18045_Seneca Place_Phase II ESA_20150421

Phase II
Environmental Site Assessment

Seneca Place Shopping Center
5021 and 5033 South Boulevard
Charlotte, North Carolina

H&H Job No. AZA-002
April 21, 2015

Phase II Environmental Site Assessment Seneca Place Shopping Center
5021 and 5033 South Boulevard
Charlotte, North Carolina H&H Job No. AZA-002
Table of Contents

1.0 Introduction ............................................................................................................................ 1
2.0 Sampling Activities ................................................................................................................ 2
2.1 Soil Sampling Activities ...................................................................................................... 2
2.2 Groundwater Sampling Activities........................................................................................ 2
3.0 Analytical Results................................................................................................................... 4
3.1 Soil Sample Results .............................................................................................................. 4
3.2 Groundwater Sample Results ............................................................................................... 4
4.0 Summary and Recommendations ......................................................................................... 6

List of Tables

Table 1 Summary of Soil Analytical Data
Table 2 Summary of Groundwater Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Soil Sample Location Map
Figure 3 Groundwater Sample Location Map

List of Appendices
Appendix A Boring Logs and Well Construction Diagrams
Appendix B Laboratory Analytical Report

i
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\Phase II ESA_Seneca Place.docx
Phase II Environmental Site Assessment Seneca Place Shopping Center
5021 and 5033 South Boulevard
Charlotte, North Carolina H&H Job No. AZA-002
1.0 Introduction

This report presents the methods and results of a Phase II Environmental Site Assessment (ESA)
conducted by Hart & Hickman, PC (H&H) at the Seneca Place Shopping Center located at 5021
and 5033 South Boulevard Charlotte, North Carolina (Site). A site location map is provided as
Figure 1. The Site is currently in the North Carolina Brownfields Ready for Reuse Program
(Brownfields Project #18045-14-60). The scope of work for this Phase II ESA was approved in
an email dated March 23, 2015 from Mr. James Rudder of the North Carolina Department of
Environment and Natural Resources (DENR) Brownfields Program.

The Site is 4.21 acres in size and contains two buildings, which include Hook Tire & Service,
and a multi-tenant strip shopping center that contains the former Personal Touch Dry-Cleaning.
A site layout is provided in Figure 2. Surrounding properties include a residential neighborhood
to the east, a daycare to the north, and commercial properties to the west and south. Historic
commercial uses for the surrounding properties include the former Seneca Cleaners drycleaner to
the west (currently Pep Boys) and a former gas station to the south (currently Panda Express
restaurant).

As part of the Brownfields Program, H&H completed Phase II environmental site assessment
(ESA) activities at the site. The purpose of the Phase II ESA was to assess the potential for
impact to soil and groundwater from chlorinated solvents and/or petroleum hydrocarbons from
offsite sources and/or onsite operation of the service garage and former drycleaner. This report
details the methods and results of the Phase II ESA activities
1
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\Phase II ESA_Seneca Place.docx
2.0 Sampling Activities

H&H completed ESA activities at the site on March 30, 2015. The assessment activities
included the collection of six soil samples and seven groundwater samples. Four of the seven
groundwater samples were collected from temporary wells. The other three groundwater
samples were collected from previously installed onsite permanent monitoring wells. The
permanent monitoring wells were installed on the property in association with a petroleum
release from the former gas station located on the adjacent southern property (currently Panda
Express). The following sections detail the soil and groundwater sampling activities.

2.1 Soil Sampling Activities
On March 30, 2015 H&H advanced six soil borings at the Site (SB-1 through SB-6) using a
Direct Push technology (DPT) drill rig. The soil boring locations are shown on Figure 2. During
sampling, the recovered soil was screened in the field for the presence of odors, staining, and/or
elevated photoionization detector (PID) readings. Soil samples for laboratory analysis were
collected at the following intervals: SB-1 at 8-9 feet (ft) below ground surface (bgs); SB-2 at 10-
11 feet bgs; SB-3 at 9-10 feet bgs; SB-4 through SB-6at 5 feet bgs. These depths were based on
the anticipated depths of subsurface features and /or likely depth of impacts within the service
garage and the former dry-cleaner. Soil boring logs are included in Appendix A.

The soil samples collected from each boring were analyzed for volatile organic compounds
(VOCs) by EPA Method 8260 and semi-volatile organic compounds (SVOCs) by EPA
Method 8270. These samples were collected into laboratory supplied sample containers, placed
on ice in a cooler, and sent to TestAmerica, Inc. for analysis using chain of custody protocol.

2.2 Groundwater Sampling Activities
On March 30, 2015, H&H installed four temporary groundwater monitoring wells at the site
(TMW-1 through TMW-4). The locations of the temporary wells are shown on Figure 3. The
temporary wells were constructed with one-inch diameter PVC with 15 ft sections of screen set
to bracket the water table. Each well was set to 20 ft bgs and groundwater was encountered at
2
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\Phase II ESA_Seneca Place.docx
depths between 9.36 ft and 16.23 ft bgs. Well construction diagrams with water table depths are
provided on the boring logs included in Appendix A. Following installation, the temporary wells
were developed using standard protocol.

The temporary and permanent wells were sampled using low flow sampling techniques. Prior to
sampling the depth to water was measured in the permanent monitoring wells. Relative water
table elevations were not measured for this Phase II ESA. Historical data indicate that the
groundwater flow direction for the site is generally to the northeast which is consistent with area
topography.

The groundwater samples collected from were analyzed for VOCs by EPA Method 8260 and
SVOCs by EPA Method 8270. The samples were collected into laboratory supplied sample
containers, placed on ice in a cooler, and sent to TestAmerica, Inc. for analysis using chain of
custody protocol.

3
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\Phase II ESA_Seneca Place.docx
3.0 Analytical Results

3.1 Soil Sample Results

There were no concentrations of VOCs or SVOCs detected in the soil samples collected above
the Inactive Hazardous Sites Branch (IHSB) Residential or Industrial Preliminary Soil
Remediation Goals (PSRGs). The analytical results are summarized on Table 1, and the
laboratory report along with chain-of-custody is included in Appendix B.

Tetrachloroethylene (PCE) was detected in samples SB-1 (8-9) and SB-5 (5). Based on the
depth of the sample collected from SB-1 and the PCE concentrations detected in groundwater in
that area, it is possible the PCE concentration detected in SB-1 is from groundwater
contamination from the former Seneca Cleaners to the southwest. The PCE detected in soil
sample SB-5 appears to be associated with the former Personal Touch Dry-Cleaning. The PCE
detections in soil are shown on Figure 2.

Acetone was also detected in samples SB-2 through SB-6. Acetone is a common laboratory
introduced artifact and is not likely present in site soils. In addition, a concentration of bis(2-
ethylhexyl)phthalate was detected in samples SB-2 collected from below the Hook Tire &
Service center. This compound is also sometimes a laboratory introduced artifact. The
concentration detected was below the IHSB Residential and Industrial PSRGs.

No other compounds were detected above laboratory reporting limits in the soil samples.

3.2 Groundwater Sample Results

Concentrations of PCE were detected in samples collected from MW- 11 (8.00 µg/L), TMW-1
(35.3 µg/L), TMW-2 (85.5 µg/L), TMW-3 (11.8 µg/L), and TMW-4 (318 µg/L) above the North
Carolina 15A NCAC 2L Groundwater Standard (2L Groundwater Standard) of 0.7 µg/L. In
addition, the PCE concentrations detected in samples TMW-2 and TMW-4 exceed the Division
of Waste Management Nonresidential Vapor Intrusion Screening Level for Groundwater.

4
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\Phase II ESA_Seneca Place.docx
A concentration of trichloroethene (TCE) was detected in TMW-4 (3.99 µg/L) above the
North Carolina 2L Groundwater Standard of 3 µg/L. TCE was also detected in sample MW-11,
but at a concentration below the North Carolina 2L Groundwater Standard. Groundwater sample
MW-7 also contained a concentration of bis(2-ethylhexyl)phthalate (13.1 µg/L) above the
North Carolina 2L Groundwater Standard of 3.0 µg/L. However, as mentioned above, bis(2-
ethylhexyl)phthalate is sometimes a laboratory introduced artifact, and the laboratory control
sample result for this compounds was outside of quality control standards.

Based on the groundwater flow direction, it appears that PCE and TCE detected in TMW-1,
TMW-2, TMW-4, and MW-11, which are in the northwestern portion of the site, are associated
with a release from the former Seneca Cleaners located west of the site. PCE impacts in TMW-3
appear to be associated with the former Personal Touch Dry-Cleaning. PCE and TCE
concentrations in groundwater are shown on Figure 3.

Chloroform, cis-1,2-dichloroethene, and/or methyl tert-butyl ether were also detected in the
groundwater samples but concentrations were below the North Carolina 2L Groundwater
Standards. No other compounds, including petroleum related compounds, were detected above
laboratory reporting limits. Groundwater sample results are summarized on Table 2, and the
laboratory report along with chain-of-custody is included in Appendix B.

5
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\Phase II ESA_Seneca Place.docx
4.0 Summary and Recommendations

H&H has completed Phase II ESA sampling activities at the Seneca Place Shopping Center
located at 5021 and 5033 South Boulevard, Charlotte. The assessment activities included the
collection of six soil and seven groundwater samples at the site. Soil samples did not contain
compound concentrations above IHSB Residential or Industrial PSRGs. The groundwater
samples collected in the northwestern and eastern portions of the site contained concentrations of
PCE (up to 318 µg/l), which are above the North Carolina 2L Groundwater Standard of 0.7µg/L.
In addition, the PCE concentrations detected in two samples were above the Division of Waste
Management Nonresidential Vapor Intrusion Screening Level for Groundwater.

PCE and TCE concentrations were detected in the northwestern portion of the site which is
downgradient of the off-site former Seneca Cleaners drycleaners. Therefore, it appears that the
PCE and TCE impacts in the northwestern portion of the site are associated with a release from
the former Seneca Cleaners. The PCE concentrations detected in the eastern portion of the site
appear to be associate with a release from the former on-site Personal Touch Dry-Cleaning.

Based on the PCE concentrations present in groundwater beneath the Hook Tire & Service and
the potential PCE release identified at the former Personal Touch Dry-Cleaning, H&H
recommends completing subslab vapor testing to evaluate the vapor intrusion potential for both
site buildings. Because petroleum impacts of concern were not detected during this Phase II
ESA, H&H recommends that subslab vapor samples be analyzed for PCE, TCE, and their
daughter products.

6
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\Phase II ESA_Seneca Place.docx
Table 1
Summary of Soil Analytical Data
Seneca Place Shopping Center
Charlotte, North Carolina
H&H Job No. AZA-002
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\GW & Soil Table4/21/2015
Table 1
Hart & Hickman, PC
Sample Location
Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6
Depth (ft bgs)8-9 10-11 9-10 5 5 5
Sample Date 3/30/2015 3/30/2015 3/30/2015 3/30/2015 3/30/2015 3/30/2015 Protection of
Groundwater Residential Industrial
Units (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)
Acetone <0.0301 0.0324 0.0492 0.0396 0.0301 0.0368 24 12,000 100,000
Tetrachloroethene 0.0170*<0.00573 <0.00673 <0.00545 0.0178 <0.00611 0.005 16 78
SVOCs (8270C)
Bis(2-Ethylhexyl)phthalate <0.504 0.634 <0.532 <0.424 <0.393 <0.493 NS 38 160
Notes:
Only those compounds detected in at least one sample shown above
1) Inactive Hazardous Site Branch Preliminary Soil Remedial Goals (March 2015)
Method number follows parameter in parenthesis
*Soil sample SB-1 was collected near the top of the water table. PCE detections in SB-1 may be present due to groundwater contamination
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds
NS = screening criteria not specified
mg/kg = milligrams per kilogram
Hook & Tire Former Personal Touch Dry-Cleaning
IHSB PSRGs1
Screening Criteria
Table 2
Summary of Groundwater Analytical Data
Seneca Place Shopping Center
Charlotte, North Carolina
H&H Job No. AZA-001
S:\AAA-Master Projects\Azalea Management (AZA)\AZA.002 Seneca Place Phase II\Phase II\GW & Soil Table4/21/2015
Table 2
Hart & Hickman, PC
Sample ID MW-7 MW-8 MW-11 TMW-1 TMW-2 TMW-4 TMW-3
Sample Date 3/30/2015 3/30/2015 3/30/2015 3/30/2015 3/30/2015 3/30/2015 3/30/2015
Units (µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)(µg/L)
VOCs (8260B)Chloroform 17.4 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 70 35.5
cis-1,2-Dichloroethene <1.00 <1.00 5.05 <1.00 <1.00 <1.00 <1.00 70 NS
Methyl tert-butyl ether <1.00 <1.00 <1.00 <1.00 4.84 <1.00 <1.00 20 19,700
Tetrachloroethene <1.00 <1.00 8.00 35.3 85.5 318 11.8 0.7 48.4
Trichloroethene <1.00 <1.00 1.57 <1.00 <1.00 3.99 <1.00 3 4.35
SVOCs (8270C)Bis(2-Ethylhexyl)phthalate 13.1 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 3.0 NS
Notes:
Only those compounds detected in at least one sample shown above
1) 15A North Carolina Administrative Code 2L Groundwater Standards
2) Division of Waste Management Non-Residential Vapor Intrusion Groundwater Screening Level
Bold indicates an exceedance of the NCAC 2L Standard
Bold and highlighted indicates an exceedance of the Division of Waste Management Non-Residential Vapor Intrusion Groundwater Screening Level.
Method number follows parameter in parenthesis
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NS = Not Specified
µg/L = micrograms per liter
15A NCAC 2L1
Hook & Tire Former Personal
Touch Dry-Cleaning Screening Critera
DWM VI Groundwater
Screening Level2
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE WEST, NORTH CAROLINA 1996
TITLE
PROJECT
SITE LOCATION MAP
SENECA PLACE SHOPPING CENTER
5021 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
04-20-15 0
1AZA-002
APPENDIX A
Boring Logs and Well Construction Diagrams

ASPHALT
Dry, firm to very firm, red orange clayey SILT
Moist to very moist, firm to very firm, red orange clayeySILT
Wet, firm, red orange clayey SILT with mottling and fewdark brown minerals
Bottom of borehole at 20.0 feet.
1.1
1.3
0
0
Bentonite
Seal
1" PVCRiser
Filter Sand
Pack
1" Slotted
PVC Screen
DRAWN BY:CDO
BORING COMPLETED:3/30/15
DRILLING CONTRACTOR:Terra Sonic Remarks:
DRILL RIG/ METHOD:6620DT / HA/DPT
SAMPLING METHOD:Macro-Core Hand auger to 5ft BGS.
BORING STARTED:3/30/15
LOGGED BY:CBL
TOTAL DEPTH: 20 ft.
TOP OF CASING ELEV:
DEPTH TO WATER: 8.81 ft.DEPTH(ft)DEPTH(ft)RECOVERY (%)SAMPLE TYPENUMBERMATERIAL DESCRIPTION
LITHOLOGYSAMP.BKG.BLOWCOUNTS(N VALUE)WELL DIAGRAM
OVA (ppm)Sheet 1 of 1
BORING NUMBER SB-1/TMW-1
PROJECT:Seneca Place Shopping Center
JOB NUMBER:AZA-002
LOCATION:Charlotte, NC
WELL LOG - HART HICKMAN.GDT - 4/20/15 15:04 - S:\AAA-MASTER GINT PROJECTS\AZA-001.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
0
5
10
15
20
GB
CONCRETE
Dry, slightly firm, red brown clayey SILT
Moist, slightly firm, red orange clayey SILT with dark
brown mineral inclusions
Wet, slightly firm, tan to red orange clayey SILT with darkbrown mineral inclusions (Saprolite)
Bottom of borehole at 20.0 feet.
1.6
1.8
2.4
0
0
0
Bentonite
Seal
1" PVCRiser
Filter Sand
Pack
1" Slotted
PVC Screen
DRAWN BY:CDO
BORING COMPLETED:3/30/15
DRILLING CONTRACTOR:Terra Sonic Remarks:
DRILL RIG/ METHOD:6620DT / HA/DPT
SAMPLING METHOD:Macro-Core Hand auger to 5ft BGS. Soil samplecollected from 10ft to 11ft BGS andsubmitted for laboratory analysis.
BORING STARTED:3/30/15
LOGGED BY:CBL
TOTAL DEPTH: 20 ft.
TOP OF CASING ELEV:
DEPTH TO WATER: 13.97 ft.DEPTH(ft)DEPTH(ft)RECOVERY (%)SAMPLE TYPENUMBERMATERIAL DESCRIPTION
LITHOLOGYSAMP.BKG.BLOWCOUNTS(N VALUE)WELL DIAGRAM
OVA (ppm)Sheet 1 of 1
BORING NUMBER SB-2/TMW-2
PROJECT:Seneca Place Shopping Center
JOB NUMBER:AZA-002
LOCATION:Charlotte, NC
WELL LOG - HART HICKMAN.GDT - 4/20/15 15:04 - S:\AAA-MASTER GINT PROJECTS\AZA-001.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
0
5
10
15
20
GB
CONCRETE, GRAVEL
Dry, slightly firm, red brown clayey SILT
Slightly moist, slightly firm, tan to orange brown clayeySILT with black to dark brown mineral inclusions
Wet, slightly firm, tan to orange brown clayey SILT with
black to dark brown mineral inclusions
Bottom of borehole at 15.0 feet.
1.8
0.3
0.1
0
0
0
0
0
DRAWN BY:CDO
BORING COMPLETED:3/30/15
DRILLING CONTRACTOR:Terra Sonic Remarks:
DRILL RIG/ METHOD:6620DT / HA/DPT
SAMPLING METHOD:Macro-Core Hand auger to 5ft BGS. Soil samplecollected from 9ft to 10ft BGS andsubmitted for laboratory analysis.
BORING STARTED:3/30/15
LOGGED BY:CBL
TOTAL DEPTH: 15 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)RECOVERY (%)SAMPLE TYPENUMBERMATERIAL DESCRIPTION
LITHOLOGYSAMP.BKG.BLOWCOUNTS(N VALUE)WELL DIAGRAM
OVA (ppm)Sheet 1 of 1
BORING NUMBER SB-3
PROJECT:Seneca Place Shopping Center
JOB NUMBER:AZA-002
LOCATION:Charlotte, NC
WELL LOG - HART HICKMAN.GDT - 4/20/15 15:04 - S:\AAA-MASTER GINT PROJECTS\AZA-001.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
0
5
10
15
GB
CONCRETE, GRAVEL
Dry, slightly firm, red brown clayey SILT
Dry, firm, tan to red brown clayey SILT
Bottom of borehole at 6.0 feet.
0.7
0.8
0
0
DRAWN BY:CDO
BORING COMPLETED:3/30/15
DRILLING CONTRACTOR:Terra Sonic Remarks:
DRILL RIG/ METHOD:N/A / HA
SAMPLING METHOD:Auger Cuttings Hand auger to 5ft BGS. Soil samplecollected from 5ft BGS and submittedfor laboratory analysis.
BORING STARTED:3/30/15
LOGGED BY:CBL
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)RECOVERY (%)SAMPLE TYPENUMBERMATERIAL DESCRIPTION
LITHOLOGYSAMP.BKG.BLOWCOUNTS(N VALUE)WELL DIAGRAM
OVA (ppm)Sheet 1 of 1
BORING NUMBER SB-4
PROJECT:Seneca Place Shopping Center
JOB NUMBER:AZA-002
LOCATION:Charlotte, NC
WELL LOG - HART HICKMAN.GDT - 4/20/15 15:04 - S:\AAA-MASTER GINT PROJECTS\AZA-001.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
0.0
2.5
5.0
GB
CONCRETE, GRAVEL
Dry, slightly firm, red brown clayey SILT
Dry, firm, tan to red brown clayey SILT
Bottom of borehole at 6.0 feet.
2.3
2.5
0
0
DRAWN BY:CDO
BORING COMPLETED:3/30/15
DRILLING CONTRACTOR:Terra Sonic Remarks:
DRILL RIG/ METHOD:N/A / HA
SAMPLING METHOD:Auger Cuttings Hand auger to 5ft BGS. Soil samplecollected from 5ft BGS and submittedfor laboratory analysis.
BORING STARTED:3/30/15
LOGGED BY:CBL
TOTAL DEPTH: 6 ft.
TOP OF CASING ELEV:
DEPTH TO WATER:DEPTH(ft)DEPTH(ft)RECOVERY (%)SAMPLE TYPENUMBERMATERIAL DESCRIPTION
LITHOLOGYSAMP.BKG.BLOWCOUNTS(N VALUE)WELL DIAGRAM
OVA (ppm)Sheet 1 of 1
BORING NUMBER SB-5
PROJECT:Seneca Place Shopping Center
JOB NUMBER:AZA-002
LOCATION:Charlotte, NC
WELL LOG - HART HICKMAN.GDT - 4/20/15 15:04 - S:\AAA-MASTER GINT PROJECTS\AZA-001.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0.0
2.5
5.0
0.0
2.5
5.0
GB
ASPHALT, GRAVEL
Dry, firm, red brown clayey SILT
Dry, firm, tan to red brown clayey SILT with trace finesands and dark brown mineral inclusions
Slightly moist, firm, tan to red brown clayey SILT withtrace fine sands and dark brown mineral inclusions
Moist, very firm, tan to red orange sandy clayey SILT
Wet, soft to slightly firm, tan to orange brown sandy clayeySILT
Bottom of borehole at 20.0 feet.
0.9
1.7
1.8
1.2
0
0
0
0
Bentonite
Seal
1" PVCRiser
Filter Sand
Pack
1" Slotted
PVC Screen
DRAWN BY:CDO
BORING COMPLETED:3/30/15
DRILLING CONTRACTOR:Terra Sonic Remarks:
DRILL RIG/ METHOD:6620DT / HA/DPT
SAMPLING METHOD:Macro-Core Hand auger to 5ft BGS. Soil samplecollected from 10ft BGS and submittedfor laboratory analysis.
BORING STARTED:3/30/15
LOGGED BY:CBL
TOTAL DEPTH: 20 ft.
TOP OF CASING ELEV:
DEPTH TO WATER: 15.75 ft.DEPTH(ft)DEPTH(ft)RECOVERY (%)SAMPLE TYPENUMBERMATERIAL DESCRIPTION
LITHOLOGYSAMP.BKG.BLOWCOUNTS(N VALUE)WELL DIAGRAM
OVA (ppm)Sheet 1 of 1
BORING NUMBER SB-6/TMW-3
PROJECT:Seneca Place Shopping Center
JOB NUMBER:AZA-002
LOCATION:Charlotte, NC
WELL LOG - HART HICKMAN.GDT - 4/20/15 15:04 - S:\AAA-MASTER GINT PROJECTS\AZA-001.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
0
5
10
15
20
GB
CONCRETE, GRAVEL
Dry, firm, red brown clayey SILT
Slightly moist, firm, tan to red orange clayey SILT with
trace fine sands and dark brown mineral inclusions
Moist to very moist, firm, tan to red orange clayey SILTwith trace fine sands and dark brown mineral inclusions
Wet, firm, tan to red orange sandy clayey SILT with darkbrown mineral inclusions
Bottom of borehole at 20.0 feet.
2.5
2.6
2.3
0
0
0
Bentonite
Seal
1" PVCRiser
Filter Sand
Pack
1" Slotted
PVC Screen
DRAWN BY:CDO
BORING COMPLETED:3/30/15
DRILLING CONTRACTOR:Terra Sonic Remarks:
DRILL RIG/ METHOD:6620DT / HA/DPT
SAMPLING METHOD:Macro-Core Hand auger to 5ft BGS. Soil samplecollected from 8ft to 9ft BGS andsubmitted for laboratory analysis.
BORING STARTED:3/30/15
LOGGED BY:CBL
TOTAL DEPTH: 20 ft.
TOP OF CASING ELEV:
DEPTH TO WATER: 14.31 ft.DEPTH(ft)DEPTH(ft)RECOVERY (%)SAMPLE TYPENUMBERMATERIAL DESCRIPTION
LITHOLOGYSAMP.BKG.BLOWCOUNTS(N VALUE)WELL DIAGRAM
OVA (ppm)Sheet 1 of 1
BORING NUMBER SB-7/TMW-4
PROJECT:Seneca Place Shopping Center
JOB NUMBER:AZA-002
LOCATION:Charlotte, NC
WELL LOG - HART HICKMAN.GDT - 4/20/15 15:04 - S:\AAA-MASTER GINT PROJECTS\AZA-001.GPJ2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
3334 Hillsborough Street
Raleigh, North Carolina 27607
919-847-4241(p) 919-847-4261(f)
0
5
10
15
20
0
5
10
15
20
APPENDIX B
Laboratory Analytical Report

