8B044510323/1/18 16:24 PJFmg/kg dry 0.96Zinc110
Volatile Organic Compounds by GC/MS
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000361,1,1-Trichloroethane <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000501,1,2,2-Tetrachloroethane <0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.000561,1,2-Trichloro-1,2,2-trifluoroethane <0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000661,1,2-Trichloroethane <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000211,1-Dichloroethane <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000331,1-Dichloroethylene <0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.000421,2,3-Trichlorobenzene <0.015
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.000561,2,4-Trichlorobenzene <0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000551,2-Dibromo-3-chloropropane <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000301,2-Dibromoethane <0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.000351,2-Dichlorobenzene <0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000451,2-Dichloroethane <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.000461,2-Dichloropropane <0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.000491,3-Dichlorobenzene <0.015
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.000291,4-Dichlorobenzene <0.015
8260B P8B046010.15 2/26/18 18:23 ANGmg/kg dry 0.0151,4-Dioxane <0.15
8260B P8B046010.030 2/26/18 18:23 ANGmg/kg dry 0.0018Acetone<0.030
8260B P8B046010.0045 2/26/18 18:23 ANGmg/kg dry 0.00043Benzene<0.0045
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00041Bromochloromethane<0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00042Bromodichloromethane<0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00085Bromoform<0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00092Bromomethane<0.015
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00037Carbon disulfide <0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00037Carbon Tetrachloride <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00040Chlorobenzene<0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00062Chloroethane<0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00054Chloroform<0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00050Chloromethane<0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00032cis-1,2-Dichloroethylene <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00025cis-1,3-Dichloropropylene <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00049Cyclohexane<0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00031Dibromochloromethane<0.0075
8260B P8B046010.015 2/26/18 18:23 ANGCCVmg/kg dry 0.00034Dichlorodifluoromethane<0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00029Ethylbenzene<0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00044Isopropylbenzene (Cumene)<0.015
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00069m,p-Xylenes <0.015
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 36
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8020408-04
Prism Work Order: 8020408
Time Collected: 02/21/18 00:00
Time Submitted: 02/22/18 16:00
Dup-1
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.0011Methyl Acetate <0.0075
8260B P8B046010.075 2/26/18 18:23 ANGmg/kg dry 0.00068Methyl Butyl Ketone (2-Hexanone)<0.075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00064Methylcyclohexane<0.0075
8260B P8B046010.030 2/26/18 18:23 ANGmg/kg dry 0.00068Methyl Ethyl Ketone (2-Butanone)<0.030
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00064Methyl Isobutyl Ketone <0.015
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00042Methylene Chloride <0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00024Methyl-tert-Butyl Ether <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00031o-Xylene <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00045Styrene<0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00036Tetrachloroethylene<0.015
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00043Toluene<0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00045trans-1,2-Dichloroethylene <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00039trans-1,3-Dichloropropylene <0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00048Trichloroethylene<0.0075
8260B P8B046010.0075 2/26/18 18:23 ANGmg/kg dry 0.00048Trichlorofluoromethane<0.0075
8260B P8B046010.015 2/26/18 18:23 ANGmg/kg dry 0.00036Vinyl chloride <0.015
8260B P8B046010.022 2/26/18 18:23 ANGmg/kg dry 0.0014Xylenes, total <0.022
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-129106 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8B0460 - 5035
LCS (P8B0460-BS1)Prepared & Analyzed: 02/26/18
1,1,1-Trichloroethane mg/kg wet0.0392 0.0050 0.05000 67-13178
1,1,2,2-Tetrachloroethane mg/kg wet0.0488 0.0050 0.05000 56-12698
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0411 0.010 0.05000 70-13082
1,1,2-Trichloroethane mg/kg wet0.0440 0.0050 0.05000 70-13388
1,1-Dichloroethane mg/kg wet0.0368 0.0050 0.05000 74-12774
1,1-Dichloroethylene mg/kg wet0.0390 0.0050 0.05000 67-14978
1,2,3-Trichlorobenzene mg/kg wet0.0488 0.010 0.05000 68-13097
1,2,4-Trichlorobenzene mg/kg wet0.0503 0.010 0.05000 66-125101
1,2-Dibromo-3-chloropropane mg/kg wet0.0504 0.0050 0.05000 55-157101
1,2-Dibromoethane mg/kg wet0.0438 0.0050 0.05000 70-13288
1,2-Dichlorobenzene mg/kg wet0.0496 0.010 0.05000 72-12399
1,2-Dichloroethane mg/kg wet0.0396 0.0050 0.05000 68-12879
1,2-Dichloropropane mg/kg wet0.0401 0.0050 0.05000 73-13080
1,3-Dichlorobenzene mg/kg wet0.0499 0.010 0.05000 71-120100
1,4-Dichlorobenzene mg/kg wet0.0496 0.010 0.05000 71-12399
1,4-Dioxane mg/kg wet0.448 0.10 0.5000 70-13090
Acetone mg/kg wet0.0775 0.020 0.1000 29-19878
Benzene mg/kg wet0.0401 0.0030 0.05000 74-12780
Bromochloromethane mg/kg wet0.0407 0.0050 0.05000 72-13481
Bromodichloromethane mg/kg wet0.0430 0.0050 0.05000 75-12286
Bromoform mg/kg wet0.0518 0.0050 0.05000 66-135104
Bromomethane mg/kg wet0.0407 0.010 0.05000 20-18081
Carbon disulfide mg/kg wet0.0404 0.010 0.05000 61-12981
Carbon Tetrachloride mg/kg wet0.0427 0.0050 0.05000 64-14385
Chlorobenzene mg/kg wet0.0442 0.0050 0.05000 74-11888
Chloroethane mg/kg wet0.0446 0.010 0.05000 33-14989
Chloroform mg/kg wet0.0409 0.0050 0.05000 73-12782
Chloromethane mg/kg wet0.0394 0.010 0.05000 45-14379
cis-1,2-Dichloroethylene mg/kg wet0.0383 0.0050 0.05000 76-13477
cis-1,3-Dichloropropylene mg/kg wet0.0407 0.0050 0.05000 71-12581
Cyclohexane mg/kg wet0.0392 0.0050 0.05000 70-13078
Dibromochloromethane mg/kg wet0.0488 0.0050 0.05000 73-12298
Dichlorodifluoromethane mg/kg wet0.0340 0.010 0.05000 26-14668
Ethylbenzene mg/kg wet0.0442 0.0050 0.05000 74-12888
Isopropylbenzene (Cumene)mg/kg wet0.0505 0.010 0.05000 68-126101
m,p-Xylenes mg/kg wet0.0898 0.010 0.1000 75-12490
Methyl Acetate mg/kg wet0.0402 0.0050 0.05000 70-13080
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0402 0.050 0.05000 J61-15780
Methylcyclohexane mg/kg wet0.0386 0.0050 0.05000 70-13077
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0358 0.020 0.05000 63-14972
Methyl Isobutyl Ketone mg/kg wet0.0386 0.010 0.05000 57-16277
Methylene Chloride mg/kg wet0.0374 0.010 0.05000 74-12975
Methyl-tert-Butyl Ether mg/kg wet0.0402 0.0050 0.05000 70-13080
o-Xylene mg/kg wet0.0441 0.0050 0.05000 74-12688
Styrene mg/kg wet0.0451 0.0050 0.05000 77-12190
Tetrachloroethylene mg/kg wet0.0390 0.010 0.05000 68-13078
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8B0460 - 5035
LCS (P8B0460-BS1)Prepared & Analyzed: 02/26/18
Toluene mg/kg wet0.0428 0.0050 0.05000 71-12986
trans-1,2-Dichloroethylene mg/kg wet0.0394 0.0050 0.05000 73-13279
trans-1,3-Dichloropropylene mg/kg wet0.0410 0.0050 0.05000 68-12382
Trichloroethylene mg/kg wet0.0410 0.0050 0.05000 75-13382
Trichlorofluoromethane mg/kg wet0.0444 0.0050 0.05000 44-14689
Vinyl chloride mg/kg wet0.0430 0.010 0.05000 48-14786
Xylenes, total mg/kg wet0.134 0.015 0.1500 74-12689
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10049.9
ug/L 50.00 76-129Surrogate: Toluene-d8 10854.2
LCS Dup (P8B0460-BSD1)Prepared & Analyzed: 02/26/18
1,1,1-Trichloroethane mg/kg wet0.0392 0.0050 0.05000 2067-13178 0.08
1,1,2,2-Tetrachloroethane mg/kg wet0.0497 0.0050 0.05000 2056-12699 2
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0397 0.010 0.05000 2070-13079 4
1,1,2-Trichloroethane mg/kg wet0.0446 0.0050 0.05000 2070-13389 1
1,1-Dichloroethane mg/kg wet0.0371 0.0050 0.05000 2074-12774 1
1,1-Dichloroethylene mg/kg wet0.0393 0.0050 0.05000 2067-14979 0.9
1,2,3-Trichlorobenzene mg/kg wet0.0498 0.010 0.05000 2068-130100 2
1,2,4-Trichlorobenzene mg/kg wet0.0510 0.010 0.05000 2066-125102 1
1,2-Dibromo-3-chloropropane mg/kg wet0.0517 0.0050 0.05000 2055-157103 2
1,2-Dibromoethane mg/kg wet0.0437 0.0050 0.05000 2070-13287 0.02
1,2-Dichlorobenzene mg/kg wet0.0505 0.010 0.05000 2072-123101 2
1,2-Dichloroethane mg/kg wet0.0403 0.0050 0.05000 2068-12881 2
1,2-Dichloropropane mg/kg wet0.0412 0.0050 0.05000 2073-13082 3
1,3-Dichlorobenzene mg/kg wet0.0499 0.010 0.05000 2071-120100 0.1
1,4-Dichlorobenzene mg/kg wet0.0506 0.010 0.05000 2071-123101 2
1,4-Dioxane mg/kg wet0.445 0.10 0.5000 2070-13089 0.8
Acetone mg/kg wet0.0765 0.020 0.1000 2029-19876 1
Benzene mg/kg wet0.0406 0.0030 0.05000 2074-12781 1
Bromochloromethane mg/kg wet0.0411 0.0050 0.05000 2072-13482 0.9
Bromodichloromethane mg/kg wet0.0433 0.0050 0.05000 2075-12287 0.9
Bromoform mg/kg wet0.0520 0.0050 0.05000 2066-135104 0.5
Bromomethane mg/kg wet0.0436 0.010 0.05000 2020-18087 7
Carbon disulfide mg/kg wet0.0378 0.010 0.05000 2061-12976 7
Carbon Tetrachloride mg/kg wet0.0425 0.0050 0.05000 2064-14385 0.6
Chlorobenzene mg/kg wet0.0441 0.0050 0.05000 2074-11888 0.07
Chloroethane mg/kg wet0.0455 0.010 0.05000 2033-14991 2
Chloroform mg/kg wet0.0414 0.0050 0.05000 2073-12783 1
Chloromethane mg/kg wet0.0376 0.010 0.05000 2045-14375 5
cis-1,2-Dichloroethylene mg/kg wet0.0389 0.0050 0.05000 2076-13478 2
cis-1,3-Dichloropropylene mg/kg wet0.0419 0.0050 0.05000 2071-12584 3
Cyclohexane mg/kg wet0.0394 0.0050 0.05000 2070-13079 0.6
Dibromochloromethane mg/kg wet0.0492 0.0050 0.05000 2073-12298 0.7
Dichlorodifluoromethane mg/kg wet0.0345 0.010 0.05000 2026-14669 2
Ethylbenzene mg/kg wet0.0441 0.0050 0.05000 2074-12888 0.2
Isopropylbenzene (Cumene)mg/kg wet0.0504 0.010 0.05000 2068-126101 0.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8B0460 - 5035
