MO-6615_27296_CA_MRP_20171108_GWSamplingReport

J.T. Ryerson & Son, Inc.
Free Product Recovery and Groundwater
Monitoring Report
November 2017
Former Integris Metals Facility
527 Atando Avenue
Charlotte, North Carolina
Delivering sustainable solutions in a more competitive world
ERM

Site Information
Site Identification
Date of Report: November 8, 2017
Facility I.D. None Incident Number 27296 Site Risk/Priority Risk Intermediate
Site Name: Former Inteeris Metals
Site Street Address: 527 Atando Avenue
City/Town: Charlotte Zip Code: 28206
County: Mecklenburg
Description of Geographical Data Point (e.g., diesel fill port): Fuel Oil #2 UST
Location Method (GPS, topographical map, other): Site reconnaissance and website
Latitude: 35.25785 Longitude:-80.816810 (Source Area Location)
Information about Contacts Associated With the Leaking UST System
UST Owner:
Joseph T. Ryerson & Son, Inc.
Address:
227 W. Monroe Street, Chicago, IL
Tel:
[phone]
UST Operator:
Joseph T. Ryerson & Son, Inc
Address:
227 W. Monroe Street, Chicago, IL
Tel:
[phone]
Property Owner:
Advantage Machinery Services
Address:
1407 Highway 601 South, Yadkinville, NC 27055
Tel:
[phone]
Property Occupant: Sunbelt -Turret Steel
Address:
527 Atando Avenue, Charlotte, NC 28206
Tel:
[phone]
Consultant/Contractor: ERM NC, Inc.
Address:
15720 Brixham Hill Avenue, Suite 120, Charlotte, NC 28277
Tel:
[phone]
Information about Release
Date Discovered: November 13, 2002
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Dispenser/Piping/UST): UST
Sizes and contents of UST system(s) from which the release occurred: 12,000 gallon Fuel Oil UST
Certification
I, Rick Tarravechia a Professional Engineer icensed Geolo i (circle one) for ERM NC, Inc.,
do certify that the information contained in this report is correct and accurate to the best of my
knowledge. (Affix Seal and Signature)
CA
01.
SEAL = ?
ERM NC, Inc. is licensed to practice geology and engineering in North Carolina. The certification
number of the company or corporation is C-470.
ERM NC, Inc. 1 GW Sampling Report - Atando Ave. 10-2017.docx

1.0 FREE PRODUCT RECOVERY ACTIVITIES
An absorbent sock has been installed in monitor well MW-1 since the surfactant injection and
recovery event that took place in December 2016. Access to the well has been limited by the
building's current tenant, a granite slab storage and distribution company which claims that
their overhead cranes don't work properly and therefore they cannot move the slabs which
block access. Also, they state that they are unwilling or unable to store their granite slabs in a
different location so that the 8-inch diameter monitor well cover can be accessed. Therefore,
ERM has not been able to gauge MW-1 for free product or change the absorbent sock until the
recent site -wide sampling event (September 5, 2017), at which time ERM did not observe
product on the absorbent sock or within the well. The absorbent sock was removed from the
well during the September monitoring event.
2.0 GROUNDWATER MONITORING ACTIVITIES
2.1 GROUNDWATER ELEVATION MEASUREMENTS
Water level measurements were obtained in the site monitor wells prior to well purging and
sampling on September 5, 2017 using a decontaminated electronic water level meter. Using top
of casing elevations and the depth to water measurements, site groundwater elevations and
hydraulic gradients in the saprolite aquifer were calculated. Monitor well construction
information is presented in Table B-7. No free product was measured in monitor well MW-1;
therefore, it was included in the sampling network.
2.2 GROUNDWATER SAMPLE COLLECTION
The monitor wells were purged and sampled using low flow techniques with a peristaltic
pump and new polyethylene tubing dedicated to each well. Flow rates during purging
averaged 100 milliliters per minute. General groundwater quality parameters (pH,
temperature, conductivity, dissolved oxygen, and turbidity) were measured in the field
during purging using a flow -through sampling cell. Sampling was performed once the
parameters had stabilized. Low -flow samples were collected directly from the polyethylene
tubing. Field sampling sheets are included in Appendix A.
The samples were immediately placed on ice inside insulated shipping containers and then
delivered under the appropriate chain -of- custody protocol to Shealy Environmental Services,
Inc. (Shealy) in West Columbia, South Columbia for analyses. The samples were analyzed for
the following:
• Volatile organic compounds (VOCs) by EPA Method 8260B for the EPA 602 plus
xylenes list;
• Semi -volatile organic compounds (SVOCs) by EPA Method 625; and
• Volatile petroleum hydrocarbons (VPH) and extractable hydrocarbons (EPH) by the
Massachusetts Department of Environmental Protection (MADEP) Methods.
ERM NC, Inc. 2 GW Sampling Report - Atando Ave. 10-2017.docx

A copy of the laboratory report is in Appendix B.
3.0 GROUNDWATER MONITORING RESULTS
3.1 GROUNDWATER ELEVATIONS AND FLOW
The depth to groundwater in the saprolite zone varies across the monitoring area from 12.99
feet below ground surface (bgs) in monitor well MW-4 to 18.10 feet bgs in monitor well MW-2.
Groundwater in the saprolite aquifer flows to the south toward an intermittent stream that is
located approximately 250 feet west of the source area, on the west side of the railroad tracks.
Groundwater flows under an average hydraulic gradient of 0.014 as shown in Figure 3.
Groundwater elevation data are summarized in Table B-7.
3.2 GROUNDWATER RESULTS
Laboratory analysis of groundwater samples detected target compounds in four of the six wells
sampled at the site. The highest concentrations of VOCs and SVOCs were in MW-1 and MW-2,
which are located downgradient from UST-1. The current and historical groundwater results are
summarized in Table B-4. Figure 4 illustrates analytical results from the September 2017 event.
The historical comparison of analytical results between samples collected from MW-1 between
June 2016 and September 2017 indicate that semi -volatile hydrocarbons have been reduced by one
or more orders of magnitude. Several VPH and EPH fractions continue to decrease in
concentration since June 2016. This reduction appears to be the result of the surfactant
injection/extraction event that took place in December 2016. Benzene, fluorene, naphthalene, and
VPH/EPH exceeded 2L groundwater standards in several wells.
4.0 CONCLUSIONS
Groundwater samples collected from MW-1 continue to show a notable decrease in SVOC
concentrations since the June 2016 event. Benzene and several SVOCs still exceed 2L
groundwater standards in several wells across the site. However, all concentrations are below
gross contamination levels. Based on the results of three sampling events: one before the injection
event, one immediately after the event, and one nine months after the event, it appears that free
product has been removed from the source area, and SVOC concentrations have been significantly
reduced in monitor well MW-1. ERM proposes to request closure of this incident, based on the lack
of free product and groundwater concentrations below the gross contamination levels.
ERM NC, Inc. 3 GW Sampling Report - Atando Ave. 10-2017.docx

Figures

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FIGURE 1
ERM NC, Inc. Site Location Map
ERM 527 7 Ata is Metals
Atando Avenue
Charlotte, North Carolina
DATE: 10/11/2017 SCALE: AS SHOWN DRAWN: AFreemen
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FIGURE 2
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ERM Integris Metals
527 Atando Avenue
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Shallow Well
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September 2017
Groundwater Elevation Contours
(dashed in areas of less certainty)
�— Approximate direction of groundwater flow
UST
Site
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� f �
t t
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UST-1 MW-1
(88a56) MW-2
S (86.40)
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Basemap Mecklenburg County.
Mecklenburg County: 2015Aerial, Site Features, Property lines
FIGURE 3
f ERM NC, Inc. Groundwater Elevation
Contour Map
ERM Integris Metals
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M W-1 9/5/2017 M W-2 9/5/2017
VOCs - EPA Method 602 (ug4) / 8260B VO Cs - EPA Method 602 (NgA) / 8260B
Benzene 47 Benzene 59
- MW-5 - Ethylbenzene 28 Ethylbenzene 14
Xylenes (total) 6.7 Xylenes (total) 5.6
M W-5 9/5/2017 SVOCs - EPA Method 625 (NgA) SVOCs - EPA Method 625
VOCs - EPA Method 602 (NgA) / 8260T Naphthalene 240 (pg//)
Naphthalene 84
Benzene 1.2 Phenanthrene 98
Phenanthrene 8.4
SVOCs -EPA Method (NgA) MADEP VPH/EPH (NgA) MADEP VPH/EPH (NgA)
Not Detected
- C9-C12 Aliphatics - VPH 950
MADEP VPH/EPH (ygA) C5-C8 Aliphatics VPH 92
_ C9-Cl Aliphatics - �H 7,700 C9-C12 Aliphatics - VPH 280',
C5-C8 Aliphatics VPH 2,000 C9-Cl0 Aromatics - VPH 730
UST-1 C9-C10 Aromatics -VPH 290
C11-C22 Aromatics - H EEP950
C11-C22 Aromatics - EPH 600
MW-1 MW-2
UST-2 i
ML
MW-3 -
O M W-3 9/5/2017
4 M W-4 9/5/2017 M W-4 -Y� VOCs - EPA Method 602 (NgA) / 8260B
-
4 VOCs -EPA Method (NDW1 Benzene 3.2
y/I) / 82608 Q Q SVOCs - EPA Method 625 (NgA)
Not Detected
d DW-1 9/5/2017 Naphthalene 4.6
SVOCs - EPA Method 625 (NgA) VOCs - EPA Method 602 (Nene gA) / 8260B MADEP VPene (ugA)
Benzo(a)anthracene 2.3 - Not Detected Not Detected
Benzo(a)pyrene 3.3 -, SVOCs - EPA Method 625 (ugA)
Explanation
Benzo(b)fluoranthene 6.2 Not Detected 25 50
Benzo(g,h,i)perylene 1.7 MADEP VPH/EPH(Ng4)
Benzo(k)fluoranthene 2.0 C5-C8 Aliphatics VPH 140 Feet
Shallow Well Chrysene 3.2
bis(2-Bhylhexyl)phthalate 1.7 Basemap Mecklenburg County.
O Deep Well Fluoranthene 4.3 Mecklenburg County: 2015Aerial, Site Features, Property lines
Indeno(1,2,3-c,d)pyrene 1.7 _
UST
MADEP VPH/EPH (NgA) FIGURE 4
Not Detected
Site ERM NC, Inc. Recent Groundwater
Building W Concentrations Map
ERM Integris Metals
Paved 527 Atando Avenue
SCALE: AS SHOWN DRAWN: AFreeman DATE: 10/11 /2017
Charlotte, North Carolina
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Tables

TABLE B-1 SITE HISTORY - UST SYSTEM AND OTHER RELEASE INFORMATION
Facility I.D.: Not established
Date: September 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Was
Release
Associated
Description of
with UST
UST ID
Current/
Capacity
Construction
Associated Piping
System?
Number
Last Contents *
(gallons)
Details
and Pumps
Date Installed
Status of UST
(Yes/No)
1
Fuel Oil #2
6,000
Steel
dispensers.
1966 or as
Removed
Yes
2
Fuel Oil #2
6,000
Steel :[Noo
dispensers. **
early as 1949
Closed in Place
Yes
Incident
Material
Date of
Number
Released
Release
Description of Release
27296
Fuel Oil
11/13/2002
The release was discovered as part of due diligence for a property transaction in 2002. The amount of
product released from the UST is not known.
TABLE B-2 SITE HISTORY - OWNER/OPERATOR AND OTHER RESPONSIBLE PARTY INFORMATION
(most recent first) Facility I.D.: Not established
Date: September 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
UST ID Number
I Name of Owner or Operator
JDates of Ownership/Operation
Owner or Operator?
1 and 2
lJoseph T. Ryerson & Son, Inc.
Present
Owner
Address
Telephone Number
227 W. Monroe Street, Chicago, IL
Date of Release 11/13/2002
[phone]
ERM Page 1 of 6

