08022-Reeves_MonRpt 2014 with LOT and LURU-r

To: Shirley Liggins, Admin. Asst.
Firm: NCDENR, DWM, Brownfields Program
Location: 1646 Mail Service Center
Raleigh, NC 27699-1646
From: Al Quarles
Date: 2/14/14
Project: Reeves Site
Brownfield Agreement # 08022-04-06

WE ARE SENDING YOU: Attached Under a Separate cover via: the Following Items:

Maps Prints Plans Samples Invoice
Copy of Letter Copy of Report Proposal
COPIES DATE DESCRIPTION
1 2/14/14 Annual Monitoring Report for 2014 Sampling
1 Land Use Restrictions (“LUR”) Update

THESE ARE TRANSMITTED AS CHECKED BELOW:
For Your Approval For Review and Comment
For Your Use For Bids Due:
As Requested
Comments: See attached Annual Monitoring Report and Land Use Restrictions Update
For the referenced project.
Copies to: Dennis Hayford, Polymers Center of Excellence; Carolyn Minnich (email)
S&ME Project #:
S&ME Proposal #:
4335-14-018
43-1400047 Signed:

S&ME, Inc.
9751 Southern Pine Boulevard
Charlotte, North Carolina 28273
704.523.4726
Fax: [phone]
Letter of Transmittal
IF ENCLOSURES ARE NOT AS NOTED, PLEASE NOTIFY US AT ONCE.
This Letter of Transmittal and the documents accompanying this Letter of Transmittal contain
information from S&ME, Inc., which is confidential and legally privileged. The information is intended
only for use of the individual or entity named on this Letter of Transmittal. If you are not the intended
recipient, you are hereby notified that any disclosure, copying, distribution or the taking of any action in reliance on these documents is strictly prohibited.
Now with 26
Locations
throughout the
Southeast!
Brownfields Project #: 08022-04-60
Brownfields Property: Reeves Site, 8900 Research Drive
Property Owner (In whole or part): Polymers Center of Excellence, Inc.

LAND USE RESTRICTIONS (“LUR”) UPDATE – JANUARY 2014

Page 1 of 5

LUR 1: No use may be made of the Brownfields Property other than for
commercial and office space.

a. Commercial use is herein defined as an occupation, employment or
enterprise that is carried on for profit by the owner, lessee or licensee.

b. Office use is herein defined as use for the conduct or rendering of
business or professional services.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 2: Surface water and underground water at the Brownfields Property may
not be used for any purpose without the approval of the Department of Environment and
Natural Resources (“DENR”) or its successor in function.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 3: No activities that encounter, expose, remove or use groundwater (for
example, installation of water supply wells, fountains, ponds, lakes or swimming pools,
or construction or excavation activities that encounter or expose groundwater) may occur
on the Brownfields Property without prior sampling and analysis of groundwater to the
satisfaction of DENR or its successor in function in any areas proposed for such
activities, and submittal of the analytical results to DENR or its successor in function. If
such results disclose to DENR or its successor in function contamination in excess of
North Carolina’s groundwater quality standards, the proposed activities may not occur
without the approval of DENR or its successor in function on such conditions as DENR
or its successor in function imposes, including at a minimum compliance with plans and
procedures, approved pursuant to applicable law, to protect public health and the
environment during the proposed activities.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

Brownfields Project #: 08022-04-60
Brownfields Property: Reeves Site, 8900 Research Drive
Property Owner (In whole or part): Polymers Center of Excellence, Inc.

LAND USE RESTRICTIONS (“LUR”) UPDATE – JANUARY 2014

Page 2 of 5

LUR 4: No mining may be conducted on or under the Brownfields Property,
including, without limitation, extraction of coal, oil, gas or any other minerals or non-
mineral substances.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 5: No basements may be constructed on the Brownfields Property unless
they are, as determined by DENR or its successor in function, vented in conformance
with applicable building codes.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 6: None of the contaminants known to be present in the environmental
media at the Brownfields Property, including those listed in paragraph 11 of the
Brownfields Agreement (“Agreement”), may be used or stored at the Brownfields
Property without the prior approval of DENR or its successor in function, except in de
minimis amounts for cleaning and other routine housekeeping activities.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 7: The Brownfields Property may not be used as a park or for sports of
any kind, including, but not limited to, golf, football, soccer and baseball, without the
approval of DENR or its successor in function.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

Brownfields Project #: 08022-04-60
Brownfields Property: Reeves Site, 8900 Research Drive
Property Owner (In whole or part): Polymers Center of Excellence, Inc.

LAND USE RESTRICTIONS (“LUR”) UPDATE – JANUARY 2014

Page 3 of 5

LUR 8: The Brownfields Property may not be used for agriculture, grazing,
timbering or timber production.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 9: The Brownfields Property may not be used as a playground, or for child
care centers or schools.

In compliance __X__ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 10: The Brownfields Property may not be used for kennels, private animal
pens or horse-riding.

In compliance _X___ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

LUR 11: Beginning in January following the year in which the Notice of
Brownfields Property (“Notice”) is recorded, and in every other January unless and until
DENR determines in writing, after a minimum of five (5) sampling events, that
protection of public health and the environment no longer requires such sampling, the
owner(s) of the Brownfields Property shall effect sampling of monitoring wells MW-5B,
Mw-5C, MW-6, and MW-7 and sampling of the adjacent stream in accordance with the
most current version of the Guidelines of the Inactive Hazardous Sites Branch of DENR's
Superfund Section. The groundwater and stream samples collected shall be analyzed by
EPA Method 8260 or by another method approved in advance, in writing, by DENR or
its successor in function.

In compliance __X__ Out of compliance ____

Remarks: _______________________________________________________________
________________________________________________________________________

Brownfields Project #: 08022-04-60
Brownfields Property: Reeves Site, 8900 Research Drive
Property Owner (In whole or part): Polymers Center of Excellence, Inc.

LAND USE RESTRICTIONS (“LUR”) UPDATE – JANUARY 2014

Page 4 of 5

LUR 12: During January of each year after the Notice is recorded, the then
current owner of any part of the Brownfields Property shall submit a notarized Land Use
Restrictions Update to DENR or its successor in function certifying that the Notice
remains recorded at the Mecklenburg County Register of Deeds office, and that the land
use restrictions are being complied with. In years when sampling is required by the
preceding land use restriction, a report setting forth the procedures and results of the
sampling shall accompany the Land Use Restrictions Update.

In compliance __X__ Out of compliance ____

Remarks: Note that the monitor well and surface water sampling (see LUR 11 above)
was performed on January 24, 2014, with the laboratory report received on February 3,
2014.

Notarized signing and submittal of this Land Use Restrictions Update constitutes
certification that the Notice remains recorded at the Mecklenburg County Register of
Deeds office and that the Land Use Restrictions are being complied with.

S&ME, INC. / 9751 Southern Pine Blvd / Charlotte, NC / p 704.523.4726 / f 704.525.3953 / www.smeinc.com

ANNUAL MONITORING REPORT (2014) FORMER REEVES SITE BROWNFIELDS SITE NO. 08022-04-60 8900 RESEARCH DRIVE CHARLOTTE, MECKLENBURG CO, NC S&ME PROJECT 4335-14-018

Prepared for:

Polymers Center of Excellence
8900 Research Drive
Charlotte, North Carolina 28104-6015

Prepared by:

S&ME, Inc.
9711 Southern Pine Boulevard
Charlotte, North Carolina 28273-5560

February 14, 2014

S&ME, INC. / 9751 Southern Pine Blvd / Charlotte, NC / p 704.523.4726 / f 704.525.3953 / www.smeinc.com

February 14, 2014

Polymers Center of Excellence
8900 Research Drive
Charlotte, NC 28104-6015

Attention: Mr. Dennis Hayford

Reference: 2014 Annual Monitoring Report
Reeves Site (Brownfields Site No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg County, North Carolina
S&ME Project No. 4335-14-018

Dear Mr. Hayford:

S&ME, Inc. (S&ME) submits this monitoring report in accordance with S&ME’s
Proposal No. 14-1400047, dated January 15, 2014. The report provides the methods and
results of our surface water and groundwater sampling associated with the referenced
Brownfields project.