LCS Dup (P8B0460-BSD1)Prepared & Analyzed: 02/26/18
m,p-Xylenes mg/kg wet0.0895 0.010 0.1000 2075-12490 0.3
Methyl Acetate mg/kg wet0.0337 0.0050 0.05000 2070-13067 18
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0401 0.050 0.05000 20 J61-15780 0.1
Methylcyclohexane mg/kg wet0.0389 0.0050 0.05000 2070-13078 0.8
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0359 0.020 0.05000 2063-14972 0.3
Methyl Isobutyl Ketone mg/kg wet0.0391 0.010 0.05000 2057-16278 1
Methylene Chloride mg/kg wet0.0376 0.010 0.05000 2074-12975 0.6
Methyl-tert-Butyl Ether mg/kg wet0.0409 0.0050 0.05000 2070-13082 2
o-Xylene mg/kg wet0.0441 0.0050 0.05000 2074-12688 0.05
Styrene mg/kg wet0.0451 0.0050 0.05000 2077-12190 0.1
Tetrachloroethylene mg/kg wet0.0394 0.010 0.05000 2068-13079 1
Toluene mg/kg wet0.0434 0.0050 0.05000 2071-12987 1
trans-1,2-Dichloroethylene mg/kg wet0.0395 0.0050 0.05000 2073-13279 0.1
trans-1,3-Dichloropropylene mg/kg wet0.0422 0.0050 0.05000 2068-12384 3
Trichloroethylene mg/kg wet0.0415 0.0050 0.05000 2075-13383 1
Trichlorofluoromethane mg/kg wet0.0441 0.0050 0.05000 2044-14688 0.7
Vinyl chloride mg/kg wet0.0429 0.010 0.05000 2048-14786 0.4
Xylenes, total mg/kg wet0.134 0.015 0.1500 2074-12689 0.2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10050.1
ug/L 50.00 76-129Surrogate: Toluene-d8 10753.4
Matrix Spike (P8B0460-MS1)Prepared & Analyzed: 02/26/18 Source: 8020408-04
1,1,1-Trichloroethane mg/kg dry0.0531 0.0083 0.08274 BRL 52-13964
1,1,2,2-Tetrachloroethane mg/kg dry0.0660 0.0083 0.08274 BRL 39-13580
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg dry0.0581 0.017 0.08274 BRL 70-13070
1,1,2-Trichloroethane mg/kg dry0.0583 0.0083 0.08274 BRL 44-14070
1,1-Dichloroethane mg/kg dry0.0491 0.0083 0.08274 BRL 59-13759
1,1-Dichloroethylene mg/kg dry0.0541 0.0083 0.08274 BRL 54-16265
1,2,3-Trichlorobenzene mg/kg dry0.0637 0.017 0.08274 BRL 34-12077
1,2,4-Trichlorobenzene mg/kg dry0.0655 0.017 0.08274 BRL 35-11679
1,2-Dibromo-3-chloropropane mg/kg dry0.0623 0.0083 0.08274 BRL 27-13275
1,2-Dibromoethane mg/kg dry0.0569 0.0083 0.08274 BRL 49-13269
1,2-Dichlorobenzene mg/kg dry0.0666 0.017 0.08274 BRL 42-13081
1,2-Dichloroethane mg/kg dry0.0529 0.0083 0.08274 BRL 51-13164
1,2-Dichloropropane mg/kg dry0.0545 0.0083 0.08274 BRL 55-13866
1,3-Dichlorobenzene mg/kg dry0.0663 0.017 0.08274 BRL 41-12980
1,4-Dichlorobenzene mg/kg dry0.0668 0.017 0.08274 BRL 44-13481
1,4-Dioxane mg/kg dry0.577 0.17 0.8274 BRL 70-13070
Acetone mg/kg dry0.105 0.033 0.1655 BRL 34-14363
Benzene mg/kg dry0.0545 0.0050 0.08274 BRL 60-13566
Bromochloromethane mg/kg dry0.0539 0.0083 0.08274 BRL 55-13665
Bromodichloromethane mg/kg dry0.0554 0.0083 0.08274 BRL 55-12767
Bromoform mg/kg dry0.0631 0.0083 0.08274 BRL 40-13676
Bromomethane mg/kg dry0.0546 0.017 0.08274 BRL 30-13766
Carbon disulfide mg/kg dry0.0564 0.017 0.08274 BRL 49-13968
Carbon Tetrachloride mg/kg dry0.0562 0.0083 0.08274 BRL 48-15368
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8B0460 - 5035
Matrix Spike (P8B0460-MS1)Prepared & Analyzed: 02/26/18 Source: 8020408-04
Chlorobenzene mg/kg dry0.0592 0.0083 0.08274 BRL 57-12572
Chloroethane mg/kg dry0.0595 0.017 0.08274 BRL 16-17772
Chloroform mg/kg dry0.0546 0.0083 0.08274 BRL 56-13766
Chloromethane mg/kg dry0.0512 0.017 0.08274 BRL 40-14562
cis-1,2-Dichloroethylene mg/kg dry0.0520 0.0083 0.08274 BRL 58-14063
cis-1,3-Dichloropropylene mg/kg dry0.0530 0.0083 0.08274 BRL 42-13564
Cyclohexane mg/kg dry0.0542 0.0083 0.08274 BRL M70-13065
Dibromochloromethane mg/kg dry0.0620 0.0083 0.08274 BRL 49-12775
Dichlorodifluoromethane mg/kg dry0.0450 0.017 0.08274 BRL CCV25-15154
Ethylbenzene mg/kg dry0.0594 0.0083 0.08274 BRL 44-14472
Isopropylbenzene (Cumene)mg/kg dry0.0690 0.017 0.08274 BRL 41-14083
m,p-Xylenes mg/kg dry0.120 0.017 0.1655 BRL 36-14872
Methyl Acetate mg/kg dry0.0479 0.0083 0.08274 BRL M70-13058
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0508 0.083 0.08274 BRL J30-14761
Methylcyclohexane mg/kg dry0.0539 0.0083 0.08274 BRL M70-13065
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0464 0.033 0.08274 BRL 24-16056
Methyl Isobutyl Ketone mg/kg dry0.0490 0.017 0.08274 BRL 25-16359
Methylene Chloride mg/kg dry0.0496 0.017 0.08274 BRL 53-14460
Methyl-tert-Butyl Ether mg/kg dry0.0485 0.0083 0.08274 BRL 49-13559
o-Xylene mg/kg dry0.0584 0.0083 0.08274 BRL 43-14371
Styrene mg/kg dry0.0593 0.0083 0.08274 BRL 42-13272
Tetrachloroethylene mg/kg dry0.0525 0.017 0.08274 BRL 47-14263
Toluene mg/kg dry0.0571 0.0083 0.08274 BRL 57-13569
trans-1,2-Dichloroethylene mg/kg dry0.0528 0.0083 0.08274 BRL 58-14164
trans-1,3-Dichloropropylene mg/kg dry0.0527 0.0083 0.08274 BRL 41-12464
Trichloroethylene mg/kg dry0.0558 0.0083 0.08274 BRL 38-16467
Trichlorofluoromethane mg/kg dry0.0638 0.0083 0.08274 BRL 30-15777
Vinyl chloride mg/kg dry0.0562 0.017 0.08274 BRL 40-15668
Xylenes, total mg/kg dry0.178 0.025 0.2482 BRL 36-14872
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10050.2
ug/L 50.00 76-129Surrogate: Toluene-d8 10753.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8B0460 - 5035
Matrix Spike Dup (P8B0460-MSD1)Prepared & Analyzed: 02/26/18 Source: 8020408-04
1,1,1-Trichloroethane mg/kg dry0.0672 0.0081 0.08139 BRL 21 D52-13983 23
1,1,2,2-Tetrachloroethane mg/kg dry0.0813 0.0081 0.08139 BRL 2239-135100 21
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg dry0.0757 0.016 0.08139 BRL 20 D70-13093 26
1,1,2-Trichloroethane mg/kg dry0.0719 0.0081 0.08139 BRL 21 D44-14088 21
1,1-Dichloroethane mg/kg dry0.0621 0.0081 0.08139 BRL 21 D59-13776 23
1,1-Dichloroethylene mg/kg dry0.0700 0.0081 0.08139 BRL 22 D54-16286 26
1,2,3-Trichlorobenzene mg/kg dry0.0820 0.016 0.08139 BRL 4134-120101 25
1,2,4-Trichlorobenzene mg/kg dry0.0834 0.016 0.08139 BRL 6235-116102 24
1,2-Dibromo-3-chloropropane mg/kg dry0.0788 0.0081 0.08139 BRL 2527-13297 23
1,2-Dibromoethane mg/kg dry0.0707 0.0081 0.08139 BRL 15 D49-13287 22
1,2-Dichlorobenzene mg/kg dry0.0852 0.016 0.08139 BRL 21 D42-130105 24
1,2-Dichloroethane mg/kg dry0.0654 0.0081 0.08139 BRL 13 D51-13180 21
1,2-Dichloropropane mg/kg dry0.0682 0.0081 0.08139 BRL 16 D55-13884 22
1,3-Dichlorobenzene mg/kg dry0.0838 0.016 0.08139 BRL 24 D41-129103 23
1,4-Dichlorobenzene mg/kg dry0.0847 0.016 0.08139 BRL 21 D44-134104 24
1,4-Dioxane mg/kg dry0.706 0.16 0.8139 BRL 20 D70-13087 20
Acetone mg/kg dry0.126 0.033 0.1628 BRL 4934-14377 18
Benzene mg/kg dry0.0679 0.0049 0.08139 BRL 20 D60-13583 22
Bromochloromethane mg/kg dry0.0671 0.0081 0.08139 BRL 18 D55-13682 22
Bromodichloromethane mg/kg dry0.0709 0.0081 0.08139 BRL 17 D55-12787 24
Bromoform mg/kg dry0.0809 0.0081 0.08139 BRL 3540-13699 25
Bromomethane mg/kg dry0.0673 0.016 0.08139 BRL 3030-13783 21
Carbon disulfide mg/kg dry0.0740 0.016 0.08139 BRL 26 D49-13991 27
Carbon Tetrachloride mg/kg dry0.0710 0.0081 0.08139 BRL 23 D48-15387 23
Chlorobenzene mg/kg dry0.0747 0.0081 0.08139 BRL 14 D57-12592 23
Chloroethane mg/kg dry0.0776 0.016 0.08139 BRL 4716-17795 27
Chloroform mg/kg dry0.0685 0.0081 0.08139 BRL 18 D56-13784 23
Chloromethane mg/kg dry0.0677 0.016 0.08139 BRL 26 D40-14583 28
cis-1,2-Dichloroethylene mg/kg dry0.0653 0.0081 0.08139 BRL 2858-14080 23
cis-1,3-Dichloropropylene mg/kg dry0.0674 0.0081 0.08139 BRL 3242-13583 24
Cyclohexane mg/kg dry0.0682 0.0081 0.08139 BRL 20 D70-13084 23
Dibromochloromethane mg/kg dry0.0782 0.0081 0.08139 BRL 24 D49-12796 23
Dichlorodifluoromethane mg/kg dry0.0568 0.016 0.08139 BRL 37 CCV25-15170 23
Ethylbenzene mg/kg dry0.0743 0.0081 0.08139 BRL 19 D44-14491 22
Isopropylbenzene (Cumene)mg/kg dry0.0873 0.016 0.08139 BRL 2741-140107 23
m,p-Xylenes mg/kg dry0.150 0.016 0.1628 BRL 20 D36-14892 23
Methyl Acetate mg/kg dry0.0632 0.0081 0.08139 BRL 20 D70-13078 27
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0614 0.081 0.08139 BRL 42 J30-14775 19
Methylcyclohexane mg/kg dry0.0674 0.0081 0.08139 BRL 20 D70-13083 22
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0562 0.033 0.08139 BRL 4224-16069 19
Methyl Isobutyl Ketone mg/kg dry0.0596 0.016 0.08139 BRL 4425-16373 19
Methylene Chloride mg/kg dry0.0624 0.016 0.08139 BRL 14 D53-14477 23
Methyl-tert-Butyl Ether mg/kg dry0.0625 0.0081 0.08139 BRL 22 D49-13577 25
o-Xylene mg/kg dry0.0735 0.0081 0.08139 BRL 17 D43-14390 23
Styrene mg/kg dry0.0751 0.0081 0.08139 BRL 2842-13292 24
Tetrachloroethylene mg/kg dry0.0658 0.016 0.08139 BRL 2647-14281 22
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8B0460 - 5035
Matrix Spike Dup (P8B0460-MSD1)Prepared & Analyzed: 02/26/18 Source: 8020408-04
Toluene mg/kg dry0.0721 0.0081 0.08139 BRL 22 D57-13589 23
trans-1,2-Dichloroethylene mg/kg dry0.0668 0.0081 0.08139 BRL 18 D58-14182 24
trans-1,3-Dichloropropylene mg/kg dry0.0669 0.0081 0.08139 BRL 20 D41-12482 24
Trichloroethylene mg/kg dry0.0696 0.0081 0.08139 BRL 18 D38-16486 22
Trichlorofluoromethane mg/kg dry0.0808 0.0081 0.08139 BRL 2730-15799 23
Vinyl chloride mg/kg dry0.0720 0.016 0.08139 BRL 3540-15688 25
Xylenes, total mg/kg dry0.224 0.024 0.2442 BRL 20 D36-14892 23
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10552.7
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10049.8
ug/L 50.00 76-129Surrogate: Toluene-d8 10753.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Batch P8C0010 - 5035
Blank (P8C0010-BLK1)Prepared & Analyzed: 02/28/18
Cyclohexane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
o-Xylene mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10552.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.5
ug/L 50.00 70-130Surrogate: Toluene-d8 10652.8
LCS (P8C0010-BS1)Prepared & Analyzed: 02/28/18
Cyclohexane mg/kg wet0.0390 0.0050 0.05000 70-13078
Ethylbenzene mg/kg wet0.0455 0.0050 0.05000 69-12591
m,p-Xylenes mg/kg wet0.0912 0.010 0.1000 64-12591
o-Xylene mg/kg wet0.0449 0.0050 0.05000 69-12190
Xylenes, total mg/kg wet0.136 0.015 0.1500 74-12691
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10552.5
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10050.1
ug/L 50.00 70-130Surrogate: Toluene-d8 10853.8
LCS Dup (P8C0010-BSD1)Prepared & Analyzed: 02/28/18
Cyclohexane mg/kg wet0.0375 0.0050 0.05000 2070-13075 4
Ethylbenzene mg/kg wet0.0440 0.0050 0.05000 2069-12588 3
m,p-Xylenes mg/kg wet0.0887 0.010 0.1000 2064-12589 3
o-Xylene mg/kg wet0.0437 0.0050 0.05000 2069-12187 3
Xylenes, total mg/kg wet0.132 0.015 0.1500 20074-12688 3
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10452.1
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.5