TABLE B-4-1 SUMMARY OF GROUND WATER SAMPLING RESULTS - VOCs and SVOCs
Date: September 2017
Facility I.D.:
Incident Number and Name:
Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Analytical Method
VOCs - EPA Method 602 (pg/1) / 8260B
SVOCs - EPA Method 625 (pg/1)
6
Co
0
c
C
N
c
T
O
N
y
C
N
C
T
7
C
t
L
C
C\
C
N
N
C
N
Vl
U
p_
(0
Co
4
O)
Y
Q
C
z
NO
NCN
ONO
N
C
Ll
O
Co
Sample ID
Source
Date
Ca
>+
L
X
¢
¢
N
m
N
m
N
m
N
Co
CD
Co
LC
U
N
a
N
o
O
FL
O
F
N
5
.
(pO
z
C
LE
a
NC Ground
Water Standard (2L)
1
600
600
500
2,000
80
0.05
0.05
0.05
200
0.5
5
Gross Contamination Level
5,000
84,500
260,000
85,500
2,000
2,120
4.7
0.81
0.75
200
0.5
5
170
NE
300
990
6,000
6,000
410
1 /3/2003
Not Sampled Due to Free Product
MW-1
MW
6/14/2016
66
90
ND
ND
460
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
570
ND
2,100
2,100
12/29/2016
70
48
2.3
14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
200
61
9/5/2017
47
28
ND
6.7
21
19
ND
ND
ND
ND
ND
ND
ND
ND
ND
36
ND
240
98
1/3/2003
55
15
2.0
98
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
18
ND
92
39
MW-2
MW
6/14/2016
61
19
ND
8
ND
ND
ND
ND
ND
ND
ND
ND
ND
11
ND
4.2
ND
41
3.8
12/29/2016
60
10
ND
3.7
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
54
10
9/5/2017
59
14
ND
5.6
ND
1.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.5
ND
84
8.4
1/22/2003
1.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
11
ND
ND
ND
ND
ND
ND
MW-3
MW
6/14/2016
1.6
ND
2.1
2.1
ND
ND
ND
ND
ND
ND
ND
ND
1.6
ND
ND
ND
ND
3.5
ND
12/29/2016
9.7
ND
ND
3.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
7.5
ND
9/5/2017
3.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.6
ND
1/22/2003
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-4
MW
6/14/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2017
ND
ND
ND
ND
ND
ND
2.3
3.3
6.2
1.7
2.0
3.2
1.7
ND
4.3
ND
1.7
ND
ND
1/22/2003
3.6
ND
1.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-5
MW
6/14/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12/29/2016
Not Sample Due to
Standing Water Around Wellhead
9/5/2017
1.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1/22/2003
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DW-1
MW
6/14/2016
ND
1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
9/5/2017
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Only detected compounds are included in table. NA = Not Applicable NA = Not NA = Not Applicable
pg/L = micrograms per liter Results shown in bold exceed the applicable Ground Water Standard (T15A 2L)
ND = Not detected
NE - Not Established
ERM Page 2 of 6

TABLE B-4-2
Date: September 2017
SUMMARY OF GROUND WATER SAMPLING RESULTS - MADEP
Facility I.D.: 0 Facility I.D.: Not established
Incident Number and Name: Incident Nur # 27296 / 527 Atando Avenue, Charlotte, NC
Analytical Method
MADEP VPH/EPH (pg/1)
N
y
U
Q
W
o
O
W
U
.0
.0
CO M
N
co
M
O
N
U
M
U co
U Q
U=
U C
U=
_
d Q
Sample ID
P
Source
Date
"' =
U Q
rn
U>
—
0 Q
o
0 >
0
U W
U Q
NC Groundwater Standard (2L)
400
700
200
10,000
Gross Contamination Level
NA
NA
NA
NA
1/3/2003
Not Sampled Due to Free Product
6/14/2016
1,700 13,000 1,400,000 8,200 600,000
180,000
MW-1
MW
12/29/2016
ND 4,000 2,800 1,900 2,200
ND
9/5/2017
ND 950 7,700 730 950
950
1/3/2003
ND
1,100
770
1,600
ND
MW-2
MW
6/14/2016
ND
210
120
250
510
ND
12/29/2016
86
260
260
220
540
ND
9/5/2017
92
280
290
600
ND
1/22/2003
ND
ND
—
—
—
ND
MW-3
MW
6/14/2016
ND
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
9/5/2017
ND
ND
ND
ND
ND
ND
1/22/2003
ND
ND
ND
ND
ND
ND
MW-4
MW
6/14/2016
ND
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
9/5/2017
ND
ND
ND
ND
ND
ND
1/22/2003
3,500 ND ND ND ND ND
MW-5
MW
6/14/2016
2,400 ND ND ND ND ND
12/29/2016
Not Sample Due to Standing Water Around Wellhead
9/5/2017
2,000
1 ND
ND
ND
ND
ND
1/22/2003
ND
ND
ND
ND
ND
ND
DW-1
MW
6/14/2016
150
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
9/5/2017
140
ND
ND
ND
ND
ND
Only detected compounds are included in table.
pg/L = micrograms per liter
ND = Not detected
NE - Not Established
NA = Not Applicable NA = Not Applicable
Results shown in bold exceed the applicable Ground Water Standard (T15A 2L)
ERM Page 3 of 6

TABLE B-7 WELL CONSTRUCTION INFORMATION
Date: September 2017 Incident Number and Name: Not established
Facility ID#: # 27296 / 527 Atando Avenue, Charlotte, NC
Monitor
Well ID
Date Installed
Date Water
Level
Measured
Well Casing
Depth
(feet BGS)
Screened
Interval
(feet BGS)
Bottom of Well
(feet BGS)
Top of
Casing
Elevation
(feet*)
Depth to
Water
(feet
BTOC)
Product
Thicknes
s
(feet)
Ground
Water
Elevation
* (feet)
Comments
MW-1
1/22/03
9/5/17
19
19-34
34
104.50
15.94
ND
88.56
MW-2
1 1/22/03
9/5/17
19
19-34
34
104.50
1 18.10
ND
86.40
MW-3
1/22/03
9/5/17
17
17-32
32
99.72
13.36
ND
86.36
MW-4
1/22/03
9/5/17
17
17-32
32
99.90
12.99
ND
86.91
MW-5
1/22/03
9/5/17
17
17-32
32
101.79
10.40
ND
91.39
DW-1
1/22/03
9/5/17
81
81-86
88
100.00
12.28
ND
87.72
Reference point for elevation measurements: 100 feet
If free product is present, ground water elevation should be calculated by: [top of casing elevation - depth to water] + [ free product thickness x 0.8581]
Feet BGS = Below Ground Surface Feet BTOC = Below Top of Casing
ERM Page 4 of 6

TABLE B-8 FREE PRODUCT RECOVERY RESULTS
Date: September 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Free Product Recovery Method: Bailer/Passive Skimmer/Sock/AFVR Facility ID#: Not established
Method of Measurement: Bailer / Interface probe
Well ID
Product Type
Date of
Recovery
Casing
Diameter
(inches)
Product
Thickness
Before
Recovery (ft.)
Product
Thickness After
Recovery (ft.)
Amount of
Product
Recovered
(gallons)
Depth to Water
from Top of
Casing (ft.)
Comments
MW-1
Fuel Oil
1/3/03
2 0.05 0.00 <0.25 21.32
Bailer
1/22/03
2 0.02 0.00 <0.25 16.23
Bailer
3/10/03
2 0.04 0.00 <0.25 14.07
Bailer
3/25/03
2 0.00 0.00 <0.25 12.99
Bailer
4/4/03
2 0.03 0.00 <0.25 12.68
Bailer
5/30/03
2 0.01 0.00 <0.25 11.01
Bailer
6/27/03
2 0.02 0.00 <0.25 11.24
Bailer
7/17/03
2 0.01 0.00 <0.25 11.71
Bailer
8/26/03
2 0.01 0.00 <0.25 11.15
Bailer
9/2/03
2 0.01 0.00 <0.25 12.18
Bailer
11/14/03
2 0.01 0.00 <0.25 15.23
Bailer
11/24/03
2 0.01 0.00 <0.25 15.10
Bailer
12/19/03
2 0.04 0.00 <0.25 14.74
Bailer
1/29/04
2 0.05 0.00 <0.25 15.05
Bailer
3/9/04
2 0.00 0.00 <0.25 13.19
AFVR
4/8/04
2 0.04 0.00 <0.25 13.07
Bailer
5/10 to 5/19/04
Source Removal: UST and 416 tons of contaminated soil removed to depth of 17
feet.
5/24/04
2 0.08 0.00 0.20 13.22
Bailer
6/23/04
2 0.07 0.00 <0.25 15.00
Bailer
7/28/04
2 0.05 0.00 <0.25 15.75
Bailer
8/27/04
2 0.12 0.00 0.25 15.52
Bailer
10/5/04
2 0.05 0.00 <0.25 14.14
Bailer
11/1/04
2 0.10 0.00 0.25 14.67
Bailer
12/2/04
2 0.03 0.00 <0.25 14.53
Bailer
11/17/13
2 0.55 0.00 <0.25 17.89
Bailer
2/5/14
2 0.67 0.00 <0.25 15.34
Passive Skmr
2/17/14
2 <0.01 0.00 <0.25 14.55
Passive Skmr
2/27/14
2 <0.01 0.00 <0.25 14.01
Passive Skmr
3/27/14
2 <0.01 0.00 <0.25 13.60
Passive Skmr
8/6/14
2 <0.01 0.00 <0.25 14.45
Passive Skmr
4/10/15
2 <0.01 0.00 <0.25 14.01
Passive Skmr
5/27/15
2 0.01 0.00 <0.25 14.76
Passive Skmr
7/28/15
2 0.08 0.00 <0.25 17.72
Passive Skmr
1/28/16
2 0.19 0.00 0.00 12.92
Passive Skmr
2/18/16
2 0.13 0.00 0.00 13.22
Passive Skmr
3/25/16
2 <0.01 0.00 0.00 13.01
Sock
3/31/16
2 <0.01 0.00 0.00 12.91
Sock
4/14/16
2 <0.01 0.00 0.00 13.40
Sock
5/5/16
2 <0.01 0.00 0.00 13.66
Sock
6/14/16
2 0.02 0.00 0.00 13.92
Sock
12/27/16
2 0.015 0.00 0.00 16.62
Sock
12/27-12/28/16
Surfactant injection/extraction event
12/29/16
2 <0.01 0 0.00 17.80
AFVR
9/5/17
2 <0.01 0 0.00 15.94
Sock

