08022_Reeves_LURU Monitoring Rpt_20110831

ANNUAL MONITORING REPORT (2011) FORMER REEVES BROTHERS BROWNFIELDS SITE NO. 08022-04-60 8900 RESEARCH DRIVE CHARLOTTE, MECKLENBURG CO, NC S&ME PROJECT 1354-11-006

Prepared for:

Polymers Center of Excellence
8900 Research Drive
Charlotte, North Carolina 28104-6015

Prepared by:

S&ME, Inc.
9711 Southern Pine Boulevard
Charlotte, North Carolina 28273-5560

January 31, 2011
2011 Annual Monitoring Report S&ME Project No. 1354-11-006
Reeves Site, Brownfields Site No. 08022-04-60, Charlotte, NC January 31, 2011

2
with the Notice of Brownfields Property. The April 25, 2006 letter indicated that four
monitoring wells (MW-5B, MW-5C, MW-6, and MW-7) and the adjacent stream are to
be sampled annually and analyzed for volatile organic compounds (VOCs) by
Environmental Protection Agency (EPA) Method 8260 or equivalent. The monitor wells
and stream sample locations are illustrated on Figure 3.

2. SCOPE OF SERVICES
2.1 Surface Water and Groundwater Sampling
On January 20, 2011, S&ME collected one upstream sample (SW-U) and one
downstream (SW-D) surface water sample at the approximate locations shown on Figure
3. The SW-U sample was collected from the bridge, using a disposable bailer. The SW-
D sample was collected by directly dipping the sample container into the stream with
care not to allow sediment to enter the sample containers and not to allow overfilling to
prevent the loss of any preservatives, if present. Sample containers with appropriate
preservatives were provided by the laboratory.

On January 20, 2011, S&ME also collected groundwater samples from the following
monitor wells: MW-5B, MW-5C, MW-6, and MW-7. Prior to sampling, the depth to
water in each well was measured from the top of the well casing (TOC) and the
monitoring wells were purged of three to five well volumes (or until dry) using a
disposable bailer. The samples were submitted to Pace Analytical Laboratories, Inc.
(Pace) in Huntersville, North Carolina, a North Carolina-certified laboratory, for the
analysis of VOCs by EPA Method 8260. In addition to the four monitor well samples,
one duplicate sample of MW-5C (identified as Duplicate) was additionally analyzed for
quality control purposes. Copies of the field sampling forms are included in Appendix
II.

The purge water was contained in a 55-gallon drum for off-site disposal. A purgewater
sample was collected for laboratory analysis for disposal purposes. The purge water will
be disposed off-site at a permitted facility as appropriate for hazardous or non-hazardous
waste. Documentation of disposal, (i.e., waste manifest and invoice), will be provided to
Polymers Center of Excellence upon receipt by the disposal company. S&ME will also
provide a copy of that documentation to the NCDENR, if requested by the NCDENR.

3. RESULTS
3.1 Groundwater Flow
The depth to water in the surficial aquifer ranged from 10.45 feet below the top of casing
(flush mount well) in monitor well MW-7, to 30.42 feet below the top of casing (~2.5
feet stickup) in the monitor well MW-5B. The January 2011 groundwater levels ranged
from approximately 3 to 4 feet lower than the January 2010 groundwater levels. Based
2011 Annual Monitoring Report S&ME Project No. 1354-11-006
Reeves Site, Brownfields Site No. 08022-04-60, Charlotte, NC January 31, 2011

3
on the top of casing elevations and the depth to water (Table 1), the groundwater flow is
generally toward the east-southeast in the general direction of Doby Creek under a
hydraulic gradient of approximately 0.043 ft/ft between monitoring wells MW-5B and
MW-6, and approximately 0.016 ft/ft between monitoring wells MW-6 and MW-7
(Figure 3).

The local vertical hydraulic gradient calculated using water levels measured in nested
monitoring wells MW-5B and MW-5C is approximately 0.004 ft/ft in the downward
direction.
3.2 Surface Water Quality
VOCs were not detected in the two surface water samples (SW-U and SW-D). The
results are summarized in Table 2, and a copy of the laboratory report is included in
Appendix I.
3.3 Groundwater Quality
No VOCs were detected in the groundwater samples from the downgradient monitor well
MW-7. Tetrachloroethene was detected in monitor wells MW-5B [17.1 micrograms per
liter (µg/L)], MW-5C (1.1 ug/L), and MW-6 (35.9 µg/L), compared to the 15A NCAC 2L
.0202 groundwater quality standard (2L Standard) of 0.7 µg/L. The levels of
tetrachloroethene are depicted on Figure 4. Chloroform was detected in MW-5C (1.1
ug/L) and the duplicate of MW-5C (1 ug/L). No other VOCs were detected in
monitoring wells MW-5B, MW-5C, or MW-6. The results are summarized in Table 2,
and a copy of the laboratory report and the Chain-of-Custody form are included in
Appendix I.

The sample results for the drummed purge water (IDW –DRUM) indicated 6.1 µg/L of
tetrachloroethene.

The 2011 concentrations of tetrachloroethene were higher than those detected in 2011;
however, historical concentrations have been higher than the 2011 concentrations.