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-75581-1
TestAmerica Sample Delivery Group: AZA-001
Client Project/Site: Seneca Place Shopping Center
Revision: 1
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: John Lopez
Authorized for release by:
4/8/2015 5:45:57 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
1
2
3
4
5
6
7
8
9
10
11
12
13
Table of Contents
Client: Hart & Hickman, PC
Project/Site: Seneca Place Shopping Center
TestAmerica Job ID: 490-75581-1
SDG: AZA-001
Page 2 of 86 TestAmerica Nashville4/8/2015
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .51
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .76
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .79
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .82
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .83
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .84
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .86
1
2
3
4
5
6
7
8
9
10
11
12
13
Sample Summary
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-75581-1 SB-2 (10-11)Solid 03/30/15 10:30 04/01/15 08:00
490-75581-2 SB-3 (9-10)Solid 03/30/15 11:00 04/01/15 08:00
490-75581-3 SB-4 (5)Solid 03/30/15 13:00 04/01/15 08:00
490-75581-4 SB-5 (5)Solid 03/30/15 13:20 04/01/15 08:00
490-75581-5 SB-6 (10)Solid 03/30/15 13:45 04/01/15 08:00
490-75581-6 SB-1 (8-9)Solid 03/30/15 14:20 04/01/15 08:00
490-75581-7 MW-7 Water 03/30/15 09:10 04/01/15 08:00
490-75581-8 TMW-1 Water 03/30/15 12:10 04/01/15 08:00
490-75581-9 TMW-2 Water 03/30/15 14:00 04/01/15 08:00
490-75581-10 TMW-3 Water 03/30/15 14:50 04/01/15 08:00
490-75581-11 TMW-4 Water 03/30/15 15:50 04/01/15 08:00
490-75581-12 MW-11 Water 03/30/15 16:50 04/01/15 08:00
490-75581-13 MW-8 Water 03/30/15 17:15 04/01/15 08:00
TestAmerica Nashville
Page 3 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-75581-1
Project/Site: Seneca Place Shopping Center SDG: AZA-001
Job ID: 490-75581-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-75581-1
REVISED REPORT: Revised to change the sample ID on sample 490-75581-13 from MW-6 to MW-8 due to error reading handwritten
chain. This report replaces the one generated on 04/07/15 @ 1559.
Comments
No additional comments.
Receipt
The samples were received on 3/31/2015 6:45 PM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 2 coolers at receipt time were 1.6º C and 2.8º C.
GC/MS VOA
Method(s) 8260B: The laboratory control sample (LCS) for batch 252212 recovered outside control limits for five analytes. These analytes
were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method(s) 8270D: The continuing calibration verification (CCV) associated with batch 252258 recovered outside acceptance criteria, low
biased, for Indeno(1,2,3-cd)pyrene, Benzo(g,h,i)perylene, Chrysene, Bis(2-chloroethoxy)methane and Dibenz(a,h)anthracene. A reporting
limit (RL) standard was analyzed, and the target analyte was detected. Since the associated samples were non-detect for this analyte, the
data have been reported.
Method(s) 8270D: The continuing calibration verification (CCV) associated with batch 252322 recovered outside acceptance criteria, low
biased, for 3,3'-Dichlorobenzidine. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the
associated samples were non-detect for this analyte, the data have been reported.
Method(s) 8270D: The following analyte(s) recovered outside control limits for the LCS/LCSD associated with batch 251993:
Hexachloroethane and 1,4-Dichlorobenzene. This is not indicative of a systematic control problem because these were random marginal
exceedances. Qualified results have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
Method(s) 3520C, 625: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated
with batch 251993.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica NashvillePage 4 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Definitions/Glossary
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Qualifiers
GC/MS VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
F1 MS and/or MSD Recovery exceeds the control limits
*LCS or LCSD exceeds the control limits
GC/MS Semi VOA
Qualifier Description
F1 MS and/or MSD Recovery exceeds the control limits
Qualifier
*LCS or LCSD exceeds the control limits
*RPD of the LCS and LCSD exceeds the control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Nashville
Page 5 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-1Client Sample ID: SB-2 (10-11)
Matrix: SolidDate Collected: 03/30/15 10:30
Percent Solids: 71.0Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 32.4 28.6 ug/Kg ☼04/05/15 09:40 04/05/15 11:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Benzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Bromobenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Bromochloromethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Bromodichloromethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Bromoform ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Bromomethane ND
28.6 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼2-Butanone (MEK)ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Carbon disulfide ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Carbon tetrachloride ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Chlorobenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Chlorodibromomethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Chloroethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Chloroform ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Chloromethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼2-Chlorotoluene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼4-Chlorotoluene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼cis-1,2-Dichloroethene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼cis-1,3-Dichloropropene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2-Dibromo-3-Chloropropane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2-Dibromoethane (EDB)ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Dibromomethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2-Dichlorobenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,3-Dichlorobenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,4-Dichlorobenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Dichlorodifluoromethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,1-Dichloroethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2-Dichloroethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,1-Dichloroethene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2-Dichloroethene, Total ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2-Dichloropropane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,3-Dichloropropane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼2,2-Dichloropropane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,1-Dichloropropene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Diisopropyl ether ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Ethylbenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Hexachlorobutadiene ND
28.6 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼2-Hexanone ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Isopropylbenzene ND
17.2 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Methylene Chloride ND
28.6 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼4-Methyl-2-pentanone (MIBK)ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Methyl tert-butyl ether ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Naphthalene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼n-Butylbenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼N-Propylbenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼p-Isopropyltoluene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼sec-Butylbenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Styrene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼tert-Butylbenzene ND
TestAmerica Nashville
Page 6 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-1Client Sample ID: SB-2 (10-11)
Matrix: SolidDate Collected: 03/30/15 10:30
Percent Solids: 71.0Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 5.73 ug/Kg ☼04/05/15 09:40 04/05/15 11:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,1,2,2-Tetrachloroethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Tetrachloroethene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Toluene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼trans-1,2-Dichloroethene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼trans-1,3-Dichloropropene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2,3-Trichlorobenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2,4-Trichlorobenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,1,1-Trichloroethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,1,2-Trichloroethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Trichloroethene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Trichlorofluoromethane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2,3-Trichloropropane ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,2,4-Trimethylbenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼1,3,5-Trimethylbenzene ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Vinyl chloride ND
5.73 ug/Kg 04/05/15 09:40 04/05/15 11:35 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)107 50-150 04/05/15 09:40 04/05/15 11:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)100 04/05/15 09:40 04/05/15 11:35 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.453 mg/Kg ☼04/03/15 09:35 04/06/15 22:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Acenaphthylene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Anthracene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Benzo[a]anthracene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Benzo[a]pyrene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Benzo[b]fluoranthene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Benzo[g,h,i]perylene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Benzo[k]fluoranthene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Bis(2-chloroethoxy)methane ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Bis(2-chloroethyl)ether ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼bis (2-chloroisopropyl) ether ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Bis(2-ethylhexyl) phthalate 0.634
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼4-Bromophenyl phenyl ether ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Butyl benzyl phthalate ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Carbazole ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼4-Chloroaniline ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼4-Chloro-3-methylphenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2-Chloronaphthalene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2-Chlorophenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼4-Chlorophenyl phenyl ether ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Chrysene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Dibenz(a,h)anthracene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Dibenzofuran ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼1,2-Dichlorobenzene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼1,3-Dichlorobenzene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼1,4-Dichlorobenzene ND
TestAmerica Nashville
Page 7 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-1Client Sample ID: SB-2 (10-11)
Matrix: SolidDate Collected: 03/30/15 10:30
Percent Solids: 71.0Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.453 mg/Kg ☼04/03/15 09:35 04/06/15 22:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2,4-Dichlorophenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Diethyl phthalate ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2,4-Dimethylphenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Dimethyl phthalate ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Di-n-butyl phthalate ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼4,6-Dinitro-2-methylphenol ND
1.36 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2,4-Dinitrophenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2,4-Dinitrotoluene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2,6-Dinitrotoluene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Di-n-octyl phthalate ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Fluoranthene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Fluorene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Hexachlorobenzene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Hexachlorobutadiene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Hexachlorocyclopentadiene ND F1
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Hexachloroethane ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Indeno[1,2,3-cd]pyrene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Isophorone ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼1-Methylnaphthalene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2-Methylnaphthalene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2-Methylphenol ND
0.907 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼3 & 4 Methylphenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Naphthalene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2-Nitroaniline ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼3-Nitroaniline ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼4-Nitroaniline ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Nitrobenzene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2-Nitrophenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼4-Nitrophenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼N-Nitrosodi-n-propylamine ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.907 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Pentachlorophenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Phenanthrene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Phenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼Pyrene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼1,2,4-Trichlorobenzene ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2,4,5-Trichlorophenol ND
0.453 mg/Kg 04/03/15 09:35 04/06/15 22:56 1☼2,4,6-Trichlorophenol ND
2-Fluorophenol (Surr)68 25-128 04/03/15 09:35 04/06/15 22:56 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)68 04/03/15 09:35 04/06/15 22:56 115-136
Phenol-d5 (Surr)71 04/03/15 09:35 04/06/15 22:56 129-130
Terphenyl-d14 (Surr)74 04/03/15 09:35 04/06/15 22:56 124-146
2,4,6-Tribromophenol (Surr)64 04/03/15 09:35 04/06/15 22:56 110-150
TestAmerica Nashville
Page 8 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-1Client Sample ID: SB-2 (10-11)
Matrix: SolidDate Collected: 03/30/15 10:30
Date Received: 04/01/15 08:00
General Chemistry
RL MDL
Percent Moisture 29 0.10 %04/03/15 09:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 9 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-2Client Sample ID: SB-3 (9-10)
Matrix: SolidDate Collected: 03/30/15 11:00
Percent Solids: 61.3Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 49.2 33.6 ug/Kg ☼04/05/15 09:40 04/05/15 12:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Benzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Bromobenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Bromochloromethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Bromodichloromethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Bromoform ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Bromomethane ND
33.6 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼2-Butanone (MEK)ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Carbon disulfide ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Carbon tetrachloride ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Chlorobenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Chlorodibromomethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Chloroethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Chloroform ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Chloromethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼2-Chlorotoluene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼4-Chlorotoluene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼cis-1,2-Dichloroethene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼cis-1,3-Dichloropropene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2-Dibromo-3-Chloropropane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2-Dibromoethane (EDB)ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Dibromomethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2-Dichlorobenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,3-Dichlorobenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,4-Dichlorobenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Dichlorodifluoromethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,1-Dichloroethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2-Dichloroethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,1-Dichloroethene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2-Dichloroethene, Total ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2-Dichloropropane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,3-Dichloropropane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼2,2-Dichloropropane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,1-Dichloropropene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Diisopropyl ether ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Ethylbenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Hexachlorobutadiene ND
33.6 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼2-Hexanone ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Isopropylbenzene ND
20.2 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Methylene Chloride ND
33.6 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼4-Methyl-2-pentanone (MIBK)ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Methyl tert-butyl ether ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Naphthalene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼n-Butylbenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼N-Propylbenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼p-Isopropyltoluene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼sec-Butylbenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Styrene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼tert-Butylbenzene ND
TestAmerica Nashville
Page 10 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-2Client Sample ID: SB-3 (9-10)
Matrix: SolidDate Collected: 03/30/15 11:00
Percent Solids: 61.3Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 6.73 ug/Kg ☼04/05/15 09:40 04/05/15 12:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,1,2,2-Tetrachloroethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Tetrachloroethene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Toluene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼trans-1,2-Dichloroethene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼trans-1,3-Dichloropropene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2,3-Trichlorobenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2,4-Trichlorobenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,1,1-Trichloroethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,1,2-Trichloroethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Trichloroethene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Trichlorofluoromethane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2,3-Trichloropropane ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,2,4-Trimethylbenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼1,3,5-Trimethylbenzene ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Vinyl chloride ND
6.73 ug/Kg 04/05/15 09:40 04/05/15 12:00 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)106 50-150 04/05/15 09:40 04/05/15 12:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)101 04/05/15 09:40 04/05/15 12:00 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.532 mg/Kg ☼04/03/15 09:35 04/06/15 23:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Acenaphthylene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Anthracene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Benzo[a]anthracene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Benzo[a]pyrene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Benzo[b]fluoranthene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Benzo[g,h,i]perylene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Benzo[k]fluoranthene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Bis(2-chloroethoxy)methane ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Bis(2-chloroethyl)ether ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼bis (2-chloroisopropyl) ether ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Bis(2-ethylhexyl) phthalate ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼4-Bromophenyl phenyl ether ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Butyl benzyl phthalate ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Carbazole ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼4-Chloroaniline ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼4-Chloro-3-methylphenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2-Chloronaphthalene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2-Chlorophenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼4-Chlorophenyl phenyl ether ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Chrysene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Dibenz(a,h)anthracene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Dibenzofuran ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼1,2-Dichlorobenzene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼1,3-Dichlorobenzene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼1,4-Dichlorobenzene ND
TestAmerica Nashville
Page 11 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-2Client Sample ID: SB-3 (9-10)
Matrix: SolidDate Collected: 03/30/15 11:00
Percent Solids: 61.3Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.532 mg/Kg ☼04/03/15 09:35 04/06/15 23:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2,4-Dichlorophenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Diethyl phthalate ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2,4-Dimethylphenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Dimethyl phthalate ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Di-n-butyl phthalate ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼4,6-Dinitro-2-methylphenol ND
1.60 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2,4-Dinitrophenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2,4-Dinitrotoluene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2,6-Dinitrotoluene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Di-n-octyl phthalate ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Fluoranthene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Fluorene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Hexachlorobenzene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Hexachlorobutadiene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Hexachlorocyclopentadiene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Hexachloroethane ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Indeno[1,2,3-cd]pyrene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Isophorone ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼1-Methylnaphthalene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2-Methylnaphthalene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2-Methylphenol ND
1.06 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼3 & 4 Methylphenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Naphthalene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2-Nitroaniline ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼3-Nitroaniline ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼4-Nitroaniline ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Nitrobenzene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2-Nitrophenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼4-Nitrophenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼N-Nitrosodi-n-propylamine ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
1.06 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Pentachlorophenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Phenanthrene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Phenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼Pyrene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼1,2,4-Trichlorobenzene ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2,4,5-Trichlorophenol ND
0.532 mg/Kg 04/03/15 09:35 04/06/15 23:32 1☼2,4,6-Trichlorophenol ND
2-Fluorophenol (Surr)80 25-128 04/03/15 09:35 04/06/15 23:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)85 04/03/15 09:35 04/06/15 23:32 115-136
Phenol-d5 (Surr)84 04/03/15 09:35 04/06/15 23:32 129-130
Terphenyl-d14 (Surr)80 04/03/15 09:35 04/06/15 23:32 124-146
2,4,6-Tribromophenol (Surr)64 04/03/15 09:35 04/06/15 23:32 110-150
TestAmerica Nashville
Page 12 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-2Client Sample ID: SB-3 (9-10)
Matrix: SolidDate Collected: 03/30/15 11:00
Date Received: 04/01/15 08:00
General Chemistry
RL MDL
Percent Moisture 39 0.10 %04/03/15 09:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 13 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-3Client Sample ID: SB-4 (5)
Matrix: SolidDate Collected: 03/30/15 13:00
Percent Solids: 76.9Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 39.6 27.3 ug/Kg ☼04/05/15 09:40 04/05/15 12:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Benzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Bromobenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Bromochloromethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Bromodichloromethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Bromoform ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Bromomethane ND
27.3 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼2-Butanone (MEK)ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Carbon disulfide ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Carbon tetrachloride ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Chlorobenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Chlorodibromomethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Chloroethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Chloroform ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Chloromethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼2-Chlorotoluene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼4-Chlorotoluene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼cis-1,2-Dichloroethene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼cis-1,3-Dichloropropene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2-Dibromo-3-Chloropropane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2-Dibromoethane (EDB)ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Dibromomethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2-Dichlorobenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,3-Dichlorobenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,4-Dichlorobenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Dichlorodifluoromethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,1-Dichloroethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2-Dichloroethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,1-Dichloroethene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2-Dichloroethene, Total ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2-Dichloropropane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,3-Dichloropropane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼2,2-Dichloropropane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,1-Dichloropropene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Diisopropyl ether ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Ethylbenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Hexachlorobutadiene ND
27.3 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼2-Hexanone ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Isopropylbenzene ND
16.4 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Methylene Chloride ND
27.3 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼4-Methyl-2-pentanone (MIBK)ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Methyl tert-butyl ether ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Naphthalene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼n-Butylbenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼N-Propylbenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼p-Isopropyltoluene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼sec-Butylbenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Styrene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼tert-Butylbenzene ND