TABLE B-8 cont. FREE PRODUCT RECOVERY RESULTS
Date: September 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Free Product Recovery Method: Bailer/Passive Skimmer/Sock/AFVR Facility ID#: Not established
Method of Measurement: Bailer / Interface probe
Well ID
Product Type
Date of
Recovery
Casing
Diameter
(inches)
Product
Thickness
Before
Recovery (ft.)
Product
Thickness After
Recovery (ft.)
Amount of
Product
Recovered
(gallons)
Depth to Water
from Top of
Casing (ft.)
Comments
RW-1
Fuel Oil
11/24/03
4
0.05
0
0.25
15.20
Bailer
12/19/03
4
0.15
0
0.25
15.32
Bailer
1/29/04
4
0.42
0
0.25
15.56
Bailer
3/9/04
4
0.05
0
2.00
13.32
AFVR
4/8/04
4
0.15
0
0.25
13.29
Bailer
5/10 to 5/19/04
Source Removal:
UST and 416
tons of contaminated
soil removed
to depth of 17
feet.
5/24/04
4
0.17
0
0.30
13.43
Bailer
6/23/04
4
0.23
0
0.30
15.38
Bailer
7/28/04
4
0.27
0
0.30
15.46
Bailer
8/27/04
4
0.29
0
0.30
15.75
Bailer
10/5/04
4
0.15
0
0.30
13.87
Bailer
11/1/04
4
0.17
0
0.30
14.91
Bailer
12/2/04
4
0.03
0
<0.25
14.74
Bailer
2/27/14
4
<0.01
0
0.00
14.00
---
5/27/15
4
0.01
0
0.00
14.68
---
7/28/15
4
0.01
0
0.00
17.31
---
1/28/15
4
<0.01
0
0.00
13.41
---
2/28/16
4
<0.01
0
0.00
13.49
---
3/31/16
4
<0.01
0
0.00
13.23
---
4/14/16
4
<0.01
0
0.00
13.27
---
5/5/16
4
<0.01
0
0.00
13.66
---
6/14/16
4
<0.01
0
0.00
13.90
---
5/5/16
4
<0.01
0
0.00
13.66
---
12/29/16
4
<0.01
0
0.00
13.62
---
9/5/17
4
<0.01
0
0.00
15.82
---
Total Gallons Recovered to Date: Approximately 6.25 gallons

Appendix A
Field Sampling Sheets

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: Job #:
Sample Type: Circle one -(Monitor Well, DPT, Surface Water, Potable WSW; other)
Sample ID: QI/
Date: ' < t.
Sampling Personnel:
Weather Conditions: un
Partly Cloudy, Cloudy, Rain; Other
Time:
valo
Well Type: Flush S a a
Completion, Stick Up Completion
Well Tag Present:
es No
Well Locked: es No
Lock Present: Yes, No
Well ID info. on Tag: ed, No
Well Bolted: Jb
Well Cap: Yes, No
Well Cap Condition:
O o& Replace Other;
Well Pad Condition: o d
Cracked, Replace, Other:
Well Location: Grass, Asphalt, C
n re ,
Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Jq
Screen Length:
51 10, 05
20
feet -other:
Depth to Water D.T.W :
P!z
Well Diameter:
4, 6, 8
Inches -other:
Field Parameters measured with: ;c
Casing Type:
kV.U, Steel
other:
Purge Rate: /cc>
mL/min
Sampling Device:
Per stal c, Monsoon,
Grundfos, Bailer, Other:
Tubing Type: Poly yl ne,
Teflon, Other:
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.): ®
Color: CCU
Odor:
es, No sl .c ZAM c6w
Time:
min
Volume
Purged
DTW:
feet
Temp
CC)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(gallons)
(see note
below)3
+/-
3%
+/-
0.1 unit
+/-
3%
+/-
10%
+/-
10 mV
+/-
10%"
, �-(
J �
ji 6 l
/
4r
�a
�
r.7Y
4 ®
�
r�
r
L
y
3�1025I
c
oe
v
In
Official Sampling Date &Time:
Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab:
UG" S
YOK � ff/6el
CoP�+ AA13 bgoe dd; l 1 wa�rr Vogvhe�a Qb)oe�
Notes: 8&�6 4c, 56/ A"4_ CJUNlly/ops
(1) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2) - Stabilization criteria based on three most recent consecutive measurements. .
(3) - Total drawdown in well to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep drawdown below 0.1 m (0.32 ft). �(, L� ` 04s
(4) +/- 10 %when turbidity is over 10 NTUs.

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name:
Sample Type: Circle one -
(Monitor Well,
Job #:
DPT, Surface Water, Potable WSW; other)
Sample ID:
Date: ��d1
Sampling Personnel:
Weather Conditions: nn
, Partly Cloudy,
Cloudy, Rain; Other
Time: `Et3
Well Type: Flush qQde
Completion, Stick
Up Completion
Well Tag Present:
Ye , No
Well Locked: No
Lock Present: 4;�) No
Well ID info. on Tag:�YF211`l No
Well Bolted: Yes, o
Well Cap:
es, No
Well Cap Condition,
ood,
Replace, Other;
Well Pad Condition: ood,
Cracked, Replace, Other:
Well Location: Grass, Asphalt, C cr Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
51 10, 15 20 feet -other:
Depth to Water D.T.W : (')
ry .4*z
Well Diameter:
, 41 61 8 Inches -other:
Field Parameters measured with:
Casing Type:
Steel other:
Purge Rate: 4�09-
mUmin
Sampling Device:
Pe st Itic, Monsoon, Grundfos, Bailer, Other:
Tubing Type: Polyethylene,
Teflon, Other:
Measuring Point:
TOC other:
Pump Intake (ft below M.P.): 3X3
Color: l 11
Odor: es No w
Time:
min
Volume
Purged
DTW:
feet
Temp
CC)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(gallons)
(see note+/-
3%
0.1 unit
3%
10%
10 mV
1 °o
O
v
/below)'
/
Iq
�t
J . 2��^^^^��
GO
c)
"Don
7 ,al
��•
r
I
1Cis41/
Official Sampling Date &Time: V5/7 ` J'
Samples Collected: Analysis Requested: Preservative: Hold Time (days):
Notes•
(1) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2) -Stabilization cdteda based on three most recent consecutive measurements.
(3) -Total drawdown in well to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep drawdown below 0.1 m (0.32 fl).
(4) +/- 10%when turbidity is over 10 NTUs.
Lab:

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name:
Sample Type: Circle one -
Job #:
(Monitor Well, DPT, Surface Water, Potable WSW; other)
Sample ID:
Date: .o�
l
Sampling Personnel:
Weather Conditions: Sunny, Partly Cloudy, Cloudy,
Rain; Other
Time:
Well Type: Flush(suace
Completion, Stick Up Completion
Well Tag Present:
No
Well Locked: No
Lock Present: es,
No.
Well ID info. on Tag:
�D, No
Well Bolted: es, No
Well Cap: CesjNo
Well Cap Condition:
Gi&), Replace, Other;
Well Pad Condition: tob
Cracked, Replace, Other:
Well Location: Grass, Asphalt, Concrete,
Woods, Other; c
Additional Comments,
Total Depth of Well (T.D.):
Screen Length:
5, 10, 51 20
feet -other:
Depth to Water D.T.W . ('I
_
Well Diameter:
2 4, 6, s
Inches -other:
Field Parameters measured with:
Casing Type:
vC, Steel
other:
Purge Rate:
mL/min
Sampling Device:
P vista ic, Monsoon,
Grundfos, Bailer, Other:
Tubing Type: Polyet ne,
Teflon, Other:
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.):
Color: C y(J
Odor:
Yes, CO)
Time:
min
Volume
Purged
DTW:
feet
Temp
CC)
pH
std units
SPC
uS/cm
DO
mg/L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(gallons)
(see note
below)3
+/-
3%
+/-
0.1 unit
+/-
3%
+/-
10%
+/-
10 my
+/-
10%4
�2a4j
( Ji
�/
. SD
l
�.
/A r.
, 77
Q
r 2�
i �� .�
a?
z"liq
© q 7
�
i
3
i -
2Z
03
-�
r
Fj
Official Sampling Date &Time: 112 /
Samples Collected: Analysis Requested: Preservative:
Notes:
(i) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines Ihat may be resting on the well bottom.
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) -Total drawdown in well to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep tlrawdown below 0.1 m (0.32 ft).
Hold

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name:
Sample Type: Circle one - (Monitor Well,
DPT, Surface Water,
Potable WSW; other)
Job
#:
Sample ID:
Date:
Sampling Personnel:
Weather Conditions: Sunny, Partly Cloudy,
Cloudy,
Rain; Other
Time: 2
Well Type: F sh u ce
Completion, Stick Up Completion
Well Tag Present:
No
Well Locked: Y No
Lock Present: Yes,
No
Well ID info. on Tag:
s No
Well Bolted: es No
Well Cap:
Yes, No
Well Cap Condition:
Goo , Replace, Other;
Well Pad Condition: Good,
tack , Replace, Other:
Well Location: Grass,
Asphalt,
Concrete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
51 10,
20
feet -other:
Depth to Water D.T.W : (1)
3 f
Well Diameter:
21 41 s,
a
Inches -other:
Field Parameters measured with:
VCasing
Type:
PVC, Steel
other:
Purge Rate:
mUrnin
Sampling Device:
Peristaltic,
Monsoon, Grundfos, Bailer, Other:
Tubing Type: Polyethylene,
Teflon, Other:
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.):
Color:
Odor:
Yes, No
Time:
min
Volume
Purged
DTW:
feet
Temp
(eC)
pH
std units
SPC
uS/cm
DO
mg/L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria`
(gallons)
(see note+/
below)'
3%
0.1 unit
3%
10%
10 mV
-
10%4
t
or
T
�f� a
s
'At
Ke
Official Sampling Date &Time: � Lf
Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab:
Notes:
(1) - Do not measure depth to bottom of well unfit after purging and sampling to reduce resuspending fines that maybe resting on the well bottom.
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) -Total drawdown in well to be less than 0.1 m (0.32 fl). Purging rate to be lowered as necessary to keep drawdown below 0.1 m (0.32 ft).
(4) +/-10% when turbidity is over 10 NTUs.

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name:
Sample Type: Circle one - (Monitor Well, DPT, Surface Water, Potable WSW; other)
Job #:
Sample ID: v —
Date: � �/
Sampling Personnel:
Weather Conditions: S n , Partly Cloudy, Cloudy, Rain; Other
Time:
Well Type: Flush &Ace
Completion, Stick Up Completion
Well Tag Present:
e , No
Well Locked: e , No
Lock Present: W, No
Well ID info. on Tag:
Yes, No C►*
Well Bolted: ta No
Well Cap: es No
Well Cap Condition:G(Lod)
Replace, Other;
Well Pad Condition: Good,
Cx cke , Replace, Other:
Well Location: Grass,
Asphalt, Concrete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
51 10, 20
feet -other:
Dept to Water D.T.W : t+l
Well Diameter:
41 s, s
Inches -other:
Field Parameters measured with:
Casing Type:
09 Steel
other:
Purge Rate: too
mUmin
Sampling Device:
Per' 'c, Monsoon, Grundfos, Bailer, Other:
Tubing Type: Poly toy
ne,
Teflon, Other:
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.):
Color: eerjr Odor:
Yes, No OL
Time:
min
Volume
Purged
DTW:
feet
Temp
(eC)
pH
std units
SPC
uS/cm
DO
mg/L
ORP
mV
Turb
NTU
Comments:
Stabalization
(gallons)
(see noteCriteria`
below)3
3%
0.1 unit
3%
10%
10 my
10%4
e
?
l
�/yy
V!
!
u
r
!�
®.
1
J
%
7
r7/71
,
Official Samplinq Date &Time:
Samples Collected: Analysis Requested: Preservative: Hold Time (days): Lab:
Notes:
(1) - Do not measure depth to bottom of vrell until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2) -Stabilization crfteda based on three most recent consecutive measurements.
(3) -Total drawdo�m In well l0 6e less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep drawdotm below 0.1 m (0.32 ft).
(4) +/- 10% when turbldily Is over 10 NTUs.