1. PROPERTY DESCRIPTION
The site is located at 8900 Research Drive in Charlotte, North Carolina and is listed as
Tax Parcel No. 04714103 by the Mecklenburg County GIS system. The location of the
site is illustrated on Figure 1 (USGS Topographic Map) and Figure 2 (County
Topographic Map). A 2013 aerial of the site and surrounding properties is presented on
Figure 3 (County Aerial Map). We understand that a previous release of
tetrachloroethene at the site has impacted the groundwater. In addition, we understand
that the site is in the North Carolina Department of Environment and Natural Resources
(NCDENR) Brownfields Program (Brownfield Project No. 08022-04-60). S&ME
obtained an electronic copy (AutoCAD®) of the Notice of Brownfields Property, filed on
June 21, 2005, from the surveyor (R.B. Pharr & Associates, P.A.). We understand that
this notice remains recorded at the Mecklenburg County Register of Deeds. A copy of
the “Unofficial Document” version of the Exhibit “B” To The Notice of Brownfields
Property – Survey Plat obtained from the Mecklenburg County Register of Deeds website
is included in Appendix I.
2014 Annual Monitoring Report S&ME Project No. 4335-14-018
Reeves Site, Brownfields Site No. 08022-04-60, Charlotte, NC February 14, 2013

2

S&ME’s services for this project were based on the Annual Sampling Required by Land
Use Restriction letter, dated April 25, 2006 from Ms. Carolyn Minnich, NCDENR
Brownfield Project Manager, requesting the sampling of surface water and groundwater
in accordance with the Notice of Brownfields Property. The April 25, 2006 letter
indicated that four monitoring wells (MW-5B, MW-5C, MW-6, and MW-7) and the
adjacent stream are to be sampled annually and analyzed for volatile organic compounds
(VOCs) by Environmental Protection Agency (EPA) Method 8260 or equivalent. The
locations of the monitor wells and stream sample locations are illustrated on Figure 4 and
Figure 5.
2. SCOPE OF SERVICES
2.1 Surface Water and Groundwater Sampling
On January 24, 2014, S&ME collected one upstream surface water sample (SW-U) and
one downstream (SW-D) surface water sample at the approximate locations shown on
Figure 4. The surface water samples were collected by dipping the sample containers
directly into the stream pointing upstream with care not to allow sediment to enter the
sample containers and not to allow overfilling to prevent the loss of any preservatives, if
present. Sample containers with appropriate preservatives were provided by the
laboratory.

On January 24, 2014, S&ME also collected groundwater samples from the following
monitor wells: MW-5B, MW-5C, MW-6, and MW-7. Prior to sampling, the depth to
water in each well was measured from the top of the well casing (TOC) and the monitor
wells were purged of three to five well volumes (or until dry) using a disposable bailer.
The samples were submitted to Pace Analytical Laboratories, Inc. (Pace) in Huntersville,
North Carolina, a North Carolina-certified laboratory, for the analysis of VOCs by EPA
Method 8260. In addition to the four monitor well samples, one duplicate sample of
MW-6 (identified as DUP-1) was additionally analyzed for quality control purposes.
Copies of the field sampling forms are included in Appendix II.

The purge water was contained in a secured and labeled 55-gallon drum that was stored
on-site awaiting removal for off-site disposal. The drum of purge water will be disposed
off-site by Haz~Mat Environmental in February 2014. S&ME will provide a copy of the
waste manifest to the NCDENR, if requested by the NCDENR.

3. RESULTS
3.1 Groundwater Flow
The depth to water in the surficial aquifer ranged from 6.40 feet below the top of casing
in monitor well MW-7 (a flush-mounted well), to 28.41 feet below the top of casing in
the monitor well MW-5C. The January 24, 2014 groundwater levels were approximately
2014 Annual Monitoring Report S&ME Project No. 4335-14-018
Reeves Site, Brownfields Site No. 08022-04-60, Charlotte, NC February 14, 2013

3
3.2 feet higher than the January 11, 2013 groundwater levels. Based on the top of casing
elevations and the depth to water (Table 1), the groundwater flow is generally toward the
east-southeast in the general direction of Doby Creek under a hydraulic gradient of
approximately 0.038 ft/ft between monitoring wells MW-5B and MW-6, and
approximately 0.0024 ft/ft between monitoring wells MW-6 and MW-7 (Figure 4). The
vertical hydraulic gradient at nested monitoring wells MW-5B and MW-5C is
approximately 0.009 ft/ft (Table 1).
3.2 Surface Water Quality
VOCs were not detected above laboratory reporting limits in the two surface water
samples (SW-U and SW-D). The results are summarized in Table 2, and a copy of the
laboratory report is included in Appendix III.
3.3 Groundwater Quality
No VOCs were detected above laboratory reporting limits in the groundwater samples
from the downgradient monitor well MW-7. Tetrachloroethene was detected in
monitoring wells MW-5B and MW-6 [5.2 and 14.0 micrograms per liter (µg/L),
respectively] compared to the 15A NCAC 2L .0202 groundwater quality standard (2L
Standard) of 0.7 µg/L. Tetrachloroethene was also detected in the deeper monitor well
MW-5C [1.4 µg/L]. Chloroform was detected in MW-5C [1.0 µg/L] compared to the 2L
Standard of 70 µg/L. The results are summarized in Table 2, and illustrated on Figure 5.
A copy of the laboratory report and Chain-of-Custody form are included in Appendix I.

The 2014 concentration of tetrachloroethene was approximately 28% lower than the 2013
concentration in monitor well MW-6. The 2014 concentration of tetrachloroethene was
approximately 68% lower than the 2012 concentration in monitor well MW-5 (not
sampled in 2013).

Both sample MW-6 and its duplicate resulted in concentrations above the laboratory
reporting limits for tetrachloroethene, with a relative percent difference of approximately
7%. No VOCs were detected in the trip blank. All of the laboratory internal quality
controls were within acceptable limits.

A sample from the drummed purge water indicated a concentration of 3.1 µg/L of
tetrachloroethene.

