18045_Seneca Place_Limited Phase II Subsurface Investigation_20140625

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June 25, 2014

LIMITED PHASE II SUBSURFACE
INVESTIGATION

Property Identification:
Seneca Place Shopping Center
5021 and 5033 South Boulevard
Charlotte, Mecklenburg County, North Carolina 28210

AEI Project No. 330810

Prepared for:
United Federal Credit Union (UFCU)
2807 South State Street
Saint Joseph, Michigan 49085

Prepared by:
AEI Consultants
301 McCullough Drive 4th Floor
Charlotte, NC 28262
[phone]
TABLE OF CONTENTS
1.0 SITE DESCRIPTION ............................................................................................................. 1
2.0 BACKGROUND AND PURPOSE ............................................................................................. 2
3.0 INVESTIGATION EFFORTS .................................................................................................. 3
3.1 Health and Safety Plan .................................................................................................................. 3 3.2 Utility Clearance............................................................................................................................ 3 3.3 Geophysical Survey ....................................................................................................................... 4 3.4 Drilling and Soil Sample Collection ................................................................................................. 4
3.5 Groundwater Sample Collection ..................................................................................................... 5
3.6 Boring Destruction ........................................................................................................................ 5
3.7 Laboratory Analyses ...................................................................................................................... 6
3.8 Investigation Derived Wastes ........................................................................................................ 6
4.0 FINDINGS ............................................................................................................................ 7
4.1 Geology and Hydrogeology ............................................................................................................ 7
4.2 Soil Sample Analytical Results ........................................................................................................ 7
4.3 Groundwater Sample Analytical Results .......................................................................................... 8
5.0 SUMMARY AND CONCLUSIONS ........................................................................................... 9
6.0 RECOMMENDATIONS ........................................................................................................10
7.0 REPORT LIMITATIONS AND RELIANCE .............................................................................10
FIGURES
Figure 1 Site Location Map
Figure 2 Site Map

TABLES
Table 1 Summary of Soil Analytical Results - VOCs by USEPA Method 8270
Table 2 Summary of Soil Analytical Results - SVOCs by USEPA Method 8270
Table 3 Summary of Soil Analytical Results – TPH GRO/TPH DRO by USEPA Method 8015 Table 4 Summary of Groundwater Analytical Results - VOCs by USEPA Approved Method 8260 Table 5 Summary of Groundwater Analytical Results - SVOCs by USEPA Approved Method 8270 Table 6 Summary of Groundwater Analytical Results – TPH GRO/TPH DRO by USEPA Method 8015
APPENDICES
Appendix A Laboratory Analytical Reports
Appendix B Boring Logs

June 25, 2014

United Federal Credit Union (NCFCU)
2807 South State Street
Saint Joseph, Michigan 49085 Subject: Limited Phase II Subsurface Investigation
Seneca Place Shopping Center
5021 and 5033 South Boulevard
Charlotte, Mecklenburg County, North Carolina 28210
AEI Project No. 330810
AEI Consultants (AEI) is pleased to provide this report which describes the activities and results
of the Limited Phase II Subsurface Investigation (Phase II) performed at the above referenced
subject property (Figures 1 and 2). This investigation was completed in general accordance
with the authorized scope of services outlined in our proposal number 37582.
1.0 SITE DESCRIPTION
The subject property consists of a multi-tent commercial retail shopping center that is located
on the northeast corner of South Boulevard and Seneca Place in a mixed commercial and residential area of Charlotte, Mecklenburg County, North Carolina. The property totals
approximately 4.21 acres and is improved with two buildings totaling approximately 46,700
square feet in size. The building is constructed on concrete slab-on-grade with brick veneer.
The subject property is currently occupied by Goodyear Hook Tire & Auto, Toppers Pizza, Jasmine Grill, Rapid Tax, Kim Hair Designer, Super Relax, Sharonview, Federal Credit Union and
Happy Nails. In addition to the subject property building, the property is improved with
asphalt-paved parking areas and associated landscaping (Figure 2).
Based on a review of the US Geological Survey (USGS) Charlotte West & Charlotte East, North
Carolina topographic maps, the subject property is situated approximately 723 to 730 feet
above mean sea level (amsl). The local topography is sloped to the northeast and east toward
an unnamed/intermittent stream located approximately 1,800 feet northeast of the subject
property. Based upon topographic map interpretation, the direction of groundwater flow
beneath the subject property is inferred to be to the east.
According to information obtained from the USGS, the area surrounding the subject property is
underlain by igneous deposits of the Paleozoic-era. Based on a review of the USDA Soil Survey,
the soils in the vicinity of the subject property are classified as the Urban series. Soils from this
series are characterized as areas where the soil has been cut, filled, graded and/or covered with
buildings and pavement

Project No. 330810 June 25, 2014 Page 2
Please refer to Section 4.1 below for additional information on the site geology and
groundwater conditions.
2.0 BACKGROUND AND PURPOSE
A Phase I Environmental Site Assessment (ESA) was performed by AEI for the subject property
and documented in a report dated June 2014 (AEI Project Number 330810). As detailed in the Phase I ESA, the subject property was identified as agricultural land from 1938 through 1956.
A residence was constructed on the southern portion of the property in 1956. Residences and
small commercial structures including a doctors’ office, dentist’s office, and a deli occupied the
property from the 1960s until the current structures were built in 1984 and 1985. The building
at 5021 South Boulevard has been operated as Hook Tire and Auto since its initial construction
(~1985). The building at 5033 South Boulevard has been a shopping center with retail,
restaurant and service tenants since construction. Two historical shopping center tenants of
note included Personal Touch Dry Cleaners that occupied Suite D from 1991 until 2002 and
Olan Mills (photo studio) that occupied Suite N during the 1990s.

The subject property was identified on the following databases: underground storage tank
(UST), leaking UST (LUST), Incident Management Database (IMD), US Historical Auto Station,
Resource Conservation Recovery Act (RCRA) – Conditionally-Exempt Small Quantity Generator
(CESQG), US Historical Dry Cleaners.
AEI’s Phase I ESA revealed the following Recognized Environmental Conditions (RECs)
associated with the site and/or nearby properties:

• The Quick Shoppe #5 (adjoining southwest property) operated as a gasoline station from
1957 until 1997. The Responsible Party (RP) was identified as Atlantic Richfield Company
c/o BP Products North America, Inc. (BP). The USTs were removed from this property in
October 1997. The structure was razed in 2007 and redeveloped into a Panda Express
restaurant. Several subsurface investigations have been performed at this facility, which
included the use of an air-sparge/soil vapor extraction (AS/SVE) system to reduce
contaminants in soil and groundwater. The petroleum impacts from the Quick Shoppe #5
have extended onto the subject property. Subsequently, seven groundwater monitoring
wells have been installed on the site (Seneca Place Shopping Center) in order to delineate
these petroleum impacts in groundwater. It should be noted that a Responsible Party has
been identified and has historically taken responsibility for this petroleum release.
• Personal Touch Dry Cleaning formerly occupied Suite “D” on the subject property and was
listed as being a RCRA-CESQG facility that used the dry cleaning solvent tetrachloroethylene
(PCE) from at least March 13, 1991 until approximately 2002. No violations or releases
were reported for this facility. However, based on review of a 2003 Phase I ESA conducted
on the subject property, “housekeeping and chemical management practices by the
operators of the dry cleaning facility were poor”. Though no releases were reported and based on the length of operation (~11 years), there is a potential for an undiscovered
release of dry cleaning solvents at the subject property. It should be noted that AEI
sampled a cross-gradient monitoring well (referred to as MW-10) during the completion of
the Phase I ESA. Results of this sampling did not reveal the presence of petroleum and/or hazardous constituents in groundwater at this cross-gradient location.

Project No. 330810 June 25, 2014 Page 3

• Hook Tire and Auto has performed auto repair at the subject property for approximately 30
years. Onsite personnel reported that surface spills have occurred from broken seals at one
of the four on-site hydraulic lifts. This leaking lift was reportedly repaired approximately
five years ago. In addition, floor drains were observed in the service area of this facility. These floor drains can act as a conduit for hazardous materials to impact the subsurface.

• The adjacent property to the west was identified to previously contain a refinery (referred to
as C&T Refinery) since the 1930, a drum company, and a chemical distribution company.
The area closest to the subject property (identified as Area “C”), was a paint manufacturing
facility (Reichhold Chemical). Reichhold Chemical occupied this area until C&T Refinery
purchased this site in 1990. Various metals, volatiles and polynuclear aromatic
hydrocarbons have been historically identified in soil, groundwater and/or soil gas samples
collected on or adjacent to this facility. Groundwater was identified to flow in an east-
northeasterly direction (towards and away from the subject property). Currently, this
facility is listed as an Inactive Hazardous Waste Sites Priority list.
• Two additional sites located south of the former refinery [Seneca Cleaners (currently a Pep
Boys and U-Haul)] were also identified during a review of NCDENR records to have releases
of petroleum and/or hazardous constituents to soil and/or groundwater. Groundwater at
these sites was variable, with flows to the northeast and east at the former Seneca Cleaners
site and westerly at the U-Haul facility.
To address the RECs identified on or adjacent to the subject property, AEI proposed the
collection of both soil and groundwater samples from beneath the site. The scope of work
proposed for this limited assessment included the installation of nine soil borings to facilitate the
collection of soil and/or groundwater samples and the sampling of three (3) existing on-site monitoring wells associated with the off-site adjoining open LUST case. Six (6) soil samples
and ten (10) groundwater samples were collected during this limited assessment and were
submitted to the laboratory for analysis. 3.0 INVESTIGATION EFFORTS
3.1 Health and Safety Plan
A site-specific health and safety plan was prepared, reviewed by onsite personnel, and kept onsite for the duration of the fieldwork.
3.2 Utility Clearance
On June 12, 2014, AEI contacted North Carolina 811 (NC 811) to identify any public utilities that may adversely impact the proposed subsurface investigation work proposed during this
assessment. NC 811 assigned a utility locate clearance numbers A141632023 and A141632049
for this site. In addition to the required public utility locate services, AEI also contracted with
Suburban Infrastructure Renewal (SIR) to complete private utility clearing services in the area of the proposed borings.

Project No. 330810 June 25, 2014 Page 4
3.3 Geophysical Survey
On June 19, 2014, SIR completed a geophysical survey on the subject property. The survey
conducted by SIR utilized a Noggin Smart Cart with a shielded 250 MHz antenna (GPR) and a
Schonstedt Magnetic Locator. The survey was conducted on the east, south and western sides
of the Hook Tire and Auto building. The objective of the geophysical survey was to evaluate the presence or absence of a suspected/potential septic system or oil/water separator in the
areas surveyed. The geophysical survey identified the presence of an anomaly on the west side
of the building (likely representing a 1,000-gallon waste-oil UST previously addressed by
others). However, no evidence of a current or former septic system and/or oil/water separator was identified during this geophysical survey.

3.4 Drilling and Soil Sample Collection
On June 19, 2014, nine (9) borings (SP-1 through SP-9) were advanced on the subject property
(Figure 2). The borings were advanced by Probe Technology, Inc. (Probe Tech) of Concord,
North Carolina using a Geoprobe® Model 6600 truck mounted direct push rig and Geoprobe®
Model 42M cart. The borings were advanced to depths ranging from 5 to 28 feet below land surface (bls). The location and purpose of each boring are listed below:

• Boring SP-1 was installed in the parking area located along the west-central property
boundary to address possible migration onto the property from the adjacent off-site RECs.

• Boring SP-2 was installed in the parking area located along the northwestern property
boundary to address possible migration onto the property from the adjacent off-site RECs.
• Boring SP-3 was installed in the northwestern corner of the property to address possible
migration onto the property from the adjacent off-site RECs.

• Boring SP-4 was installed adjacent to in-ground hydraulic lift located within the eastern
central portion of the Hook Tire and Auto service area.

• Boring SP-5 was installed near a floor drain located within the northeast portion of the Hook
Tire and Auto service area.

• Boring SP-6 was installed adjacent to the reported leaking in-ground hydraulic lift located within the east-central portion of the Hook Tire and Auto service area.

• Boring SP-7 was installed adjacent to the eastern exterior of Suite “D” that was formerly
occupied by the Personal Touch Dry Cleaning facility.

• Boring SP-8 was installed within the northeastern interior of Suite “D” that was formerly
occupied by the Personal Touch Dry Cleaning facility.
• Boring SP-9 was installed within the southeastern interior of Suite “D” that was formerly
occupied by the Personal Touch Dry Cleaning facility.

Project No. 330810 June 25, 2014 Page 5
The borings installed during this assessment were advanced through both asphalt and concrete
surfaces. Soil samples were collected during the installation of the borings using a 5-foot long
by 2.25-inch diameter Geoprobe® MacroCore™ sampler equipped with a 5-foot long polyvinyl
chloride (PVC) sample sleeve (exterior soil borings) or a 3-foot long by 2.25-inch diameter
Geoprobe® MacroCore™ sampler equipped with a 3-foot long PVC sample sleeve (interior borings). To collect a sample, the sampling device was driven into the subsurface using the
percussion of the direct-push drill rig. Once at the target depth, the sampler was removed from
the ground and the PVC sample sleeve was extracted with the soil inside. A new sleeve was
placed in the sample tube and the sampler was advanced to the last depth of penetration by
adding a 1.5-inch steel drive rod. This procedure was repeated until the sampler reached the
desired target depth or the point of equipment refusal.

To inspect and collect the sample, a section of the PVC liner was removed with a splitting tool
to expose the soil. The soil column was then visually inspected for discoloration, monitored for
odors, measured for organic compounds using a MiniRae® 3000 photoionization detector (PID),
and classified in accordance with the Unified Soil Classification System (USCS). The soil sample exhibiting the highest PID concentration above the observed soil/water interface was selected
for laboratory analysis. PID readings at this site ranged from 0.0 parts per million (ppm) to
10.9 ppm.

All down-hole equipment was decontaminated and rinsed with potable water between each
boring location.
3.5 Groundwater Sample Collection
On June 19, 2014, AEI collected ten (10) groundwater samples from the site, seven from
borings (SP-1 through SP-7) and three from existing monitoring wells (MW-7, MW-8 and MW-
11) installed by other associated with the open LUST case. Groundwater samples were
collected from the site borings utilizing a Geoprobe® SP-16 (SP-16) groundwater sampling
device. To facilitate the collection of groundwater samples, the SP-16 was advanced to a depth
below the surface of the water table utilizing the percussion of the direct push rig. Once at this
depth, the sheath covering the SP-16 screen was removed, thus exposing the internal stainless
steel screen. With the screen exposed, a groundwater sample was collected utilizing a
peristaltic pump and clean disposable tubing.

Groundwater samples were collected from the three (3) monitoring wells by purging with new
single use disposable bailers. A minimum of three volumes of groundwater was purged from
each monitoring well prior to sampling.
3.6 Boring Destruction
Upon completion, each of the borings was backfilled in accordance with the requirements and
resurfaced to match the existing material.

Project No. 330810 June 25, 2014 Page 6
3.7 Laboratory Analyses
The soil and groundwater samples were labeled and placed into a cooler with ice following
sampling. Once sampling was completed, the samples were transferred under appropriate
chain-of-custody documentation to TestAmerica Laboratories, Inc. of Pensacola, Florida.
Laboratory analytical documentation is provided in Appendix A.
The laboratory analysis of collected samples consisted of the following:

Monitoring Well (MW-7 & MW-11) – Groundwater Only
• Volatile Organic Compounds (VOCs) by USEPA approved Method 6200B
• Semi-Volatile Organic Compounds (SVOCs) by USEPA Method 8270
Monitoring Well (MW-8) – Groundwater Only
• VOCs by USEPA approved Method 6200B

Borings SP-1 through SP-3 – Groundwater Only
• VOCs by USEPA approved Method 6200B
• SVOCs by USEPA Method 8270

Borings SP-4 through SP-6 – Soil and Groundwater
• VOCs by USEPA Method 8260 (soil)
• VOCs by USEPA approved Method 6200B (groundwater)
• SVOCs by USEPA Method 8270
• Total Petroleum Hydrocarbons (TPH) Gasoline Range Organics (GRO) by USEPA Method
8015
• Total Petroleum Hydrocarbons (TPH) Diesel Range Organics (DRO) by USEPA Method 8015
Collected and placed on “Hold” at the analyzing laboratory:
• Volatile Petroleum Hydrocarbons (VPH) by the Massachusetts Department of Environmental
Protection (MADEP) Method (MADEP VPH)
• Extractable Petroleum Hydrocarbons (EPH) by the MADEP Method (MADEP EPH)
Borings SP-7 Soil and Groundwater
• VOCs by USEPA Method 8260 (soil)
• VOCs by USEPA approved Method 6200B (groundwater) Borings SP-8 and SP-9 Soil Only
• VOCs by USEPA Method 8260
3.8 Investigation Derived Wastes
A significant amount of investigation derived waste was not generated during this investigation.

Project No. 330810 June 25, 2014 Page 7
4.0 FINDINGS
For the purpose of providing context to the data obtained during this investigation, analytical
results were compared to regulatory screening levels, where available.

The North Carolina Department of Environment and Natural Resources (NCDENR) Inactive Hazardous Site’s Branch utilizes both the Preliminary Health-Base Preliminary Soil Remediation
Goals (PSRG1) and the Protection of Groundwater (PSRG2) for comparison levels for soil
contaminant concentrations at non-UST sites.
NCDENR Division of Waste Management - Underground Storage Tank (NCDENR-DWM-UST)
Section regulates petroleum impacts from USTs in North Carolina in accordance with the
Guidelines for Assessment of Corrective Action, NCDENR UST Section dated July 2008. The NCDENR-DWM-UST section maintains specific standards for TPH petroleum constituents
released from a UST system during site checks, tank closures and initial responses. According
to NCDENR-DWM-UST guidance document Guidelines for Site Checks, Tank Closure, and Initial
Response and Abatement for UST Releases dated March 1, 2007 Version Change 5, Appendix C, Effective August 1, 2012, hydraulic fluid is excluded from the NCDENR UST regulations if used
for operating purposes in equipment or machinery. Although USTs were not identified during
the Phase I ESA, AEI compared the TPH soil concentrations identified at this site to the
comparison levels found in the above referenced document.

The NCDENR utilizes the North Carolina Administrative Code 2L Standards (NCAC 2L Standards)
for evaluation of impacts to groundwater. 4.1 Geology and Hydrogeology
Sediment encountered in each of the borings generally consisted of a brown to light brown to
tan silt and clay of varying amounts. Groundwater was encountered during this assessment at
a depths ranging from 11 to 14 feet bls. Please see the boring logs included as Appendix B for
additional details on the soils encountered during this limited assessment.
4.2 Soil Sample Analytical Results
The following information is a summary of the soil sample analytical test results provided in
Appendix A. This information has also been included in Tables 1 through 3.

• The VOCs acetone and tetrachloroethene (PCE), a chlorinated solvent, by USEPA method 8260 were identified in the soil samples collected during this limited assessment at
concentrations ranging from 0.0079 milligrams per kilogram (mg/kg) to 0.032J1 mg/kg. Of
the VOCs identified in the soil samples collected during this limited assessment, only
concentrations of tetrachloroethene identified in the soil samples collected from borings SP-
6 (9 to 10 feet bls) and SP-9 (5 feet bls) exceeded the comparison level.

• The SVOCs bis(2-ethylhexyl) phthalate and/or n-octadecane by USEPA method 8270 were
identified in each of the soil samples collected inside the Hook Tire and Auto service area at
1 J - Result is less than the RL but greater than or equal to the MDL & the concentration is an approximate value.

Project No. 330810 June 25, 2014 Page 8
concentrations ranging from 0.087J mg/kg to 0.33 JB2 mg/kg. Neither of the SVOC
concentrations identified in these soil samples exceeded their respective comparison levels.

• TPH DRO by USEPA method 8015 was identified in the soil sample SP-4 (9 to 10 feet bls)
and SP-6 (9 to 10 feet bls) collected adjacent to in-ground hydraulic lifts located inside the Hook Tire and Auto service area at concentrations of 120 mg/kg and 59 mg/kg,
respectively. Each of the TPH DRO concentrations identified in these soil samples exceeded
the comparison level.

• TPH GRO was not identified in any of the soil samples collected from inside the Hook Tire
and Auto service area.

It should be noted that TPH DRO and TPH GRO were not collected for analysis from any of the
soil samples collected outside the Hook Tire and Auto service area.
4.3 Groundwater Sample Analytical Results
The following information is a summary of the groundwater sample analytical test results
provided in Appendix A. This information has also been included in Tables 4 through 6.

• The VOCs 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, benzene, chloroform,
ethylbenzene, isopropylbenzene, m-xylene & p-xylene, naphthalene, N-propylbenzene, o-
xylene, p-cymene, tetrachloroethene, trichloroethene, toluene, total xylenes and cis-1,2-
dichloroethene by USEPA approved Method 6200B were identified in the groundwater
samples collected during this limited assessment at concentrations ranging from 0.91J micrograms per liter (µg/l) to 1,500 µg/l. Of the VOCs identified in the groundwater
samples collected during this limited assessment, only concentrations of benzene,
naphthalene, tetrachloroethene and trichloroethene exceeded their respective comparison
levels.

• The SVOC diethyl phthalate by USEPA Method 8270 was identified in the groundwater
samples collected from borings SP-1 through SP-3 (along the western property boundary) at
concentrations ranging from 0.71J µg/l to 0.79 µg/l. None of the concentrations of diethyl
phthalate exceeded their respective comparison level.

• TPH GRO by USEPA method 8015 was identified in the groundwater sample collected from boring SP-6 (SP-6W) at a concentration of 370 µg/l. There is not a groundwater
comparison level for TPH GRO published in the NCDENR-DWM-UST guidance document
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases dated March 1, 2007 Version Change 5, Appendix C, Effective August 1, 2012.

• TPH DRO was not identified in the groundwater samples collected during this limited
assessment.
2 B - Compound was found in the blank and sample.

Project No. 330810 June 25, 2014 Page 9
As previously indicated, it should be noted that TPH DRO and TPH GRO were not collected for
analysis from any of the soil samples collected outside the Hook Tire and Auto service area.
5.0 SUMMARY AND CONCLUSIONS
AEI has completed a Limited Phase II at the subject property to evaluate the potential impacts
to the subsurface beneath the site from the off-site RECs, historical and/or current use of the site for automotive repair as well as a former onsite dry cleaner. A total of six soil samples and
ten groundwater samples were collected during this limited assessment for analytical testing of
the following:

• VOCs by USEPA Method 8260 (soil)
• VOCs by USEPA approved Method 6200B (groundwater)
• SVOCs by USEPA Method 8270
• TPH GRO and TPH DRO by USEPA Method 8015

The soil analytical results were compared to the NCDENR’s PSRG1, PSRG2. Although hydraulic
fluid is excluded from the UST regulations (if used for operating purposes in equipment or
machinery, the TPH soil concentrations were compared to the level identified in the NCDENR-
DWM-UST guidance document Guidelines for Site Checks, Tank Closure, and Initial Response
and Abatement for UST Releases dated March 1, 2007 Version Change 5, Appendix C, Effective
August 1, 2012.

Exceedances of the comparison levels were limited to the following:
Soils
• The VOC tetrachloroethene (PCE), a chlorinated solvent, by USEPA Method 8260 that was
identified in the soil sample collected from boring SP-6 at a concentration of 0.021 mg/kg
(inside the Hook Tire and Auto service area) and from boring SP-9 at a concentration of
0.0079 mg/kg (within the former dry cleaning facility).

• TPH DRO by USEPA Method 8015 that was identified in the soil samples collected from
borings SP-4 and SP-6 at concentrations of 120 mg/kg and 59 mg/kg, respectively (inside
the Hook Tire and Auto service area). As of the date of this report, the additional three soil
samples collected from this site for MADEP VPH and MADEP EPH and submitted to the
analyzing laboratory on a hold basis have not been removed from their hold at the laboratory. If the client requires the additional analysis, this could be performed upon
request for an additional charge.

Groundwater
• The VOCs benzene, naphthalene, tetrachloroethene (PCE) and/or trichloroethene (TCE) by
USEPA approved Method 6200B each exceeded their respective comparison levels. It
should be noted that the benzene and naphthalene concentrations, both petroleum related compounds, were identified in the groundwater sample collected from MW-8 (installed by
others). These concentrations may likely be attributable to the documented petroleum
release at the adjacent former Quick Stop facility. With the exception of the groundwater
sample collected from boring SP-7 (in the apparent downgradient direction from the former dry cleaner) tetrachloroethene was identified in each of the groundwater samples collected

Project No. 330810 June 25, 2014 Page 10
from this site in excess of the established comparison levels (i.e. downgradient of the offsite
RECs and within the Hook Tire and Auto service area). Trichloroethene was identified in
excess of the comparison level in the groundwater sample collected from boring SP-3 that
was collected from the northeastern corner of the subject property and in the apparent
downgradient direction from the offsite RECs.
Based on the findings from this assessment, it appears that the soil and groundwater beneath
the site have been adversely impacted by historical onsite and offsite operations.
6.0 RECOMMENDATIONS
Based on the findings of this limited assessment, AEI recommends that any interested parties
involved discuss the possible options for additional assessment or regulatory reporting with an
environmental attorney.

Although soil gas was not evaluated during this Limited Phase II Subsurface Investigation, if it
is the desire of the interested parties involved to evaluate the potential presence of soil gas
concentrations beneath the site buildings, a soil gas assessment would be required.
7.0 REPORT LIMITATIONS AND RELIANCE
This report presents a summary of work completed by AEI Consultants. The completed work
includes observations and descriptions of site conditions encountered. Where appropriate, it
includes analytical results for samples taken during the course of the work. The number and
location of samples are chosen to provide the requested information, subject to scope of work
for which AEI was retained and limitations inherent in this type of work, but it cannot be
assumed that they are representative of areas not sampled. This report should not be regarded as a guarantee that no further contamination beyond that which could have been detected
within the scope of this investigation is present beneath the subject property. Undocumented,
unauthorized releases of hazardous material, the remains of which are not readily identifiable
by visual inspection and are of different chemical constituents, are difficult and often impossible
to detect within the scope of a chemical specific investigation.

Any conclusions and/or recommendations are based on these analyses and observations, and the governing regulations. Conclusions beyond those stated and reported herein should not be
inferred from this document. These services were performed in accordance with generally
accepted practices, in the environmental engineering and construction field, which existed at
the time and location of the work. No other warranty, either expressed or implied, has been
made.

This investigation was prepared for the sole use and benefit of United Federal Credit Union. All reports, both verbal and written, whether in draft or final, are for the benefit of United Federal
Credit Union. This report has no other purpose and may not be relied upon by any other
person or entity without the written consent of AEI. Either verbally or in writing, third parties
may come into possession of this report or all or part of the information generated as a result of
this work. In the absence of a written agreement with AEI granting such rights, no third parties
shall have rights of recourse or recovery whatsoever under any course of action against AEI, its
officers, employees, vendors, successors or assigns. Reliance is provided in accordance with

Project No. 330810 June 25, 2014 Page 11
AEI’s Proposal and Standard Terms & Conditions executed by United Federal Credit Union on
June 11, 2014. The limitation of liability defined in the Terms and Conditions is the aggregate limit
of AEI’s liability to the client and all relying parties.

If there are any questions regarding our investigation, please do not hesitate to contact either of the undersigned at 678.279.2825.

