20056_Retreat at Renaissance_Final Grade Sampling Report_2018.11.16

Aptus Management, PLLC
Aptus Management, PLLC 109 Amber Court Carrboro, NC 27510
Sent Via Email: [e-mail]
Environmental Management Solutions
November 16, 2018
Joselyn Harriger Brownfields Program NC Department of Environmental Quality
SUBJECT: FINAL AT-GRADE SOIL SAMPLING REPORT RETREAT AT RENAISSANCE
BROWNFIELDS PROJECT # 200056-16-92
Dear Ms. Harriger:
Provided below is the summary of the surficial soil testing conducted at the Stanley Martin Homes
Brownfields Property in Wake Forest. As indicated, we found no contamination by VOCs, SVOCs or RCRA metals which would pose an unacceptable risk, or which were measured above the IHSB Residential Health Based Preliminary Soil Remediation Goals (PSRGs)1.
BACKGROUND INFORMATION
The Notice of Brownfields Property for the Retreat at Renaissance Brownfields was recorded on October 5, 2017. The approximately 11-acre site is in Wake Forest. Construction of 85 townhouse units is currently underway. The primary concern at the property is subsurface groundwater contamination. A small area of petroleum-impacted soil and sediment was cleaned up prior to the start of site development in August 2017. Otherwise, there were no known soil impacts at the site.
The intent of this assessment was to evaluate final at-grade surficial soil conditions and demonstrate that no unacceptable risks exist at the Retreat at Renaissance townhouse development site.
SAMPLING
On June 5, 2018, we collected six (6) surficial soil samples, S-1 through S-6, and one duplicate at location S-3 as shown in the attached figure of the townhouse development site. Soil samples were collected with a hand auger at 0.5 to 2.0 feet below the land surface.
All samples were collected using a field-decontaminated hand auger. The SVOC and metals samples were collected from the auger bucket and placed directly into laboratory-provided glassware. Samples for VOC analysis were collected directly from the hand-auger bucket using a laboratory-provided discrete VOC sampling device. There were no visual or olfactory observations indicating possible contamination.
Samples were packed on ice and shipped under chain-of-custody to Prism Laboratories in
Charlotte, NC for analyses.
1 Naturally occurring background levels of arsenic were measured above the residential PSRG.
Soil Testing Report November 16, 2018
Retreat at Renaissance
Aptus Management, PLLC Page 2
RESULTS
As summarized in Table 1, acetone, a common lab anomaly, was measured at low levels in four
of the seven samples, and a low concentration of benzoic acid was reported in four samples, but in each case at a fraction of their respective PSRGs. Two other SVOCs, 1-methylnaphthalene and 2-methylnaphthalene, were reported in our duplicate sample only, but
well below their PSRGs. No other SVOCs were found. Except for arsenic, all metals were below their respective IHSB PSRGs. Arsenic was measured in all soil samples above its residential PSRG (0.68 mg/kg) at concentrations ranging from 1.5 mg/kg to 2.5 mg/kg, which
is within expected background naturally occurring levels.
Many of the detections were below the Laboratory Reporting Limit; therefore, results were estimated concentrations (CLP J-Flag).
In summary, we found no contamination by VOCs or SVOCs above residential PSRGs. Similarly, except for arsenic at naturally occurring levels, no RCRA metals were measured above residential PSRGs.
Provided as attachments are the laboratory report and data summary in Excel format along with this report.
If you have questions, please feel free to contact me at [phone].
Sincerely, APTUS MANAGEMENT, PLLC
John Gallagher, PE Engineer of Record
Aptus Management, PLLC
SOIL SAMPLING LOCATIONS
Figure – Sampling Plan Source: Withers & Ravenal Grading Plan Scale: As Shown
Retreat at Renaissance 398 South Franklin Street Wake Forest, North Carolina NCBF No. 20056-16-92
LEGEND:
S-1 Proposed Soil Sample Location
2 Building Number
S-1
S-3
S-2
S-5
S-6
S-4
Aptus Management, PLLC
Soil Test Summary Table
S-1 S-2 S-3 S-4 S-5 S-6 Dupe
VOCs (mg/Kg)
Acetone 12,000 140,000 0.099 0.068 BRL 0.068 BRL BRL 0.063
SVOCs (mg/Kg)----
Benzoic Acid 51,000 660,000 0.25 J 0.80 0.14 J 0.24 J BRL BRL BRL
1-Methylnaphthalene 18 73 BRL BRL BRL BRL BRL BRL 0.24 J
2-Methylnaphthalene 48 600 BRL BRL BRL BRL BRL BRL 0.44
RCRA Metals, Total (mg/Kg)
Arsenic 0.68 3.0 1.5 J 2.4 2.3 1.6 J 2.5 2.0 2.5
Barium 3,000 44,000 69 77 72 120 95 81 59
Cadmium 14 200 0.033 J 0.057 J 0.053 J BRL BRL 0.024 J 0.054 J
Chromium 23,000 350,000 19 17 16 32 24 22 13
Lead 400 800 22 18 20 18 16 17 16
Selenium 78 1,200 0.84 J 1.6 1.8 2.1 1.8 1.3 1.4
Silver 78 1,200 0.040 J 0.12 J 0.052 J BRL BRL 0.023 J 0.039 J
Mercury 1.9 3.1 0.024 0.028 0.034 0.030 0.031 0.026 0.030
NOTES:
* Preliminary Soil Remediation Goals (PSRG) per Inactive Hazardous Sites Branch
J - Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL - Below Laboratory Reporting Limit. See Laboratory Report
Bolded and Shaded concentrations exceed one or more IHSB PSRG health-based soil remediation goals
IHSB PSRG -
Residential *
(mg/kg)
IHSB PSRG -
Industrial*
(mg/kg)
Table 1Soil Sample Analytical ResultsRetreat at Renaissance
Raleigh, North Carolina
Constituent
Sample ID

Aptus Management, PLLC
Prism Lab Report
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
06/18/2018
Proctor Environmental Services, Inc.
Tom Proctor
5113 Yachtsman Ct.
Raleigh, NC 27615
Project: Retreat @ Renaissance
Lab Submittal Date: 06/07/2018
Prism Work Order: 8060117
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
DATA SUBJECT TO CHANGE
Reviewed ByDRAFT REPORT DRAFT REPORT
VP Laboratory Services
Data Qualifiers Key Reference:
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
M Matrix spike outside of the control limits.
MC Sample concentration too high for recovery evaluation.
Method Detection LimitMDL
Not Detected at the MDLU
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 53
Sample Receipt Summary
06/18/2018
Prism Work Order: 8060117
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
8060117-01 06/05/18S-1 @77 06/07/18Solid
8060117-02 06/05/18S-2 @11 06/07/18Solid
8060117-03 06/05/18S-6 @27 06/07/18Solid
8060117-04 06/05/18S-4 @36 06/07/18Solid
8060117-05 06/05/18S-5 06/07/18Solid
8060117-06 06/05/18S-3@52 06/07/18Solid
8060117-07 06/05/18DUPE 06/07/18Solid
Samples were received in good condition at 3.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 53
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8060117
06/18/2018
Summary of Detections
0.25 J mg/kg dry8060117-01 S-1 @77 Benzoic Acid 8270D
0.024 mg/kg dry8060117-01 S-1 @77 Mercury 7471B
1.5 J mg/kg dry8060117-01 S-1 @77 Arsenic 6020B
69 mg/kg dry8060117-01 S-1 @77 Barium 6020B
0.033 J mg/kg dry8060117-01 S-1 @77 Cadmium 6020B
19 mg/kg dry8060117-01 S-1 @77 Chromium 6020B
22 mg/kg dry8060117-01 S-1 @77 Lead 6020B
0.84 J mg/kg dry8060117-01 S-1 @77 Selenium 6020B
0.040 J mg/kg dry8060117-01 S-1 @77 Silver 6020B
0.099 mg/kg dry8060117-01 S-1 @77 Acetone 8260B
0.80 mg/kg dry8060117-02 S-2 @11 Benzoic Acid 8270D
0.028 mg/kg dry8060117-02 S-2 @11 Mercury 7471B
2.4 mg/kg dry8060117-02 S-2 @11 Arsenic 6020B
77 mg/kg dry8060117-02 S-2 @11 Barium 6020B
0.057 J mg/kg dry8060117-02 S-2 @11 Cadmium 6020B
17 mg/kg dry8060117-02 S-2 @11 Chromium 6020B
18 mg/kg dry8060117-02 S-2 @11 Lead 6020B
1.6 mg/kg dry8060117-02 S-2 @11 Selenium 6020B
0.12 J mg/kg dry8060117-02 S-2 @11 Silver 6020B
0.068 mg/kg dry8060117-02 S-2 @11 Acetone 8260B
0.026 mg/kg dry8060117-03 S-6 @27 Mercury 7471B
2.0 mg/kg dry8060117-03 S-6 @27 Arsenic 6020B
81 mg/kg dry8060117-03 S-6 @27 Barium 6020B
0.024 J mg/kg dry8060117-03 S-6 @27 Cadmium 6020B
22 mg/kg dry8060117-03 S-6 @27 Chromium 6020B
17 mg/kg dry8060117-03 S-6 @27 Lead 6020B
1.3 mg/kg dry8060117-03 S-6 @27 Selenium 6020B
0.023 J mg/kg dry8060117-03 S-6 @27 Silver 6020B
0.24 J mg/kg dry8060117-04 S-4 @36 Benzoic Acid 8270D
0.030 mg/kg dry8060117-04 S-4 @36 Mercury 7471B
1.6 J mg/kg dry8060117-04 S-4 @36 Arsenic 6020B
120 mg/kg dry8060117-04 S-4 @36 Barium 6020B
32 mg/kg dry8060117-04 S-4 @36 Chromium 6020B
18 mg/kg dry8060117-04 S-4 @36 Lead 6020B
2.1 mg/kg dry8060117-04 S-4 @36 Selenium 6020B
0.068 mg/kg dry8060117-04 S-4 @36 Acetone 8260B
0.031 mg/kg dry8060117-05 S-5 Mercury 7471B
2.5 mg/kg dry8060117-05 S-5 Arsenic 6020B
95 mg/kg dry8060117-05 S-5 Barium 6020B
24 mg/kg dry8060117-05 S-5 Chromium 6020B
16 mg/kg dry8060117-05 S-5 Lead 6020B
1.8 mg/kg dry8060117-05 S-5 Selenium 6020B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 53
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8060117
06/18/2018
Summary of Detections
0.14 J mg/kg dry8060117-06 S-3@52 Benzoic Acid 8270D
0.034 mg/kg dry8060117-06 S-3@52 Mercury 7471B
2.3 mg/kg dry8060117-06 S-3@52 Arsenic 6020B
72 mg/kg dry8060117-06 S-3@52 Barium 6020B
0.053 J mg/kg dry8060117-06 S-3@52 Cadmium 6020B
16 mg/kg dry8060117-06 S-3@52 Chromium 6020B
20 mg/kg dry8060117-06 S-3@52 Lead 6020B
1.8 mg/kg dry8060117-06 S-3@52 Selenium 6020B
0.052 J mg/kg dry8060117-06 S-3@52 Silver 6020B
0.24 J mg/kg dry8060117-07 DUPE 1-Methylnaphthalene 8270D
0.44 mg/kg dry8060117-07 DUPE 2-Methylnaphthalene 8270D
0.030 mg/kg dry8060117-07 DUPE Mercury 7471B
2.5 mg/kg dry8060117-07 DUPE Arsenic 6020B
59 mg/kg dry8060117-07 DUPE Barium 6020B
0.054 J mg/kg dry8060117-07 DUPE Cadmium 6020B
13 mg/kg dry8060117-07 DUPE Chromium 6020B
16 mg/kg dry8060117-07 DUPE Lead 6020B
1.4 mg/kg dry8060117-07 DUPE Selenium 6020B
0.039 J mg/kg dry8060117-07 DUPE Silver 6020B
0.063 mg/kg dry8060117-07 DUPE Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-01
Prism Work Order: 8060117
Time Collected: 06/05/18 11:00
Time Submitted: 06/07/18 10:30
S-1 @77
General Chemistry Parameters
SM2540 G P8F025110.100 6/13/18 15:00 BJC% by
Weight
0.100% Solids 80.9
Semivolatile Organic Compounds by GC/MS
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene 0.064 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0621,2-Dichlorobenzene 0.062 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0571,3-Dichlorobenzene 0.057 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0601,4-Dichlorobenzene 0.060 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0791-Methylnaphthalene 0.079 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0762,4,6-Trichlorophenol 0.076 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0792,4-Dichlorophenol 0.079 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0622,4-Dimethylphenol 0.062 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0572,4-Dinitrophenol 0.057 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0502,4-Dinitrotoluene 0.050 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0542,6-Dinitrotoluene 0.054 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0592-Chloronaphthalene 0.059 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0582-Chlorophenol 0.058 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0652-Methylnaphthalene 0.065 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0522-Methylphenol 0.052 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0742-Nitrophenol 0.074 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0813,3’-Dichlorobenzidine 0.081 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0503/4-Methylphenol 0.050 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol 0.061 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether 0.070 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0574-Chloro-3-methylphenol 0.057 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0494-Chloroaniline 0.049 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether 0.053 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.0634-Nitrophenol 0.063 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.055Acenaphthene0.055 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.059Acenaphthylene0.059 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.066Anthracene0.066 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.054Azobenzene0.054 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.053Benzo(a)anthracene 0.053 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.044Benzo(a)pyrene 0.044 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.047Benzo(b)fluoranthene 0.047 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.045Benzo(g,h,i)perylene 0.045 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.053Benzo(k)fluoranthene 0.053 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.034Benzoic Acid 0.25 J
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.054Benzyl alcohol 0.054 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane 0.071 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether 0.058 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether 0.070 UCCV
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate 0.061 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-01
Prism Work Order: 8060117
Time Collected: 06/05/18 11:00
Time Submitted: 06/07/18 10:30
S-1 @77
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.058Butyl benzyl phthalate 0.058 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.051Chrysene0.051 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene 0.050 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.062Dibenzofuran0.062 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.056Diethyl phthalate 0.056 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.054Dimethyl phthalate 0.054 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.058Di-n-butyl phthalate 0.058 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.050Di-n-octyl phthalate 0.050 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.052Fluoranthene0.052 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.059Fluorene0.059 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.065Hexachlorobenzene0.065 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.073Hexachlorobutadiene0.073 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.073Hexachlorocyclopentadiene0.073 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.068Hexachloroethane0.068 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene 0.047 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.055Isophorone0.055 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.066Naphthalene0.066 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.058Nitrobenzene0.058 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.064N-Nitroso-di-n-propylamine 0.064 UCCV
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.062N-Nitrosodiphenylamine 0.062 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.048Pentachlorophenol0.048 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.053Phenanthrene0.053 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.060Phenol0.060 U
8270D P8F019010.41 6/13/18 21:22 JMVmg/kg dry 0.054Pyrene0.054 U
Surrogate Recovery Control Limits
39-13265 %2,4,6-Tribromophenol
44-11573 %2-Fluorobiphenyl
35-11570 %2-Fluorophenol
37-12265 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12766 %Terphenyl-d14
Total Metals
7471B P8F018810.024 6/12/18 13:11 JABmg/kg dry 0.0023Mercury0.024
6020B P8F0130101.8 6/11/18 16:48 JABmg/kg dry 0.17Arsenic1.5 J
6020B P8F013010126/11/18 16:48 JABmg/kg dry 0.075Barium69
6020B P8F0130100.31 6/11/18 16:48 JABmg/kg dry 0.023Cadmium0.033 J
6020B P8F0130100.61 6/11/18 16:48 JABmg/kg dry 0.034Chromium19
6020B P8F0130100.31 6/11/18 16:48 JABmg/kg dry 0.070Lead22
6020B P8F0130101.2 6/11/18 16:48 JABmg/kg dry 0.25Selenium0.84 J
6020B P8F0130100.31 6/11/18 16:48 JABmg/kg dry 0.023Silver0.040 J
Volatile Organic Compounds by GC/MS
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000481,1,1,2-Tetrachloroethane 0.00048 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-01
Prism Work Order: 8060117
Time Collected: 06/05/18 11:00
Time Submitted: 06/07/18 10:30
S-1 @77