TABLES
Table 1
Summary of Field Parameters (January 20, 2011)
Former Reeves Property (Brownfields Project No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg Co., North Carolina
S&ME Project No. 1354-11-006
Monitoring Well ID
MW-5B MW-5C MW-6 MW-7
Depth to Water ft below TOC 30.42 30.41 11.91 10.45
TOC Elevation ft above MSL 632.17 632.06 609.54 605.74
BOS Elevation ft above MSL 599.85 571.77 591.04 589.54
Total Depth ft below TOC 32.35 57.00 19.07 16.40
Water Column feet 1.93 26.59 7.16 5.95
Water Level Elevation ft above MSL 601.75 601.65 597.63 595.29
Mid Point-Sampling Interval feet 600.8 575.27 NA NA
Change in Water Level
Elevation feet -0.1 NA NA
Vertical Gradient feet/feet -0.004 NA NA
Notes:
ft : feet
TOC : Top of Casing of the well
MSL : Mean Sea Level
NA - Not Applicable
Parameter Unit
S:\1354\PROJECT\2011\11-001 - 11-050\11-006 Reeves Site Polymers Ctr\11-006 Tables.xls, Field Parameters
Table 2Summary of Water Sampling ResultsFormer Reeves Property (Brownfields Project No. 08022-04-60)8900 Research DriveCharlotte, Mecklenburg Co., North CarolinaS&ME Project No. 1354-11-006Well / Surface Water Sample ID StandardsMW-5B MW-5C MW-6 MW-7 SW-U SW-D 2L05/04/04150 2.7 24 5.4--- ---05/08/0650 1.2 15<0.16 <0.16 <0.1608/09/0742.8 1 38.3<1.0 <1.0 <1.003/11/0892<1.038<1.0 <1.0 <1.001/29/0931.6<1.027.8<1.0 <1.0 <1.002/24/1013.2<1.025.9<1.0 <1.0 <1.001/20/1117.1 1.1 35.9<1.0 <1.0 <1.005/08/06 <0.26 <0.262.7<0.26 <0.26 <0.2608/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.003/11/08 <1.0 <1.0 <1.0 <1.0 <1.0 <1.001/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.002/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.001/20/11 <1.0 <1.0 <1.0 <1.0 <1.0 <1.005/08/0613<0.35 <0.35 <0.35 <0.35 <0.3508/09/075.5<1.0 <1.0 <1.0 <1.0 <1.003/11/086.9<1.0 <1.0 <1.0 <1.0 <1.001/29/092.3<1.0 <1.0 <1.0 <1.0 <1.002/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.001/20/11 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0DateTrichloroethene1,1,1-TrichloroethaneCompound Unitµg/Lµg/Lµg/LTetrachloroethene0.73200
Table 2Summary of Water Sampling ResultsFormer Reeves Property (Brownfields Project No. 08022-04-60)8900 Research DriveCharlotte, Mecklenburg Co., North CarolinaS&ME Project No. 1354-11-006Well / Surface Water Sample ID StandardsMW-5B MW-5C MW-6 MW-7 SW-U SW-D 2LDateCompound Unit05/08/06 <0.33 <0.331.2<0.33 <0.33 <0.3308/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.003/11/08 <1.0 <1.0 <1.0 <1.0 <1.0 <1.001/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.002/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.001/20/11 <1.0 <1.0 <1.0 <1.0 <1.0 <1.005/08/061.4<0.39 <0.39 <0.39 <0.39 <0.3908/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.003/11/081.3<1.0 <1.0 <1.0 <1.0 <1.001/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.002/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.001/20/11 <1.0 <1.0 <1.0 <1.0 <1.0 <1.005/04/04--- 1.1--- --- --- ---05/08/06 <0.291.1<0.29 <0.29 <0.29 <0.2908/09/07 <1.01.1<1.0 <1.0 <1.0 <1.003/11/08 <1.01.0<1.0 <1.0 <1.0 <1.001/29/09 <1.01.0<1.0 <1.0 <1.0 <1.002/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.001/20/11 <1.01.1<1.0 <1.0 <1.0 <1.0Notes:The May 4, 2004 data obtained from the Notice of Brownfields Propertyµg/L : micrograms per liter2L Standard : 15A NCAC 2L .0202 Groundwater Quality StandardHighlighted values exceed 2L Standardscis-1,2-Dichloroethene1,1-Dichloroetheneµg/Lµg/L707Chloroformµg/L70

FIGURES

.