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name:
Sample Type: Circle one -
(Monitor Well,
DPT, Surface Water, Potable WSW; other)
Job #:
Sample ID:
Date: j
Sampling Personnel:
Weather Conditions: Senn
, Partly Cloudy,
Cloudy, Rain; Other
Time:
Well Type: Flush urfac
Completion, Stick Up Completion
Well Tag Present:
Yes,
Well Locked: Yes, Q
Lock Present: es, No
Well ID info. on Tag:
Yes, o
Well Bolted: es, No
W I Cap:
Yes, No
Well Cap Condition:
Good, Re
I Other;
Well Pad Condition: Good,
Cracik Replace, Other:
Well Location: Grass,
Asphalt, Concrete, Woods, Other;44 41
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
5, % 15,
20
feet -other:
Depth to Water D.T.W : t�l
Well Diameter:
4, 61 8
Inches -other:
Field Parameters measured with:
Casing Type:
I N Steel
other:
Purge Rate: 1
mumin
Sampling Device:
PCs! Itic, Monsoon, Grundfos, Bailer, Other:
Tubing Type: Polyethylene,
Teflon, Other:
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.): 11,35
Color:
Odor:
Yes, No
Time:
min
Volume
Purged
DTW:
feet
Temp
(eC)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(gallons)
(see note+/-
below)'
3%
0.1 unit
3%
10%
10 my
10%4
(00
t6
&'70'r
.d0
,
0
l
rbQ
�
-S�
/
c J
/
-7
s
l
1
/
,
Official Sampling Date &Time: 7 S
Samples Collected: Analysis Requested: Preservative: Hold Time (days) Lab:
Notes:
(1) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines that may he resting on the vrell bottom.
(2) -Stabilization crdeda based on three most recent consecutive measurements.
(3) -Total drawdown In well to be less than 0.1 m (0.32 fl). Purging rate to be lowered as necessary to keep drawdo5m below 0.1 m (0.32 ft).
(4) +/-10%when turbidity Is over 10 NTUs.

Appendix B
Laboratory Analytical Report

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM NC, Inc.
Ballantyne One
15720 Brixham Hill Avenue, Suite 120
Charlotte, NC 28277
Attention: Michael Pressley
Project Name: Atando Avenue
Project Number: 345276
Lot Number:S106112
Date Completed:09/19/2017
09/19/2017 12:58 PM
Approved and released by:
Project Manager: Kelly M. Nance
pCCRF
LABORATORY
ACCREDITATION
RFCRRXIIIR BUREAU adlvision of A-S-R
qe ACCREDITED FSaIFEC,7o25
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 84

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
ERM NC, Inc.
Lot Number: S106112
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative.
The sample receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC
standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating
procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the
results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Volatiles
Sample -001 was diluted 5x due to matrix interference. The report limits have been raised accordingly.
Semivolatiles
The LCS associated with batch 50990 had 2-chloronaphthalene recovered marginally outside of the acceptance
limits. Due to the large number of analytes in the LCS, there is a high statistical probability of a few analytes outside
of control limits. Per SW-846 Update V 8000D- 23 Revision 4 July 2014, a number of analytes should be allowed to
marginally fail the limits without requirement for corrective action. The laboratory's SOP allows for 10% of analytes
to recover marginally outside criteria.
Sample -001 was diluted 10x due to matrix interference. The reporting limits have been raised accordingly. As a result, the
associated surrogate was recovered outside of the acceptance limits. No corrective action was required, as dilutions
of 5x and greater impact recovery accuracy.
MA-EPH
Samples -001, -004 and -005 had surrogates recovered outside of the acceptance limits due to confirmed matrix interference.
MA-VPH
Sample -001 was diluted 10x due to matrix interference. The reporting limits have been raised accordingly.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 84

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM NC, Inc.
Lot Number: S106112
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
MW-1
Aqueous
09/05/20171210
09/06/2017
002
MW-2
Aqueous
09/05/20171315
09/06/2017
003
MW-3
Aqueous
09/05/20171050
09/06/2017
004
MW-4
Aqueous
09/05/20171450
09/06/2017
005
MW-5
Aqueous
09/05/20171530
09/06/2017
006
DW-1
Aqueous
09/05/20171405
09/06/2017
(6 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 84

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
ERM NC, Inc.
Lot Number: S106112
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
MW-1
Aqueous
Benzene
8260B
47
ug/L
6
001
MW-1
Aqueous
Ethylbenzene
8260B
28
ug/L
6
001
MW-1
Aqueous
Xylenes (total)
8260B
6.7
ug/L
6
001
MW-1
Aqueous
Acenaphthene
625
19
ug/L
7
001
MW-1
Aqueous
Anthracene
625
21
ug/L
7
001
MW-1
Aqueous
Fluorene
625
36
ug/L
7
001
MW-1
Aqueous
Naphthalene
625
240
ug/L
8
001
MW-1
Aqueous
Phenanthrene
625
98
ug/L
8
001
MW-1
Aqueous
C9 - C18 Aliphatics
MADEP-EPH-
7700
ug/L
9
001
MW-1
Aqueous
C19 - C36 Aliphatics
MADEP-EPH-
950
ug/L
9
001
MW-1
Aqueous
C11 - C22 Aromatics
MADEP-EPH-
5000
ug/L
10
001
MW-1
Aqueous
C9 - C12 Aliphatics
MADEP-VPH-
950
ug/L
11
001
MW-1
Aqueous
C9 - C10 Aromatics
MADEP-VPH-
730
ug/L
12
002
MW-2
Aqueous
Benzene
8260B
59
ug/L
13
002
MW-2
Aqueous
Ethylbenzene
8260B
14
ug/L
13
002
MW-2
Aqueous
Xylenes (total)
8260B
5.6
ug/L
13
002
MW-2
Aqueous
Acenaphthene
625
1.8
ug/L
14
002
MW-2
Aqueous
Fluorene
625
7.5
ug/L
14
002
MW-2
Aqueous
Naphthalene
625
84
ug/L
15
002
MW-2
Aqueous
Phenanthrene
625
8.4
ug/L
15
002
MW-2
Aqueous
C11 - C22 Aromatics
MADEP-EPH-
600
ug/L
17
002
MW-2
Aqueous
C5 - C8 Aliphatics
MADEP-VPH-
92
ug/L
18
002
MW-2
Aqueous
C9 - C12 Aliphatics
MADEP-VPH-
280
ug/L
18
002
MW-2
Aqueous
C9 - C10 Aromatics
MADEP-VPH-
290
ug/L
19
003
MW-3
Aqueous
Benzene
8260B
3.2
ug/L
20
003
MW-3
Aqueous
Naphthalene
625
4.6
ug/L
22
004
MW-4
Aqueous
Benzo(a)anthracene
625
2.3
ug/L
28
004
MW-4
Aqueous
Benzo(a)pyrene
625
3.3
ug/L
28
004
MW-4
Aqueous
Benzo(b)fluoranthene
625
6.2
ug/L
28
004
MW-4
Aqueous
Benzo(g,h,i)perylene
625
1.7
ug/L
28
004
MW-4
Aqueous
Benzo(k)fluoranthene
625
2.0
ug/L
28
004
MW-4
Aqueous
Chrysene
625
3.2
ug/L
28
004
MW-4
Aqueous
bis(2-Ethylhexyl)phthalate
625
1.7
ug/L
28
004
MW-4
Aqueous
Fluoranthene
625
4.3
ug/L
28
004
MW-4
Aqueous
Indeno(1,2,3-c,d)pyrene
625
1.7
ug/L
28
004
MW-4
Aqueous
Pyrene
625
3.3
ug/L
29
005
MW-5
Aqueous
Benzene
8260B
1.2
ug/L
34
005
MW-5
Aqueous
C5 - C8 Aliphatics
MADEP-VPH-
2000
ug/L
39
006
DW-1
Aqueous
C5 - C8 Aliphatics
MADEP-VPH-
140
ug/L
46
(39 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 84

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-001
Description: MW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1210
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 5 09/13/2017 0446 ECP 51234
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Benzene
71-43-2
8260B
47
5.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
5.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
5.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
5.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
5.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
5.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
5.0
ug/L
1
Ethylbenzene
100-41-4
8260B
28
5.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
5.0
ug/L
1
Toluene
108-88-3
8260B
ND
5.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
6.7
5.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 98 70-130
Bromofluorobenzene 104 70-130
Toluene-d8 102 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-001
Description: MW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1210
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 10 09/12/2017 2123 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
625
19
16
ug/L
1
Acenaphthylene
208-96-8
625
ND
16
ug/L
1
Anthracene
120-12-7
625
21
16
ug/L
1
Benzidine
92-87-5
625
ND
80
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
16
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
16
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
16
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
16
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
16
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
16
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
16
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
16
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
16
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
16
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
16
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
16
ug/L
1
2-Chlorophenol
95-57-8
625
ND
16
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
16
ug/L
1
Chrysene
218-01-9
625
ND
16
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
16
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
16
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
16
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
16
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
80
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
16
ug/L
1
Diethylphthalate
84-66-2
625
ND
16
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
16
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
16
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
16
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
80
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
80
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
32
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
32
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
16
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
16
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
16
ug/L
1
Fluoranthene
206-44-0
625
ND
16
ug/L
1
Fluorene
86-73-7
625
36
16
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
16
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
16
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
80
ug/L
1
Hexachloroethane
67-72-1
625
ND
16
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
16
ug/L
1
Isophorone
78-59-1
625
ND
16
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-001
Description: MW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1210
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 10 09/12/2017 2123 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Naphthalene
91-20-3
625
240
16
ug/L
1
Nitrobenzene
98-95-3
625
ND
16
ug/L
1
2-Nitrophenol
88-75-5
625
ND
32
ug/L
1
4-Nitrophenol
100-02-7
625
ND
80
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
16
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
16
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
16
ug/L
1
Pentachlorophenol
87-86-5
625
ND
80
ug/L
1
Phenanthrene
85-01-8
625
98
16
ug/L
1
Phenol
108-95-2
625
ND
16
ug/L
1
Pyrene
129-00-0
625
ND
16
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
16
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
16
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
60
37-129
2-Fluorophenol
43
24-127
Nitrobenzene-d5
62
38-127
Phenol-d5
54
28-128
Terphenyl-d14
58
10-148
2,4,6-Tribromophenol
N 151
41-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 84

MADEP EPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-001
Description: MW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1210
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 5 09/14/2017 1935 PMS 09/13/2017 1402 51276
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-0 7700 560 ug/L 2
C19 - C36 Aliphatics MADEP-EPH-0 950 560 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) N 2.4 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 84

MADEP EPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-001
Description: MW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1210
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 5 09/14/2017 2205 PMS 09/13/2017 1402 51275
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-0 5000 560 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) N 25 40-140
2-Fluorobiphenyl (fractionation 1) 93 40-140
2-Bromonaphthalene (fractionation 2) 65 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 84

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-001
Description: MW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1210
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 10 09/12/2017 2212 JJG 51240
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 750 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- 950 750 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
90 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 84

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-001
Description: MW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1210
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 10 09/12/2017 2212 JJG 51239
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH- 730 250 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
83 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 84

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-002
Description: MW-2 Matrix: Aqueous
Date Sampled:09/05/2017 1315
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/13/2017 0422 ECP 51234
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Benzene
71-43-2
8260B
59
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
14
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
5.6
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 70-130
Bromofluorobenzene 108 70-130
Toluene-d8 105 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-002
Description: MW-2 Matrix: Aqueous
Date Sampled:09/05/2017 1315
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/12/2017 2147 CMP2 09/08/2017 1640 50990
2 625 625 5 09/13/2017 1836 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
625
1.8
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
1.6
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
ug/L
1
Fluorene
86-73-7
625
7.5
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 13 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-002
Description: MW-2 Matrix: Aqueous
Date Sampled:09/05/2017 1315
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/12/2017 2147 CMP2 09/08/2017 1640 50990
2 625 625 5 09/13/2017 1836 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Isophorone
78-59-1
625
ND
1.6
ug/L
1
Naphthalene
91-20-3
625
84
8.0
ug/L
2
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
8.4
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
ND
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1
Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery
Limits Q
% Recovery
Limits
2-Fluorobiphenyl
49
37-129
73
37-129
2-Fluorophenol
54
24-127
50
24-127
Nitrobenzene-d5
63
38-127
79
38-127
Phenol-d5
56
28-128
73
28-128
Terphenyl-d14
70
10-148
74
10-148
2,4,6-Tribromophenol
97
41-144
84
41-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 14 of 84