TABLES
Table 1
Summary of Field Parameters (January 24, 2014)
Former Reeves Property (Brownfields Project No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg Co., North Carolina
S&ME Project No. 4335-14-018
Monitoring Well ID
MW-5B MW-5C MW-6 MW-7
Depth to Water ft below TOC 28.29 28.41 9.50 6.40
TOC Elevation ft above MSL 632.17 632.06 609.54 605.74
BOS Elevation ft above MSL 599.85 571.77 591.04 589.54
Total Depth (measured)ft below TOC 31.55 59.95 19.00 16.40
Water Column feet 3.26 31.54 9.50 10.00
Water Level Elevation ft above MSL 603.88 603.65 600.04 599.34
Mid Point-Sampling Interval feet 601.87 575.27 NA NA
Change in Water Level
Elevation feet -0.23 NA NA
Vertical Gradient feet/feet -0.009 NA NA
Temperature °C 12.39 11.08 12.73 12.3
pH Standard Units 6.1 5.7 6.0 5.4
Conductivity µS/cm 0.238 0.313 0.279 0.256
Notes:
ft : feet
TOC : Top of Casing of the well
MSL : Mean Sea Level
°C : Degrees Celcius
µS/cm: micro siemens per centimeter
NA - Not Applicable
Parameter Unit
S:\2430\PROJECT\2014\001 - 050\4335-14-018 Reeves Brownfield Sampling\14-018 Tables.xls, Field Parameters
Table 2
Summary of Water Sampling Results
Former Reeves Property (Brownfields Project No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg Co., North Carolina
S&ME Project No. 4335-14-018
Well / Surface Water Sample ID 2L
MW-5B DUPLICATE MW-5C MW-6 MW-7 SW-U SW-D Standard
05/04/04 150 150 2.7 24 5.4 ------
05/08/06 50 71 1.2 15 <0.16 <0.16 <0.16
08/09/07 42.8 38.9 1 38.3 <1.0 <1.0 <1.0
03/11/08 92 <1.0 (7)<1.0 38 <1.0 <1.0 <1.0
01/29/09 31.6 31.9 <1.0 27.8 <1.0 <1.0 <1.0
02/24/10 13.2 11.9 <1.0 25.9 <1.0 <1.0 <1.0
01/20/11 17.1 <1.0 (5C)1.1 35.9 <1.0 <1.0 <1.0
01/06/12 16.1 14.6 <1.0 21.1 <1.0 <1.0 <1.0
01/11/13 NS <1.0 (5C)<1.0 19.3 <1.0 <1.0 <1.0
01/24/14 5.2 13.1 (6)1.4 14.0 <1.0 <1.0 <1.0
05/08/06 <0.26 <0.26 <0.26 2.7 <0.26 <0.26 <0.26
08/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 <1.0 <1.0 (7)<1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/11/13 NS <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/24/14 <1.0 <1.0 (6)<1.0 <1.0 <1.0 <1.0 <1.0
05/08/06 13 17 <0.35 <0.35 <0.35 <0.35 <0.35
08/09/07 5.5 4.9 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 6.9 <1.0 (7)<1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 2.3 2.3 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/11/13 NS <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/24/14 <1.0 <1.0 (6)<1.0 <1.0 <1.0 <1.0 <1.0
05/08/06 <0.33 <0.33 <0.33 1.2 <0.33 <0.33 <0.33
08/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 <1.0 <1.0 (7)<1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/11/13 NS <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/24/14 <1.0 <1.0 (6)<1.0 <1.0 <1.0 <1.0 <1.0
0.7
Trichloro-
ethene µg/L
cis-1,2-
Dichloro-
ethene
Tetrachloro-
ethene
µg/L
DateCompoundUnit
1,1,1-Trichloro-
ethane µg/L
µg/L
3
200
70
1,1-Dichloro-
ethene µg/L 7
Page 1 of 2
Table 2
Summary of Water Sampling Results
Former Reeves Property (Brownfields Project No. 08022-04-60)
8900 Research Drive
Charlotte, Mecklenburg Co., North Carolina
S&ME Project No. 4335-14-018
Well / Surface Water Sample ID 2L
MW-5B DUPLICATE MW-5C MW-6 MW-7 SW-U SW-D Standard
0.7Tetrachloro-
ethene
DateCompoundUnit
µg/L
05/08/06 1.4 1.9 <0.39 <0.39 <0.39 <0.39 <0.39
08/09/07 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
03/11/08 1.3 <1.0 (7)<1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/11/13 NS <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/24/14 <1.0 <1.0 (6)<1.0 <1.0 <1.0 <1.0 <1.0
05/04/04 ------1.1 ------------
05/08/06 <0.29 <0.29 1.1 <0.29 <0.29 <0.29 <0.29
08/09/07 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0
03/11/08 <1.0 <1.0 (7)1.0 <1.0 <1.0 <1.0 <1.0
01/29/09 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 <1.0
02/24/10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/20/11 <1.0 1.0 (5C)1.1 <1.0 <1.0 <1.0 <1.0
01/06/12 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0
01/11/13 NS <1.0 (5C)<1.0 <1.0 <1.0 <1.0 <1.0
01/24/14 <1.0 <1.0 (6)1.0 <1.0 <1.0 <1.0 <1.0
Notes:
The May 4, 2004 data obtained from the Notice of Brownfields Property
Sample ID "Duplicate" is a duplicate of MW-5B, unless noted otherwise with the well # in parentheses (7) = (MW-7)
µg/L : micrograms per liter
2L Standard : 15A NCAC 2L .0202 Groundwater Quality Standard
NS : Not Sampled, insufficient water in well
Underlined values exceed 2L Standards
Chloroform µg/L 70
1,1-Dichloro-
ethene µg/L 7
Page 2 of 2

FIGURES

.

Circles are ~1000 ft, 1500 ft, and 1 mile radii centered near
monitor wells MW-5A, MW-5B and MW-5C

Scale: As Shown
hown
Checked by: WAQ
Drawn by: CSM
Date: 01-14-2014
USGS TOPOGRAPHIC MAP
Reeves Site
8900 Research Drive
Charlotte, North Carolina

Figure

1
S&ME Job No.: 4335-14-018

Source: USGS Topographic Map obtained from http://terraserver-usa.com

NCDENR Brownfield Site No. 08022-04-60
1,500 Feet

Scale: As Shown
hown
Checked by: WAQ
Drawn by: CSM
Date: 02-12-2014
COUNTY TOPOGRAPHIC MAP
Reeves Site
8900 Research Drive
Charlotte, North Carolina

Figure

2
S&ME Job No.: 4335-14-018

Source: Mecklenburg County POLARIS3G website

NCDENR Brownfield Site No. 08022-04-60
SITE
200 Feet

Area of MW-5
Monitor Wells

Scale: As Shown
hown
Checked by: WAQ
Drawn by: CSM
Date: 02-12-2014
COUNTY AERIAL MAP
Reeves Site
8900 Research Drive
Charlotte, North Carolina

Figure

3
S&ME Job No.: 4335-14-018

Source: Mecklenburg County POLARIS3G website

NCDENR Brownfield Site No. 08022-04-60
SITE
200 Feet

Area of MW-5
Monitor Wells
$4+&)''%/'+2'+20+40+40+45614;%10%4'6'$7+.&+0)ž&7-'219'449&$Ä Ä&1$;%4''-FUND II AND FUND II-OWDB: 5758-409TAX NO: 047-141-10E.D.S. REALTY CORPORATIONDB: 5383-865TAX NO: 047-141-150+40+4(NOW OR FORMERLY)(NOW OR FORMERLY)0+40+4'+2603.88600.04599.34603.65NMNMNM600
603
601
602
LEGENDMONITOR WELL LOCATIONSURFACE WATER SAMPLE LOCATIONGROUNDWATER ELEVATION (FT) ONJANUARY 24, 2014GROUNDWATER SURFACE CONTOURNOT MEASURED603.88NM
$4+&)''%/'+2'+20+40+40+45614;%10%4'6'$7+.&+0)ž&7-'219'449&$Ä Ä&1$;%4''-FUND II AND FUND II-OWDB: 5758-409TAX NO: 047-141-10E.D.S. REALTY CORPORATIONDB: 5383-865TAX NO: 047-141-150+40+4(NOW OR FORMERLY)(NOW OR FORMERLY)0+40+4'+25.214.0<1.0<1.01.4<1.0NSNSNSLEGENDMONITOR WELL LOCATIONSURFACE WATER SAMPLE LOCATION7(75$&+/252(7+(1(/(9(/—J/ON JANUARY 24, 2014NOT SAMPLED14.0NS