Circles are ~1000 ft, 1500 ft, and 1 mile radii centered near
monitor wells MW-5A, MW-5B and MW-5C
Scale: As Shown
Checked by: MNM
Drawn by: WAQ
Date: 01-31-2011
SITE LOCATION MAP
Reeves Site (BF# 08022-04-60)
8900 Research Drive
Charlotte, North Carolina

Figure

1
S&ME Job No.: 1354-11-006

Source: USGS Topographic Map obtained from http://terraserver-usa.com

1,500 Feet

Scale: As Shown
Checked by: MNM
Drawn by: WAQ
Date: 01-31-2011
SITE AERIAL MAP
Reeves Site (BF# 08022-04-60)
8900 Research Drive
Charlotte, North Carolina

Figure

2
S&ME Job No.: 1354-11-006

Source: Mecklenburg County POLARIS website250 Feet
SITE

APPENDICES

APPENDIX I

Laboratory Report and Chain of Custody
January 24, 2011
LIMS USE: FR - AL QUARLES
LIMS OBJECT ID: 9286151
9286151
Project:
Pace Project No.:
RE:
Mr. Al Quarles
S&ME, Inc.
9751 Southern Pine Blvd.
Charlotte, NC 28273
FORMER
Dear Mr. Quarles:
Enclosed are the analytical results for sample(s) received by the laboratory on January 20, 2011.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brandon Helton for
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9286151
FORMER
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213
Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9286151
FORMER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9286151001 MW-5B EPA 8260 63 PASI-CMCK
9286151002 MW-5C EPA 8260 63 PASI-CMCK
9286151003 DUPLICATE EPA 8260 63 PASI-CMCK
9286151004 MW-6 EPA 8260 63 PASI-CMCK
9286151005 MW-7 EPA 8260 63 PASI-CMCK
9286151006 SW-U EPA 8260 63 PASI-CMCK
9286151007 SW-D EPA 8260 63 PASI-CMCK
9286151008 IDW-DRUM EPA 8260 63 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
HITS ONLY
Pace Project No.:
Project:
9286151
FORMER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
9286151001 MW-5B
Tetrachloroethene 17.1 ug/L 01/21/11 16:331.0EPA 8260
9286151002 MW-5C
Chloroform 1.1 ug/L 01/21/11 16:571.0EPA 8260
Tetrachloroethene 1.1 ug/L 01/21/11 16:571.0EPA 8260
9286151003 DUPLICATE
Chloroform 1.0 ug/L 01/21/11 17:221.0EPA 8260
9286151004 MW-6
Tetrachloroethene 35.9 ug/L 01/21/11 17:461.0EPA 8260
9286151008 IDW-DRUM
Tetrachloroethene 6.1 ug/L 01/21/11 19:231.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PROJECT NARRATIVE
Pace Project No.:
Project:
9286151
FORMER
Method:
Client:S&ME, Inc.
EPA 8260
Date:January 24, 2011
Description:8260 MSV Low Level
General Information:
8 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-5B Lab ID:9286151001 Collected:01/20/11 11:42 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 16:33 67-64-125.0
Benzene ND ug/L 1 01/21/11 16:33 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 16:33 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 16:33 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 16:33 75-27-41.0
Bromoform ND ug/L 1 01/21/11 16:33 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 16:33 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 16:33 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 16:33 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 16:33 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 16:33 75-00-31.0
Chloroform ND ug/L 1 01/21/11 16:33 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 16:33 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 16:33 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 16:33 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 16:33 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 16:33 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 16:33 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 16:33 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 16:33 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 16:33 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 16:33 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 16:33 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 16:33 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 16:33 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 16:33 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 16:33 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 16:33 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 16:33 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 16:33 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 16:33 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 16:33 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 16:33 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 16:33 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 16:33 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 16:33 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 16:33 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 16:33 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 16:33 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 16:33 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 16:33 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 16:33 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 16:33 91-20-31.0
Styrene ND ug/L 1 01/21/11 16:33 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 16:33 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 16:33 79-34-51.0
Tetrachloroethene 17.1 ug/L 1 01/21/11 16:33 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 6 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-5B Lab ID:9286151001 Collected:01/20/11 11:42 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 16:33 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 16:33 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 16:33 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 16:33 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 16:33 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 16:33 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 16:33 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 16:33 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 16:33 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 16:33 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 16:33 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 16:33 95-47-61.0
4-Bromofluorobenzene (S)99 %1 01/21/11 16:33 460-00-470-130
Dibromofluoromethane (S)104 %1 01/21/11 16:33 1868-53-770-130
1,2-Dichloroethane-d4 (S)103 %1 01/21/11 16:33 17060-07-070-130
Toluene-d8 (S)101 %1 01/21/11 16:33 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 7 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-5C Lab ID:9286151002 Collected:01/20/11 11:35 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 16:57 67-64-125.0
Benzene ND ug/L 1 01/21/11 16:57 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 16:57 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 16:57 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 16:57 75-27-41.0
Bromoform ND ug/L 1 01/21/11 16:57 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 16:57 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 16:57 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 16:57 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 16:57 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 16:57 75-00-31.0