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000281,1,1-Trichloroethane 0.00028 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane 0.00040 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000521,1,2-Trichloroethane 0.00052 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000161,1-Dichloroethane 0.00016 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000261,1-Dichloroethylene 0.00026 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000321,1-Dichloropropylene 0.00032 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000331,2,3-Trichlorobenzene 0.00033 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000751,2,3-Trichloropropane 0.00075 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene 0.00044 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000451,2,4-Trimethylbenzene 0.00045 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000241,2-Dibromoethane 0.00024 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000281,2-Dichlorobenzene 0.00028 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000351,2-Dichloroethane 0.00035 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000361,2-Dichloropropane 0.00036 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000441,3,5-Trimethylbenzene 0.00044 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000391,3-Dichlorobenzene 0.00039 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000291,3-Dichloropropane 0.00029 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000231,4-Dichlorobenzene 0.00023 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000282,2-Dichloropropane 0.00028 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000302-Chlorotoluene 0.00030 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000354-Chlorotoluene 0.00035 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.000284-Isopropyltoluene 0.00028 U
8260B P8F025310.059 6/14/18 13:59 ANGmg/kg dry 0.0014Acetone0.099
8260B P8F025310.0035 6/14/18 13:59 ANGmg/kg dry 0.00034Benzene0.00034 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00049Bromobenzene0.00049 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00032Bromochloromethane0.00032 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00033Bromodichloromethane0.00033 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00067Bromoform0.00067 U
8260B P8F025310.012 6/14/18 13:59 ANGmg/kg dry 0.00072Bromomethane0.00072 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00029Carbon Tetrachloride 0.00029 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00031Chlorobenzene0.00031 U
8260B P8F025310.012 6/14/18 13:59 ANGmg/kg dry 0.00049Chloroethane0.00049 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00042Chloroform0.00042 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00039Chloromethane0.00039 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene 0.00025 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene 0.00020 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00024Dibromochloromethane0.00024 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00027Dichlorodifluoromethane0.00027 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00023Ethylbenzene0.00023 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00024Isopropyl Ether 0.00024 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene)0.00035 U
8260B P8F025310.012 6/14/18 13:59 ANGmg/kg dry 0.00054m,p-Xylenes 0.00054 U
8260B P8F025310.059 6/14/18 13:59 ANGmg/kg dry 0.00053Methyl Butyl Ketone (2-Hexanone)0.00053 U
8260B P8F025310.12 6/14/18 13:59 ANGmg/kg dry 0.00053Methyl Ethyl Ketone (2-Butanone)0.00053 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-01
Prism Work Order: 8060117
Time Collected: 06/05/18 11:00
Time Submitted: 06/07/18 10:30
S-1 @77
8260B P8F025310.059 6/14/18 13:59 ANGmg/kg dry 0.00050Methyl Isobutyl Ketone 0.00050 U
8260B P8F025310.012 6/14/18 13:59 ANGmg/kg dry 0.00033Methylene Chloride 0.00033 U
8260B P8F025310.012 6/14/18 13:59 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether 0.00019 U
8260B P8F025310.012 6/14/18 13:59 ANGmg/kg dry 0.00019Naphthalene0.00019 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00030n-Butylbenzene 0.00030 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00035n-Propylbenzene 0.00035 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00024o-Xylene 0.00024 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00028sec-Butylbenzene 0.00028 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00035Styrene0.00035 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00020tert-Butylbenzene 0.00020 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00028Tetrachloroethylene0.00028 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00034Toluene0.00034 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00035trans-1,2-Dichloroethylene 0.00035 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene 0.00031 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00038Trichloroethylene0.00038 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00038Trichlorofluoromethane0.00038 U
8260B P8F025310.029 6/14/18 13:59 ANGmg/kg dry 0.00080Vinyl acetate 0.00080 U
8260B P8F025310.0059 6/14/18 13:59 ANGmg/kg dry 0.00028Vinyl chloride 0.00028 U
8260B P8F025310.018 6/14/18 13:59 ANGmg/kg dry 0.0011Xylenes, total 0.0011 U
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12998 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-02
Prism Work Order: 8060117
Time Collected: 06/05/18 11:20
Time Submitted: 06/07/18 10:30
S-2 @11
General Chemistry Parameters
SM2540 G P8F025110.100 6/13/18 15:00 BJC% by
Weight
0.100% Solids 83.2
Semivolatile Organic Compounds by GC/MS
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0621,2,4-Trichlorobenzene 0.062 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0601,2-Dichlorobenzene 0.060 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0561,3-Dichlorobenzene 0.056 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0581,4-Dichlorobenzene 0.058 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0761-Methylnaphthalene 0.076 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0742,4,6-Trichlorophenol 0.074 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0772,4-Dichlorophenol 0.077 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0612,4-Dimethylphenol 0.061 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0552,4-Dinitrophenol 0.055 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0482,4-Dinitrotoluene 0.048 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0532,6-Dinitrotoluene 0.053 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0572-Chloronaphthalene 0.057 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0562-Chlorophenol 0.056 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0632-Methylnaphthalene 0.063 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0512-Methylphenol 0.051 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0722-Nitrophenol 0.072 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0783,3’-Dichlorobenzidine 0.078 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0493/4-Methylphenol 0.049 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol 0.059 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0684-Bromophenyl phenyl ether 0.068 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0564-Chloro-3-methylphenol 0.056 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0484-Chloroaniline 0.048 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether 0.051 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.0614-Nitrophenol 0.061 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.054Acenaphthene0.054 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.057Acenaphthylene0.057 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.064Anthracene0.064 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.052Azobenzene0.052 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.052Benzo(a)anthracene 0.052 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.043Benzo(a)pyrene 0.043 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.046Benzo(b)fluoranthene 0.046 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.043Benzo(g,h,i)perylene 0.043 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.052Benzo(k)fluoranthene 0.052 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.033Benzoic Acid 0.80
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.052Benzyl alcohol 0.052 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.069bis(2-Chloroethoxy)methane 0.069 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether 0.056 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether 0.068 UCCV
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate 0.059 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-02
Prism Work Order: 8060117
Time Collected: 06/05/18 11:20
Time Submitted: 06/07/18 10:30
S-2 @11
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.056Butyl benzyl phthalate 0.056 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.050Chrysene0.050 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene 0.048 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.060Dibenzofuran0.060 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.055Diethyl phthalate 0.055 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.052Dimethyl phthalate 0.052 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.056Di-n-butyl phthalate 0.056 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.049Di-n-octyl phthalate 0.049 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.050Fluoranthene0.050 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.057Fluorene0.057 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.063Hexachlorobenzene0.063 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.071Hexachlorobutadiene0.071 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.071Hexachlorocyclopentadiene0.071 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.066Hexachloroethane0.066 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene 0.045 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.054Isophorone0.054 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.064Naphthalene0.064 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.056Nitrobenzene0.056 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine 0.062 UCCV
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.060N-Nitrosodiphenylamine 0.060 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.047Pentachlorophenol0.047 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.051Phenanthrene0.051 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.058Phenol0.058 U
8270D P8F019010.40 6/13/18 21:44 JMVmg/kg dry 0.052Pyrene0.052 U
Surrogate Recovery Control Limits
39-13270 %2,4,6-Tribromophenol
44-11580 %2-Fluorobiphenyl
35-11575 %2-Fluorophenol
37-12277 %Nitrobenzene-d5
34-12174 %Phenol-d5
54-12772 %Terphenyl-d14
Total Metals
7471B P8F018810.024 6/12/18 13:16 JABmg/kg dry 0.0023Mercury0.028
6020B P8F0130101.8 6/11/18 17:12 JABmg/kg dry 0.16Arsenic2.4
6020B P8F013010126/11/18 17:12 JABmg/kg dry 0.073Barium77
6020B P8F0130100.30 6/11/18 17:12 JABmg/kg dry 0.023Cadmium0.057 J
6020B P8F0130100.59 6/11/18 17:12 JABmg/kg dry 0.033Chromium17
6020B P8F0130100.30 6/11/18 17:12 JABmg/kg dry 0.068Lead18
6020B P8F0130101.2 6/11/18 17:12 JABmg/kg dry 0.24Selenium1.6
6020B P8F0130100.30 6/11/18 17:12 JABmg/kg dry 0.023Silver0.12 J
Volatile Organic Compounds by GC/MS
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000531,1,1,2-Tetrachloroethane 0.00053 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-02
Prism Work Order: 8060117
Time Collected: 06/05/18 11:20
Time Submitted: 06/07/18 10:30
S-2 @11
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000311,1,1-Trichloroethane 0.00031 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000441,1,2,2-Tetrachloroethane 0.00044 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000581,1,2-Trichloroethane 0.00058 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000181,1-Dichloroethane 0.00018 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000291,1-Dichloroethylene 0.00029 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000361,1-Dichloropropylene 0.00036 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000371,2,3-Trichlorobenzene 0.00037 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000831,2,3-Trichloropropane 0.00083 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000481,2,4-Trichlorobenzene 0.00048 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000501,2,4-Trimethylbenzene 0.00050 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000261,2-Dibromoethane 0.00026 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000311,2-Dichlorobenzene 0.00031 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000391,2-Dichloroethane 0.00039 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000401,2-Dichloropropane 0.00040 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000491,3,5-Trimethylbenzene 0.00049 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000431,3-Dichlorobenzene 0.00043 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000331,3-Dichloropropane 0.00033 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000261,4-Dichlorobenzene 0.00026 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000312,2-Dichloropropane 0.00031 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000342-Chlorotoluene 0.00034 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000394-Chlorotoluene 0.00039 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.000314-Isopropyltoluene 0.00031 U
8260B P8F025310.065 6/14/18 14:27 ANGmg/kg dry 0.0016Acetone0.068
8260B P8F025310.0039 6/14/18 14:27 ANGmg/kg dry 0.00038Benzene0.00038 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00054Bromobenzene0.00054 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00036Bromochloromethane0.00036 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00036Bromodichloromethane0.00036 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00074Bromoform0.00074 U
8260B P8F025310.013 6/14/18 14:27 ANGmg/kg dry 0.00080Bromomethane0.00080 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00032Carbon Tetrachloride 0.00032 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00034Chlorobenzene0.00034 U
8260B P8F025310.013 6/14/18 14:27 ANGmg/kg dry 0.00054Chloroethane0.00054 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00047Chloroform0.00047 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00044Chloromethane0.00044 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00028cis-1,2-Dichloroethylene 0.00028 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00022cis-1,3-Dichloropropylene 0.00022 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00027Dibromochloromethane0.00027 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00030Dichlorodifluoromethane0.00030 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00025Ethylbenzene0.00025 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00027Isopropyl Ether 0.00027 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00038Isopropylbenzene (Cumene)0.00038 U
8260B P8F025310.013 6/14/18 14:27 ANGmg/kg dry 0.00060m,p-Xylenes 0.00060 U
8260B P8F025310.065 6/14/18 14:27 ANGmg/kg dry 0.00059Methyl Butyl Ketone (2-Hexanone)0.00059 U
8260B P8F025310.13 6/14/18 14:27 ANGmg/kg dry 0.00059Methyl Ethyl Ketone (2-Butanone)0.00059 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-02
Prism Work Order: 8060117
Time Collected: 06/05/18 11:20
Time Submitted: 06/07/18 10:30
S-2 @11
8260B P8F025310.065 6/14/18 14:27 ANGmg/kg dry 0.00055Methyl Isobutyl Ketone 0.00055 U
8260B P8F025310.013 6/14/18 14:27 ANGmg/kg dry 0.00037Methylene Chloride 0.00037 U
8260B P8F025310.013 6/14/18 14:27 ANGmg/kg dry 0.00021Methyl-tert-Butyl Ether 0.00021 U
8260B P8F025310.013 6/14/18 14:27 ANGmg/kg dry 0.00021Naphthalene0.00021 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00033n-Butylbenzene 0.00033 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00039n-Propylbenzene 0.00039 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00027o-Xylene 0.00027 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00031sec-Butylbenzene 0.00031 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00039Styrene0.00039 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00022tert-Butylbenzene 0.00022 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00031Tetrachloroethylene0.00031 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00037Toluene0.00037 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00039trans-1,2-Dichloroethylene 0.00039 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00034trans-1,3-Dichloropropylene 0.00034 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00042Trichloroethylene0.00042 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00042Trichlorofluoromethane0.00042 U
8260B P8F025310.033 6/14/18 14:27 ANGmg/kg dry 0.00089Vinyl acetate 0.00089 U
8260B P8F025310.0065 6/14/18 14:27 ANGmg/kg dry 0.00031Vinyl chloride 0.00031 U
8260B P8F025310.020 6/14/18 14:27 ANGmg/kg dry 0.0012Xylenes, total 0.0012 U