MADEP EPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-002
Description: MW-2 Matrix: Aqueous
Date Sampled:09/05/2017 1315
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/13/2017 1128 PMS 09/07/2017 1342 51167
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) 44 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 15 of 84

MADEP EPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-002
Description: MW-2 Matrix: Aqueous
Date Sampled:09/05/2017 1315
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/13/2017 1400 PMS 09/07/2017 1342 51168
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-0 600 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) 67 40-140
2-Fluorobiphenyl (fractionation 1) 77 40-140
2-Bromonaphthalene (fractionation 2) 69 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 16 of 84

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-002
Description: MW-2 Matrix: Aqueous
Date Sampled:09/05/2017 1315
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/12/2017 2240 JJG 51240
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH- 92 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- 280 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
122 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 17 of 84

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-002
Description: MW-2 Matrix: Aqueous
Date Sampled:09/05/2017 1315
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/12/2017 2240 JJG 51239
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH- 290 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
96 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 18 of 84

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-003
Description: MW-3 Matrix: Aqueous
Date Sampled:09/05/2017 1050
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/13/2017 0248 ECP 51234
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Benzene
71-43-2
8260B
3.2
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 100 70-130
Bromofluorobenzene 103 70-130
Toluene-d8 101 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 19 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-003
Description: MW-3 Matrix: Aqueous
Date Sampled:09/05/2017 1050
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/13/2017 1901 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
625
ND
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
1.6
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
ug/L
1
Fluorene
86-73-7
625
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
ug/L
1
Isophorone
78-59-1
625
ND
1.6
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 20 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-003
Description: MW-3 Matrix: Aqueous
Date Sampled:09/05/2017 1050
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/13/2017 1901 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Naphthalene
91-20-3
625
4.6
1.6
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
ND
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
68
37-129
2-Fluorophenol
48
24-127
Nitrobenzene-d5
77
38-127
Phenol-d5
58
28-128
Terphenyl-d14
72
10-148
2,4,6-Tribromophenol
76
41-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 21 of 84

MADEP EPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-003
Description: MW-3 Matrix: Aqueous
Date Sampled:09/05/2017 1050
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/13/2017 1158 PMS 09/07/2017 1342 51167
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) 60 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 22 of 84

MADEP EPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-003
Description: MW-3 Matrix: Aqueous
Date Sampled:09/05/2017 1050
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/13/2017 1430 PMS 09/07/2017 1342 51168
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-0 ND 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) 78 40-140
2-Fluorobiphenyl (fractionation 1) 77 40-140
2-Bromonaphthalene (fractionation 2) 64 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 23 of 84

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-003
Description: MW-3 Matrix: Aqueous
Date Sampled:09/05/2017 1050
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/12/2017 2308 JJG 51240
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
105 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 24 of 84

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-003
Description: MW-3 Matrix: Aqueous
Date Sampled:09/05/2017 1050
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/12/2017 2308 JJG 51239
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
92 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 25 of 84

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-004
Description: MW-4 Matrix: Aqueous
Date Sampled:09/05/2017 1450
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 09/13/2017 0312 ECP 51234
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Benzene
71-43-2
8260B
ND
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 105 70-130
Toluene-d8 102 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 26 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-004
Description: MW-4 Matrix: Aqueous
Date Sampled:09/05/2017 1450
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/13/2017 1951 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
625
ND
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
2.3
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
3.3
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
6.2
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
1.7
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
2.0
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
3.2
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
1.7
1.6
ug/L
1
Fluoranthene
206-44-0
625
4.3
1.6
ug/L
1
Fluorene
86-73-7
625
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
1.7
1.6
ug/L
1
Isophorone
78-59-1
625
ND
1.6
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 27 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-004
Description: MW-4 Matrix: Aqueous
Date Sampled:09/05/2017 1450
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/13/2017 1951 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Naphthalene
91-20-3
625
ND
1.6
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
3.3
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
67
37-129
2-Fluorophenol
63
24-127
Nitrobenzene-d5
76
38-127
Phenol-d5
74
28-128
Terphenyl-d14
70
10-148
2,4,6-Tribromophenol
72
41-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 28 of 84

MADEP EPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-004
Description: MW-4 Matrix: Aqueous
Date Sampled:09/05/2017 1450
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 1 09/14/2017 2005 PMS 09/13/2017 1402 51276
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-0 ND 110 ug/L 2
C19 - C36 Aliphatics MADEP-EPH-0 ND 110 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) N 5.5 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 29 of 84

MADEP EPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-004
Description: MW-4 Matrix: Aqueous
Date Sampled:09/05/2017 1450
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 1 09/14/2017 2235 PMS 09/13/2017 1402 51275
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-0 ND 110 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) 50 40-140
2-Fluorobiphenyl (fractionation 1) 84 40-140
2-Bromonaphthalene (fractionation 2) 71 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 30 of 84

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-004
Description: MW-4 Matrix: Aqueous
Date Sampled:09/05/2017 1450
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/12/2017 2337 JJG 51240
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
92 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 31 of 84

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-004
Description: MW-4 Matrix: Aqueous
Date Sampled:09/05/2017 1450
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/12/2017 2337 JJG 51239
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
85 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 32 of 84

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-005
Description: MW-5 Matrix: Aqueous
Date Sampled:09/05/2017 1530
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 5030B 8260B 1 09/14/20171052 BWS 51394
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Benzene
71-43-2
8260B
1.2
1.0
ug/L
2
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
2
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
2
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
2
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
2
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
2
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
2
Ethylbenzene
100-41-4
8260B
ND
1.0
ug/L
2
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
2
Toluene
108-88-3
8260B
ND
1.0
ug/L
2
Xylenes (total)
1330-20-7
8260B
ND
1.0
ug/L
2
Run 2 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 70-130
Bromofluorobenzene 100 70-130
Toluene-d8 103 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 33 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-005
Description: MW-5 Matrix: Aqueous
Date Sampled:09/05/2017 1530
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/13/2017 2015 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
625
ND
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
1.6
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
ug/L
1
Fluorene
86-73-7
625
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
ug/L
1
Isophorone
78-59-1
625
ND
1.6
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 34 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-005
Description: MW-5 Matrix: Aqueous
Date Sampled:09/05/2017 1530
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/13/2017 2015 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Naphthalene
91-20-3
625
ND
1.6
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
ND
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
62
37-129
2-Fluorophenol
44
24-127
Nitrobenzene-d5
71
38-127
Phenol-d5
64
28-128
Terphenyl-d14
68
10-148
2,4,6-Tribromophenol
68
41-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 35 of 84

MADEP EPH (aliphatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: S106112-005
Description: MW-5 Matrix: Aqueous
Date Sampled:09/05/2017 1530
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/11/2017 1840 PMS 09/07/2017 1342 50826
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C19 - C36 Aliphatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
C9 - C18 Aliphatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) - UnfractionatedN 20 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 36 of 84

MADEP EPH (aromatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: S106112-005
Description: MW-5 Matrix: Aqueous
Date Sampled:09/05/2017 1530
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/11/2017 1840 PMS 09/07/2017 1342 50828
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) - Unfractionated 68 40-140
2-Fluorobiphenyl (fractionation 1) 83 40-140
2-Bromonaphthalene (fractionation 2) 80 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 37 of 84

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-005
Description: MW-5 Matrix: Aqueous
Date Sampled:09/05/2017 1530
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 5 09/13/2017 0005 JJG 51240
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH- 2000 380 ug/L 1
C9 - C12 Aliphatics MADEP-VPH-0 ND 380 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
96 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 38 of 84

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-005
Description: MW-5 Matrix: Aqueous
Date Sampled:09/05/2017 1530
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 5 09/13/2017 0005 JJG 51239
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 130 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
88 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 39 of 84

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-006
Description: DW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1405
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 5030B 8260B 1 09/14/20171115 BWS 51394
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Benzene
71-43-2
8260B
ND
1.0
ug/L
2
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
2
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
2
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
2
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
2
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
2
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
2
Ethylbenzene
100-41-4
8260B
ND
1.0
ug/L
2
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
2
Toluene
108-88-3
8260B
ND
1.0
ug/L
2
Xylenes (total)
1330-20-7
8260B
ND
1.0
ug/L
2
Run 2 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 102 70-130
Bromofluorobenzene 107 70-130
Toluene-d8 104 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 40 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-006
Description: DW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1405
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/14/2017 1246 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
625
ND
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
1.6
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
ug/L
1
Fluorene
86-73-7
625
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
ug/L
1
Isophorone
78-59-1
625
ND
1.6
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 41 of 84

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: S106112-006
Description: DW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1405
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 09/14/2017 1246 CMP2 09/08/2017 1640 50990
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Naphthalene
91-20-3
625
ND
1.6
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
ND
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
72
37-129
2-Fluorophenol
66
24-127
Nitrobenzene-d5
81
38-127
Phenol-d5
75
28-128
Terphenyl-d14
80
10-148
2,4,6-Tribromophenol
75
41-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 42 of 84

MADEP EPH (aliphatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: S106112-006
Description: DW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1405
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/11/2017 1910 PMS 09/07/2017 1342 50826
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C19 - C36 Aliphatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
C9 - C18 Aliphatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) - Unfractionated 43 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 43 of 84

MADEP EPH (aromatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: S106112-006
Description: DW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1405
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 09/11/2017 1910 PMS 09/07/2017 1342 50828
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) - Unfractionated 64 40-140
2-Fluorobiphenyl (fractionation 1) 78 40-140
2-Bromonaphthalene (fractionation 2) 74 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 44 of 84

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: S106112-006
Description: DW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1405
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/13/2017 0033 JJG 51240
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH- 140 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
92 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 45 of 84

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: S106112-006
Description: DW-1 Matrix: Aqueous
Date Sampled:09/05/2017 1405
Date Received:09/06/2017
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 09/13/2017 0033 JJG 51239
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
85 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 46 of 84

QC Summary
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 47 of 84

Volatile Organic Compounds by GC/MS - MB
Sample ID: SQ51234-001 Matrix: Aqueous
Batch51234 Prep Method: 5030E
Analytical Method: 8260B
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Benzene
ND
1
1.0
ug/L
09/12/2017 2040
Chlorobenzene
ND
1
1.0
ug/L
09/12/2017 2040
1,2-Dibromoethane (EDB)
ND
1
1.0
ug/L
09/12/2017 2040
1,2-Dichlorobenzene
ND
1
1.0
ug/L
09/12/2017 2040
1,3-Dichlorobenzene
ND
1
1.0
ug/L
09/12/2017 2040
1,4-Dichlorobenzene
ND
1
1.0
ug/L
09/12/2017 2040
Diisopropyl ether (IPE)
ND
1
1.0
ug/L
09/12/2017 2040
Ethylbenzene
ND
1
1.0
ug/L
09/12/2017 2040
Methyl tertiary butyl ether (MTBE)
ND
1
1.0
ug/L
09/12/2017 2040
Toluene
ND
1
1.0
ug/L
09/12/2017 2040
Xylenes (total)
ND
1
1.0
ug/L
09/12/2017 2040
Acceptance
Surrogate
0
Q /o Rec
Limit
1,2-Dichloroethane-d4 98 70-130
Bromofluorobenzene 102 70-130
Toluene-d8 99 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 48 of 84