ug/L 50.00 70-130Surrogate: Toluene-d8 10854.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8B0484 - 3546
LCS (P8B0484-BS2)Prepared & Analyzed: 02/28/18
1,1’-Biphenyl mg/kg wet1.26 0.33 1.667 40-11776
2,3,4,6-Tetrachlorophenol mg/kg wet1.34 0.33 1.667 44-12580
Atrazine mg/kg wet1.31 0.33 1.667 47-12779
Benzaldehyde mg/kg wet1.12 0.33 1.667 35-11567
Caprolactam mg/kg wet1.14 0.33 1.667 46-11768
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 832.76
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 841.40
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 852.83
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 721.20
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 802.65
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 901.51
LCS Dup (P8B0484-BSD2)Prepared & Analyzed: 02/28/18
1,1’-Biphenyl mg/kg wet1.13 0.33 1.667 2040-11768 11
2,3,4,6-Tetrachlorophenol mg/kg wet1.18 0.33 1.667 2044-12571 13
Atrazine mg/kg wet1.23 0.33 1.667 2047-12774 7
Benzaldehyde mg/kg wet1.04 0.33 1.667 2035-11562 7
Caprolactam mg/kg wet1.07 0.33 1.667 2046-11764 6
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 742.47
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 751.26
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 782.58
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 661.10
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 742.45
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 811.35
Matrix Spike (P8B0484-MS1)Prepared & Analyzed: 02/27/18 Source: 8020408-01
2,4,5-Trichlorophenol mg/kg dry1.47 0.42 2.114 BRL 41-12470
2,4,6-Trichlorophenol mg/kg dry1.36 0.42 2.114 BRL 39-12665
2,4-Dichlorophenol mg/kg dry1.28 0.42 2.114 BRL 40-12261
2,4-Dimethylphenol mg/kg dry1.56 0.42 2.114 BRL 30-12774
2,4-Dinitrophenol mg/kg dry1.02 0.42 2.114 BRL 27-12948
2,4-Dinitrotoluene mg/kg dry1.26 0.42 2.114 BRL 48-12660
2,6-Dinitrotoluene mg/kg dry1.34 0.42 2.114 BRL 46-12463
2-Chloronaphthalene mg/kg dry1.46 0.42 2.114 BRL 41-11469
2-Chlorophenol mg/kg dry1.27 0.42 2.114 BRL 34-12160
2-Methylnaphthalene mg/kg dry1.24 0.42 2.114 BRL 38-12259
2-Methylphenol mg/kg dry1.37 0.42 2.114 BRL 32-12265
2-Nitroaniline mg/kg dry1.28 0.42 2.114 BRL 44-12761
2-Nitrophenol mg/kg dry1.19 0.42 2.114 BRL 36-12356
3,3’-Dichlorobenzidine mg/kg dry0.758 0.42 2.114 BRL 22-12136
3/4-Methylphenol mg/kg dry1.16 0.42 2.114 BRL 34-11955
3-Nitroaniline mg/kg dry1.03 0.42 2.114 BRL 33-11949
4,6-Dinitro-2-methylphenol mg/kg dry0.995 0.42 2.114 BRL 29-13247
4-Bromophenyl phenyl ether mg/kg dry1.37 0.42 2.114 BRL 46-12465
4-Chloro-3-methylphenol mg/kg dry1.28 0.42 2.114 BRL 45-12261
4-Chloroaniline mg/kg dry0.867 0.42 2.114 BRL 17-10641
4-Chlorophenyl phenyl ether mg/kg dry1.31 0.42 2.114 BRL 45-12162
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8B0484 - 3546
Matrix Spike (P8B0484-MS1)Prepared & Analyzed: 02/27/18 Source: 8020408-01
4-Nitroaniline mg/kg dry0.979 0.42 2.114 BRL M63-14746
4-Nitrophenol mg/kg dry1.40 0.42 2.114 BRL 30-13266
Acenaphthene mg/kg dry1.38 0.42 2.114 BRL 40-12365
Acenaphthylene mg/kg dry1.45 0.42 2.114 BRL 32-13268
Acetophenone mg/kg dry1.20 0.42 2.114 BRL 33-11557
Anthracene mg/kg dry1.46 0.42 2.114 BRL 47-12369
Benzo(a)anthracene mg/kg dry1.54 0.42 2.114 BRL 49-12673
Benzo(a)pyrene mg/kg dry1.41 0.42 2.114 BRL 45-12967
Benzo(b)fluoranthene mg/kg dry1.48 0.42 2.114 BRL 45-13270
Benzo(g,h,i)perylene mg/kg dry1.14 0.42 2.114 BRL 43-13454
Benzo(k)fluoranthene mg/kg dry1.32 0.42 2.114 BRL 47-13262
bis(2-Chloroethoxy)methane mg/kg dry1.21 0.42 2.114 BRL 36-12157
Bis(2-Chloroethyl)ether mg/kg dry2.13 0.42 2.114 BRL 31-120101
Bis(2-chloroisopropyl)ether mg/kg dry1.09 0.42 2.114 BRL 33-13152
Bis(2-Ethylhexyl)phthalate mg/kg dry1.50 0.42 2.114 BRL 51-13371
Butyl benzyl phthalate mg/kg dry1.32 0.42 2.114 BRL 48-13263
Carbazole mg/kg dry1.41 0.42 2.114 BRL 50-12367
Chrysene mg/kg dry1.50 0.42 2.114 BRL 50-12471
Dibenzo(a,h)anthracene mg/kg dry0.959 0.42 2.114 BRL 45-13445
Dibenzofuran mg/kg dry1.33 0.42 2.114 BRL 44-12063
Diethyl phthalate mg/kg dry1.30 0.42 2.114 BRL 50-12461
Dimethyl phthalate mg/kg dry1.32 0.42 2.114 BRL 48-12462
Di-n-butyl phthalate mg/kg dry1.44 0.42 2.114 BRL 51-12868
Di-n-octyl phthalate mg/kg dry1.47 0.42 2.114 BRL 45-14070
Fluoranthene mg/kg dry1.52 0.42 2.114 BRL 50-12772
Fluorene mg/kg dry1.36 0.42 2.114 BRL 43-12564
Hexachlorobenzene mg/kg dry1.29 0.42 2.114 BRL 45-12261
Hexachlorobutadiene mg/kg dry1.21 0.42 2.114 BRL 32-12357
Hexachlorocyclopentadiene mg/kg dry0.128 0.42 2.114 BRL M, J32-1176
Hexachloroethane mg/kg dry1.01 0.42 2.114 BRL 28-11748
Indeno(1,2,3-cd)pyrene mg/kg dry1.45 0.42 2.114 BRL 45-13369
Isophorone mg/kg dry1.15 0.42 2.114 BRL 30-12254
Naphthalene mg/kg dry1.27 0.42 2.114 BRL 35-12360
Nitrobenzene mg/kg dry1.01 0.42 2.114 BRL 34-12248
N-Nitroso-di-n-propylamine mg/kg dry1.15 0.42 2.114 BRL 36-12055
N-Nitrosodiphenylamine mg/kg dry2.80 0.42 2.114 0.752 38-12797
Pentachlorophenol mg/kg dry1.77 0.42 2.114 BRL 25-13384
Phenanthrene mg/kg dry1.55 0.42 2.114 BRL 50-12174
Phenol mg/kg dry1.28 0.42 2.114 BRL 34-12161
Pyrene mg/kg dry1.45 0.42 2.114 BRL 47-12768
mg/kg dry 4.229 37-131Surrogate: 2,4,6-Tribromophenol 582.46
mg/kg dry 2.114 47-130Surrogate: 2-Fluorobiphenyl 571.21
mg/kg dry 4.229 44-117Surrogate: 2-Fluorophenol 552.33
mg/kg dry 2.114 45-121Surrogate: Nitrobenzene-d5 460.965
mg/kg dry 4.229 37-127Surrogate: Phenol-d5 512.17
mg/kg dry 2.114 38-135Surrogate: Terphenyl-d14 561.19
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8B0484 - 3546
Matrix Spike Dup (P8B0484-MSD1)Prepared & Analyzed: 02/27/18 Source: 8020408-01
2,4,5-Trichlorophenol mg/kg dry1.50 0.42 2.118 BRL 2041-12471 2
2,4,6-Trichlorophenol mg/kg dry1.40 0.42 2.118 BRL 2039-12666 3
2,4-Dichlorophenol mg/kg dry1.32 0.42 2.118 BRL 2040-12262 3
2,4-Dimethylphenol mg/kg dry1.65 0.42 2.118 BRL 2030-12778 6
2,4-Dinitrophenol mg/kg dry1.12 0.42 2.118 BRL 2027-12953 9
2,4-Dinitrotoluene mg/kg dry1.31 0.42 2.118 BRL 2048-12662 4
2,6-Dinitrotoluene mg/kg dry1.39 0.42 2.118 BRL 2046-12466 4
2-Chloronaphthalene mg/kg dry1.50 0.42 2.118 BRL 2041-11471 3
2-Chlorophenol mg/kg dry1.31 0.42 2.118 BRL 2034-12162 2
2-Methylnaphthalene mg/kg dry1.30 0.42 2.118 BRL 2038-12262 5
2-Methylphenol mg/kg dry1.39 0.42 2.118 BRL 2032-12266 2
2-Nitroaniline mg/kg dry1.32 0.42 2.118 BRL 2044-12762 3
2-Nitrophenol mg/kg dry1.29 0.42 2.118 BRL 2036-12361 8
3,3’-Dichlorobenzidine mg/kg dry1.32 0.42 2.118 BRL 20 D22-12163 54
3/4-Methylphenol mg/kg dry1.17 0.42 2.118 BRL 2034-11955 1
3-Nitroaniline mg/kg dry1.21 0.42 2.118 BRL 2033-11957 16
4,6-Dinitro-2-methylphenol mg/kg dry1.12 0.42 2.118 BRL 2029-13253 12
4-Bromophenyl phenyl ether mg/kg dry1.40 0.42 2.118 BRL 2046-12466 2
4-Chloro-3-methylphenol mg/kg dry1.30 0.42 2.118 BRL 2045-12261 1
4-Chloroaniline mg/kg dry1.07 0.42 2.118 BRL 20 D17-10650 21
4-Chlorophenyl phenyl ether mg/kg dry1.32 0.42 2.118 BRL 2045-12162 0.7
4-Nitroaniline mg/kg dry1.14 0.42 2.118 BRL 20 M63-14754 15
4-Nitrophenol mg/kg dry1.38 0.42 2.118 BRL 2030-13265 1
Acenaphthene mg/kg dry1.43 0.42 2.118 BRL 2040-12367 3
Acenaphthylene mg/kg dry1.49 0.42 2.118 BRL 2032-13271 3
Acetophenone mg/kg dry1.19 0.42 2.118 BRL 2033-11556 0.5
Anthracene mg/kg dry1.49 0.42 2.118 BRL 2047-12370 2
Benzo(a)anthracene mg/kg dry1.49 0.42 2.118 BRL 2049-12670 3
Benzo(a)pyrene mg/kg dry1.43 0.42 2.118 BRL 2045-12968 1
Benzo(b)fluoranthene mg/kg dry1.49 0.42 2.118 BRL 2045-13271 1
Benzo(g,h,i)perylene mg/kg dry1.17 0.42 2.118 BRL 2043-13455 3
Benzo(k)fluoranthene mg/kg dry1.31 0.42 2.118 BRL 2047-13262 1
bis(2-Chloroethoxy)methane mg/kg dry1.26 0.42 2.118 BRL 2036-12160 4
Bis(2-Chloroethyl)ether mg/kg dry1.19 0.42 2.118 BRL 20 D31-12056 56
Bis(2-chloroisopropyl)ether mg/kg dry1.08 0.42 2.118 BRL 2033-13151 1
Bis(2-Ethylhexyl)phthalate mg/kg dry1.50 0.42 2.118 BRL 2051-13371 0.4
Butyl benzyl phthalate mg/kg dry1.32 0.42 2.118 BRL 2048-13262 0.4
Carbazole mg/kg dry1.44 0.42 2.118 BRL 2050-12368 2
Chrysene mg/kg dry1.50 0.42 2.118 BRL 2050-12471 0.4
Dibenzo(a,h)anthracene mg/kg dry0.961 0.42 2.118 BRL 2045-13445 0.3
Dibenzofuran mg/kg dry1.35 0.42 2.118 BRL 2044-12064 2
Diethyl phthalate mg/kg dry1.29 0.42 2.118 BRL 2050-12461 0.5
Dimethyl phthalate mg/kg dry1.34 0.42 2.118 BRL 2048-12463 1
Di-n-butyl phthalate mg/kg dry1.45 0.42 2.118 BRL 2051-12868 0.4
Di-n-octyl phthalate mg/kg dry1.48 0.42 2.118 BRL 2045-14070 0.8
Fluoranthene mg/kg dry1.53 0.42 2.118 BRL 2050-12772 0.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8B0484 - 3546
Matrix Spike Dup (P8B0484-MSD1)Prepared & Analyzed: 02/27/18 Source: 8020408-01
Fluorene mg/kg dry1.38 0.42 2.118 BRL 2043-12565 2
Hexachlorobenzene mg/kg dry1.33 0.42 2.118 BRL 2045-12263 3
Hexachlorobutadiene mg/kg dry1.27 0.42 2.118 BRL 2032-12360 5
Hexachlorocyclopentadiene mg/kg dryBRL0.42 2.118 BRL 20 D32-117
Hexachloroethane mg/kg dry1.05 0.42 2.118 BRL 2028-11749 3
Indeno(1,2,3-cd)pyrene mg/kg dry1.49 0.42 2.118 BRL 2045-13370 2
Isophorone mg/kg dry1.20 0.42 2.118 BRL 2030-12257 5
Naphthalene mg/kg dry1.37 0.42 2.118 BRL 2035-12365 8
Nitrobenzene mg/kg dry1.07 0.42 2.118 BRL 2034-12250 5
N-Nitroso-di-n-propylamine mg/kg dry1.16 0.42 2.118 BRL 2036-12055 0.8
N-Nitrosodiphenylamine mg/kg dry2.49 0.42 2.118 0.752 2038-12782 12
Pentachlorophenol mg/kg dry1.77 0.42 2.118 BRL 2025-13384 0.1
Phenanthrene mg/kg dry1.55 0.42 2.118 BRL 2050-12173 0.4
Phenol mg/kg dry1.33 0.42 2.118 BRL 2034-12163 3
Pyrene mg/kg dry1.44 0.42 2.118 BRL 2047-12768 0.07
mg/kg dry 4.236 37-131Surrogate: 2,4,6-Tribromophenol 723.06
mg/kg dry 2.118 47-130Surrogate: 2-Fluorobiphenyl 701.48
mg/kg dry 4.236 44-117Surrogate: 2-Fluorophenol 662.81
mg/kg dry 2.118 45-121Surrogate: Nitrobenzene-d5 571.22
mg/kg dry 4.236 37-127Surrogate: Phenol-d5 632.66
mg/kg dry 2.118 38-135Surrogate: Terphenyl-d14 671.43
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8B0445 - 3050B
Blank (P8B0445-BLK1)Prepared: 02/26/18 Analyzed: 03/01/18
Antimony mg/kg wet0.488 0.50 A, J
Arsenic mg/kg wetBRL1.5
Beryllium mg/kg wetBRL0.25
Cadmium mg/kg wet0.0362 0.25 J
Chromium mg/kg wet0.260 0.50 BH, J
Copper mg/kg wet0.312 0.50 BH, J
Lead mg/kg wet0.0880 0.25 J
Manganese mg/kg wet1.23 2.5 J
Nickel mg/kg wet0.193 0.25 BH, J
Selenium mg/kg wetBRL1.0
Silver mg/kg wet0.0675 0.25 J
Thallium mg/kg wet0.0345 0.25 J
Zinc mg/kg wet2.09 20 J
LCS (P8B0445-BS1)Prepared: 02/26/18 Analyzed: 03/01/18
Antimony mg/kg wet14.4 0.50 12.50 B80-120115