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-03
Prism Work Order: 8060117
Time Collected: 06/05/18 11:40
Time Submitted: 06/07/18 10:30
S-6 @27
General Chemistry Parameters
SM2540 G P8F025110.100 6/13/18 15:00 BJC% by
Weight
0.100% Solids 81.9
Semivolatile Organic Compounds by GC/MS
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene 0.063 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0611,2-Dichlorobenzene 0.061 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0571,3-Dichlorobenzene 0.057 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0591,4-Dichlorobenzene 0.059 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0781-Methylnaphthalene 0.078 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0762,4,6-Trichlorophenol 0.076 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0782,4-Dichlorophenol 0.078 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0622,4-Dimethylphenol 0.062 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0562,4-Dinitrophenol 0.056 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0492,4-Dinitrotoluene 0.049 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0542,6-Dinitrotoluene 0.054 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0582-Chloronaphthalene 0.058 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0572-Chlorophenol 0.057 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0642-Methylnaphthalene 0.064 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0522-Methylphenol 0.052 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0732-Nitrophenol 0.073 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0803,3’-Dichlorobenzidine 0.080 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0503/4-Methylphenol 0.050 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol 0.061 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0694-Bromophenyl phenyl ether 0.069 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0574-Chloro-3-methylphenol 0.057 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0484-Chloroaniline 0.048 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether 0.052 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.0624-Nitrophenol 0.062 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.055Acenaphthene0.055 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.058Acenaphthylene0.058 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.065Anthracene0.065 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.053Azobenzene0.053 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.053Benzo(a)anthracene 0.053 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.044Benzo(a)pyrene 0.044 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.047Benzo(b)fluoranthene 0.047 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.044Benzo(g,h,i)perylene 0.044 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.053Benzo(k)fluoranthene 0.053 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.034Benzoic Acid 0.034 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.053Benzyl alcohol 0.053 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane 0.070 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether 0.057 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether 0.069 UCCV
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate 0.060 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-03
Prism Work Order: 8060117
Time Collected: 06/05/18 11:40
Time Submitted: 06/07/18 10:30
S-6 @27
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.057Butyl benzyl phthalate 0.057 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.051Chrysene0.051 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene 0.049 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.061Dibenzofuran0.061 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.056Diethyl phthalate 0.056 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.053Dimethyl phthalate 0.053 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.057Di-n-butyl phthalate 0.057 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.050Di-n-octyl phthalate 0.050 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.051Fluoranthene0.051 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.058Fluorene0.058 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.064Hexachlorobenzene0.064 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.072Hexachlorobutadiene0.072 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.072Hexachlorocyclopentadiene0.072 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.068Hexachloroethane0.068 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene 0.046 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.055Isophorone0.055 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.065Naphthalene0.065 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.057Nitrobenzene0.057 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine 0.063 UCCV
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.061N-Nitrosodiphenylamine 0.061 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.048Pentachlorophenol0.048 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.052Phenanthrene0.052 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.059Phenol0.059 U
8270D P8F019010.40 6/13/18 18:47 JMVmg/kg dry 0.053Pyrene0.053 U
Surrogate Recovery Control Limits
39-13268 %2,4,6-Tribromophenol
44-11566 %2-Fluorobiphenyl
35-11563 %2-Fluorophenol
37-12259 %Nitrobenzene-d5
34-12164 %Phenol-d5
54-12770 %Terphenyl-d14
Total Metals
7471B P8F018810.024 6/12/18 13:20 JABmg/kg dry 0.0022Mercury0.026
6020B P8F0130101.8 6/11/18 17:19 JABmg/kg dry 0.17Arsenic2.0
6020B P8F013010126/11/18 17:19 JABmg/kg dry 0.074Barium81
6020B P8F0130100.31 6/11/18 17:19 JABmg/kg dry 0.023Cadmium0.024 J
6020B P8F0130100.61 6/11/18 17:19 JABmg/kg dry 0.034Chromium22
6020B P8F0130100.31 6/11/18 17:19 JABmg/kg dry 0.070Lead17
6020B P8F0130101.2 6/11/18 17:19 JABmg/kg dry 0.25Selenium1.3
6020B P8F0130100.31 6/11/18 17:19 JABmg/kg dry 0.023Silver0.023 J
Volatile Organic Compounds by GC/MS
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000491,1,1,2-Tetrachloroethane 0.00049 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-03
Prism Work Order: 8060117
Time Collected: 06/05/18 11:40
Time Submitted: 06/07/18 10:30
S-6 @27
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000291,1,1-Trichloroethane 0.00029 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane 0.00040 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000531,1,2-Trichloroethane 0.00053 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000171,1-Dichloroethane 0.00017 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000261,1-Dichloroethylene 0.00026 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000331,1-Dichloropropylene 0.00033 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene 0.00034 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000761,2,3-Trichloropropane 0.00076 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene 0.00044 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000451,2,4-Trimethylbenzene 0.00045 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000241,2-Dibromoethane 0.00024 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000281,2-Dichlorobenzene 0.00028 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000351,2-Dichloroethane 0.00035 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000371,2-Dichloropropane 0.00037 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000451,3,5-Trimethylbenzene 0.00045 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000391,3-Dichlorobenzene 0.00039 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000301,3-Dichloropropane 0.00030 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000231,4-Dichlorobenzene 0.00023 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000282,2-Dichloropropane 0.00028 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000312-Chlorotoluene 0.00031 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000354-Chlorotoluene 0.00035 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.000294-Isopropyltoluene 0.00029 U
8260B P8F025310.060 6/14/18 14:55 ANGmg/kg dry 0.0015Acetone0.0015 U
8260B P8F025310.0036 6/14/18 14:55 ANGmg/kg dry 0.00035Benzene0.00035 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00050Bromobenzene0.00050 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00033Bromochloromethane0.00033 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00033Bromodichloromethane0.00033 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00068Bromoform0.00068 U
8260B P8F025310.012 6/14/18 14:55 ANGmg/kg dry 0.00073Bromomethane0.00073 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00030Carbon Tetrachloride 0.00030 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00032Chlorobenzene0.00032 U
8260B P8F025310.012 6/14/18 14:55 ANGmg/kg dry 0.00050Chloroethane0.00050 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00043Chloroform0.00043 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00040Chloromethane0.00040 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene 0.00025 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene 0.00020 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00025Dibromochloromethane0.00025 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00027Dichlorodifluoromethane0.00027 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00023Ethylbenzene0.00023 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00024Isopropyl Ether 0.00024 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene)0.00035 U
8260B P8F025310.012 6/14/18 14:55 ANGmg/kg dry 0.00055m,p-Xylenes 0.00055 U
8260B P8F025310.060 6/14/18 14:55 ANGmg/kg dry 0.00054Methyl Butyl Ketone (2-Hexanone)0.00054 U
8260B P8F025310.12 6/14/18 14:55 ANGmg/kg dry 0.00054Methyl Ethyl Ketone (2-Butanone)0.00054 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-03
Prism Work Order: 8060117
Time Collected: 06/05/18 11:40
Time Submitted: 06/07/18 10:30
S-6 @27
8260B P8F025310.060 6/14/18 14:55 ANGmg/kg dry 0.00051Methyl Isobutyl Ketone 0.00051 U
8260B P8F025310.012 6/14/18 14:55 ANGmg/kg dry 0.00033Methylene Chloride 0.00033 U
8260B P8F025310.012 6/14/18 14:55 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether 0.00019 U
8260B P8F025310.012 6/14/18 14:55 ANGmg/kg dry 0.00019Naphthalene0.00019 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00030n-Butylbenzene 0.00030 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00035n-Propylbenzene 0.00035 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00024o-Xylene 0.00024 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00029sec-Butylbenzene 0.00029 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00036Styrene0.00036 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00020tert-Butylbenzene 0.00020 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00028Tetrachloroethylene0.00028 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00034Toluene0.00034 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00036trans-1,2-Dichloroethylene 0.00036 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene 0.00031 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00039Trichloroethylene0.00039 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00038Trichlorofluoromethane0.00038 U
8260B P8F025310.030 6/14/18 14:55 ANGmg/kg dry 0.00082Vinyl acetate 0.00082 U
8260B P8F025310.0060 6/14/18 14:55 ANGmg/kg dry 0.00029Vinyl chloride 0.00029 U
8260B P8F025310.018 6/14/18 14:55 ANGmg/kg dry 0.0011Xylenes, total 0.0011 U
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-04
Prism Work Order: 8060117
Time Collected: 06/05/18 12:00
Time Submitted: 06/07/18 10:30
S-4 @36
General Chemistry Parameters
SM2540 G P8F025110.100 6/13/18 15:00 BJC% by
Weight
0.100% Solids 82.0
Semivolatile Organic Compounds by GC/MS
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene 0.063 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0611,2-Dichlorobenzene 0.061 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0571,3-Dichlorobenzene 0.057 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0591,4-Dichlorobenzene 0.059 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0771-Methylnaphthalene 0.077 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0752,4,6-Trichlorophenol 0.075 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0782,4-Dichlorophenol 0.078 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0622,4-Dimethylphenol 0.062 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0562,4-Dinitrophenol 0.056 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0492,4-Dinitrotoluene 0.049 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0532,6-Dinitrotoluene 0.053 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0582-Chloronaphthalene 0.058 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0572-Chlorophenol 0.057 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0642-Methylnaphthalene 0.064 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0512-Methylphenol 0.051 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0732-Nitrophenol 0.073 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0793,3’-Dichlorobenzidine 0.079 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0503/4-Methylphenol 0.050 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol 0.060 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0694-Bromophenyl phenyl ether 0.069 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0564-Chloro-3-methylphenol 0.056 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0484-Chloroaniline 0.048 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether 0.052 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.0624-Nitrophenol 0.062 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.055Acenaphthene0.055 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.058Acenaphthylene0.058 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.065Anthracene0.065 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.053Azobenzene0.053 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.053Benzo(a)anthracene 0.053 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.043Benzo(a)pyrene 0.043 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.047Benzo(b)fluoranthene 0.047 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.044Benzo(g,h,i)perylene 0.044 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.053Benzo(k)fluoranthene 0.053 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.034Benzoic Acid 0.24 J
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.053Benzyl alcohol 0.053 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane 0.070 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether 0.057 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether 0.069 UCCV
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate 0.060 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-04
Prism Work Order: 8060117
Time Collected: 06/05/18 12:00
Time Submitted: 06/07/18 10:30
S-4 @36
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.057Butyl benzyl phthalate 0.057 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.051Chrysene0.051 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene 0.049 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.061Dibenzofuran0.061 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.055Diethyl phthalate 0.055 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.053Dimethyl phthalate 0.053 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.057Di-n-butyl phthalate 0.057 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.049Di-n-octyl phthalate 0.049 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.051Fluoranthene0.051 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.058Fluorene0.058 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.064Hexachlorobenzene0.064 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.072Hexachlorobutadiene0.072 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.072Hexachlorocyclopentadiene0.072 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.067Hexachloroethane0.067 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene 0.046 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.054Isophorone0.054 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.065Naphthalene0.065 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.057Nitrobenzene0.057 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine 0.063 UCCV