Chloroform 1.1 ug/L 1 01/21/11 16:57 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 16:57 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 16:57 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 16:57 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 16:57 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 16:57 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 16:57 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 16:57 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 16:57 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 16:57 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 16:57 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 16:57 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 16:57 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 16:57 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 16:57 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 16:57 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 16:57 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 16:57 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 16:57 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 16:57 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 16:57 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 16:57 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 16:57 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 16:57 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 16:57 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 16:57 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 16:57 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 16:57 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 16:57 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 16:57 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 16:57 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 16:57 91-20-31.0
Styrene ND ug/L 1 01/21/11 16:57 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 16:57 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 16:57 79-34-51.0
Tetrachloroethene 1.1 ug/L 1 01/21/11 16:57 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 8 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-5C Lab ID:9286151002 Collected:01/20/11 11:35 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 16:57 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 16:57 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 16:57 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 16:57 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 16:57 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 16:57 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 16:57 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 16:57 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 16:57 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 16:57 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 16:57 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 16:57 95-47-61.0
4-Bromofluorobenzene (S)98 %1 01/21/11 16:57 460-00-470-130
Dibromofluoromethane (S)103 %1 01/21/11 16:57 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %1 01/21/11 16:57 17060-07-070-130
Toluene-d8 (S)101 %1 01/21/11 16:57 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 9 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:DUPLICATE Lab ID:9286151003 Collected:01/20/11 11:35 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 17:22 67-64-125.0
Benzene ND ug/L 1 01/21/11 17:22 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 17:22 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 17:22 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 17:22 75-27-41.0
Bromoform ND ug/L 1 01/21/11 17:22 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 17:22 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 17:22 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 17:22 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 17:22 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 17:22 75-00-31.0
Chloroform 1.0 ug/L 1 01/21/11 17:22 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 17:22 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 17:22 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 17:22 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 17:22 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 17:22 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 17:22 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 17:22 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 17:22 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 17:22 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 17:22 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 17:22 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 17:22 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 17:22 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 17:22 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 17:22 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 17:22 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 17:22 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 17:22 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 17:22 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 17:22 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 17:22 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 17:22 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 17:22 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 17:22 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 17:22 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 17:22 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 17:22 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 17:22 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 17:22 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 17:22 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 17:22 91-20-31.0
Styrene ND ug/L 1 01/21/11 17:22 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 17:22 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 17:22 79-34-51.0
Tetrachloroethene ND ug/L 1 01/21/11 17:22 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 10 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:DUPLICATE Lab ID:9286151003 Collected:01/20/11 11:35 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 17:22 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 17:22 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 17:22 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 17:22 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 17:22 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 17:22 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 17:22 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 17:22 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 17:22 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 17:22 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 17:22 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 17:22 95-47-61.0