TestAmerica Nashville
Page 14 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-3Client Sample ID: SB-4 (5)
Matrix: SolidDate Collected: 03/30/15 13:00
Percent Solids: 76.9Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 5.45 ug/Kg ☼04/05/15 09:40 04/05/15 12:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,1,2,2-Tetrachloroethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Tetrachloroethene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Toluene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼trans-1,2-Dichloroethene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼trans-1,3-Dichloropropene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2,3-Trichlorobenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2,4-Trichlorobenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,1,1-Trichloroethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,1,2-Trichloroethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Trichloroethene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Trichlorofluoromethane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2,3-Trichloropropane ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,2,4-Trimethylbenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼1,3,5-Trimethylbenzene ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Vinyl chloride ND
5.45 ug/Kg 04/05/15 09:40 04/05/15 12:26 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)111 50-150 04/05/15 09:40 04/05/15 12:26 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)103 04/05/15 09:40 04/05/15 12:26 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.424 mg/Kg ☼04/03/15 09:35 04/05/15 18:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Acenaphthylene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Anthracene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Benzo[a]anthracene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Benzo[a]pyrene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Benzo[b]fluoranthene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Benzo[g,h,i]perylene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Benzo[k]fluoranthene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Bis(2-chloroethoxy)methane ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Bis(2-chloroethyl)ether ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼bis (2-chloroisopropyl) ether ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Bis(2-ethylhexyl) phthalate ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼4-Bromophenyl phenyl ether ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Butyl benzyl phthalate ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Carbazole ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼4-Chloroaniline ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼4-Chloro-3-methylphenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2-Chloronaphthalene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2-Chlorophenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼4-Chlorophenyl phenyl ether ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Chrysene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Dibenz(a,h)anthracene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Dibenzofuran ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼1,2-Dichlorobenzene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼1,3-Dichlorobenzene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼1,4-Dichlorobenzene ND
TestAmerica Nashville
Page 15 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-3Client Sample ID: SB-4 (5)
Matrix: SolidDate Collected: 03/30/15 13:00
Percent Solids: 76.9Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.424 mg/Kg ☼04/03/15 09:35 04/05/15 18:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2,4-Dichlorophenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Diethyl phthalate ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2,4-Dimethylphenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Dimethyl phthalate ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Di-n-butyl phthalate ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼4,6-Dinitro-2-methylphenol ND
1.27 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2,4-Dinitrophenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2,4-Dinitrotoluene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2,6-Dinitrotoluene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Di-n-octyl phthalate ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Fluoranthene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Fluorene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Hexachlorobenzene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Hexachlorobutadiene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Hexachlorocyclopentadiene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Hexachloroethane ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Indeno[1,2,3-cd]pyrene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Isophorone ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼1-Methylnaphthalene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2-Methylnaphthalene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2-Methylphenol ND
0.847 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼3 & 4 Methylphenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Naphthalene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2-Nitroaniline ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼3-Nitroaniline ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼4-Nitroaniline ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Nitrobenzene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2-Nitrophenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼4-Nitrophenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼N-Nitrosodi-n-propylamine ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.847 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Pentachlorophenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Phenanthrene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Phenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼Pyrene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼1,2,4-Trichlorobenzene ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2,4,5-Trichlorophenol ND
0.424 mg/Kg 04/03/15 09:35 04/05/15 18:35 1☼2,4,6-Trichlorophenol ND
2-Fluorophenol (Surr)87 25-128 04/03/15 09:35 04/05/15 18:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)88 04/03/15 09:35 04/05/15 18:35 115-136
Phenol-d5 (Surr)90 04/03/15 09:35 04/05/15 18:35 129-130
Terphenyl-d14 (Surr)90 04/03/15 09:35 04/05/15 18:35 124-146
2,4,6-Tribromophenol (Surr)68 04/03/15 09:35 04/05/15 18:35 110-150
TestAmerica Nashville
Page 16 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-3Client Sample ID: SB-4 (5)
Matrix: SolidDate Collected: 03/30/15 13:00
Date Received: 04/01/15 08:00
General Chemistry
RL MDL
Percent Moisture 23 0.10 %04/03/15 09:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 17 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-4Client Sample ID: SB-5 (5)
Matrix: SolidDate Collected: 03/30/15 13:20
Percent Solids: 81.5Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 30.1 24.1 ug/Kg ☼04/05/15 09:40 04/05/15 12:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Benzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Bromobenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Bromochloromethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Bromodichloromethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Bromoform ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Bromomethane ND
24.1 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼2-Butanone (MEK)ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Carbon disulfide ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Carbon tetrachloride ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Chlorobenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Chlorodibromomethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Chloroethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Chloroform ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Chloromethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼2-Chlorotoluene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼4-Chlorotoluene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼cis-1,2-Dichloroethene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼cis-1,3-Dichloropropene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2-Dibromo-3-Chloropropane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2-Dibromoethane (EDB)ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Dibromomethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2-Dichlorobenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,3-Dichlorobenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,4-Dichlorobenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Dichlorodifluoromethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,1-Dichloroethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2-Dichloroethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,1-Dichloroethene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2-Dichloroethene, Total ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2-Dichloropropane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,3-Dichloropropane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼2,2-Dichloropropane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,1-Dichloropropene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Diisopropyl ether ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Ethylbenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Hexachlorobutadiene ND
24.1 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼2-Hexanone ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Isopropylbenzene ND
14.5 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Methylene Chloride ND
24.1 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼4-Methyl-2-pentanone (MIBK)ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Methyl tert-butyl ether ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Naphthalene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼n-Butylbenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼N-Propylbenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼p-Isopropyltoluene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼sec-Butylbenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Styrene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼tert-Butylbenzene ND
TestAmerica Nashville
Page 18 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-4Client Sample ID: SB-5 (5)
Matrix: SolidDate Collected: 03/30/15 13:20
Percent Solids: 81.5Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 4.82 ug/Kg ☼04/05/15 09:40 04/05/15 12:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,1,2,2-Tetrachloroethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Tetrachloroethene 17.8
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Toluene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼trans-1,2-Dichloroethene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼trans-1,3-Dichloropropene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2,3-Trichlorobenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2,4-Trichlorobenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,1,1-Trichloroethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,1,2-Trichloroethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Trichloroethene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Trichlorofluoromethane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2,3-Trichloropropane ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,2,4-Trimethylbenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼1,3,5-Trimethylbenzene ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Vinyl chloride ND
4.82 ug/Kg 04/05/15 09:40 04/05/15 12:51 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)112 50-150 04/05/15 09:40 04/05/15 12:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)99 04/05/15 09:40 04/05/15 12:51 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.393 mg/Kg ☼04/03/15 09:35 04/05/15 19:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Acenaphthylene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Anthracene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Benzo[a]anthracene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Benzo[a]pyrene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Benzo[b]fluoranthene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Benzo[g,h,i]perylene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Benzo[k]fluoranthene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Bis(2-chloroethoxy)methane ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Bis(2-chloroethyl)ether ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼bis (2-chloroisopropyl) ether ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Bis(2-ethylhexyl) phthalate ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼4-Bromophenyl phenyl ether ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Butyl benzyl phthalate ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Carbazole ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼4-Chloroaniline ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼4-Chloro-3-methylphenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2-Chloronaphthalene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2-Chlorophenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼4-Chlorophenyl phenyl ether ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Chrysene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Dibenz(a,h)anthracene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Dibenzofuran ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼1,2-Dichlorobenzene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼1,3-Dichlorobenzene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼1,4-Dichlorobenzene ND
TestAmerica Nashville
Page 19 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-4Client Sample ID: SB-5 (5)
Matrix: SolidDate Collected: 03/30/15 13:20
Percent Solids: 81.5Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.393 mg/Kg ☼04/03/15 09:35 04/05/15 19:12 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2,4-Dichlorophenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Diethyl phthalate ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2,4-Dimethylphenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Dimethyl phthalate ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Di-n-butyl phthalate ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼4,6-Dinitro-2-methylphenol ND
1.18 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2,4-Dinitrophenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2,4-Dinitrotoluene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2,6-Dinitrotoluene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Di-n-octyl phthalate ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Fluoranthene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Fluorene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Hexachlorobenzene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Hexachlorobutadiene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Hexachlorocyclopentadiene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Hexachloroethane ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Indeno[1,2,3-cd]pyrene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Isophorone ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼1-Methylnaphthalene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2-Methylnaphthalene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2-Methylphenol ND
0.786 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼3 & 4 Methylphenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Naphthalene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2-Nitroaniline ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼3-Nitroaniline ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼4-Nitroaniline ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Nitrobenzene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2-Nitrophenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼4-Nitrophenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼N-Nitrosodi-n-propylamine ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.786 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Pentachlorophenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Phenanthrene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Phenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼Pyrene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼1,2,4-Trichlorobenzene ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2,4,5-Trichlorophenol ND
0.393 mg/Kg 04/03/15 09:35 04/05/15 19:12 1☼2,4,6-Trichlorophenol ND
2-Fluorophenol (Surr)78 25-128 04/03/15 09:35 04/05/15 19:12 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)81 04/03/15 09:35 04/05/15 19:12 115-136
Phenol-d5 (Surr)80 04/03/15 09:35 04/05/15 19:12 129-130
Terphenyl-d14 (Surr)87 04/03/15 09:35 04/05/15 19:12 124-146
2,4,6-Tribromophenol (Surr)61 04/03/15 09:35 04/05/15 19:12 110-150
TestAmerica Nashville
Page 20 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-4Client Sample ID: SB-5 (5)
Matrix: SolidDate Collected: 03/30/15 13:20
Date Received: 04/01/15 08:00
General Chemistry
RL MDL
Percent Moisture 19 0.10 %04/03/15 09:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 21 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-5Client Sample ID: SB-6 (10)
Matrix: SolidDate Collected: 03/30/15 13:45
Percent Solids: 66.6Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 36.8 30.5 ug/Kg ☼04/05/15 09:40 04/05/15 13:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Benzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Bromobenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Bromochloromethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Bromodichloromethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Bromoform ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Bromomethane ND
30.5 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼2-Butanone (MEK)ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Carbon disulfide ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Carbon tetrachloride ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Chlorobenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Chlorodibromomethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Chloroethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Chloroform ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Chloromethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼2-Chlorotoluene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼4-Chlorotoluene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼cis-1,2-Dichloroethene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼cis-1,3-Dichloropropene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2-Dibromo-3-Chloropropane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2-Dibromoethane (EDB)ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Dibromomethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2-Dichlorobenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,3-Dichlorobenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,4-Dichlorobenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Dichlorodifluoromethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,1-Dichloroethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2-Dichloroethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,1-Dichloroethene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2-Dichloroethene, Total ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2-Dichloropropane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,3-Dichloropropane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼2,2-Dichloropropane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,1-Dichloropropene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Diisopropyl ether ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Ethylbenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Hexachlorobutadiene ND
30.5 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼2-Hexanone ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Isopropylbenzene ND
18.3 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Methylene Chloride ND
30.5 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼4-Methyl-2-pentanone (MIBK)ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Methyl tert-butyl ether ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Naphthalene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼n-Butylbenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼N-Propylbenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼p-Isopropyltoluene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼sec-Butylbenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Styrene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼tert-Butylbenzene ND
TestAmerica Nashville
Page 22 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-5Client Sample ID: SB-6 (10)
Matrix: SolidDate Collected: 03/30/15 13:45
Percent Solids: 66.6Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 6.11 ug/Kg ☼04/05/15 09:40 04/05/15 13:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,1,2,2-Tetrachloroethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Tetrachloroethene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Toluene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼trans-1,2-Dichloroethene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼trans-1,3-Dichloropropene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2,3-Trichlorobenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2,4-Trichlorobenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,1,1-Trichloroethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,1,2-Trichloroethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Trichloroethene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Trichlorofluoromethane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2,3-Trichloropropane ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,2,4-Trimethylbenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼1,3,5-Trimethylbenzene ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Vinyl chloride ND
6.11 ug/Kg 04/05/15 09:40 04/05/15 13:17 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)109 50-150 04/05/15 09:40 04/05/15 13:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)100 04/05/15 09:40 04/05/15 13:17 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.493 mg/Kg ☼04/03/15 09:35 04/05/15 19:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Acenaphthylene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Anthracene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Benzo[a]anthracene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Benzo[a]pyrene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Benzo[b]fluoranthene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Benzo[g,h,i]perylene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Benzo[k]fluoranthene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Bis(2-chloroethoxy)methane ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Bis(2-chloroethyl)ether ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼bis (2-chloroisopropyl) ether ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Bis(2-ethylhexyl) phthalate ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼4-Bromophenyl phenyl ether ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Butyl benzyl phthalate ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Carbazole ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼4-Chloroaniline ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼4-Chloro-3-methylphenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2-Chloronaphthalene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2-Chlorophenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼4-Chlorophenyl phenyl ether ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Chrysene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Dibenz(a,h)anthracene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Dibenzofuran ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼1,2-Dichlorobenzene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼1,3-Dichlorobenzene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼1,4-Dichlorobenzene ND
TestAmerica Nashville
Page 23 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-5Client Sample ID: SB-6 (10)
Matrix: SolidDate Collected: 03/30/15 13:45
Percent Solids: 66.6Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.493 mg/Kg ☼04/03/15 09:35 04/05/15 19:48 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2,4-Dichlorophenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Diethyl phthalate ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2,4-Dimethylphenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Dimethyl phthalate ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Di-n-butyl phthalate ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼4,6-Dinitro-2-methylphenol ND
1.48 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2,4-Dinitrophenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2,4-Dinitrotoluene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2,6-Dinitrotoluene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Di-n-octyl phthalate ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Fluoranthene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Fluorene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Hexachlorobenzene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Hexachlorobutadiene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Hexachlorocyclopentadiene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Hexachloroethane ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Indeno[1,2,3-cd]pyrene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Isophorone ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼1-Methylnaphthalene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2-Methylnaphthalene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2-Methylphenol ND
0.986 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼3 & 4 Methylphenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Naphthalene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2-Nitroaniline ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼3-Nitroaniline ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼4-Nitroaniline ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Nitrobenzene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2-Nitrophenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼4-Nitrophenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼N-Nitrosodi-n-propylamine ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.986 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Pentachlorophenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Phenanthrene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Phenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼Pyrene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼1,2,4-Trichlorobenzene ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2,4,5-Trichlorophenol ND
0.493 mg/Kg 04/03/15 09:35 04/05/15 19:48 1☼2,4,6-Trichlorophenol ND
2-Fluorophenol (Surr)69 25-128 04/03/15 09:35 04/05/15 19:48 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)69 04/03/15 09:35 04/05/15 19:48 115-136
Phenol-d5 (Surr)70 04/03/15 09:35 04/05/15 19:48 129-130
Terphenyl-d14 (Surr)80 04/03/15 09:35 04/05/15 19:48 124-146
2,4,6-Tribromophenol (Surr)54 04/03/15 09:35 04/05/15 19:48 110-150
TestAmerica Nashville
Page 24 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-5Client Sample ID: SB-6 (10)
Matrix: SolidDate Collected: 03/30/15 13:45
Date Received: 04/01/15 08:00
General Chemistry
RL MDL
Percent Moisture 33 0.10 %04/03/15 11:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 25 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-6Client Sample ID: SB-1 (8-9)
Matrix: SolidDate Collected: 03/30/15 14:20
Percent Solids: 64.5Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 30.1 ug/Kg ☼04/05/15 09:40 04/05/15 13:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Benzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Bromobenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Bromochloromethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Bromodichloromethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Bromoform ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Bromomethane ND