Arsenic mg/kg wet12.8 1.5 12.50 80-120102
Beryllium mg/kg wet12.2 0.25 12.50 80-12098
Cadmium mg/kg wet13.4 0.25 12.50 80-120107
Chromium mg/kg wet13.2 0.50 12.50 B80-120106
Copper mg/kg wet14.2 0.50 12.50 B80-120114
Lead mg/kg wet13.6 0.25 12.50 80-120109
Manganese mg/kg wet13.2 2.5 12.50 80-120106
Nickel mg/kg wet13.8 0.25 12.50 B80-120111
Selenium mg/kg wet12.9 1.0 12.50 80-120103
Silver mg/kg wet5.63 0.25 5.000 80-120113
Thallium mg/kg wet13.5 0.25 12.50 80-120108
Zinc mg/kg wet14.3 20 12.50 J80-120114
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8B0445 - 3050B
Matrix Spike (P8B0445-MS1)Prepared: 02/26/18 Analyzed: 03/01/18 Source: 8020408-01
Antimony mg/kg dry3.42 0.63 15.81 0.634 M, B75-12518
Arsenic mg/kg dry13.6 1.9 15.81 1.79 75-12575
Beryllium mg/kg dry17.7 0.32 15.80 1.75 75-125101
Cadmium mg/kg dry16.9 0.32 15.81 0.114 75-125106
Chromium mg/kg dry20.4 0.63 15.81 3.44 B75-125107
Copper mg/kg dry75.5 0.63 15.81 40.6 M, B75-125221
Lead mg/kg dry37.0 0.32 15.81 16.4 M75-125130
Manganese mg/kg dry3943.2 15.81 316 MC75-125495
Nickel mg/kg dry35.8 0.32 15.81 15.4 M, B75-125129
Selenium mg/kg dry18.4 1.3 15.81 5.34 75-12583
Silver mg/kg dry6.73 0.32 6.324 0.0490 75-125106
Thallium mg/kg dry16.9 0.32 15.81 0.0458 75-125107
Zinc mg/kg dry51825 15.81 345 MC75-125NR
Matrix Spike Dup (P8B0445-MSD1)Prepared: 02/26/18 Analyzed: 03/01/18 Source: 8020408-01
Antimony mg/kg dry1.63 0.63 15.81 0.634 20 D, M, B75-1256 71
Arsenic mg/kg dry13.4 1.9 15.81 1.79 20 M75-12574 1
Beryllium mg/kg dry17.8 0.32 15.80 1.75 2075-125102 0.4
Cadmium mg/kg dry17.4 0.32 15.81 0.114 2075-125109 3
Chromium mg/kg dry22.7 0.63 15.81 3.44 20 B75-125122 11
Copper mg/kg dry66.2 0.63 15.81 40.6 20 M, B75-125162 13
Lead mg/kg dry35.0 0.32 15.81 16.4 2075-125117 6
Manganese mg/kg dry4283.2 15.81 316 20 MC75-125707 8
Nickel mg/kg dry36.3 0.32 15.81 15.4 20 M, B75-125132 1
Selenium mg/kg dry17.3 1.3 15.81 5.34 2075-12576 6
Silver mg/kg dry6.95 0.32 6.324 0.0490 2075-125109 3
Thallium mg/kg dry17.4 0.32 15.81 0.0458 2075-125110 3
Zinc mg/kg dry43325 15.81 345 20 MC75-125558 18
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8B0445 - 3050B
Post Spike (P8B0445-PS1)Prepared: 02/26/18 Analyzed: 03/01/18 Source: 8020408-01
Antimony ug/L107 100.0 1.99 B80-120105
Arsenic ug/L104 100.0 5.62 80-12099
Beryllium ug/L111 100.0 5.50 80-120105
Cadmium ug/L101 100.0 0.359 80-120101
Chromium ug/L112 100.0 10.8 B80-120101
Copper ug/L235 100.0 128 B80-120108
Lead ug/L153 100.0 51.8 80-120102
Manganese ug/L1130 100.0 995 MC80-120139
Nickel ug/L155 100.0 48.5 B80-120106
Selenium ug/L115 100.0 16.8 80-12099
Silver ug/L106 100.0 0.154 80-120106
Thallium ug/L102 100.0 0.144 80-120102
Zinc ug/L1210 100.0 1090 MC80-120121
Batch P8B0496 - 7471B
Blank (P8B0496-BLK1)Prepared & Analyzed: 02/28/18
Mercury mg/kg wetBRL0.020
LCS (P8B0496-BS1)Prepared & Analyzed: 02/28/18
Mercury mg/kg wet0.448 0.020 0.4167 80-120108
Matrix Spike (P8B0496-MS1)Prepared & Analyzed: 02/28/18 Source: 8020408-01
Mercury mg/kg dry0.598 0.025 0.5296 BRL 80-120113
Matrix Spike Dup (P8B0496-MSD1)Prepared & Analyzed: 02/28/18 Source: 8020408-01
Mercury mg/kg dry0.574 0.025 0.5126 BRL 2080-120112 4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 36
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8020408
Time Submitted: 2/22/2018 4:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P8B0458 - Solids, Dry Weight
Duplicate (P8B0458-DUP2)Prepared & Analyzed: 02/23/18 Source: 8020408-01
% Solids % by Weight80.0 0.100 78.7 202
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 36
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P8B04588020408-01 02/23/18 15:133030gg
P8B04588020408-02 02/23/18 15:133030gg
P8B04588020408-03 02/23/18 15:133030gg
P8B04588020408-04 02/23/18 15:133030gg
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P8B04848020408-01 02/27/18 10:5730.02 1g mL
P8B04848020408-01 02/27/18 10:5730.02 1g mL
P8B04848020408-02 02/27/18 10:5730.04 1g mL
P8B04848020408-02 02/27/18 10:5730.04 1g mL
P8B04848020408-03 02/27/18 10:5730.03 1g mL
P8B04848020408-03 02/27/18 10:5730.03 1g mL
P8B04848020408-04 02/27/18 10:5730.01 1g mL
P8B04848020408-04 02/27/18 10:5730.01 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P8B04458020408-01 02/27/18 7:452.01 50g mL
P8B04458020408-02 02/27/18 7:452.02 50g mL
P8B04458020408-03 02/27/18 7:452.01 50g mL
P8B04458020408-03 02/27/18 7:452.01 50g mL
P8B04458020408-04 02/27/18 7:452.01 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P8B04968020408-01 02/28/18 8:050.62 50g mL
P8B04968020408-02 02/28/18 8:050.64 50g mL
P8B04968020408-03 02/28/18 8:050.55 50g mL
P8B04968020408-04 02/28/18 8:050.65 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P8B04608020408-01 02/26/18 9:225.58 5g mL
P8B04608020408-02 02/26/18 9:226.02 5g mL
P8B04608020408-03 02/26/18 9:223.04 5g mL
P8B04608020408-04 02/26/18 9:225.34 5g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P8C00108020408-01 02/28/18 9:555.48 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 36
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
03/28/2018
Hart & Hickman (Charlotte)
John Lopez
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: LRC-006 Continental Tire
Lab Submittal Date: 03/14/2018
Prism Work Order: 8030236
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 19
Sample Receipt Summary
03/28/2018
Prism Work Order: 8030236
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
8030236-01 03/14/18TMW-3 03/14/18Water
8030236-02 03/14/18TMW-4 03/14/18Water
8030236-03 03/14/18Dup-1 03/14/18Water
8030236-04 03/14/18Trip Blank 03/14/18Water
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-01
Prism Work Order: 8030236
Time Collected: 03/14/18 13:45
Time Submitted: 03/14/18 16:35
TMW-3
Volatile Organic Compounds by GC/MS
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0611,1,1-Trichloroethane 2.8
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0361,1,2,2-Tetrachloroethane <1.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.0791,1,2-Trichloro-1,2,2-trifluoroethane <5.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0661,1,2-Trichloroethane <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0831,1-Dichloroethane 2.6
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0831,1-Dichloroethylene 2.3
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.401,2,3-Trichlorobenzene <2.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.131,2,4-Trichlorobenzene <1.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.171,2-Dibromo-3-chloropropane <2.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0511,2-Dibromoethane <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0761,2-Dichlorobenzene <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0661,2-Dichloroethane <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.111,2-Dichloropropane <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0541,3-Dichlorobenzene <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.0501,4-Dichlorobenzene <1.0
8260B P8C031811503/20/18 15:34 KDMug/L 141,4-Dioxane <150
8260B P8C03181103/20/18 15:34 KDMug/L 0.31Acetone14
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.048Benzene<1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.14Bromochloromethane<1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.062Bromodichloromethane<1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.040Bromoform<1.0
8260B P8C031813.0 3/20/18 15:34 KDMug/L 0.18Bromomethane<3.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.075Carbon disulfide <5.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.11Carbon Tetrachloride <2.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.062Chlorobenzene<1.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.22Chloroethane<5.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.076Chloroform<1.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.079Chloromethane<2.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.056cis-1,2-Dichloroethylene 3.1
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.079cis-1,3-Dichloropropylene <1.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.022Cyclohexane<5.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.081Dibromochloromethane<1.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.11Dichlorodifluoromethane<2.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.061Ethylbenzene<1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.054Isopropylbenzene (Cumene)<1.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.12m,p-Xylenes <2.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.24Methyl Acetate <5.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)<5.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.076Methylcyclohexane<5.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)<5.0
8260B P8C031815.0 3/20/18 15:34 KDMug/L 0.078Methyl Isobutyl Ketone <5.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.083Methylene Chloride <2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-01
Prism Work Order: 8030236
Time Collected: 03/14/18 13:45
Time Submitted: 03/14/18 16:35
TMW-3
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.042Methyl-tert-Butyl Ether <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.044o-Xylene <1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.047Styrene<1.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.098Tetrachloroethylene4.1
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.044Toluene<1.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.094trans-1,2-Dichloroethylene <2.0
8260B P8C031811.0 3/20/18 15:34 KDMug/L 0.070trans-1,3-Dichloropropylene <1.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.078Trichloroethylene15
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.062Trichlorofluoromethane<2.0
8260B P8C031812.0 3/20/18 15:34 KDMug/L 0.097Vinyl chloride <2.0
8260B P8C031813.0 3/20/18 15:34 KDMug/L 0.15Xylenes, total <3.0
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129102 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-02
Prism Work Order: 8030236
Time Collected: 03/14/18 15:50
Time Submitted: 03/14/18 16:35
TMW-4
Volatile Organic Compounds by GC/MS
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0611,1,1-Trichloroethane 3.2
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane <1.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.0791,1,2-Trichloro-1,2,2-trifluoroethane <5.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0661,1,2-Trichloroethane <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0831,1-Dichloroethane 3.3