Volatile Organic Compounds by GC/MS - LCS
Sample ID: SQ51234-002
Matrix: Aqueous
Batch51234
Prep Method:
5030E
Analytical Method: 8260B
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Benzene
50
49
1
97
70-130
09/12/2017 1943
Chlorobenzene
50
48
1
96
70-130
09/12/2017 1943
1,2-Dibromoethane (EDB)
50
48
1
97
70-130
09/12/2017 1943
1,2-Dichlorobenzene
50
47
1
93
70-130
09/12/2017 1943
1,3-Dichlorobenzene
50
46
1
93
70-130
09/12/2017 1943
1,4-Dichlorobenzene
50
47
1
93
70-130
09/12/2017 1943
Diisopropyl ether (IPE)
50
46
1
92
70-130
09/12/2017 1943
Ethylbenzene
50
48
1
97
70-130
09/12/2017 1943
Methyl tertiary butyl ether (MTBE)
50
42
1
85
70-130
09/12/2017 1943
Toluene
50
49
1
98
70-130
09/12/2017 1943
Xylenes (total)
100
94
1
94
70-130
09/12/2017 1943
Acceptance
Surrogate
0
Q /o Rec
Limit
1,2-Dichloroethane-d4 95 70-130
Bromofluorobenzene 102 70-130
Toluene-d8 98 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 49 of 84

Volatile Organic Compounds by GC/MS - MB
Sample ID: SQ51394-001 Matrix: Aqueous
Batch51394 Prep Method: 5030E
Analytical Method: 8260B
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Benzene
ND
1
1.0
ug/L
09/14/2017 0927
Chlorobenzene
ND
1
1.0
ug/L
09/14/2017 0927
1,2-Dibromoethane (EDB)
ND
1
1.0
ug/L
09/14/2017 0927
1,2-Dichlorobenzene
ND
1
1.0
ug/L
09/14/2017 0927
1,3-Dichlorobenzene
ND
1
1.0
ug/L
09/14/2017 0927
1,4-Dichlorobenzene
ND
1
1.0
ug/L
09/14/2017 0927
Diisopropyl ether (IPE)
ND
1
1.0
ug/L
09/14/2017 0927
Ethylbenzene
ND
1
1.0
ug/L
09/14/2017 0927
Methyl tertiary butyl ether (MTBE)
ND
1
1.0
ug/L
09/14/2017 0927
Toluene
ND
1
1.0
ug/L
09/14/2017 0927
Xylenes (total)
ND
1
1.0
ug/L
09/14/2017 0927
Acceptance
Surrogate
0
Q /o Rec
Limit
1,2-Dichloroethane-d4 100 70-130
Bromofluorobenzene 103 70-130
Toluene-d8 101 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 50 of 84

Volatile Organic Compounds by GC/MS - LCS
Sample ID: SQ51394-002
Matrix: Aqueous
Batch51394
Prep Method:
5030E
Analytical Method: 8260B
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Benzene
20
20
1
102
70-130
09/14/2017 0831
Chlorobenzene
20
20
1
100
70-130
09/14/2017 0831
1,2-Dibromoethane (EDB)
20
20
1
98
70-130
09/14/2017 0831
1,2-Dichlorobenzene
20
19
1
97
70-130
09/14/2017 0831
1,3-Dichlorobenzene
20
20
1
99
70-130
09/14/2017 0831
1,4-Dichlorobenzene
20
20
1
99
70-130
09/14/2017 0831
Diisopropyl ether (IPE)
20
19
1
94
70-130
09/14/2017 0831
Ethylbenzene
20
20
1
101
70-130
09/14/2017 0831
Methyl tertiary butyl ether (MTBE)
20
17
1
86
70-130
09/14/2017 0831
Toluene
20
20
1
100
70-130
09/14/2017 0831
Xylenes (total)
40
39
1
98
70-130
09/14/2017 0831
Acceptance
Surrogate
0
Q /o Rec
Limit
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 104 70-130
Toluene-d8 100 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 51 of 84

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: SQ50990-001 Matrix: Aqueous
Batch50990 Prep Method: 625
Analytical Method: 625 Prep Date: 09/08/2017 1640
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Acenaphthene
ND
1
1.6
ug/L
09/12/2017 1222
Acenaphthylene
ND
1
1.6
ug/L
09/12/2017 1222
Anthracene
ND
1
1.6
ug/L
09/12/2017 1222
Benzidine
ND
1
8.0
ug/L
09/12/2017 1222
Benzo(a)anthracene
ND
1
1.6
ug/L
09/12/2017 1222
Benzo(a)pyrene
ND
1
1.6
ug/L
09/12/2017 1222
Benzo(b)fluoranthene
ND
1
1.6
ug/L
09/12/2017 1222
Benzo(g,h,i)perylene
ND
1
1.6
ug/L
09/12/2017 1222
Benzo(k)fluoranthene
ND
1
1.6
ug/L
09/12/2017 1222
4-Bromophenyl phenyl ether
ND
1
1.6
ug/L
09/12/2017 1222
Butyl benzyl phthalate
ND
1
1.6
ug/L
09/12/2017 1222
bis (2-Chloro-1-methylethyl) ether
ND
1
1.6
ug/L
09/12/2017 1222
4-Chloro-3-methyl phenol
ND
1
1.6
ug/L
09/12/2017 1222
bis(2-Chloroethoxy)methane
ND
1
1.6
ug/L
09/12/2017 1222
bis(2-Chloroethyl)ether
ND
1
1.6
ug/L
09/12/2017 1222
2-Chloronaphthalene
ND
1
1.6
ug/L
09/12/2017 1222
2-Chlorophenol
ND
1
1.6
ug/L
09/12/2017 1222
4-Chlorophenyl phenyl ether
ND
1
1.6
ug/L
09/12/2017 1222
Chrysene
ND
1
1.6
ug/L
09/12/2017 1222
Dibenzo(a,h)anthracene
ND
1
1.6
ug/L
09/12/2017 1222
1,2-Dichlorobenzene
ND
1
1.6
ug/L
09/12/2017 1222
1,3-Dichlorobenzene
ND
1
1.6
ug/L
09/12/2017 1222
1,4-Dichlorobenzene
ND
1
1.6
ug/L
09/12/2017 1222
3,3'-Dichlorobenzidine
ND
1
8.0
ug/L
09/12/2017 1222
2,4-Dichlorophenol
ND
1
1.6
ug/L
09/12/2017 1222
Diethylphthalate
ND
1
1.6
ug/L
09/12/2017 1222
Dimethyl phthalate
ND
1
1.6
ug/L
09/12/2017 1222
2,4-Dimethylphenol
ND
1
1.6
ug/L
09/12/2017 1222
Di-n-butyl phthalate
ND
1
1.6
ug/L
09/12/2017 1222
4,6-Dinitro-2-methyl phenol
ND
1
8.0
ug/L
09/12/2017 1222
2,4-Dinitrophenol
ND
1
8.0
ug/L
09/12/2017 1222
2,4-Dinitrotoluene
ND
1
3.2
ug/L
09/12/2017 1222
2,6-Dinitrotoluene
ND
1
3.2
ug/L
09/12/2017 1222
Di-n-octylphthalate
ND
1
1.6
ug/L
09/12/2017 1222
1,2-Diphenylhydrazine(as azobenzene)
ND
1
1.6
ug/L
09/12/2017 1222
bis(2-Ethylhexyl)phthalate
ND
1
1.6
ug/L
09/12/2017 1222
Fluoranthene
ND
1
1.6
ug/L
09/12/2017 1222
Fluorene
ND
1
1.6
ug/L
09/12/2017 1222
Hexachlorobenzene
ND
1
1.6
ug/L
09/12/2017 1222
Hexachlorobutadiene
ND
1
1.6
ug/L
09/12/2017 1222
Hexachlorocyclopentadiene
ND
1
8.0
ug/L
09/12/2017 1222
Hexachloroethane
ND
1
1.6
ug/L
09/12/2017 1222
Indeno(1,2,3-c,d)pyrene
ND
1
1.6
ug/L
09/12/2017 1222
Isophorone
ND
1
1.6
ug/L
09/12/2017 1222
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 52 of 84

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: SQ50990-001 Matrix: Aqueous
Batch50990 Prep Method: 625
Analytical Method: 625 Prep Date: 09/08/2017 1640
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Naphthalene
ND
1
1.6
ug/L
09/12/20171222
Nitrobenzene
ND
1
1.6
ug/L
09/12/20171222
2-Nitrophenol
ND
1
3.2
ug/L
09/12/20171222
4-Nitrophenol
ND
1
8.0
ug/L
09/12/20171222
N-Nitrosodimethylamine
ND
1
1.6
ug/L
09/12/20171222
N-Nitrosodi-n-propylamine
ND
1
1.6
ug/L
09/12/20171222
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
1.6
ug/L
09/12/2017 1222
Pentachlorophenol
ND
1
8.0
ug/L
09/12/20171222
Phenanthrene
ND
1
1.6
ug/L
09/12/20171222
Phenol
ND
1
1.6
ug/L
09/12/20171222
Pyrene
ND
1
1.6
ug/L
09/12/20171222
1,2,4-Trichlorobenzene
ND
1
1.6
ug/L
09/12/20171222
2,4,6-Trichlorophenol
ND
1
1.6
ug/L
09/12/20171222
Acceptance
Surrogate
0
Q /o Rec
Limit
2-Fluorobiphenyl
57
37-129
2-Fluorophenol
33
24-127
Nitrobenzene-d5
57
38-127
Phenol-d5
46
28-128
Terphenyl-d 14
69
10-148
2,4,6-Tribromophenol
67
41-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 53 of 84

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: SQ50990-002
Matrix: Aqueous
Batch50990
Prep Method:
625
Analytical Method: 625
Prep Date: 09/08/2017 1640
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
20
12
1
59
47-145
09/12/2017 1247
Acenaphthylene
20
11
1
57
33-145
09/12/2017 1247
Anthracene
20
12
1
61
27-133
09/12/2017 1247
Benzidine
100
30
1
30
1-150
09/12/2017 1247
Benzo(a)anthracene
20
14
1
69
33-143
09/12/2017 1247
Benzo(a)pyrene
20
14
1
68
17-163
09/12/2017 1247
Benzo(b)fluoranthene
20
15
1
75
24-159
09/12/2017 1247
Benzo(g,h,i)perylene
20
15
1
75
0-219
09/12/2017 1247
Benzo(k)fluoranthene
20
16
1
78
11-162
09/12/2017 1247
4-Bromophenyl phenyl ether
20
14
1
70
53-127
09/12/2017 1247
Butyl benzyl phthalate
20
12
1
59
0-152
09/12/2017 1247
bis (2-Chloro-1-methylethyl) ether
20
18
1
89
36-166
09/12/2017 1247
4-Chloro-3-methyl phenol
20
14
1
72
22-147
09/12/2017 1247
bis(2-Chloroethoxy)methane
20
14
1
71
33-184
09/12/2017 1247
bis(2-Chloroethyl)ether
20
13
1
66
12-158
09/12/2017 1247
2-Chloronaphthalene
20
11
N 1
55
60-118
09/12/2017 1247
2-Chlorophenol
20
11
1
53
23-134
09/12/2017 1247
4-Chlorophenyl phenyl ether
20
14
1
72
25-158
09/12/2017 1247
Chrysene
20
14
1
70
17-168
09/12/2017 1247
Dibenzo(a,h)anthracene
20
15
1
77
0-227
09/12/2017 1247
1,2-Dichlorobenzene
20
14
1
68
32-129
09/12/2017 1247
1,3-Dichlorobenzene
20
10
1
52
0-172
09/12/2017 1247
1,4-Dichlorobenzene
20
11
1
53
20-124
09/12/2017 1247
3,3'-Dichlorobenzidine
20
11
1
55
0-262
09/12/2017 1247
2,4-Dichlorophenol
20
13
1
66
39-135
09/12/2017 1247
Diethylphthalate
20
13
1
67
0-114
09/12/2017 1247
Dimethyl phthalate
20
13
1
66
0-112
09/12/2017 1247
2,4-Dimethylphenol
20
14
1
69
32-119
09/12/2017 1247
Di-n-butyl phthalate
20
13
1
65
1-118
09/12/2017 1247
4,6-Dinitro-2-methyl phenol
20
14
1
71
0-181
09/12/2017 1247
2,4-Dinitrophenol
40
24
1
61
0-191
09/12/2017 1247
2,4-Dinitrotoluene
20
13
1
67
39-139
09/12/2017 1247
2,6-Dinitrotoluene
20
13
1
63
50-158
09/12/2017 1247
Di-n-octylphthalate
20
13
1
67
4-146
09/12/2017 1247
1,2-Diphenylhydrazine(as azobenzene)
20
11
1
55
30-130
09/12/2017 1247
bis(2-Ethylhexyl)phthalate
20
12
1
61
8-158
09/12/2017 1247
Fluoranthene
20
14
1
70
26-137
09/12/2017 1247
Fluorene
20
13
1
63
59-121
09/12/2017 1247
Hexachlorobenzene
20
17
1
85
0-152
09/12/2017 1247
Hexachlorobutadiene
20
12
1
58
24-116
09/12/2017 1247
Hexachlorocyclopentadiene
100
45
1
45
1-150
09/12/2017 1247
Hexachloroethane
20
14
1
72
40-113
09/12/2017 1247
Indeno(1,2,3-c,d)pyrene
20
15
1
75
0-171
09/12/2017 1247
Isophorone
20
15
1
74
21-196
09/12/2017 1247
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 54 of 84

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: SQ50990-002
Matrix: Aqueous
Batch50990
Prep Method:
625
Analytical Method: 625
Prep Date: 09/08/2017 1640
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Naphthalene
20
13
1
64
21-133
09/12/20171247
Nitrobenzene
20
14
1
69
35-180
09/12/20171247
2-Nitrophenol
20
14
1
69
29-182
09/12/20171247
4-Nitrophenol
40
26
1
66
0-132
09/12/20171247
N-Nitrosodimethylamine
20
13
1
66
1-150
09/12/20171247
N-Nitrosodi-n-propylamine
20
20
1
101
0-230
09/12/20171247
N-Nitrosodiphenylamine (Diphenylamine) 20
10
1
51
1-150
09/12/2017 1247
Pentachlorophenol
40
29
1
74
14-176
09/12/20171247
Phenanthrene
20
12
1
62
54-120
09/12/20171247
Phenol
20
11
1
56
5-112
09/12/20171247
Pyrene
20
13
1
66
52-115
09/12/20171247
1,2,4-Trichlorobenzene
20
12
1
60
44-142
09/12/20171247
2,4,6-Trichlorophenol
20
13
1
67
37-144
09/12/20171247
Acceptance
Surrogate
0
Q /o Rec
Limit
2-Fluorobiphenyl
58
37-129
2-Fluorophenol
31
24-127
Nitrobenzene-d5
65
38-127
Phenol-d5
51
28-128
Terphenyl-d 14
72
10-148
2,4,6-Tribromophenol
76
41-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 55 of 84

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: S106112-003MS
Matrix: Aqueous
Batch50990
Prep Method: 625
Analytical Method: 625
Prep Date: 09/08/2017 1640
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
ND
20
15
1
73
47-145
09/13/2017 1926
Acenaphthylene
ND
20
15
1
76
33-145
09/13/2017 1926
Anthracene
ND
20
16
1
79
27-133
09/13/2017 1926
Benzidine
ND
100
43
1
43
1-150
09/13/2017 1926
Benzo(a)anthracene
ND
20
16
1
80
33-143
09/13/2017 1926
Benzo(a)pyrene
ND
20
14
1
71
17-163
09/13/2017 1926
Benzo(b)fluoranthene
ND
20
18
1
91
24-159
09/13/2017 1926
Benzo(g,h,i)perylene
ND
20
11
1
54
0-219
09/13/2017 1926
Benzo(k)fluoranthene
ND
20
19
1
94
11-162
09/13/2017 1926
4-Bromophenyl phenyl ether
ND
20
15
1
74
53-127
09/13/2017 1926
Butyl benzyl phthalate
ND
20
17
1
85
0-152
09/13/2017 1926
bis (2-Chloro-1-methylethyl) ether
ND
20
18
1
89
36-166
09/13/2017 1926
4-Chloro-3-methyl phenol
ND
20
16
1
78
22-147
09/13/2017 1926
bis(2-Chloroethoxy)methane
ND
20
16
1
81
33-184
09/13/2017 1926
bis(2-Chloroethyl)ether
ND
20
18
1
88
12-158
09/13/2017 1926
2-Chloronaphthalene
ND
20
14
1
70
60-118
09/13/2017 1926
2-Chlorophenol
ND
20
14
1
72
23-134
09/13/2017 1926
4-Chlorophenyl phenyl ether
ND
20
15
1
74
25-158
09/13/2017 1926
Chrysene
ND
20
16
1
81
17-168
09/13/2017 1926
Dibenzo(a,h)anthracene
ND
20
12
1
59
0-227
09/13/2017 1926
1,2-Dichlorobenzene
ND
20
13
1
66
32-129
09/13/2017 1926
1,3-Dichlorobenzene
ND
20
13
1
64
0-172
09/13/2017 1926
1,4-Dichlorobenzene
ND
20
13
1
64
20-124
09/13/2017 1926
3,3'-Dichlorobenzidine
ND
20
13
1
65
0-262
09/13/2017 1926
2,4-Dichlorophenol
ND
20
14
1
68
39-135
09/13/2017 1926
Diethylphthalate
ND
20
17
1
87
0-114
09/13/2017 1926
Dimethyl phthalate
ND
20
16
1
82
0-112
09/13/2017 1926
2,4-Dimethylphenol
ND
20
14
1
69
32-119
09/13/2017 1926
Di-n-butyl phthalate
ND
20
19
1
97
1-118
09/13/2017 1926
4,6-Dinitro-2-methyl phenol
ND
20
11
1
53
0-181
09/13/2017 1926
2,4-Dinitrophenol
ND
40
16
1
39
0-191
09/13/2017 1926
2,4-Dinitrotoluene
ND
20
17
1
85
39-139
09/13/2017 1926
2,6-Dinitrotoluene
ND
20
16
1
81
50-158
09/13/2017 1926
Di-n-octylphthalate
ND
20
19
1
94
4-146
09/13/2017 1926
1,2-Diphenylhydrazine(as azobenzene)
ND
20
17
1
84
30-130
09/13/2017 1926
bis(2-Ethylhexyl)phthalate
ND
20
17
1
84
8-158
09/13/2017 1926
Fluoranthene
ND
20
17
1
84
26-137
09/13/2017 1926
Fluorene
ND
20
15
1
77
59-121
09/13/2017 1926
Hexachlorobenzene
ND
20
15
1
74
0-152
09/13/2017 1926
Hexachlorobutadiene
ND
20
13
1
64
24-116
09/13/2017 1926
Hexachlorocyclopentadiene
ND
100
38
1
38
1-150
09/13/2017 1926
Hexachloroethane
ND
20
17
1
86
40-113
09/13/2017 1926
Indeno(1,2,3-c,d)pyrene
ND
20
12
1
59
0-171
09/13/2017 1926
Isophorone
ND
20
17
1
85
21-196
09/13/2017 1926
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 56 of 84

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: S106112-003MS
Matrix: Aqueous
Batch50990
Prep Method: 625
Analytical Method: 625
Prep Date: 09/08/2017 1640
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Naphthalene
4.6
20
19
1
70
21-133
09/13/20171926
Nitrobenzene
ND
20
16
1
79
35-180
09/13/20171926
2-Nitrophenol
ND
20
15
1
77
29-182
09/13/20171926
4-Nitrophenol
ND
40
34
1
85
0-132
09/13/20171926
N-Nitrosodimethylamine
ND
20
16
1
80
1-150
09/13/20171926
N-Nitrosodi-n-propylamine
ND
20
19
1
95
0-230
09/13/20171926
N-Nitrosodiphenylamine (Diphenylamine)
ND
20
14
1
69
1-150
09/13/2017 1926
Pentachlorophenol
ND
40
27
1
67
14-176
09/13/20171926
Phenanthrene
ND
20
16
1
79
54-120
09/13/20171926
Phenol
ND
20
15
1
74
5-112
09/13/20171926
Pyrene
ND
20
15
1
73
52-115
09/13/20171926
1,2,4-Trichlorobenzene
ND
20
13
1
67
44-142
09/13/20171926
2,4,6-Trichlorophenol
ND
20
14
1
68
37-144
09/13/20171926
Acceptance
Surrogate
0
Q /o Rec
Limit
2-Fluorobiphenyl
69
37-129
2-Fluorophenol
48
24-127
Nitrobenzene-d5
79
38-127
Phenol-d5
73
28-128
Terphenyl-d 14
68
10-148
2,4,6-Tribromophenol
76
41-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 57 of 84

MADEP EPH (aliphatics) - Unfractionated - MB
Sample ID: SQ50826-001 Matrix: Aqueous
Batch50826 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/07/2017 1342
Parameter Result Q Dil LOQ Units Analysis Date
C19 - C36 Aliphatics - Unfractionated ND 1 100 ug/L 09/11/2017 1509
C9 - C18 Aliphatics - Unfractionated ND 1 100 ug/L 09/11/2017 1509
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 69 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 58 of 84

MADEP EPH (aliphatics) - Unfractionated - LCS
Sample ID: SQ50826-002
Matrix: Aqueous
Batch50826
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/07/2017 1342
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
860
1 96
40-140 09/11/2017 1540
C9 - C18 Aliphatics - Unfractionated
650
480
1 73
40-140 09/11/2017 1540
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 94 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 59 of 84

MADEP EPH (aliphatics) - Unfractionated - LCSD
Sample ID: SQ50826-003
Matrix: Aqueous
Batch50826
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/07/2017 1342
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
860
1 96 0.11 40-140
25 09/11/2017 1610
C9 - C18 Aliphatics - Unfractionated
650
500
1 76 4.3 40-140
25 09/11/2017 1610
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 88 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 60 of 84

MADEP EPH (aromatics) - Unfractionated - MB
Sample ID: SQ50828-001 Matrix: Aqueous
Batch50828 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/07/2017 1342
Parameter Result Q Dil LOQ Units Analysis Date
C11 - C22 Aromatics - Unfractionated ND 1 100 ug/L 09/11/2017 1509
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) - Unfractionated
71
40-140
2-Fluorobiphenyl (fractionation 1)
81
40-140
2-Bromonaphthalene (fractionation 2)
77
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 61 of 84

MADEP EPH (aromatics) - Unfractionated - LCS
Sample ID: SQ50828-002
Matrix: Aqueous
Batch50828
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/07/2017 1342
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics - Unfractionated
1400
930
1 66 40-140 09/11/2017 1540
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) - Unfractionated
73
40-140
2-Fluorobiphenyl (fractionation 1)
82
40-140
2-Bromonaphthalene (fractionation 2)
78
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 62 of 84

MADEP EPH (aromatics) - Unfractionated - LCSD
Sample ID: SQ50828-003 Matrix: Aqueous
Batch50828 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/07/2017 1342
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics - Unfractionated 1400 940 1 67 1.7 40-140 25 09/11/2017 1610
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) - Unfractionated
73
40-140
2-Fluorobiphenyl (fractionation 1)
81
40-140
2-Bromonaphthalene (fractionation 2)
78
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 63 of 84