30.1 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼2-Butanone (MEK)ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Carbon disulfide ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Carbon tetrachloride ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Chlorobenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Chlorodibromomethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Chloroethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Chloroform ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Chloromethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼2-Chlorotoluene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼4-Chlorotoluene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼cis-1,2-Dichloroethene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼cis-1,3-Dichloropropene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2-Dibromo-3-Chloropropane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2-Dibromoethane (EDB)ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Dibromomethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2-Dichlorobenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,3-Dichlorobenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,4-Dichlorobenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Dichlorodifluoromethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,1-Dichloroethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2-Dichloroethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,1-Dichloroethene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2-Dichloroethene, Total ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2-Dichloropropane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,3-Dichloropropane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼2,2-Dichloropropane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,1-Dichloropropene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Diisopropyl ether ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Ethylbenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Hexachlorobutadiene ND
30.1 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼2-Hexanone ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Isopropylbenzene ND
18.1 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Methylene Chloride ND
30.1 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼4-Methyl-2-pentanone (MIBK)ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Methyl tert-butyl ether ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Naphthalene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼n-Butylbenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼N-Propylbenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼p-Isopropyltoluene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼sec-Butylbenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Styrene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼tert-Butylbenzene ND
TestAmerica Nashville
Page 26 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-6Client Sample ID: SB-1 (8-9)
Matrix: SolidDate Collected: 03/30/15 14:20
Percent Solids: 64.5Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 6.02 ug/Kg ☼04/05/15 09:40 04/05/15 13:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,1,2,2-Tetrachloroethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Tetrachloroethene 17.0
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Toluene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼trans-1,2-Dichloroethene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼trans-1,3-Dichloropropene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2,3-Trichlorobenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2,4-Trichlorobenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,1,1-Trichloroethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,1,2-Trichloroethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Trichloroethene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Trichlorofluoromethane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2,3-Trichloropropane ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,2,4-Trimethylbenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼1,3,5-Trimethylbenzene ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Vinyl chloride ND
6.02 ug/Kg 04/05/15 09:40 04/05/15 13:41 1☼Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)105 50-150 04/05/15 09:40 04/05/15 13:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)101 04/05/15 09:40 04/05/15 13:41 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.504 mg/Kg ☼04/03/15 09:35 04/05/15 20:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Acenaphthylene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Anthracene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Benzo[a]anthracene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Benzo[a]pyrene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Benzo[b]fluoranthene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Benzo[g,h,i]perylene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Benzo[k]fluoranthene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Bis(2-chloroethoxy)methane ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Bis(2-chloroethyl)ether ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼bis (2-chloroisopropyl) ether ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Bis(2-ethylhexyl) phthalate ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼4-Bromophenyl phenyl ether ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Butyl benzyl phthalate ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Carbazole ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼4-Chloroaniline ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼4-Chloro-3-methylphenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2-Chloronaphthalene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2-Chlorophenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼4-Chlorophenyl phenyl ether ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Chrysene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Dibenz(a,h)anthracene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Dibenzofuran ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼1,2-Dichlorobenzene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼1,3-Dichlorobenzene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼1,4-Dichlorobenzene ND
TestAmerica Nashville
Page 27 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-6Client Sample ID: SB-1 (8-9)
Matrix: SolidDate Collected: 03/30/15 14:20
Percent Solids: 64.5Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
3,3'-Dichlorobenzidine ND 0.504 mg/Kg ☼04/03/15 09:35 04/05/15 20:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2,4-Dichlorophenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Diethyl phthalate ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2,4-Dimethylphenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Dimethyl phthalate ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Di-n-butyl phthalate ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼4,6-Dinitro-2-methylphenol ND
1.51 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2,4-Dinitrophenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2,4-Dinitrotoluene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2,6-Dinitrotoluene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Di-n-octyl phthalate ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Fluoranthene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Fluorene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Hexachlorobenzene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Hexachlorobutadiene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Hexachlorocyclopentadiene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Hexachloroethane ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Indeno[1,2,3-cd]pyrene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Isophorone ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼1-Methylnaphthalene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2-Methylnaphthalene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2-Methylphenol ND
1.01 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼3 & 4 Methylphenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Naphthalene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2-Nitroaniline ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼3-Nitroaniline ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼4-Nitroaniline ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Nitrobenzene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2-Nitrophenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼4-Nitrophenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼N-Nitrosodi-n-propylamine ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
1.01 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Pentachlorophenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Phenanthrene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Phenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼Pyrene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼1,2,4-Trichlorobenzene ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2,4,5-Trichlorophenol ND
0.504 mg/Kg 04/03/15 09:35 04/05/15 20:24 1☼2,4,6-Trichlorophenol ND
2-Fluorophenol (Surr)93 25-128 04/03/15 09:35 04/05/15 20:24 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)94 04/03/15 09:35 04/05/15 20:24 115-136
Phenol-d5 (Surr)95 04/03/15 09:35 04/05/15 20:24 129-130
Terphenyl-d14 (Surr)92 04/03/15 09:35 04/05/15 20:24 124-146
2,4,6-Tribromophenol (Surr)74 04/03/15 09:35 04/05/15 20:24 110-150
TestAmerica Nashville
Page 28 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-6Client Sample ID: SB-1 (8-9)
Matrix: SolidDate Collected: 03/30/15 14:20
Date Received: 04/01/15 08:00
General Chemistry
RL MDL
Percent Moisture 35 0.10 %04/03/15 11:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
TestAmerica Nashville
Page 29 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-7Client Sample ID: MW-7
Matrix: WaterDate Collected: 03/30/15 09:10
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 04/04/15 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 16:51 1BenzeneND
1.00 ug/L 04/04/15 16:51 1BromobenzeneND*
1.00 ug/L 04/04/15 16:51 1BromochloromethaneND
1.00 ug/L 04/04/15 16:51 1BromodichloromethaneND
5.00 ug/L 04/04/15 16:51 1BromoformND*
1.00 ug/L 04/04/15 16:51 1BromomethaneND
25.0 ug/L 04/04/15 16:51 12-Butanone (MEK)ND
1.00 ug/L 04/04/15 16:51 1Carbon disulfide ND
1.00 ug/L 04/04/15 16:51 1Carbon tetrachloride ND
1.00 ug/L 04/04/15 16:51 1ChlorobenzeneND
1.00 ug/L 04/04/15 16:51 1ChlorodibromomethaneND
1.00 ug/L 04/04/15 16:51 1ChloroethaneND
1.00 ug/L 04/04/15 16:51 1Chloroform17.4
1.00 ug/L 04/04/15 16:51 1ChloromethaneND
1.00 ug/L 04/04/15 16:51 12-Chlorotoluene ND
1.00 ug/L 04/04/15 16:51 14-Chlorotoluene ND
1.00 ug/L 04/04/15 16:51 1cis-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 16:51 1cis-1,3-Dichloropropene ND
5.00 ug/L 04/04/15 16:51 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 04/04/15 16:51 11,2-Dibromoethane (EDB)ND *
5.00 ug/L 04/04/15 16:51 1DibromomethaneND
1.00 ug/L 04/04/15 16:51 11,2-Dichlorobenzene ND
1.00 ug/L 04/04/15 16:51 11,3-Dichlorobenzene ND
1.00 ug/L 04/04/15 16:51 11,4-Dichlorobenzene ND
1.00 ug/L 04/04/15 16:51 1DichlorodifluoromethaneND
1.00 ug/L 04/04/15 16:51 11,1-Dichloroethane ND
1.00 ug/L 04/04/15 16:51 11,2-Dichloroethane ND
1.00 ug/L 04/04/15 16:51 11,1-Dichloroethene ND
1.00 ug/L 04/04/15 16:51 11,2-Dichloroethene, Total ND
1.00 ug/L 04/04/15 16:51 11,2-Dichloropropane ND
1.00 ug/L 04/04/15 16:51 11,3-Dichloropropane ND
1.00 ug/L 04/04/15 16:51 12,2-Dichloropropane ND
1.00 ug/L 04/04/15 16:51 11,1-Dichloropropene ND
1.00 ug/L 04/04/15 16:51 1Diisopropyl ether ND
1.00 ug/L 04/04/15 16:51 1EthylbenzeneND
5.00 ug/L 04/04/15 16:51 1HexachlorobutadieneND
25.0 ug/L 04/04/15 16:51 12-Hexanone ND
1.00 ug/L 04/04/15 16:51 1IsopropylbenzeneND
5.00 ug/L 04/04/15 16:51 1Methylene Chloride ND
25.0 ug/L 04/04/15 16:51 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 04/04/15 16:51 1Methyl tert-butyl ether ND
1.00 ug/L 04/04/15 16:51 1NaphthaleneND*
1.00 ug/L 04/04/15 16:51 1n-Butylbenzene ND
1.00 ug/L 04/04/15 16:51 1N-Propylbenzene ND
1.00 ug/L 04/04/15 16:51 1p-Isopropyltoluene ND
1.00 ug/L 04/04/15 16:51 1sec-Butylbenzene ND
1.00 ug/L 04/04/15 16:51 1StyreneND
1.00 ug/L 04/04/15 16:51 1tert-Butylbenzene ND
TestAmerica Nashville
Page 30 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-7Client Sample ID: MW-7
Matrix: WaterDate Collected: 03/30/15 09:10
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 04/04/15 16:51 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 16:51 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 04/04/15 16:51 1TetrachloroetheneND
1.00 ug/L 04/04/15 16:51 1TolueneND
1.00 ug/L 04/04/15 16:51 1trans-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 16:51 1trans-1,3-Dichloropropene ND
1.00 ug/L 04/04/15 16:51 11,2,3-Trichlorobenzene ND *
1.00 ug/L 04/04/15 16:51 11,2,4-Trichlorobenzene ND
1.00 ug/L 04/04/15 16:51 11,1,1-Trichloroethane ND
5.00 ug/L 04/04/15 16:51 11,1,2-Trichloroethane ND
1.00 ug/L 04/04/15 16:51 1TrichloroetheneND
1.00 ug/L 04/04/15 16:51 1TrichlorofluoromethaneND
5.00 ug/L 04/04/15 16:51 11,2,3-Trichloropropane ND
1.00 ug/L 04/04/15 16:51 11,2,4-Trimethylbenzene ND
1.00 ug/L 04/04/15 16:51 11,3,5-Trimethylbenzene ND
1.00 ug/L 04/04/15 16:51 1Vinyl chloride ND
5.00 ug/L 04/04/15 16:51 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)98 67-134 04/04/15 16:51 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)109 04/04/15 16:51 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 11,2,4-Trichlorobenzene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 11,2-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 11,3-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 11,4-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 11-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12,4,5-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12,4,6-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12,4-Dichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12,4-Dimethylphenol ND
30.0 ug/L 04/02/15 11:06 04/06/15 18:41 12,4-Dinitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12,4-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12,6-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12-Chloronaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12-Chlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12-Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 12-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 13,3'-Dichlorobenzidine ND
20.0 ug/L 04/02/15 11:06 04/06/15 18:41 13 & 4 Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 13-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 14,6-Dinitro-2-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 14-Bromophenyl phenyl ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 14-Chloro-3-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 14-Chloroaniline ND
TestAmerica Nashville
Page 31 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-7Client Sample ID: MW-7
Matrix: WaterDate Collected: 03/30/15 09:10
Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Chlorophenyl phenyl ether ND 10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 14-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 14-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1AcenaphthyleneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1AnthraceneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Benzo[a]anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Benzo[a]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Benzo[b]fluoranthene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Benzo[g,h,i]perylene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Benzo[k]fluoranthene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Bis(2-chloroethoxy)methane ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Bis(2-chloroethyl)ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Butyl benzyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Bis(2-ethylhexyl) phthalate 13.1 *
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1CarbazoleND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1ChryseneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Dibenz(a,h)anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1DibenzofuranND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Diethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Dimethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Di-n-butyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1FluorantheneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1FluoreneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1HexachlorobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1HexachlorobutadieneND
20.0 ug/L 04/02/15 11:06 04/06/15 18:41 1HexachlorocyclopentadieneND*
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1HexachloroethaneND*
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Indeno[1,2,3-cd]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1IsophoroneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1NaphthaleneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1NitrobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1N-Nitrosodi-n-propylamine ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.0 ug/L 04/02/15 11:06 04/06/15 18:41 1PentachlorophenolND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1PhenanthreneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1PhenolND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1PyreneND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1Di-n-octyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 18:41 1bis (2-chloroisopropyl) ether ND
2,4,6-Tribromophenol (Surr)66 26-150 04/02/15 11:06 04/06/15 18:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)63 04/02/15 11:06 04/06/15 18:41 113-113
Nitrobenzene-d5 (Surr)84 04/02/15 11:06 04/06/15 18:41 136-126
Phenol-d5 (Surr)79 04/02/15 11:06 04/06/15 18:41 117-127
Terphenyl-d14 (Surr)100 04/02/15 11:06 04/06/15 18:41 144-149
TestAmerica Nashville
Page 32 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-8Client Sample ID: TMW-1
Matrix: WaterDate Collected: 03/30/15 12:10
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 04/04/15 17:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 17:17 1BenzeneND
1.00 ug/L 04/04/15 17:17 1BromobenzeneND*
1.00 ug/L 04/04/15 17:17 1BromochloromethaneND
1.00 ug/L 04/04/15 17:17 1BromodichloromethaneND
5.00 ug/L 04/04/15 17:17 1BromoformND*
1.00 ug/L 04/04/15 17:17 1BromomethaneND
25.0 ug/L 04/04/15 17:17 12-Butanone (MEK)ND
1.00 ug/L 04/04/15 17:17 1Carbon disulfide ND
1.00 ug/L 04/04/15 17:17 1Carbon tetrachloride ND
1.00 ug/L 04/04/15 17:17 1ChlorobenzeneND
1.00 ug/L 04/04/15 17:17 1ChlorodibromomethaneND
1.00 ug/L 04/04/15 17:17 1ChloroethaneND
1.00 ug/L 04/04/15 17:17 1ChloroformND
1.00 ug/L 04/04/15 17:17 1ChloromethaneND
1.00 ug/L 04/04/15 17:17 12-Chlorotoluene ND
1.00 ug/L 04/04/15 17:17 14-Chlorotoluene ND
1.00 ug/L 04/04/15 17:17 1cis-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 17:17 1cis-1,3-Dichloropropene ND
5.00 ug/L 04/04/15 17:17 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 04/04/15 17:17 11,2-Dibromoethane (EDB)ND *
5.00 ug/L 04/04/15 17:17 1DibromomethaneND
1.00 ug/L 04/04/15 17:17 11,2-Dichlorobenzene ND
1.00 ug/L 04/04/15 17:17 11,3-Dichlorobenzene ND
1.00 ug/L 04/04/15 17:17 11,4-Dichlorobenzene ND
1.00 ug/L 04/04/15 17:17 1DichlorodifluoromethaneND
1.00 ug/L 04/04/15 17:17 11,1-Dichloroethane ND
1.00 ug/L 04/04/15 17:17 11,2-Dichloroethane ND
1.00 ug/L 04/04/15 17:17 11,1-Dichloroethene ND
1.00 ug/L 04/04/15 17:17 11,2-Dichloroethene, Total ND
1.00 ug/L 04/04/15 17:17 11,2-Dichloropropane ND
1.00 ug/L 04/04/15 17:17 11,3-Dichloropropane ND
1.00 ug/L 04/04/15 17:17 12,2-Dichloropropane ND
1.00 ug/L 04/04/15 17:17 11,1-Dichloropropene ND
1.00 ug/L 04/04/15 17:17 1Diisopropyl ether ND
1.00 ug/L 04/04/15 17:17 1EthylbenzeneND
5.00 ug/L 04/04/15 17:17 1HexachlorobutadieneND
25.0 ug/L 04/04/15 17:17 12-Hexanone ND
1.00 ug/L 04/04/15 17:17 1IsopropylbenzeneND
5.00 ug/L 04/04/15 17:17 1Methylene Chloride ND
25.0 ug/L 04/04/15 17:17 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 04/04/15 17:17 1Methyl tert-butyl ether ND
1.00 ug/L 04/04/15 17:17 1NaphthaleneND*
1.00 ug/L 04/04/15 17:17 1n-Butylbenzene ND
1.00 ug/L 04/04/15 17:17 1N-Propylbenzene ND
1.00 ug/L 04/04/15 17:17 1p-Isopropyltoluene ND
1.00 ug/L 04/04/15 17:17 1sec-Butylbenzene ND
1.00 ug/L 04/04/15 17:17 1StyreneND
1.00 ug/L 04/04/15 17:17 1tert-Butylbenzene ND
TestAmerica Nashville
Page 33 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-8Client Sample ID: TMW-1
Matrix: WaterDate Collected: 03/30/15 12:10
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 04/04/15 17:17 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 17:17 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 04/04/15 17:17 1Tetrachloroethene35.3
1.00 ug/L 04/04/15 17:17 1TolueneND
1.00 ug/L 04/04/15 17:17 1trans-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 17:17 1trans-1,3-Dichloropropene ND
1.00 ug/L 04/04/15 17:17 11,2,3-Trichlorobenzene ND *
1.00 ug/L 04/04/15 17:17 11,2,4-Trichlorobenzene ND
1.00 ug/L 04/04/15 17:17 11,1,1-Trichloroethane ND
5.00 ug/L 04/04/15 17:17 11,1,2-Trichloroethane ND
1.00 ug/L 04/04/15 17:17 1TrichloroetheneND
1.00 ug/L 04/04/15 17:17 1TrichlorofluoromethaneND
5.00 ug/L 04/04/15 17:17 11,2,3-Trichloropropane ND
1.00 ug/L 04/04/15 17:17 11,2,4-Trimethylbenzene ND
1.00 ug/L 04/04/15 17:17 11,3,5-Trimethylbenzene ND
1.00 ug/L 04/04/15 17:17 1Vinyl chloride ND
5.00 ug/L 04/04/15 17:17 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)97 67-134 04/04/15 17:17 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)106 04/04/15 17:17 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 11,2,4-Trichlorobenzene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 11,2-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 11,3-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 11,4-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 11-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12,4,5-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12,4,6-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12,4-Dichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12,4-Dimethylphenol ND
30.0 ug/L 04/02/15 11:06 04/06/15 19:18 12,4-Dinitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12,4-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12,6-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12-Chloronaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12-Chlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12-Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 12-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 13,3'-Dichlorobenzidine ND
20.0 ug/L 04/02/15 11:06 04/06/15 19:18 13 & 4 Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 13-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 14,6-Dinitro-2-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 14-Bromophenyl phenyl ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 14-Chloro-3-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 14-Chloroaniline ND
TestAmerica Nashville
Page 34 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-8Client Sample ID: TMW-1
Matrix: WaterDate Collected: 03/30/15 12:10
Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Chlorophenyl phenyl ether ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 14-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 14-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1AcenaphthyleneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1AnthraceneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Benzo[a]anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Benzo[a]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Benzo[b]fluoranthene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Benzo[g,h,i]perylene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Benzo[k]fluoranthene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Bis(2-chloroethoxy)methane ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Bis(2-chloroethyl)ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Butyl benzyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Bis(2-ethylhexyl) phthalate ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1CarbazoleND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1ChryseneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Dibenz(a,h)anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1DibenzofuranND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Diethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Dimethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Di-n-butyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1FluorantheneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1FluoreneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1HexachlorobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1HexachlorobutadieneND
20.0 ug/L 04/02/15 11:06 04/06/15 19:18 1HexachlorocyclopentadieneND*
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1HexachloroethaneND*
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Indeno[1,2,3-cd]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1IsophoroneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1NaphthaleneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1NitrobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1N-Nitrosodi-n-propylamine ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.0 ug/L 04/02/15 11:06 04/06/15 19:18 1PentachlorophenolND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1PhenanthreneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1PhenolND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1PyreneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1Di-n-octyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:18 1bis (2-chloroisopropyl) ether ND
2,4,6-Tribromophenol (Surr)78 26-150 04/02/15 11:06 04/06/15 19:18 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)64 04/02/15 11:06 04/06/15 19:18 113-113
Nitrobenzene-d5 (Surr)91 04/02/15 11:06 04/06/15 19:18 136-126
Phenol-d5 (Surr)83 04/02/15 11:06 04/06/15 19:18 117-127
Terphenyl-d14 (Surr)89 04/02/15 11:06 04/06/15 19:18 144-149
TestAmerica Nashville
Page 35 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-9Client Sample ID: TMW-2
Matrix: WaterDate Collected: 03/30/15 14:00
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 04/04/15 17:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 17:42 1BenzeneND
1.00 ug/L 04/04/15 17:42 1BromobenzeneND*
1.00 ug/L 04/04/15 17:42 1BromochloromethaneND
1.00 ug/L 04/04/15 17:42 1BromodichloromethaneND
5.00 ug/L 04/04/15 17:42 1BromoformND*
1.00 ug/L 04/04/15 17:42 1BromomethaneND
25.0 ug/L 04/04/15 17:42 12-Butanone (MEK)ND
1.00 ug/L 04/04/15 17:42 1Carbon disulfide ND
1.00 ug/L 04/04/15 17:42 1Carbon tetrachloride ND
1.00 ug/L 04/04/15 17:42 1ChlorobenzeneND
1.00 ug/L 04/04/15 17:42 1ChlorodibromomethaneND
1.00 ug/L 04/04/15 17:42 1ChloroethaneND
1.00 ug/L 04/04/15 17:42 1ChloroformND
1.00 ug/L 04/04/15 17:42 1ChloromethaneND
1.00 ug/L 04/04/15 17:42 12-Chlorotoluene ND
1.00 ug/L 04/04/15 17:42 14-Chlorotoluene ND
1.00 ug/L 04/04/15 17:42 1cis-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 17:42 1cis-1,3-Dichloropropene ND
5.00 ug/L 04/04/15 17:42 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 04/04/15 17:42 11,2-Dibromoethane (EDB)ND *
5.00 ug/L 04/04/15 17:42 1DibromomethaneND
1.00 ug/L 04/04/15 17:42 11,2-Dichlorobenzene ND
1.00 ug/L 04/04/15 17:42 11,3-Dichlorobenzene ND
1.00 ug/L 04/04/15 17:42 11,4-Dichlorobenzene ND
1.00 ug/L 04/04/15 17:42 1DichlorodifluoromethaneND
1.00 ug/L 04/04/15 17:42 11,1-Dichloroethane ND
1.00 ug/L 04/04/15 17:42 11,2-Dichloroethane ND
1.00 ug/L 04/04/15 17:42 11,1-Dichloroethene ND
1.00 ug/L 04/04/15 17:42 11,2-Dichloroethene, Total ND
1.00 ug/L 04/04/15 17:42 11,2-Dichloropropane ND
1.00 ug/L 04/04/15 17:42 11,3-Dichloropropane ND
1.00 ug/L 04/04/15 17:42 12,2-Dichloropropane ND
1.00 ug/L 04/04/15 17:42 11,1-Dichloropropene ND
1.00 ug/L 04/04/15 17:42 1Diisopropyl ether ND
1.00 ug/L 04/04/15 17:42 1EthylbenzeneND
5.00 ug/L 04/04/15 17:42 1HexachlorobutadieneND
25.0 ug/L 04/04/15 17:42 12-Hexanone ND
1.00 ug/L 04/04/15 17:42 1IsopropylbenzeneND
5.00 ug/L 04/04/15 17:42 1Methylene Chloride ND
25.0 ug/L 04/04/15 17:42 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 04/04/15 17:42 1Methyl tert-butyl ether 4.84
1.00 ug/L 04/04/15 17:42 1NaphthaleneND*
1.00 ug/L 04/04/15 17:42 1n-Butylbenzene ND
1.00 ug/L 04/04/15 17:42 1N-Propylbenzene ND
1.00 ug/L 04/04/15 17:42 1p-Isopropyltoluene ND
1.00 ug/L 04/04/15 17:42 1sec-Butylbenzene ND
1.00 ug/L 04/04/15 17:42 1StyreneND
1.00 ug/L 04/04/15 17:42 1tert-Butylbenzene ND
TestAmerica Nashville
Page 36 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-9Client Sample ID: TMW-2
Matrix: WaterDate Collected: 03/30/15 14:00
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 04/04/15 17:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 17:42 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 04/04/15 17:42 1Tetrachloroethene85.5
