21045 Woodfin Auto PRI 20180226

PHASE I
ENVIRONMENTAL
SITE ASSESSMENT
of
WOODFIN AUTO & SALVAGE
PROPERTY
1420 & 1430 Riverside Drive
Woodfin, Buncombe County,
North Carolina 28804
Prepared for:
French Broad River Academy
2000 Riverside Drive
Woodfin, North Carolina 28804
February 26, 2018
Project # SEI-858
SIN LETON ENVIRONMENTAL, INC.

TABLE OF CONTENTS
EXECUTIVE SUMMARY
1.0 Introduction
1.1 Purpose
1.2 Scope
1.3 Limitations and Exceptions
1.4 Special Terms and Conditions
1.5 User Reliance
2.0 Site Description
2.1 Location and Legal Description
2.2 Site Description
2.3 Site and General Vicinity Characteristics
2.4 Current Use of the Site
2.5 Current Uses of Adjoining Properties
3.0 User -Provided Information
3.1 Title Records
3.2 Environmental Liens and Activity and Land Use Limitations (AULs)
3.3 Specialized Knowledge
3.4 Commonly Known or Reasonably Ascertainable Information
3.5 Valuation Reduction for Environmental Issues
3.6 Reason for Performing Phase I ESA
4.0 Records Review
4.1 Environmental Records Sources
4.2 State Databases
4.3 Regional and Local Environmental Record Resources
4.4 Vapor Encroachment Screening
4.5 Physical Setting Sources
4.5.1 Historical Aerial Photographs
4.5.2 Historical Topographical Maps
4.5.3 City Directories
4.5.4 Historical Sanborn Fire Insurance Maps
4.6 Facility Environmental Reports and Records
4.7 Historical Use Information for the Subject Site and Adjoining Properties
5.0 Site Reconnaissance
5.1 Methodology and Limiting Conditions
5.2 General Site Setting
5.3 Exterior Observations
5.4 Interior Observations
6.0 Interviews
6.1 Summary of Interview with Site Owner
6.2 Summary of Interview with Local Government Officials
7.0 Findings
8.0 Opinion
9.0 Conclusions
10.0 References
11.0 Signature Page
APPENDICES
Appendix A. 7.5' USGS Topographic Map
Appendix B. Historic Aerials Photographs
Appendix C. Photographs of Site
Appendix D. Site Radius Report
Appendix E. Questionnaires
Appendix F. Limited Phase II ESAs
Appendix G. Resumes of Environmental Professionals
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EXECUTIVE SUMMARY
Singleton Environmental, Inc. (SEI) conducted a Phase I Environmental Site Assessment (ESA) in general
accordance with the American Society for Testing and Materials (ASTM) Practice E1527-13 for the
property located at 1420 and 1430 Riverside Drive in Woodfin, North Carolina. The Subject Site consists
of two parcels located in Buncombe County, North Carolina. According to the Buncombe County
Geographic Information System (GIS), the Subject Site totals approximately 3.23 acres and is identified by
Parcel Identification Numbers (PINS):
• 9730-02-2096 — 2.66 acres — Buncombe County
• 9730-02-1277 — 0.57 acres — Buncombe County
The site is currently listed as mostly vacant commercial land containing one single -wide mobile home and
one partial block structure located in Woodfin, North Carolina. Appendix A illustrates the general location
of the Subject Site on a 7.5' USGS Topographic Map.
A regulatory database search report was provided by GeoSearch, Inc. (GEOSEARCH). The GEOSEARCH
report is discussed in further detail in Section 4.0 of this report. The GEOSEARCH report did identify the
following the Subject Site on the following database lists:
• Brownfields Sites — Current owner entering both parcels into the Brownfields program.
• NCDEQ Leaking Above Ground Storage Tanks List — NCDEQ officials observed hydraulic oil pools
at the Site in 2007 and 2009. Cleanup was requested during both Site visits.
• Resource Conservation & Recovery Act database — No Violations listed.
• EPA Enforcement & Compliance History Information database — No Violations listed.
The purpose of this Phase I ESA was to identify the presence or likely presence of hazardous substances
or petroleum products on the Subject Site under conditions that indicate an existing release, a past
release, or a material threat of a release of hazardous substances or petroleum products into structures
on the Subject Site or into the ground, groundwater, or surface water of the Subject Site as defined in
ASTM Practice E1527-13 as a recognized environmental conditions (RECs), potential/controlled
recognized environmental conditions (PECs), historical recognized environmental conditions (HRECs), and
other notable issues.
Items for consideration that are RECs, PECs, HRECs and notable issues at the site:
• According to aerial photographs, both parcels have been used in the auto salvage industry since
the late 1950s or early 1960s. Oils, solvents and heavy metals related to auto fluids have been
discovered on both parcels during 2017 Limited Phase II Environmental Site Assessments. Both
previous parcel owner's did not respond by phone or email when messages were left. Given the
time gaps associated with both parcels and the limited nature of the previous assessments,
Singleton Environmental recommends further soil and groundwater assessment on both parcels
that will satisfy the Brownfields Program requirements.
1

1.0 INTRODUCTION
This report documents the findings and conclusions of a Phase I Environmental Site Assessment (ESA) of
two commercial properties located at 1420 and 1430 Riverside Drive in Woodfin, North Carolina totaling
approximately 3.23 acres in area and identified as Buncombe County Parcel Identification Number (PIN):
• 9730-02-2096 — 2.66 acres — Buncombe County
• 9730-02-1277 — 0.57 acres — Buncombe County
1.1 Purpose
Singleton Environmental, Inc. conducted a Phase I ESA in general accordance with the American Society
for Testing and Materials (ASTM) Practice E1527-13. The purpose of this Phase I ESA was to identify
recognized environmental conditions (RECs), potential environmental concerns (PECs), historical
recognized environmental conditions (HRECs), and other notable issues in connection with the Subject
Site as defined by ASTM Practice E1527-13.
1.2 Scope
This Phase I ESA included the following principal tasks:
• Review of published information on the physical and environmental setting of the Subject Site
• Review of pertinent state and federal regulatory agency databases and public records
• Review of local and regional sources of public records
• Review of historical aerial photographs, historical city directories, Sanborn Fire Insurance Maps,
and United States Geological Survey (USGS) topographic maps
• A physical review of the Subject Site to observe current conditions and to verify information
obtained from the regulatory databases and historical searches and other historical information.
• Interviews with persons knowledgeable about the history and current condition of the Subject
Site and surrounding properties
• Review of facility environmental records and reports
1.3 Limitations and Exceptions
This Phase I ESA was conducted in general accordance with the guidelines published in the ASTM Standard
previously referenced. Sources of information utilized in the Phase I ESA were reasonably ascertainable
and are not to be considered exhaustive. Sampling and laboratory analyses of materials and
environmental media were not included in the assessment. The assessment was limited to the area
described in Section 1.0 of this report.
Some environmental issues or conditions (such as asbestos, lead -based paint, lead in drinking water, mold,
compliance with environmental regulations, and radon gas) fall outside the scope of a Phase I ESA. The
ASTM Standard states that assessment of such considerations is not required for an appropriate inquiry
as defined by the Standard. However, these conditions can represent potential environmental liabilities.
As defined in ASTM E1527-13, Section 6, "User's Responsibilities", the User of this assessment has specific
obligations to perform tasks during this assessment that will help identify the possibility of RECs and PECs
2

in connection with the Subject Site. Failure by the User to fully comply with the requirements may affect
the User's ability to qualify for Landowner Liability Protections (LLPs) under the Comprehensive
Environmental Response, Compensation, and Liability Act (CERCLA).
The ASTM guidance requires identifying the use of the Site at 5-year intervals back to the first use or 1940,
whichever is earlier. Reasonably ascertainable information reviewed as part of this Phase I ESA dates back
to 1951. However, documentation was not obtained on at least a 5-year interval. This exception
represents a "data gap" as defined in the ASTM standard, Singleton Environmental, Inc. does consider the
identified data gap to be significant.
1.4 Special Terms and Conditions
Due to the limited nature of a Phase I ESA, Singleton Environmental, Inc. can make no statement of
warranty or guarantee, either expressed or implied, that the Subject Site is free from possible latent
sources of environmental liability.
1.5 User Reliance
This Phase I ESA was prepared for the exclusive use of the French Broad River Academy and the North
Carolina Department of Environmental Quality Division of Waste Management Brownfields Program.
3

2.0 Site Description
2.1 Location and Legal Description
Subject Site Address: 1420 and 1430 Riverside Drive in Woodfin, North Carolina.
Current Owner: French Broad River Academy (FBRA).
Land Area: Approximately 3.23 acres.
2.2 Site Description
According to the Property Record Card, the Subject Site contains no permanent structures and covers
approximately 3.23 acres of land located within Buncombe County, North Carolina. A chain link fence
surrounds the majority of both parcels. A single -wide mobile home and a partial block structure are
located on the 1420 Riverside Drive parcel. The Subject Site is currently listed as a commercial.
Appendix A illustrates the general location of the Subject Site. Based on the USGS topographical map, the
Subject Site is located at an elevation averaging 1,950 feet.
Topographically, the land surface slopes to the west-southwest. Storm water runoff from the property
would also flow to the west-southwest.
2.3 Site and General Vicinity Characteristics
The Subject Site is located in a mostly commercial area. Surrounding properties consist of mostly
commercial properties and one residential property to the northeast. The French Broad River is the west -
southwestern border of both parcels.
2.4 Current Use of the Site
Currently, both parcels are vacant with automotive debris covering both parcels.
2.5 Current Uses of Adjoining Properties
Surrounding properties consist of mostly commercial properties with a residential located to the
northeast.
• The property located to the north of the site is an auto repair and tire facility.
• The properties located to the north and northeast are a commercial storage facility and a
residential property located across Riverside Drive.
• The property located to the east is a residential property located across Riverside Drive.
• The property located to the south and southeast are a State of North Carolina owned facility and
a small commercial lot with a small storage shed.
• The property to the west of the site is the French Broad River.
4

3.0 User -Provided Information
3.1 Title Records
Title records were not provided to SEI, nor was SEI contracted to obtain title records associated with the
Subject Site. However, according to the current property deeds, 1420 Riverside Drive was purchased on
December 14, 2017, and 1430 Riverside Drive was purchased on November 17, 2017. Both parcels were
purchased by FBRA. This information was confirmed on the Buncombe County Register of Deeds website.
3.2 Environmental Liens and Activity and Land Use Limitations (AULs)
Mr. Will Yeiser stated there were no AULs.
3.3 Specialized Knowledge
Mr. Yeiser did not have any specialized knowledge of the property or surrounding properties.
3.4 Commonly Known or Reasonably Ascertainable Information
Mr. Yeiser was aware of conditions indicative of environmental releases on the property.
3.5 Valuation Reduction for Environmental Issues
Mr. Yeiser indicated the properties were bought for the fair market price given their current conditions.
3.6 Reason for Performing Phase I ESA
Satisfy a requirement as a part of the NCDEQ Brownfields Agreement.

4.0 Records Review
4.1 Environmental Records Sources
This section summarizes information gathered from electronically updated databases maintained by
federal and state environmental regulatory agencies. GeoSearch, Inc. (GEOSEARCH) completed the
database search at the request of Singleton Environmental, Inc.
Regulatory agencies and GEOSEARCH periodically update their respective databases. The dates of these
updates are shown in the GEOSEARCH report. The minimum search radius for each database is
established in ASTM E1527-13 and is identified in the GEOSEARCH report. For a complete list of the
databases searched by GEOSEARCH for this assessment, see the GEOSEARCH Report in Appendix D.
The Subject Site address was identified in the regulatory records provided by GEOSEARCH.
The following sections summarize the results of the regulatory database reviews conducted by
GEOSEARCH. Only databases which list the Subject Site, adjoining properties (if applicable), or
facilities/properties which based on estimated groundwater flow direction were inferred to be located
upgradient or crossgradient to the Subject Site and within proximity to the Subject Site that could pose a
potential environmental concern for the Subject Site, are summarized.
4.2 State Databases
Underground Storage Tank (UST)
The UST database identifies USTs registered with DENR.
• The Subject Site was not identified on the UST list.
• One UST site is located to the immediate north of the site at the auto repair and tire store.
Leaking Underground Storage Tank (LUST)
The LUST database, maintained by DENR, provides a detailed explanation of current and historic activities
for facilities regarding releases from registered USTs.
• The Subject Site was not identified on the LUST list.
• Two properties were located within the search area. Both properties are located just over
mile to the east and up -river from the site.
Leaking Aboveground Storage Tank (LAST)
The LAST database, maintained by DENR, provides a detailed explanation of current and historic activities
for facilities regarding releases from registered ASTs.
• The Subject Site was identified on the LAST list. The incident was observed by NCDEQ
officials in 2007 and 2009.
0

• There were no off -site LAST sites identified in the database search area.
4.3 Regional and Local Environmental Record Resources
Local and regional sources of information and records were reviewed during the course of this Phase I
ESA. The following publicly available NCDEQ and EPA databases and GEOSEARCH records were reviewed
by Singleton Environmental, Inc. that include the property:
• Brownfields Site Database —The site is currently in the Brownfields application phase.
• RCRA Non -Generator — The Site is listed, however, no violations were listed.
• ECHO R04—The Site was listed, however, no violations were listed.
4.4 Vapor Encroachment Screening
In general accordance with the ASTM E1527-13 standard effective November 1, 2013, Singleton
Environmental, Inc. prepared a vapor encroachment screen. The vapor encroachment screen was
prepared in general accordance with the Tier 1 screening procedures described in ASTM E2600-10. The
purpose of the screen is to identify potential vapor encroachment conditions (VECs). ASTM defines a VEC
as "the presence or likely presence of COC [chemicals of concern] vapors in the subsurface of the Target
Property [the Subject Site] caused by the release of vapors from contaminated soil and/or groundwater
either on or near the target property [Subject Site]."
This vapor encroachment screening was conducted by identifying an Area of Concern (AOC). The default
AOC is set at one third of a mile (1,760 feet) from the Subject Site to any suspected sources of hazardous,
volatile contamination, and one tenth of a mile (528 feet) from the Subject Site to any petroleum
hydrocarbon contamination. The default AOC is based upon a statistical analysis conducted by ASTM of
typical contaminant plume lengths. The AOC can be reduced based on additional characteristics, including
but not limited to known or inferred groundwater flow direction away from the Subject Site, the presence
of relatively impermeable soil beneath the Subject Site, the presence of a relatively deep water table
beneath the Subject Site, and natural hydrogeologic barriers between a suspected source and the Subject
Site (e.g. a river, stream, or wetland).
Singleton Environmental, Inc. used the GEOSEARCH elevation data to prepare the screen. Singleton
Environmental, Inc. identified the Subject Site on a map prepared by GEOSEARCH. GEOSEARCH identified
the default AOC and an inferred groundwater flow direction beneath the Subject Site and Singleton
Environmental, Inc. confirmed the default AOC and inferred groundwater flow direction. Additionally,
GEOSEARCH identified on the map the locations listed in publicly available regulatory databases of
suspected sources of hazardous, volatile contamination and petroleum contamination.
The vapor encroachment screening results indicated there is the potential for VECs at the subject site if a
barrier is not installed prior to building construction.
7

4.5 Physical Setting Sources
4.5.1 Historical Aerial Photographs
Historical aerial photographs, provided by GEOSEARCH, were reviewed by Singleton Environmental, Inc.
Aerial photographs were reviewed to help identify historical land uses that may have resulted in
environmental impacts on, or adjacent to, the Subject Site. A time series of aerial photographs spanning
67 years was reviewed.
The photographs, which were taken in 1951, 1964, 1975, 1984, 1988, 1994, 1998, 2005, 2006, 2008, 2009,
2010, 2011, 2012, 2014 and 2016 were produced at various scales. The Subject Site and vicinity can be
identified in the photographs from 1951 to 2016. Prior to 1964 the Site appeared to be undeveloped.
Copies of the aerial photographs are included as Appendix B.
4.5.2 Historical Topographical Maps
A topographical map from 2013 shows the property. A copy of the topographical map is included in
Appendix A.
4.5.3 City Directories
A city directory report was provided by GEOSEARCH, 1430 Riverside Drive was listed back to 2002. The
Site was listed in 2002 as Western Carolina Recycling, in 2005 as Woodfin Auto & Salvage, and in 2011 as
being owned by Connie Ledford. 1420 Riverside Drive was not listed in the City Directory.
4.5.4 Historical Sanborn Fire Insurance Maps
A Sanborn Fire Insurance map report could not be provided by GEOSEARCH since no Sandborn Insurance
Maps are available for the property.
4.6 Facility Environmental Reports and Records
In June and July 2017, Singleton Environmental, Inc. submitted two Limited Phase II Environmental Site
Assessments (ESAs) where soil samples were collected at 1420 Riverside Drive and soil and groundwater
samples were collected at 1430 Riverside Drive. Elevated automotive compounds were detected in the
soils and groundwater at the Site. Copies of both reports are located in Appendix F.
4.7 Historical Use Information for the Subject Site and Adjoining Properties
Based on historical data described in the sections above and in the remainder of this report, Singleton
Environmental, Inc. was able to trace the historical uses of the area around the Subject Site back to 1951.
According to aerial photographs, the Subject Site and neighboring properties have historically been
commercial and residential properties or undeveloped land.
N

5.0 Site Reconnaissance
5.1 Methodology and Limiting Conditions
SEI conducted a visual reconnaissance of the Subject Site at various times between June 2017 and
February 23, 2018. The purpose of the Site reconnaissance was to determine if there were obvious visual
indications of present or past activities that may have contributed to RECs, PECs, HRECs or notable issues
at the Subject Site. Representative areas of the Subject Site were observed in general accordance with
ASTM guidelines. Exterior portions of subject property as well as neighboring properties were observed
from accessible areas of the Property.
During the Site visit, photographs were taken to document the observed conditions (Appendix Q.
Representative views of the Site are shown in the photographs. The photographs also provide a general
overview of current Site conditions and settings. In addition to information presented elsewhere in this
report, the following sections describe pertinent information that was observed during the Site
reconnaissance.
5.2 General Site Setting
The Subject Site consists of two parcels totaling approximately 3.23 acres located at 1420 and 1430
Riverside Drive in Woodfin, North Carolina. The general Site vicinity is primarily commercial with minor
residential properties located to the east.
5.3 Exterior Observations
The following items were observed during the Site reconnaissance:
• A singlewide mobile home and a partially demolished block structure are located on 1420
Riverside Drive.
• Various mounds of rock and concrete were observed on the parcels.
• Various auto parts were observed littering both parcels.
• Oil/chemical stained soils were observed on both parcels
• No water supply wells or septic systems were observed on the property, however, a septic tank is
suspected due to the mobile home and partially demolished building on 1420 Riverside Drive.
• No evidence underground storage tanks (USTs) were observed on the property, however, the fill
and vent pipes could have been covered up or cut off.
• Municipal water supply is available at the Site.
• A MSD Sewer main line runs through the western portion of both parcels near the French Broad
River.
• A chain link fence surrounds most of the two parcels.
5.4 Interior Observations
• The interior of the mobile home was not entered.
E

6.0 Interviews
6.1 Summary of Interviews.
Between June 2017 and February 2018, SEI interviewed Mr. Will Yeiser with FBRA, he communicated the
following details to SEI:
• The properties were used in the auto recycling and crushing industry for years.
• FBRA is considering building a charter school on the parcels.
• A MSD Sewer main line is on both parcels.
On February 26, 2018, The Town of Woodfin, MSD and the Buncombe County Health Department were
contacted. they communicated the following details to SEI:
• MSD did not have either addresses listed in their system, however, a sewer hookup is
shown on MSD maps on the property across the railroad tracks from the mobile home.
• The Town of Woodfin stated that 1430 Riverside Drive was being charged a sewer fee
with the water bill, but they had no information on 1420 Riverside Drive.
• Buncombe County Health Department could not find a septic permit on file for either
parcels.
6.2 Summary of Interview with Local Government Officials
In June 2017, Jan Andersen with NCDEQ was interviewed by phone, she stated the following:
• The Site was listed on the NCDEQ database as having a LAST incident. Requests were made in
2007 and in 2009 to cleanup soil contamination.
10

7.0 Findings
Singleton Environmental, Inc. did identify the following items for consideration that are RECs, PECs HRECs,
or notable issues at the sites:
• According to aerial photographs, both parcels have been used in the auto salvage industry since
the late 1950s or early 1960s. Oils, solvents and heavy metals related to auto fluids have been
discovered on both parcels during 2017 Limited Phase II Environmental Site Assessments. Both
previous parcel owner's did not respond by phone or email when messages were left.
11

8.0 Opinion
This Phase I ESA did identify possible RECs associated with the Subject Site.
Conclusions and Recommendations: This Phase I ESA identified the following on -Site RECs.
• According to aerial photographs, both parcels have been used in the auto salvage industry since
the late 1950s or early 1960s. Oils, solvents and heavy metals related to auto fluids have been
discovered on both parcels during 2017 Limited Phase II Environmental Site Assessments. Both
previous parcel owner's did not respond by phone or email when messages were left. Given the
time gaps associated with both parcels and the limited nature of the previous assessments,
Singleton Environmental recommends further soil and groundwater assessment on both parcels
that will satisfy the Brownfields Program requirements.
12

9.0 Conclusions
The ASTM standard for Phase I environmental site assessments uses the following definition of a REC:
"recognized environmental conditions" - the presence of any hazardous substances or petroleum
products on a property under conditions that indicate an existing release, a past release, or a material
threat of a release of any hazardous substances or petroleum products into structures on the property or
into the ground, ground water, or surface water of the property. The term includes hazardous substances
or petroleum products even under conditions in compliance with laws. The term is not intended to include
de minimis conditions that generally do not present a threat to human health or the environment and
that generally would not be the subject of an enforcement action if brought to the attention of
appropriate governmental agencies. Conditions determined to be de minimis are not recognized
environmental conditions."
Singleton Environmental, Inc. has performed a Phase I Environmental Site Assessment in conformance
with the scope and limitations of ASTM Practice E1527 of the Subject Site (1420 and 1430 Riverside Drive)
consisting of approximately 3.23 acres. Singleton Environmental recommends further soil and
groundwater assessment on both parcels that will satisfy the Brownfields Program requirements.
13

10.0 References
American Society for Testing and Materials (ASTM) Standard E1527-13.
• Standard Practice for Environmental Site Assessments: Phase I Environmental Site
Assessment Process. ASTM International, West Conshohocken, Pennsylvania, 2013.
GeoSearch: 1420 and 1430 Riverside Drive, Woodfin, Buncombe County, North Carolina.
GeoSearch Aerial Photographs: 1951, 1964, 1975, 1984, 1988, 1994, 1998, 2005, 2006, 2008, 2009, 2010,
2011, 2012, 2014 and 2016.
Buncombe County Register of Deeds & Geographic Information System.
North Carolina Department of Environmental Quality
United States Geological Survey, 7.5-Minute Series Map of Weaverville 2013:
Geologic Map of North Carolina, 1985.
14

1 1 .0 SIGNATURE AND QUALIFICATIONS OF THE ENVIRONMENTAL
PROFESSIONAL
The undersigned hereby declare that, to the best of our professional knowledge and belief, we meet the
definition of Environmental Professional as defined in §312.10 of 40 CFR 312, and we have the specific
qualifications based on education, training, and experience to assess a property of nature, history, and
setting of the subject property. We have developed and performed the all appropriate inquiries in
conformance with the standards and practices set forth in 40 CFR Part 312 as outlined by the ASTM
Practice E 1527-2013 standards.
Submitted by:
Christopher D. Sing%Y,ok`sional Geologist NC1928
1inb

APPENDIX A
7.5' USGS Topographic Map

Topographic Map
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Quadrangle(s): Weaverville
Source: USGS, 0610712013
Woodfin Auto & Salvage
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Brownfields Property
1430 Riverside Dr
s
Woodfin, North Carolina
28804
0' 1000, 2000' 3000'
SCALE: V - 2000'
Click here to access Satellite view
Geoearch www.geo-search.comsearch.com 888-396-0042
Order# 101912 Job# 223229 13 of 51

APPENDIX B
Aerial Photographs

GegpSearch
On time. On target. In touch"'
Historical Aerials Package
Target Property:
Woodfin Auto & Salvage Brownfields Property
1430 Riverside Dr
Woodfin, Buncombe, North Carolina 28804
Prepared For. -
Singleton Environmental Inc.
Order #: 101912
Job #: 223232
Project #: SEI-858
Date: 211912018
GeQSearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223232

Target Property Summary
Woodfin Auto & Salvage Brownfields Property
1430 Riverside Dr
Woodfin, Buncombe, North Carolina 28804
USGS Quadrangle: Weaverville
Target Property Geometry: Point
Target Property Longitude(s)/Latitude(s):
(-82.600533542, 35.626103702)
GeQSearch www..geo-search.com 888-396-0042
Order# 101912 Job# 223232

Aerial Research Summary
Date
Source
Scale
Frame
2016
USDA
1 " = 500'
N/A
2014
USDA
1 " = 500'
N/A
2012
USDA
1 " = 500'
N/A
2010
USDA
1 " = 500'
N/A
2009
USDA
1 " = 500'
N/A
2008
USDA
1 " = 500'
N/A
2006
USDA
1 " = 500'
N/A
2005
USDA
1 " = 500'
N/A
03/15/1998
USGS
1 " = 500'
N/A
03/22/1994
USGS
1 " = 500'
N/A
05/27/1988
USGS
1 " = 1000'
85-41
0412611984
USGS
1 " = 500'
191-65
0410111975
ASCS
1 " = 1000'
PI-2
1011311964
USAF
1 " = 500'
92-9011
05/09/1951
ASCS
1 " = 500'
3-15
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liable for actual, incidental, consequential, special or exemplary damages suffered by a customer resulting directly or indirectly from any
information provided by GeoSearch.
GeQSearch www..geo-search.com 888-396-0042
Order# 101912 Job# 223232

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JOB #: 223232 - 02/ 19/2018

APPENDIX C
Site Photographs

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APPENDIX D
Environmental Radius Report

GepSearch
On time. On target. In touch'"
Radius Report
Satellite view
Target Property.
Woodfin Auto & Salvage Brownfields Property
1430 Riverside Dr
Woodfin, Buncombe County, North Carolina 28804
Prepared For:
Singleton Environmental Inc.
Order #: 101912
Job #: 223229
Project #: SEI-858
Date: 0211912018
GeQSearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223229

Table of Contents
Target Property Summary . . . . . . . . . . . .
. . . . . . . . . . . . . 1
Database Summary . . . . . . . . . . . . . .
. . . . . . . . . . . . . 2
Database Radius Summary . . . . . . . . . . .
. . . . . . . . . . . . . 6
Radius Map . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . 10
Ortho Map . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . 12
Topographic Map . . . . . . . . . . . . . . .
. . . . . . . . . . . . . 13
Located Sites Summary . . . . . . . . . . . .
. . . . . . . . . . . . . 13
Elevation Summary . . . . . . . . . . . . . .
. . . . . . . . . . . . . 16
Unlocated Sites Summary . . . . . . . . . . .
. . . . . . . . . . . . . 34
Environmental Records Definitions . . . . . . . .
. . . . . . . . . . . . . 36
Unlocatable Report . . . . . . . . . . . . .
. . . . . . . . See Attachment
Zip Report . . . . . . . . . . . . . . . . .
. . . . . . . . See Attachment
Geoearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223229

Disclaimer
This report was designed by GeoSearch to meet or exceed the records search requirements of the All Appropriate Inquiries Rule (40 CFR
§312.26) and the current version of the ASTM International E1527, Standard Practice for Environmental Site Assessments: Phase 1
Environmental Site Assessment Process or, if applicable, the custom requirements requested by the entity that ordered this report. The
records and databases of records used to compile this report were collected from various federal,state and local governmental entities. It is
the goal of GeoSearch to meet or exceed the 40 CFR §312.26 and E1527 requirements for updating records by using the best available
technology. GeoSearch contacts the appropriate governmental entities on a recurring basis. Depending on the frequency with which a
record source or database of records is updated by the governmental entity, the data used to prepare this report may be updated monthly,
quarterly, semi-annually, or annually.
The information provided in this report was obtained from a variety of public sources. GeoSearch cannot ensure and makes no
warranty or representation as to the accuracy, reliability, quality, errors occurring from data conversion or the customer's interpretation of
this report. This report was made by GeoSearch for exclusive use by its clients only. Therefore, this report may not contain sufficient
information for other purposes or parties. GeoSearch and its partners, employees, officers And independent contractors cannot be held
liable For actual, incidental, consequential, special or exemplary damages suffered by a customer resulting directly or indirectly from any
information provided by GeoSearch.
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Order# 101912 Job# 223229

Target Property Summary
Target Property Information
Woodfin Auto & Salvage Brownfields Property
1430 Riverside Dr
Woodfin, North carolina 28804
Coordinates
Point (-82.600533, 35.626103)
1,950 feet above sea level
USGS Quadrangle
Weaverville, NC
Geographic Coverage Information
County/Parish: Buncombe (NC)
ZipCode(s):
Asheville NC: 28804, 28806
Radon
* Target property is located in Radon Zone 1.
Zone 1 areas have a predicted average indoor radon screening level greater than 4 pCi/L
(picocuries per liter).
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Order# 101912 Job# 223229 1 of 51

Database Summary
FEDERAL LISTING
Standard Environmental Records
Database
Acronym
Locatable
Unlocatable
Search
Radius
(miles)
EMERGENCY RESPONSE NOTIFICATION SYSTEM
ERNSNC
0
0
TP/AP
FEDERAL ENGINEERING INSTITUTIONAL CONTROL SITES
EC
0
0
TP/AP
LAND USE CONTROL INFORMATION SYSTEM
LUCIS
0
0
TP/AP
RCRA SITES WITH CONTROLS
RCRASC
0
0
TP/AP
RESOURCE CONSERVATION & RECOVERYACT- GENERATOR
RCRAGR04
0
0
0.1250
RESOURCE CONSERVATION & RECOVERYACT- NON-
RCRANGR04
2
1
0.1250
GENERATOR
FEMA OWNED STORAGE TANKS
FEMAUST
0
0
0.2500
BROWNFIELDS MANAGEMENT SYSTEM
BF
0
0
0.5000
DELISTED NATIONAL PRIORITIES LIST
DNPL
0
0
0.5000
NO LONGER REGULATED RCRA NON-CORRACTS TSD FACILITIES
NLRRCRAT
0
0
0.5000
RESOURCE CONSERVATION & RECOVERYACT- NON-CORRACTS
RCRAT
0
0
0.5000
TREATMENT, STORAGE & DISPOSAL FACILITIES
SUPERFUND ENTERPRISE MANAGEMENT SYSTEM
SEMS
0
0
0.5000
SUPERFUND ENTERPRISE MANAGEMENT SYSTEM ARCHIVED
SEMSARCH
0
0
0.5000
SITE INVENTORY
NATIONAL PRIORITIES LIST
NPL
0
0
1.0000
NO LONGER REGULATED RCRA CORRECTIVE ACTION FACILITIES
NLRRCRAC
0
0
1.0000
PROPOSED NATIONAL PRIORITIES LIST
PNPL
0
0
1.0000
RESOURCE CONSERVATION & RECOVERYACT - CORRECTIVE
RCRAC
0
0
1.0000
ACTION FACILITIES
RESOURCE CONSERVATION & RECOVERYACT - SUBJECT TO
RCRASUBC
0
0
1.0000
CORRECTIVE ACTION FACILITIES
SUB -TOTAL 1 1 2 1 1
Additional Environmental Records
Database
Acronym
Locatable
Unlocatable
Search
Radius
(miles)
AEROMETRIC INFORMATION RETRIEVAL SYSTEM/AIR FACILITY
AIRSAFS
0
0
TP/AP
SUBSYSTEM
BIENNIAL REPORTING SYSTEM
BRS
0
0
TP/AP
CERCLIS LIENS
SFLIENS
0
0
TP/AP
CLANDESTINE DRUG LABORATORY LOCATIONS
CDL
0
0
TP/AP
EPA DOCKET DATA
DOCKETS
0
0
TP/AP
ENFORCEMENT AND COMPLIANCE HISTORY INFORMATION
ECHOR04
1
0
TP/AP
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Order# 101912 Job# 223229 2 of 51

Database Summary
Database
Acronym
Locatable
Unlocatable
Search
Radius
(miles)
FACILITY REGISTRY SYSTEM
FRSNC
1
0
TP/AP
HAZARDOUS MATERIALS INCIDENT REPORTING SYSTEM
HMIRSR04
0
0
TP/AP
INTEGRATED COMPLIANCE INFORMATION SYSTEM (FORMERLY
/CIS
0
0
TP/AP
DOCKETS)
INTEGRATED COMPLIANCE INFORMATION SYSTEM NATIONAL
ICISNPDES
0
0
TP/AP
POLLUTANT DISCHARGE ELIMINATION SYSTEM
MATERIAL LICENSING TRACKING SYSTEM
MLTS
0
0
TP/AP
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
NPDESR04
0
0
TP/AP
PCB ACTIVITY DATABASE SYSTEM
PADS
0
0
TP/AP
PERMIT COMPLIANCE SYSTEM
PCSR04
0
0
TP/AP
SEMS LIEN ON PROPERTY
SEMSLIENS
0
0
TP/AP
SECTION SEVEN TRACKING SYSTEM
SSTS
0
0
TP/AP
TOXIC SUBSTANCE CONTROL ACT INVENTORY
TSCA
0
0
TP/AP
TOXICS RELEASE INVENTORY
TRI
0
0
TP/AP
ALTERNATIVE FUELING STATIONS
ALTFUELS
0
0
0.2500
HISTORICAL GAS STATIONS
HISTPST
0
0
0.2500
INTEGRATED COMPLIANCE INFORMATION SYSTEM
ICISCLEANERS
0
0
0.2500
DRYCLEANERS
MINE SAFETYAND HEALTH ADMINISTRATION MASTER INDEX FILE
MSHA
0
0
0.2500
MINERAL RESOURCE DATA SYSTEM
MRDS
0
0
0.2500
OPEN DUMP INVENTORY
ODI
0
0
0.5000
SURFACE MINING CONTROL AND RECLAMATION ACT SITES
SMCRA
0
0
0.5000
URANIUM MILL TAILINGS RADIATION CONTROL ACT SITES
USUMTRCA
0
0
0.5000
DEPARTMENT OF DEFENSE SITES
DOD
0
0
1.0000
FORMER MILITARY NIKE MISSILE SITES
NMS
0
0
1.0000
FORMERLY USED DEFENSE SITES
FUDS
0
0
1.0000
FORMERLY UTILIZED SITES REMEDIAL ACTION PROGRAM
FUSRAP
0
0
1.0000
RECORD OF DECISION SYSTEM
RODS
0
0
1.0000
SUB -TOTAL 1 1 2 1 0
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Order# 101912 Job# 223229 3 of 51

Database Summary
STATE (NCB LISTING
Standard Environmental Records
Database
Acronym
Locatable
Unlocatable
Search
Radius
(miles)
LAND USE RESTRICTED SITES
LUR
0
0
TP/AP
UNDERGROUND STORAGE TANKS
UST
1
3
0.2500
BROWNFIELD PROJECTS
BF
1
0
0.5000
HISTORIC LANDFILLS
HISTLF
0
0
0.5000
LEAKING ABOVEGROUND STORAGE TANKS
LAST
1
0
0.5000
LEAKING UNDERGROUND STORAGE TANKS
LUST
2
0
0.5000
SOLID WASTE FACILITIES
SWF
0
1
0.5000
STATE TRUST FUNDS DATABASE
LUSTFUND
1
1
0.5000
VOLUNTARY ACTION PROGRAM SITES
VAP
0
0
0.5000
HAZARDOUS SUBSTANCE DISPOSAL SITES
HSDS
0
0
1.0000
INACTIVE HAZARDOUS SITES
IHS
0
0
1.0000
SUB -TOTAL 1 1 6 1 5
Additional Environmental Records
Database
Acronym
Locatable
Unlocatable
Search
Radius
(miles)
AIR PERMITTED FACILITIES
AIRS
0
0
TP/AP
ANIMAL FEEDING OPERATION PERMITS
AFO
0
0
TP/AP
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
NPDES
0
0
TP/AP
PERMITS
SPILLS LISTING
SPILLS
0
0
TP/AP
UNDERGROUND INJECTION CONTROL WELLS
UIC
0
0
TP/AP
DRY-CLEANING SOLVENT CLEANUP ACT PROGRAM SITES
DSCASITES
0
0
0.5000
SUB -TOTAL 0 0
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Order# 101912 Job# 223229 4 of 51

Database Summary
TRIBAL LISTING
Standard Environmental Records
Search
Radius
Database
Acronym
Locatable
Unlocatable
(miles)
UNDERGROUND STORAGE TANKS ON TRIBAL LANDS
USTR04
0
0
0.2500
LEAKING UNDERGROUND STORAGE TANKS ON TRIBAL LANDS
LUSTR04
0
0
0.5000
OPEN DUMP INVENTORY ON TRIBAL LANDS
ODINDIAN
0
0
1 0.5000
SUB -TOTAL 0 0
Additional Environmental Records
Search
Radius
Database
Acronym
Locatable
Unlocatable
(miles)
INDIAN RESERVATIONS
INDIANRES
0
0
1.0000
SUB -TOTAL I0 0
TOTAL 10 1 6
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Order# 101912 Job# 223229 5 of 51

Database Radius Summary
FEDERAL LISTING
Standard environmental records are displayed in bold.
Acronym
Search
Radius
(miles)
TP/AP
(0 - 0.02)
118 Mile
(> TP/AP)
114 Mile
(> 118)
112 Mile
(> 114)
1 Mile
(> 112)
> 1 Mile
Total
AIRSAFS
0.0200
0
NS
NS
NS
NS
NS
0
BRS
0.0200
0
NS
NS
NS
NS
NS
0
CDL
0.0200
0
NS
NS
NS
NS
NS
0
DOCKETS
0.0200
0
NS
NS
NS
NS
NS
0
EC
0.0200
0
NS
NS
NS
NS
NS
0
ECHOR04
0.0200
1
NS
NS
NS
NS
NS
1
ERNSNC
0.0200
0
NS
NS
NS
NS
NS
0
FRSNC
0.0200
1
NS
NS
NS
NS
NS
1
HMIRSR04
0.0200
0
NS
NS
NS
NS
NS
0
ICIS
0.0200
0
NS
NS
NS
NS
NS
0
ICISNPDES
0.0200
0
NS
NS
NS
NS
NS
0
LUCIS
0.0200
0
NS
NS
NS
NS
NS
0
MLTS
0.0200
0
NS
NS
NS
NS
NS
0
NPDESR04
0.0200
0
NS
NS
NS
NS
NS
0
PADS
0.0200
0
NS
NS
NS
NS
NS
0
PCSR04
0.0200
0
NS
NS
NS
NS
NS
0
RCRASC
0.0200
0
NS
NS
NS
NS
NS
0
SEMSLIENS
0.0200
0
NS
NS
NS
NS
NS
0
SFLIENS
0.0200
0
NS
NS
NS
NS
NS
0
SSTS
0.0200
0
NS
NS
NS
NS
NS
0
TRI
0.0200
0
NS
NS
NS
NS
NS
0
TSCA
0.0200
0
NS
NS
NS
NS
NS
0
RCRAGR04
0.1250
0
0
NS
NS
NS
NS
0
RCRANGR04
0.1250
1
1
NS
NS
NS
NS
2
ALTFUELS
0.2500
0
0
0
NS
NS
NS
0
FEMAUST
0.2500
0
0
0
NS
NS
NS
0
HISTPST
0.2500
0
0
0
NS
NS
NS
0
ICISCLEANERS
0.2500
0
0
0
NS
NS
NS
0
MRDS
0.2500
0
0
0
NS
NS
NS
0
MSHA
0.2500
0
0
0
NS
NS
NS
0
BF
0.5000
0
0
0
0
NS
NS
0
DNPL
0.5000
0
0
0
0
NS
NS
0
NLRRCRAT
0.5000
0
0
0
0
NS
NS
0
ODI
0.5000
0
0
0
0
NS
NS
0
RCRAT
0.5000
0
0
0
0
NS
NS
0
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Order# 101912 Job# 223229 6 of 51

Database Radius Summary
Acronym
Search
Radius
(miles)
TP/AP
(0 - 0.02)
1/8 Mile
(> TP/AP)
1/4 Mile
(> 118)
112 Mile
(> 114)
1 Mile
(> 112)
> 1 Mile
Total
SEMS
0.5000
0
0
0
0
NS
NS
0
SEMSARCH
0.5000
0
0
0
0
NS
NS
0
SMCRA
0.5000
0
0
0
0
NS
NS
0
USUMTRCA
0.5000
0
0
0
0
NS
NS
0
DOD
1.0000
0
0
0
0
0
NS
0
FUDS
1.0000
0
0
0
0
0
NS
0
FUSRAP
1.0000
0
0
0
0
0
NS
0
NLRRCRAC
1.0000
0
0
0
0
0
NS
0
NMS
1.0000
0
0
0
0
0
NS
0
NPL
1.0000
0
0
0
0
0
NS
0
PNPL
1.0000
0
0
0
0
0
NS
0
RCRAC
1.0000
0
0
0
0
0
NS
0
RCRASUBC
1.0000
0
0
0
0
0
NS
0
RODS
1.0000
0
0
0
0
0
NS
0
SUB -TOTAL 1 1 3 1 1 1 0 1 0 1 0 1 0 1 4
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Order# 101912 Job# 223229 7 of 51

Database Radius Summary
STATE (NCB LISTING
Standard environmental records are displayed in bold.
Acronym
Search
Radius
(miles)
TP/AP
(0 - 0.02)
118 Mile
(> TP/AP)
114 Mile
(> 1/8)
112 Mile
(> 1/4)
1 Mile
(> 112)
> 1 Mile
Total
AFO
0.0200
0
NS
NS
NS
NS
NS
0
AIRS
0.0200
0
NS
NS
NS
NS
NS
0
LUR
0.0200
0
NS
NS
NS
NS
NS
0
NPDES
0.0200
0
NS
NS
NS
NS
NS
0
SPILLS
0.0200
0
NS
NS
NS
NS
NS
0
UIC
0.0200
0
NS
NS
NS
NS
NS
0
UST
0.2500
0
0
1
NS
NS
NS
1
BF
0.5000
1
0
0
0
NS
NS
1
DSCASITES
0.5000
0
0
0
0
NS
NS
0
HISTLF
0.5000
0
0
0
0
NS
NS
0
LAST
0.5000
1
0
0
0
NS
NS
1
LUST
0.5000
0
0
0
2
NS
NS
2
LUSTFUND
0.5000
0
0
0
1
NS
NS
1
SWF
0.5000
0
0
0
0
NS
NS
0
VA
0.5000
0
0
0
0
NS
NS
0
HSDS
1.0000
0
0
0
0
0
NS
0
IHS
1.0000
0
0
0
0
0
NS
0
SUB -TOTAL 1 1 2 1 0 1 1 1 3 1 0 1 0 1 6
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Order# 101912 Job# 223229 8 of 51

Database Radius Summary
TRIBAL LISTING
Standard environmental records are displayed in bold.
Acronym
Search
TP/AP
118 Mile
114 Mile
112 Mile
1 Mile
Total
Radius
(0 - 0.02)
(> TP/AP)
(> 1/8)
(> 1/4)
(> 112)
> 1 Mile
(miles)
USTR04
0.2500
0
0
0
NS
NS
NS
0
LUSTR04
0.5000
0
0
0
0
NS
NS
0
ODINDIAN
0.5000
0
0
0
0
NS
NS
0
INDIANRES
1.0000
0
0
0
0
0
NS
0
TOTAL 1 1 5 1 1 1 1 1 3 1 0 1 0 1 10
NOTES:
NS = NOT SEARCHED
TP/AP = TARGET PROPERTY/ADJACENT PROPERTY
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Order# 101912 Job# 223229 9 of 51

Radius Map 1
® Target Property (TP) Woodfin Auto & Salvage
❑ RGRANGR04 Brownfields Property N
Q UST 1430 Riverside Dr w�QAE
LUST Woodfin, North Carolina ���III
28804 s
0' 1000, 2000' 3000'
SCALE: 1"T 2000'
Click here to access Satellite view
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Order# 101912 Job# 223229 10 of 51

® Target Property (TP) Woodfin Auto & Salvage
❑ RGRANGR04 Brownfields Property N
Q UST 1430 Riverside Dr w�QAE
LUST Woodfin, North Carolina ���III
28804 s
0' 500, 1000, 1500'
SCALE: 1"T 1000'
Click here to access Satellite view
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Order# 101912 Job# 223229 11 of 51

* Target Property (TP) Quadrangle(s): Weaverville
❑ RCRANGR04 Woodfin Auto & Salvage N
Q UST Brownfields Property w E
LUST 1430 Riverside Dr
Woodfin, North Carolina s
28804
0' 500' 1000' 1500'
SCALE: V - 1000'
Click here to access Satellite view
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Order# 101912 Job# 223229 12 of 51

Topographic Map
, ; Q 6EAVERDnM CRfflf Rtr
YMile 0 Bair
Cav
4t .� roo / z ik
fFrC rF�Q
1/2N16al? odfn
Craggyfffc;
- ---Rhodes Cem sr� i Y4 MY.
w' 0 \ po r x
L v y � � r..J 4
1/8 Mik _ ill 70
So 0M
�GIR''
6 1.
Buniombe
County Horne
a,P ✓ r/ r l
r
z
-
f �IJV.
f
'} k�
..?.ilxl
.�• %
VAJ7Ji RD Fore Cem r
.
chmand
hilt
Dryman
Mountain
RD
m
ma`s .' Bingham
a
WIL54N 4Dy�
�a Heights p
1
--
� 2300
6RIOGE RD
h4
-2
* Target Property (TP)
Quadrangle(s): Weaverville
Source: USGS, 0610712013
Woodfin Auto & Salvage
N
w E
Brownfields Property
1430 Riverside Dr
s
Woodfin, North Carolina
28804
0' 1000, 2000' 3000'
SCALE: V - 2000'
Click here to access Satellite view
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Order# 101912 Job# 223229 13 of 51

Located Sites Summary
NOTE: Standard environmental records are displayed in bold.
Map Database Site ID# Relative Distance Site Name Address PAGE
ID# Name Elevation From Site #
1 BF
21045-17-11
Equal
TP
WOODFIN AUTO &
1420 & 1430 RIVERSIDE DRIVE,
16
(1,950 ft.)
SALVAGE
ASHEVILLE, NC
1 ECHOR04
110039582555
Equal
TP
WOODFIN AUTO &
1430 RIVERSIDE DR, ASHEVILLE,
17
(1,950 ft.)
SALVAGE INC
NC 28801
1 FRSNC
110039582555
Equal
TP
WOODFIN AUTO &
1430 RIVERSIDE DR, ASHEVILLE,
18
(1,950 ft.)
SALVAGE INC
NC 28801
1 LAST
AS-88068
Equal
TP
WOODFIN AUTO
1430 RIVERSIDE DRIVE,
19
(1,950 ft.)
SALVAGE
ASHEVILLE, NC 20084
1 RCRANGR04
NCS000001447
Equal
TP
WOODFIN AUTO &
1430 RIVERSIDE DR, ASHEVILLE,
22
(1,950 ft.)
SALVAGE INC
NC 28801
2 RCRANGR04
NCS000001395
Equal
0.068 mi. NW
CRAGGY MOTORS
1444 RIVERSIDE DR, ACHEVILLE,
24
(1,950 ft.)
(359 ft.)
NC 28804
3 UST
00-0-
Higher
0.135 mi. N
WALDROPS
RIVERSIDE DR AT CRAGG,
26
0000007884
(1,968 ft.)
(713 ft.)
GROCERY
ASHEVILLE, NC 28804
4 LUST
AS-365
Higher
0.27 mi. E
CRAGGY PRISON
HWY 251-N, ASHEVILLE, NC 28814
28
(2,062 ft.)
(1426 ft.)
LAUNDRY
4 LUSTFUND
5741
Higher
0.27 mi. E
CRAGGY PRISON
HWY 251, RIVERSIDE D,
32
(2,062 ft.)
(1426 ft.)
LAUNDRY
ASHEVILLE, NC
5 LUST
AS-1026
Lower
0.277 mi.
NCDOT MAINT.
CRAGGY ROAD, ASHEVILLE, NC
33
(1,949 ft.)
ESE
YARD-ASHEVILLE
28804
(1463 ft.)
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Order# 101912 Job# 223229 14 of 51

Elevation Summary
Elevations are collected from the USGS 3D Elevation Program 113 arc -second (approximately 10 meters) layer hosted at the NGTOC
Target Property Elevation: 1950 ft.
NOTE: Standard environmental records are displayed in bold.
EQUAL/HIGHER ELEVATION
Map
Database Name
Elevation
Site Name
Address
Page
ID#
#
1
BF
1,950 ft.
WOODFIN AUTO & SALVAGE
1420 & 1430 RIVERSIDE DRIVE,
16
ASHEVILLE, NC
1
ECHOR04
1,950 ft.
WOODFIN AUTO & SALVAGE INC
1430 RIVERSIDE DR, ASHEVILLE, NC
17
28801
1
FRSNC
1,950 ft.
WOODFIN AUTO & SALVAGE INC
1430 RIVERSIDE DR, ASHEVILLE, NC
18
28801
1
LAST
1,950 ft.
WOODFIN AUTO SALVAGE
1430 RIVERSIDE DRIVE, ASHEVILLE,
19
NC 20084
1
RCRANGR04
1,950 ft.
WOODFIN AUTO & SALVAGE INC
1430 RIVERSIDE DR, ASHEVILLE, NC
22
28801
2
RCRANGR04
1,950 ft.
CRAGGY MOTORS
1444 RIVERSIDE DR, ACHEVILLE, NC
24
28804
3
UST
1,968 ft.
WALDROPS GROCERY
RIVERSIDE DR AT CRAGG,
26
ASHEVILLE, NC 28804
4
LUST
2,062 ft.
CRAGGY PRISON LAUNDRY
HWY 251-N, ASHEVILLE, NC 28814
28
4
LUSTFUND
2,062 ft.
CRAGGY PRISON LAUNDRY
HWY 251, RIVERSIDE D, ASHEVILLE,
32
NC
LOWER ELEVATION
Map
Database Name
Elevation
Site Name
Address
Page
I D#
#
5
LUST
1,949 ft.
NCDOT MAINT. YARD-ASHEVILLE
CRAGGY ROAD, ASHEVILLE, NC 28804
33
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Order# 101912 Job# 223229 15 of 51