Sincerely,
AEI Consultants

James D. Cole, P.G. Steven Yekich
National Client Manager Senior Author

FIGURES

TABLES

Sample Date Acetone Tetrachloroethene
Location Collected (mg/kg)(mg/kg)
SP-4-9-10 6/19/2014 0.032 J ND
SP-5-10-11 6/19/2014 0.019 J ND
SP-6-9-10 6/19/2014 0.013 J 0.021
SP-7-10 6/19/2014 0.026 J 0.0042 J
SP-8-5 6/19/2014 0.014 J ND
SP-9-5 6/19/2014 0.024 J 0.0079
12,000 17
24 0.005
Notes:
mg/kg - milligrams per kilogram, or parts per million
Analysis by USEPA SW 846 method 8260
ND - Non Detect
J - Result is less than the RL but greater than or equal to the MDL & the concentration is an approximate value.
PSRG1 = Inactive Hazardous Site’s Branch Preliminary Health-Based Soil Remediation Goals (PSRG) Residential dated January 2014
PSRG2 = Inactive Hazardous Site’s Branch Protection of Groundwater Soil Remediation Goals dated January 2014
TABLE 1
SUMMARY OF SOIL ANALYTICAL RESULTS
VOLATILE ORGANIC COMPOUNDS BY METHOD 8260
Seneca Place Shopping Center
5021 and 5033 South Boulevard
Charlotte, Mecklenburg County, North Carolina 28210
PSRG1
PSRG2
Project No.: 330810
Sample Date Bis(2-ethylhexyl)phthalate n-Octadecane
Location Collected (mg/kg)(mg/kg)
SP-4-9-10 6/19/2014 0.33 JB ND
SP-5-10-11 6/19/2014 0.33 JB ND
SP-6-9-10 6/19/2014 ND 0.087 J
35 NE
7NE
Notes:
mg/kg - milligrams per kilogram, or parts per million
Analysis by USEPA SW 846 method 8270
NE - Not Established
ND - Non Detect
J-Result is less than the RL but greater than or equal to the MDL & the concentration is an approximate value.
B - Compound was found in the blank and sample.
PSRG1 = Inactive Hazardous Site’s Branch Preliminary Health-Based Soil Remediation Goals (PSRG) Residential dated January 2014
PSRG2 = Inactive Hazardous Site’s Branch Protection of Groundwater Soil Remediation Goals dated January 2014
PSRG2
5021 and 5033 South Boulevard
Seneca Place Shopping CenterSEMI-VOLATILE ORGANIC COMPOUNDS BY METHOD 8270
SUMMARY OF SOIL ANALYTICAL RESULTS TABLE 2
Project No.: 330810
Charlotte, Mecklenburg County, North Carolina 28210
PSRG1
TPH GRO TPH DRO
Sample Date C6-C10 C10-C28
Identification Collected (mg/Kg)(mg/Kg)
SP-4-9-10 6/19/2014 ND 120
SP-5-10-11 6/19/2014 ND ND
SP-6-9-10 6/19/2014 ND 59
10 10
Notes:
mg/kg - milligrams per kilogram, or parts per million
GRO - Gasoline Range Organics
DRO - Diesel Range Organics
TPH - Total Petroleum Hydrocarbons
Analysis by USEPA method 8015
ND - Non Detect
Bold results exceed comparison levels
NCDENR UST Reporting Level-Guidelines for Site Checks, Tank Closure, And Initial Response And Abatement For UST Releases-UST Section
North Carolina Department Of Environment And Natural Resources Division Of Waste Management, March 1, 2007 Version Change 5, $SSHQGL[&Effective $XJXVW 1, 201
NCDENR UST Reporting Level
Charlotte, Mecklenburg County, North Carolina 28210
Project No.: 330810
TABLE 3SUMMARY OF SOIL ANALYTICAL RESULTS
TPH GRO & TPH DRO BY METHOD 8015Seneca Place Shopping Center
5021 and 5033 South Boulevard
SampleDate1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Benzene Chloroform cis-1,2-Dichloroethene Ethylbenzene Isopropylbenzene m-Xylene & p-XyleneLocationCollected(µg/l)(µg/l)(µg/l) (µg/l)(µg/l)(µg/l)(µg/l)(µg/l)MW-76/19/2014NDNDNDNDNDNDNDNDMW-86/19/20143149.60.95 JND81.365MW-116/19/2014NDNDND 0.94 J7.3NDNDNDSP-1W6/19/2014NDNDND7.6NDNDNDNDSP-2W6/19/2014NDNDND2.5NDNDNDNDSP-3W6/19/2014NDNDND2.212NDNDNDSP-4W6/19/2014NDNDNDNDNDNDNDNDSP-5W6/19/2014NDND6.4NDNDNDNDNDSP-6W6/19/2014NDNDNDNDNDNDNDNDSP-7W6/19/2014NDNDND29NDNDNDND4004001707060070500*Notes:µg/l - micrograms per liter or parts per billionAnalysis by USEPA Approved method 6200BND - Non DetectNE - Not Established* - Standard is for total XylenesJ-Result is less than the RL but greater than or equal to the MDL & the concentration is an approximate value.Bold results exceed standard2L Standard - Groundwater Classifications and Standards in the North Carolina Administrative Code, Title 15a, Department of Environment, Health, and Natural Resources Subchapter 2LNCDENR 2L StandardTABLE 4SUMMARY OF GROUNDWATER ANALYTICAL RESULTS VOLATILE ORGANIC COMPOUNDS BY METHOD 6200BSeneca Place Shopping Center5021 and 5033 South BoulevardCharlotte, Mecklenburg County, North Carolina 28210Project No.: 330810
SampleDateNaphthalene N-Propylbenzene o-Xylene p-Cymene Tetrachloroethene Trichloroethene Toluene Xylenes, TotalLocationCollected(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)(µg/l)MW-76/19/2014NDNDNDND2NDNDNDMW-86/19/20148.41.9430.91 J1ND3.2110MW-116/19/2014NDNDNDND9.42.1NDNDSP-1W6/19/2014NDNDNDND2.3NDNDNDSP-2W6/19/2014NDNDNDND17NDNDNDSP-3W6/19/2014NDNDNDND1805.4NDNDSP-4W6/19/2014NDNDNDND3.8NDNDNDSP-5W6/19/2014NDNDNDND58NDNDNDSP-6W6/19/2014NDNDNDND1500NDNDNDSP-7W6/19/2014NDNDNDNDNDNDNDND670500*NE0.73600500*Notes:µg/l - micrograms per liter or parts per billionAnalysis by USEPA Approved method 6200BND - Non DetectNE - Not Established* - Standard is for total XylenesJ-Result is less than the RL but greater than or equal to the MDL & the concentration is an approximate value.Bold results exceed standard2L Standard - Groundwater Classifications and Standards in the North Carolina Administrative Code, Title 15a, Department of Environment, Health, and Natural Resources Subchapter 2LNCDENR 2L StandardTABLE 4 (Continued)SUMMARY OF GROUNDWATER ANALYTICAL RESULTS VOLATILE ORGANIC COMPOUNDS BY METHOD 6200BSeneca Place Shopping Center5021 and 5033 South BoulevardCharlotte, Mecklenburg County, North Carolina 28210Project No.: 330810
Sample Date Diethyl phthalate
Location Collected (µg/l)
MW-7 6/19/2014 ND
MW-11 6/19/2014 ND
SP-1W 6/19/2014 0.77 J
SP-2W 6/19/2014 0.79 J
SP-3W 6/19/2014 0.71 J
SP-4W 6/19/2014 ND
SP-5W 6/19/2014 ND
SP-6W 6/19/2014 ND
NCDENR 2L Standard 6,000
Notes:
ug/l - micrograms per liter, or parts per billion
Analysis by USEPA SW 846 method 8270
ND - Non Detect
NE - Not Established
J-Result is less than the RL but greater than or equal to the MDL & the concentration is an approximate value.
2L Standard - Groundwater Classifications and Standards in the North Carolina Administrative Code, Title 15a,
Department Of Environment, Health, and Natural Resources Subchapter 2l
Seneca Place Shopping Center
5021 and 5033 South BoulevardCharlotte, Mecklenburg County, North Carolina 28210
TABLE 5SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
SEMI-VOLATILE ORGANIC COMPOUNDS BY METHOD 8270
Project No.: 330810
Sample Date TPH GRO TPH DROLocationCollected(µg/l)(µg/l)
SP-4W 6/19/2014 ND ND
SP-5W 6/19/2014 ND ND
SP-6W 6/19/2014 370 ND
NE NE
Notes:
µg/l - micrograms per liter or parts per billion
GRO - Gasoline Range Organics
DRO - Diesel Range Organics
TPH - Total Petroleum Hydrocarbons
GRO Analysis by USEPA method 8015
DRO Analysis by USEPA method 8015
ND - Non Detect
NE - Not Established
Charlotte, Mecklenburg County, North Carolina 28210
TABLE 6SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
TPH GRO and TPH DRO by METHOD 8015Seneca Place Shopping Center
5021 and 5033 South Boulevard
Standard
Project No.: 330810