APPENDICES

APPENDIX I
EXHIBIT B OF THE FILED NOTICE OF BROWNFIELDS PROPERTY

APPENDIX II
FIELD SAMPLING LOGS

APPENDIX III
LABORATORY REPORT AND CHAIN OF CUSTODY
#=CL#
February 03, 2014
LIMS USE: FR - AL QUARLES
LIMS OBJECT ID: 92187715
92187715
Project:
Pace Project No.:
RE:
Mr. Al Quarles
S&ME, Inc.
9751 Southern Pine Blvd.
Charlotte, NC 28273
REEVES BROWNFIELD 4335-14-01B
Dear Mr. Quarles:
Enclosed are the analytical results for sample(s) received by the laboratory on January 27, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Roger Smith, S&ME, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 35
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92187715001 MW-5B EPA 8260 63 PASI-CMCK
92187715002 MW-5C EPA 8260 63 PASI-CMCK
92187715003 MW-6 EPA 8260 63 PASI-CMCK
92187715004 MW-7 EPA 8260 63 PASI-CMCK
92187715005 SW-D EPA 8260 63 PASI-CMCK
92187715006 SW-U EPA 8260 63 PASI-CMCK
92187715007 DUP-1 EPA 8260 63 PASI-CMCK
92187715008 DRUM EPA 8260 63 PASI-CMCK
92187715009 TRIP BLANK EPA 8260 63 PASI-CMCK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 35
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92187715001 MW-5B
Tetrachloroethene 5.2 ug/L 01/29/14 13:341.0EPA 8260
92187715002 MW-5C
Chloroform 1.0 ug/L 01/29/14 13:501.0EPA 8260
Tetrachloroethene 1.4 ug/L 01/29/14 13:501.0EPA 8260
92187715003 MW-6
Tetrachloroethene 14.0 ug/L 01/29/14 14:061.0EPA 8260
92187715005 SW-D
Chloromethane <1.0 ug/L 01/29/14 14:371.0EPA 8260
92187715007 DUP-1
Tetrachloroethene 13.1 ug/L 01/29/14 15:091.0EPA 8260
92187715008 DRUM
Chloroform <1.0 ug/L 01/31/14 04:391.0EPA 8260
Tetrachloroethene 3.1 ug/L 01/31/14 04:391.0EPA 8260
92187715009 TRIP BLANK
Chloromethane <1.0 ug/L 01/29/14 11:591.0EPA 8260
Methylene Chloride <2.0 ug/L 01/29/14 11:592.0EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 35
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Method:
Client:S&ME, Inc.
EPA 8260
Date:February 03, 2014
Description:8260 MSV Low Level
General Information:
9 samples were analyzed for EPA 8260. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: MSV/25658
S0: Surrogate recovery outside laboratory control limits.
• BLANK (Lab ID: 1130522)
• 1,2-Dichloroethane-d4 (S)
• 4-Bromofluorobenzene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: MSV/25633
L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
• LCS (Lab ID: 1129508)
• Vinyl acetate
QC Batch: MSV/25658
L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
• LCS (Lab ID: 1130523)
• Vinyl acetate
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 35
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Method:
Client:S&ME, Inc.
EPA 8260
Date:February 03, 2014
Description:8260 MSV Low Level
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-5B Lab ID:92187715001 Collected:01/24/14 11:30 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 13:34 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 13:34 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 13:34 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 13:34 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 13:34 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 13:34 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 13:34 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 13:34 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 13:34 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 13:34 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 13:34 75-00-31.0 1
Chloroform <1.0 ug/L 01/29/14 13:34 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 13:34 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 13:34 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 13:34 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 13:34 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 13:34 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 13:34 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 13:34 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 13:34 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 13:34 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 13:34 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 13:34 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 13:34 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 13:34 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 13:34 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 13:34 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 13:34 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 13:34 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 13:34 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 13:34 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 13:34 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 13:34 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 13:34 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 13:34 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 13:34 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 13:34 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 13:34 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 13:34 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 13:34 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 13:34 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 13:34 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 13:34 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 13:34 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 13:34 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 13:34 79-34-51.0 1
Tetrachloroethene 5.2 ug/L 01/29/14 13:34 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-5B Lab ID:92187715001 Collected:01/24/14 11:30 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 13:34 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 13:34 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 13:34 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 13:34 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 13:34 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 13:34 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 13:34 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 13:34 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 13:34 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 13:34 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 13:34 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 13:34 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 13:34 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)97 %01/29/14 13:34 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %01/29/14 13:34 17060-07-070-130 1
Toluene-d8 (S)97 %01/29/14 13:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-5C Lab ID:92187715002 Collected:01/24/14 11:05 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 13:50 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 13:50 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 13:50 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 13:50 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 13:50 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 13:50 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 13:50 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 13:50 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 13:50 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 13:50 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 13:50 75-00-31.0 1
Chloroform 1.0 ug/L 01/29/14 13:50 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 13:50 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 13:50 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 13:50 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 13:50 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 13:50 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 13:50 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 13:50 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 13:50 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 13:50 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 13:50 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 13:50 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 13:50 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 13:50 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 13:50 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 13:50 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 13:50 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 13:50 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 13:50 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 13:50 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 13:50 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 13:50 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 13:50 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 13:50 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 13:50 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 13:50 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 13:50 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 13:50 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 13:50 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 13:50 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 13:50 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 13:50 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 13:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 13:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 13:50 79-34-51.0 1
Tetrachloroethene 1.4 ug/L 01/29/14 13:50 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-5C Lab ID:92187715002 Collected:01/24/14 11:05 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 13:50 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 13:50 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 13:50 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 13:50 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 13:50 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 13:50 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 13:50 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 13:50 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 13:50 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 13:50 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 13:50 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 13:50 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 13:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %01/29/14 13:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %01/29/14 13:50 17060-07-070-130 1