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0831,1-Dichloroethylene <1.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.401,2,3-Trichlorobenzene <2.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.131,2,4-Trichlorobenzene <1.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.171,2-Dibromo-3-chloropropane <2.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0511,2-Dibromoethane <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0761,2-Dichlorobenzene <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0661,2-Dichloroethane <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.111,2-Dichloropropane <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0541,3-Dichlorobenzene <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.0501,4-Dichlorobenzene <1.0
8260B P8C029811503/19/18 14:51 KDMug/L 141,4-Dioxane <150
8260B P8C02981103/19/18 14:51 KDMug/L 0.31Acetone150
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.048Benzene<1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.14Bromochloromethane<1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.062Bromodichloromethane<1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.040Bromoform<1.0
8260B P8C029813.0 3/19/18 14:51 KDMug/L 0.18Bromomethane<3.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.075Carbon disulfide <5.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.11Carbon Tetrachloride <2.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.062Chlorobenzene<1.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.22Chloroethane<5.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.076Chloroform<1.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.079Chloromethane<2.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.056cis-1,2-Dichloroethylene 5.2
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.079cis-1,3-Dichloropropylene <1.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.022Cyclohexane<5.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.081Dibromochloromethane<1.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.11Dichlorodifluoromethane<2.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.061Ethylbenzene<1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.054Isopropylbenzene (Cumene)<1.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.12m,p-Xylenes <2.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.24Methyl Acetate <5.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)<5.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.076Methylcyclohexane<5.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)<5.0
8260B P8C029815.0 3/19/18 14:51 KDMug/L 0.078Methyl Isobutyl Ketone <5.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.083Methylene Chloride <2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-02
Prism Work Order: 8030236
Time Collected: 03/14/18 15:50
Time Submitted: 03/14/18 16:35
TMW-4
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.042Methyl-tert-Butyl Ether <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.044o-Xylene <1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.047Styrene<1.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.098Tetrachloroethylene2.6
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.044Toluene<1.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.094trans-1,2-Dichloroethylene <2.0
8260B P8C029811.0 3/19/18 14:51 KDMug/L 0.070trans-1,3-Dichloropropylene <1.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.078Trichloroethylene8.3
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.062Trichlorofluoromethane<2.0
8260B P8C029812.0 3/19/18 14:51 KDMug/L 0.097Vinyl chloride <2.0
8260B P8C029813.0 3/19/18 14:51 KDMug/L 0.15Xylenes, total <3.0
Surrogate Recovery Control Limits
80-12499 %4-Bromofluorobenzene
75-129104 %Dibromofluoromethane
77-12393 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-03
Prism Work Order: 8030236
Time Collected: 03/14/18 00:00
Time Submitted: 03/14/18 16:35
Dup-1
Volatile Organic Compounds by GC/MS
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0611,1,1-Trichloroethane 2.1
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0361,1,2,2-Tetrachloroethane <1.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.0791,1,2-Trichloro-1,2,2-trifluoroethane <5.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0661,1,2-Trichloroethane <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0831,1-Dichloroethane 2.8
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0831,1-Dichloroethylene 1.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.401,2,3-Trichlorobenzene <2.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.131,2,4-Trichlorobenzene <1.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.171,2-Dibromo-3-chloropropane <2.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0511,2-Dibromoethane <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0761,2-Dichlorobenzene <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0661,2-Dichloroethane <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.111,2-Dichloropropane <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0541,3-Dichlorobenzene <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.0501,4-Dichlorobenzene <1.0
8260B P8C029811503/19/18 15:25 KDMug/L 141,4-Dioxane <150
8260B P8C02981103/19/18 15:25 KDMug/L 0.31Acetone18
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.048Benzene<1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.14Bromochloromethane<1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.062Bromodichloromethane<1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.040Bromoform<1.0
8260B P8C029813.0 3/19/18 15:25 KDMug/L 0.18Bromomethane<3.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.075Carbon disulfide <5.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.11Carbon Tetrachloride <2.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.062Chlorobenzene<1.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.22Chloroethane<5.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.076Chloroform<1.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.079Chloromethane<2.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.056cis-1,2-Dichloroethylene 3.4
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.079cis-1,3-Dichloropropylene <1.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.022Cyclohexane<5.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.081Dibromochloromethane<1.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.11Dichlorodifluoromethane<2.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.061Ethylbenzene<1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.054Isopropylbenzene (Cumene)<1.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.12m,p-Xylenes <2.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.24Methyl Acetate <5.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)<5.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.076Methylcyclohexane<5.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)<5.0
8260B P8C029815.0 3/19/18 15:25 KDMug/L 0.078Methyl Isobutyl Ketone <5.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.083Methylene Chloride <2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-03
Prism Work Order: 8030236
Time Collected: 03/14/18 00:00
Time Submitted: 03/14/18 16:35
Dup-1
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.042Methyl-tert-Butyl Ether <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.044o-Xylene <1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.047Styrene<1.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.098Tetrachloroethylene4.2
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.044Toluene<1.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.094trans-1,2-Dichloroethylene <2.0
8260B P8C029811.0 3/19/18 15:25 KDMug/L 0.070trans-1,3-Dichloropropylene <1.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.078Trichloroethylene16
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.062Trichlorofluoromethane<2.0
8260B P8C029812.0 3/19/18 15:25 KDMug/L 0.097Vinyl chloride <2.0
8260B P8C029813.0 3/19/18 15:25 KDMug/L 0.15Xylenes, total <3.0
Surrogate Recovery Control Limits
80-12497 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-12392 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-04
Prism Work Order: 8030236
Time Collected: 03/14/18 00:00
Time Submitted: 03/14/18 16:35
Trip Blank
Volatile Organic Compounds by GC/MS
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0611,1,1-Trichloroethane <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0361,1,2,2-Tetrachloroethane <1.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.0791,1,2-Trichloro-1,2,2-trifluoroethane <5.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0661,1,2-Trichloroethane <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0831,1-Dichloroethane <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0831,1-Dichloroethylene <1.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.401,2,3-Trichlorobenzene <2.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.131,2,4-Trichlorobenzene <1.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.171,2-Dibromo-3-chloropropane <2.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0511,2-Dibromoethane <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0761,2-Dichlorobenzene <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0661,2-Dichloroethane <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.111,2-Dichloropropane <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0541,3-Dichlorobenzene <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.0501,4-Dichlorobenzene <1.0
8260B P8C029811503/19/18 14:17 KDMug/L 141,4-Dioxane <150
8260B P8C02981103/19/18 14:17 KDMug/L 0.31Acetone<10
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.048Benzene<1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.14Bromochloromethane<1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.062Bromodichloromethane<1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.040Bromoform<1.0