APPENDIX A

LABORATORY ANALYTICAL REPORTS
ANALYTICAL REPORT
Job Number: 400-92351-1
Job Description: Seneca Place
For:
AEI Consultants
6065 Roswell Road
Suite 940
Atlanta, GA 30328-4013
Attention: Steve Yekich
_____________________________________________
Approved for release.
Marty P Edwards
Manager of Project Management
6/24/2014 10:31 PM
Marty P Edwards, Manager of Project Management
3355 McLemore Drive, Pensacola, FL, 32514
[phone]
[e-mail]
06/24/2014
The test results in this report meet all NELAP requirements for accredited parameters, unless otherwise noted, and
relate only to the referenced samples. Pursuant to NELAP, this report may not be reproduced, except in full, without
written approval from the laboratory. For questions please contact the Project Manager at the e-mail address listed on
this page, or the telephone number at the bottom of the page.
TestAmerica Pensacola Certifications and Approvals: Alabama (40150), Arizona (AZ0710), Arkansas (88-0689), Florida
(E81010), Illinois (200041), Iowa (367), Kansas (E-10253), Kentucky UST (53), Louisiana (30748), Maryland (233),
Massachusetts (M-FL094), Michigan (9912), New Hampshire (250507), New Jersey (FL006), North Carolina (314),
Oklahoma (9810), Pennsylvania (68-00467), Rhode Island (LAO00307), South Carolina (96026), Tennessee
(TN02907), Texas (T104704286-09-1), Virginia (00008), Washington (C915), West Virginia (136), USDA Foreign Soil
Permit (P330-08-00006).
TestAmerica Laboratories, Inc.
TestAmerica Pensacola 3355 McLemore Drive, Pensacola, FL 32514
Tel [phone] Fax [phone] www.testamericainc.com
Page 1 of 70
Job Narrative
400-92351-1
Comments
No additional comments.
Receipt
The samples were received on 6/20/2014 8:21 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 0.0º C, 2.0º C and 2.5º C.
GC/MS VOA
Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 400-221058.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: The method blank for batch 400-221232 contained Di-n-butyl phthalate and Bis(2-ethylhexyl) phthalate above the method
detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of
samples was not performed.
Method 8270D: The continuing calibration verification (CCV) associated with batch 400-221174 recovered above the upper control limit
for sulfolane, 1,4-dioxane, and dibenz(a,h)acridine. The samples associated with this CCV were non-detects for the affected analytes;
therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Page 2 of 70
EXECUTIVE SUMMARY - Detections
Client: AEI Consultants Job Number: 400-92351-1
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
400-92351-11 SP-4-9-10
0.033 mg/Kg 8260B0.032 JAcetone
0.52 mg/Kg 8270D0.33 J BBis(2-ethylhexyl) phthalate
16 mg/Kg 8015C120Diesel Range Organics [C10-C28]
0.10 %Moisture36Percent Moisture
400-92351-12 SP-5-10-11
0.031 mg/Kg 8260B0.019 JAcetone
0.46 mg/Kg 8270D0.33 J BBis(2-ethylhexyl) phthalate
0.10 %Moisture29Percent Moisture
400-92351-13 SP-6-9-10
0.029 mg/Kg 8260B0.013 JAcetone
0.0057 mg/Kg 8260B0.021Tetrachloroethene
0.45 mg/Kg 8270D0.21 J BBis(2-ethylhexyl) phthalate
0.45 mg/Kg 8270D0.087 Jn-Octadecane
14 mg/Kg 8015C59Diesel Range Organics [C10-C28]
0.10 %Moisture27Percent Moisture
400-92351-14 SP-7-10
0.031 mg/Kg 8260B0.026 JAcetone
0.0062 mg/Kg 8260B0.0042 JTetrachloroethene
0.10 %Moisture31Percent Moisture
400-92351-15 SP-8-5
0.025 mg/Kg 8260B0.014 JAcetone
0.10 %Moisture20Percent Moisture
400-92351-16 SP-9-5
0.038 mg/Kg 8260B0.024 JAcetone
0.0075 mg/Kg 8260B0.0079Tetrachloroethene
0.10 %Moisture22Percent Moisture
TestAmerica Pensacola Page 3 of 70
METHOD SUMMARY
Client: AEI Consultants Job Number: 400-92351-1
Preparation MethodMethodLab LocationDescription
Matrix:Solid
Volatile Organic Compounds (GC/MS)TAL PEN SW846 8260B
Closed System Purge and Trap TAL PEN SW846 5035
Semivolatile Organic Compounds (GC/MS)TAL PEN SW846 8270D
Ultrasonic Extraction TAL PEN SW846 3550C
GRO by 8015C TAL PEN SW846 8015C
Closed System Purge and Trap TAL PEN SW846 5035
Nonhalogenated Organics using GC/FID -Modified (Diesel
Range Organics)
TAL PEN SW846 8015C
Microwave Extraction TAL PEN SW846 3546
Percent Moisture TAL PEN EPA Moisture
Lab References:
TAL PEN = TestAmerica Pensacola
Method References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Pensacola Page 4 of 70
METHOD / ANALYST SUMMARY
Client: AEI Consultants Job Number: 400-92351-1
Method Analyst Analyst ID
Rodriguez, Cassie A CARSW846 8260B
Waite, Daniel H DHWSW846 8270D
Khramova, Galina R GRKSW846 8015C
Reeves, Isaiah D IDRSW846 8015C
Crawford, Lauren E LECEPA Moisture
TestAmerica Pensacola
Page 5 of 70
SAMPLE SUMMARY
Client: AEI Consultants Job Number: 400-92351-1
Client Sample IDLab Sample ID Client Matrix Sampled Received
Date/Time Date/Time
400-92351-11 SP-4-9-10 Solid 06/19/2014 1130 06/20/2014 0821
400-92351-12 SP-5-10-11 Solid 06/19/2014 1228 06/20/2014 0821
400-92351-13 SP-6-9-10 Solid 06/19/2014 1350 06/20/2014 0821
400-92351-14 SP-7-10 Solid 06/19/2014 1500 06/20/2014 0821
400-92351-15 SP-8-5 Solid 06/19/2014 1340 06/20/2014 0821
400-92351-16 SP-9-5 Solid 06/19/2014 1610 06/20/2014 0821
TestAmerica Pensacola Page 6 of 70
SAMPLE RESULTS
TestAmerica Pensacola
Page 7 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-4-9-10
Client Matrix:% Moisture:36.1
400-92351-11
Solid
Date Sampled: 06/19/2014 1130
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2018
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221424.D
5.849 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.0033 0.00670.00331,1,1,2-Tetrachloroethane
<0.0015 0.00670.00151,1,1-Trichloroethane
<0.0033 0.00670.00331,1,2,2-Tetrachloroethane
<0.0033 0.00670.00331,1,2-Trichloroethane
<0.0011 0.00670.00111,1-Dichloroethane
<0.0033 0.00670.00331,1-Dichloroethene
<0.0033 0.00670.00331,1-Dichloropropene
<0.0033 0.00670.00331,2,3-Trichlorobenzene
<0.0040 0.00670.00401,2,3-Trichloropropane
<0.0027 0.00670.00271,2,4-Trichlorobenzene
<0.0013 0.00670.00131,2,4-Trimethylbenzene
<0.0044 0.00670.00441,2-Dibromo-3-Chloropropane
<0.00095 0.00670.000951,2-Dichlorobenzene
<0.0011 0.00670.00111,2-Dichloroethane
<0.0033 0.00670.00331,2-Dichloropropane
<0.0011 0.00670.00111,3,5-Trimethylbenzene
<0.0013 0.00670.00131,3-Dichlorobenzene
<0.0013 0.00670.00131,3-Dichloropropane
<0.0033 0.00670.00331,4-Dichlorobenzene
<0.0033 0.00670.00332,2-Dichloropropane
<0.0033 0.00670.00332-Chlorotoluene
<0.0067 0.0330.00672-Hexanone
<0.0013 0.00670.00134-Chlorotoluene
0.032 J 0.0330.0098Acetone
<0.0015 0.00670.0015Benzene
<0.0017 0.00670.0017Bromobenzene
<0.0033 0.00670.0033Bromochloromethane
<0.0033 0.00670.0033Bromodichloromethane
<0.0033 0.00670.0033Bromoform
<0.0033 0.00670.0033Bromomethane
<0.0033 0.00670.0033Carbon disulfide
<0.0023 0.00670.0023Carbon tetrachloride
<0.00070 0.00670.00070Chlorobenzene
<0.0033 0.00670.0033Chloroethane
<0.0033 0.00670.0033Chloroform
<0.0013 0.00670.0013Chloromethane
<0.0010 0.00670.0010cis-1,2-Dichloroethene
<0.0016 0.00670.0016cis-1,3-Dichloropropene
<0.0033 0.00670.0033Dibromochloromethane
<0.0033 0.00670.0033Dibromomethane
<0.0017 0.00670.0017Dichlorodifluoromethane
<0.00082 0.00670.00082Ethylbenzene
<0.0013 0.00670.0013Ethylene Dibromide
<0.0033 0.00670.0033Hexachlorobutadiene
<0.0045 0.00670.0045Iodomethane
<0.00074 0.00670.00074Isopropyl ether
TestAmerica Pensacola Page 8 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-4-9-10
Client Matrix:% Moisture:36.1
400-92351-11
Solid
Date Sampled: 06/19/2014 1130
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2018
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221424.D
5.849 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.00091 0.00670.00091Isopropylbenzene
<0.0080 0.0330.0080Methyl Ethyl Ketone
<0.0067 0.0330.0067methyl isobutyl ketone
<0.0013 0.00670.0013Methyl tert-butyl ether
<0.013 0.0200.013Methylene Chloride
<0.0017 0.0130.0017m-Xylene & p-Xylene
<0.0027 0.00670.0027Naphthalene
<0.0013 0.00670.0013n-Butylbenzene
<0.0012 0.00670.0012N-Propylbenzene
<0.0013 0.00670.0013o-Xylene
<0.0013 0.00670.0013p-Cymene
<0.0013 0.00670.0013sec-Butylbenzene
<0.0013 0.00670.0013Styrene
<0.0033 0.00670.0033tert-Butylbenzene
<0.0033 0.00670.0033Tetrachloroethene
<0.0013 0.00670.0013Toluene
<0.0033 0.00670.0033trans-1,2-Dichloroethene
<0.0033 0.00670.0033trans-1,3-Dichloropropene
<0.0013 0.00670.0013Trichloroethene
<0.0033 0.00670.0033Trichlorofluoromethane
<0.012 0.0330.012Vinyl acetate
<0.0033 0.00670.0033Vinyl chloride
<0.0025 0.0130.0025Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
101 72 - 1224-Bromofluorobenzene
97 79 - 123Dibromofluoromethane
96 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 9 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-5-10-11
Client Matrix:% Moisture:28.6
400-92351-12
Solid
Date Sampled: 06/19/2014 1228
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2043
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221425.D
5.556 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.0031 0.00630.00311,1,1,2-Tetrachloroethane
<0.0014 0.00630.00141,1,1-Trichloroethane
<0.0031 0.00630.00311,1,2,2-Tetrachloroethane
<0.0031 0.00630.00311,1,2-Trichloroethane
<0.0010 0.00630.00101,1-Dichloroethane
<0.0031 0.00630.00311,1-Dichloroethene
<0.0031 0.00630.00311,1-Dichloropropene
<0.0031 0.00630.00311,2,3-Trichlorobenzene
<0.0038 0.00630.00381,2,3-Trichloropropane
<0.0025 0.00630.00251,2,4-Trichlorobenzene
<0.0013 0.00630.00131,2,4-Trimethylbenzene
<0.0042 0.00630.00421,2-Dibromo-3-Chloropropane
<0.00089 0.00630.000891,2-Dichlorobenzene
<0.0010 0.00630.00101,2-Dichloroethane
<0.0031 0.00630.00311,2-Dichloropropane
<0.0010 0.00630.00101,3,5-Trimethylbenzene
<0.0012 0.00630.00121,3-Dichlorobenzene
<0.0013 0.00630.00131,3-Dichloropropane
<0.0031 0.00630.00311,4-Dichlorobenzene
<0.0031 0.00630.00312,2-Dichloropropane
<0.0031 0.00630.00312-Chlorotoluene
<0.0063 0.0310.00632-Hexanone
<0.0012 0.00630.00124-Chlorotoluene
0.019 J 0.0310.0092Acetone
<0.0014 0.00630.0014Benzene
<0.0016 0.00630.0016Bromobenzene
<0.0031 0.00630.0031Bromochloromethane
<0.0031 0.00630.0031Bromodichloromethane
<0.0031 0.00630.0031Bromoform
<0.0031 0.00630.0031Bromomethane
<0.0031 0.00630.0031Carbon disulfide
<0.0021 0.00630.0021Carbon tetrachloride
<0.00066 0.00630.00066Chlorobenzene
<0.0031 0.00630.0031Chloroethane
<0.0031 0.00630.0031Chloroform
<0.0013 0.00630.0013Chloromethane
<0.00096 0.00630.00096cis-1,2-Dichloroethene
<0.0015 0.00630.0015cis-1,3-Dichloropropene
<0.0031 0.00630.0031Dibromochloromethane
<0.0031 0.00630.0031Dibromomethane
<0.0016 0.00630.0016Dichlorodifluoromethane
<0.00077 0.00630.00077Ethylbenzene
<0.0013 0.00630.0013Ethylene Dibromide
<0.0031 0.00630.0031Hexachlorobutadiene
<0.0043 0.00630.0043Iodomethane
<0.00069 0.00630.00069Isopropyl ether
TestAmerica Pensacola Page 10 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-5-10-11
Client Matrix:% Moisture:28.6
400-92351-12
Solid
Date Sampled: 06/19/2014 1228
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2043
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221425.D
5.556 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.00086 0.00630.00086Isopropylbenzene
<0.0076 0.0310.0076Methyl Ethyl Ketone
<0.0063 0.0310.0063methyl isobutyl ketone
<0.0013 0.00630.0013Methyl tert-butyl ether
<0.013 0.0190.013Methylene Chloride
<0.0016 0.0130.0016m-Xylene & p-Xylene
<0.0025 0.00630.0025Naphthalene
<0.0012 0.00630.0012n-Butylbenzene
<0.0011 0.00630.0011N-Propylbenzene
<0.0013 0.00630.0013o-Xylene
<0.0013 0.00630.0013p-Cymene
<0.0012 0.00630.0012sec-Butylbenzene
<0.0013 0.00630.0013Styrene
<0.0031 0.00630.0031tert-Butylbenzene
<0.0031 0.00630.0031Tetrachloroethene
<0.0013 0.00630.0013Toluene
<0.0031 0.00630.0031trans-1,2-Dichloroethene
<0.0031 0.00630.0031trans-1,3-Dichloropropene
<0.0013 0.00630.0013Trichloroethene
<0.0031 0.00630.0031Trichlorofluoromethane
<0.011 0.0310.011Vinyl acetate
<0.0031 0.00630.0031Vinyl chloride
<0.0024 0.0130.0024Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
104 72 - 1224-Bromofluorobenzene
99 79 - 123Dibromofluoromethane
95 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 11 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-6-9-10
Client Matrix:% Moisture:27.0
400-92351-13
Solid
Date Sampled: 06/19/2014 1350
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2108
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221426.D
5.999 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.0029 0.00570.00291,1,1,2-Tetrachloroethane
<0.0013 0.00570.00131,1,1-Trichloroethane
<0.0029 0.00570.00291,1,2,2-Tetrachloroethane
<0.0029 0.00570.00291,1,2-Trichloroethane
<0.00095 0.00570.000951,1-Dichloroethane
<0.0029 0.00570.00291,1-Dichloroethene
<0.0029 0.00570.00291,1-Dichloropropene
<0.0029 0.00570.00291,2,3-Trichlorobenzene
<0.0034 0.00570.00341,2,3-Trichloropropane
<0.0023 0.00570.00231,2,4-Trichlorobenzene
<0.0011 0.00570.00111,2,4-Trimethylbenzene
<0.0038 0.00570.00381,2-Dibromo-3-Chloropropane
<0.00081 0.00570.000811,2-Dichlorobenzene
<0.00094 0.00570.000941,2-Dichloroethane
<0.0029 0.00570.00291,2-Dichloropropane
<0.00095 0.00570.000951,3,5-Trimethylbenzene
<0.0011 0.00570.00111,3-Dichlorobenzene
<0.0011 0.00570.00111,3-Dichloropropane
<0.0029 0.00570.00291,4-Dichlorobenzene
<0.0029 0.00570.00292,2-Dichloropropane
<0.0029 0.00570.00292-Chlorotoluene
<0.0057 0.0290.00572-Hexanone
<0.0011 0.00570.00114-Chlorotoluene
0.013 J 0.0290.0083Acetone
<0.0013 0.00570.0013Benzene
<0.0015 0.00570.0015Bromobenzene
<0.0029 0.00570.0029Bromochloromethane
<0.0029 0.00570.0029Bromodichloromethane
<0.0029 0.00570.0029Bromoform
<0.0029 0.00570.0029Bromomethane
<0.0029 0.00570.0029Carbon disulfide
<0.0019 0.00570.0019Carbon tetrachloride
<0.00059 0.00570.00059Chlorobenzene
<0.0029 0.00570.0029Chloroethane
<0.0029 0.00570.0029Chloroform
<0.0011 0.00570.0011Chloromethane
<0.00087 0.00570.00087cis-1,2-Dichloroethene
<0.0014 0.00570.0014cis-1,3-Dichloropropene
<0.0029 0.00570.0029Dibromochloromethane
<0.0029 0.00570.0029Dibromomethane
<0.0015 0.00570.0015Dichlorodifluoromethane
<0.00070 0.00570.00070Ethylbenzene
<0.0011 0.00570.0011Ethylene Dibromide
<0.0029 0.00570.0029Hexachlorobutadiene
<0.0039 0.00570.0039Iodomethane
<0.00063 0.00570.00063Isopropyl ether
TestAmerica Pensacola Page 12 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-6-9-10
Client Matrix:% Moisture:27.0
400-92351-13
Solid
Date Sampled: 06/19/2014 1350
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2108
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221426.D
5.999 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.00078 0.00570.00078Isopropylbenzene
<0.0068 0.0290.0068Methyl Ethyl Ketone
<0.0057 0.0290.0057methyl isobutyl ketone
<0.0011 0.00570.0011Methyl tert-butyl ether
<0.011 0.0170.011Methylene Chloride
<0.0015 0.0110.0015m-Xylene & p-Xylene
<0.0023 0.00570.0023Naphthalene
<0.0011 0.00570.0011n-Butylbenzene
<0.0010 0.00570.0010N-Propylbenzene
<0.0011 0.00570.0011o-Xylene
<0.0011 0.00570.0011p-Cymene
<0.0011 0.00570.0011sec-Butylbenzene
<0.0011 0.00570.0011Styrene
<0.0029 0.00570.0029tert-Butylbenzene
0.021 0.00570.0029Tetrachloroethene
<0.0011 0.00570.0011Toluene
<0.0029 0.00570.0029trans-1,2-Dichloroethene
<0.0029 0.00570.0029trans-1,3-Dichloropropene
<0.0011 0.00570.0011Trichloroethene
<0.0029 0.00570.0029Trichlorofluoromethane
<0.010 0.0290.010Vinyl acetate
<0.0029 0.00570.0029Vinyl chloride
<0.0022 0.0110.0022Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
103 72 - 1224-Bromofluorobenzene
98 79 - 123Dibromofluoromethane
92 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 13 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-7-10
Client Matrix:% Moisture:30.6
400-92351-14
Solid
Date Sampled: 06/19/2014 1500
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2132
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221427.D
5.832 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.0031 0.00620.00311,1,1,2-Tetrachloroethane
<0.0014 0.00620.00141,1,1-Trichloroethane
<0.0031 0.00620.00311,1,2,2-Tetrachloroethane
<0.0031 0.00620.00311,1,2-Trichloroethane
<0.0010 0.00620.00101,1-Dichloroethane
<0.0031 0.00620.00311,1-Dichloroethene
<0.0031 0.00620.00311,1-Dichloropropene
<0.0031 0.00620.00311,2,3-Trichlorobenzene
<0.0037 0.00620.00371,2,3-Trichloropropane
<0.0025 0.00620.00251,2,4-Trichlorobenzene
<0.0012 0.00620.00121,2,4-Trimethylbenzene
<0.0041 0.00620.00411,2-Dibromo-3-Chloropropane
<0.00088 0.00620.000881,2-Dichlorobenzene
<0.0010 0.00620.00101,2-Dichloroethane
<0.0031 0.00620.00311,2-Dichloropropane
<0.0010 0.00620.00101,3,5-Trimethylbenzene
<0.0012 0.00620.00121,3-Dichlorobenzene
<0.0012 0.00620.00121,3-Dichloropropane
<0.0031 0.00620.00311,4-Dichlorobenzene
<0.0031 0.00620.00312,2-Dichloropropane
<0.0031 0.00620.00312-Chlorotoluene
<0.0062 0.0310.00622-Hexanone
<0.0012 0.00620.00124-Chlorotoluene
0.026 J 0.0310.0090Acetone
<0.0014 0.00620.0014Benzene
<0.0016 0.00620.0016Bromobenzene
<0.0031 0.00620.0031Bromochloromethane
<0.0031 0.00620.0031Bromodichloromethane
<0.0031 0.00620.0031Bromoform
<0.0031 0.00620.0031Bromomethane
<0.0031 0.00620.0031Carbon disulfide
<0.0021 0.00620.0021Carbon tetrachloride
<0.00064 0.00620.00064Chlorobenzene
<0.0031 0.00620.0031Chloroethane
<0.0031 0.00620.0031Chloroform
<0.0012 0.00620.0012Chloromethane
<0.00094 0.00620.00094cis-1,2-Dichloroethene
<0.0015 0.00620.0015cis-1,3-Dichloropropene
<0.0031 0.00620.0031Dibromochloromethane
<0.0031 0.00620.0031Dibromomethane
<0.0016 0.00620.0016Dichlorodifluoromethane
<0.00075 0.00620.00075Ethylbenzene
<0.0012 0.00620.0012Ethylene Dibromide
<0.0031 0.00620.0031Hexachlorobutadiene
<0.0042 0.00620.0042Iodomethane
<0.00068 0.00620.00068Isopropyl ether
TestAmerica Pensacola Page 14 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-7-10
Client Matrix:% Moisture:30.6
400-92351-14
Solid
Date Sampled: 06/19/2014 1500
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/22/2014 2132
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06221427.D
5.832 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221047
400-221058
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.00084 0.00620.00084Isopropylbenzene
<0.0074 0.0310.0074Methyl Ethyl Ketone
<0.0062 0.0310.0062methyl isobutyl ketone
<0.0012 0.00620.0012Methyl tert-butyl ether
<0.012 0.0190.012Methylene Chloride
<0.0016 0.0120.0016m-Xylene & p-Xylene
<0.0025 0.00620.0025Naphthalene
<0.0012 0.00620.0012n-Butylbenzene
<0.0011 0.00620.0011N-Propylbenzene
<0.0012 0.00620.0012o-Xylene
<0.0012 0.00620.0012p-Cymene
<0.0012 0.00620.0012sec-Butylbenzene
<0.0012 0.00620.0012Styrene
<0.0031 0.00620.0031tert-Butylbenzene
0.0042 J 0.00620.0031Tetrachloroethene
<0.0012 0.00620.0012Toluene
<0.0031 0.00620.0031trans-1,2-Dichloroethene
<0.0031 0.00620.0031trans-1,3-Dichloropropene
<0.0012 0.00620.0012Trichloroethene
<0.0031 0.00620.0031Trichlorofluoromethane
<0.011 0.0310.011Vinyl acetate
<0.0031 0.00620.0031Vinyl chloride
<0.0023 0.0120.0023Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
100 72 - 1224-Bromofluorobenzene
100 79 - 123Dibromofluoromethane
93 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 15 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-8-5
Client Matrix:% Moisture:19.9
400-92351-15
Solid
Date Sampled: 06/19/2014 1340
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/23/2014 1224
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06231406.D
6.326 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221091
400-221146
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.0025 0.00490.00251,1,1,2-Tetrachloroethane
<0.0011 0.00490.00111,1,1-Trichloroethane
<0.0025 0.00490.00251,1,2,2-Tetrachloroethane
<0.0025 0.00490.00251,1,2-Trichloroethane
<0.00082 0.00490.000821,1-Dichloroethane
<0.0025 0.00490.00251,1-Dichloroethene
<0.0025 0.00490.00251,1-Dichloropropene
<0.0025 0.00490.00251,2,3-Trichlorobenzene
<0.0030 0.00490.00301,2,3-Trichloropropane
<0.0020 0.00490.00201,2,4-Trichlorobenzene
<0.00099 0.00490.000991,2,4-Trimethylbenzene
<0.0033 0.00490.00331,2-Dibromo-3-Chloropropane
<0.00070 0.00490.000701,2-Dichlorobenzene
<0.00081 0.00490.000811,2-Dichloroethane
<0.0025 0.00490.00251,2-Dichloropropane
<0.00082 0.00490.000821,3,5-Trimethylbenzene
<0.00094 0.00490.000941,3-Dichlorobenzene
<0.00099 0.00490.000991,3-Dichloropropane
<0.0025 0.00490.00251,4-Dichlorobenzene
<0.0025 0.00490.00252,2-Dichloropropane
<0.0025 0.00490.00252-Chlorotoluene
<0.0049 0.0250.00492-Hexanone
<0.00097 0.00490.000974-Chlorotoluene
0.014 J 0.0250.0072Acetone
<0.0011 0.00490.0011Benzene
<0.0013 0.00490.0013Bromobenzene
<0.0025 0.00490.0025Bromochloromethane
<0.0025 0.00490.0025Bromodichloromethane
<0.0025 0.00490.0025Bromoform
<0.0025 0.00490.0025Bromomethane
<0.0025 0.00490.0025Carbon disulfide
<0.0017 0.00490.0017Carbon tetrachloride
<0.00051 0.00490.00051Chlorobenzene
<0.0025 0.00490.0025Chloroethane
<0.0025 0.00490.0025Chloroform
<0.00099 0.00490.00099Chloromethane
<0.00075 0.00490.00075cis-1,2-Dichloroethene
<0.0012 0.00490.0012cis-1,3-Dichloropropene
<0.0025 0.00490.0025Dibromochloromethane
<0.0025 0.00490.0025Dibromomethane
<0.0013 0.00490.0013Dichlorodifluoromethane
<0.00060 0.00490.00060Ethylbenzene
<0.00099 0.00490.00099Ethylene Dibromide
<0.0025 0.00490.0025Hexachlorobutadiene
<0.0034 0.00490.0034Iodomethane
<0.00054 0.00490.00054Isopropyl ether
TestAmerica Pensacola Page 16 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-8-5
Client Matrix:% Moisture:19.9
400-92351-15
Solid
Date Sampled: 06/19/2014 1340
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/23/2014 1224
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06231406.D
6.326 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221091
400-221146
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.00067 0.00490.00067Isopropylbenzene
<0.0059 0.0250.0059Methyl Ethyl Ketone
<0.0049 0.0250.0049methyl isobutyl ketone
<0.00099 0.00490.00099Methyl tert-butyl ether
<0.0099 0.0150.0099Methylene Chloride
<0.0013 0.00990.0013m-Xylene & p-Xylene
<0.0020 0.00490.0020Naphthalene
<0.00095 0.00490.00095n-Butylbenzene
<0.00089 0.00490.00089N-Propylbenzene
<0.00099 0.00490.00099o-Xylene
<0.00099 0.00490.00099p-Cymene
<0.00094 0.00490.00094sec-Butylbenzene
<0.00099 0.00490.00099Styrene
<0.0025 0.00490.0025tert-Butylbenzene
<0.0025 0.00490.0025Tetrachloroethene
<0.00099 0.00490.00099Toluene
<0.0025 0.00490.0025trans-1,2-Dichloroethene
<0.0025 0.00490.0025trans-1,3-Dichloropropene
<0.00099 0.00490.00099Trichloroethene
<0.0025 0.00490.0025Trichlorofluoromethane
<0.0090 0.0250.0090Vinyl acetate
<0.0025 0.00490.0025Vinyl chloride
<0.0019 0.00990.0019Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
104 72 - 1224-Bromofluorobenzene
99 79 - 123Dibromofluoromethane
92 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 17 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-9-5
Client Matrix:% Moisture:22.0
400-92351-16
Solid
Date Sampled: 06/19/2014 1610
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/23/2014 1250
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06231407.D
4.247 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221091
400-221146
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.0038 0.00750.00381,1,1,2-Tetrachloroethane
<0.0017 0.00750.00171,1,1-Trichloroethane
<0.0038 0.00750.00381,1,2,2-Tetrachloroethane
<0.0038 0.00750.00381,1,2-Trichloroethane
<0.0013 0.00750.00131,1-Dichloroethane
<0.0038 0.00750.00381,1-Dichloroethene
<0.0038 0.00750.00381,1-Dichloropropene
<0.0038 0.00750.00381,2,3-Trichlorobenzene
<0.0045 0.00750.00451,2,3-Trichloropropane
<0.0030 0.00750.00301,2,4-Trichlorobenzene
<0.0015 0.00750.00151,2,4-Trimethylbenzene
<0.0050 0.00750.00501,2-Dibromo-3-Chloropropane
<0.0011 0.00750.00111,2-Dichlorobenzene
<0.0012 0.00750.00121,2-Dichloroethane
<0.0038 0.00750.00381,2-Dichloropropane
<0.0013 0.00750.00131,3,5-Trimethylbenzene
<0.0014 0.00750.00141,3-Dichlorobenzene
<0.0015 0.00750.00151,3-Dichloropropane
<0.0038 0.00750.00381,4-Dichlorobenzene
<0.0038 0.00750.00382,2-Dichloropropane
<0.0038 0.00750.00382-Chlorotoluene
<0.0075 0.0380.00752-Hexanone
<0.0015 0.00750.00154-Chlorotoluene
0.024 J 0.0380.011Acetone
<0.0017 0.00750.0017Benzene
<0.0020 0.00750.0020Bromobenzene
<0.0038 0.00750.0038Bromochloromethane
<0.0038 0.00750.0038Bromodichloromethane
<0.0038 0.00750.0038Bromoform
<0.0038 0.00750.0038Bromomethane
<0.0038 0.00750.0038Carbon disulfide
<0.0026 0.00750.0026Carbon tetrachloride
<0.00078 0.00750.00078Chlorobenzene
<0.0038 0.00750.0038Chloroethane
<0.0038 0.00750.0038Chloroform
<0.0015 0.00750.0015Chloromethane
<0.0011 0.00750.0011cis-1,2-Dichloroethene
<0.0018 0.00750.0018cis-1,3-Dichloropropene
<0.0038 0.00750.0038Dibromochloromethane
<0.0038 0.00750.0038Dibromomethane
<0.0020 0.00750.0020Dichlorodifluoromethane
<0.00092 0.00750.00092Ethylbenzene
<0.0015 0.00750.0015Ethylene Dibromide
<0.0038 0.00750.0038Hexachlorobutadiene
<0.0051 0.00750.0051Iodomethane
<0.00083 0.00750.00083Isopropyl ether
TestAmerica Pensacola Page 18 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-9-5
Client Matrix:% Moisture:22.0
400-92351-16
Solid
Date Sampled: 06/19/2014 1610
Date Received: 06/20/2014 0821
8260B Volatile Organic Compounds (GC/MS)
Dilution:
06/21/2014 1815
06/23/2014 1250
1.0
8260B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06231407.D
4.247 g
5.00 g
5035
CH_WASP
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221091
400-221146
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.0010 0.00750.0010Isopropylbenzene
<0.0091 0.0380.0091Methyl Ethyl Ketone
<0.0075 0.0380.0075methyl isobutyl ketone
<0.0015 0.00750.0015Methyl tert-butyl ether
<0.015 0.0230.015Methylene Chloride
<0.0020 0.0150.0020m-Xylene & p-Xylene
<0.0030 0.00750.0030Naphthalene
<0.0014 0.00750.0014n-Butylbenzene
<0.0014 0.00750.0014N-Propylbenzene
<0.0015 0.00750.0015o-Xylene
<0.0015 0.00750.0015p-Cymene
<0.0014 0.00750.0014sec-Butylbenzene
<0.0015 0.00750.0015Styrene
<0.0038 0.00750.0038tert-Butylbenzene
0.0079 0.00750.0038Tetrachloroethene
<0.0015 0.00750.0015Toluene
<0.0038 0.00750.0038trans-1,2-Dichloroethene
<0.0038 0.00750.0038trans-1,3-Dichloropropene
<0.0015 0.00750.0015Trichloroethene
<0.0038 0.00750.0038Trichlorofluoromethane
<0.014 0.0380.014Vinyl acetate
<0.0038 0.00750.0038Vinyl chloride
<0.0029 0.0150.0029Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
102 72 - 1224-Bromofluorobenzene
100 79 - 123Dibromofluoromethane
94 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 19 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-4-9-10
Client Matrix:% Moisture:36.1
400-92351-11
Solid
Date Sampled: 06/19/2014 1130
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/23/2014 1726
06/24/2014 1140
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-11.D
30.07 g
1 mL
1 uL
3550C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-221232
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.052 0.520.0521,1'-Biphenyl
<0.052 0.520.0521,2,4,5-Tetrachlorobenzene
<0.052 0.520.0521,2,4-Trichlorobenzene
<0.052 0.520.0521,2-Dichlorobenzene
<0.052 0.520.0521,3-Dichlorobenzene
<0.052 0.520.0521,3-Dinitrobenzene
<0.052 0.520.0521,4-Dichlorobenzene
<0.052 0.520.0521,4-Dioxane
<0.031 0.520.0311-Methylnaphthalene
<0.052 0.520.0522,3,4,6-Tetrachlorophenol
<0.052 0.520.0522,4,5-Trichlorophenol
<0.052 0.520.0522,4,6-Trichlorophenol
<0.052 0.520.0522,4-Dichlorophenol
<0.052 0.520.0522,4-Dimethylphenol
<0.45 1.50.452,4-Dinitrophenol
<0.052 0.520.0522,4-Dinitrotoluene
<0.052 0.520.0522,6-Dinitrotoluene
<0.052 0.520.0522-Chloronaphthalene
<0.052 0.520.0522-Chlorophenol
<0.028 0.520.0282-Methylnaphthalene
<0.052 0.520.0522-Methylphenol
<0.052 0.520.0522-Nitroaniline
<0.052 0.520.0522-Nitrophenol
<0.052 1.00.0523 & 4 Methylphenol
<0.094 0.520.0944,6-Dinitro-2-methylphenol
<0.052 0.520.0524-Bromophenyl phenyl ether
<0.052 0.520.0524-Chloro-3-methylphenol
<0.052 0.520.0524-Chlorophenyl phenyl ether
<0.23 0.520.234-Nitrophenol
<0.031 0.520.031Acenaphthene
<0.031 0.520.031Acenaphthylene
<0.052 0.520.052Acetophenone
<0.031 0.520.031Anthracene
<0.052 0.520.052Azobenzene
<0.052 0.520.052Benzaldehyde
<0.031 0.520.031Benzo[a]anthracene
<0.031 0.520.031Benzo[a]pyrene
<0.039 0.520.039Benzo[b]fluoranthene
<0.047 0.520.047Benzo[g,h,i]perylene
<0.034 0.520.034Benzo[k]fluoranthene
<0.55 1.50.55Benzoic acid
<0.078 0.520.078Benzyl alcohol
<0.052 0.520.052bis (2-chloroisopropyl) ether
<0.052 0.520.052Bis(2-chloroethoxy)methane
<0.052 0.520.052Bis(2-chloroethyl)ether
0.33 J B 0.520.052Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 20 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-4-9-10
Client Matrix:% Moisture:36.1
400-92351-11
Solid
Date Sampled: 06/19/2014 1130
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/23/2014 1726
06/24/2014 1140
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-11.D
30.07 g
1 mL
1 uL
3550C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-221232
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.052 0.520.052Butyl benzyl phthalate
<0.078 0.520.078Carbazole
<0.034 0.520.034Chrysene
<0.039 0.520.039Dibenz(a,h)anthracene
<0.052 0.520.052Dibenzofuran
<0.052 0.520.052Diethyl phthalate
<0.052 0.520.052Dimethyl phthalate
<0.052 0.520.052Di-n-butyl phthalate
<0.052 0.520.052Di-n-octyl phthalate
<0.039 0.520.039Fluoranthene
<0.031 0.520.031Fluorene
<0.16 0.520.16Hexachlorobenzene
<0.052 0.520.052Hexachlorobutadiene
<0.10 0.520.10Hexachlorocyclopentadiene
<0.16 0.520.16Hexachloroethane