Toluene-d8 (S)97 %01/29/14 13:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-6 Lab ID:92187715003 Collected:01/24/14 12:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 14:06 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 14:06 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 14:06 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 14:06 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 14:06 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 14:06 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 14:06 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 14:06 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 14:06 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 14:06 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 14:06 75-00-31.0 1
Chloroform <1.0 ug/L 01/29/14 14:06 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 14:06 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 14:06 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 14:06 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 14:06 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 14:06 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 14:06 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 14:06 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 14:06 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 14:06 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 14:06 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 14:06 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 14:06 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 14:06 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 14:06 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:06 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:06 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 14:06 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 14:06 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 14:06 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 14:06 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:06 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:06 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 14:06 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 14:06 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 14:06 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 14:06 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 14:06 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 14:06 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 14:06 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 14:06 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 14:06 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 14:06 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:06 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:06 79-34-51.0 1
Tetrachloroethene 14.0 ug/L 01/29/14 14:06 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 11 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-6 Lab ID:92187715003 Collected:01/24/14 12:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 14:06 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 14:06 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 14:06 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 14:06 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 14:06 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 14:06 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 14:06 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 14:06 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 14:06 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 14:06 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 14:06 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 14:06 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 14:06 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %01/29/14 14:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %01/29/14 14:06 17060-07-070-130 1
Toluene-d8 (S)95 %01/29/14 14:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 12 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-7 Lab ID:92187715004 Collected:01/24/14 12:40 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 14:21 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 14:21 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 14:21 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 14:21 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 14:21 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 14:21 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 14:21 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 14:21 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 14:21 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 14:21 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 14:21 75-00-31.0 1
Chloroform <1.0 ug/L 01/29/14 14:21 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 14:21 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 14:21 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 14:21 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 14:21 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 14:21 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 14:21 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 14:21 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 14:21 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 14:21 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 14:21 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 14:21 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 14:21 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 14:21 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 14:21 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:21 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:21 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 14:21 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 14:21 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 14:21 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 14:21 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:21 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:21 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 14:21 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 14:21 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 14:21 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 14:21 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 14:21 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 14:21 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 14:21 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 14:21 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 14:21 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 14:21 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:21 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:21 79-34-51.0 1
Tetrachloroethene <1.0 ug/L 01/29/14 14:21 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 13 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:MW-7 Lab ID:92187715004 Collected:01/24/14 12:40 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 14:21 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 14:21 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 14:21 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 14:21 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 14:21 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 14:21 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 14:21 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 14:21 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 14:21 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 14:21 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 14:21 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 14:21 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 14:21 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/29/14 14:21 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %01/29/14 14:21 17060-07-070-130 1
Toluene-d8 (S)96 %01/29/14 14:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 14 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:SW-D Lab ID:92187715005 Collected:01/24/14 13:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 14:37 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 14:37 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 14:37 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 14:37 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 14:37 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 14:37 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 14:37 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 14:37 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 14:37 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 14:37 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 14:37 75-00-31.0 1
Chloroform <1.0 ug/L 01/29/14 14:37 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 14:37 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 14:37 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 14:37 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 14:37 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 14:37 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 14:37 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 14:37 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 14:37 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 14:37 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 14:37 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 14:37 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 14:37 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 14:37 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 14:37 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:37 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:37 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 14:37 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 14:37 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 14:37 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 14:37 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:37 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:37 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 14:37 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 14:37 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 14:37 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 14:37 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 14:37 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 14:37 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 14:37 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 14:37 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 14:37 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 14:37 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:37 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:37 79-34-51.0 1
Tetrachloroethene <1.0 ug/L 01/29/14 14:37 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 15 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:SW-D Lab ID:92187715005 Collected:01/24/14 13:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 14:37 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 14:37 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 14:37 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 14:37 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 14:37 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 14:37 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 14:37 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 14:37 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 14:37 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 14:37 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 14:37 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 14:37 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 14:37 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/29/14 14:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %01/29/14 14:37 17060-07-070-130 1
Toluene-d8 (S)97 %01/29/14 14:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 16 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:SW-U Lab ID:92187715006 Collected:01/24/14 13:20 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 14:53 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 14:53 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 14:53 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 14:53 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 14:53 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 14:53 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 14:53 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 14:53 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 14:53 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 14:53 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 14:53 75-00-31.0 1
Chloroform <1.0 ug/L 01/29/14 14:53 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 14:53 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 14:53 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 14:53 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 14:53 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 14:53 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 14:53 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 14:53 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 14:53 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 14:53 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 14:53 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 14:53 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 14:53 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 14:53 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 14:53 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:53 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 14:53 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 14:53 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 14:53 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 14:53 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 14:53 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:53 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 14:53 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 14:53 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 14:53 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 14:53 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 14:53 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 14:53 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 14:53 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 14:53 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 14:53 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 14:53 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 14:53 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:53 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 14:53 79-34-51.0 1
Tetrachloroethene <1.0 ug/L 01/29/14 14:53 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
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Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 17 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:SW-U Lab ID:92187715006 Collected:01/24/14 13:20 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 14:53 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 14:53 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 14:53 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 14:53 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 14:53 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 14:53 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 14:53 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 14:53 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 14:53 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 14:53 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 14:53 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 14:53 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 14:53 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %01/29/14 14:53 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %01/29/14 14:53 17060-07-070-130 1
Toluene-d8 (S)96 %01/29/14 14:53 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 18 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:DUP-1 Lab ID:92187715007 Collected:01/24/14 12:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 15:09 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 15:09 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 15:09 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 15:09 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 15:09 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 15:09 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 15:09 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 15:09 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 15:09 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 15:09 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 15:09 75-00-31.0 1
Chloroform <1.0 ug/L 01/29/14 15:09 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 15:09 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 15:09 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 15:09 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 15:09 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 15:09 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 15:09 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 15:09 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 15:09 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 15:09 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 15:09 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 15:09 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 15:09 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 15:09 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 15:09 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 15:09 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 15:09 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 15:09 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 15:09 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 15:09 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 15:09 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 15:09 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 15:09 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 15:09 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 15:09 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 15:09 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 15:09 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 15:09 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 15:09 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 15:09 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 15:09 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 15:09 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 15:09 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 15:09 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 15:09 79-34-51.0 1
Tetrachloroethene 13.1 ug/L 01/29/14 15:09 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 19 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:DUP-1 Lab ID:92187715007 Collected:01/24/14 12:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 15:09 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 15:09 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 15:09 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 15:09 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 15:09 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 15:09 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 15:09 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 15:09 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 15:09 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 15:09 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 15:09 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 15:09 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 15:09 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %01/29/14 15:09 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %01/29/14 15:09 17060-07-070-130 1
Toluene-d8 (S)99 %01/29/14 15:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 20 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:DRUM Lab ID:92187715008 Collected:01/24/14 14:50 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/31/14 04:39 67-64-125.0 1
Benzene <1.0 ug/L 01/31/14 04:39 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/31/14 04:39 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/31/14 04:39 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/31/14 04:39 75-27-41.0 1
Bromoform <1.0 ug/L 01/31/14 04:39 75-25-21.0 1
Bromomethane <2.0 ug/L 01/31/14 04:39 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/31/14 04:39 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/31/14 04:39 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/31/14 04:39 108-90-71.0 1
Chloroethane <1.0 ug/L 01/31/14 04:39 75-00-31.0 1
Chloroform <1.0 ug/L 01/31/14 04:39 67-66-31.0 1
Chloromethane <1.0 ug/L 01/31/14 04:39 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/31/14 04:39 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/31/14 04:39 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/31/14 04:39 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/31/14 04:39 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/31/14 04:39 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/31/14 04:39 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/31/14 04:39 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/31/14 04:39 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/31/14 04:39 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/31/14 04:39 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/31/14 04:39 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/31/14 04:39 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/31/14 04:39 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/31/14 04:39 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/31/14 04:39 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/31/14 04:39 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/31/14 04:39 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/31/14 04:39 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/31/14 04:39 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/31/14 04:39 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/31/14 04:39 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/31/14 04:39 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/31/14 04:39 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/31/14 04:39 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/31/14 04:39 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/31/14 04:39 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/31/14 04:39 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/31/14 04:39 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/31/14 04:39 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/31/14 04:39 91-20-31.0 1
Styrene <1.0 ug/L 01/31/14 04:39 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/31/14 04:39 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/31/14 04:39 79-34-51.0 1
Tetrachloroethene 3.1 ug/L 01/31/14 04:39 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 21 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:DRUM Lab ID:92187715008 Collected:01/24/14 14:50 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/31/14 04:39 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/31/14 04:39 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/31/14 04:39 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/31/14 04:39 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/31/14 04:39 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/31/14 04:39 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/31/14 04:39 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/31/14 04:39 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/31/14 04:39 108-05-4 L32.0 1
Vinyl chloride <1.0 ug/L 01/31/14 04:39 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/31/14 04:39 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/31/14 04:39 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/31/14 04:39 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %01/31/14 04:39 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %01/31/14 04:39 17060-07-070-130 1
Toluene-d8 (S)100 %01/31/14 04:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 22 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:TRIP BLANK Lab ID:92187715009 Collected:01/24/14 00:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Acetone <25.0 ug/L 01/29/14 11:59 67-64-125.0 1
Benzene <1.0 ug/L 01/29/14 11:59 71-43-21.0 1
Bromobenzene <1.0 ug/L 01/29/14 11:59 108-86-11.0 1
Bromochloromethane <1.0 ug/L 01/29/14 11:59 74-97-51.0 1
Bromodichloromethane <1.0 ug/L 01/29/14 11:59 75-27-41.0 1
Bromoform <1.0 ug/L 01/29/14 11:59 75-25-21.0 1
Bromomethane <2.0 ug/L 01/29/14 11:59 74-83-92.0 1
2-Butanone (MEK)<5.0 ug/L 01/29/14 11:59 78-93-35.0 1
Carbon tetrachloride <1.0 ug/L 01/29/14 11:59 56-23-51.0 1
Chlorobenzene <1.0 ug/L 01/29/14 11:59 108-90-71.0 1
Chloroethane <1.0 ug/L 01/29/14 11:59 75-00-31.0 1
Chloroform <1.0 ug/L 01/29/14 11:59 67-66-31.0 1
Chloromethane <1.0 ug/L 01/29/14 11:59 74-87-31.0 1
2-Chlorotoluene <1.0 ug/L 01/29/14 11:59 95-49-81.0 1
4-Chlorotoluene <1.0 ug/L 01/29/14 11:59 106-43-41.0 1
1,2-Dibromo-3-chloropropane <5.0 ug/L 01/29/14 11:59 96-12-85.0 1
Dibromochloromethane <1.0 ug/L 01/29/14 11:59 124-48-11.0 1
1,2-Dibromoethane (EDB)<1.0 ug/L 01/29/14 11:59 106-93-41.0 1
Dibromomethane <1.0 ug/L 01/29/14 11:59 74-95-31.0 1
1,2-Dichlorobenzene <1.0 ug/L 01/29/14 11:59 95-50-11.0 1
1,3-Dichlorobenzene <1.0 ug/L 01/29/14 11:59 541-73-11.0 1
1,4-Dichlorobenzene <1.0 ug/L 01/29/14 11:59 106-46-71.0 1
Dichlorodifluoromethane <1.0 ug/L 01/29/14 11:59 75-71-81.0 1
1,1-Dichloroethane <1.0 ug/L 01/29/14 11:59 75-34-31.0 1
1,2-Dichloroethane <1.0 ug/L 01/29/14 11:59 107-06-21.0 1
1,1-Dichloroethene <1.0 ug/L 01/29/14 11:59 75-35-41.0 1
cis-1,2-Dichloroethene <1.0 ug/L 01/29/14 11:59 156-59-21.0 1
trans-1,2-Dichloroethene <1.0 ug/L 01/29/14 11:59 156-60-51.0 1
1,2-Dichloropropane <1.0 ug/L 01/29/14 11:59 78-87-51.0 1
1,3-Dichloropropane <1.0 ug/L 01/29/14 11:59 142-28-91.0 1
2,2-Dichloropropane <1.0 ug/L 01/29/14 11:59 594-20-71.0 1
1,1-Dichloropropene <1.0 ug/L 01/29/14 11:59 563-58-61.0 1
cis-1,3-Dichloropropene <1.0 ug/L 01/29/14 11:59 10061-01-51.0 1
trans-1,3-Dichloropropene <1.0 ug/L 01/29/14 11:59 10061-02-61.0 1
Diisopropyl ether <1.0 ug/L 01/29/14 11:59 108-20-31.0 1
Ethylbenzene <1.0 ug/L 01/29/14 11:59 100-41-41.0 1
Hexachloro-1,3-butadiene <1.0 ug/L 01/29/14 11:59 87-68-31.0 1
2-Hexanone <5.0 ug/L 01/29/14 11:59 591-78-65.0 1
p-Isopropyltoluene <1.0 ug/L 01/29/14 11:59 99-87-61.0 1
Methylene Chloride <2.0 ug/L 01/29/14 11:59 75-09-22.0 1
4-Methyl-2-pentanone (MIBK)<5.0 ug/L 01/29/14 11:59 108-10-15.0 1
Methyl-tert-butyl ether <1.0 ug/L 01/29/14 11:59 1634-04-41.0 1
Naphthalene <1.0 ug/L 01/29/14 11:59 91-20-31.0 1
Styrene <1.0 ug/L 01/29/14 11:59 100-42-51.0 1
1,1,1,2-Tetrachloroethane <1.0 ug/L 01/29/14 11:59 630-20-61.0 1
1,1,2,2-Tetrachloroethane <1.0 ug/L 01/29/14 11:59 79-34-51.0 1
Tetrachloroethene <1.0 ug/L 01/29/14 11:59 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 23 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Sample:TRIP BLANK Lab ID:92187715009 Collected:01/24/14 00:00 Received:01/27/14 13:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260 MSV Low Level Analytical Method: EPA 8260
Toluene <1.0 ug/L 01/29/14 11:59 108-88-31.0 1
1,2,3-Trichlorobenzene <1.0 ug/L 01/29/14 11:59 87-61-61.0 1
1,2,4-Trichlorobenzene <1.0 ug/L 01/29/14 11:59 120-82-11.0 1
1,1,1-Trichloroethane <1.0 ug/L 01/29/14 11:59 71-55-61.0 1
1,1,2-Trichloroethane <1.0 ug/L 01/29/14 11:59 79-00-51.0 1
Trichloroethene <1.0 ug/L 01/29/14 11:59 79-01-61.0 1
Trichlorofluoromethane <1.0 ug/L 01/29/14 11:59 75-69-41.0 1
1,2,3-Trichloropropane <1.0 ug/L 01/29/14 11:59 96-18-41.0 1
Vinyl acetate <2.0 ug/L 01/29/14 11:59 108-05-42.0 1
Vinyl chloride <1.0 ug/L 01/29/14 11:59 75-01-41.0 1
Xylene (Total)<2.0 ug/L 01/29/14 11:59 1330-20-72.0 1
m&p-Xylene <2.0 ug/L 01/29/14 11:59 179601-23-12.0 1
o-Xylene <1.0 ug/L 01/29/14 11:59 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %01/29/14 11:59 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %01/29/14 11:59 17060-07-070-130 1
Toluene-d8 (S)96 %01/29/14 11:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 24 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25633
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92187715001, 92187715002, 92187715003, 92187715004, 92187715005, 92187715006, 92187715007,
92187715009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1129507
Associated Lab Samples:92187715001, 92187715002, 92187715003, 92187715004, 92187715005, 92187715006, 92187715007,
92187715009
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L <1.0 1.0 01/29/14 11:43
1,1,1-Trichloroethane ug/L <1.0 1.0 01/29/14 11:43
1,1,2,2-Tetrachloroethane ug/L <1.0 1.0 01/29/14 11:43
1,1,2-Trichloroethane ug/L <1.0 1.0 01/29/14 11:43
1,1-Dichloroethane ug/L <1.0 1.0 01/29/14 11:43
1,1-Dichloroethene ug/L <1.0 1.0 01/29/14 11:43
1,1-Dichloropropene ug/L <1.0 1.0 01/29/14 11:43
1,2,3-Trichlorobenzene ug/L <1.0 1.0 01/29/14 11:43
1,2,3-Trichloropropane ug/L <1.0 1.0 01/29/14 11:43
1,2,4-Trichlorobenzene ug/L <1.0 1.0 01/29/14 11:43
1,2-Dibromo-3-chloropropane ug/L <5.0 5.0 01/29/14 11:43
1,2-Dibromoethane (EDB)ug/L <1.0 1.0 01/29/14 11:43
1,2-Dichlorobenzene ug/L <1.0 1.0 01/29/14 11:43
1,2-Dichloroethane ug/L <1.0 1.0 01/29/14 11:43
1,2-Dichloropropane ug/L <1.0 1.0 01/29/14 11:43
1,3-Dichlorobenzene ug/L <1.0 1.0 01/29/14 11:43
1,3-Dichloropropane ug/L <1.0 1.0 01/29/14 11:43
1,4-Dichlorobenzene ug/L <1.0 1.0 01/29/14 11:43
2,2-Dichloropropane ug/L <1.0 1.0 01/29/14 11:43
2-Butanone (MEK)ug/L <5.0 5.0 01/29/14 11:43
2-Chlorotoluene ug/L <1.0 1.0 01/29/14 11:43
2-Hexanone ug/L <5.0 5.0 01/29/14 11:43
4-Chlorotoluene ug/L <1.0 1.0 01/29/14 11:43
4-Methyl-2-pentanone (MIBK)ug/L <5.0 5.0 01/29/14 11:43
Acetone ug/L <25.0 25.0 01/29/14 11:43
Benzene ug/L <1.0 1.0 01/29/14 11:43
Bromobenzene ug/L <1.0 1.0 01/29/14 11:43
Bromochloromethane ug/L <1.0 1.0 01/29/14 11:43
Bromodichloromethane ug/L <1.0 1.0 01/29/14 11:43
Bromoform ug/L <1.0 1.0 01/29/14 11:43
Bromomethane ug/L <2.0 2.0 01/29/14 11:43
Carbon tetrachloride ug/L <1.0 1.0 01/29/14 11:43
Chlorobenzene ug/L <1.0 1.0 01/29/14 11:43
Chloroethane ug/L <1.0 1.0 01/29/14 11:43
Chloroform ug/L <1.0 1.0 01/29/14 11:43
Chloromethane ug/L <1.0 1.0 01/29/14 11:43
cis-1,2-Dichloroethene ug/L <1.0 1.0 01/29/14 11:43
cis-1,3-Dichloropropene ug/L <1.0 1.0 01/29/14 11:43
Dibromochloromethane ug/L <1.0 1.0 01/29/14 11:43
Dibromomethane ug/L <1.0 1.0 01/29/14 11:43
Dichlorodifluoromethane ug/L <1.0 1.0 01/29/14 11:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 25 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1129507
Associated Lab Samples:92187715001, 92187715002, 92187715003, 92187715004, 92187715005, 92187715006, 92187715007,
92187715009
Matrix:Water
Analyzed
Diisopropyl ether ug/L <1.0 1.0 01/29/14 11:43
Ethylbenzene ug/L <1.0 1.0 01/29/14 11:43
Hexachloro-1,3-butadiene ug/L <1.0 1.0 01/29/14 11:43
m&p-Xylene ug/L <2.0 2.0 01/29/14 11:43
Methyl-tert-butyl ether ug/L <1.0 1.0 01/29/14 11:43
Methylene Chloride ug/L <2.0 2.0 01/29/14 11:43
Naphthalene ug/L <1.0 1.0 01/29/14 11:43
o-Xylene ug/L <1.0 1.0 01/29/14 11:43
p-Isopropyltoluene ug/L <1.0 1.0 01/29/14 11:43
Styrene ug/L <1.0 1.0 01/29/14 11:43