MADEP EPH (aliphatics) - MB
Sample ID: SQ51167-001 Matrix: Aqueous
Batch51167 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/07/2017 1342
Parameter Result Q Dil LOQ Units Analysis Date
C9 - C18 Aliphatics ND 1 100 ug/L 09/13/2017 0957
C19 - C36 Aliphatics ND 1 100 ug/L 09/13/2017 0957
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 56 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 64 of 84

MADEP EPH (aliphatics) - LCS
Sample ID: SQ51167-002
Matrix: Aqueous
Batch51167
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/07/2017 1342
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
180
1 59
40-140 09/13/2017 1027
C19 - C36 Aliphatics
400
340
1 85
40-140 09/13/2017 1027
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 85 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 65 of 84

MADEP EPH (aliphatics) - LCSD
Sample ID: SQ51167-003
Matrix: Aqueous
Batch51167
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/07/2017 1342
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
180
1 60 1.4 40-140
25 09/13/2017 1057
C19 - C36 Aliphatics
400
340
1 84 0.64 40-140
25 09/13/2017 1057
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 77 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 66 of 84

MADEP EPH (aromatics) - MB
Sample ID: SQ51168-001 Matrix: Aqueous
Batch51168 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/07/2017 1342
Parameter Result Q Dil LOQ Units Analysis Date
C11 - C22 Aromatics ND 1 100 ug/L 09/13/2017 1228
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 76 40-140
2-Fluorobiphenyl (fractionation 1) 75 40-140
2-Bromonaphthalene (fractionation 2) 57 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 67 of 84

MADEP EPH (aromatics) - LCS
Sample ID: SQ51168-002
Matrix: Aqueous
Batch51168
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/07/2017 1342
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
850
620
1 73 40-140 09/13/2017 1259
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 80 40-140
2-Fluorobiphenyl (fractionation 1) 76 40-140
2-Bromonaphthalene (fractionation 2) 66 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 68 of 84

MADEP EPH (aromatics) - LCSD
Sample ID: SQ51168-003 Matrix: Aqueous
Batch51168 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/07/2017 1342
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 850 620 1 73 0.87 40-140 25 09/13/2017 1329
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 78 40-140
2-Fluorobiphenyl (fractionation 1) 76 40-140
2-Bromonaphthalene (fractionation 2) 70 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 69 of 84

MADEP EPH (aromatics) - MB
Sample ID: SQ51275-001 Matrix: Aqueous
Batch51275 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/13/2017 1402
Parameter Result Q Dil LOQ Units Analysis Date
C11 - C22 Aromatics ND 1 100 ug/L 09/14/2017 2035
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 82 40-140
2-Fluorobiphenyl (fractionation 1) 89 40-140
2-Bromonaphthalene (fractionation 2) 77 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 70 of 84

MADEP EPH (aromatics) - LCS
Sample ID: SQ51275-002
Matrix: Aqueous
Batch51275
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/13/2017 1402
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
850
670
1 78 40-140 09/14/2017 2105
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 81 40-140
2-Fluorobiphenyl (fractionation 1) 87 40-140
2-Bromonaphthalene (fractionation 2) 76 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 71 of 84

MADEP EPH (aromatics) - LCSD
Sample ID: SQ51275-003 Matrix: Aqueous
Batch51275 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/13/2017 1402
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 850 670 1 79 0.57 40-140 25 09/14/2017 2135
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 82 40-140
2-Fluorobiphenyl (fractionation 1) 87 40-140
2-Bromonaphthalene (fractionation 2) 65 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 72 of 84

MADEP EPH (aliphatics) - MB
Sample ID: SQ51276-001 Matrix: Aqueous
Batch51276 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 09/13/2017 1402
Parameter Result Q Dil LOQ Units Analysis Date
C9 - C18 Aliphatics ND 1 100 ug/L 09/14/2017 1803
C19 - C36 Aliphatics ND 1 100 ug/L 09/14/2017 1803
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 58 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 73 of 84

MADEP EPH (aliphatics) - LCS
Sample ID: SQ51276-002
Matrix: Aqueous
Batch51276
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/13/2017 1402
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
140
1 45
40-140 09/14/2017 1834
C19 - C36 Aliphatics
400
310
1 77
40-140 09/14/2017 1834
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 66 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 74 of 84

MADEP EPH (aliphatics) - LCSD
Sample ID: SQ51276-003
Matrix: Aqueous
Batch51276
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 09/13/2017 1402
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
140
1 47 4.8 40-140
25 09/14/2017 1904
C19 - C36 Aliphatics
400
310
1 78 2.2 40-140
25 09/14/2017 1904
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 61 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 75 of 84

MADEP VPH (aromatics) - MB
Sample ID: SQ51239-001 Matrix: Aqueous
Batch51239 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil LOQ Units Analysis Date
C9 - C10 Aromatics ND 1 25 ug/L 09/12/2017 1838
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 88 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 76 of 84

MADEP VPH (aromatics) - LCS
Sample ID: SQ51239-002 Matrix: Aqueous
Batch51239 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 21 1 83 70-130 09/12/2017 1742
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 81 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 77 of 84

MADEP VPH (aromatics) - LCSD
Sample ID: SQ51239-003 Matrix: Aqueous
Batch51239 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 25 22 1 86 3.8 70-130 25 09/12/2017 1810
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 85 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 78 of 84

MADEP VPH (aliphatics) - MB
Sample ID: SQ51240-001 Matrix: Aqueous
Batch51240 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil LOQ Units Analysis Date
C5 - C8 Aliphatics ND 1 75 ug/L 09/12/2017 1838
C9 - C12 Aliphatics ND 1 75 ug/L 09/12/2017 1838
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 98 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 79 of 84

MADEP VPH (aliphatics) - LCS
Sample ID: SQ51240-002
Matrix: Aqueous
Batch51240
Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
C5 - C8 Aliphatics
150
150
1 97
70-130 09/12/2017 1742
C9 - C12 Aliphatics
180
150
1 86
70-130 09/12/2017 1742
Surrogate
Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID) 88 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 80 of 84

MADEP VPH (aliphatics) - LCSD
Sample ID: SQ51240-003
Matrix: Aqueous
Batch51240
Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics
150
150
1 99 2.0
70-130
25 09/12/2017 1810
C9 - C12 Aliphatics
180
160
1 90 4.7
70-130
25 09/12/2017 1810
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 92 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 81 of 84

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 82 of 84

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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 83 of 84

SHEALY ENVIRONMENTAL SERVICES, INC.
tihral}v RviromrncnLO geMcex, inn.
Documer,!.Vji J MI-tll)1$f:4)R
Pis 1 t rr 1
hflmi:ae U-AL- D-,.'2&2017
Exy-r7 a]atc: C"r2at2b..22
Samplo Ueceipt Checklist (SRC)
€'lieJIT; C CL)uhTln,,j)ected by/dat C -(• 1 1) Lot hl:'3 1 Q� t j
Mtl un-c nfTMC-ipt- WSLSI r. CliLMt ❑ UPS t I T'edT?x rr I)tltcr
yos C No I 1 1. Were cu6tndv .;cR2,4 �srnt on the cooler?
Y,7s No ❑ NrSr 2, If custody 11s >r+cra grrscnt, were they' iutati and rrnhr(ken?
pH stttl ip II). _ i� [ ] strip II).
Coulcr ID/Original t2irnNtatum. upon
rr+eceip?,Oeriyud (uorreeLeS) Lzrnperatnre upon receipt-
Method: 'T'elnperararc Stank - .4t�ijin31 Buttics 1R Gun TD; C IR Crun C;nrraction Paator:
M%:tlxjd of cxxalarr.: Woo -Ice ❑ t3Jue rce r Dry iu: I -a None
Yes ❑
r r I I
Tr
N,i LT,
- 1f telrsperrrlurc 4 5 f Kkny omler exceeded 6_0°C, was Project-Manaxr;r Norified'2
P1 NI ivas Notificd by-' horn / emah I face-lo- ace [citclu anti).
1 4. Ts the rommeLrOal c•ourier:s packing blip alCvuhofl to this t6rrn?
5. V4'crc L)per cu.�tndv parnrcdures (relinquishedircLcuivcd) followed'?
Yrs ❑
NO o
Yes 12"
NU u
Y'a,-
No ❑
6. Wore wirnplc Ws listed CM the COC?
?, Were sample II)s listed on 2JI samVlec4ttttainc,-B7
8, War colleeti(nk daiti & th ie lht) id ort ilu CDC?
9. Was ca lecdon dab- & time listed on nll ~ample cont-ainers'?
Yes a
No ❑
_ t:sj.�'
No ❑
No n
Yes
Y.Cs
No a
10- skid all container label irrfurmation (ID, dale, time.) 1) M with the COC?
1 1- ltdcrc tests to be perforruod listed on the co('12
12. Laid uli samlllrs arrive in the proper containers for tc.11 Hnd/or in goad Condition
(UTIt o)i' lids on, etc.)?
11 V4 as ad dare sample vulumc avai[able?
14. Were Al samples received wili)in 12 the holding* rirna of •14 hour€, whicllever Lwnrics first's
] 5. RTtiro any samples Conudnors missinglexce:{ (uirClc cmc) samples Not Iistcd on COC?
16. %Alcm bubbles pa.eSeE)t >°'peU_b:iu" (1f "or Timm in di,mrtcr) in any VOA vials?
Yes J�
Yer-_W.
No j
No ❑
Ycs
N, ❑
NA
'r
NO ❑
Yes ❑
Nil
Yes ❑
NO ❑
Ycs_Q-�_
Yes ❑ 1
Flo ❑
ETA 1'
1 . Were all DRO.hneGaI S nulricnl sam Ics r.ce.ved at a pH of f 2?
18. Were all cvanidle samples rem ivrd q4 a pH :- 12 and sutlide samples Mae ived9 AC H PU } 9'2,
No ❑
AT,-%r-
Ycr r
NO ❑
�-%. —`
19. Worn id applicable NjivrKNicymiduiphenol, 13NA (< MmDrL-) samples free of residual
cla.'sxrinc?
2ll. Wcre coIleci.Ull lernpuaiures documented 4-r1 liar. COC for N( .;arnlllcs?
yCS ❑
NO U
tiA
Yes ❑
No _j
NA.d__.
2 1 - Wcr; c]ientrensarkshequnsl�,: (i,c, requested dtluticn3. M&'NISD desip»aticros, ctc,,,)
correcxt • transcribed froui the COCI intrr iii�_ c, mrre; rt section in LIMS?
Yea
Nn
22. Was the quo1f. number usLd taken tirrrn The, corrtahier label?
Ae Frwervatiott (Mml bu co plcted for
inrOrreCtly I)1'eiUNI-0 ur With
F—pl-(s) _ - +4ffmrcccivMl incora+ectly prustTvcd and were adjugrd accordingly in
salnr,ln rdco.iving with (HzSOa, }jNO.,, I1C1, K90H) using SK 6 _
sample(s) +, err. rcucivA wiih bubhles rttru :}b in diameter.
samplcs(s) taON received with TRC !>- 0.5 n;gr7. (if921 isN-u) and were
adfusted >ti ,.n Tingly in sample receiving with sodium rhl&tiul fats: with Shealy IT]:
SC Drcnl irq, Wul rProjeet Sarnple(s)pH YcrMcd to be -� 2 by 17a1u;
Sam IV1 aM V�l N11t rtx.eived at a p1l of =2 and wti,w adiust€d acwoingly ming skPr
Sample 12b[AS applied by — — Date- `F t f, • j
Caaltaawili.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 84 of 84