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.061N-Nitrosodiphenylamine 0.061 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.047Pentachlorophenol0.047 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.052Phenanthrene0.052 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.059Phenol0.059 U
8270D P8F019010.40 6/13/18 22:06 JMVmg/kg dry 0.053Pyrene0.053 U
Surrogate Recovery Control Limits
39-13271 %2,4,6-Tribromophenol
44-11580 %2-Fluorobiphenyl
35-11577 %2-Fluorophenol
37-12273 %Nitrobenzene-d5
34-12174 %Phenol-d5
54-12772 %Terphenyl-d14
Total Metals
7471B P8F018810.024 6/12/18 13:25 JABmg/kg dry 0.0023Mercury0.030
6020B P8F0130101.8 6/11/18 17:27 JABmg/kg dry 0.17Arsenic1.6 J
6020B P8F013010126/11/18 17:27 JABmg/kg dry 0.074Barium120
6020B P8F0130100.30 6/11/18 17:27 JABmg/kg dry 0.023Cadmium0.023 U
6020B P8F0130100.61 6/11/18 17:27 JABmg/kg dry 0.034Chromium32
6020B P8F0130100.30 6/11/18 17:27 JABmg/kg dry 0.069Lead18
6020B P8F0130101.2 6/11/18 17:27 JABmg/kg dry 0.25Selenium2.1
6020B P8F0130100.30 6/11/18 17:27 JABmg/kg dry 0.023Silver0.023 U
Volatile Organic Compounds by GC/MS
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000451,1,1,2-Tetrachloroethane 0.00045 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000271,1,1-Trichloroethane 0.00027 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-04
Prism Work Order: 8060117
Time Collected: 06/05/18 12:00
Time Submitted: 06/07/18 10:30
S-4 @36
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000371,1,2,2-Tetrachloroethane 0.00037 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000491,1,2-Trichloroethane 0.00049 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000151,1-Dichloroethane 0.00015 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000241,1-Dichloroethylene 0.00024 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000301,1-Dichloropropylene 0.00030 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000311,2,3-Trichlorobenzene 0.00031 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000711,2,3-Trichloropropane 0.00071 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000411,2,4-Trichlorobenzene 0.00041 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000421,2,4-Trimethylbenzene 0.00042 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000221,2-Dibromoethane 0.00022 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000261,2-Dichlorobenzene 0.00026 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000331,2-Dichloroethane 0.00033 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000341,2-Dichloropropane 0.00034 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000421,3,5-Trimethylbenzene 0.00042 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000371,3-Dichlorobenzene 0.00037 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000281,3-Dichloropropane 0.00028 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000221,4-Dichlorobenzene 0.00022 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000262,2-Dichloropropane 0.00026 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000292-Chlorotoluene 0.00029 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000334-Chlorotoluene 0.00033 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.000274-Isopropyltoluene 0.00027 U
8260B P8F025310.055 6/14/18 15:23 ANGmg/kg dry 0.0013Acetone0.068
8260B P8F025310.0033 6/14/18 15:23 ANGmg/kg dry 0.00032Benzene0.00032 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00046Bromobenzene0.00046 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00030Bromochloromethane0.00030 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00031Bromodichloromethane0.00031 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00063Bromoform0.00063 U
8260B P8F025310.011 6/14/18 15:23 ANGmg/kg dry 0.00068Bromomethane0.00068 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00028Carbon Tetrachloride 0.00028 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00029Chlorobenzene0.00029 U
8260B P8F025310.011 6/14/18 15:23 ANGmg/kg dry 0.00046Chloroethane0.00046 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00040Chloroform0.00040 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00037Chloromethane0.00037 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene 0.00024 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene 0.00019 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00023Dibromochloromethane0.00023 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00025Dichlorodifluoromethane0.00025 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00021Ethylbenzene0.00021 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00023Isopropyl Ether 0.00023 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00033Isopropylbenzene (Cumene)0.00033 U
8260B P8F025310.011 6/14/18 15:23 ANGmg/kg dry 0.00051m,p-Xylenes 0.00051 U
8260B P8F025310.055 6/14/18 15:23 ANGmg/kg dry 0.00050Methyl Butyl Ketone (2-Hexanone)0.00050 U
8260B P8F025310.11 6/14/18 15:23 ANGmg/kg dry 0.00050Methyl Ethyl Ketone (2-Butanone)0.00050 U
8260B P8F025310.055 6/14/18 15:23 ANGmg/kg dry 0.00047Methyl Isobutyl Ketone 0.00047 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-04
Prism Work Order: 8060117
Time Collected: 06/05/18 12:00
Time Submitted: 06/07/18 10:30
S-4 @36
8260B P8F025310.011 6/14/18 15:23 ANGmg/kg dry 0.00031Methylene Chloride 0.00031 U
8260B P8F025310.011 6/14/18 15:23 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether 0.00018 U
8260B P8F025310.011 6/14/18 15:23 ANGmg/kg dry 0.00017Naphthalene0.00017 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00028n-Butylbenzene 0.00028 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00033n-Propylbenzene 0.00033 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00023o-Xylene 0.00023 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00027sec-Butylbenzene 0.00027 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00033Styrene0.00033 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00019tert-Butylbenzene 0.00019 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00026Tetrachloroethylene0.00026 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00032Toluene0.00032 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00033trans-1,2-Dichloroethylene 0.00033 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00029trans-1,3-Dichloropropylene 0.00029 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00036Trichloroethylene0.00036 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00036Trichlorofluoromethane0.00036 U
8260B P8F025310.028 6/14/18 15:23 ANGmg/kg dry 0.00076Vinyl acetate 0.00076 U
8260B P8F025310.0055 6/14/18 15:23 ANGmg/kg dry 0.00027Vinyl chloride 0.00027 U
8260B P8F025310.017 6/14/18 15:23 ANGmg/kg dry 0.0010Xylenes, total 0.0010 U
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-05
Prism Work Order: 8060117
Time Collected: 06/05/18 12:20
Time Submitted: 06/07/18 10:30
S-5
General Chemistry Parameters
SM2540 G P8F025110.100 6/13/18 15:00 BJC% by
Weight
0.100% Solids 86.4
Semivolatile Organic Compounds by GC/MS
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0591,2,4-Trichlorobenzene 0.059 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0581,2-Dichlorobenzene 0.058 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0541,3-Dichlorobenzene 0.054 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0561,4-Dichlorobenzene 0.056 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0731-Methylnaphthalene 0.073 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0712,4,6-Trichlorophenol 0.071 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0742,4-Dichlorophenol 0.074 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0582,4-Dimethylphenol 0.058 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0532,4-Dinitrophenol 0.053 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0462,4-Dinitrotoluene 0.046 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0512,6-Dinitrotoluene 0.051 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0552-Chloronaphthalene 0.055 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0542-Chlorophenol 0.054 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0612-Methylnaphthalene 0.061 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0492-Methylphenol 0.049 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0692-Nitrophenol 0.069 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0753,3’-Dichlorobenzidine 0.075 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0473/4-Methylphenol 0.047 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0574,6-Dinitro-2-methylphenol 0.057 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0654-Bromophenyl phenyl ether 0.065 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0534-Chloro-3-methylphenol 0.053 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0464-Chloroaniline 0.046 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0504-Chlorophenyl phenyl ether 0.050 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.0594-Nitrophenol 0.059 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.052Acenaphthene0.052 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.055Acenaphthylene0.055 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.061Anthracene0.061 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.050Azobenzene0.050 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.050Benzo(a)anthracene 0.050 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.041Benzo(a)pyrene 0.041 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.044Benzo(b)fluoranthene 0.044 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.042Benzo(g,h,i)perylene 0.042 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.050Benzo(k)fluoranthene 0.050 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.032Benzoic Acid 0.032 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.050Benzyl alcohol 0.050 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.066bis(2-Chloroethoxy)methane 0.066 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.054Bis(2-Chloroethyl)ether 0.054 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.065Bis(2-chloroisopropyl)ether 0.065 UCCV
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.057Bis(2-Ethylhexyl)phthalate 0.057 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-05
Prism Work Order: 8060117
Time Collected: 06/05/18 12:20
Time Submitted: 06/07/18 10:30
S-5
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.054Butyl benzyl phthalate 0.054 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.048Chrysene0.048 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene 0.046 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.058Dibenzofuran0.058 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.053Diethyl phthalate 0.053 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.050Dimethyl phthalate 0.050 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.054Di-n-butyl phthalate 0.054 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.047Di-n-octyl phthalate 0.047 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.049Fluoranthene0.049 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.055Fluorene0.055 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.060Hexachlorobenzene0.060 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.068Hexachlorobutadiene0.068 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.068Hexachlorocyclopentadiene0.068 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.064Hexachloroethane0.064 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.044Indeno(1,2,3-cd)pyrene 0.044 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.052Isophorone0.052 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.061Naphthalene0.061 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.054Nitrobenzene0.054 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.060N-Nitroso-di-n-propylamine 0.060 UCCV
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.058N-Nitrosodiphenylamine 0.058 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.045Pentachlorophenol0.045 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.050Phenanthrene0.050 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.056Phenol0.056 U
8270D P8F019010.38 6/13/18 19:09 JMVmg/kg dry 0.050Pyrene0.050 U
Surrogate Recovery Control Limits
39-13266 %2,4,6-Tribromophenol
44-11579 %2-Fluorobiphenyl
35-11566 %2-Fluorophenol
37-12269 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12770 %Terphenyl-d14
Total Metals
7471B P8F018810.023 6/12/18 13:29 JABmg/kg dry 0.0022Mercury0.031
6020B P8F0130101.7 6/11/18 17:35 JABmg/kg dry 0.16Arsenic2.5
6020B P8F013010126/11/18 17:35 JABmg/kg dry 0.071Barium95
6020B P8F0130100.29 6/11/18 17:35 JABmg/kg dry 0.022Cadmium0.022 U
6020B P8F0130100.58 6/11/18 17:35 JABmg/kg dry 0.032Chromium24
6020B P8F0130100.29 6/11/18 17:35 JABmg/kg dry 0.066Lead16
6020B P8F0130101.2 6/11/18 17:35 JABmg/kg dry 0.24Selenium1.8
6020B P8F0130100.29 6/11/18 17:35 JABmg/kg dry 0.022Silver0.022 U
Volatile Organic Compounds by GC/MS
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000491,1,1,2-Tetrachloroethane 0.00049 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000291,1,1-Trichloroethane 0.00029 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-05
Prism Work Order: 8060117
Time Collected: 06/05/18 12:20
Time Submitted: 06/07/18 10:30
S-5
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000401,1,2,2-Tetrachloroethane 0.00040 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000531,1,2-Trichloroethane 0.00053 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000171,1-Dichloroethane 0.00017 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000261,1-Dichloroethylene 0.00026 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000331,1-Dichloropropylene 0.00033 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000341,2,3-Trichlorobenzene 0.00034 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000761,2,3-Trichloropropane 0.00076 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000441,2,4-Trichlorobenzene 0.00044 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000461,2,4-Trimethylbenzene 0.00046 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000241,2-Dibromoethane 0.00024 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000281,2-Dichlorobenzene 0.00028 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000361,2-Dichloroethane 0.00036 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000371,2-Dichloropropane 0.00037 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000451,3,5-Trimethylbenzene 0.00045 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000401,3-Dichlorobenzene 0.00040 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000301,3-Dichloropropane 0.00030 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000241,4-Dichlorobenzene 0.00024 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000282,2-Dichloropropane 0.00028 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000312-Chlorotoluene 0.00031 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000364-Chlorotoluene 0.00036 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.000294-Isopropyltoluene 0.00029 U
8260B P8F025310.060 6/14/18 15:51 ANGmg/kg dry 0.0015Acetone0.0015 U
8260B P8F025310.0036 6/14/18 15:51 ANGmg/kg dry 0.00035Benzene0.00035 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00050Bromobenzene0.00050 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00033Bromochloromethane0.00033 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00033Bromodichloromethane0.00033 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00068Bromoform0.00068 U
8260B P8F025310.012 6/14/18 15:51 ANGmg/kg dry 0.00074Bromomethane0.00074 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00030Carbon Tetrachloride 0.00030 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00032Chlorobenzene0.00032 U
8260B P8F025310.012 6/14/18 15:51 ANGmg/kg dry 0.00050Chloroethane0.00050 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00043Chloroform0.00043 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00040Chloromethane0.00040 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00025cis-1,2-Dichloroethylene 0.00025 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00020cis-1,3-Dichloropropylene 0.00020 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00025Dibromochloromethane0.00025 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00027Dichlorodifluoromethane0.00027 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00023Ethylbenzene0.00023 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00024Isopropyl Ether 0.00024 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00035Isopropylbenzene (Cumene)0.00035 U