Brownfield Projects (BF)
MAP ID# 1 Distance from Property: 0 mi. (0 ft.) X
Elevation: 1,950 ft. (Equal to TP)
SITE INFORMATION
GEOSEARCH ID: 21045-17-11
PROJECT NUMBER: 21045-17-11
PROJECT NAME: WOODFIN AUTO & SALVAGE
ADDRESS: 1420 & 1430 RIVERSIDE DRIVE
ASHEVILLE, NC
COUNTY: BUNCOMBE
SITE DETAILS
STATUS: PENDING ELIGIBILITY
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Order# 101912 Job# 223229 16 of 51

Enforcement and Compliance History Information (ECHOR04)
MAP ID# 1 Distance from Property: 0 mi. (0 ft.) X
Elevation: 11950 ft. (Equal to TP)
FACILITY INFORMATION
UNIQUE ID: 110039582555
REGISTRY ID: 110039582555
NAME: WOODFIN AUTO & SALVAGE INC
ADDRESS: 1430 RIVERSIDE DR
ASHEVILLE, NC 28801
COUNTY: BUNCOMBE
FACILITY LINK: Facility Detail Report
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Order# 101912 Job# 223229 17 of 51

Facility Registry System (FRSNC)
MAP ID# 1 Distance from Property: 0 mi. (0 ft.) X
Elevation: 1,950 ft. (Equal to TP)
FACILITY INFORMATION
REGISTRY ID: 110039582555
NAME: WOODFIN AUTO & SALVAGE INC
LOCATION ADDRESS: 1430 RIVERSIDE DR
ASHEVILLE, NC 28801
COUNTY: BUNCOMBE
EPA REGION: 04
FEDERAL FACILITY: NOT REPORTED
TRIBAL LAND: NOT REPORTED
ALTERNATIVE NAME/S:
WOODFIN AUTO & SALVAGE INC
PROGRAM/S LISTED FOR THIS FACILITY
RCRAINFO - RESOURCE CONSERVATION AND RECOVERY ACT INFORMATION SYSTEM
STANDARD INDUSTRIAL CLASSIFICATION/S (SIC)
NO SIC DATA REPORTED
NORTH AMERICAN INDUSTRY CLASS I FICATION/S (NAICS)
NO NAICS DATA REPORTED
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Order# 101912 Job# 223229 18 of 51

Leaking Aboveground Storage Tanks (LAST)
MAP ID# 1 Distance from Property: 0 mi. (0 ft.) X
Elevation: 1,950 ft. (Equal to TP)
SITE INFORMATION
GEOSEARCH ID: AS-88068
FACILITY ID: N/A
SITE NAME: WOODFIN AUTO SALVAGE
ADDRESS: 1430 RIVERSIDE DRIVE
ASHEVILLE, NC 20084
REGIONAL OFFICE: ASH
SITE DETAILS
INCIDENT NUMBER: 88068 RESPONSIBLE PARTY: WOODFIN AUTO AND SALVAGE
UST NUMBER: AS-88068 RESPONSIBLE ADDRESS: 1430 RIVERSIDE DRIVE
DATE OCCURRED: 4/18/2007 ASHEVILLE, NC 20084
DATE REPORTED: 4/18/2007 RESPONSIBLE PARTY LANDOWNER?: FALSE
LAND USE: RES RESPONSIBLE PARTY OWNER?: FALSE
DATE CLEANUP: NOT REPORTED RESPONSIBLE PARTY OPERATOR?: FALSE
DATE CASE CLOSED: NOT REPORTED RESPONSIBLE PARTY CONTACT: CONNIE LEDFORD
DATE CLOSURE REQUESTED: NOT REPORTED CONTACT NUMBER: NOT REPORTED
DATE LAND USE RESTRICTION FILED: NOT REPORTED
TANK REGULATED STATUS: N NUMBER OF SUPPLY WELLS: NOT REPORTED
PRODUCT TYPE: PETROLEUM POLLUTANT TYPE: OTHER INORGANICS
CONTAMINATION TYPE: SOIL SITE PRIORITY: NOT REPORTED
COMMERCIAL/NON-COMMERCIAL TANK: N PHASE OF LSA REQUIRED: NOT REPORTED
NOTICE OF REGULATORY ISSUED: NOT REPORTED NOTICE OF VIOLATION ISSUED: NOT REPORTED
POLLUTANT TYPE PRESENT: OTHER PETROLEUM PROD CURRENT STATUS: CURRENT RECORD
MTBE IN WELL: NOT REPORTED MTBE IN GROUNDWATER: UNKNOWN
RELEASE CODE DESCRIPTION: NOT REPORTED
RBCA DESCRIPTION: NOT REPORTED CURRENT RISK CONDITION: LOW
INITIAL REPORTED RISK OF INCIDENT: LOW RBCA GW DESCRIPTION: NOT REPORTED
CORRECTIVE ACTION PLAN TYPE: NOT REPORTED
COMMENTS: A COMPLAINT CAME IN TO DWM-UST DUE TO PETROLEUM SPILLAGE ON THE GROUND AT THIS
CRUSHER/AUTO SALVAGE FACILITY. THE FACILITY WAS INSPECTED BY SURFACE WATER PROTECTION AND THE
INFORMATION WAS FORWARDED TO UST. SITE VISIT CONDUCTED ON 4118/07 REVEALED LARGE AREAS OF PETROLEUM
IMPACTED SOILS DUE TO ACTIVITIES AT THE FACILITY. NO REAL COLLECTION SYSTEM FOR CONTAINMENT/RECYCLING OF
FLUIDS OBSERVED AT THE SITE. ISSUANCE OF AN OIL SPILL NOV BEING DONE. 09/10/07 - LETTER DOCUMENTING UPDATE
OF RECENT ACTIVITIES AT SITE. TO DATE: APPROX. 45% OF TIRES AND DEBRIS ON PERIMETER OF SITE, REMOVAL OF 80%
METAL ALONG RR SIDING, RELOCATED CAR CRUSHER TO CONCRETE PAD, UPDATED OIL COLLECTION SYSTEM.
PROPOSED ACTIVITES: REMOVAL OF 300+ TONS IMPACTED SOIL AND ADDITIONAL SAMPLING, REMOVAL OF REMAINING
DEBRIS, SITE GRADING, BUILD CONCRETE PAD WITH STORMWATER CONTROL, OIL SKIMMER, OFF -SITE STORMWATER
RUNOFF DIVERSION. 06/09/09 - CED CONDUCTED SITE VISIT WITH SUSAN WILSON. CLEANUP OF THE SITE WAS STILL
BEING CONDUCTED. NO OBVIOUS SOIL STAINING, HOWEVER, HYDRAULIC FLUID WAS EVIDENT IN A POOL ADJ TO
EQUIPMENT. ASKED OWNER TO PUMP OFF WATER AND DIG UP SOIL SURROUNDING THIS AREA. SHE SAID THEY WOULD
CALL ONCE COMPLETED. CED TO CONDUCT ADDITIONAL SITE VISIT IN FEW MONTHS. 07/07/17 -
ESA: 10 SOIL BORINGS ADVANCED THROUGHOUT THE SITE ON 6/14/17 FOR PROPERTY TRANSACTION, RESULTING IN
COLLECTION OF 6 SAMPLES. AUGER REFUSAL WAS ENCOUNTERED AT 2-4' BLS IN EACH LOCATION. SAMPLES WERE
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Order# 101912 Job# 223229 19 of 51

Leaking Aboveground Storage Tanks (LAST)
COLLECTED AT 1-2'. SOILS > S-GW MSCCS AND BENZENE IN SB-1 WAS > RES MSCCS. RECOMMENDATION IS TO EXCAVATE
SOIL AROUND SB-1 AND RE -SAMPLE. IF SOIL IS < RES MSCCS THEN THE SITE COULD BE CLOSED OUT WITH NCS FOR SOIL
AND GW.
PIRF
DATE OCCURRED: NOT REPORTED
DATE SUBMITTED: NOT REPORTED
UST NUMBER: AS-88068
OWNER/OPERATOR: NOT REPORTED
OWNERSHIP: FEDERAL
OPERATION TYPE: 8
TYPE: NOT REPORTED
LOCATION: NOT REPORTED
DESCRIPTION OF INCIDENT:
NOT REPORTED
SITE PRIORITY: NOD
PRIORITY UPDATE DATE: NOT REPORTED
WELLS AFFECTED?: NOT REPORTED
PIRF/MIN SOIL?: NOT REPORTED
HOW RELEASE DISCOVERED?: NOT REPORTED
CAUSE: NOT REPORTED
SOURCE: NOT REPORTED
RISK RANK ABATE - NO RISK RANK ABATE INFORMATION REPORTED
STATUS INFORMATION
LAST MODIFIED: 4/23/2007
INCIDENT PHASE: AS
NOTICE OF REGULATORY ISSUED: NOT REPORTED
NOTICE OF VIOLATION ISSUED: 4/30/2007
45 DAY REPORT: NR PUBLIC MEETING HELD: NR CORRECTIVE ACTION PLANNED: NR
SOC SIGNED: NR RECLASSIFICATION REPORT: NR RS DESIGNATION: NR
CLOSURE REQUESTED DATE: NR CLOSE OUT DATE: NR
REPORTS INFORMATION
REPORT TYPE: SOIL ASSMT REPORT -LOW ONLY
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 7/7/2017 REVIEWED DATE: 7/10/2017
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
10 SOIL BORINGS ADVANCED THROUGHOUT THE SITE ON 6/14117 FOR PROPERTY TRANSACTION, RESULTING IN
COLLECTION OF 6 SAMPLES. AUGER REFUSAL WAS ENCOUNTERED AT 2-4' BLS IN EACH LOCATION. SAMPLES WERE
COLLECTED AT 1-2'. SOILS > S-GW MSCCS AND BENZENE IN SB-1 WAS > RES MSCCS. RECOMMENDATION IS TO EXCAVATE
SOIL AROUND SB-1 AND RE -SAMPLE. IF SOIL IS < RES MSCCS THEN THE SITE COULD BE CLOSED OUT WITH NCS FOR SOIL
AND GW.
REPORT TYPE: OTHER (COMMENTS REQUIRED)
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 6/9/2009 REVIEWED DATE: NOT REPORTED
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
CED CONDUCTED SITE VISIT WITH SUSAN WILSON WQ. CLEANUP OF THE SITE WAS STILL BEING CONDUCTED. NO
OBVIOUS SOIL STAINING, HOWEVER, HYDRAULIC FLUID WAS EVIDENT IN A POOL ADJ TO EQUIPMENT. ASKED OWNER TO
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Order# 101912 Job# 223229 20 of 51

Leaking Aboveground Storage Tanks (LAST)
PUMP OFF WATER AND DIG UP SOIL SURROUNDING THIS AREA. SHE SAID THEY WOULD CALL ONCE COMPLETED. CED TO
CONDUCT ADDITIONAL SITE VISIT IN FEW MONTHS.
REPORT TYPE: OTHER (COMMENTS REQUIRED)
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 9/10/2007 REVIEWED DATE: NOT REPORTED
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
LETTER DOCUMENTING UPDATE OF RECENT ACTIVITIES AT SITE. TO DATE: APPROX. 45% OF TIRES AND DEBRIS ON
PERIMETER OF SITE, REMOVAL OF 80% METAL ALONG RR SIDING, RELOCATED CAR CRUSHER TO CONCRETE PAD,
UPDATED OIL COLLECTION SYSTEM. PROPOSED ACTIVITIES: REMOVAL OF 300+ TONS IMPACTED SOIL AND SAMPLING,
REMOVAL OF REMAINING DEBRIS, SITE GRADING, BUILD CONCRETE PAD WITH STORMWATER CONTROL, OIL SKIMMER,
OFF -SITE STORMWATER RUNOFF DIVERSION.
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Order# 101912 Job# 223229 21 of 51

Resource Conservation & Recovery Act - Non -Generator (RCRANGR04)
MAP ID# 1 Distance from Property: 0 mi. (0 ft.) X
Elevation: 11950 ft. (Equal to TP)
FACILITY INFORMATION
EPA ID#: NCS000001447
NAME: WOODFIN AUTO & SALVAGE INC
ADDRESS: 1430 RIVERSIDE DR
ASHEVILLE, NC 28801
CONTACT NAME: ERNIE LAWRENCE
CONTACT ADDRESS: 1430 RIVERSIDE DR
ASHEVILLE NC 28801
CONTACT PHONE: [phone]
NON-NOTIFIER: NOT A NON-NOTIFIER
DATE RECEIVED BY AGENCY: 10/03/2008
CERTIFICATION
CERTIFICATION NAME: CERTIFICATION TITLE:
ERNIE LAWRENCE NCDENR
OWNER TYPE: NOT REPORTED
OWNER NAME: NOT REPORTED
OPERATOR TYPE: NOT REPORTED
OPERATOR NAME: NOT REPORTED
CERTIFICATION SIGNED DATE:
10/03/2008
INDUSTRY CLASSIFICATION (NAILS) - NO NAICS INFORMATION REPORTED -
CURRENT ACTIVITY INFORMATION
GENERATOR STATUS: NON -GENERATOR LAST UPDATED DATE: 09/25/2013
SUBJECT TO CORRECTIVE ACTION UNIVERSE: NO
TDSFs POTENTIALLY SUBJECT TO CORRECTIVE ACTION UNDER 3004 (u)/(v) UNIVERSE: NO
TDSFs ONLY SUBJECT TO CORRECTIVE ACTION UNDER DISCRETIONARY AUTHORITIES UNIVERSE: NO
NON TSDFs WHERE RCRA CORRECTIVE ACTION HAS BEEN IMPOSED UNIVERSE: NO
CORRECTIVE ACTION WORKLOAD UNIVERSE: NO
IMPORTER: NO
MIXED WASTE GENERATOR: NO
RECYCLER:NO
TRANSPORTER:NO
ONSITE BURNER EXEMPTION: NO
FURNACE EXEMPTION: NO
USED OIL REFINER: NO
USED OIL TRANSFER FACILITY: NO
UNDERGROUND INJECTION: NO
UNIVERSAL WASTE DESTINATION FACILITY: NO
TRANSFER FACILITY: NO
USED OIL FUEL BURNER: NO
USED OIL PROCESSOR: NO
USED OIL FUEL MARKETER TO BURNER: NO
SPECIFICATION USED OIL MARKETER: NO
USED OIL TRANSPORTER: NO
COMPLIANCE, MONITORING AND ENFORCEMENT INFORMATION
EVALUATIONS
07/05/2012 FCI FOCUSED COMPLIANCE INSPECTION
05/12/2010 FCI FOCUSED COMPLIANCE INSPECTION
10/03/2008 FCI FOCUSED COMPLIANCE INSPECTION
VIOLATIONS - NO VIOLATIONS REPORTED -
ENFORCEMENTS - NO ENFORCEMENTS REPORTED -
HAZARDOUS WASTE
- NO HAZARDOUS WASTE INFORMATION REPORTED -
UNIVERSAL WASTE
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Order# 101912 Job# 223229 22 of 51

Resource Conservation & Recovery Act - Non -Generator (RCRANGR04)
WASTE TYPE:
ACCUMULATED
GENERATED
SOURCE TYPE:
WASTE ON -SITE:
WASTE ON -SITE:
BATTERIES
NO
NOT REPORTED
IMPLEMENTER
LAMPS
NO
NOT REPORTED
IMPLEMENTER
PESTICIDES
NO
NOT REPORTED
IMPLEMENTER
MERCURY CONTAINING
NO
NOT REPORTED
IMPLEMENTER
EQUIPMENT
CORRECTIVE ACTION AREA - NO CORRECTIVE ACTION AREA INFORMATION REPORTED -
CORRECTIVE ACTION EVENT - NO CORRECTIVE ACTION EVENT REPORTED -
Back to Report Summary
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Order# 101912 Job# 223229 23 of 51

Resource Conservation & Recovery Act - Non -Generator (RCRANGR04)
MAP ID# 2 Distance from Property: 0.068 mi. (359 ft.) NW
Elevation: 11950 ft. (Equal to TP)
FACILITY INFORMATION
EPA ID#: NCS000001395
NAME: CRAGGY MOTORS
ADDRESS: 1444 RIVERSIDE DR
ACHEVILLE, NC 28804
CONTACT NAME: ANDY SILVER
CONTACT ADDRESS: 1444 RIVERSIDE DR
ACHEVILLE NC
CONTACT PHONE: [phone]
NON-NOTIFIER: NOT A NON-NOTIFIER
DATE RECEIVED BY AGENCY: 11/25/2008
CERTIFICATION
CERTIFICATION NAME: CERTIFICATION TITLE:
ANDY SILVER MGR
OWNER TYPE: NOT REPORTED
OWNER NAME: NOT REPORTED
OPERATOR TYPE: NOT REPORTED
OPERATOR NAME: NOT REPORTED
CERTIFICATION SIGNED DATE:
11 /25/2008
INDUSTRY CLASSIFICATION (NAILS)
42114 - MOTOR VEHICLE PARTS (USED) WHOLESALERS
42193 - RECYCLABLE MATERIAL WHOLESALERS
44112 - USED CAR DEALERS
CURRENT ACTIVITY INFORMATION
GENERATOR STATUS: NON -GENERATOR LAST UPDATED DATE: 04/28/2015
SUBJECT TO CORRECTIVE ACTION UNIVERSE: NO
TDSFs POTENTIALLY SUBJECT TO CORRECTIVE ACTION UNDER 3004 (u)/(v) UNIVERSE: NO
TDSFs ONLY SUBJECT TO CORRECTIVE ACTION UNDER DISCRETIONARY AUTHORITIES UNIVERSE: NO
NON TSDFs WHERE RCRA CORRECTIVE ACTION HAS BEEN IMPOSED UNIVERSE: NO
CORRECTIVE ACTION WORKLOAD UNIVERSE: NO
IMPORTER: NO
MIXED WASTE GENERATOR: NO
RECYCLER:NO
TRANSPORTER:NO
ONSITE BURNER EXEMPTION: NO
FURNACE EXEMPTION: NO
USED OIL REFINER: NO
USED OIL TRANSFER FACILITY: NO
UNDERGROUND INJECTION: NO
UNIVERSAL WASTE DESTINATION FACILITY: NO
TRANSFER FACILITY: NO
USED OIL FUEL BURNER: NO
USED OIL PROCESSOR: NO
USED OIL FUEL MARKETER TO BURNER: NO
SPECIFICATION USED OIL MARKETER: NO
USED OIL TRANSPORTER: NO
COMPLIANCE, MONITORING AND ENFORCEMENT INFORMATION
EVALUATIONS
03/20/2014
FCI
FOCUSED COMPLIANCE INSPECTION
07/05/2012
FCI
FOCUSED COMPLIANCE INSPECTION
05/12/2010
FCI
FOCUSED COMPLIANCE INSPECTION
11/25/2008
FCI
FOCUSED COMPLIANCE INSPECTION
VIOLATIONS - NO VIOLATIONS REPORTED -
ENFORCEMENTS -NO ENFORCEMENTS REPORTED -
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Order# 101912 Job# 223229 24 of 51

Resource Conservation & Recovery Act - Non -Generator (RCRANGR04)
HAZARDOUS WASTE
- NO HAZARDOUS WASTE INFORMATION REPORTED -
UNIVERSAL WASTE
WASTE TYPE:
ACCUMULATED
GENERATED
SOURCE TYPE:
WASTE ON -SITE:
WASTE ON -SITE:
BATTERIES
NO
NOT REPORTED
IMPLEMENTER
LAMPS
NO
NOT REPORTED
IMPLEMENTER
PESTICIDES
NO
NOT REPORTED
IMPLEMENTER
MERCURY CONTAINING
NO
NOT REPORTED
IMPLEMENTER
EQUIPMENT
CORRECTIVE ACTION AREA - NO CORRECTIVE ACTION AREA INFORMATION REPORTED -
CORRECTIVE ACTION EVENT - NO CORRECTIVE ACTION EVENT REPORTED -
Back to Report Summary
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Order# 101912 Job# 223229 25 of 51

Underground Storage Tanks (UST)
MAP ID# 3 Distance from Property: 0.135 mi. (713 ft.) N
Elevation: 11968 ft. (Higher than TP)
SITE INFORMATION
FACILITY ID: 00-0-0000007884
SITE NAME: WALDROPS GROCERY
ADDRESS: RIVERSIDE DR AT CRAGG
ASHEVILLE, NC 28804
COUNTY: BUNCOMBE
CONTACT NAME: WALDROPS GROCERY
CONTACT ADDRESS: PO BOX 8431
ASHEVILLE, NC 28814
TANK INFORMATION
TANK ID: 1
INSTALLED DATE: 5/14/1971
TANK STATUS: REMOVED
PRODUCT NAME: GASOLINE, GAS MIX
TANK CAPACITY: 2000
MAIN TANK: NOT REPORTED
ROOT TANK ID: NOT REPORTED
PERMANENT CLOSED DATE: 4/14/1992
COMPARTMENT TANK: NOT REPORTED
MANIFOLD TANK: NOT REPORTED
TANK CONSTRUCTION: SINGLE WALL STEEL
PIPING CONSTRUCTION: UNKNOWN
PIPING SYSTEM: UNKNOWN
OTHER CP TANK: NOT REPORTED
SPILL PROTECTION: UNKNOWN
PRESSURIZED LEAK DETECTION: UNKNOWN
OVERFILL PROTECTION: UNKNOWN
COMMERCIAL?: YES
REGULATED?: YES
CERTIFICATION NUMBER: NOT REPORTED
TANK ID: 2
INSTALLED DATE: 5/14/1971
TANK STATUS: REMOVED
PRODUCT NAME: GASOLINE, GAS MIX
TANK CAPACITY: 2000
MAIN TANK: NOT REPORTED
ROOT TANK ID: NOT REPORTED
PERMANENT CLOSED DATE: 4/14/1992
COMPARTMENT TANK: NOT REPORTED
MANIFOLD TANK: NOT REPORTED
TANK CONSTRUCTION: SINGLE WALL STEEL
PIPING CONSTRUCTION: UNKNOWN
PIPING SYSTEM: UNKNOWN
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Order# 101912 Job# 223229 26 of 51

Underground Storage Tanks (UST)
OTHER CP TANK: NOT REPORTED
SPILL PROTECTION: UNKNOWN
PRESSURIZED LEAK DETECTION: UNKNOWN
OVERFILL PROTECTION: UNKNOWN
COMMERCIAL?: YES
REGULATED?: YES
CERTIFICATION NUMBER: NOT REPORTED
TANK ID: 3
INSTALLED DATE: 5/11/1981
TANK STATUS: REMOVED
PRODUCT NAME: GASOLINE, GAS MIX
TANK CAPACITY: 1000
MAIN TANK: NOT REPORTED
ROOT TANK ID: NOT REPORTED
PERMANENT CLOSED DATE: 4/14/1992
COMPARTMENT TANK: NOT REPORTED
MANIFOLD TANK: NOT REPORTED
TANK CONSTRUCTION: SINGLE WALL STEEL
PIPING CONSTRUCTION: UNKNOWN
PIPING SYSTEM: UNKNOWN
OTHER CP TANK: NOT REPORTED
SPILL PROTECTION: UNKNOWN
PRESSURIZED LEAK DETECTION: UNKNOWN
OVERFILL PROTECTION: UNKNOWN
COMMERCIAL?: YES
REGULATED?: YES
CERTIFICATION NUMBER: NOT REPORTED
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Order# 101912 Job# 223229 27 of 51

Leaking Underground Storage Tanks (LUST)
MAP ID# 4 Distance from Property: 0.27 mi. (1,426 ft.) E
Elevation: 21062 ft. (Higher than TP)
SITE INFORMATION
GEOSEARCH ID: AS-365
FACILITY ID: 00-0-0000025968
SITE NAME: CRAGGY PRISON LAUNDRY
ADDRESS: HWY 251-N
ASHEVILLE, NC 28814
REGIONAL OFFICE: ASH
SITE DETAILS
INCIDENT NUMBER: 5741 RESPONSIBLE PARTY: MR. KENNETH HART
UST NUMBER: AS-365 RESPONSIBLE ADDRESS: 4216 MAIL SERVICE CENTER
DATE OCCURRED: 4/25/1990 RALEIGH NC 27699
DATE REPORTED: 5/15/1990 RESPONSIBLE PARTY LANDOWNER?: NO
LAND USE: IND RESPONSIBLE PARTY OWNER?: NO
DATE CLEANUP: 5/1511990 RESPONSIBLE PARTY OPERATOR?: NO
DATE CASE CLOSED: NOT REPORTED RESPONSIBLE PARTY CONTACT: NC DEPARTMENT OF PUBLIC SAFETY
DATE CLOSURE REQUESTED: NOT REPORTED CONTACT NUMBER: 9197163400
DATE LAND USE RESTRICTION FILED: NOT REPORTED
TANK REGULATED STATUS: REGULATED NUMBER OF SUPPLY WELLS: NOT REPORTED
PRODUCT TYPE: PETROLEUM POLLUTANT TYPE: LEAK, UST
CONTAMINATION TYPE: GROUNDWATER/BOTH SITE PRIORITY: 70 E
COMMERCIAL/NON-COMMERCIAL TANK: COMMERCIAL PHASE OF LSA REQUIRED: 2
NOTICE OF REGULATORY ISSUED: NOT REPORTED NOTICE OF VIOLATION ISSUED: NOT REPORTED
POLLUTANT TYPE PRESENT: GASOLINE/DIESEL/KEROSENE CURRENT STATUS: CURRENT RECORD
MTBE IN WELL: NOT REPORTED MTBE IN GROUNDWATER: NO
RELEASE CODE DESCRIPTION: NOT REPORTED
RBCA DESCRIPTION: NOT REPORTED CURRENT RISK CONDITION: INTERMEDIATE
INITIAL REPORTED RISK OF INCIDENT: INTERMEDIATE RBCA GW DESCRIPTION: NOT REPORTED
CORRECTIVE ACTTION PLAN TYPE: NOT REPORTED
COMMENTS: FREE PRODUCT RECOVERY REQUIRED - FPRA RANK OF 300. FP RECOVERY BY AFVR TO CONTINUE AS
NEEDED. PER MARCH 9, 2017 LETTER: - 1. CONDUCT SEMI-ANNUAL FREE PRODUCT LEVEL CHECKS ON MW-1, MW-13 &
MW-14, ONLY, IN MAY AND
NOVEMBER 2017. 2. CONDUCT SEMI-ANNUAL AFVR EVENTS ON EACH AFOREMENTIONED WELL THAT CONTAINS FREE
PRODUCT (THICKNESS OF 1/8" OR MORE) IN JUNE AND DECEMBER 2017. 3. SUBMIT AN ANNUAL FREE PRODUCT RECOVERY
REPORT DETAILING BOTH AFVR EVENTS TO THIS OFFICE BY JANUARY 31, 2018.
PIRF
DATE OCCURRED: 4/25/1990
DATE SUBMITTED: 7/17/1990
UST NUMBER: AS-365
OWNER/OPERATOR: MS. KAREN BROWN
OWNERSHIP: 7
OPERATION TYPE: 6
TYPE: 4
LOCATION: 1
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Order# 101912 Job# 223229 28 of 51

Leaking Underground Storage Tanks (LUST)
DESCRIPTION OF INCIDENT:
PRIOR TO CLOSING A 15,000 GAL. UST SOIL SAMPLES SHOWED TPFH LEVELS OF 43,96, AND 142 PPM.
SITE PRIORITY: 70 E
PRIORITY UPDATE DATE: 4/15/1998
WELLS AFFECTED?: NO
PIRF/MIN SOIL?: PIRF
HOW RELEASE DISCOVERED?: NOT REPORTED
CAUSE: NOT REPORTED
SOURCE: NOT REPORTED
RISK RANK ABATE
RRA DATE: 7/11/2008
RRA INIT: MES
RRA RISK: INTERMEDIATE
RRA RANK: 0180
RRA ABATE: UST RELEASE HAS BEEN ABATED. HOWEVER, CONTAMINATED SOIL CONTINUES TO RELEASE PRODUCT OR
CONTAMINANTS INTO THE ENVIRONMENT
STATUS INFORMATION
LAST MODIFIED: 9/26/1990
INCIDENT PHASE: FOLLOW UP
NOTICE OF REGULATORY ISSUED: NOT REPORTED
NOTICE OF VIOLATION ISSUED: 7/19/1990
45 DAY REPORT: NR PUBLIC MEETING HELD: NR CORRECTIVE ACTION PLANNED: NR
SOC SIGNED: NR RECLASSIFICATION REPORT: NR RS DESIGNATION: NR
CLOSURE REQUESTED DATE: NR CLOSE OUT DATE: NR
REPORTS INFORMATION
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 1/17/2013 REVIEWED DATE: 2/11/2013
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 2/12/2007 REVIEWED DATE: NOT REPORTED
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 1/18/2008 REVIEWED DATE: NOT REPORTED
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 7/8/2008 REVIEWED DATE: NOT REPORTED
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
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Leaking Underground Storage Tanks (LUST)
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 9/2/2009 REVIEWED DATE: 9/9/2009
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 1/5/2009 REVIEWED DATE: NOT REPORTED
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 1/7/2011 REVIEWED DATE: 2/7/2011
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 1/11/2012 REVIEWED DATE: 2/13/2012
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 1/27/2012 REVIEWED DATE: 2/22/2012
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 2/11/2016 REVIEWED DATE: 2/22/2016
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 3/4/2014 REVIEWED DATE: 3/10/2014
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
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Leaking Underground Storage Tanks (LUST)
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 2/17/2015 REVIEWED DATE: 3/5/2015
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: FPRS
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 1/3/2017 REVIEWED DATE: 1/30/2017
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: NOT REPORTED DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
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Order# 101912 Job# 223229 31 of 51

State Trust Funds Database (LUSTFUND)
MAP ID# 4 Distance from Property: 0.27 mi. (1,426 ft.) E
Elevation: 21062 ft. (Higher than TP)
SITE INFORMATION
INCIDENT NUMBER: 5741
SITE NAME: CRAGGY PRISON LAUNDRY
ADDRESS: HWY 251, RIVERSIDE D
ASHEVILLE, NC
COUNTY: BUNCOMBE
SITE ELIGIBLE?: YES
COMMERCIAL FUND: 100% COMMERCIAL
DEDUCTABLE AMOUNT: 50000
THIRD PARTY DEDUCTABLE AMOUNT: NOT REPORTED
SUM OF THIRD PARTY AMOUNT APPLIED: NOT REPORTED
PRIORITY RANK: L
REIMBURSEMENT IDENTIFICATION FORM ON FILE?: YES
STATE ARCHIVE SUBMITTAL NUMBER: NA
SITE NOTES: NOT REPORTED
OWNER INFORMATION
COMPANY NAME: NC DEPT. OF PUBLIC SAFETY
MAILING ADDRESS: 4216 MSC
RALEIGH NC
NAME: WILLIAM STOVALL
PHONE: [phone]
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Leaking Underground Storage Tanks (LUST)
MAP ID# 5 Distance from Property: 0.277 mi. (1,463 ft.) ESE
Elevation: 11949 ft. (Lower than TP)
SITE INFORMATION
GEOSEARCH ID: AS-1026
FACILITY ID: NOT REPORTED
SITE NAME: NCDOT MAINT. YARD-ASHEVILLE
ADDRESS: CRAGGY ROAD
ASHEVILLE, NC 28804
REGIONAL OFFICE: ASH
SITE DETAILS
INCIDENT NUMBER: 11201
RESPONSIBLE PARTY: NCDOT
UST NUMBER: AS-1026
RESPONSIBLE ADDRESS: 4809 BERYL ROAD
DATE OCCURRED: 7/12/1992
RALEIGH NC 27606
DATE REPORTED: 7/12/1992
RESPONSIBLE PARTY LANDOWNER?: NO
LAND USE: IND
RESPONSIBLE PARTY OWNER?: NO
DATE CLEANUP: 7/12/1992
RESPONSIBLE PARTY OPERATOR?: NO
DATE CASE CLOSED: NOT REPORTED
RESPONSIBLE PARTY CONTACT: NC DEPT. OF TRANSPORTATION
DATE CLOSURE REQUESTED: NOT REPORTED
CONTACT NUMBER: 919-733-2220
DATE LAND USE RESTRICTION FILED: NOT REPORTED
TANK REGULATED STATUS: REGULATED
NUMBER OF SUPPLY WELLS: NOT REPORTED
PRODUCT TYPE: PETROLEUM
POLLUTANT TYPE: LEAK, UST
CONTAMINATION TYPE: GROUNDWATER/BOTH
SITE PRIORITY: 70 E
COMMERCIAL/NON-COMMERCIAL TANK: COMMERCIAL
PHASE OF LSA REQUIRED: NOT REPORTED
NOTICE OF REGULATORY ISSUED: NOT REPORTED
NOTICE OF VIOLATION ISSUED: NOT REPORTED
POLLUTANT TYPE PRESENT: GASOLINE/DIESEL/KEROSENE CURRENT STATUS: CURRENT RECORD
MTBE IN WELL: NOT REPORTED
MTBE IN GROUNDWATER: UNKNOWN
RELEASE CODE DESCRIPTION: NOT REPORTED
RBCA DESCRIPTION: NOT REPORTED
CURRENT RISK CONDITION: LOW
INITIAL REPORTED RISK OF INCIDENT: INTERMEDIATE RBCA GW DESCRIPTION: NOT REPORTED
CORRECTIVE ACTTION PLAN TYPE: SV
COMMENTS: SITE VISIT ON 3/8/01-AS/SVE SYSTEM WAS RUNNING
PIRF
DATE OCCURRED: 7/12/1992
DATE SUBMITTED: 11/9/1993
UST NUMBER: AS-1026
OWNER/OPERATOR: JONH M. BURNS, JR.
OWNERSHIP: 7
OPERATION TYPE: 1
TYPE: 3
LOCATION: 1
DESCRIPTION OF INCIDENT:
UPON REMOVAL OF 6 USTS, SOIL AND GW WERE FOUND TO BE CONTAMINATED. NOV WAS ISSUED.
SITE PRIORITY: 70 E
PRIORITY UPDATE DATE: 4/15/1998
WELLS AFFECTED?: NO
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Leaking Underground Storage Tanks (LUST)
PIRF/MIN SOIL?: PIRF
HOW RELEASE DISCOVERED?: NOT REPORTED
CAUSE: NOT REPORTED
SOURCE: NOT REPORTED
RISK RANK ABATE
RRA DATE: 7/9/2008
RRA INIT: DPM
RRA RISK: INTERMEDIATE
RRA RANK: 0075
RRA ABATE: UST RELEASE HAS BEEN ABATED. CONTAMINATED SOIL HAS BEEN REMOVED OR REMEDIATED
STATUS INFORMATION
LAST MODIFIED: 6/10/1996
INCIDENT PHASE: REMEDIAL ACTION
NOTICE OF REGULATORY ISSUED: NOT REPORTED
NOTICE OF VIOLATION ISSUED: 11/4/1993
45 DAY REPORT: NR PUBLIC MEETING HELD: NR CORRECTIVE ACTION PLANNED: 5/6/1996
SOC SIGNED: NR RECLASSIFICATION REPORT: NR RS DESIGNATION: NR
CLOSURE REQUESTED DATE: NR CLOSE OUT DATE: NR
REPORTS INFORMATION
REPORT TYPE: CAP
REQUESTED DATE: NOT REPORTED RECEIVED DATE: 3/23/1995 REVIEWED DATE: NOT REPORTED
APPROVED DATE: NOT REPORTED IMPLEMENTED DATE: 12/5/1995 DUE DATE: NOT REPORTED
COMMENTS:
NOT REPORTED
REPORT TYPE: REMEDIATION MONITORING REPORT
REQUESTED DATE: 6/17/2003 RECEIVED DATE: NOT REPORTED REVIEWED DATE: NOT REPORTED
APPROVED DATE: 6/17/2003 IMPLEMENTED DATE: NOT REPORTED DUE DATE: 10/30/2003
COMMENTS:
NOT REPORTED
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Unlocated Sites Summary
This list contains sites that could not be mapped due to limited or incomplete address information.
Database
Name
Site ID#
Site Name
Address
City/State/Zip/County
LUSTFUND
11201
NCDOT-CRAGGY
NC HIGHWAY 251
ASHEVILLE
RCRANGR04
NCD000276535"
ASHEVILLE METRO
NC HWY 191 N AT WOODFIN
WOODFIN 28804 Buncombe
NG
SEWERAGE DISTRICT
SWF
11A-LCID-
L T PARROTT DEMO
HWY 191
ASHEVILLE
LANDFILL
UST
00-0-0000011147
ASHEVILLE UNDERGROUND
RIVERSIDE DRIVE
ASHEVILLE 28806
CREW QRTRS
Buncombe
UST
00-0-0000001778
LANDFILL
HWY 251
ASHEVILLE 28804
Buncombe
UST
00-0-0000024712
N.C. DOT HIGHWAY
191 NORTH OF ASHEVILLE 4
CRAGGY 28804 Buncombe
EQUIPMENT DIV.
MILES
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Environmental Records Definitions - FEDERAL
AIRSAFS Aerometric Information Retrieval System / Air Facility Subsystem
VERSION DATE: 10/20/14
The United States Environmental Protection Agency (EPA) modified the Aerometric Information Retrieval
System (AIRS) to a database that exclusively tracks the compliance of stationary sources of air pollution with
EPA regulations: the Air Facility Subsystem (AFS). Since this change in 2001, the management of the
AIRS/AFS database was assigned to EPA's Office of Enforcement and Compliance Assurance.
BRS Biennial Reporting System
VERSION DATE: 12/31/11
The United States Environmental Protection Agency (EPA), in cooperation with the States, biennially collects
information regarding the generation, management, and final disposition of hazardous wastes regulated under
the Resource Conservation and Recovery Act of 1976 (RCRA), as amended. The Biennial Report captures
detailed data on the generation of hazardous waste from large quantity generators and data on waste
management practices from treatment, storage and disposal facilities. Currently, the EPA states that data
collected between 1991 and 1997 was originally a part of the defunct Biennial Reporting System and is now
incorporated into the RCRAInfo data system.
CDL Clandestine Drug Laboratory Locations
VERSION DATE: 07/01/16
The U.S. Department of Justice ("the Department") provides this information as a public service. It contains
addresses of some locations where law enforcement agencies reported they found chemicals or other items that
indicated the presence of either clandestine drug laboratories or dumpsites. In most cases, the source of the
entries is not the Department, and the Department has not verified the entry and does not guarantee its
accuracy. Members of the public must verify the accuracy of all entries by, for example, contacting local law
enforcement and local health departments. The Department does not establish, implement, enforce, or certify
compliance with clean-up or remediation standards for contaminated sites; the public should contact a state or
local health department or environmental protection agency for that information.
DOCKETS EPA Docket Data
VERSION DATE: 12/22/05
The United States Environmental Protection Agency Docket data lists Civil Case Defendants, filing dates as far
back as 1971, laws broken including section, violations that occurred, pollutants involved, penalties assessed
and superfund awards by facility and location. Please refer to ICIS database as source of current data.
EC Federal Engineering Institutional Control Sites
VERSION DATE: 08/03/15
This database includes site locations where Engineering and/or Institutional Controls have been identified as part
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Environmental Records Definitions - FEDERAL
of a selected remedy for the site as defined by United States Environmental Protection Agency official remedy
decision documents. A site listing does not indicate that the institutional and engineering controls are currently in
place nor will be in place once the remedy is complete; it only indicates that the decision to include either of them
in the remedy is documented as of the completed date of the document. Institutional controls are actions, such
as legal controls, that help minimize the potential for human exposure to contamination by ensuring appropriate
land or resource use. Engineering controls include caps, barriers, or other device engineering to prevent access,
exposure, or continued migration of contamination.
ECHOR04 Enforcement and Compliance History Information
VERSION DATE: 08/26/17
The EPA's Enforcement and Compliance History Online (ECHO) database, provides compliance and
enforcement information for facilities nationwide. This database includes facilities regulated as Clean Air Act
stationary sources, Clean Water Act direct dischargers, Resource Conservation and Recovery Act hazardous
waste handlers, Safe Drinking Water Act public water systems along with other data, such as Toxics Release
Inventory releases.
ERNSNC Emergency Response Notification System
VERSION DATE: 10/15/17
This National Response Center database contains data on reported releases of oil, chemical, radiological,
biological, and/or etiological discharges into the environment anywhere in the United States and its territories.
The data comes from spill reports made to the U.S. Environmental Protection Agency, U.S. Coast Guard, the
National Response Center and/or the U.S. Department of Transportation.
FRSNC Facility Registry System
VERSION DATE: 09/06/17
The United States Environmental Protection Agency's Office of Environmental Information (OEI) developed the
Facility Registry System (FRS) as the centrally managed database that identifies facilities, sites or places subject
to environmental regulations or of environmental interest. The Facility Registry System replaced the Facility
Index System or FINDS database.
HMIRSR04 Hazardous Materials Incident Reporting System
VERSION DATE: 08/30/17
The HMIRS database contains unintentional hazardous materials release information reported to the U.S.
Department of Transportation located in EPA Region 4. This region includes the following states: Alabama,
Florida, Georgia, Kentucky, Mississippi, North Carolina, South Carolina, and Tennessee.
ICIS Integrated Compliance Information System (formerly DOCKETS)
VERSION DATE: 09/23/17
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Environmental Records Definitions - FEDERAL
ICIS is a case activity tracking and management system for civil, judicial, and administrative federal
Environmental Protection Agency enforcement cases. ICIS contains information on federal administrative and
federal judicial cases under the following environmental statutes: the Clean Air Act, the Clean Water Act, the
Resource Conservation and Recovery Act, the Emergency Planning and Community Right -to -Know Act - Section
313, the Toxic Substances Control Act, the Federal Insecticide, Fungicide, and Rodenticide Act, the
Comprehensive Environmental Response, Compensation, and Liability Act, the Safe Drinking Water Act, and the
Marine Protection, Research, and Sanctuaries Act.
ICISNPDES Integrated Compliance Information System National Pollutant Discharge Elimination System
VERSION DATE: 07/09/17
Authorized by the Clean Water Act, the National Pollutant Discharge Elimination System (NPDES) permit
program controls water pollution by regulating point sources that discharge pollutants into waters of the United
States.
LUCIS Land Use Control Information System
VERSION DATE: 09/01/06
The LUCIS database is maintained by the U.S. Department of the Navy and contains information for former Base
Realignment and Closure (BRAC) properties across the United States.
MILTS Material Licensing Tracking System
VERSION DATE: 06/29/17
MILTS is a list of approximately 8,100 sites which have or use radioactive materials subject to the United States
Nuclear Regulatory Commission (NRC) licensing requirements.
NPDESR04 National Pollutant Discharge Elimination System
VERSION DATE: 04/01/07
Authorized by the Clean Water Act, the National Pollutant Discharge Elimination System (NPDES) permit
program controls water pollution by regulating point sources that discharge pollutants into waters of the United
States. The NPDES database was collected from December 2002 until April 2007. Refer to the PCS and/or ICIS-
NPDES database as source of current data. This database includes permitted facilities located in EPA Region 4.
This region includes the following states: Alabama, Florida, Georgia, Kentucky, Mississippi, North Carolina,
South Carolina, and Tennessee.
PADS PCB Activity Database System
VERSION DATE: 07/18/17
PADS Identifies generators, transporters, commercial storers and/or brokers and disposers of PCB's who are
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Environmental Records Definitions - FEDERAL
required to notify the EPA of such activities.
PCSR04 Permit Compliance System
VERSION DATE: 08/01/12
The Permit Compliance System is used in tracking enforcement status and permit compliance of facilities
controlled by the National Pollutant Discharge Elimination System (NPDES) under the Clean Water Act and is
maintained by the United States Environmental Protection Agency's Office of Compliance. PCS is designed to
support the NPDES program at the state, regional, and national levels. This database includes permitted
facilities located in EPA Region 4. This region includes the following states: Alabama, Florida, Georgia,
Kentucky, Mississippi, North Carolina, South Carolina, and Tennessee. PCS has been modernized, and no
longer exists. National Pollutant Discharge Elimination System (ICIS-NPDES) data can now be found in
Integrated Compliance Information System (ICIS).
RCRASC RCRA Sites with Controls
VERSION DATE: 11/21/17
The Resource Conservation and Recovery Act (RCRA) gives EPA the authority to control hazardous waste from
the "cradle -to -grave." This includes the generation, transportation, treatment, storage, and disposal of hazardous
waste. RCRA also set forth a framework for the management of non -hazardous solid wastes. The 1986
amendments to RCRA enabled EPA to address environmental problems that could result from underground
tanks storing petroleum and other hazardous substances. This listing refers to facilities with institutional controls
in place.
SEMSLIENS SEMS Lien on Property
VERSION DATE: 12/11/17
The U.S. Environmental Protections Agency's (EPA) Office of Solid Waste and Emergency Response, Office of
Superfund Remediation and Technology Innovation (OSRTI), has implemented The Superfund Enterprise
Management System (SEMS), formerly known as CERCLIS (Comprehensive Environmental Response,
Compensation and Liability Information System) to track and report on clean-up and enforcement activities
taking place at Superfund sites. SEMS represents a joint development and ongoing collaboration between
Superfund's Remedial, Removal, Federal Facilities, Enforcement and Emergency Response programs. This is a
listing of SEMS sites with a lien on the property.
SFLIENS CERCLIS Liens
VERSION DATE: 06/08/12
A Federal CERCLA ("Superfund") lien can exist by operation of law at any site or property at which United States
Environmental Protection Agency has spent Superfund monies. These monies are spent to investigate and
address releases and threatened releases of contamination. CERCLIS provides information as to the identity of
these sites and properties. This database contains those CERCLIS sites where the Lien on Property action is
complete.
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Environmental Records Definitions - FEDERAL
SSTS Section Seven Tracking System
VERSION DATE: 02/01/17
The United States Environmental Protection Agency tracks information on pesticide establishments through the
Section Seven Tracking System (SSTS). SSTS records the registration of new establishments and records
pesticide production at each establishment. The Federal Insecticide, Fungicide and Rodenticide Act (FIFRA)
requires that production of pesticides or devices be conducted in a registered pesticide -producing or device -
producing establishment. ("Production" includes formulation, packaging, repackaging, and relabeling.)
TRI Toxics Release Inventory
VERSION DATE: 12/31/16
The Toxics Release Inventory, provided by the United States Environmental Protection Agency, includes data on
toxic chemical releases and waste management activities from certain industries as well as federal and tribal
facilities. This inventory contains information about the types and amounts of toxic chemicals that are released
each year to the air, water, and land as well as information on the quantities of toxic chemicals sent to other
facilities for further waste management.
TSCA Toxic Substance Control Act Inventory
VERSION DATE: 12/31/12
The Toxic Substances Control Act (TSCA) was enacted in 1976 to ensure that chemicals manufactured,
imported, processed, or distributed in commerce, or used or disposed of in the United States do not pose any
unreasonable risks to human health or the environment. TSCA section 8(b) provides the United States
Environmental Protection Agency authority to "compile, keep current, and publish a list of each chemical
substance that is manufactured or processed in the United States." This TSCA Chemical Substance Inventory
contains non -confidential information on the production amount of toxic chemicals from each manufacturer and
importer site.
RCRAGR04 Resource Conservation & Recovery Act - Generator
VERSION DATE: 10/17/17
The Resource Conservation and Recovery Act (RCRA) gives EPA the authority to control hazardous waste from
the "cradle -to -grave." This includes the generation, transportation, treatment, storage, and disposal of hazardous
waste. RCRA also set forth a framework for the management of non -hazardous solid wastes. The 1986
amendments to RCRA enabled EPA to address environmental problems that could result from underground
tanks storing petroleum and other hazardous substances. This listing refers to facilities currently generating
hazardous waste. EPA Region 4 includes the following states: Alabama, Florida, Georgia, Kentucky, Mississippi,
North Carolina, South Carolina, and Tennessee.
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Environmental Records Definitions - FEDERAL
RCRANGR04 Resource Conservation & Recovery Act - Non -Generator
VERSION DATE: 10/17/17
The Resource Conservation and Recovery Act (RCRA) gives EPA the authority to control hazardous waste from
the "cradle -to -grave." This includes the generation, transportation, treatment, storage, and disposal of hazardous
waste. RCRA also set forth a framework for the management of non -hazardous solid wastes. The 1986
amendments to RCRA enabled EPA to address environmental problems that could result from underground
tanks storing petroleum and other hazardous substances. This listing refers to facilities classified as non -
generators. Non -Generators do not presently generate hazardous waste. EPA Region 4 includes the following
states: Alabama, Florida, Georgia, Kentucky, Mississippi, North Carolina, South Carolina, and Tennessee.
ALTFUELS Alternative Fueling Stations
VERSION DATE: 01/22/18
Nationwide list of alternative fueling stations made available by the US Department of Energy's Office of Energy
Efficiency & Renewable Energy. Includes Biodiesel stations, Ethanol (E85) stations, Liquefied Petroleum Gas
(Propane) stations, Ethanol (E85) stations, Natural Gas stations, Hydrogen stations, and
Electric Vehicle Supply Equipment (EVSE).
FEMAUST FEMA Owned Storage Tanks
VERSION DATE: 12/01/16
This is a listing of FEMA owned underground and aboveground storage tank sites. For security reasons, address
information is not released to the public according to the U.S. Department of Homeland Security.
HISTPST Historical Gas Stations
VERSION DATE: NR
This historic directory of service stations is provided by the Cities Service Company. The directory includes
Cities Service filling stations that were located throughout the United States in 1930.
ICISCLEANERS Integrated Compliance Information System Drycleaners
VERSION DATE: 09/23/17
This is a listing of drycleaner facilities from the Integrated Compliance Information System (ICIS). The
Environmental Protection Agency (EPA) tracks facilities that
possess NAIC and SIC codes that classify businesses as drycleaner establishments.
MRDS Mineral Resource Data System
VERSION DATE: 03/15/16
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Environmental Records Definitions - FEDERAL
MRDS (Mineral Resource Data System) is a collection of reports describing metallic and nonmetallic mineral
resources throughout the world. Included are deposit name, location, commodity, deposit description, geologic
characteristics, production, reserves, resources, and references. This database contains the records previously
provided in the Mineral Resource Data System (MRDS) of USGS and the Mineral Availability System/Mineral
Industry Locator System (MAS/MILS) originated in the U.S. Bureau of Mines, which is now part of USGS.
MSHA Mine Safety and Health Administration Master Index File
VERSION DATE: 09/01/17
The Mine dataset lists all Coal and Metal/Non-Metal mines under MSHA's jurisdiction since 1/1/1970. It includes
such information as the current status of each mine (Active, Abandoned, NonProducing, etc.), the current owner
and operating company, commodity codes and physical attributes of the mine. Mine ID is the unique key for this
data. This information is provided by the United States Department of Labor - Mine Safety and Health
Administration (MSHA).
BF Brownfields Management System
VERSION DATE: 11/21/17
Brownfields are real property, the expansion, redevelopment, or reuse of which may be complicated by the
presence or potential presence of a hazardous substance, pollutant, or contaminant. Cleaning up and reinvesting
in these properties takes development pressures off of undeveloped, open land, and both improves and protects
the environment. The United States Environmental Protection Agency maintains this database to track activities
in the various brown field grant programs including grantee assessment, site cleanup and site redevelopment.
This database included tribal brownfield sites.
DNPL Delisted National Priorities List
VERSION DATE: 12/11/17
This database includes sites from the United States Environmental Protection Agency's Final National Priorities
List (NPL) where remedies have proven to be satisfactory or sites where the original analyses were inaccurate,
and the site is no longer appropriate for inclusion on the NPL, and final publication in the Federal Register has
occurred.
NLRRCRAT No Longer Regulated RCRA Non-CORRACTS TSD Facilities
VERSION DATE: 10/17/17
This database includes RCRA Non -Corrective Action TSD facilities that are no longer regulated by the United
States Environmental Protection Agency or do not meet other RCRA reporting requirements. This listing
includes facilities that formerly treated, stored or disposed of hazardous waste.
ODI Open Dump Inventory
VERSION DATE: 06/01/85
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Environmental Records Definitions - FEDERAL
The open dump inventory was published by the United States Environmental Protection Agency. An "open dump"
is defined as a facility or site where solid waste is disposed of which is not a sanitary landfill which meets the
criteria promulgated under section 4004 of the Solid Waste Disposal Act (42 U.S.C. 6944) and which is not a
facility for disposal of hazardous waste. This inventory has not been updated since June 1985.
RCRAT Resource Conservation & Recovery Act - Non-CORRACTS Treatment, Storage & Disposal Facilities
VERSION DATE: 10/17/17
The Resource Conservation and Recovery Act (RCRA) gives EPA the authority to control hazardous waste from
the "cradle -to -grave." This includes the generation, transportation, treatment, storage, and disposal of hazardous
waste. RCRA also set forth a framework for the management of non -hazardous solid wastes. The 1986
amendments to RCRA enabled EPA to address environmental problems that could result from underground
tanks storing petroleum and other hazardous substances. This listing refers to facilities recognized as hazardous
waste treatment, storage, and disposal sites (TSD).
SEMS Superfund Enterprise Management System
VERSION DATE: 12/11/17
The U.S. Environmental Protections Agency's (EPA) Office of Solid Waste and Emergency Response, Office of
Superfund Remediation and Technology Innovation (OSRTI), has implemented The Superfund Enterprise
Management System (SEMS), formerly known as CERCLIS (Comprehensive Environmental Response,
Compensation and Liability Information System) to track and report on clean-up and enforcement activities
taking place at Superfund sites. SEMS represents a joint development and ongoing collaboration between
Superfund's Remedial, Removal, Federal Facilities, Enforcement and Emergency Response programs.
SEMSARCH Superfund Enterprise Management System Archived Site Inventory
VERSION DATE: 12/11/17
The Superfund Enterprise Management System Archive listing (SEMS-ARCHIVE) has replaced the CERCLIS
NFRAP reporting system in 2015. This listing reflect sites that have been assessed and no further remediation is
planned and is of no further interest under the Superfund program.
SMCRA Surface Mining Control and Reclamation Act Sites
VERSION DATE: 08/25/17
An inventory of land and water impacted by past mining (primarily coal mining) is maintained by OSMRE to
provide information needed to implement the Surface Mining Control and Reclamation Act of 1977 (SMCRA).
The inventory contains information on the location, type, and extent of AML impacts, as well as, information on
the cost associated with the reclamation of those problems. The inventory is based upon field surveys by State,
Tribal, and OSMRE program officials. It is dynamic to the extent that it is modified as new problems are identified
and existing problems are reclaimed.
Geoearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223229 43 of 51