1.00 ug/L 04/04/15 17:42 1TolueneND
1.00 ug/L 04/04/15 17:42 1trans-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 17:42 1trans-1,3-Dichloropropene ND
1.00 ug/L 04/04/15 17:42 11,2,3-Trichlorobenzene ND *
1.00 ug/L 04/04/15 17:42 11,2,4-Trichlorobenzene ND
1.00 ug/L 04/04/15 17:42 11,1,1-Trichloroethane ND
5.00 ug/L 04/04/15 17:42 11,1,2-Trichloroethane ND
1.00 ug/L 04/04/15 17:42 1TrichloroetheneND
1.00 ug/L 04/04/15 17:42 1TrichlorofluoromethaneND
5.00 ug/L 04/04/15 17:42 11,2,3-Trichloropropane ND
1.00 ug/L 04/04/15 17:42 11,2,4-Trimethylbenzene ND
1.00 ug/L 04/04/15 17:42 11,3,5-Trimethylbenzene ND
1.00 ug/L 04/04/15 17:42 1Vinyl chloride ND
5.00 ug/L 04/04/15 17:42 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)97 67-134 04/04/15 17:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)104 04/04/15 17:42 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 11,2,4-Trichlorobenzene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 11,2-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 11,3-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 11,4-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 11-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12,4,5-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12,4,6-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12,4-Dichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12,4-Dimethylphenol ND
30.0 ug/L 04/02/15 11:06 04/06/15 19:54 12,4-Dinitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12,4-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12,6-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12-Chloronaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12-Chlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12-Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 12-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 13,3'-Dichlorobenzidine ND
20.0 ug/L 04/02/15 11:06 04/06/15 19:54 13 & 4 Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 13-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 14,6-Dinitro-2-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 14-Bromophenyl phenyl ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 14-Chloro-3-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 14-Chloroaniline ND
TestAmerica Nashville
Page 37 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-9Client Sample ID: TMW-2
Matrix: WaterDate Collected: 03/30/15 14:00
Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Chlorophenyl phenyl ether ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 14-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 14-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1AcenaphthyleneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1AnthraceneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Benzo[a]anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Benzo[a]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Benzo[b]fluoranthene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Benzo[g,h,i]perylene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Benzo[k]fluoranthene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Bis(2-chloroethoxy)methane ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Bis(2-chloroethyl)ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Butyl benzyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Bis(2-ethylhexyl) phthalate ND *
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1CarbazoleND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1ChryseneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Dibenz(a,h)anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1DibenzofuranND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Diethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Dimethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Di-n-butyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1FluorantheneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1FluoreneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1HexachlorobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1HexachlorobutadieneND
20.0 ug/L 04/02/15 11:06 04/06/15 19:54 1HexachlorocyclopentadieneND*
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1HexachloroethaneND*
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Indeno[1,2,3-cd]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1IsophoroneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1NaphthaleneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1NitrobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1N-Nitrosodi-n-propylamine ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.0 ug/L 04/02/15 11:06 04/06/15 19:54 1PentachlorophenolND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1PhenanthreneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1PhenolND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1PyreneND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1Di-n-octyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 19:54 1bis (2-chloroisopropyl) ether ND
2,4,6-Tribromophenol (Surr)86 26-150 04/02/15 11:06 04/06/15 19:54 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)83 04/02/15 11:06 04/06/15 19:54 113-113
Nitrobenzene-d5 (Surr)105 04/02/15 11:06 04/06/15 19:54 136-126
Phenol-d5 (Surr)99 04/02/15 11:06 04/06/15 19:54 117-127
Terphenyl-d14 (Surr)114 04/02/15 11:06 04/06/15 19:54 144-149
TestAmerica Nashville
Page 38 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-10Client Sample ID: TMW-3
Matrix: WaterDate Collected: 03/30/15 14:50
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 04/04/15 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 18:08 1BenzeneND
1.00 ug/L 04/04/15 18:08 1BromobenzeneND*
1.00 ug/L 04/04/15 18:08 1BromochloromethaneND
1.00 ug/L 04/04/15 18:08 1BromodichloromethaneND
5.00 ug/L 04/04/15 18:08 1BromoformND*
1.00 ug/L 04/04/15 18:08 1BromomethaneND
25.0 ug/L 04/04/15 18:08 12-Butanone (MEK)ND
1.00 ug/L 04/04/15 18:08 1Carbon disulfide ND
1.00 ug/L 04/04/15 18:08 1Carbon tetrachloride ND
1.00 ug/L 04/04/15 18:08 1ChlorobenzeneND
1.00 ug/L 04/04/15 18:08 1ChlorodibromomethaneND
1.00 ug/L 04/04/15 18:08 1ChloroethaneND
1.00 ug/L 04/04/15 18:08 1ChloroformND
1.00 ug/L 04/04/15 18:08 1ChloromethaneND
1.00 ug/L 04/04/15 18:08 12-Chlorotoluene ND
1.00 ug/L 04/04/15 18:08 14-Chlorotoluene ND
1.00 ug/L 04/04/15 18:08 1cis-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 18:08 1cis-1,3-Dichloropropene ND
5.00 ug/L 04/04/15 18:08 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 04/04/15 18:08 11,2-Dibromoethane (EDB)ND *
5.00 ug/L 04/04/15 18:08 1DibromomethaneND
1.00 ug/L 04/04/15 18:08 11,2-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:08 11,3-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:08 11,4-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:08 1DichlorodifluoromethaneND
1.00 ug/L 04/04/15 18:08 11,1-Dichloroethane ND
1.00 ug/L 04/04/15 18:08 11,2-Dichloroethane ND
1.00 ug/L 04/04/15 18:08 11,1-Dichloroethene ND
1.00 ug/L 04/04/15 18:08 11,2-Dichloroethene, Total ND
1.00 ug/L 04/04/15 18:08 11,2-Dichloropropane ND
1.00 ug/L 04/04/15 18:08 11,3-Dichloropropane ND
1.00 ug/L 04/04/15 18:08 12,2-Dichloropropane ND
1.00 ug/L 04/04/15 18:08 11,1-Dichloropropene ND
1.00 ug/L 04/04/15 18:08 1Diisopropyl ether ND
1.00 ug/L 04/04/15 18:08 1EthylbenzeneND
5.00 ug/L 04/04/15 18:08 1HexachlorobutadieneND
25.0 ug/L 04/04/15 18:08 12-Hexanone ND
1.00 ug/L 04/04/15 18:08 1IsopropylbenzeneND
5.00 ug/L 04/04/15 18:08 1Methylene Chloride ND
25.0 ug/L 04/04/15 18:08 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 04/04/15 18:08 1Methyl tert-butyl ether ND
1.00 ug/L 04/04/15 18:08 1NaphthaleneND*
1.00 ug/L 04/04/15 18:08 1n-Butylbenzene ND
1.00 ug/L 04/04/15 18:08 1N-Propylbenzene ND
1.00 ug/L 04/04/15 18:08 1p-Isopropyltoluene ND
1.00 ug/L 04/04/15 18:08 1sec-Butylbenzene ND
1.00 ug/L 04/04/15 18:08 1StyreneND
1.00 ug/L 04/04/15 18:08 1tert-Butylbenzene ND
TestAmerica Nashville
Page 39 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-10Client Sample ID: TMW-3
Matrix: WaterDate Collected: 03/30/15 14:50
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 04/04/15 18:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 18:08 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 04/04/15 18:08 1Tetrachloroethene11.8
1.00 ug/L 04/04/15 18:08 1TolueneND
1.00 ug/L 04/04/15 18:08 1trans-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 18:08 1trans-1,3-Dichloropropene ND
1.00 ug/L 04/04/15 18:08 11,2,3-Trichlorobenzene ND *
1.00 ug/L 04/04/15 18:08 11,2,4-Trichlorobenzene ND
1.00 ug/L 04/04/15 18:08 11,1,1-Trichloroethane ND
5.00 ug/L 04/04/15 18:08 11,1,2-Trichloroethane ND
1.00 ug/L 04/04/15 18:08 1TrichloroetheneND
1.00 ug/L 04/04/15 18:08 1TrichlorofluoromethaneND
5.00 ug/L 04/04/15 18:08 11,2,3-Trichloropropane ND
1.00 ug/L 04/04/15 18:08 11,2,4-Trimethylbenzene ND
1.00 ug/L 04/04/15 18:08 11,3,5-Trimethylbenzene ND
1.00 ug/L 04/04/15 18:08 1Vinyl chloride ND
5.00 ug/L 04/04/15 18:08 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)95 67-134 04/04/15 18:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)108 04/04/15 18:08 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 11,2,4-Trichlorobenzene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 11,2-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 11,3-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 11,4-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 11-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12,4,5-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12,4,6-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12,4-Dichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12,4-Dimethylphenol ND
30.0 ug/L 04/02/15 11:06 04/06/15 20:30 12,4-Dinitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12,4-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12,6-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12-Chloronaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12-Chlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12-Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 12-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 13,3'-Dichlorobenzidine ND
20.0 ug/L 04/02/15 11:06 04/06/15 20:30 13 & 4 Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 13-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 14,6-Dinitro-2-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 14-Bromophenyl phenyl ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 14-Chloro-3-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 14-Chloroaniline ND
TestAmerica Nashville
Page 40 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-10Client Sample ID: TMW-3
Matrix: WaterDate Collected: 03/30/15 14:50
Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Chlorophenyl phenyl ether ND 10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 14-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 14-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1AcenaphthyleneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1AnthraceneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Benzo[a]anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Benzo[a]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Benzo[b]fluoranthene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Benzo[g,h,i]perylene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Benzo[k]fluoranthene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Bis(2-chloroethoxy)methane ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Bis(2-chloroethyl)ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Butyl benzyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Bis(2-ethylhexyl) phthalate ND *
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1CarbazoleND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1ChryseneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Dibenz(a,h)anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1DibenzofuranND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Diethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Dimethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Di-n-butyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1FluorantheneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1FluoreneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1HexachlorobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1HexachlorobutadieneND
20.0 ug/L 04/02/15 11:06 04/06/15 20:30 1HexachlorocyclopentadieneND*
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1HexachloroethaneND*
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Indeno[1,2,3-cd]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1IsophoroneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1NaphthaleneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1NitrobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1N-Nitrosodi-n-propylamine ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.0 ug/L 04/02/15 11:06 04/06/15 20:30 1PentachlorophenolND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1PhenanthreneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1PhenolND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1PyreneND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1Di-n-octyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 20:30 1bis (2-chloroisopropyl) ether ND
2,4,6-Tribromophenol (Surr)69 26-150 04/02/15 11:06 04/06/15 20:30 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)64 04/02/15 11:06 04/06/15 20:30 113-113
Nitrobenzene-d5 (Surr)88 04/02/15 11:06 04/06/15 20:30 136-126
Phenol-d5 (Surr)82 04/02/15 11:06 04/06/15 20:30 117-127
Terphenyl-d14 (Surr)94 04/02/15 11:06 04/06/15 20:30 144-149
TestAmerica Nashville
Page 41 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-11Client Sample ID: TMW-4
Matrix: WaterDate Collected: 03/30/15 15:50
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 50.0 ug/L 04/04/15 19:51 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 ug/L 04/04/15 19:51 2BenzeneND
2.00 ug/L 04/04/15 19:51 2BromobenzeneND*
2.00 ug/L 04/04/15 19:51 2BromochloromethaneND
2.00 ug/L 04/04/15 19:51 2BromodichloromethaneND
10.0 ug/L 04/04/15 19:51 2BromoformND*
2.00 ug/L 04/04/15 19:51 2BromomethaneND
50.0 ug/L 04/04/15 19:51 22-Butanone (MEK)ND
2.00 ug/L 04/04/15 19:51 2Carbon disulfide ND
2.00 ug/L 04/04/15 19:51 2Carbon tetrachloride ND
2.00 ug/L 04/04/15 19:51 2ChlorobenzeneND
2.00 ug/L 04/04/15 19:51 2ChlorodibromomethaneND
2.00 ug/L 04/04/15 19:51 2ChloroethaneND
2.00 ug/L 04/04/15 19:51 2ChloroformND
2.00 ug/L 04/04/15 19:51 2ChloromethaneND
2.00 ug/L 04/04/15 19:51 22-Chlorotoluene ND
2.00 ug/L 04/04/15 19:51 24-Chlorotoluene ND
2.00 ug/L 04/04/15 19:51 2cis-1,2-Dichloroethene ND
10.0 ug/L 04/04/15 19:51 2cis-1,3-Dichloropropene ND
10.0 ug/L 04/04/15 19:51 21,2-Dibromo-3-Chloropropane ND
2.00 ug/L 04/04/15 19:51 21,2-Dibromoethane (EDB)ND *
10.0 ug/L 04/04/15 19:51 2DibromomethaneND
2.00 ug/L 04/04/15 19:51 21,2-Dichlorobenzene ND
2.00 ug/L 04/04/15 19:51 21,3-Dichlorobenzene ND
2.00 ug/L 04/04/15 19:51 21,4-Dichlorobenzene ND
2.00 ug/L 04/04/15 19:51 2DichlorodifluoromethaneND
2.00 ug/L 04/04/15 19:51 21,1-Dichloroethane ND
2.00 ug/L 04/04/15 19:51 21,2-Dichloroethane ND
2.00 ug/L 04/04/15 19:51 21,1-Dichloroethene ND
2.00 ug/L 04/04/15 19:51 21,2-Dichloroethene, Total ND
2.00 ug/L 04/04/15 19:51 21,2-Dichloropropane ND
2.00 ug/L 04/04/15 19:51 21,3-Dichloropropane ND
2.00 ug/L 04/04/15 19:51 22,2-Dichloropropane ND
2.00 ug/L 04/04/15 19:51 21,1-Dichloropropene ND
2.00 ug/L 04/04/15 19:51 2Diisopropyl ether ND
2.00 ug/L 04/04/15 19:51 2EthylbenzeneND
10.0 ug/L 04/04/15 19:51 2HexachlorobutadieneND
50.0 ug/L 04/04/15 19:51 22-Hexanone ND
2.00 ug/L 04/04/15 19:51 2IsopropylbenzeneND
10.0 ug/L 04/04/15 19:51 2Methylene Chloride ND
50.0 ug/L 04/04/15 19:51 24-Methyl-2-pentanone (MIBK)ND
2.00 ug/L 04/04/15 19:51 2Methyl tert-butyl ether ND
2.00 ug/L 04/04/15 19:51 2NaphthaleneND*
2.00 ug/L 04/04/15 19:51 2n-Butylbenzene ND
2.00 ug/L 04/04/15 19:51 2N-Propylbenzene ND
2.00 ug/L 04/04/15 19:51 2p-Isopropyltoluene ND
2.00 ug/L 04/04/15 19:51 2sec-Butylbenzene ND
2.00 ug/L 04/04/15 19:51 2StyreneND
2.00 ug/L 04/04/15 19:51 2tert-Butylbenzene ND
TestAmerica Nashville
Page 42 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-11Client Sample ID: TMW-4
Matrix: WaterDate Collected: 03/30/15 15:50
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 2.00 ug/L 04/04/15 19:51 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.00 ug/L 04/04/15 19:51 21,1,2,2-Tetrachloroethane ND
2.00 ug/L 04/04/15 19:51 2Tetrachloroethene318
2.00 ug/L 04/04/15 19:51 2TolueneND
2.00 ug/L 04/04/15 19:51 2trans-1,2-Dichloroethene ND
10.0 ug/L 04/04/15 19:51 2trans-1,3-Dichloropropene ND
2.00 ug/L 04/04/15 19:51 21,2,3-Trichlorobenzene ND *
2.00 ug/L 04/04/15 19:51 21,2,4-Trichlorobenzene ND
2.00 ug/L 04/04/15 19:51 21,1,1-Trichloroethane ND
10.0 ug/L 04/04/15 19:51 21,1,2-Trichloroethane ND
2.00 ug/L 04/04/15 19:51 2Trichloroethene3.99
2.00 ug/L 04/04/15 19:51 2TrichlorofluoromethaneND
10.0 ug/L 04/04/15 19:51 21,2,3-Trichloropropane ND
2.00 ug/L 04/04/15 19:51 21,2,4-Trimethylbenzene ND
2.00 ug/L 04/04/15 19:51 21,3,5-Trimethylbenzene ND
2.00 ug/L 04/04/15 19:51 2Vinyl chloride ND
10.0 ug/L 04/04/15 19:51 2Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)98 67-134 04/04/15 19:51 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)104 04/04/15 19:51 280-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 11,2,4-Trichlorobenzene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 11,2-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 11,3-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 11,4-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 11-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12,4,5-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12,4,6-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12,4-Dichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12,4-Dimethylphenol ND
30.0 ug/L 04/02/15 11:06 04/06/15 21:07 12,4-Dinitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12,4-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12,6-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12-Chloronaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12-Chlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12-Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 12-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 13,3'-Dichlorobenzidine ND
20.0 ug/L 04/02/15 11:06 04/06/15 21:07 13 & 4 Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 13-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 14,6-Dinitro-2-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 14-Bromophenyl phenyl ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 14-Chloro-3-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 14-Chloroaniline ND
TestAmerica Nashville
Page 43 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-11Client Sample ID: TMW-4
Matrix: WaterDate Collected: 03/30/15 15:50
Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Chlorophenyl phenyl ether ND 10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 14-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 14-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1AcenaphthyleneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1AnthraceneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Benzo[a]anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Benzo[a]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Benzo[b]fluoranthene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Benzo[g,h,i]perylene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Benzo[k]fluoranthene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Bis(2-chloroethoxy)methane ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Bis(2-chloroethyl)ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Butyl benzyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Bis(2-ethylhexyl) phthalate ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1CarbazoleND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1ChryseneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Dibenz(a,h)anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1DibenzofuranND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Diethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Dimethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Di-n-butyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1FluorantheneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1FluoreneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1HexachlorobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1HexachlorobutadieneND
20.0 ug/L 04/02/15 11:06 04/06/15 21:07 1HexachlorocyclopentadieneND*
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1HexachloroethaneND*
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Indeno[1,2,3-cd]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1IsophoroneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1NaphthaleneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1NitrobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1N-Nitrosodi-n-propylamine ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.0 ug/L 04/02/15 11:06 04/06/15 21:07 1PentachlorophenolND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1PhenanthreneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1PhenolND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1PyreneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1Di-n-octyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:07 1bis (2-chloroisopropyl) ether ND
2,4,6-Tribromophenol (Surr)82 26-150 04/02/15 11:06 04/06/15 21:07 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)56 04/02/15 11:06 04/06/15 21:07 113-113
Nitrobenzene-d5 (Surr)91 04/02/15 11:06 04/06/15 21:07 136-126
Phenol-d5 (Surr)83 04/02/15 11:06 04/06/15 21:07 117-127
Terphenyl-d14 (Surr)107 04/02/15 11:06 04/06/15 21:07 144-149
TestAmerica Nashville
Page 44 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-12Client Sample ID: MW-11
Matrix: WaterDate Collected: 03/30/15 16:50
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 04/04/15 18:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 18:34 1BenzeneND
1.00 ug/L 04/04/15 18:34 1BromobenzeneND*
1.00 ug/L 04/04/15 18:34 1BromochloromethaneND
1.00 ug/L 04/04/15 18:34 1BromodichloromethaneND
5.00 ug/L 04/04/15 18:34 1BromoformND*
1.00 ug/L 04/04/15 18:34 1BromomethaneND
25.0 ug/L 04/04/15 18:34 12-Butanone (MEK)ND
1.00 ug/L 04/04/15 18:34 1Carbon disulfide ND
1.00 ug/L 04/04/15 18:34 1Carbon tetrachloride ND
1.00 ug/L 04/04/15 18:34 1ChlorobenzeneND
1.00 ug/L 04/04/15 18:34 1ChlorodibromomethaneND
1.00 ug/L 04/04/15 18:34 1ChloroethaneND
1.00 ug/L 04/04/15 18:34 1ChloroformND
1.00 ug/L 04/04/15 18:34 1ChloromethaneND
1.00 ug/L 04/04/15 18:34 12-Chlorotoluene ND
1.00 ug/L 04/04/15 18:34 14-Chlorotoluene ND
1.00 ug/L 04/04/15 18:34 1cis-1,2-Dichloroethene 5.05
5.00 ug/L 04/04/15 18:34 1cis-1,3-Dichloropropene ND
5.00 ug/L 04/04/15 18:34 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 04/04/15 18:34 11,2-Dibromoethane (EDB)ND *
5.00 ug/L 04/04/15 18:34 1DibromomethaneND
1.00 ug/L 04/04/15 18:34 11,2-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:34 11,3-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:34 11,4-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:34 1DichlorodifluoromethaneND
1.00 ug/L 04/04/15 18:34 11,1-Dichloroethane ND
1.00 ug/L 04/04/15 18:34 11,2-Dichloroethane ND
1.00 ug/L 04/04/15 18:34 11,1-Dichloroethene ND
1.00 ug/L 04/04/15 18:34 11,2-Dichloroethene, Total 5.05
1.00 ug/L 04/04/15 18:34 11,2-Dichloropropane ND
1.00 ug/L 04/04/15 18:34 11,3-Dichloropropane ND
1.00 ug/L 04/04/15 18:34 12,2-Dichloropropane ND
1.00 ug/L 04/04/15 18:34 11,1-Dichloropropene ND
1.00 ug/L 04/04/15 18:34 1Diisopropyl ether ND
1.00 ug/L 04/04/15 18:34 1EthylbenzeneND
5.00 ug/L 04/04/15 18:34 1HexachlorobutadieneND
25.0 ug/L 04/04/15 18:34 12-Hexanone ND
1.00 ug/L 04/04/15 18:34 1IsopropylbenzeneND
5.00 ug/L 04/04/15 18:34 1Methylene Chloride ND
25.0 ug/L 04/04/15 18:34 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 04/04/15 18:34 1Methyl tert-butyl ether ND
1.00 ug/L 04/04/15 18:34 1NaphthaleneND*
1.00 ug/L 04/04/15 18:34 1n-Butylbenzene ND
1.00 ug/L 04/04/15 18:34 1N-Propylbenzene ND
1.00 ug/L 04/04/15 18:34 1p-Isopropyltoluene ND
1.00 ug/L 04/04/15 18:34 1sec-Butylbenzene ND
1.00 ug/L 04/04/15 18:34 1StyreneND
1.00 ug/L 04/04/15 18:34 1tert-Butylbenzene ND
TestAmerica Nashville
Page 45 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-12Client Sample ID: MW-11
Matrix: WaterDate Collected: 03/30/15 16:50
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 04/04/15 18:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 18:34 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 04/04/15 18:34 1Tetrachloroethene8.00
1.00 ug/L 04/04/15 18:34 1TolueneND
1.00 ug/L 04/04/15 18:34 1trans-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 18:34 1trans-1,3-Dichloropropene ND
1.00 ug/L 04/04/15 18:34 11,2,3-Trichlorobenzene ND *
1.00 ug/L 04/04/15 18:34 11,2,4-Trichlorobenzene ND
1.00 ug/L 04/04/15 18:34 11,1,1-Trichloroethane ND
5.00 ug/L 04/04/15 18:34 11,1,2-Trichloroethane ND
1.00 ug/L 04/04/15 18:34 1Trichloroethene1.57
1.00 ug/L 04/04/15 18:34 1TrichlorofluoromethaneND
5.00 ug/L 04/04/15 18:34 11,2,3-Trichloropropane ND
1.00 ug/L 04/04/15 18:34 11,2,4-Trimethylbenzene ND
1.00 ug/L 04/04/15 18:34 11,3,5-Trimethylbenzene ND
1.00 ug/L 04/04/15 18:34 1Vinyl chloride ND
5.00 ug/L 04/04/15 18:34 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)96 67-134 04/04/15 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)107 04/04/15 18:34 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 11,2,4-Trichlorobenzene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 11,2-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 11,3-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 11,4-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 11-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12,4,5-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12,4,6-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12,4-Dichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12,4-Dimethylphenol ND
30.0 ug/L 04/02/15 11:06 04/06/15 21:43 12,4-Dinitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12,4-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12,6-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12-Chloronaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12-Chlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12-Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 12-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 13,3'-Dichlorobenzidine ND
20.0 ug/L 04/02/15 11:06 04/06/15 21:43 13 & 4 Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 13-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 14,6-Dinitro-2-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 14-Bromophenyl phenyl ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 14-Chloro-3-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 14-Chloroaniline ND
TestAmerica Nashville
Page 46 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-12Client Sample ID: MW-11
Matrix: WaterDate Collected: 03/30/15 16:50
Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Chlorophenyl phenyl ether ND 10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 14-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 14-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1AcenaphthyleneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1AnthraceneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Benzo[a]anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Benzo[a]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Benzo[b]fluoranthene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Benzo[g,h,i]perylene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Benzo[k]fluoranthene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Bis(2-chloroethoxy)methane ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Bis(2-chloroethyl)ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Butyl benzyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Bis(2-ethylhexyl) phthalate ND *
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1CarbazoleND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1ChryseneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Dibenz(a,h)anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1DibenzofuranND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Diethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Dimethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Di-n-butyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1FluorantheneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1FluoreneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1HexachlorobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1HexachlorobutadieneND
20.0 ug/L 04/02/15 11:06 04/06/15 21:43 1HexachlorocyclopentadieneND*