8260B P8F025310.012 6/14/18 15:51 ANGmg/kg dry 0.00055m,p-Xylenes 0.00055 U
8260B P8F025310.060 6/14/18 15:51 ANGmg/kg dry 0.00054Methyl Butyl Ketone (2-Hexanone)0.00054 U
8260B P8F025310.12 6/14/18 15:51 ANGmg/kg dry 0.00054Methyl Ethyl Ketone (2-Butanone)0.00054 U
8260B P8F025310.060 6/14/18 15:51 ANGmg/kg dry 0.00051Methyl Isobutyl Ketone 0.00051 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-05
Prism Work Order: 8060117
Time Collected: 06/05/18 12:20
Time Submitted: 06/07/18 10:30
S-5
8260B P8F025310.012 6/14/18 15:51 ANGmg/kg dry 0.00034Methylene Chloride 0.00034 U
8260B P8F025310.012 6/14/18 15:51 ANGmg/kg dry 0.00019Methyl-tert-Butyl Ether 0.00019 U
8260B P8F025310.012 6/14/18 15:51 ANGmg/kg dry 0.00019Naphthalene0.00019 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00031n-Butylbenzene 0.00031 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00036n-Propylbenzene 0.00036 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00025o-Xylene 0.00025 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00029sec-Butylbenzene 0.00029 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00036Styrene0.00036 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00020tert-Butylbenzene 0.00020 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00028Tetrachloroethylene0.00028 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00034Toluene0.00034 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00036trans-1,2-Dichloroethylene 0.00036 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00031trans-1,3-Dichloropropylene 0.00031 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00039Trichloroethylene0.00039 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00039Trichlorofluoromethane0.00039 U
8260B P8F025310.030 6/14/18 15:51 ANGmg/kg dry 0.00082Vinyl acetate 0.00082 U
8260B P8F025310.0060 6/14/18 15:51 ANGmg/kg dry 0.00029Vinyl chloride 0.00029 U
8260B P8F025310.018 6/14/18 15:51 ANGmg/kg dry 0.0011Xylenes, total 0.0011 U
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12995 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-06
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
S-3@52
General Chemistry Parameters
SM2540 G P8F025110.100 6/13/18 15:00 BJC% by
Weight
0.100% Solids 88.5
Semivolatile Organic Compounds by GC/MS
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0581,2,4-Trichlorobenzene 0.058 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0571,2-Dichlorobenzene 0.057 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0521,3-Dichlorobenzene 0.052 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0551,4-Dichlorobenzene 0.055 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0721-Methylnaphthalene 0.072 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0702,4,6-Trichlorophenol 0.070 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0722,4-Dichlorophenol 0.072 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0572,4-Dimethylphenol 0.057 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0522,4-Dinitrophenol 0.052 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0452,4-Dinitrotoluene 0.045 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0502,6-Dinitrotoluene 0.050 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0542-Chloronaphthalene 0.054 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0532-Chlorophenol 0.053 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0602-Methylnaphthalene 0.060 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0482-Methylphenol 0.048 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0682-Nitrophenol 0.068 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0743,3’-Dichlorobenzidine 0.074 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0463/4-Methylphenol 0.046 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0564,6-Dinitro-2-methylphenol 0.056 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0644-Bromophenyl phenyl ether 0.064 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0524-Chloro-3-methylphenol 0.052 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0454-Chloroaniline 0.045 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0484-Chlorophenyl phenyl ether 0.048 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.0574-Nitrophenol 0.057 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.051Acenaphthene0.051 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.054Acenaphthylene0.054 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.060Anthracene0.060 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.049Azobenzene0.049 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.049Benzo(a)anthracene 0.049 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.040Benzo(a)pyrene 0.040 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.043Benzo(b)fluoranthene 0.043 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.041Benzo(g,h,i)perylene 0.041 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.049Benzo(k)fluoranthene 0.049 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.031Benzoic Acid 0.14 J
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.049Benzyl alcohol 0.049 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.065bis(2-Chloroethoxy)methane 0.065 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether 0.053 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.064Bis(2-chloroisopropyl)ether 0.064 UCCV
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.055Bis(2-Ethylhexyl)phthalate 0.055 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-06
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
S-3@52
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.053Butyl benzyl phthalate 0.053 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.047Chrysene0.047 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.045Dibenzo(a,h)anthracene 0.045 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.057Dibenzofuran0.057 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.051Diethyl phthalate 0.051 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.049Dimethyl phthalate 0.049 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.053Di-n-butyl phthalate 0.053 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.046Di-n-octyl phthalate 0.046 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.048Fluoranthene0.048 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.053Fluorene0.053 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.059Hexachlorobenzene0.059 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.067Hexachlorobutadiene0.067 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.066Hexachlorocyclopentadiene0.066 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.062Hexachloroethane0.062 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.043Indeno(1,2,3-cd)pyrene 0.043 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.050Isophorone0.050 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.060Naphthalene0.060 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.053Nitrobenzene0.053 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.059N-Nitroso-di-n-propylamine 0.059 UCCV
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.057N-Nitrosodiphenylamine 0.057 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.044Pentachlorophenol0.044 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.048Phenanthrene0.048 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.055Phenol0.055 U
8270D P8F019010.37 6/13/18 19:31 JMVmg/kg dry 0.049Pyrene0.049 U
Surrogate Recovery Control Limits
39-13264 %2,4,6-Tribromophenol
44-11575 %2-Fluorobiphenyl
35-11570 %2-Fluorophenol
37-12269 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12766 %Terphenyl-d14
Total Metals
7471B P8F018810.023 6/12/18 13:34 JABmg/kg dry 0.0021Mercury0.034
6020B P8F0130101.7 6/11/18 17:43 JABmg/kg dry 0.15Arsenic2.3
6020B P8F013010116/11/18 17:43 JABmg/kg dry 0.069Barium72
6020B P8F0130100.28 6/11/18 17:43 JABmg/kg dry 0.021Cadmium0.053 J
6020B P8F0130100.56 6/11/18 17:43 JABmg/kg dry 0.032Chromium16
6020B P8F0130100.28 6/11/18 17:43 JABmg/kg dry 0.064Lead20
6020B P8F0130101.1 6/11/18 17:43 JABmg/kg dry 0.23Selenium1.8
6020B P8F0130100.28 6/11/18 17:43 JABmg/kg dry 0.021Silver0.052 J
Volatile Organic Compounds by GC/MS
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000531,1,1,2-Tetrachloroethane 0.00053 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-06
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
S-3@52
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000311,1,1-Trichloroethane 0.00031 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000441,1,2,2-Tetrachloroethane 0.00044 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000581,1,2-Trichloroethane 0.00058 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000181,1-Dichloroethane 0.00018 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000291,1-Dichloroethylene 0.00029 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000361,1-Dichloropropylene 0.00036 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000371,2,3-Trichlorobenzene 0.00037 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000831,2,3-Trichloropropane 0.00083 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000481,2,4-Trichlorobenzene 0.00048 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000501,2,4-Trimethylbenzene 0.00050 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000261,2-Dibromoethane 0.00026 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000311,2-Dichlorobenzene 0.00031 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000391,2-Dichloroethane 0.00039 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000401,2-Dichloropropane 0.00040 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000491,3,5-Trimethylbenzene 0.00049 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000431,3-Dichlorobenzene 0.00043 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000331,3-Dichloropropane 0.00033 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000261,4-Dichlorobenzene 0.00026 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000312,2-Dichloropropane 0.00031 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000342-Chlorotoluene 0.00034 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000394-Chlorotoluene 0.00039 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.000314-Isopropyltoluene 0.00031 U
8260B P8F025310.065 6/14/18 16:18 ANGmg/kg dry 0.0016Acetone0.0016 U
8260B P8F025310.0039 6/14/18 16:18 ANGmg/kg dry 0.00038Benzene0.00038 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00054Bromobenzene0.00054 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00036Bromochloromethane0.00036 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00036Bromodichloromethane0.00036 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00074Bromoform0.00074 U
8260B P8F025310.013 6/14/18 16:18 ANGmg/kg dry 0.00080Bromomethane0.00080 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00032Carbon Tetrachloride 0.00032 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00034Chlorobenzene0.00034 U
8260B P8F025310.013 6/14/18 16:18 ANGmg/kg dry 0.00054Chloroethane0.00054 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00047Chloroform0.00047 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00044Chloromethane0.00044 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00028cis-1,2-Dichloroethylene 0.00028 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00022cis-1,3-Dichloropropylene 0.00022 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00027Dibromochloromethane0.00027 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00029Dichlorodifluoromethane0.00029 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00025Ethylbenzene0.00025 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00026Isopropyl Ether 0.00026 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00038Isopropylbenzene (Cumene)0.00038 U
8260B P8F025310.013 6/14/18 16:18 ANGmg/kg dry 0.00060m,p-Xylenes 0.00060 U
8260B P8F025310.065 6/14/18 16:18 ANGmg/kg dry 0.00059Methyl Butyl Ketone (2-Hexanone)0.00059 U
8260B P8F025310.13 6/14/18 16:18 ANGmg/kg dry 0.00059Methyl Ethyl Ketone (2-Butanone)0.00059 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-06
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
S-3@52
8260B P8F025310.065 6/14/18 16:18 ANGmg/kg dry 0.00055Methyl Isobutyl Ketone 0.00055 U
8260B P8F025310.013 6/14/18 16:18 ANGmg/kg dry 0.00036Methylene Chloride 0.00036 U
8260B P8F025310.013 6/14/18 16:18 ANGmg/kg dry 0.00021Methyl-tert-Butyl Ether 0.00021 U
8260B P8F025310.013 6/14/18 16:18 ANGmg/kg dry 0.00021Naphthalene0.00021 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00033n-Butylbenzene 0.00033 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00039n-Propylbenzene 0.00039 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00027o-Xylene 0.00027 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00031sec-Butylbenzene 0.00031 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00039Styrene0.00039 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00022tert-Butylbenzene 0.00022 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00031Tetrachloroethylene0.00031 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00037Toluene0.00037 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00039trans-1,2-Dichloroethylene 0.00039 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00034trans-1,3-Dichloropropylene 0.00034 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00042Trichloroethylene0.00042 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00042Trichlorofluoromethane0.00042 U
8260B P8F025310.032 6/14/18 16:18 ANGmg/kg dry 0.00089Vinyl acetate 0.00089 U
8260B P8F025310.0065 6/14/18 16:18 ANGmg/kg dry 0.00031Vinyl chloride 0.00031 U
8260B P8F025310.019 6/14/18 16:18 ANGmg/kg dry 0.0012Xylenes, total 0.0012 U
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-07
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
DUPE
General Chemistry Parameters
SM2540 G P8F025110.100 6/13/18 15:00 BJC% by
Weight
0.100% Solids 87.8
Semivolatile Organic Compounds by GC/MS
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0591,2,4-Trichlorobenzene 0.059 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0571,2-Dichlorobenzene 0.057 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0531,3-Dichlorobenzene 0.053 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0551,4-Dichlorobenzene 0.055 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0721-Methylnaphthalene 0.24 J
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0702,4,6-Trichlorophenol 0.070 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0732,4-Dichlorophenol 0.073 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0582,4-Dimethylphenol 0.058 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0522,4-Dinitrophenol 0.052 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0462,4-Dinitrotoluene 0.046 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0502,6-Dinitrotoluene 0.050 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0542-Chloronaphthalene 0.054 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0532-Chlorophenol 0.053 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0602-Methylnaphthalene 0.44