Environmental Records Definitions - FEDERAL
USUMTRCA Uranium Mill Tailings Radiation Control Act Sites
VERSION DATE: 03/04/17
The Legacy Management Office of the Department of Energy (DOE) manages radioactive and chemical waste,
environmental contamination, and hazardous material at over 100 sites across the U.S. The L.M. Office
manages this database of sites registered under the Uranium Mill Tailings Control Act (UMTRCA).
DOD Department of Defense Sites
VERSION DATE: 12/01/14
This information originates from the National Atlas of the United States Federal Lands data, which includes lands
owned or administered by the Federal government. Army DOD, Army Corps of Engineers DOD, Air Force DOD,
Navy DOD and Marine DOD areas of 640 acres or more are included.
FUDS Formerly Used Defense Sites
VERSION DATE: 06/01/15
The Formerly Used Defense Sites (FUDS) inventory includes properties previously owned by or leased to the
United States and under Secretary of Defense Jurisdiction, as well as Munitions Response Areas (MRAs). The
remediation of these properties is the responsibility of the Department of Defense. This data is provided by the
U.S. Army Corps of Engineers (USACE), the boundaries/polygon data are based on preliminary findings and not
all properties currently have polygon data available. DISCLAIMER: This data represents the results of data
collection/processing for a specific USACE activity and is in no way to be considered comprehensive or to be
used in any legal or official capacity as presented on this site. While the USACE has made a reasonable effort to
insure the accuracy of the maps and associated data, it should be explicitly noted that USACE makes no
warranty, representation or guaranty, either expressed or implied, as to the content, sequence, accuracy,
timeliness or completeness of any of the data provided herein. For additional information on Formerly Used
Defense Sites please contact the USACE Public Affairs Office at [phone].
FUSRAP Formerly Utilized Sites Remedial Action Program
VERSION DATE: 03/04/17
The U.S. DOE established the Formerly Utilized Sites Remedial Action Program (FUSRAP) in 1974 to remediate
sites where radioactive contamination remained from the Manhattan Project and early U.S. Atomic Energy
Commission (AEC) operations. The DOE Office of Legacy Management (LM) established long-term surveillance
and maintenance (LTS&M) requirements for remediated FUSRAP sites. DOE evaluates the final site conditions
of a remediated site on the basis of risk for different future uses. DOE then confirms that LTS&M requirements
will maintain protectiveness.
NLRRCRAC No Longer Regulated RCRA Corrective Action Facilities
VERSION DATE: 10/17/17
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Order# 101912 Job# 223229 44 of 51

Environmental Records Definitions - FEDERAL
This database includes RCRA Corrective Action facilities that are no longer regulated by the United States
Environmental Protection Agency or do not meet other RCRA reporting requirements.
NMS Former Military Nike Missile Sites
VERSION DATE: 12/01/84
This information was taken from report DRXTH-AS-IA-83AO16 (Historical Overview of the Nike Missile System,
12/1984) which was performed by Environmental Science and Engineering, Inc. for the U.S. Army Toxic and
Hazardous Materials Agency Assessment Division. The Nike system was deployed between 1954 and the mid-
1970's. Among the substances used or stored on Nike sites were liquid missile fuel (JP-4); starter fluids (UDKH,
aniline, and furfuryl alcohol); oxidizer (IRFNA); hydrocarbons (motor oil, hydraulic fluid, diesel fuel, gasoline,
heating oil); solvents (carbon tetrachloride, trichloroethylene, trichloroethane, stoddard solvent); and battery
electrolyte. The quantities of material a disposed of and procedures for disposal are not documented in
published reports. Virtually all information concerning the potential for contamination at Nike sites is confined to
personnel who were assigned to Nike sites.
During deactivation most hardware was shipped to depot -level supply points. There were reportedly instances
where excess materials were disposed of on or near the site itself at closure. There was reportedly no routine
site decontamination.
NPL National Priorities List
VERSION DATE: 12/11/17
This database includes United States Environmental Protection Agency (EPA) National Priorities List sites that
fall under the EPA's Superfund program, established to fund the cleanup of the most serious uncontrolled or
abandoned hazardous waste sites identified for possible long-term remedial action.
PNPL Proposed National Priorities List
VERSION DATE: 12/11/17
This database contains sites proposed to be included on the National Priorities List (NPL) in the Federal
Register. The United States Environmental Protection Agency investigates these sites to determine if they may
present long-term threats to public health or the environment.
RCRAC Resource Conservation & Recovery Act - Corrective Action Facilities
VERSION DATE: 10/17/17
The Resource Conservation and Recovery Act (RCRA) gives EPA the authority to control hazardous waste from
the "cradle -to -grave." This includes the generation, transportation, treatment, storage, and disposal of hazardous
waste. RCRA also set forth a framework for the management of non -hazardous solid wastes. The 1986
amendments to RCRA enabled EPA to address environmental problems that could result from underground
tanks storing petroleum and other hazardous substances. This listing refers to facilities with corrective action
activity.
Geoearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223229 45 of 51

Environmental Records Definitions - FEDERAL
RCRASUBC Resource Conservation & Recovery Act - Subject to Corrective Action Facilities
VERSION DATE: 10/17/17
The Resource Conservation and Recovery Act (RCRA) gives EPA the authority to control hazardous waste from
the "cradle -to -grave." This includes the generation, transportation, treatment, storage, and disposal of hazardous
waste. RCRA also set forth a framework for the management of non -hazardous solid wastes. The 1986
amendments to RCRA enabled EPA to address environmental problems that could result from underground
tanks storing petroleum and other hazardous substances. This listing refers to facilities subject to corrective
actions.
RODS Record of Decision System
VERSION DATE: 12/11/17
These decision documents maintained by the United States Environmental Protection Agency describe the
chosen remedy for NPL (Superfund) site remediation. They also include site history, site description, site
characteristics, community participation, enforcement activities, past and present activities, contaminated media,
the contaminants present, and scope and role of response action.
Geoearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223229 46 of 51

Environmental Records Definitions - STATE (NC)
AFO Animal Feeding Operation Permits
VERSION DATE: 11/04/16
This list of animal feeding operation permits is provided by the Water Quality Division of the North Carolina
Department of Environment and Natural Resources.
AIRS Air Permitted Facilities
VERSION DATE: 10/05/17
This list of facilities with air quality permits is provided by the Air Quality Division of the North Carolina
Department of Environment and Natural Resources.
LUR Land Use Restricted Sites
VERSION DATE: 10/03/16
This listing includes sites from the Inactive Hazardous Sites Inventory with a No Further Action Restricted Use
status. The inventory is maintained by the Superfund Section of the Division of Waste Management in the North
Carolina Department of Environment and Natural Resources (DENR). The DENR defines "Inactive Hazardous
Sites" as areas where a hazardous substance release has come to be located and would include active and
inactive facilities and a variety of property types. The term "inactive" refers to the fact that cleanup was inactive at
large numbers of sites at the time of program enactment. After cleanup is complete, the site is transferred to a
"No Further Action" status.
NPDES National Pollutant Discharge Elimination System Permits
VERSION DATE: 10/01/17
The Water Quality Division of the North Carolina Department of Environment and Natural Resources provides
this list of National Pollutant Discharge Elimination System (NPDES) Permits. Authorized by the Clean Water
Act, the National Pollutant Discharge Elimination System (NPDES) permit program controls water pollution by
regulating point sources that discharge pollutants into waters of the United States.
SPILLS Spills listing
VERSION DATE: 04/12/17
This spills tracking database is provided by the Division of Water Quality's Emergency Response Section of the
North Carolina Department of Environment and Natural Resources (DENR). The data contains spills reported to
the DENR since April of 2007.
UIC Underground Injection Control Wells
VERSION DATE: 04/01/17
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Order# 101912 Job# 223229 47 of 51

Environmental Records Definitions - STATE (NC)
This list of Underground Injection Control Wells is provided by the North Carolina Department of Environment
and Natural Resources.
UST Underground Storage Tanks
VERSION DATE: 01/12/18
This Registered Tanks Database is maintained by the North Carolina Department of Environment and Natural
Resources' Division of Waste Management. The Underground Storage Tank Section in this Division issues
permits, collects annual fees and handles requests for information for regulated and /or commercial underground
storage tanks. The section ensures compliance with all relevant state and federal laws, policies, rules and
regulations by assisting owners and operators in complying with operational standards (leak detection, spill and
overfill detection, etc.).
BF Brownfield Projects
VERSION DATE: 10/02/17
The North Carolina Brownfields Program, which is administered by the Division of Waste Management of the
Department of Environment and Natural Resources, works with prospective developers to place brownfields
sites back into reuse. A "brownfields site" is an abandoned, idled or underused property where the threat of
environmental contamination has hindered its redevelopment. The prospective developer, as defined by the
Brownfields Property Reuse Act of 1997, is any person who desires to buy or sell a brownfields property for the
purpose of redeveloping it and who did not cause or contribute to the contamination at the property.
DSCASITES Dry -Cleaning Solvent Cleanup Act Program Sites
VERSION DATE: 04/04/17
The Dry-cleaning Solvent Cleanup Act (DSCA) Program of the North Carolina Department of Environment and
Natural Resources was established to help fund the cleanup of contamination at dry cleaning sites. Participation
in the DSCA cleanup program is voluntary and is available to past and present facility owners, operators and
property owners of both active and former dry cleaning and wholesale solvent distribution facilities. DSCA also
established minimum management practices that all dry cleaning and wholesale solvent distribution facilities
must follow in order to prevent environmental contamination.
HISTLF Historic Landfills
VERSION DATE: NR
According to the Department of Environment and Natural Resources, Legislation in 2007 (SB1492) established a
program to address pre -regulatory landfills that closed prior to January 1, 1983 when waste disposal permitting
regulations commenced. This legislation adds new provisions to the Inactive Hazardous Sites Response Act for
addressing these landfills. The program will be implemented by the Pre -Regulatory Landfill Unit within the
Inactive Hazardous Sites Branch. This Pre-1983 landfill report contains only preliminary information and cannot
be relied on to be complete or accurate.
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Order# 101912 Job# 223229 48 of 51

Environmental Records Definitions - STATE (NC)
LAST Leaking Aboveground Storage Tanks
VERSION DATE: 10/13/17
This Regional Aboveground Storage Tanks Incident Management Database is maintained by the North Carolina
Department of Environment and Natural Resources' Division of Waste Management. The Corrective Action
Program oversees the assessment and cleanup of sites where releases to the environment have occurred.
LUST Leaking Underground Storage Tanks
VERSION DATE: 10/13/17
This Regional Underground Storage Tanks Incident Management Database (IMD) is maintained by the North
Carolina Department of Environment and Natural Resources' Division of Waste Management. The UST
Corrective Action Program in this Division oversees the assessment and cleanup of sites where releases to the
environment have occurred.
LUSTFUND State Trust Funds Database
VERSION DATE: 10/13/17
The North Carolina Department of Environment and Natural Resources' Underground Storage Tank Program
provides cleanup funds for reimbursement costs incurred during the cleanup of soil and groundwater
contamination resulting from a release of petroleum from an underground storage tank. Two funds, the
Commercial Trust Fund and the Noncommercial Trust Fund, have been established to reimburse tank owners,
operators, and landowners for costs associated with cleanups. Commercial underground storage tanks include
USTs containing petroleum products for resale, farm or residential motor fuel tanks with a capacity greater than
1,100 gallons, heating oil tanks greater than 1,100 gallons (unless they serve four or fewer households).
Noncommercial underground storage tanks include heating oil tanks with a capacity of 1,100 gallons or less,
heating oil tanks with a capacity greater than 1,100 gallons that serve one to four households, farm or residential
motor fuel tanks with a capacity of 1,100 gallons or less.
SWF Solid Waste Facilities
VERSION DATE: 09/28/17
The North Carolina Department of Environment and Natural Resources' Division of Waste Management provides
this list of solid waste permitted facilities.
VAP Voluntary Action Program Sites
VERSION DATE: 10/03/16
This listing includes sites from the Inactive Hazardous Sites Inventory with a Voluntary Action Under Agreement
status. The inventory is maintained by the Superfund Section of the Division of Waste Management in the North
Carolina Department of Environment and Natural Resources (DENR). The DENR defines "Inactive Hazardous
Sites" as areas where a hazardous substance release has come to be located and would include active and
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Order# 101912 Job# 223229 49 of 51

Environmental Records Definitions - STATE (NC)
inactive facilities and a variety of property types. The term "inactive" refers to the fact that cleanup was inactive at
large numbers of sites at the time of program enactment. If a party volunteers to clean up a site and enters into
an agreement with the Inactive Hazardous Sites Branch, the site is then transferred to the Voluntary Action
category.
HSDS Hazardous Substance Disposal Sites
VERSION DATE: 01/01/98
The North Carolina Department of Environment, Health, and Natural Resources, Division of Waste Management,
Superfund Section in cooperation with the North Carolina Center for Geographic Information and Analysis
(CGIA) developed the Hazardous Substance Disposal Sites data set, to enhance planning, siting, and impact
analysis in areas directly affected by Hazardous Substance Disposal Sites. This dataset identifies locations of
uncontrolled and unregulated, hazardous waste sites (formerly called superfund sites) in North Carolina, sites on
the CERCLA Information System (CERCLIS), the National Priorities List, the State Inactive Hazardous Sites List,
the Sites Priority List, and some Department of Defense sites. While efforts have been made to ensure that
these data are accurate and reliable within the state of the art, CGIA cannot assume liability for any damages or
misrepresentation caused by any inaccuracies in the data or as a result of changes to the data caused by
system transfers.
IHS Inactive Hazardous Sites
VERSION DATE: 12/15/17
The Inactive Hazardous Sites Inventory is maintained by the Superfund Section of the Division of Waste
Management in the North Carolina Department of Environment and Natural Resources (DENR). The DENR
defines "Inactive Hazardous Sites" as areas where a hazardous substance release has come to be located and
would include active and inactive facilities and a variety of property types. The term "inactive" refers to the fact
that cleanup was inactive at large numbers of sites at the time of program enactment. This inventory also
includes site status information for those sites listed on the October 2012 Report to the North Carolina General
Assembly as they are transferred to the Sites Priority List; to the Voluntary Action category; and/or after cleanup
is complete, to one of the "No Further Action" categories.
Geoearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223229 50 of 51

Environmental Records Definitions - TRIBAL
USTR04 Underground Storage Tanks On Tribal Lands
VERSION DATE: 10/14/16
Underground storage tanks on Tribal lands located in Region 4 include the following states: Alabama, Florida,
Georgia, Kentucky, Mississippi, North Carolina, South Carolina, and Tennessee.
LUSTR04 Leaking Underground Storage Tanks On Tribal Lands
VERSION DATE: 11/14/16
Leaking underground storage tanks on Tribal lands located in Region 4 include the following states: Alabama,
Florida, Georgia, Kentucky, Mississippi, North Carolina, South Carolina, and Tennessee.
ODINDIAN Open Dump Inventory on Tribal Lands
VERSION DATE: 11/08/06
This Indian Health Service database contains information about facilities and sites on tribal lands where solid
waste is disposed of, which are not sanitary landfills or hazardous waste disposal facilities, and which meet the
criteria promulgated under section 4004 of the Solid Waste Disposal Act (42 U.S.C. 6944).
INDIANRES Indian Reservations
VERSION DATE: 01/01/00
The Department of Interior and Bureau of Indian Affairs maintains this database that includes American Indian
Reservations, off -reservation trust lands, public domain allotments, Alaska Native Regional Corporations and
Recognized State Reservations.
Geoearch www.geo-search.com 888-396-0042
Order# 101912 Job# 223229 51 of 51

GepSearch
On time. On target. In touch:"
City Directory Target Property Address
Target Property:
1430 Riverside Dr,
Asheville, NC 28804
Prepared For:
Singleton Environmental Inc.
Order #: 101912
Project #: SEI-858
Date: 212012018
888-396-0042 www.geo-search.com
Page 1 of 5
2/20/2018 1:59:27 PM

City Directory Target Property Address
1430 Riverside Dr, Asheville, NC 28804
1 RIVERSIDE DR
1945 RANGE NOT LISTED- ENDS WITH 237 PIEDMONT ASHEVILLE
DIRECTORY, CO
1940 RANGE NOT LISTED- ENDS WITH 237 PIEDMONT ASHEVILLE
DIRECTORY, CO
1077 RIVERSIDE DR
1960
DONELL FRANCES B MRS
HILL DIRECTORY
ASHEVILLE
CO.
1960
X [JONESTOWN RD ENDS]
HILL DIRECTORY
ASHEVILLE
CO.
1955
BROWN ROBT L
PIEDMONT
ASHEVILLE
DIRECTORY, CO
1955
X [JONESTOWN RD ENDS]
PIEDMONT
ASHEVILLE
DIRECTORY, CO
1950
BROWN ROBT L
PIEDMONT
ASHEVILLE
DIRECTORY, CO
1950
X [JONESTOWN RD ENDS]
PIEDMONT
ASHEVILLE
DIRECTORY, CO
1083 RIVERSIDE DR
1970 RICE PAUL HILL DIRECTORY ASHEVILLE
CO.
1970 X [JONESTOWN RD ENDS] HILL DIRECTORY ASHEVILLE
CO.
1125 RIVERSIDE DR
1975 GARREN BONNIE G MRS HILL DIRECTORY ASHEVILLE
CO.
1975 X [JONESTOWN RD ENDS] HILL DIRECTORY ASHEVILLE
CO.
1965 GARREN FORREST B HILL DIRECTORY ASHEVILLE
CO.
1201 RIVERSIDE DR
2016
CHURCH -THE REDEEMER EPISCOPAL
R.L.
POLK & CO.
ASHEVILLE
[CHURCHES]
2016
X [PINEY HILL RD INTS]
R.L.
POLK & CO.
ASHEVILLE
2011
CHURCH -THE REDEEMER EPISCOPAL
R.L.
POLK & CO.
ASHEVILLE
[CHURCHES]
2005
CHURCH -THE REDEEMER EPISCOPAL
R.L.
POLK & CO.
ASHEVILLE
[CHURCHES]
2005
X [PIG HILL RD INTS]
R.L.
POLK & CO.
ASHEVILLE
2005
Y [OLD LEICESTER HWY BEGINS]
R.L.
POLK & CO.
ASHEVILLE
2005
Z [W CITY VIEW DR INTS]
R.L.
POLK & CO.
ASHEVILLE
888-396-0042
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City Directory Target Property Address
1430 Riverside Dr, Asheville, NC 28804
2002
CHURCH OF THE REDEEMER EPISCOPAL
R.L. POLK & CO.
GREATER
ASHEVILLE AND
VICINITY
1996
EPISCOPAL CHURCH OF THE REDEMEER
R.L. POLK & CO.
ASHEVILLE
1990
EPISCOPAL CHURCH OF THE REDEEMER
R.L. POLK & CO.
ASHEVILLE
1985
ESPISCOPAL CHURCH OF THE REDEEMER
R.L. POLK & CO.
ASHEVILLE
1980
EPISCOPAL CHURCH OF THE REDEEMER
HILL DIRECTORY
ASHEVILLE
CO.
1980
X [JONESTOWN RD ENDS]
HILL DIRECTORY
ASHEVILLE
CO.
2005
TRANSPORTATION -LAND SCAPE DEPT
R.L.
POLK & CO.
ASHEVILLE
[ROAD BUILDING CONTRACTORS]
1407 RIVERSIDE DR
2016
N C DOT-DIV-HWY BRIDGE IN
R.L.
POLK & CO.
ASHEVILLE
[GOVERNMENT OFFICES -STATE]
2011
N C DOT-DIVISION-HWY BRIDGE IN
R.L.
POLK & CO.
ASHEVILLE
[GOVERNMENT OFFICES -STATE]
1415 RIVERSIDE DR
2016
JONES FRED B JR & DIANE E
R.L.
POLK & CO.
ASHEVILLE
2011
JONES FRED B
R.L.
POLK & CO.
ASHEVILLE
2005
JONES FRED B
R.L.
POLK & CO.
ASHEVILLE
2005
NEW LIFE COMMUNITY CHURCH
R.L.
POLK & CO.
ASHEVILLE
[CHURCHES]
2002
JONES FRED B
R.L.
POLK & CO.
GREATER
ASHEVILLE AND
VICINITY
1417 RIVERSIDE DR
2016
NEW LIFE OF ASHEVILLE [CHURCHES]
R.L.
POLK & CO.
ASHEVILLE
2016
WINCE KATHLEEN
R.L.
POLK & CO.
ASHEVILLE
2011
NEW LIFE COMMUNITY CHURCH
R.L.
POLK & CO.
ASHEVILLE
[CHURCHES]
1421 RIVERSIDE DR
2016
FREESE SHAUN P & ANITA H
R.L.
POLK & CO.
ASHEVILLE
2011
FREESE SHAUN P & ANITA H
R.L.
POLK & CO.
ASHEVILLE
2005
FREESE SHAUN P & ANITA H
R.L.
POLK & CO.
ASHEVILLE
1425 RIVERSIDE DR
2005
ROBERTS PAUL D
R.L.
POLK & CO.
ASHEVILLE
888-396-0042
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www.geo-search.com

City Directory Target Property Address
1430 Riverside Dr, Asheville, NC 28804
1430 RIVERSIDE DR
2011 LEDFORD CONNIE R R.L. POLK & CO. ASHEVILLE
2005 WOODFIN AUTO & SALVAGE [AUTO PARTS. R.L. POLK & CO. ASHEVILLE
USED & REBUILT]
2002 WESTERN CAROLINA RECYCLING R.L. POLK & CO. GREATER
ASHEVILLE AND
VICINITY
1444 RIVERSIDE DR
2016
CRAGGY MOTORS [AUTO GLASS-SERV &
R.L.
POLK & CO.
ASHEVILLE
INSTALLATION]
2011
CRAGGY MOTORS [GLASS]
R.L.
POLK & CO.
ASHEVILLE
2005
CRAGGY MOTORS [AUTO BODY-RPR &
R.L.
POLK & CO.
ASHEVILLE
PAINTING]
2002
CRAGGY MOTORS
R.L.
POLK & CO.
GREATER
ASHEVILLE AND
VICINITY
1996
CRAGGY MOTORS
R.L.
POLK & CO.
ASHEVILLE
1475 RIVERSIDE DR
2016
MEADOWS TRANSMISSION [AUTO RPR &
R.L.
POLK & CO.
ASHEVILLE
SERV]
2011
MEADOWS TRANSMISSION SVC [AUTO
R.L.
POLK & CO.
ASHEVILLE
RPR & SERV]
2005
MEADOWS TRANSMISSION
R.L.
POLK & CO.
ASHEVILLE
[TRANSMISSIONS -AUTO]
1476 RIVERSIDE DR
2016
BLUE RIDGE CAF? [RESTAURANTS]
R.L.
POLK & CO.
ASHEVILLE
2005
WYATT WASTE CONTAINER [GARABE
R.L.
POLK & CO.
ASHEVILLE
COLLECTION]
2002
WYATT WASTE CONTAINER
R.L.
POLK & CO.
GREATER
ASHEVILLE AND
VICINITY
2002
WYATT WASTE CONTAINER
R.L.
POLK & CO.
GREATER
ASHEVILLE AND
VICINITY
1480 RIVERSIDE DR
2016
WALDROP'S GROCERY [GROCERS -RETAIL:
R.L.
POLK & CO.
ASHEVILLE
2016
X [OLD LEICESTER HWY INTS]
R.L.
POLK & CO.
ASHEVILLE
2016
Y [W CITY VIEW DR INTS]
R.L.
POLK & CO.
ASHEVILLE
2011
WALDROP'S GROCERY [GROCERS -RETAIL:
R.L.
POLK & CO.
ASHEVILLE
2011
X [OLD LEICESTER HWY INTS]
R.L.
POLK & CO.
ASHEVILLE
888-396-0042
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City Directory Target Property Address
1430 Riverside Dr, Asheville, NC 28804
2011
Y [W CITY VIEW DR INTS]
R.L.
POLK & CO.
ASHEVILLE
2005
FOX JOHN W
R.L.
POLK & CO.
ASHEVILLE
2005
FOX CALLIE L
R.L.
POLK & CO.
ASHEVILLE
2005
X [7TH ST ENDS]
R.L.
POLK & CO.
ASHEVILLE
2005
Y [RAILROAD CROSSES]
R.L.
POLK & CO.
ASHEVILLE
1996
WALDROP'S GROCERY
R.L.
POLK & CO.
ASHEVILLE
1501 RIVERSIDE DR
2016
NO CURRENT LISTING
R.L.
POLK & CO.
ASHEVILLE
2011
TYLER BRITT A
R.L.
POLK & CO.
ASHEVILLE
2011
X [RIVER WALK DR INTS]
R.L.
POLK & CO.
ASHEVILLE
2005
FOX JOHN W
R.L.
POLK & CO.
ASHEVILLE
2005
FOX CALLIE L
R.L.
POLK & CO.
ASHEVILLE
2002
FOX C L
R.L.
POLK & CO.
GREATER
ASHEVILLE AND
VICINITY
1909 RIVERSIDE DR
1996
GRACE FELLOWSHIP BAPTIST CHURCH
R.L.
POLK & CO.
ASHEVILLE
1996
X [NORTON ST INTS]
R.L.
POLK & CO.
ASHEVILLE
1990
GRACE FELLOWSHIP BAPTIST CHURCH
R.L.
POLK & CO.
ASHEVILLE
1985
GRACE FELLOWSHIP BAPTIST CHURCH
R.L.
POLK & CO.
ASHEVILLE
1980
FRYE JOHN F
HILL DIRECTORY
ASHEVILLE
CO.
2000 RIVERSIDE DR
1975
BURLINGTON INDUSTRIES ASHEVILLE
HILL DIRECTORY
ASHEVILLE
PLANT [COTTON GDS]
CO.
1970
BURLINGTON INDUSTRIES ASHEVILLE
HILL DIRECTORY
ASHEVILLE
PLANT
CO.
1965
ASHEVILLE MILL DIVISION OF
HILL DIRECTORY
ASHEVILLE
BURLINGTON INDUSTRIES COTTON GDS
CO.
1960
ASHV MILL DIV OF BURLINGTON
HILL DIRECTORY
ASHEVILLE
INDUSTRIES COTTON GDS]
CO.
1955
MARTEL MILLS CORP [COTTON GDS
PIEDMONT
ASHEVILLE
MFRS]
DIRECTORY, CO
1950
MARTEL MILLS CORP [COTTON GDS
PIEDMONT
ASHEVILLE
MFRS]
DIRECTORY, CO
Comment: Listed in Asheville not Woodfin.
888-396-0042
Page 5 of 5
2/20/2018 1:59:30 PM
www.geo-search.com

GegpSearch
On time. On target. In touch:"
FIM Abstract
Target Property:
Woodfin Auto & Salvage Brownfields Property
1430 Riverside Dr
Woodfin, Buncombe County, North Carolina 28804
Prepared For:
Singleton Environmental Inc.
Order #: 101912
Job #: 223231
Project #: SEI-858
Date: 0211912018
phone: [phone] • fax: [phone] • www.geo-search.com

Woodfin Auto & Salvage Brownfields Property
1430 Riverside Dr
Woodfin, Buncombe County, North Carolina 28804
USGS Quadrangle: Weaverville, NC
Target Property Geometry:Point
Target Property Longitude (s)/Latitude (s):
(-82.600534, 35.626104)
County/Parish Covered:
Buncombe (NC)
Zipcode(s) Covered:
Asheville NC: 28804, 28806
State(s) Covered:
NC
*Target property is located in Radon Zone 1.
Zone 1 areas have a predicted average indoor radon screening level greater than 4 pCi/L
(picocuries per liter).
Disclaimer - The information provided in this report was obtained from a variety of public sources. GeoSearch cannot ensure and makes no
warranty or representation as to the accuracy, reliability, quality, errors occurring from data conversion or the customer's interpretation of
this report. This report was made by GeoSearch for exclusive use by its clients only. Therefore, this report may not contain sufficient
information for other purposes or parties. GeoSearch and its partners, employees, officers and independent contractors cannot be held
liable for actual, incidental, consequential, special or exemplary damages suffered by a customer resulting directly or indirectly from any
information provided by GeoSearch.
GeQSearch www.geo-search.com • phone: [phone] • fax: [phone]

GegpSearch FIM
Date: 02/19/18
GS Job Number: 101912
Company Name: Singleton Environmental Inc.
Project Number: SEI-858
Site Information: Woodfin Auto & Salvage Brownfields Property
1430 Riverside Dr, Woodfin, Buncombe, North Carolina, 28804
The collections of fire insurance maps listed below were reviewed according to the site
information supplied by client. Based on the information provided, no coverage is available.
Library of Congress
University Publications of America
Other Libraries (universities, state, local, etc.).
Disclaimer — The information in this report was obtained from a variety of public sources. GeoSearch cannot insure or makes no warranty or
representation as to the accuracy, reliability, quality, errors occurring from data conversion or the customers interpretation of this report. Therefore,
this report may not contain sufficient information for other purposes or parties. GeoSearch and its partners, employees, officers and independent
contractors cannot be held liable for actual, incidental, consequential, special or exemplary damages suffered by a customer resulting directly or
indirectly from any information provided by GeoSearch.
888-396-0042 * FAX [phone] * www.Geo-Search.com

APPENDIX E
Questionnaires

ASTM E1527-13
Phase I Environmental Site Assessment
User Questionnaire
INTRODUCTION
In order to qualify for one of the Landowner Liability Protections (LLPs/ offered by the Small
Business Liability Relief and Brownfields Revitalization Act of 2001 (the 'Brownfields
Amendments"), z the user must conduct the following inquiries required by 40 CFR 312.25,
312.28, 312.29, 312.30, and 312.31. These inquiries must also be conducted by EPA
Brownfield Assessment and Characterization grantees. The user should provide the following
information to the environmental professional. Failure to conduct these inquiries could result in a
determination that "a// appropriate inquiries" is not complete.
(1.) Environmental liens that are filed or recorded against the property (40 CFR 312.25).
Did a search of recorded land title records (orjudicial records where appropriate, see Note 1
below) identify any environmental liens filed or recorded against the property under federal,
tribal, state or local law?
No
(2.) Activity and use limitations that are in place on the property or that have been filed or
recorded against the property (40 CFR 312.26(a)(1)(v) and vi)).
Did a search of recorded land title records (orjudicial records where appropriate, see Note 1
above) identify any AULs, such as engineering controls, land use restrictions or institutional
controls that are in place at the property and/or have been filed or recorded against the property
under federal, tribal, state or local law?
No
(3.) Specialized knowledge or experience of the person seeking to qualify for the LLP (40
CFR 312.28).
Do you have any specialized knowledge or experience related to the property or nearby
properties? For example, are you involved in the same line of business as the current or former
occupants of the property or an adjoining property so that you would have specialized
knowledge of the chemicals and processes used by this type of business?
No
(4.) Relationship of the purchase price to the fair market value of the property if it were
Page 1of3

ASTM E1527-13
Phase (Environmental Site Assessment
User Questionnaire
Does the purchase price being paid for this property reasonably reflect the fair market value of
the property? If you conclude that there is a difference, have you considered whether the lower
purchase price is because contamination is known or believed to be present at the property?
YC15
(5.) Commonly known or reasonably ascertainable information about the property (40
CFR 312.30).
Are you aware of commonly known or reasonably ascertainable information about the property
that would help the environmental professional to identify conditions indicative of releases or
threatened releases?
Yes
For example,
(a.) Do you know the past uses of the property? Yee 1+ S Ot�Ce '1�Q 6� O� C. CGr
(b.) Do you know of specific chemicals that are present or once were present ::3I the property?
Iv C)
(c.) Do you know of spills or other chemical releases that have taken place at the property?
lv�
(d.) Do you know of any environmental cleanups that have taken place at the property?
NO
(6.) The degree of obviousness of the presence or likely presence of contaminabn at the
property, and the ability to detect the contamination by appropriate investigation (40 CFR
312.31).
Based on your knowledge and experience related to the property are there any obvious
indicators that point to the presence or likely presence of releases at the property?
O
In addition, certain information should be collected, if available, and provided to the
environmental professional conductingthe Phase /Environmental SiteAssessment. This
Page 2 of 3

ASTM E1527-13
Phase IEnvironmentalSite Assessment
User Questionnaire
information is intended to assist the environmental professional, but is not necessarily
required to qualify for one of the LLPs. The information includes:
(a) the reason why the Phase I is being performed, P�QV•w.s k�O
(b) the type of property and type of property transaction, for example, sale, purchase, exchange, etc., 7JC
(c) the complete and correct address for the property (a map or other do umentation showing
property location and boundaries is helpful), 1420 ♦ 1430 (L;�s;jC Dr
(d) the scope of services desired for the Phase I (including whether any parties to the property
transaction may have a required standard scope of services or whether any considerations beyond
the requirements of Practice El 527 are to be considered) , ee
(e) identification of all parties who will rely on the Phase I report, F,,e^ . �oad� Zkrx NCJevn �bE Q
(0 identification of the site contact and how the contact can be reached, Wlw %e;C,r $2$.'113. Rl13y
(g) any special terms and conditions which must be agreed upon by the environmental
professional, and
(h) any other knowledge or experience with the property that may be pertinent to the environmental
professional (for example, copies of any available prior environmental site assessment reports,
documents, correspondence, etc., concerning the property and is environmental condition).
The USER QUESTIONNAIRE was completed by:
Narne ADate V2011-6
User represents that to the best of the user's knowledge the above statements and facts are true
and correct, and, to the best of the user's knowledge, no material facts have been suppressed or
misstated.
Page 3 of 3

APPENDIX F
Limited Phase II ESAs

LIMITED PHASE II
ENVIRONMENTAL SITE
ASSESSMENT REPORT
For The
Former Auto Crusher Facility
1420 Riverside Drive
Woodfin, NC 28804
PROJECT # SEI-783
PREPARED FOR:
French Broad River Academy
2000 Riverside Drive
Woodfin, NC 28804
PREPARED BY. -
Singleton Environmental, Inc.
PO BOX 2012
Enka, NC 28728
[phone]
June 27, 2017
SIN LETON ENVIRONMENTAL,, INC

Soil Assessment Report
June 27, 2017
UST Incident Number: NA
Facility ID Number: NA
Site Name & Address:
Consultant/Contractor:
Analytical Laboratory:
Date Release Discovered:
Estimated Quantity of Release:
Cause/Source of Release:
Size & Contents of UST System:
Geographical Data Point:
Latitude:
Longitude:
Location Method:
Former Auto Crusher Facility
1420 Riverside Drive
Woodfin, Buncombe County, NC 28804
Singleton Environmental, Inc.
PO Box 2012
Enka, NC 28728
Telephone: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Not Applicable
Not Applicable
Not Applicable
Not Applicable
Not Applicable
35.6258° North
-82.6005' West
Google Earth
Signature and Seal of Certifying Professional Geologist:
I, Christopher D. Singleton, a North Carolina P,Ofe*jal Geologist, do certify that the
information contained in this report is correc ' e best of my knowledge.
'- AL .
ChristV , P.G. #1928
Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The
certification number of the company is C-443.

TABLE OF CONTENTS
Introduction..................................................................................................................................... 1
SoilAssessment Field Work...................................................................................................... 1
SiteGeology............................................................................................................................... 2
LaboratoryAnalysis................................................................................................................... 2
Conclusion................................................................................................................................. 2
ClosingStatements..................................................................................................................... 3
Signature.................................................................................................................................... 3
Table
Table 1: Soil Analytical Results
Figures
Figure l : 7.5' USGS Topographic Map
Figure 2: Site Map
Appendices
Appendix A: Laboratory Analytical Report and Chain of Custody Documentation

INTRODUCTION
Singleton Environmental, Inc. (SEI) was contracted to perform a Limited Phase II
Environmental Site Assessment for a former auto crusher facility located at 1420
Riverside Drive in Woodfin, North Carolina. The soil assessment was requested to
determine if any environmental impacts were found on the property as a result of its past
use. The property subject to this investigation is being considered as an addition to the
French Broad River Academy.
The focus of this Soil Assessment is to assess whether the soil contains contaminants that
could prevent the purchase of the property for use as a school. Field work for this
assessment was completed on June 14, 2017. Soil samples were delivered to Pace
Analytical located in Asheville, North Carolina for analysis of volatile organic
compounds (VOCs), semi -volatile organic compounds (SVOCs) and 8 RCRA Metals.
ASSESSMENT FIELD WORK
The soil samples were collected using a Giddings direct push drill rig. The drilling was
performed by Chris Singleton with SEI, a North Carolina licensed drilling contractor. A
total of ten (10) soil borings were advanced at the site resulting in the collection of six (6)
soil samples. The soil borings were advanced in a predetermined pattern inside the
property boundaries where the most evidence of crushing activities was apparent. Auger
refusal was encountered at each soil boring location at depths ranging between 2 to 4 feet.
The soil samples were collected at depths ranging from 1 to 2 feet. Figure 1 shows the
locations of the soil boring/sample collection sites. Table 1 shows the laboratory analysis
and the sample depths.
The Giddings® system used at the site consists of a series of hydraulically -pushed tools
which collect samples at continuous intervals to a predetermined depth. During soil
sampling, the 4-foot soil macro sampler can be advanced into the subsurface to a
predetermined depth. The locking probe point is then released and the sample tube is then
pushed to the terminal depth. The soil sample is retained within a clear plastic liner. The
sampling apparatus is then withdrawn to the surface upon completion of probing. The soil
can remain in the plastic liner or be removed for analysis and field screening. In this case,
upon removal of the sample tube and liner, the sample was screened using a PID,
collected from the liner and placed in EPA approved sample containers.
SITE GEOLOGY
The site is located within the Blue Ridge Geologic Belt. According to the Geologic Map
of North Carolina, the site is located within the Ashe Metamorphic Suite and Tallulah
Falls Formation formation (Zatm) of the Blue Ridge Belt of North Carolina. The bedrock
underlying the site is muscovite-biotite gneiss and is locally sulfidic; interlayed and
gradational with mica schist, minor amphibolite, and horneblende gneiss.

The surficial soils at the site consist of loamy sands mixed with auto parts and fluids. The
soil drainage class is well drained soil while also being occasionally flooded. Soils have a
low water holding capacity. Depth to groundwater is undetermined at the site due to the
shallow refusal.
LABORATORY ANALYSIS
The soil samples collected on -site were submitted to Pace Analytical, a North Carolina
certified analytical laboratory. Soil samples SB-1 through SB-6 were analyzed for
Volatile Organic Compounds (VOCs), semi -Volatile Organic Compounds (SVOCs), and
8 RCRA Metals to determine if the samples contained any compounds exceeding the
North Carolina Department of Environmental Quality (NCDEQ) Soil -to -Groundwater
criteria, Residential or Commercial Maximum Soil Contaminant Concentrations
(MSCCs) listed in the April 2016 Preliminary Soil Remediation Goals.
Several VOC, SVOC and metal concentrations in each sample exceeded the soil -to -
groundwater MSCCs. Concentrations of benzene in SB-1 exceeded the residential
MSCCs. Concentrations of lead in samples SB-2 and SB-5 also exceeded the residential
MSCCs. Concentrations of arsenic exceeded the commercial MSCCs in all sample
locations. Concentrations of lead also exceeded the commercial MSCCs in samples SB-
1, SB-3, and SB-6.
Please see Table 1 for all summarized soil sampling results and Figure 2 for the
corresponding sampling locations. The laboratory analytical results packages are
attached to this report in Appendix A.
CONCLUSIONS
Based on the results of the soil analysis on the property, this report needs to be submitted
to the NCDEQ-UST Section Asheville Regional Office for further direction.
CLOSING STATEMENTS
This work was performed in general accordance with existing geological and
environmental standards of practice currently existing. The results found herein are
limited to the specific site and the boring locations as shown on the attached diagram.
However, it is a well know fact that variations in both geology and hydrogeology may
occur across the site between boring locations. It is also a well-known fact that changes in
groundwater and subsurface conditions can and do occur through time. These chiefly are
regarding groundwater flow and velocity, groundwater elevations and changes in
groundwater quality at various locations on a given site. The conclusions drawn from the
data presented in this report as well as the reporting methodology are in general
accordance with the existing standards and accepted hydrogeologic and environmental
engineering practices in use at the current time. Should, at some point in the future,
changes occur which require revision of this report or the conclusions drawn from it, we

reserve the right to make the necessary changes given the data showing the changes and
conditions and revise the conclusions drawn from the data as may be required.
SIGNATURE AND SEAL OF PROFESSIONAL GEOLOGIST:
I, Christopher D. Singleton, a Professional Geologist, do certify that the information
contained in this report is correct and accuratga;`,� of my knowledge.
P.G. #1928
s

Volatile
(EPA Me
8 RCRA
(EPA Me
TABLE 1
SOIL ANALYTICAL RESULTS
1420 Riverside Drive
Woodfin, North Carolina
S13-1
6/14/2017
1 -2 ft-bsg
& Semi -Volatile Organic Compounds
thods 8260 & 8270)
Benzene
n-Butylbenzene
SB-2
6/14/2017
1 -2 ft-bsg
0.25
SB-3
6/14/2017
1 -2 ft-bsg
1.5
4.4
S113-4
6/14/2017
1 -2 ft-bsg
S113-5
6/14/2017
1 -2 ft-bsg
S113-6
6/14/2017
1 -2 ft-bsg
Non -Detect
Soil-to-GW
Max Soil Cont.
Level
(mg/kg)
Residen '
Max Soil Cont.
Level
(mg/kg)
Max Soil Cont.
Level
(mg/kg)
0.0056
4.3
626
164
16,350
sec-Butylbenzene
2.3
0.083
0.073
3.3
626
16,350
Ethylbenzene
63.7
2.2
3.9
4.9 1
1,560
40,000
Isopropylbenzene
6.5
0.15
0.5
0.1
1.7
1,564
40,880
p-Isopropyltoluene
6.1
0.2
1.7
1.8
0.12
100
4,000
Naphthalene
24.5
4
6.9
0.16
313
8,176
n-Propylbenzene
25.2
1.1
1.5
2.4
1.7
626
16,350
Tetrachloroethene
0.36
0.0074
1.1
10
Toluene
204
6.3
7.7
7.6
4.3
1,200
32,000
1,2,3-Trichloropropane
49.3
14.6
N/A
N/A
N/A
1,2,4-Trimethyl benzene
155
8.2
28.2
39.4
8.5
782
20,440
1,3,5-Trimethyl benzene
50.2
2.6
12.2
14.9
8.3
782
20,440
Total Xylenes
329
12.8
48.1
48.7
4.6
3,129
81,760
Anthracene
4.5
940
4,600
122,000
bis(2-Ethylhexyl)phthalate
7.2
6.6
46
410
Flouranthene
16
290
620
16,400
2-Methylnaphthalene
6.5
4.7
3.6
63
1,635
Naphthalene
6.8
3.7
0.16
313
8,176
Phenanthrene
18
56
469
12,264
Pyrene
9.5
270
469
12,264
Metals
thods 6010 & 7471)
Arsenic
Barium
136
176
226
109
97
138
0.68
31
N/A
469
12264
Cadmium
2.7
5.1
6.9
0.17
3.2
4.1
N/A
N/A
N/A
Chromium
Lead
Selenium
22.3
ND
44.3
ND
57.8
ND
7.2
74.1
ND
39.7
ND
41.0
ND
5.4
270
N/A
47
N/A
1226
N/A
Silver
ND
0.86
3.6
ND
0.84
1
78
N/A
1,160
Mercury
0.025
0.12
0.18
0.02
0.17
0.16
2.2
N/A
3.3
Note: 1. Bolded values indicate concentrations which have exceeded at least one maximum allowable
soil concentration. Bolded standards indicate those which have been exceeded.
2. ND = Non -Detect
3. N/A = Not Applicable

FIGURES

••11 �
i 1 �
f�
' B
fl
SB-6 _ + SB-3
-- a SB-1
k 'T�.�
SB-2 '� 8B•
_
1 —
LEGEND:
SOIL SAMPLE LOCATIONS © SHRUB
WATER WELL NORTH
TREE
SCALE (f-t"`)��L✓✓✓
DRAWN BY: C. Singleton
FIGURE 2
o �s so CHECKED BY: C. SINGLETON 1420 Riverside Drive
SINGLETON ENVIRONMENTAL, INC Asheville, Buncombe County, NC
UST SYSTEM
(Tank Pit, Product Lines, etc.)