<0.052 0.520.052Hexadecane
<0.52 0.520.52Indene
<0.039 0.520.039Indeno[1,2,3-cd]pyrene
<0.052 0.520.052Isophorone
<0.034 0.520.034Naphthalene
<0.052 0.520.052n-Decane
<0.052 0.520.052Nitrobenzene
<0.10 0.520.10N-Nitrosodimethylamine
<0.17 0.520.17N-Nitrosodi-n-propylamine
<0.052 0.520.052N-Nitrosodiphenylamine
<0.052 0.520.052n-Octadecane
<0.10 1.00.10Pentachlorophenol
<0.031 0.520.031Phenanthrene
<0.052 0.520.052Phenol
<0.039 0.520.039Pyrene
<0.23 0.520.23Pyridine
<0.052 0.520.052Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
76 32 - 1332,4,6-Tribromophenol (Surr)
79 44 - 1202-Fluorobiphenyl
72 25 - 1202-Fluorophenol (Surr)
76 27 - 120Nitrobenzene-d5 (Surr)
78 37 - 120Phenol-d5 (Surr)
71 36 - 134Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 21 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-5-10-11
Client Matrix:% Moisture:28.6
400-92351-12
Solid
Date Sampled: 06/19/2014 1228
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/23/2014 1726
06/24/2014 1219
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-12.D
30.18 g
1 mL
1 uL
3550C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-221232
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.046 0.460.0461,1'-Biphenyl
<0.046 0.460.0461,2,4,5-Tetrachlorobenzene
<0.046 0.460.0461,2,4-Trichlorobenzene
<0.046 0.460.0461,2-Dichlorobenzene
<0.046 0.460.0461,3-Dichlorobenzene
<0.046 0.460.0461,3-Dinitrobenzene
<0.046 0.460.0461,4-Dichlorobenzene
<0.046 0.460.0461,4-Dioxane
<0.028 0.460.0281-Methylnaphthalene
<0.046 0.460.0462,3,4,6-Tetrachlorophenol
<0.046 0.460.0462,4,5-Trichlorophenol
<0.046 0.460.0462,4,6-Trichlorophenol
<0.046 0.460.0462,4-Dichlorophenol
<0.046 0.460.0462,4-Dimethylphenol
<0.40 1.40.402,4-Dinitrophenol
<0.046 0.460.0462,4-Dinitrotoluene
<0.046 0.460.0462,6-Dinitrotoluene
<0.046 0.460.0462-Chloronaphthalene
<0.046 0.460.0462-Chlorophenol
<0.025 0.460.0252-Methylnaphthalene
<0.046 0.460.0462-Methylphenol
<0.046 0.460.0462-Nitroaniline
<0.046 0.460.0462-Nitrophenol
<0.046 0.920.0463 & 4 Methylphenol
<0.083 0.460.0834,6-Dinitro-2-methylphenol
<0.046 0.460.0464-Bromophenyl phenyl ether
<0.046 0.460.0464-Chloro-3-methylphenol
<0.046 0.460.0464-Chlorophenyl phenyl ether
<0.21 0.460.214-Nitrophenol
<0.028 0.460.028Acenaphthene
<0.028 0.460.028Acenaphthylene
<0.046 0.460.046Acetophenone
<0.028 0.460.028Anthracene
<0.046 0.460.046Azobenzene
<0.046 0.460.046Benzaldehyde
<0.028 0.460.028Benzo[a]anthracene
<0.028 0.460.028Benzo[a]pyrene
<0.035 0.460.035Benzo[b]fluoranthene
<0.042 0.460.042Benzo[g,h,i]perylene
<0.031 0.460.031Benzo[k]fluoranthene
<0.49 1.40.49Benzoic acid
<0.070 0.460.070Benzyl alcohol
<0.046 0.460.046bis (2-chloroisopropyl) ether
<0.046 0.460.046Bis(2-chloroethoxy)methane
<0.046 0.460.046Bis(2-chloroethyl)ether
0.33 J B 0.460.046Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 22 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-5-10-11
Client Matrix:% Moisture:28.6
400-92351-12
Solid
Date Sampled: 06/19/2014 1228
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/23/2014 1726
06/24/2014 1219
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-12.D
30.18 g
1 mL
1 uL
3550C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-221232
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.046 0.460.046Butyl benzyl phthalate
<0.070 0.460.070Carbazole
<0.031 0.460.031Chrysene
<0.035 0.460.035Dibenz(a,h)anthracene
<0.046 0.460.046Dibenzofuran
<0.046 0.460.046Diethyl phthalate
<0.046 0.460.046Dimethyl phthalate
<0.046 0.460.046Di-n-butyl phthalate
<0.046 0.460.046Di-n-octyl phthalate
<0.035 0.460.035Fluoranthene
<0.028 0.460.028Fluorene
<0.14 0.460.14Hexachlorobenzene
<0.046 0.460.046Hexachlorobutadiene
<0.092 0.460.092Hexachlorocyclopentadiene
<0.14 0.460.14Hexachloroethane
<0.046 0.460.046Hexadecane
<0.46 0.460.46Indene
<0.035 0.460.035Indeno[1,2,3-cd]pyrene
<0.046 0.460.046Isophorone
<0.031 0.460.031Naphthalene
<0.046 0.460.046n-Decane
<0.046 0.460.046Nitrobenzene
<0.092 0.460.092N-Nitrosodimethylamine
<0.15 0.460.15N-Nitrosodi-n-propylamine
<0.046 0.460.046N-Nitrosodiphenylamine
<0.046 0.460.046n-Octadecane
<0.092 0.920.092Pentachlorophenol
<0.028 0.460.028Phenanthrene
<0.046 0.460.046Phenol
<0.035 0.460.035Pyrene
<0.21 0.460.21Pyridine
<0.046 0.460.046Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
89 32 - 1332,4,6-Tribromophenol (Surr)
94 44 - 1202-Fluorobiphenyl
88 25 - 1202-Fluorophenol (Surr)
94 27 - 120Nitrobenzene-d5 (Surr)
100 37 - 120Phenol-d5 (Surr)
84 36 - 134Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 23 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-6-9-10
Client Matrix:% Moisture:27.0
400-92351-13
Solid
Date Sampled: 06/19/2014 1350
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/23/2014 1726
06/24/2014 1258
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-13.D
30.29 g
1 mL
1 uL
3550C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-221232
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.045 0.450.0451,1'-Biphenyl
<0.045 0.450.0451,2,4,5-Tetrachlorobenzene
<0.045 0.450.0451,2,4-Trichlorobenzene
<0.045 0.450.0451,2-Dichlorobenzene
<0.045 0.450.0451,3-Dichlorobenzene
<0.045 0.450.0451,3-Dinitrobenzene
<0.045 0.450.0451,4-Dichlorobenzene
<0.045 0.450.0451,4-Dioxane
<0.027 0.450.0271-Methylnaphthalene
<0.045 0.450.0452,3,4,6-Tetrachlorophenol
<0.045 0.450.0452,4,5-Trichlorophenol
<0.045 0.450.0452,4,6-Trichlorophenol
<0.045 0.450.0452,4-Dichlorophenol
<0.045 0.450.0452,4-Dimethylphenol
<0.39 1.30.392,4-Dinitrophenol
<0.045 0.450.0452,4-Dinitrotoluene
<0.045 0.450.0452,6-Dinitrotoluene
<0.045 0.450.0452-Chloronaphthalene
<0.045 0.450.0452-Chlorophenol
<0.024 0.450.0242-Methylnaphthalene
<0.045 0.450.0452-Methylphenol
<0.045 0.450.0452-Nitroaniline
<0.045 0.450.0452-Nitrophenol
<0.045 0.900.0453 & 4 Methylphenol
<0.081 0.450.0814,6-Dinitro-2-methylphenol
<0.045 0.450.0454-Bromophenyl phenyl ether
<0.045 0.450.0454-Chloro-3-methylphenol
<0.045 0.450.0454-Chlorophenyl phenyl ether
<0.20 0.450.204-Nitrophenol
<0.027 0.450.027Acenaphthene
<0.027 0.450.027Acenaphthylene
<0.045 0.450.045Acetophenone
<0.027 0.450.027Anthracene
<0.045 0.450.045Azobenzene
<0.045 0.450.045Benzaldehyde
<0.027 0.450.027Benzo[a]anthracene
<0.027 0.450.027Benzo[a]pyrene
<0.034 0.450.034Benzo[b]fluoranthene
<0.041 0.450.041Benzo[g,h,i]perylene
<0.030 0.450.030Benzo[k]fluoranthene
<0.47 1.30.47Benzoic acid
<0.068 0.450.068Benzyl alcohol
<0.045 0.450.045bis (2-chloroisopropyl) ether
<0.045 0.450.045Bis(2-chloroethoxy)methane
<0.045 0.450.045Bis(2-chloroethyl)ether
0.21 J B 0.450.045Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 24 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-6-9-10
Client Matrix:% Moisture:27.0
400-92351-13
Solid
Date Sampled: 06/19/2014 1350
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/23/2014 1726
06/24/2014 1258
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-13.D
30.29 g
1 mL
1 uL
3550C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-221232
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.045 0.450.045Butyl benzyl phthalate
<0.068 0.450.068Carbazole
<0.030 0.450.030Chrysene
<0.034 0.450.034Dibenz(a,h)anthracene
<0.045 0.450.045Dibenzofuran
<0.045 0.450.045Diethyl phthalate
<0.045 0.450.045Dimethyl phthalate
<0.045 0.450.045Di-n-butyl phthalate
<0.045 0.450.045Di-n-octyl phthalate
<0.034 0.450.034Fluoranthene
<0.027 0.450.027Fluorene
<0.14 0.450.14Hexachlorobenzene
<0.045 0.450.045Hexachlorobutadiene
<0.090 0.450.090Hexachlorocyclopentadiene
<0.14 0.450.14Hexachloroethane
<0.045 0.450.045Hexadecane
<0.45 0.450.45Indene
<0.034 0.450.034Indeno[1,2,3-cd]pyrene
<0.045 0.450.045Isophorone
<0.030 0.450.030Naphthalene
<0.045 0.450.045n-Decane
<0.045 0.450.045Nitrobenzene
<0.090 0.450.090N-Nitrosodimethylamine
<0.15 0.450.15N-Nitrosodi-n-propylamine
<0.045 0.450.045N-Nitrosodiphenylamine
0.087 J 0.450.045n-Octadecane
<0.090 0.900.090Pentachlorophenol
<0.027 0.450.027Phenanthrene
<0.045 0.450.045Phenol
<0.034 0.450.034Pyrene
<0.20 0.450.20Pyridine
<0.045 0.450.045Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
75 32 - 1332,4,6-Tribromophenol (Surr)
71 44 - 1202-Fluorobiphenyl
70 25 - 1202-Fluorophenol (Surr)
76 27 - 120Nitrobenzene-d5 (Surr)
77 37 - 120Phenol-d5 (Surr)
71 36 - 134Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 25 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-4-9-10
Client Matrix:% Moisture:36.1
400-92351-11
Solid
Date Sampled: 06/19/2014 1130
Date Received: 06/20/2014 0821
8015C GRO by 8015C
Dilution:
8015C
5035
1.0
06/21/2014 0046
06/20/2014 1500
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
5.08 g
5.0 g
5 mL
CH_RITA
Analysis Date:
Prep Date:
Analysis Batch: 400-220959
400-220960Prep Batch:
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.077 0.150.077Gasoline Range Organics (GRO)-C6-C10
Surrogate %Rec Acceptance LimitsQualifier
94 65 - 125a,a,a-Trifluorotoluene (fid)
TestAmerica Pensacola Page 26 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-5-10-11
Client Matrix:% Moisture:28.6
400-92351-12
Solid
Date Sampled: 06/19/2014 1228
Date Received: 06/20/2014 0821
8015C GRO by 8015C
Dilution:
8015C
5035
1.0
06/21/2014 0113
06/20/2014 1500
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
5.84 g
5.0 g
5 mL
CH_RITA
Analysis Date:
Prep Date:
Analysis Batch: 400-220959
400-220960Prep Batch:
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.060 0.120.060Gasoline Range Organics (GRO)-C6-C10
Surrogate %Rec Acceptance LimitsQualifier
90 65 - 125a,a,a-Trifluorotoluene (fid)
TestAmerica Pensacola Page 27 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-6-9-10
Client Matrix:% Moisture:27.0
400-92351-13
Solid
Date Sampled: 06/19/2014 1350
Date Received: 06/20/2014 0821
8015C GRO by 8015C
Dilution:
8015C
5035
1.0
06/21/2014 0140
06/20/2014 1500
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
5.64 g
5.0 g
5 mL
CH_RITA
Analysis Date:
Prep Date:
Analysis Batch: 400-220959
400-220960Prep Batch:
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<0.061 0.120.061Gasoline Range Organics (GRO)-C6-C10
Surrogate %Rec Acceptance LimitsQualifier
82 65 - 125a,a,a-Trifluorotoluene (fid)
TestAmerica Pensacola Page 28 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-4-9-10
Client Matrix:% Moisture:36.1
400-92351-11
Solid
Date Sampled: 06/19/2014 1130
Date Received: 06/20/2014 0821
8015C Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Dilution:
8015C
3546
1.0
06/23/2014 2150
06/22/2014 1407
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
14.91 g
2 mL
1 uL
WALLE
Analysis Date:
Prep Date:
Analysis Batch: 400-221123
400-221077Prep Batch:
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
120 165.4Diesel Range Organics [C10-C28]
Surrogate %Rec Acceptance LimitsQualifier
114 27 - 151o-Terphenyl (Surr)
TestAmerica Pensacola Page 29 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-5-10-11
Client Matrix:% Moisture:28.6
400-92351-12
Solid
Date Sampled: 06/19/2014 1228
Date Received: 06/20/2014 0821
8015C Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Dilution:
8015C
3546
1.0
06/23/2014 2200
06/22/2014 1407
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
15.12 g
2 mL
1 uL
WALLE
Analysis Date:
Prep Date:
Analysis Batch: 400-221123
400-221077Prep Batch:
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
<4.7 144.7Diesel Range Organics [C10-C28]
Surrogate %Rec Acceptance LimitsQualifier
112 27 - 151o-Terphenyl (Surr)
TestAmerica Pensacola Page 30 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
Client Sample ID:
Lab Sample ID:
SP-6-9-10
Client Matrix:% Moisture:27.0
400-92351-13
Solid
Date Sampled: 06/19/2014 1350
Date Received: 06/20/2014 0821
8015C Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Dilution:
8015C
3546
1.0
06/23/2014 2210
06/22/2014 1407
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
15.16 g
2 mL
1 uL
WALLE
Analysis Date:
Prep Date:
Analysis Batch: 400-221123
400-221077Prep Batch:
Analysis Method:
Prep Method:
Analyte DryWt Corrected: Y Result (mg/Kg)Qualifier MDL RL
59 144.6Diesel Range Organics [C10-C28]
Surrogate %Rec Acceptance LimitsQualifier
118 27 - 151o-Terphenyl (Surr)
TestAmerica Pensacola Page 31 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
General Chemistry
Client Sample ID:
Lab Sample ID:
SP-4-9-10
Client Matrix:
400-92351-11
Solid
Date Sampled: 06/19/2014 1130
Date Received: 06/20/2014 0821
Analyte Result Qual Units MDL RL Dil Method
Percent Moisture 36 %0.10 0.10 1.0 Moisture
DryWt Corrected: NAnalysis Date: 06/20/2014 1647Analysis Batch: 400-220944
TestAmerica Pensacola Page 32 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
General Chemistry
Client Sample ID:
Lab Sample ID:
SP-5-10-11
Client Matrix:
400-92351-12
Solid
Date Sampled: 06/19/2014 1228
Date Received: 06/20/2014 0821
Analyte Result Qual Units MDL RL Dil Method
Percent Moisture 29 %0.10 0.10 1.0 Moisture
DryWt Corrected: NAnalysis Date: 06/20/2014 1647Analysis Batch: 400-220944
TestAmerica Pensacola Page 33 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
General Chemistry
Client Sample ID:
Lab Sample ID:
SP-6-9-10
Client Matrix:
400-92351-13
Solid
Date Sampled: 06/19/2014 1350
Date Received: 06/20/2014 0821
Analyte Result Qual Units MDL RL Dil Method
Percent Moisture 27 %0.10 0.10 1.0 Moisture
DryWt Corrected: NAnalysis Date: 06/20/2014 1647Analysis Batch: 400-220944
TestAmerica Pensacola Page 34 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
General Chemistry
Client Sample ID:
Lab Sample ID:
SP-7-10
Client Matrix:
400-92351-14
Solid
Date Sampled: 06/19/2014 1500
Date Received: 06/20/2014 0821
Analyte Result Qual Units MDL RL Dil Method
Percent Moisture 31 %0.10 0.10 1.0 Moisture
DryWt Corrected: NAnalysis Date: 06/20/2014 1647Analysis Batch: 400-220944
TestAmerica Pensacola Page 35 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
General Chemistry
Client Sample ID:
Lab Sample ID:
SP-8-5
Client Matrix:
400-92351-15
Solid
Date Sampled: 06/19/2014 1340
Date Received: 06/20/2014 0821
Analyte Result Qual Units MDL RL Dil Method
Percent Moisture 20 %0.10 0.10 1.0 Moisture
DryWt Corrected: NAnalysis Date: 06/20/2014 1647Analysis Batch: 400-220944
TestAmerica Pensacola Page 36 of 70
Analytical Data
Client: AEI Consultants Job Number: 400-92351-1
General Chemistry
Client Sample ID:
Lab Sample ID:
SP-9-5
Client Matrix:
400-92351-16
Solid
Date Sampled: 06/19/2014 1610
Date Received: 06/20/2014 0821
Analyte Result Qual Units MDL RL Dil Method
Percent Moisture 22 %0.10 0.10 1.0 Moisture
DryWt Corrected: NAnalysis Date: 06/20/2014 1647Analysis Batch: 400-220944
TestAmerica Pensacola Page 37 of 70
QUALITY CONTROL RESULTS
TestAmerica Pensacola
Page 38 of 70
Quality Control Results
Client: AEI Consultants Job Number: 400-92351-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Analysis Batch:400-221047
Lab Control Sample Solid 400-2210588260BLCS 400-221058/18-A T
Lab Control Sample Duplicate Solid 400-2210588260BLCSD 400-221058/19-A T
Method Blank Solid 400-2210588260BMB 400-221058/17-A T
Solid 400-221058SP-4-9-10 8260B400-92351-11 T
Solid 400-221058SP-5-10-11 8260B400-92351-12 T
Solid 400-221058SP-6-9-10 8260B400-92351-13 T
Solid 400-221058SP-7-10 8260B400-92351-14 T
Prep Batch: 400-221058
Lab Control Sample Solid 5035LCS 400-221058/18-A T
Lab Control Sample Duplicate Solid 5035LCSD 400-221058/19-A T
Method Blank Solid 5035MB 400-221058/17-A T
SolidSP-4-9-10 5035400-92351-11 T
SolidSP-5-10-11 5035400-92351-12 T
SolidSP-6-9-10 5035400-92351-13 T
SolidSP-7-10 5035400-92351-14 T
Analysis Batch:400-221091
Lab Control Sample Solid 400-2211468260BLCS 400-221146/24-A T
Method Blank Solid 400-2211468260BMB 400-221146/23-A T
Matrix Spike Solid 400-2211468260B400-92338-B-1-C MS T
Matrix Spike Duplicate Solid 400-2211468260B400-92338-B-1-D MSD T
Solid 400-221146SP-8-5 8260B400-92351-15 T
Solid 400-221146SP-9-5 8260B400-92351-16 T
Prep Batch: 400-221146
Lab Control Sample Solid 5035LCS 400-221146/24-A T
Method Blank Solid 5035MB 400-221146/23-A T
Matrix Spike Solid 5035400-92338-B-1-C MS T
Matrix Spike Duplicate Solid 5035400-92338-B-1-D MSD T
SolidSP-8-5 5035400-92351-15 T
SolidSP-9-5 5035400-92351-16 T
Report Basis
T = Total
TestAmerica Pensacola
Page 39 of 70
Quality Control Results
Client: AEI Consultants Job Number: 400-92351-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS Semi VOA
Analysis Batch:400-221174
Lab Control Sample Solid 400-2212328270DLCS 400-221232/2-A T
Method Blank Solid 400-2212328270DMB 400-221232/1-A T
Solid 400-221232SP-4-9-10 8270D400-92351-11 T
Solid 400-221232SP-5-10-11 8270D400-92351-12 T
Solid 400-221232SP-6-9-10 8270D400-92351-13 T
Prep Batch: 400-221232
Lab Control Sample Solid 3550CLCS 400-221232/2-A T
Method Blank Solid 3550CMB 400-221232/1-A T
SolidSP-4-9-10 3550C400-92351-11 T
SolidSP-5-10-11 3550C400-92351-12 T
SolidSP-6-9-10 3550C400-92351-13 T
Report Basis
T = Total
GC VOA
Analysis Batch:400-220959
Lab Control Sample Solid 400-2209608015CLCS 400-220960/2-A T
Method Blank Solid 400-2209608015CMB 400-220960/1-A T
Matrix Spike Solid 400-2209608015C400-92344-A-2-B MS T
Matrix Spike Duplicate Solid 400-2209608015C400-92344-A-2-C MSD T
Solid 400-220960SP-4-9-10 8015C400-92351-11 T
Solid 400-220960SP-5-10-11 8015C400-92351-12 T
Solid 400-220960SP-6-9-10 8015C400-92351-13 T
Prep Batch: 400-220960
Lab Control Sample Solid 5035LCS 400-220960/2-A T
Method Blank Solid 5035MB 400-220960/1-A T
Matrix Spike Solid 5035400-92344-A-2-B MS T
Matrix Spike Duplicate Solid 5035400-92344-A-2-C MSD T
SolidSP-4-9-10 5035400-92351-11 T
SolidSP-5-10-11 5035400-92351-12 T
SolidSP-6-9-10 5035400-92351-13 T
Report Basis
T = Total
TestAmerica Pensacola
Page 40 of 70
Quality Control Results
Client: AEI Consultants Job Number: 400-92351-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC Semi VOA
Prep Batch: 400-221077
Lab Control Sample Solid 3546LCS 400-221077/2-A T
Method Blank Solid 3546MB 400-221077/1-A T
Matrix Spike Solid 3546400-92269-A-1-A MS T
Matrix Spike Duplicate Solid 3546400-92269-A-1-B MSD T
SolidSP-4-9-10 3546400-92351-11 T
SolidSP-5-10-11 3546400-92351-12 T
SolidSP-6-9-10 3546400-92351-13 T
Analysis Batch:400-221123
Lab Control Sample Solid 400-2210778015CLCS 400-221077/2-A T
Method Blank Solid 400-2210778015CMB 400-221077/1-A T
Matrix Spike Solid 400-2210778015C400-92269-A-1-A MS T
Matrix Spike Duplicate Solid 400-2210778015C400-92269-A-1-B MSD T
Solid 400-221077SP-4-9-10 8015C400-92351-11 T
Solid 400-221077SP-5-10-11 8015C400-92351-12 T
Solid 400-221077SP-6-9-10 8015C400-92351-13 T
Report Basis
T = Total
General Chemistry
Analysis Batch:400-220944
SolidSP-4-9-10 Moisture400-92351-11 T
SolidSP-5-10-11 Moisture400-92351-12 T
SolidSP-6-9-10 Moisture400-92351-13 T
SolidSP-7-10 Moisture400-92351-14 T
SolidSP-8-5 Moisture400-92351-15 T
SolidSP-9-5 Moisture400-92351-16 T
Report Basis
T = Total
TestAmerica Pensacola
Page 41 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221058
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06221409.D
5.00 g
5.00 gUnits:mg/Kg
Method: 8260B
Preparation: 5035
CH_WASPMB 400-221058/17-A
Analysis Date: 06/22/2014 1411
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221047
400-221058
Prep Date:
Leach Date:
06/21/2014 1815
N/A
Analyte RLMDLQualResult
<0.0025 0.00500.00251,1,1,2-Tetrachloroethane
<0.0011 0.00500.00111,1,1-Trichloroethane
<0.0025 0.00500.00251,1,2,2-Tetrachloroethane
<0.0025 0.00500.00251,1,2-Trichloroethane
<0.00083 0.00500.000831,1-Dichloroethane
<0.0025 0.00500.00251,1-Dichloroethene
<0.0025 0.00500.00251,1-Dichloropropene
<0.0025 0.00500.00251,2,3-Trichlorobenzene
<0.0030 0.00500.00301,2,3-Trichloropropane
<0.0020 0.00500.00201,2,4-Trichlorobenzene
<0.0010 0.00500.00101,2,4-Trimethylbenzene
<0.0033 0.00500.00331,2-Dibromo-3-Chloropropane
<0.00071 0.00500.000711,2-Dichlorobenzene
<0.00082 0.00500.000821,2-Dichloroethane
<0.0025 0.00500.00251,2-Dichloropropane
<0.00083 0.00500.000831,3,5-Trimethylbenzene
<0.00095 0.00500.000951,3-Dichlorobenzene
<0.0010 0.00500.00101,3-Dichloropropane
<0.0025 0.00500.00251,4-Dichlorobenzene
<0.0025 0.00500.00252,2-Dichloropropane
<0.0025 0.00500.00252-Chlorotoluene
<0.0050 0.0250.00502-Hexanone
<0.00098 0.00500.000984-Chlorotoluene
<0.0073 0.0250.0073Acetone
<0.0011 0.00500.0011Benzene
<0.0013 0.00500.0013Bromobenzene
<0.0025 0.00500.0025Bromochloromethane
<0.0025 0.00500.0025Bromodichloromethane
<0.0025 0.00500.0025Bromoform
<0.0025 0.00500.0025Bromomethane
<0.0025 0.00500.0025Carbon disulfide
<0.0017 0.00500.0017Carbon tetrachloride
<0.00052 0.00500.00052Chlorobenzene
<0.0025 0.00500.0025Chloroethane
<0.0025 0.00500.0025Chloroform
<0.0010 0.00500.0010Chloromethane
<0.00076 0.00500.00076cis-1,2-Dichloroethene
<0.0012 0.00500.0012cis-1,3-Dichloropropene
<0.0025 0.00500.0025Dibromochloromethane
<0.0025 0.00500.0025Dibromomethane
<0.0013 0.00500.0013Dichlorodifluoromethane
<0.00061 0.00500.00061Ethylbenzene
<0.0010 0.00500.0010Ethylene Dibromide
<0.0025 0.00500.0025Hexachlorobutadiene
<0.0034 0.00500.0034Iodomethane
TestAmerica Pensacola Page 42 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221058
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06221409.D
5.00 g
5.00 gUnits:mg/Kg
Method: 8260B
Preparation: 5035
CH_WASPMB 400-221058/17-A
Analysis Date: 06/22/2014 1411
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221047
400-221058
Prep Date:
Leach Date:
06/21/2014 1815
N/A
Analyte RLMDLQualResult
<0.00055 0.00500.00055Isopropyl ether
<0.00068 0.00500.00068Isopropylbenzene
<0.0060 0.0250.0060Methyl Ethyl Ketone
<0.0050 0.0250.0050methyl isobutyl ketone
<0.0010 0.00500.0010Methyl tert-butyl ether
<0.010 0.0150.010Methylene Chloride
<0.0013 0.0100.0013m-Xylene & p-Xylene
<0.0020 0.00500.0020Naphthalene
<0.00096 0.00500.00096n-Butylbenzene
<0.00090 0.00500.00090N-Propylbenzene
<0.0010 0.00500.0010o-Xylene
<0.0010 0.00500.0010p-Cymene
<0.00095 0.00500.00095sec-Butylbenzene
<0.0010 0.00500.0010Styrene
<0.0025 0.00500.0025tert-Butylbenzene
<0.0025 0.00500.0025Tetrachloroethene
<0.0010 0.00500.0010Toluene
<0.0025 0.00500.0025trans-1,2-Dichloroethene
<0.0025 0.00500.0025trans-1,3-Dichloropropene
<0.0010 0.00500.0010Trichloroethene
<0.0025 0.00500.0025Trichlorofluoromethane
<0.0091 0.0250.0091Vinyl acetate
<0.0025 0.00500.0025Vinyl chloride
<0.0019 0.0100.0019Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 102 72 - 122
Dibromofluoromethane 96 79 - 123
Toluene-d8 (Surr)95 80 - 120
TestAmerica Pensacola Page 43 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 400-221058
1.0
1.0
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Solid
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/Kg
06221402-LCS.d
5.00 g
5.00 g
5 mL
06221403.D
5.00 g
5.00 g
5 mL
mg/Kg
Method: 8260B
Preparation: 5035
CH_WASP
CH_WASP
LCS 400-221058/18-A
LCSD 400-221058/19-A
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1109
06/21/2014 1815
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221047
400-221058
N/A
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1144
06/21/2014 1815
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221047
400-221058
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
10398 76 - 124 4 301,1,1,2-Tetrachloroethane
9998 72 - 121 1 301,1,1-Trichloroethane
111104 67 - 120 7 301,1,2,2-Tetrachloroethane
107101 75 - 118 6 301,1,2-Trichloroethane
9694 61 - 128 2 301,1-Dichloroethane
9697 62 - 130 1 301,1-Dichloroethene
101101 72 - 122 0 301,1-Dichloropropene
116109 72 - 124 7 301,2,3-Trichlorobenzene
104100 61 - 123 3 301,2,3-Trichloropropane
116111 72 - 126 5 301,2,4-Trichlorobenzene
112109 74 - 121 3 301,2,4-Trimethylbenzene
114102 57 - 123 12 301,2-Dibromo-3-Chloropropane
105102 76 - 120 3 301,2-Dichlorobenzene
104100 70 - 125 3 301,2-Dichloroethane
106104 64 - 129 3 301,2-Dichloropropane
111109 75 - 122 2 301,3,5-Trimethylbenzene
110106 78 - 118 4 301,3-Dichlorobenzene
10397 75 - 117 5 301,3-Dichloropropane
108103 77 - 118 4 301,4-Dichlorobenzene
9796 66 - 127 2 302,2-Dichloropropane
109106 72 - 119 3 302-Chlorotoluene
114107 54 - 140 6 302-Hexanone
112108 72 - 124 4 304-Chlorotoluene
118110 43 - 150 7 30Acetone
105104 74 - 119 1 30Benzene
109107 76 - 121 2 30Bromobenzene
10699 78 - 119 6 30Bromochloromethane
108107 68 - 128 2 30Bromodichloromethane
108105 54 - 125 3 30Bromoform
9992 25 - 150 8 30Bromomethane
9998 26 - 150 1 30Carbon disulfide
9999 70 - 128 0 30Carbon tetrachloride
105101 80 - 116 4 30Chlorobenzene
102109 22 - 150 7 30Chloroethane
10098 74 - 119 2 30Chloroform
9597 36 - 147 2 30Chloromethane
TestAmerica Pensacola Page 44 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 400-221058
1.0
1.0
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Solid
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/Kg
06221402-LCS.d
5.00 g
5.00 g
5 mL
06221403.D
5.00 g
5.00 g
5 mL
mg/Kg
Method: 8260B
Preparation: 5035
CH_WASP
CH_WASP
LCS 400-221058/18-A
LCSD 400-221058/19-A
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1109
06/21/2014 1815
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221047
400-221058
N/A
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1144
06/21/2014 1815
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221047
400-221058
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
102100 68 - 126 2 30cis-1,2-Dichloroethene
108104 68 - 125 4 30cis-1,3-Dichloropropene
10398 65 - 131 5 30Dibromochloromethane
106102 76 - 117 4 30Dibromomethane
8285 44 - 145 4 30Dichlorodifluoromethane
109107 78 - 120 2 30Ethylbenzene
107101 78 - 119 6 30Ethylene Dibromide
129126 61 - 140 3 30Hexachlorobutadiene
10091 42 - 150 10 30Iodomethane
10197 46 - 144 3 30Isopropyl ether
112111 78 - 119 1 30Isopropylbenzene
114103 62 - 126 10 30Methyl Ethyl Ketone
119113 56 - 137 5 30methyl isobutyl ketone
9894 69 - 124 4 30Methyl tert-butyl ether
111111 45 - 150 1 30Methylene Chloride
113109 70 - 120 4 30m-Xylene & p-Xylene
109101 64 - 126 8 30Naphthalene
120118 62 - 136 2 30n-Butylbenzene
115112 73 - 121 3 30N-Propylbenzene
112109 70 - 120 3 30o-Xylene
114111 77 - 123 2 30p-Cymene
113112 75 - 121 1 30sec-Butylbenzene
113109 66 - 132 3 30Styrene
111107 76 - 120 4 30tert-Butylbenzene
106105 74 - 126 1 30Tetrachloroethene
101100 76 - 120 1 30Toluene
10098 65 - 130 1 30trans-1,2-Dichloroethene
10297 65 - 126 5 30trans-1,3-Dichloropropene
107105 76 - 122 2 30Trichloroethene
9296 65 - 132 4 30Trichlorofluoromethane
99102 46 - 145 4 30Vinyl acetate
97100 52 - 134 3 30Vinyl chloride
112109 70 - 120 3 30Xylenes, Total
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 103 103 72 - 122
TestAmerica Pensacola Page 45 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
Dibromofluoromethane 98 96 79 - 123
Toluene-d8 (Surr)93 94 80 - 120
TestAmerica Pensacola Page 46 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
06/22/2014 1109
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Solid
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 400-221058
Method: 8260B
Preparation: 5035
Units:mg/KgLCS 400-221058/18-A LCSD 400-221058/19-ALCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
06/21/2014 1815
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1144
06/21/2014 1815
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
0.05130.04920.0500 0.05001,1,1,2-Tetrachloroethane
0.04950.04920.0500 0.05001,1,1-Trichloroethane
0.05550.05180.0500 0.05001,1,2,2-Tetrachloroethane
0.05360.05030.0500 0.05001,1,2-Trichloroethane
0.04820.04700.0500 0.05001,1-Dichloroethane
0.04790.04840.0500 0.05001,1-Dichloroethene
0.05050.05050.0500 0.05001,1-Dichloropropene
0.05800.05430.0500 0.05001,2,3-Trichlorobenzene
0.05200.05020.0500 0.05001,2,3-Trichloropropane
0.05820.05540.0500 0.05001,2,4-Trichlorobenzene
0.05590.05450.0500 0.05001,2,4-Trimethylbenzene
0.05720.05090.0500 0.05001,2-Dibromo-3-Chloropropane
0.05260.05100.0500 0.05001,2-Dichlorobenzene
0.05200.05020.0500 0.05001,2-Dichloroethane
0.05320.05190.0500 0.05001,2-Dichloropropane
0.05570.05460.0500 0.05001,3,5-Trimethylbenzene
0.05500.05290.0500 0.05001,3-Dichlorobenzene
0.05140.04870.0500 0.05001,3-Dichloropropane
0.05390.05170.0500 0.05001,4-Dichlorobenzene
0.04860.04790.0500 0.05002,2-Dichloropropane
0.05450.05300.0500 0.05002-Chlorotoluene
0.2280.2140.200 0.2002-Hexanone
0.05620.05400.0500 0.05004-Chlorotoluene
0.2360.2190.200 0.200Acetone
0.05260.05200.0500 0.0500Benzene
0.05440.05330.0500 0.0500Bromobenzene
0.05280.04960.0500 0.0500Bromochloromethane
0.05420.05330.0500 0.0500Bromodichloromethane
0.05400.05250.0500 0.0500Bromoform
0.04950.04590.0500 0.0500Bromomethane
0.04940.04890.0500 0.0500Carbon disulfide
0.04960.04960.0500 0.0500Carbon tetrachloride
0.05270.05050.0500 0.0500Chlorobenzene
0.05080.05430.0500 0.0500Chloroethane
0.04990.04880.0500 0.0500Chloroform
0.04730.04830.0500 0.0500Chloromethane
0.05110.05000.0500 0.0500cis-1,2-Dichloroethene
0.05400.05200.0500 0.0500cis-1,3-Dichloropropene
0.05140.04900.0500 0.0500Dibromochloromethane
TestAmerica Pensacola Page 47 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
06/22/2014 1109
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Solid
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 400-221058
Method: 8260B
Preparation: 5035
Units:mg/KgLCS 400-221058/18-A LCSD 400-221058/19-ALCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
06/21/2014 1815
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1144
06/21/2014 1815
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
0.05300.05120.0500 0.0500Dibromomethane