8260B P8C029813.0 3/19/18 14:17 KDMug/L 0.18Bromomethane<3.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.075Carbon disulfide <5.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.11Carbon Tetrachloride <2.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.062Chlorobenzene<1.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.22Chloroethane<5.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.076Chloroform<1.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.079Chloromethane<2.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.056cis-1,2-Dichloroethylene <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.079cis-1,3-Dichloropropylene <1.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.022Cyclohexane<5.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.081Dibromochloromethane<1.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.11Dichlorodifluoromethane<2.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.061Ethylbenzene<1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.054Isopropylbenzene (Cumene)<1.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.12m,p-Xylenes <2.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.24Methyl Acetate <5.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)<5.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.076Methylcyclohexane<5.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)<5.0
8260B P8C029815.0 3/19/18 14:17 KDMug/L 0.078Methyl Isobutyl Ketone <5.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.083Methylene Chloride <2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 19
Laboratory Report
03/28/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Sample Matrix: Water
Client Sample ID:
Prism Sample ID: 8030236-04
Prism Work Order: 8030236
Time Collected: 03/14/18 00:00
Time Submitted: 03/14/18 16:35
Trip Blank
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.042Methyl-tert-Butyl Ether <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.044o-Xylene <1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.047Styrene<1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.098Tetrachloroethylene<1.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.044Toluene<1.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.094trans-1,2-Dichloroethylene <2.0
8260B P8C029811.0 3/19/18 14:17 KDMug/L 0.070trans-1,3-Dichloropropylene <1.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.078Trichloroethylene<2.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.062Trichlorofluoromethane<2.0
8260B P8C029812.0 3/19/18 14:17 KDMug/L 0.097Vinyl chloride <2.0
8260B P8C029813.0 3/19/18 14:17 KDMug/L 0.15Xylenes, total <3.0
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-129103 %Dibromofluoromethane
77-12392 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0298 - 5030B
Blank (P8C0298-BLK1)Prepared & Analyzed: 03/19/18
1,1,1-Trichloroethane ug/LBRL1.0
1,1,2,2-Tetrachloroethane ug/LBRL1.0
1,1,2-Trichloro-1,2,2-trifluoroethane ug/LBRL5.0
1,1,2-Trichloroethane ug/LBRL1.0
1,1-Dichloroethane ug/LBRL1.0
1,1-Dichloroethylene ug/LBRL1.0
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL1.0
1,2-Dichlorobenzene ug/LBRL1.0
1,2-Dichloroethane ug/LBRL1.0
1,2-Dichloropropane ug/LBRL1.0
1,3-Dichlorobenzene ug/LBRL1.0
1,4-Dichlorobenzene ug/LBRL1.0
1,4-Dioxane ug/LBRL150
Acetone ug/LBRL10
Benzene ug/LBRL1.0
Bromochloromethane ug/LBRL1.0
Bromodichloromethane ug/LBRL1.0
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL3.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL2.0
Chlorobenzene ug/LBRL1.0
Chloroethane ug/LBRL5.0
Chloroform ug/LBRL1.0
Chloromethane ug/LBRL2.0
cis-1,2-Dichloroethylene ug/LBRL1.0
cis-1,3-Dichloropropylene ug/LBRL1.0
Cyclohexane ug/LBRL5.0
Dibromochloromethane ug/LBRL1.0
Dichlorodifluoromethane ug/LBRL2.0
Ethylbenzene ug/LBRL1.0
Isopropylbenzene (Cumene)ug/LBRL1.0
m,p-Xylenes ug/LBRL2.0
Methyl Acetate ug/LBRL5.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methylcyclohexane ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
o-Xylene ug/LBRL1.0
Styrene ug/LBRL1.0
Tetrachloroethylene ug/LBRL1.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0298 - 5030B
Blank (P8C0298-BLK1)Prepared & Analyzed: 03/19/18
Toluene ug/LBRL1.0
trans-1,2-Dichloroethylene ug/LBRL2.0
trans-1,3-Dichloropropylene ug/LBRL1.0
Trichloroethylene ug/LBRL2.0
Trichlorofluoromethane ug/LBRL2.0
Vinyl chloride ug/LBRL2.0
Xylenes, total ug/LBRL3.0
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10251.2
ug/L 50.00 77-123Surrogate: Toluene-d8 9045.0
LCS (P8C0298-BS1)Prepared & Analyzed: 03/19/18
1,1,1-Trichloroethane ug/L23.0 1.0 20.00 75-136115
1,1,2,2-Tetrachloroethane ug/L20.9 1.0 20.00 62-127104
1,1,2-Trichloro-1,2,2-trifluoroethane ug/L23.1 5.0 20.00 70-130116
1,1,2-Trichloroethane ug/L23.8 1.0 20.00 70-140119
1,1-Dichloroethane ug/L21.2 1.0 20.00 78-130106
1,1-Dichloroethylene ug/L23.0 1.0 20.00 70-154115
1,2,3-Trichlorobenzene ug/L19.8 2.0 20.00 58-14499
1,2,4-Trichlorobenzene ug/L19.8 1.0 20.00 66-13999
1,2-Dibromo-3-chloropropane ug/L18.7 2.0 20.00 63-13494
1,2-Dibromoethane ug/L21.2 1.0 20.00 77-135106
1,2-Dichlorobenzene ug/L20.5 1.0 20.00 78-128102
1,2-Dichloroethane ug/L23.4 1.0 20.00 68-131117
1,2-Dichloropropane ug/L23.2 1.0 20.00 77-130116
1,3-Dichlorobenzene ug/L19.8 1.0 20.00 77-12599
1,4-Dichlorobenzene ug/L19.5 1.0 20.00 75-12698
1,4-Dioxane ug/L223150 200.0 70-130112
Acetone ug/L45.3 10 40.00 40-166113
Benzene ug/L23.7 1.0 20.00 77-128118
Bromochloromethane ug/L24.3 1.0 20.00 78-135122
Bromodichloromethane ug/L23.6 1.0 20.00 76-138118
Bromoform ug/L21.7 1.0 20.00 71-135109
Bromomethane ug/L24.2 3.0 20.00 41-168121
Carbon disulfide ug/L24.4 5.0 20.00 59-135122
Carbon Tetrachloride ug/L21.8 2.0 20.00 72-142109
Chlorobenzene ug/L21.3 1.0 20.00 78-119106
Chloroethane ug/L22.4 5.0 20.00 57-142112
Chloroform ug/L23.6 1.0 20.00 77-130118
Chloromethane ug/L23.5 2.0 20.00 47-145118
cis-1,2-Dichloroethylene ug/L23.0 1.0 20.00 76-141115
cis-1,3-Dichloropropylene ug/L23.2 1.0 20.00 65-140116
Cyclohexane ug/L21.7 5.0 20.00 70-130108
Dibromochloromethane ug/L22.7 1.0 20.00 75-134114
Dichlorodifluoromethane ug/L22.8 2.0 20.00 28-163114
Ethylbenzene ug/L21.5 1.0 20.00 80-127107
Isopropylbenzene (Cumene)ug/L20.7 1.0 20.00 70-130104
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0298 - 5030B
LCS (P8C0298-BS1)Prepared & Analyzed: 03/19/18
m,p-Xylenes ug/L43.8 2.0 40.00 77-133109
Methyl Acetate ug/L21.1 5.0 20.00 70-130105
Methyl Butyl Ketone (2-Hexanone)ug/L18.8 5.0 20.00 64-13794
Methylcyclohexane ug/L22.0 5.0 20.00 70-130110
Methyl Ethyl Ketone (2-Butanone)ug/L21.6 5.0 20.00 71-134108
Methyl Isobutyl Ketone ug/L21.9 5.0 20.00 69-134109
Methylene Chloride ug/L22.9 2.0 20.00 73-131115
Methyl-tert-Butyl Ether ug/L23.1 1.0 20.00 68-135116
o-Xylene ug/L20.9 1.0 20.00 78-128104
Styrene ug/L20.7 1.0 20.00 78-129103
Tetrachloroethylene ug/L19.9 1.0 20.00 80-129100
Toluene ug/L24.2 1.0 20.00 76-131121
trans-1,2-Dichloroethylene ug/L23.2 2.0 20.00 76-135116
trans-1,3-Dichloropropylene ug/L23.8 1.0 20.00 67-140119
Trichloroethylene ug/L23.2 2.0 20.00 77-133116
Trichlorofluoromethane ug/L23.9 2.0 20.00 62-148119
Vinyl chloride ug/L23.8 2.0 20.00 57-141119
Xylenes, total ug/L64.6 3.0 60.00 77-133108
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9849.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10251.0
ug/L 50.00 77-123Surrogate: Toluene-d8 9246.0
LCS Dup (P8C0298-BSD1)Prepared & Analyzed: 03/19/18
1,1,1-Trichloroethane ug/L22.5 1.0 20.00 2075-136113 2
1,1,2,2-Tetrachloroethane ug/L21.4 1.0 20.00 2062-127107 3
1,1,2-Trichloro-1,2,2-trifluoroethane ug/L21.9 5.0 20.00 2070-130110 5
1,1,2-Trichloroethane ug/L24.6 1.0 20.00 2070-140123 3
1,1-Dichloroethane ug/L21.0 1.0 20.00 2078-130105 0.5
1,1-Dichloroethylene ug/L22.1 1.0 20.00 2070-154111 4
1,2,3-Trichlorobenzene ug/L20.3 2.0 20.00 2058-144102 3
1,2,4-Trichlorobenzene ug/L19.8 1.0 20.00 2066-13999 0.3
1,2-Dibromo-3-chloropropane ug/L19.2 2.0 20.00 2063-13496 2
1,2-Dibromoethane ug/L20.8 1.0 20.00 2077-135104 2
1,2-Dichlorobenzene ug/L20.1 1.0 20.00 2078-128100 2
1,2-Dichloroethane ug/L23.0 1.0 20.00 2068-131115 2
1,2-Dichloropropane ug/L23.1 1.0 20.00 2077-130116 0.5
1,3-Dichlorobenzene ug/L19.8 1.0 20.00 2077-12599 0.05
1,4-Dichlorobenzene ug/L20.1 1.0 20.00 2075-126100 3
1,4-Dioxane ug/L238150 200.0 2070-130119 6
Acetone ug/L47.8 10 40.00 2040-166120 5
Benzene ug/L22.9 1.0 20.00 2077-128114 3
Bromochloromethane ug/L24.3 1.0 20.00 2078-135121 0.08
Bromodichloromethane ug/L23.6 1.0 20.00 2076-138118 0.2
Bromoform ug/L22.3 1.0 20.00 2071-135112 3
Bromomethane ug/L24.4 3.0 20.00 2041-168122 1
Carbon disulfide ug/L23.4 5.0 20.00 2059-135117 4
Carbon Tetrachloride ug/L20.8 2.0 20.00 2072-142104 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0298 - 5030B
LCS Dup (P8C0298-BSD1)Prepared & Analyzed: 03/19/18
Chlorobenzene ug/L21.2 1.0 20.00 2078-119106 0.4
Chloroethane ug/L22.2 5.0 20.00 2057-142111 0.9
Chloroform ug/L23.0 1.0 20.00 2077-130115 2
Chloromethane ug/L22.4 2.0 20.00 2047-145112 5
cis-1,2-Dichloroethylene ug/L22.5 1.0 20.00 2076-141112 2
cis-1,3-Dichloropropylene ug/L22.6 1.0 20.00 2065-140113 2
Cyclohexane ug/L20.7 5.0 20.00 2070-130103 5
Dibromochloromethane ug/L22.4 1.0 20.00 2075-134112 1
Dichlorodifluoromethane ug/L22.0 2.0 20.00 2028-163110 4
Ethylbenzene ug/L21.5 1.0 20.00 2080-127108 0.2
Isopropylbenzene (Cumene)ug/L20.0 1.0 20.00 2070-130100 4
m,p-Xylenes ug/L43.4 2.0 40.00 2077-133108 0.9
Methyl Acetate ug/L25.3 5.0 20.00 2070-130127 18
Methyl Butyl Ketone (2-Hexanone)ug/L19.6 5.0 20.00 2064-13798 4
Methylcyclohexane ug/L21.0 5.0 20.00 2070-130105 5
Methyl Ethyl Ketone (2-Butanone)ug/L22.4 5.0 20.00 2071-134112 4
Methyl Isobutyl Ketone ug/L21.5 5.0 20.00 2069-134108 2
Methylene Chloride ug/L21.6 2.0 20.00 2073-131108 6
Methyl-tert-Butyl Ether ug/L23.3 1.0 20.00 2068-135116 0.7
o-Xylene ug/L20.6 1.0 20.00 2078-128103 2
Styrene ug/L20.4 1.0 20.00 2078-129102 1
Tetrachloroethylene ug/L19.8 1.0 20.00 2080-12999 0.8
Toluene ug/L23.2 1.0 20.00 2076-131116 4
trans-1,2-Dichloroethylene ug/L22.3 2.0 20.00 2076-135111 4
trans-1,3-Dichloropropylene ug/L23.5 1.0 20.00 2067-140118 1
Trichloroethylene ug/L22.8 2.0 20.00 2077-133114 2
Trichlorofluoromethane ug/L23.3 2.0 20.00 2062-148116 3
Vinyl chloride ug/L23.1 2.0 20.00 2057-141115 3
Xylenes, total ug/L63.9 3.0 60.00 2077-133107 1
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9748.5
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.7
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0318 - 5030B
Blank (P8C0318-BLK1)Prepared & Analyzed: 03/20/18
1,1,1-Trichloroethane ug/LBRL1.0