APPENDIX A

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
June 21, 2017
Chris Singleton
Singleton Environmental
P.O. Box 2012
Enka, NC 28728
RE: Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on June 14, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Revised Report. Units revised on 8260 and 8270.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
--F>�
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
1420 Riverside Dr.
92344137
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92344137001
S13-1
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92344137002
S13-2
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92344137003
S13-3
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92344137004
S13-4
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92344137005
S13-5
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92344137006
S13-6
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 55

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-1 Lab ID: 92344137001 Collected: 06/14/17 09:30 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
8.4
mg/kg
0.70
1
06/15/17 17:15
06/20/17 02:11
7440-38-2
Barium
136
mg/kg
0.35
1
06/15/17 17:15
06/20/17 02:11
7440-39-3
Cadmium
2.7
mg/kg
0.070
1
06/15/17 17:15
06/20/17 02:11
7440-43-9
Chromium
22.3
mg/kg
0.35
1
06/15/17 17:15
06/20/17 02:11
7440-47-3
Lead
443
mg/kg
0.35
1
06/15/17 17:15
06/20/17 02:11
7439-92-1
Selenium
ND
mg/kg
0.70
1
06/15/17 17:15
06/20/17 02:11
7782-49-2
Silver
ND
mg/kg
0.35
1
06/15/17 17:15
06/20/17 02:11
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.025
mg/kg
0.0049
1
06/14/17 16:09
06/15/17 08:07
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
83-32-9
Acenaphthylene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
208-96-8
Aniline
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
62-53-3
Anthracene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
120-12-7
Benzo(a)anthracene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
56-55-3
Benzo(a)pyrene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
207-08-9
Benzoic Acid
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
65-85-0
Benzyl alcohol
ND
mg/kg
7.8
10
06/15/17 09:19
06/16/17 17:32
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
101-55-3
Butylbenzylphthalate
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
7.8
10
06/15/17 09:19
06/16/17 17:32
59-50-7
4-Chloroaniline
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
111-44-4
2-Chloronaphthalene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
91-58-7
2-Chlorophenol
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
7005-72-3
Chrysene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
53-70-3
Dibenzofuran
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
91-94-1
2,4-Dichlorophenol
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
120-83-2
Diethylphthalate
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
84-66-2
2,4-Dimethylphenol
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
105-67-9
Dimethylphthalate
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
131-11-3
Di-n-butylphthalate
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
7.8
10
06/15/17 09:19
06/16/17 17:32
534-52-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 55

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ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-1
Lab ID: 92344137001 Collected: 06/14/17 09:30
Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
606-20-2
Di-n-octylphthalate
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
117-84-0
bis(2- Ethyl hexyl)phthalate
7.2
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
117-81-7
Fluoranthene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
206-44-0
Fluorene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
87-68-3
Hexachlorobenzene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
77-47-4
Hexachloroethane
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
193-39-5
Isophorone
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
78-59-1
1-Methylnaphthalene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
90-12-0
2-Methylnaphthalene
6.5
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
15831-10-4
Naphthalene
6.8
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
91-20-3
2-Nitroaniline
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
88-74-4
3-Nitroaniline
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
99-09-2
4-Nitroaniline
ND
mg/kg
7.8
10
06/15/17 09:19
06/16/17 17:32
100-01-6
Nitrobenzene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
98-95-3
2-Nitrophenol
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
88-75-5
4-Nitrophenol
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
108-60-1
Pentachlorophenol
ND
mg/kg
19.4
10
06/15/17 09:19
06/16/17 17:32
87-86-5
Phenanthrene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
85-01-8
Phenol
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
108-95-2
Pyrene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
3.9
10
06/15/17 09:19
06/16/17 17:32
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
06/15/17 09:19
06/16/17 17:32
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
06/15/17 09:19
06/16/17 17:32
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
06/15/17 09:19
06/16/17 17:32
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
06/15/17 09:19
06/16/17 17:32
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
06/15/17 09:19
06/16/17 17:32
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
06/15/17 09:19
06/16/17 17:32
118-79-6
S4
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
3.9
25
06/15/1714:32
67-64-1
Benzene
22.8
mg/kg
7.7
1000
06/16/1715:39
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 55

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-1 Lab ID: 92344137001 Collected: 06/14/17 09:30 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.19
25
06/15/17 14:32
108-86-1
Bromochloromethane
ND
mg/kg
0.19
25
06/15/17 14:32
74-97-5
Bromodichloromethane
ND
mg/kg
0.19
25
06/15/17 14:32
75-27-4
Bromoform
ND
mg/kg
0.19
25
06/15/17 14:32
75-25-2
Bromomethane
ND
mg/kg
0.39
25
06/15/17 14:32
74-83-9
2-Butanone (MEK)
ND
mg/kg
3.9
25
06/15/17 14:32
78-93-3
n-Butylbenzene
ND
mg/kg
0.19
25
06/15/17 14:32
104-51-8
sec-Butylbenzene
2.3
mg/kg
0.19
25
06/15/17 14:32
135-98-8
tert-Butyl benzene
ND
mg/kg
0.19
25
06/15/17 14:32
98-06-6
Carbon tetrachloride
ND
mg/kg
0.19
25
06/15/17 14:32
56-23-5
Chlorobenzene
ND
mg/kg
0.19
25
06/15/17 14:32
108-90-7
Chloroethane
ND
mg/kg
0.39
25
06/15/17 14:32
75-00-3
Chloroform
ND
mg/kg
0.19
25
06/15/17 14:32
67-66-3
Chloromethane
ND
mg/kg
0.39
25
06/15/17 14:32
74-87-3
2-Chlorotoluene
ND
mg/kg
0.19
25
06/15/17 14:32
95-49-8
4-Chlorotoluene
ND
mg/kg
0.19
25
06/15/17 14:32
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.19
25
06/15/17 14:32
96-12-8
Dibromochloromethane
ND
mg/kg
0.19
25
06/15/17 14:32
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.19
25
06/15/17 14:32
106-93-4
Dibromomethane
ND
mg/kg
0.19
25
06/15/17 14:32
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.19
25
06/15/17 14:32
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.19
25
06/15/17 14:32
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.19
25
06/15/17 14:32
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.39
25
06/15/17 14:32
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.19
25
06/15/17 14:32
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.19
25
06/15/17 14:32
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.19
25
06/15/17 14:32
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.19
25
06/15/17 14:32
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.19
25
06/15/17 14:32
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.19
25
06/15/17 14:32
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.19
25
06/15/17 14:32
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.19
25
06/15/17 14:32
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.19
25
06/15/17 14:32
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.19
25
06/15/17 14:32
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.19
25
06/15/17 14:32
10061-02-6
Diisopropyl ether
ND
mg/kg
0.19
25
06/15/17 14:32
108-20-3
Ethylbenzene
63.7
mg/kg
7.7
1000
06/16/1715:39
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.19
25
06/15/17 14:32
87-68-3
2-Hexanone
ND
mg/kg
1.9
25
06/15/17 14:32
591-78-6
Isopropylbenzene (Cumene)
6.5
mg/kg
0.19
25
06/15/17 14:32
98-82-8
p-Isopropyltoluene
6.1
mg/kg
0.19
25
06/15/17 14:32
99-87-6
Methylene Chloride
ND
mg/kg
0.77
25
06/15/17 14:32
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
1.9
25
06/15/17 14:32
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.19
25
06/15/17 14:32
1634-04-4
Naphthalene
24.5
mg/kg
7.7
1000
06/16/1715:39
91-20-3
n-Propylbenzene
25.2
mg/kg
7.7
1000
06/16/1715:39
103-65-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 55

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-1 Lab ID: 92344137001 Collected: 06/14/17 09:30 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 06/21 /2017 08:13 AM
Analytical Method: EPA 8260
ND
mg/kg
0.19
25
06/15/1714:32
100-42-5
ND
mg/kg
0.19
25
06/15/1714:32
630-20-6
ND
mg/kg
0.19
25
06/15/1714:32
79-34-5
0.36
mg/kg
0.19
25
06/15/1714:32
127-18-4 L2
204
mg/kg
7.7
1000
06/16/1715:39
108-88-3
ND
mg/kg
0.19
25
06/15/1714:32
87-61-6
ND
mg/kg
0.19
25
06/15/1714:32
120-82-1
ND
mg/kg
0.19
25
06/15/1714:32
71-55-6
ND
mg/kg
0.19
25
06/15/1714:32
79-00-5
ND
mg/kg
0.19
25
06/15/1714:32
79-01-6
ND
mg/kg
0.19
25
06/15/1714:32
75-69-4
49.3
mg/kg
7.7
1000
06/16/1715:39
96-18-4
155
mg/kg
7.7
1000
06/16/1715:39
95-63-6
50.2
mg/kg
7.7
1000
06/16/1715:39
108-67-8
ND
mg/kg
1.9
25
06/15/1714:32
108-05-4
ND
mg/kg
0.39
25
06/15/1714:32
75-01-4
329
mg/kg
15.4
1000
06/16/1715:39
1330-20-7
230
mg/kg
15.4
1000
06/16/1715:39
179601-23-1
98.8
mg/kg
7.7
1000
06/16/1715:39
95-47-6
83
%
70-130
25
06/15/1714:32
2037-26-5
143
%
70-130
25
06/15/1714:32
460-00-4 S1
261
%
70-132
25
06/15/1714:32
17060-07-0 S1
Analytical Method: ASTM D2974-87
14.9 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/17 07:25
Page 7 of 55

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-2 Lab ID: 92344137002 Collected: 06/14/17 10:10 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
10.1
mg/kg
0.74
1
06/15/17 17:15
06/20/17 02:14
7440-38-2
Barium
176
mg/kg
0.37
1
06/15/17 17:15
06/20/17 02:14
7440-39-3
Cadmium
5.1
mg/kg
0.074
1
06/15/17 17:15
06/20/17 02:14
7440-43-9
Chromium
44.3
mg/kg
0.37
1
06/15/17 17:15
06/20/17 02:14
7440-47-3
Lead
717
mg/kg
0.37
1
06/15/17 17:15
06/20/17 02:14
7439-92-1
Selenium
ND
mg/kg
0.74
1
06/15/17 17:15
06/20/17 02:14
7782-49-2
Silver
0.86
mg/kg
0.37
1
06/15/17 17:15
06/20/17 02:14
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.12
mg/kg
0.0055
1
06/14/17 16:09
06/15/17 08:09
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
83-32-9
Acenaphthylene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
208-96-8
Aniline
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
62-53-3
Anthracene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
120-12-7
Benzo(a)anthracene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
56-55-3
Benzo(a)pyrene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
207-08-9
Benzoic Acid
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
65-85-0
Benzyl alcohol
ND
mg/kg
8.2
10
06/15/17 09:19
06/16/17 18:02
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
101-55-3
Butylbenzylphthalate
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
8.2
10
06/15/17 09:19
06/16/17 18:02
59-50-7
4-Chloroaniline
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
111-44-4
2-Chloronaphthalene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
91-58-7
2-Chlorophenol
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
7005-72-3
Chrysene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
53-70-3
Dibenzofuran
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
91-94-1
2,4-Dichlorophenol
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
120-83-2
Diethylphthalate
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
84-66-2
2,4-Dimethylphenol
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
105-67-9
Dimethylphthalate
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
131-11-3
Di-n-butylphthalate
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
8.2
10
06/15/17 09:19
06/16/17 18:02
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 55

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ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-2
Lab ID: 92344137002 Collected: 06/14/17
10:10
Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
606-20-2
Di-n-octylphthalate
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
117-81-7
Fluoranthene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
206-44-0
Fluorene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
87-68-3
Hexachlorobenzene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
77-47-4
Hexachloroethane
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
193-39-5
Isophorone
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
78-59-1
1-Methylnaphthalene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
90-12-0
2-Methylnaphthalene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
15831-10-4
Naphthalene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
91-20-3
2-Nitroaniline
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
88-74-4
3-Nitroaniline
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
99-09-2
4-Nitroaniline
ND
mg/kg
8.2
10
06/15/17 09:19
06/16/17 18:02
100-01-6
Nitrobenzene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
98-95-3
2-Nitrophenol
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
88-75-5
4-Nitrophenol
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
108-60-1
Pentachlorophenol
ND
mg/kg
20.6
10
06/15/17 09:19
06/16/17 18:02
87-86-5
Phenanthrene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
85-01-8
Phenol
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
108-95-2
Pyrene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
4.1
10
06/15/17 09:19
06/16/17 18:02
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
06/15/17 09:19
06/16/17 18:02
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
06/15/17 09:19
06/16/17 18:02
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
06/15/17 09:19
06/16/17 18:02
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
06/15/17 09:19
06/16/17 18:02
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
06/15/17 09:19
06/16/17 18:02
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
06/15/17 09:19
06/16/17 18:02
118-79-6
S4
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.14
1
06/15/1714:51
67-64-1
Benzene
0.25
mg/kg
0.0069
1
06/15/1714:51
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 55

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Pace Analytical Services, LLC
2225 Riverside Dr.
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[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-2 Lab ID: 92344137002 Collected: 06/14/17 10:10 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0069
1
06/15/17 14:51
108-86-1
Bromochloromethane
ND
mg/kg
0.0069
1
06/15/17 14:51
74-97-5
Bromodichloromethane
ND
mg/kg
0.0069
1
06/15/17 14:51
75-27-4
Bromoform
ND
mg/kg
0.0069
1
06/15/17 14:51
75-25-2
Bromomethane
ND
mg/kg
0.014
1
06/15/17 14:51
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.14
1
06/15/17 14:51
78-93-3
n-Butylbenzene
ND
mg/kg
0.0069
1
06/15/17 14:51
104-51-8
sec-Butylbenzene
0.083
mg/kg
0.0069
1
06/15/17 14:51
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0069
1
06/15/17 14:51
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0069
1
06/15/17 14:51
56-23-5
Chlorobenzene
ND
mg/kg
0.0069
1
06/15/17 14:51
108-90-7
Chloroethane
ND
mg/kg
0.014
1
06/15/17 14:51
75-00-3
Chloroform
ND
mg/kg
0.0069
1
06/15/17 14:51
67-66-3
Chloromethane
ND
mg/kg
0.014
1
06/15/17 14:51
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0069
1
06/15/17 14:51
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0069
1
06/15/17 14:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0069
1
06/15/17 14:51
96-12-8
Dibromochloromethane
ND
mg/kg
0.0069
1
06/15/17 14:51
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0069
1
06/15/17 14:51
106-93-4
Dibromomethane
ND
mg/kg
0.0069
1
06/15/17 14:51
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0069
1
06/15/17 14:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0069
1
06/15/17 14:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0069
1
06/15/17 14:51
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.014
1
06/15/17 14:51
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0069
1
06/15/17 14:51
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0069
1
06/15/17 14:51
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0069
1
06/15/17 14:51
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0069
1
06/15/17 14:51
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0069
1
06/15/17 14:51
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0069
1
06/15/17 14:51
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0069
1
06/15/17 14:51
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0069
1
06/15/17 14:51
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0069
1
06/15/17 14:51
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0069
1
06/15/17 14:51
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0069
1
06/15/17 14:51
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0069
1
06/15/17 14:51
108-20-3
Ethylbenzene
2.2
mg/kg
0.69
100
06/15/1718:30
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0069
1
06/15/17 14:51
87-68-3
2-Hexanone
ND
mg/kg
0.069
1
06/15/17 14:51
591-78-6
Isopropylbenzene (Cumene)
0.15
mg/kg
0.0069
1
06/15/17 14:51
98-82-8
p-Isopropyltoluene
0.20
mg/kg
0.0069
1
06/15/17 14:51
99-87-6
Methylene Chloride
ND
mg/kg
0.028
1
06/15/17 14:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.069
1
06/15/17 14:51
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0069
1
06/15/17 14:51
1634-04-4
Naphthalene
7.7
mg/kg
0.69
100
06/15/1718:30
91-20-3
n-Propylbenzene
1.1
mg/kg
0.69
100
06/15/1718:30
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 55

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-2 Lab ID: 92344137002 Collected: 06/14/17 10:10 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 06/21 /2017 08:13 AM
Analytical Method: EPA 8260
ND
mg/kg
0.0069
1
06/15/1714:51
100-42-5
ND
mg/kg
0.0069
1
06/15/1714:51
630-20-6
ND
mg/kg
0.0069
1
06/15/1714:51
79-34-5
ND
mg/kg
0.0069
1
06/15/1714:51
127-18-4 L2
6.3
mg/kg
0.69
100
06/15/1718:30
108-88-3
ND
mg/kg
0.0069
1
06/15/1714:51
87-61-6
ND
mg/kg
0.0069
1
06/15/1714:51
120-82-1
ND
mg/kg
0.0069
1
06/15/1714:51
71-55-6
ND
mg/kg
0.0069
1
06/15/1714:51
79-00-5
ND
mg/kg
0.0069
1
06/15/1714:51
79-01-6
ND
mg/kg
0.0069
1
06/15/1714:51
75-69-4
ND
mg/kg
0.0069
1
06/15/1714:51
96-18-4
8.2
mg/kg
0.69
100
06/15/1718:30
95-63-6
2.6
mg/kg
0.69
100
06/15/1718:30
108-67-8
ND
mg/kg
0.069
1
06/15/1714:51
108-05-4
ND
mg/kg
0.014
1
06/15/1714:51
75-01-4
12.8
mg/kg
1.4
100
06/15/1718:30
1330-20-7
8.7
mg/kg
1.4
100
06/15/1718:30
179601-23-1
4.0
mg/kg
0.69
100
06/15/1718:30
95-47-6
84
%
70-130
1
06/15/1714:51
2037-26-5 10
88
%
70-130
1
06/15/1714:51
460-00-4
180
%
70-132
1
06/15/1714:51
17060-07-0 S1
Analytical Method: ASTM D2974-87
19.9 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/17 07:25
Page 11 of 55

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-3 Lab ID: 92344137003 Collected: 06/14/17 10:40 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
7.4
mg/kg
0.94
1
06/15/17 17:15
06/20/17 02:17
7440-38-2
Barium
226
mg/kg
0.47
1
06/15/17 17:15
06/20/17 02:17
7440-39-3
Cadmium
6.9
mg/kg
0.094
1
06/15/17 17:15
06/20/17 02:17
7440-43-9
Chromium
57.8
mg/kg
0.47
1
06/15/17 17:15
06/20/17 02:17
7440-47-3
Lead
1390
mg/kg
4.7
10
06/15/17 17:15
06/20/1713:13
7439-92-1
Selenium
ND
mg/kg
0.94
1
06/15/17 17:15
06/20/17 02:17
7782-49-2
Silver
3.6
mg/kg
0.47
1
06/15/17 17:15
06/20/17 02:17
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.18
mg/kg
0.010
2
06/14/17 16:09
06/15/17 09:16
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
83-32-9
Acenaphthylene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
208-96-8
Aniline
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
62-53-3
Anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
120-12-7
Benzo(a)anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
56-55-3
Benzo(a)pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
207-08-9
Benzoic Acid
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
65-85-0
Benzyl alcohol
ND
mg/kg
7.3
10
06/15/17 09:19
06/16/17 18:31
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
101-55-3
Butylbenzylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
7.3
10
06/15/17 09:19
06/16/17 18:31
59-50-7
4-Chloroaniline
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
111-44-4
2-Chloronaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
91-58-7
2-Chlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
7005-72-3
Chrysene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
53-70-3
Dibenzofuran
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
91-94-1
2,4-Dichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
120-83-2
Diethylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
84-66-2
2,4-Dimethylphenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
105-67-9
Dimethylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
131-11-3
Di-n-butylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
7.3
10
06/15/17 09:19
06/16/17 18:31
534-52-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 55

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ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-3
Lab ID: 92344137003 Collected: 06/14/17
10:40
Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
606-20-2
Di-n-octylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
117-81-7
Fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
206-44-0
Fluorene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
87-68-3
Hexachlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
77-47-4
Hexachloroethane
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
193-39-5
Isophorone
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
78-59-1
1-Methylnaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
90-12-0
2-Methylnaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
15831-10-4
Naphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
91-20-3
2-Nitroaniline
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
88-74-4
3-Nitroaniline
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
99-09-2
4-Nitroaniline
ND
mg/kg
7.3
10
06/15/17 09:19
06/16/17 18:31
100-01-6
Nitrobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
98-95-3
2-Nitrophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
88-75-5
4-Nitrophenol
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
108-60-1
Pentachlorophenol
ND
mg/kg
18.2
10
06/15/17 09:19
06/16/17 18:31
87-86-5
Phenanthrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
85-01-8
Phenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
108-95-2
Pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 18:31
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
06/15/17 09:19
06/16/17 18:31
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
06/15/17 09:19
06/16/17 18:31
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
06/15/17 09:19
06/16/17 18:31
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
06/15/17 09:19
06/16/17 18:31
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
06/15/17 09:19
06/16/17 18:31
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
06/15/17 09:19
06/16/17 18:31
118-79-6
S4
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
4.8
25
06/15/1715:11
67-64-1
Benzene
1.5
mg/kg
0.24
25
06/15/1715:11
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 55

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2225 Riverside Dr.
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[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-3 Lab ID: 92344137003 Collected: 06/14/17 10:40 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.24
25
06/15/17 15:11
108-86-1
Bromochloromethane
ND
mg/kg
0.24
25
06/15/17 15:11
74-97-5
Bromodichloromethane
ND
mg/kg
0.24
25
06/15/17 15:11
75-27-4
Bromoform
ND
mg/kg
0.24
25
06/15/17 15:11
75-25-2
Bromomethane
ND
mg/kg
0.48
25
06/15/17 15:11
74-83-9
2-Butanone (MEK)
ND
mg/kg
4.8
25
06/15/17 15:11
78-93-3
n-Butylbenzene
ND
mg/kg
0.24
25
06/15/17 15:11
104-51-8
sec-Butylbenzene
ND
mg/kg
0.24
25
06/15/17 15:11
135-98-8
tert-Butyl benzene
ND
mg/kg
0.24
25
06/15/17 15:11
98-06-6
Carbon tetrachloride
ND
mg/kg
0.24
25
06/15/17 15:11
56-23-5
Chlorobenzene
ND
mg/kg
0.24
25
06/15/17 15:11
108-90-7
Chloroethane
ND
mg/kg
0.48
25
06/15/17 15:11
75-00-3
Chloroform
ND
mg/kg
0.24
25
06/15/17 15:11
67-66-3
Chloromethane
ND
mg/kg
0.48
25
06/15/17 15:11
74-87-3
2-Chlorotoluene
ND
mg/kg
0.24
25
06/15/17 15:11
95-49-8
4-Chlorotoluene
ND
mg/kg
0.24
25
06/15/17 15:11
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.24
25
06/15/17 15:11
96-12-8
Dibromochloromethane
ND
mg/kg
0.24
25
06/15/17 15:11
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.24
25
06/15/17 15:11
106-93-4
Dibromomethane
ND
mg/kg
0.24
25
06/15/17 15:11
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.24
25
06/15/17 15:11
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.24
25
06/15/17 15:11
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.24
25
06/15/17 15:11
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.48
25
06/15/17 15:11
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.24
25
06/15/17 15:11
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.24
25
06/15/17 15:11
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.24
25
06/15/17 15:11
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.24
25
06/15/17 15:11
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.24
25
06/15/17 15:11
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.24
25
06/15/17 15:11
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.24
25
06/15/17 15:11
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.24
25
06/15/17 15:11
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.24
25
06/15/17 15:11
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.24
25
06/15/17 15:11
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.24
25
06/15/17 15:11
10061-02-6
Diisopropyl ether
ND
mg/kg
0.24
25
06/15/17 15:11
108-20-3
Ethylbenzene
4.4
mg/kg
0.24
25
06/15/17 15:11
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.24
25
06/15/17 15:11
87-68-3
2-Hexanone
ND
mg/kg
2.4
25
06/15/17 15:11
591-78-6
Isopropylbenzene (Cumene)
0.50
mg/kg
0.24
25
06/15/17 15:11
98-82-8
p-Isopropyltoluene
1.7
mg/kg
0.24
25
06/15/17 15:11
99-87-6
Methylene Chloride
ND
mg/kg
0.95
25
06/15/17 15:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
2.4
25
06/15/17 15:11
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.24
25
06/15/17 15:11
1634-04-4
Naphthalene
4.0
mg/kg
0.24
25
06/15/17 15:11
91-20-3
n-Propylbenzene
1.5
mg/kg
0.24
25
06/15/17 15:11
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 55

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-3 Lab ID: 92344137003 Collected: 06/14/17 10:40 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 06/21 /2017 08:13 AM
Analytical Method: EPA 8260
ND
mg/kg
0.24
25
06/15/1715:11
100-42-5
ND
mg/kg
0.24
25
06/15/1715:11
630-20-6
ND
mg/kg
0.24
25
06/15/1715:11
79-34-5
ND
mg/kg
0.24
25
06/15/1715:11
127-18-4 L2
7.7
mg/kg
0.24
25
06/15/1715:11
108-88-3
ND
mg/kg
0.24
25
06/15/1715:11
87-61-6
ND
mg/kg
0.24
25
06/15/1715:11
120-82-1
ND
mg/kg
0.24
25
06/15/1715:11
71-55-6
ND
mg/kg
0.24
25
06/15/1715:11
79-00-5
ND
mg/kg
0.24
25
06/15/1715:11
79-01-6
ND
mg/kg
0.24
25
06/15/1715:11
75-69-4
ND
mg/kg
0.24
25
06/15/1715:11
96-18-4
28.2
mg/kg
4.8
500
06/15/1718:50
95-63-6
12.2
mg/kg
4.8
500
06/15/1718:50
108-67-8
ND
mg/kg
2.4
25
06/15/1715:11
108-05-4
ND
mg/kg
0.48
25
06/15/1715:11
75-01-4
48.1
mg/kg
9.5
500
06/15/1718:50
1330-20-7
30.7
mg/kg
9.5
500
06/15/1718:50
179601-23-1
17.4
mg/kg
4.8
500
06/15/1718:50
95-47-6
97
%
70-130
25
06/15/1715:11
2037-26-5
110
%
70-130
25
06/15/1715:11
460-00-4
119
%
70-132
25
06/15/1715:11
17060-07-0
Analytical Method: ASTM D2974-87
9.4 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/17 07:26
Page 15 of 55

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-4 Lab ID: 92344137004 Collected: 06/14/17 11:00 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
7.9
mg/kg
0.71
1
06/15/17 17:15
06/20/17 02:21
7440-38-2
Barium
109
mg/kg
0.36
1
06/15/17 17:15
06/20/17 02:21
7440-39-3
Cadmium
0.17
mg/kg
0.071
1
06/15/17 17:15
06/20/17 02:21
7440-43-9
Chromium
7.2
mg/kg
0.36
1
06/15/17 17:15
06/20/17 02:21
7440-47-3
Lead
74.1
mg/kg
0.36
1
06/15/17 17:15
06/20/17 02:21
7439-92-1
Selenium
ND
mg/kg
0.71
1
06/15/17 17:15
06/20/17 02:21
7782-49-2
Silver
ND
mg/kg
0.36
1
06/15/17 17:15
06/20/17 02:21
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.020
mg/kg
0.0043
1
06/14/17 16:09
06/15/17 08:14
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
83-32-9
Acenaphthylene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
208-96-8
Aniline
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
62-53-3
Anthracene
4.5
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
120-12-7
Benzo(a)anthracene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
56-55-3
Benzo(a)pyrene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
207-08-9
Benzoic Acid
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
65-85-0
Benzyl alcohol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:01
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
101-55-3
Butylbenzylphthalate
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:01
59-50-7
4-Chloroaniline
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
111-44-4
2-Chloronaphthalene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
91-58-7
2-Chlorophenol
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
7005-72-3
Chrysene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
53-70-3
Dibenzofuran
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
91-94-1
2,4-Dichlorophenol
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
120-83-2
Diethylphthalate
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
84-66-2
2,4-Dimethylphenol
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
105-67-9
Dimethylphthalate
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
131-11-3
Di-n-butylphthalate
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:01
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 55

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ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-4
Lab ID: 92344137004 Collected: 06/14/17
11:00
Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
606-20-2
Di-n-octylphthalate
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
117-81-7
Fluoranthene
16.0
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
206-44-0
Fluorene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
87-68-3
Hexachlorobenzene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
77-47-4
Hexachloroethane
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
193-39-5
Isophorone
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
78-59-1
1-Methylnaphthalene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
90-12-0
2-Methylnaphthalene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
15831-10-4
Naphthalene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
91-20-3
2-Nitroaniline
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
88-74-4
3-Nitroaniline
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
99-09-2
4-Nitroaniline
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:01
100-01-6
Nitrobenzene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
98-95-3
2-Nitrophenol
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
88-75-5
4-Nitrophenol
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
108-60-1
Pentachlorophenol
ND
mg/kg
17.6
10
06/15/17 09:19
06/16/17 19:01
87-86-5
Phenanthrene
18.0
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
85-01-8
Phenol
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
108-95-2
Pyrene
9.5
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
3.5
10
06/15/17 09:19
06/16/17 19:01
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
06/15/17 09:19
06/16/17 19:01
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
06/15/17 09:19
06/16/17 19:01
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
06/15/17 09:19
06/16/17 19:01
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
06/15/17 09:19
06/16/17 19:01
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
06/15/17 09:19
06/16/17 19:01
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
06/15/17 09:19
06/16/17 19:01
118-79-6
S4
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.21
1
06/16/1718:37
67-64-1
Benzene
ND
mg/kg
0.010
1
06/16/1718:37
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 55

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ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-4 Lab ID: 92344137004 Collected: 06/14/17 11:00 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.010
1
06/16/17 18:37
108-86-1
Bromochloromethane
ND
mg/kg
0.010
1
06/16/17 18:37
74-97-5
Bromodichloromethane
ND
mg/kg
0.010
1
06/16/17 18:37
75-27-4
Bromoform
ND
mg/kg
0.010
1
06/16/17 18:37
75-25-2
Bromomethane
ND
mg/kg
0.021
1
06/16/17 18:37
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.21
1
06/16/17 18:37
78-93-3
n-Butylbenzene
ND
mg/kg
0.010
1
06/16/17 18:37
104-51-8
sec-Butylbenzene
ND
mg/kg
0.010
1
06/16/17 18:37
135-98-8
tert-Butyl benzene
ND
mg/kg
0.010
1
06/16/17 18:37
98-06-6
Carbon tetrachloride
ND
mg/kg
0.010
1
06/16/17 18:37
56-23-5
Chlorobenzene
ND
mg/kg
0.010
1
06/16/17 18:37
108-90-7
Chloroethane
ND
mg/kg
0.021
1
06/16/17 18:37
75-00-3
Chloroform
ND
mg/kg
0.010
1
06/16/17 18:37
67-66-3
Chloromethane
ND
mg/kg
0.021
1
06/16/17 18:37
74-87-3
2-Chlorotoluene
ND
mg/kg
0.010
1
06/16/17 18:37
95-49-8
4-Chlorotoluene
ND
mg/kg
0.010
1
06/16/17 18:37
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.010
1
06/16/17 18:37
96-12-8
Dibromochloromethane
ND
mg/kg
0.010
1
06/16/17 18:37
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.010
1
06/16/17 18:37
106-93-4
Dibromomethane
ND
mg/kg
0.010
1
06/16/17 18:37
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.010
1
06/16/17 18:37
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.010
1
06/16/17 18:37
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.010
1
06/16/17 18:37
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.021
1
06/16/17 18:37
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.010
1
06/16/17 18:37
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.010
1
06/16/17 18:37
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.010
1
06/16/17 18:37
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.010
1
06/16/17 18:37
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.010
1
06/16/17 18:37
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.010
1
06/16/17 18:37
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.010
1
06/16/17 18:37
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.010
1
06/16/17 18:37
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.010
1
06/16/17 18:37
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.010
1
06/16/17 18:37
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.010
1
06/16/17 18:37
10061-02-6
Diisopropyl ether
ND
mg/kg
0.010
1
06/16/17 18:37
108-20-3
Ethylbenzene
ND
mg/kg
0.010
1
06/16/17 18:37
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.010
1
06/16/17 18:37
87-68-3
2-Hexanone
ND
mg/kg
0.10
1
06/16/17 18:37
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.010
1
06/16/17 18:37
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.010
1
06/16/17 18:37
99-87-6
Methylene Chloride
ND
mg/kg
0.041
1
06/16/17 18:37
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.10
1
06/16/17 18:37
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.010
1
06/16/17 18:37
1634-04-4
Naphthalene
ND
mg/kg
0.010
1
06/16/17 18:37
91-20-3
n-Propylbenzene
ND
mg/kg
0.010
1
06/16/17 18:37
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 55

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ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-4 Lab ID: 92344137004 Collected: 06/14/17 11:00 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 06/21 /2017 08:13 AM
Analytical Method: EPA 8260
ND
mg/kg
0.010
1
06/16/1718:37
100-42-5
ND
mg/kg
0.010
1
06/16/1718:37
630-20-6
ND
mg/kg
0.010
1
06/16/1718:37
79-34-5
ND
mg/kg
0.010
1
06/16/1718:37
127-18-4 L2
ND
mg/kg
0.010
1
06/16/1718:37
108-88-3
ND
mg/kg
0.010
1
06/16/1718:37
87-61-6
ND
mg/kg
0.010
1
06/16/1718:37
120-82-1
ND
mg/kg
0.010
1
06/16/1718:37
71-55-6
ND
mg/kg
0.010
1
06/16/1718:37
79-00-5
ND
mg/kg
0.010
1
06/16/1718:37
79-01-6
ND
mg/kg
0.010
1
06/16/1718:37
75-69-4
ND
mg/kg
0.010
1
06/16/1718:37
96-18-4
ND
mg/kg
0.010
1
06/16/1718:37
95-63-6
ND
mg/kg
0.010
1
06/16/1718:37
108-67-8
ND
mg/kg
0.10
1
06/16/1718:37
108-05-4
ND
mg/kg
0.021
1
06/16/1718:37
75-01-4
ND
mg/kg
0.021
1
06/16/1718:37
1330-20-7
ND
mg/kg
0.021
1
06/16/1718:37
179601-23-1
ND
mg/kg
0.010
1
06/16/1718:37
95-47-6
97
%
70-130
1
06/16/1718:37
2037-26-5 1g
89
%
70-130
1
06/16/1718:37
460-00-4
124
%
70-132
1
06/16/1718:37
17060-07-0
Analytical Method: ASTM D2974-87
6.5 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/17 07:26
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aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-5 Lab ID: 92344137005 Collected: 06/14/17 11:30 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
4.9
mg/kg
0.83
1
06/15/17 17:15
06/20/17 02:24
7440-38-2
Barium
97.0
mg/kg
0.41
1
06/15/17 17:15
06/20/17 02:24
7440-39-3
Cadmium
3.2
mg/kg
0.083
1
06/15/17 17:15
06/20/17 02:24
7440-43-9
Chromium
39.7
mg/kg
0.41
1
06/15/17 17:15
06/20/17 02:24
7440-47-3
Lead
523
mg/kg
0.41
1
06/15/17 17:15
06/20/17 02:24
7439-92-1
Selenium
ND
mg/kg
0.83
1
06/15/17 17:15
06/20/17 02:24
7782-49-2
Silver
0.84
mg/kg
0.41
1
06/15/17 17:15
06/20/17 02:24
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.17
mg/kg
0.0068
2
06/14/17 16:09
06/15/17 09:19
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
83-32-9
Acenaphthylene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
208-96-8
Aniline
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
62-53-3
Anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
120-12-7
Benzo(a)anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
56-55-3
Benzo(a)pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
207-08-9
Benzoic Acid
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
65-85-0
Benzyl alcohol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:31
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
101-55-3
Butylbenzylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:31
59-50-7
4-Chloroaniline
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
111-44-4
2-Chloronaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
91-58-7
2-Chlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
7005-72-3
Chrysene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
53-70-3
Dibenzofuran
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
91-94-1
2,4-Dichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
120-83-2
Diethylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
84-66-2
2,4-Dimethylphenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
105-67-9
Dimethylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
131-11-3
Di-n-butylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:31
534-52-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-5
Lab ID: 92344137005 Collected: 06/14/17
11:30
Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
606-20-2
Di-n-octylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
117-81-7
Fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
206-44-0
Fluorene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
87-68-3
Hexachlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
77-47-4
Hexachloroethane
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
193-39-5
Isophorone
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
78-59-1
1-Methylnaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
90-12-0
2-Methylnaphthalene
4.7
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
15831-10-4
Naphthalene
3.7
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
91-20-3
2-Nitroaniline
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
88-74-4
3-Nitroaniline
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
99-09-2
4-Nitroaniline
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 19:31
100-01-6
Nitrobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
98-95-3
2-Nitrophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
88-75-5
4-Nitrophenol
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
108-60-1
Pentachlorophenol
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 19:31
87-86-5
Phenanthrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
85-01-8
Phenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
108-95-2
Pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 19:31
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
06/15/17 09:19
06/16/17 19:31
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
06/15/17 09:19
06/16/17 19:31
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
06/15/17 09:19
06/16/17 19:31
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
06/15/17 09:19
06/16/17 19:31
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
06/15/17 09:19
06/16/17 19:31
367-12-4
S4
2,4,6-Tribromophenol (S)
15
%
27-110
10
06/15/17 09:19
06/16/17 19:31
118-79-6
S4
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.12
1
06/15/1715:51
67-64-1
Benzene
ND
mg/kg
1.4
250
06/16/1713:40
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 55

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-5 Lab ID: 92344137005 Collected: 06/14/17 11:30 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0062
1
06/15/17 15:51
108-86-1
Bromochloromethane
ND
mg/kg
0.0062
1
06/15/17 15:51
74-97-5
Bromodichloromethane
ND
mg/kg
0.0062
1
06/15/17 15:51
75-27-4
Bromoform
ND
mg/kg
0.0062
1
06/15/17 15:51
75-25-2
Bromomethane
ND
mg/kg
0.012
1
06/15/17 15:51
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.12
1
06/15/17 15:51
78-93-3
n-Butylbenzene
ND
mg/kg
0.0062
1
06/15/17 15:51
104-51-8
sec-Butylbenzene
0.073
mg/kg
0.0062
1
06/15/17 15:51
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0062
1
06/15/17 15:51
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0062
1
06/15/17 15:51
56-23-5
Chlorobenzene
ND
mg/kg
0.0062
1
06/15/17 15:51
108-90-7
Chloroethane
ND
mg/kg
0.012
1
06/15/17 15:51
75-00-3
Chloroform
ND
mg/kg
0.0062
1
06/15/17 15:51
67-66-3
Chloromethane
ND
mg/kg
0.012
1
06/15/17 15:51
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0062
1
06/15/17 15:51
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0062
1
06/15/17 15:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0062
1
06/15/17 15:51
96-12-8
Dibromochloromethane
ND
mg/kg
0.0062
1
06/15/17 15:51
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0062
1
06/15/17 15:51
106-93-4
Dibromomethane
ND
mg/kg
0.0062
1
06/15/17 15:51
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0062
1
06/15/17 15:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0062
1
06/15/17 15:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0062
1
06/15/17 15:51
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
1
06/15/17 15:51
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0062
1
06/15/17 15:51
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0062
1
06/15/17 15:51
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0062
1
06/15/17 15:51
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0062
1
06/15/17 15:51
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0062
1
06/15/17 15:51
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0062
1
06/15/17 15:51
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0062
1
06/15/17 15:51
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0062
1
06/15/17 15:51
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0062
1
06/15/17 15:51
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0062
1
06/15/17 15:51
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0062
1
06/15/17 15:51
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0062
1
06/15/17 15:51
108-20-3
Ethylbenzene
3.9
mg/kg
1.4
250
06/16/1713:40
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0062
1
06/15/17 15:51
87-68-3
2-Hexanone
ND
mg/kg
0.062
1
06/15/17 15:51
591-78-6
Isopropylbenzene (Cumene)
0.10
mg/kg
0.0062
1
06/15/17 15:51
98-82-8
p-Isopropyltoluene
1.8
mg/kg
1.4
250
06/16/1713:40
99-87-6
Methylene Chloride
ND
mg/kg
0.025
1
06/15/17 15:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.062
1
06/15/17 15:51
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0062
1
06/15/17 15:51
1634-04-4
Naphthalene
6.9
mg/kg
1.4
250
06/16/1713:40
91-20-3
n-Propylbenzene
2.4
mg/kg
1.4
250
06/16/1713:40
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-5 Lab ID: 92344137005 Collected: 06/14/17 11:30 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 06/21 /2017 08:13 AM
Analytical Method: EPA 8260
ND
mg/kg
0.0062
1
06/15/1715:51
100-42-5
ND
mg/kg
0.0062
1
06/15/1715:51
630-20-6
ND
mg/kg
0.0062
1
06/15/1715:51
79-34-5
ND
mg/kg
0.0062
1
06/15/1715:51
127-18-4
L2
7.6
mg/kg
1.4
250
06/16/1713:40
108-88-3
ND
mg/kg
0.0062
1
06/15/1715:51
87-61-6
ND
mg/kg
0.0062
1
06/15/1715:51
120-82-1
ND
mg/kg
0.0062
1
06/15/1715:51
71-55-6
ND
mg/kg
0.0062
1
06/15/1715:51
79-00-5
ND
mg/kg
0.0062
1
06/15/1715:51
79-01-6
ND
mg/kg
0.0062
1
06/15/1715:51
75-69-4
14.6
mg/kg
1.4
250
06/16/1713:40
96-18-4
39.4
mg/kg
1.4
250
06/16/1713:40
95-63-6
14.9
mg/kg
1.4
250
06/16/1713:40
108-67-8
ND
mg/kg
0.062
1
06/15/1715:51
108-05-4
ND
mg/kg
0.012
1
06/15/1715:51
75-01-4
48.7
mg/kg
2.9
250
06/16/1713:40
1330-20-7
32.8
mg/kg
2.9
250
06/16/1713:40
179601-23-1
15.9
mg/kg
1.4
250
06/16/1713:40
95-47-6
71
%
70-130
1
06/15/1715:51
2037-26-5
10
134
%
70-130
1
06/15/1715:51
460-00-4
S1
321
%
70-132
1
06/15/1715:51
17060-07-0
S1
Analytical Method: ASTM D2974-87
7.1 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/17 07:27
Page 23 of 55

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2225 Riverside Dr.
Asheville, NC 28804
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ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-6 Lab ID: 92344137006 Collected: 06/14/17 11:45 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
5.7
mg/kg
0.76
1
06/15/17 17:15
06/20/17 02:27
7440-38-2
Barium
138
mg/kg
0.38
1
06/15/17 17:15
06/20/17 02:27
7440-39-3
Cadmium
4.1
mg/kg
0.076
1
06/15/17 17:15
06/20/17 02:27
7440-43-9
Chromium
41.0
mg/kg
0.38
1
06/15/17 17:15
06/20/17 02:27
7440-47-3
Lead
1070
mg/kg
3.8
10
06/15/17 17:15
06/20/1713:25
7439-92-1
Selenium
ND
mg/kg
0.76
1
06/15/17 17:15
06/20/17 02:27
7782-49-2
Silver
1.0
mg/kg
0.38
1
06/15/17 17:15
06/20/17 02:27
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.16
mg/kg
0.0090
2
06/14/17 16:09
06/15/17 09:21
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
83-32-9
Acenaphthylene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
208-96-8
Aniline
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
62-53-3
Anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
120-12-7
Benzo(a)anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
56-55-3
Benzo(a)pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
207-08-9
Benzoic Acid
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
65-85-0
Benzyl alcohol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 20:00
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
101-55-3
Butylbenzylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 20:00
59-50-7
4-Chloroaniline
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
111-44-4
2-Chloronaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
91-58-7
2-Chlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
7005-72-3
Chrysene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
53-70-3
Dibenzofuran
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
91-94-1
2,4-Dichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
120-83-2
Diethylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
84-66-2
2,4-Dimethylphenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
105-67-9
Dimethylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
131-11-3
Di-n-butylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 20:00
534-52-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 55

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: SB-6
Lab ID: 92344137006 Collected: 06/14/17
11:45
Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis
and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
606-20-2
Di-n-octylphthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
117-81-7
Fluoranthene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
206-44-0
Fluorene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
87-68-3
Hexachlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
77-47-4
Hexachloroethane
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
193-39-5
Isophorone
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
78-59-1
1-Methylnaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
90-12-0
2-Methylnaphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
15831-10-4
Naphthalene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
91-20-3
2-Nitroaniline
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
88-74-4
3-Nitroaniline
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
99-09-2
4-Nitroaniline
ND
mg/kg
7.1
10
06/15/17 09:19
06/16/17 20:00
100-01-6
Nitrobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
98-95-3
2-Nitrophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
88-75-5
4-Nitrophenol
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
108-60-1
Pentachlorophenol
ND
mg/kg
17.8
10
06/15/17 09:19
06/16/17 20:00
87-86-5
Phenanthrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
85-01-8
Phenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
108-95-2
Pyrene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
3.6
10
06/15/17 09:19
06/16/17 20:00
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
06/15/17 09:19
06/16/17 20:00
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
06/15/17 09:19
06/16/17 20:00
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
06/15/17 09:19
06/16/17 20:00
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
06/15/17 09:19
06/16/17 20:00
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
06/15/17 09:19
06/16/17 20:00
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
06/15/17 09:19
06/16/17 20:00
118-79-6
S4
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.12
1
06/16/1718:57
67-64-1
Benzene
ND
mg/kg
0.0061
1
06/16/1718:57
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 55

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-6 Lab ID: 92344137006 Collected: 06/14/17 11:45 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
108-86-1
Bromochloromethane
ND
mg/kg
0.0061
1
06/16/17 18:57
74-97-5
Bromodichloromethane
ND
mg/kg
0.0061
1
06/16/17 18:57
75-27-4
Bromoform
ND
mg/kg
0.0061
1
06/16/17 18:57
75-25-2
Bromomethane
ND
mg/kg
0.012
1
06/16/17 18:57
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.12
1
06/16/17 18:57
78-93-3
n-Butylbenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0061
1
06/16/17 18:57
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0061
1
06/16/17 18:57
56-23-5
Chlorobenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
108-90-7
Chloroethane
ND
mg/kg
0.012
1
06/16/17 18:57
75-00-3
Chloroform
ND
mg/kg
0.0061
1
06/16/17 18:57
67-66-3
Chloromethane
ND
mg/kg
0.012
1
06/16/17 18:57
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0061
1
06/16/17 18:57
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0061
1
06/16/17 18:57
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0061
1
06/16/17 18:57
96-12-8
Dibromochloromethane
ND
mg/kg
0.0061
1
06/16/17 18:57
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0061
1
06/16/17 18:57
106-93-4
Dibromomethane
ND
mg/kg
0.0061
1
06/16/17 18:57
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
1
06/16/17 18:57
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0061
1
06/16/17 18:57
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0061
1
06/16/17 18:57
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0061
1
06/16/17 18:57
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0061
1
06/16/17 18:57
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0061
1
06/16/17 18:57
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0061
1
06/16/17 18:57
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0061
1
06/16/17 18:57
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0061
1
06/16/17 18:57
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0061
1
06/16/17 18:57
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0061
1
06/16/17 18:57
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0061
1
06/16/17 18:57
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0061
1
06/16/17 18:57
108-20-3
Ethylbenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0061
1
06/16/17 18:57
87-68-3
2-Hexanone
ND
mg/kg
0.061
1
06/16/17 18:57
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0061
1
06/16/17 18:57
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0061
1
06/16/17 18:57
99-87-6
Methylene Chloride
ND
mg/kg
0.024
1
06/16/17 18:57
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.061
1
06/16/17 18:57
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0061
1
06/16/17 18:57
1634-04-4
Naphthalene
ND
mg/kg
0.0061
1
06/16/17 18:57
91-20-3
n-Propylbenzene
ND
mg/kg
0.0061
1
06/16/17 18:57
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
Sample: S13-6 Lab ID: 92344137006 Collected: 06/14/17 11:45 Received: 06/14/17 12:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 06/21 /2017 08:13 AM
Analytical Method: EPA 8260
ND
mg/kg
0.0061
1
06/16/1718:57
100-42-5
ND
mg/kg
0.0061
1
06/16/1718:57
630-20-6
ND
mg/kg
0.0061
1
06/16/1718:57
79-34-5
ND
mg/kg
0.0061
1
06/16/1718:57
127-18-4 L2
ND
mg/kg
0.0061
1
06/16/1718:57
108-88-3
ND
mg/kg
0.0061
1
06/16/1718:57
87-61-6
ND
mg/kg
0.0061
1
06/16/1718:57
120-82-1
ND
mg/kg
0.0061
1
06/16/1718:57
71-55-6
ND
mg/kg
0.0061
1
06/16/1718:57
79-00-5
ND
mg/kg
0.0061
1
06/16/1718:57
79-01-6
ND
mg/kg
0.0061
1
06/16/1718:57
75-69-4
ND
mg/kg
0.0061
1
06/16/1718:57
96-18-4
ND
mg/kg
0.0061
1
06/16/1718:57
95-63-6
ND
mg/kg
0.0061
1
06/16/1718:57
108-67-8
ND
mg/kg
0.061
1
06/16/1718:57
108-05-4
ND
mg/kg
0.012
1
06/16/1718:57
75-01-4
ND
mg/kg
0.012
1
06/16/1718:57
1330-20-7
ND
mg/kg
0.012
1
06/16/1718:57
179601-23-1
ND
mg/kg
0.0061
1
06/16/1718:57
95-47-6
92
%
70-130
1
06/16/1718:57
2037-26-5 1g
88
%
70-130
1
06/16/1718:57
460-00-4
108
%
70-132
1
06/16/1718:57
17060-07-0
Analytical Method: ASTM D2974-87
7.2 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
06/16/17 07:27
Page 27 of 55

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
QC Batch: 364821
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 92344137001, 92344137002,
92344137003, 92344137004, 92344137005, 92344137006
METHOD BLANK: 2022539
Matrix: Solid
Associated Lab Samples: 92344137001, 92344137002,
92344137003, 92344137004, 92344137005, 92344137006
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mercury mg/kg
ND 0.0060 06/15/17 07:50
LABORATORY CONTROL SAMPLE: 2022540
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury mg/kg
.083 0.077 92 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2022541 2022542
MS MSD
92344107001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg ND
.058 .057 0.020 0.024 34 43 75-125 19 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC.
Page 28 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
QC Batch: 364868 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137004, 92344137005, 92344137006
METHOD BLANK: 2022937
Matrix:
Solid
Associated Lab Samples:
92344137001, 92344137002,
92344137003, 92344137004, 92344137005,
92344137006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
06/20/17 01:44
Barium
mg/kg
ND
0.50
06/20/17 01:44
Cadmium
mg/kg
ND
0.10
06/20/17 01:44
Chromium
mg/kg
ND
0.50
06/20/17 01:44
Lead
mg/kg
ND
0.50
06/20/17 01:44
Selenium
mg/kg
ND
1.0
06/20/17 01:44
Silver
mg/kg
ND
0.50
06/20/17 01:44
LABORATORY CONTROL SAMPLE: 2022938
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
48.8
98
80-120
Barium
mg/kg
50
49.9
100
80-120
Cadmium
mg/kg
50
49.2
98
80-120
Chromium
mg/kg
50
50.7
101
80-120
Lead
mg/kg
50
49.5
99
80-120
Selenium
mg/kg
50
51.2
102
80-120
Silver
mg/kg
25
26.8
107
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2022939 2022940
MS
MSD
92343940001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
42.5
77.2
42.0
74.9
99
97
75-125
56 R1
Barium
mg/kg
80.7
42.5
77.2
57.1
91.2
-55
14
75-125
46 M1,R1
Cadmium
mg/kg
ND
42.5
77.2
40.9
73.9
96
96
75-125
58 R1
Chromium
mg/kg
0.67
42.5
77.2
41.2
74.1
95
95
75-125
57 R1
Lead
mg/kg
0.79
42.5
77.2
41.2
73.2
95
94
75-125
56 R1
Selenium
mg/kg
ND
42.5
77.2
47.1
82.3
108
105
75-125
54 R1
Silver
mg/kg
ND
21.3
38.5
21.8
39.4
103
102
75-125
57 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC.
Page 29 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
QC Batch: 364974 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137005
METHOD BLANK: 2023481 Matrix: Solid
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137005
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0054
06/15/17 12:13
1,1,1-Trichloroethane
mg/kg
ND
0.0054
06/15/17 12:13
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0054
06/15/17 12:13
1,1,2-Trichloroethane
mg/kg
ND
0.0054
06/15/17 12:13
1,1-Dichloroethane
mg/kg
ND
0.0054
06/15/17 12:13
1,1-Dichloroethene
mg/kg
ND
0.0054
06/15/17 12:13
1,1-Dichloropropene
mg/kg
ND
0.0054
06/15/17 12:13
1,2,3-Trichlorobenzene
mg/kg
ND
0.0054
06/15/17 12:13
1,2,3-Trichloropropane
mg/kg
ND
0.0054
06/15/17 12:13
1,2,4-Trichlorobenzene
mg/kg
ND
0.0054
06/15/17 12:13
1,2,4-Trimethylbenzene
mg/kg
ND
0.0054
06/15/17 12:13
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0054
06/15/17 12:13
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0054
06/15/17 12:13
1,2-Dichlorobenzene
mg/kg
ND
0.0054
06/15/17 12:13
1,2-Dichloroethane
mg/kg
ND
0.0054
06/15/17 12:13
1,2-Dichloropropane
mg/kg
ND
0.0054
06/15/17 12:13
1,3,5-Trimethylbenzene
mg/kg
ND
0.0054
06/15/17 12:13
1,3-Dichlorobenzene
mg/kg
ND
0.0054
06/15/17 12:13
1,3-Dichloropropane
mg/kg
ND
0.0054
06/15/17 12:13
1,4-Dichlorobenzene
mg/kg
ND
0.0054
06/15/17 12:13
2,2-Dichloropropane
mg/kg
ND
0.0054
06/15/17 12:13
2-Butanone (MEK)
mg/kg
ND
0.11
06/15/17 12:13
2-Chlorotoluene
mg/kg
ND
0.0054
06/15/17 12:13
2-Hexanone
mg/kg
ND
0.054
06/15/17 12:13
4-Chlorotoluene
mg/kg
ND
0.0054
06/15/17 12:13
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.054
06/15/17 12:13
Acetone
mg/kg
ND
0.11
06/15/17 12:13
Benzene
mg/kg
ND
0.0054
06/15/17 12:13
Bromobenzene
mg/kg
ND
0.0054
06/15/17 12:13
Bromochloromethane
mg/kg
ND
0.0054
06/15/17 12:13
Bromodichloromethane
mg/kg
ND
0.0054
06/15/17 12:13
Bromoform
mg/kg
ND
0.0054
06/15/17 12:13
Bromomethane
mg/kg
ND
0.011
06/15/17 12:13
Carbon tetrachloride
mg/kg
ND
0.0054
06/15/17 12:13
Chlorobenzene
mg/kg
ND
0.0054
06/15/17 12:13
Chloroethane
mg/kg
ND
0.011
06/15/17 12:13
Chloroform
mg/kg
ND
0.0054
06/15/17 12:13
Chloromethane
mg/kg
ND
0.011
06/15/17 12:13
cis-1,2-Dichloroethene
mg/kg
ND
0.0054
06/15/17 12:13
cis-1,3-Dichloropropene
mg/kg
ND
0.0054
06/15/17 12:13
Dibromochloromethane
mg/kg
ND
0.0054
06/15/17 12:13
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
METHOD BLANK: 2023481 Matrix: Solid
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137005
Blank Reporting
Parameter Units Result Limit
Analyzed
Dibromomethane
mg/kg
ND
0.0054
06/15/17 12:13
Dichlorodifluoromethane
mg/kg
ND
0.011
06/15/17 12:13
Diisopropyl ether
mg/kg
ND
0.0054
06/15/17 12:13
Ethylbenzene
mg/kg
ND
0.0054
06/15/17 12:13
Hexachloro-1,3-butadiene
mg/kg
ND
0.0054
06/15/17 12:13
Isopropylbenzene (Cumene)
mg/kg
ND
0.0054
06/15/17 12:13
m&p-Xylene
mg/kg
ND
0.011
06/15/17 12:13
Methyl-tert-butyl ether
mg/kg
ND
0.0054
06/15/17 12:13
Methylene Chloride
mg/kg
ND
0.022
06/15/17 12:13
n-Butylbenzene
mg/kg
ND
0.0054
06/15/17 12:13
n-Propylbenzene
mg/kg
ND
0.0054
06/15/17 12:13
Naphthalene
mg/kg
ND
0.0054
06/15/17 12:13
o-Xylene
mg/kg
ND
0.0054
06/15/17 12:13
p-Isopropyltoluene
mg/kg
ND
0.0054
06/15/17 12:13
sec-Butylbenzene
mg/kg
ND
0.0054
06/15/17 12:13
Styrene
mg/kg
ND
0.0054
06/15/17 12:13
tert-Butyl benzene
mg/kg
ND
0.0054
06/15/17 12:13
Tetrachloroethene
mg/kg
ND
0.0054
06/15/17 12:13
Toluene
mg/kg
ND
0.0054
06/15/17 12:13
trans-1,2-Dichloroethene
mg/kg
ND
0.0054
06/15/17 12:13
trans- 1,3-Dichloropropene
mg/kg
ND
0.0054
06/15/17 12:13
Trichloroethene
mg/kg
ND
0.0054
06/15/17 12:13
Trichlorofluoromethane
mg/kg
ND
0.0054
06/15/17 12:13
Vinyl acetate
mg/kg
ND
0.054
06/15/17 12:13
Vinyl chloride
mg/kg
ND
0.011
06/15/17 12:13
Xylene (Total)
mg/kg
ND
0.011
06/15/17 12:13
1,2-Dichloroethane-d4 (S)
%
98
70-132
06/15/17 12:13
4-Bromofluorobenzene (S)
%
100
70-130
06/15/17 12:13
Toluene-d8 (S)
%
102
70-130
06/15/17 12:13
Qualifiers
LABORATORY CONTROL SAMPLE:
2023482
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
.062
0.061
98
74-137
1,1,1-Trichloroethane
mg/kg
.062
0.060
96
67-140
1,1,2,2-Tetrachloroethane
mg/kg
.062
0.064
103
72-141
1,1,2-Trichloroethane
mg/kg
.062
0.062
100
78-138
1,1-Dichloroethane
mg/kg
.062
0.063
102
69-134
1,1-Dichloroethene
mg/kg
.062
0.062
100
67-138
1,1-Dichloropropene
mg/kg
.062
0.062
99
69-139
1,2,3-Trichlorobenzene
mg/kg
.062
0.063
102
70-146
1,2,3-Trichloropropane
mg/kg
.062
0.061
99
69-144
1,2,4-Trichlorobenzene
mg/kg
.062
0.061
99
68-148
1,2,4-Trimethylbenzene
mg/kg
.062
0.063
101
74-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
LABORATORY CONTROL SAMPLE:
Parameter
2023482
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
mg/kg
.062
0.065
105
65-140
1,2-Dibromoethane (EDB)
mg/kg
.062
0.062
99
77-135
1,2-Dichlorobenzene
mg/kg
.062
0.062
99
77-141
1,2-Dichloroethane
mg/kg
.062
0.062
100
65-137
1,2-Dichloropropane
mg/kg
.062
0.063
102
72-136
1,3,5-Trimethylbenzene
mg/kg
.062
0.062
100
76-133
1,3-Dichlorobenzene
mg/kg
.062
0.061
99
74-138
1,3-Dichloropropane
mg/kg
.062
0.065
105
71-139
1,4-Dichlorobenzene
mg/kg
.062
0.062
100
76-138
2,2-Dichloropropane
mg/kg
.062
0.060
97
68-137
2-Butanone (MEK)
mg/kg
.12
0.13
108
58-147
2-Chlorotoluene
mg/kg
.062
0.063
102
73-139
2-Hexanone
mg/kg
.12
0.14
112
62-145
4-Chlorotoluene
mg/kg
.062
0.062
100
76-141
4-Methyl-2-pentanone (MIBK)
mg/kg
.12
0.14
115
64-149
Acetone
mg/kg
.12
ND
93
53-153
Benzene
mg/kg
.062
0.061
99
73-135
Bromobenzene
mg/kg
.062
0.061
98
75-133
Bromochloromethane
mg/kg
.062
0.064
103
73-134
Bromodichloromethane
mg/kg
.062
0.064
102
71-135
Bromoform
mg/kg
.062
0.059
95
66-141
Bromomethane
mg/kg
.062
0.064
103
53-160
Carbon tetrachloride
mg/kg
.062
0.060
96
60-145
Chlorobenzene
mg/kg
.062
0.062
100
78-130
Chloroethane
mg/kg
.062
0.063
101
64-149
Chloroform
mg/kg
.062
0.062
99
70-134
Chloromethane
mg/kg
.062
0.069
110
52-150
cis-1,2-Dichloroethene
mg/kg
.062
0.062
100
70-133
cis-1,3-Dichloropropene
mg/kg
.062
0.065
104
68-134
Dibromochloromethane
mg/kg
.062
0.065
104
71-138
Dibromomethane
mg/kg
.062
0.060
97
74-130
Dichlorodifluoromethane
mg/kg
.062
0.053
85
40-160
Diisopropyl ether
mg/kg
.062
0.069
110
69-141
Ethylbenzene
mg/kg
.062
0.062
100
75-133
Hexachloro-1,3-butadiene
mg/kg
.062
0.060
96
68-143
Isopropylbenzene (Cumene)
mg/kg
.062
0.062
99
76-143
m&p-Xylene
mg/kg
.12
0.12
99
75-136
Methyl-tert-butyl ether
mg/kg
.062
0.063
102
68-144
Methylene Chloride
mg/kg
.062
0.058
94
45-154
n-Butylbenzene
mg/kg
.062
0.063
102
72-137
n-Propylbenzene
mg/kg
.062
0.062
100
76-136
Naphthalene
mg/kg
.062
0.066
106
68-151
o-Xylene
mg/kg
.062
0.061
99
76-141
p-Isopropyltoluene
mg/kg
.062
0.063
101
76-140
sec-Butylbenzene
mg/kg
.062
0.062
100
79-139
Styrene
mg/kg
.062
0.059
95
79-137
tert-Butyl benzene
mg/kg
.062
0.059
95
74-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 55

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
LABORATORY CONTROL SAMPLE:
Parameter
2023482
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
mg/kg
.062
0.037
60
71-138 L2
Toluene
mg/kg
.062
0.062
99
74-131
trans-1,2-Dichloroethene
mg/kg
.062
0.064
102
67-135
trans- 1,3-Dichloropropene
mg/kg
.062
0.064
103
65-146
Trichloroethene
mg/kg
.062
0.061
98
67-135
Trichlorofluoromethane
mg/kg
.062
0.062
100
59-144
Vinyl acetate
mg/kg
.12
0.15
124
40-160
Vinyl chloride
mg/kg
.062
0.060
97
56-141
Xylene (Total)
mg/kg
.19
0.18
99
76-137
1,2-Dichloroethane-d4 (S)
%
102
70-132
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
Parameter
2024087
Units
92344173002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
.025
0.022
87
70-130
1,1,1-Trichloroethane
mg/kg
ND
.025
0.023
91
70-130
1,1,2,2-Tetrachloroethane
mg/kg
ND
.025
0.021
84
70-130
1,1,2-Trichloroethane
mg/kg
ND
.025
0.021
83
70-130
1,1-Dichloroethane
mg/kg
ND
.025
0.024
98
70-130
1,1-Dichloroethene
mg/kg
ND
.025
0.023
92
49-180
1,1-Dichloropropene
mg/kg
ND
.025
0.022
87
70-130
1,2,3-Trichlorobenzene
mg/kg
ND
.025
0.011
43
70-130 M1
1,2,3-Trichloropropane
mg/kg
ND
.025
0.020
81
70-130
1,2,4-Trichlorobenzene
mg/kg
ND
.025
0.012
47
70-130 M1
1,2,4-Trimethylbenzene
mg/kg
ND
.025
0.021
85
70-130
1,2-Dibromo-3-chloropropane
mg/kg
ND
.025
0.017
69
70-130 M1
1,2-Dibromoethane (EDB)
mg/kg
ND
.025
0.019
76
70-130
1,2-Dichlorobenzene
mg/kg
ND
.025
0.016
63
70-130 M1
1,2-Dichloroethane
mg/kg
ND
.025
0.020
81
70-130
1,2-Dichloropropane
mg/kg
ND
.025
0.023
91
70-130
1,3,5-Trimethylbenzene
mg/kg
ND
.025
0.022
88
70-130
1,3-Dichlorobenzene
mg/kg
ND
.025
0.016
63
70-130 M1
1,3-Dichloropropane
mg/kg
ND
.025
0.022
89
70-130
1,4-Dichlorobenzene
mg/kg
ND
.025
0.016
63
70-130 M1
2,2-Dichloropropane
mg/kg
ND
.025
0.022
90
70-130
2-Butanone (MEK)
mg/kg
ND
.051
.042J
84
70-130
2-Chlorotoluene
mg/kg
ND
.025
0.021
86
70-130
2-Hexanone
mg/kg
ND
.051
.031J
61
70-130 M1
4-Chlorotoluene
mg/kg
ND
.025
0.018
74
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
.051
.041J
81
70-130
Acetone
mg/kg
ND
.051
.058J
116
70-130
Benzene
mg/kg
ND
.025
0.023
93
50-166
Bromobenzene
mg/kg
ND
.025
0.018
71
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
MATRIX SPIKE SAMPLE: 2024087
92344173002 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Bromochloromethane
mg/kg
ND
.025
0.023
92
70-130
Bromodichloromethane
mg/kg
ND
.025
0.022
86
70-130
Bromoform
mg/kg
ND
.025
0.016
65
70-130 M1
Bromomethane
mg/kg
ND
.025
0.021
84
70-130
Carbon tetrachloride
mg/kg
ND
.025
0.023
92
70-130
Chlorobenzene
mg/kg
ND
.025
0.019
76
43-169
Chloroethane
mg/kg
ND
.025
0.025
99
70-130
Chloroform
mg/kg
ND
.025
0.024
94
70-130
Chloromethane
mg/kg
ND
.025
0.024
96
70-130
cis-1,2-Dichloroethene
mg/kg
ND
.025
0.021
85
70-130
cis-1,3-Dichloropropene
mg/kg
ND
.025
0.019
76
70-130
Dibromochloromethane
mg/kg
ND
.025
0.019
77
70-130
Dibromomethane
mg/kg
ND
.025
0.021
84
70-130
Dichlorodifluoromethane
mg/kg
ND
.025
0.019
75
70-130
Diisopropyl ether
mg/kg
ND
.025
0.025
102
70-130
Ethylbenzene
mg/kg
ND
.025
0.022
88
70-130
Hexachloro-1,3-butadiene
mg/kg
ND
.025
0.020
78
70-130
Isopropylbenzene (Cumene)
mg/kg
ND
.025
0.022
86
70-130
m&p-Xylene
mg/kg
ND
.051
0.043
85
70-130
Methyl-tert-butyl ether
mg/kg
ND
.025
0.024
94
70-130
Methylene Chloride
mg/kg
ND
.025
.0191
75
70-130
n-Butylbenzene
mg/kg
ND
.025
0.021
84
70-130
n-Propylbenzene
mg/kg
ND
.025
0.023
90
70-130
Naphthalene
mg/kg
1.9J ug/kg
.025
0.011
35
70-130 M1
o-Xylene
mg/kg
ND
.025
0.021
83
70-130
p-Isopropyltoluene
mg/kg
ND
.025
0.022
89
70-130
sec-Butylbenzene
mg/kg
ND
.025
0.023
92
70-130
Styrene
mg/kg
ND
.025
0.016
64
70-130 M1
tert-Butyl benzene
mg/kg
ND
.025
0.023
90
70-130
Tetrachloroethene
mg/kg
ND
.025
0.014
55
70-130 MO
Toluene
mg/kg
ND
.025
0.022
89
52-163
trans-1,2-Dichloroethene
mg/kg
ND
.025
0.022
87
70-130
trans- 1,3-Dichloropropene
mg/kg
ND
.025
0.016
66
70-130 M1
Trichloroethene
mg/kg
ND
.025
0.020
81
49-167
Trichlorofluoromethane
mg/kg
ND
.025
0.023
93
70-130
Vinyl acetate
mg/kg
ND
.051
.016J
32
70-130 M1
Vinyl chloride
mg/kg
ND
.025
0.022
89
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-132
4-Bromofluorobenzene (S)
%
95
70-130
Toluene-d8(S)
%
101
70-130
SAMPLE DUPLICATE: 2024563
92344173001 Dup
Parameter Units Result Result RPD Qualifiers
1,1,1,2-Tetrachloroethane mg/kg ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
SAMPLE DUPLICATE: 2024563
Parameter
Units
92344173001
Result
Dup
Result
1,1,1-Trichloroethane
mg/kg
ND
ND
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
1,1,2-Trichloroethane
mg/kg
ND
ND
1,1-Dichloroethane
mg/kg
ND
ND
1,1-Dichloroethene
mg/kg
ND
ND
1,1-Dichloropropene
mg/kg
ND
ND
1,2,3-Trichlorobenzene
mg/kg
ND
ND
1,2,3-Trichloropropane
mg/kg
ND
ND
1,2,4-Trichlorobenzene
mg/kg
ND
ND
1,2,4-Trimethylbenzene
mg/kg
ND
ND
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
1,2-Dichlorobenzene
mg/kg
ND
ND
1,2-Dichloroethane
mg/kg
ND
ND
1,2-Dichloropropane
mg/kg
ND
ND
1,3,5-Trimethylbenzene
mg/kg
ND
ND
1,3-Dichlorobenzene
mg/kg
ND
ND
1,3-Dichloropropane
mg/kg
ND
ND
1,4-Dichlorobenzene
mg/kg
ND
ND
2,2-Dichloropropane
mg/kg
ND
ND
2-Butanone (MEK)
mg/kg
ND
ND
2-Chlorotoluene
mg/kg
ND
ND
2-Hexanone
mg/kg
ND
ND
4-Chlorotoluene
mg/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
Acetone
mg/kg
ND
ND
Benzene
mg/kg
ND
ND
Bromobenzene
mg/kg
ND
ND
Bromochloromethane
mg/kg
ND
ND
Bromodichloromethane
mg/kg
ND
ND
Bromoform
mg/kg
ND
ND
Bromomethane
mg/kg
ND
ND
Carbon tetrachloride
mg/kg
ND
ND
Chlorobenzene
mg/kg
ND
ND
Chloroethane
mg/kg
ND
ND
Chloroform
mg/kg
ND
ND
Chloromethane
mg/kg
ND
ND
cis-1,2-Dichloroethene
mg/kg
ND
ND
cis-1,3-Dichloropropene
mg/kg
ND
ND
Dibromochloromethane
mg/kg
ND
ND
Dibromomethane
mg/kg
ND
ND
Dichlorodifluoromethane
mg/kg
ND
ND
Diisopropyl ether
mg/kg
ND
ND
Ethylbenzene
mg/kg
ND
ND
Hexachloro-1,3-butadiene
mg/kg
ND
ND
Isopropylbenzene (Cumene)
mg/kg
ND
ND
m&p-Xylene
mg/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
SAMPLE DUPLICATE: 2024563
Parameter
Units
92344173001
Result
Dup
Result
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
3.7J ug/kg
ND
o-Xylene
mg/kg
ND
ND
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
ND
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
101
100
4-Bromofluorobenzene (S)
%
91
96
Toluene-d8 (S)
%
99
99
RPD Qualifiers
79
83
79
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC.
Page 36 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
QC Batch: 365182 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92344137004, 92344137006
METHOD BLANK: 2024773
Associated Lab Samples: 92344137004, 92344137006
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0064
06/16/17 13:20
1,1,1-Trichloroethane
mg/kg
ND
0.0064
06/16/17 13:20
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0064
06/16/17 13:20
1,1,2-Trichloroethane
mg/kg
ND
0.0064
06/16/17 13:20
1,1-Dichloroethane
mg/kg
ND
0.0064
06/16/17 13:20
1,1-Dichloroethene
mg/kg
ND
0.0064
06/16/17 13:20
1,1-Dichloropropene
mg/kg
ND
0.0064
06/16/17 13:20
1,2,3-Trichlorobenzene
mg/kg
ND
0.0064
06/16/17 13:20
1,2,3-Trichloropropane
mg/kg
ND
0.0064
06/16/17 13:20
1,2,4-Trichlorobenzene
mg/kg
ND
0.0064
06/16/17 13:20
1,2,4-Trimethylbenzene
mg/kg
ND
0.0064
06/16/17 13:20
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0064
06/16/17 13:20
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0064
06/16/17 13:20
1,2-Dichlorobenzene
mg/kg
ND
0.0064
06/16/17 13:20
1,2-Dichloroethane
mg/kg
ND
0.0064
06/16/17 13:20
1,2-Dichloropropane
mg/kg
ND
0.0064
06/16/17 13:20
1,3,5-Trimethylbenzene
mg/kg
ND
0.0064
06/16/17 13:20
1,3-Dichlorobenzene
mg/kg
ND
0.0064
06/16/17 13:20
1,3-Dichloropropane
mg/kg
ND
0.0064
06/16/17 13:20
1,4-Dichlorobenzene
mg/kg
ND
0.0064
06/16/17 13:20
2,2-Dichloropropane
mg/kg
ND
0.0064
06/16/17 13:20
2-Butanone (MEK)
mg/kg
ND
0.13
06/16/17 13:20
2-Chlorotoluene
mg/kg
ND
0.0064
06/16/17 13:20
2-Hexanone
mg/kg
ND
0.064
06/16/17 13:20
4-Chlorotoluene
mg/kg
ND
0.0064
06/16/17 13:20
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.064
06/16/17 13:20
Acetone
mg/kg
ND
0.13
06/16/17 13:20
Benzene
mg/kg
ND
0.0064
06/16/17 13:20
Bromobenzene
mg/kg
ND
0.0064
06/16/17 13:20
Bromochloromethane
mg/kg
ND
0.0064
06/16/17 13:20
Bromodichloromethane
mg/kg
ND
0.0064
06/16/17 13:20
Bromoform
mg/kg
ND
0.0064
06/16/17 13:20
Bromomethane
mg/kg
ND
0.013
06/16/17 13:20
Carbon tetrachloride
mg/kg
ND
0.0064
06/16/17 13:20
Chlorobenzene
mg/kg
ND
0.0064
06/16/17 13:20
Chloroethane
mg/kg
ND
0.013
06/16/17 13:20
Chloroform
mg/kg
ND
0.0064
06/16/17 13:20
Chloromethane
mg/kg
ND
0.013
06/16/17 13:20
cis-1,2-Dichloroethene
mg/kg
ND
0.0064
06/16/17 13:20
cis-1,3-Dichloropropene
mg/kg
ND
0.0064
06/16/17 13:20
Dibromochloromethane
mg/kg
ND
0.0064
06/16/17 13:20
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
METHOD BLANK: 2024773
Associated Lab Samples: 92344137004, 92344137006
Parameter Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Dibromomethane
mg/kg
ND
0.0064
06/16/17 13:20
Dichlorodifluoromethane
mg/kg
ND
0.013
06/16/17 13:20
Diisopropyl ether
mg/kg
ND
0.0064
06/16/17 13:20
Ethylbenzene
mg/kg
ND
0.0064
06/16/17 13:20
Hexachloro-1,3-butadiene
mg/kg
ND
0.0064
06/16/17 13:20
Isopropylbenzene (Cumene)
mg/kg
ND
0.0064
06/16/17 13:20
m&p-Xylene
mg/kg
ND
0.013
06/16/17 13:20
Methyl-tert-butyl ether
mg/kg
ND
0.0064
06/16/17 13:20
Methylene Chloride
mg/kg
ND
0.026
06/16/17 13:20
n-Butylbenzene
mg/kg
ND
0.0064
06/16/17 13:20
n-Propylbenzene
mg/kg
ND
0.0064
06/16/17 13:20
Naphthalene
mg/kg
ND
0.0064
06/16/17 13:20
o-Xylene
mg/kg
ND
0.0064
06/16/17 13:20
p-Isopropyltoluene
mg/kg
ND
0.0064
06/16/17 13:20
sec-Butylbenzene
mg/kg
ND
0.0064
06/16/17 13:20
Styrene
mg/kg
ND
0.0064
06/16/17 13:20
tert-Butyl benzene
mg/kg
ND
0.0064
06/16/17 13:20
Tetrachloroethene
mg/kg
ND
0.0064
06/16/17 13:20
Toluene
mg/kg
ND
0.0064
06/16/17 13:20
trans-1,2-Dichloroethene
mg/kg
ND
0.0064
06/16/17 13:20
trans- 1,3-Dichloropropene
mg/kg
ND
0.0064
06/16/17 13:20
Trichloroethene
mg/kg
ND
0.0064
06/16/17 13:20
Trichlorofluoromethane
mg/kg
ND
0.0064
06/16/17 13:20
Vinyl acetate
mg/kg
ND
0.064
06/16/17 13:20
Vinyl chloride
mg/kg
ND
0.013
06/16/17 13:20
Xylene (Total)
mg/kg
ND
0.013
06/16/17 13:20
1,2-Dichloroethane-d4 (S)
%
98
70-132
06/16/17 13:20
4-Bromofluorobenzene (S)
%
97
70-130
06/16/17 13:20
Toluene-d8 (S)
%
101
70-130
06/16/17 13:20
Qualifiers
LABORATORY CONTROL SAMPLE:
2024774
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
.059
0.056
96
74-137
1,1,1-Trichloroethane
mg/kg
.059
0.055
95
67-140
1,1,2,2-Tetrachloroethane
mg/kg
.059
0.060
102
72-141
1,1,2-Trichloroethane
mg/kg
.059
0.057
97
78-138
1,1-Dichloroethane
mg/kg
.059
0.060
102
69-134
1,1-Dichloroethene
mg/kg
.059
0.059
101
67-138
1,1-Dichloropropene
mg/kg
.059
0.059
100
69-139
1,2,3-Trichlorobenzene
mg/kg
.059
0.060
102
70-146
1,2,3-Trichloropropane
mg/kg
.059
0.059
101
69-144
1,2,4-Trichlorobenzene
mg/kg
.059
0.059
100
68-148
1,2,4-Trimethylbenzene
mg/kg
.059
0.060
102
74-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 55

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
LABORATORY CONTROL SAMPLE:
Parameter
2024774
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
mg/kg
.059
0.058
99
65-140
1,2-Dibromoethane (EDB)
mg/kg
.059
0.057
98
77-135
1,2-Dichlorobenzene
mg/kg
.059
0.059
100
77-141
1,2-Dichloroethane
mg/kg
.059
0.056
95
65-137
1,2-Dichloropropane
mg/kg
.059
0.059
100
72-136
1,3,5-Trimethylbenzene
mg/kg
.059
0.060
103
76-133
1,3-Dichlorobenzene
mg/kg
.059
0.059
101
74-138
1,3-Dichloropropane
mg/kg
.059
0.060
103
71-139
1,4-Dichlorobenzene
mg/kg
.059
0.060
102
76-138
2,2-Dichloropropane
mg/kg
.059
0.057
97
68-137
2-Butanone (MEK)
mg/kg
.12
0.12
102
58-147
2-Chlorotoluene
mg/kg
.059
0.061
105
73-139
2-Hexanone
mg/kg
.12
0.12
104
62-145
4-Chlorotoluene
mg/kg
.059
0.060
102
76-141
4-Methyl-2-pentanone (MIBK)
mg/kg
.12
0.12
107
64-149
Acetone
mg/kg
.12
.111
94
53-153
Benzene
mg/kg
.059
0.060
102
73-135
Bromobenzene
mg/kg
.059
0.060
103
75-133
Bromochloromethane
mg/kg
.059
0.062
106
73-134
Bromodichloromethane
mg/kg
.059
0.058
100
71-135
Bromoform
mg/kg
.059
0.054
93
66-141
Bromomethane
mg/kg
.059
0.062
106
53-160
Carbon tetrachloride
mg/kg
.059
0.056
95
60-145
Chlorobenzene
mg/kg
.059
0.059
101
78-130
Chloroethane
mg/kg
.059
0.061
105
64-149
Chloroform
mg/kg
.059
0.058
99
70-134
Chloromethane
mg/kg
.059
0.065
111
52-150
cis-1,2-Dichloroethene
mg/kg
.059
0.060
102
70-133
cis-1,3-Dichloropropene
mg/kg
.059
0.060
103
68-134
Dibromochloromethane
mg/kg
.059
0.059
100
71-138
Dibromomethane
mg/kg
.059
0.058
100
74-130
Dichlorodifluoromethane
mg/kg
.059
0.055
93
40-160
Diisopropyl ether
mg/kg
.059
0.063
108
69-141
Ethylbenzene
mg/kg
.059
0.060
102
75-133
Hexachloro-1,3-butadiene
mg/kg
.059
0.060
102
68-143
Isopropylbenzene (Cumene)
mg/kg
.059
0.059
101
76-143
m&p-Xylene
mg/kg
.12
0.12
101
75-136
Methyl-tert-butyl ether
mg/kg
.059
0.058
100
68-144
Methylene Chloride
mg/kg
.059
0.054
92
45-154
n-Butylbenzene
mg/kg
.059
0.061
104
72-137
n-Propylbenzene
mg/kg
.059
0.060
103
76-136
Naphthalene
mg/kg
.059
0.061
103
68-151
o-Xylene
mg/kg
.059
0.059
101
76-141
p-Isopropyltoluene
mg/kg
.059
0.060
103
76-140
sec-Butylbenzene
mg/kg
.059
0.060
102
79-139
Styrene
mg/kg
.059
0.056
96
79-137
tert-Butyl benzene
mg/kg
.059
0.057
97
74-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 55

aceAnalytical
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2225 Riverside Dr.
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[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
LABORATORY CONTROL SAMPLE:
Parameter
2024774
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
mg/kg
.059
0.036
62
71-138 L2
Toluene
mg/kg
.059
0.060
103
74-131
trans-1,2-Dichloroethene
mg/kg
.059
0.060
102
67-135
trans- 1,3-Dichloropropene
mg/kg
.059
0.059
100
65-146
Trichloroethene
mg/kg
.059
0.058
99
67-135
Trichlorofluoromethane
mg/kg
.059
0.059
100
59-144
Vinyl acetate
mg/kg
.12
0.14
116
40-160
Vinyl chloride
mg/kg
.059
0.058
99
56-141
Xylene (Total)
mg/kg
.18
0.18
101
76-137
1,2-Dichloroethane-d4 (S)
%
97
70-132
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
2025427
Units
92344347001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
.018
0.011
65
70-130 M1
1,1,1-Trichloroethane
mg/kg
ND
.018
0.015
83
70-130
1,1,2,2-Tetrachloroethane
mg/kg
ND
.018
0.012
70
70-130
1,1,2-Trichloroethane
mg/kg
ND
.018
0.011
63
70-130 M1
1,1-Dichloroethane
mg/kg
ND
.018
0.013
73
70-130
1,1-Dichloroethene
mg/kg
ND
.018
0.014
82
49-180
1,1-Dichloropropene
mg/kg
ND
.018
0.015
85
70-130
1,2,3-Trichlorobenzene
mg/kg
ND
.018
0.011
61
70-130 M1
1,2,3-Trichloropropane
mg/kg
ND
.018
0.013
75
70-130
1,2,4-Trichlorobenzene
mg/kg
ND
.018
0.011
61
70-130 M1
1,2,4-Trimethylbenzene
mg/kg
ND
.018
0.019
110
70-130
1,2-Dibromo-3-chloropropane
mg/kg
ND
.018
0.010
58
70-130 M1
1,2-Dibromoethane (EDB)
mg/kg
ND
.018
0.011
62
70-130 M1
1,2-Dichlorobenzene
mg/kg
ND
.018
0.012
66
70-130 M1
1,2-Dichloroethane
mg/kg
ND
.018
0.012
68
70-130 M1
1,2-Dichloropropane
mg/kg
ND
.018
0.012
69
70-130 M1
1,3,5-Trimethylbenzene
mg/kg
ND
.018
0.013
73
70-130
1,3-Dichlorobenzene
mg/kg
ND
.018
0.012
67
70-130 M1
1,3-Dichloropropane
mg/kg
ND
.018
0.012
65
70-130 M1
1,4-Dichlorobenzene
mg/kg
ND
.018
0.012
67
70-130 M1
2,2-Dichloropropane
mg/kg
ND
.018
0.014
82
70-130
2-Butanone (MEK)
mg/kg
ND
.035
.03J
86
70-130
2-Chlorotoluene
mg/kg
ND
.018
0.013
73
70-130
2-Hexanone
mg/kg
ND
.035
.025J
71
70-130
4-Chlorotoluene
mg/kg
ND
.018
0.012
69
70-130 M1
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
.035
.024J
69
70-130 M1
Acetone
mg/kg
ND
.035
.051J
-5
70-130 M1
Benzene
mg/kg
ND
.018
0.013
73
50-166
Bromobenzene
mg/kg
ND
.018
0.011
64
70-130 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
MATRIX SPIKE SAMPLE: 2025427
92344347001 Spike MS MS % Rec
Parameter Units Result Conc. Result % Rec Limits Qualifiers
Bromochloromethane
mg/kg
ND
.018
0.012
67
70-130 M1
Bromodichloromethane
mg/kg
ND
.018
0.012
69
70-130 M1
Bromoform
mg/kg
ND
.018
0.010
58
70-130 M1
Bromomethane
mg/kg
ND
.018
.0072J
41
70-130 M1
Carbon tetrachloride
mg/kg
ND
.018
0.015
83
70-130
Chlorobenzene
mg/kg
ND
.018
0.013
71
43-169
Chloroethane
mg/kg
ND
.018
0.013
75
70-130
Chloroform
mg/kg
ND
.018
0.012
70
70-130
Chloromethane
mg/kg
ND
.018
0.011
61
70-130 M1
cis-1,2-Dichloroethene
mg/kg
ND
.018
0.013
71
70-130
cis-1,3-Dichloropropene
mg/kg
ND
.018
0.012
67
70-130 M1
Dibromochloromethane
mg/kg
ND
.018
0.011
64
70-130 M1
Dibromomethane
mg/kg
ND
.018
0.011
62
70-130 M1
Dichlorodifluoromethane
mg/kg
ND
.018
.0068J
38
70-130 M1
Diisopropyl ether
mg/kg
ND
.018
0.013
72
70-130
Ethylbenzene
mg/kg
ND
.018
0.013
76
70-130
Hexachloro-1,3-butadiene
mg/kg
ND
.018
0.014
77
70-130
Isopropylbenzene (Cumene)
mg/kg
ND
.018
0.014
77
70-130
m&p-Xylene
mg/kg
ND
.035
0.026
74
70-130
Methyl-tert-butyl ether
mg/kg
ND
.018
0.010
58
70-130 M1
Methylene Chloride
mg/kg
ND
.018
0.019
67
70-130 M1
n-Butylbenzene
mg/kg
ND
.018
0.014
80
70-130
n-Propylbenzene
mg/kg
ND
.018
0.014
79
70-130
Naphthalene
mg/kg
ND
.018
0.010
58
70-130 M1
o-Xylene
mg/kg
ND
.018
0.012
71
70-130
p-Isopropyltoluene
mg/kg
ND
.018
0.014
78
70-130
sec-Butylbenzene
mg/kg
ND
.018
0.014
82
70-130
Styrene
mg/kg
ND
.018
0.011
64
70-130 M1
tert-Butyl benzene
mg/kg
ND
.018
0.013
74
70-130
Tetrachloroethene
mg/kg
ND
.018
0.0088
50
70-130 MO
Toluene
mg/kg
ND
.018
0.013
75
52-163
trans-1,2-Dichloroethene
mg/kg
ND
.018
0.014
77
70-130
trans- 1,3-Dichloropropene
mg/kg
ND
.018
0.011
63
70-130 M1
Trichloroethene
mg/kg
ND
.018
0.013
74
49-167
Trichlorofluoromethane
mg/kg
ND
.018
0.015
82
70-130
Vinyl acetate
mg/kg
ND
.035
.04J
114
70-130
Vinyl chloride
mg/kg
ND
.018
0.011
63
70-130 M1
1,2-Dichloroethane-d4 (S)
%
105
70-132
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 2025426
92344307001 Dup
Parameter Units Result Result RPD Qualifiers
1,1,1,2-Tetrachloroethane mg/kg ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
SAMPLE DUPLICATE: 2025426
Parameter
Units
92344307001
Result
Dup
Result
1,1,1-Trichloroethane
mg/kg
ND
ND
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
1,1,2-Trichloroethane
mg/kg
ND
ND
1,1-Dichloroethane
mg/kg
ND
ND
1,1-Dichloroethene
mg/kg
ND
ND
1,1-Dichloropropene
mg/kg
ND
ND
1,2,3-Trichlorobenzene
mg/kg
ND
ND
1,2,3-Trichloropropane
mg/kg
ND
ND
1,2,4-Trichlorobenzene
mg/kg
ND
ND
1,2,4-Trimethylbenzene
mg/kg
ND
ND
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
1,2-Dichlorobenzene
mg/kg
ND
ND
1,2-Dichloroethane
mg/kg
ND
ND
1,2-Dichloropropane
mg/kg
ND
ND
1,3,5-Trimethylbenzene
mg/kg
ND
ND
1,3-Dichlorobenzene
mg/kg
ND
ND
1,3-Dichloropropane
mg/kg
ND
ND
1,4-Dichlorobenzene
mg/kg
ND
ND
2,2-Dichloropropane
mg/kg
ND
ND
2-Butanone (MEK)
mg/kg
ND
ND
2-Chlorotoluene
mg/kg
ND
ND
2-Hexanone
mg/kg
ND
ND
4-Chlorotoluene
mg/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
Acetone
mg/kg
ND
.039J
Benzene
mg/kg
ND
ND
Bromobenzene
mg/kg
ND
ND
Bromochloromethane
mg/kg
ND
ND
Bromodichloromethane
mg/kg
ND
ND
Bromoform
mg/kg
ND
ND
Bromomethane
mg/kg
ND
ND
Carbon tetrachloride
mg/kg
ND
ND
Chlorobenzene
mg/kg
ND
ND
Chloroethane
mg/kg
ND
ND
Chloroform
mg/kg
ND
ND
Chloromethane
mg/kg
ND
ND
cis-1,2-Dichloroethene
mg/kg
ND
ND
cis-1,3-Dichloropropene
mg/kg
ND
ND
Dibromochloromethane
mg/kg
ND
ND
Dibromomethane
mg/kg
ND
ND
Dichlorodifluoromethane
mg/kg
ND
ND
Diisopropyl ether
mg/kg
ND
ND
Ethylbenzene
mg/kg
ND
ND
Hexachloro-1,3-butadiene
mg/kg
ND
ND
Isopropylbenzene (Cumene)
mg/kg
ND
ND
m&p-Xylene
mg/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
SAMPLE DUPLICATE: 2025426
Parameter
Units
92344307001
Result
Dup
Result
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
.0066J
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
o-Xylene
mg/kg
ND
ND
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
ND
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
94
103
4-Bromofluorobenzene (S)
%
99
98
Toluene-d8 (S)
%
100
101
RPD Qualifiers
7
2
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC.
Page 43 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
QC Batch: 364950 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137004, 92344137005, 92344137006
METHOD BLANK: 2023230 Matrix: Solid
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137004, 92344137005, 92344137006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
06/15/17 15:39
1,2-Dichlorobenzene
mg/kg
ND
0.33
06/15/17 15:39
1,3-Dichlorobenzene
mg/kg
ND
0.33
06/15/17 15:39
1,4-Dichlorobenzene
mg/kg
ND
0.33
06/15/17 15:39
1-Methylnaphthalene
mg/kg
ND
0.33
06/15/17 15:39
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
06/15/17 15:39
2,4,5-Trichlorophenol
mg/kg
ND
0.33
06/15/17 15:39
2,4,6-Trichlorophenol
mg/kg
ND
0.33
06/15/17 15:39
2,4-Dichlorophenol
mg/kg
ND
0.33
06/15/17 15:39
2,4-Dimethylphenol
mg/kg
ND
0.33
06/15/17 15:39
2,4-Dinitrophenol
mg/kg
ND
1.6
06/15/17 15:39
2,4-Dinitrotoluene
mg/kg
ND
0.33
06/15/17 15:39
2,6-Dinitrotoluene
mg/kg
ND
0.33
06/15/17 15:39
2-Chloronaphthalene
mg/kg
ND
0.33
06/15/17 15:39
2-Chlorophenol
mg/kg
ND
0.33
06/15/17 15:39
2-Methylnaphthalene
mg/kg
ND
0.33
06/15/17 15:39
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
06/15/17 15:39
2-Nitroaniline
mg/kg
ND
1.6
06/15/17 15:39
2-Nitrophenol
mg/kg
ND
0.33
06/15/17 15:39
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
0.33
06/15/17 15:39
3,3'-Dichlorobenzidine
mg/kg
ND
1.6
06/15/17 15:39
3-Nitroaniline
mg/kg
ND
1.6
06/15/17 15:39
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.66
06/15/17 15:39
4-Bromophenylphenyl ether
mg/kg
ND
0.33
06/15/17 15:39
4-Chloro-3-methyl phenol
mg/kg
ND
0.66
06/15/17 15:39
4-Chloroaniline
mg/kg
ND
1.6
06/15/17 15:39
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
06/15/17 15:39
4-Nitroaniline
mg/kg
ND
0.66
06/15/17 15:39
4-Nitrophenol
mg/kg
ND
1.6
06/15/17 15:39
Acenaphthene
mg/kg
ND
0.33
06/15/17 15:39
Acenaphthylene
mg/kg
ND
0.33
06/15/17 15:39
Aniline
mg/kg
ND
0.33
06/15/17 15:39
Anthracene
mg/kg
ND
0.33
06/15/17 15:39
Benzo(a)anthracene
mg/kg
ND
0.33
06/15/17 15:39
Benzo(a)pyrene
mg/kg
ND
0.33
06/15/17 15:39
Benzo(b)fluoranthene
mg/kg
ND
0.33
06/15/17 15:39
Benzo(g,h,i)perylene
mg/kg
ND
0.33
06/15/17 15:39
Benzo(k)fluoranthene
mg/kg
ND
0.33
06/15/17 15:39
Benzoic Acid
mg/kg
ND
1.6
06/15/17 15:39
Benzyl alcohol
mg/kg
ND
0.66
06/15/17 15:39
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
06/15/17 15:39
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
METHOD BLANK: 2023230 Matrix: Solid
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137004, 92344137005, 92344137006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
06/15/17 15:39
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
06/15/17 15:39
Butylbenzylphthalate
mg/kg
ND
0.33
06/15/17 15:39
Chrysene
mg/kg
ND
0.33
06/15/17 15:39
Di-n-butylphthalate
mg/kg
ND
0.33
06/15/17 15:39
Di-n-octylphthalate
mg/kg
ND
0.33
06/15/17 15:39
Dibenz(a,h)anthracene
mg/kg
ND
0.33
06/15/17 15:39
Dibenzofuran
mg/kg
ND
0.33
06/15/17 15:39
Diethylphthalate
mg/kg
ND
0.33
06/15/17 15:39
Dimethylphthalate
mg/kg
ND
0.33
06/15/17 15:39
Fluoranthene
mg/kg
ND
0.33
06/15/17 15:39
Fluorene
mg/kg
ND
0.33
06/15/17 15:39
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
06/15/17 15:39
Hexachlorobenzene
mg/kg
ND
0.33
06/15/17 15:39
Hexachlorocyclopentadiene
mg/kg
ND
0.33
06/15/17 15:39
Hexachloroethane
mg/kg
ND
0.33
06/15/17 15:39
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
06/15/17 15:39
Isophorone
mg/kg
ND
0.33
06/15/17 15:39
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
06/15/17 15:39
N-Nitrosodimethylamine
mg/kg
ND
0.33
06/15/17 15:39
N-Nitrosodiphenylamine
mg/kg
ND
0.33
06/15/17 15:39
Naphthalene
mg/kg
ND
0.33
06/15/17 15:39
Nitrobenzene
mg/kg
ND
0.33
06/15/17 15:39
Pentachlorophenol
mg/kg
ND
1.6
06/15/17 15:39
Phenanthrene
mg/kg
ND
0.33
06/15/17 15:39
Phenol
mg/kg
ND
0.33
06/15/17 15:39
Pyrene
mg/kg
ND
0.33
06/15/17 15:39
2,4,6-Tribromophenol (S)
%
78
27-110
06/15/17 15:39
2-Fluorobiphenyl (S)
%
76
30-110
06/15/17 15:39
2-Fluorophenol (S)
%
69
13-110
06/15/17 15:39
Nitrobenzene-d5 (S)
%
67
23-110
06/15/17 15:39
Phenol-d6 (S)
%
68
22-110
06/15/17 15:39
Terphenyl-d14 (S)
%
90
28-110
06/15/17 15:39
LABORATORY CONTROL SAMPLE:
2023231
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.1
69
36-120
1,2-Dichlorobenzene
mg/kg
1.7
1.1
66
41-120
1,3-Dichlorobenzene
mg/kg
1.7
1.1
66
66-120
1,4-Dichlorobenzene
mg/kg
1.7
1.1
64
42-120
1-Methylnaphthalene
mg/kg
1.7
1.2
73
40-120
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
0.87
52
17-120
2,4,5-Trichlorophenol
mg/kg
1.7
1.3
78
37-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 55

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
LABORATORY CONTROL SAMPLE:
Parameter
2023231
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,6-TrichIorophenol
mg/kg
1.7
1.4
87
40-120
2,4-DichIorophenol
mg/kg
1.7
1.3
75
33-120
2,4-Dimethylphenol
mg/kg
1.7
1.3
77
36-120
2,4-Dinitrophenol
mg/kg
8.3
7.2
86
22-121
2,4-Dinitrotoluene
mg/kg
1.7
1.5
88
60-120
2,6-Dinitrotoluene
mg/kg
1.7
1.5
88
54-120
2-Chloronaphthalene
mg/kg
1.7
1.2
73
41-120
2-Chlorophenol
mg/kg
1.7
1.3
77
39-120
2-Methylnaphthalene
mg/kg
1.7
1.2
71
26-120
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.2
71
41-120
2-Nitroaniline
mg/kg
3.3
2.7
81
45-120
2-Nitrophenol
mg/kg
1.7
1.2
73
35-120
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
1.2
71
35-120
3,3'-Dichlorobenzidine
mg/kg
3.3
2.6
78
16-125
3-Nitroaniline
mg/kg
3.3
2.8
85
45-120
4,6-Dinitro-2-methyl phenol
mg/kg
3.3
2.7
81
46-120
4-Bromophenylphenyl ether
mg/kg
1.7
1.0
61
36-120
4-Chloro-3-methylphenol
mg/kg
3.3
2.7
80
37-120
4-Chloroaniline
mg/kg
3.3
2.3
70
35-120
4-Chlorophenylphenyl ether
mg/kg
1.7
1.3
78
30-120
4-Nitroaniline
mg/kg
3.3
3.1
92
48-120
4-Nitrophenol
mg/kg
8.3
7.5
90
43-120
Acenaphthene
mg/kg
1.7
1.3
80
46-120
Acenaphthylene
mg/kg
1.7
1.3
76
46-120
Aniline
mg/kg
1.7
1.0
61
33-120
Anthracene
mg/kg
1.7
1.2
72
63-120
Benzo(a)anthracene
mg/kg
1.7
1.2
74
61-120
Benzo(a)pyrene
mg/kg
1.7
1.3
77
59-120
Benzo(b)fluoranthene
mg/kg
1.7
1.2
75
55-120
Benzo(g,h,i)perylene
mg/kg
1.7
1.3
75
57-120
Benzo(k)fluoranthene
mg/kg
1.7
1.3
77
56-120
Benzoic Acid
mg/kg
8.3
5.2
62
13-120
Benzyl alcohol
mg/kg
3.3
2.6
77
34-120
bis(2-Chloroethoxy)methane
mg/kg
1.7
0.95
57
21-120
bis(2-Chloroethyl) ether
mg/kg
1.7
0.99
60
25-120
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.4
84
56-123
Butylbenzylphthalate
mg/kg
1.7
1.4
83
57-120
Chrysene
mg/kg
1.7
1.2
75
64-120
Di-n-butylphthalate
mg/kg
1.7
1.4
82
58-120
Di-n-octylphthalate
mg/kg
1.7
1.3
79
47-121
Dibenz(a,h)anthracene
mg/kg
1.7
1.3
79
56-120
Dibenzofuran
mg/kg
1.7
1.4
83
43-120
Diethylphthalate
mg/kg
1.7
1.5
91
55-120
Dimethylphthalate
mg/kg
1.7
1.5
89
54-120
Fluoranthene
mg/kg
1.7
1.3
77
61-120
Fluorene
mg/kg
1.7
1.4
82
51-120
Hexachloro-1,3-butadiene
mg/kg
1.7
1.1
69
22-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
LABORATORY CONTROL SAMPLE:
Parameter
2023231
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachlorobenzene
mg/kg
1.7
1.2
73
53-120
Hexachlorocyclopentadiene
mg/kg
1.7
1.1
64
18-150
Hexachloroethane
mg/kg
1.7
1.1
66
39-120
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.3
79
58-120
Isophorone
mg/kg
1.7
1.1
67
38-120
N-Nitroso-di-n-propylamine
mg/kg
1.7
1.2
74
30-120
N-Nitrosodimethylamine
mg/kg
1.7
1.1
65
32-120
N-Nitrosodiphenylamine
mg/kg
1.7
1.2
73
50-120
Naphthalene
mg/kg
1.7
1.1
68
38-120
Nitrobenzene
mg/kg
1.7
1.1
63
37-120
Pentachlorophenol
mg/kg
3.3
2.7
82
10-120
Phenanthrene
mg/kg
1.7
1.2
73
62-120
Phenol
mg/kg
1.7
1.3
76
37-120
Pyrene
mg/kg
1.7
1.2
70
63-120
2,4,6-Tribromophenol (S)
%
86
27-110
2-Fluorobiphenyl (S)
%
73
30-110
2-Fluorophenol(S)
%
75
13-110
Nitrobenzene-d5 (S)
%
67
23-110
Phenol-d6 (S)
%
76
22-110
Terphenyl-d14 (S)
%
88
28-110
SAMPLE DUPLICATE: 2023233
Parameter
Units
92344173002
Result
Dup
Result RPD Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
ND
1,2-Dichlorobenzene
mg/kg
ND
ND
1,3-Dichlorobenzene
mg/kg
ND
ND
1,4-Dichlorobenzene
mg/kg
ND
ND
1-Methylnaphthalene
mg/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
ND
2,4,5-Trichlorophenol
mg/kg
ND
ND
2,4,6-Trichlorophenol
mg/kg
ND
ND
2,4-Dichlorophenol
mg/kg
ND
ND
2,4-Dimethylphenol
mg/kg
ND
ND
2,4-Dinitrophenol
mg/kg
ND
ND
2,4-Dinitrotoluene
mg/kg
ND
ND
2,6-Dinitrotoluene
mg/kg
ND
ND
2-Chloronaphthalene
mg/kg
ND
ND
2-Chlorophenol
mg/kg
ND
ND
2-Methylnaphthalene
mg/kg
ND
ND
2-Methylphenol(o-Cresol)
mg/kg
ND
ND
2-Nitroaniline
mg/kg
ND
ND
2-Nitrophenol
mg/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
ND
3,3'-Dichlorobenzidine
mg/kg
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
SAMPLE DUPLICATE: 2023233
Parameter
Units
92344173002
Result
Dup
Result
3-Nitroaniline
mg/kg
ND
ND
4,6-Dinitro-2-methyl phenol
mg/kg
ND
ND
4-Bromophenylphenyl ether
mg/kg
ND
ND
4-Chloro-3-methylphenol
mg/kg
ND
ND
4-Chloroaniline
mg/kg
ND
ND
4-Chlorophenylphenyl ether
mg/kg
ND
ND
4-Nitroaniline
mg/kg
ND
ND
4-Nitrophenol
mg/kg
ND
ND
Acenaphthene
mg/kg
ND
ND
Acenaphthylene
mg/kg
ND
ND
Aniline
mg/kg
ND
ND
Anthracene
mg/kg
ND
ND
Benzo(a)anthracene
mg/kg
ND
ND
Benzo(a)pyrene
mg/kg
ND
ND
Benzo(b)fluoranthene
mg/kg
ND
ND
Benzo(g,h,i)perylene
mg/kg
ND
ND
Benzo(k)fluoranthene
mg/kg
ND
ND
Benzoic Acid
mg/kg
ND
ND
Benzyl alcohol
mg/kg
ND
ND
bis(2-Chloroethoxy)methane
mg/kg
ND
ND
bis(2-Chloroethyl) ether
mg/kg
ND
ND
bis(2-Ethylhexyl)phthalate
mg/kg
ND
ND
Butylbenzylphthalate
mg/kg
ND
ND
Chrysene
mg/kg
ND
ND
Di-n-butylphthalate
mg/kg
ND
ND
Di-n-octylphthalate
mg/kg
ND
ND
Dibenz(a,h)anthracene
mg/kg
ND
ND
Dibenzofuran
mg/kg
ND
ND
Diethylphthalate
mg/kg
ND
ND
Dimethylphthalate
mg/kg
ND
ND
Fluoranthene
mg/kg
ND
ND
Fluorene
mg/kg
ND
ND
Hexachloro-1,3-butadiene
mg/kg
ND
ND
Hexachlorobenzene
mg/kg
ND
ND
Hexachlorocyclopentadiene
mg/kg
ND
ND
Hexachloroethane
mg/kg
ND
ND
Indeno(1,2,3-cd)pyrene
mg/kg
ND
ND
Isophorone
mg/kg
ND
ND
N-Nitroso-di-n-propylamine
mg/kg
ND
ND
N-Nitrosodimethylamine
mg/kg
ND
ND
N-Nitrosodiphenylamine
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
Nitrobenzene
mg/kg
ND
ND
Pentachlorophenol
mg/kg
ND
ND
Phenanthrene
mg/kg
ND
ND
Phenol
mg/kg
ND
ND
Pyrene
mg/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 48 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
SAMPLE DUPLICATE: 2023233
92344173002
Dup
Parameter
Units
Result
Result
RPD Qualifiers
2,4,6-Tribromophenol (S)
%
0
0
S4
2-Fluorobiphenyl (S)
%
0
0
S4
2-Fluorophenol(S)
%
0
0
S4
Nitrobenzene-d5 (S)
%
0
0
D3,S4
Phenol-d6 (S)
%
0
0
S4
Terphenyl-d14 (S)
%
0
0
S4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC.
Page 49 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
QC Batch: 364980 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92344137001, 92344137002, 92344137003, 92344137004, 92344137005, 92344137006
SAMPLE DUPLICATE: 2023516
92344208001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 13.6 13.8 2
SAMPLE DUPLICATE: 2023517
92344237002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 90.8 90.8 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 55

Pace Analytical Services, LLC
ceAnalX cal ® hevi Riverside 04
Asheville, NC 28804
www.pacelabs.com [phone]
QUALIFIERS
Project: 1420 Riverside Dr.
Pace Project No.: 92344137
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
1g The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
10 The internal standard response was outside the laboratory acceptance limits confirmed by reanalysis. The results
reported are from the most QC compliant analysis.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
S1 Surrogate recovery outside laboratory control limits (confirmed by re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/21 /2017 08:13 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 55

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
1420 Riverside Dr.
92344137
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92344137001
SB-1
EPA 3050
364868
EPA 6010
365483
92344137002
SB-2
EPA 3050
364868
EPA 6010
365483
92344137003
SB-3
EPA 3050
364868
EPA 6010
365483
92344137004
SB-4
EPA 3050
364868
EPA 6010
365483
92344137005
SB-5
EPA 3050
364868
EPA 6010
365483
92344137006
SB-6
EPA 3050
364868
EPA 6010
365483
92344137001
SB-1
EPA 7471
364821
EPA 7471
364888
92344137002
SB-2
EPA 7471
364821
EPA 7471
364888
92344137003
SB-3
EPA 7471
364821
EPA 7471
364888
92344137004
SB-4
EPA 7471
364821
EPA 7471
364888
92344137005
SB-5
EPA 7471
364821
EPA 7471
364888
92344137006
SB-6
EPA 7471
364821
EPA 7471
364888
92344137001
SB-1
EPA 3546
364950
EPA 8270
365031
92344137002
SB-2
EPA 3546
364950
EPA 8270
365031
92344137003
SB-3
EPA 3546
364950
EPA 8270
365031
92344137004
SB-4
EPA 3546
364950
EPA 8270
365031
92344137005
SB-5
EPA 3546
364950
EPA 8270
365031
92344137006
SB-6
EPA 3546
364950
EPA 8270
365031
92344137001
SB-1
EPA 8260
364974
92344137002
SB-2
EPA 8260
364974
92344137003
SB-3
EPA 8260
364974
92344137004
SB-4
EPA 8260
365182
92344137005
SB-5
EPA 8260
364974
92344137006
SB-6
EPA 8260
365182
92344137001
SB-1
ASTM D2974-87
364980
92344137002
SB-2
ASTM D2974-87
364980
92344137003
SB-3
ASTM D2974-87
364980
92344137004
SB-4
ASTM D2974-87
364980
92344137005
SB-5
ASTM D2974-87
364980
92344137006
SB-6
ASTM D2974-87
364980
Date: 06/21 /2017 08:13 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 52 of 55

Document Name:
Sample Condition Upon Receipt(SCUR)
Document No.:
F-CAR-CS-033-Rev.01
Document Revised: Sept. 21, 2016
Page 1 of 2
Issuing Authority:
Pace Quality Office
Laboratory receiving samples:
Asheville Eden❑
Greenwood ❑ Huntersville ❑
Raleigh❑ Mechanicsville[]
ConditionSample Client Dame:Receipt �_ I,l Proje Wo # ' 9234411 7
Courier: ❑Fed Ex _[]UPS ,�]cllent 1111111111111111111111
❑ Commercial ❑Pace ❑0ther:
92344137
Custody Seal Present? ❑Yes ❑JII�Seals Intact? []Yes No
�
Date/Initials Person ten
Packing Material: ❑Bubble Wrap ubble Bags ❑None ❑Other:
Thermometer: ❑glue ❑None ❑Samples on ice, cooling process has begun
❑ IR Gun ID: Type of Ice:
Correction Factor: Cooler Temp Corrected (°Cl: Biological Tissue Frozen? []Yes ❑No �1V/A
Temp should be above freezing to 6°C
USDA Regulated Soil�N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
I—IyPc rlNn including Hawaii and Puerto Rico)? [-]Yes ❑Na
Comments/Discrepancy:
Chain of Custody Present?
es
[]No
❑N/A
1,
Samples Arrived within Hold Time?
es
[IN.
❑N/A
2.
Short Hold Time Analysis (<72 hr,)?
❑Yes
o
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
❑N/A
A.
Sufficient Volume?
es
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
,EJ s
E%e,
❑No
❑No
[]N/A
❑N/A
6.
Containers Intact?
es
❑No
❑NIA
7.
Samples Field Filtered?
❑Yes
❑N/A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
-Includes €7ate/Time/iD%Analysis Matrix:
ffYe,
[:]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
<
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
la
,ENo
El N/A
❑N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Date:
Date: l
Field Data Required? Des gNo
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
out of hold, incorrect preservative, out of temp, incorrect containers)
Page 53 of 55

Document Name: Document Revised: Sept. 21, 2016
Analytical Sample Condition Upon Receipt(SOUR) Page 2 of 2
Analytical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.01 Pace Quality Office
Tcneck mark top halt of box if pH and/or dechlorination
is
ProjectWO#
�}�}
: 923 /� /� 1 3 7
verified and within the acceptance
range for
_
preservation samples.
PMI: UP
Due
Dale: 06/21/17
**Bottom half of box is
to list number
of
bottles
CLIENT:
93-Singleton
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5 of 55

LIMITED PHASE II
ENVIRONMENTAL SITE
ASSESSMENT REPORT
For The
BUCKNER SITE
1430 Riverside Drive
Woodfin, NC 28804
PROJECT # SEI-788
PREPARED FOR:
French Broad River Academy
2000 Riverside Drive
Woodfin, NC 28804
PREPARED BY.
Singleton Environmental, Inc.
PO Box 2012
Enka, NC 28728
[phone]
July 24, 2017
SINGLETONENVIRONMENTAL, INC

Soil Assessment Report
July 24, 2017
UST Incident Number: NA
Facility ID Number: NA
Site Name & Address:
Consultant/Contractor:
Analytical Laboratory:
Date Release Discovered:
Estimated Quantity of Release:
Cause/Source of Release:
Size & Contents of UST System:
Geographical Data Point:
Latitude:
Longitude:
Location Method:
Buckner Site
1430 Riverside Drive
Woodfin, Buncombe County, NC
Singleton Environmental, Inc.
PO Box 2012
Enka, NC 28728
Telephone: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Not Applicable
Not Applicable
Not Applicable
Not Applicable
Not Applicable
35.6263' North
-82.6008' West
Google Earth
Signature and Seal of Certifying Professional Geologist:
I, Christopher D. Singleton, a North Carolina fvggi al Geologist, do certify that the
information contained in this report is correc 0 e best of my knowledge.
r �
L
Christy , P.G. #1928
'•.Ot r A
Singleton Environmental, Inc. is licensed to practice geology in North Carolina. The
certification number of the company is C-443.

TABLE OF CONTENTS
Introduction..................................................................................................................................... 1
SoilAssessment Field Work...................................................................................................... 1
SiteGeology............................................................................................................................... 2
LaboratoryAnalysis................................................................................................................... 2
Conclusion................................................................................................................................. 2
ClosingStatements..................................................................................................................... 3
Signature.................................................................................................................................... 3
Table
Table 1: Soil Analytical Results
Table 2: Groundwater Analytical Results
Figures
Figure 1: 7.5' USGS Topographic Map
Figure 2: Site Map
Appendices
Appendix A: Laboratory Analytical Report and Chain of Custody Documentation

INTRODUCTION
Singleton Environmental, Inc. (SEI) was contracted to perform a Limited Phase II
Environmental Site Assessment for the Buckner Site located at 1430 Riverside Drive in
Woodfin, North Carolina. The soil and groundwater assessment was requested to
determine if any environmental impacts were found on the property as a result of its past
use. The property subject to this investigation is being considered as an addition to the
French Broad River Academy.
The focus of this Assessment is to determine whether the soil and groundwater contains
contaminants that could prevent the purchase of the property for use as a school. Field
work for this assessment was completed on July 11, 2017. Soil samples were delivered to
Pace Analytical located in Asheville, North Carolina for analysis of volatile organic
compounds (VOCs), semi -volatile organic compounds (SVOCs) and 8 RCRA Metals.
ASSESSMENT FIELD WORK
Soil samples were collected using a Giddings probe/drill rig. The field work associated
with the assessment was completed on July 11, 2017. A total of five (5) soil borings were
performed at the subject property. Soil samples SB-1 through SB-5 were collected from
previously selected locations at the Site. The soil samples were screened to a depth of 8
feet using a photo -ionization detector (PID) to determine if Volatile Organic Compounds
(VOCs) were present. The PID readings detected only de minimis levels of volatile
organic compounds present in the soil samples which could be attributed to background
interference. Soil samples were collected at a depth of 1.0 to 2.0 feet to determine if any
chemicals were spilled on the surface since deeper PID readings were low. Soil boring
SB-1 was advanced to a depth of 20 feet to collect a groundwater sample (TMW-1) at the
Site. Refer to Figure 2 in the Figures section for the soil and groundwater sampling
locations.
A temporary monitoring well groundwater sampling point TMW-1 was installed to a
depth of approximately 20 feet below surface grade in the same location as SB-I. A two
inch (2") diameter well screen and riser was installed directly in a soil boring and filter
sand used around the well screen as required. The temporary monitoring well was
allowed to equilibrate for approximately 1 hour prior to the sampling event. Upon
sampling, the well was purged of approximately three (3) well volumes in order to obtain
a representative sample. The sample was then obtained using a 1" polyethylene bailer.
The sample was immediately transferred to sampling containers with the appropriate
preservative and placed on ice. The temporary monitoring wells was abandoned the same
day with bentonite.
The Giddings system used at the site consists of a series of hydraulically -pushed tools
which collect samples at continuous intervals to a predetermined depth. During soil
sampling, the 4-foot soil macro sampler can be advanced into the subsurface to a
predetermined depth. The locking probe point is then released and the sample tube is then

pushed to the terminal depth. The soil sample is retained within a clear plastic liner. The
sampling apparatus is then withdrawn to the surface upon completion of probing. The soil
can remain in the plastic liner or be removed for analysis and field screening. In this case,
upon removal of the sample tube and liner, the sample was screened using a PID,
collected from the liner and placed in EPA approved sample containers.
SITE GEOLOGY
The site is located within the Blue Ridge Geologic Belt. According to the Geologic Map
of North Carolina, the site is located within the Ashe Metamorphic Suite and Tallulah
Falls Formation formation (Zatm) of the Blue Ridge Belt of North Carolina. The bedrock
underlying the site is muscovite-biotite gneiss and is locally sulfidic; interlayed and
gradational with mica schist, minor amphibolite, and horneblende gneiss.
The surficial soils at the site consist of loamy sands mixed with auto parts and fluids. The
soil drainage class is well drained soil while also being occasionally flooded. Soils have a
low water holding capacity. Groundwater was encountered at a depth of approximately
17 feet in sampling location TMW-1.
LABORATORY ANALYSIS
The soil and groundwater samples collected on -site were submitted to Pace Analytical, a
North Carolina certified analytical laboratory. Soil samples SB-1 through SB-5 and
groundwater sample TMW-1 were analyzed for Volatile Organic Compounds (VOCs),
semi -Volatile Organic Compounds (SVOCs), and 8 RCRA Metals to determine if the
samples contained any compounds exceeding the North Carolina Department of
Environmental Quality (NCDEQ) Soil -to -Groundwater criteria, Residential or
Commercial Maximum Soil Contaminant Concentrations (MSCCs), and the NCAC 2L
Groundwater Standards.
Several metal concentrations in each soil sample exceeded the soil -to -groundwater
MSCCs, however, none of the soil samples exceeded the residential MSCCs or the the
commercial MSCCs. None of the VOC or SVOC compounds exceeded the soil -to -
groundwater MSCCs in the soil samples.
Chromium and lead exceeded the NCAC 2L Groundwater Standards in groundwater
sample TMW-1. None of the metals detected exceeded the Gross Contamination Levels.
None of the VOC and SVOC analysis detected any compounds above the minimum
laboratory detection levels.
Please see Tables 1 and 2 for all summarized soil and groundwater sampling results and
Figure 2 for the corresponding sampling locations. The laboratory analytical results
packages are attached to this report in Appendix A.

CONCLUSIONS
Based on the results of the soil analysis on the property, this report needs to be submitted
to the NCDEQ-UST Section Asheville Regional Office for further direction.
CLOSING STATEMENTS
This work was performed in general accordance with existing geological and
environmental standards of practice currently existing. The results found herein are
limited to the specific site and the boring locations as shown on the attached diagram.
However, it is a well know fact that variations in both geology and hydrogeology may
occur across the site between boring locations. It is also a well-known fact that changes in
groundwater and subsurface conditions can and do occur through time. These chiefly are
regarding groundwater flow and velocity, groundwater elevations and changes in
groundwater quality at various locations on a given site. The conclusions drawn from the
data presented in this report as well as the reporting methodology are in general
accordance with the existing standards and accepted hydrogeologic and environmental
engineering practices in use at the current time. Should, at some point in the future,
changes occur which require revision of this report or the conclusions drawn from it, we
reserve the right to make the necessary changes given the data showing the changes and
conditions and revise the conclusions drawn from the data as may be required.
SIGNATURE AND SEAL OF PROFESSIONAL GEOLOGIST:
I, Christopher D. Singleton, a Professional Geologist, do certify that the information
contained in this report is correct and accuratW*rQof my knowledge.
P.G. #1928
OZAS

TABLE 1
SOIL ANALYTICAL RESULTS
1430 Riverside Drive
Woodfin, North Carolina
SB-1 SB-2 SB-3 SB-4 SB-5
7/11/2017 7/11/2017 7/11/2017 7/11/2017 7/11/2017
1 -2 ft-bsg 1 -2 ft-bsg 1 -2 ft-bsg 1 -2 ft-bsg 1 -2 ft-bsg
Volatile & Semi -Volatile Organic Compounds
(EPA Methods 8260 & 8270) Non -Detect Non -Detect Non -Detect
Butylbenzylphthalate 0.7
Di-n-octvlphthalate 1.3
8 RCRA Metals
(EPA Methods 6010 & 7471)
Arsenic
1.1
2
1.5
Barium
88.3
157
216
154
76.5
Cadmium
0.96
Chromium
14.0
31.3
8.6
23.6
29.9
Lead
9.8
11.4
7
199
10.7
Selenium
1.8
1.7
2.1
2.2
Mercury
0.036
0.024
0.044
0.061
0.035
Note: 1. Bolded values indicate concentrations which
have exceeded at least
one maximum
allowable
soil concentration. Bolded
standards indicate those which
have been exceeded.
2. ND = Non -Detect
3. N/A = Not Applicable
Soil-to-GW
Max Soil Cont.
Level
(mg/kg)
N/A
N/A
Max Soil Cont.
Level
(mg/kg)
N/A
N/A
Max Soil Cont.
Level
(mg/kg)
N/A
N/A
0.68
N/A
3
31
469
12264
N/A
N/A
N/A
5.4
47
1226
270
400
400
N/A
N/A
N/A
2.2
N/A
3.3

TABLE 2
GROUNDWATER ANALYTICAL RESULTS
1430 Riverside Drive
Woodfin, North Carolina
SB-1
6/14/2017
1 -2 ft-bsg
NCAC 2L
Max GW Cont. Contamination
Volatile & Semi -Volatile Organic Compounds Level Level
(EPA Methods 6200 & 625) Non Detect (ug/1) (ug/1)
8 RCRA Metals
(EPA Methods 200.7 & 245.1)
Barium 3440
700
700000
Chromium 264.0
10
10000
Lead 207
Mercury 1.1
15
15000
N/A
N/A
Note: 1. Bolded values indicate concentrations which have exceeded at least one maximum allowable
soil concentration. Bolded standards indicate those which have been exceeded.
2. ND = Non -Detect
3. N/A = Not Applicable

FIGURES

LEGEND:
SOIL SAMPLE LOCATIONS Q SHRUB
S WATER WELL
TREE
SCALE (feet)
0 25 50
UST SYSTEM
(Tank Pit, Product Lines, etc.)
t
I ' "
4—
f
L ■� 'a I i.
• rc,
Y �
••.yL y -
DRAWN BY: C. Singleton
CHECKED BY: C. SINGLETON11 SINGLETON ENVIRONMENTAL, INC
NORTH
rig
FIGURE 2
1430 Riverside Drive
Weaverville, Buncombe County, NC

APPENDIX A

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
July 24, 2017
Chris Singleton
Singleton Environmental
P.O. Box 2012
Enka, NC 28728
RE: Project: 1430 Riverside Drive
Pace Project No.: 92347102
Dear Chris Singleton:
Enclosed are the analytical results for sample(s) received by the laboratory on July 11, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
�pQ AC RFb
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
1430 Riverside Drive
92347102
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92347102001
S13-1
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
CLW
1
PASI-C
92347102002
SB-2
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
CLW
1
PASI-C
92347102003
S13-3
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
CLW
1
PASI-C
92347102004
S13-4
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
CLW
1
PASI-C
92347102005
S13-5
EPA6010
SH1
7
PASI-A
EPA 7471
WAB
1
PASI-A
EPA 8270
BPJ
74
PASI-C
EPA 8260
DLK
70
PASI-C
ASTM D2974-87
CLW
1
PASI-C
92347102006
TMW-1
EPA200.7
SH1
7
PASI-A
EPA245.1
KAL
1
PASI-A
EPA 625
BPJ
58
PASI-C
SM 6200B
GAW
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-1 Lab ID: 92347102001 Collected: 07/11/17 09:00 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
1.1
mg/kg
0.59
1
07/13/17 17:45
07/16/17 01:36
7440-38-2
Barium
88.3
mg/kg
0.30
1
07/13/17 17:45
07/16/17 01:36
7440-39-3
Cadmium
ND
mg/kg
0.059
1
07/13/17 17:45
07/16/17 01:36
7440-43-9
Chromium
14.0
mg/kg
0.30
1
07/13/17 17:45
07/16/17 01:36
7440-47-3
Lead
9.8
mg/kg
0.30
1
07/13/17 17:45
07/16/17 01:36
7439-92-1
Selenium
1.8
mg/kg
0.59
1
07/13/17 17:45
07/16/17 01:36
7782-49-2
Silver
ND
mg/kg
0.30
1
07/13/17 17:45
07/16/17 01:36
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.036
mg/kg
0.0057
1
07/13/17 17:06
07/14/17 08:22
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
83-32-9
Acenaphthylene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
208-96-8
Aniline
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
62-53-3
Anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
207-08-9
Benzoic Acid
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
65-85-0
Benzyl alcohol
ND
mg/kg
0.77
1
07/17/17 13:10
07/18/17 10:35
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.77
1
07/17/17 13:10
07/18/17 10:35
59-50-7
4-Chloroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
91-58-7
2-Chlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
7005-72-3
Chrysene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
53-70-3
Dibenzofuran
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
120-83-2
Diethylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
105-67-9
Dimethylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.77
1
07/17/17 13:10
07/18/17 10:35
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 60

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ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-1
Lab ID: 92347102001 Collected: 07/11/17
09:00
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
117-81-7
Fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
206-44-0
Fluorene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
87-68-3
Hexachlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
77-47-4
Hexachloroethane
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
193-39-5
Isophorone
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
15831-10-4
Naphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
99-09-2
4-Nitroaniline
ND
mg/kg
0.77
1
07/17/17 13:10
07/18/17 10:35
100-01-6 L1
Nitrobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
98-95-3
2-Nitrophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
108-60-1
Pentachlorophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 10:35
87-86-5
Phenanthrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
85-01-8
Phenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
108-95-2
Pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 10:35
88-06-2
Surrogates
Nitrobenzene-d5 (S)
57
%
23-110
1
07/17/17 13:10
07/18/17 10:35
4165-60-0
2-Fluorobiphenyl (S)
49
%
30-110
1
07/17/17 13:10
07/18/17 10:35
321-60-8
Terphenyl-d14 (S)
79
%
28-110
1
07/17/17 13:10
07/18/17 10:35
1718-51-0
Phenol-d6 (S)
49
%
22-110
1
07/17/17 13:10
07/18/17 10:35
13127-88-3
2-Fluorophenol (S)
54
%
13-110
1
07/17/17 13:10
07/18/17 10:35
367-12-4
2,4,6-Tribromophenol (S)
59
%
27-110
1
07/17/17 13:10
07/18/17 10:35
118-79-6
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.11
1
07/12/1717:51
67-64-1 M1
Benzene
ND
mg/kg
0.0055
1
07/12/1717:51
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-1
Lab ID: 92347102001 Collected: 07/11/17
09:00
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No.
Qual
8260/5035A Volatile Organics
Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
108-86-1
Bromochloromethane
ND
mg/kg
0.0055
1
07/12/17 17:51
74-97-5
Bromodichloromethane
ND
mg/kg
0.0055
1
07/12/17 17:51
75-27-4
Bromoform
ND
mg/kg
0.0055
1
07/12/17 17:51
75-25-2
Bromomethane
ND
mg/kg
0.011
1
07/12/17 17:51
74-83-9
M1
2-Butanone (MEK)
ND
mg/kg
0.11
1
07/12/17 17:51
78-93-3
n-Butylbenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0055
1
07/12/17 17:51
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0055
1
07/12/17 17:51
56-23-5
Chlorobenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
108-90-7
Chloroethane
ND
mg/kg
0.011
1
07/12/17 17:51
75-00-3
Chloroform
ND
mg/kg
0.0055
1
07/12/17 17:51
67-66-3
Chloromethane
ND
mg/kg
0.011
1
07/12/17 17:51
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0055
1
07/12/17 17:51
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0055
1
07/12/17 17:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0055
1
07/12/17 17:51
96-12-8
M1
Dibromochloromethane
ND
mg/kg
0.0055
1
07/12/17 17:51
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0055
1
07/12/17 17:51
106-93-4
Dibromomethane
ND
mg/kg
0.0055
1
07/12/17 17:51
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.011
1
07/12/17 17:51
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0055
1
07/12/17 17:51
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0055
1
07/12/17 17:51
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0055
1
07/12/17 17:51
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0055
1
07/12/17 17:51
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0055
1
07/12/17 17:51
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0055
1
07/12/17 17:51
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0055
1
07/12/17 17:51
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0055
1
07/12/17 17:51
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0055
1
07/12/17 17:51
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0055
1
07/12/17 17:51
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0055
1
07/12/17 17:51
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0055
1
07/12/17 17:51
108-20-3
Ethylbenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0055
1
07/12/17 17:51
87-68-3
M1
2-Hexanone
ND
mg/kg
0.055
1
07/12/17 17:51
591-78-6
M1
Isopropylbenzene (Cumene)
ND
mg/kg
0.0055
1
07/12/17 17:51
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0055
1
07/12/17 17:51
99-87-6
Methylene Chloride
ND
mg/kg
0.022
1
07/12/17 17:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.055
1
07/12/17 17:51
108-10-1
M1
Methyl-tert-butyl ether
ND
mg/kg
0.0055
1
07/12/17 17:51
1634-04-4
Naphthalene
ND
mg/kg
0.0055
1
07/12/17 17:51
91-20-3
n-Propylbenzene
ND
mg/kg
0.0055
1
07/12/17 17:51
103-65-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-1 Lab ID: 92347102001 Collected: 07/11/17 09:00 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
mg/kg
0.0055
1
07/12/1717:51
100-42-5
ND
mg/kg
0.0055
1
07/12/1717:51
630-20-6
ND
mg/kg
0.0055
1
07/12/1717:51
79-34-5
ND
mg/kg
0.0055
1
07/12/1717:51
127-18-4
ND
mg/kg
0.0055
1
07/12/1717:51
108-88-3
ND
mg/kg
0.0055
1
07/12/1717:51
87-61-6
ND
mg/kg
0.0055
1
07/12/1717:51
120-82-1
ND
mg/kg
0.0055
1
07/12/1717:51
71-55-6
ND
mg/kg
0.0055
1
07/12/1717:51
79-00-5
ND
mg/kg
0.0055
1
07/12/1717:51
79-01-6
ND
mg/kg
0.0055
1
07/12/1717:51
75-69-4
ND
mg/kg
0.0055
1
07/12/1717:51
96-18-4
ND
mg/kg
0.0055
1
07/12/1717:51
95-63-6
ND
mg/kg
0.0055
1
07/12/1717:51
108-67-8
ND
mg/kg
0.055
1
07/12/1717:51
108-05-4 M1
ND
mg/kg
0.011
1
07/12/1717:51
75-01-4
ND
mg/kg
0.011
1
07/12/1717:51
1330-20-7
ND
mg/kg
0.011
1
07/12/1717:51
179601-23-1
ND
mg/kg
0.0055
1
07/12/1717:51
95-47-6
103
%
70-130
1
07/12/1717:51
2037-26-5
101
%
70-130
1
07/12/1717:51
460-00-4
127
%
70-132
1
07/12/1717:51
17060-07-0
Analytical Method: ASTM D2974-87
14.0 % 0.10 1
REPORT OF LABORATORY ANALYSIS
07/13/17 08:00
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-2
Lab ID: 92347102002
Collected: 07/11/17
10:00
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND
mg/kg
6.7
10
07/13/17 17:45
07/17/1714:38
7440-38-2
D3
Barium
157
mg/kg
3.3
10
07/13/17 17:45
07/16/17 20:27
7440-39-3
Cadmium
ND
mg/kg
0.67
10
07/13/17 17:45
07/16/17 20:27
7440-43-9
D3
Chromium
31.3
mg/kg
3.3
10
07/13/17 17:45
07/16/17 20:27
7440-47-3
Lead
11.4
mg/kg
3.3
10
07/13/17 17:45
07/16/17 20:27
7439-92-1
Selenium
ND
mg/kg
6.7
10
07/13/17 17:45
07/16/17 20:27
7782-49-2
D3
Silver
ND
mg/kg
3.3
10
07/13/17 17:45
07/16/17 20:27
7440-22-4
D3
7471 Mercury
Analytical Method: EPA 7471
Preparation Method: EPA 7471
Mercury
0.024
mg/kg
0.0051
1
07/13/17 17:06
07/14/17 08:24
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method: EPA 3546
Acenaphthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
83-32-9
Acenaphthylene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
208-96-8
Aniline
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
62-53-3
Anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
207-08-9
Benzoic Acid
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
65-85-0
Benzyl alcohol
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 11:35
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 11:35
59-50-7
4-Chloroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
91-58-7
2-Chlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
7005-72-3
Chrysene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
53-70-3
Dibenzofuran
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
120-83-2
Diethylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
105-67-9
Dimethylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 11:35
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 60

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ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-2
Lab ID: 92347102002 Collected: 07/11/17
10:00
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
117-81-7
Fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
206-44-0
Fluorene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
87-68-3
Hexachlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
77-47-4
Hexachloroethane
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
193-39-5
Isophorone
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
15831-10-4
Naphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
99-09-2
4-Nitroaniline
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 11:35
100-01-6 L1
Nitrobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
98-95-3
2-Nitrophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
108-60-1
Pentachlorophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 11:35
87-86-5
Phenanthrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
85-01-8
Phenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
108-95-2
Pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 11:35
88-06-2
Surrogates
Nitrobenzene-d5 (S)
53
%
23-110
1
07/17/17 13:10
07/18/17 11:35
4165-60-0
2-Fluorobiphenyl (S)
33
%
30-110
1
07/17/17 13:10
07/18/17 11:35
321-60-8
Terphenyl-d14 (S)
70
%
28-110
1
07/17/17 13:10
07/18/17 11:35
1718-51-0
Phenol-d6 (S)
48
%
22-110
1
07/17/17 13:10
07/18/17 11:35
13127-88-3
2-Fluorophenol (S)
50
%
13-110
1
07/17/17 13:10
07/18/17 11:35
367-12-4
2,4,6-Tribromophenol (S)
71
%
27-110
1
07/17/17 13:10
07/18/17 11:35
118-79-6
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.14
1
07/12/1718:11
67-64-1
Benzene
ND
mg/kg
0.0069
1
07/12/1718:11
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-2 Lab ID: 92347102002 Collected: 07/11/17 10:00 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
108-86-1
Bromochloromethane
ND
mg/kg
0.0069
1
07/12/17 18:11
74-97-5
Bromodichloromethane
ND
mg/kg
0.0069
1
07/12/17 18:11
75-27-4
Bromoform
ND
mg/kg
0.0069
1
07/12/17 18:11
75-25-2
Bromomethane
ND
mg/kg
0.014
1
07/12/17 18:11
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.14
1
07/12/17 18:11
78-93-3
n-Butylbenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0069
1
07/12/17 18:11
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0069
1
07/12/17 18:11
56-23-5
Chlorobenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
108-90-7
Chloroethane
ND
mg/kg
0.014
1
07/12/17 18:11
75-00-3
Chloroform
ND
mg/kg
0.0069
1
07/12/17 18:11
67-66-3
Chloromethane
ND
mg/kg
0.014
1
07/12/17 18:11
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0069
1
07/12/17 18:11
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0069
1
07/12/17 18:11
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0069
1
07/12/17 18:11
96-12-8
Dibromochloromethane
ND
mg/kg
0.0069
1
07/12/17 18:11
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0069
1
07/12/17 18:11
106-93-4
Dibromomethane
ND
mg/kg
0.0069
1
07/12/17 18:11
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.014
1
07/12/17 18:11
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0069
1
07/12/17 18:11
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0069
1
07/12/17 18:11
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0069
1
07/12/17 18:11
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0069
1
07/12/17 18:11
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0069
1
07/12/17 18:11
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0069
1
07/12/17 18:11
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0069
1
07/12/17 18:11
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0069
1
07/12/17 18:11
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0069
1
07/12/17 18:11
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0069
1
07/12/17 18:11
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0069
1
07/12/17 18:11
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0069
1
07/12/17 18:11
108-20-3
Ethylbenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0069
1
07/12/17 18:11
87-68-3
2-Hexanone
ND
mg/kg
0.069
1
07/12/17 18:11
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0069
1
07/12/17 18:11
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0069
1
07/12/17 18:11
99-87-6
Methylene Chloride
ND
mg/kg
0.028
1
07/12/17 18:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.069
1
07/12/17 18:11
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0069
1
07/12/17 18:11
1634-04-4
Naphthalene
ND
mg/kg
0.0069
1
07/12/17 18:11
91-20-3
n-Propylbenzene
ND
mg/kg
0.0069
1
07/12/17 18:11
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-2 Lab ID: 92347102002 Collected: 07/11/17 10:00 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
mg/kg
0.0069
1
07/12/1718:11
100-42-5
ND
mg/kg
0.0069
1
07/12/1718:11
630-20-6
ND
mg/kg
0.0069
1
07/12/1718:11
79-34-5
ND
mg/kg
0.0069
1
07/12/1718:11
127-18-4
ND
mg/kg
0.0069
1
07/12/1718:11
108-88-3
ND
mg/kg
0.0069
1
07/12/1718:11
87-61-6
ND
mg/kg
0.0069
1
07/12/1718:11
120-82-1
ND
mg/kg
0.0069
1
07/12/1718:11
71-55-6
ND
mg/kg
0.0069
1
07/12/1718:11
79-00-5
ND
mg/kg
0.0069
1
07/12/1718:11
79-01-6
ND
mg/kg
0.0069
1
07/12/1718:11
75-69-4
ND
mg/kg
0.0069
1
07/12/1718:11
96-18-4
ND
mg/kg
0.0069
1
07/12/1718:11
95-63-6
ND
mg/kg
0.0069
1
07/12/1718:11
108-67-8
ND
mg/kg
0.069
1
07/12/1718:11
108-05-4
ND
mg/kg
0.014
1
07/12/1718:11
75-01-4
ND
mg/kg
0.014
1
07/12/1718:11
1330-20-7
ND
mg/kg
0.014
1
07/12/1718:11
179601-23-1
ND
mg/kg
0.0069
1
07/12/1718:11
95-47-6
103
%
70-130
1
07/12/1718:11
2037-26-5
95
%
70-130
1
07/12/1718:11
460-00-4
136
%
70-132
1
07/12/1718:11
17060-07-0 S3
Analytical Method: ASTM D2974-87
11.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
07/13/17 08:00
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-3 Lab ID: 92347102003 Collected: 07/11/17 10:45 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
ND
mg/kg
1.1
1
07/13/17 17:45
07/16/17 01:42
7440-38-2
Barium
216
mg/kg
0.55
1
07/13/17 17:45
07/16/17 01:42
7440-39-3
Cadmium
ND
mg/kg
0.11
1
07/13/17 17:45
07/16/17 01:42
7440-43-9
Chromium
8.6
mg/kg
0.55
1
07/13/17 17:45
07/16/17 01:42
7440-47-3
Lead
7.0
mg/kg
0.55
1
07/13/17 17:45
07/16/17 01:42
7439-92-1
Selenium
1.7
mg/kg
1.1
1
07/13/17 17:45
07/16/17 01:42
7782-49-2
Silver
ND
mg/kg
0.55
1
07/13/17 17:45
07/16/17 01:42
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.044
mg/kg
0.0056
1
07/13/17 17:06
07/14/17 08:27
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
83-32-9
Acenaphthylene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
208-96-8
Aniline
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
62-53-3
Anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
207-08-9
Benzoic Acid
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
65-85-0
Benzyl alcohol
ND
mg/kg
0.76
1
07/17/17 13:10
07/18/17 12:05
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.76
1
07/17/17 13:10
07/18/17 12:05
59-50-7
4-Chloroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
91-58-7
2-Chlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
7005-72-3
Chrysene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
53-70-3
Dibenzofuran
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
120-83-2
Diethylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
105-67-9
Dimethylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.76
1
07/17/17 13:10
07/18/17 12:05
534-52-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-3
Lab ID: 92347102003 Collected: 07/11/17
10:45
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
117-81-7
Fluoranthene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
206-44-0
Fluorene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
87-68-3
Hexachlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
77-47-4
Hexachloroethane
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
193-39-5
Isophorone
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
15831-10-4
Naphthalene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
99-09-2
4-Nitroaniline
ND
mg/kg
0.76
1
07/17/17 13:10
07/18/17 12:05
100-01-6 L1
Nitrobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
98-95-3
2-Nitrophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
108-60-1
Pentachlorophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 12:05
87-86-5
Phenanthrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
85-01-8
Phenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
108-95-2
Pyrene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.38
1
07/17/17 13:10
07/18/17 12:05
88-06-2
Surrogates
Nitrobenzene-d5 (S)
78
%
23-110
1
07/17/17 13:10
07/18/17 12:05
4165-60-0
2-Fluorobiphenyl (S)
72
%
30-110
1
07/17/17 13:10
07/18/17 12:05
321-60-8
Terphenyl-d14 (S)
100
%
28-110
1
07/17/17 13:10
07/18/17 12:05
1718-51-0
Phenol-d6 (S)
65
%
22-110
1
07/17/17 13:10
07/18/17 12:05
13127-88-3
2-Fluorophenol (S)
66
%
13-110
1
07/17/17 13:10
07/18/17 12:05
367-12-4
2,4,6-Tribromophenol (S)
67
%
27-110
1
07/17/17 13:10
07/18/17 12:05
118-79-6
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.11
1
07/12/1718:30
67-64-1
Benzene
ND
mg/kg
0.0054
1
07/12/1718:30
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-3 Lab ID: 92347102003 Collected: 07/11/17 10:45 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
108-86-1
Bromochloromethane
ND
mg/kg
0.0054
1
07/12/17 18:30
74-97-5
Bromodichloromethane
ND
mg/kg
0.0054
1
07/12/17 18:30
75-27-4
Bromoform
ND
mg/kg
0.0054
1
07/12/17 18:30
75-25-2
Bromomethane
ND
mg/kg
0.011
1
07/12/17 18:30
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.11
1
07/12/17 18:30
78-93-3
n-Butylbenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0054
1
07/12/17 18:30
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0054
1
07/12/17 18:30
56-23-5
Chlorobenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
108-90-7
Chloroethane
ND
mg/kg
0.011
1
07/12/17 18:30
75-00-3
Chloroform
ND
mg/kg
0.0054
1
07/12/17 18:30
67-66-3
Chloromethane
ND
mg/kg
0.011
1
07/12/17 18:30
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0054
1
07/12/17 18:30
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0054
1
07/12/17 18:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0054
1
07/12/17 18:30
96-12-8
Dibromochloromethane
ND
mg/kg
0.0054
1
07/12/17 18:30
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0054
1
07/12/17 18:30
106-93-4
Dibromomethane
ND
mg/kg
0.0054
1
07/12/17 18:30
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.011
1
07/12/17 18:30
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0054
1
07/12/17 18:30
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0054
1
07/12/17 18:30
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0054
1
07/12/17 18:30
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0054
1
07/12/17 18:30
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0054
1
07/12/17 18:30
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0054
1
07/12/17 18:30
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0054
1
07/12/17 18:30
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0054
1
07/12/17 18:30
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0054
1
07/12/17 18:30
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0054
1
07/12/17 18:30
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0054
1
07/12/17 18:30
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0054
1
07/12/17 18:30
108-20-3
Ethylbenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0054
1
07/12/17 18:30
87-68-3
2-Hexanone
ND
mg/kg
0.054
1
07/12/17 18:30
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0054
1
07/12/17 18:30
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0054
1
07/12/17 18:30
99-87-6
Methylene Chloride
ND
mg/kg
0.022
1
07/12/17 18:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.054
1
07/12/17 18:30
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0054
1
07/12/17 18:30
1634-04-4
Naphthalene
ND
mg/kg
0.0054
1
07/12/17 18:30
91-20-3
n-Propylbenzene
ND
mg/kg
0.0054
1
07/12/17 18:30
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-3 Lab ID: 92347102003 Collected: 07/11/17 10:45 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
mg/kg
0.0054
1
07/12/1718:30
100-42-5
ND
mg/kg
0.0054
1
07/12/1718:30
630-20-6
ND
mg/kg
0.0054
1
07/12/1718:30
79-34-5
ND
mg/kg
0.0054
1
07/12/1718:30
127-18-4
ND
mg/kg
0.0054
1
07/12/1718:30
108-88-3
ND
mg/kg
0.0054
1
07/12/1718:30
87-61-6
ND
mg/kg
0.0054
1
07/12/1718:30
120-82-1
ND
mg/kg
0.0054
1
07/12/1718:30
71-55-6
ND
mg/kg
0.0054
1
07/12/1718:30
79-00-5
ND
mg/kg
0.0054
1
07/12/1718:30
79-01-6
ND
mg/kg
0.0054
1
07/12/1718:30
75-69-4
ND
mg/kg
0.0054
1
07/12/1718:30
96-18-4
ND
mg/kg
0.0054
1
07/12/1718:30
95-63-6
ND
mg/kg
0.0054
1
07/12/1718:30
108-67-8
ND
mg/kg
0.054
1
07/12/1718:30
108-05-4
ND
mg/kg
0.011
1
07/12/1718:30
75-01-4
ND
mg/kg
0.011
1
07/12/1718:30
1330-20-7
ND
mg/kg
0.011
1
07/12/1718:30
179601-23-1
ND
mg/kg
0.0054
1
07/12/1718:30
95-47-6
105
%
70-130
1
07/12/1718:30
2037-26-5
103
%
70-130
1
07/12/1718:30
460-00-4
129
%
70-132
1
07/12/1718:30
17060-07-0
Analytical Method: ASTM D2974-87
13.6 % 0.10 1
REPORT OF LABORATORY ANALYSIS
07/13/17 08:57
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 60

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ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-4 Lab ID: 92347102004 Collected: 07/11/17 11:00 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
2.0
mg/kg
0.90
1
07/13/17 17:45
07/16/17 01:45
7440-38-2
Barium
154
mg/kg
0.45
1
07/13/17 17:45
07/16/17 01:45
7440-39-3
Cadmium
0.96
mg/kg
0.090
1
07/13/17 17:45
07/16/17 01:45
7440-43-9
Chromium
23.6
mg/kg
0.45
1
07/13/17 17:45
07/16/17 01:45
7440-47-3
Lead
199
mg/kg
0.45
1
07/13/17 17:45
07/16/17 01:45
7439-92-1
Selenium
2.1
mg/kg
0.90
1
07/13/17 17:45
07/16/17 01:45
7782-49-2
Silver
ND
mg/kg
0.45
1
07/13/17 17:45
07/16/17 01:45
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.061
mg/kg
0.0050
1
07/13/17 17:06
07/14/17 08:29
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
83-32-9
Acenaphthylene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
208-96-8
Aniline
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
62-53-3
Anthracene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
207-08-9
Benzoic Acid
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
65-85-0
Benzyl alcohol
ND
mg/kg
0.71
1
07/17/17 13:10
07/18/17 12:35
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
101-55-3
Butylbenzylphthalate
0.70
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.71
1
07/17/17 13:10
07/18/17 12:35
59-50-7
4-Chloroaniline
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
91-58-7
2-Chlorophenol
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
7005-72-3
Chrysene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
53-70-3
Dibenzofuran
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
120-83-2
Diethylphthalate
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
105-67-9
Dimethylphthalate
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.71
1
07/17/17 13:10
07/18/17 12:35
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 60