0.04100.04260.0500 0.0500Dichlorodifluoromethane
0.05460.05360.0500 0.0500Ethylbenzene
0.05340.05030.0500 0.0500Ethylene Dibromide
0.06470.06300.0500 0.0500Hexachlorobutadiene
0.04980.04530.0500 0.0500Iodomethane
0.05040.04860.0500 0.0500Isopropyl ether
0.05600.05540.0500 0.0500Isopropylbenzene
0.2270.2060.200 0.200Methyl Ethyl Ketone
0.2380.2260.200 0.200methyl isobutyl ketone
0.04900.04720.0500 0.0500Methyl tert-butyl ether
0.05560.05530.0500 0.0500Methylene Chloride
0.05650.05440.0500 0.0500m-Xylene & p-Xylene
0.05460.05050.0500 0.0500Naphthalene
0.05980.05880.0500 0.0500n-Butylbenzene
0.05760.05600.0500 0.0500N-Propylbenzene
0.05580.05430.0500 0.0500o-Xylene
0.05690.05570.0500 0.0500p-Cymene
0.05650.05600.0500 0.0500sec-Butylbenzene
0.05640.05470.0500 0.0500Styrene
0.05530.05340.0500 0.0500tert-Butylbenzene
0.05280.05240.0500 0.0500Tetrachloroethene
0.05050.05000.0500 0.0500Toluene
0.04980.04920.0500 0.0500trans-1,2-Dichloroethene
0.05100.04850.0500 0.0500trans-1,3-Dichloropropene
0.05330.05230.0500 0.0500Trichloroethene
0.04590.04790.0500 0.0500Trichlorofluoromethane
0.09870.1020.100 0.100Vinyl acetate
0.04850.04980.0500 0.0500Vinyl chloride
0.1120.1090.100 0.100Xylenes, Total
TestAmerica Pensacola Page 48 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221146
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06231404.D
5.00 g
5.00 gUnits:mg/Kg
Method: 8260B
Preparation: 5035
CH_WASPMB 400-221146/23-A
Analysis Date: 06/23/2014 1134
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221091
400-221146
Prep Date:
Leach Date:
06/21/2014 1815
N/A
Analyte RLMDLQualResult
<0.0025 0.00500.00251,1,1,2-Tetrachloroethane
<0.0011 0.00500.00111,1,1-Trichloroethane
<0.0025 0.00500.00251,1,2,2-Tetrachloroethane
<0.0025 0.00500.00251,1,2-Trichloroethane
<0.00083 0.00500.000831,1-Dichloroethane
<0.0025 0.00500.00251,1-Dichloroethene
<0.0025 0.00500.00251,1-Dichloropropene
<0.0025 0.00500.00251,2,3-Trichlorobenzene
<0.0030 0.00500.00301,2,3-Trichloropropane
<0.0020 0.00500.00201,2,4-Trichlorobenzene
<0.0010 0.00500.00101,2,4-Trimethylbenzene
<0.0033 0.00500.00331,2-Dibromo-3-Chloropropane
<0.00071 0.00500.000711,2-Dichlorobenzene
<0.00082 0.00500.000821,2-Dichloroethane
<0.0025 0.00500.00251,2-Dichloropropane
<0.00083 0.00500.000831,3,5-Trimethylbenzene
<0.00095 0.00500.000951,3-Dichlorobenzene
<0.0010 0.00500.00101,3-Dichloropropane
<0.0025 0.00500.00251,4-Dichlorobenzene
<0.0025 0.00500.00252,2-Dichloropropane
<0.0025 0.00500.00252-Chlorotoluene
<0.0050 0.0250.00502-Hexanone
<0.00098 0.00500.000984-Chlorotoluene
<0.0073 0.0250.0073Acetone
<0.0011 0.00500.0011Benzene
<0.0013 0.00500.0013Bromobenzene
<0.0025 0.00500.0025Bromochloromethane
<0.0025 0.00500.0025Bromodichloromethane
<0.0025 0.00500.0025Bromoform
<0.0025 0.00500.0025Bromomethane
<0.0025 0.00500.0025Carbon disulfide
<0.0017 0.00500.0017Carbon tetrachloride
<0.00052 0.00500.00052Chlorobenzene
<0.0025 0.00500.0025Chloroethane
<0.0025 0.00500.0025Chloroform
<0.0010 0.00500.0010Chloromethane
<0.00076 0.00500.00076cis-1,2-Dichloroethene
<0.0012 0.00500.0012cis-1,3-Dichloropropene
<0.0025 0.00500.0025Dibromochloromethane
<0.0025 0.00500.0025Dibromomethane
<0.0013 0.00500.0013Dichlorodifluoromethane
<0.00061 0.00500.00061Ethylbenzene
<0.0010 0.00500.0010Ethylene Dibromide
<0.0025 0.00500.0025Hexachlorobutadiene
<0.0034 0.00500.0034Iodomethane
TestAmerica Pensacola Page 49 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221146
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06231404.D
5.00 g
5.00 gUnits:mg/Kg
Method: 8260B
Preparation: 5035
CH_WASPMB 400-221146/23-A
Analysis Date: 06/23/2014 1134
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221091
400-221146
Prep Date:
Leach Date:
06/21/2014 1815
N/A
Analyte RLMDLQualResult
<0.00055 0.00500.00055Isopropyl ether
<0.00068 0.00500.00068Isopropylbenzene
<0.0060 0.0250.0060Methyl Ethyl Ketone
<0.0050 0.0250.0050methyl isobutyl ketone
<0.0010 0.00500.0010Methyl tert-butyl ether
<0.010 0.0150.010Methylene Chloride
<0.0013 0.0100.0013m-Xylene & p-Xylene
<0.0020 0.00500.0020Naphthalene
<0.00096 0.00500.00096n-Butylbenzene
<0.00090 0.00500.00090N-Propylbenzene
<0.0010 0.00500.0010o-Xylene
<0.0010 0.00500.0010p-Cymene
<0.00095 0.00500.00095sec-Butylbenzene
<0.0010 0.00500.0010Styrene
<0.0025 0.00500.0025tert-Butylbenzene
<0.0025 0.00500.0025Tetrachloroethene
<0.0010 0.00500.0010Toluene
<0.0025 0.00500.0025trans-1,2-Dichloroethene
<0.0025 0.00500.0025trans-1,3-Dichloropropene
<0.0010 0.00500.0010Trichloroethene
<0.0025 0.00500.0025Trichlorofluoromethane
<0.0091 0.0250.0091Vinyl acetate
<0.0025 0.00500.0025Vinyl chloride
<0.0019 0.0100.0019Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 102 72 - 122
Dibromofluoromethane 96 79 - 123
Toluene-d8 (Surr)94 80 - 120
TestAmerica Pensacola Page 50 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
1.0
Lab Control Sample - Batch: 400-221146
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06231410.D
5.00 g
5.00 gUnits:mg/Kg
Method: 8260B
Preparation: 5035
CH_WASPLCS 400-221146/24-A
Analysis Date: 06/23/2014 1407
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
Prep Date:
Leach Date:
06/21/2014 1815
N/A
Analyte QualLimit% Rec.ResultSpike Amount
0.0500 0.0502 100 76 - 1241,1,1,2-Tetrachloroethane
0.0500 0.0499 100 72 - 1211,1,1-Trichloroethane
0.0500 0.0564 113 67 - 1201,1,2,2-Tetrachloroethane
0.0500 0.0530 106 75 - 1181,1,2-Trichloroethane
0.0500 0.0501 100 61 - 1281,1-Dichloroethane
0.0500 0.0506 101 62 - 1301,1-Dichloroethene
0.0500 0.0500 100 72 - 1221,1-Dichloropropene
0.0500 0.0502 100 72 - 1241,2,3-Trichlorobenzene
0.0500 0.0533 107 61 - 1231,2,3-Trichloropropane
0.0500 0.0483 97 72 - 1261,2,4-Trichlorobenzene
0.0500 0.0471 94 74 - 1211,2,4-Trimethylbenzene
0.0500 0.0541 108 57 - 1231,2-Dibromo-3-Chloropropane
0.0500 0.0476 95 76 - 1201,2-Dichlorobenzene
0.0500 0.0535 107 70 - 1251,2-Dichloroethane
0.0500 0.0552 110 64 - 1291,2-Dichloropropane
0.0500 0.0471 94 75 - 1221,3,5-Trimethylbenzene
0.0500 0.0481 96 78 - 1181,3-Dichlorobenzene
0.0500 0.0523 105 75 - 1171,3-Dichloropropane
0.0500 0.0459 92 77 - 1181,4-Dichlorobenzene
0.0500 0.0490 98 66 - 1272,2-Dichloropropane
0.0500 0.0473 95 72 - 1192-Chlorotoluene
0.200 0.228 114 54 - 1402-Hexanone
0.0500 0.0476 95 72 - 1244-Chlorotoluene
0.200 0.230 115 43 - 150Acetone
0.0500 0.0533 107 74 - 119Benzene
0.0500 0.0511 102 76 - 121Bromobenzene
0.0500 0.0544 109 78 - 119Bromochloromethane
0.0500 0.0530 106 68 - 128Bromodichloromethane
0.0500 0.0533 107 54 - 125Bromoform
0.0500 0.0612 122 25 - 150Bromomethane
0.0500 0.0482 96 26 - 150Carbon disulfide
0.0500 0.0498 100 70 - 128Carbon tetrachloride
0.0500 0.0492 98 80 - 116Chlorobenzene
0.0500 0.0535 107 22 - 150Chloroethane
0.0500 0.0518 104 74 - 119Chloroform
0.0500 0.0456 91 36 - 147Chloromethane
0.0500 0.0539 108 68 - 126cis-1,2-Dichloroethene
0.0500 0.0543 109 68 - 125cis-1,3-Dichloropropene
0.0500 0.0514 103 65 - 131Dibromochloromethane
0.0500 0.0548 110 76 - 117Dibromomethane
0.0500 0.0413 83 44 - 145Dichlorodifluoromethane
0.0500 0.0494 99 78 - 120Ethylbenzene
0.0500 0.0540 108 78 - 119Ethylene Dibromide
0.0500 0.0428 86 61 - 140Hexachlorobutadiene
0.0500 0.0498 100 42 - 150Iodomethane
0.0500 0.0533 107 46 - 144Isopropyl ether
TestAmerica Pensacola Page 51 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
1.0
Lab Control Sample - Batch: 400-221146
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06231410.D
5.00 g
5.00 gUnits:mg/Kg
Method: 8260B
Preparation: 5035
CH_WASPLCS 400-221146/24-A
Analysis Date: 06/23/2014 1407
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
Prep Date:
Leach Date:
06/21/2014 1815
N/A
Analyte QualLimit% Rec.ResultSpike Amount
0.0500 0.0480 96 78 - 119Isopropylbenzene
0.200 0.230 115 62 - 126Methyl Ethyl Ketone
0.200 0.240 120 56 - 137methyl isobutyl ketone
0.0500 0.0518 104 69 - 124Methyl tert-butyl ether
0.0500 0.0546 109 45 - 150Methylene Chloride
0.0500 0.0505 101 70 - 120m-Xylene & p-Xylene
0.0500 0.0529 106 64 - 126Naphthalene
0.0500 0.0423 85 62 - 136n-Butylbenzene
0.0500 0.0477 95 73 - 121N-Propylbenzene
0.0500 0.0510 102 70 - 120o-Xylene
0.0500 0.0437 87 77 - 123p-Cymene
0.0500 0.0443 89 75 - 121sec-Butylbenzene
0.0500 0.0515 103 66 - 132Styrene
0.0500 0.0460 92 76 - 120tert-Butylbenzene
0.0500 0.0530 106 74 - 126Tetrachloroethene
0.0500 0.0491 98 76 - 120Toluene
0.0500 0.0512 102 65 - 130trans-1,2-Dichloroethene
0.0500 0.0524 105 65 - 126trans-1,3-Dichloropropene
0.0500 0.0532 106 76 - 122Trichloroethene
0.0500 0.0485 97 65 - 132Trichlorofluoromethane
0.100 0.101 101 46 - 145Vinyl acetate
0.0500 0.0501 100 52 - 134Vinyl chloride
0.100 0.101 101 70 - 120Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 104 72 - 122
Dibromofluoromethane 96 79 - 123
Toluene-d8 (Surr)95 80 - 120
TestAmerica Pensacola Page 52 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Dilution:
Dilution:
Solid
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Solid
06231408.D
4.565 g
5.00 mL
5 mL
06231409.D
5.117 g
5.00 mL
5 mL
Method: 8260B
Preparation: 5035
CH_WASP
CH_WASP
400-92338-B-1-C MS
400-92338-B-1-D MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221146
06/23/2014 1315
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 1341
06/20/2014 1500
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
06/20/2014 1500
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
98 95 32 - 125 15 281,1,1,2-Tetrachloroethane
102 99 52 - 120 15 181,1,1-Trichloroethane
126 120 28 - 120 16 20 F11,1,2,2-Tetrachloroethane
112 99 42 - 120 23 22 F21,1,2-Trichloroethane
100 93 45 - 120 19 16 F21,1-Dichloroethane
101 98 39 - 122 14 171,1-Dichloroethene
105 101 40 - 120 15 251,1-Dichloropropene
101 95 10 - 131 18 471,2,3-Trichlorobenzene
121 112 31 - 120 20 25 F11,2,3-Trichloropropane
100 94 10 - 131 17 561,2,4-Trichlorobenzene
87 138 10 - 135 25 82 F11,2,4-Trimethylbenzene
134 123 14 - 125 20 25 F11,2-Dibromo-3-Chloropropane
99 94 10 - 131 17 501,2-Dichlorobenzene
110 105 48 - 120 15 181,2-Dichloroethane
107 104 44 - 120 14 191,2-Dichloropropane
96 116 10 - 130 7 751,3,5-Trimethylbenzene
99 96 10 - 129 14 591,3-Dichlorobenzene
107 100 41 - 120 18 211,3-Dichloropropane
96 94 10 - 129 14 591,4-Dichlorobenzene
99 95 48 - 120 16 172,2-Dichloropropane
98 106 10 - 123 4 612-Chlorotoluene
137 124 29 - 130 21 36 F12-Hexanone
102 103 10 - 134 10 674-Chlorotoluene
95 75 11 - 149 20 22Acetone
176 301 42 - 120 41 20 F1 F1 F2Benzene
105 100 13 - 127 16 44Bromobenzene
107 99 44 - 123 19 18 F2Bromochloromethane
108 102 39 - 120 16 21Bromodichloromethane
112 106 18 - 123 17 27Bromoform
96 99 10 - 150 9 28Bromomethane
101 103 10 - 136 10 20Carbon disulfide
101 100 47 - 120 13 22Carbon tetrachloride
98 95 24 - 123 15 41Chlorobenzene
TestAmerica Pensacola Page 53 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Dilution:
Dilution:
Solid
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Solid
06231408.D
4.565 g
5.00 mL
5 mL
06231409.D
5.117 g
5.00 mL
5 mL
Method: 8260B
Preparation: 5035
CH_WASP
CH_WASP
400-92338-B-1-C MS
400-92338-B-1-D MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221146
06/23/2014 1315
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 1341
06/20/2014 1500
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
06/20/2014 1500
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
102 101 15 - 148 13 19Chloroethane
109 106 47 - 120 14 17Chloroform
90 86 14 - 130 15 20Chloromethane
102 87 47 - 120 27 18 F2cis-1,2-Dichloroethene
105 101 30 - 120 15 23cis-1,3-Dichloropropene
103 94 28 - 127 21 24Dibromochloromethane
109 103 42 - 120 16 18Dibromomethane
85 84 29 - 130 13 17Dichlorodifluoromethane
106 134 19 - 124 11 53 F1Ethylbenzene
113 104 38 - 124 20 22Ethylene Dibromide
119 118 10 - 133 12 117Hexachlorobutadiene
73 78 18 - 124 6 36Iodomethane
103 99 32 - 126 16 40Isopropyl ether
106 105 13 - 127 12 66Isopropylbenzene
129 110 42 - 120 20 20 F1Methyl Ethyl Ketone
141 132 36 - 125 18 27 F1 F1methyl isobutyl ketone
456 437 44 - 123 15 17 F1 F1Methyl tert-butyl ether
104 107 35 - 126 9 19Methylene Chloride
113 278 15 - 125 63 60 F1 F2m-Xylene & p-Xylene
120 113 10 - 136 17 41Naphthalene
106 108 10 - 150 9 110n-Butylbenzene
105 112 10 - 130 5 79N-Propylbenzene
116 185 18 - 124 32 49 F1o-Xylene
105 105 10 - 138 12 93p-Cymene
106 107 10 - 133 11 86sec-Butylbenzene
103 101 12 - 135 13 52Styrene
106 111 10 - 130 7 73tert-Butylbenzene
101 97 30 - 123 16 46Tetrachloroethene
153 336 34 - 120 62 36 F1 F1 F2Toluene
102 97 38 - 126 16 18trans-1,2-Dichloroethene
101 94 26 - 120 19 26trans-1,3-Dichloropropene
107 102 46 - 120 16 27Trichloroethene
100 92 48 - 126 19 16 F2Trichlorofluoromethane
TestAmerica Pensacola Page 54 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Dilution:
Dilution:
Solid
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Solid
06231408.D
4.565 g
5.00 mL
5 mL
06231409.D
5.117 g
5.00 mL
5 mL
Method: 8260B
Preparation: 5035
CH_WASP
CH_WASP
400-92338-B-1-C MS
400-92338-B-1-D MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221146
06/23/2014 1315
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 1341
06/20/2014 1500
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221091
400-221146
N/A
06/20/2014 1500
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
92 90 10 - 150 14 74Vinyl acetate
100 99 32 - 122 13 16Vinyl chloride
114 231 10 - 150 50 56 F1Xylenes, Total
Surrogate Acceptance LimitsMS % Rec MSD % Rec
4-Bromofluorobenzene 105 105 72 - 122
Dibromofluoromethane 99 98 79 - 123
Toluene-d8 (Surr)95 94 80 - 120
TestAmerica Pensacola Page 55 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
06/23/2014 1315 06/23/2014 1341
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Solid
Method: 8260B
Preparation: 5035
Units:mg/Kg400-92338-B-1-C MS 400-92338-B-1-D MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221146
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1500
N/A
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1500
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
<0.0035 0.0723 0.0645 0.0709 0.06131,1,1,2-Tetrachloroethane
<0.0016 0.0723 0.0645 0.0739 0.06361,1,1-Trichloroethane
<0.0035 0.0723 0.0645 0.0908 0.0771F11,1,2,2-Tetrachloroethane
<0.0035 0.0723 0.0645 0.0806 0.0637 F21,1,2-Trichloroethane
<0.0012 0.0723 0.0645 0.0722 0.0599 F21,1-Dichloroethane
<0.0035 0.0723 0.0645 0.0732 0.06341,1-Dichloroethene
<0.0035 0.0723 0.0645 0.0761 0.06531,1-Dichloropropene
<0.0035 0.0723 0.0645 0.0732 0.06121,2,3-Trichlorobenzene
<0.0043 0.0723 0.0645 0.0876 0.0719F11,2,3-Trichloropropane
<0.0028 0.0723 0.0645 0.0719 0.06091,2,4-Trichlorobenzene
0.025 0.0723 0.0645 0.0881 0.114 F11,2,4-Trimethylbenzene
<0.0047 0.0723 0.0645 0.0966 0.0793F11,2-Dibromo-3-Chloropropane
<0.0010 0.0723 0.0645 0.0713 0.06041,2-Dichlorobenzene
<0.0012 0.0723 0.0645 0.0792 0.06801,2-Dichloroethane
<0.0035 0.0723 0.0645 0.0772 0.06691,2-Dichloropropane
0.011 0.0723 0.0645 0.0798 0.08541,3,5-Trimethylbenzene
<0.0013 0.0723 0.0645 0.0716 0.06201,3-Dichlorobenzene
<0.0014 0.0723 0.0645 0.0771 0.06431,3-Dichloropropane
<0.0035 0.0723 0.0645 0.0695 0.06061,4-Dichlorobenzene
<0.0035 0.0723 0.0645 0.0719 0.06112,2-Dichloropropane
0.0041 J 0.0723 0.0645 0.0751 0.07252-Chlorotoluene
0.0075 J 0.289 0.258 0.403 0.328F12-Hexanone
<0.0014 0.0723 0.0645 0.0740 0.06674-Chlorotoluene
0.17 0.289 0.258 0.441 0.360Acetone
0.0030 J 0.0723 0.0645 0.130 0.197F1 F1 F2Benzene
<0.0018 0.0723 0.0645 0.0758 0.0643Bromobenzene
<0.0035 0.0723 0.0645 0.0777 0.0641 F2Bromochloromethane
<0.0035 0.0723 0.0645 0.0778 0.0660Bromodichloromethane
<0.0035 0.0723 0.0645 0.0813 0.0685Bromoform
<0.0035 0.0723 0.0645 0.0694 0.0636Bromomethane
<0.0035 0.0723 0.0645 0.0730 0.0662Carbon disulfide
<0.0024 0.0723 0.0645 0.0732 0.0644Carbon tetrachloride
<0.00074 0.0723 0.0645 0.0711 0.0614Chlorobenzene
<0.0035 0.0723 0.0645 0.0740 0.0651Chloroethane
<0.0035 0.0723 0.0645 0.0789 0.0684Chloroform
<0.0014 0.0723 0.0645 0.0649 0.0557Chloromethane
<0.0011 0.0723 0.0645 0.0737 0.0561 F2cis-1,2-Dichloroethene
<0.0017 0.0723 0.0645 0.0758 0.0652cis-1,3-Dichloropropene
<0.0035 0.0723 0.0645 0.0747 0.0605Dibromochloromethane
<0.0035 0.0723 0.0645 0.0785 0.0666Dibromomethane
<0.0018 0.0723 0.0645 0.0615 0.0542Dichlorodifluoromethane
0.0046 J 0.0723 0.0645 0.0810 0.0906 F1Ethylbenzene
<0.0014 0.0723 0.0645 0.0818 0.0671Ethylene Dibromide
TestAmerica Pensacola Page 56 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
06/23/2014 1315 06/23/2014 1341
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Solid
Method: 8260B
Preparation: 5035
Units:mg/Kg400-92338-B-1-C MS 400-92338-B-1-D MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221146
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1500
N/A
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1500
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
<0.0035 0.0723 0.0645 0.0857 0.0761Hexachlorobutadiene
<0.0048 0.0723 0.0645 0.0531 0.0502Iodomethane
<0.00078 0.0723 0.0645 0.0748 0.0635Isopropyl ether
0.0010 J 0.0723 0.0645 0.0775 0.0684Isopropylbenzene
0.11 0.289 0.258 0.482 0.394F1Methyl Ethyl Ketone
0.010 J 0.289 0.258 0.418 0.350F1 F1methyl isobutyl ketone
0.016 0.0723 0.0645 0.345 0.297F1 F1Methyl tert-butyl ether
<0.014 0.0723 0.0645 0.0753 0.0689Methylene Chloride
0.025 0.0723 0.0645 0.106 0.204 F1 F2m-Xylene & p-Xylene
<0.0028 0.0723 0.0645 0.0864 0.0729Naphthalene
0.0024 J 0.0723 0.0645 0.0794 0.0724n-Butylbenzene
0.0039 J 0.0723 0.0645 0.0801 0.0763N-Propylbenzene
0.0099 0.0723 0.0645 0.0938 0.129 F1o-Xylene
<0.0014 0.0723 0.0645 0.0762 0.0678p-Cymene
<0.0013 0.0723 0.0645 0.0764 0.0687sec-Butylbenzene
<0.0014 0.0723 0.0645 0.0744 0.0653Styrene
<0.0035 0.0723 0.0645 0.0766 0.0715tert-Butylbenzene
<0.0035 0.0723 0.0645 0.0731 0.0625Tetrachloroethene
0.0085 0.0723 0.0645 0.119 0.225F1 F1 F2Toluene
<0.0035 0.0723 0.0645 0.0739 0.0628trans-1,2-Dichloroethene
<0.0035 0.0723 0.0645 0.0727 0.0603trans-1,3-Dichloropropene
<0.0014 0.0723 0.0645 0.0771 0.0659Trichloroethene
<0.0035 0.0723 0.0645 0.0720 0.0595 F2Trichlorofluoromethane
<0.013 0.145 0.129 0.133 0.116Vinyl acetate
<0.0035 0.0723 0.0645 0.0723 0.0637Vinyl chloride
0.035 0.145 0.129 0.200 0.333 F1Xylenes, Total
TestAmerica Pensacola Page 57 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221232
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mb 221232.D
30.0 g
1 mLUnits:mg/Kg
Method: 8270D
Preparation: 3550C
PigpenMB 400-221232/1-A
Analysis Date: 06/24/2014 1023
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221174
400-221232
Prep Date:Injection Volume:1 uL
Leach Date:
06/23/2014 1726
N/A
Analyte RLMDLQualResult
<0.033 0.330.0331,1'-Biphenyl
<0.033 0.330.0331,2,4,5-Tetrachlorobenzene
<0.033 0.330.0331,2,4-Trichlorobenzene
<0.033 0.330.0331,2-Dichlorobenzene
<0.033 0.330.0331,3-Dichlorobenzene
<0.033 0.330.0331,3-Dinitrobenzene
<0.033 0.330.0331,4-Dichlorobenzene
<0.033 0.330.0331,4-Dioxane
<0.020 0.330.0201-Methylnaphthalene
<0.033 0.330.0332,3,4,6-Tetrachlorophenol
<0.033 0.330.0332,4,5-Trichlorophenol
<0.033 0.330.0332,4,6-Trichlorophenol
<0.033 0.330.0332,4-Dichlorophenol
<0.033 0.330.0332,4-Dimethylphenol
<0.29 0.990.292,4-Dinitrophenol
<0.033 0.330.0332,4-Dinitrotoluene
<0.033 0.330.0332,6-Dinitrotoluene
<0.033 0.330.0332-Chloronaphthalene
<0.033 0.330.0332-Chlorophenol
<0.018 0.330.0182-Methylnaphthalene
<0.033 0.330.0332-Methylphenol
<0.033 0.330.0332-Nitroaniline
<0.033 0.330.0332-Nitrophenol
<0.033 0.660.0333 & 4 Methylphenol
<0.060 0.330.0604,6-Dinitro-2-methylphenol
<0.033 0.330.0334-Bromophenyl phenyl ether
<0.033 0.330.0334-Chloro-3-methylphenol
<0.033 0.330.0334-Chlorophenyl phenyl ether
<0.15 0.330.154-Nitrophenol
<0.020 0.330.020Acenaphthene
<0.020 0.330.020Acenaphthylene
<0.033 0.330.033Acetophenone
<0.020 0.330.020Anthracene
<0.033 0.330.033Azobenzene
<0.033 0.330.033Benzaldehyde
<0.020 0.330.020Benzo[a]anthracene
<0.020 0.330.020Benzo[a]pyrene
<0.025 0.330.025Benzo[b]fluoranthene
<0.030 0.330.030Benzo[g,h,i]perylene
<0.022 0.330.022Benzo[k]fluoranthene
<0.35 0.990.35Benzoic acid
<0.050 0.330.050Benzyl alcohol
<0.033 0.330.033bis (2-chloroisopropyl) ether
<0.033 0.330.033Bis(2-chloroethoxy)methane
<0.033 0.330.033Bis(2-chloroethyl)ether
TestAmerica Pensacola Page 58 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221232
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mb 221232.D
30.0 g
1 mLUnits:mg/Kg
Method: 8270D
Preparation: 3550C
PigpenMB 400-221232/1-A
Analysis Date: 06/24/2014 1023
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221174
400-221232
Prep Date:Injection Volume:1 uL
Leach Date:
06/23/2014 1726
N/A
Analyte RLMDLQualResult
0.0506 J 0.330.033Bis(2-ethylhexyl) phthalate
<0.033 0.330.033Butyl benzyl phthalate
<0.050 0.330.050Carbazole
<0.022 0.330.022Chrysene
<0.025 0.330.025Dibenz(a,h)anthracene
<0.033 0.330.033Dibenzofuran
<0.033 0.330.033Diethyl phthalate
<0.033 0.330.033Dimethyl phthalate
0.0419 J 0.330.033Di-n-butyl phthalate
<0.033 0.330.033Di-n-octyl phthalate
<0.025 0.330.025Fluoranthene
<0.020 0.330.020Fluorene
<0.10 0.330.10Hexachlorobenzene
<0.033 0.330.033Hexachlorobutadiene
<0.066 0.330.066Hexachlorocyclopentadiene
<0.10 0.330.10Hexachloroethane
<0.033 0.330.033Hexadecane
<0.33 0.330.33Indene
<0.025 0.330.025Indeno[1,2,3-cd]pyrene
<0.033 0.330.033Isophorone
<0.022 0.330.022Naphthalene
<0.033 0.330.033n-Decane
<0.033 0.330.033Nitrobenzene
<0.066 0.330.066N-Nitrosodimethylamine
<0.11 0.330.11N-Nitrosodi-n-propylamine
<0.033 0.330.033N-Nitrosodiphenylamine
<0.033 0.330.033n-Octadecane
<0.066 0.660.066Pentachlorophenol
<0.020 0.330.020Phenanthrene
<0.033 0.330.033Phenol
<0.025 0.330.025Pyrene
<0.15 0.330.15Pyridine
<0.033 0.330.033Sulfolane
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol (Surr)91 32 - 133
2-Fluorobiphenyl 103 44 - 120
2-Fluorophenol (Surr)91 25 - 120
Nitrobenzene-d5 (Surr)100 27 - 120
Phenol-d5 (Surr)99 37 - 120
Terphenyl-d14 (Surr)91 36 - 134
TestAmerica Pensacola Page 59 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
1.0
Lab Control Sample - Batch: 400-221232
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
lcs 221233.D
30.0 g
1 mLUnits:mg/Kg
Method: 8270D
Preparation: 3550C
PigpenLCS 400-221232/2-A
Analysis Date: 06/24/2014 1101
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-221232
N/A
Prep Date:Injection Volume:1 uL
Leach Date:
06/23/2014 1726
N/A
Analyte QualLimit% Rec.ResultSpike Amount
1.00 0.772 77 64 - 1201,1'-Biphenyl
1.00 0.795 79 63 - 1201,2,4,5-Tetrachlorobenzene
1.00 0.762 76 62 - 1201,2,4-Trichlorobenzene
1.00 0.719 72 58 - 1201,2-Dichlorobenzene
1.00 0.704 70 56 - 1201,3-Dichlorobenzene
1.00 0.751 75 42 - 1361,3-Dinitrobenzene
1.00 0.741 74 58 - 1201,4-Dichlorobenzene
1.00 0.526 53 10 - 1321,4-Dioxane
1.00 0.743 74 66 - 1201-Methylnaphthalene
1.00 0.835 84 46 - 1262,3,4,6-Tetrachlorophenol
1.00 0.835 84 62 - 1202,4,5-Trichlorophenol
1.00 0.851 85 59 - 1202,4,6-Trichlorophenol
1.00 0.836 84 67 - 1202,4-Dichlorophenol
1.00 0.844 84 65 - 1202,4-Dimethylphenol
2.00 1.13 56 23 - 1242,4-Dinitrophenol
1.00 0.802 80 59 - 1282,4-Dinitrotoluene
1.00 0.784 78 51 - 1302,6-Dinitrotoluene
1.00 0.769 77 34 - 1372-Chloronaphthalene
1.00 0.806 81 60 - 1202-Chlorophenol
1.00 0.730 73 64 - 1202-Methylnaphthalene
1.00 0.834 83 55 - 1202-Methylphenol
1.00 0.814 81 51 - 1282-Nitroaniline
1.00 0.777 78 56 - 1202-Nitrophenol
1.00 0.827 83 47 - 1343 & 4 Methylphenol
2.00 1.63 82 40 - 1264,6-Dinitro-2-methylphenol
1.00 0.836 84 51 - 1304-Bromophenyl phenyl ether
1.00 0.832 83 66 - 1214-Chloro-3-methylphenol
1.00 0.781 78 62 - 1224-Chlorophenyl phenyl ether
2.00 1.87 94 34 - 1484-Nitrophenol
1.00 0.773 77 62 - 120Acenaphthene
1.00 0.757 76 61 - 120Acenaphthylene
1.00 0.813 81 66 - 120Acetophenone
1.00 0.809 81 68 - 120Anthracene
1.00 0.817 82 39 - 145Azobenzene
1.00 0.374 37 10 - 200Benzaldehyde
1.00 0.802 80 67 - 120Benzo[a]anthracene
1.00 0.858 86 64 - 120Benzo[a]pyrene
1.00 0.846 85 58 - 121Benzo[b]fluoranthene
1.00 0.973 97 49 - 151Benzo[g,h,i]perylene
1.00 0.796 80 61 - 123Benzo[k]fluoranthene
1.00 <0.35 32 10 - 120Benzoic acid
1.00 0.805 81 52 - 120Benzyl alcohol
1.00 0.742 74 20 - 140bis (2-chloroisopropyl) ether
1.00 0.801 80 60 - 120Bis(2-chloroethoxy)methane
1.00 0.716 72 55 - 120Bis(2-chloroethyl)ether
1.00 1.01 101 59 - 136Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 60 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Solid
1.0
Lab Control Sample - Batch: 400-221232
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
lcs 221233.D
30.0 g
1 mLUnits:mg/Kg
Method: 8270D
Preparation: 3550C
PigpenLCS 400-221232/2-A
Analysis Date: 06/24/2014 1101
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-221232
N/A
Prep Date:Injection Volume:1 uL
Leach Date:
06/23/2014 1726
N/A
Analyte QualLimit% Rec.ResultSpike Amount
1.00 0.825 83 55 - 135Butyl benzyl phthalate
1.00 0.738 74 69 - 121Carbazole
1.00 0.811 81 65 - 120Chrysene
1.00 1.00 100 58 - 130Dibenz(a,h)anthracene
1.00 0.769 77 65 - 120Dibenzofuran
1.00 0.720 72 62 - 124Diethyl phthalate
1.00 0.742 74 52 - 123Dimethyl phthalate
1.00 0.850 85 67 - 132Di-n-butyl phthalate
1.00 0.995 99 58 - 132Di-n-octyl phthalate
1.00 0.843 84 67 - 123Fluoranthene
1.00 0.766 77 64 - 120Fluorene
1.00 0.801 80 57 - 131Hexachlorobenzene
1.00 0.794 79 56 - 120Hexachlorobutadiene
1.00 0.521 52 10 - 153Hexachlorocyclopentadiene
1.00 0.734 73 53 - 120Hexachloroethane
1.00 0.851 85 19 - 154Hexadecane
1.00 0.695 69 36 - 126Indene
1.00 0.974 97 55 - 133Indeno[1,2,3-cd]pyrene
1.00 0.773 77 63 - 120Isophorone
1.00 0.757 76 59 - 120Naphthalene
1.00 0.643 64 17 - 131n-Decane
1.00 0.791 79 53 - 125Nitrobenzene
1.00 0.699 70 26 - 140N-Nitrosodimethylamine
1.00 0.799 80 34 - 150N-Nitrosodi-n-propylamine
0.500 0.421 84 16 - 160N-Nitrosodiphenylamine
1.00 0.828 83 26 - 151n-Octadecane
2.00 2.06 103 30 - 136Pentachlorophenol
1.00 0.806 81 62 - 130Phenanthrene
1.00 0.813 81 54 - 120Phenol
1.00 0.720 72 57 - 127Pyrene
1.00 0.527 53 16 - 120Pyridine
1.05 1.04 99 50 - 150Sulfolane
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol (Surr)91 32 - 133
2-Fluorobiphenyl 96 44 - 120
2-Fluorophenol (Surr)94 25 - 120
Nitrobenzene-d5 (Surr)98 27 - 120
Phenol-d5 (Surr)100 37 - 120
Terphenyl-d14 (Surr)94 36 - 134
TestAmerica Pensacola Page 61 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-220960
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
R062015.D
5.0 g
5.0 gUnits:mg/Kg
Method: 8015C
Preparation: 5035
CH_RITAMB 400-220960/1-A
Analysis Date: 06/20/2014 1728
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-220959
400-220960
Prep Date:Injection Volume:5 mL
Leach Date:
06/20/2014 1500
N/A PRIMARYColumn ID:
Analyte RLMDLQualResult
<0.050 0.100.050Gasoline Range Organics (GRO)-C6-C10
Surrogate % Rec Acceptance Limits
a,a,a-Trifluorotoluene (fid)94 65 - 125
Solid
1.0
Lab Control Sample - Batch: 400-220960
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
R062017.D
5.0 g
5.0 gUnits:mg/Kg
Method: 8015C
Preparation: 5035
CH_RITALCS 400-220960/2-A
Analysis Date: 06/20/2014 1823
Analysis Batch:
Prep Batch:
Leach Batch:
400-220959
400-220960
N/A
Prep Date:Injection Volume:5 mL
Column ID:PRIMARYLeach Date:
06/20/2014 1500
N/A
Analyte QualLimit% Rec.ResultSpike Amount
1.00 1.02 102 62 - 141Gasoline Range Organics (GRO)-C6-C10
Surrogate % Rec Acceptance Limits
a,a,a-Trifluorotoluene (fid)88 65 - 125
TestAmerica Pensacola Page 62 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Dilution:
Dilution:
Solid
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix:Solid
R062020.D
5.11 g
5.0 g
5 mL
PRIMARY
R062021.D
5.18 g
5.0 g
5 mL
PRIMARY
Method: 8015C
Preparation: 5035
CH_RITA
CH_RITA
400-92344-A-2-B MS
400-92344-A-2-C MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-220960
06/20/2014 1945
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-220959
400-220960
N/A
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 2012
06/20/2014 1500
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-220959
400-220960
N/A
06/20/2014 1500
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
104 108 10 - 150 2 32Gasoline Range Organics (GRO)-C6-C10
Surrogate Acceptance LimitsMS % Rec MSD % Rec
a,a,a-Trifluorotoluene (fid)93 96 65 - 125
Solid
06/20/2014 1945 06/20/2014 2012
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Solid
Method: 8015C
Preparation: 5035
Units:mg/Kg400-92344-A-2-B MS 400-92344-A-2-C MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-220960
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1500
N/A
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1500
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
<0.051 1.04 1.03 1.08 1.11Gasoline Range Organics (GRO)-C6-C10
TestAmerica Pensacola Page 63 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
SolidClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221077
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MB 400-2210771-A_049.d
15.0 g
2 mLUnits:mg/Kg
Method: 8015C
Preparation: 3546
WALLEMB 400-221077/1-A
Analysis Date: 06/23/2014 1153
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221123
400-221077
Prep Date:Injection Volume:1 uL
Leach Date:
06/22/2014 1407
N/A PRIMARYColumn ID:
Analyte RLMDLQualResult
<3.4 103.4Diesel Range Organics [C10-C28]
Surrogate % Rec Acceptance Limits
o-Terphenyl (Surr)144 27 - 151
Solid
1.0
Lab Control Sample - Batch: 400-221077
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
LCS 400-2210772-A_050.d
15.0 g
2 mLUnits:mg/Kg