1,1,2,2-Tetrachloroethane ug/LBRL1.0
1,1,2-Trichloro-1,2,2-trifluoroethane ug/LBRL5.0
1,1,2-Trichloroethane ug/LBRL1.0
1,1-Dichloroethane ug/LBRL1.0
1,1-Dichloroethylene ug/LBRL1.0
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL1.0
1,2-Dichlorobenzene ug/LBRL1.0
1,2-Dichloroethane ug/LBRL1.0
1,2-Dichloropropane ug/LBRL1.0
1,3-Dichlorobenzene ug/LBRL1.0
1,4-Dichlorobenzene ug/LBRL1.0
1,4-Dioxane ug/LBRL150
Acetone ug/LBRL10
Benzene ug/LBRL1.0
Bromochloromethane ug/LBRL1.0
Bromodichloromethane ug/LBRL1.0
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL3.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL2.0
Chlorobenzene ug/LBRL1.0
Chloroethane ug/LBRL5.0
Chloroform ug/LBRL1.0
Chloromethane ug/LBRL2.0
cis-1,2-Dichloroethylene ug/LBRL1.0
cis-1,3-Dichloropropylene ug/LBRL1.0
Cyclohexane ug/LBRL5.0
Dibromochloromethane ug/LBRL1.0
Dichlorodifluoromethane ug/LBRL2.0
Ethylbenzene ug/LBRL1.0
Isopropylbenzene (Cumene)ug/LBRL1.0
m,p-Xylenes ug/LBRL2.0
Methyl Acetate ug/LBRL5.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methylcyclohexane ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
o-Xylene ug/LBRL1.0
Styrene ug/LBRL1.0
Tetrachloroethylene ug/LBRL1.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0318 - 5030B
Blank (P8C0318-BLK1)Prepared & Analyzed: 03/20/18
Toluene ug/LBRL1.0
trans-1,2-Dichloroethylene ug/LBRL2.0
trans-1,3-Dichloropropylene ug/LBRL1.0
Trichloroethylene ug/LBRL2.0
Trichlorofluoromethane ug/LBRL2.0
Vinyl chloride ug/LBRL2.0
Xylenes, total ug/LBRL3.0
Heptane ug/L0.00
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9748.5
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.3
ug/L 50.00 77-123Surrogate: Toluene-d8 9648.0
LCS (P8C0318-BS1)Prepared & Analyzed: 03/20/18
1,1,1-Trichloroethane ug/L21.1 1.0 20.00 75-136106
1,1,2,2-Tetrachloroethane ug/L21.4 1.0 20.00 62-127107
1,1,2-Trichloro-1,2,2-trifluoroethane ug/L24.0 5.0 20.00 70-130120
1,1,2-Trichloroethane ug/L24.1 1.0 20.00 70-140121
1,1-Dichloroethane ug/L22.6 1.0 20.00 78-130113
1,1-Dichloroethylene ug/L21.3 1.0 20.00 70-154107
1,2,3-Trichlorobenzene ug/L23.0 2.0 20.00 58-144115
1,2,4-Trichlorobenzene ug/L23.6 1.0 20.00 66-139118
1,2-Dibromo-3-chloropropane ug/L18.4 2.0 20.00 63-13492
1,2-Dibromoethane ug/L22.8 1.0 20.00 77-135114
1,2-Dichlorobenzene ug/L22.3 1.0 20.00 78-128112
1,2-Dichloroethane ug/L23.7 1.0 20.00 68-131118
1,2-Dichloropropane ug/L24.2 1.0 20.00 77-130121
1,3-Dichlorobenzene ug/L22.6 1.0 20.00 77-125113
1,4-Dichlorobenzene ug/L22.4 1.0 20.00 75-126112
1,4-Dioxane ug/L203150 200.0 70-130102
Acetone ug/L42.8 10 40.00 40-166107
Benzene ug/L24.3 1.0 20.00 77-128121
Bromochloromethane ug/L25.2 1.0 20.00 78-135126
Bromodichloromethane ug/L23.8 1.0 20.00 76-138119
Bromoform ug/L20.2 1.0 20.00 71-135101
Bromomethane ug/L24.3 3.0 20.00 41-168121
Carbon disulfide ug/L23.6 5.0 20.00 59-135118
Carbon Tetrachloride ug/L21.0 2.0 20.00 72-142105
Chlorobenzene ug/L23.7 1.0 20.00 78-119118
Chloroethane ug/L19.2 5.0 20.00 57-14296
Chloroform ug/L22.2 1.0 20.00 77-130111
Chloromethane ug/L20.5 2.0 20.00 47-145103
cis-1,2-Dichloroethylene ug/L23.9 1.0 20.00 76-141120
cis-1,3-Dichloropropylene ug/L22.1 1.0 20.00 65-140110
Cyclohexane ug/L21.2 5.0 20.00 70-130106
Dibromochloromethane ug/L21.5 1.0 20.00 75-134108
Dichlorodifluoromethane ug/L14.9 2.0 20.00 28-16375
Ethylbenzene ug/L24.3 1.0 20.00 80-127122
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0318 - 5030B
LCS (P8C0318-BS1)Prepared & Analyzed: 03/20/18
Isopropylbenzene (Cumene)ug/L21.4 1.0 20.00 70-130107
m,p-Xylenes ug/L49.8 2.0 40.00 77-133125
Methyl Acetate ug/L22.6 5.0 20.00 70-130113
Methyl Butyl Ketone (2-Hexanone)ug/L20.6 5.0 20.00 64-137103
Methylcyclohexane ug/L22.7 5.0 20.00 70-130113
Methyl Ethyl Ketone (2-Butanone)ug/L22.6 5.0 20.00 71-134113
Methyl Isobutyl Ketone ug/L22.4 5.0 20.00 69-134112
Methylene Chloride ug/L23.3 2.0 20.00 73-131116
Methyl-tert-Butyl Ether ug/L23.5 1.0 20.00 68-135117
o-Xylene ug/L22.1 1.0 20.00 78-128110
Styrene ug/L21.3 1.0 20.00 78-129106
Tetrachloroethylene ug/L21.1 1.0 20.00 80-129105
Toluene ug/L24.6 1.0 20.00 76-131123
trans-1,2-Dichloroethylene ug/L22.0 2.0 20.00 76-135110
trans-1,3-Dichloropropylene ug/L21.1 1.0 20.00 67-140106
Trichloroethylene ug/L24.7 2.0 20.00 77-133124
Trichlorofluoromethane ug/L23.1 2.0 20.00 62-148115
Vinyl chloride ug/L20.1 2.0 20.00 57-141101
Xylenes, total ug/L71.9 3.0 60.00 77-133120
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9547.7
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10150.5
ug/L 50.00 77-123Surrogate: Toluene-d8 9849.1
LCS Dup (P8C0318-BSD1)Prepared & Analyzed: 03/20/18
1,1,1-Trichloroethane ug/L20.4 1.0 20.00 2075-136102 3
1,1,2,2-Tetrachloroethane ug/L21.8 1.0 20.00 2062-127109 2
1,1,2-Trichloro-1,2,2-trifluoroethane ug/L22.9 5.0 20.00 2070-130114 5
1,1,2-Trichloroethane ug/L23.1 1.0 20.00 2070-140115 4
1,1-Dichloroethane ug/L21.3 1.0 20.00 2078-130107 6
1,1-Dichloroethylene ug/L20.2 1.0 20.00 2070-154101 5
1,2,3-Trichlorobenzene ug/L22.7 2.0 20.00 2058-144114 1
1,2,4-Trichlorobenzene ug/L23.1 1.0 20.00 2066-139116 2
1,2-Dibromo-3-chloropropane ug/L18.2 2.0 20.00 2063-13491 1
1,2-Dibromoethane ug/L21.6 1.0 20.00 2077-135108 5
1,2-Dichlorobenzene ug/L22.3 1.0 20.00 2078-128111 0.09
1,2-Dichloroethane ug/L22.8 1.0 20.00 2068-131114 4
1,2-Dichloropropane ug/L23.5 1.0 20.00 2077-130118 3
1,3-Dichlorobenzene ug/L21.8 1.0 20.00 2077-125109 3
1,4-Dichlorobenzene ug/L21.4 1.0 20.00 2075-126107 4
1,4-Dioxane ug/L173150 200.0 2070-13087 16
Acetone ug/L40.9 10 40.00 2040-166102 5
Benzene ug/L23.1 1.0 20.00 2077-128115 5
Bromochloromethane ug/L23.9 1.0 20.00 2078-135120 5
Bromodichloromethane ug/L23.4 1.0 20.00 2076-138117 2
Bromoform ug/L19.3 1.0 20.00 2071-13597 4
Bromomethane ug/L24.6 3.0 20.00 2041-168123 1
Carbon disulfide ug/L22.7 5.0 20.00 2059-135113 4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 19
3/28/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: LRC-006 Continental TireHart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: John Lopez
Prism Work Order: 8030236
Time Submitted: 3/14/2018 4:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8C0318 - 5030B
LCS Dup (P8C0318-BSD1)Prepared & Analyzed: 03/20/18
Carbon Tetrachloride ug/L20.3 2.0 20.00 2072-142102 3
Chlorobenzene ug/L21.9 1.0 20.00 2078-119109 8
Chloroethane ug/L18.7 5.0 20.00 2057-14294 2
Chloroform ug/L21.3 1.0 20.00 2077-130107 4
Chloromethane ug/L20.5 2.0 20.00 2047-145102 0.1
cis-1,2-Dichloroethylene ug/L22.6 1.0 20.00 2076-141113 6
cis-1,3-Dichloropropylene ug/L21.2 1.0 20.00 2065-140106 4
Cyclohexane ug/L20.4 5.0 20.00 2070-130102 4
Dibromochloromethane ug/L20.5 1.0 20.00 2075-134103 5
Dichlorodifluoromethane ug/L14.8 2.0 20.00 2028-16374 1
Ethylbenzene ug/L22.8 1.0 20.00 2080-127114 6
Isopropylbenzene (Cumene)ug/L21.0 1.0 20.00 2070-130105 2
m,p-Xylenes ug/L46.6 2.0 40.00 2077-133116 7
Methyl Acetate ug/L23.3 5.0 20.00 2070-130117 3
Methyl Butyl Ketone (2-Hexanone)ug/L19.6 5.0 20.00 2064-13798 5
Methylcyclohexane ug/L21.2 5.0 20.00 2070-130106 7
Methyl Ethyl Ketone (2-Butanone)ug/L20.1 5.0 20.00 2071-134100 12
Methyl Isobutyl Ketone ug/L21.6 5.0 20.00 2069-134108 4
Methylene Chloride ug/L22.0 2.0 20.00 2073-131110 6
Methyl-tert-Butyl Ether ug/L22.6 1.0 20.00 2068-135113 4
o-Xylene ug/L20.7 1.0 20.00 2078-128103 7
Styrene ug/L20.1 1.0 20.00 2078-129100 6
Tetrachloroethylene ug/L19.7 1.0 20.00 2080-12999 7
Toluene ug/L23.2 1.0 20.00 2076-131116 6
trans-1,2-Dichloroethylene ug/L21.3 2.0 20.00 2076-135106 3
trans-1,3-Dichloropropylene ug/L20.5 1.0 20.00 2067-140103 3
Trichloroethylene ug/L23.2 2.0 20.00 2077-133116 6
Trichlorofluoromethane ug/L22.3 2.0 20.00 2062-148112 3
Vinyl chloride ug/L19.7 2.0 20.00 2057-14198 2
Xylenes, total ug/L67.2 3.0 60.00 2077-133112 7
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10050.1
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10250.8
ug/L 50.00 77-123Surrogate: Toluene-d8 9748.6
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P8C03188030236-01 03/20/18 9:321010mLmL
P8C02988030236-02 03/19/18 9:161010mLmL
P8C02988030236-03 03/19/18 9:161010mLmL
P8C02988030236-04 03/19/18 9:161010mLmL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 19
EMSL Analytical, Inc.
200 Route 130 North Cinnaminson, NJ 08077
Phone/Fax: [phone]
http://www.EMSL.com / [e-mail]
EMSL Order:041805464
Customer ID:TURN51
Customer PO:
Project ID:
Attention:John Lopez Phone:[phone]
Hart & Hickman Fax:
2923 S. Tryon Street Received:02/20/2018 9:25 AM
Charlotte, NC 28203 Analysis Date:02/23/2018
Collected:02/13/2018
Project:LRC-006
Test Report: Asbestos Analysis of Soils via EPA 600/R-93/116 Method using PLM and
Milling Prep. Quantitation using 400 Point Count Procedure
Sample Description Appearance % Fibrous % Non-Fibrous % Type
Non-Asbestos Asbestos
Brown
Non-Fibrous
Homogeneous
SoilArea-1
041805464-0001
None DetectedNon-fibrous (Other)100%
Brown
Non-Fibrous
Homogeneous
SoilArea-2
041805464-0002
None DetectedNon-fibrous (Other)100%
Analyst(s)
Frank Dicrescenzo (1)
Juli Patel (1)
Benjamin Ellis, Laboratory Manager
or other approved signatory
Disclaimer:Some samples may contain asbestos fibers present in dimensions below PLM resolution limits. The limit of detection as stated in the method is 0.25%. EMSL Analytical Inc suggests
that samples reported as <0.25% or none detected undergo additional analysis via TEM. The above test report relates only to the items tested. This report may not be reproduced, except in full,
without written approval of EMSL Analytical Inc. This test report must not be used by the client to claim product endorsement by NVLAP or any agency of the United States Government . EMSL
Analytical Inc., bears no responsibility for sample collection activities, analytical method limitations, or the accuracy of results when requested to separate layered samples. EMSL Analytical
Inc., liability is limited to the cost of sample analysis.The test results contained within this report meet the requirements of NELAC unless otherwise noted. Samples received in good condition
unless otherwise noted. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample.
Samples analyzed by EMSL Analytical, Inc. Cinnaminson, NJ NVLAP Lab Code 101048-0, AIHA-LAP, LLC-IHLAP Lab 100194, NYS ELAP 10872, NJ DEP 03036, PA ID# 68-00367
Initial report from: 02/23/2018 14:18:27
ASB_PLMPC_0006_0003 Printed 2/23/2018 2:18:29PM Page 1 of 1
OrderID: 041805464
Page 1 Of 1
EMSL Analytical, Inc.