4-Bromofluorobenzene (S)96 %1 01/21/11 17:22 460-00-470-130
Dibromofluoromethane (S)104 %1 01/21/11 17:22 1868-53-770-130
1,2-Dichloroethane-d4 (S)107 %1 01/21/11 17:22 17060-07-070-130
Toluene-d8 (S)100 %1 01/21/11 17:22 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 11 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-6 Lab ID:9286151004 Collected:01/20/11 13:15 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 17:46 67-64-125.0
Benzene ND ug/L 1 01/21/11 17:46 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 17:46 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 17:46 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 17:46 75-27-41.0
Bromoform ND ug/L 1 01/21/11 17:46 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 17:46 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 17:46 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 17:46 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 17:46 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 17:46 75-00-31.0
Chloroform ND ug/L 1 01/21/11 17:46 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 17:46 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 17:46 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 17:46 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 17:46 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 17:46 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 17:46 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 17:46 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 17:46 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 17:46 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 17:46 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 17:46 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 17:46 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 17:46 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 17:46 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 17:46 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 17:46 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 17:46 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 17:46 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 17:46 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 17:46 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 17:46 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 17:46 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 17:46 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 17:46 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 17:46 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 17:46 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 17:46 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 17:46 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 17:46 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 17:46 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 17:46 91-20-31.0
Styrene ND ug/L 1 01/21/11 17:46 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 17:46 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 17:46 79-34-51.0
Tetrachloroethene 35.9 ug/L 1 01/21/11 17:46 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 12 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-6 Lab ID:9286151004 Collected:01/20/11 13:15 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 17:46 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 17:46 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 17:46 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 17:46 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 17:46 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 17:46 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 17:46 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 17:46 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 17:46 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 17:46 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 17:46 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 17:46 95-47-61.0
4-Bromofluorobenzene (S)98 %1 01/21/11 17:46 460-00-470-130
Dibromofluoromethane (S)104 %1 01/21/11 17:46 1868-53-770-130
1,2-Dichloroethane-d4 (S)105 %1 01/21/11 17:46 17060-07-070-130
Toluene-d8 (S)102 %1 01/21/11 17:46 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 13 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-7 Lab ID:9286151005 Collected:01/20/11 13:40 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 18:11 67-64-125.0
Benzene ND ug/L 1 01/21/11 18:11 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 18:11 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 18:11 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 18:11 75-27-41.0
Bromoform ND ug/L 1 01/21/11 18:11 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 18:11 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 18:11 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 18:11 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 18:11 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 18:11 75-00-31.0
Chloroform ND ug/L 1 01/21/11 18:11 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 18:11 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 18:11 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 18:11 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 18:11 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 18:11 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 18:11 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 18:11 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 18:11 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 18:11 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 18:11 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 18:11 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 18:11 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 18:11 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 18:11 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 18:11 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 18:11 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 18:11 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 18:11 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 18:11 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 18:11 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 18:11 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 18:11 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 18:11 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 18:11 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 18:11 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 18:11 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 18:11 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 18:11 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 18:11 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 18:11 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 18:11 91-20-31.0