Method: 8015C
Preparation: 3546
WALLELCS 400-221077/2-A
Analysis Date: 06/23/2014 1203
Analysis Batch:
Prep Batch:
Leach Batch:
400-221123
400-221077
N/A
Prep Date:Injection Volume:1 uL
Column ID:PRIMARYLeach Date:
06/22/2014 1407
N/A
Analyte QualLimit% Rec.ResultSpike Amount
337 335 100 63 - 153Diesel Range Organics [C10-C28]
Surrogate % Rec Acceptance Limits
o-Terphenyl (Surr)146 27 - 151
TestAmerica Pensacola Page 64 of 70
Quality Control Results
Job Number: 400-92351-1Client: AEI Consultants
Dilution:
Dilution:
Solid
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix:Solid
400-92269-A-1-D MS_052.d
14.95 g
2 mL
1 uL
PRIMARY
400-92269-A-1-E MSD_053.d
15.06 g
2 mL
1 uL
PRIMARY
Method: 8015C
Preparation: 3546
WALLE
WALLE
400-92269-A-1-A MS
400-92269-A-1-B MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221077
06/23/2014 1223
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221123
400-221077
N/A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 1233
06/22/2014 1407
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221123
400-221077
N/A
06/22/2014 1407
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
90 93 62 - 204 2 30Diesel Range Organics [C10-C28]
Surrogate Acceptance LimitsMS % Rec MSD % Rec
o-Terphenyl (Surr)122 123 27 - 151
Solid
06/23/2014 1223 06/23/2014 1233
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Solid
Method: 8015C
Preparation: 3546
Units:mg/Kg400-92269-A-1-A MS 400-92269-A-1-B MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221077
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1407
N/A
Analysis Date:
Prep Date:
Leach Date:
06/22/2014 1407
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
27 403 400 391 401Diesel Range Organics [C10-C28]
TestAmerica Pensacola Page 65 of 70
DATA REPORTING QUALIFIERS
Client: AEI Consultants Job Number: 400-92351-1
Lab Section Qualifier Description
GC/MS VOA
MS and/or MSD Recovery exceeds the control limitsF1
MS/MSD RPD exceeds control limitsF2
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
GC/MS Semi VOA
Compound was found in the blank and sample.B
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
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Login Sample Receipt Checklist
Client: AEI Consultants Job Number: 400-92351-1
Login Number: 92351
Question Answer Comment
Creator: Summers, Dustin H
List Source: TestAmerica Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.2.5°C/2.0°C/0.0°C IR-5
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Pensacola Page 70 of 70
ANALYTICAL REPORT
Job Number: 400-92351-2
Job Description: Seneca Place
For:
AEI Consultants
6065 Roswell Road
Suite 940
Atlanta, GA 30328-4013
Attention: Steve Yekich
_____________________________________________
Approved for release.
Marty P Edwards
Manager of Project Management
6/24/2014 10:40 PM
Marty P Edwards, Manager of Project Management
3355 McLemore Drive, Pensacola, FL, 32514
[phone]
[e-mail]
06/24/2014
The test results in this report meet all NELAP requirements for accredited parameters, unless otherwise noted, and
relate only to the referenced samples. Pursuant to NELAP, this report may not be reproduced, except in full, without
written approval from the laboratory. For questions please contact the Project Manager at the e-mail address listed on
this page, or the telephone number at the bottom of the page.
TestAmerica Pensacola Certifications and Approvals: Alabama (40150), Arizona (AZ0710), Arkansas (88-0689), Florida
(E81010), Illinois (200041), Iowa (367), Kansas (E-10253), Kentucky UST (53), Louisiana (30748), Maryland (233),
Massachusetts (M-FL094), Michigan (9912), New Hampshire (250507), New Jersey (FL006), North Carolina (314),
Oklahoma (9810), Pennsylvania (68-00467), Rhode Island (LAO00307), South Carolina (96026), Tennessee
(TN02907), Texas (T104704286-09-1), Virginia (00008), Washington (C915), West Virginia (136), USDA Foreign Soil
Permit (P330-08-00006).
TestAmerica Laboratories, Inc.
TestAmerica Pensacola 3355 McLemore Drive, Pensacola, FL 32514
Tel [phone] Fax [phone] www.testamericainc.com
Page 1 of 81
Job Narrative
400-92351-2
Comments
No additional comments.
Receipt
The samples were received on 6/20/2014 8:21 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 3 coolers at receipt time were 0.0º C, 2.0º C and 2.5º C.
GC/MS VOA
Method 8260B: The continuing calibration verification (CCV) associated with batch 400-221089 recovered above the upper control limit
for Bromomethane. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been
reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: The surrogate recovery for the blank associated with batch 400-220899 was outside the control limits. All associated
sample surrogates fell within acceptance criteria or are biased high and non-detect; therefore, the data have been reported.
Method 8270D: The flagged analytes recovered outside control limits for the LCS/LCSD associated with batch 400-220899. This is not
indicative of a systematic control problem because these were random marginal exceedances. Qualified results have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
GC Semi VOA
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
Method 3520C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with batch400- 220899.
Method 3520C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MS/MSD/DUP) associated with batch 400-220901.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Page 2 of 81
EXECUTIVE SUMMARY - Detections
Client: AEI Consultants Job Number: 400-92351-2
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
400-92351-1 MW-8
1.0 ug/L SM 6200B311,2,4-Trimethylbenzene
1.0 ug/L SM 6200B4.01,3,5-Trimethylbenzene
1.0 ug/L SM 6200B9.6Benzene
1.0 ug/L SM 6200B0.95 JChloroform
1.0 ug/L SM 6200B8.0Ethylbenzene
1.0 ug/L SM 6200B1.3Isopropylbenzene
5.0 ug/L SM 6200B65m-Xylene & p-Xylene
1.0 ug/L SM 6200B8.4Naphthalene
1.0 ug/L SM 6200B1.9N-Propylbenzene
5.0 ug/L SM 6200B43o-Xylene
1.0 ug/L SM 6200B0.91 Jp-Cymene
1.0 ug/L SM 6200B1.0Tetrachloroethene
1.0 ug/L SM 6200B3.2Toluene
10 ug/L SM 6200B110Xylenes, Total
400-92351-2 MW-11
1.0 ug/L SM 6200B0.94 JChloroform
1.0 ug/L SM 6200B7.3cis-1,2-Dichloroethene
1.0 ug/L SM 6200B9.4Tetrachloroethene
1.0 ug/L SM 6200B2.1Trichloroethene
400-92351-3 SP-1W
1.0 ug/L SM 6200B7.6Chloroform
1.0 ug/L SM 6200B2.3Tetrachloroethene
9.5 ug/L 8270D0.77 JDiethyl phthalate
400-92351-4 SP-2W
1.0 ug/L SM 6200B2.5Chloroform
1.0 ug/L SM 6200B17Tetrachloroethene
9.5 ug/L 8270D0.79 JDiethyl phthalate
400-92351-5 SP-3W
1.0 ug/L SM 6200B2.2Chloroform
1.0 ug/L SM 6200B12cis-1,2-Dichloroethene
1.0 ug/L SM 6200B180Tetrachloroethene
1.0 ug/L SM 6200B5.4Trichloroethene
9.5 ug/L 8270D0.71 JDiethyl phthalate
400-92351-6 SP-4W
1.0 ug/L SM 6200B3.8Tetrachloroethene
TestAmerica Pensacola Page 3 of 81
EXECUTIVE SUMMARY - Detections
Client: AEI Consultants Job Number: 400-92351-2
Analyte Result
Reporting
Limit Units Method
Lab Sample ID Client Sample ID
Qualifier
400-92351-7 SP-5W
1.0 ug/L SM 6200B6.4Benzene
1.0 ug/L SM 6200B58Tetrachloroethene
400-92351-8 SP-6W
10 ug/L SM 6200B1500Tetrachloroethene
100 ug/L 8015C370Gasoline Range Organics (GRO)-C6-C10
400-92351-9 SP-7W
1.0 ug/L SM 6200B29Chloroform
400-92351-10 MW-7
1.0 ug/L SM 6200B2.0Tetrachloroethene
TestAmerica Pensacola Page 4 of 81
METHOD SUMMARY
Client: AEI Consultants Job Number: 400-92351-2
Preparation MethodMethodLab LocationDescription
Matrix:Water
SM 6200B TAL PEN SM21 SM 6200B
Purge and Trap TAL PEN SW846 5030B
Semivolatile Organic Compounds (GC/MS)TAL PEN SW846 8270D
Liquid-Liquid Extraction (Continuous)TAL PEN SW846 3520C
GRO by 8015C TAL PEN SW846 8015C
Purge and Trap TAL PEN SW846 5030B
Nonhalogenated Organics using GC/FID -Modified (Diesel
Range Organics)
TAL PEN SW846 8015C
Liquid-Liquid Extraction (Continuous)TAL PEN SW846 3520C
Lab References:
TAL PEN = TestAmerica Pensacola
Method References:
SM21 = Standard Methods For The Examination Of Water And Wastewater, 21st Edition
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica Pensacola Page 5 of 81
METHOD / ANALYST SUMMARY
Client: AEI Consultants Job Number: 400-92351-2
Method Analyst Analyst ID
Noble, Carl L CLNSM21 SM 6200B
Waite, Daniel H DHWSW846 8270D
Arbuckle, Mardy K MKASW846 8015C
Khramova, Galina R GRKSW846 8015C
Reeves, Isaiah D IDRSW846 8015C
TestAmerica Pensacola
Page 6 of 81
SAMPLE SUMMARY
Client: AEI Consultants Job Number: 400-92351-2
Client Sample IDLab Sample ID Client Matrix Sampled Received
Date/Time Date/Time
400-92351-1 MW-8 Water 06/19/2014 0710 06/20/2014 0821
400-92351-2 MW-11 Water 06/19/2014 0750 06/20/2014 0821
400-92351-3 SP-1W Water 06/19/2014 0830 06/20/2014 0821
400-92351-4 SP-2W Water 06/19/2014 0930 06/20/2014 0821
400-92351-5 SP-3W Water 06/19/2014 1044 06/20/2014 0821
400-92351-6 SP-4W Water 06/19/2014 1151 06/20/2014 0821
400-92351-7 SP-5W Water 06/19/2014 1300 06/20/2014 0821
400-92351-8 SP-6W Water 06/19/2014 1422 06/20/2014 0821
400-92351-9 SP-7W Water 06/19/2014 1510 06/20/2014 0821
400-92351-10 MW-7 Water 06/19/2014 1652 06/20/2014 0821
TestAmerica Pensacola Page 7 of 81
SAMPLE RESULTS
TestAmerica Pensacola
Page 8 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-8
Client Matrix:
400-92351-1
Water
Date Sampled: 06/19/2014 0710
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1434
06/24/2014 1434
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241414.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
31 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
4.0 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
9.6 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
0.95 J 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
8.0 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 9 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-8
Client Matrix:
400-92351-1
Water
Date Sampled: 06/19/2014 0710
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1434
06/24/2014 1434
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241414.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
1.3 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
65 5.01.6m-Xylene & p-Xylene
8.4 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
1.9 1.00.69N-Propylbenzene
43 5.00.60o-Xylene
0.91 J 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
1.0 1.00.58Tetrachloroethene
3.2 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
110 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
97 78 - 1184-Bromofluorobenzene
100 81 - 121Dibromofluoromethane
98 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 10 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-11
Client Matrix:
400-92351-2
Water
Date Sampled: 06/19/2014 0750
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1459
06/24/2014 1459
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241415.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
0.94 J 1.00.60Chloroform
<0.83 1.00.83Chloromethane
7.3 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 11 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-11
Client Matrix:
400-92351-2
Water
Date Sampled: 06/19/2014 0750
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1459
06/24/2014 1459
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241415.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
9.4 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
2.1 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
100 78 - 1184-Bromofluorobenzene
103 81 - 121Dibromofluoromethane
99 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 12 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-1W
Client Matrix:
400-92351-3
Water
Date Sampled: 06/19/2014 0830
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1523
06/24/2014 1523
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241416.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
7.6 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 13 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-1W
Client Matrix:
400-92351-3
Water
Date Sampled: 06/19/2014 0830
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1523
06/24/2014 1523
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241416.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
2.3 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
98 78 - 1184-Bromofluorobenzene
101 81 - 121Dibromofluoromethane
97 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 14 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-2W
Client Matrix:
400-92351-4
Water
Date Sampled: 06/19/2014 0930
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1548
06/24/2014 1548
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241417.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
2.5 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 15 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-2W
Client Matrix:
400-92351-4
Water
Date Sampled: 06/19/2014 0930
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1548
06/24/2014 1548
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241417.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
17 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
101 78 - 1184-Bromofluorobenzene
101 81 - 121Dibromofluoromethane
98 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 16 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-3W
Client Matrix:
400-92351-5
Water
Date Sampled: 06/19/2014 1044
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1613
06/24/2014 1613
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241418.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
2.2 1.00.60Chloroform
<0.83 1.00.83Chloromethane
12 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 17 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-3W
Client Matrix:
400-92351-5
Water
Date Sampled: 06/19/2014 1044
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1613
06/24/2014 1613
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241418.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
180 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
5.4 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
101 78 - 1184-Bromofluorobenzene
99 81 - 121Dibromofluoromethane
99 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 18 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-4W
Client Matrix:
400-92351-6
Water
Date Sampled: 06/19/2014 1151
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1059
06/24/2014 1059
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241406.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
<0.60 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 19 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-4W
Client Matrix:
400-92351-6
Water
Date Sampled: 06/19/2014 1151
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1059
06/24/2014 1059
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241406.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
3.8 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
99 78 - 1184-Bromofluorobenzene
100 81 - 121Dibromofluoromethane
99 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 20 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-5W
Client Matrix:
400-92351-7
Water
Date Sampled: 06/19/2014 1300
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1203
06/24/2014 1203
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241408.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
6.4 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
<0.60 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 21 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-5W
Client Matrix:
400-92351-7
Water
Date Sampled: 06/19/2014 1300
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1203
06/24/2014 1203
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241408.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
58 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
99 78 - 1184-Bromofluorobenzene
101 81 - 121Dibromofluoromethane
97 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 22 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-6W
Client Matrix:
400-92351-8
Water
Date Sampled: 06/19/2014 1422
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1731
06/24/2014 1731
10
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241419.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<5.2 105.21,1,1,2-Tetrachloroethane
<5.0 105.01,1,1-Trichloroethane
<5.0 105.01,1,2,2-Tetrachloroethane
<5.0 105.01,1,2-Trichloroethane
<5.0 105.01,1-Dichloroethane
<5.0 105.01,1-Dichloroethene
<5.0 105.01,1-Dichloropropene
<7.0 107.01,2,3-Trichlorobenzene
<8.4 108.41,2,3-Trichloropropane
<8.2 108.21,2,4-Trichlorobenzene
<8.2 108.21,2,4-Trimethylbenzene
<15 10151,2-Dibromo-3-Chloropropane
<5.0 105.01,2-Dichlorobenzene
<5.0 105.01,2-Dichloroethane
<5.0 105.01,2-Dichloropropane
<5.6 105.61,3,5-Trimethylbenzene
<5.4 105.41,3-Dichlorobenzene
<5.0 105.01,3-Dichloropropane
<6.4 106.41,4-Dichlorobenzene
<5.0 105.02,2-Dichloropropane
<5.7 105.72-Chlorotoluene
<31 200312-Hexanone
<5.6 105.64-Chlorotoluene
<100 200100Acetone
<3.4 103.4Benzene
<5.4 105.4Bromobenzene
<5.2 105.2Bromochloromethane
<5.0 105.0Bromodichloromethane
<7.1 107.1Bromoform
<9.8 109.8Bromomethane
<5.0 105.0Carbon disulfide
<5.0 105.0Carbon tetrachloride
<5.0 105.0Chlorobenzene
<7.6 107.6Chloroethane
<6.0 106.0Chloroform
<8.3 108.3Chloromethane
<5.0 105.0cis-1,2-Dichloroethene
<5.0 105.0cis-1,3-Dichloropropene
<5.0 105.0Dibromochloromethane
<5.9 105.9Dibromomethane
<8.5 108.5Dichlorodifluoromethane
<5.0 105.0Ethylbenzene
<5.0 105.0Ethylene Dibromide
<9.0 109.0Hexachlorobutadiene
<6.8 106.8Iodomethane
<7.0 107.0Isopropyl ether
TestAmerica Pensacola Page 23 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-6W
Client Matrix:
400-92351-8
Water
Date Sampled: 06/19/2014 1422
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1731
06/24/2014 1731
10
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241419.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<5.3 105.3Isopropylbenzene
<26 20026Methyl Ethyl Ketone
<18 20018methyl isobutyl ketone
<7.4 107.4Methyl tert-butyl ether
<30 5030Methylene Chloride
<16 5016m-Xylene & p-Xylene
<10 1010Naphthalene
<7.6 107.6n-Butylbenzene
<6.9 106.9N-Propylbenzene
<6.0 506.0o-Xylene
<7.1 107.1p-Cymene
<7.0 107.0sec-Butylbenzene
<10 1010Styrene
<6.3 106.3tert-Butylbenzene
1500 105.8Tetrachloroethene
<7.0 107.0Toluene
<5.0 105.0trans-1,2-Dichloroethene
<5.0 105.0trans-1,3-Dichloropropene
<5.0 105.0Trichloroethene
<5.2 105.2Trichlorofluoromethane
<20 5020Vinyl acetate
<5.0 105.0Vinyl chloride
<16 10016Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
101 78 - 1184-Bromofluorobenzene
98 81 - 121Dibromofluoromethane
98 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 24 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-7W
Client Matrix:
400-92351-9
Water
Date Sampled: 06/19/2014 1510
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1344
06/24/2014 1344
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241412.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
29 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 25 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-7W
Client Matrix:
400-92351-9
Water
Date Sampled: 06/19/2014 1510
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1344
06/24/2014 1344
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241412.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
<0.58 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
96 78 - 1184-Bromofluorobenzene
103 81 - 121Dibromofluoromethane
96 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 26 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-7
Client Matrix:
400-92351-10
Water
Date Sampled: 06/19/2014 1652
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1409
06/24/2014 1409
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241413.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
<0.60 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
<0.70 1.00.70Isopropyl ether
TestAmerica Pensacola Page 27 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-7
Client Matrix:
400-92351-10
Water
Date Sampled: 06/19/2014 1652
Date Received: 06/20/2014 0821
SM 6200B SM 6200B
Dilution:
06/24/2014 1409
06/24/2014 1409
1.0
SM 6200B
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
06241413.D
5 mL
5 mL
5030B
CH_TAN
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221257
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL MQL
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
2.0 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
98 78 - 1184-Bromofluorobenzene
103 81 - 121Dibromofluoromethane
96 80 - 120Toluene-d8 (Surr)
TestAmerica Pensacola Page 28 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-11
Client Matrix:
400-92351-2
Water
Date Sampled: 06/19/2014 0750
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1614
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-2.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.38 9.50.381,1'-Biphenyl
<0.50 9.50.501,2,4,5-Tetrachlorobenzene
<0.50 9.50.501,2,4-Trichlorobenzene
<0.54 9.50.541,2-Dichlorobenzene
<0.45 9.50.451,3-Dichlorobenzene
<0.95 9.50.951,3-Dinitrobenzene
<0.50 9.50.501,4-Dichlorobenzene
<0.95 9.50.951,4-Dioxane
<0.48 9.50.481-Methylnaphthalene
<0.61 9.50.612,3,4,6-Tetrachlorophenol
<3.5 9.53.52,4,5-Trichlorophenol
<3.3 9.53.32,4,6-Trichlorophenol
<2.9 9.52.92,4-Dichlorophenol
<3.3 9.53.32,4-Dimethylphenol
<3.2 293.22,4-Dinitrophenol
<1.8 9.51.82,4-Dinitrotoluene
<1.8 9.51.82,6-Dinitrotoluene
<0.50 9.50.502-Chloronaphthalene
<2.1 9.52.12-Chlorophenol
<0.51 9.50.512-Methylnaphthalene
<1.7 9.51.72-Methylphenol
<2.1 9.52.12-Nitroaniline
<0.62 9.50.622-Nitrophenol
<0.99 190.993 & 4 Methylphenol
<1.9 9.51.94,6-Dinitro-2-methylphenol
<0.30 9.50.304-Bromophenyl phenyl ether
<3.6 9.53.64-Chloro-3-methylphenol
<1.9 9.51.94-Chlorophenyl phenyl ether
<2.0 9.52.04-Nitrophenol
<0.44 9.50.44Acenaphthene
<0.53 9.50.53Acenaphthylene
<0.59 9.50.59Acetophenone
<0.40 9.50.40Anthracene
<0.95 9.50.95Azobenzene
<1.2 *9.51.2Benzaldehyde
<0.32 9.50.32Benzo[a]anthracene
<0.41 9.50.41Benzo[a]pyrene
<0.36 9.50.36Benzo[b]fluoranthene
<1.0 9.51.0Benzo[g,h,i]perylene
<0.51 9.50.51Benzo[k]fluoranthene
<7.0 297.0Benzoic acid
<1.9 9.51.9Benzyl alcohol
<0.77 9.50.77bis (2-chloroisopropyl) ether
<0.66 9.50.66Bis(2-chloroethoxy)methane
<0.70 9.50.70Bis(2-chloroethyl)ether
<2.2 9.52.2Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 29 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-11
Client Matrix:
400-92351-2
Water
Date Sampled: 06/19/2014 0750
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1614
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-2.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.66 9.50.66Butyl benzyl phthalate
<0.83 9.50.83Carbazole
<0.47 9.50.47Chrysene
<1.1 9.51.1Dibenz(a,h)anthracene
<0.50 9.50.50Dibenzofuran
<0.67 9.50.67Diethyl phthalate
<0.57 9.50.57Dimethyl phthalate
<2.6 9.52.6Di-n-butyl phthalate
<0.42 9.50.42Di-n-octyl phthalate
<0.73 9.50.73Fluoranthene
<0.53 9.50.53Fluorene
<0.24 9.50.24Hexachlorobenzene
<3.4 9.53.4Hexachlorobutadiene
<2.5 192.5Hexachlorocyclopentadiene
<4.0 9.54.0Hexachloroethane
<0.95 9.50.95Hexadecane
<0.95 9.50.95Indene
<0.97 9.50.97Indeno[1,2,3-cd]pyrene
<0.54 9.50.54Isophorone
<0.60 9.50.60Naphthalene
<0.95 9.50.95n-Decane
<0.52 9.50.52Nitrobenzene
<3.3 9.53.3N-Nitrosodimethylamine
<3.1 9.53.1N-Nitrosodi-n-propylamine
<0.45 9.50.45N-Nitrosodiphenylamine
<0.95 9.50.95n-Octadecane
<1.7 191.7Pentachlorophenol
<0.39 9.50.39Phenanthrene
<2.5 9.52.5Phenol
<1.0 9.51.0Pyrene
<3.0 9.53.0Pyridine
<0.55 9.50.55Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
100 15 - 1352,4,6-Tribromophenol (Surr)
111 34 - 1202-Fluorobiphenyl
71 10 - 1202-Fluorophenol (Surr)
116 27 - 120Nitrobenzene-d5 (Surr)
100 10 - 120Phenol-d5 (Surr)
118 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 30 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-1W
Client Matrix:
400-92351-3
Water
Date Sampled: 06/19/2014 0830
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1702
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-3.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.38 9.50.381,1'-Biphenyl
<0.50 9.50.501,2,4,5-Tetrachlorobenzene
<0.50 9.50.501,2,4-Trichlorobenzene
<0.54 9.50.541,2-Dichlorobenzene
<0.45 9.50.451,3-Dichlorobenzene
<0.95 9.50.951,3-Dinitrobenzene
<0.50 9.50.501,4-Dichlorobenzene
<0.95 9.50.951,4-Dioxane
<0.48 9.50.481-Methylnaphthalene
<0.61 9.50.612,3,4,6-Tetrachlorophenol
<3.5 9.53.52,4,5-Trichlorophenol
<3.3 9.53.32,4,6-Trichlorophenol
<2.9 9.52.92,4-Dichlorophenol
<3.3 9.53.32,4-Dimethylphenol
<3.2 293.22,4-Dinitrophenol
<1.8 9.51.82,4-Dinitrotoluene
<1.8 9.51.82,6-Dinitrotoluene
<0.50 9.50.502-Chloronaphthalene
<2.1 9.52.12-Chlorophenol
<0.51 9.50.512-Methylnaphthalene
<1.7 9.51.72-Methylphenol
<2.1 9.52.12-Nitroaniline
<0.62 9.50.622-Nitrophenol
<0.99 190.993 & 4 Methylphenol
<1.9 9.51.94,6-Dinitro-2-methylphenol
<0.30 9.50.304-Bromophenyl phenyl ether
<3.6 9.53.64-Chloro-3-methylphenol
<1.9 9.51.94-Chlorophenyl phenyl ether
<2.0 9.52.04-Nitrophenol
<0.44 9.50.44Acenaphthene
<0.53 9.50.53Acenaphthylene
<0.59 9.50.59Acetophenone
<0.40 9.50.40Anthracene
<0.95 9.50.95Azobenzene
<1.2 *9.51.2Benzaldehyde
<0.32 9.50.32Benzo[a]anthracene
<0.41 9.50.41Benzo[a]pyrene
<0.36 9.50.36Benzo[b]fluoranthene
<1.0 9.51.0Benzo[g,h,i]perylene
<0.51 9.50.51Benzo[k]fluoranthene
<7.0 297.0Benzoic acid
<1.9 9.51.9Benzyl alcohol
<0.77 9.50.77bis (2-chloroisopropyl) ether
<0.66 9.50.66Bis(2-chloroethoxy)methane
<0.70 9.50.70Bis(2-chloroethyl)ether
<2.2 9.52.2Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 31 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-1W
Client Matrix:
400-92351-3
Water
Date Sampled: 06/19/2014 0830
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1702
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-3.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.66 9.50.66Butyl benzyl phthalate
<0.83 9.50.83Carbazole
<0.47 9.50.47Chrysene
<1.1 9.51.1Dibenz(a,h)anthracene
<0.50 9.50.50Dibenzofuran
0.77 J 9.50.67Diethyl phthalate
<0.57 9.50.57Dimethyl phthalate
<2.6 9.52.6Di-n-butyl phthalate
<0.42 9.50.42Di-n-octyl phthalate
<0.73 9.50.73Fluoranthene
<0.53 9.50.53Fluorene
<0.24 9.50.24Hexachlorobenzene
<3.4 9.53.4Hexachlorobutadiene
<2.5 192.5Hexachlorocyclopentadiene
<4.0 9.54.0Hexachloroethane
<0.95 9.50.95Hexadecane
<0.95 9.50.95Indene
<0.97 9.50.97Indeno[1,2,3-cd]pyrene
<0.54 9.50.54Isophorone
<0.60 9.50.60Naphthalene
<0.95 9.50.95n-Decane
<0.52 9.50.52Nitrobenzene
<3.3 9.53.3N-Nitrosodimethylamine
<3.1 9.53.1N-Nitrosodi-n-propylamine
<0.45 9.50.45N-Nitrosodiphenylamine
<0.95 9.50.95n-Octadecane
<1.7 191.7Pentachlorophenol
<0.39 9.50.39Phenanthrene
<2.5 9.52.5Phenol
<1.0 9.51.0Pyrene
<3.0 9.53.0Pyridine
<0.55 9.50.55Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
95 15 - 1352,4,6-Tribromophenol (Surr)
89 34 - 1202-Fluorobiphenyl
51 10 - 1202-Fluorophenol (Surr)
94 27 - 120Nitrobenzene-d5 (Surr)
78 10 - 120Phenol-d5 (Surr)
94 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 32 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-2W
Client Matrix:
400-92351-4
Water
Date Sampled: 06/19/2014 0930
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1741
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-4.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.38 9.50.381,1'-Biphenyl
<0.50 9.50.501,2,4,5-Tetrachlorobenzene
<0.50 9.50.501,2,4-Trichlorobenzene
<0.54 9.50.541,2-Dichlorobenzene
<0.45 9.50.451,3-Dichlorobenzene
<0.95 9.50.951,3-Dinitrobenzene
<0.50 9.50.501,4-Dichlorobenzene
<0.95 9.50.951,4-Dioxane
<0.48 9.50.481-Methylnaphthalene
<0.61 9.50.612,3,4,6-Tetrachlorophenol
<3.5 9.53.52,4,5-Trichlorophenol
<3.3 9.53.32,4,6-Trichlorophenol
<2.9 9.52.92,4-Dichlorophenol
<3.3 9.53.32,4-Dimethylphenol
<3.2 293.22,4-Dinitrophenol
<1.8 9.51.82,4-Dinitrotoluene
<1.8 9.51.82,6-Dinitrotoluene
<0.50 9.50.502-Chloronaphthalene
<2.1 9.52.12-Chlorophenol
<0.51 9.50.512-Methylnaphthalene
<1.7 9.51.72-Methylphenol
<2.1 9.52.12-Nitroaniline
<0.62 9.50.622-Nitrophenol
<0.99 190.993 & 4 Methylphenol
<1.9 9.51.94,6-Dinitro-2-methylphenol
<0.30 9.50.304-Bromophenyl phenyl ether
<3.6 9.53.64-Chloro-3-methylphenol
<1.9 9.51.94-Chlorophenyl phenyl ether
<2.0 9.52.04-Nitrophenol
<0.44 9.50.44Acenaphthene
<0.53 9.50.53Acenaphthylene
<0.59 9.50.59Acetophenone
<0.40 9.50.40Anthracene
<0.95 9.50.95Azobenzene
<1.2 *9.51.2Benzaldehyde
<0.32 9.50.32Benzo[a]anthracene
<0.41 9.50.41Benzo[a]pyrene
<0.36 9.50.36Benzo[b]fluoranthene
<1.0 9.51.0Benzo[g,h,i]perylene
<0.51 9.50.51Benzo[k]fluoranthene
<7.0 297.0Benzoic acid
<1.9 9.51.9Benzyl alcohol
<0.77 9.50.77bis (2-chloroisopropyl) ether
<0.66 9.50.66Bis(2-chloroethoxy)methane
<0.70 9.50.70Bis(2-chloroethyl)ether
<2.2 9.52.2Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 33 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-2W
Client Matrix:
400-92351-4
Water
Date Sampled: 06/19/2014 0930
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1741
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-4.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.66 9.50.66Butyl benzyl phthalate
<0.83 9.50.83Carbazole
<0.47 9.50.47Chrysene
<1.1 9.51.1Dibenz(a,h)anthracene
<0.50 9.50.50Dibenzofuran
0.79 J 9.50.67Diethyl phthalate
<0.57 9.50.57Dimethyl phthalate