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2225 Riverside Dr.
Asheville, NC 28804
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ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-4
Lab ID: 92347102004 Collected: 07/11/17
11:00
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
606-20-2
Di-n-octylphthalate
1.3
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
117-81-7
Fluoranthene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
206-44-0
Fluorene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
87-68-3
Hexachlorobenzene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
77-47-4
Hexachloroethane
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
193-39-5
Isophorone
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
15831-10-4
Naphthalene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
91-20-3
2-Nitroaniline
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
88-74-4
3-Nitroaniline
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
99-09-2
4-Nitroaniline
ND
mg/kg
0.71
1
07/17/17 13:10
07/18/17 12:35
100-01-6 L1
Nitrobenzene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
98-95-3
2-Nitrophenol
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
88-75-5
4-Nitrophenol
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
108-60-1
Pentachlorophenol
ND
mg/kg
1.8
1
07/17/17 13:10
07/18/17 12:35
87-86-5
Phenanthrene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
85-01-8
Phenol
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
108-95-2
Pyrene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.36
1
07/17/17 13:10
07/18/17 12:35
88-06-2
Surrogates
Nitrobenzene-d5 (S)
81
%
23-110
1
07/17/17 13:10
07/18/17 12:35
4165-60-0
2-Fluorobiphenyl (S)
74
%
30-110
1
07/17/17 13:10
07/18/17 12:35
321-60-8
Terphenyl-d14 (S)
69
%
28-110
1
07/17/17 13:10
07/18/17 12:35
1718-51-0
Phenol-d6 (S)
68
%
22-110
1
07/17/17 13:10
07/18/17 12:35
13127-88-3
2-Fluorophenol (S)
73
%
13-110
1
07/17/17 13:10
07/18/17 12:35
367-12-4
2,4,6-Tribromophenol (S)
73
%
27-110
1
07/17/17 13:10
07/18/17 12:35
118-79-6
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.12
1
07/12/1718:50
67-64-1
Benzene
ND
mg/kg
0.0058
1
07/12/1718:50
71-43-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-4 Lab ID: 92347102004 Collected: 07/11/17 11:00 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
108-86-1
Bromochloromethane
ND
mg/kg
0.0058
1
07/12/17 18:50
74-97-5
Bromodichloromethane
ND
mg/kg
0.0058
1
07/12/17 18:50
75-27-4
Bromoform
ND
mg/kg
0.0058
1
07/12/17 18:50
75-25-2
Bromomethane
ND
mg/kg
0.012
1
07/12/17 18:50
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.12
1
07/12/17 18:50
78-93-3
n-Butylbenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0058
1
07/12/17 18:50
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0058
1
07/12/17 18:50
56-23-5
Chlorobenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
108-90-7
Chloroethane
ND
mg/kg
0.012
1
07/12/17 18:50
75-00-3
Chloroform
ND
mg/kg
0.0058
1
07/12/17 18:50
67-66-3
Chloromethane
ND
mg/kg
0.012
1
07/12/17 18:50
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0058
1
07/12/17 18:50
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0058
1
07/12/17 18:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0058
1
07/12/17 18:50
96-12-8
Dibromochloromethane
ND
mg/kg
0.0058
1
07/12/17 18:50
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0058
1
07/12/17 18:50
106-93-4
Dibromomethane
ND
mg/kg
0.0058
1
07/12/17 18:50
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
1
07/12/17 18:50
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0058
1
07/12/17 18:50
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0058
1
07/12/17 18:50
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0058
1
07/12/17 18:50
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0058
1
07/12/17 18:50
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0058
1
07/12/17 18:50
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0058
1
07/12/17 18:50
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0058
1
07/12/17 18:50
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0058
1
07/12/17 18:50
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0058
1
07/12/17 18:50
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0058
1
07/12/17 18:50
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0058
1
07/12/17 18:50
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0058
1
07/12/17 18:50
108-20-3
Ethylbenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0058
1
07/12/17 18:50
87-68-3
2-Hexanone
ND
mg/kg
0.058
1
07/12/17 18:50
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0058
1
07/12/17 18:50
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0058
1
07/12/17 18:50
99-87-6
Methylene Chloride
ND
mg/kg
0.023
1
07/12/17 18:50
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.058
1
07/12/17 18:50
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0058
1
07/12/17 18:50
1634-04-4
Naphthalene
ND
mg/kg
0.0058
1
07/12/17 18:50
91-20-3
n-Propylbenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-4
Lab ID: 92347102004 Collected:
07/11/17 11:00
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Styrene
ND
mg/kg
0.0058
1
07/12/17 18:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0058
1
07/12/17 18:50
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0058
1
07/12/17 18:50
79-34-5
Tetrachloroethene
ND
mg/kg
0.0058
1
07/12/17 18:50
127-18-4
Toluene
ND
mg/kg
0.0058
1
07/12/17 18:50
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0058
1
07/12/17 18:50
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0058
1
07/12/17 18:50
79-00-5
Trichloroethene
ND
mg/kg
0.0058
1
07/12/17 18:50
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0058
1
07/12/17 18:50
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0058
1
07/12/17 18:50
96-18-4
1,2,4-Trimethylbenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0058
1
07/12/17 18:50
108-67-8
Vinyl acetate
ND
mg/kg
0.058
1
07/12/17 18:50
108-05-4
Vinyl chloride
ND
mg/kg
0.012
1
07/12/17 18:50
75-01-4
Xylene (Total)
ND
mg/kg
0.012
1
07/12/17 18:50
1330-20-7
m&p-Xylene
ND
mg/kg
0.012
1
07/12/17 18:50
179601-23-1
o-Xylene
ND
mg/kg
0.0058
1
07/12/17 18:50
95-47-6
Surrogates
Toluene-d8 (S)
96
%
70-130
1
07/12/17 18:50
2037-26-5 1g
4-Bromofluorobenzene (S)
85
%
70-130
1
07/12/17 18:50
460-00-4
1,2-Dichloroethane-d4 (S)
151
%
70-132
1
07/12/17 18:50
17060-07-0 S3
Percent Moisture
Analytical Method:
ASTM D2974-87
Percent Moisture
7.5
%
0.10
1
07/13/17 08:58
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-5 Lab ID: 92347102005 Collected: 07/11/17 11:05 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
1.5
mg/kg
0.94
1
07/13/17 17:45
07/16/17 01:48
7440-38-2
Barium
76.5
mg/kg
0.47
1
07/13/17 17:45
07/16/17 01:48
7440-39-3
Cadmium
ND
mg/kg
0.094
1
07/13/17 17:45
07/16/17 01:48
7440-43-9
Chromium
29.9
mg/kg
0.47
1
07/13/17 17:45
07/16/17 01:48
7440-47-3
Lead
10.7
mg/kg
0.47
1
07/13/17 17:45
07/16/17 01:48
7439-92-1
Selenium
2.2
mg/kg
0.94
1
07/13/17 17:45
07/16/17 01:48
7782-49-2
Silver
ND
mg/kg
0.47
1
07/13/17 17:45
07/16/17 01:48
7440-22-4
7471 Mercury
Analytical Method: EPA 7471
Preparation Method:
EPA 7471
Mercury
0.035
mg/kg
0.0052
1
07/13/17 17:06
07/14/17 08:36
7439-97-6
8270 MSSV Microwave
Analytical Method:
EPA 8270
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
83-32-9
Acenaphthylene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
208-96-8
Aniline
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
62-53-3
Anthracene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
207-08-9
Benzoic Acid
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
65-85-0
Benzyl alcohol
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 13:05
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 13:05
59-50-7
4-Chloroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
106-47-8
bis(2-Chloroethoxy)methane
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
91-58-7
2-Chlorophenol
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
7005-72-3
Chrysene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
53-70-3
Dibenzofuran
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
120-83-2
Diethylphthalate
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
105-67-9
Dimethylphthalate
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 13:05
534-52-1
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 20 of 60

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2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: SB-5
Lab ID: 92347102005 Collected: 07/11/17
11:05
Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
2,4-Dinitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
117-81-7
Fluoranthene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
206-44-0
Fluorene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
87-68-3
Hexachlorobenzene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
77-47-4
Hexachloroethane
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
193-39-5
Isophorone
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
78-59-1
1-Methylnaphthalene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
90-12-0
2-Methylnaphthalene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
15831-10-4
Naphthalene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
91-20-3
2-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
88-74-4
3-Nitroaniline
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
99-09-2
4-Nitroaniline
ND
mg/kg
0.75
1
07/17/17 13:10
07/18/17 13:05
100-01-6 L1
Nitrobenzene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
98-95-3
2-Nitrophenol
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
88-75-5
4-Nitrophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
108-60-1
Pentachlorophenol
ND
mg/kg
1.9
1
07/17/17 13:10
07/18/17 13:05
87-86-5
Phenanthrene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
85-01-8
Phenol
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
108-95-2
Pyrene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
129-00-0
1,2,4-Trichlorobenzene
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.37
1
07/17/17 13:10
07/18/17 13:05
88-06-2
Surrogates
Nitrobenzene-d5 (S)
49
%
23-110
1
07/17/17 13:10
07/18/17 13:05
4165-60-0
2-Fluorobiphenyl (S)
50
%
30-110
1
07/17/17 13:10
07/18/17 13:05
321-60-8
Terphenyl-d14 (S)
79
%
28-110
1
07/17/17 13:10
07/18/17 13:05
1718-51-0
Phenol-d6 (S)
44
%
22-110
1
07/17/17 13:10
07/18/17 13:05
13127-88-3
2-Fluorophenol (S)
49
%
13-110
1
07/17/17 13:10
07/18/17 13:05
367-12-4
2,4,6-Tribromophenol (S)
71
%
27-110
1
07/17/17 13:10
07/18/17 13:05
118-79-6
8260/5035A Volatile Organics
Analytical Method:
EPA 8260
Acetone
ND
mg/kg
0.12
1
07/12/1719:10
67-64-1
Benzene
ND
mg/kg
0.0060
1
07/12/1719:10
71-43-2
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-5 Lab ID: 92347102005 Collected: 07/11/17 11:05 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
108-86-1
Bromochloromethane
ND
mg/kg
0.0060
1
07/12/17 19:10
74-97-5
Bromodichloromethane
ND
mg/kg
0.0060
1
07/12/17 19:10
75-27-4
Bromoform
ND
mg/kg
0.0060
1
07/12/17 19:10
75-25-2
Bromomethane
ND
mg/kg
0.012
1
07/12/17 19:10
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.12
1
07/12/17 19:10
78-93-3
n-Butylbenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0060
1
07/12/17 19:10
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0060
1
07/12/17 19:10
56-23-5
Chlorobenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
108-90-7
Chloroethane
ND
mg/kg
0.012
1
07/12/17 19:10
75-00-3
Chloroform
ND
mg/kg
0.0060
1
07/12/17 19:10
67-66-3
Chloromethane
ND
mg/kg
0.012
1
07/12/17 19:10
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0060
1
07/12/17 19:10
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0060
1
07/12/17 19:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0060
1
07/12/17 19:10
96-12-8
Dibromochloromethane
ND
mg/kg
0.0060
1
07/12/17 19:10
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0060
1
07/12/17 19:10
106-93-4
Dibromomethane
ND
mg/kg
0.0060
1
07/12/17 19:10
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
1
07/12/17 19:10
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0060
1
07/12/17 19:10
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0060
1
07/12/17 19:10
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0060
1
07/12/17 19:10
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0060
1
07/12/17 19:10
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0060
1
07/12/17 19:10
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0060
1
07/12/17 19:10
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0060
1
07/12/17 19:10
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0060
1
07/12/17 19:10
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0060
1
07/12/17 19:10
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0060
1
07/12/17 19:10
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0060
1
07/12/17 19:10
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0060
1
07/12/17 19:10
108-20-3
Ethylbenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0060
1
07/12/17 19:10
87-68-3
2-Hexanone
ND
mg/kg
0.060
1
07/12/17 19:10
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0060
1
07/12/17 19:10
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0060
1
07/12/17 19:10
99-87-6
Methylene Chloride
ND
mg/kg
0.024
1
07/12/17 19:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.060
1
07/12/17 19:10
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0060
1
07/12/17 19:10
1634-04-4
Naphthalene
ND
mg/kg
0.0060
1
07/12/17 19:10
91-20-3
n-Propylbenzene
ND
mg/kg
0.0060
1
07/12/17 19:10
103-65-1
REPORT OF LABORATORY ANALYSIS
Qual
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 22 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: S13-5 Lab ID: 92347102005 Collected: 07/11/17 11:05 Received: 07/11/17 11:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260
ND
mg/kg
0.0060
1
07/12/1719:10
100-42-5
ND
mg/kg
0.0060
1
07/12/1719:10
630-20-6
ND
mg/kg
0.0060
1
07/12/1719:10
79-34-5
ND
mg/kg
0.0060
1
07/12/1719:10
127-18-4
ND
mg/kg
0.0060
1
07/12/1719:10
108-88-3
ND
mg/kg
0.0060
1
07/12/1719:10
87-61-6
ND
mg/kg
0.0060
1
07/12/1719:10
120-82-1
ND
mg/kg
0.0060
1
07/12/1719:10
71-55-6
ND
mg/kg
0.0060
1
07/12/1719:10
79-00-5
ND
mg/kg
0.0060
1
07/12/1719:10
79-01-6
ND
mg/kg
0.0060
1
07/12/1719:10
75-69-4
ND
mg/kg
0.0060
1
07/12/1719:10
96-18-4
ND
mg/kg
0.0060
1
07/12/1719:10
95-63-6
ND
mg/kg
0.0060
1
07/12/1719:10
108-67-8
ND
mg/kg
0.060
1
07/12/1719:10
108-05-4
ND
mg/kg
0.012
1
07/12/1719:10
75-01-4
ND
mg/kg
0.012
1
07/12/1719:10
1330-20-7
ND
mg/kg
0.012
1
07/12/1719:10
179601-23-1
ND
mg/kg
0.0060
1
07/12/1719:10
95-47-6
106
%
70-130
1
07/12/1719:10
2037-26-5
101
%
70-130
1
07/12/1719:10
460-00-4
129
%
70-132
1
07/12/1719:10
17060-07-0
Analytical Method: ASTM D2974-87
11.8 % 0.10 1
REPORT OF LABORATORY ANALYSIS
07/13/17 08:58
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 60

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ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: TMW-1
Lab ID: 92347102006 Collected: 07/11/17
10:30
Received: 07/11/17 11:13 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
200.7 MET ICP
Analytical Method:
EPA 200.7
Preparation Method: EPA 200.7
Arsenic
ND
ug/L
100
10
07/12/17 15:55
07/14/17 22:18
7440-38-2
D3
Barium
3440
ug/L
50.0
10
07/12/17 15:55
07/14/17 22:18
7440-39-3
M6
Cadmium
ND
ug/L
10.0
10
07/12/17 15:55
07/14/17 22:18
7440-43-9
D3
Chromium
264
ug/L
50.0
10
07/12/17 15:55
07/14/17 22:18
7440-47-3
Lead
207
ug/L
50.0
10
07/12/17 15:55
07/15/1715:47
7439-92-1
Selenium
ND
ug/L
100
10
07/12/17 15:55
07/14/17 22:18
7782-49-2
D3,M6
Silver
ND
ug/L
50.0
10
07/12/17 15:55
07/14/17 22:18
7440-22-4
D3
245.1 Mercury
Analytical Method:
EPA 245.1
Preparation Method: EPA 245.1
Mercury
1.1
ug/L
0.20
1
07/13/17 11:52
07/14/17 07:17
7439-97-6
625 MSSV
Analytical Method:
EPA 625 Preparation Method: EPA 625
Acenaphthene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
208-96-8
Anthracene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
07/13/17 14:00
07/14/17 23:15
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
7005-72-3
Chrysene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
07/13/17 14:00
07/14/17 23:15
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
07/13/17 14:00
07/14/17 23:15
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
07/13/17 14:00
07/14/17 23:15
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
07/13/17 14:00
07/14/17 23:15
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
117-81-7
Fluoranthene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
206-44-0
Fluorene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
118-74-1
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 60

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ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: TMW-1
Lab ID: 92347102006 Collected:
07/11/17
10:30
Received: 07/11/17 11:13 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
625 MSSV
Analytical Method:
EPA 625 Preparation Method: EPA 625
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
07/13/17 14:00
07/14/17 23:15
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
193-39-5
Isophorone
ND
ug/L
10.0
1
07/13/17 14:00
07/14/17 23:15
78-59-1
Naphthalene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
07/13/17 14:00
07/14/17 23:15
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
07/13/17 14:00
07/14/17 23:15
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
07/13/17 14:00
07/14/17 23:15
87-86-5
Phenanthrene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
85-01-8
Phenol
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
108-95-2
Pyrene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
07/13/17 14:00
07/14/17 23:15
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
07/13/17 14:00
07/14/17 23:15
88-06-2
Surrogates
Nitrobenzene-d5 (S)
34
%
10-120
1
07/13/17 14:00
07/14/17 23:15
4165-60-0
2-Fluorobiphenyl (S)
32
%
15-120
1
07/13/17 14:00
07/14/17 23:15
321-60-8
Terphenyl-d14 (S)
30
%
11-131
1
07/13/17 14:00
07/14/17 23:15
1718-51-0
Phenol-d6 (S)
9
%
10-120
1
07/13/17 14:00
07/14/17 23:15
13127-88-3 SO
2-Fluorophenol (S)
11
%
10-120
1
07/13/17 14:00
07/14/17 23:15
367-12-4
2,4,6-Tribromophenol (S)
23
%
10-137
1
07/13/17 14:00
07/14/17 23:15
118-79-6
6200B MSV
Analytical Method:
SM 6200B
Benzene
ND
ug/L
0.50
1
07/14/17 16:49
71-43-2
Bromobenzene
ND
ug/L
0.50
1
07/14/17 16:49
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
07/14/17 16:49
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
07/14/17 16:49
75-27-4
Bromoform
ND
ug/L
0.50
1
07/14/17 16:49
75-25-2
Bromomethane
ND
ug/L
5.0
1
07/14/17 16:49
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
07/14/17 16:49
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
07/14/17 16:49
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
07/14/17 16:49
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
07/14/17 16:49
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
07/14/17 16:49
108-90-7
Chloroethane
ND
ug/L
1.0
1
07/14/17 16:49
75-00-3
Chloroform
ND
ug/L
0.50
1
07/14/17 16:49
67-66-3
Chloromethane
ND
ug/L
1.0
1
07/14/17 16:49
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
07/14/17 16:49
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
07/14/17 16:49
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
07/14/17 16:49
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
07/14/17 16:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
07/14/17 16:49
106-93-4
Dibromomethane
ND
ug/L
0.50
1
07/14/17 16:49
74-95-3
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 60

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ANALYTICAL RESULTS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
Sample: TMW-1 Lab ID: 92347102006 Collected: 07/11/17 10:30 Received: 07/11/17 11:13 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 07/24/2017 10:03 AM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
109 %
101 %
106 %
0.50
1
07/14/17 16:49
95-50-1
0.50
1
07/14/17 16:49
541-73-1
0.50
1
07/14/17 16:49
106-46-7
0.50
1
07/14/17 16:49
75-71-8
0.50
1
07/14/17 16:49
75-34-3
0.50
1
07/14/17 16:49
107-06-2
0.50
1
07/14/17 16:49
75-35-4
0.50
1
07/14/17 16:49
156-59-2
0.50
1
07/14/17 16:49
156-60-5
0.50
1
07/14/17 16:49
78-87-5
0.50
1
07/14/17 16:49
142-28-9
0.50
1
07/14/17 16:49
594-20-7
0.50
1
07/14/17 16:49
563-58-6
0.50
1
07/14/17 16:49
10061-01-5
0.50
1
07/14/17 16:49
10061-02-6
0.50
1
07/14/17 16:49
108-20-3
0.50
1
07/14/17 16:49
100-41-4
2.0
1
07/14/17 16:49
87-68-3
0.50
1
07/14/17 16:49
98-82-8
2.0
1
07/14/17 16:49
75-09-2
0.50
1
07/14/17 16:49
1634-04-4
2.0
1
07/14/17 16:49
91-20-3
0.50
1
07/14/17 16:49
103-65-1
0.50
1
07/14/17 16:49
100-42-5
0.50
1
07/14/17 16:49
630-20-6
0.50
1
07/14/17 16:49
79-34-5
0.50
1
07/14/17 16:49
127-18-4
0.50
1
07/14/17 16:49
108-88-3
2.0
1
07/14/17 16:49
87-61-6
2.0
1
07/14/17 16:49
120-82-1
0.50
1
07/14/17 16:49
71-55-6
0.50
1
07/14/17 16:49
79-00-5
0.50
1
07/14/17 16:49
79-01-6
1.0
1
07/14/17 16:49
75-69-4
0.50
1
07/14/17 16:49
96-18-4
0.50
1
07/14/17 16:49
95-63-6
0.50
1
07/14/17 16:49
108-67-8
1.0
1
07/14/17 16:49
75-01-4
1.0
1
07/14/17 16:49
179601-23-1
0.50
1
07/14/17 16:49
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
07/14/17 16:49 17060-07-0
07/14/17 16:49 460-00-4
07/14/17 16:49 2037-26-5
Page 26 of 60

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QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368810 Analysis Method: EPA 245.1
QC Batch Method: EPA 245.1 Analysis Description: 245.1 Mercury
Associated Lab Samples: 92347102006
METHOD BLANK: 2043946 Matrix: Water
Associated Lab Samples: 92347102006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 07/14/17 06:45
LABORATORY CONTROL SAMPLE: 2043947
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 105 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2043948 2043949
MS MSD
92346920003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.6 99 102 70-130 4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2043950 2043951
MS MSD
92347278001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.7 2.7 105 104 70-130 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 27 of 60

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Asheville, NC 28804
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QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368895
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471 Mercury
Associated Lab Samples: 92347102001, 92347102002,
92347102003, 92347102004, 92347102005
METHOD BLANK: 2044301
Matrix: Solid
Associated Lab Samples: 92347102001, 92347102002,
92347102003, 92347102004, 92347102005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mercury mg/kg
ND 0.0060 07/14/17 07:46
LABORATORY CONTROL SAMPLE: 2044302
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury mg/kg
.083 0.087 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2044303 2044304
MS MSD
92346788001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.033
.22 .2 0.22 0.18 85 72 75-125 19 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 28 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368574 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92347102006
METHOD BLANK: 2042687
Matrix:
Water
Associated Lab Samples: 92347102006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
ug/L
ND
10.0
07/14/17 22:02
Barium
ug/L
ND
5.0
07/14/17 22:02
Cadmium
ug/L
ND
1.0
07/14/17 22:02
Chromium
ug/L
ND
5.0
07/14/17 22:02
Lead
ug/L
ND
5.0
07/15/1715:41
Selenium
ug/L
ND
10.0
07/14/17 22:02
Silver
ug/L
ND
5.0
07/14/17 22:02
LABORATORY CONTROL SAMPLE:
2042688
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
ug/L
500
494
99
85-115
Barium
ug/L
500
519
104
85-115
Cadmium
ug/L
500
513
103
85-115
Chromium
ug/L
500
497
99
85-115
Lead
ug/L
500
521
104
85-115
Selenium
ug/L
500
526
105
85-115
Silver
ug/L
250
258
103
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2042689
2042690
MS
MSD
92347102006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
ug/L
ND
500
500
483
458
83
78
70-130
5
Barium
ug/L
3440
500
500
4150
3980
141
108
70-130
4 M6
Cadmium
ug/L
ND
500
500
487
436
97
87
70-130
11
Chromium
ug/L
264
500
500
749
687
97
85
70-130
9
Lead
ug/L
207
500
500
676
655
94
90
70-130
3
Selenium
ug/L
ND
500
500
435
356
84
68
70-130
20 M6
Silver
ug/L
ND
250
250
232
211
93
84
70-130
10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2042691
2042692
MS
MSD
92346828002 Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec
% Rec Limits RPD Qual
Arsenic ug/L ND 500
500
7.6J
5.7J 1
1 70-130 M1
Barium ug/L 590 500
500
575
579 -3
-2 70-130 1 M1
Results presented on this page are in the units indicated by the
"Units" column except where
an alternate unit is presented
to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 29 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2042691
2042692
MS
MSD
92346828002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cadmium ug/L
ND
500
500
ND
ND
0
0
70-130
M1
Chromium ug/L
24300
500
500
23000
23800
-256
-90
70-130
4 M6
Lead ug/L
132
500
500
131
132
0
0
70-130
1 M1
Selenium ug/L
87.3
500
500
80.9
84.9
-1
0
70-130
5 M1
Silver ug/L
ND
250
250
ND
ND
0
0
70-130
M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 30 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368720 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92347102001, 92347102002, 92347102003, 92347102004, 92347102005
METHOD BLANK: 2043367
Matrix:
Solid
Associated Lab Samples:
92347102001, 92347102002,
92347102003, 92347102004, 92347102005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
1.0
07/16/17 01:00
Barium
mg/kg
ND
0.50
07/16/17 01:00
Cadmium
mg/kg
ND
0.10
07/16/17 01:00
Chromium
mg/kg
ND
0.50
07/16/17 01:00
Lead
mg/kg
ND
0.50
07/16/17 01:00
Selenium
mg/kg
ND
1.0
07/16/17 01:00
Silver
mg/kg
ND
0.50
07/16/17 01:00
LABORATORY CONTROL SAMPLE:
2043368
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
48.6
97
80-120
Barium
mg/kg
50
52.7
105
80-120
Cadmium
mg/kg
50
51.0
102
80-120
Chromium
mg/kg
50
50.5
101
80-120
Lead
mg/kg
50
49.7
99
80-120
Selenium
mg/kg
50
50.9
102
80-120
Silver
mg/kg
25
25.8
103
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2043369
2043370
MS
MSD
92347036003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
2.1
48.2
43
37.0
31.1
72
67
75-125
17 M1
Barium
mg/kg
78.3
48.2
43
118
107
83
67
75-125
10 M1
Cadmium
mg/kg
ND
48.2
43
38.5
32.3
80
75
75-125
17
Chromium
mg/kg
18.2
48.2
43
57.1
49.9
81
74
75-125
14 M1
Lead
mg/kg
15.8
48.2
43
51.6
46.4
74
71
75-125
10 M1
Selenium
mg/kg
ND
48.2
43
38.0
31.8
77
72
75-125
18 M1
Silver
mg/kg
ND
24.1
21.4
19.6
16.7
81
77
75-125
16
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 31 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368943 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92347102006
METHOD BLANK: 2044698
Associated Lab Samples: 92347102006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
07/14/17 14:15
1,1,1-Trichloroethane
ug/L
ND
0.50
07/14/17 14:15
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
07/14/17 14:15
1,1,2-Trichloroethane
ug/L
ND
0.50
07/14/17 14:15
1,1-Dichloroethane
ug/L
ND
0.50
07/14/17 14:15
1,1-Dichloroethene
ug/L
ND
0.50
07/14/17 14:15
1,1-Dichloropropene
ug/L
ND
0.50
07/14/17 14:15
1,2,3-Trichlorobenzene
ug/L
ND
2.0
07/14/17 14:15
1,2,3-Trichloropropane
ug/L
ND
0.50
07/14/17 14:15
1,2,4-Trichlorobenzene
ug/L
ND
2.0
07/14/17 14:15
1,2,4-Trimethylbenzene
ug/L
ND
0.50
07/14/17 14:15
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
07/14/17 14:15
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
07/14/17 14:15
1,2-Dichlorobenzene
ug/L
ND
0.50
07/14/17 14:15
1,2-Dichloroethane
ug/L
ND
0.50
07/14/17 14:15
1,2-Dichloropropane
ug/L
ND
0.50
07/14/17 14:15
1,3,5-Trimethylbenzene
ug/L
ND
0.50
07/14/17 14:15
1,3-Dichlorobenzene
ug/L
ND
0.50
07/14/17 14:15
1,3-Dichloropropane
ug/L
ND
0.50
07/14/17 14:15
1,4-Dichlorobenzene
ug/L
ND
0.50
07/14/17 14:15
2,2-Dichloropropane
ug/L
ND
0.50
07/14/17 14:15
2-Chlorotoluene
ug/L
ND
0.50
07/14/17 14:15
4-Chlorotoluene
ug/L
ND
0.50
07/14/17 14:15
Benzene
ug/L
ND
0.50
07/14/17 14:15
Bromobenzene
ug/L
ND
0.50
07/14/17 14:15
Bromochloromethane
ug/L
ND
0.50
07/14/17 14:15
Bromodichloromethane
ug/L
ND
0.50
07/14/17 14:15
Bromoform
ug/L
ND
0.50
07/14/17 14:15
Bromomethane
ug/L
ND
5.0
07/14/17 14:15
Carbon tetrachloride
ug/L
ND
0.50
07/14/17 14:15
Chlorobenzene
ug/L
ND
0.50
07/14/17 14:15
Chloroethane
ug/L
ND
1.0
07/14/17 14:15
Chloroform
ug/L
ND
0.50
07/14/17 14:15
Chloromethane
ug/L
ND
1.0
07/14/17 14:15
cis-1,2-Dichloroethene
ug/L
ND
0.50
07/14/17 14:15
cis-1,3-Dichloropropene
ug/L
ND
0.50
07/14/17 14:15
Dibromochloromethane
ug/L
ND
0.50
07/14/17 14:15
Dibromomethane
ug/L
ND
0.50
07/14/17 14:15
Dichlorodifluoromethane
ug/L
ND
0.50
07/14/17 14:15
Diisopropyl ether
ug/L
ND
0.50
07/14/17 14:15
Ethylbenzene
ug/L
ND
0.50
07/14/17 14:15
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
METHOD BLANK: 2044698
Associated Lab Samples: 92347102006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
07/14/17 14:15
Isopropylbenzene (Cumene)
ug/L
ND
0.50
07/14/17 14:15
m&p-Xylene
ug/L
ND
1.0
07/14/17 14:15
Methyl-tert-butyl ether
ug/L
ND
0.50
07/14/17 14:15
Methylene Chloride
ug/L
ND
2.0
07/14/17 14:15
n-Butylbenzene
ug/L
ND
0.50
07/14/17 14:15
n-Propylbenzene
ug/L
ND
0.50
07/14/17 14:15
Naphthalene
ug/L
ND
2.0
07/14/17 14:15
o-Xylene
ug/L
ND
0.50
07/14/17 14:15
sec-Butylbenzene
ug/L
ND
0.50
07/14/17 14:15
Styrene
ug/L
ND
0.50
07/14/17 14:15
tert-Butyl benzene
ug/L
ND
0.50
07/14/17 14:15
Tetrachloroethene
ug/L
ND
0.50
07/14/17 14:15
Toluene
ug/L
ND
0.50
07/14/17 14:15
trans-1,2-Dichloroethene
ug/L
ND
0.50
07/14/17 14:15
trans- 1,3-Dichloropropene
ug/L
ND
0.50
07/14/17 14:15
Trichloroethene
ug/L
ND
0.50
07/14/17 14:15
Trichlorofluoromethane
ug/L
ND
1.0
07/14/17 14:15
Vinyl chloride
ug/L
ND
1.0
07/14/17 14:15
1,2-Dichloroethane-d4 (S)
%
104
70-130
07/14/17 14:15
4-Bromofluorobenzene (S)
%
102
70-130
07/14/17 14:15
Toluene-d8 (S)
%
105
70-130
07/14/17 14:15
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2044699
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
50.0
100
60-140
1,1,1-Trichloroethane
ug/L
50
54.7
109
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
48.7
97
60-140
1,1,2-Trichloroethane
ug/L
50
50.8
102
60-140
1,1-Dichloroethane
ug/L
50
55.8
112
60-140
1,1-Dichloroethene
ug/L
50
51.5
103
60-140
1,1-Dichloropropene
ug/L
50
55.9
112
60-140
1,2,3-Trichlorobenzene
ug/L
50
49.4
99
60-140
1,2,3-Trichloropropane
ug/L
50
48.8
98
60-140
1,2,4-Trichlorobenzene
ug/L
50
46.9
94
60-140
1,2,4-Trimethylbenzene
ug/L
50
51.0
102
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
45.9
92
60-140
1,2-Dibromoethane (EDB)
ug/L
50
49.1
98
60-140
1,2-Dichlorobenzene
ug/L
50
47.5
95
60-140
1,2-Dichloroethane
ug/L
50
50.2
100
60-140
1,2-Dichloropropane
ug/L
50
51.4
103
60-140
1,3,5-Trimethylbenzene
ug/L
50
50.4
101
60-140
1,3-Dichlorobenzene
ug/L
50
47.8
96
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
LABORATORY CONTROL SAMPLE:
Parameter
2044699
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
52.3
105
60-140
1,4-Dichlorobenzene
ug/L
50
48.4
97
60-140
2,2-Dichloropropane
ug/L
50
56.2
112
60-140
2-Chlorotoluene
ug/L
50
52.1
104
60-140
4-Chlorotoluene
ug/L
50
50.5
101
60-140
Benzene
ug/L
50
52.0
104
60-140
Bromobenzene
ug/L
50
48.5
97
60-140
Bromochloromethane
ug/L
50
54.9
110
60-140
Bromodichloromethane
ug/L
50
53.4
107
60-140
Bromoform
ug/L
50
48.9
98
60-140
Bromomethane
ug/L
50
49.6
99
60-140
Carbon tetrachloride
ug/L
50
50.0
100
60-140
Chlorobenzene
ug/L
50
49.6
99
60-140
Chloroethane
ug/L
50
49.1
98
60-140
Chloroform
ug/L
50
55.0
110
60-140
Chloromethane
ug/L
50
49.1
98
60-140
cis-1,2-Dichloroethene
ug/L
50
54.8
110
60-140
cis-1,3-Dichloropropene
ug/L
50
55.8
112
60-140
Dibromochloromethane
ug/L
50
54.5
109
60-140
Dibromomethane
ug/L
50
48.1
96
60-140
Dichlorodifluoromethane
ug/L
50
54.7
109
60-140
Diisopropyl ether
ug/L
50
58.2
116
60-140
Ethylbenzene
ug/L
50
50.9
102
60-140
Hexachloro-1,3-butadiene
ug/L
50
46.6
93
60-140
Isopropylbenzene (Cumene)
ug/L
50
49.5
99
60-140
m&p-Xylene
ug/L
100
99.6
100
60-140
Methyl-tert-butyl ether
ug/L
50
56.4
113
60-140
Methylene Chloride
ug/L
50
58.4
117
60-140
n-Butylbenzene
ug/L
50
50.3
101
60-140
n-Propylbenzene
ug/L
50
49.9
100
60-140
Naphthalene
ug/L
50
49.4
99
60-140
o-Xylene
ug/L
50
49.3
99
60-140
sec-Butylbenzene
ug/L
50
49.2
98
60-140
Styrene
ug/L
50
50.6
101
60-140
tert-Butyl benzene
ug/L
50
41.3
83
60-140
Tetrachloroethene
ug/L
50
42.9
86
60-140
Toluene
ug/L
50
50.9
102
60-140
trans-1,2-Dichloroethene
ug/L
50
54.2
108
60-140
trans- 1,3-Dichloropropene
ug/L
50
56.5
113
60-140
Trichloroethene
ug/L
50
50.2
100
60-140
Trichlorofluoromethane
ug/L
50
49.1
98
60-140
Vinyl chloride
ug/L
50
52.2
104
60-140
1,2-Dichloroethane-d4 (S)
%
107
70-130
4-Bromofluorobenzene (S)
%
104
70-130
Toluene-d8 (S)
%
102
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2046900
2046901
MS
MSD
92347293003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD
Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.4
21.5
112
107
60-140
4
1,1,1-Trichloroethane
ug/L
ND
20
20
25.9
25.2
130
126
60-140
3
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.6
20.9
108
104
60-140
3
1,1,2-Trichloroethane
ug/L
ND
20
20
21.9
21.1
109
105
60-140
4
1,1-Dichloroethane
ug/L
ND
20
20
25.6
24.5
128
122
60-140
5
1,1-Dichloroethene
ug/L
ND
20
20
25.1
23.7
126
118
60-140
6
1,1-Dichloropropene
ug/L
ND
20
20
26.6
25.5
133
128
60-140
4
1,2,3-Trichlorobenzene
ug/L
ND
20
20
23.2
23.5
116
117
60-140
1
1,2,3-Trichloropropane
ug/L
ND
20
20
21.4
21.3
107
107
60-140
0
1,2,4-Trichlorobenzene
ug/L
ND
20
20
22.0
21.5
110
107
60-140
2
1,2,4-Trimethylbenzene
ug/L
ND
20
20
24.5
23.2
122
116
60-140
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
20.8
20.1
104
101
60-140
3
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
22.0
21.4
110
107
60-140
3
1,2-Dichlorobenzene
ug/L
ND
20
20
22.4
20.9
112
104
60-140
7
1,2-Dichloroethane
ug/L
ND
20
20
22.3
21.5
111
108
60-140
3
1,2-Dichloropropane
ug/L
ND
20
20
23.2
22.3
116
111
60-140
4
1,3,5-Trimethylbenzene
ug/L
ND
20
20
24.4
23.2
122
116
60-140
5
1,3-Dichlorobenzene
ug/L
ND
20
20
22.5
21.3
113
107
60-140
5
1,3-Dichloropropane
ug/L
ND
20
20
23.2
22.9
116
115
60-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
23.0
21.7
115
108
60-140
6
2,2-Dichloropropane
ug/L
ND
20
20
26.0
24.5
130
123
60-140
6
2-Chlorotoluene
ug/L
ND
20
20
24.9
23.9
124
120
60-140
4
4-Chlorotoluene
ug/L
ND
20
20
24.2
23.3
121
117
60-140
4
Benzene
ug/L
ND
20
20
23.5
23.0
118
115
60-140
2
Bromobenzene
ug/L
ND
20
20
23.2
22.4
116
112
60-140
4
Bromochloromethane
ug/L
ND
20
20
24.5
23.6
123
118
60-140
4
Bromodichloromethane
ug/L
ND
20
20
23.4
22.8
117
114
60-140
3
Bromoform
ug/L
ND
20
20
21.1
19.1
105
96
60-140
10
Bromomethane
ug/L
ND
20
20
22.4
21.9
112
109
60-140
2
Carbon tetrachloride
ug/L
ND
20
20
24.0
23.3
120
117
60-140
3
Chlorobenzene
ug/L
ND
20
20
22.8
21.7
114
109
60-140
5
Chloroethane
ug/L
ND
20
20
24.3
22.1
122
111
60-140
9
Chloroform
ug/L
ND
20
20
25.3
24.1
127
121
60-140
5
Chloromethane
ug/L
ND
20
20
17.9
13.4
90
67
60-140
29
cis-1,2-Dichloroethene
ug/L
ND
20
20
25.3
24.2
127
121
60-140
5
cis-1,3-Dichloropropene
ug/L
ND
20
20
23.5
22.8
117
114
60-140
3
Dibromochloromethane
ug/L
ND
20
20
23.5
22.7
117
113
60-140
3
Dibromomethane
ug/L
ND
20
20
20.8
19.7
104
99
60-140
5
Dichlorodifluoromethane
ug/L
ND
20
20
24.5
23.0
123
115
60-140
7
Diisopropyl ether
ug/L
ND
20
20
25.6
24.7
128
124
60-140
3
Ethylbenzene
ug/L
ND
20
20
24.1
22.9
120
115
60-140
5
Hexachloro-1,3-butadiene
ug/L
ND
20
20
22.6
22.7
113
113
60-140
1
Isopropylbenzene (Cumene)
ug/L
ND
20
20
23.2
22.1
116
111
60-140
5
m&p-Xylene
ug/L
ND
40
40
47.1
44.6
118
111
60-140
5
Methyl-tert-butyl ether
ug/L
ND
20
20
25.3
24.4
126
122
60-140
4
Methylene Chloride
ug/L
ND
20
20
24.6
20.1
123
100
60-140
20
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 60

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[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2046900
2046901
MS
MSD
92347293003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
24.9
23.6
124
118
60-140
5
n-Propylbenzene
ug/L
ND
20
20
25.1
23.9
126
119
60-140
5
Naphthalene
ug/L
ND
20
20
23.2
23.2
116
116
60-140
0
o-Xylene
ug/L
ND
20
20
22.7
21.2
113
106
60-140
7
sec-Butylbenzene
ug/L
0.91
20
20
25.9
24.6
125
119
60-140
5
Styrene
ug/L
ND
20
20
22.5
21.3
112
107
60-140
5
tert-Butyl benzene
ug/L
ND
20
20
20.5
19.8
102
99
60-140
3
Tetrachloroethene
ug/L
ND
20
20
20.6
20.3
101
100
60-140
1
Toluene
ug/L
ND
20
20
23.0
22.1
115
111
60-140
4
trans-1,2-Dichloroethene
ug/L
ND
20
20
25.7
25.1
128
125
60-140
2
trans- 1,3-Dichloropropene
ug/L
ND
20
20
23.0
22.5
115
112
60-140
2
Trichloroethene
ug/L
ND
20
20
22.5
22.2
112
111
60-140
1
Trichlorofluoromethane
ug/L
ND
20
20
24.2
22.7
121
114
60-140
6
Vinyl chloride
ug/L
ND
20
20
24.2
23.1
121
115
60-140
5
1,2-Dichloroethane-d4 (S)
%
112
110
70-130
4-Bromofluorobenzene (S)
%
103
101
70-130
Toluene-d8(S)
%
102
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 60

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368648 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92347102001, 92347102002, 92347102003, 92347102004, 92347102005
METHOD BLANK: 2043044 Matrix: Solid
Associated Lab Samples: 92347102001, 92347102002, 92347102003, 92347102004, 92347102005
Blank Reporting
Parameter Units Result Limit Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0051
07/12/17 12:35
1,1,1-Trichloroethane
mg/kg
ND
0.0051
07/12/17 12:35
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0051
07/12/17 12:35
1,1,2-Trichloroethane
mg/kg
ND
0.0051
07/12/17 12:35
1,1-Dichloroethane
mg/kg
ND
0.0051
07/12/17 12:35
1,1-Dichloroethene
mg/kg
ND
0.0051
07/12/17 12:35
1,1-Dichloropropene
mg/kg
ND
0.0051
07/12/17 12:35
1,2,3-Trichlorobenzene
mg/kg
ND
0.0051
07/12/17 12:35
1,2,3-Trichloropropane
mg/kg
ND
0.0051
07/12/17 12:35
1,2,4-Trichlorobenzene
mg/kg
ND
0.0051
07/12/17 12:35
1,2,4-Trimethylbenzene
mg/kg
ND
0.0051
07/12/17 12:35
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0051
07/12/17 12:35
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0051
07/12/17 12:35
1,2-Dichlorobenzene
mg/kg
ND
0.0051
07/12/17 12:35
1,2-Dichloroethane
mg/kg
ND
0.0051
07/12/17 12:35
1,2-Dichloropropane
mg/kg
ND
0.0051
07/12/17 12:35
1,3,5-Trimethylbenzene
mg/kg
ND
0.0051
07/12/17 12:35
1,3-Dichlorobenzene
mg/kg
ND
0.0051
07/12/17 12:35
1,3-Dichloropropane
mg/kg
ND
0.0051
07/12/17 12:35
1,4-Dichlorobenzene
mg/kg
ND
0.0051
07/12/17 12:35
2,2-Dichloropropane
mg/kg
ND
0.0051
07/12/17 12:35
2-Butanone (MEK)
mg/kg
ND
0.10
07/12/17 12:35
2-Chlorotoluene
mg/kg
ND
0.0051
07/12/17 12:35
2-Hexanone
mg/kg
ND
0.051
07/12/17 12:35
4-Chlorotoluene
mg/kg
ND
0.0051
07/12/17 12:35
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.051
07/12/17 12:35
Acetone
mg/kg
ND
0.10
07/12/17 12:35
Benzene
mg/kg
ND
0.0051
07/12/17 12:35
Bromobenzene
mg/kg
ND
0.0051
07/12/17 12:35
Bromochloromethane
mg/kg
ND
0.0051
07/12/17 12:35
Bromodichloromethane
mg/kg
ND
0.0051
07/12/17 12:35
Bromoform
mg/kg
ND
0.0051
07/12/17 12:35
Bromomethane
mg/kg
ND
0.010
07/12/17 12:35
Carbon tetrachloride
mg/kg
ND
0.0051
07/12/17 12:35
Chlorobenzene
mg/kg
ND
0.0051
07/12/17 12:35
Chloroethane
mg/kg
ND
0.010
07/12/17 12:35
Chloroform
mg/kg
ND
0.0051
07/12/17 12:35
Chloromethane
mg/kg
ND
0.010
07/12/17 12:35
cis-1,2-Dichloroethene
mg/kg
ND
0.0051
07/12/17 12:35
cis-1,3-Dichloropropene
mg/kg
ND
0.0051
07/12/17 12:35
Dibromochloromethane
mg/kg
ND
0.0051
07/12/17 12:35
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
METHOD BLANK: 2043044 Matrix: Solid
Associated Lab Samples: 92347102001, 92347102002, 92347102003, 92347102004, 92347102005
Blank Reporting
Parameter Units Result Limit Analyzed
Dibromomethane
mg/kg
ND
0.0051
07/12/17 12:35
Dichlorodifluoromethane
mg/kg
ND
0.010
07/12/17 12:35
Diisopropyl ether
mg/kg
ND
0.0051
07/12/17 12:35
Ethylbenzene
mg/kg
ND
0.0051
07/12/17 12:35
Hexachloro-1,3-butadiene
mg/kg
ND
0.0051
07/12/17 12:35
Isopropylbenzene (Cumene)
mg/kg
ND
0.0051
07/12/17 12:35
m&p-Xylene
mg/kg
ND
0.010
07/12/17 12:35
Methyl-tert-butyl ether
mg/kg
ND
0.0051
07/12/17 12:35
Methylene Chloride
mg/kg
ND
0.020
07/12/17 12:35
n-Butylbenzene
mg/kg
ND
0.0051
07/12/17 12:35
n-Propylbenzene
mg/kg
ND
0.0051
07/12/17 12:35
Naphthalene
mg/kg
ND
0.0051
07/12/17 12:35
o-Xylene
mg/kg
ND
0.0051
07/12/17 12:35
p-Isopropyltoluene
mg/kg
ND
0.0051
07/12/17 12:35
sec-Butylbenzene
mg/kg
ND
0.0051
07/12/17 12:35
Styrene
mg/kg
ND
0.0051
07/12/17 12:35
tert-Butyl benzene
mg/kg
ND
0.0051
07/12/17 12:35
Tetrachloroethene
mg/kg
ND
0.0051
07/12/17 12:35
Toluene
mg/kg
ND
0.0051
07/12/17 12:35
trans-1,2-Dichloroethene
mg/kg
ND
0.0051
07/12/17 12:35
trans- 1,3-Dichloropropene
mg/kg
ND
0.0051
07/12/17 12:35
Trichloroethene
mg/kg
ND
0.0051
07/12/17 12:35
Trichlorofluoromethane
mg/kg
ND
0.0051
07/12/17 12:35
Vinyl acetate
mg/kg
ND
0.051
07/12/17 12:35
Vinyl chloride
mg/kg
ND
0.010
07/12/17 12:35
Xylene (Total)
mg/kg
ND
0.010
07/12/17 12:35
1,2-Dichloroethane-d4 (S)
%
119
70-132
07/12/17 12:35
4-Bromofluorobenzene (S)
%
104
70-130
07/12/17 12:35
Toluene-d8 (S)
%
103
70-130
07/12/17 12:35
Qualifiers
LABORATORY CONTROL SAMPLE:
2043045
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
.05
0.046
93
74-137
1,1,1-Trichloroethane
mg/kg
.05
0.050
102
67-140
1,1,2,2-Tetrachloroethane
mg/kg
.05
0.042
84
72-141
1,1,2-Trichloroethane
mg/kg
.05
0.045
90
78-138
1,1-Dichloroethane
mg/kg
.05
0.042
84
69-134
1,1-Dichloroethene
mg/kg
.05
0.045
90
67-138
1,1-Dichloropropene
mg/kg
.05
0.050
101
69-139
1,2,3-Trichlorobenzene
mg/kg
.05
0.050
100
70-146
1,2,3-Trichloropropane
mg/kg
.05
0.049
99
69-144
1,2,4-Trichlorobenzene
mg/kg
.05
0.050
100
68-148
1,2,4-Trimethylbenzene
mg/kg
.05
0.051
104
74-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 60

aceAnalytical
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
LABORATORY CONTROL SAMPLE:
Parameter
2043045
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
mg/kg
.05
0.050
100
65-140
1,2-Dibromoethane (EDB)
mg/kg
.05
0.049
100
77-135
1,2-Dichlorobenzene
mg/kg
.05
0.047
95
77-141
1,2-Dichloroethane
mg/kg
.05
0.051
103
65-137
1,2-Dichloropropane
mg/kg
.05
0.049
98
72-136
1,3,5-Trimethylbenzene
mg/kg
.05
0.049
98
76-133
1,3-Dichlorobenzene
mg/kg
.05
0.048
97
74-138
1,3-Dichloropropane
mg/kg
.05
0.050
100
71-139
1,4-Dichlorobenzene
mg/kg
.05
0.048
96
76-138
2,2-Dichloropropane
mg/kg
.05
0.053
106
68-137
2-Butanone (MEK)
mg/kg
.099
0.10
103
58-147
2-Chlorotoluene
mg/kg
.05
0.051
103
73-139
2-Hexanone
mg/kg
.099
0.10
101
62-145
4-Chlorotoluene
mg/kg
.05
0.051
103
76-141
4-Methyl-2-pentanone (MIBK)
mg/kg
.099
0.10
101
64-149
Acetone
mg/kg
.099
0.12
119
53-153
Benzene
mg/kg
.05
0.048
96
73-135
Bromobenzene
mg/kg
.05
0.048
97
75-133
Bromochloromethane
mg/kg
.05
0.045
91
73-134
Bromodichloromethane
mg/kg
.05
0.050
101
71-135
Bromoform
mg/kg
.05
0.043
87
66-141
Bromomethane
mg/kg
.05
0.039
78
53-160
Carbon tetrachloride
mg/kg
.05
0.052
105
60-145
Chlorobenzene
mg/kg
.05
0.049
98
78-130
Chloroethane
mg/kg
.05
0.038
76
64-149
Chloroform
mg/kg
.05
0.048
97
70-134
Chloromethane
mg/kg
.05
0.045
90
52-150
cis-1,2-Dichloroethene
mg/kg
.05
0.051
102
70-133
cis-1,3-Dichloropropene
mg/kg
.05
0.052
105
68-134
Dibromochloromethane
mg/kg
.05
0.047
95
71-138
Dibromomethane
mg/kg
.05
0.046
93
74-130
Dichlorodifluoromethane
mg/kg
.05
0.036
72
40-160
Diisopropyl ether
mg/kg
.05
0.045
92
69-141
Ethylbenzene
mg/kg
.05
0.048
98
75-133
Hexachloro-1,3-butadiene
mg/kg
.05
0.049
99
68-143
Isopropylbenzene (Cumene)
mg/kg
.05
0.046
93
76-143
m&p-Xylene
mg/kg
.099
0.097
98
75-136
Methyl-tert-butyl ether
mg/kg
.05
0.042
85
68-144
Methylene Chloride
mg/kg
.05
0.044
89
45-154
n-Butylbenzene
mg/kg
.05
0.049
98
72-137
n-Propylbenzene
mg/kg
.05
0.048
97
76-136
Naphthalene
mg/kg
.05
0.050
101
68-151
o-Xylene
mg/kg
.05
0.046
93
76-141
p-Isopropyltoluene
mg/kg
.05
0.049
98
76-140
sec-Butylbenzene
mg/kg
.05
0.047
95
79-139
Styrene
mg/kg
.05
0.047
96
79-137
tert-Butyl benzene
mg/kg
.05
0.042
85
74-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
LABORATORY CONTROL SAMPLE:
2043045
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Tetrachloroethene
mg/kg
.05
0.040
80
71-138
Toluene
mg/kg
.05
0.049
98
74-131
trans-1,2-Dichloroethene
mg/kg
.05
0.043
87
67-135
trans- 1,3-Dichloropropene
mg/kg
.05
0.050
102
65-146
Trichloroethene
mg/kg
.05
0.047
95
67-135
Trichlorofluoromethane
mg/kg
.05
0.044
89
59-144
Vinyl acetate
mg/kg
.099
0.086
87
40-160
Vinyl chloride
mg/kg
.05
0.042
85
56-141
Xylene (Total)
mg/kg
.15
0.14
96
76-137
1,2-Dichloroethane-d4 (S)
%
116
70-132
4-Bromofluorobenzene (S)
%
106
70-130
Toluene-d8(S)
%
104
70-130
MATRIX SPIKE SAMPLE:
2044056
92347102001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
.021
0.018
87
70-130
1,1,1-Trichloroethane
mg/kg
ND
.021
0.020
96
70-130
1,1,2,2-Tetrachloroethane
mg/kg
ND
.021
0.023
111
70-130
1,1,2-Trichloroethane
mg/kg
ND
.021
0.020
98
70-130
1,1-Dichloroethane
mg/kg
ND
.021
0.016
79
70-130
1,1-Dichloroethene
mg/kg
ND
.021
0.019
92
49-180
1,1-Dichloropropene
mg/kg
ND
.021
0.020
97
70-130
1,2,3-Trichlorobenzene
mg/kg
ND
.021
0.014
70
70-130
1,2,3-Trichloropropane
mg/kg
ND
.021
0.022
106
70-130
1,2,4-Trichlorobenzene
mg/kg
ND
.021
0.015
74
70-130
1,2,4-Trimethylbenzene
mg/kg
ND
.021
0.019
94
70-130
1,2-Dibromo-3-chloropropane
mg/kg
ND
.021
0.027
134
70-130 M1
1,2-Dibromoethane (EDB)
mg/kg
ND
.021
0.023
111
70-130
1,2-Dichlorobenzene
mg/kg
ND
.021
0.017
86
70-130
1,2-Dichloroethane
mg/kg
ND
.021
0.023
112
70-130
1,2-Dichloropropane
mg/kg
ND
.021
0.019
95
70-130
1,3,5-Trimethylbenzene
mg/kg
ND
.021
0.018
90
70-130
1,3-Dichlorobenzene
mg/kg
ND
.021
0.018
87
70-130
1,3-Dichloropropane
mg/kg
ND
.021
0.022
108
70-130
1,4-Dichlorobenzene
mg/kg
ND
.021
0.018
88
70-130
2,2-Dichloropropane
mg/kg
ND
.021
0.020
100
70-130
2-Butanone (MEK)
mg/kg
ND
.041
.058J
127
70-130
2-Chlorotoluene
mg/kg
ND
.021
0.019
95
70-130
2-Hexanone
mg/kg
ND
.041
0.067
163
70-130 M1
4-Chlorotoluene
mg/kg
ND
.021
0.020
97
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
.041
0.057
140
70-130 M1
Acetone
mg/kg
ND
.041
.088J
56
70-130 M1
Benzene
mg/kg
ND
.021
0.019
91
50-166
Bromobenzene
mg/kg
ND
.021
0.020
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
MATRIX SPIKE SAMPLE:
2044056
92347102001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
mg/kg
ND
.021
0.019
94
70-130
Bromodichloromethane
mg/kg
ND
.021
0.020
97
70-130
Bromoform
mg/kg
ND
.021
0.019
91
70-130
Bromomethane
mg/kg
ND
.021
0.014
68
70-130 M1
Carbon tetrachloride
mg/kg
ND
.021
0.019
93
70-130
Chlorobenzene
mg/kg
ND
.021
0.018
89
43-169
Chloroethane
mg/kg
ND
.021
0.017
82
70-130
Chloroform
mg/kg
ND
.021
0.020
96
70-130
Chloromethane
mg/kg
ND
.021
0.020
96
70-130
cis-1,2-Dichloroethene
mg/kg
ND
.021
0.020
99
70-130
cis-1,3-Dichloropropene
mg/kg
ND
.021
0.020
98
70-130
Dibromochloromethane
mg/kg
ND
.021
0.020
96
70-130
Dibromomethane
mg/kg
ND
.021
0.021
101
70-130
Dichlorodifluoromethane
mg/kg
ND
.021
0.017
84
70-130
Diisopropyl ether
mg/kg
ND
.021
0.020
97
70-130
Ethylbenzene
mg/kg
ND
.021
0.018
87
70-130
Hexachloro-1,3-butadiene
mg/kg
ND
.021
0.012
59
70-130 M1
Isopropylbenzene (Cumene)
mg/kg
ND
.021
0.016
81
70-130
m&p-Xylene
mg/kg
ND
.041
0.037
90
70-130
Methyl-tert-butyl ether
mg/kg
ND
.021
0.021
104
70-130
Methylene Chloride
mg/kg
ND
.021
.017J
86
70-130
n-Butylbenzene
mg/kg
ND
.021
0.016
80
70-130
n-Propylbenzene
mg/kg
ND
.021
0.018
88
70-130
Naphthalene
mg/kg
ND
.021
0.021
103
70-130
o-Xylene
mg/kg
ND
.021
0.017
84
70-130
p-Isopropyltoluene
mg/kg
ND
.021
0.017
83
70-130
sec-Butylbenzene
mg/kg
ND
.021
0.016
81
70-130
Styrene
mg/kg
ND
.021
0.016
76
70-130
tert-Butyl benzene
mg/kg
ND
.021
0.015
75
70-130
Tetrachloroethene
mg/kg
ND
.021
0.015
75
70-130
Toluene
mg/kg
ND
.021
0.019
95
52-163
trans-1,2-Dichloroethene
mg/kg
ND
.021
0.018
86
70-130
trans- 1,3-Dichloropropene
mg/kg
ND
.021
0.021
102
70-130
Trichloroethene
mg/kg
ND
.021
0.017
84
49-167
Trichlorofluoromethane
mg/kg
ND
.021
0.019
92
70-130
Vinyl acetate
mg/kg
ND
.041
0.059
145
70-130 M1
Vinyl chloride
mg/kg
ND
.021
0.018
87
70-130
1,2-Dichloroethane-d4 (S)
%
125
70-132
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8(S)
%
101
70-130
SAMPLE DUPLICATE: 2044055
92347036001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane mg/kg ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
SAMPLE DUPLICATE: 2044055
Parameter
Units
92347036001
Result
Dup
Result
1,1,1-Trichloroethane
mg/kg
ND
ND
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
1,1,2-Trichloroethane
mg/kg
ND
ND
1,1-Dichloroethane
mg/kg
ND
ND
1,1-Dichloroethene
mg/kg
ND
ND
1,1-Dichloropropene
mg/kg
ND
ND
1,2,3-Trichlorobenzene
mg/kg
ND
ND
1,2,3-Trichloropropane
mg/kg
ND
ND
1,2,4-Trichlorobenzene
mg/kg
ND
ND
1,2,4-Trimethylbenzene
mg/kg
ND
ND
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
1,2-Dichlorobenzene
mg/kg
ND
ND
1,2-Dichloroethane
mg/kg
ND
ND
1,2-Dichloropropane
mg/kg
ND
ND
1,3,5-Trimethylbenzene
mg/kg
ND
ND
1,3-Dichlorobenzene
mg/kg
ND
ND
1,3-Dichloropropane
mg/kg
ND
ND
1,4-Dichlorobenzene
mg/kg
ND
ND
2,2-Dichloropropane
mg/kg
ND
ND
2-Butanone (MEK)
mg/kg
ND
ND
2-Chlorotoluene
mg/kg
ND
ND
2-Hexanone
mg/kg
ND
ND
4-Chlorotoluene
mg/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
Acetone
mg/kg
0.59
0.79
Benzene
mg/kg
ND
ND
Bromobenzene
mg/kg
ND
ND
Bromochloromethane
mg/kg
ND
ND
Bromodichloromethane
mg/kg
ND
ND
Bromoform
mg/kg
ND
ND
Bromomethane
mg/kg
ND
ND
Carbon tetrachloride
mg/kg
ND
ND
Chlorobenzene
mg/kg
ND
ND
Chloroethane
mg/kg
ND
ND
Chloroform
mg/kg
ND
ND
Chloromethane
mg/kg
ND
ND
cis-1,2-Dichloroethene
mg/kg
ND
ND
cis-1,3-Dichloropropene
mg/kg
ND
ND
Dibromochloromethane
mg/kg
ND
ND
Dibromomethane
mg/kg
ND
ND
Dichlorodifluoromethane
mg/kg
ND
ND
Diisopropyl ether
mg/kg
ND
ND
Ethylbenzene
mg/kg
ND
ND
Hexachloro-1,3-butadiene
mg/kg
ND
ND
Isopropylbenzene (Cumene)
mg/kg
ND
ND
m&p-Xylene
mg/kg
ND
ND
RPD Qualifiers
28 E
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
SAMPLE DUPLICATE: 2044055
Parameter
Units
92347036001
Result
Dup
Result
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
ND
.0016J
o-Xylene
mg/kg
ND
ND
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
ND
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
122
115
4-Bromofluorobenzene (S)
%
98
96
Toluene-d8(S)
%
101
102
RPD Qualifiers
23
21
17
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 43 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368922 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92347102006
METHOD BLANK: 2044474
Associated Lab Samples: 92347102006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
07/14/17 21:20
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
07/14/17 21:20
2,4,6-Trichlorophenol
ug/L
ND
10.0
07/14/17 21:20
2,4-Dichlorophenol
ug/L
ND
5.0
07/14/17 21:20
2,4-Dimethylphenol
ug/L
ND
10.0
07/14/17 21:20
2,4-Dinitrophenol
ug/L
ND
50.0
07/14/17 21:20
2,4-Dinitrotoluene
ug/L
ND
5.0
07/14/17 21:20
2,6-Dinitrotoluene
ug/L
ND
5.0
07/14/17 21:20
2-Chloronaphthalene
ug/L
ND
5.0
07/14/17 21:20
2-Chlorophenol
ug/L
ND
5.0
07/14/17 21:20
2-Nitrophenol
ug/L
ND
5.0
07/14/17 21:20
3,3'-Dichlorobenzidine
ug/L
ND
25.0
07/14/17 21:20
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
07/14/17 21:20
4-Bromophenylphenyl ether
ug/L
ND
5.0
07/14/17 21:20
4-Chloro-3-methylphenol
ug/L
ND
5.0
07/14/17 21:20
4-Chlorophenylphenyl ether
ug/L
ND
5.0
07/14/17 21:20
4-Nitrophenol
ug/L
ND
50.0
07/14/17 21:20
Acenaphthene
ug/L
ND
5.0
07/14/17 21:20
Acenaphthylene
ug/L
ND
5.0
07/14/17 21:20
Anthracene
ug/L
ND
5.0
07/14/17 21:20
Benzo(a)anthracene
ug/L
ND
5.0
07/14/17 21:20
Benzo(a)pyrene
ug/L
ND
5.0
07/14/17 21:20
Benzo(b)fluoranthene
ug/L
ND
5.0
07/14/17 21:20
Benzo(g,h,i)perylene
ug/L
ND
5.0
07/14/17 21:20
Benzo(k)fluoranthene
ug/L
ND
5.0
07/14/17 21:20
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
07/14/17 21:20
bis(2-Chloroethyl) ether
ug/L
ND
5.0
07/14/17 21:20
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
07/14/17 21:20
Butylbenzylphthalate
ug/L
ND
5.0
07/14/17 21:20
Chrysene
ug/L
ND
5.0
07/14/17 21:20
Di-n-butylphthalate
ug/L
ND
5.0
07/14/17 21:20
Di-n-octylphthalate
ug/L
ND
5.0
07/14/17 21:20
Dibenz(a,h)anthracene
ug/L
ND
5.0
07/14/17 21:20
Diethylphthalate
ug/L
ND
5.0
07/14/17 21:20
Dimethylphthalate
ug/L
ND
5.0
07/14/17 21:20
Fluoranthene
ug/L
ND
5.0
07/14/17 21:20
Fluorene
ug/L
ND
5.0
07/14/17 21:20
Hexachloro-1,3-butadiene
ug/L
ND
5.0
07/14/17 21:20
Hexachlorobenzene
ug/L
ND
5.0
07/14/17 21:20
Hexachlorocyclopentadiene
ug/L
ND
10.0
07/14/17 21:20
Hexachloroethane
ug/L
ND
5.0
07/14/17 21:20
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
METHOD BLANK: 2044474
Matrix:
Water
Associated Lab Samples: 92347102006
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
07/14/17 21:20
Isophorone
ug/L
ND
10.0
07/14/17 21:20
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
07/14/17 21:20
N-Nitrosodimethylamine
ug/L
ND
5.0
07/14/17 21:20
N-Nitrosodiphenylamine
ug/L
ND
10.0
07/14/17 21:20
Naphthalene
ug/L
ND
5.0
07/14/17 21:20
Nitrobenzene
ug/L
ND
5.0
07/14/17 21:20
Pentachlorophenol
ug/L
ND
10.0
07/14/17 21:20
Phenanthrene
ug/L
ND
5.0
07/14/17 21:20
Phenol
ug/L
ND
5.0
07/14/17 21:20
Pyrene
ug/L
ND
5.0
07/14/17 21:20
2,4,6-Tribromophenol (S)
%
88
10-137
07/14/17 21:20
2-Fluorobiphenyl (S)
%
90
15-120
07/14/17 21:20
2-Fluorophenol (S)
%
43
10-120
07/14/17 21:20
Nitrobenzene-d5 (S)
%
86
10-120
07/14/17 21:20
Phenol-d6 (S)
%
29
10-120
07/14/17 21:20
Terphenyl-d14 (S)
%
91
11-131
07/14/17 21:20
LABORATORY CONTROL SAMPLE & LCSD:
2044475
2044476
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
29.9
36.7
60 73
44-142
20
30
2,2'-Oxybis(1-chloropropane)
ug/L
50
34.0
39.6
68 79
36-166
15
30
2,4,6-Trichlorophenol
ug/L
50
44.1
53.3
88 107
37-144
19
30
2,4-Dichlorophenol
ug/L
50
36.3
45.1
73 90
1-191
22
30
2,4-Dimethylphenol
ug/L
50
37.6
48.5
75 97
32-119
25
30
2,4-Dinitrophenol
ug/L
250
210
272
84 109
1-181
26
30
2,4-Dinitrotoluene
ug/L
50
43.8
51.6
88 103
39-139
16
30
2,6-Dinitrotoluene
ug/L
50
44.1
51.8
88 104
50-158
16
30
2-Chloronaphthalene
ug/L
50
38.7
46.1
77 92
60-118
17
30
2-Chlorophenol
ug/L
50
36.2
42.2
72 84
23-134
15
30
2-Nitrophenol
ug/L
50
35.3
43.9
71 88
29-182
22
30
3,3'-Dichlorobenzidine
ug/L
100
77.1
87.8
77 88
1-262
13
30
4,6-Dinitro-2-methyl phenol
ug/L
100
77.9
99.9
78 100
1-181
25
30
4-Bromophenylphenyl ether
ug/L
50
31.9
36.1
64 72
53-127
12
30
4-ChIoro-3-methyl phenol
ug/L
100
74.0
88.2
74 88
22-147
18
30
4-Chlorophenylphenyl ether
ug/L
50
40.4
46.7
81 93
25-158
15
30
4-Nitrophenol
ug/L
250
97.9
119
39 48
1-132
19
30
Acenaphthene
ug/L
50
42.9
51.2
86 102
47-145
18
30
Acenaphthylene
ug/L
50
41.1
48.6
82 97
33-145
17
30
Anthracene
ug/L
50
39.5
45.7
79 91
1-166
14
30
Benzo(a)anthracene
ug/L
50
36.9
42.3
74 85
33-143
14
30
Benzo(a)pyrene
ug/L
50
36.9
41.6
74 83
17-163
12
30
Benzo(b)fluoranthene
ug/L
50
36.9
41.6
74 83
24-159
12
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
LABORATORY CONTROL SAMPLE & LCSD:
2044475
2044476
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Benzo(g,h,i)perylene
ug/L
50
38.7
42.8
77
86
1-219
10
30
Benzo(k)fluoranthene
ug/L
50
37.7
42.5
75
85
11-162
12
30
bis(2-Chloroethoxy)methane
ug/L
50
30.6
37.6
61
75
33-184
20
30
bis(2-Chloroethyl) ether
ug/L
50
33.6
39.0
67
78
12-158
15
30
bis(2-Ethylhexyl)phthalate
ug/L
50
37.4
44.1
75
88
8-158
17
30
Butylbenzylphthalate
ug/L
50
38.0
45.1
76
90
1-152
17
30
Chrysene
ug/L
50
36.5
41.8
73
84
17-168
14
30
Di-n-butylphthalate
ug/L
50
43.5
48.9
87
98
1-118
12
30
Di-n-octylphthalate
ug/L
50
35.7
41.8
71
84
4-146
16
30
Dibenz(a,h)anthracene
ug/L
50
40.5
45.0
81
90
1-227
11
30
Diethylphthalate
ug/L
50
45.8
52.6
92
105
1-114
14
30
Dimethylphthalate
ug/L
50
46.0
53.9
92
108
1-112
16
30
Fluoranthene
ug/L
50
42.3
48.5
85
97
26-137
14
30
Fluorene
ug/L
50
43.1
50.8
86
102
59-121
16
30
Hexachloro-1,3-butadiene
ug/L
50
28.4
34.8
57
70
24-116
20
30
Hexachlorobenzene
ug/L
50
37.2
44.2
74
88
1-152
17
30
Hexachlorocyclopentadiene
ug/L
50
27.8
39.8
56
80
25-150
36
30 R1
Hexachloroethane
ug/L
50
28.7
33.5
57
67
40-113
15
30
Indeno(1,2,3-cd)pyrene
ug/L
50
41.2
45.3
82
91
1-171
10
30
Isophorone
ug/L
50
36.5
44.6
73
89
21-196
20
30
N-Nitroso-di-n-propylamine
ug/L
50
43.5
51.8
87
104
1-230
17
30
N-Nitrosodimethylamine
ug/L
50
25.4
30.8
51
62
25-150
19
30
N-Nitrosodiphenylamine
ug/L
50
40.5
46.6
81
93
25-150
14
30
Naphthalene
ug/L
50
33.7
41.4
67
83
21-133
21
30
Nitrobenzene
ug/L
50
35.1
43.3
70
87
35-180
21
30
Pentachlorophenol
ug/L
100
85.9
106
86
106
14-176
21
30
Phenanthrene
ug/L
50
40.2
46.1
80
92
54-120
14
30
Phenol
ug/L
50
17.1
20.6
34
41
5-112
19
30
Pyrene
ug/L
50
38.4
44.3
77
89
52-115
14
30
2,4,6-Tribromophenol (S)
%
80
93
10-137
2-Fluorobiphenyl (S)
%
83
98
15-120
2-Fluorophenol(S)
%
44
51
10-120
Nitrobenzene-d5(S)
%
73
90
10-120
Phenol-d6 (S)
%
31
38
10-120
Terphenyl-d14(S)
%
88
99
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC.
Page 46 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 369337 Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92347102001, 92347102002, 92347102003, 92347102004, 92347102005
METHOD BLANK: 2046605 Matrix: Solid
Associated Lab Samples: 92347102001, 92347102002, 92347102003, 92347102004, 92347102005
Blank Reporting
Parameter Units Result Limit Analyzed
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
07/18/17 09:36
1,2-Dichlorobenzene
mg/kg
ND
0.33
07/18/17 09:36
1,3-Dichlorobenzene
mg/kg
ND
0.33
07/18/17 09:36
1,4-Dichlorobenzene
mg/kg
ND
0.33
07/18/17 09:36
1-Methylnaphthalene
mg/kg
ND
0.33
07/18/17 09:36
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
07/18/17 09:36
2,4,5-Trichlorophenol
mg/kg
ND
0.33
07/18/17 09:36
2,4,6-Trichlorophenol
mg/kg
ND
0.33
07/18/17 09:36
2,4-Dichlorophenol
mg/kg
ND
0.33
07/18/17 09:36
2,4-Dimethylphenol
mg/kg
ND
0.33
07/18/17 09:36
2,4-Dinitrophenol
mg/kg
ND
1.6
07/18/17 09:36
2,4-Dinitrotoluene
mg/kg
ND
0.33
07/18/17 09:36
2,6-Dinitrotoluene
mg/kg
ND
0.33
07/18/17 09:36
2-Chloronaphthalene
mg/kg
ND
0.33
07/18/17 09:36
2-Chlorophenol
mg/kg
ND
0.33
07/18/17 09:36
2-Methylnaphthalene
mg/kg
ND
0.33
07/18/17 09:36
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
07/18/17 09:36
2-Nitroaniline
mg/kg
ND
1.6
07/18/17 09:36
2-Nitrophenol
mg/kg
ND
0.33
07/18/17 09:36
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
0.33
07/18/17 09:36
3,3'-Dichlorobenzidine
mg/kg
ND
1.6
07/18/17 09:36
3-Nitroaniline
mg/kg
ND
1.6
07/18/17 09:36
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.66
07/18/17 09:36
4-Bromophenylphenyl ether
mg/kg
ND
0.33
07/18/17 09:36
4-Chloro-3-methyl phenol
mg/kg
ND
0.66
07/18/17 09:36
4-Chloroaniline
mg/kg
ND
1.6
07/18/17 09:36
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
07/18/17 09:36
4-Nitroaniline
mg/kg
ND
0.66
07/18/17 09:36
4-Nitrophenol
mg/kg
ND
1.6
07/18/17 09:36
Acenaphthene
mg/kg
ND
0.33
07/18/17 09:36
Acenaphthylene
mg/kg
ND
0.33
07/18/17 09:36
Aniline
mg/kg
ND
0.33
07/18/17 09:36
Anthracene
mg/kg
ND
0.33
07/18/17 09:36
Benzo(a)anthracene
mg/kg
ND
0.33
07/18/17 09:36
Benzo(a)pyrene
mg/kg
ND
0.33
07/18/17 09:36
Benzo(b)fluoranthene
mg/kg
ND
0.33
07/18/17 09:36
Benzo(g,h,i)perylene
mg/kg
ND
0.33
07/18/17 09:36
Benzo(k)fluoranthene
mg/kg
ND
0.33
07/18/17 09:36
Benzoic Acid
mg/kg
ND
1.6
07/18/17 09:36
Benzyl alcohol
mg/kg
ND
0.66
07/18/17 09:36
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
07/18/17 09:36
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
METHOD BLANK: 2046605 Matrix: Solid
Associated Lab Samples: 92347102001, 92347102002, 92347102003, 92347102004, 92347102005
Blank Reporting
Parameter Units Result Limit Analyzed
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
07/18/17 09:36
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
07/18/17 09:36
Butylbenzylphthalate
mg/kg
ND
0.33
07/18/17 09:36
Chrysene
mg/kg
ND
0.33
07/18/17 09:36
Di-n-butylphthalate
mg/kg
ND
0.33
07/18/17 09:36
Di-n-octylphthalate
mg/kg
ND
0.33
07/18/17 09:36
Dibenz(a,h)anthracene
mg/kg
ND
0.33
07/18/17 09:36
Dibenzofuran
mg/kg
ND
0.33
07/18/17 09:36
Diethylphthalate
mg/kg
ND
0.33
07/18/17 09:36
Dimethylphthalate
mg/kg
ND
0.33
07/18/17 09:36
Fluoranthene
mg/kg
ND
0.33
07/18/17 09:36
Fluorene
mg/kg
ND
0.33
07/18/17 09:36
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
07/18/17 09:36
Hexachlorobenzene
mg/kg
ND
0.33
07/18/17 09:36
Hexachlorocyclopentadiene
mg/kg
ND
0.33
07/18/17 09:36
Hexachloroethane
mg/kg
ND
0.33
07/18/17 09:36
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
07/18/17 09:36
Isophorone
mg/kg
ND
0.33
07/18/17 09:36
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
07/18/17 09:36
N-Nitrosodimethylamine
mg/kg
ND
0.33
07/18/17 09:36
N-Nitrosodiphenylamine
mg/kg
ND
0.33
07/18/17 09:36
Naphthalene
mg/kg
ND
0.33
07/18/17 09:36
Nitrobenzene
mg/kg
ND
0.33
07/18/17 09:36
Pentachlorophenol
mg/kg
ND
1.6
07/18/17 09:36
Phenanthrene
mg/kg
ND
0.33
07/18/17 09:36
Phenol
mg/kg
ND
0.33
07/18/17 09:36
Pyrene
mg/kg
ND
0.33
07/18/17 09:36
2,4,6-Tribromophenol (S)
%
76
27-110
07/18/17 09:36
2-Fluorobiphenyl (S)
%
88
30-110
07/18/17 09:36
2-Fluorophenol (S)
%
79
13-110
07/18/17 09:36
Nitrobenzene-d5 (S)
%
80
23-110
07/18/17 09:36
Phenol-d6 (S)
%
75
22-110
07/18/17 09:36
Terphenyl-d14 (S)
%
110
28-110
07/18/17 09:36
Qualifiers
LABORATORY CONTROL SAMPLE:
2046606
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.5
88
36-120
1,2-Dichlorobenzene
mg/kg
1.7
1.5
87
41-120
1,3-Dichlorobenzene
mg/kg
1.7
1.4
86
66-120
1,4-Dichlorobenzene
mg/kg
1.7
1.4
85
42-120
1-Methylnaphthalene
mg/kg
1.7
1.7
101
40-120
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
1.3
77
17-120
2,4,5-Trichlorophenol
mg/kg
1.7
1.8
105
37-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 48 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
LABORATORY CONTROL SAMPLE:
Parameter
2046606
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,6-TrichIorophenol
mg/kg
1.7
1.8
110
40-120
2,4-DichIorophenol
mg/kg
1.7
1.6
93
33-120
2,4-Dimethylphenol
mg/kg
1.7
1.7
102
36-120
2,4-Dinitrophenol
mg/kg
8.3
8.8
106
22-121
2,4-Dinitrotoluene
mg/kg
1.7
1.9
111
60-120
2,6-Dinitrotoluene
mg/kg
1.7
1.8
111
54-120
2-Chloronaphthalene
mg/kg
1.7
1.6
99
41-120
2-Chlorophenol
mg/kg
1.7
1.6
93
39-120
2-Methylnaphthalene
mg/kg
1.7
1.6
97
26-120
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.5
90
41-120
2-Nitroaniline
mg/kg
3.3
3.7
112
45-120
2-Nitrophenol
mg/kg
1.7
1.6
95
35-120
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
1.5
89
35-120
3,3'-Dichlorobenzidine
mg/kg
3.3
3.0
89
16-125
3-Nitroaniline
mg/kg
3.3
3.8
115
45-120
4,6-Dinitro-2-methyl phenol
mg/kg
3.3
3.3
99
46-120
4-Bromophenylphenyl ether
mg/kg
1.7
1.3
76
36-120
4-Chloro-3-methylphenol
mg/kg
3.3
3.7
110
37-120
4-Chloroaniline
mg/kg
3.3
3.2
95
35-120
4-Chlorophenylphenyl ether
mg/kg
1.7
1.6
99
30-120
4-Nitroaniline
mg/kg
3.3
4.2
125
48-120 L1
4-Nitrophenol
mg/kg
8.3
9.9
119
43-120
Acenaphthene
mg/kg
1.7
1.8
109
46-120
Acenaphthylene
mg/kg
1.7
1.8
106
46-120
Aniline
mg/kg
1.7
1.4
83
33-120
Anthracene
mg/kg
1.7
1.7
100
63-120
Benzo(a)anthracene
mg/kg
1.7
1.5
92
61-120
Benzo(a)pyrene
mg/kg
1.7
1.7
100
59-120
Benzo(b)fluoranthene
mg/kg
1.7
1.5
91
55-120
Benzo(g,h,i)perylene
mg/kg
1.7
1.6
93
57-120
Benzo(k)fluoranthene
mg/kg
1.7
1.6
97
56-120
Benzoic Acid
mg/kg
8.3
5.4
65
13-120
Benzyl alcohol
mg/kg
3.3
3.2
97
34-120
bis(2-Chloroethoxy)methane
mg/kg
1.7
1.3
78
21-120
bis(2-Chloroethyl) ether
mg/kg
1.7
1.3
81
25-120
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.7
103
56-123
Butylbenzylphthalate
mg/kg
1.7
1.7
104
57-120
Chrysene
mg/kg
1.7
1.6
93
64-120
Di-n-butylphthalate
mg/kg
1.7
1.8
107
58-120
Di-n-octylphthalate
mg/kg
1.7
1.6
99
47-121
Dibenz(a,h)anthracene
mg/kg
1.7
1.5
93
56-120
Dibenzofuran
mg/kg
1.7
1.8
110
43-120
Diethylphthalate
mg/kg
1.7
1.9
113
55-120
Dimethylphthalate
mg/kg
1.7
2.0
117
54-120
Fluoranthene
mg/kg
1.7
1.7
104
61-120
Fluorene
mg/kg
1.7
1.8
108
51-120
Hexachloro-1,3-butadiene
mg/kg
1.7
1.5
87
22-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 60

Pace Analytical Services, LLC
ceAnalX cal ® hevi Riverside 04
Asheville, NC 28804
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
LABORATORY CONTROL SAMPLE:
Parameter
2046606
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachlorobenzene
mg/kg
1.7
1.5
91
53-120
Hexachlorocyclopentadiene
mg/kg
1.7
1.4
85
18-150
Hexachloroethane
mg/kg
1.7
1.5
88
39-120
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.7
100
58-120
Isophorone
mg/kg
1.7
1.6
98
38-120
N-Nitroso-di-n-propylamine
mg/kg
1.7
1.7
101
30-120
N-Nitrosodimethylamine
mg/kg
1.7
1.6
93
32-120
N-Nitrosodiphenylamine
mg/kg
1.7
1.6
98
50-120
Naphthalene
mg/kg
1.7
1.6
94
38-120
Nitrobenzene
mg/kg
1.7
1.5
91
37-120
Pentachlorophenol
mg/kg
3.3
3.5
104
10-120
Phenanthrene
mg/kg
1.7
1.6
98
62-120
Phenol
mg/kg
1.7
1.7
102
37-120
Pyrene
mg/kg
1.7
1.6
94
63-120
2,4,6-Tribromophenol (S)
%
99
27-110
2-Fluorobiphenyl (S)
%
100
30-110
2-Fluorophenol(S)
%
93
13-110
Nitrobenzene-d5 (S)
%
93
23-110
Phenol-d6 (S)
%
96
22-110
Terphenyl-d14 (S)
%
109
28-110
MATRIX SPIKE SAMPLE:
Parameter
2046607
Units
92347036006
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
ND
2
1.5
73
18-119
1,2-Dichlorobenzene
mg/kg
ND
2
1.4
71
50-110
1,3-Dichlorobenzene
mg/kg
ND
2
1.4
71
27-110
1,4-Dichlorobenzene
mg/kg
ND
2
1.4
70
28-110
1-Methylnaphthalene
mg/kg
ND
2
1.4
72
24-116
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
2
1.3
67
50-150
2,4,5-Trichlorophenol
mg/kg
ND
2
1.8
91
28-110
2,4,6-Trichlorophenol
mg/kg
ND
2
2.0
99
17-117
2,4-Dichlorophenol
mg/kg
ND
2
1.7
88
21-128
2,4-Dimethylphenol
mg/kg
ND
2
1.5
74
10-120
2,4-Dinitrophenol
mg/kg
ND
9.8
8.6
87
10-107
2,4-Dinitrotoluene
mg/kg
ND
2
1.8
92
36-109
2,6-Dinitrotoluene
mg/kg
ND
2
1.8
92
32-110
2-Chloronaphthalene
mg/kg
ND
2
1.6
80
30-107
2-Chlorophenol
mg/kg
ND
2
1.7
84
14-106
2-Methylnaphthalene
mg/kg
ND
2
1.4
72
10-135
2-Methylphenol(o-Cresol)
mg/kg
ND
2
1.5
76
10-124
2-Nitroaniline
mg/kg
ND
3.9
4.1
104
26-116
2-Nitrophenol
mg/kg
ND
2
1.6
82
28-103
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
2
1.5
75
10-109
3,3'-Dichlorobenzidine
mg/kg
ND
3.9
2.5
63
10-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 60

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
MATRIX SPIKE SAMPLE:
2046607
92347036006
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
3-Nitroaniline
mg/kg
ND
3.9
3.9
98
22-110
4,6-Dinitro-2-methyl phenol
mg/kg
ND
3.9
3.6
91
13-121
4-Bromophenylphenyl ether
mg/kg
ND
2
1.2
63
31-109
4-Chloro-3-methylphenol
mg/kg
ND
3.9
3.5
88
13-128
4-Chloroaniline
mg/kg
ND
3.9
3.1
78
18-102
4-Chlorophenylphenyl ether
mg/kg
ND
2
1.5
77
29-112
4-Nitroaniline
mg/kg
ND
3.9
4.0
101
16-111
4-Nitrophenol
mg/kg
ND
9.8
10.1
102
14-135
Acenaphthene
mg/kg
ND
2
1.7
85
26-114
Acenaphthylene
mg/kg
ND
2
1.6
83
32-108
Aniline
mg/kg
ND
2
0.90
46
10-107
Anthracene
mg/kg
ND
2
1.5
78
32-111
Benzo(a)anthracene
mg/kg
ND
2
1.6
74
25-117
Benzo(a)pyrene
mg/kg
ND
2
1.5
73
25-106
Benzo(b)fluoranthene
mg/kg
ND
2
1.6
73
24-110
Benzo(g,h,i)perylene
mg/kg
ND
2
1.5
73
19-112
Benzo(k)fluoranthene
mg/kg
ND
2
1.5
72
24-114
Benzoic Acid
mg/kg
ND
9.8
4.8
49
10-110
Benzyl alcohol
mg/kg
ND
3.9
3.4
86
24-106
bis(2-Chloroethoxy)methane
mg/kg
ND
2
1.4
70
13-119
bis(2-Chloroethyl) ether
mg/kg
ND
2
1.4
70
10-134
bis(2-Ethylhexyl)phthalate
mg/kg
ND
2
1.5
74
10-125
Butylbenzylphthalate
mg/kg
ND
2
1.5
74
18-110
Chrysene
mg/kg
ND
2
1.5
72
30-110
Di-n-butylphthalate
mg/kg
ND
2
1.6
79
19-112
Di-n-octylphthalate
mg/kg
ND
2
1.3
67
17-105
Dibenz(a,h)anthracene
mg/kg
ND
2
1.6
79
23-111
Dibenzofuran
mg/kg
ND
2
1.7
87
35-103
Diethylphthalate
mg/kg
ND
2
1.8
89
27-113
Dimethylphthalate
mg/kg
ND
2
1.9
98
26-111
Fluoranthene
mg/kg
ND
2
1.9
83
33-109
Fluorene
mg/kg
ND
2
1.7
84
32-113
Hexachloro-1,3-butadiene
mg/kg
ND
2
1.4
71
16-116
Hexachlorobenzene
mg/kg
ND
2
1.5
76
27-120
Hexachlorocyclopentadiene
mg/kg
ND
2
1.4
70
10-108
Hexachloroethane
mg/kg
ND
2
1.3
66
10-117
Indeno(1,2,3-cd)pyrene
mg/kg
ND
2
1.6
77
10-122
Isophorone
mg/kg
ND
2
1.6
79
28-114
N-Nitroso-di-n-propylamine
mg/kg
ND
2
1.7
86
27-113
N-Nitrosodimethylamine
mg/kg
ND
2
1.7
88
10-109
N-Nitrosodiphenylamine
mg/kg
ND
2
1.5
78
10-128
Naphthalene
mg/kg
ND
2
1.5
76
25-110
Nitrobenzene
mg/kg
ND
2
1.6
81
18-114
Pentachlorophenol
mg/kg
ND
3.9
3.5
89
10-122
Phenanthrene
mg/kg
ND
2
1.7
82
30-114
Phenol
mg/kg
ND
2
1.6
81
11-102
Pyrene
mg/kg
ND
2
1.8
82
25-116
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
MATRIX SPIKE SAMPLE:
Parameter
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
2046607
Units
92347036006 Spike MS MS
Result Conc. Result % Rec
% Rec
Limits
%
85
27-110
%
75
30-110
%
83
13-110
%
84
23-110
%
86
22-110
%
78
28-110
SAMPLE DUPLICATE: 2046608
Parameter
Units
92347102001
Result
Dup
Result
1,2,4-Trichlorobenzene
mg/kg
ND
ND
1,2-Dichlorobenzene
mg/kg
ND
ND
1,3-Dichlorobenzene
mg/kg
ND
ND
1,4-Dichlorobenzene
mg/kg
ND
ND
1-Methylnaphthalene
mg/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
ND
2,4,5-Trichlorophenol
mg/kg
ND
ND
2,4,6-Trichlorophenol
mg/kg
ND
ND
2,4-Dichlorophenol
mg/kg
ND
ND
2,4-Dimethylphenol
mg/kg
ND
ND
2,4-Dinitrophenol
mg/kg
ND
ND
2,4-Dinitrotoluene
mg/kg
ND
ND
2,6-Dinitrotoluene
mg/kg
ND
ND
2-Chloronaphthalene
mg/kg
ND
ND
2-Chlorophenol
mg/kg
ND
ND
2-Methylnaphthalene
mg/kg
ND
ND
2-Methylphenol(o-Cresol)
mg/kg
ND
ND
2-Nitroaniline
mg/kg
ND
ND
2-Nitrophenol
mg/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
ND
3,3'-Dichlorobenzidine
mg/kg
ND
ND
3-Nitroaniline
mg/kg
ND
ND
4,6-Dinitro-2-methyl phenol
mg/kg
ND
ND
4-Bromophenylphenyl ether
mg/kg
ND
ND
4-Chloro-3-methyl phenol
mg/kg
ND
ND
4-Chloroaniline
mg/kg
ND
ND
4-Chlorophenylphenyl ether
mg/kg
ND
ND
4-Nitroaniline
mg/kg
ND
ND
4-Nitrophenol
mg/kg
ND
ND
Acenaphthene
mg/kg
ND
ND
Acenaphthylene
mg/kg
ND
ND
Aniline
mg/kg
ND
ND
Anthracene
mg/kg
ND
ND
Benzo(a)anthracene
mg/kg
ND
ND
Benzo(a)pyrene
mg/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 52 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
SAMPLE DUPLICATE: 2046608
Parameter
Units
92347102001
Result
Dup
Result
Benzo(b)fluoranthene
mg/kg
ND
ND
Benzo(g,h,i)perylene
mg/kg
ND
ND
Benzo(k)fluoranthene
mg/kg
ND
ND
Benzoic Acid
mg/kg
ND
ND
Benzyl alcohol
mg/kg
ND
ND
bis(2-Chloroethoxy)methane
mg/kg
ND
ND
bis(2-Chloroethyl) ether
mg/kg
ND
ND
bis(2-Ethylhexyl)phthalate
mg/kg
ND
ND
Butylbenzylphthalate
mg/kg
ND
ND
Chrysene
mg/kg
ND
ND
Di-n-butylphthalate
mg/kg
ND
ND
Di-n-octylphthalate
mg/kg
ND
ND
Dibenz(a,h)anthracene
mg/kg
ND
ND
Dibenzofuran
mg/kg
ND
ND
Diethylphthalate
mg/kg
ND
ND
Dimethylphthalate
mg/kg
ND
ND
Fluoranthene
mg/kg
ND
ND
Fluorene
mg/kg
ND
ND
Hexachloro-1,3-butadiene
mg/kg
ND
ND
Hexachlorobenzene
mg/kg
ND
ND
Hexachlorocyclopentadiene
mg/kg
ND
ND
Hexachloroethane
mg/kg
ND
ND
Indeno(1,2,3-cd)pyrene
mg/kg
ND
ND
Isophorone
mg/kg
ND
ND
N-Nitroso-di-n-propylamine
mg/kg
ND
ND
N-Nitrosodimethylamine
mg/kg
ND
ND
N-Nitrosodiphenylamine
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
Nitrobenzene
mg/kg
ND
ND
Pentachlorophenol
mg/kg
ND
ND
Phenanthrene
mg/kg
ND
ND
Phenol
mg/kg
ND
ND
Pyrene
mg/kg
ND
ND
2,4,6-Tribromophenol (S)
%
59
65
2-Fluorobiphenyl (S)
%
49
57
2-Fluorophenol(S)
%
54
62
Nitrobenzene-d5 (S)
%
57
65
Phenol-d6 (S)
%
49
57
Terphenyl-d14 (S)
%
79
86
RPD Qualifiers
9
16
14
12
15
9
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 53 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368620 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92347102001, 92347102002
SAMPLE DUPLICATE: 2042864
92346857003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 13.0 12.9 1
SAMPLE DUPLICATE: 2042865
92347102002 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 11.6 12.6 8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: 1430 Riverside Drive
Pace Project No.: 92347102
QC Batch: 368677 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92347102003, 92347102004, 92347102005
SAMPLE DUPLICATE: 2043184
92346788001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 65.3 68.0 4
SAMPLE DUPLICATE: 2043185
92347291012 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 26.1 26.0 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 55 of 60

Pace Analytical Services, LLC
ceAnalX cal ® hevi Riverside 04
Asheville, NC 28804
www.pacelabs.com [phone]
QUALIFIERS
Project: 1430 Riverside Drive
Pace Project No.: 92347102
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
1g The internal standard response is below criteria. No hits associated with this internal standard. Results unaffected by
high bias.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2017 10:03 AM without the written consent of Pace Analytical Services, LLC. Page 56 of 60

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
1430 Riverside Drive
92347102
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92347102006
TMW-1
EPA 200.7
368574
EPA 200.7
368982
92347102001
SB-1
EPA 3050
368720
EPA 6010
369219
92347102002
SB-2
EPA 3050
368720
EPA 6010
369219
92347102003
SB-3
EPA 3050
368720
EPA 6010
369219
92347102004
SB-4
EPA 3050
368720
EPA 6010
369219
92347102005
SB-5
EPA 3050
368720
EPA 6010
369219
92347102006
TMW-1
EPA 245.1
368810
EPA 245.1
368928
92347102001
SB-1
EPA 7471
368895
EPA 7471
369007
92347102002
SB-2
EPA 7471
368895
EPA 7471
369007
92347102003
SB-3
EPA 7471
368895
EPA 7471
369007
92347102004
SB-4
EPA 7471
368895
EPA 7471
369007
92347102005
SB-5
EPA 7471
368895
EPA 7471
369007
92347102006
TMW-1
EPA 625
368922
EPA 625
369111
92347102001
SB-1
EPA 3546
369337
EPA 8270
369443
92347102002
SB-2
EPA 3546
369337
EPA 8270
369443
92347102003
SB-3
EPA 3546
369337
EPA 8270
369443
92347102004
SB-4
EPA 3546
369337
EPA 8270
369443
92347102005
SB-5
EPA 3546
369337
EPA 8270
369443
92347102006
TMW-1
SM 6200E
368943
92347102001
SB-1
EPA 8260
368648
92347102002
SB-2
EPA 8260
368648
92347102003
SB-3
EPA 8260
368648
92347102004
SB-4
EPA 8260
368648
92347102005
SB-5
EPA 8260
368648
92347102001
SB-1
ASTM D2974-87
368620
92347102002
SB-2
ASTM D2974-87
368620
92347102003
SB-3
ASTM D2974-87
368677
92347102004
SB-4
ASTM D2974-87
368677
92347102005
SB-5
ASTM D2974-87
368677
Date: 07/24/2017 10:03 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 57 of 60

Document Name:
Document Revised: Sept.21, 2016
o
aceAnalgica!
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.01
Pace Quality Office
Laboratory receiving sarnn es:
11She,.6i11„ J Eden[] Greentvood ❑ Huntersville-❑ Ralelgh❑ Mechanirsville❑
ConditionSample Client Name: WO# : 923471Q,2
Receipt�, A � Projec'
�` Illlllll�lll IIII lllill
Courier, d x I ❑UPS ❑USPS Client 92347102
❑ Commercial ❑Pace ❑Other:
I
Custody Seal Present? ❑Yes No Seals Inta t? ❑Yes No )
Date/initials PersoExamining contents:
Packing Material: ❑Bubble Wrap Bubble Bags -]None []Other:
Thermometer:
El IR Gun ID: Type of Ice: �et ❑Blue [:]None❑Samples on ice, cooling process has begun
Correction Factor: Cooler Temp Corrected (°C): ,� Biological Tissue Frozen? ❑Yes ❑No _-QN/A
Temp should be above freezing to 6°C
USDA Regulated Soil (❑ N/A, water sample)
Did samples oriaode in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source {internation
I —Iv— including Hawaii and Puerto Rico)? ❑Yes o
Comments/Discrepancy:
Chain of Custody Present?
Yes
No
❑NIA
1.
Samples Arrived within Hold Time?
es
❑N
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
No
❑N/A
3.
Rush Turn Around Time Requested?
Dyes
No
❑N/A
4.
Sufficient Volume?
Yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
AETYes
es
❑No
No
❑N/A
❑N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7.
Samples Field Filtered?
Dyes
No
❑N/A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC? I
-Includes Date iviati ix: S v
Headspace in VOA Vials (>5-6mm)7
n! Yes
y v__I._.
[]'Yes --
[:]No❑N/A
a No
❑N/A
9.
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
No
❑No
ZN1
1i.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepa ncy:
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? LjYes�No
Date/Time:
Date: ,i
Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
out of hold, incorrect preservative, out of temp, incorrect containers)
Page 58 of 60

Document Name:
Document Revised: Sept. 21, 2016
o
aceRnalytical
Sample Condition Upon Receipt(SCUR)
Page 2 of 2
Document No.:
F-CAR-CS-033-Rev.01
Issuing Authority:
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range ,for
preservation samples.
**Bottom half of box is to list number of bottles
Project t Wo# ; 92347102
PP: LAP Due Date: 07/18/17
CLIENT: 83-Singleton
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Page 60 of 60

APPENDIX G
Resume of Environmental Professional

Christopher D. Singleton, P.G.
Hydrogeologist/Project Manager
Education:
Bachelor of Science in Geology, University of
Tennessee at Knoxville, 1995
Continuing Education:
EPA Contractor SOP and Overview Workshop
40-hour OSHA 29 CFR 1910.120 H&S
Certified UST Manager, State of Georgia
Phase I Environmental Site Assessments Update -
Workshop, 2007
Professional Registration:
Licensed Geologist, State of North Carolina,
License #1928
Professional Geologist, State of Georgia,
License # 1752
Professional Geologist, State of Tennessee,
License # 3807
Licensed Well Driller, State of North Carolina,
License # 3328-B
Employment History:
2005 — Present
Hydrogeologist/Senior Project President —
Singleton Environmental Inc., Enka, North
Carolina.
2001— 2005
Hydrogeologist/Senior Project Manager —
Mountain Environmental, Waynesville, NC
1998 — 2001
Hydrogeologist/Project Manager — SEI
Environmental, Inc., Atlanta, GA.
1996 —1998
Hydrogeologist/Senior Technician —
Environmental Systems Corporation,
Knoxville, Tennessee.
1995 —1996
Hydrogeologist — R&A Environmental
Services, Inc., Greensboro, North Carolina.
Current Responsibilities:
As a Hydrogeologist/Licensed Driller with
Singleton Environmental, Inc, Mr. Singleton's
current responsibilities include project review
and over site, coordination of field assessment
activities, analytical data interpretation, UST and
groundwater regulatory compliance, final report
preparation, client/regulatory liaison, and
providing all company drilling needs.
Professional Qualifications:
Mr. Singleton's work experience spans 21 years
in the geosciences industry including
management and professional staff positions in
environmental consultation. His range of project
experience includes leaking underground storage
tank (UST) assessment, real estate transaction
environmental assessments, soil and
groundwater assessment, and all drilling
activities that require supervision of a licensed
well driller.
Areas of Competence:
• Underground Storage Tank Site Assessment
• Soil and Groundwater Assessments
• Phase I & II Environmental Assessments
• Drilling and direct push technologies.

Christopher D. Singleton, P.G.
Hydrogeologist/Project Manager
Project Experience:
Benfield Industries (EPA Superfund Site) — Waynesville, NC
Performed remediation system O&M and semi-annual groundwater assessments in
compliance with EPA standard operating procedures. Delineated dissolved phase vertical
and lateral extent of contamination from the former industrial site.
Travel Centers of America — Candler, NC
Performed soil and groundwater release assessment of leaking USTs from a commercial
truck stop facility. Assessment and remediation included free product monitoring and
removal, and supervised installation and monitoring of air sparging and soil vapor
extraction (AS/SVE) remediation system. Reporting used standard comprehensive site
assessment protocol, including groundwater flow maps, contaminant isoconcentration
maps, and chemical analytical results.
Beacon Manufacturing Fire — Swannanoa, NC
Supervised cleanup of #6 oil that was released into the Swannanoa River during the fire
that destroyed the plant in September 2003. Tasks included coordinating cleanup efforts
with local fire departments and health & safety officials, managing different
environmental contractors assisting with cleanup, and assisting general public with
environmental concerns relating to the oil spill.
Town of Forest City — Forest City, NC
Soil and groundwater assessment for a former dry cleaning facility adjacent to the former
Cone Manufacturing facility. Responsibilities include coordinating with regulatory
agencies to create an assessment scope -of -work to enter the North Carolina Brownfields
Program.
Barnardsville Elementary School — Barnardsville, NC
Soil and groundwater assessment of non-commercial UST release of # 2 fuel oil at the
Barnardsville Elementary School. The Comprehensive Site Assessment delineated the
vertical and horizontal extent of soil and groundwater contamination, including
groundwater flow maps, contaminant isoconcentration maps, and chemical analytical
results. Additional responsibilities included all field activities including the installation of
on -site monitoring wells.
Elf Lubricant Spill — Knoxville, TN
Supervised cleanup of 72,000 gallons of hydraulic oil that was released near the
Tennessee River at the Elf Lubricant facility in Knoxville, Tennessee on July 4, 1999.
Tasks included coordinating cleanup efforts with local fire departments and health &
safety officials, managing different environmental contractors assisting with cleanup, and
assisting general public with environmental concerns relating to the oil spill.
2