Styrene ND ug/L 1 01/21/11 18:11 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 18:11 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 18:11 79-34-51.0
Tetrachloroethene ND ug/L 1 01/21/11 18:11 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 14 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:MW-7 Lab ID:9286151005 Collected:01/20/11 13:40 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 18:11 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 18:11 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 18:11 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 18:11 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 18:11 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 18:11 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 18:11 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 18:11 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 18:11 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 18:11 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 18:11 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 18:11 95-47-61.0
4-Bromofluorobenzene (S)97 %1 01/21/11 18:11 460-00-470-130
Dibromofluoromethane (S)103 %1 01/21/11 18:11 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %1 01/21/11 18:11 17060-07-070-130
Toluene-d8 (S)101 %1 01/21/11 18:11 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 15 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:SW-U Lab ID:9286151006 Collected:01/20/11 13:20 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 18:35 67-64-125.0
Benzene ND ug/L 1 01/21/11 18:35 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 18:35 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 18:35 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 18:35 75-27-41.0
Bromoform ND ug/L 1 01/21/11 18:35 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 18:35 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 18:35 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 18:35 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 18:35 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 18:35 75-00-31.0
Chloroform ND ug/L 1 01/21/11 18:35 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 18:35 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 18:35 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 18:35 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 18:35 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 18:35 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 18:35 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 18:35 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 18:35 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 18:35 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 18:35 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 18:35 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 18:35 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 18:35 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 18:35 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 18:35 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 18:35 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 18:35 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 18:35 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 18:35 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 18:35 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 18:35 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 18:35 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 18:35 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 18:35 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 18:35 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 18:35 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 18:35 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 18:35 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 18:35 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 18:35 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 18:35 91-20-31.0
Styrene ND ug/L 1 01/21/11 18:35 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 18:35 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 18:35 79-34-51.0
Tetrachloroethene ND ug/L 1 01/21/11 18:35 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 16 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:SW-U Lab ID:9286151006 Collected:01/20/11 13:20 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 18:35 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 18:35 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 18:35 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 18:35 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 18:35 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 18:35 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 18:35 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 18:35 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 18:35 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 18:35 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 18:35 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 18:35 95-47-61.0
4-Bromofluorobenzene (S)98 %1 01/21/11 18:35 460-00-470-130
Dibromofluoromethane (S)103 %1 01/21/11 18:35 1868-53-770-130
1,2-Dichloroethane-d4 (S)103 %1 01/21/11 18:35 17060-07-070-130
Toluene-d8 (S)101 %1 01/21/11 18:35 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 17 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:SW-D Lab ID:9286151007 Collected:01/20/11 13:50 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 18:59 67-64-125.0
Benzene ND ug/L 1 01/21/11 18:59 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 18:59 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 18:59 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 18:59 75-27-41.0
Bromoform ND ug/L 1 01/21/11 18:59 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 18:59 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 18:59 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 18:59 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 18:59 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 18:59 75-00-31.0
Chloroform ND ug/L 1 01/21/11 18:59 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 18:59 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 18:59 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 18:59 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 18:59 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 18:59 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 18:59 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 18:59 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 18:59 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 18:59 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 18:59 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 18:59 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 18:59 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 18:59 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 18:59 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 18:59 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 18:59 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 18:59 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 18:59 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 18:59 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 18:59 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 18:59 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 18:59 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 18:59 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 18:59 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 18:59 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 18:59 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 18:59 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 18:59 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 18:59 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 18:59 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 18:59 91-20-31.0