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0482-Methylphenol 0.048 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0682-Nitrophenol 0.068 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0743,3’-Dichlorobenzidine 0.074 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0463/4-Methylphenol 0.046 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0564,6-Dinitro-2-methylphenol 0.056 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0654-Bromophenyl phenyl ether 0.065 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0534-Chloro-3-methylphenol 0.053 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0454-Chloroaniline 0.045 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0494-Chlorophenyl phenyl ether 0.049 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.0584-Nitrophenol 0.058 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.051Acenaphthene0.051 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.054Acenaphthylene0.054 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.061Anthracene0.061 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.050Azobenzene0.050 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.049Benzo(a)anthracene 0.049 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.041Benzo(a)pyrene 0.041 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.044Benzo(b)fluoranthene 0.044 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.041Benzo(g,h,i)perylene 0.041 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.049Benzo(k)fluoranthene 0.049 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.032Benzoic Acid 0.032 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.050Benzyl alcohol 0.050 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.065bis(2-Chloroethoxy)methane 0.065 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.053Bis(2-Chloroethyl)ether 0.053 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.064Bis(2-chloroisopropyl)ether 0.064 UCCV
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.056Bis(2-Ethylhexyl)phthalate 0.056 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-07
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
DUPE
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.053Butyl benzyl phthalate 0.053 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.047Chrysene0.047 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.046Dibenzo(a,h)anthracene 0.046 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.057Dibenzofuran0.057 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.052Diethyl phthalate 0.052 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.050Dimethyl phthalate 0.050 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.053Di-n-butyl phthalate 0.053 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.046Di-n-octyl phthalate 0.046 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.048Fluoranthene0.048 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.054Fluorene0.054 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.060Hexachlorobenzene0.060 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.067Hexachlorobutadiene0.067 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.067Hexachlorocyclopentadiene0.067 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.063Hexachloroethane0.063 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.043Indeno(1,2,3-cd)pyrene 0.043 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.051Isophorone0.051 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.060Naphthalene0.060 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.053Nitrobenzene0.053 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.059N-Nitroso-di-n-propylamine 0.059 UCCV
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.057N-Nitrosodiphenylamine 0.057 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.044Pentachlorophenol0.044 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.049Phenanthrene0.049 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.055Phenol0.055 U
8270D P8F019010.38 6/13/18 20:16 JMVmg/kg dry 0.050Pyrene0.050 U
Surrogate Recovery Control Limits
39-13260 %2,4,6-Tribromophenol
44-11570 %2-Fluorobiphenyl
35-11568 %2-Fluorophenol
37-12265 %Nitrobenzene-d5
34-12167 %Phenol-d5
54-12763 %Terphenyl-d14
Total Metals
7471B P8F018810.022 6/12/18 13:38 JABmg/kg dry 0.0021Mercury0.030
6020B P8F0130101.7 6/11/18 17:51 JABmg/kg dry 0.15Arsenic2.5
6020B P8F013010116/11/18 17:51 JABmg/kg dry 0.069Barium59
6020B P8F0130100.28 6/11/18 17:51 JABmg/kg dry 0.021Cadmium0.054 J
6020B P8F0130100.56 6/11/18 17:51 JABmg/kg dry 0.032Chromium13
6020B P8F0130100.28 6/11/18 17:51 JABmg/kg dry 0.064Lead16
6020B P8F0130101.1 6/11/18 17:51 JABmg/kg dry 0.23Selenium1.4
6020B P8F0130100.28 6/11/18 17:51 JABmg/kg dry 0.021Silver0.039 J
Volatile Organic Compounds by GC/MS
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000391,1,1,2-Tetrachloroethane 0.00039 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-07
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
DUPE
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000231,1,1-Trichloroethane 0.00023 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000321,1,2,2-Tetrachloroethane 0.00032 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000431,1,2-Trichloroethane 0.00043 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000131,1-Dichloroethane 0.00013 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000211,1-Dichloroethylene 0.00021 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000261,1-Dichloropropylene 0.00026 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000271,2,3-Trichlorobenzene 0.00027 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000611,2,3-Trichloropropane 0.00061 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000361,2,4-Trichlorobenzene 0.00036 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000371,2,4-Trimethylbenzene 0.00037 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000191,2-Dibromoethane 0.00019 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000231,2-Dichlorobenzene 0.00023 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000291,2-Dichloroethane 0.00029 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000301,2-Dichloropropane 0.00030 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000361,3,5-Trimethylbenzene 0.00036 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000321,3-Dichlorobenzene 0.00032 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000241,3-Dichloropropane 0.00024 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000191,4-Dichlorobenzene 0.00019 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000232,2-Dichloropropane 0.00023 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000252-Chlorotoluene 0.00025 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000294-Chlorotoluene 0.00029 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.000234-Isopropyltoluene 0.00023 U
8260B P8F025310.048 6/14/18 16:46 ANGmg/kg dry 0.0012Acetone0.063
8260B P8F025310.0029 6/14/18 16:46 ANGmg/kg dry 0.00028Benzene0.00028 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00040Bromobenzene0.00040 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00026Bromochloromethane0.00026 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00027Bromodichloromethane0.00027 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00055Bromoform0.00055 U
8260B P8F025310.0096 6/14/18 16:46 ANGmg/kg dry 0.00059Bromomethane0.00059 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00024Carbon Tetrachloride 0.00024 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00025Chlorobenzene0.00025 U
8260B P8F025310.0096 6/14/18 16:46 ANGmg/kg dry 0.00040Chloroethane0.00040 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00035Chloroform0.00035 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00032Chloromethane0.00032 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00020cis-1,2-Dichloroethylene 0.00020 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00016cis-1,3-Dichloropropylene 0.00016 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00020Dibromochloromethane0.00020 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00022Dichlorodifluoromethane0.00022 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00018Ethylbenzene0.00018 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00020Isopropyl Ether 0.00020 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00028Isopropylbenzene (Cumene)0.00028 U
8260B P8F025310.0096 6/14/18 16:46 ANGmg/kg dry 0.00044m,p-Xylenes 0.00044 U
8260B P8F025310.048 6/14/18 16:46 ANGmg/kg dry 0.00043Methyl Butyl Ketone (2-Hexanone)0.00043 U
8260B P8F025310.096 6/14/18 16:46 ANGmg/kg dry 0.00043Methyl Ethyl Ketone (2-Butanone)0.00043 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 53
Laboratory Report
06/18/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8060117-07
Prism Work Order: 8060117
Time Collected: 06/05/18 12:40
Time Submitted: 06/07/18 10:30
DUPE
8260B P8F025310.048 6/14/18 16:46 ANGmg/kg dry 0.00041Methyl Isobutyl Ketone 0.00041 U
8260B P8F025310.0096 6/14/18 16:46 ANGmg/kg dry 0.00027Methylene Chloride 0.00027 U
8260B P8F025310.0096 6/14/18 16:46 ANGmg/kg dry 0.00015Methyl-tert-Butyl Ether 0.00015 U
8260B P8F025310.0096 6/14/18 16:46 ANGmg/kg dry 0.00015Naphthalene0.00015 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00024n-Butylbenzene 0.00024 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00029n-Propylbenzene 0.00029 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00020o-Xylene 0.00020 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00023sec-Butylbenzene 0.00023 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00029Styrene0.00029 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00016tert-Butylbenzene 0.00016 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00023Tetrachloroethylene0.00023 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00028Toluene0.00028 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00029trans-1,2-Dichloroethylene 0.00029 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00025trans-1,3-Dichloropropylene 0.00025 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00031Trichloroethylene0.00031 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00031Trichlorofluoromethane0.00031 U
8260B P8F025310.024 6/14/18 16:46 ANGmg/kg dry 0.00066Vinyl acetate 0.00066 U
8260B P8F025310.0048 6/14/18 16:46 ANGmg/kg dry 0.00023Vinyl chloride 0.00023 U
8260B P8F025310.014 6/14/18 16:46 ANGmg/kg dry 0.00090Xylenes, total 0.00090 U
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123109 %Dibromofluoromethane
76-12995 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
Blank (P8F0253-BLK1)Prepared & Analyzed: 06/14/18
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
Blank (P8F0253-BLK1)Prepared & Analyzed: 06/14/18
Methylene Chloride mg/kg wetBRL0.010
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.7
ug/L 50.00 76-129Surrogate: Toluene-d8 9648.0
LCS (P8F0253-BS1)Prepared & Analyzed: 06/14/18
1,1,1,2-Tetrachloroethane mg/kg wet0.0513 0.0050 0.05000 72-115103
1,1,1-Trichloroethane mg/kg wet0.0522 0.0050 0.05000 67-131104
1,1,2,2-Tetrachloroethane mg/kg wet0.0489 0.0050 0.05000 56-12698
1,1,2-Trichloroethane mg/kg wet0.0491 0.0050 0.05000 70-13398
1,1-Dichloroethane mg/kg wet0.0514 0.0050 0.05000 74-127103
1,1-Dichloroethylene mg/kg wet0.0565 0.0050 0.05000 67-149113
1,1-Dichloropropylene mg/kg wet0.0535 0.0050 0.05000 71-130107
1,2,3-Trichlorobenzene mg/kg wet0.0490 0.0050 0.05000 68-13098
1,2,3-Trichloropropane mg/kg wet0.0481 0.0050 0.05000 60-13796
1,2,4-Trichlorobenzene mg/kg wet0.0488 0.0050 0.05000 66-12598
1,2,4-Trimethylbenzene mg/kg wet0.0521 0.0050 0.05000 69-129104
1,2-Dibromoethane mg/kg wet0.0490 0.0050 0.05000 70-13298
1,2-Dichlorobenzene mg/kg wet0.0481 0.0050 0.05000 72-12396
1,2-Dichloroethane mg/kg wet0.0504 0.0050 0.05000 68-128101
1,2-Dichloropropane mg/kg wet0.0532 0.0050 0.05000 73-130106
1,3,5-Trimethylbenzene mg/kg wet0.0507 0.0050 0.05000 69-128101
1,3-Dichlorobenzene mg/kg wet0.0486 0.0050 0.05000 71-12097
1,3-Dichloropropane mg/kg wet0.0511 0.0050 0.05000 75-124102
1,4-Dichlorobenzene mg/kg wet0.0480 0.0050 0.05000 71-12396
2,2-Dichloropropane mg/kg wet0.0543 0.0050 0.05000 50-142109
2-Chlorotoluene mg/kg wet0.0491 0.0050 0.05000 67-12498
4-Chlorotoluene mg/kg wet0.0498 0.0050 0.05000 71-126100
4-Isopropyltoluene mg/kg wet0.0523 0.0050 0.05000 68-129105
Acetone mg/kg wet0.0770 0.050 0.1000 29-19877
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
LCS (P8F0253-BS1)Prepared & Analyzed: 06/14/18
Benzene mg/kg wet0.0539 0.0030 0.05000 74-127108
Bromobenzene mg/kg wet0.0492 0.0050 0.05000 73-12598
Bromochloromethane mg/kg wet0.0511 0.0050 0.05000 72-134102
Bromodichloromethane mg/kg wet0.0532 0.0050 0.05000 75-122106
Bromoform mg/kg wet0.0518 0.0050 0.05000 66-135104
Bromomethane mg/kg wet0.0544 0.010 0.05000 20-180109
Carbon Tetrachloride mg/kg wet0.0547 0.0050 0.05000 64-143109
Chlorobenzene mg/kg wet0.0497 0.0050 0.05000 74-11899
Chloroethane mg/kg wet0.0625 0.010 0.05000 33-149125
Chloroform mg/kg wet0.0524 0.0050 0.05000 73-127105
Chloromethane mg/kg wet0.0562 0.0050 0.05000 45-143112
cis-1,2-Dichloroethylene mg/kg wet0.0527 0.0050 0.05000 76-134105
cis-1,3-Dichloropropylene mg/kg wet0.0541 0.0050 0.05000 71-125108
Dibromochloromethane mg/kg wet0.0507 0.0050 0.05000 73-122101
Dichlorodifluoromethane mg/kg wet0.0838 0.0050 0.05000 LH26-146168
Ethylbenzene mg/kg wet0.0516 0.0050 0.05000 74-128103
Isopropyl Ether mg/kg wet0.0510 0.0050 0.05000 59-159102
Isopropylbenzene (Cumene)mg/kg wet0.0519 0.0050 0.05000 68-126104
m,p-Xylenes mg/kg wet0.106 0.010 0.1000 75-124106
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0395 0.050 0.05000 J61-15779
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0406 0.10 0.05000 J63-14981
Methyl Isobutyl Ketone mg/kg wet0.0490 0.050 0.05000 J57-16298
Methylene Chloride mg/kg wet0.0514 0.010 0.05000 74-129103
Methyl-tert-Butyl Ether mg/kg wet0.0463 0.010 0.05000 70-13093
Naphthalene mg/kg wet0.0482 0.010 0.05000 57-15796
n-Butylbenzene mg/kg wet0.0528 0.0050 0.05000 65-135106
n-Propylbenzene mg/kg wet0.0512 0.0050 0.05000 67-130102
o-Xylene mg/kg wet0.0525 0.0050 0.05000 74-126105
sec-Butylbenzene mg/kg wet0.0517 0.0050 0.05000 66-131103
Styrene mg/kg wet0.0531 0.0050 0.05000 77-121106
tert-Butylbenzene mg/kg wet0.0506 0.0050 0.05000 67-132101
Tetrachloroethylene mg/kg wet0.0487 0.0050 0.05000 68-13097
Toluene mg/kg wet0.0532 0.0050 0.05000 71-129106
trans-1,2-Dichloroethylene mg/kg wet0.0536 0.0050 0.05000 73-132107
trans-1,3-Dichloropropylene mg/kg wet0.0532 0.0050 0.05000 68-123106
Trichloroethylene mg/kg wet0.0515 0.0050 0.05000 75-133103
Trichlorofluoromethane mg/kg wet0.0579 0.0050 0.05000 44-146116
Vinyl acetate mg/kg wet0.0584 0.025 0.05000 85-161117
Vinyl chloride mg/kg wet0.0681 0.0050 0.05000 48-147136
Xylenes, total mg/kg wet0.158 0.015 0.1500 74-126105
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.6
ug/L 50.00 76-129Surrogate: Toluene-d8 9848.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
LCS Dup (P8F0253-BSD1)Prepared & Analyzed: 06/14/18
1,1,1,2-Tetrachloroethane mg/kg wet0.0520 0.0050 0.05000 2072-115104 1
1,1,1-Trichloroethane mg/kg wet0.0494 0.0050 0.05000 2067-13199 6
1,1,2,2-Tetrachloroethane mg/kg wet0.0514 0.0050 0.05000 2056-126103 5
1,1,2-Trichloroethane mg/kg wet0.0510 0.0050 0.05000 2070-133102 4
1,1-Dichloroethane mg/kg wet0.0499 0.0050 0.05000 2074-127100 3
1,1-Dichloroethylene mg/kg wet0.0553 0.0050 0.05000 2067-149111 2
1,1-Dichloropropylene mg/kg wet0.0514 0.0050 0.05000 2071-130103 4
1,2,3-Trichlorobenzene mg/kg wet0.0493 0.0050 0.05000 2068-13099 0.5
1,2,3-Trichloropropane mg/kg wet0.0506 0.0050 0.05000 2060-137101 5
1,2,4-Trichlorobenzene mg/kg wet0.0490 0.0050 0.05000 2066-12598 0.4
1,2,4-Trimethylbenzene mg/kg wet0.0510 0.0050 0.05000 2069-129102 2
1,2-Dibromoethane mg/kg wet0.0508 0.0050 0.05000 2070-132102 4
1,2-Dichlorobenzene mg/kg wet0.0486 0.0050 0.05000 2072-12397 1
1,2-Dichloroethane mg/kg wet0.0508 0.0050 0.05000 2068-128102 0.9
1,2-Dichloropropane mg/kg wet0.0516 0.0050 0.05000 2073-130103 3
1,3,5-Trimethylbenzene mg/kg wet0.0499 0.0050 0.05000 2069-128100 2
1,3-Dichlorobenzene mg/kg wet0.0474 0.0050 0.05000 2071-12095 2
1,3-Dichloropropane mg/kg wet0.0520 0.0050 0.05000 2075-124104 2
1,4-Dichlorobenzene mg/kg wet0.0477 0.0050 0.05000 2071-12395 0.5
2,2-Dichloropropane mg/kg wet0.0508 0.0050 0.05000 2050-142102 7
2-Chlorotoluene mg/kg wet0.0482 0.0050 0.05000 2067-12496 2
4-Chlorotoluene mg/kg wet0.0489 0.0050 0.05000 2071-12698 2
4-Isopropyltoluene mg/kg wet0.0507 0.0050 0.05000 2068-129101 3
Acetone mg/kg wet0.0779 0.050 0.1000 2029-19878 1
Benzene mg/kg wet0.0522 0.0030 0.05000 2074-127104 3
Bromobenzene mg/kg wet0.0486 0.0050 0.05000 2073-12597 1
Bromochloromethane mg/kg wet0.0508 0.0050 0.05000 2072-134102 0.7
Bromodichloromethane mg/kg wet0.0524 0.0050 0.05000 2075-122105 2
Bromoform mg/kg wet0.0547 0.0050 0.05000 2066-135109 6
Bromomethane mg/kg wet0.0528 0.010 0.05000 2020-180106 3
Carbon Tetrachloride mg/kg wet0.0517 0.0050 0.05000 2064-143103 6
Chlorobenzene mg/kg wet0.0494 0.0050 0.05000 2074-11899 0.6
Chloroethane mg/kg wet0.0577 0.010 0.05000 2033-149115 8
Chloroform mg/kg wet0.0509 0.0050 0.05000 2073-127102 3
Chloromethane mg/kg wet0.0481 0.0050 0.05000 2045-14396 16
cis-1,2-Dichloroethylene mg/kg wet0.0507 0.0050 0.05000 2076-134101 4