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1HexachloroethaneND*
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Indeno[1,2,3-cd]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1IsophoroneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1NaphthaleneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1NitrobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1N-Nitrosodi-n-propylamine ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.0 ug/L 04/02/15 11:06 04/06/15 21:43 1PentachlorophenolND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1PhenanthreneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1PhenolND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1PyreneND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1Di-n-octyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 21:43 1bis (2-chloroisopropyl) ether ND
2,4,6-Tribromophenol (Surr)79 26-150 04/02/15 11:06 04/06/15 21:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)70 04/02/15 11:06 04/06/15 21:43 113-113
Nitrobenzene-d5 (Surr)96 04/02/15 11:06 04/06/15 21:43 136-126
Phenol-d5 (Surr)90 04/02/15 11:06 04/06/15 21:43 117-127
Terphenyl-d14 (Surr)113 04/02/15 11:06 04/06/15 21:43 144-149
TestAmerica Nashville
Page 47 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-13Client Sample ID: MW-8
Matrix: WaterDate Collected: 03/30/15 17:15
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 04/04/15 18:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 18:59 1BenzeneND
1.00 ug/L 04/04/15 18:59 1BromobenzeneND*
1.00 ug/L 04/04/15 18:59 1BromochloromethaneND
1.00 ug/L 04/04/15 18:59 1BromodichloromethaneND
5.00 ug/L 04/04/15 18:59 1BromoformND*
1.00 ug/L 04/04/15 18:59 1BromomethaneND
25.0 ug/L 04/04/15 18:59 12-Butanone (MEK)ND
1.00 ug/L 04/04/15 18:59 1Carbon disulfide ND
1.00 ug/L 04/04/15 18:59 1Carbon tetrachloride ND
1.00 ug/L 04/04/15 18:59 1ChlorobenzeneND
1.00 ug/L 04/04/15 18:59 1ChlorodibromomethaneND
1.00 ug/L 04/04/15 18:59 1ChloroethaneND
1.00 ug/L 04/04/15 18:59 1ChloroformND
1.00 ug/L 04/04/15 18:59 1ChloromethaneND
1.00 ug/L 04/04/15 18:59 12-Chlorotoluene ND
1.00 ug/L 04/04/15 18:59 14-Chlorotoluene ND
1.00 ug/L 04/04/15 18:59 1cis-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 18:59 1cis-1,3-Dichloropropene ND
5.00 ug/L 04/04/15 18:59 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 04/04/15 18:59 11,2-Dibromoethane (EDB)ND *
5.00 ug/L 04/04/15 18:59 1DibromomethaneND
1.00 ug/L 04/04/15 18:59 11,2-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:59 11,3-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:59 11,4-Dichlorobenzene ND
1.00 ug/L 04/04/15 18:59 1DichlorodifluoromethaneND
1.00 ug/L 04/04/15 18:59 11,1-Dichloroethane ND
1.00 ug/L 04/04/15 18:59 11,2-Dichloroethane ND
1.00 ug/L 04/04/15 18:59 11,1-Dichloroethene ND
1.00 ug/L 04/04/15 18:59 11,2-Dichloroethene, Total ND
1.00 ug/L 04/04/15 18:59 11,2-Dichloropropane ND
1.00 ug/L 04/04/15 18:59 11,3-Dichloropropane ND
1.00 ug/L 04/04/15 18:59 12,2-Dichloropropane ND
1.00 ug/L 04/04/15 18:59 11,1-Dichloropropene ND
1.00 ug/L 04/04/15 18:59 1Diisopropyl ether ND
1.00 ug/L 04/04/15 18:59 1EthylbenzeneND
5.00 ug/L 04/04/15 18:59 1HexachlorobutadieneND
25.0 ug/L 04/04/15 18:59 12-Hexanone ND
1.00 ug/L 04/04/15 18:59 1IsopropylbenzeneND
5.00 ug/L 04/04/15 18:59 1Methylene Chloride ND
25.0 ug/L 04/04/15 18:59 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 04/04/15 18:59 1Methyl tert-butyl ether ND
1.00 ug/L 04/04/15 18:59 1NaphthaleneND*
1.00 ug/L 04/04/15 18:59 1n-Butylbenzene ND
1.00 ug/L 04/04/15 18:59 1N-Propylbenzene ND
1.00 ug/L 04/04/15 18:59 1p-Isopropyltoluene ND
1.00 ug/L 04/04/15 18:59 1sec-Butylbenzene ND
1.00 ug/L 04/04/15 18:59 1StyreneND
1.00 ug/L 04/04/15 18:59 1tert-Butylbenzene ND
TestAmerica Nashville
Page 48 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-13Client Sample ID: MW-8
Matrix: WaterDate Collected: 03/30/15 17:15
Date Received: 04/01/15 08:00
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 04/04/15 18:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 04/04/15 18:59 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 04/04/15 18:59 1TetrachloroetheneND
1.00 ug/L 04/04/15 18:59 1TolueneND
1.00 ug/L 04/04/15 18:59 1trans-1,2-Dichloroethene ND
5.00 ug/L 04/04/15 18:59 1trans-1,3-Dichloropropene ND
1.00 ug/L 04/04/15 18:59 11,2,3-Trichlorobenzene ND *
1.00 ug/L 04/04/15 18:59 11,2,4-Trichlorobenzene ND
1.00 ug/L 04/04/15 18:59 11,1,1-Trichloroethane ND
5.00 ug/L 04/04/15 18:59 11,1,2-Trichloroethane ND
1.00 ug/L 04/04/15 18:59 1TrichloroetheneND
1.00 ug/L 04/04/15 18:59 1TrichlorofluoromethaneND
5.00 ug/L 04/04/15 18:59 11,2,3-Trichloropropane ND
1.00 ug/L 04/04/15 18:59 11,2,4-Trimethylbenzene ND
1.00 ug/L 04/04/15 18:59 11,3,5-Trimethylbenzene ND
1.00 ug/L 04/04/15 18:59 1Vinyl chloride ND
5.00 ug/L 04/04/15 18:59 1Xylenes, Total ND
1,2-Dichloroethane-d4 (Surr)95 67-134 04/04/15 18:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Toluene-d8 (Surr)108 04/04/15 18:59 180-120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 11,2,4-Trichlorobenzene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 11,2-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 11,3-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 11,4-Dichlorobenzene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 11-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12,4,5-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12,4,6-Trichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12,4-Dichlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12,4-Dimethylphenol ND
30.0 ug/L 04/02/15 11:06 04/06/15 22:19 12,4-Dinitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12,4-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12,6-Dinitrotoluene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12-Chloronaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12-Chlorophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12-Methylnaphthalene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12-Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 12-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 13,3'-Dichlorobenzidine ND
20.0 ug/L 04/02/15 11:06 04/06/15 22:19 13 & 4 Methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 13-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 14,6-Dinitro-2-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 14-Bromophenyl phenyl ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 14-Chloro-3-methylphenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 14-Chloroaniline ND
TestAmerica Nashville
Page 49 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Client Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Lab Sample ID: 490-75581-13Client Sample ID: MW-8
Matrix: WaterDate Collected: 03/30/15 17:15
Date Received: 04/01/15 08:00
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
4-Chlorophenyl phenyl ether ND 10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 14-Nitroaniline ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 14-Nitrophenol ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1AcenaphthyleneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1AnthraceneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Benzo[a]anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Benzo[a]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Benzo[b]fluoranthene ND *
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Benzo[g,h,i]perylene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Benzo[k]fluoranthene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Bis(2-chloroethoxy)methane ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Bis(2-chloroethyl)ether ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Butyl benzyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Bis(2-ethylhexyl) phthalate ND *
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1CarbazoleND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1ChryseneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Dibenz(a,h)anthracene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1DibenzofuranND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Diethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Dimethyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Di-n-butyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1FluorantheneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1FluoreneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1HexachlorobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1HexachlorobutadieneND
20.0 ug/L 04/02/15 11:06 04/06/15 22:19 1HexachlorocyclopentadieneND*
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1HexachloroethaneND*
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Indeno[1,2,3-cd]pyrene ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1IsophoroneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1NaphthaleneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1NitrobenzeneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1N-Nitrosodi-n-propylamine ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1n-Nitrosodiphenylamine(as
diphenylamine)
ND
20.0 ug/L 04/02/15 11:06 04/06/15 22:19 1PentachlorophenolND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1PhenanthreneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1PhenolND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1PyreneND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1Di-n-octyl phthalate ND
10.0 ug/L 04/02/15 11:06 04/06/15 22:19 1bis (2-chloroisopropyl) ether ND
2,4,6-Tribromophenol (Surr)58 26-150 04/02/15 11:06 04/06/15 22:19 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)53 04/02/15 11:06 04/06/15 22:19 113-113
Nitrobenzene-d5 (Surr)73 04/02/15 11:06 04/06/15 22:19 136-126
Phenol-d5 (Surr)68 04/02/15 11:06 04/06/15 22:19 117-127
Terphenyl-d14 (Surr)81 04/02/15 11:06 04/06/15 22:19 144-149
TestAmerica Nashville
Page 50 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 400-252212/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
RL MDL
Acetone ND 25.0 ug/L 04/04/15 09:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 04/04/15 09:54 1Benzene
ND 1.00 ug/L 04/04/15 09:54 1Bromobenzene
ND 1.00 ug/L 04/04/15 09:54 1Bromochloromethane
ND 1.00 ug/L 04/04/15 09:54 1Bromodichloromethane
ND 5.00 ug/L 04/04/15 09:54 1Bromoform
ND 1.00 ug/L 04/04/15 09:54 1Bromomethane
ND 25.0 ug/L 04/04/15 09:54 12-Butanone (MEK)
ND 1.00 ug/L 04/04/15 09:54 1Carbon disulfide
ND 1.00 ug/L 04/04/15 09:54 1Carbon tetrachloride
ND 1.00 ug/L 04/04/15 09:54 1Chlorobenzene
ND 1.00 ug/L 04/04/15 09:54 1Chlorodibromomethane
ND 1.00 ug/L 04/04/15 09:54 1Chloroethane
ND 1.00 ug/L 04/04/15 09:54 1Chloroform
ND 1.00 ug/L 04/04/15 09:54 1Chloromethane
ND 1.00 ug/L 04/04/15 09:54 12-Chlorotoluene
ND 1.00 ug/L 04/04/15 09:54 14-Chlorotoluene
ND 1.00 ug/L 04/04/15 09:54 1cis-1,2-Dichloroethene
ND 5.00 ug/L 04/04/15 09:54 1cis-1,3-Dichloropropene
ND 5.00 ug/L 04/04/15 09:54 11,2-Dibromo-3-Chloropropane
ND 1.00 ug/L 04/04/15 09:54 11,2-Dibromoethane (EDB)
ND 5.00 ug/L 04/04/15 09:54 1Dibromomethane
ND 1.00 ug/L 04/04/15 09:54 11,2-Dichlorobenzene
ND 1.00 ug/L 04/04/15 09:54 11,3-Dichlorobenzene
ND 1.00 ug/L 04/04/15 09:54 11,4-Dichlorobenzene
ND 1.00 ug/L 04/04/15 09:54 1Dichlorodifluoromethane
ND 1.00 ug/L 04/04/15 09:54 11,1-Dichloroethane
ND 1.00 ug/L 04/04/15 09:54 11,2-Dichloroethane
ND 1.00 ug/L 04/04/15 09:54 11,1-Dichloroethene
ND 1.00 ug/L 04/04/15 09:54 11,2-Dichloroethene, Total
ND 1.00 ug/L 04/04/15 09:54 11,2-Dichloropropane
ND 1.00 ug/L 04/04/15 09:54 11,3-Dichloropropane
ND 1.00 ug/L 04/04/15 09:54 12,2-Dichloropropane
ND 1.00 ug/L 04/04/15 09:54 11,1-Dichloropropene
ND 1.00 ug/L 04/04/15 09:54 1Diisopropyl ether
ND 1.00 ug/L 04/04/15 09:54 1Ethylbenzene
ND 5.00 ug/L 04/04/15 09:54 1Hexachlorobutadiene
ND 25.0 ug/L 04/04/15 09:54 12-Hexanone
ND 1.00 ug/L 04/04/15 09:54 1Isopropylbenzene
ND 5.00 ug/L 04/04/15 09:54 1Methylene Chloride
ND 25.0 ug/L 04/04/15 09:54 14-Methyl-2-pentanone (MIBK)
ND 1.00 ug/L 04/04/15 09:54 1Methyl tert-butyl ether
ND 1.00 ug/L 04/04/15 09:54 1Naphthalene
ND 1.00 ug/L 04/04/15 09:54 1n-Butylbenzene
ND 1.00 ug/L 04/04/15 09:54 1N-Propylbenzene
ND 1.00 ug/L 04/04/15 09:54 1p-Isopropyltoluene
ND 1.00 ug/L 04/04/15 09:54 1sec-Butylbenzene
ND 1.00 ug/L 04/04/15 09:54 1Styrene
TestAmerica Nashville
Page 51 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-252212/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
RL MDL
tert-Butylbenzene ND 1.00 ug/L 04/04/15 09:54 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 04/04/15 09:54 11,1,1,2-Tetrachloroethane
ND 1.00 ug/L 04/04/15 09:54 11,1,2,2-Tetrachloroethane
ND 1.00 ug/L 04/04/15 09:54 1Tetrachloroethene
ND 1.00 ug/L 04/04/15 09:54 1Toluene
ND 1.00 ug/L 04/04/15 09:54 1trans-1,2-Dichloroethene
ND 5.00 ug/L 04/04/15 09:54 1trans-1,3-Dichloropropene
ND 1.00 ug/L 04/04/15 09:54 11,2,3-Trichlorobenzene
ND 1.00 ug/L 04/04/15 09:54 11,2,4-Trichlorobenzene
ND 1.00 ug/L 04/04/15 09:54 11,1,1-Trichloroethane
ND 5.00 ug/L 04/04/15 09:54 11,1,2-Trichloroethane
ND 1.00 ug/L 04/04/15 09:54 1Trichloroethene
ND 1.00 ug/L 04/04/15 09:54 1Trichlorofluoromethane
ND 5.00 ug/L 04/04/15 09:54 11,2,3-Trichloropropane
ND 1.00 ug/L 04/04/15 09:54 11,2,4-Trimethylbenzene
ND 1.00 ug/L 04/04/15 09:54 11,3,5-Trimethylbenzene
ND 1.00 ug/L 04/04/15 09:54 1Vinyl chloride
ND 5.00 ug/L 04/04/15 09:54 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)96 67-134 04/04/15 09:54 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
108 04/04/15 09:54 1Toluene-d8 (Surr)80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252212/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
Acetone 200 203.7 ug/L 102 24 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 45.93 ug/L 92 79 -120
Bromobenzene 50.0 64.93 *ug/L 130 80 -121
Bromochloromethane 50.0 50.43 ug/L 101 80 -120
Bromodichloromethane 50.0 50.51 ug/L 101 75 -127
Bromoform 50.0 60.93 *ug/L 122 65 -121
Bromomethane 50.0 48.56 ug/L 97 10 -150
2-Butanone (MEK)200 207.6 ug/L 104 62 -137
Carbon disulfide 50.0 49.40 ug/L 99 41 -140
Carbon tetrachloride 50.0 53.36 ug/L 107 46 -141
Chlorobenzene 50.0 55.41 ug/L 111 80 -120
Chlorodibromomethane 50.0 59.25 ug/L 119 63 -125
Chloroethane 50.0 47.81 ug/L 96 37 -150
Chloroform 50.0 45.73 ug/L 91 73 -122
Chloromethane 50.0 48.15 ug/L 96 49 -141
2-Chlorotoluene 50.0 51.52 ug/L 103 75 -126
4-Chlorotoluene 50.0 54.60 ug/L 109 80 -125
cis-1,2-Dichloroethene 50.0 47.54 ug/L 95 78 -122
cis-1,3-Dichloropropene 50.0 52.21 ug/L 104 70 -122
1,2-Dibromo-3-Chloropropane 50.0 59.32 ug/L 119 52 -124
TestAmerica Nashville
Page 52 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252212/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
1,2-Dibromoethane (EDB)50.0 60.99 *ug/L 122 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Dibromomethane 50.0 50.04 ug/L 100 78 -120
1,2-Dichlorobenzene 50.0 57.35 ug/L 115 80 -121
1,3-Dichlorobenzene 50.0 58.20 ug/L 116 77 -124
1,4-Dichlorobenzene 50.0 57.87 ug/L 116 79 -120
Dichlorodifluoromethane 50.0 48.68 ug/L 97 27 -144
1,1-Dichloroethane 50.0 47.49 ug/L 95 75 -126
1,2-Dichloroethane 50.0 47.19 ug/L 94 69 -128
1,1-Dichloroethene 50.0 52.98 ug/L 106 50 -134
1,2-Dichloropropane 50.0 47.44 ug/L 95 77 -126
1,3-Dichloropropane 50.0 55.86 ug/L 112 77 -120
2,2-Dichloropropane 50.0 49.40 ug/L 99 52 -135
1,1-Dichloropropene 50.0 47.06 ug/L 94 74 -121
Diisopropyl ether 50.0 45.41 ug/L 91 69 -143
Ethylbenzene 50.0 53.10 ug/L 106 80 -120
Hexachlorobutadiene 50.0 56.97 ug/L 114 35 -150
2-Hexanone 200 248.1 ug/L 124 60 -150
Isopropylbenzene 50.0 54.32 ug/L 109 76 -120
Methylene Chloride 50.0 48.35 ug/L 97 70 -130
4-Methyl-2-pentanone (MIBK)200 213.2 ug/L 107 63 -150
Methyl tert-butyl ether 50.0 50.39 ug/L 101 70 -124
Naphthalene 50.0 66.95 *ug/L 134 45 -131
n-Butylbenzene 50.0 53.56 ug/L 107 76 -138
N-Propylbenzene 50.0 55.53 ug/L 111 75 -128
p-Isopropyltoluene 50.0 57.05 ug/L 114 78 -120
sec-Butylbenzene 50.0 56.18 ug/L 112 78 -128
Styrene 50.0 55.31 ug/L 111 79 -124
tert-Butylbenzene 50.0 55.77 ug/L 112 80 -120
1,1,1,2-Tetrachloroethane 50.0 58.76 ug/L 118 66 -126
1,1,2,2-Tetrachloroethane 50.0 58.47 ug/L 117 68 -132
Tetrachloroethene 50.0 59.50 ug/L 119 76 -124
Toluene 50.0 53.16 ug/L 106 80 -120
trans-1,2-Dichloroethene 50.0 51.76 ug/L 104 70 -126
trans-1,3-Dichloropropene 50.0 56.90 ug/L 114 64 -120
1,2,3-Trichlorobenzene 50.0 65.72 *ug/L 131 62 -130
1,2,4-Trichlorobenzene 50.0 64.11 ug/L 128 69 -128
1,1,1-Trichloroethane 50.0 49.98 ug/L 100 66 -130
1,1,2-Trichloroethane 50.0 56.09 ug/L 112 80 -120
Trichloroethene 50.0 55.08 ug/L 110 77 -120
Trichlorofluoromethane 50.0 48.23 ug/L 96 26 -150
1,2,3-Trichloropropane 50.0 58.17 ug/L 116 72 -125
1,2,4-Trimethylbenzene 50.0 55.13 ug/L 110 77 -127
1,3,5-Trimethylbenzene 50.0 56.16 ug/L 112 80 -120
Vinyl chloride 50.0 48.95 ug/L 98 60 -128
Xylenes, Total 100 106.6 ug/L 107 70 -130
1,2-Dichloroethane-d4 (Surr)67 -134
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
TestAmerica Nashville
Page 53 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252212/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
Toluene-d8 (Surr)80 -120
Surrogate
105
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 490-75126-A-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
Acetone ND 200 190.1 ug/L 95 10 -150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene ND 50.0 43.91 ug/L 88 10 -150
Bromobenzene ND *50.0 62.63 ug/L 125 38 -135
Bromochloromethane ND 50.0 48.25 ug/L 96 75 -120
Bromodichloromethane ND 50.0 47.68 ug/L 95 61 -133
Bromoform ND *50.0 57.12 ug/L 114 54 -125
Bromomethane ND 50.0 50.31 ug/L 101 10 -150
2-Butanone (MEK)ND 200 185.4 ug/L 93 10 -150
Carbon disulfide ND 50.0 48.05 ug/L 96 10 -150
Carbon tetrachloride ND 50.0 50.48 ug/L 101 40 -138
Chlorobenzene ND 50.0 53.95 ug/L 108 10 -150
Chlorodibromomethane ND 50.0 56.48 ug/L 113 50 -130
Chloroethane ND 50.0 51.52 ug/L 103 38 -150
Chloroform ND 50.0 43.19 ug/L 86 10 -150
Chloromethane ND 50.0 48.30 ug/L 97 26 -150
2-Chlorotoluene ND 50.0 51.88 ug/L 104 10 -150
4-Chlorotoluene ND 50.0 54.30 ug/L 109 17 -145
cis-1,2-Dichloroethene ND 50.0 45.31 ug/L 91 10 -150
cis-1,3-Dichloropropene ND 50.0 48.90 ug/L 98 52 -130
1,2-Dibromo-3-Chloropropane ND 50.0 54.44 ug/L 109 50 -133
1,2-Dibromoethane (EDB)ND *50.0 58.83 ug/L 118 70 -125
Dibromomethane ND 50.0 48.05 ug/L 96 69 -123
1,2-Dichlorobenzene ND 50.0 55.32 ug/L 111 10 -150
1,3-Dichlorobenzene ND 50.0 57.96 ug/L 116 25 -136
1,4-Dichlorobenzene ND 50.0 56.81 ug/L 114 10 -150
Dichlorodifluoromethane ND 50.0 49.46 ug/L 99 10 -150
1,1-Dichloroethane ND 50.0 45.52 ug/L 91 10 -150
1,2-Dichloroethane ND 50.0 44.53 ug/L 89 10 -150
1,1-Dichloroethene ND 50.0 50.39 ug/L 101 10 -150
1,2-Dichloropropane ND 50.0 44.52 ug/L 89 65 -132
1,3-Dichloropropane ND 50.0 54.41 ug/L 109 67 -127
2,2-Dichloropropane ND 50.0 47.36 ug/L 95 46 -132
1,1-Dichloropropene ND 50.0 45.23 ug/L 90 59 -126
Diisopropyl ether ND 50.0 43.98 ug/L 88 10 -150
Ethylbenzene ND 50.0 52.54 ug/L 105 10 -150
Hexachlorobutadiene ND 50.0 55.88 ug/L 112 10 -150
2-Hexanone ND 200 221.4 ug/L 111 24 -150
Isopropylbenzene ND 50.0 53.85 ug/L 108 10 -150
Methylene Chloride ND 50.0 45.68 ug/L 91 10 -150
4-Methyl-2-pentanone (MIBK)ND 200 195.2 ug/L 98 20 -150
Methyl tert-butyl ether ND 50.0 47.33 ug/L 95 10 -150
TestAmerica Nashville
Page 54 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-75126-A-6 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
Naphthalene ND *50.0 63.11 ug/L 126 10 -150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
n-Butylbenzene ND 50.0 53.70 ug/L 107 10 -150
N-Propylbenzene ND 50.0 55.10 ug/L 110 10 -150
p-Isopropyltoluene ND 50.0 56.08 ug/L 112 10 -150
sec-Butylbenzene ND 50.0 55.40 ug/L 111 10 -150
Styrene ND 50.0 54.41 ug/L 109 24 -147
tert-Butylbenzene ND 50.0 56.97 ug/L 114 10 -150
1,1,1,2-Tetrachloroethane ND 50.0 57.71 ug/L 115 42 -135
1,1,2,2-Tetrachloroethane ND 50.0 55.99 ug/L 112 52 -148
Tetrachloroethene ND 50.0 57.30 ug/L 115 10 -150
Toluene ND 50.0 51.96 ug/L 104 10 -150
trans-1,2-Dichloroethene ND 50.0 49.12 ug/L 98 66 -126
trans-1,3-Dichloropropene ND 50.0 55.35 ug/L 111 45 -128
1,2,3-Trichlorobenzene ND * F1 50.0 62.44 ug/L 123 30 -137
1,2,4-Trichlorobenzene ND 50.0 62.45 ug/L 125 20 -139
1,1,1-Trichloroethane ND 50.0 47.74 ug/L 95 60 -131
1,1,2-Trichloroethane ND 50.0 53.75 ug/L 107 68 -127
Trichloroethene ND 50.0 51.92 ug/L 104 10 -150
Trichlorofluoromethane ND 50.0 47.75 ug/L 96 29 -144
1,2,3-Trichloropropane ND 50.0 55.38 ug/L 111 67 -130
1,2,4-Trimethylbenzene ND 50.0 54.58 ug/L 109 10 -150
1,3,5-Trimethylbenzene ND 50.0 55.78 ug/L 112 10 -150
Vinyl chloride ND 50.0 48.25 ug/L 97 46 -136
Xylenes, Total ND 100 106.3 ug/L 106 10 -150
1,2-Dichloroethane-d4 (Surr)67 -134
Surrogate
94
MS MS
Qualifier Limits%Recovery
107Toluene-d8 (Surr)80 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-75126-A-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
Acetone ND 200 187.3 ug/L 94 10 -150 1 22
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Benzene ND 50.0 46.63 ug/L 93 10 -150 6 19
Bromobenzene ND *50.0 64.72 ug/L 129 38 -135 3 35
Bromochloromethane ND 50.0 49.69 ug/L 99 75 -120 3 17
Bromodichloromethane ND 50.0 49.56 ug/L 99 61 -133 4 19
Bromoform ND *50.0 56.68 ug/L 113 54 -125 1 19
Bromomethane ND 50.0 57.04 ug/L 114 10 -150 13 24
2-Butanone (MEK)ND 200 182.5 ug/L 91 10 -150 2 21
Carbon disulfide ND 50.0 51.24 ug/L 102 10 -150 6 23
Carbon tetrachloride ND 50.0 51.87 ug/L 104 40 -138 3 21
Chlorobenzene ND 50.0 54.51 ug/L 109 10 -150 1 30
Chlorodibromomethane ND 50.0 55.74 ug/L 111 50 -130 1 21
Chloroethane ND 50.0 54.52 ug/L 109 38 -150 6 23
Chloroform ND 50.0 46.14 ug/L 92 10 -150 7 18
TestAmerica Nashville
Page 55 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-75126-A-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
Chloromethane ND 50.0 51.25 ug/L 103 26 -150 6 23
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2-Chlorotoluene ND 50.0 53.97 ug/L 108 10 -150 4 47
4-Chlorotoluene ND 50.0 56.09 ug/L 112 17 -145 3 51
cis-1,2-Dichloroethene ND 50.0 47.88 ug/L 96 10 -150 6 20
cis-1,3-Dichloropropene ND 50.0 51.31 ug/L 103 52 -130 5 20
1,2-Dibromo-3-Chloropropane ND 50.0 51.93 ug/L 104 50 -133 5 30
1,2-Dibromoethane (EDB)ND *50.0 56.99 ug/L 114 70 -125 3 21
Dibromomethane ND 50.0 49.10 ug/L 98 69 -123 2 18
1,2-Dichlorobenzene ND 50.0 57.24 ug/L 114 10 -150 3 38
1,3-Dichlorobenzene ND 50.0 59.79 ug/L 120 25 -136 3 44
1,4-Dichlorobenzene ND 50.0 59.55 ug/L 119 10 -150 5 45
Dichlorodifluoromethane ND 50.0 54.00 ug/L 108 10 -150 9 23
1,1-Dichloroethane ND 50.0 48.24 ug/L 96 10 -150 6 18
1,2-Dichloroethane ND 50.0 46.18 ug/L 92 10 -150 4 19
1,1-Dichloroethene ND 50.0 56.28 ug/L 113 10 -150 11 19
1,2-Dichloropropane ND 50.0 49.05 ug/L 98 65 -132 10 18
1,3-Dichloropropane ND 50.0 55.58 ug/L 111 67 -127 2 20
2,2-Dichloropropane ND 50.0 49.76 ug/L 100 46 -132 5 20
1,1-Dichloropropene ND 50.0 48.48 ug/L 97 59 -126 7 22
Diisopropyl ether ND 50.0 47.40 ug/L 95 10 -150 7 24
Ethylbenzene ND 50.0 54.23 ug/L 108 10 -150 3 40
Hexachlorobutadiene ND 50.0 66.34 ug/L 133 10 -150 17 92
2-Hexanone ND 200 225.8 ug/L 113 24 -150 2 24
Isopropylbenzene ND 50.0 55.66 ug/L 111 10 -150 3 46
Methylene Chloride ND 50.0 47.34 ug/L 95 10 -150 4 18
4-Methyl-2-pentanone (MIBK)ND 200 197.5 ug/L 99 20 -150 1 20
Methyl tert-butyl ether ND 50.0 49.14 ug/L 98 10 -150 4 18
Naphthalene ND *50.0 66.40 ug/L 133 10 -150 5 53
n-Butylbenzene ND 50.0 57.56 ug/L 115 10 -150 7 76
N-Propylbenzene ND 50.0 57.61 ug/L 115 10 -150 4 57
p-Isopropyltoluene ND 50.0 60.23 ug/L 120 10 -150 7 62
sec-Butylbenzene ND 50.0 58.26 ug/L 117 10 -150 5 64
Styrene ND 50.0 56.26 ug/L 113 24 -147 3 40
tert-Butylbenzene ND 50.0 60.25 ug/L 121 10 -150 6 54
1,1,1,2-Tetrachloroethane ND 50.0 59.03 ug/L 118 42 -135 2 23
1,1,2,2-Tetrachloroethane ND 50.0 55.52 ug/L 111 52 -148 1 20
Tetrachloroethene ND 50.0 58.33 ug/L 117 10 -150 2 35
Toluene ND 50.0 53.81 ug/L 108 10 -150 4 26
trans-1,2-Dichloroethene ND 50.0 51.16 ug/L 102 66 -126 4 19
trans-1,3-Dichloropropene ND 50.0 56.39 ug/L 113 45 -128 2 20
1,2,3-Trichlorobenzene ND * F1 50.0 70.42 F1 ug/L 139 30 -137 12 44
1,2,4-Trichlorobenzene ND 50.0 68.85 ug/L 138 20 -139 10 44
1,1,1-Trichloroethane ND 50.0 49.79 ug/L 100 60 -131 4 20
1,1,2-Trichloroethane ND 50.0 54.10 ug/L 108 68 -127 1 19
Trichloroethene ND 50.0 53.06 ug/L 106 10 -150 2 22
Trichlorofluoromethane ND 50.0 50.95 ug/L 102 29 -144 6 20
1,2,3-Trichloropropane ND 50.0 55.62 ug/L 111 67 -130 0 22
1,2,4-Trimethylbenzene ND 50.0 57.65 ug/L 115 10 -150 5 54
TestAmerica Nashville
Page 56 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-75126-A-6 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252212
1,3,5-Trimethylbenzene ND 50.0 58.40 ug/L 117 10 -150 5 53
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Vinyl chloride ND 50.0 52.07 ug/L 104 46 -136 8 20
Xylenes, Total ND 100 110.0 ug/L 110 10 -150 3 41
1,2-Dichloroethane-d4 (Surr)67 -134
Surrogate
96
MSD MSD
Qualifier Limits%Recovery
106Toluene-d8 (Surr)80 -120
Client Sample ID: Method BlankLab Sample ID: MB 400-252235/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
RL MDL
Acetone ND 25.0 ug/Kg 04/05/15 09:40 04/05/15 11:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Benzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Bromobenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Bromochloromethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Bromodichloromethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Bromoform
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Bromomethane
ND 25.0 ug/Kg 04/05/15 09:40 04/05/15 11:09 12-Butanone (MEK)
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Carbon disulfide
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Carbon tetrachloride
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Chlorobenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Chlorodibromomethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Chloroethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Chloroform
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Chloromethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 12-Chlorotoluene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 14-Chlorotoluene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1cis-1,2-Dichloroethene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1cis-1,3-Dichloropropene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2-Dibromo-3-Chloropropane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2-Dibromoethane (EDB)
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Dibromomethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2-Dichlorobenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,3-Dichlorobenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,4-Dichlorobenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Dichlorodifluoromethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,1-Dichloroethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2-Dichloroethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,1-Dichloroethene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2-Dichloroethene, Total
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2-Dichloropropane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,3-Dichloropropane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 12,2-Dichloropropane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,1-Dichloropropene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Diisopropyl ether
TestAmerica Nashville
Page 57 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-252235/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
RL MDL
Ethylbenzene ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Hexachlorobutadiene
ND 25.0 ug/Kg 04/05/15 09:40 04/05/15 11:09 12-Hexanone
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Isopropylbenzene
ND 15.0 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Methylene Chloride
ND 25.0 ug/Kg 04/05/15 09:40 04/05/15 11:09 14-Methyl-2-pentanone (MIBK)
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Methyl tert-butyl ether
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Naphthalene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1n-Butylbenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1N-Propylbenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1p-Isopropyltoluene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1sec-Butylbenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Styrene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1tert-Butylbenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,1,1,2-Tetrachloroethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,1,2,2-Tetrachloroethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Tetrachloroethene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Toluene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1trans-1,2-Dichloroethene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1trans-1,3-Dichloropropene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2,3-Trichlorobenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2,4-Trichlorobenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,1,1-Trichloroethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,1,2-Trichloroethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Trichloroethene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Trichlorofluoromethane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2,3-Trichloropropane
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,2,4-Trimethylbenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 11,3,5-Trimethylbenzene
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Vinyl chloride
ND 5.00 ug/Kg 04/05/15 09:40 04/05/15 11:09 1Xylenes, Total
1,2-Dichloroethane-d4 (Surr)104 50-150 04/05/15 11:09 1
MB MB
Surrogate
04/05/15 09:40
Dil FacPreparedAnalyzedQualifierLimits%Recovery
102 04/05/15 09:40 04/05/15 11:09 1Toluene-d8 (Surr)80-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252235/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
Acetone 200 176.8 ug/Kg 88 43 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 50.0 54.24 ug/Kg 108 74 -119
Bromobenzene 50.0 57.75 ug/Kg 115 76 -121
Bromochloromethane 50.0 53.72 ug/Kg 107 78 -119
Bromodichloromethane 50.0 45.33 ug/Kg 91 68 -128
Bromoform 50.0 51.64 ug/Kg 103 54 -125
Bromomethane 50.0 65.12 ug/Kg 130 25 -150
TestAmerica Nashville
Page 58 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252235/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
2-Butanone (MEK)200 178.8 ug/Kg 89 62 -126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Carbon disulfide 50.0 54.43 ug/Kg 109 26 -150
Carbon tetrachloride 50.0 43.75 ug/Kg 87 70 -128
Chlorobenzene 50.0 57.61 ug/Kg 115 80 -116
Chlorodibromomethane 50.0 45.14 ug/Kg 90 65 -131
Chloroethane 50.0 51.77 ug/Kg 104 22 -150
Chloroform 50.0 45.66 ug/Kg 91 74 -119
Chloromethane 50.0 51.61 ug/Kg 103 36 -147
2-Chlorotoluene 50.0 57.07 ug/Kg 114 72 -119
4-Chlorotoluene 50.0 57.59 ug/Kg 115 72 -124
cis-1,2-Dichloroethene 50.0 55.17 ug/Kg 110 68 -126
cis-1,3-Dichloropropene 50.0 46.83 ug/Kg 94 68 -125
1,2-Dibromo-3-Chloropropane 50.0 47.63 ug/Kg 95 57 -123
1,2-Dibromoethane (EDB)50.0 52.70 ug/Kg 105 78 -119
Dibromomethane 50.0 50.45 ug/Kg 101 76 -117
1,2-Dichlorobenzene 50.0 55.16 ug/Kg 110 76 -120
1,3-Dichlorobenzene 50.0 56.13 ug/Kg 112 78 -118
1,4-Dichlorobenzene 50.0 55.60 ug/Kg 111 77 -118
Dichlorodifluoromethane 50.0 45.77 ug/Kg 92 44 -145
1,1-Dichloroethane 50.0 44.11 ug/Kg 88 61 -128
1,2-Dichloroethane 50.0 48.82 ug/Kg 98 70 -125
1,1-Dichloroethene 50.0 51.29 ug/Kg 103 62 -130
1,2-Dichloropropane 50.0 54.30 ug/Kg 109 64 -129
1,3-Dichloropropane 50.0 51.47 ug/Kg 103 75 -117
2,2-Dichloropropane 50.0 50.67 ug/Kg 101 66 -127
1,1-Dichloropropene 50.0 52.54 ug/Kg 105 72 -122
Diisopropyl ether 50.0 48.32 ug/Kg 97 46 -144
Ethylbenzene 50.0 58.56 ug/Kg 117 78 -120
Hexachlorobutadiene 50.0 56.60 ug/Kg 113 61 -140
2-Hexanone 200 181.2 ug/Kg 91 54 -140
Isopropylbenzene 50.0 58.24 ug/Kg 116 78 -119
Methylene Chloride 50.0 49.27 ug/Kg 99 45 -150
4-Methyl-2-pentanone (MIBK)200 184.5 ug/Kg 92 56 -137
Methyl tert-butyl ether 50.0 50.71 ug/Kg 101 69 -124
Naphthalene 50.0 48.87 ug/Kg 98 64 -126
n-Butylbenzene 50.0 56.15 ug/Kg 112 62 -136
N-Propylbenzene 50.0 60.27 ug/Kg 121 73 -121
p-Isopropyltoluene 50.0 57.88 ug/Kg 116 77 -123
sec-Butylbenzene 50.0 58.83 ug/Kg 118 75 -121
Styrene 50.0 49.79 ug/Kg 100 66 -132
tert-Butylbenzene 50.0 58.59 ug/Kg 117 76 -120
1,1,1,2-Tetrachloroethane 50.0 49.48 ug/Kg 99 76 -124
1,1,2,2-Tetrachloroethane 50.0 50.73 ug/Kg 101 67 -120
Tetrachloroethene 50.0 59.48 ug/Kg 119 74 -126
Toluene 50.0 55.82 ug/Kg 112 76 -120
trans-1,2-Dichloroethene 50.0 44.63 ug/Kg 89 65 -130
trans-1,3-Dichloropropene 50.0 45.70 ug/Kg 91 65 -126
1,2,3-Trichlorobenzene 50.0 55.03 ug/Kg 110 72 -124
TestAmerica Nashville
Page 59 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252235/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
1,2,4-Trichlorobenzene 50.0 55.26 ug/Kg 111 72 -126
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,1,1-Trichloroethane 50.0 45.95 ug/Kg 92 72 -121
1,1,2-Trichloroethane 50.0 52.68 ug/Kg 105 75 -118
Trichloroethene 50.0 47.46 ug/Kg 95 76 -122
Trichlorofluoromethane 50.0 52.65 ug/Kg 105 65 -132
1,2,3-Trichloropropane 50.0 51.56 ug/Kg 103 61 -123
1,2,4-Trimethylbenzene 50.0 57.88 ug/Kg 116 74 -121
1,3,5-Trimethylbenzene 50.0 58.14 ug/Kg 116 75 -122
Vinyl chloride 50.0 49.74 ug/Kg 99 52 -134
Xylenes, Total 100 113.6 ug/Kg 114 70 -120
1,2-Dichloroethane-d4 (Surr)50 -150
Surrogate
92
LCS LCS
Qualifier Limits%Recovery
100Toluene-d8 (Surr)80 -120
Client Sample ID: Matrix SpikeLab Sample ID: 400-103725-A-3-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
Acetone ND F2 206 201.1 ug/Kg 98 30 -175☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene ND 51.4 55.67 ug/Kg 108 56 -130☼
Bromobenzene ND 51.4 53.82 ug/Kg 105 52 -130☼
Bromochloromethane ND 51.4 55.76 ug/Kg 108 52 -130☼
Bromodichloromethane ND 51.4 45.06 ug/Kg 88 51 -130☼
Bromoform ND 51.4 48.94 ug/Kg 95 40 -130☼
Bromomethane ND 51.4 67.75 ug/Kg 132 14 -185☼
2-Butanone (MEK)ND 206 168.1 ug/Kg 82 26 -151☼
Carbon disulfide ND 51.4 54.62 ug/Kg 106 56 -130☼
Carbon tetrachloride ND 51.4 46.87 ug/Kg 91 52 -133☼
Chlorobenzene ND 51.4 54.54 ug/Kg 106 55 -130☼
Chlorodibromomethane ND 51.4 44.16 ug/Kg 86 49 -130☼
Chloroethane ND 51.4 53.11 ug/Kg 103 39 -157☼
Chloroform ND 51.4 48.98 ug/Kg 95 54 -130☼
Chloromethane ND 51.4 53.09 ug/Kg 103 37 -137☼
2-Chlorotoluene ND 51.4 53.38 ug/Kg 104 47 -130☼
4-Chlorotoluene ND 51.4 53.18 ug/Kg 103 46 -130☼
cis-1,2-Dichloroethene ND 51.4 49.67 ug/Kg 97 48 -130☼
cis-1,3-Dichloropropene ND 51.4 46.68 ug/Kg 91 48 -130☼
1,2-Dibromo-3-Chloropropane ND 51.4 44.37 ug/Kg 86 28 -133☼
1,2-Dibromoethane (EDB)ND 51.4 50.89 ug/Kg 99 52 -130☼
Dibromomethane ND 51.4 50.16 ug/Kg 98 51 -130☼
1,2-Dichlorobenzene ND 51.4 47.29 ug/Kg 92 41 -130☼
1,3-Dichlorobenzene ND 51.4 49.70 ug/Kg 97 43 -130☼
1,4-Dichlorobenzene ND 51.4 48.88 ug/Kg 95 42 -130☼
Dichlorodifluoromethane ND 51.4 46.41 ug/Kg 90 44 -133☼
1,1-Dichloroethane ND 51.4 47.17 ug/Kg 92 53 -130☼
1,2-Dichloroethane ND 51.4 52.54 ug/Kg 102 52 -130☼
TestAmerica Nashville
Page 60 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 400-103725-A-3-A MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
1,1-Dichloroethene ND 51.4 51.50 ug/Kg 100 57 -133☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dichloropropane ND 51.4 52.32 ug/Kg 102 52 -130☼
1,3-Dichloropropane ND 51.4 50.79 ug/Kg 99 55 -130☼
2,2-Dichloropropane ND 51.4 54.07 ug/Kg 105 49 -130☼
1,1-Dichloropropene ND 51.4 54.70 ug/Kg 106 59 -130☼
Diisopropyl ether ND 51.4 51.81 ug/Kg 101 40 -133☼
Ethylbenzene ND 51.4 57.36 ug/Kg 110 50 -130☼
Hexachlorobutadiene ND 51.4 39.61 ug/Kg 77 24 -136☼
2-Hexanone ND 206 182.5 ug/Kg 89 16 -163☼
Isopropylbenzene ND 51.4 52.99 ug/Kg 103 53 -130☼
Methylene Chloride ND 51.4 51.10 ug/Kg 99 52 -130☼
4-Methyl-2-pentanone (MIBK)ND 206 186.7 ug/Kg 91 27 -146☼
Methyl tert-butyl ether ND 51.4 52.19 ug/Kg 101 52 -130☼
Naphthalene ND 51.4 37.23 ug/Kg 72 25 -130☼
n-Butylbenzene ND 51.4 47.45 ug/Kg 92 40 -130☼
N-Propylbenzene ND 51.4 55.10 ug/Kg 107 48 -130☼
p-Isopropyltoluene ND 51.4 50.50 ug/Kg 98 45 -130☼
sec-Butylbenzene ND 51.4 50.61 ug/Kg 98 45 -130☼
Styrene ND 51.4 47.09 ug/Kg 92 50 -130☼
tert-Butylbenzene ND 51.4 53.72 ug/Kg 104 45 -130☼
1,1,1,2-Tetrachloroethane ND 51.4 47.91 ug/Kg 93 56 -130☼
1,1,2,2-Tetrachloroethane ND 51.4 50.80 ug/Kg 99 10 -155☼
Tetrachloroethene ND 51.4 53.02 ug/Kg 103 30 -157☼
Toluene ND 51.4 54.97 ug/Kg 107 55 -130☼
trans-1,2-Dichloroethene ND 51.4 49.08 ug/Kg 95 60 -130☼
trans-1,3-Dichloropropene ND 51.4 45.11 ug/Kg 88 47 -130☼
1,2,3-Trichlorobenzene ND 51.4 36.83 ug/Kg 72 19 -130☼
1,2,4-Trichlorobenzene ND 51.4 39.54 ug/Kg 77 21 -130☼
1,1,1-Trichloroethane ND 51.4 47.66 ug/Kg 93 53 -130☼
1,1,2-Trichloroethane ND 51.4 51.82 ug/Kg 101 49 -130☼
Trichloroethene ND 51.4 48.66 ug/Kg 95 41 -145☼
Trichlorofluoromethane ND 51.4 53.44 ug/Kg 104 55 -132☼
1,2,3-Trichloropropane ND 51.4 49.39 ug/Kg 96 46 -130☼
1,2,4-Trimethylbenzene ND 51.4 53.21 ug/Kg 103 40 -130☼
1,3,5-Trimethylbenzene ND 51.4 53.89 ug/Kg 105 47 -130☼
Vinyl chloride ND 51.4 52.40 ug/Kg 102 50 -141☼
Xylenes, Total ND 103 115.4 ug/Kg 108 51 -130☼
1,2-Dichloroethane-d4 (Surr)50 -150
Surrogate
95
MS MS
Qualifier Limits%Recovery
100Toluene-d8 (Surr)80 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 400-103725-A-3-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
Acetone ND F2 242 280.3 F2 ug/Kg 116 30 -175 33 31☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
TestAmerica Nashville
Page 61 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 400-103725-A-3-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
Benzene ND 60.6 61.43 ug/Kg 101 56 -130 10 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Bromobenzene ND 60.6 58.46 ug/Kg 96 52 -130 8 30☼
Bromochloromethane ND 60.6 61.77 ug/Kg 102 52 -130 10 30☼
Bromodichloromethane ND 60.6 49.88 ug/Kg 82 51 -130 10 30☼
Bromoform ND 60.6 51.38 ug/Kg 85 40 -130 5 30☼
Bromomethane ND 60.6 89.04 ug/Kg 147 14 -185 27 44☼
2-Butanone (MEK)ND 242 198.8 ug/Kg 82 26 -151 17 36☼
Carbon disulfide ND 60.6 63.31 ug/Kg 104 56 -130 15 30☼
Carbon tetrachloride ND 60.6 46.89 ug/Kg 77 52 -133 0 30☼
Chlorobenzene ND 60.6 62.66 ug/Kg 103 55 -130 14 30☼
Chlorodibromomethane ND 60.6 48.73 ug/Kg 80 49 -130 10 30☼
Chloroethane ND 60.6 66.88 ug/Kg 110 39 -157 23 55☼
Chloroform ND 60.6 50.39 ug/Kg 83 54 -130 3 30☼
Chloromethane ND 60.6 70.84 ug/Kg 117 37 -137 29 30☼
2-Chlorotoluene ND 60.6 58.86 ug/Kg 97 47 -130 10 30☼
4-Chlorotoluene ND 60.6 59.08 ug/Kg 97 46 -130 11 30☼
cis-1,2-Dichloroethene ND 60.6 62.43 ug/Kg 103 48 -130 23 30☼
cis-1,3-Dichloropropene ND 60.6 54.41 ug/Kg 90 48 -130 15 30☼
1,2-Dibromo-3-Chloropropane ND 60.6 48.21 ug/Kg 80 28 -133 8 30☼
1,2-Dibromoethane (EDB)ND 60.6 56.84 ug/Kg 94 52 -130 11 30☼
Dibromomethane ND 60.6 59.01 ug/Kg 97 51 -130 16 30☼
1,2-Dichlorobenzene ND 60.6 52.00 ug/Kg 86 41 -130 9 30☼
1,3-Dichlorobenzene ND 60.6 53.80 ug/Kg 89 43 -130 8 31☼
1,4-Dichlorobenzene ND 60.6 52.90 ug/Kg 87 42 -130 8 31☼
Dichlorodifluoromethane ND 60.6 60.60 ug/Kg 100 44 -133 27 30☼
1,1-Dichloroethane ND 60.6 50.64 ug/Kg 84 53 -130 7 30☼
1,2-Dichloroethane ND 60.6 56.86 ug/Kg 94 52 -130 8 30☼
1,1-Dichloroethene ND 60.6 59.26 ug/Kg 98 57 -133 14 30☼
1,2-Dichloropropane ND 60.6 61.33 ug/Kg 101 52 -130 16 30☼
1,3-Dichloropropane ND 60.6 55.23 ug/Kg 91 55 -130 8 30☼
2,2-Dichloropropane ND 60.6 55.62 ug/Kg 92 49 -130 3 30☼
1,1-Dichloropropene ND 60.6 55.55 ug/Kg 92 59 -130 2 30☼
Diisopropyl ether ND 60.6 58.38 ug/Kg 96 40 -133 12 30☼
Ethylbenzene ND 60.6 66.88 ug/Kg 109 50 -130 15 30☼
Hexachlorobutadiene ND 60.6 50.73 ug/Kg 84 24 -136 25 53☼
2-Hexanone ND 242 203.8 ug/Kg 84 16 -163 11 37☼
Isopropylbenzene ND 60.6 64.00 ug/Kg 106 53 -130 19 30☼
Methylene Chloride ND 60.6 61.44 ug/Kg 101 52 -130 18 30☼
4-Methyl-2-pentanone (MIBK)ND 242 235.5 ug/Kg 97 27 -146 23 32☼
Methyl tert-butyl ether ND 60.6 56.55 ug/Kg 93 52 -130 8 30☼
Naphthalene ND 60.6 38.52 ug/Kg 64 25 -130 3 31☼
n-Butylbenzene ND 60.6 54.61 ug/Kg 90 40 -130 14 40☼
N-Propylbenzene ND 60.6 62.08 ug/Kg 102 48 -130 12 32☼
p-Isopropyltoluene ND 60.6 59.15 ug/Kg 98 45 -130 16 37☼
sec-Butylbenzene ND 60.6 60.35 ug/Kg 100 45 -130 18 37☼
Styrene ND 60.6 54.42 ug/Kg 90 50 -130 14 30☼
tert-Butylbenzene ND 60.6 61.15 ug/Kg 101 45 -130 13 31☼
1,1,1,2-Tetrachloroethane ND 60.6 52.94 ug/Kg 87 56 -130 10 30☼
TestAmerica Nashville
Page 62 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 400-103725-A-3-B MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252244 Prep Batch: 252235
1,1,2,2-Tetrachloroethane ND 60.6 53.71 ug/Kg 89 10 -155 6 57☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Tetrachloroethene ND 60.6 58.08 ug/Kg 96 30 -157 9 30☼
Toluene ND 60.6 63.16 ug/Kg 104 55 -130 14 30☼
trans-1,2-Dichloroethene ND 60.6 47.87 ug/Kg 79 60 -130 2 30☼
trans-1,3-Dichloropropene ND 60.6 48.54 ug/Kg 80 47 -130 7 30☼
1,2,3-Trichlorobenzene ND 60.6 38.76 ug/Kg 64 19 -130 5 36☼
1,2,4-Trichlorobenzene ND 60.6 41.23 ug/Kg 68 21 -130 4 39☼
1,1,1-Trichloroethane ND 60.6 49.13 ug/Kg 81 53 -130 3 30☼
1,1,2-Trichloroethane ND 60.6 57.14 ug/Kg 94 49 -130 10 30☼
Trichloroethene ND 60.6 51.67 ug/Kg 85 41 -145 6 30☼
Trichlorofluoromethane ND 60.6 60.12 ug/Kg 99 55 -132 12 30☼
1,2,3-Trichloropropane ND 60.6 55.01 ug/Kg 91 46 -130 11 30☼
1,2,4-Trimethylbenzene ND 60.6 60.51 ug/Kg 100 40 -130 13 33☼
1,3,5-Trimethylbenzene ND 60.6 61.96 ug/Kg 102 47 -130 14 31☼
Vinyl chloride ND 60.6 68.43 ug/Kg 113 50 -141 27 30☼
Xylenes, Total ND 121 137.0 ug/Kg 109 51 -130 17 30☼
1,2-Dichloroethane-d4 (Surr)50 -150
Surrogate
89
MSD MSD
Qualifier Limits%Recovery
97Toluene-d8 (Surr)80 -120
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 400-251993/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252371 Prep Batch: 251993
RL MDL
Acenaphthene ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12-Chloronaphthalene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12-Chlorophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 11,2-Dichlorobenzene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 11,3-Dichlorobenzene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 11,4-Dichlorobenzene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 14-Bromophenyl phenyl ether
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 13,3'-Dichlorobenzidine
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 14-Chloro-3-methylphenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12,4-Dichlorophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 14-Chloroaniline
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 14-Chlorophenyl phenyl ether
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12,4-Dimethylphenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Acenaphthylene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 14,6-Dinitro-2-methylphenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Anthracene
ND 30.0 ug/L 04/02/15 11:06 04/06/15 19:03 12,4-Dinitrophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Benzo[a]anthracene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12,4-Dinitrotoluene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Benzo[a]pyrene
TestAmerica Nashville
Page 63 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-251993/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252371 Prep Batch: 251993
RL MDL
2,6-Dinitrotoluene ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Benzo[b]fluoranthene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Benzo[g,h,i]perylene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Benzo[k]fluoranthene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Bis(2-chloroethoxy)methane
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Bis(2-chloroethyl)ether
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Butyl benzyl phthalate
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Bis(2-ethylhexyl) phthalate
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Carbazole
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Chrysene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Dibenz(a,h)anthracene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Dibenzofuran
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 11-Methylnaphthalene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Diethyl phthalate
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12-Methylnaphthalene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Dimethyl phthalate
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12-Methylphenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Di-n-butyl phthalate
ND 20.0 ug/L 04/02/15 11:06 04/06/15 19:03 13 & 4 Methylphenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Fluoranthene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Fluorene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12-Nitroaniline
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Hexachlorobenzene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 13-Nitroaniline
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Hexachlorobutadiene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 14-Nitroaniline
ND 20.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Hexachlorocyclopentadiene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Hexachloroethane
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Indeno[1,2,3-cd]pyrene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12-Nitrophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Isophorone
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 14-Nitrophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Naphthalene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Nitrobenzene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1N-Nitrosodi-n-propylamine
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 20.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Pentachlorophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Phenanthrene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Phenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Pyrene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 11,2,4-Trichlorobenzene
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12,4,5-Trichlorophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1Di-n-octyl phthalate
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 12,4,6-Trichlorophenol
ND 10.0 ug/L 04/02/15 11:06 04/06/15 19:03 1bis (2-chloroisopropyl) ether
TestAmerica Nashville
Page 64 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-251993/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252371 Prep Batch: 251993
2-Fluorophenol (Surr)59 13-113 04/06/15 19:03 1
MB MB
Surrogate
04/02/15 11:06
Dil FacPreparedAnalyzedQualifierLimits%Recovery
108 04/02/15 11:06 04/06/15 19:03 1Nitrobenzene-d5 (Surr)36-126
91 04/02/15 11:06 04/06/15 19:03 1Phenol-d5 (Surr)17-127
108 04/02/15 11:06 04/06/15 19:03 12,4,6-Tribromophenol (Surr)26-150
125 04/02/15 11:06 04/06/15 19:03 1Terphenyl-d14 (Surr)44-149
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-251993/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 251993
Acenaphthene 120 126.5 ug/L 105 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2-Chloronaphthalene 120 115.9 ug/L 97 62 -130
2-Chlorophenol 120 122.0 ug/L 102 60 -130
1,2-Dichlorobenzene 120 57.73 ug/L 48 46 -130
1,3-Dichlorobenzene 120 54.65 ug/L 46 43 -130
1,4-Dichlorobenzene 120 49.37 *ug/L 41 45 -130
4-Bromophenyl phenyl ether 120 136.1 ug/L 113 62 -134
3,3'-Dichlorobenzidine 120 159.1 ug/L 133 10 -150
4-Chloro-3-methylphenol 120 144.3 ug/L 120 70 -130
2,4-Dichlorophenol 120 132.3 ug/L 110 67 -130
4-Chloroaniline 120 120.7 ug/L 101 10 -150
4-Chlorophenyl phenyl ether 120 134.9 ug/L 112 67 -130
2,4-Dimethylphenol 120 141.3 ug/L 118 52 -132
Acenaphthylene 120 123.1 ug/L 103 63 -130
4,6-Dinitro-2-methylphenol 240 211.5 ug/L 88 37 -150
Anthracene 120 133.7 ug/L 111 70 -130
2,4-Dinitrophenol 314 223.1 ug/L 71 15 -150
Benzo[a]anthracene 120 145.8 ug/L 121 70 -130
2,4-Dinitrotoluene 120 138.4 ug/L 115 66 -140
Benzo[a]pyrene 120 146.5 ug/L 122 70 -130
2,6-Dinitrotoluene 120 127.9 ug/L 107 70 -130
Benzo[g,h,i]perylene 120 120.3 ug/L 100 10 -150
Benzo[k]fluoranthene 120 155.7 ug/L 130 70 -130
Bis(2-chloroethoxy)methane 120 131.8 ug/L 110 53 -130
Bis(2-chloroethyl)ether 120 129.7 ug/L 108 55 -130
Butyl benzyl phthalate 120 165.6 ug/L 138 59 -145
Carbazole 120 145.1 ug/L 121 10 -150
Chrysene 120 141.1 ug/L 118 70 -130
Dibenz(a,h)anthracene 120 137.1 ug/L 114 59 -130
Dibenzofuran 120 131.7 ug/L 110 69 -130
1-Methylnaphthalene 120 119.6 ug/L 100 68 -130
Diethyl phthalate 120 147.3 ug/L 123 70 -133
2-Methylnaphthalene 120 118.1 ug/L 98 49 -140
Dimethyl phthalate 120 133.8 ug/L 112 69 -130
2-Methylphenol 120 135.7 ug/L 113 62 -130
Di-n-butyl phthalate 120 149.6 ug/L 125 68 -132
3 & 4 Methylphenol 120 134.0 ug/L 112 62 -130
TestAmerica Nashville
Page 65 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-251993/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 251993
Fluoranthene 120 136.9 ug/L 114 67 -132
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Fluorene 120 139.7 ug/L 116 70 -130
2-Nitroaniline 120 128.3 ug/L 107 55 -132
Hexachlorobenzene 120 134.4 ug/L 112 67 -132
3-Nitroaniline 120 124.2 ug/L 104 10 -150
Hexachlorobutadiene 120 57.85 ug/L 48 34 -150
4-Nitroaniline 120 143.9 ug/L 120 10 -150
Hexachlorocyclopentadiene 120 36.84 ug/L 31 1-150
Hexachloroethane 120 37.16 *ug/L 31 34 -133
Indeno[1,2,3-cd]pyrene 120 132.1 ug/L 110 57 -130
2-Nitrophenol 120 118.8 ug/L 99 62 -130
Isophorone 120 134.1 ug/L 112 60 -130
4-Nitrophenol 240 298.4 ug/L 124 31 -150
Naphthalene 120 93.09 ug/L 78 61 -130
Nitrobenzene 120 128.9 ug/L 107 61 -130
N-Nitrosodi-n-propylamine 120 143.8 ug/L 120 59 -130
n-Nitrosodiphenylamine(as
diphenylamine)
381 445.4 ug/L 117 36 -150
Pentachlorophenol 240 202.7 ug/L 84 46 -136
Phenanthrene 120 135.5 ug/L 113 70 -130
Phenol 120 111.5 ug/L 93 34 -137
Pyrene 120 151.4 ug/L 126 60 -138
1,2,4-Trichlorobenzene 120 74.16 ug/L 62 57 -130
2,4,5-Trichlorophenol 120 121.6 ug/L 101 67 -130
Di-n-octyl phthalate 120 164.3 ug/L 137 57 -148
2,4,6-Trichlorophenol 120 118.7 ug/L 99 67 -130
bis (2-chloroisopropyl) ether 120 114.9 ug/L 96 39 -136
2-Fluorophenol (Surr)13 -113
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
119Nitrobenzene-d5 (Surr)36 -126
108Phenol-d5 (Surr)17 -127
1072,4,6-Tribromophenol (Surr)26 -150
134Terphenyl-d14 (Surr)44 -149
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-251993/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252371 Prep Batch: 251993
Benzo[b]fluoranthene 120 150.5 ug/L 125 69 -133
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Bis(2-ethylhexyl) phthalate 120 138.3 ug/L 115 62 -139
TestAmerica Nashville
Page 66 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-251993/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 251993
Acenaphthene 120 119.6 ug/L 100 70 -130 6 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
2-Chloronaphthalene 120 113.0 ug/L 94 62 -130 3 30
2-Chlorophenol 120 112.5 ug/L 94 60 -130 8 30
1,2-Dichlorobenzene 120 57.49 ug/L 48 46 -130 0 30
1,3-Dichlorobenzene 120 53.91 ug/L 45 43 -130 1 30
1,4-Dichlorobenzene 120 49.59 *ug/L 41 45 -130 0 30
4-Bromophenyl phenyl ether 120 131.3 ug/L 109 62 -134 4 30
3,3'-Dichlorobenzidine 120 156.5 ug/L 130 10 -150 2 30
4-Chloro-3-methylphenol 120 130.5 ug/L 109 70 -130 10 30
2,4-Dichlorophenol 120 121.5 ug/L 101 67 -130 9 30
4-Chloroaniline 120 114.3 ug/L 95 10 -150 6 30
4-Chlorophenyl phenyl ether 120 127.5 ug/L 106 67 -130 6 30
2,4-Dimethylphenol 120 132.9 ug/L 111 52 -132 6 30
Acenaphthylene 120 116.7 ug/L 97 63 -130 5 30
4,6-Dinitro-2-methylphenol 240 191.3 ug/L 80 37 -150 10 30
Anthracene 120 128.8 ug/L 107 70 -130 4 30
2,4-Dinitrophenol 314 166.1 ug/L 53 15 -150 29 30
Benzo[a]anthracene 120 138.9 ug/L 116 70 -130 5 30
2,4-Dinitrotoluene 120 127.3 ug/L 106 66 -140 8 30
Benzo[a]pyrene 120 137.1 ug/L 114 70 -130 7 30
2,6-Dinitrotoluene 120 121.2 ug/L 101 70 -130 5 30
Benzo[b]fluoranthene 120 155.7 ug/L 130 69 -133 8 30
Benzo[g,h,i]perylene 120 120.7 ug/L 101 10 -150 0 30
Benzo[k]fluoranthene 120 139.2 ug/L 116 70 -130 11 30
Bis(2-chloroethoxy)methane 120 126.6 ug/L 106 53 -130 4 30
Bis(2-chloroethyl)ether 120 126.4 ug/L 105 55 -130 3 30
Butyl benzyl phthalate 120 164.5 ug/L 137 59 -145 1 30
Carbazole 120 132.8 ug/L 111 10 -150 9 30
Chrysene 120 134.2 ug/L 112 70 -130 5 30
Dibenz(a,h)anthracene 120 134.0 ug/L 112 59 -130 2 30
Dibenzofuran 120 123.4 ug/L 103 69 -130 7 30
1-Methylnaphthalene 120 118.2 ug/L 98 68 -130 1 30
Diethyl phthalate 120 141.8 ug/L 118 70 -133 4 30
2-Methylnaphthalene 120 116.0 ug/L 97 49 -140 2 30
Dimethyl phthalate 120 129.1 ug/L 108 69 -130 4 30
2-Methylphenol 120 123.1 ug/L 103 62 -130 10 30
Di-n-butyl phthalate 120 153.6 ug/L 128 68 -132 3 30
3 & 4 Methylphenol 120 120.2 ug/L 100 62 -130 11 30
Fluoranthene 120 135.4 ug/L 113 67 -132 1 30
Fluorene 120 130.6 ug/L 109 70 -130 7 30
2-Nitroaniline 120 115.7 ug/L 96 55 -132 10 30
Hexachlorobenzene 120 133.2 ug/L 111 67 -132 1 30
3-Nitroaniline 120 106.2 ug/L 89 10 -150 16 30
Hexachlorobutadiene 120 61.35 ug/L 51 34 -150 6 30
4-Nitroaniline 120 119.6 ug/L 100 10 -150 18 30
Hexachloroethane 120 36.92 *ug/L 31 34 -133 1 30
Indeno[1,2,3-cd]pyrene 120 128.6 ug/L 107 57 -130 3 30
2-Nitrophenol 120 110.3 ug/L 92 62 -130 7 30
TestAmerica Nashville
Page 67 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-251993/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 251993
Isophorone 120 131.5 ug/L 110 60 -130 2 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
4-Nitrophenol 240 227.9 ug/L 95 31 -150 27 30
Naphthalene 120 93.59 ug/L 78 61 -130 1 30
Nitrobenzene 120 124.1 ug/L 103 61 -130 4 30
N-Nitrosodi-n-propylamine 120 130.5 ug/L 109 59 -130 10 30
n-Nitrosodiphenylamine(as
diphenylamine)
381 424.5 ug/L 112 36 -150 5 30
Pentachlorophenol 240 175.0 ug/L 73 46 -136 15 30
Phenanthrene 120 130.1 ug/L 108 70 -130 4 30
Phenol 120 116.4 ug/L 97 34 -137 4 30
Pyrene 120 139.6 ug/L 116 60 -138 8 30
1,2,4-Trichlorobenzene 120 77.03 ug/L 64 57 -130 4 30
2,4,5-Trichlorophenol 120 108.3 ug/L 90 67 -130 12 30
Di-n-octyl phthalate 120 176.3 ug/L 147 57 -148 7 30
2,4,6-Trichlorophenol 120 106.2 ug/L 89 67 -130 11 30
bis (2-chloroisopropyl) ether 120 112.5 ug/L 94 39 -136 2 30
2-Fluorophenol (Surr)13 -113
Surrogate
86
LCSD LCSD
Qualifier Limits%Recovery
114Nitrobenzene-d5 (Surr)36 -126
98Phenol-d5 (Surr)17 -127
972,4,6-Tribromophenol (Surr)26 -150
122Terphenyl-d14 (Surr)44 -149
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-251993/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 252371 Prep Batch: 251993
Bis(2-ethylhexyl) phthalate 120 128.5 ug/L 107 62 -139 7 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Hexachlorocyclopentadiene 120 71.75 ug/L 60 1-150 5 30
Client Sample ID: Method BlankLab Sample ID: MB 400-252126/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252322 Prep Batch: 252126
RL MDL
Acenaphthene ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12-Chloronaphthalene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12-Chlorophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 11,2-Dichlorobenzene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 11,3-Dichlorobenzene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 11,4-Dichlorobenzene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 14-Bromophenyl phenyl ether
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 13,3'-Dichlorobenzidine
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 14-Chloro-3-methylphenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12,4-Dichlorophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 14-Chloroaniline
TestAmerica Nashville
Page 68 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-252126/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252322 Prep Batch: 252126
RL MDL
4-Chlorophenyl phenyl ether ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12,4-Dimethylphenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Acenaphthylene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 14,6-Dinitro-2-methylphenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Anthracene
ND 0.990 mg/Kg 04/03/15 09:35 04/06/15 16:15 12,4-Dinitrophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Benzo[a]anthracene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12,4-Dinitrotoluene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Benzo[a]pyrene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12,6-Dinitrotoluene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Benzo[b]fluoranthene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Benzo[g,h,i]perylene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Benzo[k]fluoranthene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Bis(2-chloroethoxy)methane
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Bis(2-chloroethyl)ether
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Butyl benzyl phthalate
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Bis(2-ethylhexyl) phthalate
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Carbazole
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Chrysene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Dibenz(a,h)anthracene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Dibenzofuran
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 11-Methylnaphthalene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Diethyl phthalate
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12-Methylnaphthalene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Dimethyl phthalate
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12-Methylphenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Di-n-butyl phthalate
ND 0.660 mg/Kg 04/03/15 09:35 04/06/15 16:15 13 & 4 Methylphenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Fluoranthene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Fluorene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12-Nitroaniline
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Hexachlorobenzene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 13-Nitroaniline
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Hexachlorobutadiene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 14-Nitroaniline
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Hexachlorocyclopentadiene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Hexachloroethane
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Indeno[1,2,3-cd]pyrene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12-Nitrophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Isophorone
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 14-Nitrophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Naphthalene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Nitrobenzene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1N-Nitrosodi-n-propylamine
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.660 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Pentachlorophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Phenanthrene
TestAmerica Nashville
Page 69 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-252126/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252322 Prep Batch: 252126
RL MDL
Phenol ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Pyrene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 11,2,4-Trichlorobenzene
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12,4,5-Trichlorophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1Di-n-octyl phthalate
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 12,4,6-Trichlorophenol
ND 0.330 mg/Kg 04/03/15 09:35 04/06/15 16:15 1bis (2-chloroisopropyl) ether
2-Fluorophenol (Surr)89 25-128 04/06/15 16:15 1
MB MB
Surrogate
04/03/15 09:35
Dil FacPreparedAnalyzedQualifierLimits%Recovery
89 04/03/15 09:35 04/06/15 16:15 1Nitrobenzene-d5 (Surr)15-136
92 04/03/15 09:35 04/06/15 16:15 1Phenol-d5 (Surr)29-130
74 04/03/15 09:35 04/06/15 16:15 12,4,6-Tribromophenol (Surr)10-150
98 04/03/15 09:35 04/06/15 16:15 1Terphenyl-d14 (Surr)24-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252126/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 252126
Acenaphthene 2.00 1.700 mg/Kg 85 59 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
2-Chloronaphthalene 2.00 1.626 mg/Kg 81 60 -130
2-Chlorophenol 2.00 1.657 mg/Kg 83 57 -130
1,2-Dichlorobenzene 2.00 1.625 mg/Kg 81 53 -104
1,3-Dichlorobenzene 2.00 1.653 mg/Kg 83 55 -101
1,4-Dichlorobenzene 2.00 1.565 mg/Kg 78 56 -130
4-Bromophenyl phenyl ether 2.00 1.863 mg/Kg 93 45 -134
3,3'-Dichlorobenzidine 2.00 1.799 mg/Kg 90 23 -150
4-Chloro-3-methylphenol 2.00 1.845 mg/Kg 92 30 -150
2,4-Dichlorophenol 2.00 1.761 mg/Kg 88 56 -130
4-Chloroaniline 2.00 1.443 mg/Kg 72 29 -130
4-Chlorophenyl phenyl ether 2.00 1.736 mg/Kg 87 58 -130
2,4-Dimethylphenol 2.00 1.849 mg/Kg 92 43 -130
Acenaphthylene 2.00 1.729 mg/Kg 86 60 -130
4,6-Dinitro-2-methylphenol 4.00 2.681 mg/Kg 67 10 -142
Anthracene 2.00 1.907 mg/Kg 95 64 -130
2,4-Dinitrophenol 5.23 1.970 mg/Kg 38 10 -130
Benzo[a]anthracene 2.00 1.914 mg/Kg 96 64 -130
2,4-Dinitrotoluene 2.00 1.734 mg/Kg 87 56 -130
Benzo[a]pyrene 2.00 1.941 mg/Kg 97 56 -130
2,6-Dinitrotoluene 2.00 1.665 mg/Kg 83 65 -130
Benzo[b]fluoranthene 2.00 2.059 mg/Kg 103 62 -130
Benzo[g,h,i]perylene 2.00 1.510 mg/Kg 76 39 -132
Benzo[k]fluoranthene 2.00 2.026 mg/Kg 101 60 -130
Bis(2-chloroethoxy)methane 2.00 1.728 mg/Kg 86 47 -130
Bis(2-chloroethyl)ether 2.00 1.626 mg/Kg 81 37 -130
Butyl benzyl phthalate 2.00 2.064 mg/Kg 103 57 -139
Bis(2-ethylhexyl) phthalate 2.00 2.235 mg/Kg 112 62 -140
TestAmerica Nashville
Page 70 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-252126/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 252126
Carbazole 2.00 1.979 mg/Kg 99 43 -150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Chrysene 2.00 1.829 mg/Kg 91 65 -130
Dibenz(a,h)anthracene 2.00 1.688 mg/Kg 84 43 -133
Dibenzofuran 2.00 1.717 mg/Kg 86 37 -137
1-Methylnaphthalene 2.00 1.776 mg/Kg 89 56 -130
Diethyl phthalate 2.00 1.956 mg/Kg 98 63 -130
2-Methylnaphthalene 2.00 1.781 mg/Kg 89 56 -130
Dimethyl phthalate 2.00 1.776 mg/Kg 89 65 -130
2-Methylphenol 2.00 1.700 mg/Kg 85 34 -130
Di-n-butyl phthalate 2.00 2.137 mg/Kg 107 62 -131
3 & 4 Methylphenol 2.00 1.682 mg/Kg 84 10 -150
Fluoranthene 2.00 1.957 mg/Kg 98 61 -130
Fluorene 2.00 1.800 mg/Kg 90 59 -130
2-Nitroaniline 2.00 1.645 mg/Kg 82 46 -133
Hexachlorobenzene 2.00 1.852 mg/Kg 93 44 -136
3-Nitroaniline 2.00 1.525 mg/Kg 76 10 -150
Hexachlorobutadiene 2.00 1.815 mg/Kg 91 44 -130
4-Nitroaniline 2.00 1.666 mg/Kg 83 10 -150
Hexachlorocyclopentadiene 2.00 0.8287 mg/Kg 41 1-150
Hexachloroethane 2.00 1.609 mg/Kg 80 44 -130
Indeno[1,2,3-cd]pyrene 2.00 1.649 mg/Kg 82 43 -131
2-Nitrophenol 2.00 1.539 mg/Kg 77 54 -130
Isophorone 2.00 1.783 mg/Kg 89 48 -130
4-Nitrophenol 4.00 3.401 mg/Kg 85 10 -150
Naphthalene 2.00 1.728 mg/Kg 86 45 -130
Nitrobenzene 2.00 1.719 mg/Kg 86 49 -130
N-Nitrosodi-n-propylamine 2.00 1.730 mg/Kg 86 44 -130
n-Nitrosodiphenylamine(as
diphenylamine)
4.00 3.853 mg/Kg 96 49 -148
Pentachlorophenol 4.00 2.759 mg/Kg 69 10 -150
Phenanthrene 2.00 1.882 mg/Kg 94 63 -130
Phenol 2.00 1.668 mg/Kg 83 43 -130
Pyrene 2.00 1.896 mg/Kg 95 47 -135
1,2,4-Trichlorobenzene 2.00 1.703 mg/Kg 85 50 -112
2,4,5-Trichlorophenol 2.00 1.638 mg/Kg 82 51 -130
Di-n-octyl phthalate 2.00 2.194 mg/Kg 110 57 -140
2,4,6-Trichlorophenol 2.00 1.533 mg/Kg 77 57 -130
bis (2-chloroisopropyl) ether 2.00 1.586 mg/Kg 79 14 -149
2-Fluorophenol (Surr)25 -128
Surrogate
88
LCS LCS
Qualifier Limits%Recovery
96Nitrobenzene-d5 (Surr)15 -136
88Phenol-d5 (Surr)29 -130
842,4,6-Tribromophenol (Surr)10 -150
102Terphenyl-d14 (Surr)24 -146
TestAmerica Nashville
Page 71 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SB-2 (10-11)Lab Sample ID: 490-75581-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 252126
Acenaphthene ND 2.78 2.269 mg/Kg 82 40 -140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
2-Chloronaphthalene ND 2.78 2.150 mg/Kg 77 40 -140☼
2-Chlorophenol ND 2.78 2.186 mg/Kg 79 40 -140☼
1,2-Dichlorobenzene ND 2.78 2.055 mg/Kg 74 40 -140☼
1,3-Dichlorobenzene ND 2.78 2.089 mg/Kg 75 40 -140☼
1,4-Dichlorobenzene ND 2.78 1.974 mg/Kg 71 40 -140☼
4-Bromophenyl phenyl ether ND 2.78 2.587 mg/Kg 93 40 -140☼
3,3'-Dichlorobenzidine ND 2.78 2.623 mg/Kg 94 40 -140☼
4-Chloro-3-methylphenol ND 2.78 2.606 mg/Kg 94 40 -140☼
2,4-Dichlorophenol ND 2.78 2.353 mg/Kg 85 40 -140☼
4-Chloroaniline ND 2.78 1.878 mg/Kg 68 40 -140☼
4-Chlorophenyl phenyl ether ND 2.78 2.397 mg/Kg 86 40 -140☼
2,4-Dimethylphenol ND 2.78 2.460 mg/Kg 89 40 -140☼
Acenaphthylene ND 2.78 2.298 mg/Kg 83 40 -140☼
4,6-Dinitro-2-methylphenol ND 5.55 4.050 mg/Kg 73 40 -140☼
Anthracene ND 2.78 2.682 mg/Kg 97 40 -140☼
2,4-Dinitrophenol ND 7.26 3.389 mg/Kg 47 40 -140☼
Benzo[a]anthracene ND 2.78 2.668 mg/Kg 96 40 -140☼
2,4-Dinitrotoluene ND 2.78 2.509 mg/Kg 90 40 -140☼
Benzo[a]pyrene ND 2.78 2.773 mg/Kg 100 40 -140☼
2,6-Dinitrotoluene ND 2.78 2.333 mg/Kg 84 40 -140☼
Benzo[b]fluoranthene ND 2.78 2.896 mg/Kg 104 40 -140☼
Benzo[g,h,i]perylene ND 2.78 2.322 mg/Kg 84 40 -140☼
Benzo[k]fluoranthene ND 2.78 2.869 mg/Kg 103 40 -140☼
Bis(2-chloroethoxy)methane ND 2.78 2.261 mg/Kg 81 40 -140☼
Bis(2-chloroethyl)ether ND 2.78 2.095 mg/Kg 75 40 -140☼
Butyl benzyl phthalate ND 2.78 2.903 mg/Kg 101 40 -140☼
Bis(2-ethylhexyl) phthalate 0.634 2.78 3.764 mg/Kg 113 40 -140☼
Carbazole ND 2.78 2.874 mg/Kg 104 40 -140☼
Chrysene ND 2.78 2.603 mg/Kg 94 40 -140☼
Dibenz(a,h)anthracene ND 2.78 2.553 mg/Kg 92 40 -140☼
Dibenzofuran ND 2.78 2.346 mg/Kg 85 40 -140☼
1-Methylnaphthalene ND 2.78 2.370 mg/Kg 85 40 -140☼
Diethyl phthalate ND 2.78 2.775 mg/Kg 100 40 -140☼
2-Methylnaphthalene ND 2.78 2.385 mg/Kg 86 40 -140☼
Dimethyl phthalate ND 2.78 2.478 mg/Kg 89 40 -140☼
2-Methylphenol ND 2.78 2.337 mg/Kg 84 40 -140☼
Di-n-butyl phthalate ND 2.78 3.008 mg/Kg 108 40 -140☼
3 & 4 Methylphenol ND 2.78 2.252 mg/Kg 81 40 -140☼
Fluoranthene ND 2.78 2.774 mg/Kg 100 40 -140☼
Fluorene ND 2.78 2.496 mg/Kg 90 40 -140☼
2-Nitroaniline ND 2.78 2.317 mg/Kg 83 40 -140☼
Hexachlorobenzene ND 2.78 2.584 mg/Kg 93 40 -140☼
3-Nitroaniline ND 2.78 2.128 mg/Kg 77 40 -140☼
Hexachlorobutadiene ND 2.78 2.324 mg/Kg 84 40 -140☼
4-Nitroaniline ND 2.78 2.446 mg/Kg 88 40 -140☼
Hexachlorocyclopentadiene ND F1 2.78 1.054 F1 mg/Kg 38 40 -140☼
Hexachloroethane ND 2.78 2.052 mg/Kg 74 40 -140☼
TestAmerica Nashville
Page 72 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SB-2 (10-11)Lab Sample ID: 490-75581-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 252126
Indeno[1,2,3-cd]pyrene ND 2.78 2.478 mg/Kg 89 40 -140☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
2-Nitrophenol ND 2.78 2.026 mg/Kg 73 40 -140☼
Isophorone ND 2.78 2.334 mg/Kg 84 40 -140☼
4-Nitrophenol ND 5.55 4.969 mg/Kg 89 40 -140☼
Naphthalene ND 2.78 2.253 mg/Kg 81 40 -140☼
Nitrobenzene ND 2.78 2.227 mg/Kg 80 40 -140☼
N-Nitrosodi-n-propylamine ND 2.78 2.283 mg/Kg 82 40 -140☼
n-Nitrosodiphenylamine(as
diphenylamine)
ND 5.55 5.502 mg/Kg 99 40 -140☼
Pentachlorophenol ND 5.55 4.133 mg/Kg 74 40 -140☼
Phenanthrene ND 2.78 2.672 mg/Kg 96 40 -140☼
Phenol ND 2.78 2.215 mg/Kg 80 40 -140☼
Pyrene ND 2.78 2.512 mg/Kg 90 40 -140☼
1,2,4-Trichlorobenzene ND 2.78 2.201 mg/Kg 79 40 -140☼
2,4,5-Trichlorophenol ND 2.78 2.275 mg/Kg 82 40 -140☼
Di-n-octyl phthalate ND 2.78 3.170 mg/Kg 114 40 -140☼
2,4,6-Trichlorophenol ND 2.78 2.174 mg/Kg 78 40 -140☼
bis (2-chloroisopropyl) ether ND 2.78 2.045 mg/Kg 74 40 -140☼
2-Fluorophenol (Surr)25 -128
Surrogate
84
MS MS
Qualifier Limits%Recovery
91Nitrobenzene-d5 (Surr)15 -136
84Phenol-d5 (Surr)29 -130
892,4,6-Tribromophenol (Surr)10 -150
102Terphenyl-d14 (Surr)24 -146
Client Sample ID: SB-2 (10-11)Lab Sample ID: 490-75581-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 252126
Acenaphthene ND 2.76 2.340 mg/Kg 85 40 -140 3 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2-Chloronaphthalene ND 2.76 2.211 mg/Kg 80 40 -140 3 30☼
2-Chlorophenol ND 2.76 2.323 mg/Kg 84 40 -140 6 30☼
1,2-Dichlorobenzene ND 2.76 2.195 mg/Kg 79 40 -140 7 30☼
1,3-Dichlorobenzene ND 2.76 2.219 mg/Kg 80 40 -140 6 30☼
1,4-Dichlorobenzene ND 2.76 2.106 mg/Kg 76 40 -140 6 30☼
4-Bromophenyl phenyl ether ND 2.76 2.641 mg/Kg 96 40 -140 2 30☼
3,3'-Dichlorobenzidine ND 2.76 2.618 mg/Kg 95 40 -140 0 30☼
4-Chloro-3-methylphenol ND 2.76 2.699 mg/Kg 98 40 -140 4 30☼
2,4-Dichlorophenol ND 2.76 2.497 mg/Kg 90 40 -140 6 30☼
4-Chloroaniline ND 2.76 1.864 mg/Kg 67 40 -140 1 30☼
4-Chlorophenyl phenyl ether ND 2.76 2.463 mg/Kg 89 40 -140 3 30☼
2,4-Dimethylphenol ND 2.76 2.584 mg/Kg 93 40 -140 5 30☼
Acenaphthylene ND 2.76 2.366 mg/Kg 86 40 -140 3 30☼
4,6-Dinitro-2-methylphenol ND 5.53 4.290 mg/Kg 78 40 -140 6 30☼
Anthracene ND 2.76 2.711 mg/Kg 98 40 -140 1 30☼
2,4-Dinitrophenol ND 7.22 3.870 mg/Kg 54 40 -140 13 30☼
TestAmerica Nashville
Page 73 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SB-2 (10-11)Lab Sample ID: 490-75581-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 252126
Benzo[a]anthracene ND 2.76 2.675 mg/Kg 97 40 -140 0 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2,4-Dinitrotoluene ND 2.76 2.516 mg/Kg 91 40 -140 0 30☼
Benzo[a]pyrene ND 2.76 2.745 mg/Kg 99 40 -140 1 30☼
2,6-Dinitrotoluene ND 2.76 2.380 mg/Kg 86 40 -140 2 30☼
Benzo[b]fluoranthene ND 2.76 2.867 mg/Kg 104 40 -140 1 30☼
Benzo[g,h,i]perylene ND 2.76 2.363 mg/Kg 86 40 -140 2 30☼
Benzo[k]fluoranthene ND 2.76 2.797 mg/Kg 101 40 -140 3 30☼
Bis(2-chloroethoxy)methane ND 2.76 2.382 mg/Kg 86 40 -140 5 30☼
Bis(2-chloroethyl)ether ND 2.76 2.174 mg/Kg 79 40 -140 4 30☼
Butyl benzyl phthalate ND 2.76 3.050 mg/Kg 107 40 -140 5 30☼
Bis(2-ethylhexyl) phthalate 0.634 2.76 3.763 mg/Kg 113 40 -140 0 30☼
Carbazole ND 2.76 2.883 mg/Kg 104 40 -140 0 30☼
Chrysene ND 2.76 2.576 mg/Kg 93 40 -140 1 30☼
Dibenz(a,h)anthracene ND 2.76 2.579 mg/Kg 93 40 -140 1 30☼
Dibenzofuran ND 2.76 2.401 mg/Kg 87 40 -140 2 30☼
1-Methylnaphthalene ND 2.76 2.463 mg/Kg 89 40 -140 4 30☼
Diethyl phthalate ND 2.76 2.808 mg/Kg 102 40 -140 1 30☼
2-Methylnaphthalene ND 2.76 2.458 mg/Kg 89 40 -140 3 30☼
Dimethyl phthalate ND 2.76 2.520 mg/Kg 91 40 -140 2 30☼
2-Methylphenol ND 2.76 2.451 mg/Kg 89 40 -140 5 30☼
Di-n-butyl phthalate ND 2.76 3.020 mg/Kg 109 40 -140 0 30☼
3 & 4 Methylphenol ND 2.76 2.439 mg/Kg 88 40 -140 8 30☼
Fluoranthene ND 2.76 2.774 mg/Kg 100 40 -140 0 30☼
Fluorene ND 2.76 2.547 mg/Kg 92 40 -140 2 30☼
2-Nitroaniline ND 2.76 2.360 mg/Kg 85 40 -140 2 30☼
Hexachlorobenzene ND 2.76 2.602 mg/Kg 94 40 -140 1 30☼
3-Nitroaniline ND 2.76 2.070 mg/Kg 75 40 -140 3 30☼
Hexachlorobutadiene ND 2.76 2.431 mg/Kg 88 40 -140 4 30☼
4-Nitroaniline ND 2.76 2.423 mg/Kg 88 40 -140 1 30☼
Hexachlorocyclopentadiene ND F1 2.76 1.098 mg/Kg 40 40 -140 4 30☼
Hexachloroethane ND 2.76 2.177 mg/Kg 79 40 -140 6 30☼
Indeno[1,2,3-cd]pyrene ND 2.76 2.495 mg/Kg 90 40 -140 1 30☼
2-Nitrophenol ND 2.76 2.163 mg/Kg 78 40 -140 7 30☼
Isophorone ND 2.76 2.439 mg/Kg 88 40 -140 4 30☼
4-Nitrophenol ND 5.53 4.880 mg/Kg 88 40 -140 2 30☼
Naphthalene ND 2.76 2.362 mg/Kg 85 40 -140 5 30☼
Nitrobenzene ND 2.76 2.348 mg/Kg 85 40 -140 5 30☼
N-Nitrosodi-n-propylamine ND 2.76 2.437 mg/Kg 88 40 -140 7 30☼
n-Nitrosodiphenylamine(as
diphenylamine)
ND 5.53 5.567 mg/Kg 101 40 -140 1 30☼
Pentachlorophenol ND 5.53 4.312 mg/Kg 78 40 -140 4 30☼
Phenanthrene ND 2.76 2.695 mg/Kg 98 40 -140 1 30☼
Phenol ND 2.76 2.174 mg/Kg 79 40 -140 2 30☼
Pyrene ND 2.76 2.649 mg/Kg 96 40 -140 5 30☼
1,2,4-Trichlorobenzene ND 2.76 2.286 mg/Kg 83 40 -140 4 30☼
2,4,5-Trichlorophenol ND 2.76 2.364 mg/Kg 86 40 -140 4 30☼
Di-n-octyl phthalate ND 2.76 3.215 mg/Kg 116 40 -140 1 30☼
2,4,6-Trichlorophenol ND 2.76 2.227 mg/Kg 81 40 -140 2 30☼
TestAmerica Nashville
Page 74 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Sample Results
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SB-2 (10-11)Lab Sample ID: 490-75581-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252261 Prep Batch: 252126
bis (2-chloroisopropyl) ether ND 2.76 2.157 mg/Kg 78 40 -140 5 30☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2-Fluorophenol (Surr)25 -128
Surrogate
85
MSD MSD
Qualifier Limits%Recovery
91Nitrobenzene-d5 (Surr)15 -136
86Phenol-d5 (Surr)29 -130
872,4,6-Tribromophenol (Surr)10 -150
102Terphenyl-d14 (Surr)24 -146
Method: Moisture - Percent Moisture
Client Sample ID: DuplicateLab Sample ID: 400-103661-A-2 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252125
Percent Moisture 38 36 %4 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 400-103728-A-40 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 252125
Percent Moisture 7.3 7.6 %4 10
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Nashville
Page 75 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
GC/MS VOA
Analysis Batch: 252212
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-75126-A-6 MS Matrix Spike Total/NA
Water 8260B490-75126-A-6 MSD Matrix Spike Duplicate Total/NA
Water 8260B490-75581-7 MW-7 Total/NA
Water 8260B490-75581-8 TMW-1 Total/NA
Water 8260B490-75581-9 TMW-2 Total/NA
Water 8260B490-75581-10 TMW-3 Total/NA
Water 8260B490-75581-11 TMW-4 Total/NA
Water 8260B490-75581-12 MW-11 Total/NA
Water 8260B490-75581-13 MW-8 Total/NA
Water 8260BLCS 400-252212/1002 Lab Control Sample Total/NA
Water 8260BMB 400-252212/4 Method Blank Total/NA
Prep Batch: 252235
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035400-103725-A-3-A MS Matrix Spike Total/NA
Solid 5035400-103725-A-3-B MSD Matrix Spike Duplicate Total/NA
Solid 5035490-75581-1 SB-2 (10-11)Total/NA
Solid 5035490-75581-2 SB-3 (9-10)Total/NA
Solid 5035490-75581-3 SB-4 (5)Total/NA
Solid 5035490-75581-4 SB-5 (5)Total/NA
Solid 5035490-75581-5 SB-6 (10)Total/NA
Solid 5035490-75581-6 SB-1 (8-9)Total/NA
Solid 5035LCS 400-252235/2-A Lab Control Sample Total/NA
Solid 5035MB 400-252235/1-A Method Blank Total/NA
Analysis Batch: 252244
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 252235400-103725-A-3-A MS Matrix Spike Total/NA
Solid 8260B 252235400-103725-A-3-B MSD Matrix Spike Duplicate Total/NA
Solid 8260B 252235490-75581-1 SB-2 (10-11)Total/NA
Solid 8260B 252235490-75581-2 SB-3 (9-10)Total/NA
Solid 8260B 252235490-75581-3 SB-4 (5)Total/NA
Solid 8260B 252235490-75581-4 SB-5 (5)Total/NA
Solid 8260B 252235490-75581-5 SB-6 (10)Total/NA
Solid 8260B 252235490-75581-6 SB-1 (8-9)Total/NA
Solid 8260B 252235LCS 400-252235/2-A Lab Control Sample Total/NA
Solid 8260B 252235MB 400-252235/1-A Method Blank Total/NA
GC/MS Semi VOA
Prep Batch: 251993
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520C490-75581-7 MW-7 Total/NA
Water 3520C490-75581-8 TMW-1 Total/NA
Water 3520C490-75581-9 TMW-2 Total/NA
Water 3520C490-75581-10 TMW-3 Total/NA
Water 3520C490-75581-11 TMW-4 Total/NA
Water 3520C490-75581-12 MW-11 Total/NA
Water 3520C490-75581-13 MW-8 Total/NA
Water 3520CLCS 400-251993/2-A Lab Control Sample Total/NA
TestAmerica Nashville
Page 76 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
GC/MS Semi VOA (Continued)
Prep Batch: 251993 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3520CLCSD 400-251993/3-A Lab Control Sample Dup Total/NA
Water 3520CMB 400-251993/1-A Method Blank Total/NA
Prep Batch: 252126
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546490-75581-1 SB-2 (10-11)Total/NA
Solid 3546490-75581-1 MS SB-2 (10-11)Total/NA
Solid 3546490-75581-1 MSD SB-2 (10-11)Total/NA
Solid 3546490-75581-2 SB-3 (9-10)Total/NA
Solid 3546490-75581-3 SB-4 (5)Total/NA
Solid 3546490-75581-4 SB-5 (5)Total/NA
Solid 3546490-75581-5 SB-6 (10)Total/NA
Solid 3546490-75581-6 SB-1 (8-9)Total/NA
Solid 3546LCS 400-252126/2-A Lab Control Sample Total/NA
Solid 3546MB 400-252126/1-A Method Blank Total/NA
Analysis Batch: 252258
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 252126490-75581-3 SB-4 (5)Total/NA
Solid 8270D 252126490-75581-4 SB-5 (5)Total/NA
Solid 8270D 252126490-75581-5 SB-6 (10)Total/NA
Solid 8270D 252126490-75581-6 SB-1 (8-9)Total/NA
Analysis Batch: 252261
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 252126490-75581-1 MS SB-2 (10-11)Total/NA
Solid 8270D 252126490-75581-1 MSD SB-2 (10-11)Total/NA
Water 8270D 251993LCS 400-251993/2-A Lab Control Sample Total/NA
Solid 8270D 252126LCS 400-252126/2-A Lab Control Sample Total/NA
Water 8270D 251993LCSD 400-251993/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 252322
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 252126490-75581-1 SB-2 (10-11)Total/NA
Solid 8270D 252126490-75581-2 SB-3 (9-10)Total/NA
Water 8270D 251993490-75581-7 MW-7 Total/NA
Water 8270D 251993490-75581-8 TMW-1 Total/NA
Water 8270D 251993490-75581-9 TMW-2 Total/NA
Water 8270D 251993490-75581-10 TMW-3 Total/NA
Water 8270D 251993490-75581-11 TMW-4 Total/NA
Water 8270D 251993490-75581-12 MW-11 Total/NA
Water 8270D 251993490-75581-13 MW-8 Total/NA
Solid 8270D 252126MB 400-252126/1-A Method Blank Total/NA
Analysis Batch: 252371
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 251993LCS 400-251993/2-A Lab Control Sample Total/NA
Water 8270D 251993LCSD 400-251993/3-A Lab Control Sample Dup Total/NA
Water 8270D 251993MB 400-251993/1-A Method Blank Total/NA
TestAmerica Nashville
Page 77 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
QC Association Summary
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
General Chemistry
Analysis Batch: 252125
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture400-103661-A-2 DU Duplicate Total/NA
Solid Moisture400-103728-A-40 DU Duplicate Total/NA
Solid Moisture490-75581-1 SB-2 (10-11)Total/NA
Solid Moisture490-75581-2 SB-3 (9-10)Total/NA
Solid Moisture490-75581-3 SB-4 (5)Total/NA
Solid Moisture490-75581-4 SB-5 (5)Total/NA
Solid Moisture490-75581-5 SB-6 (10)Total/NA
Solid Moisture490-75581-6 SB-1 (8-9)Total/NA
TestAmerica Nashville
Page 78 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-75581-1
Project/Site: Seneca Place Shopping Center SDG: AZA-001
Client Sample ID: SB-2 (10-11)Lab Sample ID: 490-75581-1
Matrix: SolidDate Collected: 03/30/15 10:30
Percent Solids: 71.0Date Received: 04/01/15 08:00
Prep 5035 LRC04/05/15 09:40 TAL PEN252235
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.149 g 5.00 mL
Analysis 8260B 1 252244 04/05/15 11:35 LRC TAL PENTotal/NA 6.149 g 5.00 mL
Prep 3546 252126 04/03/15 09:35 VC1 TAL PENTotal/NA 15.38 g 1.0 mL
Analysis 8270D 1 252322 04/06/15 22:56 AJR TAL PENTotal/NA 15.38 g 1.0 mL
Analysis Moisture 1 252125 04/03/15 09:29 TMP TAL PENTotal/NA
Client Sample ID: SB-3 (9-10)Lab Sample ID: 490-75581-2
Matrix: SolidDate Collected: 03/30/15 11:00
Percent Solids: 61.3Date Received: 04/01/15 08:00
Prep 5035 LRC04/05/15 09:40 TAL PEN252235
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.059 g 5.00 mL
Analysis 8260B 1 252244 04/05/15 12:00 LRC TAL PENTotal/NA 6.059 g 5.00 mL
Prep 3546 252126 04/03/15 09:35 VC1 TAL PENTotal/NA 15.18 g 1.0 mL
Analysis 8270D 1 252322 04/06/15 23:32 AJR TAL PENTotal/NA 15.18 g 1.0 mL
Analysis Moisture 1 252125 04/03/15 09:29 TMP TAL PENTotal/NA
Client Sample ID: SB-4 (5)Lab Sample ID: 490-75581-3
Matrix: SolidDate Collected: 03/30/15 13:00
Percent Solids: 76.9Date Received: 04/01/15 08:00
Prep 5035 LRC04/05/15 09:40 TAL PEN252235
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.964 g 5.00 mL
Analysis 8260B 1 252244 04/05/15 12:26 LRC TAL PENTotal/NA 5.964 g 5.00 mL
Prep 3546 252126 04/03/15 09:35 VC1 TAL PENTotal/NA 15.20 g 1.0 mL
Analysis 8270D 1 252258 04/05/15 18:35 AJR TAL PENTotal/NA 15.20 g 1.0 mL
Analysis Moisture 1 252125 04/03/15 09:29 TMP TAL PENTotal/NA
Client Sample ID: SB-5 (5)Lab Sample ID: 490-75581-4
Matrix: SolidDate Collected: 03/30/15 13:20
Percent Solids: 81.5Date Received: 04/01/15 08:00
Prep 5035 LRC04/05/15 09:40 TAL PEN252235
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.368 g 5.00 mL
Analysis 8260B 1 252244 04/05/15 12:51 LRC TAL PENTotal/NA 6.368 g 5.00 mL
Prep 3546 252126 04/03/15 09:35 VC1 TAL PENTotal/NA 15.46 g 1.0 mL
Analysis 8270D 1 252258 04/05/15 19:12 AJR TAL PENTotal/NA 15.46 g 1.0 mL
Analysis Moisture 1 252125 04/03/15 09:29 TMP TAL PENTotal/NA
TestAmerica Nashville
Page 79 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-75581-1
Project/Site: Seneca Place Shopping Center SDG: AZA-001
Client Sample ID: SB-6 (10)Lab Sample ID: 490-75581-5
Matrix: SolidDate Collected: 03/30/15 13:45
Percent Solids: 66.6Date Received: 04/01/15 08:00
Prep 5035 LRC04/05/15 09:40 TAL PEN252235
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.143 g 5.00 mL
Analysis 8260B 1 252244 04/05/15 13:17 LRC TAL PENTotal/NA 6.143 g 5.00 mL
Prep 3546 252126 04/03/15 09:35 VC1 TAL PENTotal/NA 15.07 g 1.0 mL
Analysis 8270D 1 252258 04/05/15 19:48 AJR TAL PENTotal/NA 15.07 g 1.0 mL
Analysis Moisture 1 252125 04/03/15 11:01 TMP TAL PENTotal/NA
Client Sample ID: SB-1 (8-9)Lab Sample ID: 490-75581-6
Matrix: SolidDate Collected: 03/30/15 14:20
Percent Solids: 64.5Date Received: 04/01/15 08:00
Prep 5035 LRC04/05/15 09:40 TAL PEN252235
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.437 g 5.00 mL
Analysis 8260B 1 252244 04/05/15 13:41 LRC TAL PENTotal/NA 6.437 g 5.00 mL
Prep 3546 252126 04/03/15 09:35 VC1 TAL PENTotal/NA 15.22 g 1.0 mL
Analysis 8270D 1 252258 04/05/15 20:24 AJR TAL PENTotal/NA 15.22 g 1.0 mL
Analysis Moisture 1 252125 04/03/15 11:01 TMP TAL PENTotal/NA
Client Sample ID: MW-7 Lab Sample ID: 490-75581-7
Matrix: WaterDate Collected: 03/30/15 09:10
Date Received: 04/01/15 08:00
Analysis 8260B CLN04/04/15 16:511 TAL PEN252212
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 251993 04/02/15 11:06 KH1 TAL PENTotal/NA 250 mL 1 mL
Analysis 8270D 1 252322 04/06/15 18:41 AJR TAL PENTotal/NA 250 mL 1 mL
Client Sample ID: TMW-1 Lab Sample ID: 490-75581-8
Matrix: WaterDate Collected: 03/30/15 12:10
Date Received: 04/01/15 08:00
Analysis 8260B CLN04/04/15 17:171 TAL PEN252212
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 251993 04/02/15 11:06 KH1 TAL PENTotal/NA 250 mL 1 mL
Analysis 8270D 1 252322 04/06/15 19:18 AJR TAL PENTotal/NA 250 mL 1 mL
Client Sample ID: TMW-2 Lab Sample ID: 490-75581-9
Matrix: WaterDate Collected: 03/30/15 14:00
Date Received: 04/01/15 08:00
Analysis 8260B CLN04/04/15 17:421 TAL PEN252212
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 251993 04/02/15 11:06 KH1 TAL PENTotal/NA 250 mL 1 mL
TestAmerica Nashville
Page 80 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-75581-1
Project/Site: Seneca Place Shopping Center SDG: AZA-001
Client Sample ID: TMW-2 Lab Sample ID: 490-75581-9
Matrix: WaterDate Collected: 03/30/15 14:00
Date Received: 04/01/15 08:00
Analysis 8270D AJR04/06/15 19:541 TAL PEN252322
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 250 mL 1 mL
Client Sample ID: TMW-3 Lab Sample ID: 490-75581-10
Matrix: WaterDate Collected: 03/30/15 14:50
Date Received: 04/01/15 08:00
Analysis 8260B CLN04/04/15 18:081 TAL PEN252212
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 251993 04/02/15 11:06 KH1 TAL PENTotal/NA 250 mL 1 mL
Analysis 8270D 1 252322 04/06/15 20:30 AJR TAL PENTotal/NA 250 mL 1 mL
Client Sample ID: TMW-4 Lab Sample ID: 490-75581-11
Matrix: WaterDate Collected: 03/30/15 15:50
Date Received: 04/01/15 08:00
Analysis 8260B CLN04/04/15 19:512 TAL PEN252212
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 251993 04/02/15 11:06 KH1 TAL PENTotal/NA 250 mL 1 mL
Analysis 8270D 1 252322 04/06/15 21:07 AJR TAL PENTotal/NA 250 mL 1 mL
Client Sample ID: MW-11 Lab Sample ID: 490-75581-12
Matrix: WaterDate Collected: 03/30/15 16:50
Date Received: 04/01/15 08:00
Analysis 8260B CLN04/04/15 18:341 TAL PEN252212
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 251993 04/02/15 11:06 KH1 TAL PENTotal/NA 250 mL 1 mL
Analysis 8270D 1 252322 04/06/15 21:43 AJR TAL PENTotal/NA 250 mL 1 mL
Client Sample ID: MW-8 Lab Sample ID: 490-75581-13
Matrix: WaterDate Collected: 03/30/15 17:15
Date Received: 04/01/15 08:00
Analysis 8260B CLN04/04/15 18:591 TAL PEN252212
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3520C 251993 04/02/15 11:06 KH1 TAL PENTotal/NA 250 mL 1 mL
Analysis 8270D 1 252322 04/06/15 22:19 AJR TAL PENTotal/NA 250 mL 1 mL
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TestAmerica Nashville
Page 81 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Method Summary
TestAmerica Job ID: 490-75581-1Client: Hart & Hickman, PC
SDG: AZA-001Project/Site: Seneca Place Shopping Center
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL PEN
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL PEN
EPAMoisturePercent Moisture TAL PEN
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = TestAmerica Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
TestAmerica Nashville
Page 82 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-75581-1
Project/Site: Seneca Place Shopping Center SDG: AZA-001
Laboratory: TestAmerica Nashville
The certifications listed below are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
North Carolina (WW/SW)3874State Program 12-31-15
Laboratory: TestAmerica Pensacola
All certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
Alabama 401504State Program 06-30-15
Arizona State Program 9 AZ0710 01-11-16
Arkansas DEQ State Program 6 88-0689 09-01-15
Florida NELAP 4 E81010 06-30-15
Georgia State Program 4 N/A 06-30-15
Illinois NELAP 5 200041 10-09-15
Iowa State Program 7 367 07-31-16
Kansas NELAP 7 E-10253 04-30-15
Kentucky (UST)State Program 4 53 06-30-15
Kentucky (WW)State Program 4 98030 12-31-15
Louisiana NELAP 6 30976 06-30-15
Maryland State Program 3 233 09-30-15
Michigan State Program 5 9912 06-30-15
New Jersey NELAP 2 FL006 06-30-15
North Carolina (WW/SW)State Program 4 314 12-31-15
Oklahoma State Program 6 9810 08-31-15
Pennsylvania NELAP 3 68-00467 01-31-16
Rhode Island State Program 1 LAO00307 12-30-15
South Carolina State Program 4 96026 06-30-15
Tennessee State Program 4 TN02907 06-30-15
Texas NELAP 6 T104704286-12-5 09-30-15
USDA Federal P330-13-00193 07-01-16
Virginia NELAP 3 460166 06-14-15
West Virginia DEP State Program 3 136 06-30-15
TestAmerica Nashville
Page 83 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 84 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Page 85 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13
Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-75581-1
SDG Number: AZA-001
Login Number: 75581
Question Answer Comment
Creator: Hayes, Ken
List Source: TestAmerica Nashville
List Number: 1
Radioactivity wasn't checked or is </= background as measured by a survey
meter.
The cooler's custody seal, if present, is intact.
Sample custody seals, if present, are intact.
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
Cooler Temperature is acceptable.
Cooler Temperature is recorded.
COC is present.
COC is filled out in ink and legible.
COC is filled out with all pertinent information.
Is the Field Sampler's name present on COC?
There are no discrepancies between the containers received and the COC.
Samples are received within Holding Time.
Sample containers have legible labels.
Containers are not broken or leaking.
Sample collection date/times are provided.
Appropriate sample containers are used.
Sample bottles are completely filled.
Sample Preservation Verified.
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
Samples do not require splitting or compositing.
Residual Chlorine Checked.
TestAmerica Nashville
Page 86 of 86 4/8/2015
1
2
3
4
5
6
7
8
9
10
11
12
13