Styrene ND ug/L 1 01/21/11 18:59 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 18:59 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 18:59 79-34-51.0
Tetrachloroethene ND ug/L 1 01/21/11 18:59 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 18 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:SW-D Lab ID:9286151007 Collected:01/20/11 13:50 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 18:59 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 18:59 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 18:59 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 18:59 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 18:59 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 18:59 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 18:59 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 18:59 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 18:59 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 18:59 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 18:59 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 18:59 95-47-61.0
4-Bromofluorobenzene (S)96 %1 01/21/11 18:59 460-00-470-130
Dibromofluoromethane (S)99 %1 01/21/11 18:59 1868-53-770-130
1,2-Dichloroethane-d4 (S)104 %1 01/21/11 18:59 17060-07-070-130
Toluene-d8 (S)100 %1 01/21/11 18:59 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 19 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:IDW-DRUM Lab ID:9286151008 Collected:01/20/11 14:00 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 1 01/21/11 19:23 67-64-125.0
Benzene ND ug/L 1 01/21/11 19:23 71-43-21.0
Bromobenzene ND ug/L 1 01/21/11 19:23 108-86-11.0
Bromochloromethane ND ug/L 1 01/21/11 19:23 74-97-51.0
Bromodichloromethane ND ug/L 1 01/21/11 19:23 75-27-41.0
Bromoform ND ug/L 1 01/21/11 19:23 75-25-21.0
Bromomethane ND ug/L 1 01/21/11 19:23 74-83-92.0
2-Butanone (MEK)ND ug/L 1 01/21/11 19:23 78-93-35.0
Carbon tetrachloride ND ug/L 1 01/21/11 19:23 56-23-51.0
Chlorobenzene ND ug/L 1 01/21/11 19:23 108-90-71.0
Chloroethane ND ug/L 1 01/21/11 19:23 75-00-31.0
Chloroform ND ug/L 1 01/21/11 19:23 67-66-31.0
Chloromethane ND ug/L 1 01/21/11 19:23 74-87-31.0
2-Chlorotoluene ND ug/L 1 01/21/11 19:23 95-49-81.0
4-Chlorotoluene ND ug/L 1 01/21/11 19:23 106-43-41.0
1,2-Dibromo-3-chloropropane ND ug/L 1 01/21/11 19:23 96-12-85.0
Dibromochloromethane ND ug/L 1 01/21/11 19:23 124-48-11.0
1,2-Dibromoethane (EDB)ND ug/L 1 01/21/11 19:23 106-93-41.0
Dibromomethane ND ug/L 1 01/21/11 19:23 74-95-31.0
1,2-Dichlorobenzene ND ug/L 1 01/21/11 19:23 95-50-11.0
1,3-Dichlorobenzene ND ug/L 1 01/21/11 19:23 541-73-11.0
1,4-Dichlorobenzene ND ug/L 1 01/21/11 19:23 106-46-71.0
Dichlorodifluoromethane ND ug/L 1 01/21/11 19:23 75-71-81.0
1,1-Dichloroethane ND ug/L 1 01/21/11 19:23 75-34-31.0
1,2-Dichloroethane ND ug/L 1 01/21/11 19:23 107-06-21.0
1,1-Dichloroethene ND ug/L 1 01/21/11 19:23 75-35-41.0
cis-1,2-Dichloroethene ND ug/L 1 01/21/11 19:23 156-59-21.0
trans-1,2-Dichloroethene ND ug/L 1 01/21/11 19:23 156-60-51.0
1,2-Dichloropropane ND ug/L 1 01/21/11 19:23 78-87-51.0
1,3-Dichloropropane ND ug/L 1 01/21/11 19:23 142-28-91.0
2,2-Dichloropropane ND ug/L 1 01/21/11 19:23 594-20-71.0
1,1-Dichloropropene ND ug/L 1 01/21/11 19:23 563-58-61.0
cis-1,3-Dichloropropene ND ug/L 1 01/21/11 19:23 10061-01-51.0
trans-1,3-Dichloropropene ND ug/L 1 01/21/11 19:23 10061-02-61.0
Diisopropyl ether ND ug/L 1 01/21/11 19:23 108-20-31.0
Ethylbenzene ND ug/L 1 01/21/11 19:23 100-41-41.0
Hexachloro-1,3-butadiene ND ug/L 1 01/21/11 19:23 87-68-31.0
2-Hexanone ND ug/L 1 01/21/11 19:23 591-78-65.0
p-Isopropyltoluene ND ug/L 1 01/21/11 19:23 99-87-61.0
Methylene Chloride ND ug/L 1 01/21/11 19:23 75-09-22.0
4-Methyl-2-pentanone (MIBK)ND ug/L 1 01/21/11 19:23 108-10-15.0
Methyl-tert-butyl ether ND ug/L 1 01/21/11 19:23 1634-04-41.0
Naphthalene ND ug/L 1 01/21/11 19:23 91-20-31.0
Styrene ND ug/L 1 01/21/11 19:23 100-42-51.0
1,1,1,2-Tetrachloroethane ND ug/L 1 01/21/11 19:23 630-20-61.0
1,1,2,2-Tetrachloroethane ND ug/L 1 01/21/11 19:23 79-34-51.0
Tetrachloroethene 6.1 ug/L 1 01/21/11 19:23 127-18-41.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 20 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9286151
FORMER
Sample:IDW-DRUM Lab ID:9286151008 Collected:01/20/11 14:00 Received:01/20/11 14:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene ND ug/L 1 01/21/11 19:23 108-88-31.0
1,2,3-Trichlorobenzene ND ug/L 1 01/21/11 19:23 87-61-61.0
1,2,4-Trichlorobenzene ND ug/L 1 01/21/11 19:23 120-82-11.0
1,1,1-Trichloroethane ND ug/L 1 01/21/11 19:23 71-55-61.0
1,1,2-Trichloroethane ND ug/L 1 01/21/11 19:23 79-00-51.0
Trichloroethene ND ug/L 1 01/21/11 19:23 79-01-61.0
Trichlorofluoromethane ND ug/L 1 01/21/11 19:23 75-69-41.0
1,2,3-Trichloropropane ND ug/L 1 01/21/11 19:23 96-18-41.0
Vinyl acetate ND ug/L 1 01/21/11 19:23 108-05-42.0
Vinyl chloride ND ug/L 1 01/21/11 19:23 75-01-41.0
m&p-Xylene ND ug/L 1 01/21/11 19:23 179601-23-12.0
o-Xylene ND ug/L 1 01/21/11 19:23 95-47-61.0
4-Bromofluorobenzene (S)97 %1 01/21/11 19:23 460-00-470-130
Dibromofluoromethane (S)102 %1 01/21/11 19:23 1868-53-770-130
1,2-Dichloroethane-d4 (S)106 %1 01/21/11 19:23 17060-07-070-130
Toluene-d8 (S)101 %1 01/21/11 19:23 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 21 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286151
FORMER
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/13799
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:9286151001, 9286151002, 9286151003, 9286151004, 9286151005, 9286151006, 9286151007, 9286151008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:554008
Associated Lab Samples:9286151001, 9286151002, 9286151003, 9286151004, 9286151005, 9286151006, 9286151007, 9286151008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 01/21/11 11:17
1,1,1-Trichloroethane ug/L ND 1.0 01/21/11 11:17
1,1,2,2-Tetrachloroethane ug/L ND 1.0 01/21/11 11:17
1,1,2-Trichloroethane ug/L ND 1.0 01/21/11 11:17
1,1-Dichloroethane ug/L ND 1.0 01/21/11 11:17
1,1-Dichloroethene ug/L ND 1.0 01/21/11 11:17
1,1-Dichloropropene ug/L ND 1.0 01/21/11 11:17
1,2,3-Trichlorobenzene ug/L ND 1.0 01/21/11 11:17