cis-1,3-Dichloropropylene mg/kg wet0.0534 0.0050 0.05000 2071-125107 1
Dibromochloromethane mg/kg wet0.0524 0.0050 0.05000 2073-122105 3
Dichlorodifluoromethane mg/kg wet0.0814 0.0050 0.05000 20 LH26-146163 3
Ethylbenzene mg/kg wet0.0510 0.0050 0.05000 2074-128102 1
Isopropyl Ether mg/kg wet0.0508 0.0050 0.05000 2059-159102 0.5
Isopropylbenzene (Cumene)mg/kg wet0.0508 0.0050 0.05000 2068-126102 2
m,p-Xylenes mg/kg wet0.104 0.010 0.1000 2075-124104 2
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0434 0.050 0.05000 20 J61-15787 9
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0429 0.10 0.05000 20 J63-14986 5
Methyl Isobutyl Ketone mg/kg wet0.0528 0.050 0.05000 2057-162106 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
LCS Dup (P8F0253-BSD1)Prepared & Analyzed: 06/14/18
Methylene Chloride mg/kg wet0.0511 0.010 0.05000 2074-129102 0.6
Methyl-tert-Butyl Ether mg/kg wet0.0456 0.010 0.05000 2070-13091 1
Naphthalene mg/kg wet0.0512 0.010 0.05000 2057-157102 6
n-Butylbenzene mg/kg wet0.0517 0.0050 0.05000 2065-135103 2
n-Propylbenzene mg/kg wet0.0498 0.0050 0.05000 2067-130100 3
o-Xylene mg/kg wet0.0524 0.0050 0.05000 2074-126105 0.2
sec-Butylbenzene mg/kg wet0.0504 0.0050 0.05000 2066-131101 3
Styrene mg/kg wet0.0528 0.0050 0.05000 2077-121106 0.5
tert-Butylbenzene mg/kg wet0.0498 0.0050 0.05000 2067-132100 2
Tetrachloroethylene mg/kg wet0.0474 0.0050 0.05000 2068-13095 3
Toluene mg/kg wet0.0518 0.0050 0.05000 2071-129104 3
trans-1,2-Dichloroethylene mg/kg wet0.0521 0.0050 0.05000 2073-132104 3
trans-1,3-Dichloropropylene mg/kg wet0.0533 0.0050 0.05000 2068-123107 0.2
Trichloroethylene mg/kg wet0.0501 0.0050 0.05000 2075-133100 3
Trichlorofluoromethane mg/kg wet0.0566 0.0050 0.05000 2044-146113 2
Vinyl acetate mg/kg wet0.0582 0.025 0.05000 2085-161116 0.3
Vinyl chloride mg/kg wet0.0646 0.0050 0.05000 2048-147129 5
Xylenes, total mg/kg wet0.156 0.015 0.1500 2074-126104 1
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.3
ug/L 50.00 76-129Surrogate: Toluene-d8 9848.8
Matrix Spike (P8F0253-MS1)Prepared & Analyzed: 06/14/18 Source: 8060117-01
1,1,1,2-Tetrachloroethane mg/kg dry0.0266 0.0057 0.05711 BRL M60-12047
1,1,1-Trichloroethane mg/kg dry0.0366 0.0057 0.05711 BRL 52-13964
1,1,2,2-Tetrachloroethane mg/kg dry0.0212 0.0057 0.05711 BRL M39-13537
1,1,2-Trichloroethane mg/kg dry0.0287 0.0057 0.05711 BRL 44-14050
1,1-Dichloroethane mg/kg dry0.0374 0.0057 0.05711 BRL 59-13766
1,1-Dichloroethylene mg/kg dry0.0433 0.0057 0.05711 BRL 54-16276
1,1-Dichloropropylene mg/kg dry0.0364 0.0057 0.05711 BRL 55-13764
1,2,3-Trichlorobenzene mg/kg dry0.00639 0.0057 0.05711 BRL M34-12011
1,2,3-Trichloropropane mg/kg dry0.0234 0.0057 0.05711 BRL M45-13941
1,2,4-Trichlorobenzene mg/kg dry0.00693 0.0057 0.05711 BRL M35-11612
1,2,4-Trimethylbenzene mg/kg dry0.0193 0.0057 0.05711 BRL M38-14234
1,2-Dibromoethane mg/kg dry0.0256 0.0057 0.05711 BRL M49-13245
1,2-Dichlorobenzene mg/kg dry0.0137 0.0057 0.05711 BRL M42-13024
1,2-Dichloroethane mg/kg dry0.0331 0.0057 0.05711 BRL 51-13158
1,2-Dichloropropane mg/kg dry0.0349 0.0057 0.05711 BRL 55-13861
1,3,5-Trimethylbenzene mg/kg dry0.0202 0.0057 0.05711 BRL M44-14035
1,3-Dichlorobenzene mg/kg dry0.0149 0.0057 0.05711 BRL M41-12926
1,3-Dichloropropane mg/kg dry0.0300 0.0057 0.05711 BRL 53-12953
1,4-Dichlorobenzene mg/kg dry0.0146 0.0057 0.05711 BRL M44-13426
2,2-Dichloropropane mg/kg dry0.0378 0.0057 0.05711 BRL 30-14766
2-Chlorotoluene mg/kg dry0.0195 0.0057 0.05711 BRL M46-13234
4-Chlorotoluene mg/kg dry0.0177 0.0057 0.05711 BRL M44-13531
4-Isopropyltoluene mg/kg dry0.0164 0.0057 0.05711 BRL M32-14429
Acetone mg/kg dry0.0532 0.057 0.1142 0.0990 M, J34-143NR
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
Matrix Spike (P8F0253-MS1)Prepared & Analyzed: 06/14/18 Source: 8060117-01
Benzene mg/kg dry0.0383 0.0034 0.05711 BRL 60-13567
Bromobenzene mg/kg dry0.0196 0.0057 0.05711 BRL M45-13534
Bromochloromethane mg/kg dry0.0352 0.0057 0.05711 BRL 55-13662
Bromodichloromethane mg/kg dry0.0323 0.0057 0.05711 BRL 55-12757
Bromoform mg/kg dry0.0201 0.0057 0.05711 BRL M40-13635
Bromomethane mg/kg dry0.0268 0.011 0.05711 BRL 30-13747
Carbon Tetrachloride mg/kg dry0.0352 0.0057 0.05711 BRL 48-15362
Chlorobenzene mg/kg dry0.0253 0.0057 0.05711 BRL M57-12544
Chloroethane mg/kg dry0.0459 0.011 0.05711 BRL 16-17780
Chloroform mg/kg dry0.0360 0.0057 0.05711 BRL 56-13763
Chloromethane mg/kg dry0.0398 0.0057 0.05711 BRL 40-14570
cis-1,2-Dichloroethylene mg/kg dry0.0366 0.0057 0.05711 BRL 58-14064
cis-1,3-Dichloropropylene mg/kg dry0.0218 0.0057 0.05711 BRL M42-13538
Dibromochloromethane mg/kg dry0.0253 0.0057 0.05711 BRL M49-12744
Dichlorodifluoromethane mg/kg dry0.0650 0.0057 0.05711 BRL 25-151114
Ethylbenzene mg/kg dry0.0275 0.0057 0.05711 BRL 44-14448
Isopropyl Ether mg/kg dry0.0341 0.0057 0.05711 BRL 51-15560
Isopropylbenzene (Cumene)mg/kg dry0.0242 0.0057 0.05711 BRL 41-14042
m,p-Xylenes mg/kg dry0.0542 0.011 0.1142 BRL 36-14847
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.00832 0.057 0.05711 BRL M, J30-14715
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0211 0.11 0.05711 BRL J24-16037
Methyl Isobutyl Ketone mg/kg dry0.0135 0.057 0.05711 BRL M, J25-16324
Methylene Chloride mg/kg dry0.0384 0.011 0.05711 BRL 53-14467
Methyl-tert-Butyl Ether mg/kg dry0.0321 0.011 0.05711 BRL 49-13556
Naphthalene mg/kg dry0.00666 0.011 0.05711 BRL M, J32-12712
n-Butylbenzene mg/kg dry0.0155 0.0057 0.05711 BRL 23-14827
n-Propylbenzene mg/kg dry0.0216 0.0057 0.05711 BRL 35-14438
o-Xylene mg/kg dry0.0254 0.0057 0.05711 BRL 43-14344
sec-Butylbenzene mg/kg dry0.0197 0.0057 0.05711 BRL 34-14435
Styrene mg/kg dry0.0167 0.0057 0.05711 BRL M42-13229
tert-Butylbenzene mg/kg dry0.0208 0.0057 0.05711 BRL 36-15036
Tetrachloroethylene mg/kg dry0.0275 0.0057 0.05711 BRL 47-14248
Toluene mg/kg dry0.0330 0.0057 0.05711 BRL 57-13558
trans-1,2-Dichloroethylene mg/kg dry0.0410 0.0057 0.05711 BRL 58-14172
trans-1,3-Dichloropropylene mg/kg dry0.0232 0.0057 0.05711 BRL 41-12441
Trichloroethylene mg/kg dry0.0351 0.0057 0.05711 BRL 38-16461
Trichlorofluoromethane mg/kg dry0.0410 0.0057 0.05711 BRL 30-15772
Vinyl acetate mg/kg dryBRL0.029 0.05711 BRL M61-154
Vinyl chloride mg/kg dry0.0539 0.0057 0.05711 BRL 40-15694
Xylenes, total mg/kg dry0.0796 0.017 0.1713 BRL 36-14846
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10050.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9748.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
Matrix Spike Dup (P8F0253-MSD1)Prepared & Analyzed: 06/14/18 Source: 8060117-01
1,1,1,2-Tetrachloroethane mg/kg dry0.0285 0.0058 0.05830 BRL 15 M60-12049 7
1,1,1-Trichloroethane mg/kg dry0.0378 0.0058 0.05830 BRL 2152-13965 3
1,1,2,2-Tetrachloroethane mg/kg dry0.0239 0.0058 0.05830 BRL 2239-13541 12
1,1,2-Trichloroethane mg/kg dry0.0302 0.0058 0.05830 BRL 2144-14052 5
1,1-Dichloroethane mg/kg dry0.0389 0.0058 0.05830 BRL 2159-13767 4
1,1-Dichloroethylene mg/kg dry0.0447 0.0058 0.05830 BRL 2254-16277 3
1,1-Dichloropropylene mg/kg dry0.0387 0.0058 0.05830 BRL 1955-13766 6
1,2,3-Trichlorobenzene mg/kg dry0.00728 0.0058 0.05830 BRL 41 M34-12012 13
1,2,3-Trichloropropane mg/kg dry0.0264 0.0058 0.05830 BRL 2545-13945 12
1,2,4-Trichlorobenzene mg/kg dry0.00812 0.0058 0.05830 BRL 62 M35-11614 16
1,2,4-Trimethylbenzene mg/kg dry0.0211 0.0058 0.05830 BRL 24 M38-14236 9
1,2-Dibromoethane mg/kg dry0.0283 0.0058 0.05830 BRL 1549-13249 10
1,2-Dichlorobenzene mg/kg dry0.0155 0.0058 0.05830 BRL 21 M42-13027 12
1,2-Dichloroethane mg/kg dry0.0341 0.0058 0.05830 BRL 1351-13158 3
1,2-Dichloropropane mg/kg dry0.0360 0.0058 0.05830 BRL 1655-13862 3
1,3,5-Trimethylbenzene mg/kg dry0.0220 0.0058 0.05830 BRL 29 M44-14038 9
1,3-Dichlorobenzene mg/kg dry0.0166 0.0058 0.05830 BRL 24 M41-12929 11
1,3-Dichloropropane mg/kg dry0.0316 0.0058 0.05830 BRL 1553-12954 5
1,4-Dichlorobenzene mg/kg dry0.0166 0.0058 0.05830 BRL 21 M44-13428 13
2,2-Dichloropropane mg/kg dry0.0396 0.0058 0.05830 BRL 2030-14768 5
2-Chlorotoluene mg/kg dry0.0214 0.0058 0.05830 BRL 29 M46-13237 9
4-Chlorotoluene mg/kg dry0.0203 0.0058 0.05830 BRL 23 M44-13535 13
4-Isopropyltoluene mg/kg dry0.0184 0.0058 0.05830 BRL 2232-14432 12
Acetone mg/kg dry0.0523 0.058 0.1166 0.0990 49 M, J34-143NR 2
Benzene mg/kg dry0.0390 0.0035 0.05830 BRL 2060-13567 2
Bromobenzene mg/kg dry0.0222 0.0058 0.05830 BRL 25 M45-13538 12
Bromochloromethane mg/kg dry0.0364 0.0058 0.05830 BRL 1855-13662 3
Bromodichloromethane mg/kg dry0.0336 0.0058 0.05830 BRL 1755-12758 4
Bromoform mg/kg dry0.0235 0.0058 0.05830 BRL 3540-13640 16
Bromomethane mg/kg dry0.0320 0.012 0.05830 BRL 3030-13755 18
Carbon Tetrachloride mg/kg dry0.0373 0.0058 0.05830 BRL 2348-15364 6
Chlorobenzene mg/kg dry0.0277 0.0058 0.05830 BRL 14 M57-12548 9
Chloroethane mg/kg dry0.0449 0.012 0.05830 BRL 4716-17777 2
Chloroform mg/kg dry0.0373 0.0058 0.05830 BRL 1856-13764 4
Chloromethane mg/kg dry0.0410 0.0058 0.05830 BRL 2640-14570 3
cis-1,2-Dichloroethylene mg/kg dry0.0372 0.0058 0.05830 BRL 2858-14064 2
cis-1,3-Dichloropropylene mg/kg dry0.0248 0.0058 0.05830 BRL 3242-13543 13
Dibromochloromethane mg/kg dry0.0275 0.0058 0.05830 BRL 24 M49-12747 9
Dichlorodifluoromethane mg/kg dry0.0652 0.0058 0.05830 BRL 3725-151112 0.4
Ethylbenzene mg/kg dry0.0297 0.0058 0.05830 BRL 1944-14451 8
Isopropyl Ether mg/kg dry0.0345 0.0058 0.05830 BRL 1351-15559 1
Isopropylbenzene (Cumene)mg/kg dry0.0260 0.0058 0.05830 BRL 2741-14045 7
m,p-Xylenes mg/kg dry0.0581 0.012 0.1166 BRL 2036-14850 7
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.00998 0.058 0.05830 BRL 42 M, J30-14717 18
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0233 0.12 0.05830 BRL 42 J24-16040 10
Methyl Isobutyl Ketone mg/kg dry0.0169 0.058 0.05830 BRL 44 J25-16329 22
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8F0253 - 5035
Matrix Spike Dup (P8F0253-MSD1)Prepared & Analyzed: 06/14/18 Source: 8060117-01
Methylene Chloride mg/kg dry0.0394 0.012 0.05830 BRL 1453-14468 3
Methyl-tert-Butyl Ether mg/kg dry0.0316 0.012 0.05830 BRL 2249-13554 2
Naphthalene mg/kg dry0.00830 0.012 0.05830 BRL 44 M, J32-12714 22
n-Butylbenzene mg/kg dry0.0171 0.0058 0.05830 BRL 3923-14829 10
n-Propylbenzene mg/kg dry0.0235 0.0058 0.05830 BRL 2735-14440 8
o-Xylene mg/kg dry0.0274 0.0058 0.05830 BRL 1743-14347 8
sec-Butylbenzene mg/kg dry0.0212 0.0058 0.05830 BRL 2834-14436 7
Styrene mg/kg dry0.0196 0.0058 0.05830 BRL 28 M42-13234 16
tert-Butylbenzene mg/kg dry0.0224 0.0058 0.05830 BRL 2936-15038 7
Tetrachloroethylene mg/kg dry0.0303 0.0058 0.05830 BRL 2647-14252 10
Toluene mg/kg dry0.0350 0.0058 0.05830 BRL 2257-13560 6
trans-1,2-Dichloroethylene mg/kg dry0.0410 0.0058 0.05830 BRL 1858-14170 0.03
trans-1,3-Dichloropropylene mg/kg dry0.0266 0.0058 0.05830 BRL 2041-12446 14
Trichloroethylene mg/kg dry0.0368 0.0058 0.05830 BRL 1838-16463 5
Trichlorofluoromethane mg/kg dry0.0425 0.0058 0.05830 BRL 2730-15773 4
Vinyl acetate mg/kg dryBRL0.029 0.05830 BRL 35 M61-154
Vinyl chloride mg/kg dry0.0545 0.0058 0.05830 BRL 3540-15694 1
Xylenes, total mg/kg dry0.0855 0.017 0.1749 BRL 2036-14849 7
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.2
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.5
ug/L 50.00 76-129Surrogate: Toluene-d8 9647.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
Blank (P8F0190-BLK1)Prepared: 06/12/18 Analyzed: 06/13/18
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
Blank (P8F0190-BLK1)Prepared: 06/12/18 Analyzed: 06/13/18
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 792.65
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 851.42
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 842.80
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 781.30
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 842.79
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 831.39
LCS (P8F0190-BS1)Prepared: 06/12/18 Analyzed: 06/13/18
1,2,4-Trichlorobenzene mg/kg wet1.14 0.33 1.667 34-11869
1,2-Dichlorobenzene mg/kg wet1.09 0.33 1.667 33-11766
1,3-Dichlorobenzene mg/kg wet1.05 0.33 1.667 30-11563
1,4-Dichlorobenzene mg/kg wet1.08 0.33 1.667 31-11565
1-Methylnaphthalene mg/kg wet1.30 0.33 1.667 40-11978
2,4,6-Trichlorophenol mg/kg wet1.34 0.33 1.667 39-12681
2,4-Dichlorophenol mg/kg wet1.27 0.33 1.667 40-12276
2,4-Dimethylphenol mg/kg wet1.72 0.33 1.667 30-127103
2,4-Dinitrophenol mg/kg wet1.06 0.33 1.667 27-12964
2,4-Dinitrotoluene mg/kg wet1.38 0.33 1.667 48-12683
2,6-Dinitrotoluene mg/kg wet1.38 0.33 1.667 46-12483
2-Chloronaphthalene mg/kg wet1.27 0.33 1.667 41-11476
2-Chlorophenol mg/kg wet1.26 0.33 1.667 34-12176
2-Methylnaphthalene mg/kg wet1.26 0.33 1.667 38-12275
2-Methylphenol mg/kg wet1.35 0.33 1.667 32-12281
2-Nitrophenol mg/kg wet1.16 0.33 1.667 36-12370
3,3’-Dichlorobenzidine mg/kg wet1.29 0.33 1.667 22-12178
3/4-Methylphenol mg/kg wet1.24 0.33 1.667 34-11974
4,6-Dinitro-2-methylphenol mg/kg wet1.16 0.33 1.667 29-13269
4-Bromophenyl phenyl ether mg/kg wet1.29 0.33 1.667 46-12477
4-Chloro-3-methylphenol mg/kg wet1.31 0.33 1.667 45-12279
4-Chloroaniline mg/kg wet1.39 0.33 1.667 17-10683
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
LCS (P8F0190-BS1)Prepared: 06/12/18 Analyzed: 06/13/18
4-Chlorophenyl phenyl ether mg/kg wet1.30 0.33 1.667 45-12178
4-Nitrophenol mg/kg wet1.25 0.33 1.667 30-13275
Acenaphthene mg/kg wet1.32 0.33 1.667 40-12379
Acenaphthylene mg/kg wet1.37 0.33 1.667 32-13282
Anthracene mg/kg wet1.47 0.33 1.667 47-12388
Azobenzene mg/kg wet1.39 0.33 1.667 39-12584
Benzo(a)anthracene mg/kg wet1.38 0.33 1.667 49-12683
Benzo(a)pyrene mg/kg wet1.45 0.33 1.667 45-12987
Benzo(b)fluoranthene mg/kg wet1.46 0.33 1.667 45-13287
Benzo(g,h,i)perylene mg/kg wet1.47 0.33 1.667 43-13488
Benzo(k)fluoranthene mg/kg wet1.35 0.33 1.667 47-13281
Benzoic Acid mg/kg wet0.513 0.33 1.667 10-8331
Benzyl alcohol mg/kg wet1.30 0.33 1.667 29-12278
bis(2-Chloroethoxy)methane mg/kg wet1.31 0.33 1.667 36-12179
Bis(2-Chloroethyl)ether mg/kg wet1.03 0.33 1.667 31-12062
Bis(2-chloroisopropyl)ether mg/kg wet1.17 0.33 1.667 33-13170
Bis(2-Ethylhexyl)phthalate mg/kg wet1.35 0.33 1.667 51-13381
Butyl benzyl phthalate mg/kg wet1.36 0.33 1.667 48-13282
Chrysene mg/kg wet1.38 0.33 1.667 50-12483
Dibenzo(a,h)anthracene mg/kg wet1.34 0.33 1.667 45-13480
Dibenzofuran mg/kg wet1.38 0.33 1.667 44-12083
Diethyl phthalate mg/kg wet1.32 0.33 1.667 50-12479
Dimethyl phthalate mg/kg wet1.33 0.33 1.667 48-12480
Di-n-butyl phthalate mg/kg wet1.37 0.33 1.667 51-12882
Di-n-octyl phthalate mg/kg wet1.54 0.33 1.667 45-14093
Fluoranthene mg/kg wet1.39 0.33 1.667 50-12783
Fluorene mg/kg wet1.39 0.33 1.667 43-12583
Hexachlorobenzene mg/kg wet1.31 0.33 1.667 45-12279
Hexachlorobutadiene mg/kg wet1.14 0.33 1.667 32-12368
Hexachlorocyclopentadiene mg/kg wet0.852 0.33 1.667 32-11751
Hexachloroethane mg/kg wet1.04 0.33 1.667 28-11762
Indeno(1,2,3-cd)pyrene mg/kg wet1.68 0.33 1.667 45-133100
Isophorone mg/kg wet1.30 0.33 1.667 30-12278
Naphthalene mg/kg wet1.21 0.33 1.667 35-12372
Nitrobenzene mg/kg wet1.16 0.33 1.667 34-12269
N-Nitroso-di-n-propylamine mg/kg wet1.31 0.33 1.667 36-12079
N-Nitrosodiphenylamine mg/kg wet1.70 0.33 1.667 38-127102
Pentachlorophenol mg/kg wet1.38 0.33 1.667 25-13383
Phenanthrene mg/kg wet1.43 0.33 1.667 50-12186
Phenol mg/kg wet1.29 0.33 1.667 34-12177
Pyrene mg/kg wet1.38 0.33 1.667 47-12783
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 712.38
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 751.25
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 722.41
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 671.12
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 712.37
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
LCS (P8F0190-BS1)Prepared: 06/12/18 Analyzed: 06/13/18
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 721.20
LCS Dup (P8F0190-BSD1)Prepared: 06/12/18 Analyzed: 06/13/18
1,2,4-Trichlorobenzene mg/kg wet1.20 0.33 1.667 2034-11872 5
1,2-Dichlorobenzene mg/kg wet1.13 0.33 1.667 2033-11768 3
1,3-Dichlorobenzene mg/kg wet1.09 0.33 1.667 2030-11566 4
1,4-Dichlorobenzene mg/kg wet1.10 0.33 1.667 2031-11566 3
1-Methylnaphthalene mg/kg wet1.30 0.33 1.667 2040-11978 0.08
2,4,6-Trichlorophenol mg/kg wet1.35 0.33 1.667 2039-12681 0.7
2,4-Dichlorophenol mg/kg wet1.31 0.33 1.667 2040-12278 3
2,4-Dimethylphenol mg/kg wet1.72 0.33 1.667 2030-127103 0.08
2,4-Dinitrophenol mg/kg wet1.05 0.33 1.667 2027-12963 1
2,4-Dinitrotoluene mg/kg wet1.41 0.33 1.667 2048-12685 2
2,6-Dinitrotoluene mg/kg wet1.41 0.33 1.667 2046-12485 2