<2.6 9.52.6Di-n-butyl phthalate
<0.42 9.50.42Di-n-octyl phthalate
<0.73 9.50.73Fluoranthene
<0.53 9.50.53Fluorene
<0.24 9.50.24Hexachlorobenzene
<3.4 9.53.4Hexachlorobutadiene
<2.5 192.5Hexachlorocyclopentadiene
<4.0 9.54.0Hexachloroethane
<0.95 9.50.95Hexadecane
<0.95 9.50.95Indene
<0.97 9.50.97Indeno[1,2,3-cd]pyrene
<0.54 9.50.54Isophorone
<0.60 9.50.60Naphthalene
<0.95 9.50.95n-Decane
<0.52 9.50.52Nitrobenzene
<3.3 9.53.3N-Nitrosodimethylamine
<3.1 9.53.1N-Nitrosodi-n-propylamine
<0.45 9.50.45N-Nitrosodiphenylamine
<0.95 9.50.95n-Octadecane
<1.7 191.7Pentachlorophenol
<0.39 9.50.39Phenanthrene
<2.5 9.52.5Phenol
<1.0 9.51.0Pyrene
<3.0 9.53.0Pyridine
<0.55 9.50.55Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
106 15 - 1352,4,6-Tribromophenol (Surr)
106 34 - 1202-Fluorobiphenyl
56 10 - 1202-Fluorophenol (Surr)
104 27 - 120Nitrobenzene-d5 (Surr)
88 10 - 120Phenol-d5 (Surr)
103 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 34 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-3W
Client Matrix:
400-92351-5
Water
Date Sampled: 06/19/2014 1044
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1819
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-5.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.38 9.50.381,1'-Biphenyl
<0.50 9.50.501,2,4,5-Tetrachlorobenzene
<0.50 9.50.501,2,4-Trichlorobenzene
<0.54 9.50.541,2-Dichlorobenzene
<0.45 9.50.451,3-Dichlorobenzene
<0.95 9.50.951,3-Dinitrobenzene
<0.50 9.50.501,4-Dichlorobenzene
<0.95 9.50.951,4-Dioxane
<0.48 9.50.481-Methylnaphthalene
<0.61 9.50.612,3,4,6-Tetrachlorophenol
<3.5 9.53.52,4,5-Trichlorophenol
<3.3 9.53.32,4,6-Trichlorophenol
<2.9 9.52.92,4-Dichlorophenol
<3.3 9.53.32,4-Dimethylphenol
<3.2 293.22,4-Dinitrophenol
<1.8 9.51.82,4-Dinitrotoluene
<1.8 9.51.82,6-Dinitrotoluene
<0.50 9.50.502-Chloronaphthalene
<2.1 9.52.12-Chlorophenol
<0.51 9.50.512-Methylnaphthalene
<1.7 9.51.72-Methylphenol
<2.1 9.52.12-Nitroaniline
<0.62 9.50.622-Nitrophenol
<0.99 190.993 & 4 Methylphenol
<1.9 9.51.94,6-Dinitro-2-methylphenol
<0.30 9.50.304-Bromophenyl phenyl ether
<3.6 9.53.64-Chloro-3-methylphenol
<1.9 9.51.94-Chlorophenyl phenyl ether
<2.0 9.52.04-Nitrophenol
<0.44 9.50.44Acenaphthene
<0.53 9.50.53Acenaphthylene
<0.59 9.50.59Acetophenone
<0.40 9.50.40Anthracene
<0.95 9.50.95Azobenzene
<1.2 *9.51.2Benzaldehyde
<0.32 9.50.32Benzo[a]anthracene
<0.41 9.50.41Benzo[a]pyrene
<0.36 9.50.36Benzo[b]fluoranthene
<1.0 9.51.0Benzo[g,h,i]perylene
<0.51 9.50.51Benzo[k]fluoranthene
<7.0 297.0Benzoic acid
<1.9 9.51.9Benzyl alcohol
<0.77 9.50.77bis (2-chloroisopropyl) ether
<0.66 9.50.66Bis(2-chloroethoxy)methane
<0.70 9.50.70Bis(2-chloroethyl)ether
<2.2 9.52.2Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 35 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-3W
Client Matrix:
400-92351-5
Water
Date Sampled: 06/19/2014 1044
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1819
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-5.D
1050 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.66 9.50.66Butyl benzyl phthalate
<0.83 9.50.83Carbazole
<0.47 9.50.47Chrysene
<1.1 9.51.1Dibenz(a,h)anthracene
<0.50 9.50.50Dibenzofuran
0.71 J 9.50.67Diethyl phthalate
<0.57 9.50.57Dimethyl phthalate
<2.6 9.52.6Di-n-butyl phthalate
<0.42 9.50.42Di-n-octyl phthalate
<0.73 9.50.73Fluoranthene
<0.53 9.50.53Fluorene
<0.24 9.50.24Hexachlorobenzene
<3.4 9.53.4Hexachlorobutadiene
<2.5 192.5Hexachlorocyclopentadiene
<4.0 9.54.0Hexachloroethane
<0.95 9.50.95Hexadecane
<0.95 9.50.95Indene
<0.97 9.50.97Indeno[1,2,3-cd]pyrene
<0.54 9.50.54Isophorone
<0.60 9.50.60Naphthalene
<0.95 9.50.95n-Decane
<0.52 9.50.52Nitrobenzene
<3.3 9.53.3N-Nitrosodimethylamine
<3.1 9.53.1N-Nitrosodi-n-propylamine
<0.45 9.50.45N-Nitrosodiphenylamine
<0.95 9.50.95n-Octadecane
<1.7 191.7Pentachlorophenol
<0.39 9.50.39Phenanthrene
<2.5 9.52.5Phenol
<1.0 9.51.0Pyrene
<3.0 9.53.0Pyridine
<0.55 9.50.55Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
96 15 - 1352,4,6-Tribromophenol (Surr)
99 34 - 1202-Fluorobiphenyl
36 10 - 1202-Fluorophenol (Surr)
96 27 - 120Nitrobenzene-d5 (Surr)
73 10 - 120Phenol-d5 (Surr)
95 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 36 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-4W
Client Matrix:
400-92351-6
Water
Date Sampled: 06/19/2014 1151
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1859
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-6.D
1030 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.39 9.70.391,1'-Biphenyl
<0.50 9.70.501,2,4,5-Tetrachlorobenzene
<0.51 9.70.511,2,4-Trichlorobenzene
<0.55 9.70.551,2-Dichlorobenzene
<0.46 9.70.461,3-Dichlorobenzene
<0.97 9.70.971,3-Dinitrobenzene
<0.50 9.70.501,4-Dichlorobenzene
<0.97 9.70.971,4-Dioxane
<0.49 9.70.491-Methylnaphthalene
<0.62 9.70.622,3,4,6-Tetrachlorophenol
<3.6 9.73.62,4,5-Trichlorophenol
<3.4 9.73.42,4,6-Trichlorophenol
<2.9 9.72.92,4-Dichlorophenol
<3.4 9.73.42,4-Dimethylphenol
<3.3 293.32,4-Dinitrophenol
<1.8 9.71.82,4-Dinitrotoluene
<1.8 9.71.82,6-Dinitrotoluene
<0.50 9.70.502-Chloronaphthalene
<2.1 9.72.12-Chlorophenol
<0.52 9.70.522-Methylnaphthalene
<1.7 9.71.72-Methylphenol
<2.1 9.72.12-Nitroaniline
<0.63 9.70.632-Nitrophenol
<1.0 191.03 & 4 Methylphenol
<1.9 9.71.94,6-Dinitro-2-methylphenol
<0.31 9.70.314-Bromophenyl phenyl ether
<3.7 9.73.74-Chloro-3-methylphenol
<1.9 9.71.94-Chlorophenyl phenyl ether
<2.0 9.72.04-Nitrophenol
<0.45 9.70.45Acenaphthene
<0.54 9.70.54Acenaphthylene
<0.60 9.70.60Acetophenone
<0.41 9.70.41Anthracene
<0.97 9.70.97Azobenzene
<1.3 *9.71.3Benzaldehyde
<0.33 9.70.33Benzo[a]anthracene
<0.42 9.70.42Benzo[a]pyrene
<0.37 9.70.37Benzo[b]fluoranthene
<1.0 9.71.0Benzo[g,h,i]perylene
<0.52 9.70.52Benzo[k]fluoranthene
<7.1 297.1Benzoic acid
<1.9 9.71.9Benzyl alcohol
<0.79 9.70.79bis (2-chloroisopropyl) ether
<0.67 9.70.67Bis(2-chloroethoxy)methane
<0.72 9.70.72Bis(2-chloroethyl)ether
<2.2 9.72.2Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 37 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-4W
Client Matrix:
400-92351-6
Water
Date Sampled: 06/19/2014 1151
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1859
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-6.D
1030 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.67 9.70.67Butyl benzyl phthalate
<0.84 9.70.84Carbazole
<0.48 9.70.48Chrysene
<1.1 9.71.1Dibenz(a,h)anthracene
<0.50 9.70.50Dibenzofuran
<0.68 9.70.68Diethyl phthalate
<0.58 9.70.58Dimethyl phthalate
<2.6 9.72.6Di-n-butyl phthalate
<0.43 9.70.43Di-n-octyl phthalate
<0.75 9.70.75Fluoranthene
<0.54 9.70.54Fluorene
<0.24 9.70.24Hexachlorobenzene
<3.5 9.73.5Hexachlorobutadiene
<2.5 192.5Hexachlorocyclopentadiene
<4.1 9.74.1Hexachloroethane
<0.97 9.70.97Hexadecane
<0.97 9.70.97Indene
<0.99 9.70.99Indeno[1,2,3-cd]pyrene
<0.55 9.70.55Isophorone
<0.61 9.70.61Naphthalene
<0.97 9.70.97n-Decane
<0.53 9.70.53Nitrobenzene
<3.4 9.73.4N-Nitrosodimethylamine
<3.2 9.73.2N-Nitrosodi-n-propylamine
<0.46 9.70.46N-Nitrosodiphenylamine
<0.97 9.70.97n-Octadecane
<1.8 191.8Pentachlorophenol
<0.40 9.70.40Phenanthrene
<2.5 9.72.5Phenol
<1.1 9.71.1Pyrene
<3.1 9.73.1Pyridine
<0.56 9.70.56Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
111 15 - 1352,4,6-Tribromophenol (Surr)
109 34 - 1202-Fluorobiphenyl
72 10 - 1202-Fluorophenol (Surr)
103 27 - 120Nitrobenzene-d5 (Surr)
85 10 - 120Phenol-d5 (Surr)
120 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 38 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-5W
Client Matrix:
400-92351-7
Water
Date Sampled: 06/19/2014 1300
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1938
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-7.D
1030 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.39 9.70.391,1'-Biphenyl
<0.50 9.70.501,2,4,5-Tetrachlorobenzene
<0.51 9.70.511,2,4-Trichlorobenzene
<0.55 9.70.551,2-Dichlorobenzene
<0.46 9.70.461,3-Dichlorobenzene
<0.97 9.70.971,3-Dinitrobenzene
<0.50 9.70.501,4-Dichlorobenzene
<0.97 9.70.971,4-Dioxane
<0.49 9.70.491-Methylnaphthalene
<0.62 9.70.622,3,4,6-Tetrachlorophenol
<3.6 9.73.62,4,5-Trichlorophenol
<3.4 9.73.42,4,6-Trichlorophenol
<2.9 9.72.92,4-Dichlorophenol
<3.4 9.73.42,4-Dimethylphenol
<3.3 293.32,4-Dinitrophenol
<1.8 9.71.82,4-Dinitrotoluene
<1.8 9.71.82,6-Dinitrotoluene
<0.50 9.70.502-Chloronaphthalene
<2.1 9.72.12-Chlorophenol
<0.52 9.70.522-Methylnaphthalene
<1.7 9.71.72-Methylphenol
<2.1 9.72.12-Nitroaniline
<0.63 9.70.632-Nitrophenol
<1.0 191.03 & 4 Methylphenol
<1.9 9.71.94,6-Dinitro-2-methylphenol
<0.31 9.70.314-Bromophenyl phenyl ether
<3.7 9.73.74-Chloro-3-methylphenol
<1.9 9.71.94-Chlorophenyl phenyl ether
<2.0 9.72.04-Nitrophenol
<0.45 9.70.45Acenaphthene
<0.54 9.70.54Acenaphthylene
<0.60 9.70.60Acetophenone
<0.41 9.70.41Anthracene
<0.97 9.70.97Azobenzene
<1.3 *9.71.3Benzaldehyde
<0.33 9.70.33Benzo[a]anthracene
<0.42 9.70.42Benzo[a]pyrene
<0.37 9.70.37Benzo[b]fluoranthene
<1.0 9.71.0Benzo[g,h,i]perylene
<0.52 9.70.52Benzo[k]fluoranthene
<7.1 297.1Benzoic acid
<1.9 9.71.9Benzyl alcohol
<0.79 9.70.79bis (2-chloroisopropyl) ether
<0.67 9.70.67Bis(2-chloroethoxy)methane
<0.72 9.70.72Bis(2-chloroethyl)ether
<2.2 9.72.2Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 39 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-5W
Client Matrix:
400-92351-7
Water
Date Sampled: 06/19/2014 1300
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 1938
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-7.D
1030 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.67 9.70.67Butyl benzyl phthalate
<0.84 9.70.84Carbazole
<0.48 9.70.48Chrysene
<1.1 9.71.1Dibenz(a,h)anthracene
<0.50 9.70.50Dibenzofuran
<0.68 9.70.68Diethyl phthalate
<0.58 9.70.58Dimethyl phthalate
<2.6 9.72.6Di-n-butyl phthalate
<0.43 9.70.43Di-n-octyl phthalate
<0.75 9.70.75Fluoranthene
<0.54 9.70.54Fluorene
<0.24 9.70.24Hexachlorobenzene
<3.5 9.73.5Hexachlorobutadiene
<2.5 192.5Hexachlorocyclopentadiene
<4.1 9.74.1Hexachloroethane
<0.97 9.70.97Hexadecane
<0.97 9.70.97Indene
<0.99 9.70.99Indeno[1,2,3-cd]pyrene
<0.55 9.70.55Isophorone
<0.61 9.70.61Naphthalene
<0.97 9.70.97n-Decane
<0.53 9.70.53Nitrobenzene
<3.4 9.73.4N-Nitrosodimethylamine
<3.2 9.73.2N-Nitrosodi-n-propylamine
<0.46 9.70.46N-Nitrosodiphenylamine
<0.97 9.70.97n-Octadecane
<1.8 191.8Pentachlorophenol
<0.40 9.70.40Phenanthrene
<2.5 9.72.5Phenol
<1.1 9.71.1Pyrene
<3.1 9.73.1Pyridine
<0.56 9.70.56Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
100 15 - 1352,4,6-Tribromophenol (Surr)
96 34 - 1202-Fluorobiphenyl
66 10 - 1202-Fluorophenol (Surr)
97 27 - 120Nitrobenzene-d5 (Surr)
87 10 - 120Phenol-d5 (Surr)
99 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 40 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-6W
Client Matrix:
400-92351-8
Water
Date Sampled: 06/19/2014 1422
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 2017
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-8.D
1000 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.40 100.401,1'-Biphenyl
<0.52 100.521,2,4,5-Tetrachlorobenzene
<0.53 100.531,2,4-Trichlorobenzene
<0.57 100.571,2-Dichlorobenzene
<0.47 100.471,3-Dichlorobenzene
<1.0 101.01,3-Dinitrobenzene
<0.52 100.521,4-Dichlorobenzene
<1.0 101.01,4-Dioxane
<0.50 100.501-Methylnaphthalene
<0.64 100.642,3,4,6-Tetrachlorophenol
<3.7 103.72,4,5-Trichlorophenol
<3.5 103.52,4,6-Trichlorophenol
<3.0 103.02,4-Dichlorophenol
<3.5 103.52,4-Dimethylphenol
<3.4 303.42,4-Dinitrophenol
<1.9 101.92,4-Dinitrotoluene
<1.9 101.92,6-Dinitrotoluene
<0.52 100.522-Chloronaphthalene
<2.2 102.22-Chlorophenol
<0.54 100.542-Methylnaphthalene
<1.8 101.82-Methylphenol
<2.2 102.22-Nitroaniline
<0.65 100.652-Nitrophenol
<1.0 201.03 & 4 Methylphenol
<2.0 102.04,6-Dinitro-2-methylphenol
<0.32 100.324-Bromophenyl phenyl ether
<3.8 103.84-Chloro-3-methylphenol
<2.0 102.04-Chlorophenyl phenyl ether
<2.1 102.14-Nitrophenol
<0.46 100.46Acenaphthene
<0.56 100.56Acenaphthylene
<0.62 100.62Acetophenone
<0.42 100.42Anthracene
<1.0 101.0Azobenzene
<1.3 *101.3Benzaldehyde
<0.34 100.34Benzo[a]anthracene
<0.43 100.43Benzo[a]pyrene
<0.38 100.38Benzo[b]fluoranthene
<1.1 101.1Benzo[g,h,i]perylene
<0.54 100.54Benzo[k]fluoranthene
<7.3 307.3Benzoic acid
<2.0 102.0Benzyl alcohol
<0.81 100.81bis (2-chloroisopropyl) ether
<0.69 100.69Bis(2-chloroethoxy)methane
<0.74 100.74Bis(2-chloroethyl)ether
<2.3 102.3Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 41 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-6W
Client Matrix:
400-92351-8
Water
Date Sampled: 06/19/2014 1422
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 2017
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-8.D
1000 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.69 100.69Butyl benzyl phthalate
<0.87 100.87Carbazole
<0.49 100.49Chrysene
<1.2 101.2Dibenz(a,h)anthracene
<0.52 100.52Dibenzofuran
<0.70 100.70Diethyl phthalate
<0.60 100.60Dimethyl phthalate
<2.7 102.7Di-n-butyl phthalate
<0.44 100.44Di-n-octyl phthalate
<0.77 100.77Fluoranthene
<0.56 100.56Fluorene
<0.25 100.25Hexachlorobenzene
<3.6 103.6Hexachlorobutadiene
<2.6 202.6Hexachlorocyclopentadiene
<4.2 104.2Hexachloroethane
<1.0 101.0Hexadecane
<1.0 101.0Indene
<1.0 101.0Indeno[1,2,3-cd]pyrene
<0.57 100.57Isophorone
<0.63 100.63Naphthalene
<1.0 101.0n-Decane
<0.55 100.55Nitrobenzene
<3.5 103.5N-Nitrosodimethylamine
<3.3 103.3N-Nitrosodi-n-propylamine
<0.47 100.47N-Nitrosodiphenylamine
<1.0 101.0n-Octadecane
<1.8 201.8Pentachlorophenol
<0.41 100.41Phenanthrene
<2.6 102.6Phenol
<1.1 101.1Pyrene
<3.2 103.2Pyridine
<0.58 100.58Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
85 15 - 1352,4,6-Tribromophenol (Surr)
99 34 - 1202-Fluorobiphenyl
73 10 - 1202-Fluorophenol (Surr)
95 27 - 120Nitrobenzene-d5 (Surr)
84 10 - 120Phenol-d5 (Surr)
110 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 42 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-7
Client Matrix:
400-92351-10
Water
Date Sampled: 06/19/2014 1652
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 2055
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-10.D
1000 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.40 100.401,1'-Biphenyl
<0.52 100.521,2,4,5-Tetrachlorobenzene
<0.53 100.531,2,4-Trichlorobenzene
<0.57 100.571,2-Dichlorobenzene
<0.47 100.471,3-Dichlorobenzene
<1.0 101.01,3-Dinitrobenzene
<0.52 100.521,4-Dichlorobenzene
<1.0 101.01,4-Dioxane
<0.50 100.501-Methylnaphthalene
<0.64 100.642,3,4,6-Tetrachlorophenol
<3.7 103.72,4,5-Trichlorophenol
<3.5 103.52,4,6-Trichlorophenol
<3.0 103.02,4-Dichlorophenol
<3.5 103.52,4-Dimethylphenol
<3.4 303.42,4-Dinitrophenol
<1.9 101.92,4-Dinitrotoluene
<1.9 101.92,6-Dinitrotoluene
<0.52 100.522-Chloronaphthalene
<2.2 102.22-Chlorophenol
<0.54 100.542-Methylnaphthalene
<1.8 101.82-Methylphenol
<2.2 102.22-Nitroaniline
<0.65 100.652-Nitrophenol
<1.0 201.03 & 4 Methylphenol
<2.0 102.04,6-Dinitro-2-methylphenol
<0.32 100.324-Bromophenyl phenyl ether
<3.8 103.84-Chloro-3-methylphenol
<2.0 102.04-Chlorophenyl phenyl ether
<2.1 102.14-Nitrophenol
<0.46 100.46Acenaphthene
<0.56 100.56Acenaphthylene
<0.62 100.62Acetophenone
<0.42 100.42Anthracene
<1.0 101.0Azobenzene
<1.3 *101.3Benzaldehyde
<0.34 100.34Benzo[a]anthracene
<0.43 100.43Benzo[a]pyrene
<0.38 100.38Benzo[b]fluoranthene
<1.1 101.1Benzo[g,h,i]perylene
<0.54 100.54Benzo[k]fluoranthene
<7.3 307.3Benzoic acid
<2.0 102.0Benzyl alcohol
<0.81 100.81bis (2-chloroisopropyl) ether
<0.69 100.69Bis(2-chloroethoxy)methane
<0.74 100.74Bis(2-chloroethyl)ether
<2.3 102.3Bis(2-ethylhexyl) phthalate
TestAmerica Pensacola Page 43 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
MW-7
Client Matrix:
400-92351-10
Water
Date Sampled: 06/19/2014 1652
Date Received: 06/20/2014 0821
8270D Semivolatile Organic Compounds (GC/MS)
Dilution:
06/20/2014 1340
06/24/2014 2055
1.0
8270D
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
400-92351-l-10.D
1000 mL
1.0 mL
1 uL
3520C
Pigpen
Analysis Date:
Prep Date:
Analysis Batch:
Prep Batch:
400-221174
400-220899
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<0.69 100.69Butyl benzyl phthalate
<0.87 100.87Carbazole
<0.49 100.49Chrysene
<1.2 101.2Dibenz(a,h)anthracene
<0.52 100.52Dibenzofuran
<0.70 100.70Diethyl phthalate
<0.60 100.60Dimethyl phthalate
<2.7 102.7Di-n-butyl phthalate
<0.44 100.44Di-n-octyl phthalate
<0.77 100.77Fluoranthene
<0.56 100.56Fluorene
<0.25 100.25Hexachlorobenzene
<3.6 103.6Hexachlorobutadiene
<2.6 202.6Hexachlorocyclopentadiene
<4.2 104.2Hexachloroethane
<1.0 101.0Hexadecane
<1.0 101.0Indene
<1.0 101.0Indeno[1,2,3-cd]pyrene
<0.57 100.57Isophorone
<0.63 100.63Naphthalene
<1.0 101.0n-Decane
<0.55 100.55Nitrobenzene
<3.5 103.5N-Nitrosodimethylamine
<3.3 103.3N-Nitrosodi-n-propylamine
<0.47 100.47N-Nitrosodiphenylamine
<1.0 101.0n-Octadecane
<1.8 201.8Pentachlorophenol
<0.41 100.41Phenanthrene
<2.6 102.6Phenol
<1.1 101.1Pyrene
<3.2 103.2Pyridine
<0.58 100.58Sulfolane
Surrogate %Rec Acceptance LimitsQualifier
115 15 - 1352,4,6-Tribromophenol (Surr)
120 34 - 1202-Fluorobiphenyl
90 10 - 1202-Fluorophenol (Surr)
113 27 - 120Nitrobenzene-d5 (Surr)
102 10 - 120Phenol-d5 (Surr)
117 53 - 125Terphenyl-d14 (Surr)
TestAmerica Pensacola Page 44 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-4W
Client Matrix:
400-92351-6
Water
Date Sampled: 06/19/2014 1151
Date Received: 06/20/2014 0821
8015C GRO by 8015C
Dilution:
8015C
5030B
1.0
06/21/2014 0237
06/21/2014 0237
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
5 mL
5 mL
5 mL
CH_JOAN
Analysis Date:
Prep Date:
Analysis Batch: 400-220858
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<47 10047Gasoline Range Organics (GRO)-C6-C10
Surrogate %Rec Acceptance LimitsQualifier
90 78 - 119a,a,a-Trifluorotoluene (fid)
TestAmerica Pensacola Page 45 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-5W
Client Matrix:
400-92351-7
Water
Date Sampled: 06/19/2014 1300
Date Received: 06/20/2014 0821
8015C GRO by 8015C
Dilution:
8015C
5030B
1.0
06/21/2014 0310
06/21/2014 0310
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
5 mL
5 mL
5 mL
CH_JOAN
Analysis Date:
Prep Date:
Analysis Batch: 400-220858
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<47 10047Gasoline Range Organics (GRO)-C6-C10
Surrogate %Rec Acceptance LimitsQualifier
87 78 - 119a,a,a-Trifluorotoluene (fid)
TestAmerica Pensacola Page 46 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-6W
Client Matrix:
400-92351-8
Water
Date Sampled: 06/19/2014 1422
Date Received: 06/20/2014 0821
8015C GRO by 8015C
Dilution:
8015C
5030B
1.0
06/23/2014 1710
06/23/2014 1710
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
5 mL
5 mL
5 mL
CH_CAROL
Analysis Date:
Prep Date:
Analysis Batch: 400-221120
N/A
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
370 10047Gasoline Range Organics (GRO)-C6-C10
Surrogate %Rec Acceptance LimitsQualifier
101 78 - 119a,a,a-Trifluorotoluene (fid)
TestAmerica Pensacola Page 47 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-4W
Client Matrix:
400-92351-6
Water
Date Sampled: 06/19/2014 1151
Date Received: 06/20/2014 0821
8015C Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Dilution:
8015C
3520C
1.0
06/23/2014 2120
06/20/2014 1346
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
1050 mL
5.0 mL
1 uL
WALLE
Analysis Date:
Prep Date:
Analysis Batch: 400-221123
400-220901Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<41 12041Diesel Range Organics [C10-C28]
Surrogate %Rec Acceptance LimitsQualifier
107 49 - 134o-Terphenyl (Surr)
TestAmerica Pensacola Page 48 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-5W
Client Matrix:
400-92351-7
Water
Date Sampled: 06/19/2014 1300
Date Received: 06/20/2014 0821
8015C Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Dilution:
8015C
3520C
1.0
06/23/2014 2130
06/20/2014 1346
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
1050 mL
5.0 mL
1 uL
WALLE
Analysis Date:
Prep Date:
Analysis Batch: 400-221123
400-220901Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<41 12041Diesel Range Organics [C10-C28]
Surrogate %Rec Acceptance LimitsQualifier
110 49 - 134o-Terphenyl (Surr)
TestAmerica Pensacola Page 49 of 81
Analytical Data
Client: AEI Consultants Job Number: 400-92351-2
Client Sample ID:
Lab Sample ID:
SP-6W
Client Matrix:
400-92351-8
Water
Date Sampled: 06/19/2014 1422
Date Received: 06/20/2014 0821
8015C Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics)
Dilution:
8015C
3520C
1.0
06/23/2014 2140
06/20/2014 1346
Instrument ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Result Type:PRIMARY
1000 mL
5.0 mL
1 uL
WALLE
Analysis Date:
Prep Date:
Analysis Batch: 400-221123
400-220901Prep Batch:
Analysis Method:
Prep Method:
Analyte Result (ug/L)Qualifier MDL RL
<43 13043Diesel Range Organics [C10-C28]
Surrogate %Rec Acceptance LimitsQualifier
117 49 - 134o-Terphenyl (Surr)
TestAmerica Pensacola Page 50 of 81
QUALITY CONTROL RESULTS
TestAmerica Pensacola
Page 51 of 81
Quality Control Results
Client: AEI Consultants Job Number: 400-92351-2
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Analysis Batch:400-221257
Lab Control Sample Water SM 6200BLCS 400-221257/1002 T
Method Blank Water SM 6200BMB 400-221257/7 T
WaterMW-8 SM 6200B400-92351-1 T
WaterMW-11 SM 6200B400-92351-2 T
WaterSP-1W SM 6200B400-92351-3 T
WaterSP-2W SM 6200B400-92351-4 T
WaterSP-3W SM 6200B400-92351-5 T
WaterSP-4W SM 6200B400-92351-6 T
Matrix Spike Water SM 6200B400-92351-6MS T
Matrix Spike Duplicate Water SM 6200B400-92351-6MSD T
WaterSP-5W SM 6200B400-92351-7 T
WaterSP-6W SM 6200B400-92351-8 T
WaterSP-7W SM 6200B400-92351-9 T
WaterMW-7 SM 6200B400-92351-10 T
Report Basis
T = Total
TestAmerica Pensacola
Page 52 of 81
Quality Control Results
Client: AEI Consultants Job Number: 400-92351-2
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS Semi VOA
Prep Batch: 400-220899
Lab Control Sample Water 3520CLCS 400-220899/2-A T
Lab Control Sample Duplicate Water 3520CLCSD 400-220899/3-A T
Method Blank Water 3520CMB 400-220899/1-A T
WaterMW-11 3520C400-92351-2 T
WaterSP-1W 3520C400-92351-3 T
WaterSP-2W 3520C400-92351-4 T
WaterSP-3W 3520C400-92351-5 T
WaterSP-4W 3520C400-92351-6 T
WaterSP-5W 3520C400-92351-7 T
WaterSP-6W 3520C400-92351-8 T
WaterMW-7 3520C400-92351-10 T
Analysis Batch:400-221174
Lab Control Sample Water 400-2208998270DLCS 400-220899/2-A T
Lab Control Sample Duplicate Water 400-2208998270DLCSD 400-220899/3-A T
Method Blank Water 400-2208998270DMB 400-220899/1-A T
Water 400-220899MW-11 8270D400-92351-2 T
Water 400-220899SP-1W 8270D400-92351-3 T
Water 400-220899SP-2W 8270D400-92351-4 T
Water 400-220899SP-3W 8270D400-92351-5 T
Water 400-220899SP-4W 8270D400-92351-6 T
Water 400-220899SP-5W 8270D400-92351-7 T
Water 400-220899SP-6W 8270D400-92351-8 T
Water 400-220899MW-7 8270D400-92351-10 T
Report Basis
T = Total
TestAmerica Pensacola
Page 53 of 81
Quality Control Results
Client: AEI Consultants Job Number: 400-92351-2
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC VOA
Analysis Batch:400-220858
Lab Control Sample Water 8015CLCS 400-220858/1003 T
Method Blank Water 8015CMB 400-220858/4 T
Matrix Spike Water 8015C400-91930-B-5 MS T
Matrix Spike Duplicate Water 8015C400-91930-B-5 MSD T
WaterSP-4W 8015C400-92351-6 T
WaterSP-5W 8015C400-92351-7 T
Analysis Batch:400-221120
Lab Control Sample Water 8015CLCS 400-221120/1001 T
Method Blank Water 8015CMB 400-221120/2 T
WaterSP-6W 8015C400-92351-8 T
Matrix Spike Water 8015C400-92351-8MS T
Matrix Spike Duplicate Water 8015C400-92351-8MSD T
Report Basis
T = Total
GC Semi VOA
Prep Batch: 400-220901
Lab Control Sample Water 3520CLCS 400-220901/2-A T
Lab Control Sample Duplicate Water 3520CLCSD 400-220901/3-A T
Method Blank Water 3520CMB 400-220901/1-A T
WaterSP-4W 3520C400-92351-6 T
WaterSP-5W 3520C400-92351-7 T
WaterSP-6W 3520C400-92351-8 T
Analysis Batch:400-221123
Lab Control Sample Water 400-2209018015CLCS 400-220901/2-A T
Lab Control Sample Duplicate Water 400-2209018015CLCSD 400-220901/3-A T
Method Blank Water 400-2209018015CMB 400-220901/1-A T
Water 400-220901SP-4W 8015C400-92351-6 T
Water 400-220901SP-5W 8015C400-92351-7 T
Water 400-220901SP-6W 8015C400-92351-8 T
Report Basis
T = Total
TestAmerica Pensacola
Page 54 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221257
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06241407.D
5 mL
5 mLUnits:ug/L
Method: SM 6200B
Preparation: 5030B
CH_TANMB 400-221257/7
Analysis Date: 06/24/2014 1128
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
400-221257
Prep Date:
Leach Date:
06/24/2014 1128
N/A
Analyte MQLMDLQualResult
<0.52 1.00.521,1,1,2-Tetrachloroethane
<0.50 1.00.501,1,1-Trichloroethane
<0.50 1.00.501,1,2,2-Tetrachloroethane
<0.50 1.00.501,1,2-Trichloroethane
<0.50 1.00.501,1-Dichloroethane
<0.50 1.00.501,1-Dichloroethene
<0.50 1.00.501,1-Dichloropropene
<0.70 1.00.701,2,3-Trichlorobenzene
<0.84 1.00.841,2,3-Trichloropropane
<0.82 1.00.821,2,4-Trichlorobenzene
<0.82 1.00.821,2,4-Trimethylbenzene
<1.5 1.01.51,2-Dibromo-3-Chloropropane
<0.50 1.00.501,2-Dichlorobenzene
<0.50 1.00.501,2-Dichloroethane
<0.50 1.00.501,2-Dichloropropane
<0.56 1.00.561,3,5-Trimethylbenzene
<0.54 1.00.541,3-Dichlorobenzene
<0.50 1.00.501,3-Dichloropropane
<0.64 1.00.641,4-Dichlorobenzene
<0.50 1.00.502,2-Dichloropropane
<0.57 1.00.572-Chlorotoluene
<3.1 203.12-Hexanone
<0.56 1.00.564-Chlorotoluene
<10 2010Acetone
<0.34 1.00.34Benzene
<0.54 1.00.54Bromobenzene
<0.52 1.00.52Bromochloromethane
<0.50 1.00.50Bromodichloromethane
<0.71 1.00.71Bromoform
<0.98 1.00.98Bromomethane
<0.50 1.00.50Carbon disulfide
<0.50 1.00.50Carbon tetrachloride
<0.50 1.00.50Chlorobenzene
<0.76 1.00.76Chloroethane
<0.60 1.00.60Chloroform
<0.83 1.00.83Chloromethane
<0.50 1.00.50cis-1,2-Dichloroethene
<0.50 1.00.50cis-1,3-Dichloropropene
<0.50 1.00.50Dibromochloromethane
<0.59 1.00.59Dibromomethane
<0.85 1.00.85Dichlorodifluoromethane
<0.50 1.00.50Ethylbenzene
<0.50 1.00.50Ethylene Dibromide
<0.90 1.00.90Hexachlorobutadiene
<0.68 1.00.68Iodomethane
TestAmerica Pensacola Page 55 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221257
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06241407.D
5 mL
5 mLUnits:ug/L
Method: SM 6200B
Preparation: 5030B
CH_TANMB 400-221257/7
Analysis Date: 06/24/2014 1128
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
400-221257
Prep Date:
Leach Date:
06/24/2014 1128
N/A
Analyte MQLMDLQualResult
<0.70 1.00.70Isopropyl ether
<0.53 1.00.53Isopropylbenzene
<2.6 202.6Methyl Ethyl Ketone
<1.8 201.8methyl isobutyl ketone
<0.74 1.00.74Methyl tert-butyl ether
<3.0 5.03.0Methylene Chloride
<1.6 5.01.6m-Xylene & p-Xylene
<1.0 1.01.0Naphthalene
<0.76 1.00.76n-Butylbenzene
<0.69 1.00.69N-Propylbenzene
<0.60 5.00.60o-Xylene
<0.71 1.00.71p-Cymene
<0.70 1.00.70sec-Butylbenzene
<1.0 1.01.0Styrene
<0.63 1.00.63tert-Butylbenzene
<0.58 1.00.58Tetrachloroethene
<0.70 1.00.70Toluene
<0.50 1.00.50trans-1,2-Dichloroethene
<0.50 1.00.50trans-1,3-Dichloropropene
<0.50 1.00.50Trichloroethene
<0.52 1.00.52Trichlorofluoromethane
<2.0 5.02.0Vinyl acetate
<0.50 1.00.50Vinyl chloride
<1.6 101.6Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 101 78 - 118
Dibromofluoromethane 97 81 - 121
Toluene-d8 (Surr)96 80 - 120
TestAmerica Pensacola Page 56 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Water
1.0
Lab Control Sample - Batch: 400-221257
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06241403-LCS.d
5 mL
5 mLUnits:ug/L
Method: SM 6200B
Preparation: 5030B
CH_TANLCS 400-221257/1002
Analysis Date: 06/24/2014 0934
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
Prep Date:
Leach Date:
06/24/2014 0934
N/A
Analyte QualLimit% Rec.ResultSpike Amount
50.0 48.5 97 66 - 1261,1,1,2-Tetrachloroethane
50.0 41.8 84 66 - 1301,1,1-Trichloroethane
50.0 54.1 108 68 - 1321,1,2,2-Tetrachloroethane
50.0 50.7 101 80 - 1201,1,2-Trichloroethane
50.0 44.9 90 75 - 1261,1-Dichloroethane
50.0 45.3 91 50 - 1341,1-Dichloroethene
50.0 47.1 94 74 - 1211,1-Dichloropropene
50.0 57.0 114 62 - 1301,2,3-Trichlorobenzene
50.0 57.9 116 72 - 1251,2,3-Trichloropropane
50.0 56.3 113 69 - 1281,2,4-Trichlorobenzene
50.0 48.7 97 77 - 1271,2,4-Trimethylbenzene
50.0 58.2 116 52 - 1241,2-Dibromo-3-Chloropropane
50.0 49.8 100 80 - 1211,2-Dichlorobenzene
50.0 46.7 93 69 - 1281,2-Dichloroethane
50.0 46.3 93 77 - 1261,2-Dichloropropane
50.0 48.0 96 80 - 1201,3,5-Trimethylbenzene
50.0 50.4 101 77 - 1241,3-Dichlorobenzene
50.0 52.3 105 77 - 1201,3-Dichloropropane
50.0 51.5 103 79 - 1201,4-Dichlorobenzene
50.0 39.0 78 52 - 1352,2-Dichloropropane
50.0 46.2 92 75 - 1262-Chlorotoluene
200 255 128 60 - 1502-Hexanone
50.0 46.7 93 80 - 1254-Chlorotoluene
200 261 130 24 - 150Acetone
50.0 46.6 93 79 - 120Benzene
50.0 54.2 108 80 - 121Bromobenzene
50.0 53.0 106 80 - 120Bromochloromethane
50.0 42.8 86 75 - 127Bromodichloromethane
50.0 41.0 82 65 - 121Bromoform
50.0 58.6 117 10 - 150Bromomethane
50.0 46.8 94 41 - 140Carbon disulfide
50.0 42.7 85 46 - 141Carbon tetrachloride
50.0 50.3 101 80 - 120Chlorobenzene
50.0 44.2 88 37 - 150Chloroethane
50.0 43.3 87 73 - 122Chloroform
50.0 38.9 78 49 - 141Chloromethane
50.0 47.7 95 78 - 122cis-1,2-Dichloroethene
50.0 46.0 92 70 - 122cis-1,3-Dichloropropene
50.0 46.7 93 63 - 125Dibromochloromethane
50.0 47.9 96 78 - 120Dibromomethane
50.0 47.7 95 27 - 144Dichlorodifluoromethane
50.0 48.9 98 80 - 120Ethylbenzene
50.0 53.1 106 80 - 120Ethylene Dibromide
50.0 55.6 111 35 - 150Hexachlorobutadiene
50.0 57.8 116 58 - 141Iodomethane
50.0 47.4 95 69 - 143Isopropyl ether
TestAmerica Pensacola Page 57 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Water
1.0
Lab Control Sample - Batch: 400-221257
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
06241403-LCS.d
5 mL
5 mLUnits:ug/L
Method: SM 6200B
Preparation: 5030B
CH_TANLCS 400-221257/1002
Analysis Date: 06/24/2014 0934
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
Prep Date:
Leach Date:
06/24/2014 0934
N/A
Analyte QualLimit% Rec.ResultSpike Amount
50.0 48.6 97 76 - 120Isopropylbenzene
200 254 127 62 - 137Methyl Ethyl Ketone
200 250 125 63 - 150methyl isobutyl ketone
50.0 47.7 95 70 - 124Methyl tert-butyl ether
50.0 50.5 101 70 - 130Methylene Chloride
50.0 47.4 95 70 - 130m-Xylene & p-Xylene
50.0 56.1 112 45 - 131Naphthalene
50.0 49.7 99 76 - 138n-Butylbenzene
50.0 48.0 96 75 - 128N-Propylbenzene
50.0 48.0 96 70 - 130o-Xylene
50.0 50.7 101 78 - 120p-Cymene
50.0 49.1 98 78 - 128sec-Butylbenzene
50.0 47.8 96 79 - 124Styrene
50.0 48.7 97 80 - 120tert-Butylbenzene
50.0 58.8 118 76 - 124Tetrachloroethene
50.0 46.0 92 80 - 120Toluene
50.0 47.4 95 70 - 126trans-1,2-Dichloroethene
50.0 46.0 92 64 - 120trans-1,3-Dichloropropene
50.0 55.1 110 77 - 120Trichloroethene
50.0 45.6 91 26 - 150Trichlorofluoromethane
100 107 107 54 - 140Vinyl acetate
50.0 43.8 88 60 - 128Vinyl chloride
100 95.3 95 70 - 130Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 92 78 - 118
Dibromofluoromethane 101 81 - 121
Toluene-d8 (Surr)98 80 - 120
TestAmerica Pensacola Page 58 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
06241409.D
5 mL
5 mL
5 mL
06241410.D
5 mL
5 mL
5 mL
Method: SM 6200B
Preparation: 5030B
CH_TAN
CH_TAN
400-92351-6
400-92351-6
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221257
06/24/2014 1230
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1255
06/24/2014 1255
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
06/24/2014 1230
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
103 108 42 - 135 5 231,1,1,2-Tetrachloroethane
88 91 60 - 131 2 201,1,1-Trichloroethane
104 102 52 - 148 2 201,1,2,2-Tetrachloroethane
101 106 68 - 127 5 191,1,2-Trichloroethane
94 97 10 - 150 4 181,1-Dichloroethane
92 98 10 - 150 6 191,1-Dichloroethene
99 103 59 - 126 4 221,1-Dichloropropene
117 118 30 - 137 1 441,2,3-Trichlorobenzene
109 103 67 - 130 6 221,2,3-Trichloropropane
117 119 20 - 139 1 441,2,4-Trichlorobenzene
104 109 10 - 150 4 541,2,4-Trimethylbenzene
95 92 50 - 133 3 301,2-Dibromo-3-Chloropropane
105 108 10 - 150 2 381,2-Dichlorobenzene
95 95 10 - 150 0 191,2-Dichloroethane
95 100 65 - 132 5 181,2-Dichloropropane
104 107 10 - 150 3 531,3,5-Trimethylbenzene
109 110 25 - 136 1 441,3-Dichlorobenzene
107 111 67 - 127 4 201,3-Dichloropropane
112 112 10 - 150 0 451,4-Dichlorobenzene
81 85 46 - 132 5 202,2-Dichloropropane
101 104 10 - 150 3 472-Chlorotoluene
106 101 24 - 150 4 242-Hexanone
101 106 17 - 145 5 514-Chlorotoluene
100 101 10 - 150 0 22Acetone
97 99 10 - 150 2 19Benzene
115 117 38 - 135 1 35Bromobenzene
108 107 75 - 120 1 17Bromochloromethane
86 89 61 - 133 3 19Bromodichloromethane
74 77 54 - 125 3 19Bromoform
147 178 10 - 150 19 24 F1Bromomethane
98 99 10 - 150 1 23Carbon disulfide
87 91 40 - 138 5 21Carbon tetrachloride
109 113 10 - 150 4 30Chlorobenzene
TestAmerica Pensacola Page 59 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
06241409.D
5 mL
5 mL
5 mL
06241410.D
5 mL
5 mL
5 mL
Method: SM 6200B
Preparation: 5030B
CH_TAN
CH_TAN
400-92351-6
400-92351-6
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221257
06/24/2014 1230
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1255
06/24/2014 1255
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
06/24/2014 1230
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
94 97 38 - 150 3 23Chloroethane
91 94 10 - 150 3 18Chloroform
81 86 26 - 150 6 23Chloromethane
97 100 10 - 150 4 20cis-1,2-Dichloroethene
90 93 52 - 130 3 20cis-1,3-Dichloropropene
93 97 50 - 130 5 21Dibromochloromethane
94 95 69 - 123 1 18Dibromomethane
100 97 10 - 150 3 23Dichlorodifluoromethane
105 109 10 - 150 4 40Ethylbenzene
106 105 70 - 125 2 21Ethylene Dibromide
122 125 10 - 150 3 92Hexachlorobutadiene
116 126 37 - 145 8 36Iodomethane
97 101 10 - 150 4 24Isopropyl ether
106 110 10 - 150 4 46Isopropylbenzene
106 98 10 - 150 8 21Methyl Ethyl Ketone
106 98 20 - 150 8 20methyl isobutyl ketone
94 93 10 - 150 0 18Methyl tert-butyl ether
105 105 10 - 150 0 18Methylene Chloride
102 107 10 - 150 5 43m-Xylene & p-Xylene
107 104 10 - 150 3 53Naphthalene
107 111 10 - 150 3 76n-Butylbenzene
105 108 10 - 150 3 57N-Propylbenzene
104 108 10 - 150 4 39o-Xylene
110 114 10 - 150 4 62p-Cymene
107 110 10 - 150 3 64sec-Butylbenzene
102 105 24 - 147 3 40Styrene
105 110 10 - 150 5 54tert-Butylbenzene
121 126 10 - 150 4 35Tetrachloroethene
99 105 10 - 150 5 26Toluene
101 102 66 - 126 1 19trans-1,2-Dichloroethene
92 97 45 - 128 5 20trans-1,3-Dichloropropene
113 115 10 - 150 1 22Trichloroethene
94 99 29 - 144 4 20Trichlorofluoromethane
TestAmerica Pensacola Page 60 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix:Water
06241409.D
5 mL
5 mL
5 mL
06241410.D
5 mL
5 mL
5 mL
Method: SM 6200B
Preparation: 5030B
CH_TAN
CH_TAN
400-92351-6
400-92351-6
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221257
06/24/2014 1230
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1255
06/24/2014 1255
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221257
N/A
N/A
06/24/2014 1230
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
97 97 10 - 150 0 44Vinyl acetate
92 95 46 - 136 4 20Vinyl chloride
103 107 10 - 150 4 41Xylenes, Total
Surrogate Acceptance LimitsMS % Rec MSD % Rec
4-Bromofluorobenzene 92 92 78 - 118
Dibromofluoromethane 97 98 81 - 121
Toluene-d8 (Surr)98 102 80 - 120
TestAmerica Pensacola Page 61 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Water
06/24/2014 1230 06/24/2014 1255
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: SM 6200B
Preparation: 5030B
Units:ug/L400-92351-6 400-92351-6MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221257
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1230
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1255
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
<0.52 50.0 50.0 51.4 53.81,1,1,2-Tetrachloroethane
<0.50 50.0 50.0 44.2 45.31,1,1-Trichloroethane
<0.50 50.0 50.0 51.9 50.91,1,2,2-Tetrachloroethane
<0.50 50.0 50.0 50.5 52.81,1,2-Trichloroethane
<0.50 50.0 50.0 46.8 48.71,1-Dichloroethane
<0.50 50.0 50.0 46.0 49.01,1-Dichloroethene
<0.50 50.0 50.0 49.5 51.41,1-Dichloropropene
<0.70 50.0 50.0 58.4 58.91,2,3-Trichlorobenzene
<0.84 50.0 50.0 54.6 51.61,2,3-Trichloropropane
<0.82 50.0 50.0 58.5 59.41,2,4-Trichlorobenzene
<0.82 50.0 50.0 52.1 54.41,2,4-Trimethylbenzene
<1.5 50.0 50.0 47.6 46.21,2-Dibromo-3-Chloropropane
<0.50 50.0 50.0 52.7 54.01,2-Dichlorobenzene
<0.50 50.0 50.0 47.5 47.51,2-Dichloroethane
<0.50 50.0 50.0 47.4 49.81,2-Dichloropropane
<0.56 50.0 50.0 51.8 53.51,3,5-Trimethylbenzene
<0.54 50.0 50.0 54.3 55.01,3-Dichlorobenzene
<0.50 50.0 50.0 53.6 55.61,3-Dichloropropane
<0.64 50.0 50.0 56.2 56.11,4-Dichlorobenzene
<0.50 50.0 50.0 40.5 42.42,2-Dichloropropane
<0.57 50.0 50.0 50.6 52.12-Chlorotoluene
<3.1 200 200 212 2032-Hexanone
<0.56 50.0 50.0 50.4 52.84-Chlorotoluene
<10 200 200 200 201Acetone
<0.34 50.0 50.0 48.6 49.5Benzene
<0.54 50.0 50.0 57.7 58.4Bromobenzene
<0.52 50.0 50.0 54.1 53.4Bromochloromethane
<0.50 50.0 50.0 43.1 44.6Bromodichloromethane
<0.71 50.0 50.0 37.1 38.3Bromoform
<0.98 50.0 50.0 73.5 88.8 F1Bromomethane
<0.50 50.0 50.0 49.0 49.4Carbon disulfide
<0.50 50.0 50.0 43.4 45.5Carbon tetrachloride
<0.50 50.0 50.0 54.4 56.4Chlorobenzene
<0.76 50.0 50.0 46.8 48.4Chloroethane
<0.60 50.0 50.0 45.6 46.9Chloroform
<0.83 50.0 50.0 40.4 42.8Chloromethane
<0.50 50.0 50.0 48.3 50.1cis-1,2-Dichloroethene
<0.50 50.0 50.0 45.1 46.3cis-1,3-Dichloropropene
<0.50 50.0 50.0 46.5 48.7Dibromochloromethane
<0.59 50.0 50.0 47.0 47.3Dibromomethane
<0.85 50.0 50.0 50.1 48.4Dichlorodifluoromethane
<0.50 50.0 50.0 52.5 54.7Ethylbenzene
<0.50 50.0 50.0 53.1 52.3Ethylene Dibromide
TestAmerica Pensacola Page 62 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Water
06/24/2014 1230 06/24/2014 1255
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: SM 6200B
Preparation: 5030B
Units:ug/L400-92351-6 400-92351-6MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221257
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1230
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1255
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
<0.90 50.0 50.0 61.1 62.7Hexachlorobutadiene
<0.68 50.0 50.0 57.9 62.9Iodomethane
<0.70 50.0 50.0 48.3 50.4Isopropyl ether
<0.53 50.0 50.0 53.0 55.1Isopropylbenzene
<2.6 200 200 212 196Methyl Ethyl Ketone
<1.8 200 200 212 196methyl isobutyl ketone
<0.74 50.0 50.0 46.9 46.7Methyl tert-butyl ether
<3.0 50.0 50.0 52.4 52.3Methylene Chloride
<1.6 50.0 50.0 50.9 53.3m-Xylene & p-Xylene
<1.0 50.0 50.0 53.4 52.1Naphthalene
<0.76 50.0 50.0 53.6 55.3n-Butylbenzene
<0.69 50.0 50.0 52.5 54.2N-Propylbenzene
<0.60 50.0 50.0 51.9 53.9o-Xylene
<0.71 50.0 50.0 54.9 57.1p-Cymene
<0.70 50.0 50.0 53.6 55.1sec-Butylbenzene
<1.0 50.0 50.0 51.0 52.7Styrene
<0.63 50.0 50.0 52.4 55.0tert-Butylbenzene
3.8 50.0 50.0 64.4 66.9Tetrachloroethene
<0.70 50.0 50.0 49.7 52.4Toluene
<0.50 50.0 50.0 50.3 50.9trans-1,2-Dichloroethene
<0.50 50.0 50.0 46.0 48.3trans-1,3-Dichloropropene
<0.50 50.0 50.0 56.6 57.4Trichloroethene
<0.52 50.0 50.0 47.2 49.3Trichlorofluoromethane
<2.0 100 100 96.9 96.6Vinyl acetate
<0.50 50.0 50.0 45.8 47.6Vinyl chloride
<1.6 100 100 103 107Xylenes, Total
TestAmerica Pensacola Page 63 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-220899
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mb 220899.D
1000 mL
1.0 mLUnits:ug/L
Method: 8270D
Preparation: 3520C
PigpenMB 400-220899/1-A
Analysis Date: 06/24/2014 1337
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221174
400-220899
Prep Date:Injection Volume:1 uL
Leach Date:
06/20/2014 1340
N/A
Analyte RLMDLQualResult
<0.40 100.401,1'-Biphenyl
<0.52 100.521,2,4,5-Tetrachlorobenzene
<0.53 100.531,2,4-Trichlorobenzene
<0.57 100.571,2-Dichlorobenzene
<0.47 100.471,3-Dichlorobenzene
<1.0 101.01,3-Dinitrobenzene
<0.52 100.521,4-Dichlorobenzene
<1.0 101.01,4-Dioxane
<0.50 100.501-Methylnaphthalene
<0.64 100.642,3,4,6-Tetrachlorophenol
<3.7 103.72,4,5-Trichlorophenol
<3.5 103.52,4,6-Trichlorophenol
<3.0 103.02,4-Dichlorophenol
<3.5 103.52,4-Dimethylphenol
<3.4 303.42,4-Dinitrophenol
<1.9 101.92,4-Dinitrotoluene
<1.9 101.92,6-Dinitrotoluene
<0.52 100.522-Chloronaphthalene
<2.2 102.22-Chlorophenol
<0.54 100.542-Methylnaphthalene
<1.8 101.82-Methylphenol
<2.2 102.22-Nitroaniline
<0.65 100.652-Nitrophenol
<1.0 201.03 & 4 Methylphenol
<2.0 102.04,6-Dinitro-2-methylphenol
<0.32 100.324-Bromophenyl phenyl ether
<3.8 103.84-Chloro-3-methylphenol
<2.0 102.04-Chlorophenyl phenyl ether
<2.1 102.14-Nitrophenol
<0.46 100.46Acenaphthene
<0.56 100.56Acenaphthylene
<0.62 100.62Acetophenone
<0.42 100.42Anthracene
<1.0 101.0Azobenzene
<1.3 101.3Benzaldehyde
<0.34 100.34Benzo[a]anthracene
<0.43 100.43Benzo[a]pyrene
<0.38 100.38Benzo[b]fluoranthene
<1.1 101.1Benzo[g,h,i]perylene
<0.54 100.54Benzo[k]fluoranthene
<7.3 307.3Benzoic acid
<2.0 102.0Benzyl alcohol
<0.81 100.81bis (2-chloroisopropyl) ether
<0.69 100.69Bis(2-chloroethoxy)methane
<0.74 100.74Bis(2-chloroethyl)ether
TestAmerica Pensacola Page 64 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-220899
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mb 220899.D
1000 mL
1.0 mLUnits:ug/L
Method: 8270D
Preparation: 3520C
PigpenMB 400-220899/1-A
Analysis Date: 06/24/2014 1337
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221174
400-220899
Prep Date:Injection Volume:1 uL
Leach Date:
06/20/2014 1340
N/A
Analyte RLMDLQualResult
4.50 J 102.3Bis(2-ethylhexyl) phthalate
<0.69 100.69Butyl benzyl phthalate
<0.87 100.87Carbazole
<0.49 100.49Chrysene
<1.2 101.2Dibenz(a,h)anthracene
<0.52 100.52Dibenzofuran
<0.70 100.70Diethyl phthalate
<0.60 100.60Dimethyl phthalate
<2.7 102.7Di-n-butyl phthalate
<0.44 100.44Di-n-octyl phthalate
<0.77 100.77Fluoranthene
<0.56 100.56Fluorene
<0.25 100.25Hexachlorobenzene
<3.6 103.6Hexachlorobutadiene
<2.6 202.6Hexachlorocyclopentadiene
<4.2 104.2Hexachloroethane
<1.0 101.0Hexadecane
<1.0 101.0Indene
<1.0 101.0Indeno[1,2,3-cd]pyrene
<0.57 100.57Isophorone
<0.63 100.63Naphthalene
<1.0 101.0n-Decane
<0.55 100.55Nitrobenzene
<3.5 103.5N-Nitrosodimethylamine
<3.3 103.3N-Nitrosodi-n-propylamine
<0.47 100.47N-Nitrosodiphenylamine
<1.0 101.0n-Octadecane
<1.8 201.8Pentachlorophenol
<0.41 100.41Phenanthrene
<2.6 102.6Phenol
<1.1 101.1Pyrene
<3.2 103.2Pyridine
<0.58 100.58Sulfolane
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol (Surr)0 15 - 135X
2-Fluorobiphenyl 100 34 - 120
2-Fluorophenol (Surr)0 10 - 120X
Nitrobenzene-d5 (Surr)94 27 - 120
Phenol-d5 (Surr)0 10 - 120X
Terphenyl-d14 (Surr)97 53 - 125
TestAmerica Pensacola Page 65 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 400-220899
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/L
lcs 220899.D
1000 mL
1.0 mL
1 uL
lcsd 220899.D
1000 mL
1.0 mL
1 uL
ug/L
Method: 8270D
Preparation: 3520C
Pigpen
Pigpen
LCS 400-220899/2-A
LCSD 400-220899/3-A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1456
06/20/2014 1340
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-220899
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1535
06/20/2014 1340
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-220899
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9993 58 - 121 6 301,1'-Biphenyl
10193 54 - 128 8 301,2,4,5-Tetrachlorobenzene
9690 57 - 120 6 301,2,4-Trichlorobenzene
8885 53 - 120 4 301,2-Dichlorobenzene
8684 51 - 120 3 301,3-Dichlorobenzene
10395 59 - 130 7 301,3-Dinitrobenzene
9189 51 - 120 3 301,4-Dichlorobenzene
7171 10 - 130 0 301,4-Dioxane
9895 59 - 120 4 301-Methylnaphthalene
110103 46 - 131 6 302,3,4,6-Tetrachlorophenol
10697 53 - 130 9 302,4,5-Trichlorophenol
10998 52 - 131 11 302,4,6-Trichlorophenol
10394 52 - 125 8 302,4-Dichlorophenol
8676 52 - 121 12 302,4-Dimethylphenol
10890 22 - 146 19 302,4-Dinitrophenol
10699 54 - 141 7 302,4-Dinitrotoluene
10497 61 - 130 7 302,6-Dinitrotoluene
9889 24 - 150 10 302-Chloronaphthalene
9482 45 - 120 13 302-Chlorophenol
9792 58 - 123 6 302-Methylnaphthalene
10189 38 - 121 12 302-Methylphenol
10798 52 - 135 8 302-Nitroaniline
10494 47 - 129 10 302-Nitrophenol
10190 43 - 126 12 303 & 4 Methylphenol
108102 46 - 136 6 304,6-Dinitro-2-methylphenol
10498 62 - 132 6 304-Bromophenyl phenyl ether
10499 47 - 135 5 304-Chloro-3-methylphenol
10195 61 - 133 6 304-Chlorophenyl phenyl ether
113106 34 - 137 6 304-Nitrophenol
10192 57 - 125 9 30Acenaphthene
10093 59 - 125 8 30Acenaphthylene
10095 53 - 127 5 30Acetophenone
9993 65 - 128 7 30Anthracene
10295 55 - 139 7 30Azobenzene
45 10 - 158 10 30 J **Benzaldehyde
9993 63 - 126 7 30Benzo[a]anthracene
TestAmerica Pensacola Page 66 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 400-220899
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/L
lcs 220899.D
1000 mL
1.0 mL
1 uL
lcsd 220899.D
1000 mL
1.0 mL
1 uL
ug/L
Method: 8270D
Preparation: 3520C
Pigpen
Pigpen
LCS 400-220899/2-A
LCSD 400-220899/3-A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1456
06/20/2014 1340
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-220899
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1535
06/20/2014 1340
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-220899
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
10497 61 - 125 8 30Benzo[a]pyrene
107100 49 - 140 6 30Benzo[b]fluoranthene
126108 51 - 149 15 30Benzo[g,h,i]perylene
9891 56 - 138 7 30Benzo[k]fluoranthene
10980 10 - 120 30 30 JBenzoic acid
10496 51 - 121 8 30Benzyl alcohol
9689 20 - 142 7 30bis (2-chloroisopropyl) ether
10399 54 - 123 4 30Bis(2-chloroethoxy)methane
9186 47 - 120 7 30Bis(2-chloroethyl)ether
129120 62 - 140 7 30Bis(2-ethylhexyl) phthalate
107100 51 - 150 7 30Butyl benzyl phthalate
8983 57 - 136 7 30Carbazole
9892 60 - 126 5 30Chrysene
130115 57 - 133 12 30Dibenz(a,h)anthracene
9992 62 - 124 8 30Dibenzofuran
9890 55 - 140 8 30Diethyl phthalate
9893 50 - 133 5 30Dimethyl phthalate
10196 59 - 144 5 30Di-n-butyl phthalate
134123 55 - 140 9 30Di-n-octyl phthalate
10094 66 - 131 6 30Fluoranthene
9893 60 - 132 6 30Fluorene
9893 60 - 138 6 30Hexachlorobenzene
9693 48 - 126 3 30Hexachlorobutadiene
4638 19 - 139 18 30 J JHexachlorocyclopentadiene
9291 46 - 121 1 30Hexachloroethane
10396 14 - 167 7 30Hexadecane
9086 17 - 141 5 30Indene
125110 55 - 135 12 30Indeno[1,2,3-cd]pyrene
10196 57 - 122 5 30Isophorone
9692 55 - 125 4 30Naphthalene
7877 14 - 133 1 30n-Decane
9894 52 - 128 4 30Nitrobenzene
8285 21 - 134 3 30N-Nitrosodimethylamine
10497 41 - 143 6 30N-Nitrosodi-n-propylamine
108100 10 - 185 7 30N-Nitrosodiphenylamine
10599 27 - 156 7 30n-Octadecane
TestAmerica Pensacola Page 67 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 400-220899
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/L
lcs 220899.D
1000 mL
1.0 mL
1 uL
lcsd 220899.D
1000 mL
1.0 mL
1 uL
ug/L
Method: 8270D
Preparation: 3520C
Pigpen
Pigpen
LCS 400-220899/2-A
LCSD 400-220899/3-A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1456
06/20/2014 1340
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-220899
N/A
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1535
06/20/2014 1340
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221174
400-220899
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
125117 38 - 138 6 30Pentachlorophenol
9994 64 - 133 5 30Phenanthrene
9368 37 - 120 30 30Phenol
9387 55 - 142 7 30Pyrene
7773 10 - 127 5 30Pyridine
120116 50 - 150 3 30Sulfolane
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
2,4,6-Tribromophenol (Surr)121 130 15 - 135
2-Fluorobiphenyl 117 123 34 - 120X
2-Fluorophenol (Surr)68 89 10 - 120
Nitrobenzene-d5 (Surr)123 127 27 - 120XX
Phenol-d5 (Surr)106 121 10 - 120X
Terphenyl-d14 (Surr)122 127 53 - 125X
TestAmerica Pensacola Page 68 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Water
06/24/2014 1456
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 400-220899
Method: 8270D
Preparation: 3520C
Units:ug/LLCS 400-220899/2-A LCSD 400-220899/3-ALCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1340
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1535
06/20/2014 1340
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
29.627.830.0 30.01,1'-Biphenyl
30.328.030.0 30.01,2,4,5-Tetrachlorobenzene
28.727.130.0 30.01,2,4-Trichlorobenzene
26.525.630.0 30.01,2-Dichlorobenzene
25.825.130.0 30.01,3-Dichlorobenzene
30.828.630.0 30.01,3-Dinitrobenzene
27.426.630.0 30.01,4-Dichlorobenzene
21.321.330.0 30.01,4-Dioxane
29.528.430.0 30.01-Methylnaphthalene
33.131.030.0 30.02,3,4,6-Tetrachlorophenol
31.829.030.0 30.02,4,5-Trichlorophenol
32.729.430.0 30.02,4,6-Trichlorophenol
30.828.330.0 30.02,4-Dichlorophenol
25.822.830.0 30.02,4-Dimethylphenol
65.053.860.0 60.02,4-Dinitrophenol
31.729.630.0 30.02,4-Dinitrotoluene
31.329.130.0 30.02,6-Dinitrotoluene
29.526.830.0 30.02-Chloronaphthalene
28.124.530.0 30.02-Chlorophenol
29.227.630.0 30.02-Methylnaphthalene
30.326.830.0 30.02-Methylphenol
32.129.530.0 30.02-Nitroaniline
31.128.330.0 30.02-Nitrophenol
30.427.130.0 30.03 & 4 Methylphenol
64.860.960.0 60.04,6-Dinitro-2-methylphenol
31.129.430.0 30.04-Bromophenyl phenyl ether
31.229.730.0 30.04-Chloro-3-methylphenol
30.328.630.0 30.04-Chlorophenyl phenyl ether
67.963.960.0 60.04-Nitrophenol
30.227.730.0 30.0Acenaphthene
30.027.830.0 30.0Acenaphthylene
30.028.630.0 30.0Acetophenone
29.827.930.0 30.0Anthracene
30.628.630.0 30.0Azobenzene
J **<1.31.4030.0 30.0Benzaldehyde
29.627.830.0 30.0Benzo[a]anthracene
31.329.030.0 30.0Benzo[a]pyrene
32.130.130.0 30.0Benzo[b]fluoranthene
37.732.530.0 30.0Benzo[g,h,i]perylene
TestAmerica Pensacola Page 69 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Water
06/24/2014 1456
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 400-220899
Method: 8270D
Preparation: 3520C
Units:ug/LLCS 400-220899/2-A LCSD 400-220899/3-ALCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1340
Analysis Date:
Prep Date:
Leach Date:
06/24/2014 1535
06/20/2014 1340
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
29.327.430.0 30.0Benzo[k]fluoranthene
J 32.624.130.0 30.0Benzoic acid
31.328.930.0 30.0Benzyl alcohol
28.726.730.0 30.0bis (2-chloroisopropyl) ether
31.029.630.0 30.0Bis(2-chloroethoxy)methane
27.425.730.0 30.0Bis(2-chloroethyl)ether
38.735.930.0 30.0Bis(2-ethylhexyl) phthalate
32.029.930.0 30.0Butyl benzyl phthalate
26.724.930.0 30.0Carbazole
29.327.730.0 30.0Chrysene
38.934.530.0 30.0Dibenz(a,h)anthracene
29.727.530.0 30.0Dibenzofuran
29.427.130.0 30.0Diethyl phthalate
29.427.830.0 30.0Dimethyl phthalate
30.428.830.0 30.0Di-n-butyl phthalate
40.336.830.0 30.0Di-n-octyl phthalate
30.028.230.0 30.0Fluoranthene
29.527.830.0 30.0Fluorene
29.527.830.0 30.0Hexachlorobenzene
28.727.930.0 30.0Hexachlorobutadiene
J J13.811.530.0 30.0Hexachlorocyclopentadiene
27.627.330.0 30.0Hexachloroethane
30.928.930.0 30.0Hexadecane
27.025.730.0 30.0Indene
37.433.130.0 30.0Indeno[1,2,3-cd]pyrene
30.328.730.0 30.0Isophorone
28.727.530.0 30.0Naphthalene
23.323.030.0 30.0n-Decane
29.528.330.0 30.0Nitrobenzene
24.725.630.0 30.0N-Nitrosodimethylamine
31.129.230.0 30.0N-Nitrosodi-n-propylamine
16.115.015.0 15.0N-Nitrosodiphenylamine
31.629.630.0 30.0n-Octadecane
75.070.560.0 60.0Pentachlorophenol
29.628.330.0 30.0Phenanthrene
27.820.530.0 30.0Phenol
27.926.030.0 30.0Pyrene
23.222.030.0 30.0Pyridine
37.836.531.6 31.6Sulfolane
TestAmerica Pensacola Page 70 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-220858
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
J062004.D
5 mL
5 mLUnits:ug/L
Method: 8015C
Preparation: 5030B
CH_JOANMB 400-220858/4
Analysis Date: 06/20/2014 1212
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
400-220858
Prep Date:Injection Volume:5 mL
Leach Date:
06/20/2014 1212
N/A PRIMARYColumn ID:
Analyte RLMDLQualResult
<47 10047Gasoline Range Organics (GRO)-C6-C10
Surrogate % Rec Acceptance Limits
a,a,a-Trifluorotoluene (fid)93 78 - 119
Water
1.0
Lab Control Sample - Batch: 400-220858
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
J062003-LCS.d
5 mL
5 mLUnits:ug/L
Method: 8015C
Preparation: 5030B
CH_JOANLCS 400-220858/1003
Analysis Date: 06/20/2014 1133
Analysis Batch:
Prep Batch:
Leach Batch:
400-220858
N/A
N/A
Prep Date:Injection Volume:5 mL
Column ID:PRIMARYLeach Date:
06/20/2014 1133
N/A
Analyte QualLimit% Rec.ResultSpike Amount
1000 1010 101 85 - 115Gasoline Range Organics (GRO)-C6-C10
Surrogate % Rec Acceptance Limits
a,a,a-Trifluorotoluene (fid)96 78 - 119
TestAmerica Pensacola Page 71 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix:Water
J062009.D
5 mL
5 mL
5 mL
PRIMARY
J062010.D
5 mL
5 mL
5 mL
PRIMARY
Method: 8015C
Preparation: 5030B
CH_JOAN
CH_JOAN
400-91930-B-5 MS
400-91930-B-5 MSD
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-220858
06/20/2014 1502
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-220858
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1535
06/20/2014 1535
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-220858
N/A
N/A
06/20/2014 1502
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
130 132 35 - 150 1 15Gasoline Range Organics (GRO)-C6-C10
Surrogate Acceptance LimitsMS % Rec MSD % Rec
a,a,a-Trifluorotoluene (fid)99 99 78 - 119
Water
06/20/2014 1502 06/20/2014 1535
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 8015C
Preparation: 5030B
Units:ug/L400-91930-B-5 MS 400-91930-B-5 MSDMS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-220858
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1502
N/A
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1535
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
170 1000 1000 1470 1490Gasoline Range Organics (GRO)-C6-C10
TestAmerica Pensacola Page 72 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-221120
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
C062302.D
5 mL
5 mLUnits:ug/L
Method: 8015C
Preparation: 5030B
CH_CAROLMB 400-221120/2
Analysis Date: 06/23/2014 1150
Analysis Batch:
Prep Batch:
Leach Batch:
N/A
N/A
400-221120
Prep Date:Injection Volume:5 mL
Leach Date:
06/23/2014 1150
N/A PRIMARYColumn ID:
Analyte RLMDLQualResult
<47 10047Gasoline Range Organics (GRO)-C6-C10
Surrogate % Rec Acceptance Limits
a,a,a-Trifluorotoluene (fid)103 78 - 119
Water
1.0
Lab Control Sample - Batch: 400-221120
Client Matrix:
Lab Sample ID:
Dilution:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
C062301-LCS.d
5 mL
5 mLUnits:ug/L
Method: 8015C
Preparation: 5030B
CH_CAROLLCS 400-221120/1001
Analysis Date: 06/23/2014 0935
Analysis Batch:
Prep Batch:
Leach Batch:
400-221120
N/A
N/A
Prep Date:Injection Volume:5 mL
Column ID:PRIMARYLeach Date:
06/23/2014 0935
N/A
Analyte QualLimit% Rec.ResultSpike Amount
800 788 99 85 - 115Gasoline Range Organics (GRO)-C6-C10
Surrogate % Rec Acceptance Limits
a,a,a-Trifluorotoluene (fid)104 78 - 119
TestAmerica Pensacola Page 73 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Dilution:
Dilution:
Water
1.0
1.0
Client Matrix:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix:Water
C062308.D
5 mL
5 mL
5 mL
PRIMARY
C062309.D
5 mL
5 mL
5 mL
PRIMARY
Method: 8015C
Preparation: 5030B
CH_CAROL
CH_CAROL
400-92351-8
400-92351-8
MS Lab Sample ID:
MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221120
06/23/2014 1814
N/A
Analysis Date:
Prep Date:
Leach Date:
Analysis Batch:
Prep Batch:
Leach Batch:
400-221120
N/A
N/A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 1919
06/23/2014 1919
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221120
N/A
N/A
06/23/2014 1814
Analyte RPD LimitRPDLimit
% Rec.
MS MSD MS Qual MSD Qual
93 97 35 - 150 3 15Gasoline Range Organics (GRO)-C6-C10
Surrogate Acceptance LimitsMS % Rec MSD % Rec
a,a,a-Trifluorotoluene (fid)98 101 78 - 119
Water
06/23/2014 1814 06/23/2014 1919
Dilution:Dilution:1.0 1.0
Client Matrix:Client Matrix:Water
Method: 8015C
Preparation: 5030B
Units:ug/L400-92351-8 400-92351-8MS Lab Sample ID:MSD Lab Sample ID:
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 400-221120
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 1814
N/A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 1919
N/A
Amount
Sample
Analyte Result/Qual Amount Result/Qual Result/Qual
MS MSDMS Spike MSD Spike
370 800 800 1120 1150Gasoline Range Organics (GRO)-C6-C10
TestAmerica Pensacola Page 74 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
WaterClient Matrix:
1.0Dilution:
Lab Sample ID:
Method Blank - Batch: 400-220901
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
MB 400-2209011-A_096.d
1000 mL
5.0 mLUnits:ug/L
Method: 8015C
Preparation: 3520C
WALLEMB 400-220901/1-A
Analysis Date: 06/23/2014 2050
Analysis Batch:
Prep Batch:
Leach Batch:N/A
400-221123
400-220901
Prep Date:Injection Volume:1 uL
Leach Date:
06/20/2014 1346
N/A PRIMARYColumn ID:
Analyte RLMDLQualResult
<43 13043Diesel Range Organics [C10-C28]
Surrogate % Rec Acceptance Limits
o-Terphenyl (Surr)120 49 - 134
Dilution:
Dilution:
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 400-220901
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
Client Matrix:Water
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Column ID:
ug/L
LCS 400-2209012-A_097.d
1000 mL
5.0 mL
1 uL
PRIMARY
LCSD 400-2209013-A_098.d
1000 mL
5.0 mL
1 uL
PRIMARY
ug/L
Method: 8015C
Preparation: 3520C
WALLE
WALLE
LCS 400-220901/2-A
LCSD 400-220901/3-A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 2100
06/20/2014 1346
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221123
400-220901
N/A
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 2110
06/20/2014 1346
N/A
Analysis Batch:
Prep Batch:
Leach Batch:
400-221123
400-220901
N/A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
102103 63 - 138 1 30Diesel Range Organics [C10-C28]
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
o-Terphenyl (Surr)118 111 49 - 134
TestAmerica Pensacola Page 75 of 81
Quality Control Results
Job Number: 400-92351-2Client: AEI Consultants
Water
06/23/2014 2100
Dilution:Dilution:1.0 1.0
Client Matrix:
LCSD Lab Sample ID:
Client Matrix:Water
Laboratory Control/
Laboratory Duplicate Data Report - Batch: 400-220901
Method: 8015C
Preparation: 3520C
Units:ug/LLCS 400-220901/2-A LCSD 400-220901/3-ALCS Lab Sample ID:
Analysis Date:
Prep Date:
Leach Date:
06/20/2014 1346
Analysis Date:
Prep Date:
Leach Date:
06/23/2014 2110
06/20/2014 1346
N/AN/A
LCSD
Result/Qual
LCS
Result/Qual
LCSD Spike
Amount
LCS Spike
AmountAnalyte
10300104001010010100Diesel Range Organics [C10-C28]
TestAmerica Pensacola Page 76 of 81
DATA REPORTING QUALIFIERS
Client: AEI Consultants Job Number: 400-92351-2
Lab Section Qualifier Description
GC/MS VOA
MS and/or MSD Recovery exceeds the control limitsF1
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
GC/MS Semi VOA
LCS or LCSD exceeds the control limits*
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
Surrogate is outside control limitsX
TestAmerica Pensacola Page 77 of 81
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Login Sample Receipt Checklist
Client: AEI Consultants Job Number: 400-92351-2
Login Number: 92351
Question Answer Comment
Creator: Summers, Dustin H
List Source: TestAmerica Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.2.5°C/2.0°C/0.0°C IR-5
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Pensacola Page 81 of 81

APPENDIX B

BORING LOGS