Tetrachloroethene ug/L <1.0 1.0 01/29/14 11:43
Toluene ug/L <1.0 1.0 01/29/14 11:43
trans-1,2-Dichloroethene ug/L <1.0 1.0 01/29/14 11:43
trans-1,3-Dichloropropene ug/L <1.0 1.0 01/29/14 11:43
Trichloroethene ug/L <1.0 1.0 01/29/14 11:43
Trichlorofluoromethane ug/L <1.0 1.0 01/29/14 11:43
Vinyl acetate ug/L <2.0 2.0 01/29/14 11:43
Vinyl chloride ug/L <1.0 1.0 01/29/14 11:43
Xylene (Total)ug/L <2.0 2.0 01/29/14 11:43
1,2-Dichloroethane-d4 (S)%96 70-130 01/29/14 11:43
4-Bromofluorobenzene (S)%99 70-130 01/29/14 11:43
Toluene-d8 (S)%97 70-130 01/29/14 11:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1129508LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.450 101 70-130
1,1,1-Trichloroethane ug/L 47.550 95 70-130
1,1,2,2-Tetrachloroethane ug/L 51.450 103 70-130
1,1,2-Trichloroethane ug/L 49.650 99 70-130
1,1-Dichloroethane ug/L 46.650 93 70-130
1,1-Dichloroethene ug/L 47.550 95 70-132
1,1-Dichloropropene ug/L 49.250 98 70-130
1,2,3-Trichlorobenzene ug/L 52.850 106 70-135
1,2,3-Trichloropropane ug/L 50.850 102 70-130
1,2,4-Trichlorobenzene ug/L 51.050 102 70-134
1,2-Dibromo-3-chloropropane ug/L 52.150 104 70-130
1,2-Dibromoethane (EDB)ug/L 51.250 102 70-130
1,2-Dichlorobenzene ug/L 52.150 104 70-130
1,2-Dichloroethane ug/L 47.350 95 70-130
1,2-Dichloropropane ug/L 49.550 99 70-130
1,3-Dichlorobenzene ug/L 49.050 98 70-130
1,3-Dichloropropane ug/L 49.650 99 70-130
1,4-Dichlorobenzene ug/L 50.550 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 26 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1129508LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 50.050 100 58-145
2-Butanone (MEK)ug/L 93.0100 93 70-145
2-Chlorotoluene ug/L 48.050 96 70-130
2-Hexanone ug/L 96.4100 96 70-144
4-Chlorotoluene ug/L 50.950 102 70-130
4-Methyl-2-pentanone (MIBK)ug/L 97.6100 98 70-140
Acetone ug/L 90.4100 90 50-175
Benzene ug/L 49.750 99 70-130
Bromobenzene ug/L 50.550 101 70-130
Bromochloromethane ug/L 46.550 93 70-130
Bromodichloromethane ug/L 50.350 101 70-130
Bromoform ug/L 52.350 105 70-130
Bromomethane ug/L 48.150 96 54-130
Carbon tetrachloride ug/L 48.950 98 70-132
Chlorobenzene ug/L 48.850 98 70-130
Chloroethane ug/L 34.750 69 64-134
Chloroform ug/L 47.250 94 70-130
Chloromethane ug/L 43.850 88 64-130
cis-1,2-Dichloroethene ug/L 45.450 91 70-131
cis-1,3-Dichloropropene ug/L 49.950 100 70-130
Dibromochloromethane ug/L 51.050 102 70-130
Dibromomethane ug/L 50.450 101 70-131
Dichlorodifluoromethane ug/L 44.750 89 56-130
Diisopropyl ether ug/L 48.050 96 70-130
Ethylbenzene ug/L 47.850 96 70-130
Hexachloro-1,3-butadiene ug/L 54.350 109 70-130
m&p-Xylene ug/L 98.9100 99 70-130
Methyl-tert-butyl ether ug/L 49.450 99 70-130
Methylene Chloride ug/L 44.250 88 63-130
Naphthalene ug/L 51.350 103 70-138
o-Xylene ug/L 48.650 97 70-130
p-Isopropyltoluene ug/L 52.850 106 70-130
Styrene ug/L 50.350 101 70-130
Tetrachloroethene ug/L 50.250 100 70-130
Toluene ug/L 48.650 97 70-130
trans-1,2-Dichloroethene ug/L 44.950 90 70-130
trans-1,3-Dichloropropene ug/L 50.950 102 70-132
Trichloroethene ug/L 49.050 98 70-130
Trichlorofluoromethane ug/L 44.150 88 62-133
Vinyl acetate ug/L 190 F3,L310019066-157
Vinyl chloride ug/L 46.650 93 69-130
Xylene (Total)ug/L 148150 98 70-130
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 27 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1129509MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92187923001
1129510
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1-Dichloroethene ug/L 50 83 70-16682 150ND41.6 41.0
Benzene ug/L 50 105 70-148103 150ND52.4 51.7
Chlorobenzene ug/L 50 108 70-146107 150ND54.0 53.5
Toluene ug/L 50 102 70-155101 150ND51.2 50.7
Trichloroethene ug/L 50 108 69-151104 450ND54.1 52.1
1,2-Dichloroethane-d4 (S)%107 70-130108
4-Bromofluorobenzene (S)%95 70-13095
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 28 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/25658
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples:92187715008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1130522
Associated Lab Samples:92187715008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L <1.0 1.0 01/31/14 02:19
1,1,1-Trichloroethane ug/L <1.0 1.0 01/31/14 02:19
1,1,2,2-Tetrachloroethane ug/L <1.0 1.0 01/31/14 02:19
1,1,2-Trichloroethane ug/L <1.0 1.0 01/31/14 02:19
1,1-Dichloroethane ug/L <1.0 1.0 01/31/14 02:19
1,1-Dichloroethene ug/L <1.0 1.0 01/31/14 02:19
1,1-Dichloropropene ug/L <1.0 1.0 01/31/14 02:19
1,2,3-Trichlorobenzene ug/L 6.8 1.0 01/31/14 02:19
1,2,3-Trichloropropane ug/L <1.0 1.0 01/31/14 02:19
1,2,4-Trichlorobenzene ug/L 5.5 1.0 01/31/14 02:19
1,2-Dibromo-3-chloropropane ug/L <5.0 5.0 01/31/14 02:19
1,2-Dibromoethane (EDB)ug/L <1.0 1.0 01/31/14 02:19
1,2-Dichlorobenzene ug/L <1.0 1.0 01/31/14 02:19
1,2-Dichloroethane ug/L <1.0 1.0 01/31/14 02:19
1,2-Dichloropropane ug/L <1.0 1.0 01/31/14 02:19
1,3-Dichlorobenzene ug/L <1.0 1.0 01/31/14 02:19
1,3-Dichloropropane ug/L <1.0 1.0 01/31/14 02:19
1,4-Dichlorobenzene ug/L <1.0 1.0 01/31/14 02:19
2,2-Dichloropropane ug/L <1.0 1.0 01/31/14 02:19
2-Butanone (MEK)ug/L <5.0 5.0 01/31/14 02:19
2-Chlorotoluene ug/L <1.0 1.0 01/31/14 02:19
2-Hexanone ug/L <5.0 5.0 01/31/14 02:19
4-Chlorotoluene ug/L <1.0 1.0 01/31/14 02:19
4-Methyl-2-pentanone (MIBK)ug/L <5.0 5.0 01/31/14 02:19
Acetone ug/L <25.0 25.0 01/31/14 02:19
Benzene ug/L <1.0 1.0 01/31/14 02:19
Bromobenzene ug/L <1.0 1.0 01/31/14 02:19
Bromochloromethane ug/L <1.0 1.0 01/31/14 02:19
Bromodichloromethane ug/L <1.0 1.0 01/31/14 02:19
Bromoform ug/L <1.0 1.0 01/31/14 02:19
Bromomethane ug/L <2.0 2.0 01/31/14 02:19
Carbon tetrachloride ug/L <1.0 1.0 01/31/14 02:19
Chlorobenzene ug/L <1.0 1.0 01/31/14 02:19
Chloroethane ug/L <1.0 1.0 01/31/14 02:19
Chloroform ug/L <1.0 1.0 01/31/14 02:19
Chloromethane ug/L <1.0 1.0 01/31/14 02:19
cis-1,2-Dichloroethene ug/L <1.0 1.0 01/31/14 02:19
cis-1,3-Dichloropropene ug/L <1.0 1.0 01/31/14 02:19
Dibromochloromethane ug/L <1.0 1.0 01/31/14 02:19
Dibromomethane ug/L <1.0 1.0 01/31/14 02:19
Dichlorodifluoromethane ug/L <1.0 1.0 01/31/14 02:19
Diisopropyl ether ug/L <1.0 1.0 01/31/14 02:19
Ethylbenzene ug/L <1.0 1.0 01/31/14 02:19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 29 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1130522
Associated Lab Samples:92187715008
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L <1.0 1.0 01/31/14 02:19
m&p-Xylene ug/L <2.0 2.0 01/31/14 02:19
Methyl-tert-butyl ether ug/L <1.0 1.0 01/31/14 02:19
Methylene Chloride ug/L <2.0 2.0 01/31/14 02:19
Naphthalene ug/L 5.3 1.0 01/31/14 02:19
o-Xylene ug/L <1.0 1.0 01/31/14 02:19
p-Isopropyltoluene ug/L <1.0 1.0 01/31/14 02:19
Styrene ug/L <1.0 1.0 01/31/14 02:19
Tetrachloroethene ug/L <1.0 1.0 01/31/14 02:19
Toluene ug/L <1.0 1.0 01/31/14 02:19
trans-1,2-Dichloroethene ug/L <1.0 1.0 01/31/14 02:19
trans-1,3-Dichloropropene ug/L <1.0 1.0 01/31/14 02:19
Trichloroethene ug/L <1.0 1.0 01/31/14 02:19
Trichlorofluoromethane ug/L <1.0 1.0 01/31/14 02:19
Vinyl acetate ug/L <2.0 2.0 01/31/14 02:19
Vinyl chloride ug/L <1.0 1.0 01/31/14 02:19
Xylene (Total)ug/L <2.0 2.0 01/31/14 02:19
1,2-Dichloroethane-d4 (S)%44 70-130 S001/31/14 02:19
4-Bromofluorobenzene (S)%37 70-130 S001/31/14 02:19
Toluene-d8 (S)%95 70-130 01/31/14 02:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1130523LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.850 100 70-130
1,1,1-Trichloroethane ug/L 51.850 104 70-130
1,1,2,2-Tetrachloroethane ug/L 49.550 99 70-130
1,1,2-Trichloroethane ug/L 50.650 101 70-130
1,1-Dichloroethane ug/L 51.950 104 70-130
1,1-Dichloroethene ug/L 54.950 110 70-132
1,1-Dichloropropene ug/L 52.950 106 70-130
1,2,3-Trichlorobenzene ug/L 43.350 87 70-135
1,2,3-Trichloropropane ug/L 49.450 99 70-130
1,2,4-Trichlorobenzene ug/L 44.650 89 70-134
1,2-Dibromo-3-chloropropane ug/L 49.750 99 70-130
1,2-Dibromoethane (EDB)ug/L 50.150 100 70-130
1,2-Dichlorobenzene ug/L 49.350 99 70-130
1,2-Dichloroethane ug/L 52.550 105 70-130
1,2-Dichloropropane ug/L 51.350 103 70-130
1,3-Dichlorobenzene ug/L 47.950 96 70-130
1,3-Dichloropropane ug/L 51.350 103 70-130
1,4-Dichlorobenzene ug/L 49.850 100 70-130
2,2-Dichloropropane ug/L 45.450 91 58-145
2-Butanone (MEK)ug/L 102100 102 70-145
2-Chlorotoluene ug/L 49.450 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 30 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1130523LABORATORY CONTROL SAMPLE:
LCSSpike
2-Hexanone ug/L 104100 104 70-144
4-Chlorotoluene ug/L 51.550 103 70-130
4-Methyl-2-pentanone (MIBK)ug/L 106100 106 70-140
Acetone ug/L 106100 106 50-175
Benzene ug/L 51.750 103 70-130
Bromobenzene ug/L 51.650 103 70-130
Bromochloromethane ug/L 50.250 100 70-130
Bromodichloromethane ug/L 48.150 96 70-130
Bromoform ug/L 48.350 97 70-130
Bromomethane ug/L 50.850 102 54-130
Carbon tetrachloride ug/L 50.150 100 70-132
Chlorobenzene ug/L 49.550 99 70-130
Chloroethane ug/L 49.550 99 64-134
Chloroform ug/L 50.650 101 70-130
Chloromethane ug/L 52.750 105 64-130
cis-1,2-Dichloroethene ug/L 50.750 101 70-131
cis-1,3-Dichloropropene ug/L 49.150 98 70-130
Dibromochloromethane ug/L 48.850 98 70-130
Dibromomethane ug/L 46.850 94 70-131
Dichlorodifluoromethane ug/L 50.050 100 56-130
Diisopropyl ether ug/L 56.450 113 70-130
Ethylbenzene ug/L 49.250 98 70-130
Hexachloro-1,3-butadiene ug/L 46.050 92 70-130
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 53.750 107 70-130
Methylene Chloride ug/L 57.550 115 63-130
Naphthalene ug/L 44.550 89 70-138
o-Xylene ug/L 50.450 101 70-130
p-Isopropyltoluene ug/L 50.150 100 70-130
Styrene ug/L 50.850 102 70-130
Tetrachloroethene ug/L 48.550 97 70-130
Toluene ug/L 49.050 98 70-130
trans-1,2-Dichloroethene ug/L 51.950 104 70-130
trans-1,3-Dichloropropene ug/L 49.850 100 70-132
Trichloroethene ug/L 48.150 96 70-130
Trichlorofluoromethane ug/L 50.650 101 62-133
Vinyl acetate ug/L 175 L010017566-157
Vinyl chloride ug/L 52.650 105 69-130
Xylene (Total)ug/L 152150 101 70-130
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 31 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 32 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92187715
REEVES BROWNFIELD 4335-14-01B
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92187715001 MSV/25633MW-5B EPA 8260
92187715002 MSV/25633MW-5C EPA 8260
92187715003 MSV/25633MW-6 EPA 8260
92187715004 MSV/25633MW-7 EPA 8260
92187715005 MSV/25633SW-D EPA 8260
92187715006 MSV/25633SW-U EPA 8260
92187715007 MSV/25633DUP-1 EPA 8260
92187715008 MSV/25658DRUMEPA 8260
92187715009 MSV/25633TRIP BLANK EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/03/2014 02:40 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 33 of 35
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