1,2,3-Trichloropropane ug/L ND 1.0 01/21/11 11:17
1,2,4-Trichlorobenzene ug/L ND 1.0 01/21/11 11:17
1,2-Dibromo-3-chloropropane ug/L ND 5.0 01/21/11 11:17
1,2-Dibromoethane (EDB)ug/L ND 1.0 01/21/11 11:17
1,2-Dichlorobenzene ug/L ND 1.0 01/21/11 11:17
1,2-Dichloroethane ug/L ND 1.0 01/21/11 11:17
1,2-Dichloropropane ug/L ND 1.0 01/21/11 11:17
1,3-Dichlorobenzene ug/L ND 1.0 01/21/11 11:17
1,3-Dichloropropane ug/L ND 1.0 01/21/11 11:17
1,4-Dichlorobenzene ug/L ND 1.0 01/21/11 11:17
2,2-Dichloropropane ug/L ND 1.0 01/21/11 11:17
2-Butanone (MEK)ug/L ND 5.0 01/21/11 11:17
2-Chlorotoluene ug/L ND 1.0 01/21/11 11:17
2-Hexanone ug/L ND 5.0 01/21/11 11:17
4-Chlorotoluene ug/L ND 1.0 01/21/11 11:17
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 01/21/11 11:17
Acetone ug/L ND 25.0 01/21/11 11:17
Benzene ug/L ND 1.0 01/21/11 11:17
Bromobenzene ug/L ND 1.0 01/21/11 11:17
Bromochloromethane ug/L ND 1.0 01/21/11 11:17
Bromodichloromethane ug/L ND 1.0 01/21/11 11:17
Bromoform ug/L ND 1.0 01/21/11 11:17
Bromomethane ug/L ND 2.0 01/21/11 11:17
Carbon tetrachloride ug/L ND 1.0 01/21/11 11:17
Chlorobenzene ug/L ND 1.0 01/21/11 11:17
Chloroethane ug/L ND 1.0 01/21/11 11:17
Chloroform ug/L ND 1.0 01/21/11 11:17
Chloromethane ug/L ND 1.0 01/21/11 11:17
cis-1,2-Dichloroethene ug/L ND 1.0 01/21/11 11:17
cis-1,3-Dichloropropene ug/L ND 1.0 01/21/11 11:17
Dibromochloromethane ug/L ND 1.0 01/21/11 11:17
Dibromomethane ug/L ND 1.0 01/21/11 11:17
Dichlorodifluoromethane ug/L ND 1.0 01/21/11 11:17
Diisopropyl ether ug/L ND 1.0 01/21/11 11:17
Ethylbenzene ug/L ND 1.0 01/21/11 11:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 22 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286151
FORMER
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:554008
Associated Lab Samples:9286151001, 9286151002, 9286151003, 9286151004, 9286151005, 9286151006, 9286151007, 9286151008
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 1.0 01/21/11 11:17
m&p-Xylene ug/L ND 2.0 01/21/11 11:17
Methyl-tert-butyl ether ug/L ND 1.0 01/21/11 11:17
Methylene Chloride ug/L ND 2.0 01/21/11 11:17
Naphthalene ug/L ND 1.0 01/21/11 11:17
o-Xylene ug/L ND 1.0 01/21/11 11:17
p-Isopropyltoluene ug/L ND 1.0 01/21/11 11:17
Styrene ug/L ND 1.0 01/21/11 11:17
Tetrachloroethene ug/L ND 1.0 01/21/11 11:17
Toluene ug/L ND 1.0 01/21/11 11:17
trans-1,2-Dichloroethene ug/L ND 1.0 01/21/11 11:17
trans-1,3-Dichloropropene ug/L ND 1.0 01/21/11 11:17
Trichloroethene ug/L ND 1.0 01/21/11 11:17
Trichlorofluoromethane ug/L ND 1.0 01/21/11 11:17
Vinyl acetate ug/L ND 2.0 01/21/11 11:17
Vinyl chloride ug/L ND 1.0 01/21/11 11:17
1,2-Dichloroethane-d4 (S)%102 70-130 01/21/11 11:17
4-Bromofluorobenzene (S)%98 70-130 01/21/11 11:17
Dibromofluoromethane (S)%101 70-130 01/21/11 11:17
Toluene-d8 (S)%101 70-130 01/21/11 11:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
554009LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.450 105 70-130
1,1,1-Trichloroethane ug/L 52.050 104 70-130
1,1,2,2-Tetrachloroethane ug/L 53.150 106 70-130
1,1,2-Trichloroethane ug/L 50.950 102 70-130
1,1-Dichloroethane ug/L 51.250 102 70-130
1,1-Dichloroethene ug/L 48.950 98 70-132
1,1-Dichloropropene ug/L 49.250 98 70-130
1,2,3-Trichlorobenzene ug/L 52.650 105 70-135
1,2,3-Trichloropropane ug/L 50.950 102 70-130
1,2,4-Trichlorobenzene ug/L 53.150 106 70-134
1,2-Dibromo-3-chloropropane ug/L 54.650 109 70-130
1,2-Dibromoethane (EDB)ug/L 50.750 101 70-130
1,2-Dichlorobenzene ug/L 52.150 104 70-130
1,2-Dichloroethane ug/L 50.550 101 70-130
1,2-Dichloropropane ug/L 50.050 100 70-130
1,3-Dichlorobenzene ug/L 52.250 104 70-130
1,3-Dichloropropane ug/L 51.550 103 70-130
1,4-Dichlorobenzene ug/L 52.150 104 70-130
2,2-Dichloropropane ug/L 51.950 104 58-145
2-Butanone (MEK)ug/L 125100 125 70-145
2-Chlorotoluene ug/L 52.350 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 23 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286151
FORMER
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
554009LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 123100 123 70-144
4-Chlorotoluene ug/L 52.650 105 70-130
4-Methyl-2-pentanone (MIBK)ug/L 110100 110 70-140
Acetone ug/L 139100 139 50-175
Benzene ug/L 50.250 100 70-130
Bromobenzene ug/L 52.250 104 70-130
Bromochloromethane ug/L 51.250 102 70-130
Bromodichloromethane ug/L 50.950 102 70-130
Bromoform ug/L 50.750 101 70-130
Bromomethane ug/L 37.950 76 54-130
Carbon tetrachloride ug/L 54.950 110 70-132
Chlorobenzene ug/L 52.450 105 70-130
Chloroethane ug/L 45.050 90 64-134
Chloroform ug/L 49.750 99 70-130
Chloromethane ug/L 43.150 86 64-130
cis-1,2-Dichloroethene ug/L 49.650 99 70-131
cis-1,3-Dichloropropene ug/L 53.050 106 70-130
Dibromochloromethane ug/L 49.850 100 70-130
Dibromomethane ug/L 51.850 104 70-131
Dichlorodifluoromethane ug/L 36.950 74 56-130
Diisopropyl ether ug/L 50.750 101 70-130
Ethylbenzene ug/L 52.250 104 70-130
Hexachloro-1,3-butadiene ug/L 63.350 127 70-130
m&p-Xylene ug/L 106100 106 70-130
Methyl-tert-butyl ether ug/L 46.650 93 70-130
Methylene Chloride ug/L 45.250 90 63-130
Naphthalene ug/L 50.650 101 70-138
o-Xylene ug/L 52.950 106 70-130
p-Isopropyltoluene ug/L 53.350 107 70-130
Styrene ug/L 53.150 106 70-130
Tetrachloroethene ug/L 52.850 106 70-130
Toluene ug/L 51.250 102 70-130
trans-1,2-Dichloroethene ug/L 50.050 100 70-130
trans-1,3-Dichloropropene ug/L 52.350 105 70-132
Trichloroethene ug/L 51.150 102 70-130
Trichlorofluoromethane ug/L 51.550 103 62-133
Vinyl acetate ug/L 104100 104 66-157
Vinyl chloride ug/L 52.450 105 69-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%102 70-130
Dibromofluoromethane (S)%98 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 24 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9286151
FORMER
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
554010MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9286018002
554011
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 104 70-166110 550ND52.0 54.8
Benzene ug/L 50 104 70-148108 450ND52.0 54.0
Chlorobenzene ug/L 50 102 70-146107 550ND50.8 53.3
Toluene ug/L 50 106 70-155110 450ND53.0 55.1
Trichloroethene ug/L 50 105 69-151112 650ND52.7 55.9
1,2-Dichloroethane-d4 (S)%104 70-130103
4-Bromofluorobenzene (S)%97 70-13096
Dibromofluoromethane (S)%101 70-13099
Toluene-d8 (S)%100 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 25 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9286151
FORMER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 26 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9286151
FORMER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9286151001 MSV/13799MW-5B EPA 8260
9286151002 MSV/13799MW-5C EPA 8260
9286151003 MSV/13799DUPLICATEEPA 8260
9286151004 MSV/13799MW-6 EPA 8260
9286151005 MSV/13799MW-7 EPA 8260
9286151006 MSV/13799SW-U EPA 8260
9286151007 MSV/13799SW-D EPA 8260
9286151008 MSV/13799IDW-DRUM EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 01/24/2011 03:29 PM Page 27 of 27
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]

APPENDIX II

Field Sampling Logs

APPENDIX III

Exhibit B of the Filed Notice of Brownfields Property