2-Chloronaphthalene mg/kg wet1.31 0.33 1.667 2041-11478 3
2-Chlorophenol mg/kg wet1.29 0.33 1.667 2034-12177 2
2-Methylnaphthalene mg/kg wet1.29 0.33 1.667 2038-12277 2
2-Methylphenol mg/kg wet1.40 0.33 1.667 2032-12284 3
2-Nitrophenol mg/kg wet1.20 0.33 1.667 2036-12372 3
3,3’-Dichlorobenzidine mg/kg wet1.30 0.33 1.667 2022-12178 0.6
3/4-Methylphenol mg/kg wet1.27 0.33 1.667 2034-11976 3
4,6-Dinitro-2-methylphenol mg/kg wet1.12 0.33 1.667 2029-13267 3
4-Bromophenyl phenyl ether mg/kg wet1.27 0.33 1.667 2046-12476 1
4-Chloro-3-methylphenol mg/kg wet1.32 0.33 1.667 2045-12279 1
4-Chloroaniline mg/kg wet1.41 0.33 1.667 2017-10685 2
4-Chlorophenyl phenyl ether mg/kg wet1.31 0.33 1.667 2045-12178 0.2
4-Nitrophenol mg/kg wet1.42 0.33 1.667 2030-13285 13
Acenaphthene mg/kg wet1.35 0.33 1.667 2040-12381 2
Acenaphthylene mg/kg wet1.39 0.33 1.667 2032-13284 2
Anthracene mg/kg wet1.44 0.33 1.667 2047-12387 2
Azobenzene mg/kg wet1.36 0.33 1.667 2039-12581 3
Benzo(a)anthracene mg/kg wet1.39 0.33 1.667 2049-12683 0.4
Benzo(a)pyrene mg/kg wet1.46 0.33 1.667 2045-12987 0.2
Benzo(b)fluoranthene mg/kg wet1.45 0.33 1.667 2045-13287 0.3
Benzo(g,h,i)perylene mg/kg wet1.43 0.33 1.667 2043-13486 3
Benzo(k)fluoranthene mg/kg wet1.35 0.33 1.667 2047-13281 0.6
Benzoic Acid mg/kg wet0.468 0.33 1.667 2010-8328 9
Benzyl alcohol mg/kg wet1.28 0.33 1.667 2029-12277 2
bis(2-Chloroethoxy)methane mg/kg wet1.34 0.33 1.667 2036-12180 2
Bis(2-Chloroethyl)ether mg/kg wet1.02 0.33 1.667 2031-12061 0.5
Bis(2-chloroisopropyl)ether mg/kg wet1.20 0.33 1.667 2033-13172 2
Bis(2-Ethylhexyl)phthalate mg/kg wet1.38 0.33 1.667 2051-13383 2
Butyl benzyl phthalate mg/kg wet1.40 0.33 1.667 2048-13284 3
Chrysene mg/kg wet1.38 0.33 1.667 2050-12483 0.2
Dibenzo(a,h)anthracene mg/kg wet1.31 0.33 1.667 2045-13479 2
Dibenzofuran mg/kg wet1.40 0.33 1.667 2044-12084 2
Diethyl phthalate mg/kg wet1.34 0.33 1.667 2050-12480 1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
LCS Dup (P8F0190-BSD1)Prepared: 06/12/18 Analyzed: 06/13/18
Dimethyl phthalate mg/kg wet1.32 0.33 1.667 2048-12479 0.4
Di-n-butyl phthalate mg/kg wet1.38 0.33 1.667 2051-12883 0.4
Di-n-octyl phthalate mg/kg wet1.52 0.33 1.667 2045-14091 2
Fluoranthene mg/kg wet1.36 0.33 1.667 2050-12782 2
Fluorene mg/kg wet1.41 0.33 1.667 2043-12585 2
Hexachlorobenzene mg/kg wet1.31 0.33 1.667 2045-12279 0.03
Hexachlorobutadiene mg/kg wet1.17 0.33 1.667 2032-12370 3
Hexachlorocyclopentadiene mg/kg wet0.862 0.33 1.667 2032-11752 1
Hexachloroethane mg/kg wet1.08 0.33 1.667 2028-11765 4
Indeno(1,2,3-cd)pyrene mg/kg wet1.64 0.33 1.667 2045-13398 2
Isophorone mg/kg wet1.32 0.33 1.667 2030-12279 2
Naphthalene mg/kg wet1.25 0.33 1.667 2035-12375 4
Nitrobenzene mg/kg wet1.18 0.33 1.667 2034-12271 2
N-Nitroso-di-n-propylamine mg/kg wet1.32 0.33 1.667 2036-12079 0.7
N-Nitrosodiphenylamine mg/kg wet1.66 0.33 1.667 2038-12799 2
Pentachlorophenol mg/kg wet1.30 0.33 1.667 2025-13378 6
Phenanthrene mg/kg wet1.41 0.33 1.667 2050-12185 1
Phenol mg/kg wet1.33 0.33 1.667 2034-12180 3
Pyrene mg/kg wet1.39 0.33 1.667 2047-12783 0.7
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 722.39
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 771.28
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 752.49
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 691.15
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 742.45
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 731.21
Matrix Spike (P8F0190-MS1)Prepared: 06/12/18 Analyzed: 06/13/18 Source: 8060117-04
1,2,4-Trichlorobenzene mg/kg dry1.43 0.40 2.028 BRL 34-11870
1,2-Dichlorobenzene mg/kg dry1.35 0.40 2.028 BRL 33-11766
1,3-Dichlorobenzene mg/kg dry1.26 0.40 2.028 BRL 30-11562
1,4-Dichlorobenzene mg/kg dry1.30 0.40 2.028 BRL 31-11564
1-Methylnaphthalene mg/kg dry1.57 0.40 2.028 BRL 40-11977
2,4,6-Trichlorophenol mg/kg dry1.59 0.40 2.028 BRL 39-12678
2,4-Dichlorophenol mg/kg dry1.52 0.40 2.028 BRL 40-12275
2,4-Dimethylphenol mg/kg dry1.99 0.40 2.028 BRL 30-12798
2,4-Dinitrophenol mg/kg dry0.607 0.40 2.028 BRL 27-12930
2,4-Dinitrotoluene mg/kg dry1.40 0.40 2.028 BRL 48-12669
2,6-Dinitrotoluene mg/kg dry1.40 0.40 2.028 BRL 46-12469
2-Chloronaphthalene mg/kg dry1.52 0.40 2.028 BRL 41-11475
2-Chlorophenol mg/kg dry1.53 0.40 2.028 BRL 34-12175
2-Methylnaphthalene mg/kg dry1.53 0.40 2.028 BRL 38-12276
2-Methylphenol mg/kg dry1.62 0.40 2.028 BRL 32-12280
2-Nitrophenol mg/kg dry1.33 0.40 2.028 BRL 36-12365
3,3’-Dichlorobenzidine mg/kg dryBRL0.40 2.028 BRL M22-121
3/4-Methylphenol mg/kg dry1.47 0.40 2.028 BRL 34-11972
4,6-Dinitro-2-methylphenol mg/kg dry0.490 0.40 2.028 BRL M29-13224
4-Bromophenyl phenyl ether mg/kg dry1.51 0.40 2.028 BRL 46-12474
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
Matrix Spike (P8F0190-MS1)Prepared: 06/12/18 Analyzed: 06/13/18 Source: 8060117-04
4-Chloro-3-methylphenol mg/kg dry1.52 0.40 2.028 BRL 45-12275
4-Chloroaniline mg/kg dryBRL0.40 2.028 BRL M17-106
4-Chlorophenyl phenyl ether mg/kg dry1.49 0.40 2.028 BRL 45-12173
4-Nitrophenol mg/kg dry1.65 0.40 2.028 BRL 30-13281
Acenaphthene mg/kg dry1.55 0.40 2.028 BRL 40-12377
Acenaphthylene mg/kg dry1.57 0.40 2.028 BRL 32-13277
Anthracene mg/kg dry1.70 0.40 2.028 BRL 47-12384
Azobenzene mg/kg dry1.53 0.40 2.028 BRL 39-12575
Benzo(a)anthracene mg/kg dry1.59 0.40 2.028 BRL 49-12679
Benzo(a)pyrene mg/kg dry1.67 0.40 2.028 BRL 45-12982
Benzo(b)fluoranthene mg/kg dry1.71 0.40 2.028 BRL 45-13284
Benzo(g,h,i)perylene mg/kg dry1.68 0.40 2.028 BRL 43-13483
Benzo(k)fluoranthene mg/kg dry1.63 0.40 2.028 BRL 47-13280
Benzoic Acid mg/kg dry1.99 0.40 2.028 0.239 M10-8387
Benzyl alcohol mg/kg dry1.54 0.40 2.028 BRL 29-12276
bis(2-Chloroethoxy)methane mg/kg dry1.51 0.40 2.028 BRL 36-12174
Bis(2-Chloroethyl)ether mg/kg dry1.46 0.40 2.028 BRL 31-12072
Bis(2-chloroisopropyl)ether mg/kg dry1.48 0.40 2.028 BRL 33-13173
Bis(2-Ethylhexyl)phthalate mg/kg dry1.60 0.40 2.028 BRL 51-13379
Butyl benzyl phthalate mg/kg dry1.59 0.40 2.028 BRL 48-13278
Chrysene mg/kg dry1.60 0.40 2.028 BRL 50-12479
Dibenzo(a,h)anthracene mg/kg dry1.54 0.40 2.028 BRL 45-13476
Dibenzofuran mg/kg dry1.63 0.40 2.028 BRL 44-12080
Diethyl phthalate mg/kg dry1.49 0.40 2.028 BRL 50-12473
Dimethyl phthalate mg/kg dry1.50 0.40 2.028 BRL 48-12474
Di-n-butyl phthalate mg/kg dry1.58 0.40 2.028 BRL 51-12878
Di-n-octyl phthalate mg/kg dry1.82 0.40 2.028 BRL 45-14090
Fluoranthene mg/kg dry1.61 0.40 2.028 BRL 50-12780
Fluorene mg/kg dry1.63 0.40 2.028 BRL 43-12580
Hexachlorobenzene mg/kg dry1.52 0.40 2.028 BRL 45-12275
Hexachlorobutadiene mg/kg dry1.42 0.40 2.028 BRL 32-12370
Hexachlorocyclopentadiene mg/kg dryBRL0.40 2.028 BRL M32-117
Hexachloroethane mg/kg dry0.905 0.40 2.028 BRL 28-11745
Indeno(1,2,3-cd)pyrene mg/kg dry1.93 0.40 2.028 BRL 45-13395
Isophorone mg/kg dry1.55 0.40 2.028 BRL 30-12276
Naphthalene mg/kg dry1.53 0.40 2.028 BRL 35-12376
Nitrobenzene mg/kg dry1.41 0.40 2.028 BRL 34-12269
N-Nitroso-di-n-propylamine mg/kg dry1.55 0.40 2.028 BRL 36-12076
N-Nitrosodiphenylamine mg/kg dry1.84 0.40 2.028 BRL 38-12791
Pentachlorophenol mg/kg dry2.02 0.40 2.028 BRL 25-13399
Phenanthrene mg/kg dry1.68 0.40 2.028 BRL 50-12183
Phenol mg/kg dry1.45 0.40 2.028 BRL 34-12172
Pyrene mg/kg dry1.63 0.40 2.028 BRL 47-12780
mg/kg dry 4.057 39-132Surrogate: 2,4,6-Tribromophenol 662.68
mg/kg dry 2.028 44-115Surrogate: 2-Fluorobiphenyl 731.49
mg/kg dry 4.057 35-115Surrogate: 2-Fluorophenol 712.90
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
Matrix Spike (P8F0190-MS1)Prepared: 06/12/18 Analyzed: 06/13/18 Source: 8060117-04
mg/kg dry 2.028 37-122Surrogate: Nitrobenzene-d5 671.36
mg/kg dry 4.057 34-121Surrogate: Phenol-d5 692.80
mg/kg dry 2.028 54-127Surrogate: Terphenyl-d14 691.40
Matrix Spike Dup (P8F0190-MSD1)Prepared: 06/12/18 Analyzed: 06/13/18 Source: 8060117-04
1,2,4-Trichlorobenzene mg/kg dry1.55 0.40 2.030 BRL 2034-11876 8
1,2-Dichlorobenzene mg/kg dry1.50 0.40 2.030 BRL 2033-11774 11
1,3-Dichlorobenzene mg/kg dry1.45 0.40 2.030 BRL 2030-11571 14
1,4-Dichlorobenzene mg/kg dry1.46 0.40 2.030 BRL 2031-11572 12
1-Methylnaphthalene mg/kg dry1.71 0.40 2.030 BRL 2040-11984 8
2,4,6-Trichlorophenol mg/kg dry1.71 0.40 2.030 BRL 2039-12684 8
2,4-Dichlorophenol mg/kg dry1.67 0.40 2.030 BRL 2040-12282 9
2,4-Dimethylphenol mg/kg dry2.19 0.40 2.030 BRL 2030-127108 10
2,4-Dinitrophenol mg/kg dry1.67 0.40 2.030 BRL 20 D27-12982 93
2,4-Dinitrotoluene mg/kg dry1.70 0.40 2.030 BRL 2048-12684 19
2,6-Dinitrotoluene mg/kg dry1.70 0.40 2.030 BRL 2046-12484 19
2-Chloronaphthalene mg/kg dry1.66 0.40 2.030 BRL 2041-11482 9
2-Chlorophenol mg/kg dry1.68 0.40 2.030 BRL 2034-12183 9
2-Methylnaphthalene mg/kg dry1.69 0.40 2.030 BRL 2038-12283 10
2-Methylphenol mg/kg dry1.75 0.40 2.030 BRL 2032-12286 8
2-Nitrophenol mg/kg dry1.57 0.40 2.030 BRL 2036-12377 16
3,3’-Dichlorobenzidine mg/kg dryBRL0.40 2.030 BRL 20 M22-121
3/4-Methylphenol mg/kg dry1.59 0.40 2.030 BRL 2034-11978 8
4,6-Dinitro-2-methylphenol mg/kg dry1.48 0.40 2.030 BRL 20 D29-13273 101
4-Bromophenyl phenyl ether mg/kg dry1.62 0.40 2.030 BRL 2046-12480 7
4-Chloro-3-methylphenol mg/kg dry1.63 0.40 2.030 BRL 2045-12280 7
4-Chloroaniline mg/kg dry0.643 0.40 2.030 BRL 2017-10632
4-Chlorophenyl phenyl ether mg/kg dry1.65 0.40 2.030 BRL 2045-12181 10
4-Nitrophenol mg/kg dry1.86 0.40 2.030 BRL 2030-13292 12
Acenaphthene mg/kg dry1.69 0.40 2.030 BRL 2040-12383 9
Acenaphthylene mg/kg dry1.72 0.40 2.030 BRL 2032-13285 9
Anthracene mg/kg dry1.85 0.40 2.030 BRL 2047-12391 8
Azobenzene mg/kg dry1.70 0.40 2.030 BRL 2039-12584 11
Benzo(a)anthracene mg/kg dry1.77 0.40 2.030 BRL 2049-12687 10
Benzo(a)pyrene mg/kg dry1.80 0.40 2.030 BRL 2045-12989 8
Benzo(b)fluoranthene mg/kg dry1.83 0.40 2.030 BRL 2045-13290 7
Benzo(g,h,i)perylene mg/kg dry1.80 0.40 2.030 BRL 2043-13489 7
Benzo(k)fluoranthene mg/kg dry1.77 0.40 2.030 BRL 2047-13287 9
Benzoic Acid mg/kg dry2.14 0.40 2.030 0.239 20 M10-8393 7
Benzyl alcohol mg/kg dry1.66 0.40 2.030 BRL 2029-12282 7
bis(2-Chloroethoxy)methane mg/kg dry1.74 0.40 2.030 BRL 2036-12186 14
Bis(2-Chloroethyl)ether mg/kg dry2.07 0.40 2.030 BRL 20 D31-120102 35
Bis(2-chloroisopropyl)ether mg/kg dry1.59 0.40 2.030 BRL 2033-13178 7
Bis(2-Ethylhexyl)phthalate mg/kg dry1.79 0.40 2.030 BRL 2051-13388 11
Butyl benzyl phthalate mg/kg dry1.73 0.40 2.030 BRL 2048-13285 8
Chrysene mg/kg dry1.77 0.40 2.030 BRL 2050-12487 10
Dibenzo(a,h)anthracene mg/kg dry1.64 0.40 2.030 BRL 2045-13481 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8F0190 - 3546
Matrix Spike Dup (P8F0190-MSD1)Prepared: 06/12/18 Analyzed: 06/13/18 Source: 8060117-04
Dibenzofuran mg/kg dry1.77 0.40 2.030 BRL 2044-12087 8
Diethyl phthalate mg/kg dry1.62 0.40 2.030 BRL 2050-12480 9
Dimethyl phthalate mg/kg dry1.66 0.40 2.030 BRL 2048-12482 10
Di-n-butyl phthalate mg/kg dry1.73 0.40 2.030 BRL 2051-12885 9
Di-n-octyl phthalate mg/kg dry1.98 0.40 2.030 BRL 2045-14097 8
Fluoranthene mg/kg dry1.78 0.40 2.030 BRL 2050-12788 10
Fluorene mg/kg dry1.78 0.40 2.030 BRL 2043-12588 9
Hexachlorobenzene mg/kg dry1.68 0.40 2.030 BRL 2045-12283 10
Hexachlorobutadiene mg/kg dry1.58 0.40 2.030 BRL 2032-12378 11
Hexachlorocyclopentadiene mg/kg dry0.337 0.40 2.030 BRL 20 M, J32-11717
Hexachloroethane mg/kg dry1.41 0.40 2.030 BRL 20 D28-11769 44
Indeno(1,2,3-cd)pyrene mg/kg dry2.08 0.40 2.030 BRL 2045-133102 7
Isophorone mg/kg dry1.69 0.40 2.030 BRL 2030-12283 9
Naphthalene mg/kg dry1.65 0.40 2.030 BRL 2035-12381 7
Nitrobenzene mg/kg dry1.57 0.40 2.030 BRL 2034-12277 11
N-Nitroso-di-n-propylamine mg/kg dry1.71 0.40 2.030 BRL 2036-12084 10
N-Nitrosodiphenylamine mg/kg dry2.08 0.40 2.030 BRL 2038-127102 12
Pentachlorophenol mg/kg dry2.15 0.40 2.030 BRL 2025-133106 6
Phenanthrene mg/kg dry1.81 0.40 2.030 BRL 2050-12189 7
Phenol mg/kg dry1.61 0.40 2.030 BRL 2034-12179 11
Pyrene mg/kg dry1.76 0.40 2.030 BRL 2047-12787 8
mg/kg dry 4.059 39-132Surrogate: 2,4,6-Tribromophenol 722.91
mg/kg dry 2.030 44-115Surrogate: 2-Fluorobiphenyl 781.58
mg/kg dry 4.059 35-115Surrogate: 2-Fluorophenol 773.13
mg/kg dry 2.030 37-122Surrogate: Nitrobenzene-d5 741.51
mg/kg dry 4.059 34-121Surrogate: Phenol-d5 763.07
mg/kg dry 2.030 54-127Surrogate: Terphenyl-d14 741.51
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8F0130 - 3050B
Blank (P8F0130-BLK1)Prepared: 06/08/18 Analyzed: 06/11/18
Arsenic mg/kg wetBRL1.5
Barium mg/kg wetBRL10
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wet0.0408 0.50 J
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL1.0
Silver mg/kg wet0.0402 0.25 J
LCS (P8F0130-BS1)Prepared: 06/08/18 Analyzed: 06/11/18
Arsenic mg/kg wet12.1 1.5 12.50 80-12097
Barium mg/kg wet12.1 10 12.50 80-12097
Cadmium mg/kg wet13.1 0.25 12.50 80-120104
Chromium mg/kg wet12.4 0.50 12.50 80-12099
Lead mg/kg wet13.2 0.25 12.50 80-120106
Selenium mg/kg wet12.1 1.0 12.50 80-12096
Silver mg/kg wet5.45 0.25 5.000 80-120109
Matrix Spike (P8F0130-MS1)Prepared: 06/08/18 Analyzed: 06/11/18 Source: 8060117-01
Arsenic mg/kg dry15.4 1.8 15.30 1.48 75-12591
Barium mg/kg dry10112 15.30 68.8 MC75-125212
Cadmium mg/kg dry15.6 0.31 15.30 0.0327 75-125102
Chromium mg/kg dry45.2 0.61 15.30 19.0 M75-125171
Lead mg/kg dry33.0 0.31 15.30 21.6 M75-12574
Selenium mg/kg dry15.7 1.2 15.29 0.845 75-12597
Silver mg/kg dry6.48 0.31 6.119 0.0404 75-125105
Matrix Spike Dup (P8F0130-MSD1)Prepared: 06/08/18 Analyzed: 06/11/18 Source: 8060117-01
Arsenic mg/kg dry14.7 1.8 15.30 1.48 2075-12587 4
Barium mg/kg dry98.6 12 15.30 68.8 20 MC75-125195 3
Cadmium mg/kg dry15.2 0.31 15.30 0.0327 2075-12599 3
Chromium mg/kg dry50.5 0.61 15.30 19.0 20 M75-125206 11
Lead mg/kg dry34.5 0.31 15.30 21.6 2075-12584 4
Selenium mg/kg dry14.4 1.2 15.29 0.845 2075-12589 8
Silver mg/kg dry6.29 0.31 6.119 0.0404 2075-125102 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8F0130 - 3050B
Post Spike (P8F0130-PS1)Prepared: 06/08/18 Analyzed: 06/11/18 Source: 8060117-01
Arsenic ug/L106 100.0 4.80 80-120101
Barium ug/L346 100.0 223 M80-120123
Cadmium ug/L107 100.0 0.106 80-120107
Chromium ug/L176 100.0 61.5 80-120114
Lead ug/L187 100.0 70.0 80-120117
Selenium ug/L104 100.0 2.73 80-120102
Silver ug/L110 100.0 0.131 80-120109
Batch P8F0188 - 7471B
Blank (P8F0188-BLK1)Prepared & Analyzed: 06/12/18
Mercury mg/kg wetBRL0.020
LCS (P8F0188-BS1)Prepared & Analyzed: 06/12/18
Mercury mg/kg wet0.446 0.020 0.4167 80-120107
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 53
6/18/18
Level II QC Report
5113 Yachtsman Ct.
Project: Retreat @ RenaissanceProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8060117
Time Submitted: 6/7/2018 10:30:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P8F0251 - Solids, Dry Weight
Duplicate (P8F0251-DUP1)Prepared & Analyzed: 06/13/18 Source: 8060117-06
% Solids % by Weight87.8 0.100 88.5 200.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 53
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P8F02518060117-01 06/13/18 15:0030 30g g
P8F02518060117-02 06/13/18 15:0030 30g g
P8F02518060117-03 06/13/18 15:0030 30g g
P8F02518060117-04 06/13/18 15:0030 30g g
P8F02518060117-05 06/13/18 15:0030 30g g
P8F02518060117-06 06/13/18 15:0030 30g g
P8F02518060117-07 06/13/18 15:0030 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P8F01908060117-01 06/12/18 10:3530.03 1g mL
P8F01908060117-02 06/12/18 10:3530.06 1g mL
P8F01908060117-03 06/12/18 10:3530.01 1g mL
P8F01908060117-04 06/12/18 10:3530.05 1g mL
P8F01908060117-05 06/12/18 10:3530.1 1g mL
P8F01908060117-06 06/12/18 10:3530.03 1g mL
P8F01908060117-07 06/12/18 12:4630.02 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P8F01308060117-01 06/08/18 8:452.02 50g mL
P8F01308060117-02 06/08/18 8:452.02 50g mL
P8F01308060117-03 06/08/18 8:452 50g mL
P8F01308060117-04 06/08/18 8:452 50g mL
P8F01308060117-05 06/08/18 8:452 50g mL
P8F01308060117-06 06/08/18 8:452 50g mL
P8F01308060117-07 06/08/18 8:452.02 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P8F01888060117-01 06/12/18 9:100.61 50g mL
P8F01888060117-02 06/12/18 9:100.6 50g mL
P8F01888060117-03 06/12/18 9:100.62 50g mL
P8F01888060117-04 06/12/18 9:100.6 50g mL
P8F01888060117-05 06/12/18 9:100.6 50g mL
P8F01888060117-06 06/12/18 9:100.6 50g mL
P8F01888060117-07 06/12/18 9:100.61 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P8F02538060117-01 06/14/18 8:555.26 5g mL
P8F02538060117-02 06/14/18 8:554.62 5g mL
P8F02538060117-03 06/14/18 8:555.13 5g mL
P8F02538060117-04 06/14/18 8:555.51 5g mL
P8F02538060117-05 06/14/18 8:554.84 5g mL
P8F02538060117-06 06/14/18 8:554.35 5g mL
P8F02538060117-07 06/14/18 8:555.93 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 53
Page 53 of 53