200 Route 130 North Cinnaminson, NJ 08077
Phone/Fax: [phone]
http://www.EMSL.com / [e-mail]
EMSL Order:041808739
Customer ID:TURN51
Customer PO:
Project ID:
Attention:John Lopez Phone:[phone]
Hart & Hickman Fax:
2923 S. Tryon Street Received:03/26/2018 9:00 AM
Charlotte, NC 28203 Analysis Date:03/29/2018
Collected:03/23/2018
Project:LRC-006
Test Report: Asbestos Analysis of Soils via EPA 600/R-93/116 Method using PLM and Milling
Prep. Quantitation using 400 Point Count Procedure
Sample Description Appearance % Fibrous % Non-Fibrous % Type
Non-Asbestos Asbestos
Brown/Orange
Non-Fibrous
Homogeneous
SoilArea-3
041808739-0001
None DetectedNon-fibrous (Other)100%
Analyst(s)
William Nguyen (1)Benjamin Ellis, Laboratory Manager
or other approved signatory
Disclaimer:Some samples may contain asbestos fibers present in dimensions below PLM resolution limits. The limit of detection as stated in the method is 0.25%. EMSL Analytical Inc suggests
that samples reported as <0.25% or none detected undergo additional analysis via TEM. The above test report relates only to the items tested. This report may not be reproduced, except in full,
without written approval of EMSL Analytical Inc. This test report must not be used by the client to claim product endorsement by NVLAP or any agency of the United States Government . EMSL
Analytical Inc., bears no responsibility for sample collection activities, analytical method limitations, or the accuracy of results when requested to separate layered samples. EMSL Analytical
Inc., liability is limited to the cost of sample analysis.The test results contained within this report meet the requirements of NELAC unless otherwise noted. Samples received in good condition
unless otherwise noted. Unless requested by the client, building materials manufactured with multiple layers (i.e. linoleum, wallboard, etc.) are reported as a single sample.
Samples analyzed by EMSL Analytical, Inc. Cinnaminson, NJ NVLAP Lab Code 101048-0, AIHA-LAP, LLC-IHLAP Lab 100194, NYS ELAP 10872, NJ DEP 03036, PA ID# 68-00367
Initial report from: 03/29/2018 16:49:49
ASB_PLMPC_0006_0003 Printed 3/29/2018 4:49:50PM Page 1 of 1
OrderID: 041808739
Page 1 Of 1

Appendix C
Waste Disposal Documentation

Appendix D
Well Construction Details
NOTES: Hole precleared to 5.0' on 03/14/2018 by IET using hand auger.
generated using LogitEasy.com
Client:
Project:
Address:
LRC Patriot
LRC-006
1900 Continental Blvd., Charlotte,NC
WELL LOG
Well No.
Page:
TMW-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
03/14/2018
03/14/2018
IET
Direct Push
Power Probe 9520
Sam Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
30.0
22.66
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
30.0
1.0
0.001
Sch 40 PVC
PVC Prepack
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
35
(0') ORGANIC SOIL (OL); grass/topsoil
(0.25') Silty CLAY (CLML); soft, dry, dark brown to brown
(1.5') Silty CLAY (CLML); stiff, dry, brown to light brown
(3.5') Silty SAND (SM); loose, dry, tan and brown
(8') Sandy SILT (ML); soft, moist, brown
(13') Sandy SILT (ML); soft, moist, brown and orange
(19.5') Sandy SILT (ML); soft, moist, brown and orange
(25') Sandy SILT (ML); soft, wet, brown and dark brown
(30') Boring terminated
14.3
6.5
3.0
3.6
4.4
2.8
1.7
2.4
2.8
0
5
10
15
20
25
30
35
NOTES: Hole precleared to 5.0' on 03/14/2018 by IET using hand auger.
generated using LogitEasy.com
Client:
Project:
Address:
LRC Patriot
LRC-006
1900 Continental Blvd., Charlotte,NC
WELL LOG
Well No.
Page:
TMW-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
03/14/2018
03/14/2018
IET
Direct Push
Power Probe 9520
Sam Martin
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
25.0
23.26
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
25.0
1.0
0.001
Sch 40 PVC
PVC Prepack
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
(0') ORGANIC SOIL (OL); topsoil/vegetation
(0.25') Silty CLAY (CLML); stiff, dry, brown to dark brown
(2') Silty CLAY (CLML); stiff, dry, brown and orange
(7') Silty SAND (SM); loose, dry, tan and brown, some partially weathered rock
(16.5') Silty SAND (SM); dense, moist, brown and dark brown, some black relict
structures
(22') Sandy SILT (ML); soft, moist, brown and orange
(25') Boring terminated
3.0
2.2
3.0
2.5
2.3
2.0
1.2
0.0
0
5
10
15
20
25
30

Appendix E
Vapor Intrusion Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Groundwater to Indoor Air
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID:
Exposure Unit ID: TMW-3/DUP-1
CAS #Chemical Name:Groundwater Concentration(ug/L)
Calculated Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated Carcinogenic Risk
Calculated
Non-Carcinogenic Hazard
Quotient
67-64-1 Acetone 18 0.0257562 -2.7E+04 1.9E-07
75-34-3 Dichloroethane, 1,1-2.6 0.59738354 7.7E+00 -7.8E-08
75-35-4 Dichloroethylene, 1,1-2.3 2.45421086 -1.8E+02 2.8E-03
156-59-2 Dichloroethylene, 1,2-cis-3.4 0.56712986 --
127-18-4 Tetrachloroethylene 4.2 3.03924768 4.7E+01 3.5E+01 6.4E-08 1.7E-02
71-55-6 Trichloroethane, 1,1,1-2.8 1.96892892 -4.4E+03 9.0E-05
79-01-6 Trichloroethylene 16 6.4431728 3.0E+00 1.8E+00 2.2E-06 7.4E-01
Cumulative:2.3E-06 7.6E-01
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3D
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Groundwater to Indoor Air
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID:
Exposure Unit ID: TW-4
CAS #Chemical Name:Groundwater Concentration(ug/L)
Calculated Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated Carcinogenic Risk
Calculated
Non-Carcinogenic Hazard
Quotient
67-64-1 Acetone 150 0.214635 -2.7E+04 1.6E-06
75-34-3 Dichloroethane, 1,1-3.3 0.75821757 7.7E+00 -9.9E-08
156-59-2 Dichloroethylene, 1,2-cis-5.2 0.86737508 --
127-18-4 Tetrachloroethylene 2.6 1.88143904 4.7E+01 3.5E+01 4.0E-08 1.1E-02
71-55-6 Trichloroethane, 1,1,1-3.2 2.25020448 -4.4E+03 1.0E-04
79-01-6 Trichloroethylene 8.3 3.34239589 3.0E+00 1.8E+00 1.1E-06 3.8E-01
Cumulative:1.3E-06 3.9E-01
Groundwater concentrations are in ug/L. Air concentrations are in ug/m3.
Output Form 3D
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID:
Exposure Unit ID: VMP-7
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air Concentration
(ug/m3)
Target Indoor Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 23 0.23 -2.7E+04 1.7E-0671-43-2 Benzene 0.39 0.0039 1.6E+00 2.6E+01 2.5E-09 3.0E-0575-15-0 Carbon Disulfide 1.2 0.012 -6.1E+02 3.9E-0667-66-3 Chloroform 3.9 0.039 5.3E-01 8.6E+01 7.3E-08 9.1E-0574-87-3 Chloromethane 0.34 0.0034 -7.9E+01 8.6E-0675-71-8 Dichlorodifluoromethane 0.97 0.0097 -8.8E+01 2.2E-0575-34-3 Dichloroethane, 1,1-68 0.68 7.7E+00 -8.9E-0875-35-4 Dichloroethylene, 1,1-2.6 0.026 -1.8E+02 3.0E-05156-59-2 Dichloroethylene, 1,2-cis-61 0.61 --156-60-5 Dichloroethylene, 1,2-trans-0.18 0.0018 --142-82-5 Heptane, N-1.6 0.016 -3.5E+02 9.1E-06110-54-3 Hexane, N-3.6 0.036 -6.1E+02 1.2E-05591-78-6 Hexanone, 2-0.69 0.0069 -2.6E+01 5.3E-0567-63-0 Isopropanol 2.1 0.021 -1.8E+02 2.4E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)3.7 0.037 -4.4E+03 1.7E-06
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.61 0.0061 -2.6E+03 4.6E-07
75-09-2 Methylene Chloride 0.52 0.0052 1.2E+03 5.3E+02 4.2E-12 2.0E-06115-07-1 Propylene 3.4 0.034 -2.6E+03 2.6E-06100-42-5 Styrene 0.1 0.001 -8.8E+02 2.3E-07
127-18-4 Tetrachloroethylene 640 6.4 4.7E+01 3.5E+01 1.4E-07 3.7E-02
108-88-3 Toluene 0.25 0.0025 -4.4E+03 1.1E-07
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-14 0.14 -4.4E+03 6.4E-06
71-55-6 Trichloroethane, 1,1,1-520 5.2 -4.4E+03 2.4E-04
79-00-5 Trichloroethane, 1,1,2-0.26 0.0026 7.7E-01 1.8E-01 3.4E-09 3.0E-03
79-01-6 Trichloroethylene 180 1.8 3.0E+00 1.8E+00 6.0E-07 2.1E-0195-63-6 Trimethylbenzene, 1,2,4-0.74 0.0074 -5.3E+01 2.8E-05
108-67-8 Trimethylbenzene, 1,3,5-0.24 0.0024 -5.3E+01 9.1E-06
108-38-3 Xylene, m-0.32 0.0032 -8.8E+01 7.3E-06
95-47-6 Xylene, o-0.16 0.0016 -8.8E+01 3.7E-06
Cumulative:9.1E-07 2.5E-01
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID:
Exposure Unit ID: VMP-8
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air Concentration
(ug/m3)
Target Indoor Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 11 0.11 -2.7E+04 8.1E-0771-43-2 Benzene 0.95 0.0095 1.6E+00 2.6E+01 6.0E-09 7.2E-0575-15-0 Carbon Disulfide 0.41 0.0041 -6.1E+02 1.3E-0667-66-3 Chloroform 9 0.09 5.3E-01 8.6E+01 1.7E-07 2.1E-0474-87-3 Chloromethane 0.24 0.0024 -7.9E+01 6.1E-0675-71-8 Dichlorodifluoromethane 1.3 0.013 -8.8E+01 3.0E-0575-34-3 Dichloroethane, 1,1-41 0.41 7.7E+00 -5.3E-0875-35-4 Dichloroethylene, 1,1-6.9 0.069 -1.8E+02 7.9E-05156-59-2 Dichloroethylene, 1,2-cis-24 0.24 --141-78-6 Ethyl Acetate 8.1 0.081 -6.1E+01 2.6E-04100-41-4 Ethylbenzene 0.15 0.0015 4.9E+00 8.8E+02 3.1E-10 3.4E-07142-82-5 Heptane, N-0.66 0.0066 -3.5E+02 3.8E-06110-54-3 Hexane, N-4.3 0.043 -6.1E+02 1.4E-0567-63-0 Isopropanol 2.1 0.021 -1.8E+02 2.4E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)2 0.02 -4.4E+03 9.1E-07
75-09-2 Methylene Chloride 1.6 0.016 1.2E+03 5.3E+02 1.3E-11 6.1E-06115-07-1 Propylene 2.4 0.024 -2.6E+03 1.8E-06100-42-5 Styrene 1.4 0.014 -8.8E+02 3.2E-06
127-18-4 Tetrachloroethylene 1700 17 4.7E+01 3.5E+01 3.6E-07 9.7E-02
108-88-3 Toluene 3.1 0.031 -4.4E+03 1.4E-06
76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2-1.5 0.015 -4.4E+03 6.8E-07
71-55-6 Trichloroethane, 1,1,1-420 4.2 -4.4E+03 1.9E-04
79-00-5 Trichloroethane, 1,1,2-1.2 0.012 7.7E-01 1.8E-01 1.6E-08 1.4E-02
79-01-6 Trichloroethylene 410 4.1 3.0E+00 1.8E+00 1.4E-06 4.7E-0175-69-4 Trichlorofluoromethane 2.8 0.028 --
108-38-3 Xylene, m-0.4 0.004 -8.8E+01 9.1E-06
95-47-6 Xylene, o-0.16 0.0016 -8.8E+01 3.7E-06
Cumulative:2.0E-06 5.8E-01
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator