18060_Cooper Bussmann_Suppl Phase II Activities_2014-10-09

Golder Associates NC, Inc. 5B Oak Branch Drive Greensboro, NC 27407 USA
Tel: [phone] Fax: [phone] www.golder.com
Engineering Lic. No. C-2862/Geology Lic. No. C-399
Golder, Golder Associates and the GA globe design are trademarks of Golder Associates Corporation

October 9, 2014 133-84340.01
Ms. Sue Murphy, Engineer
NCDENR
Department of Waste Management
1646 Mail Service Center
Raleigh, NC 27699-1646
RE: RESPONSE TO NOTICE OF ELIGIBILITY/RESULTS OF SUPPLEMENTAL PHASE II
ACTIVITIES
COOPER BUSSMANN GOLDSBORO FACILITY
210 DIXIE TRAIL, GOLDSBORO, NC
Dear Ms. Murphy:
Eaton Corporation (Eaton) retained Golder Associates NC, Inc. (Golder) to perform supplemental Phase II
activities at the Eaton/Cooper Bussmann facility located at 210 Dixie Trail, in Goldsboro, Wayne County,
North Carolina (Site - see Figure 1). Golder performed supplemental assessment activities to assess
potential soil and groundwater impacts identified during limited Phase II activities conducted in September
2013. Golder submitted the results of the September 2013 limited Phase II investigations to the North
Carolina Department of Environment and Natural Resources (NCDENR) Inactive Hazardous Sites Branch
(IHSB) with a completed Site Conditions Questionnaire, dated July 3, 2014. NCDENR sent a letter dated
August 12, 2014 to Eaton indicating that the Site can be cleaned up through the IHSB Registered
Environmental Consultant (REC) Program with oversight by a Registered Site Manager (RSM). The
response letter indicates that the next step is for Eaton to enter into an REC-Administrative Agreement
(AA) with NCDENR to complete voluntary cleanup and required Eaton to reply to NCDENR’s request for
an REC-AA within 60 days (i.e., by Saturday, October 11, 2014). Concurrent with NCDENR’s review of
the Site Conditions Questionnaire, Golder completed supplemental Phase II activities at the Site in July
2014. As presented below, based on the results of the supplemental Phase II activities, it does not
appear that a release has occurred at the Site. Therefore, Eaton is requesting NCDENR to evaluate this
additional information regarding the Site and reevaluate whether the Site needs to enter the REC
Program. Based on discussions between the IHSB and Richard Lovett on September 23, 2014, Golder is
providing, on-behalf of Eaton, the results of the supplemental Phase II activities as a formal response to
NCDENR’s August 12, 2014 request.
1.0 BACKGROUND
Based on review of the Site information provided by Eaton, Golder identified the following historical
information and/or potential concerns:
 McGraw Edison developed the Site in 1974.
 Cooper began operations at the Site in 1986. Eaton/Cooper owns the Site, which
manufacturers fuse holders, breakers, etc.
 Historically, trichloroethylene (TCE) was used in small quantities on rags to spot clean
and to remove adhesive labels in the 1980s to mid-1990s.
 The facility is currently in the process of ceasing manufacturing operations. The facility
formerly manufactured and distributed automotive and electrical products and
components. Key processes included horizontal injection molding presses (currently 25
presses are in use at the Site). Ancillary operations included, but were not limited to,
machining, assembly, packaging, shipping, and maintenance.
Ms. Sue Murphy October 9, 2014
NCDENR 2 133-84340.0004

A 750- to 900-gallon concrete "pit", used as a temporary holding structure for used oil, exists on the west,
exterior side of the main building (see Figure 2). The “pit” receives waste propylene glycol-hydraulic oil
mix via concrete trenches from within the Site building. Site personnel pump out the “pit” every 48 hours
into drums for pickup and off-Site management. Site personnel terminated manufacturing operations
associated with the “pit” by the end of June 2014. Closure plans for the “pit” are in progress.
1.1 Summary of Golder’s Limited Phase II Assessment Activities – September
2013
Golder performed limited Phase II assessment activities to assess the potential for releases from
operations to Site soil and groundwater in September 2013. During the September 2013 assessment
activities, Golder collected ten soil samples, installed eight temporary well points (removed after
groundwater sampling), and collected eight groundwater samples for laboratory analyses.
Since potential impacts to groundwater were unknown, Golder personnel selected eight boring locations
to provide spatial distribution throughout the Site. Golder advanced two borings (B-4 and B-6) adjacent to
the concrete “pit” discussed above, which is located on the western side of the Site building. The drillers
advanced the boreholes using direct push technology (DPT) drilling techniques. Since the potential for
groundwater contamination was unknown at the time, temporary monitoring wells were installed in each
boring to an approximate depth of 12 feet below ground surface (ft bgs). Temporary monitoring wells are
allowed under NCDENR well construction standards (NC 02C) to be installed for a period of up to seven
days for determining aquifer characteristics. Temporary monitoring wells are not required to meet the
same construction requirements for permanent monitoring wells required under NCDENR regulatory
programs. Golder personnel collected groundwater samples from each of the eight temporary monitoring
wells utilizing EPA low-flow sampling techniques. Analytical results of the limited Phase II activities
completed in September 2013 are included on the attached tables and were compared to IHSB guidance
as follows:
 The results of soil quality analyses detected two volatile organic compounds (VOCs) and
several semi-volatile organic compounds (SVOCs). There were three SVOC
compounds, at one location (B-8), which exceeded the NCDENR Inactive Hazardous
Sites Branch (IHSB) Residential Preliminary Soil Remediation Goals (PSRG) and were
reported to be below the IHSB Industrial PSRG. The remainder of the reported
detections of VOCs and SVOCs were less than the IHSB PSRGs. Arsenic exceeded the
Residential PSRG at two locations (B-5 and B-8). Three soil samples at two locations (B-
5 and B-8) exhibited concentrations of TPH Oil Range Organics (ORO).
 The results of the groundwater quality analyses indicate that a limited number of VOCs,
polycyclic aromatic hydrocarbons (PAHs) and dissolved metals were detected in the
groundwater samples submitted for laboratory analysis. There were no exceedances of
the NCDENR (NC 2L) groundwater standard with the exception of pentachlorophenol,
which was detected in the groundwater samples collected from B-2 and B-6 with
concentrations of 0.37 micrograms per liter (ug/l) and 0.30 ug/l, respectively. The NC 2L
Groundwater Standard for pentachlorophenol is 0.3 ug/L.
Based on NCDENR regulations, Eaton notified NCDENR of the soil and groundwater exceedances
identified during the limited Phase II assessment activities described above. On behalf of Eaton,
Golder submitted a Site Cleanup Checklist/Questionnaire to NCDENR to summarize the assessment
findings on July 3, 2014. Eaton requested Golder to develop a scope of work and implement a
supplemental Phase II investigation to assess whether a release had occurred at the Site.
2.0 SUPPLEMENTAL PHASE II INVESTIGATION METHODOLOGY
The following sections describe the field methodology followed during the supplemental Phase II
assessment activities completed in July 2014. The field work described herein was supervised and
performed by Golder’s staff who designed the sampling program, located boreholes, monitored the drilling
and sampling operations, logged the boreholes, screened the headspace of soil samples for organic
Ms. Sue Murphy October 9, 2014
NCDENR 3 133-84340.0004

vapors, collected the soil samples, collected water quality field parameters, and collected groundwater
samples.
2.1 Health and Safety
Prior to initiating the fieldwork, Golder developed and implemented site-specific protocols to protect the
health and safety of its employees through the development of a site-specific Health and Safety Plan.
The drilling contractor, Mid-Atlantic Drilling, Inc. Carolina Beach, North Carolina (MAD) contacted North
Carolina 811, the State’s one-call system, to conduct the utility clearances prior to initiating the fieldwork.
Golder also contracted Ground Penetrating Radar Systems, Inc. to conduct utility clearances of proposed
boring locations and met with Site representatives to assist in utility location prior to initiation of the
fieldwork.
2.2 Scope of Sampling Program
Golder developed the scope of services to confirm the presence or absence of pentachlorophenol
detected in the groundwater samples collected from temporary monitoring wells B-2 and B-6, delineate
the extent of potentially impacted soil near B-8, collect soil samples to assess Site arsenic concentrations,
assess potential glycol impacts adjacent to the “pit”, and determine groundwater flow direction in the
surficial aquifer.
2.3 Soil Sampling and Monitoring Well Installation
Golder personnel completed the monitoring well installation and soil sampling activities on July 1 and July
14/15, 2014, respectively. Golder commissioned MAD to advance 12 soil borings at the locations shown
in Figure 2. Four borings, B-17 through B-20 were advanced inside the Site building near the concrete
trenches used to convey propylene glycol-hydraulic oil. MAD used a track-mounted Geoprobe DPT rig to
push and pneumatically hammer soil borings to depths ranging from zero to six ft bgs. Golder collected
continuous soil samples from the ground surface or approximate base of the asphalt pavement or
concrete flooring, in 4-foot intervals, to the bottom of each boring. Following the lithologic description,
MAD abandoned the borings using a Portland cement/bentonite grout. The soil boring logs are provided
in Attachment 1.
Golder personnel collected composite soil samples for screening purposes from each four-foot sample
interval, placed the soil samples in 16-ounce glass containers, covered the jars with aluminum foil, and
allowed the samples to equilibrate to approximately 60 to 70 degrees Fahrenheit to permit volatilization of
VOCs, if present. Golder field screened the screening samples for the presence of VOCs using a
photoionization detector (PID) with a 10.6 eV lamp. Golder calibrated the PID in accordance with the
manufacturer’s specifications to a 100 parts per million (ppm) isobutylene reference gas at least once a
day. Soil samples were then collected from the four-foot interval with the greatest evidence of impact
(based on visual impact and total organic volatile [TOV] readings from the screening sample) for
analytical testing. Golder personnel collected VOC samples directly from the soil core using a Terra
Core® sampler with methanol preservation. Samples for other parameters were collected directly from
the soil core into unpreserved soil containers.
A Golder geologist logged the soil samples including providing soil descriptions and classifications in
general accordance with the Unified Soil Classification System (USCS) and Golder technical procedures.
Pertinent data concerning the drilling activities were recorded on field boring logs (Attachment 1).
Golder submitted 22 soil samples to ALS Group USA, Corporation (ALS) on ice in custody-sealed coolers
via FedEx for laboratory analysis. ALS analyzed the soil samples for one or more of the following
parameters, VOCs, SVOCs, arsenic, and TPH Gasoline Range Organic (GRO), Diesel Range Organics
(DRO), and Oil Range Organics (ORO) as summarized in Table 1. The analytical data is provided in
Attachment 2.

Ms. Sue Murphy October 9, 2014
NCDENR 4 133-84340.0004

MAD installed five permanent monitoring wells meeting the NC 02C standards designated MW-9 through
MW-13 using hollow-stem auger drilling techniques at the locations shown in Figure 2. Temporary
monitoring wells B-2 and B-6 were replaced with permanent monitoring wells designated MW-09 and
MW-13, respectively. MAD constructed the wells using two-inch diameter polyvinyl chloride (PVC) pipe
with ten feet of 0.01-inch slotted screen and approximately four feet of riser. MAD completed the flush-
mount monitoring wells by adding sand into the borehole approximately one foot above the top of the
screen and placing an approximate two-foot-thick bentonite seal to reduce the potential for impacts from
surface runoff. MAD developed the wells using a peristaltic pump until the water was clear. The
monitoring well construction details are summarized in Table 2 and the monitoring well logs area provided
in Attachment 3.
Golder commissioned Stantec of Raleigh, North Carolina, a licensed surveyor, to survey top of casing
elevations and ground surface elevations of the five newly installed monitoring wells and eight exterior
boring locations. The Stantec survey is based on the North American Datum (NAD) 83 North Carolina
State Plain (NAD83/2007) and the vertical datum is North American Vertical Datum (NAVD) 88. Stantec
personnel surveyed the points of interest to a vertical accuracy of 0.01 foot. Golder used these data in its
evaluation of Site groundwater flow direction.
Golder measured depth-to-water levels relative to the top-of-casing in each of the newly-installed wells
approximately 14 days after well installation on July 15, 2014. Golder calculated the groundwater
elevation measured at each monitoring well by subtracting the measured depth to groundwater from the
elevation of the top-of-casing in each respective well. The water table elevation measurements are
provided in Table 2.
2.4 Groundwater Sampling
After allowing groundwater to equilibrate for approximately two weeks following well installation, Golder
personnel collected groundwater samples from the five newly-installed monitoring wells. After measuring
the water level in each well, Golder used a peristaltic pump and dedicated polyethylene and silicon tubing
to purge and collect groundwater samples from the wells using EPA low-flow sampling techniques.
Golder monitored water quality parameters during well purging activities including temperature, specific
conductivity, pH, turbidity, ORP, and dissolved oxygen. Groundwater samples were collected following
the stabilization of field water quality parameters (to within 10 percent of the previous two readings) or
after groundwater recharged the well. The groundwater collection forms are provided in Attachment 4.
Golder submitted the groundwater samples on ice, under chain-of-custody procedures, to ALS for
analysis of one or more of the following parameters: VOCs using EPA Method 8260C, total metals using
EPA Methods 6010C/7471B (mercury), TPH using EPA Method 8015D GRO/DRO, and SVOCs using
EPA Method 8270D. Groundwater samples collected from monitoring wells MW-12 and MW-13 (nearest
the “pit”) were also analyzed for glycols using EPA Method 8015C. Golder also collected one duplicate
groundwater sample for quality assurance purposes. The laboratory analytical reports are presented in
Attachment 2.
2.5 Quality Assurance and Quality Control
Golder performed the assessment activities in general accordance with industry standard practices. To
confirm the accuracy and reproducibility of the laboratory analytical results, the analytical laboratory
implemented a Quality Assurance and Quality Control (QA/QC) program, including laboratory replicate
samples, method blanks and control standards. The laboratory QA/QC data generated during the sample
analysis are included in the laboratory analytical reports (Attachment 2) provided to Golder. Golder also
submitted a field duplicate sample and trip blank samples for chemical analysis (using EPA Method 8260
for VOCs) for quality control purposes.
Ms. Sue Murphy October 9, 2014
NCDENR 5 133-84340.0004

3.0 SUBSURFACE CONDITIONS
3.1 Geologic Setting
The Site is located in the central part of North Carolina within the Coastal Plain sediments, near the
Neuse River. The sediments are part of the Tuscaloosa Formation and are Cretaceous in age. The area
surrounding the facility is generally level, although the ground surface is slightly lower to the south of the
building. Bedrock at the Site was not encountered to a depth of 14 ft bgs.
Based on the monitoring well installation activities, the soils underlying the Site are dominated by sands
and discontinuous silty clay layers. The soils encountered generally consisted of clay (CL) to clayey
sand, with some fine sand from the ground surface to approximately two ft bgs in some borings. The
clay/clayey sand is underlain by a gray to tan well-sorted medium sand (SW) with trace pebbles. Golder
observed discontinuous clay to silty clay layers during the limited assessment performed in 2013.
3.2 Hydrogeology
Based on groundwater elevations monitored on July 15, 2014, shallow groundwater flows to the
southeast. The phreatic surface contour map is presented in Figure 3. Water levels in the shallow
monitoring wells ranged from 4.49 to 4.94 ft bgs. These shallow wells are screened in a sand unit that
produces a significant amount of water during groundwater purging and sampling without drawdown. The
groundwater flow direction is similar to the October 1981 groundwater flow direction presented in the
Investigation of Groundwater Conditions at the Sycor Building, Goldsboro, NC Report, prepared by
Geraghty & Miller, Inc., dated October 1981.
Based on review of the historical topographic map, an un-named pond is located approximately 1,600 feet
to the southeast of the Site. The Neuse River is located approximately 4,600 feet west of the Site and
meanders to the southeast of the Site (7,000 feet). The surface water flow on the Site is via sheet flow,
which infiltrates into the surrounding soil or flows to drainage ditches around the property.
4.0 RESULTS
4.1 Assessment Criteria
Golder personnel compared the soil sampling results to the NC IHSB guidance documents (Guidelines for
Assessment and Cleanup, dated April 2013). Soil data were compared to the PSRGs, dated January
2014. The IHSB does not have an established PSRG for TPH DRO or TPH ORO compounds. The
groundwater results were compared to the North Carolina 2L Groundwater Standards (NC 2L) and Interim
Maximum Allowable Concentrations (IMAC).
Copies of the laboratory analytical reports are included in Attachment 2. The analytical laboratory results
(detections only) for soil and groundwater samples are summarized in Tables 1 and 3, respectively.
4.2 Soil Quality Summary
The soil analytical laboratory results (detections only) are summarized in Table 1. All soil sample results
met the assessment criteria with the exception of arsenic.
ALS detected TPH ORO in soil samples collected from B-11 (1 to 2 ft bgs and 4.5 to 5.5 ft bgs) and B-12
(4.5 to 5.5 ft bgs). These soil sampling locations are not near a UST or the “pit”. Golder submitted these
samples for SVOC analysis to assess individual organic constituents, which were all reported to be non-
detect or below the PSRGs for the July 2014 sampling event.
ALS detected arsenic in 11 of the 15 soil samples at concentrations ranging from 0.4 mg/kg to 2.3 mg/kg.
Only six of the 15 arsenic soil samples had concentrations above the Residential Soil Remediation Goal
of 0.61 mg/kg. None of the arsenic soil concentrations exceeded the Industrial PSRG of 2.4 mg/kg or
Protection of Groundwater PSRGs of 5.8 mg/kg. Based on the historic uses, it is believed that arsenic
Ms. Sue Murphy October 9, 2014
NCDENR 6 133-84340.0004

was not used at the Site and no known release of arsenic has occurred. The low sporadic detections of
arsenic concentrations across the Site are believed to be indicative of background arsenic concentrations.
Under the IHSB guidelines, the Groundwater PSRG may not apply if it can be demonstrated that
groundwater concentrations are below the NC 2L standards. As presented in Table 3, arsenic was
reported to be non-detect or at concentrations less than the NC 2L standards in groundwater samples
indicating that the arsenic in soil is not impacting groundwater.
4.3 Groundwater Quality Summary
A summary of the detected constituents in groundwater are summarized in Table 3. ALS did not detect
any analyzed VOC, SVOC, metal, TPH, or glycol compounds at concentrations above the laboratory
reporting limit and/or above the NC 2L Groundwater Standard.
5.0 SUMMARY OF FINDINGS AND CONCLUSIONS
Golder conducted supplemental Phase II activities at the Cooper Bussmann facility located at 201 Dixie
Trail in Goldsboro, Wayne County, NC in July 2014. Based on the field observations and laboratory
analytical results obtained during the Supplemental Phase II activities, the following summary is provided:
 The geology underlying the Site is predominantly medium gray to tan sand with a few
clay lenses and/or stringers.
 Groundwater flow in the surficial aquifer is towards the southeast based on groundwater
level monitoring performed on July 15, 2014.
 Arsenic was detected in six of the 15 soil samples at concentrations above the
Residential PSRG of 0.61 mg/kg. The highest concentrations (i.e., 0.7 mg/kg to 2.3
mg/kg) are located beneath the Site building in areas covered by the concrete slab floor.
On-Site arsenic levels are likely indicative of background concentrations as a release of
arsenic has not been reported and it is believed that arsenic containing compounds were
not used at the Site based on historical operations. None of the arsenic soil
concentrations exceeded the IHSB Industrial PSRG of 2.4 mg/kg or Protection of
Groundwater PSRGs of 5.8 mg/kg.
 Soil boring B-11 was advanced adjacent to the September 2013 soil boring B-08, which
had three SVOC compounds detected at concentrations above the Residential PSRGs.
The soil samples collected from B-11 were reported to be below the IHSB PSRGs for all
SVOCs. The reported SVOC concentrations for boring B-8, which were less than the
Industrial PSRGs, are believed to be due to a layer of buried asphalt observed during
drilling. Localized impacts from the asphalt are further confirmed by the lack of SVOCs
reported in the replicate boring B-11 and nearby borings B-13 and B-14. Other than
samples attributed to B-8, SVOCs were not detected in any of the other 23 soil samples
analyzed for SVOCs at concentrations above the Residential PSRGs.
 VOC results for 15 soil samples analyzed for VOCs were reported to be less than the
IHSB PSRGs.
 Based on the Supplemental Phase II activities, there are no groundwater exceedances
on Site. The results of the groundwater quality analyses indicate that no VOCs, SVOCs,
metals, TPH, or glycols were detected at concentrations above the NC 2L Groundwater
Standards. Golder installed permanent monitoring wells MW-09 and MW-13 that meet
the NC 02C well construction standards at the same location as temporary monitoring
wells B-2 and B-6, respectively. The purpose of these two new wells was to confirm the
presence or absence of pentachlorophenol detected in temporary monitoring wells B-2
and B-6. Pentachlorophenol was not detected in any of the groundwater samples
collected from the new monitoring wells at a concentration above the laboratory reporting
limit. The low pentachlorophenol concentrations (i.e., at or just above the NC 2L
standard) detected in the groundwater samples collected from temporary monitoring
Ms. Sue Murphy October 9, 2014
NCDENR 7 133-84340.0004

wells B-2 and B-6 in September 2013 may be attributable to the temporary status of the
monitoring wells and collection of the groundwater samples on the same day as the well
installation activities. Temporary monitoring wells are not required to meet the same
construction requirements as permanent monitoring wells required under NCDENR
regulatory programs. Permanent monitoring wells MW-09 and MW-13, were installed
with hollow-stem auger drilling techniques, a sand pack, developed, and allowed to
equilibrate with the surrounding soils for approximately two weeks prior to groundwater
sampling.
 Arsenic was not detected at a concentration above the NC 2L Groundwater Standard in
any of the groundwater samples collected from the temporary or permanent monitoring
wells to date. Soil arsenic levels do not appear to be leaching to groundwater.
6.0 CLOSURE
In a good faith manner, Eaton submitted the results of the September 2013 limited Phase II activities to
NCDENR with a completed Site Conditions Questionnaire indicating that Site soil and groundwater may
be impacted. NCDENR sent a letter to Eaton indicating that they received the Site Conditions
Questionnaire and that the Site can be voluntarily cleaned up through the REC Program under the
oversight of a RSM. The response letter indicates that the next step is for Eaton to enter into an REC-AA
with NCDENR and Eaton has 60 days to reply to NCDENR’s request for an REC-AA (i.e., by Saturday,
October 11, 2014).
Based on the results of the September 2014 Supplemental Phase II activities there is no evidence of a
release to the environment from Site operations. Groundwater concentrations at the Site are below the
NC2L standards. There has been no known release of arsenic to Site soils, the reported arsenic
concentrations are attributable to native soils and are not impacting groundwater. The only exceedance
of the PSRGs for SVOCs or VOCs in soil at the Site was reported for the 2013 soil boring B-8. The
SVOC exceedance is attributed to asphalt and was not replicated in July 2014 by the installation of a
replicate boring (B-11) and nearby borings (B-13 and B-14).
Based on this additional information, Eaton believes it is unnecessary to enter into an REC-AA and
additional investigation and remediation of the Site is not warranted.
Please contact Brian Eichlin at [phone] if you have questions regarding this subject.
Sincerely
GOLDER ASSOCIATES NC, INC.

James S. Peace, P.G. Brian J. Eichlin, P.E.
Senior Hydrogeologist Principal and Senior Consultant

Frederick M. Booth, P.G.
Principal and Practice Leader

Attachments: Table 1 – Summary of Soil Analytical Detections
Table 2 – Monitoring Well Construction and Groundwater Elevation Information
Table 3 – Summary of Groundwater Analytical Detections
Figure 1 – Site Location Map
Figure 2 – Sampling and Monitoring Well Location Map
Figure 3 – 2014 Phreatic Surface Contour Map
Ms. Sue Murphy October 9, 2014
NCDENR 8 133-84340.0004

Attachment 1 – Field Boring Logs
Attachment 2 – Laboratory Analytical Reports
Attachment 3 – Monitoring Well Logs
Attachment 4 – Groundwater Sample Collection Forms
JSP/BJE/FMB

TABLES
October 2014 Table 1
Summary of Soil Analytical Detections
Cooper Bussmann
Goldsboro, North Carolina
133-84340.01
UNITSResidential Soil PSRGProtection of Groundwater PSRG------9/5/2013 9/6/2013 9/5/2013 9/5/2013 9/5/2013 9/5/2013 9/5/2013 9/5/2013 9/5/2013 9/5/2013
------5.8-6.7 4.9-6.0 4.0-4.9 3.3-4.6 0.2-1.8 5.0-5.7 4.0-5.6 4.4-5.4 0.1-1.6 4.2-5.4
Sample Type ------N
Volatile Organic Compounds (VOCs)
2-Butanone µg/kg 5,600,000 16,000 ND ND ND ND 15 ND ND ND ND NDAcetoneµg/kg 12,000,000 24,000 ND ND ND ND 62 ND ND ND ND 39
Semi Volatile Organic Compounds (SVOCs)
3&4-Methylphenol µg/kg 620000 (12)4000 (12)ND ND ND ND ND ND ND ND ND ND
Acetophenone µg/kg 1,600,000 3,500 ND ND ND ND ND ND ND ND ND ND
Anthracene µg/kg 3,400,000 660,000 ND ND ND ND ND ND ND ND 8.4 ND
Benz(a)anthracene µg/kg 150 180 ND ND ND ND 3.8 J ND ND ND 71 7.4 J
Benzaldehyde µg/kg 1,200,000 3,000 ND ND ND ND 2.2 J ND ND ND 2.4 J ND
Benzo(a)pyrene µg/kg 15 59 ND ND ND ND 5.8 J ND ND ND 90 9.9
Benzo(b)fluoranthene µg/kg 150 600 ND ND ND ND 6.2 J ND ND ND 150 16
Benzo(g,h,i)perylene µg/kg NPS 7,800,000 ND ND ND ND 6.7 J ND ND ND 75 9.2
Benzo(k)fluoranthene µg/kg 1500 5900 ND ND ND ND 5.2 J ND ND ND 49 6.6 J
Bis(2-ethylhexyl)phthalate µg/kg 35,000 7,200 31 15 18 20 48 28 41 18 36 810
Butyl benzyl phthalate µg/kg 260,000 150,000 ND ND ND 5.1 J 4.7 J ND ND ND 4.0 J 1.8 J
Caprolactam µg/kg 6,000,000 18,000 11 5.8 J 6.2 J 8.5 ND 7.9 J 7.1 J 6.4 J 7.2 10
Carbazole µg/kg NPS 370 ND ND ND ND ND ND ND ND 7.9 ND
Chrysene µg/kg 15,000 18,000 ND ND ND ND 5.7 J ND ND ND 120 14
Dibenz(a,h)anthracene µg/kg 15 190 ND ND ND ND 5.9 J ND ND ND 16 2.1 J
Diethyl phthalate µg/kg 9,800,000 37,000 2.7 J ND ND ND ND ND ND ND ND ND
Di-n-butyl phthalate µg/kg 1,200,000 19,000 ND ND ND 2.1 J 5.3 J ND ND 2.0 J 3.4 J 4.9 J
Di-n-octyl phthalate µg/kg NPS 38,000 ND ND ND ND 7.8 ND ND ND ND 7.3 J
Fluoranthene µg/kg 460,000 330,000 ND ND ND ND 2.9 J ND ND ND 200 23
Indeno(1,2,3-cd)pyrene µg/kg 150 2,000 ND ND ND ND 6.9 J ND ND ND 84 9.4
Phenanthrene µg/kg NPS 68,000 ND ND ND ND ND ND ND ND 65 7.6 J
Phenol µg/kg 3,600,000 230 ND ND ND ND ND ND 2.6 J ND 2.4 J ND
Pyrene µg/kg 340,000 220,000 ND ND ND ND 2.8 J ND ND ND 170 17
Metals
Arsenic mg/kg 0.61 5.8 0.410 J 0.360 J 0.430 J 0.432 J 0.427 J 0.633 0.246 J 0.528 J 0.942 0.427 J
Barium mg/kg 3,000 580 7.80 29.3 51.6 20.7 27.5 25.9 29.3 9.43 16.3 36.5
Cadmium mg/kg 14 3.0 ND 0.0498 J ND ND ND ND ND ND ND ND
Chromium mg/kg 24,000 360,000 4.04 7.51 8.29 3.16 3.92 8.44 8.70 2.84 3.38 5.77
Lead mg/kg 400 270 2.09 8.33 9.24 5.39 8.60 8.15 5.65 1.92 4.35 6.88
Selenium mg/kg 78 2.1 ND ND 0.273 J ND 0.353 J 0.330 J 0.228 J 0.299 J ND 0.360 J
Silver mg/kg 78 3.4 ND 0.0582 J ND ND ND ND ND ND ND ND
Mercury mg/kg 2.0 1.0 0.00349 J 0.0289 0.0215 0.0158 0.0136 0.0250 0.0237 0.00276 J 0.0110 0.0190
TPH - DRO/ORO(9)
DRO mg/kg ND 3.8 ND ND 0.80 J ND ND ND 4.0 0.62 J
ORO mg/kg ND 8.6 ND 4.4 16 ND ND ND 27 13
Notes:
1) ND - Not Detected
2) µg/Kg - micrograms per kilogram
3) mg/Kg - milligrams per kilogram
4) ft bgs - feet below ground surface
5) Bold - Indicates a detection
Branch (IHSB) Preliminary Soil Remediation Goals (PSRG) Table - January 2014,
Residential Soil and Protection of Groundwater PSGRs.
7) J - Estimated Value
8) NPS = No Proposed Standard
10) N = Normal environmental sample, Dup = field duplicate
11) NA = Not analyzed
12) The standard listed is for 3-methylphenol (m-creosol)
9) The NCDENR UST petroleum hydrocarbon action level is 10 mg/kg for TPH.
The IHSB has standards for Extractable Petroleum Hydrocarbons but no
standard for TPH, DRO or ORO.
13) TPH = Total Petroleum Hydrocarbons, DRO = Diesel Range Organics,
ORO = Oil Range Organics
6) Highlighted - Indicates detection above the NC Inactive Hazardous Sites
ANALYTE
Sample Date
Soil Depth Interval (ft bgs)B-5B-2B-1B-8B-7B-6B-4B-3P:\Projects\2013\133-84340.2 Goldsboro NC\Reports\Supplemental Assessment July 2014\Revised NCDENR Report\Tables 1 through 3 Aug-2014 - Goldsboro.xlsx Page 1 of 3
October 2014 Table 1
Summary of Soil Analytical Detections
Cooper Bussmann
Goldsboro, North Carolina
133-84340.01
UNITSResidential Soil PSRGProtection of Groundwater PSRG------
------
Sample Type ------
Volatile Organic Compounds (VOCs)
2-Butanone µg/kg 5,600,000 16,000Acetoneµg/kg 12,000,000 24,000
Semi Volatile Organic Compounds (SVOCs)
3&4-Methylphenol µg/kg 620000 (12)4000 (12)
Acetophenone µg/kg 1,600,000 3,500
Anthracene µg/kg 3,400,000 660,000
Benz(a)anthracene µg/kg 150 180
Benzaldehyde µg/kg 1,200,000 3,000
Benzo(a)pyrene µg/kg 15 59
Benzo(b)fluoranthene µg/kg 150 600
Benzo(g,h,i)perylene µg/kg NPS 7,800,000
Benzo(k)fluoranthene µg/kg 1500 5900
Bis(2-ethylhexyl)phthalate µg/kg 35,000 7,200
Butyl benzyl phthalate µg/kg 260,000 150,000
Caprolactam µg/kg 6,000,000 18,000
Carbazole µg/kg NPS 370
Chrysene µg/kg 15,000 18,000
Dibenz(a,h)anthracene µg/kg 15 190
Diethyl phthalate µg/kg 9,800,000 37,000
Di-n-butyl phthalate µg/kg 1,200,000 19,000
Di-n-octyl phthalate µg/kg NPS 38,000
Fluoranthene µg/kg 460,000 330,000
Indeno(1,2,3-cd)pyrene µg/kg 150 2,000
Phenanthrene µg/kg NPS 68,000
Phenol µg/kg 3,600,000 230
Pyrene µg/kg 340,000 220,000
Metals
Arsenic mg/kg 0.61 5.8
Barium mg/kg 3,000 580
Cadmium mg/kg 14 3.0
Chromium mg/kg 24,000 360,000
Lead mg/kg 400 270
Selenium mg/kg 78 2.1
Silver mg/kg 78 3.4
Mercury mg/kg 2.0 1.0
TPH - DRO/ORO(9)
DRO mg/kg
ORO mg/kg
Notes:
1) ND - Not Detected
2) µg/Kg - micrograms per kilogram
3) mg/Kg - milligrams per kilogram
4) ft bgs - feet below ground surface
5) Bold - Indicates a detection
Branch (IHSB) Preliminary Soil Remediation Goals (PSRG) Table - January 2014,
Residential Soil and Protection of Groundwater PSGRs.
7) J - Estimated Value
8) NPS = No Proposed Standard
10) N = Normal environmental sample, Dup = field duplicate
11) NA = Not analyzed
12) The standard listed is for 3-methylphenol (m-creosol)
9) The NCDENR UST petroleum hydrocarbon action level is 10 mg/kg for TPH.
The IHSB has standards for Extractable Petroleum Hydrocarbons but no
standard for TPH, DRO or ORO.
13) TPH = Total Petroleum Hydrocarbons, DRO = Diesel Range Organics,
ORO = Oil Range Organics
6) Highlighted - Indicates detection above the NC Inactive Hazardous Sites
ANALYTE
Sample Date
Soil Depth Interval (ft bgs)
7/15/2014 7/15/2014 7/15/2014 7/15/2014 7/15/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014
3.5 - 4 1 - 2 4 - 5 1 - 2 4.5 - 5.5 1 - 2 4.5 - 5.5 1 - 2 4.5 - 5.5 1 - 2 4.5 - 5.5
N N N N N N N N N N N
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA 2.4 J ND NA NA ND ND ND ND
NA NA NA ND ND NA NA ND 2.2 J ND ND
NA NA NA ND ND NA NA ND ND ND ND
NA NA NA 3.1 J ND NA NA ND ND ND ND
NA NA NA ND ND NA NA ND ND ND ND
NA NA NA 2.2 J ND NA NA ND ND ND ND
NA NA NA 3.9 J ND NA NA ND ND ND ND
NA NA NA ND ND NA NA ND ND ND ND
NA NA NA 2 J ND NA NA ND ND ND ND
NA NA NA 3.5 J 10 NA NA ND 3.1 J ND ND
NA NA NA ND 2.5 J NA NA ND ND ND ND
NA NA NA 26 9.6 NA NA ND 22 ND 11
NA NA NA ND ND NA NA ND ND ND ND
NA NA NA 3.8 J ND NA NA 77 J ND ND ND
NA NA NA ND ND NA NA ND ND ND ND
NA NA NA ND ND NA NA ND 2.9 J ND ND
NA NA NA 2.2 J 2.3 J NA NA ND 2.3 J ND 2.2 J
NA NA NA ND ND NA NA ND ND ND ND
NA NA NA 5.2 J 2.9 J NA NA ND ND ND ND
NA NA NA 2.2 J ND NA NA ND ND ND ND
NA NA NA 2.8 J 2.1 J NA NA ND ND ND ND
NA NA NA 1.9 J ND NA NA ND ND ND ND
NA NA NA 4.3 J 2.3 J NA NA 43 J ND ND ND
0.4 J 0.5 J ND NA NA NA NA NA NA 0.5 J ND
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NANANANANANANANANANANANA
NA NA NA 0.93 J 3 ND 1 J NA NA NA NA
NA NA NA 13 11 0.86 J 18 NA NA NA NAB-9B-10B-11B-14B-13B-12 (MW-12)P:\Projects\2013\133-84340.2 Goldsboro NC\Reports\Supplemental Assessment July 2014\Revised NCDENR Report\Tables 1 through 3 Aug-2014 - Goldsboro.xlsx Page 2 of 3
October 2014 Table 1
Summary of Soil Analytical Detections
Cooper Bussmann
Goldsboro, North Carolina
133-84340.01
UNITSResidential Soil PSRGProtection of Groundwater PSRG------
------
Sample Type ------
Volatile Organic Compounds (VOCs)
2-Butanone µg/kg 5,600,000 16,000Acetoneµg/kg 12,000,000 24,000
Semi Volatile Organic Compounds (SVOCs)
3&4-Methylphenol µg/kg 620000 (12)4000 (12)
Acetophenone µg/kg 1,600,000 3,500
Anthracene µg/kg 3,400,000 660,000
Benz(a)anthracene µg/kg 150 180
Benzaldehyde µg/kg 1,200,000 3,000
Benzo(a)pyrene µg/kg 15 59
Benzo(b)fluoranthene µg/kg 150 600
Benzo(g,h,i)perylene µg/kg NPS 7,800,000
Benzo(k)fluoranthene µg/kg 1500 5900
Bis(2-ethylhexyl)phthalate µg/kg 35,000 7,200
Butyl benzyl phthalate µg/kg 260,000 150,000
Caprolactam µg/kg 6,000,000 18,000
Carbazole µg/kg NPS 370
Chrysene µg/kg 15,000 18,000
Dibenz(a,h)anthracene µg/kg 15 190
Diethyl phthalate µg/kg 9,800,000 37,000
Di-n-butyl phthalate µg/kg 1,200,000 19,000
Di-n-octyl phthalate µg/kg NPS 38,000
Fluoranthene µg/kg 460,000 330,000
Indeno(1,2,3-cd)pyrene µg/kg 150 2,000
Phenanthrene µg/kg NPS 68,000
Phenol µg/kg 3,600,000 230
Pyrene µg/kg 340,000 220,000
Metals
Arsenic mg/kg 0.61 5.8
Barium mg/kg 3,000 580
Cadmium mg/kg 14 3.0
Chromium mg/kg 24,000 360,000
Lead mg/kg 400 270
Selenium mg/kg 78 2.1
Silver mg/kg 78 3.4
Mercury mg/kg 2.0 1.0
TPH - DRO/ORO(9)
DRO mg/kg
ORO mg/kg
Notes:
1) ND - Not Detected
2) µg/Kg - micrograms per kilogram
3) mg/Kg - milligrams per kilogram
4) ft bgs - feet below ground surface
5) Bold - Indicates a detection
Branch (IHSB) Preliminary Soil Remediation Goals (PSRG) Table - January 2014,
Residential Soil and Protection of Groundwater PSGRs.
7) J - Estimated Value
8) NPS = No Proposed Standard
10) N = Normal environmental sample, Dup = field duplicate
11) NA = Not analyzed
12) The standard listed is for 3-methylphenol (m-creosol)
9) The NCDENR UST petroleum hydrocarbon action level is 10 mg/kg for TPH.
The IHSB has standards for Extractable Petroleum Hydrocarbons but no
standard for TPH, DRO or ORO.
13) TPH = Total Petroleum Hydrocarbons, DRO = Diesel Range Organics,
ORO = Oil Range Organics
6) Highlighted - Indicates detection above the NC Inactive Hazardous Sites
ANALYTE
Sample Date
Soil Depth Interval (ft bgs)
7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014 7/14/2014
3 - 4 3 - 4 1 - 2 4.5 - 5.5 1 - 2 4.5 - 5.5 4.5 - 5.5 1 - 2 4.5 - 5.5 1 - 2 4.5 - 5.5
N N N N N DUP N N N N N
NA NA ND ND ND ND ND NA NA NA NA
NA NA ND ND ND ND ND NA NA NA NA
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND 1.6 J
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA 9 4.9 J 1.9 J 8 4.4 J 2.3 J 3.4 J 2.2 J 5.8 J
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND 8.5 11 9.8 3.8 J 6.7 J 8.9 7.8 8
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND 2.2 J
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND 1.8 J ND ND
NA NA 1.8 J ND ND 2.3 J ND ND ND 1.9 J ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
NA NA ND ND ND ND ND ND ND ND ND
ND ND 0.5 J 0.7 J 2.3 J 1.2 J 1.0 J 0.7 J 0.7 J 0.5 J 0.8 J
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NA
NA NA NA NA NA NA NA NA NA NA NANANANANANANANANANANANA
NA NA ND ND ND 0.53 J 1.1 J ND 0.76 J ND ND
NA NA 1.9 J 5.7 ND 7.9 8.8 2.6 J 4 0.64 J 0.82 J
Prepared by: ATK
Checked by:BPC
Reviewed by: BE/FMBB-19B-20B-15B-16B-17B-18P:\Projects\2013\133-84340.2 Goldsboro NC\Reports\Supplemental Assessment July 2014\Revised NCDENR Report\Tables 1 through 3 Aug-2014 - Goldsboro.xlsx Page 3 of 3
October 2014 Table 2
Monitoring Well Construction and Groundwater Elevation Information
Cooper-Bussmann
Goldsboro, NC
133-84340.01
Well ID Northing Easting
Ground Surface
Elevation (ft
msl)
Top of
Casing
Elevation (ft
msl)
Top of
Screen (ft
bgs)
Bottom of
screen (ft
bgs)
Depth to water
(ft BTOC)
WL Elevation (ft
msl)
MW-09 586534.18 2296979.21 70.771 69.881 4 14 4.89 64.99
MW-10 586361.62 2297120.45 70.358 69.758 4 14 4.94 64.82
MW-11 586120.68 2297103.76 69.649 69.398 4 14 4.80 64.60
MW-12 586158.51 2296974.69 69.753 69.336 4 14 4.52 64.82
MW-13 586234.6 2296902.17 70.096 69.369 4 14 4.49 64.88
Notes:
ft BTOC = feet below top of casing
WL = Water Level
Elevations in NAD 88 Prepared by:ATK
ft msl = feet above mean seal level Checked by BPC
ft bgs = feet below ground surface Reviewed by:BE/FMB
Depth to water measured on July 15, 2014.
P:\Projects\2013\133-84340.2 Goldsboro NC\Reports\Supplemental Assessment July 2014\Revised NCDENR Report\Tables 1 through 3 Aug-2014 - Goldsboro.xlsx
Page 1 of 1
October 2014 Table 3
Summary of Groundwater Analytical Detections
Cooper Bussmann
Goldsboro, North Carolina
133-84340.01
UnitsNC 2L Groundwater Standard----
----
Sample Type Dup N N
Volatile Organic Compounds (VOCs)
Methyl tert-butyl ether µg/L 20 ND ND ND ND ND ND 1.2 ND NA 0.62 J NA ND ND NA
Toluene µg/L 600 1.9 2.6 17 1.7 1.4 5.0 5.1 3.8 NA ND NA ND ND NA
Semi Volatile Organic Compounds (SVOCs)
3&4-Methylphenol µg/L 40 (13)ND ND ND ND ND 0.097 J ND ND ND ND ND ND ND ND
Bis(2-ethylhexyl)phthalate µg/L 3 0.75 1.8 0.23 0.63 0.37 1.2 1.0 0.31 1.6 2 0.78 0.46 0.43 2.6
Butyl benzyl phthalate µg/L 1,000 0.027 J ND ND ND ND ND ND ND ND ND ND ND ND ND
Caprolactam µg/L 4,000 ND ND ND ND 0.26 ND ND 0.14 J 0.08 J 0.079 J 0.062 J 0.2 J 0.13 J 0.1 J
Diethyl phthalate µg/L 6,000 0.11 J 0.059 J 0.071 J 0.050 J 0.050 J ND 0.065 J ND ND ND ND ND ND ND
Di-n-butyl phthalate µg/L 700 0.35 0.082 J 0.20 0.094 J ND 0.079 J 0.13 J 0.055 J 0.07 J 0.078 J ND ND ND 0.088 J
Di-n-octyl phthalate µg/L 100 0.044 J 0.055 J ND 0.046 J ND ND 0.13 J ND ND ND ND ND ND ND
Pentachlorophenol µg/L 0.3 ND 0.37 ND ND 0.056 J 0.30 ND ND ND ND ND ND ND NDPhenolµg/L 30 ND 0.064 J 0.10 J ND ND ND ND ND ND ND ND ND ND ND
Total Metals
Arsenic mg/L 0.01 ND ND ND 0.00291 J ND 0.00111 J ND 0.00195 J NA ND NA 0.0016 0.0022 NA
Barium mg/L 0.7 0.0362 0.0710 0.0365 0.0536 0.0136 0.0494 0.0567 0.0578 NA 0.0880 NA 0.0343 0.034 NA
Chromium mg/L 0.01 0.000884 J ND 0.000736 J 0.000815 J 0.000978 J 0.00101 J 0.00202 J 0.00118 J NA 0.0008 J NA 0.0006 J 0.0006 J NA
Lead mg/L 0.015 ND ND ND 0.000418 J ND ND 0.000712 J 0.000444 J NA 0.0003 J NA 0.00019 J 0.00019 J NA
TPH - GRO/ORO
GRO mg/L (8)ND ND 0.0388 J ND ND ND ND ND ND ND ND ND ND ND
ORO mg/L (8)ND ND ND ND ND ND ND 0.059 J ND ND ND ND ND ND
Glycols
Ethylene glycol mg/L 10 NA NA NA NA NA NA NA NA NA NA NA NA ND ND
Propylene glycol mg/L 140 (14)NA NA NA NA NA NA NA NA NA NA NA NA ND ND
Notes:Prepared by: ATK
1) ND - Not Detected Checked by: BPC
2) µg/L - micrograms per Liter Reviewed by: BE/FMB
3) mg/L - milligrams per Liter
4) Bold - Indicates a detection
5) Highlighted - Indicates detection above NC 2L Groundwater Standard
6) J - Estimated Value
7) ft bgs - feet below ground surface
8) The reported TPH results are less than the lowest published standards for petroleum hydrocarbon fractions
9) N = Normal Environmental Sample, Dup = Field Duplicate Sample
10) NA = Not analyzed
11) Monitoring wells B-1 through B-8 were temporary direct push wells. Monitoring wells MW-9 through MW-13 are permanent two-inch diameter wells
12) Monitoring wells installed in the same location are designated by color - B-2 and MW-9 and B-6 and MW-13
13) The NC 2L standard listed is for 4-methylphenol
14) Currently a NC 2L standard does not exist for propylene glycol, the interim maximum allowable concentration published by NCDENR is shown
Sample Depth
(screened interval or grab depth)
B-1
2 to 12 ft bgs
B-7
2 to 12 ft bgs
Sample Date
B-8
09/06/13 09/06/13 09/06/13 09/06/13 09/06/13 09/06/13 09/06/13 09/06/13
B-2 (12)B-3 B-4 B-5 B-6 (12)
TPH = Total Petroleum Hydrocarbons, GRO = Gasoline Range Organics, ORO = Oil Range Organics
2 to 12 ft bgs 2 to 12 ft bgs 2 to 12 ft bgs 2 to 12 ft bgs 2 to 12 ft bgs
ANALYTE
N N N N N N N N
2 to 12 ft bgs
MW-12 MW-13 (12)
07/15/14 07/15/14 07/15/14 07/15/14 07/15/14 07/15/14
MW-9 (12)MW-10 MW-11 MW-12
4 to 14 ft bgs 4 to 14 ft bgs
N N N
4 to 14 ft bgs 4 to 14 ft bgs 4 to 14 ft bgs 4 to 14 ft bgs
P:\Projects\2013\133-84340.2 Goldsboro NC\Reports\Supplemental Assessment July 2014\Revised NCDENR Report\Tables 1 through 3 Aug-2014 - Goldsboro.xlsx
Page 1 of 1

FIGURES
SITE
CLIENTEATON CORPORATIONSUPPLEMENTAL PHASE II ESA
LEGEND
Approximate Property Boundary
REFERENCESERVICE LAYER CREDITS: SOURCES: ESRI, HERE, DELORME,USGS, INTERMAP, INCREMENT P CORP., NRCAN, ESRI JAPAN,METI, ESRI CHINA (HONG KONG), ESRI (THAILAND), TOMTOM,MAPMYINDIA, © OPENSTREETMAP CONTRIBUTORS, AND THEGIS USER COMMUNITY
PROJECTEATON - COOPER/BUSSMANN210 DIXIE TRAILGOLDSBORO, NORTH CAROLINA
TITLE
SITE LOCATION MAP
133-8434001 1 0 1
2014-06-19
CDS
NCS
JSP
THR 1 in0Path: V:\001 GIS Projects\2013\133-8434001 Eaton Goldsboro NC\MXDs\1338434A004_Figure 1.mxd KEY MAP
IF THIS MEASUREMENT DOES NOT MATCH WHAT IS SHOWN, THE SHEET HAS BEEN MODIFIED FROM: ANSI ACONSULTANT
PROJECT No.CONTROL Rev.FIGURE
YYYY-MM-DD
PREPARED
DESIGN
REVIEW
APPROVED
SITE
1,000 0 1,000500Feet
GOLDER ASSOCIATES NC, INC,58 OAK BRANCH DR. | GREENSBORO, NC 27407ENGINEERING LIC NO. C-2862GEOLOGY LIC. NO. C-399
<
<
<
<
<
<
<
<
<
<
<
<
<
B-1 B-2
B-3
B-4
B-5
B-6
B-7
B-8
MW-9
MW-10
MW-11
MW-12
MW-13 B-10
B-11
B-14B-13
B-9
B-15B-16
B-18 B-20
B-19B-17
CLIENT EATON CORPORATIONSUPPLEMENTAL PHASE II ESA
LEGEND
Boring Location
<Monitoring Well Location
<Temporary Well/Boring installed September 2013
Approximate Property Boundary
NOTES
REFERENCE
1. TEMPORARY MONITORING WELLS INSTALLED ONSEPTEMBER 5-6, 2013, REMOVED AFTER SAMPLING ONSEPTEMBER 6, 2013
SERVICE LAYER CREDITS: SOURCE: ESRI, DIGITALGLOBE,GEOEYE, I-CUBED, EARTHSTAR GEOGRAPHICS, CNES/AIRBUSDS, USDA, USGS, AEX, GETMAPPING, AEROGRID, IGN, IGP,SWISSTOPO, AND THE GIS USER COMMUNITYESRI, HERE, DELORME, TOMTOM, MAPMYINDIA, ©
PROJECTEATON - COOPER/BUSSMANN210 DIXIE TRAILGOLDSBORO, NORTH CAROLINA
TITLESAMPLING AND MONITORING WELL LOCATION MAP
133-8434001 1 0 2
2014-07-01
CDS
NSC
JSP
THR 1 in0Path: V:\001 GIS Projects\2013\133-8434001 Eaton Goldsboro NC\MXDs\1338434A001_Figure 2.mxd IF THIS MEASUREMENT DOES NOT MATCH WHAT IS SHOWN, THE SHEET HAS BEEN MODIFIED FROM: ANSI BCONSULTANT
PROJECT No.CONTROL Rev.FIGURE
YYYY-MM-DD
PREPARED
DESIGN
REVIEW
APPROVED
SITE
North Carolina
0 100 20050Feet
GOLDER ASSOCIATES NC, INC,58 OAK BRANCH DR. | GREENSBORO, NC 27407ENGINEERING LIC NO. C-2862GEOLOGY LIC. NO. C-399
"PIT"
CLIENT EATON CORPORATIONSUPPLEMENTAL PHASE II ESA
FIGURE NARRATIVE
REFERENCE
THIS FIGURE DEPICTS THE GROUNDWATER ELEVATION, ASMEASURED IN SHALLOW GROUNDWATER MONITORING WELLS,AND IS INTENDED TO REPRESENT THE APPROXIMATEELEVATION OF THE GROUNDWATER TABLE (PHREATIC)SURFACE. THE POSTED DATA WERE CALCULATED FROMDEPTH TO WATER MEASUREMENTS MADE BY GOLDER ONJULY 15, 2014 FROM WELLS SCREENED ACROSS OR NEAR THEWATER TABLE. ONLY DATA CONSIDERED TO REPRESENTSTATIC WATER LEVEL CONDITIONS WERE USED IN THECONSTRUCTION OF THIS PHREATIC SURFACE MAP. THEDIRECTION OF HORIZONTAL GROUNDWATER FLOW AT ANDNEAR THE PHREATIC SURFACE CAN BE GENERALLYINTERPRETED AS BEING PERPENDICULAR TO THEGROUNDWATER ELEVATION CONTOURS. GOLDER INFERREDTHE ELEVATION CONTOURS BASED ON THE DATAILLUSTRATED. THE ACTUAL ELEVATION OF THE PHREATICSURFACE IS LIKELY MORE HETEROGENEOUS THAN SHOWNAND ACTUAL CONDITIONS WILL VARY. OTHERINTERPRETATIONS ARE POSSIBLE. THE DEPTH TOGROUNDWATER IS KNOWN TO VARY WITH TIME.
SERVICE LAYER CREDITS: SOURCE: ESRI, DIGITALGLOBE,GEOEYE, I-CUBED, EARTHSTAR GEOGRAPHICS, CNES/AIRBUSDS, USDA, USGS, AEX, GETMAPPING, AEROGRID, IGN, IGP,SWISSTOPO, AND THE GIS USER COMMUNITYESRI, HERE, DELORME, TOMTOM, MAPMYINDIA, ©
PROJECTEATON - COOPER/BUSSMANN210 DIXIE TRAILGOLDSBORO, NORTH CAROLINA
TITLE
2014 PHREATIC SURFACE CONTOUR MAP
133-8434001 1 0 3
2014-07-01
CDS
NSC
JSP
THR 1 in0Path: V:\001 GIS Projects\2013\133-8434001 Eaton Goldsboro NC\MXDs\1338434A002_Figure 3.mxd IF THIS MEASUREMENT DOES NOT MATCH WHAT IS SHOWN, THE SHEET HAS BEEN MODIFIED FROM: ANSI BCONSULTANT
PROJECT No.CONTROL Rev.FIGURE
YYYY-MM-DD
PREPARED
DESIGN
REVIEW
APPROVED
<
<
<
<
<
MW-9MW-964.9964.99
MW-10MW-1064.8264.82
MW-11MW-1164.664.6
MW-12MW-1264.8264.82
MW-13MW-1364.8864.8864.9064.8064.7064.6065.00LEGEND
Approximate Property Boundary
<Monitoring Well Location
Phreatic Surface Contours
100 0 10050Feet
GOLDER ASSOCIATES NC, INC,58 OAK BRANCH DR. | GREENSBORO, NC 27407ENGINEERING LIC NO. C-2862GEOLOGY LIC. NO. C-399

ATTACHMENT 1
FIELD BORING LOGS
Caption Text

ATTACHMENT 2
LABORATORY ANALYTICAL REPORTS
Caption Text
August 06, 2014
David "Dusty" Y. Reedy II
Golder Associates, Inc.
5B Oak Branch Drive
Greensboro, NC 27407
The analytical data provided relates directly to the samples received by ALS Environmental and for only
the analyses requested. Results are expressed as "as received" unless otherwise noted.
QC sample results for this data met EPA or laboratory specifications except as noted in the Case
Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be
reproduced, it should be reproduced in full unless written approval has been obtained by ALS
Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me.
Sincerely,
ALS Environmental received 29 sample(s) on Jul 15, 2014 for the analysis presented in the following
report.
Laboratory Results for:Eaton Phase II Goldsboro NC 13384340
Dear David,
Work Order:HS14070721
Generated By: Dane.Wacasey
Dane J. Wacasey
10450 Stancliff Rd. Suite 210
Houston, TX 77099
T: [phone]
F: [phone]
www.alsglobal.com
Client:Golder Associates, Inc.
Work Order:HS14070721
Project:Eaton Phase II Goldsboro NC 13384340 SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrix TagNo Date Received Hold
HS14070721-01 15-Jul-2014 17:00 15-Jul-2014 17:00MW-9 Water
HS14070721-02 15-Jul-2014 16:00 15-Jul-2014 17:00MW-10 Water
HS14070721-03 15-Jul-2014 15:05 15-Jul-2014 17:00MW-11 Water
HS14070721-04 15-Jul-2014 14:00 15-Jul-2014 17:00MW-12 Water
HS14070721-05 15-Jul-2014 14:00 15-Jul-2014 17:00MW-12 DUP Water
HS14070721-06 15-Jul-2014 13:00 15-Jul-2014 17:00MW-13 Water
HS14070721-07 14-Jul-2014 13:50 15-Jul-2014 17:00B-18A (1-2)Soil
HS14070721-08 14-Jul-2014 14:10 15-Jul-2014 17:00B-18B (4.5-5.5)Soil
HS14070721-09 14-Jul-2014 14:10 15-Jul-2014 17:00B-18B (4.5-5.5) DUP Soil
HS14070721-10 14-Jul-2014 17:45 15-Jul-2014 17:00B-17A (1-2)Soil
HS14070721-11 14-Jul-2014 17:55 15-Jul-2014 17:00B-17B (4.5-5.5)Soil
HS14070721-12 14-Jul-2014 16:53 15-Jul-2014 17:00B-19A (1-2)Soil
HS14070721-13 14-Jul-2014 17:06 15-Jul-2014 17:00B-19B (4.5-5.5)Soil
HS14070721-14 14-Jul-2014 15:30 15-Jul-2014 17:00B-20A (1-2)Soil
HS14070721-15 14-Jul-2014 15:50 15-Jul-2014 17:00B-20B (4.5-5.5)Soil
HS14070721-16 15-Jul-2014 08:35 15-Jul-2014 17:00B-9A (3.5-4.0)Soil
HS14070721-17 15-Jul-2014 10:00 15-Jul-2014 17:00B-10A (1-2)Soil
HS14070721-18 15-Jul-2014 10:05 15-Jul-2014 17:00B-10B (4-5)Soil
HS14070721-19 15-Jul-2014 09:30 15-Jul-2014 17:00B-11A Soil
HS14070721-20 15-Jul-2014 09:35 15-Jul-2014 17:00B-11B Soil
HS14070721-21 14-Jul-2014 07:30 15-Jul-2014 17:00B-12A (1-2)Soil
HS14070721-22 14-Jul-2014 07:35 15-Jul-2014 17:00B-12B (4.5-5.5)Soil
HS14070721-23 14-Jul-2014 09:20 15-Jul-2014 17:00B-13A (1-2)Soil
HS14070721-24 14-Jul-2014 09:25 15-Jul-2014 17:00B-13B (4.5-5.5)Soil
HS14070721-25 14-Jul-2014 09:05 15-Jul-2014 17:00B-14A (1-2)Soil
HS14070721-26 14-Jul-2014 09:10 15-Jul-2014 17:00B-14B (4.5-5.5)Soil
HS14070721-27 14-Jul-2014 08:55 15-Jul-2014 17:00B-15 (3-4)Soil
ALS Group USA, Corp 06-Aug-14Date:
Client:Golder Associates, Inc.
Work Order:HS14070721
Project:Eaton Phase II Goldsboro NC 13384340 SAMPLE SUMMARY
Lab Samp ID Client Sample ID Collection DateMatrix TagNo Date Received Hold
HS14070721-28 14-Jul-2014 08:30 15-Jul-2014 17:00B-16 (3-4)Soil
HS14070721-29 15-Jul-2014 00:00 15-Jul-2014 17:00Trip Blank 070714-22 Water
ALS Group USA, Corp 06-Aug-14Date:
Client:CASE NARRATIVE
Work Order:
Eaton Phase II Goldsboro NC 13384340
Golder Associates, Inc.
Project:
HS14070721
Work Order Comments
Samples submitted for the analysis of Total RCRA 8 metals and Total Arsenic were subcontracted to ALS Jacksonville, Florida. The
report is appended.
•
GC Semivolatiles by Method SW8015
Batch ID: R238322
Sample ID: LCSW-140728Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Semivolatiles by Method SW8015M
Batch ID: R237910
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
Batch ID: 84404
Sample ID: LCSD-84404
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
Batch ID: 84484
Sample ID: LCSD-84404
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GC Volatiles by Method SW8015M
Batch ID: R237931
Sample ID: HS14070768-01MS/MSDMS/MSD was performed on an unrelated sample. The LCS was acceptable.•
Batch ID: R237864
Sample ID: B-18A (1-2) (HS14070721-07MS)MS failed recovery criteria due to suspect matrix effect. The LCS was recovered within criteria. Furthermore, the MSD RPD criterion
was exceeded due to suspect sample heterogeneity, however, the recovery was in control.
•
Batch ID: R237910
Sample ID: GLCSDS1-140723
Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GCMS Sample Preparation by Method SW3541
Batch ID: 84441
Sample ID: B-13A (1-2) (HS14070721-23), B-14A (1-2) (HS14070721-25)During the concentration process, the sample extracts became viscous and could not concentrate to 1 mL.•
GCMS Semivolatiles by Method SW8270
Batch ID: 84441
Sample ID: B-13A (1-2) (HS14070721-23), B-14A (1-2) (HS14070721-25)Sample analyzed at a dilution due to matrix interference. Reporting limits are elevated relative to the analysis dilution.•
Sample ID: B-18A (1-2) (HS14070721-07MSD)
The MSD RPD criterion was exceeded for 3,3´-Dichlorobenzidine, however, the individual recoveries were within criteria. •
Batch ID: 84405a
Sample ID: HS14070861-21MS/MSD
MS/MSD was performed on an unrelated sample. The LCS was acceptable.•
ALS Group USA, Corp 06-Aug-14Date:
Client:CASE NARRATIVE
Work Order:
Eaton Phase II Goldsboro NC 13384340
Golder Associates, Inc.
Project:
HS14070721
GCMS Semivolatiles by Method SW8270
Batch ID: 84329
Sample ID: LCSD-84329Insufficient sample received to perform MS/MSD. LCS/LCSD provided as batch quality control. •
GCMS Volatiles by Method SW8260
Batch ID: R238123
Sample ID: VSTD050Bromochloromethane exceeded %D limits in CCV. The analyte was not detected in the associated samples. Slight positive bias does
not impact data quality.
•
Sample ID: HS14070715-01MSDMS/MSD was performed on an unrelated sample. The LCS was recovered within criteria.•
Batch ID: R237862
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
WetChemistry by Method SW3550
Batch ID: R238044
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.•
ALS Group USA, Corp 06-Aug-14Date:
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-9
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-01
15-Jul-2014 17:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 15:560.0321,1´-Biphenyl 0.20U
1ug/L 24-Jul-2014 15:560.0402,4,5-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 15:560.0602,4,6-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 15:560.0652,4-Dichlorophenol 0.20U
1ug/L 24-Jul-2014 15:560.0332,4-Dimethylphenol 0.20U
1ug/L 24-Jul-2014 15:560.0502,4-Dinitrophenol 1.0U
1ug/L 24-Jul-2014 15:560.0302,4-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 15:560.0502,6-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 15:560.0402-Chloronaphthalene 0.20U
1ug/L 24-Jul-2014 15:560.0402-Chlorophenol 0.20U
1ug/L 24-Jul-2014 15:560.0342-Methylnaphthalene 0.20U
1ug/L 24-Jul-2014 15:560.0332-Methylphenol 0.20U
1ug/L 24-Jul-2014 15:560.0382-Nitroaniline 0.20U
1ug/L 24-Jul-2014 15:560.0242-Nitrophenol 0.20U
1ug/L 24-Jul-2014 15:560.0303&4-Methylphenol 0.20U
1ug/L 24-Jul-2014 15:560.0243,3´-Dichlorobenzidine 0.20U
1ug/L 24-Jul-2014 15:560.0563-Nitroaniline 0.20U
1ug/L 24-Jul-2014 15:560.0734,6-Dinitro-2-methylphenol 0.20U
1ug/L 24-Jul-2014 15:560.0474-Bromophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 15:560.0224-Chloro-3-methylphenol 0.20U
1ug/L 24-Jul-2014 15:560.0214-Chloroaniline 0.20U
1ug/L 24-Jul-2014 15:560.0434-Chlorophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 15:560.0404-Nitroaniline 0.20U
1ug/L 24-Jul-2014 15:560.0604-Nitrophenol 1.0U
1ug/L 24-Jul-2014 15:560.030Acenaphthene 0.20U
1ug/L 24-Jul-2014 15:560.021Acenaphthylene 0.20U
1ug/L 24-Jul-2014 15:560.030Acetophenone 0.20U
1ug/L 24-Jul-2014 15:560.020Anthracene 0.20U
1ug/L 24-Jul-2014 15:560.040Atrazine 0.20U
1ug/L 24-Jul-2014 15:560.025Benz(a)anthracene 0.20U
1ug/L 24-Jul-2014 15:560.046Benzaldehyde 0.20U
1ug/L 24-Jul-2014 15:560.030Benzo(a)pyrene 0.20U
1ug/L 24-Jul-2014 15:560.028Benzo(b)fluoranthene 0.20U
1ug/L 24-Jul-2014 15:560.026Benzo(g,h,i)perylene 0.20U
1ug/L 24-Jul-2014 15:560.028Benzo(k)fluoranthene 0.20U
1ug/L 24-Jul-2014 15:560.022Bis(2-chloroethoxy)methane 0.20U
1ug/L 24-Jul-2014 15:560.029Bis(2-chloroethyl)ether 0.20U
1ug/L 24-Jul-2014 15:560.064Bis(2-chloroisopropyl)ether 0.20U
1ug/L 24-Jul-2014 15:560.033Bis(2-ethylhexyl)phthalate 0.201.6
1ug/L 24-Jul-2014 15:560.021Butyl benzyl phthalate 0.20U
1ug/L 24-Jul-2014 15:56J0.059Caprolactam 0.200.077
1ug/L 24-Jul-2014 15:560.025Carbazole 0.20U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-9
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-01
15-Jul-2014 17:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 15:560.046Chrysene 0.20U
1ug/L 24-Jul-2014 15:560.026Dibenz(a,h)anthracene 0.20U
1ug/L 24-Jul-2014 15:560.025Dibenzofuran 0.20U
1ug/L 24-Jul-2014 15:560.021Diethyl phthalate 0.20U
1ug/L 24-Jul-2014 15:560.030Dimethyl phthalate 0.20U
1ug/L 24-Jul-2014 15:56J0.030Di-n-butyl phthalate 0.200.069
1ug/L 24-Jul-2014 15:560.023Di-n-octyl phthalate 0.20U
1ug/L 24-Jul-2014 15:560.020Fluoranthene 0.20U
1ug/L 24-Jul-2014 15:560.021Fluorene 0.20U
1ug/L 24-Jul-2014 15:560.070Hexachlorobenzene 0.20U
1ug/L 24-Jul-2014 15:560.050Hexachlorobutadiene 0.20U
1ug/L 24-Jul-2014 15:560.054Hexachlorocyclopentadiene 0.20U
1ug/L 24-Jul-2014 15:560.034Hexachloroethane 0.20U
1ug/L 24-Jul-2014 15:560.051Indeno(1,2,3-cd)pyrene 0.20U
1ug/L 24-Jul-2014 15:560.030Isophorone 0.20U
1ug/L 24-Jul-2014 15:560.050Naphthalene 0.20U
1ug/L 24-Jul-2014 15:560.050Nitrobenzene 0.20U
1ug/L 24-Jul-2014 15:560.040N-Nitrosodi-n-propylamine 0.20U
1ug/L 24-Jul-2014 15:560.029N-Nitrosodiphenylamine 0.20U
1ug/L 24-Jul-2014 15:560.046Pentachlorophenol 0.20U
1ug/L 24-Jul-2014 15:560.020Phenanthrene 0.20U
1ug/L 24-Jul-2014 15:560.032Phenol 0.20U
1ug/L 24-Jul-2014 15:560.022Pyrene 0.20U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 15:5645.3 34-129
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 15:5640.1 40-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 15:5643.4 20-120
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 15:5664.5 40-135
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 15:5645.0 41-120
Surr: Phenol-d6 1%REC 24-Jul-2014 15:5642.8 20-120
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/L 23-Jul-2014 18:420.0100GRO (C6-C10)0.0500U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 18:4282.5 70-130
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3511 / 21-Jul-2014
1mg/L 30-Jul-2014 16:030.020TPH (Diesel Range)0.050U
1mg/L 30-Jul-2014 16:030.040TPH (Oil Range)0.10U
Surr: 2-Fluorobiphenyl 1%REC 30-Jul-2014 16:0387.7 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-10
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-02
15-Jul-2014 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: AKP
1ug/L 25-Jul-2014 18:080.201,1,1-Trichloroethane 1.0U
1ug/L 25-Jul-2014 18:080.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 25-Jul-2014 18:081.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 25-Jul-2014 18:080.301,1,2-Trichloroethane 1.0U
1ug/L 25-Jul-2014 18:080.201,1-Dichloroethane 1.0U
1ug/L 25-Jul-2014 18:080.201,1-Dichloroethene 1.0U
1ug/L 25-Jul-2014 18:080.501,2,4-Trichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:081.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 25-Jul-2014 18:080.201,2-Dibromoethane 1.0U
1ug/L 25-Jul-2014 18:080.501,2-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:080.201,2-Dichloroethane 1.0U
1ug/L 25-Jul-2014 18:080.501,2-Dichloropropane 1.0U
1ug/L 25-Jul-2014 18:080.401,3-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:080.401,4-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:080.502-Butanone 2.0U
1ug/L 25-Jul-2014 18:081.02-Hexanone 2.0U
1ug/L 25-Jul-2014 18:080.704-Methyl-2-pentanone 2.0U
1ug/L 25-Jul-2014 18:082.0Acetone 2.0U
1ug/L 25-Jul-2014 18:080.20Benzene 1.0U
1ug/L 25-Jul-2014 18:080.20Bromodichloromethane 1.0U
1ug/L 25-Jul-2014 18:080.40Bromoform 1.0U
1ug/L 25-Jul-2014 18:080.40Bromomethane 1.0U
1ug/L 25-Jul-2014 18:080.60Carbon disulfide 2.0U
1ug/L 25-Jul-2014 18:080.50Carbon tetrachloride 1.0U
1ug/L 25-Jul-2014 18:080.30Chlorobenzene 1.0U
1ug/L 25-Jul-2014 18:080.30Chloroethane 1.0U
1ug/L 25-Jul-2014 18:080.20Chloroform 1.0U
1ug/L 25-Jul-2014 18:080.20Chloromethane 1.0U
1ug/L 25-Jul-2014 18:080.20cis-1,2-Dichloroethene 1.0U
1ug/L 25-Jul-2014 18:080.10cis-1,3-Dichloropropene 1.0U
1ug/L 25-Jul-2014 18:080.30Cyclohexane 1.0U
1ug/L 25-Jul-2014 18:080.30Dibromochloromethane 1.0U
1ug/L 25-Jul-2014 18:080.30Dichlorodifluoromethane 1.0U
1ug/L 25-Jul-2014 18:080.50Dichloromethane 10U
1ug/L 25-Jul-2014 18:080.30Ethylbenzene 1.0U
1ug/L 25-Jul-2014 18:080.30Isopropylbenzene 1.0U
1ug/L 25-Jul-2014 18:080.50m,p-Xylene 2.0U
1ug/L 25-Jul-2014 18:081.0Methyl acetate 1.0U
1ug/L 25-Jul-2014 18:08J0.20Methyl tert-butyl ether 1.00.62
1ug/L 25-Jul-2014 18:080.30Methylcyclohexane 1.0U
1ug/L 25-Jul-2014 18:080.30o-Xylene 1.0U
1ug/L 25-Jul-2014 18:080.30Styrene 1.0U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-10
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-02
15-Jul-2014 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: AKP
1ug/L 25-Jul-2014 18:080.30Tetrachloroethene 1.0U
1ug/L 25-Jul-2014 18:080.20Toluene 1.0U
1ug/L 25-Jul-2014 18:080.20trans-1,2-Dichloroethene 1.0U
1ug/L 25-Jul-2014 18:080.20trans-1,3-Dichloropropene 1.0U
1ug/L 25-Jul-2014 18:080.20Trichloroethene 1.0U
1ug/L 25-Jul-2014 18:080.30Trichlorofluoromethane 1.0U
1ug/L 25-Jul-2014 18:080.20Vinyl chloride 1.0U
1ug/L 25-Jul-2014 18:080.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 25-Jul-2014 18:0810270-125
Surr: 4-Bromofluorobenzene 1%REC 25-Jul-2014 18:0896.1 72-125
Surr: Dibromofluoromethane 1%REC 25-Jul-2014 18:0898.5 71-125
Surr: Toluene-d8 1%REC 25-Jul-2014 18:0897.7 75-125
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-10
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-02
15-Jul-2014 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 16:150.0321,1´-Biphenyl 0.20U
1ug/L 24-Jul-2014 16:150.0402,4,5-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 16:150.0602,4,6-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 16:150.0652,4-Dichlorophenol 0.20U
1ug/L 24-Jul-2014 16:150.0332,4-Dimethylphenol 0.20U
1ug/L 24-Jul-2014 16:150.0502,4-Dinitrophenol 1.0U
1ug/L 24-Jul-2014 16:150.0302,4-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 16:150.0502,6-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 16:150.0402-Chloronaphthalene 0.20U
1ug/L 24-Jul-2014 16:150.0402-Chlorophenol 0.20U
1ug/L 24-Jul-2014 16:150.0342-Methylnaphthalene 0.20U
1ug/L 24-Jul-2014 16:150.0332-Methylphenol 0.20U
1ug/L 24-Jul-2014 16:150.0382-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:150.0242-Nitrophenol 0.20U
1ug/L 24-Jul-2014 16:150.0303&4-Methylphenol 0.20U
1ug/L 24-Jul-2014 16:150.0243,3´-Dichlorobenzidine 0.20U
1ug/L 24-Jul-2014 16:150.0563-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:150.0734,6-Dinitro-2-methylphenol 0.20U
1ug/L 24-Jul-2014 16:150.0474-Bromophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 16:150.0224-Chloro-3-methylphenol 0.20U
1ug/L 24-Jul-2014 16:150.0214-Chloroaniline 0.20U
1ug/L 24-Jul-2014 16:150.0434-Chlorophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 16:150.0404-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:150.0604-Nitrophenol 1.0U
1ug/L 24-Jul-2014 16:150.030Acenaphthene 0.20U
1ug/L 24-Jul-2014 16:150.021Acenaphthylene 0.20U
1ug/L 24-Jul-2014 16:150.030Acetophenone 0.20U
1ug/L 24-Jul-2014 16:150.020Anthracene 0.20U
1ug/L 24-Jul-2014 16:150.040Atrazine 0.20U
1ug/L 24-Jul-2014 16:150.025Benz(a)anthracene 0.20U
1ug/L 24-Jul-2014 16:150.046Benzaldehyde 0.20U
1ug/L 24-Jul-2014 16:150.030Benzo(a)pyrene 0.20U
1ug/L 24-Jul-2014 16:150.028Benzo(b)fluoranthene 0.20U
1ug/L 24-Jul-2014 16:150.026Benzo(g,h,i)perylene 0.20U
1ug/L 24-Jul-2014 16:150.028Benzo(k)fluoranthene 0.20U
1ug/L 24-Jul-2014 16:150.022Bis(2-chloroethoxy)methane 0.20U
1ug/L 24-Jul-2014 16:150.029Bis(2-chloroethyl)ether 0.20U
1ug/L 24-Jul-2014 16:150.064Bis(2-chloroisopropyl)ether 0.20U
1ug/L 24-Jul-2014 16:150.033Bis(2-ethylhexyl)phthalate 0.202.0
1ug/L 24-Jul-2014 16:150.021Butyl benzyl phthalate 0.20U
1ug/L 24-Jul-2014 16:15J0.059Caprolactam 0.200.079
1ug/L 24-Jul-2014 16:150.025Carbazole 0.20U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-10
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-02
15-Jul-2014 16:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 16:150.046Chrysene 0.20U
1ug/L 24-Jul-2014 16:150.026Dibenz(a,h)anthracene 0.20U
1ug/L 24-Jul-2014 16:150.025Dibenzofuran 0.20U
1ug/L 24-Jul-2014 16:150.021Diethyl phthalate 0.20U
1ug/L 24-Jul-2014 16:150.030Dimethyl phthalate 0.20U
1ug/L 24-Jul-2014 16:15J0.030Di-n-butyl phthalate 0.200.078
1ug/L 24-Jul-2014 16:150.023Di-n-octyl phthalate 0.20U
1ug/L 24-Jul-2014 16:150.020Fluoranthene 0.20U
1ug/L 24-Jul-2014 16:150.021Fluorene 0.20U
1ug/L 24-Jul-2014 16:150.070Hexachlorobenzene 0.20U
1ug/L 24-Jul-2014 16:150.050Hexachlorobutadiene 0.20U
1ug/L 24-Jul-2014 16:150.054Hexachlorocyclopentadiene 0.20U
1ug/L 24-Jul-2014 16:150.034Hexachloroethane 0.20U
1ug/L 24-Jul-2014 16:150.051Indeno(1,2,3-cd)pyrene 0.20U
1ug/L 24-Jul-2014 16:150.030Isophorone 0.20U
1ug/L 24-Jul-2014 16:150.050Naphthalene 0.20U
1ug/L 24-Jul-2014 16:150.050Nitrobenzene 0.20U
1ug/L 24-Jul-2014 16:150.040N-Nitrosodi-n-propylamine 0.20U
1ug/L 24-Jul-2014 16:150.029N-Nitrosodiphenylamine 0.20U
1ug/L 24-Jul-2014 16:150.046Pentachlorophenol 0.20U
1ug/L 24-Jul-2014 16:150.020Phenanthrene 0.20U
1ug/L 24-Jul-2014 16:150.032Phenol 0.20U
1ug/L 24-Jul-2014 16:150.022Pyrene 0.20U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 16:1555.8 34-129
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 16:1548.1 40-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 16:1550.2 20-120
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 16:1564.6 40-135
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 16:1552.0 41-120
Surr: Phenol-d6 1%REC 24-Jul-2014 16:1548.2 20-120
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/L 23-Jul-2014 18:580.0100GRO (C6-C10)0.0500U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 18:5879.6 70-130
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3511 / 21-Jul-2014
1mg/L 30-Jul-2014 16:300.020TPH (Diesel Range)0.051U
1mg/L 30-Jul-2014 16:300.041TPH (Oil Range)0.10U
Surr: 2-Fluorobiphenyl 1%REC 30-Jul-2014 16:3077.5 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-11
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-03
15-Jul-2014 15:05 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 16:340.0321,1´-Biphenyl 0.20U
1ug/L 24-Jul-2014 16:340.0402,4,5-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 16:340.0602,4,6-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 16:340.0652,4-Dichlorophenol 0.20U
1ug/L 24-Jul-2014 16:340.0332,4-Dimethylphenol 0.20U
1ug/L 24-Jul-2014 16:340.0502,4-Dinitrophenol 1.0U
1ug/L 24-Jul-2014 16:340.0302,4-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 16:340.0502,6-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 16:340.0402-Chloronaphthalene 0.20U
1ug/L 24-Jul-2014 16:340.0402-Chlorophenol 0.20U
1ug/L 24-Jul-2014 16:340.0342-Methylnaphthalene 0.20U
1ug/L 24-Jul-2014 16:340.0332-Methylphenol 0.20U
1ug/L 24-Jul-2014 16:340.0382-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:340.0242-Nitrophenol 0.20U
1ug/L 24-Jul-2014 16:340.0303&4-Methylphenol 0.20U
1ug/L 24-Jul-2014 16:340.0243,3´-Dichlorobenzidine 0.20U
1ug/L 24-Jul-2014 16:340.0563-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:340.0734,6-Dinitro-2-methylphenol 0.20U
1ug/L 24-Jul-2014 16:340.0474-Bromophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 16:340.0224-Chloro-3-methylphenol 0.20U
1ug/L 24-Jul-2014 16:340.0214-Chloroaniline 0.20U
1ug/L 24-Jul-2014 16:340.0434-Chlorophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 16:340.0404-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:340.0604-Nitrophenol 1.0U
1ug/L 24-Jul-2014 16:340.030Acenaphthene 0.20U
1ug/L 24-Jul-2014 16:340.021Acenaphthylene 0.20U
1ug/L 24-Jul-2014 16:340.030Acetophenone 0.20U
1ug/L 24-Jul-2014 16:340.020Anthracene 0.20U
1ug/L 24-Jul-2014 16:340.040Atrazine 0.20U
1ug/L 24-Jul-2014 16:340.025Benz(a)anthracene 0.20U
1ug/L 24-Jul-2014 16:340.046Benzaldehyde 0.20U
1ug/L 24-Jul-2014 16:340.030Benzo(a)pyrene 0.20U
1ug/L 24-Jul-2014 16:340.028Benzo(b)fluoranthene 0.20U
1ug/L 24-Jul-2014 16:340.026Benzo(g,h,i)perylene 0.20U
1ug/L 24-Jul-2014 16:340.028Benzo(k)fluoranthene 0.20U
1ug/L 24-Jul-2014 16:340.022Bis(2-chloroethoxy)methane 0.20U
1ug/L 24-Jul-2014 16:340.029Bis(2-chloroethyl)ether 0.20U
1ug/L 24-Jul-2014 16:340.064Bis(2-chloroisopropyl)ether 0.20U
1ug/L 24-Jul-2014 16:340.033Bis(2-ethylhexyl)phthalate 0.200.78
1ug/L 24-Jul-2014 16:340.021Butyl benzyl phthalate 0.20U
1ug/L 24-Jul-2014 16:34J0.059Caprolactam 0.200.062
1ug/L 24-Jul-2014 16:340.025Carbazole 0.20U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-11
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-03
15-Jul-2014 15:05 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 16:340.046Chrysene 0.20U
1ug/L 24-Jul-2014 16:340.026Dibenz(a,h)anthracene 0.20U
1ug/L 24-Jul-2014 16:340.025Dibenzofuran 0.20U
1ug/L 24-Jul-2014 16:340.021Diethyl phthalate 0.20U
1ug/L 24-Jul-2014 16:340.030Dimethyl phthalate 0.20U
1ug/L 24-Jul-2014 16:340.030Di-n-butyl phthalate 0.20U
1ug/L 24-Jul-2014 16:340.023Di-n-octyl phthalate 0.20U
1ug/L 24-Jul-2014 16:340.020Fluoranthene 0.20U
1ug/L 24-Jul-2014 16:340.021Fluorene 0.20U
1ug/L 24-Jul-2014 16:340.070Hexachlorobenzene 0.20U
1ug/L 24-Jul-2014 16:340.050Hexachlorobutadiene 0.20U
1ug/L 24-Jul-2014 16:340.054Hexachlorocyclopentadiene 0.20U
1ug/L 24-Jul-2014 16:340.034Hexachloroethane 0.20U
1ug/L 24-Jul-2014 16:340.051Indeno(1,2,3-cd)pyrene 0.20U
1ug/L 24-Jul-2014 16:340.030Isophorone 0.20U
1ug/L 24-Jul-2014 16:340.050Naphthalene 0.20U
1ug/L 24-Jul-2014 16:340.050Nitrobenzene 0.20U
1ug/L 24-Jul-2014 16:340.040N-Nitrosodi-n-propylamine 0.20U
1ug/L 24-Jul-2014 16:340.029N-Nitrosodiphenylamine 0.20U
1ug/L 24-Jul-2014 16:340.046Pentachlorophenol 0.20U
1ug/L 24-Jul-2014 16:340.020Phenanthrene 0.20U
1ug/L 24-Jul-2014 16:340.032Phenol 0.20U
1ug/L 24-Jul-2014 16:340.022Pyrene 0.20U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 16:3454.5 34-129
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 16:3443.0 40-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 16:3448.1 20-120
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 16:3458.8 40-135
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 16:3449.6 41-120
Surr: Phenol-d6 1%REC 24-Jul-2014 16:3446.9 20-120
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/L 23-Jul-2014 19:140.0100GRO (C6-C10)0.0500U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 19:1479.8 70-130
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3511 / 21-Jul-2014
1mg/L 30-Jul-2014 16:570.020TPH (Diesel Range)0.050U
1mg/L 30-Jul-2014 16:570.040TPH (Oil Range)0.10U
Surr: 2-Fluorobiphenyl 1%REC 30-Jul-2014 16:5774.7 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-04
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: AKP
1ug/L 25-Jul-2014 18:340.201,1,1-Trichloroethane 1.0U
1ug/L 25-Jul-2014 18:340.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 25-Jul-2014 18:341.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 25-Jul-2014 18:340.301,1,2-Trichloroethane 1.0U
1ug/L 25-Jul-2014 18:340.201,1-Dichloroethane 1.0U
1ug/L 25-Jul-2014 18:340.201,1-Dichloroethene 1.0U
1ug/L 25-Jul-2014 18:340.501,2,4-Trichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:341.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 25-Jul-2014 18:340.201,2-Dibromoethane 1.0U
1ug/L 25-Jul-2014 18:340.501,2-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:340.201,2-Dichloroethane 1.0U
1ug/L 25-Jul-2014 18:340.501,2-Dichloropropane 1.0U
1ug/L 25-Jul-2014 18:340.401,3-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:340.401,4-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 18:340.502-Butanone 2.0U
1ug/L 25-Jul-2014 18:341.02-Hexanone 2.0U
1ug/L 25-Jul-2014 18:340.704-Methyl-2-pentanone 2.0U
1ug/L 25-Jul-2014 18:342.0Acetone 2.0U
1ug/L 25-Jul-2014 18:340.20Benzene 1.0U
1ug/L 25-Jul-2014 18:340.20Bromodichloromethane 1.0U
1ug/L 25-Jul-2014 18:340.40Bromoform 1.0U
1ug/L 25-Jul-2014 18:340.40Bromomethane 1.0U
1ug/L 25-Jul-2014 18:340.60Carbon disulfide 2.0U
1ug/L 25-Jul-2014 18:340.50Carbon tetrachloride 1.0U
1ug/L 25-Jul-2014 18:340.30Chlorobenzene 1.0U
1ug/L 25-Jul-2014 18:340.30Chloroethane 1.0U
1ug/L 25-Jul-2014 18:340.20Chloroform 1.0U
1ug/L 25-Jul-2014 18:340.20Chloromethane 1.0U
1ug/L 25-Jul-2014 18:340.20cis-1,2-Dichloroethene 1.0U
1ug/L 25-Jul-2014 18:340.10cis-1,3-Dichloropropene 1.0U
1ug/L 25-Jul-2014 18:340.30Cyclohexane 1.0U
1ug/L 25-Jul-2014 18:340.30Dibromochloromethane 1.0U
1ug/L 25-Jul-2014 18:340.30Dichlorodifluoromethane 1.0U
1ug/L 25-Jul-2014 18:340.50Dichloromethane 10U
1ug/L 25-Jul-2014 18:340.30Ethylbenzene 1.0U
1ug/L 25-Jul-2014 18:340.30Isopropylbenzene 1.0U
1ug/L 25-Jul-2014 18:340.50m,p-Xylene 2.0U
1ug/L 25-Jul-2014 18:341.0Methyl acetate 1.0U
1ug/L 25-Jul-2014 18:340.20Methyl tert-butyl ether 1.0U
1ug/L 25-Jul-2014 18:340.30Methylcyclohexane 1.0U
1ug/L 25-Jul-2014 18:340.30o-Xylene 1.0U
1ug/L 25-Jul-2014 18:340.30Styrene 1.0U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-04
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: AKP
1ug/L 25-Jul-2014 18:340.30Tetrachloroethene 1.0U
1ug/L 25-Jul-2014 18:340.20Toluene 1.0U
1ug/L 25-Jul-2014 18:340.20trans-1,2-Dichloroethene 1.0U
1ug/L 25-Jul-2014 18:340.20trans-1,3-Dichloropropene 1.0U
1ug/L 25-Jul-2014 18:340.20Trichloroethene 1.0U
1ug/L 25-Jul-2014 18:340.30Trichlorofluoromethane 1.0U
1ug/L 25-Jul-2014 18:340.20Vinyl chloride 1.0U
1ug/L 25-Jul-2014 18:340.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 25-Jul-2014 18:3410270-125
Surr: 4-Bromofluorobenzene 1%REC 25-Jul-2014 18:3494.2 72-125
Surr: Dibromofluoromethane 1%REC 25-Jul-2014 18:3495.1 71-125
Surr: Toluene-d8 1%REC 25-Jul-2014 18:3496.9 75-125
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-04
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 16:530.0321,1´-Biphenyl 0.20U
1ug/L 24-Jul-2014 16:530.0402,4,5-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 16:530.0602,4,6-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 16:530.0652,4-Dichlorophenol 0.20U
1ug/L 24-Jul-2014 16:530.0332,4-Dimethylphenol 0.20U
1ug/L 24-Jul-2014 16:530.0502,4-Dinitrophenol 1.0U
1ug/L 24-Jul-2014 16:530.0302,4-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 16:530.0502,6-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 16:530.0402-Chloronaphthalene 0.20U
1ug/L 24-Jul-2014 16:530.0402-Chlorophenol 0.20U
1ug/L 24-Jul-2014 16:530.0342-Methylnaphthalene 0.20U
1ug/L 24-Jul-2014 16:530.0332-Methylphenol 0.20U
1ug/L 24-Jul-2014 16:530.0382-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:530.0242-Nitrophenol 0.20U
1ug/L 24-Jul-2014 16:530.0303&4-Methylphenol 0.20U
1ug/L 24-Jul-2014 16:530.0243,3´-Dichlorobenzidine 0.20U
1ug/L 24-Jul-2014 16:530.0563-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:530.0734,6-Dinitro-2-methylphenol 0.20U
1ug/L 24-Jul-2014 16:530.0474-Bromophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 16:530.0224-Chloro-3-methylphenol 0.20U
1ug/L 24-Jul-2014 16:530.0214-Chloroaniline 0.20U
1ug/L 24-Jul-2014 16:530.0434-Chlorophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 16:530.0404-Nitroaniline 0.20U
1ug/L 24-Jul-2014 16:530.0604-Nitrophenol 1.0U
1ug/L 24-Jul-2014 16:530.030Acenaphthene 0.20U
1ug/L 24-Jul-2014 16:530.021Acenaphthylene 0.20U
1ug/L 24-Jul-2014 16:530.030Acetophenone 0.20U
1ug/L 24-Jul-2014 16:530.020Anthracene 0.20U
1ug/L 24-Jul-2014 16:530.040Atrazine 0.20U
1ug/L 24-Jul-2014 16:530.025Benz(a)anthracene 0.20U
1ug/L 24-Jul-2014 16:530.046Benzaldehyde 0.20U
1ug/L 24-Jul-2014 16:530.030Benzo(a)pyrene 0.20U
1ug/L 24-Jul-2014 16:530.028Benzo(b)fluoranthene 0.20U
1ug/L 24-Jul-2014 16:530.026Benzo(g,h,i)perylene 0.20U
1ug/L 24-Jul-2014 16:530.028Benzo(k)fluoranthene 0.20U
1ug/L 24-Jul-2014 16:530.022Bis(2-chloroethoxy)methane 0.20U
1ug/L 24-Jul-2014 16:530.029Bis(2-chloroethyl)ether 0.20U
1ug/L 24-Jul-2014 16:530.064Bis(2-chloroisopropyl)ether 0.20U
1ug/L 24-Jul-2014 16:530.033Bis(2-ethylhexyl)phthalate 0.200.43
1ug/L 24-Jul-2014 16:530.021Butyl benzyl phthalate 0.20U
1ug/L 24-Jul-2014 16:53J0.059Caprolactam 0.200.13
1ug/L 24-Jul-2014 16:530.025Carbazole 0.20U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-04
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 16:530.046Chrysene 0.20U
1ug/L 24-Jul-2014 16:530.026Dibenz(a,h)anthracene 0.20U
1ug/L 24-Jul-2014 16:530.025Dibenzofuran 0.20U
1ug/L 24-Jul-2014 16:530.021Diethyl phthalate 0.20U
1ug/L 24-Jul-2014 16:530.030Dimethyl phthalate 0.20U
1ug/L 24-Jul-2014 16:530.030Di-n-butyl phthalate 0.20U
1ug/L 24-Jul-2014 16:530.023Di-n-octyl phthalate 0.20U
1ug/L 24-Jul-2014 16:530.020Fluoranthene 0.20U
1ug/L 24-Jul-2014 16:530.021Fluorene 0.20U
1ug/L 24-Jul-2014 16:530.070Hexachlorobenzene 0.20U
1ug/L 24-Jul-2014 16:530.050Hexachlorobutadiene 0.20U
1ug/L 24-Jul-2014 16:530.054Hexachlorocyclopentadiene 0.20U
1ug/L 24-Jul-2014 16:530.034Hexachloroethane 0.20U
1ug/L 24-Jul-2014 16:530.051Indeno(1,2,3-cd)pyrene 0.20U
1ug/L 24-Jul-2014 16:530.030Isophorone 0.20U
1ug/L 24-Jul-2014 16:530.050Naphthalene 0.20U
1ug/L 24-Jul-2014 16:530.050Nitrobenzene 0.20U
1ug/L 24-Jul-2014 16:530.040N-Nitrosodi-n-propylamine 0.20U
1ug/L 24-Jul-2014 16:530.029N-Nitrosodiphenylamine 0.20U
1ug/L 24-Jul-2014 16:530.046Pentachlorophenol 0.20U
1ug/L 24-Jul-2014 16:530.020Phenanthrene 0.20U
1ug/L 24-Jul-2014 16:530.032Phenol 0.20U
1ug/L 24-Jul-2014 16:530.022Pyrene 0.20U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 16:5363.5 34-129
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 16:5343.9 40-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 16:5347.6 20-120
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 16:5374.6 40-135
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 16:5349.6 41-120
Surr: Phenol-d6 1%REC 24-Jul-2014 16:5345.5 20-120
MISC. GCFID PARAMETERS BY
SW8015C Method:SW8015 Analyst: SE
1mg/L 28-Jul-2014 15:351.0Ethylene Glycol 1.0U
1mg/L 28-Jul-2014 15:351.0Propylene glycol 1.0U
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/L 23-Jul-2014 19:300.0100GRO (C6-C10)0.0500U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 19:3081.9 70-130
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-04
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3511 / 21-Jul-2014
1mg/L 30-Jul-2014 17:240.020TPH (Diesel Range)0.051U
1mg/L 30-Jul-2014 17:240.041TPH (Oil Range)0.10U
Surr: 2-Fluorobiphenyl 1%REC 30-Jul-2014 17:2470.3 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12 DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-05
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: AKP
1ug/L 25-Jul-2014 19:000.201,1,1-Trichloroethane 1.0U
1ug/L 25-Jul-2014 19:000.501,1,2,2-Tetrachloroethane 1.0U
1ug/L 25-Jul-2014 19:001.01,1,2-Trichlor-1,2,2-trifluoroethane 1.0U
1ug/L 25-Jul-2014 19:000.301,1,2-Trichloroethane 1.0U
1ug/L 25-Jul-2014 19:000.201,1-Dichloroethane 1.0U
1ug/L 25-Jul-2014 19:000.201,1-Dichloroethene 1.0U
1ug/L 25-Jul-2014 19:000.501,2,4-Trichlorobenzene 1.0U
1ug/L 25-Jul-2014 19:001.01,2-Dibromo-3-chloropropane 1.0U
1ug/L 25-Jul-2014 19:000.201,2-Dibromoethane 1.0U
1ug/L 25-Jul-2014 19:000.501,2-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 19:000.201,2-Dichloroethane 1.0U
1ug/L 25-Jul-2014 19:000.501,2-Dichloropropane 1.0U
1ug/L 25-Jul-2014 19:000.401,3-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 19:000.401,4-Dichlorobenzene 1.0U
1ug/L 25-Jul-2014 19:000.502-Butanone 2.0U
1ug/L 25-Jul-2014 19:001.02-Hexanone 2.0U
1ug/L 25-Jul-2014 19:000.704-Methyl-2-pentanone 2.0U
1ug/L 25-Jul-2014 19:002.0Acetone 2.0U
1ug/L 25-Jul-2014 19:000.20Benzene 1.0U
1ug/L 25-Jul-2014 19:000.20Bromodichloromethane 1.0U
1ug/L 25-Jul-2014 19:000.40Bromoform 1.0U
1ug/L 25-Jul-2014 19:000.40Bromomethane 1.0U
1ug/L 25-Jul-2014 19:000.60Carbon disulfide 2.0U
1ug/L 25-Jul-2014 19:000.50Carbon tetrachloride 1.0U
1ug/L 25-Jul-2014 19:000.30Chlorobenzene 1.0U
1ug/L 25-Jul-2014 19:000.30Chloroethane 1.0U
1ug/L 25-Jul-2014 19:000.20Chloroform 1.0U
1ug/L 25-Jul-2014 19:000.20Chloromethane 1.0U
1ug/L 25-Jul-2014 19:000.20cis-1,2-Dichloroethene 1.0U
1ug/L 25-Jul-2014 19:000.10cis-1,3-Dichloropropene 1.0U
1ug/L 25-Jul-2014 19:000.30Cyclohexane 1.0U
1ug/L 25-Jul-2014 19:000.30Dibromochloromethane 1.0U
1ug/L 25-Jul-2014 19:000.30Dichlorodifluoromethane 1.0U
1ug/L 25-Jul-2014 19:000.50Dichloromethane 10U
1ug/L 25-Jul-2014 19:000.30Ethylbenzene 1.0U
1ug/L 25-Jul-2014 19:000.30Isopropylbenzene 1.0U
1ug/L 25-Jul-2014 19:000.50m,p-Xylene 2.0U
1ug/L 25-Jul-2014 19:001.0Methyl acetate 1.0U
1ug/L 25-Jul-2014 19:000.20Methyl tert-butyl ether 1.0U
1ug/L 25-Jul-2014 19:000.30Methylcyclohexane 1.0U
1ug/L 25-Jul-2014 19:000.30o-Xylene 1.0U
1ug/L 25-Jul-2014 19:000.30Styrene 1.0U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12 DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-05
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: AKP
1ug/L 25-Jul-2014 19:000.30Tetrachloroethene 1.0U
1ug/L 25-Jul-2014 19:000.20Toluene 1.0U
1ug/L 25-Jul-2014 19:000.20trans-1,2-Dichloroethene 1.0U
1ug/L 25-Jul-2014 19:000.20trans-1,3-Dichloropropene 1.0U
1ug/L 25-Jul-2014 19:000.20Trichloroethene 1.0U
1ug/L 25-Jul-2014 19:000.30Trichlorofluoromethane 1.0U
1ug/L 25-Jul-2014 19:000.20Vinyl chloride 1.0U
1ug/L 25-Jul-2014 19:000.50Xylenes, Total 3.0U
Surr: 1,2-Dichloroethane-d4 1%REC 25-Jul-2014 19:0010470-125
Surr: 4-Bromofluorobenzene 1%REC 25-Jul-2014 19:0095.3 72-125
Surr: Dibromofluoromethane 1%REC 25-Jul-2014 19:0097.6 71-125
Surr: Toluene-d8 1%REC 25-Jul-2014 19:0098.1 75-125
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12 DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-05
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 17:120.0321,1´-Biphenyl 0.20U
1ug/L 24-Jul-2014 17:120.0402,4,5-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 17:120.0602,4,6-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 17:120.0652,4-Dichlorophenol 0.20U
1ug/L 24-Jul-2014 17:120.0332,4-Dimethylphenol 0.20U
1ug/L 24-Jul-2014 17:120.0502,4-Dinitrophenol 1.0U
1ug/L 24-Jul-2014 17:120.0302,4-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 17:120.0502,6-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 17:120.0402-Chloronaphthalene 0.20U
1ug/L 24-Jul-2014 17:120.0402-Chlorophenol 0.20U
1ug/L 24-Jul-2014 17:120.0342-Methylnaphthalene 0.20U
1ug/L 24-Jul-2014 17:120.0332-Methylphenol 0.20U
1ug/L 24-Jul-2014 17:120.0382-Nitroaniline 0.20U
1ug/L 24-Jul-2014 17:120.0242-Nitrophenol 0.20U
1ug/L 24-Jul-2014 17:120.0303&4-Methylphenol 0.20U
1ug/L 24-Jul-2014 17:120.0243,3´-Dichlorobenzidine 0.20U
1ug/L 24-Jul-2014 17:120.0563-Nitroaniline 0.20U
1ug/L 24-Jul-2014 17:120.0734,6-Dinitro-2-methylphenol 0.20U
1ug/L 24-Jul-2014 17:120.0474-Bromophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 17:120.0224-Chloro-3-methylphenol 0.20U
1ug/L 24-Jul-2014 17:120.0214-Chloroaniline 0.20U
1ug/L 24-Jul-2014 17:120.0434-Chlorophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 17:120.0404-Nitroaniline 0.20U
1ug/L 24-Jul-2014 17:120.0604-Nitrophenol 1.0U
1ug/L 24-Jul-2014 17:120.030Acenaphthene 0.20U
1ug/L 24-Jul-2014 17:120.021Acenaphthylene 0.20U
1ug/L 24-Jul-2014 17:120.030Acetophenone 0.20U
1ug/L 24-Jul-2014 17:120.020Anthracene 0.20U
1ug/L 24-Jul-2014 17:120.040Atrazine 0.20U
1ug/L 24-Jul-2014 17:120.025Benz(a)anthracene 0.20U
1ug/L 24-Jul-2014 17:120.046Benzaldehyde 0.20U
1ug/L 24-Jul-2014 17:120.030Benzo(a)pyrene 0.20U
1ug/L 24-Jul-2014 17:120.028Benzo(b)fluoranthene 0.20U
1ug/L 24-Jul-2014 17:120.026Benzo(g,h,i)perylene 0.20U
1ug/L 24-Jul-2014 17:120.028Benzo(k)fluoranthene 0.20U
1ug/L 24-Jul-2014 17:120.022Bis(2-chloroethoxy)methane 0.20U
1ug/L 24-Jul-2014 17:120.029Bis(2-chloroethyl)ether 0.20U
1ug/L 24-Jul-2014 17:120.064Bis(2-chloroisopropyl)ether 0.20U
1ug/L 24-Jul-2014 17:120.033Bis(2-ethylhexyl)phthalate 0.200.46
1ug/L 24-Jul-2014 17:120.021Butyl benzyl phthalate 0.20U
1ug/L 24-Jul-2014 17:12J0.059Caprolactam 0.200.20
1ug/L 24-Jul-2014 17:120.025Carbazole 0.20U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-12 DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-05
15-Jul-2014 14:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 17:120.046Chrysene 0.20U
1ug/L 24-Jul-2014 17:120.026Dibenz(a,h)anthracene 0.20U
1ug/L 24-Jul-2014 17:120.025Dibenzofuran 0.20U
1ug/L 24-Jul-2014 17:120.021Diethyl phthalate 0.20U
1ug/L 24-Jul-2014 17:120.030Dimethyl phthalate 0.20U
1ug/L 24-Jul-2014 17:120.030Di-n-butyl phthalate 0.20U
1ug/L 24-Jul-2014 17:120.023Di-n-octyl phthalate 0.20U
1ug/L 24-Jul-2014 17:120.020Fluoranthene 0.20U
1ug/L 24-Jul-2014 17:120.021Fluorene 0.20U
1ug/L 24-Jul-2014 17:120.070Hexachlorobenzene 0.20U
1ug/L 24-Jul-2014 17:120.050Hexachlorobutadiene 0.20U
1ug/L 24-Jul-2014 17:120.054Hexachlorocyclopentadiene 0.20U
1ug/L 24-Jul-2014 17:120.034Hexachloroethane 0.20U
1ug/L 24-Jul-2014 17:120.051Indeno(1,2,3-cd)pyrene 0.20U
1ug/L 24-Jul-2014 17:120.030Isophorone 0.20U
1ug/L 24-Jul-2014 17:120.050Naphthalene 0.20U
1ug/L 24-Jul-2014 17:120.050Nitrobenzene 0.20U
1ug/L 24-Jul-2014 17:120.040N-Nitrosodi-n-propylamine 0.20U
1ug/L 24-Jul-2014 17:120.029N-Nitrosodiphenylamine 0.20U
1ug/L 24-Jul-2014 17:120.046Pentachlorophenol 0.20U
1ug/L 24-Jul-2014 17:120.020Phenanthrene 0.20U
1ug/L 24-Jul-2014 17:120.032Phenol 0.20U
1ug/L 24-Jul-2014 17:120.022Pyrene 0.20U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 17:1264.2 34-129
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 17:1250.3 40-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 17:1248.5 20-120
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 17:1269.0 40-135
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 17:1254.2 41-120
Surr: Phenol-d6 1%REC 24-Jul-2014 17:1250.6 20-120
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/L 23-Jul-2014 19:460.0100GRO (C6-C10)0.0500U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 19:4676.8 70-130
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3511 / 21-Jul-2014
1mg/L 30-Jul-2014 17:510.020TPH (Diesel Range)0.051U
1mg/L 30-Jul-2014 17:510.041TPH (Oil Range)0.10U
Surr: 2-Fluorobiphenyl 1%REC 30-Jul-2014 17:5182.7 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-13
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-06
15-Jul-2014 13:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 17:310.0321,1´-Biphenyl 0.20U
1ug/L 24-Jul-2014 17:310.0402,4,5-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 17:310.0602,4,6-Trichlorophenol 0.20U
1ug/L 24-Jul-2014 17:310.0652,4-Dichlorophenol 0.20U
1ug/L 24-Jul-2014 17:310.0332,4-Dimethylphenol 0.20U
1ug/L 24-Jul-2014 17:310.0502,4-Dinitrophenol 1.0U
1ug/L 24-Jul-2014 17:310.0302,4-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 17:310.0502,6-Dinitrotoluene 0.20U
1ug/L 24-Jul-2014 17:310.0402-Chloronaphthalene 0.20U
1ug/L 24-Jul-2014 17:310.0402-Chlorophenol 0.20U
1ug/L 24-Jul-2014 17:310.0342-Methylnaphthalene 0.20U
1ug/L 24-Jul-2014 17:310.0332-Methylphenol 0.20U
1ug/L 24-Jul-2014 17:310.0382-Nitroaniline 0.20U
1ug/L 24-Jul-2014 17:310.0242-Nitrophenol 0.20U
1ug/L 24-Jul-2014 17:310.0303&4-Methylphenol 0.20U
1ug/L 24-Jul-2014 17:310.0243,3´-Dichlorobenzidine 0.20U
1ug/L 24-Jul-2014 17:310.0563-Nitroaniline 0.20U
1ug/L 24-Jul-2014 17:310.0734,6-Dinitro-2-methylphenol 0.20U
1ug/L 24-Jul-2014 17:310.0474-Bromophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 17:310.0224-Chloro-3-methylphenol 0.20U
1ug/L 24-Jul-2014 17:310.0214-Chloroaniline 0.20U
1ug/L 24-Jul-2014 17:310.0434-Chlorophenyl phenyl ether 0.20U
1ug/L 24-Jul-2014 17:310.0404-Nitroaniline 0.20U
1ug/L 24-Jul-2014 17:310.0604-Nitrophenol 1.0U
1ug/L 24-Jul-2014 17:310.030Acenaphthene 0.20U
1ug/L 24-Jul-2014 17:310.021Acenaphthylene 0.20U
1ug/L 24-Jul-2014 17:310.030Acetophenone 0.20U
1ug/L 24-Jul-2014 17:310.020Anthracene 0.20U
1ug/L 24-Jul-2014 17:310.040Atrazine 0.20U
1ug/L 24-Jul-2014 17:310.025Benz(a)anthracene 0.20U
1ug/L 24-Jul-2014 17:310.046Benzaldehyde 0.20U
1ug/L 24-Jul-2014 17:310.030Benzo(a)pyrene 0.20U
1ug/L 24-Jul-2014 17:310.028Benzo(b)fluoranthene 0.20U
1ug/L 24-Jul-2014 17:310.026Benzo(g,h,i)perylene 0.20U
1ug/L 24-Jul-2014 17:310.028Benzo(k)fluoranthene 0.20U
1ug/L 24-Jul-2014 17:310.022Bis(2-chloroethoxy)methane 0.20U
1ug/L 24-Jul-2014 17:310.029Bis(2-chloroethyl)ether 0.20U
1ug/L 24-Jul-2014 17:310.064Bis(2-chloroisopropyl)ether 0.20U
1ug/L 24-Jul-2014 17:310.033Bis(2-ethylhexyl)phthalate 0.202.6
1ug/L 24-Jul-2014 17:310.021Butyl benzyl phthalate 0.20U
1ug/L 24-Jul-2014 17:31J0.059Caprolactam 0.200.10
1ug/L 24-Jul-2014 17:310.025Carbazole 0.20U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
MW-13
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-06
15-Jul-2014 13:00 Matrix:Water
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3510 / 21-Jul-2014
1ug/L 24-Jul-2014 17:310.046Chrysene 0.20U
1ug/L 24-Jul-2014 17:310.026Dibenz(a,h)anthracene 0.20U
1ug/L 24-Jul-2014 17:310.025Dibenzofuran 0.20U
1ug/L 24-Jul-2014 17:310.021Diethyl phthalate 0.20U
1ug/L 24-Jul-2014 17:310.030Dimethyl phthalate 0.20U
1ug/L 24-Jul-2014 17:31J0.030Di-n-butyl phthalate 0.200.088
1ug/L 24-Jul-2014 17:310.023Di-n-octyl phthalate 0.20U
1ug/L 24-Jul-2014 17:310.020Fluoranthene 0.20U
1ug/L 24-Jul-2014 17:310.021Fluorene 0.20U
1ug/L 24-Jul-2014 17:310.070Hexachlorobenzene 0.20U
1ug/L 24-Jul-2014 17:310.050Hexachlorobutadiene 0.20U
1ug/L 24-Jul-2014 17:310.054Hexachlorocyclopentadiene 0.20U
1ug/L 24-Jul-2014 17:310.034Hexachloroethane 0.20U
1ug/L 24-Jul-2014 17:310.051Indeno(1,2,3-cd)pyrene 0.20U
1ug/L 24-Jul-2014 17:310.030Isophorone 0.20U
1ug/L 24-Jul-2014 17:310.050Naphthalene 0.20U
1ug/L 24-Jul-2014 17:310.050Nitrobenzene 0.20U
1ug/L 24-Jul-2014 17:310.040N-Nitrosodi-n-propylamine 0.20U
1ug/L 24-Jul-2014 17:310.029N-Nitrosodiphenylamine 0.20U
1ug/L 24-Jul-2014 17:310.046Pentachlorophenol 0.20U
1ug/L 24-Jul-2014 17:310.020Phenanthrene 0.20U
1ug/L 24-Jul-2014 17:310.032Phenol 0.20U
1ug/L 24-Jul-2014 17:310.022Pyrene 0.20U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 17:3164.3 34-129
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 17:3148.2 40-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 17:3153.0 20-120
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 17:3178.2 40-135
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 17:3154.5 41-120
Surr: Phenol-d6 1%REC 24-Jul-2014 17:3150.5 20-120
MISC. GCFID PARAMETERS BY
SW8015C Method:SW8015 Analyst: SE
1mg/L 28-Jul-2014 16:061.0Ethylene Glycol 1.0U
1mg/L 28-Jul-2014 16:061.0Propylene glycol 1.0U
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/L 23-Jul-2014 21:520.0100GRO (C6-C10)0.0500U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 21:5275.9 70-130
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3511 / 21-Jul-2014
1mg/L 30-Jul-2014 18:170.021TPH (Diesel Range)0.051U
1mg/L 30-Jul-2014 18:170.041TPH (Oil Range)0.10U
Surr: 2-Fluorobiphenyl 1%REC 30-Jul-2014 18:1787.1 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-07
14-Jul-2014 13:50 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 13:291.71,1,1-Trichloroethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.511,1,2,2-Tetrachloroethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.31,1,2-Trichlor-1,2,2-trifluoroethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:292.01,1,2-Trichloroethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.511,1-Dichloroethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.51,1-Dichloroethene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.921,2,4-Trichlorobenzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.31,2-Dibromo-3-chloropropane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.711,2-Dibromoethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.811,2-Dichlorobenzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.611,2-Dichloroethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.511,2-Dichloropropane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.921,3-Dichlorobenzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.711,4-Dichlorobenzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:292.22-Butanone 10U
1ug/Kg-dry 22-Jul-2014 13:291.72-Hexanone 10U
1ug/Kg-dry 22-Jul-2014 13:291.04-Methyl-2-pentanone 10U
1ug/Kg-dry 22-Jul-2014 13:294.7Acetone 20U
1ug/Kg-dry 22-Jul-2014 13:290.61Benzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.61Bromodichloromethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.71Bromoform 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.0Bromomethane 10U
1ug/Kg-dry 22-Jul-2014 13:291.6Carbon disulfide 10U
1ug/Kg-dry 22-Jul-2014 13:291.2Carbon tetrachloride 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.51Chlorobenzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.0Chloroethane 10U
1ug/Kg-dry 22-Jul-2014 13:291.8Chloroform 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.92Chloromethane 10U
1ug/Kg-dry 22-Jul-2014 13:291.5cis-1,2-Dichloroethene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.51cis-1,3-Dichloropropene 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.2Cyclohexane 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.51Dibromochloromethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.8Dichlorodifluoromethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.4Dichloromethane 10U
1ug/Kg-dry 22-Jul-2014 13:290.92Ethylbenzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.0Isopropylbenzene 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.7m,p-Xylene 10U
1ug/Kg-dry 22-Jul-2014 13:291.0Methyl acetate 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.9Methyl tert-butyl ether 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.5Methylcyclohexane 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.0o-Xylene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.61Styrene 5.1U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-07
14-Jul-2014 13:50 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 13:291.0Tetrachloroethene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.71Toluene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.92trans-1,2-Dichloroethene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.51trans-1,3-Dichloropropene 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.6Trichloroethene 5.1U
1ug/Kg-dry 22-Jul-2014 13:290.81Trichlorofluoromethane 5.1U
1ug/Kg-dry 22-Jul-2014 13:291.0Vinyl chloride 2.0U
1ug/Kg-dry 22-Jul-2014 13:292.6Xylenes, Total 15U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2014 13:2990.3 70-128
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 13:2995.1 73-126
Surr: Dibromofluoromethane 1%REC 22-Jul-2014 13:2994.6 71-128
Surr: Toluene-d8 1%REC 22-Jul-2014 13:2910473-127
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-07
14-Jul-2014 13:50 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 14:580.931,1´-Biphenyl 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.72,4,5-Trichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.12,4,6-Trichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.22,4-Dichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.732,4-Dimethylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 14:581.42,4-Dinitrotoluene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.932,6-Dinitrotoluene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.22-Chloronaphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.12-Chlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.732-Methylnaphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.22-Methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.62-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.42-Nitrophenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.13&4-Methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.933,3´-Dichlorobenzidine 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.43-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.24,6-Dinitro-2-methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.44-Bromophenyl phenyl ether 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.94-Chloro-3-methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.734-Chloroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.64-Chlorophenyl phenyl ether 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.74-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.74-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 14:580.83Acenaphthene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Acenaphthylene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Acetophenone 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.2Anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 14:582.2Atrazine 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.93Benz(a)anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.83Benzaldehyde 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.62Benzo(a)pyrene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Benzo(b)fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Benzo(g,h,i)perylene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Benzo(k)fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.93Bis(2-chloroethoxy)methane 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.83Bis(2-chloroethyl)ether 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.7Bis(2-chloroisopropyl)ether 6.9U
1ug/Kg-dry 24-Jul-2014 14:58J1.6Bis(2-ethylhexyl)phthalate 6.91.9
1ug/Kg-dry 24-Jul-2014 14:581.4Butyl benzyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.2Caprolactam 6.911
1ug/Kg-dry 24-Jul-2014 14:581.0Carbazole 6.9U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-07
14-Jul-2014 13:50 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 14:580.62Chrysene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.0Dibenz(a,h)anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.0Dibenzofuran 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Diethyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.0Dimethyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.62Di-n-butyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.62Di-n-octyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.83Fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.4Fluorene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.83Hexachlorobenzene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.1Hexachlorobutadiene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.8Hexachlorocyclopentadiene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.9Hexachloroethane 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.93Indeno(1,2,3-cd)pyrene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.93Isophorone 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.83Naphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.0Nitrobenzene 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.5N-Nitrosodi-n-propylamine 6.9U
1ug/Kg-dry 24-Jul-2014 14:581.4N-Nitrosodiphenylamine 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.93Pentachlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Phenanthrene 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.73Phenol 6.9U
1ug/Kg-dry 24-Jul-2014 14:580.62Pyrene 6.9U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 14:5882.9 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 14:5886.1 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 14:5876.1 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 14:5884.1 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 14:5894.8 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 14:5871.5 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 21:310.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 21:3177.1 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.74
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 18:580.52TPH (Diesel Range)1.8U
1mg/Kg-dry 31-Jul-2014 18:580.52TPH (Motor Oil Range)3.5U
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 18:5895.5 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-08
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 15:031.41,1,1-Trichloroethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.401,1,2,2-Tetrachloroethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.01,1,2-Trichlor-1,2,2-trifluoroethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.61,1,2-Trichloroethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.401,1-Dichloroethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.21,1-Dichloroethene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.721,2,4-Trichlorobenzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.01,2-Dibromo-3-chloropropane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.561,2-Dibromoethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.641,2-Dichlorobenzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.481,2-Dichloroethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.401,2-Dichloropropane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.721,3-Dichlorobenzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.561,4-Dichlorobenzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.82-Butanone 8.0U
1ug/Kg-dry 22-Jul-2014 15:031.42-Hexanone 8.0U
1ug/Kg-dry 22-Jul-2014 15:030.804-Methyl-2-pentanone 8.0U
1ug/Kg-dry 22-Jul-2014 15:033.7Acetone 16U
1ug/Kg-dry 22-Jul-2014 15:030.48Benzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.48Bromodichloromethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.56Bromoform 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.80Bromomethane 8.0U
1ug/Kg-dry 22-Jul-2014 15:031.3Carbon disulfide 8.0U
1ug/Kg-dry 22-Jul-2014 15:030.96Carbon tetrachloride 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.40Chlorobenzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.80Chloroethane 8.0U
1ug/Kg-dry 22-Jul-2014 15:031.4Chloroform 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.72Chloromethane 8.0U
1ug/Kg-dry 22-Jul-2014 15:031.2cis-1,2-Dichloroethene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.40cis-1,3-Dichloropropene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.96Cyclohexane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.40Dibromochloromethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.4Dichlorodifluoromethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.1Dichloromethane 8.0U
1ug/Kg-dry 22-Jul-2014 15:030.72Ethylbenzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.80Isopropylbenzene 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.4m,p-Xylene 8.0U
1ug/Kg-dry 22-Jul-2014 15:030.80Methyl acetate 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.5Methyl tert-butyl ether 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.2Methylcyclohexane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.80o-Xylene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.48Styrene 4.0U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-08
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 15:030.80Tetrachloroethene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.56Toluene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.72trans-1,2-Dichloroethene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.40trans-1,3-Dichloropropene 4.0U
1ug/Kg-dry 22-Jul-2014 15:031.3Trichloroethene 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.64Trichlorofluoromethane 4.0U
1ug/Kg-dry 22-Jul-2014 15:030.80Vinyl chloride 1.6U
1ug/Kg-dry 22-Jul-2014 15:032.1Xylenes, Total 12U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2014 15:0387.2 70-128
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 15:0391.6 73-126
Surr: Dibromofluoromethane 1%REC 22-Jul-2014 15:0392.3 71-128
Surr: Toluene-d8 1%REC 22-Jul-2014 15:0399.2 73-127
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-08
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 18:460.941,1´-Biphenyl 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.72,4,5-Trichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.12,4,6-Trichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.22,4-Dichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.732,4-Dimethylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 18:461.42,4-Dinitrotoluene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.942,6-Dinitrotoluene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.22-Chloronaphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.12-Chlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.732-Methylnaphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.22-Methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.62-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.42-Nitrophenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.13&4-Methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.943,3´-Dichlorobenzidine 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.43-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.24,6-Dinitro-2-methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.44-Bromophenyl phenyl ether 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.94-Chloro-3-methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.734-Chloroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.64-Chlorophenyl phenyl ether 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.74-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.74-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 18:460.83Acenaphthene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Acenaphthylene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Acetophenone 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.2Anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 18:462.2Atrazine 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.94Benz(a)anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.83Benzaldehyde 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.62Benzo(a)pyrene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Benzo(b)fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Benzo(g,h,i)perylene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Benzo(k)fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.94Bis(2-chloroethoxy)methane 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.83Bis(2-chloroethyl)ether 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.7Bis(2-chloroisopropyl)ether 6.9U
1ug/Kg-dry 24-Jul-2014 18:46J1.6Bis(2-ethylhexyl)phthalate 6.94.4
1ug/Kg-dry 24-Jul-2014 18:461.4Butyl benzyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 18:46J1.2Caprolactam 6.93.8
1ug/Kg-dry 24-Jul-2014 18:461.0Carbazole 6.9U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-08
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 18:460.62Chrysene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.0Dibenz(a,h)anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.0Dibenzofuran 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Diethyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.0Dimethyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.62Di-n-butyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.62Di-n-octyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.83Fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.4Fluorene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.83Hexachlorobenzene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.1Hexachlorobutadiene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.8Hexachlorocyclopentadiene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.9Hexachloroethane 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.94Indeno(1,2,3-cd)pyrene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.94Isophorone 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.83Naphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.0Nitrobenzene 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.5N-Nitrosodi-n-propylamine 6.9U
1ug/Kg-dry 24-Jul-2014 18:461.4N-Nitrosodiphenylamine 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.94Pentachlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Phenanthrene 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.73Phenol 6.9U
1ug/Kg-dry 24-Jul-2014 18:460.62Pyrene 6.9U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 18:4679.1 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 18:4676.8 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 18:4678.2 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 18:4686.9 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 18:4682.4 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 18:4676.1 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 20:110.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 20:1174.6 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.91
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 19:21J0.52TPH (Diesel Range)1.81.1
1mg/Kg-dry 31-Jul-2014 19:210.52TPH (Motor Oil Range)3.58.8
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 19:2195.9 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5) DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-09
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 15:261.21,1,1-Trichloroethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.351,1,2,2-Tetrachloroethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.901,1,2-Trichlor-1,2,2-trifluoroethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.41,1,2-Trichloroethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.351,1-Dichloroethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.01,1-Dichloroethene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.621,2,4-Trichlorobenzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.901,2-Dibromo-3-chloropropane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.481,2-Dibromoethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.551,2-Dichlorobenzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.421,2-Dichloroethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.351,2-Dichloropropane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.621,3-Dichlorobenzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.481,4-Dichlorobenzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.52-Butanone 6.9U
1ug/Kg-dry 22-Jul-2014 15:261.22-Hexanone 6.9U
1ug/Kg-dry 22-Jul-2014 15:260.694-Methyl-2-pentanone 6.9U
1ug/Kg-dry 22-Jul-2014 15:263.2Acetone 14U
1ug/Kg-dry 22-Jul-2014 15:260.42Benzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.42Bromodichloromethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.48Bromoform 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.69Bromomethane 6.9U
1ug/Kg-dry 22-Jul-2014 15:261.1Carbon disulfide 6.9U
1ug/Kg-dry 22-Jul-2014 15:260.83Carbon tetrachloride 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.35Chlorobenzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.69Chloroethane 6.9U
1ug/Kg-dry 22-Jul-2014 15:261.2Chloroform 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.62Chloromethane 6.9U
1ug/Kg-dry 22-Jul-2014 15:261.0cis-1,2-Dichloroethene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.35cis-1,3-Dichloropropene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.83Cyclohexane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.35Dibromochloromethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.2Dichlorodifluoromethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.97Dichloromethane 6.9U
1ug/Kg-dry 22-Jul-2014 15:260.62Ethylbenzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.69Isopropylbenzene 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.2m,p-Xylene 6.9U
1ug/Kg-dry 22-Jul-2014 15:260.69Methyl acetate 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.3Methyl tert-butyl ether 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.0Methylcyclohexane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.69o-Xylene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.42Styrene 3.5U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5) DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-09
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 15:260.69Tetrachloroethene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.48Toluene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.62trans-1,2-Dichloroethene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.35trans-1,3-Dichloropropene 3.5U
1ug/Kg-dry 22-Jul-2014 15:261.1Trichloroethene 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.55Trichlorofluoromethane 3.5U
1ug/Kg-dry 22-Jul-2014 15:260.69Vinyl chloride 1.4U
1ug/Kg-dry 22-Jul-2014 15:261.8Xylenes, Total 10U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2014 15:2690.7 70-128
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 15:2690.7 73-126
Surr: Dibromofluoromethane 1%REC 22-Jul-2014 15:2691.1 71-128
Surr: Toluene-d8 1%REC 22-Jul-2014 15:2610373-127
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5) DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-09
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 19:050.941,1´-Biphenyl 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.72,4,5-Trichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.22,4,6-Trichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.32,4-Dichlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.732,4-Dimethylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 19:051.42,4-Dinitrotoluene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.942,6-Dinitrotoluene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.32-Chloronaphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.22-Chlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.732-Methylnaphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.32-Methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.62-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.42-Nitrophenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.23&4-Methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.943,3´-Dichlorobenzidine 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.43-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.34,6-Dinitro-2-methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.44-Bromophenyl phenyl ether 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.94-Chloro-3-methylphenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.734-Chloroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.64-Chlorophenyl phenyl ether 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.74-Nitroaniline 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.74-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 19:050.84Acenaphthene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Acenaphthylene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Acetophenone 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.3Anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 19:052.2Atrazine 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.94Benz(a)anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.84Benzaldehyde 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.63Benzo(a)pyrene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Benzo(b)fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Benzo(g,h,i)perylene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Benzo(k)fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.94Bis(2-chloroethoxy)methane 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.84Bis(2-chloroethyl)ether 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.7Bis(2-chloroisopropyl)ether 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.6Bis(2-ethylhexyl)phthalate 6.98.0
1ug/Kg-dry 24-Jul-2014 19:051.4Butyl benzyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.3Caprolactam 6.99.8
1ug/Kg-dry 24-Jul-2014 19:051.0Carbazole 6.9U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-18B (4.5-5.5) DUP
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-09
14-Jul-2014 14:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 19:050.63Chrysene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.0Dibenz(a,h)anthracene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.0Dibenzofuran 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Diethyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.0Dimethyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 19:05J0.63Di-n-butyl phthalate 6.92.3
1ug/Kg-dry 24-Jul-2014 19:050.63Di-n-octyl phthalate 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.84Fluoranthene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.4Fluorene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.84Hexachlorobenzene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.2Hexachlorobutadiene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.8Hexachlorocyclopentadiene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.9Hexachloroethane 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.94Indeno(1,2,3-cd)pyrene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.94Isophorone 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.84Naphthalene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.0Nitrobenzene 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.5N-Nitrosodi-n-propylamine 6.9U
1ug/Kg-dry 24-Jul-2014 19:051.4N-Nitrosodiphenylamine 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.94Pentachlorophenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Phenanthrene 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.73Phenol 6.9U
1ug/Kg-dry 24-Jul-2014 19:050.63Pyrene 6.9U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 19:0570.3 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 19:0567.6 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 19:0576.7 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 19:0574.3 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 19:0573.7 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 19:0573.7 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 23-Jul-2014 14:070.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 14:0780.0 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01004.68
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 19:43J0.52TPH (Diesel Range)1.80.53
1mg/Kg-dry 31-Jul-2014 19:430.52TPH (Motor Oil Range)3.67.9
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 19:4377.6 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-10
14-Jul-2014 17:45 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 15:491.91,1,1-Trichloroethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.571,1,2,2-Tetrachloroethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.51,1,2-Trichlor-1,2,2-trifluoroethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:492.31,1,2-Trichloroethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.571,1-Dichloroethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.71,1-Dichloroethene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.01,2,4-Trichlorobenzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.51,2-Dibromo-3-chloropropane 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.791,2-Dibromoethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.911,2-Dichlorobenzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.681,2-Dichloroethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.571,2-Dichloropropane 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.01,3-Dichlorobenzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.791,4-Dichlorobenzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:492.52-Butanone 11U
1ug/Kg-dry 22-Jul-2014 15:491.92-Hexanone 11U
1ug/Kg-dry 22-Jul-2014 15:491.14-Methyl-2-pentanone 11U
1ug/Kg-dry 22-Jul-2014 15:495.2Acetone 23U
1ug/Kg-dry 22-Jul-2014 15:490.68Benzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.68Bromodichloromethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.79Bromoform 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.1Bromomethane 11U
1ug/Kg-dry 22-Jul-2014 15:491.8Carbon disulfide 11U
1ug/Kg-dry 22-Jul-2014 15:491.4Carbon tetrachloride 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.57Chlorobenzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.1Chloroethane 11U
1ug/Kg-dry 22-Jul-2014 15:492.0Chloroform 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.0Chloromethane 11U
1ug/Kg-dry 22-Jul-2014 15:491.7cis-1,2-Dichloroethene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.57cis-1,3-Dichloropropene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.4Cyclohexane 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.57Dibromochloromethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:492.0Dichlorodifluoromethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.6Dichloromethane 11U
1ug/Kg-dry 22-Jul-2014 15:491.0Ethylbenzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.1Isopropylbenzene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.9m,p-Xylene 11U
1ug/Kg-dry 22-Jul-2014 15:491.1Methyl acetate 5.7U
1ug/Kg-dry 22-Jul-2014 15:492.2Methyl tert-butyl ether 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.7Methylcyclohexane 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.1o-Xylene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.68Styrene 5.7U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-10
14-Jul-2014 17:45 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 15:491.1Tetrachloroethene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.79Toluene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.0trans-1,2-Dichloroethene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.57trans-1,3-Dichloropropene 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.8Trichloroethene 5.7U
1ug/Kg-dry 22-Jul-2014 15:490.91Trichlorofluoromethane 5.7U
1ug/Kg-dry 22-Jul-2014 15:491.1Vinyl chloride 2.3U
1ug/Kg-dry 22-Jul-2014 15:493.0Xylenes, Total 17U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2014 15:4987.5 70-128
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 15:4990.8 73-126
Surr: Dibromofluoromethane 1%REC 22-Jul-2014 15:4991.5 71-128
Surr: Toluene-d8 1%REC 22-Jul-2014 15:4999.7 73-127
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-10
14-Jul-2014 17:45 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 19:240.931,1´-Biphenyl 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.62,4,5-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.12,4,6-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.22,4-Dichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.722,4-Dimethylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 19:241.32,4-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.932,6-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.22-Chloronaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.12-Chlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.722-Methylnaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.22-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.52-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.32-Nitrophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.13&4-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.933,3´-Dichlorobenzidine 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.33-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.24,6-Dinitro-2-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.34-Bromophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.94-Chloro-3-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.724-Chloroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.54-Chlorophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.64-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.64-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 19:240.82Acenaphthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Acenaphthylene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Acetophenone 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.2Anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 19:242.2Atrazine 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.93Benz(a)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.82Benzaldehyde 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.62Benzo(a)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Benzo(b)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Benzo(g,h,i)perylene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Benzo(k)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.93Bis(2-chloroethoxy)methane 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.82Bis(2-chloroethyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.6Bis(2-chloroisopropyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.5Bis(2-ethylhexyl)phthalate 6.89.0
1ug/Kg-dry 24-Jul-2014 19:241.3Butyl benzyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.2Caprolactam 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.0Carbazole 6.8U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-10
14-Jul-2014 17:45 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 19:240.62Chrysene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.0Dibenz(a,h)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.0Dibenzofuran 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Diethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.0Dimethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:24J0.62Di-n-butyl phthalate 6.81.8
1ug/Kg-dry 24-Jul-2014 19:240.62Di-n-octyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.82Fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.3Fluorene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.82Hexachlorobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.1Hexachlorobutadiene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.7Hexachlorocyclopentadiene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.9Hexachloroethane 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.93Indeno(1,2,3-cd)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.93Isophorone 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.82Naphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.0Nitrobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.4N-Nitrosodi-n-propylamine 6.8U
1ug/Kg-dry 24-Jul-2014 19:241.3N-Nitrosodiphenylamine 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.93Pentachlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Phenanthrene 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.72Phenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:240.62Pyrene 6.8U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 19:2473.1 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 19:2464.4 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 19:2458.9 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 19:2474.9 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 19:2471.4 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 19:2466.3 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 20:430.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 20:4376.8 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.14
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 20:060.51TPH (Diesel Range)1.7U
1mg/Kg-dry 31-Jul-2014 20:06J0.51TPH (Motor Oil Range)3.51.9
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 20:0691.8 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-11
14-Jul-2014 17:55 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 16:131.71,1,1-Trichloroethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.491,1,2,2-Tetrachloroethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.31,1,2-Trichlor-1,2,2-trifluoroethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:132.01,1,2-Trichloroethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.491,1-Dichloroethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.51,1-Dichloroethene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.891,2,4-Trichlorobenzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.31,2-Dibromo-3-chloropropane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.691,2-Dibromoethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.791,2-Dichlorobenzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.591,2-Dichloroethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.491,2-Dichloropropane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.891,3-Dichlorobenzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.691,4-Dichlorobenzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:132.22-Butanone 9.8U
1ug/Kg-dry 22-Jul-2014 16:131.72-Hexanone 9.8U
1ug/Kg-dry 22-Jul-2014 16:130.984-Methyl-2-pentanone 9.8U
1ug/Kg-dry 22-Jul-2014 16:134.5Acetone 20U
1ug/Kg-dry 22-Jul-2014 16:130.59Benzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.59Bromodichloromethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.69Bromoform 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.98Bromomethane 9.8U
1ug/Kg-dry 22-Jul-2014 16:131.6Carbon disulfide 9.8U
1ug/Kg-dry 22-Jul-2014 16:131.2Carbon tetrachloride 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.49Chlorobenzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.98Chloroethane 9.8U
1ug/Kg-dry 22-Jul-2014 16:131.8Chloroform 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.89Chloromethane 9.8U
1ug/Kg-dry 22-Jul-2014 16:131.5cis-1,2-Dichloroethene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.49cis-1,3-Dichloropropene 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.2Cyclohexane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.49Dibromochloromethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.8Dichlorodifluoromethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.4Dichloromethane 9.8U
1ug/Kg-dry 22-Jul-2014 16:130.89Ethylbenzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.98Isopropylbenzene 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.7m,p-Xylene 9.8U
1ug/Kg-dry 22-Jul-2014 16:130.98Methyl acetate 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.9Methyl tert-butyl ether 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.5Methylcyclohexane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.98o-Xylene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.59Styrene 4.9U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-11
14-Jul-2014 17:55 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
TCL VOLATILES - SW8260C Method:SW8260 Analyst: WLR
1ug/Kg-dry 22-Jul-2014 16:130.98Tetrachloroethene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.69Toluene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.89trans-1,2-Dichloroethene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.49trans-1,3-Dichloropropene 4.9U
1ug/Kg-dry 22-Jul-2014 16:131.6Trichloroethene 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.79Trichlorofluoromethane 4.9U
1ug/Kg-dry 22-Jul-2014 16:130.98Vinyl chloride 2.0U
1ug/Kg-dry 22-Jul-2014 16:132.6Xylenes, Total 15U
Surr: 1,2-Dichloroethane-d4 1%REC 22-Jul-2014 16:1390.1 70-128
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 16:1390.3 73-126
Surr: Dibromofluoromethane 1%REC 22-Jul-2014 16:1393.2 71-128
Surr: Toluene-d8 1%REC 22-Jul-2014 16:1310073-127
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-11
14-Jul-2014 17:55 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 19:430.931,1´-Biphenyl 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.72,4,5-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.12,4,6-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.22,4-Dichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.722,4-Dimethylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 19:431.32,4-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.932,6-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.22-Chloronaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.12-Chlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.722-Methylnaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.22-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.52-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.32-Nitrophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.13&4-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.933,3´-Dichlorobenzidine 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.33-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.24,6-Dinitro-2-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.34-Bromophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.94-Chloro-3-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.724-Chloroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.54-Chlorophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.74-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.74-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 19:430.83Acenaphthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Acenaphthylene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Acetophenone 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.2Anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 19:432.2Atrazine 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.93Benz(a)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.83Benzaldehyde 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.62Benzo(a)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Benzo(b)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Benzo(g,h,i)perylene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Benzo(k)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.93Bis(2-chloroethoxy)methane 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.83Bis(2-chloroethyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.7Bis(2-chloroisopropyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 19:43J1.5Bis(2-ethylhexyl)phthalate 6.84.9
1ug/Kg-dry 24-Jul-2014 19:431.3Butyl benzyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.2Caprolactam 6.88.5
1ug/Kg-dry 24-Jul-2014 19:431.0Carbazole 6.8U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-17B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-11
14-Jul-2014 17:55 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 19:430.62Chrysene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.0Dibenz(a,h)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.0Dibenzofuran 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Diethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.0Dimethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.62Di-n-butyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.62Di-n-octyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.83Fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.3Fluorene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.83Hexachlorobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.1Hexachlorobutadiene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.8Hexachlorocyclopentadiene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.9Hexachloroethane 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.93Indeno(1,2,3-cd)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.93Isophorone 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.83Naphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.0Nitrobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.4N-Nitrosodi-n-propylamine 6.8U
1ug/Kg-dry 24-Jul-2014 19:431.3N-Nitrosodiphenylamine 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.93Pentachlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Phenanthrene 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.72Phenol 6.8U
1ug/Kg-dry 24-Jul-2014 19:430.62Pyrene 6.8U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 19:4376.8 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 19:4376.1 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 19:4382.5 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 19:4386.4 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 19:4384.8 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 19:4377.3 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 20:580.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 20:5878.0 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.49
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 20:280.52TPH (Diesel Range)1.8U
1mg/Kg-dry 31-Jul-2014 20:280.52TPH (Motor Oil Range)3.55.7
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 20:2879.4 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-19A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-12
14-Jul-2014 16:53 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:020.931,1´-Biphenyl 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.62,4,5-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.12,4,6-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.22,4-Dichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.722,4-Dimethylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:021.32,4-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.932,6-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.22-Chloronaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.12-Chlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.722-Methylnaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.22-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.52-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.32-Nitrophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.13&4-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.933,3´-Dichlorobenzidine 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.33-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.24,6-Dinitro-2-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.34-Bromophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.94-Chloro-3-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.724-Chloroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.54-Chlorophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.64-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.64-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:020.82Acenaphthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Acenaphthylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Acetophenone 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.2Anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:022.2Atrazine 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.93Benz(a)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.82Benzaldehyde 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.62Benzo(a)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Benzo(b)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Benzo(g,h,i)perylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Benzo(k)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.93Bis(2-chloroethoxy)methane 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.82Bis(2-chloroethyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.6Bis(2-chloroisopropyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:02J1.5Bis(2-ethylhexyl)phthalate 6.82.3
1ug/Kg-dry 24-Jul-2014 20:021.3Butyl benzyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:02J1.2Caprolactam 6.86.7
1ug/Kg-dry 24-Jul-2014 20:021.0Carbazole 6.8U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-19A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-12
14-Jul-2014 16:53 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:020.62Chrysene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.0Dibenz(a,h)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.0Dibenzofuran 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Diethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.0Dimethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.62Di-n-butyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.62Di-n-octyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.82Fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.3Fluorene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.82Hexachlorobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.1Hexachlorobutadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.7Hexachlorocyclopentadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.9Hexachloroethane 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.93Indeno(1,2,3-cd)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.93Isophorone 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.82Naphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.0Nitrobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.4N-Nitrosodi-n-propylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:021.3N-Nitrosodiphenylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.93Pentachlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Phenanthrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.72Phenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:020.62Pyrene 6.8U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 20:0270.7 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 20:0270.2 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 20:0274.7 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 20:0278.8 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 20:0277.7 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 20:0271.4 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 21:150.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 21:1575.4 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.13
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 20:510.52TPH (Diesel Range)1.8U
1mg/Kg-dry 31-Jul-2014 20:51J0.52TPH (Motor Oil Range)3.52.6
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 20:5177.6 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-19B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-13
14-Jul-2014 17:06 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:210.931,1´-Biphenyl 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.62,4,5-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.12,4,6-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.22,4-Dichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.722,4-Dimethylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:211.32,4-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.932,6-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.22-Chloronaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.12-Chlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.722-Methylnaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.22-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.52-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.32-Nitrophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.13&4-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.933,3´-Dichlorobenzidine 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.33-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.24,6-Dinitro-2-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.34-Bromophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.94-Chloro-3-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.724-Chloroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.54-Chlorophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.64-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.64-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:210.82Acenaphthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.72Acenaphthylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.72Acetophenone 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.2Anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:212.2Atrazine 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.93Benz(a)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.82Benzaldehyde 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.62Benzo(a)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.72Benzo(b)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.72Benzo(g,h,i)perylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.72Benzo(k)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.93Bis(2-chloroethoxy)methane 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.82Bis(2-chloroethyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.6Bis(2-chloroisopropyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:21J1.5Bis(2-ethylhexyl)phthalate 6.83.4
1ug/Kg-dry 24-Jul-2014 20:211.3Butyl benzyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.2Caprolactam 6.88.9
1ug/Kg-dry 24-Jul-2014 20:211.0Carbazole 6.8U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-19B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-13
14-Jul-2014 17:06 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:210.62Chrysene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.0Dibenz(a,h)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.0Dibenzofuran 6.8U
1ug/Kg-dry 24-Jul-2014 20:21J0.72Diethyl phthalate 6.81.8
1ug/Kg-dry 24-Jul-2014 20:211.0Dimethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.62Di-n-butyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.62Di-n-octyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.82Fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.3Fluorene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.82Hexachlorobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.1Hexachlorobutadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.8Hexachlorocyclopentadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.9Hexachloroethane 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.93Indeno(1,2,3-cd)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.93Isophorone 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.82Naphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.0Nitrobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.4N-Nitrosodi-n-propylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:211.3N-Nitrosodiphenylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.93Pentachlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.72Phenanthrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.72Phenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:210.62Pyrene 6.8U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 20:2182.9 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 20:2177.8 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 20:2183.8 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 20:2188.3 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 20:2184.4 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 20:2181.3 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 22:510.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 22:5178.7 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.07
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 21:14J0.52TPH (Diesel Range)1.80.76
1mg/Kg-dry 31-Jul-2014 21:140.52TPH (Motor Oil Range)3.54.0
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 21:1491.3 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-20A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-14
14-Jul-2014 15:30 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:400.931,1´-Biphenyl 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.72,4,5-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.12,4,6-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.22,4-Dichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.722,4-Dimethylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:401.32,4-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.932,6-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.22-Chloronaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.12-Chlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.722-Methylnaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.22-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.52-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.32-Nitrophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.13&4-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.933,3´-Dichlorobenzidine 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.33-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.24,6-Dinitro-2-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.34-Bromophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.94-Chloro-3-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.724-Chloroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.54-Chlorophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.74-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.74-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:400.83Acenaphthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Acenaphthylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Acetophenone 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.2Anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:402.2Atrazine 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.93Benz(a)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.83Benzaldehyde 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.62Benzo(a)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Benzo(b)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Benzo(g,h,i)perylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Benzo(k)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.93Bis(2-chloroethoxy)methane 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.83Bis(2-chloroethyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.7Bis(2-chloroisopropyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:40J1.5Bis(2-ethylhexyl)phthalate 6.82.2
1ug/Kg-dry 24-Jul-2014 20:401.3Butyl benzyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.2Caprolactam 6.87.8
1ug/Kg-dry 24-Jul-2014 20:401.0Carbazole 6.8U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-20A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-14
14-Jul-2014 15:30 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:400.62Chrysene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.0Dibenz(a,h)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.0Dibenzofuran 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Diethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.0Dimethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:40J0.62Di-n-butyl phthalate 6.81.9
1ug/Kg-dry 24-Jul-2014 20:400.62Di-n-octyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.83Fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.3Fluorene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.83Hexachlorobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.1Hexachlorobutadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.8Hexachlorocyclopentadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.9Hexachloroethane 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.93Indeno(1,2,3-cd)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.93Isophorone 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.83Naphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.0Nitrobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.4N-Nitrosodi-n-propylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:401.3N-Nitrosodiphenylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.93Pentachlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Phenanthrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.72Phenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:400.62Pyrene 6.8U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 20:4080.0 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 20:4077.6 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 20:4083.6 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 20:4087.1 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 20:4085.4 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 20:4080.6 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 23:070.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 23:0776.1 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.43
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 22:220.52TPH (Diesel Range)1.8U
1mg/Kg-dry 31-Jul-2014 22:22J0.52TPH (Motor Oil Range)3.50.64
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 22:2275.8 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-20B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-15
14-Jul-2014 15:50 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:590.931,1´-Biphenyl 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.72,4,5-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.12,4,6-Trichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.22,4-Dichlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.722,4-Dimethylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.02,4-Dinitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:591.32,4-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.932,6-Dinitrotoluene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.22-Chloronaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.12-Chlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.722-Methylnaphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.22-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.62-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.32-Nitrophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.13&4-Methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.933,3´-Dichlorobenzidine 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.33-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.24,6-Dinitro-2-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.34-Bromophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.94-Chloro-3-methylphenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.724-Chloroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.64-Chlorophenyl phenyl ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.74-Nitroaniline 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.74-Nitrophenol 14U
1ug/Kg-dry 24-Jul-2014 20:590.83Acenaphthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.72Acenaphthylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.72Acetophenone 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.2Anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:592.2Atrazine 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.93Benz(a)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.83Benzaldehyde 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.62Benzo(a)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:59J0.72Benzo(b)fluoranthene 6.81.6
1ug/Kg-dry 24-Jul-2014 20:590.72Benzo(g,h,i)perylene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.72Benzo(k)fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.93Bis(2-chloroethoxy)methane 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.83Bis(2-chloroethyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.7Bis(2-chloroisopropyl)ether 6.8U
1ug/Kg-dry 24-Jul-2014 20:59J1.6Bis(2-ethylhexyl)phthalate 6.85.8
1ug/Kg-dry 24-Jul-2014 20:591.3Butyl benzyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.2Caprolactam 6.88.0
1ug/Kg-dry 24-Jul-2014 20:591.0Carbazole 6.8U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-20B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-15
14-Jul-2014 15:50 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 20:59J0.62Chrysene 6.82.2
1ug/Kg-dry 24-Jul-2014 20:591.0Dibenz(a,h)anthracene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.0Dibenzofuran 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.72Diethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.0Dimethyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.62Di-n-butyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.62Di-n-octyl phthalate 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.83Fluoranthene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.3Fluorene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.83Hexachlorobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.1Hexachlorobutadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.8Hexachlorocyclopentadiene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.9Hexachloroethane 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.93Indeno(1,2,3-cd)pyrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.93Isophorone 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.83Naphthalene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.0Nitrobenzene 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.4N-Nitrosodi-n-propylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:591.3N-Nitrosodiphenylamine 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.93Pentachlorophenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.72Phenanthrene 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.72Phenol 6.8U
1ug/Kg-dry 24-Jul-2014 20:590.62Pyrene 6.8U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 20:5981.1 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 20:5970.0 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 20:5977.1 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 20:5989.2 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 20:5975.6 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 20:5973.7 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 23:230.010GRO (C6-C10)0.052U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 23:2377.2 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.01003.42
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 18:130.52TPH (Diesel Range)1.8U
1mg/Kg-dry 31-Jul-2014 18:13J0.52TPH (Motor Oil Range)3.50.82
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 18:1382.1 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-9A (3.5-4.0)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-16
15-Jul-2014 08:35 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-10A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-17
15-Jul-2014 10:00 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-10B (4-5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-18
15-Jul-2014 10:05 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-11A
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-19
15-Jul-2014 09:30 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 21:181.21,1´-Biphenyl 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.12,4,5-Trichlorophenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.42,4,6-Trichlorophenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.62,4-Dichlorophenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:180.912,4-Dimethylphenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.32,4-Dinitrophenol 17U
1ug/Kg-dry 24-Jul-2014 21:181.72,4-Dinitrotoluene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.22,6-Dinitrotoluene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.62-Chloronaphthalene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.42-Chlorophenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:180.912-Methylnaphthalene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.62-Methylphenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.92-Nitroaniline 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.72-Nitrophenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J1.43&4-Methylphenol 8.62.4
1ug/Kg-dry 24-Jul-2014 21:181.23,3´-Dichlorobenzidine 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.73-Nitroaniline 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.64,6-Dinitro-2-methylphenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.74-Bromophenyl phenyl ether 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.34-Chloro-3-methylphenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:180.914-Chloroaniline 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.94-Chlorophenyl phenyl ether 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.14-Nitroaniline 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.14-Nitrophenol 17U
1ug/Kg-dry 24-Jul-2014 21:181.0Acenaphthene 8.6U
1ug/Kg-dry 24-Jul-2014 21:180.91Acenaphthylene 8.6U
1ug/Kg-dry 24-Jul-2014 21:180.91Acetophenone 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.6Anthracene 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.7Atrazine 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J1.2Benz(a)anthracene 8.63.1
1ug/Kg-dry 24-Jul-2014 21:181.0Benzaldehyde 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J0.78Benzo(a)pyrene 8.62.2
1ug/Kg-dry 24-Jul-2014 21:18J0.91Benzo(b)fluoranthene 8.63.9
1ug/Kg-dry 24-Jul-2014 21:180.91Benzo(g,h,i)perylene 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J0.91Benzo(k)fluoranthene 8.62.0
1ug/Kg-dry 24-Jul-2014 21:181.2Bis(2-chloroethoxy)methane 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.0Bis(2-chloroethyl)ether 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.1Bis(2-chloroisopropyl)ether 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J1.9Bis(2-ethylhexyl)phthalate 8.63.5
1ug/Kg-dry 24-Jul-2014 21:181.7Butyl benzyl phthalate 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.6Caprolactam 8.626
1ug/Kg-dry 24-Jul-2014 21:181.3Carbazole 8.6U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-11A
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-19
15-Jul-2014 09:30 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 21:18J0.78Chrysene 8.63.8
1ug/Kg-dry 24-Jul-2014 21:181.3Dibenz(a,h)anthracene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.3Dibenzofuran 8.6U
1ug/Kg-dry 24-Jul-2014 21:180.91Diethyl phthalate 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.3Dimethyl phthalate 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J0.78Di-n-butyl phthalate 8.62.2
1ug/Kg-dry 24-Jul-2014 21:180.78Di-n-octyl phthalate 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J1.0Fluoranthene 8.65.2
1ug/Kg-dry 24-Jul-2014 21:181.7Fluorene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.0Hexachlorobenzene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.4Hexachlorobutadiene 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.2Hexachlorocyclopentadiene 8.6U
1ug/Kg-dry 24-Jul-2014 21:182.3Hexachloroethane 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J1.2Indeno(1,2,3-cd)pyrene 8.62.2
1ug/Kg-dry 24-Jul-2014 21:181.2Isophorone 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.0Naphthalene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.3Nitrobenzene 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.8N-Nitrosodi-n-propylamine 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.7N-Nitrosodiphenylamine 8.6U
1ug/Kg-dry 24-Jul-2014 21:181.2Pentachlorophenol 8.6U
1ug/Kg-dry 24-Jul-2014 21:18J0.91Phenanthrene 8.62.8
1ug/Kg-dry 24-Jul-2014 21:18J0.91Phenol 8.61.9
1ug/Kg-dry 24-Jul-2014 21:18J0.78Pyrene 8.64.3
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 21:1880.0 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 21:1873.3 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 21:1877.8 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 21:1884.1 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 21:1880.0 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 21:1875.0 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 23:390.013GRO (C6-C10)0.065U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 23:3974.7 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010022.8
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 18:35J0.65TPH (Diesel Range)2.20.93
1mg/Kg-dry 31-Jul-2014 18:350.65TPH (Motor Oil Range)4.413
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 18:3573.8 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-11B
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-20
15-Jul-2014 09:35 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 21:361.11,1´-Biphenyl 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.02,4,5-Trichlorophenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.42,4,6-Trichlorophenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.52,4-Dichlorophenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.862,4-Dimethylphenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.22,4-Dinitrophenol 16U
1ug/Kg-dry 24-Jul-2014 21:361.62,4-Dinitrotoluene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.12,6-Dinitrotoluene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.52-Chloronaphthalene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.42-Chlorophenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.862-Methylnaphthalene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.52-Methylphenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.92-Nitroaniline 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.62-Nitrophenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.43&4-Methylphenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.13,3´-Dichlorobenzidine 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.63-Nitroaniline 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.54,6-Dinitro-2-methylphenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.64-Bromophenyl phenyl ether 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.24-Chloro-3-methylphenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.864-Chloroaniline 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.94-Chlorophenyl phenyl ether 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.04-Nitroaniline 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.04-Nitrophenol 16U
1ug/Kg-dry 24-Jul-2014 21:360.99Acenaphthene 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.86Acenaphthylene 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.86Acetophenone 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.5Anthracene 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.6Atrazine 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.1Benz(a)anthracene 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.99Benzaldehyde 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.74Benzo(a)pyrene 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.86Benzo(b)fluoranthene 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.86Benzo(g,h,i)perylene 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.86Benzo(k)fluoranthene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.1Bis(2-chloroethoxy)methane 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.99Bis(2-chloroethyl)ether 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.0Bis(2-chloroisopropyl)ether 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.9Bis(2-ethylhexyl)phthalate 8.110
1ug/Kg-dry 24-Jul-2014 21:36J1.6Butyl benzyl phthalate 8.12.5
1ug/Kg-dry 24-Jul-2014 21:361.5Caprolactam 8.19.6
1ug/Kg-dry 24-Jul-2014 21:361.2Carbazole 8.1U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-11B
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-20
15-Jul-2014 09:35 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 24-Jul-2014 21:360.74Chrysene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.2Dibenz(a,h)anthracene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.2Dibenzofuran 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.86Diethyl phthalate 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.2Dimethyl phthalate 8.1U
1ug/Kg-dry 24-Jul-2014 21:36J0.74Di-n-butyl phthalate 8.12.3
1ug/Kg-dry 24-Jul-2014 21:360.74Di-n-octyl phthalate 8.1U
1ug/Kg-dry 24-Jul-2014 21:36J0.99Fluoranthene 8.12.9
1ug/Kg-dry 24-Jul-2014 21:361.6Fluorene 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.99Hexachlorobenzene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.4Hexachlorobutadiene 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.1Hexachlorocyclopentadiene 8.1U
1ug/Kg-dry 24-Jul-2014 21:362.2Hexachloroethane 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.1Indeno(1,2,3-cd)pyrene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.1Isophorone 8.1U
1ug/Kg-dry 24-Jul-2014 21:360.99Naphthalene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.2Nitrobenzene 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.7N-Nitrosodi-n-propylamine 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.6N-Nitrosodiphenylamine 8.1U
1ug/Kg-dry 24-Jul-2014 21:361.1Pentachlorophenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:36J0.86Phenanthrene 8.12.1
1ug/Kg-dry 24-Jul-2014 21:360.86Phenol 8.1U
1ug/Kg-dry 24-Jul-2014 21:36J0.74Pyrene 8.12.3
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 21:3680.3 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 21:3679.0 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 21:3683.5 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 21:3689.7 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 21:3685.4 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 21:3680.3 40-125
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 22-Jul-2014 23:550.012GRO (C6-C10)0.062U
Surr: 4-Bromofluorobenzene 1%REC 22-Jul-2014 23:5575.2 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010019.3
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 18:580.62TPH (Diesel Range)2.13.0
1mg/Kg-dry 31-Jul-2014 18:580.62TPH (Motor Oil Range)4.211
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 18:5888.2 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-12A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-21
14-Jul-2014 07:30 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 23-Jul-2014 00:110.014GRO (C6-C10)0.069U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 00:1175.4 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010027.7
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 19:210.69TPH (Diesel Range)2.3U
1mg/Kg-dry 31-Jul-2014 19:21J0.69TPH (Motor Oil Range)4.70.86
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 19:2164.1 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-12B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-22
14-Jul-2014 07:35 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
GASOLINE RANGE ORGANICS BY
SW8015C Method:SW8015M Analyst: PPM
1mg/Kg-dry 23-Jul-2014 00:270.012GRO (C6-C10)0.059U
Surr: 4-Bromofluorobenzene 1%REC 23-Jul-2014 00:2783.2 70-130
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010015.0
TPH DRO/ORO BY SW8015C Method:SW8015M Analyst: SEPrep:SW3541 / 25-Jul-2014
1mg/Kg-dry 31-Jul-2014 19:43J0.59TPH (Diesel Range)2.01.0
1mg/Kg-dry 31-Jul-2014 19:430.59TPH (Motor Oil Range)4.018
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 19:4382.8 60-135
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-13A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-23
14-Jul-2014 09:20 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
10ug/Kg-dry 31-Jul-2014 00:46211,1´-Biphenyl 150U
10ug/Kg-dry 31-Jul-2014 00:46362,4,5-Trichlorophenol 150U
10ug/Kg-dry 31-Jul-2014 00:46252,4,6-Trichlorophenol 150U
10ug/Kg-dry 31-Jul-2014 00:46272,4-Dichlorophenol 150U
10ug/Kg-dry 31-Jul-2014 00:46162,4-Dimethylphenol 150U
10ug/Kg-dry 31-Jul-2014 00:46232,4-Dinitrophenol 300U
10ug/Kg-dry 31-Jul-2014 00:46302,4-Dinitrotoluene 150U
10ug/Kg-dry 31-Jul-2014 00:46212,6-Dinitrotoluene 150U
10ug/Kg-dry 31-Jul-2014 00:46272-Chloronaphthalene 150U
10ug/Kg-dry 31-Jul-2014 00:46252-Chlorophenol 150U
10ug/Kg-dry 31-Jul-2014 00:46162-Methylnaphthalene 150U
10ug/Kg-dry 31-Jul-2014 00:46272-Methylphenol 150U
10ug/Kg-dry 31-Jul-2014 00:46342-Nitroaniline 150U
10ug/Kg-dry 31-Jul-2014 00:46302-Nitrophenol 150U
10ug/Kg-dry 31-Jul-2014 00:46253&4-Methylphenol 150U
10ug/Kg-dry 31-Jul-2014 00:46213,3´-Dichlorobenzidine 150U
10ug/Kg-dry 31-Jul-2014 00:46303-Nitroaniline 150U
10ug/Kg-dry 31-Jul-2014 00:46274,6-Dinitro-2-methylphenol 150U
10ug/Kg-dry 31-Jul-2014 00:46304-Bromophenyl phenyl ether 150U
10ug/Kg-dry 31-Jul-2014 00:46414-Chloro-3-methylphenol 150U
10ug/Kg-dry 31-Jul-2014 00:46164-Chloroaniline 150U
10ug/Kg-dry 31-Jul-2014 00:46344-Chlorophenyl phenyl ether 150U
10ug/Kg-dry 31-Jul-2014 00:46364-Nitroaniline 150U
10ug/Kg-dry 31-Jul-2014 00:46364-Nitrophenol 300U
10ug/Kg-dry 31-Jul-2014 00:4618Acenaphthene150U
10ug/Kg-dry 31-Jul-2014 00:4616Acenaphthylene150U
10ug/Kg-dry 31-Jul-2014 00:4616Acetophenone150U
10ug/Kg-dry 31-Jul-2014 00:4627Anthracene150U
10ug/Kg-dry 31-Jul-2014 00:4648Atrazine150U
10ug/Kg-dry 31-Jul-2014 00:4621Benz(a)anthracene 150U
10ug/Kg-dry 31-Jul-2014 00:4618Benzaldehyde150U
10ug/Kg-dry 31-Jul-2014 00:4614Benzo(a)pyrene 150U
10ug/Kg-dry 31-Jul-2014 00:4616Benzo(b)fluoranthene 150U
10ug/Kg-dry 31-Jul-2014 00:4616Benzo(g,h,i)perylene 150U
10ug/Kg-dry 31-Jul-2014 00:4616Benzo(k)fluoranthene 150U
10ug/Kg-dry 31-Jul-2014 00:4621Bis(2-chloroethoxy)methane 150U
10ug/Kg-dry 31-Jul-2014 00:4618Bis(2-chloroethyl)ether 150U
10ug/Kg-dry 31-Jul-2014 00:4636Bis(2-chloroisopropyl)ether 150U
10ug/Kg-dry 31-Jul-2014 00:4634Bis(2-ethylhexyl)phthalate 150U
10ug/Kg-dry 31-Jul-2014 00:4630Butyl benzyl phthalate 150U
10ug/Kg-dry 31-Jul-2014 00:4627Caprolactam150U
10ug/Kg-dry 31-Jul-2014 00:4623Carbazole150U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-13A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-23
14-Jul-2014 09:20 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
10ug/Kg-dry 31-Jul-2014 00:46J14Chrysene15077
10ug/Kg-dry 31-Jul-2014 00:4623Dibenz(a,h)anthracene 150U
10ug/Kg-dry 31-Jul-2014 00:4623Dibenzofuran150U
10ug/Kg-dry 31-Jul-2014 00:4616Diethyl phthalate 150U
10ug/Kg-dry 31-Jul-2014 00:4623Dimethyl phthalate 150U
10ug/Kg-dry 31-Jul-2014 00:4614Di-n-butyl phthalate 150U
10ug/Kg-dry 31-Jul-2014 00:4614Di-n-octyl phthalate 150U
10ug/Kg-dry 31-Jul-2014 00:4618Fluoranthene150U
10ug/Kg-dry 31-Jul-2014 00:4630Fluorene150U
10ug/Kg-dry 31-Jul-2014 00:4618Hexachlorobenzene150U
10ug/Kg-dry 31-Jul-2014 00:4625Hexachlorobutadiene150U
10ug/Kg-dry 31-Jul-2014 00:4639Hexachlorocyclopentadiene150U
10ug/Kg-dry 31-Jul-2014 00:4641Hexachloroethane150U
10ug/Kg-dry 31-Jul-2014 00:4621Indeno(1,2,3-cd)pyrene 150U
10ug/Kg-dry 31-Jul-2014 00:4621Isophorone150U
10ug/Kg-dry 31-Jul-2014 00:4618Naphthalene150U
10ug/Kg-dry 31-Jul-2014 00:4623Nitrobenzene150U
10ug/Kg-dry 31-Jul-2014 00:4632N-Nitrosodi-n-propylamine 150U
10ug/Kg-dry 31-Jul-2014 00:4630N-Nitrosodiphenylamine 150U
10ug/Kg-dry 31-Jul-2014 00:4621Pentachlorophenol150U
10ug/Kg-dry 31-Jul-2014 00:4616Phenanthrene150U
10ug/Kg-dry 31-Jul-2014 00:4616Phenol150U
10ug/Kg-dry 31-Jul-2014 00:46J14Pyrene15043
Surr: 2,4,6-Tribromophenol 10%REC 31-Jul-2014 00:46J76.4 36-126
Surr: 2-Fluorobiphenyl 10%REC 31-Jul-2014 00:4682.8 43-125
Surr: 2-Fluorophenol 10%REC 31-Jul-2014 00:46J72.1 37-125
Surr: 4-Terphenyl-d14 10%REC 31-Jul-2014 00:46J70.6 32-125
Surr: Nitrobenzene-d5 10%REC 31-Jul-2014 00:4679.4 37-125
Surr: Phenol-d6 10%REC 31-Jul-2014 00:4681.5 40-125
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010012.5
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-13B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-24
14-Jul-2014 09:25 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 31-Jul-2014 00:051.11,1´-Biphenyl 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.02,4,5-Trichlorophenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.32,4,6-Trichlorophenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.52,4-Dichlorophenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.862,4-Dimethylphenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.22,4-Dinitrophenol 16U
1ug/Kg-dry 31-Jul-2014 00:051.62,4-Dinitrotoluene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.12,6-Dinitrotoluene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.52-Chloronaphthalene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.32-Chlorophenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.862-Methylnaphthalene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.52-Methylphenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.82-Nitroaniline 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.62-Nitrophenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.33&4-Methylphenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.13,3´-Dichlorobenzidine 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.63-Nitroaniline 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.54,6-Dinitro-2-methylphenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.64-Bromophenyl phenyl ether 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.24-Chloro-3-methylphenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.864-Chloroaniline 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.84-Chlorophenyl phenyl ether 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.04-Nitroaniline 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.04-Nitrophenol 16U
1ug/Kg-dry 31-Jul-2014 00:050.98Acenaphthene 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.86Acenaphthylene 8.1U
1ug/Kg-dry 31-Jul-2014 00:05J0.86Acetophenone 8.12.2
1ug/Kg-dry 31-Jul-2014 00:051.5Anthracene 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.6Atrazine 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.1Benz(a)anthracene 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.98Benzaldehyde 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.73Benzo(a)pyrene 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.86Benzo(b)fluoranthene 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.86Benzo(g,h,i)perylene 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.86Benzo(k)fluoranthene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.1Bis(2-chloroethoxy)methane 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.98Bis(2-chloroethyl)ether 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.0Bis(2-chloroisopropyl)ether 8.1U
1ug/Kg-dry 31-Jul-2014 00:05J1.8Bis(2-ethylhexyl)phthalate 8.13.1
1ug/Kg-dry 31-Jul-2014 00:051.6Butyl benzyl phthalate 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.5Caprolactam 8.122
1ug/Kg-dry 31-Jul-2014 00:051.2Carbazole 8.1U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-13B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-24
14-Jul-2014 09:25 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
1ug/Kg-dry 31-Jul-2014 00:050.73Chrysene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.2Dibenz(a,h)anthracene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.2Dibenzofuran 8.1U
1ug/Kg-dry 31-Jul-2014 00:05J0.86Diethyl phthalate 8.12.9
1ug/Kg-dry 31-Jul-2014 00:051.2Dimethyl phthalate 8.1U
1ug/Kg-dry 31-Jul-2014 00:05J0.73Di-n-butyl phthalate 8.12.3
1ug/Kg-dry 31-Jul-2014 00:050.73Di-n-octyl phthalate 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.98Fluoranthene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.6Fluorene 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.98Hexachlorobenzene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.3Hexachlorobutadiene 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.1Hexachlorocyclopentadiene 8.1U
1ug/Kg-dry 31-Jul-2014 00:052.2Hexachloroethane 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.1Indeno(1,2,3-cd)pyrene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.1Isophorone 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.98Naphthalene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.2Nitrobenzene 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.7N-Nitrosodi-n-propylamine 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.6N-Nitrosodiphenylamine 8.1U
1ug/Kg-dry 31-Jul-2014 00:051.1Pentachlorophenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.86Phenanthrene 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.86Phenol 8.1U
1ug/Kg-dry 31-Jul-2014 00:050.73Pyrene 8.1U
Surr: 2,4,6-Tribromophenol 1%REC 31-Jul-2014 00:0591.0 36-126
Surr: 2-Fluorobiphenyl 1%REC 31-Jul-2014 00:0582.6 43-125
Surr: 2-Fluorophenol 1%REC 31-Jul-2014 00:0571.1 37-125
Surr: 4-Terphenyl-d14 1%REC 31-Jul-2014 00:0583.3 32-125
Surr: Nitrobenzene-d5 1%REC 31-Jul-2014 00:0587.9 37-125
Surr: Phenol-d6 1%REC 31-Jul-2014 00:0577.1 40-125
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010018.4
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-14A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-25
14-Jul-2014 09:05 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
10ug/Kg-dry 31-Jul-2014 00:26211,1´-Biphenyl 160U
10ug/Kg-dry 31-Jul-2014 00:26382,4,5-Trichlorophenol 160U
10ug/Kg-dry 31-Jul-2014 00:26262,4,6-Trichlorophenol 160U
10ug/Kg-dry 31-Jul-2014 00:26282,4-Dichlorophenol 160U
10ug/Kg-dry 31-Jul-2014 00:26172,4-Dimethylphenol 160U
10ug/Kg-dry 31-Jul-2014 00:26242,4-Dinitrophenol 310U
10ug/Kg-dry 31-Jul-2014 00:26312,4-Dinitrotoluene 160U
10ug/Kg-dry 31-Jul-2014 00:26212,6-Dinitrotoluene 160U
10ug/Kg-dry 31-Jul-2014 00:26282-Chloronaphthalene 160U
10ug/Kg-dry 31-Jul-2014 00:26262-Chlorophenol 160U
10ug/Kg-dry 31-Jul-2014 00:26172-Methylnaphthalene 160U
10ug/Kg-dry 31-Jul-2014 00:26282-Methylphenol 160U
10ug/Kg-dry 31-Jul-2014 00:26362-Nitroaniline 160U
10ug/Kg-dry 31-Jul-2014 00:26312-Nitrophenol 160U
10ug/Kg-dry 31-Jul-2014 00:26263&4-Methylphenol 160U
10ug/Kg-dry 31-Jul-2014 00:26213,3´-Dichlorobenzidine 160U
10ug/Kg-dry 31-Jul-2014 00:26313-Nitroaniline 160U
10ug/Kg-dry 31-Jul-2014 00:26284,6-Dinitro-2-methylphenol 160U
10ug/Kg-dry 31-Jul-2014 00:26314-Bromophenyl phenyl ether 160U
10ug/Kg-dry 31-Jul-2014 00:26434-Chloro-3-methylphenol 160U
10ug/Kg-dry 31-Jul-2014 00:26174-Chloroaniline 160U
10ug/Kg-dry 31-Jul-2014 00:26364-Chlorophenyl phenyl ether 160U
10ug/Kg-dry 31-Jul-2014 00:26384-Nitroaniline 160U
10ug/Kg-dry 31-Jul-2014 00:26384-Nitrophenol 310U
10ug/Kg-dry 31-Jul-2014 00:2619Acenaphthene160U
10ug/Kg-dry 31-Jul-2014 00:2617Acenaphthylene160U
10ug/Kg-dry 31-Jul-2014 00:2617Acetophenone160U
10ug/Kg-dry 31-Jul-2014 00:2628Anthracene160U
10ug/Kg-dry 31-Jul-2014 00:2650Atrazine160U
10ug/Kg-dry 31-Jul-2014 00:2621Benz(a)anthracene 160U
10ug/Kg-dry 31-Jul-2014 00:2619Benzaldehyde160U
10ug/Kg-dry 31-Jul-2014 00:2614Benzo(a)pyrene 160U
10ug/Kg-dry 31-Jul-2014 00:2617Benzo(b)fluoranthene 160U
10ug/Kg-dry 31-Jul-2014 00:2617Benzo(g,h,i)perylene 160U
10ug/Kg-dry 31-Jul-2014 00:2617Benzo(k)fluoranthene 160U
10ug/Kg-dry 31-Jul-2014 00:2621Bis(2-chloroethoxy)methane 160U
10ug/Kg-dry 31-Jul-2014 00:2619Bis(2-chloroethyl)ether 160U
10ug/Kg-dry 31-Jul-2014 00:2638Bis(2-chloroisopropyl)ether 160U
10ug/Kg-dry 31-Jul-2014 00:2636Bis(2-ethylhexyl)phthalate 160U
10ug/Kg-dry 31-Jul-2014 00:2631Butyl benzyl phthalate 160U
10ug/Kg-dry 31-Jul-2014 00:2628Caprolactam160U
10ug/Kg-dry 31-Jul-2014 00:2624Carbazole160U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-14A (1-2)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-25
14-Jul-2014 09:05 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LGPrep:SW3541 / 24-Jul-2014
10ug/Kg-dry 31-Jul-2014 00:2614Chrysene160U
10ug/Kg-dry 31-Jul-2014 00:2624Dibenz(a,h)anthracene 160U
10ug/Kg-dry 31-Jul-2014 00:2624Dibenzofuran160U
10ug/Kg-dry 31-Jul-2014 00:2617Diethyl phthalate 160U
10ug/Kg-dry 31-Jul-2014 00:2624Dimethyl phthalate 160U
10ug/Kg-dry 31-Jul-2014 00:2614Di-n-butyl phthalate 160U
10ug/Kg-dry 31-Jul-2014 00:2614Di-n-octyl phthalate 160U
10ug/Kg-dry 31-Jul-2014 00:2619Fluoranthene160U
10ug/Kg-dry 31-Jul-2014 00:2631Fluorene160U
10ug/Kg-dry 31-Jul-2014 00:2619Hexachlorobenzene160U
10ug/Kg-dry 31-Jul-2014 00:2626Hexachlorobutadiene160U
10ug/Kg-dry 31-Jul-2014 00:2640Hexachlorocyclopentadiene160U
10ug/Kg-dry 31-Jul-2014 00:2643Hexachloroethane160U
10ug/Kg-dry 31-Jul-2014 00:2621Indeno(1,2,3-cd)pyrene 160U
10ug/Kg-dry 31-Jul-2014 00:2621Isophorone160U
10ug/Kg-dry 31-Jul-2014 00:2619Naphthalene160U
10ug/Kg-dry 31-Jul-2014 00:2624Nitrobenzene160U
10ug/Kg-dry 31-Jul-2014 00:2633N-Nitrosodi-n-propylamine 160U
10ug/Kg-dry 31-Jul-2014 00:2631N-Nitrosodiphenylamine 160U
10ug/Kg-dry 31-Jul-2014 00:2621Pentachlorophenol160U
10ug/Kg-dry 31-Jul-2014 00:2617Phenanthrene160U
10ug/Kg-dry 31-Jul-2014 00:2617Phenol160U
10ug/Kg-dry 31-Jul-2014 00:2614Pyrene160U
Surr: 2,4,6-Tribromophenol 10%REC 31-Jul-2014 00:2685.0 36-126
Surr: 2-Fluorobiphenyl 10%REC 31-Jul-2014 00:2685.1 43-125
Surr: 2-Fluorophenol 10%REC 31-Jul-2014 00:26J56.7 37-125
Surr: 4-Terphenyl-d14 10%REC 31-Jul-2014 00:26J77.7 32-125
Surr: Nitrobenzene-d5 10%REC 31-Jul-2014 00:2690.4 37-125
Surr: Phenol-d6 10%REC 31-Jul-2014 00:26J73.2 40-125
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010015.9
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-14B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-26
14-Jul-2014 09:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LG
1ug/Kg-dry 24-Jul-2014 17:401.11,1´-Biphenyl 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.92,4,5-Trichlorophenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.32,4,6-Trichlorophenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.42,4-Dichlorophenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.822,4-Dimethylphenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.22,4-Dinitrophenol 15U
1ug/Kg-dry 24-Jul-2014 17:401.52,4-Dinitrotoluene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.12,6-Dinitrotoluene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.42-Chloronaphthalene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.32-Chlorophenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.822-Methylnaphthalene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.42-Methylphenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.82-Nitroaniline 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.52-Nitrophenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.33&4-Methylphenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.13,3´-Dichlorobenzidine 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.53-Nitroaniline 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.44,6-Dinitro-2-methylphenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.54-Bromophenyl phenyl ether 7.7U
1ug/Kg-dry 24-Jul-2014 17:402.14-Chloro-3-methylphenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.824-Chloroaniline 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.84-Chlorophenyl phenyl ether 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.94-Nitroaniline 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.94-Nitrophenol 15U
1ug/Kg-dry 24-Jul-2014 17:400.94Acenaphthene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Acenaphthylene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Acetophenone 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.4Anthracene 7.7U
1ug/Kg-dry 24-Jul-2014 17:402.5Atrazine 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.1Benz(a)anthracene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.94Benzaldehyde 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.70Benzo(a)pyrene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Benzo(b)fluoranthene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Benzo(g,h,i)perylene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Benzo(k)fluoranthene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.1Bis(2-chloroethoxy)methane 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.94Bis(2-chloroethyl)ether 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.9Bis(2-chloroisopropyl)ether 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.8Bis(2-ethylhexyl)phthalate 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.5Butyl benzyl phthalate 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.4Caprolactam 7.711
1ug/Kg-dry 24-Jul-2014 17:401.2Carbazole 7.7U
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-14B (4.5-5.5)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-26
14-Jul-2014 09:10 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
LOW-LEVEL SEMIVOLATILES Method:SW8270 Analyst: LG
1ug/Kg-dry 24-Jul-2014 17:400.70Chrysene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.2Dibenz(a,h)anthracene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.2Dibenzofuran 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Diethyl phthalate 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.2Dimethyl phthalate 7.7U
1ug/Kg-dry 24-Jul-2014 17:40J0.70Di-n-butyl phthalate 7.72.2
1ug/Kg-dry 24-Jul-2014 17:400.70Di-n-octyl phthalate 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.94Fluoranthene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.5Fluorene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.94Hexachlorobenzene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.3Hexachlorobutadiene 7.7U
1ug/Kg-dry 24-Jul-2014 17:402.0Hexachlorocyclopentadiene 7.7U
1ug/Kg-dry 24-Jul-2014 17:402.1Hexachloroethane 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.1Indeno(1,2,3-cd)pyrene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.1Isophorone 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.94Naphthalene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.2Nitrobenzene 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.6N-Nitrosodi-n-propylamine 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.5N-Nitrosodiphenylamine 7.7U
1ug/Kg-dry 24-Jul-2014 17:401.1Pentachlorophenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Phenanthrene 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.82Phenol 7.7U
1ug/Kg-dry 24-Jul-2014 17:400.70Pyrene 7.7U
Surr: 2,4,6-Tribromophenol 1%REC 24-Jul-2014 17:4077.5 36-126
Surr: 2-Fluorobiphenyl 1%REC 24-Jul-2014 17:4075.0 43-125
Surr: 2-Fluorophenol 1%REC 24-Jul-2014 17:4067.7 37-125
Surr: 4-Terphenyl-d14 1%REC 24-Jul-2014 17:4076.5 32-125
Surr: Nitrobenzene-d5 1%REC 24-Jul-2014 17:4084.4 37-125
Surr: Phenol-d6 1%REC 24-Jul-2014 17:4069.4 40-125
MOISTURE Method:SW3550 Analyst: KAH
1wt%24-Jul-2014 14:500.0100Percent Moisture 0.010014.8
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-15 (3-4)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-27
14-Jul-2014 08:55 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Sample ID:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
B-16 (3-4)
WorkOrder:
Lab ID:
Collection Date:
HS14070721
HS14070721-28
14-Jul-2014 08:30 Matrix:Soil
ANALYTICAL REPORT
ANALYSES RESULT REPORT
LIMIT
DILUTION
FACTORUNITS DATE
ANALYZEDQUALMDL
SUBCONTRACT ANALYSIS - METALS
ANALYSIS Method:NA Analyst: JML
1 05-Aug-2014 17:130Subcontract Analysis See Attached
06-Aug-14Date: ALS Group USA, Corp
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Eaton Phase II Goldsboro NC 13384340
Golder Associates, Inc.
WorkOrder:
Project:
HS14070721
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID TCLP Date DF
Batch ID 84329 Test Name :LOW-LEVEL SEMIVOLATILES Matrix:Water
21 Jul 2014 17:19 24 Jul 2014 15:56HS14070721-01 15 Jul 2014 17:00 1MW-9
21 Jul 2014 17:19 24 Jul 2014 16:15HS14070721-02 15 Jul 2014 16:00 1MW-10
21 Jul 2014 17:19 24 Jul 2014 16:34HS14070721-03 15 Jul 2014 15:05 1MW-11
21 Jul 2014 17:19 24 Jul 2014 16:53HS14070721-04 15 Jul 2014 14:00 1MW-12
21 Jul 2014 17:19 24 Jul 2014 17:12HS14070721-05 15 Jul 2014 14:00 1MW-12 DUP
21 Jul 2014 17:19 24 Jul 2014 17:31HS14070721-06 15 Jul 2014 13:00 1MW-13
Batch ID 84404 Test Name :TPH DRO/ORO BY SW8015C Matrix:Water
21 Jul 2014 10:45 30 Jul 2014 16:03HS14070721-01 15 Jul 2014 17:00 1MW-9
21 Jul 2014 10:45 30 Jul 2014 16:30HS14070721-02 15 Jul 2014 16:00 1MW-10
21 Jul 2014 10:45 30 Jul 2014 16:57HS14070721-03 15 Jul 2014 15:05 1MW-11
21 Jul 2014 10:45 30 Jul 2014 17:24HS14070721-04 15 Jul 2014 14:00 1MW-12
21 Jul 2014 10:45 30 Jul 2014 17:51HS14070721-05 15 Jul 2014 14:00 1MW-12 DUP
21 Jul 2014 10:45 30 Jul 2014 18:17HS14070721-06 15 Jul 2014 13:00 1MW-13
Batch ID 84405a Test Name :LOW-LEVEL SEMIVOLATILES Matrix:Soil
23 Jul 2014 09:04 24 Jul 2014 17:40HS14070721-26 14 Jul 2014 09:10 1B-14B (4.5-5.5)
Batch ID 84441 Test Name :LOW-LEVEL SEMIVOLATILES Matrix:Soil
24 Jul 2014 07:05 24 Jul 2014 14:58HS14070721-07 14 Jul 2014 13:50 1B-18A (1-2)
24 Jul 2014 07:05 24 Jul 2014 18:46HS14070721-08 14 Jul 2014 14:10 1B-18B (4.5-5.5)
24 Jul 2014 07:05 24 Jul 2014 19:05HS14070721-09 14 Jul 2014 14:10 1B-18B (4.5-5.5) DUP
24 Jul 2014 07:05 24 Jul 2014 19:24HS14070721-10 14 Jul 2014 17:45 1B-17A (1-2)
24 Jul 2014 07:05 24 Jul 2014 19:43HS14070721-11 14 Jul 2014 17:55 1B-17B (4.5-5.5)
24 Jul 2014 07:05 24 Jul 2014 20:02HS14070721-12 14 Jul 2014 16:53 1B-19A (1-2)
24 Jul 2014 07:05 24 Jul 2014 20:21HS14070721-13 14 Jul 2014 17:06 1B-19B (4.5-5.5)
24 Jul 2014 07:05 24 Jul 2014 20:40HS14070721-14 14 Jul 2014 15:30 1B-20A (1-2)
24 Jul 2014 07:05 24 Jul 2014 20:59HS14070721-15 14 Jul 2014 15:50 1B-20B (4.5-5.5)
24 Jul 2014 07:05 24 Jul 2014 21:18HS14070721-19 15 Jul 2014 09:30 1B-11A
24 Jul 2014 07:05 24 Jul 2014 21:36HS14070721-20 15 Jul 2014 09:35 1B-11B
24 Jul 2014 07:05 31 Jul 2014 00:46HS14070721-23 14 Jul 2014 09:20 10B-13A (1-2)
24 Jul 2014 07:05 31 Jul 2014 00:05HS14070721-24 14 Jul 2014 09:25 1B-13B (4.5-5.5)
24 Jul 2014 07:05 31 Jul 2014 00:26HS14070721-25 14 Jul 2014 09:05 10B-14A (1-2)
06-Aug-14Date: ALS Group USA, Corp
Client:
Eaton Phase II Goldsboro NC 13384340
Golder Associates, Inc.
WorkOrder:
Project:
HS14070721
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID TCLP Date DF
Batch ID 84484 Test Name :TPH DRO/ORO BY SW8015C Matrix:Soil
25 Jul 2014 07:41 31 Jul 2014 18:58HS14070721-07 14 Jul 2014 13:50 1B-18A (1-2)
25 Jul 2014 07:41 31 Jul 2014 19:21HS14070721-08 14 Jul 2014 14:10 1B-18B (4.5-5.5)
25 Jul 2014 07:41 31 Jul 2014 19:43HS14070721-09 14 Jul 2014 14:10 1B-18B (4.5-5.5) DUP
25 Jul 2014 07:41 31 Jul 2014 20:06HS14070721-10 14 Jul 2014 17:45 1B-17A (1-2)
25 Jul 2014 07:41 31 Jul 2014 20:28HS14070721-11 14 Jul 2014 17:55 1B-17B (4.5-5.5)
25 Jul 2014 07:41 31 Jul 2014 20:51HS14070721-12 14 Jul 2014 16:53 1B-19A (1-2)
25 Jul 2014 07:41 31 Jul 2014 21:14HS14070721-13 14 Jul 2014 17:06 1B-19B (4.5-5.5)
25 Jul 2014 07:41 31 Jul 2014 22:22HS14070721-14 14 Jul 2014 15:30 1B-20A (1-2)
25 Jul 2014 07:41 31 Jul 2014 18:13HS14070721-15 14 Jul 2014 15:50 1B-20B (4.5-5.5)
25 Jul 2014 07:41 31 Jul 2014 18:35HS14070721-19 15 Jul 2014 09:30 1B-11A
25 Jul 2014 07:41 31 Jul 2014 18:58HS14070721-20 15 Jul 2014 09:35 1B-11B
25 Jul 2014 07:41 31 Jul 2014 19:21HS14070721-21 14 Jul 2014 07:30 1B-12A (1-2)
25 Jul 2014 07:41 31 Jul 2014 19:43HS14070721-22 14 Jul 2014 07:35 1B-12B (4.5-5.5)
Batch ID R237862 Test Name :TCL VOLATILES - SW8260C Matrix:Soil
22 Jul 2014 13:29HS14070721-07 14 Jul 2014 13:50 1B-18A (1-2)
22 Jul 2014 15:03HS14070721-08 14 Jul 2014 14:10 1B-18B (4.5-5.5)
22 Jul 2014 15:26HS14070721-09 14 Jul 2014 14:10 1B-18B (4.5-5.5) DUP
22 Jul 2014 15:49HS14070721-10 14 Jul 2014 17:45 1B-17A (1-2)
22 Jul 2014 16:13HS14070721-11 14 Jul 2014 17:55 1B-17B (4.5-5.5)
Batch ID R237864 Test Name :GASOLINE RANGE ORGANICS BY SW8015C Matrix:Soil
22 Jul 2014 21:31HS14070721-07 14 Jul 2014 13:50 1B-18A (1-2)
22 Jul 2014 20:11HS14070721-08 14 Jul 2014 14:10 1B-18B (4.5-5.5)
22 Jul 2014 20:43HS14070721-10 14 Jul 2014 17:45 1B-17A (1-2)
22 Jul 2014 20:58HS14070721-11 14 Jul 2014 17:55 1B-17B (4.5-5.5)
22 Jul 2014 21:15HS14070721-12 14 Jul 2014 16:53 1B-19A (1-2)
22 Jul 2014 22:51HS14070721-13 14 Jul 2014 17:06 1B-19B (4.5-5.5)
22 Jul 2014 23:07HS14070721-14 14 Jul 2014 15:30 1B-20A (1-2)
22 Jul 2014 23:23HS14070721-15 14 Jul 2014 15:50 1B-20B (4.5-5.5)
22 Jul 2014 23:39HS14070721-19 15 Jul 2014 09:30 1B-11A
22 Jul 2014 23:55HS14070721-20 15 Jul 2014 09:35 1B-11B
23 Jul 2014 00:11HS14070721-21 14 Jul 2014 07:30 1B-12A (1-2)
23 Jul 2014 00:27HS14070721-22 14 Jul 2014 07:35 1B-12B (4.5-5.5)
Batch ID R237910 Test Name :GASOLINE RANGE ORGANICS BY SW8015C Matrix:Soil
23 Jul 2014 14:07HS14070721-09 14 Jul 2014 14:10 1B-18B (4.5-5.5) DUP
06-Aug-14Date: ALS Group USA, Corp
Client:
Eaton Phase II Goldsboro NC 13384340
Golder Associates, Inc.
WorkOrder:
Project:
HS14070721
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID TCLP Date DF
Batch ID R237931 Test Name :GASOLINE RANGE ORGANICS BY SW8015C Matrix:Water
23 Jul 2014 18:42HS14070721-01 15 Jul 2014 17:00 1MW-9
23 Jul 2014 18:58HS14070721-02 15 Jul 2014 16:00 1MW-10
23 Jul 2014 19:14HS14070721-03 15 Jul 2014 15:05 1MW-11
23 Jul 2014 19:30HS14070721-04 15 Jul 2014 14:00 1MW-12
23 Jul 2014 19:46HS14070721-05 15 Jul 2014 14:00 1MW-12 DUP
23 Jul 2014 21:52HS14070721-06 15 Jul 2014 13:00 1MW-13
Batch ID R238044 Test Name :MOISTURE Matrix:Soil
24 Jul 2014 14:50HS14070721-07 14 Jul 2014 13:50 1B-18A (1-2)
24 Jul 2014 14:50HS14070721-08 14 Jul 2014 14:10 1B-18B (4.5-5.5)
24 Jul 2014 14:50HS14070721-09 14 Jul 2014 14:10 1B-18B (4.5-5.5) DUP
24 Jul 2014 14:50HS14070721-10 14 Jul 2014 17:45 1B-17A (1-2)
24 Jul 2014 14:50HS14070721-11 14 Jul 2014 17:55 1B-17B (4.5-5.5)
24 Jul 2014 14:50HS14070721-12 14 Jul 2014 16:53 1B-19A (1-2)
24 Jul 2014 14:50HS14070721-13 14 Jul 2014 17:06 1B-19B (4.5-5.5)
24 Jul 2014 14:50HS14070721-14 14 Jul 2014 15:30 1B-20A (1-2)
24 Jul 2014 14:50HS14070721-15 14 Jul 2014 15:50 1B-20B (4.5-5.5)
24 Jul 2014 14:50HS14070721-19 15 Jul 2014 09:30 1B-11A
24 Jul 2014 14:50HS14070721-20 15 Jul 2014 09:35 1B-11B
24 Jul 2014 14:50HS14070721-21 14 Jul 2014 07:30 1B-12A (1-2)
24 Jul 2014 14:50HS14070721-22 14 Jul 2014 07:35 1B-12B (4.5-5.5)
24 Jul 2014 14:50HS14070721-23 14 Jul 2014 09:20 1B-13A (1-2)
24 Jul 2014 14:50HS14070721-24 14 Jul 2014 09:25 1B-13B (4.5-5.5)
24 Jul 2014 14:50HS14070721-25 14 Jul 2014 09:05 1B-14A (1-2)
24 Jul 2014 14:50HS14070721-26 14 Jul 2014 09:10 1B-14B (4.5-5.5)
Batch ID R238123 Test Name :TCL VOLATILES - SW8260C Matrix:Water
25 Jul 2014 18:08HS14070721-02 15 Jul 2014 16:00 1MW-10
25 Jul 2014 18:34HS14070721-04 15 Jul 2014 14:00 1MW-12
25 Jul 2014 19:00HS14070721-05 15 Jul 2014 14:00 1MW-12 DUP
Batch ID R238322 Test Name :MISC. GCFID PARAMETERS BY SW8015C Matrix:Water
28 Jul 2014 15:35HS14070721-04 15 Jul 2014 14:00 1MW-12
28 Jul 2014 16:06HS14070721-06 15 Jul 2014 13:00 1MW-13
06-Aug-14Date: ALS Group USA, Corp
Client:
Eaton Phase II Goldsboro NC 13384340
Golder Associates, Inc.
WorkOrder:
Project:
HS14070721
DATES REPORT
Collection Date Prep Date Analysis DateClient Samp IDSample ID TCLP Date DF
Batch ID R238684 Test Name :SUBCONTRACT ANALYSIS - METALS ANALYSIS Matrix:Soil
05 Aug 2014 17:13HS14070721-07 14 Jul 2014 13:50 1B-18A (1-2)
05 Aug 2014 17:13HS14070721-08 14 Jul 2014 14:10 1B-18B (4.5-5.5)
05 Aug 2014 17:13HS14070721-09 14 Jul 2014 14:10 1B-18B (4.5-5.5) DUP
05 Aug 2014 17:13HS14070721-10 14 Jul 2014 17:45 1B-17A (1-2)
05 Aug 2014 17:13HS14070721-11 14 Jul 2014 17:55 1B-17B (4.5-5.5)
05 Aug 2014 17:13HS14070721-12 14 Jul 2014 16:53 1B-19A (1-2)
05 Aug 2014 17:13HS14070721-13 14 Jul 2014 17:06 1B-19B (4.5-5.5)
05 Aug 2014 17:13HS14070721-14 14 Jul 2014 15:30 1B-20A (1-2)
05 Aug 2014 17:13HS14070721-15 14 Jul 2014 15:50 1B-20B (4.5-5.5)
05 Aug 2014 17:13HS14070721-16 15 Jul 2014 08:35 1B-9A (3.5-4.0)
05 Aug 2014 17:13HS14070721-17 15 Jul 2014 10:00 1B-10A (1-2)
05 Aug 2014 17:13HS14070721-18 15 Jul 2014 10:05 1B-10B (4-5)
05 Aug 2014 17:13HS14070721-25 14 Jul 2014 09:05 1B-14A (1-2)
05 Aug 2014 17:13HS14070721-26 14 Jul 2014 09:10 1B-14B (4.5-5.5)
05 Aug 2014 17:13HS14070721-27 14 Jul 2014 08:55 1B-15 (3-4)
05 Aug 2014 17:13HS14070721-28 14 Jul 2014 08:30 1B-16 (3-4)
Batch ID R238684 Test Name :SUBCONTRACT ANALYSIS - METALS ANALYSIS Matrix:Water
05 Aug 2014 17:13HS14070721-02 15 Jul 2014 16:00 1MW-10
05 Aug 2014 17:13HS14070721-04 15 Jul 2014 14:00 1MW-12
05 Aug 2014 17:13HS14070721-05 15 Jul 2014 14:00 1MW-12 DUP
06-Aug-14Date: ALS Group USA, Corp
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84404 Instrument: FID-16 Method: SW8015M
Sample ID:MBLK-84404 Units:mg/L Analysis Date:31-Jul-2014 11:48
Run ID:FID-16_238668 SeqNo:2953985 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
TPH (Diesel Range)U 0.050
TPH (Oil Range)U 0.10
0.04709 0.06061 0 77.7 60 - 1350.0050Surr: 2-Fluorobiphenyl
Sample ID:LCS-84404 Units:mg/L Analysis Date:31-Jul-2014 13:00
Run ID:FID-16_238668 SeqNo:2953986 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
TPH (Diesel Range)0.7021 0.6061 0 116 70 - 1300.050
TPH (Oil Range)0.6306 0.6061 0 104 70 - 1300.10
0.04703 0.06061 0 77.6 60 - 1350.0050Surr: 2-Fluorobiphenyl
Sample ID:LCSD-84404 Units:mg/L Analysis Date:31-Jul-2014 13:27
Run ID:FID-16_238668 SeqNo:2953987 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
TPH (Diesel Range)0.7065 0.6061 0.7021 117 70 - 130 0.7021 0.624 200.050
TPH (Oil Range)0.6187 0.6061 0.6306 102 70 - 130 0.6306 1.91 200.10
0.04576 0.06061 0.04703 75.5 60 - 135 0.04703 2.74 200.0050Surr: 2-Fluorobiphenyl
The following samples were anayzed in this batch:HS14070721-01 HS14070721-02 HS14070721-03 HS14070721-04
HS14070721-05 HS14070721-06
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84484 Instrument: FID-7 Method: SW8015M
Sample ID:MBLK-84484 Units:mg/Kg Analysis Date:31-Jul-2014 17:50
Run ID:FID-7_238536 SeqNo:2951020 PrepDate:25-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
TPH (Diesel Range)U 1.7
TPH (Motor Oil Range)U 3.4
2.885 3.33 0 86.6 60 - 1350.10Surr: 2-Fluorobiphenyl
Sample ID:LCS-84484 Units:mg/Kg Analysis Date:31-Jul-2014 18:13
Run ID:FID-7_238536 SeqNo:2951021 PrepDate:25-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
TPH (Diesel Range)30.56 33.33 0 91.7 70 - 1301.7
TPH (Motor Oil Range)26.49 33.33 0 79.5 70 - 1303.4
3.12 3.33 0 93.7 60 - 1350.10Surr: 2-Fluorobiphenyl
Sample ID:LCSD-84484 Units:mg/Kg Analysis Date:31-Jul-2014 18:35
Run ID:FID-7_238536 SeqNo:2951022 PrepDate:25-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
TPH (Diesel Range)30.37 33.33 30.56 91.1 70 - 130 30.56 0.629 301.7
TPH (Motor Oil Range)26.37 33.33 26.49 79.1 70 - 130 26.49 0.456 303.4
3.074 3.33 3.12 92.3 60 - 135 3.12 1.47 300.10Surr: 2-Fluorobiphenyl
The following samples were anayzed in this batch:HS14070721-07 HS14070721-08 HS14070721-09 HS14070721-10
HS14070721-11 HS14070721-12 HS14070721-13 HS14070721-14
HS14070721-15 HS14070721-19 HS14070721-20 HS14070721-21
HS14070721-22
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238322 Instrument: FID-1 Method: SW8015
Sample ID:BLKW-140728 Units:mg/L Analysis Date:28-Jul-2014 15:05
Run ID:FID-1_238322 SeqNo:2946370 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ethylene Glycol U 1.0
Propylene glycol U 1.0
Sample ID:LCSW-140728 Units:mg/L Analysis Date:28-Jul-2014 13:35
Run ID:FID-1_238322 SeqNo:2946368 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ethylene Glycol 20.17 25 0 80.7 70 - 1301.0
Propylene glycol 21.28 25 0 85.1 70 - 1301.0
Sample ID:LCSDW-140728 Units:mg/L Analysis Date:28-Jul-2014 14:05
Run ID:FID-1_238322 SeqNo:2946369 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Ethylene Glycol 24.17 25 20.17 96.7 70 - 130 20.17 18 201.0
Propylene glycol 21.82 25 21.28 87.3 70 - 130 21.28 2.5 201.0
The following samples were anayzed in this batch:HS14070721-04 HS14070721-06
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237864 Instrument: FID-14 Method: SW8015M
Sample ID:GBLKS1-140722 Units:mg/Kg Analysis Date:22-Jul-2014 19:22
Run ID:FID-14_237864 SeqNo:2935363 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
GRO (C6-C10)U 0.050
0.07025 0.1 0 70.3 70 - 1300.0050Surr: 4-Bromofluorobenzene
Sample ID:GLCS-140722 Units:mg/Kg Analysis Date:22-Jul-2014 19:55
Run ID:FID-14_237864 SeqNo:2935365 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
GRO (C6-C10)1.167 1 0 117 70 - 1300.050
0.08007 0.1 0 80.1 70 - 1300.0050Surr: 4-Bromofluorobenzene
Sample ID:HS14070721-07MS Units:mg/Kg Analysis Date:22-Jul-2014 21:47
Run ID:FID-14_237864 SeqNo:2935372 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:B-18A (1-2)
GRO (C6-C10)0.576 1 0 57.6 70 - 130 S 0.050
0.08174 0.1 0 81.7 70 - 1300.0050Surr: 4-Bromofluorobenzene
Sample ID:HS14070721-07MSD Units:mg/Kg Analysis Date:22-Jul-2014 22:03
Run ID:FID-14_237864 SeqNo:2935373 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:B-18A (1-2)
GRO (C6-C10)0.8226 1 0.576 82.3 70 - 130 0.576 35.3 30 R 0.050
0.08261 0.1 0.08174 82.6 70 - 130 0.08174 1.05 300.0050Surr: 4-Bromofluorobenzene
The following samples were anayzed in this batch:HS14070721-07 HS14070721-08 HS14070721-10 HS14070721-11
HS14070721-12 HS14070721-13 HS14070721-14 HS14070721-15
HS14070721-19 HS14070721-20 HS14070721-21 HS14070721-22
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237910 Instrument: FID-14 Method: SW8015M
Sample ID:GBLKS1-140723 Units:mg/Kg Analysis Date:23-Jul-2014 13:19
Run ID:FID-14_237910 SeqNo:2936473 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
GRO (C6-C10)U 0.050
0.07308 0.1 0 73.1 70 - 1300.0050Surr: 4-Bromofluorobenzene
Sample ID:GLCS1-140723 Units:mg/Kg Analysis Date:23-Jul-2014 14:55
Run ID:FID-14_237910 SeqNo:2936517 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
GRO (C6-C10)1.04 1 0 1040.050
0.08254 0.1 0 82.5 70 - 1300.0050Surr: 4-Bromofluorobenzene
Sample ID:GLCSDS1-140723 Units:mg/Kg Analysis Date:23-Jul-2014 13:51
Run ID:FID-14_237910 SeqNo:2936474 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
GRO (C6-C10)1.026 1 1.04 103 70 - 130 1.04 1.39 300.050
0.07981 0.1 0.08254 79.8 70 - 130 0.08254 3.36 300.0050Surr: 4-Bromofluorobenzene
The following samples were anayzed in this batch:HS14070721-09
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237931 Instrument: FID-14 Method: SW8015M
Sample ID:GBLKW1-140723 Units:mg/L Analysis Date:23-Jul-2014 18:11
Run ID:FID-14_237931 SeqNo:2937083 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
GRO (C6-C10)U 0.0500
0.08299 0.1 0 83.0 70 - 1300.00500Surr: 4-Bromofluorobenzene
Sample ID:GLCSW1-140723 Units:mg/L Analysis Date:23-Jul-2014 18:27
Run ID:FID-14_237931 SeqNo:2937084 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
GRO (C6-C10)1.172 1 0 117 70 - 1300.0500
0.09085 0.1 0 90.8 70 - 1300.00500Surr: 4-Bromofluorobenzene
Sample ID:HS14070768-01MS Units:mg/L Analysis Date:23-Jul-2014 20:17
Run ID:FID-14_237931 SeqNo:2937091 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
GRO (C6-C10)1.396 1 0.02547 137 70 - 130 S 0.0500
0.09062 0.1 0 90.6 70 - 1300.00500Surr: 4-Bromofluorobenzene
Sample ID:HS14070768-01MSD Units:mg/L Analysis Date:23-Jul-2014 20:33
Run ID:FID-14_237931 SeqNo:2937092 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
GRO (C6-C10)1.529 1 1.396 150 70 - 130 1.396 9.14 30 S 0.0500
0.09378 0.1 0.09062 93.8 70 - 130 0.09062 3.44 300.00500Surr: 4-Bromofluorobenzene
The following samples were anayzed in this batch:HS14070721-01 HS14070721-02 HS14070721-03 HS14070721-04
HS14070721-05 HS14070721-06
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:MBLK-84329 Units:ug/L Analysis Date:24-Jul-2014 14:53
Run ID:SV-7_238164 SeqNo:2942797 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,1´-Biphenyl U 0.20
2,4,5-Trichlorophenol U 0.20
2,4,6-Trichlorophenol U 0.20
2,4-Dichlorophenol U 0.20
2,4-Dimethylphenol U 0.20
2,4-Dinitrophenol U 1.0
2,4-Dinitrotoluene U 0.20
2,6-Dinitrotoluene U 0.20
2-Chloronaphthalene U 0.20
2-Chlorophenol U 0.20
2-Methylnaphthalene U 0.10
2-Methylphenol U 0.20
2-Nitroaniline U 0.20
2-Nitrophenol U 0.20
3&4-Methylphenol U 0.20
3,3´-Dichlorobenzidine U 0.20
3-Nitroaniline U 0.20
4,6-Dinitro-2-methylphenol U 0.20
4-Bromophenyl phenyl ether U 0.20
4-Chloro-3-methylphenol U 0.20
4-Chloroaniline U 0.20
4-Chlorophenyl phenyl ether U 0.20
4-Nitroaniline U 0.20
4-Nitrophenol U 1.0
Acenaphthene U 0.10
Acenaphthylene U 0.10
Acetophenone U 0.20
Anthracene U 0.10
Atrazine U 0.20
Benz(a)anthracene U 0.10
Benzaldehyde U 0.20
Benzo(a)pyrene U 0.10
Benzo(b)fluoranthene U 0.10
Benzo(g,h,i)perylene U 0.10
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:MBLK-84329 Units:ug/L Analysis Date:24-Jul-2014 14:53
Run ID:SV-7_238164 SeqNo:2942797 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Benzo(k)fluoranthene U 0.10
Bis(2-chloroethoxy)methane U 0.20
Bis(2-chloroethyl)ether U 0.20
Bis(2-chloroisopropyl)ether U 0.20
Bis(2-ethylhexyl)phthalate U 0.20
Butyl benzyl phthalate U 0.20
Caprolactam U 0.20
Carbazole U 0.20
Chrysene U 0.10
Dibenz(a,h)anthracene U 0.10
Dibenzofuran U 0.10
Diethyl phthalate U 0.20
Dimethyl phthalate U 0.20
Di-n-butyl phthalate U 0.20
Di-n-octyl phthalate U 0.20
Fluoranthene U 0.10
Fluorene U 0.10
Hexachlorobenzene U 0.20
Hexachlorobutadiene U 0.20
Hexachlorocyclopentadiene U 0.20
Hexachloroethane U 0.20
Indeno(1,2,3-cd)pyrene U 0.10
Isophorone U 0.20
Naphthalene U 0.10
Nitrobenzene U 0.20
N-Nitrosodi-n-propylamine U 0.20
N-Nitrosodiphenylamine U 0.20
Pentachlorophenol U 0.20
Phenanthrene U 0.10
Phenol U 0.20
Pyrene U 0.10
2.999 5 0 60.0 34 - 1290.20Surr: 2,4,6-Tribromophenol
3.352 5 0 67.0 40 - 1250.20Surr: 2-Fluorobiphenyl
4.033 5 0 80.7 20 - 1200.20Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:MBLK-84329 Units:ug/L Analysis Date:24-Jul-2014 14:53
Run ID:SV-7_238164 SeqNo:2942797 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
3.789 5 0 75.8 40 - 1350.20Surr: 4-Terphenyl-d14
3.631 5 0 72.6 41 - 1200.20Surr: Nitrobenzene-d5
3.785 5 0 75.7 20 - 1200.20Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:LCS-84329 Units:ug/L Analysis Date:24-Jul-2014 15:12
Run ID:SV-7_238164 SeqNo:2942798 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,1´-Biphenyl 3.102 5 0 62.0 45 - 1250.20
2,4,5-Trichlorophenol 2.901 5 0 58.0 46 - 1200.20
2,4,6-Trichlorophenol 3.061 5 0 61.2 42 - 1200.20
2,4-Dichlorophenol 3.021 5 0 60.4 49 - 1200.20
2,4-Dimethylphenol 2.613 5 0 52.3 35 - 1200.20
2,4-Dinitrophenol 2.963 5 0 59.3 15 - 1201.0
2,4-Dinitrotoluene 3.724 5 0 74.5 50 - 1220.20
2,6-Dinitrotoluene 3.653 5 0 73.1 50 - 1200.20
2-Chloronaphthalene 3.165 5 0 63.3 50 - 1200.20
2-Chlorophenol 3.119 5 0 62.4 40 - 1200.20
2-Methylnaphthalene 3.106 5 0 62.1 50 - 1200.10
2-Methylphenol 3.2 5 0 64.0 45 - 1200.20
2-Nitroaniline 4.777 5 0 95.5 28 - 1390.20
2-Nitrophenol 3.411 5 0 68.2 40 - 1200.20
3&4-Methylphenol 3.201 5 0 64.0 35 - 1200.20
3,3´-Dichlorobenzidine 3.354 5 0 67.1 15 - 1200.20
3-Nitroaniline 3.495 5 0 69.9 30 - 1200.20
4,6-Dinitro-2-methylphenol 3.765 5 0 75.3 25 - 1210.20
4-Bromophenyl phenyl ether 3.178 5 0 63.6 45 - 1200.20
4-Chloro-3-methylphenol 3.194 5 0 63.9 47 - 1200.20
4-Chloroaniline 3.068 5 0 61.4 20 - 1200.20
4-Chlorophenyl phenyl ether 3.075 5 0 61.5 50 - 1200.20
4-Nitroaniline 3.504 5 0 70.1 30 - 1330.20
4-Nitrophenol 4.031 5 0 80.6 30 - 1301.0
Acenaphthene 2.968 5 0 59.4 45 - 1200.10
Acenaphthylene 3.251 5 0 65.0 47 - 1200.10
Acetophenone 2.897 5 0 57.9 40 - 1200.20
Anthracene 3.237 5 0 64.7 45 - 1200.10
Atrazine 2.986 5 0 59.7 40 - 1300.20
Benz(a)anthracene 3.393 5 0 67.9 40 - 1200.10
Benzaldehyde 0.8008 5 0 16.0 15 - 1200.20
Benzo(a)pyrene 3.478 5 0 69.6 45 - 1200.10
Benzo(b)fluoranthene 3.508 5 0 70.2 50 - 1200.10
Benzo(g,h,i)perylene 3.445 5 0 68.9 42 - 1270.10
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:LCS-84329 Units:ug/L Analysis Date:24-Jul-2014 15:12
Run ID:SV-7_238164 SeqNo:2942798 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Benzo(k)fluoranthene 3.341 5 0 66.8 45 - 1270.10
Bis(2-chloroethoxy)methane 3.267 5 0 65.3 45 - 1200.20
Bis(2-chloroethyl)ether 3.505 5 0 70.1 37 - 1210.20
Bis(2-chloroisopropyl)ether 3.212 5 0 64.2 40 - 1200.20
Bis(2-ethylhexyl)phthalate 4.014 5 0 80.3 40 - 1390.20
Butyl benzyl phthalate 4.012 5 0 80.2 47 - 1230.20
Caprolactam 3.269 5 0 65.4 35 - 1340.20
Carbazole 3.196 5 0 63.9 42 - 1280.20
Chrysene 3.309 5 0 66.2 43 - 1200.10
Dibenz(a,h)anthracene 3.433 5 0 68.7 45 - 1250.10
Dibenzofuran 3.105 5 0 62.1 50 - 1200.10
Diethyl phthalate 3.42 5 0 68.4 41 - 1200.20
Dimethyl phthalate 3.24 5 0 64.8 40 - 1220.20
Di-n-butyl phthalate 3.652 5 0 73.0 45 - 1230.20
Di-n-octyl phthalate 4.256 5 0 85.1 45 - 1290.20
Fluoranthene 3.342 5 0 66.8 45 - 1250.10
Fluorene 3.16 5 0 63.2 49 - 1200.10
Hexachlorobenzene 3.09 5 0 61.8 48 - 1200.20
Hexachlorobutadiene 2.927 5 0 58.5 40 - 1200.20
Hexachlorocyclopentadiene 3.122 5 0 62.4 34 - 1360.20
Hexachloroethane 3.144 5 0 62.9 40 - 1200.20
Indeno(1,2,3-cd)pyrene 3.651 5 0 73.0 41 - 1280.10
Isophorone 3.369 5 0 67.4 40 - 1210.20
Naphthalene 3.048 5 0 61.0 45 - 1200.10
Nitrobenzene 3.397 5 0 67.9 44 - 1200.20
N-Nitrosodi-n-propylamine 3.293 5 0 65.9 40 - 1200.20
N-Nitrosodiphenylamine 3.22 5 0 64.4 40 - 1250.20
Pentachlorophenol 3.077 5 0 61.5 19 - 1210.20
Phenanthrene 3.288 5 0 65.8 45 - 1210.10
Phenol 3.517 5 0 70.3 20 - 1240.20
Pyrene 3.458 5 0 69.2 40 - 1300.10
3.531 5 0 70.6 34 - 1290.20Surr: 2,4,6-Tribromophenol
3.168 5 0 63.4 40 - 1250.20Surr: 2-Fluorobiphenyl
3.227 5 0 64.5 20 - 1200.20Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:LCS-84329 Units:ug/L Analysis Date:24-Jul-2014 15:12
Run ID:SV-7_238164 SeqNo:2942798 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
3.502 5 0 70.0 40 - 1350.20Surr: 4-Terphenyl-d14
3.405 5 0 68.1 41 - 1200.20Surr: Nitrobenzene-d5
3.173 5 0 63.5 20 - 1200.20Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:LCSD-84329 Units:ug/L Analysis Date:24-Jul-2014 15:31
Run ID:SV-7_238164 SeqNo:2942799 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
1,1´-Biphenyl 3.197 5 3.102 63.9 45 - 125 3.102 3.02 200.20
2,4,5-Trichlorophenol 3.122 5 2.901 62.4 46 - 120 2.901 7.36 200.20
2,4,6-Trichlorophenol 3.25 5 3.061 65.0 42 - 120 3.061 6 200.20
2,4-Dichlorophenol 3.297 5 3.021 65.9 49 - 120 3.021 8.73 200.20
2,4-Dimethylphenol 2.911 5 2.613 58.2 35 - 120 2.613 10.8 200.20
2,4-Dinitrophenol 3.474 5 2.963 69.5 15 - 120 2.963 15.9 501.0
2,4-Dinitrotoluene 3.945 5 3.724 78.9 50 - 122 3.724 5.76 200.20
2,6-Dinitrotoluene 3.9 5 3.653 78.0 50 - 120 3.653 6.53 200.20
2-Chloronaphthalene 3.259 5 3.165 65.2 50 - 120 3.165 2.93 200.20
2-Chlorophenol 3.289 5 3.119 65.8 40 - 120 3.119 5.3 200.20
2-Methylnaphthalene 3.321 5 3.106 66.4 50 - 120 3.106 6.69 200.10
2-Methylphenol 3.44 5 3.2 68.8 45 - 120 3.2 7.24 200.20
2-Nitroaniline 5.055 5 4.777 101 28 - 139 4.777 5.64 200.20
2-Nitrophenol 3.65 5 3.411 73.0 40 - 120 3.411 6.76 200.20
3&4-Methylphenol 3.472 5 3.201 69.4 35 - 120 3.201 8.12 200.20
3,3´-Dichlorobenzidine 3.56 5 3.354 71.2 15 - 120 3.354 5.96 200.20
3-Nitroaniline 3.626 5 3.495 72.5 30 - 120 3.495 3.67 200.20
4,6-Dinitro-2-methylphenol 4.372 5 3.765 87.4 25 - 121 3.765 14.9 300.20
4-Bromophenyl phenyl ether 3.462 5 3.178 69.2 45 - 120 3.178 8.57 200.20
4-Chloro-3-methylphenol 3.512 5 3.194 70.2 47 - 120 3.194 9.47 200.20
4-Chloroaniline 3.33 5 3.068 66.6 20 - 120 3.068 8.17 200.20
4-Chlorophenyl phenyl ether 3.202 5 3.075 64.0 50 - 120 3.075 4.03 200.20
4-Nitroaniline 3.733 5 3.504 74.7 30 - 133 3.504 6.33 200.20
4-Nitrophenol 4.272 5 4.031 85.4 30 - 130 4.031 5.8 201.0
Acenaphthene 3.139 5 2.968 62.8 45 - 120 2.968 5.59 200.10
Acenaphthylene 3.36 5 3.251 67.2 47 - 120 3.251 3.31 200.10
Acetophenone 3.107 5 2.897 62.1 40 - 120 2.897 6.98 200.20
Anthracene 3.533 5 3.237 70.7 45 - 120 3.237 8.74 200.10
Atrazine 3.308 5 2.986 66.2 40 - 130 2.986 10.2 200.20
Benz(a)anthracene 3.618 5 3.393 72.4 40 - 120 3.393 6.41 200.10
Benzaldehyde 0.7993 5 0.8008 16.0 15 - 120 0.8008 0.19 300.20
Benzo(a)pyrene 3.676 5 3.478 73.5 45 - 120 3.478 5.52 200.10
Benzo(b)fluoranthene 3.694 5 3.508 73.9 50 - 120 3.508 5.18 200.10
Benzo(g,h,i)perylene 3.594 5 3.445 71.9 42 - 127 3.445 4.24 200.10
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:LCSD-84329 Units:ug/L Analysis Date:24-Jul-2014 15:31
Run ID:SV-7_238164 SeqNo:2942799 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
Benzo(k)fluoranthene 3.513 5 3.341 70.3 45 - 127 3.341 5.02 200.10
Bis(2-chloroethoxy)methane 3.528 5 3.267 70.6 45 - 120 3.267 7.67 200.20
Bis(2-chloroethyl)ether 3.635 5 3.505 72.7 37 - 121 3.505 3.65 200.20
Bis(2-chloroisopropyl)ether 3.483 5 3.212 69.7 40 - 120 3.212 8.11 200.20
Bis(2-ethylhexyl)phthalate 4.216 5 4.014 84.3 40 - 139 4.014 4.89 200.20
Butyl benzyl phthalate 4.247 5 4.012 84.9 47 - 123 4.012 5.7 200.20
Caprolactam 3.829 5 3.269 76.6 35 - 134 3.269 15.8 200.20
Carbazole 3.457 5 3.196 69.1 42 - 128 3.196 7.84 200.20
Chrysene 3.513 5 3.309 70.3 43 - 120 3.309 5.98 200.10
Dibenz(a,h)anthracene 3.611 5 3.433 72.2 45 - 125 3.433 5.06 200.10
Dibenzofuran 3.288 5 3.105 65.8 50 - 120 3.105 5.72 200.10
Diethyl phthalate 3.553 5 3.42 71.1 41 - 120 3.42 3.83 200.20
Dimethyl phthalate 3.433 5 3.24 68.7 40 - 122 3.24 5.77 200.20
Di-n-butyl phthalate 3.972 5 3.652 79.4 45 - 123 3.652 8.4 200.20
Di-n-octyl phthalate 4.493 5 4.256 89.9 45 - 129 4.256 5.41 200.20
Fluoranthene 3.638 5 3.342 72.8 45 - 125 3.342 8.47 200.10
Fluorene 3.357 5 3.16 67.1 49 - 120 3.16 6.04 200.10
Hexachlorobenzene 3.386 5 3.09 67.7 48 - 120 3.09 9.15 200.20
Hexachlorobutadiene 3.129 5 2.927 62.6 40 - 120 2.927 6.66 200.20
Hexachlorocyclopentadiene 3.328 5 3.122 66.6 34 - 136 3.122 6.39 200.20
Hexachloroethane 3.348 5 3.144 67.0 40 - 120 3.144 6.29 200.20
Indeno(1,2,3-cd)pyrene 3.852 5 3.651 77.0 41 - 128 3.651 5.36 200.10
Isophorone 3.722 5 3.369 74.4 40 - 121 3.369 9.95 200.20
Naphthalene 3.27 5 3.048 65.4 45 - 120 3.048 7.03 200.10
Nitrobenzene 3.662 5 3.397 73.2 44 - 120 3.397 7.51 200.20
N-Nitrosodi-n-propylamine 3.552 5 3.293 71.0 40 - 120 3.293 7.59 200.20
N-Nitrosodiphenylamine 3.547 5 3.22 70.9 40 - 125 3.22 9.67 200.20
Pentachlorophenol 3.567 5 3.077 71.3 19 - 121 3.077 14.7 200.20
Phenanthrene 3.567 5 3.288 71.3 45 - 121 3.288 8.14 200.10
Phenol 3.738 5 3.517 74.8 20 - 124 3.517 6.09 200.20
Pyrene 3.536 5 3.458 70.7 40 - 130 3.458 2.22 200.10
3.526 5 3.531 70.5 34 - 129 3.531 0.1470.20Surr: 2,4,6-Tribromophenol
3.12 5 3.168 62.4 40 - 125 3.168 1.50.20Surr: 2-Fluorobiphenyl
3.323 5 3.227 66.5 20 - 120 3.227 2.910.20Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84329 Instrument: SV-7 Method: SW8270
Sample ID:LCSD-84329 Units:ug/L Analysis Date:24-Jul-2014 15:31
Run ID:SV-7_238164 SeqNo:2942799 PrepDate:21-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCSD
Client ID:
3.529 5 3.502 70.6 40 - 135 3.502 0.7650.20Surr: 4-Terphenyl-d14
3.471 5 3.405 69.4 41 - 120 3.405 1.910.20Surr: Nitrobenzene-d5
3.29 5 3.173 65.8 20 - 120 3.173 3.590.20Surr: Phenol-d6
The following samples were anayzed in this batch:HS14070721-01 HS14070721-02 HS14070721-03 HS14070721-04
HS14070721-05 HS14070721-06
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:MBLK-84405 Units:ug/Kg Analysis Date:23-Jul-2014 16:29
Run ID:SV-4_238295 SeqNo:2945428 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,1´-Biphenyl U 6.6
2,4,5-Trichlorophenol U 6.6
2,4,6-Trichlorophenol U 6.6
2,4-Dichlorophenol U 6.6
2,4-Dimethylphenol U 6.6
2,4-Dinitrophenol U 13
2,4-Dinitrotoluene U 6.6
2,6-Dinitrotoluene U 6.6
2-Chloronaphthalene U 6.6
2-Chlorophenol U 6.6
2-Methylnaphthalene U 3.3
2-Methylphenol U 6.6
2-Nitroaniline U 6.6
2-Nitrophenol U 6.6
3&4-Methylphenol U 6.6
3,3´-Dichlorobenzidine U 6.6
3-Nitroaniline U 6.6
4,6-Dinitro-2-methylphenol U 6.6
4-Bromophenyl phenyl ether U 6.6
4-Chloro-3-methylphenol U 6.6
4-Chloroaniline U 6.6
4-Chlorophenyl phenyl ether U 6.6
4-Nitroaniline U 6.6
4-Nitrophenol U 13
Acenaphthene U 3.3
Acenaphthylene U 3.3
Acetophenone U 6.6
Anthracene U 3.3
Atrazine U 6.6
Benz(a)anthracene U 3.3
Benzaldehyde U 6.6
Benzo(a)pyrene U 3.3
Benzo(b)fluoranthene U 3.3
Benzo(g,h,i)perylene U 3.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:MBLK-84405 Units:ug/Kg Analysis Date:23-Jul-2014 16:29
Run ID:SV-4_238295 SeqNo:2945428 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Benzo(k)fluoranthene U 3.3
Bis(2-chloroethoxy)methane U 6.6
Bis(2-chloroethyl)ether U 6.6
Bis(2-chloroisopropyl)ether U 6.6
Bis(2-ethylhexyl)phthalate U 6.6
Butyl benzyl phthalate U 6.6
Caprolactam U 6.6
Carbazole U 6.6
Chrysene U 3.3
Dibenz(a,h)anthracene U 3.3
Dibenzofuran U 3.3
Diethyl phthalate U 6.6
Dimethyl phthalate U 6.6
Di-n-butyl phthalate U 6.6
Di-n-octyl phthalate U 6.6
Fluoranthene U 3.3
Fluorene U 3.3
Hexachlorobenzene U 6.6
Hexachlorobutadiene U 6.6
Hexachlorocyclopentadiene U 6.6
Hexachloroethane U 6.6
Indeno(1,2,3-cd)pyrene U 3.3
Isophorone U 6.6
Naphthalene U 3.3
Nitrobenzene U 6.6
N-Nitrosodi-n-propylamine U 6.6
N-Nitrosodiphenylamine U 6.6
Pentachlorophenol U 6.6
Phenanthrene U 3.3
Phenol U 6.6
Pyrene U 3.3
114.7 167 0 68.7 36 - 1266.6Surr: 2,4,6-Tribromophenol
127 167 0 76.0 43 - 1256.6Surr: 2-Fluorobiphenyl
108.5 167 0 65.0 37 - 1256.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:MBLK-84405 Units:ug/Kg Analysis Date:23-Jul-2014 16:29
Run ID:SV-4_238295 SeqNo:2945428 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
126.2 167 0 75.6 32 - 1256.6Surr: 4-Terphenyl-d14
110.6 167 0 66.2 37 - 1256.6Surr: Nitrobenzene-d5
110.3 167 0 66.1 40 - 1256.6Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:LCS-84405 Units:ug/Kg Analysis Date:23-Jul-2014 16:49
Run ID:SV-4_238295 SeqNo:2945429 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,1´-Biphenyl 129.9 167 0 77.8 50 - 1206.6
2,4,5-Trichlorophenol 145.4 167 0 87.1 45 - 1276.6
2,4,6-Trichlorophenol 144.7 167 0 86.7 45 - 1306.6
2,4-Dichlorophenol 141.3 167 0 84.6 45 - 1256.6
2,4-Dimethylphenol 128.6 167 0 77.0 45 - 1206.6
2,4-Dinitrophenol 115.5 167 0 69.1 10 - 12613
2,4-Dinitrotoluene 148.2 167 0 88.7 50 - 1306.6
2,6-Dinitrotoluene 150.4 167 0 90.1 50 - 1256.6
2-Chloronaphthalene 131.5 167 0 78.8 50 - 1456.6
2-Chlorophenol 125.4 167 0 75.1 45 - 1206.6
2-Methylnaphthalene 130.8 167 0 78.3 50 - 1203.3
2-Methylphenol 117.9 167 0 70.6 45 - 1206.6
2-Nitroaniline 141.8 167 0 84.9 45 - 1386.6
2-Nitrophenol 154.8 167 0 92.7 45 - 1256.6
3&4-Methylphenol 119.5 167 0 71.5 45 - 1206.6
3,3´-Dichlorobenzidine 143.2 167 0 85.7 15 - 1206.6
3-Nitroaniline 131.2 167 0 78.5 40 - 1206.6
4,6-Dinitro-2-methylphenol 134.1 167 0 80.3 15 - 1356.6
4-Bromophenyl phenyl ether 146.9 167 0 88.0 50 - 1256.6
4-Chloro-3-methylphenol 133.2 167 0 79.7 45 - 1306.6
4-Chloroaniline 115.5 167 0 69.2 20 - 1206.6
4-Chlorophenyl phenyl ether 145.1 167 0 86.9 50 - 1206.6
4-Nitroaniline 95.01 167 0 56.9 50 - 1276.6
4-Nitrophenol 131.7 167 0 78.9 40 - 14713
Acenaphthene 123.5 167 0 74.0 50 - 1203.3
Acenaphthylene 135.4 167 0 81.1 50 - 1203.3
Acetophenone 111.6 167 0 66.8 50 - 1206.6
Anthracene 128.1 167 0 76.7 50 - 1233.3
Atrazine 143.6 167 0 86.0 29 - 1486.6
Benz(a)anthracene 132.5 167 0 79.3 50 - 1313.3
Benzaldehyde 38.09 167 0 22.8 22 - 1296.6
Benzo(a)pyrene 127.5 167 0 76.3 50 - 1303.3
Benzo(b)fluoranthene 139.4 167 0 83.4 50 - 1373.3
Benzo(g,h,i)perylene 140.9 167 0 84.4 50 - 1303.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:LCS-84405 Units:ug/Kg Analysis Date:23-Jul-2014 16:49
Run ID:SV-4_238295 SeqNo:2945429 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Benzo(k)fluoranthene 123.2 167 0 73.8 50 - 1433.3
Bis(2-chloroethoxy)methane 118.9 167 0 71.2 50 - 1206.6
Bis(2-chloroethyl)ether 112.5 167 0 67.4 45 - 1276.6
Bis(2-chloroisopropyl)ether 124 167 0 74.3 50 - 1206.6
Bis(2-ethylhexyl)phthalate 118.5 167 0 71.0 21 - 1486.6
Butyl benzyl phthalate 112.5 167 0 67.3 50 - 1366.6
Caprolactam 127.8 167 0 76.5 50 - 1356.6
Carbazole 92.83 167 0 55.6 50 - 1436.6
Chrysene 130.9 167 0 78.4 50 - 1303.3
Dibenz(a,h)anthracene 146.2 167 0 87.6 50 - 1303.3
Dibenzofuran 134 167 0 80.3 50 - 1253.3
Diethyl phthalate 125.7 167 0 75.3 50 - 1256.6
Dimethyl phthalate 135.4 167 0 81.1 50 - 1256.6
Di-n-butyl phthalate 122.3 167 0 73.2 50 - 1406.6
Di-n-octyl phthalate 116.5 167 0 69.8 50 - 1406.6
Fluoranthene 138.2 167 0 82.8 50 - 1313.3
Fluorene 138.3 167 0 82.8 50 - 1253.3
Hexachlorobenzene 153.1 167 0 91.7 50 - 1246.6
Hexachlorobutadiene 159.5 167 0 95.5 50 - 1256.6
Hexachlorocyclopentadiene 147.9 167 0 88.6 45 - 1356.6
Hexachloroethane 113.1 167 0 67.7 45 - 1256.6
Indeno(1,2,3-cd)pyrene 154.8 167 0 92.7 45 - 1393.3
Isophorone 118.6 167 0 71.0 45 - 1306.6
Naphthalene 137.2 167 0 82.1 50 - 1253.3
Nitrobenzene 116.2 167 0 69.6 50 - 1256.6
N-Nitrosodi-n-propylamine 115.3 167 0 69.1 45 - 1206.6
N-Nitrosodiphenylamine 124.8 167 0 74.8 50 - 1306.6
Pentachlorophenol 120.3 167 0 72.0 23 - 1366.6
Phenanthrene 133.2 167 0 79.8 50 - 1253.3
Phenol 121 167 0 72.5 45 - 1306.6
Pyrene 124.1 167 0 74.3 45 - 1303.3
156.5 167 0 93.7 36 - 1266.6Surr: 2,4,6-Tribromophenol
134.4 167 0 80.5 43 - 1256.6Surr: 2-Fluorobiphenyl
108.1 167 0 64.7 37 - 1256.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:LCS-84405 Units:ug/Kg Analysis Date:23-Jul-2014 16:49
Run ID:SV-4_238295 SeqNo:2945429 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
130.9 167 0 78.4 32 - 1256.6Surr: 4-Terphenyl-d14
116.2 167 0 69.6 37 - 1256.6Surr: Nitrobenzene-d5
112.6 167 0 67.4 40 - 1256.6Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:HS14070861-21MS Units:ug/Kg Analysis Date:23-Jul-2014 18:32
Run ID:SV-4_238295 SeqNo:2945431 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,1´-Biphenyl 94.9 166.9 0 56.9 50 - 1206.6
2,4,5-Trichlorophenol 104.6 166.9 0 62.7 45 - 1276.6
2,4,6-Trichlorophenol 105.2 166.9 0 63.0 45 - 1306.6
2,4-Dichlorophenol 104.4 166.9 0 62.6 45 - 1256.6
2,4-Dimethylphenol 92.07 166.9 0 55.2 45 - 1206.6
2,4-Dinitrophenol 34.44 166.9 0 20.6 10 - 12613
2,4-Dinitrotoluene 109.4 166.9 0 65.6 50 - 1306.6
2,6-Dinitrotoluene 115.9 166.9 0 69.5 50 - 1256.6
2-Chloronaphthalene 107.6 166.9 0 64.5 50 - 1456.6
2-Chlorophenol 95.5 166.9 0 57.2 45 - 1206.6
2-Methylnaphthalene 102.9 166.9 0 61.6 50 - 1203.3
2-Methylphenol 90.68 166.9 0 54.3 45 - 1206.6
2-Nitroaniline 105.8 166.9 0 63.4 45 - 1386.6
2-Nitrophenol 100.8 166.9 0 60.4 45 - 1256.6
3&4-Methylphenol 90.1 166.9 0 54.0 45 - 1206.6
3,3´-Dichlorobenzidine 85.14 166.9 0 51.0 15 - 1206.6
3-Nitroaniline 86.85 166.9 0 52.0 40 - 1206.6
4,6-Dinitro-2-methylphenol 63.68 166.9 0 38.2 15 - 1356.6
4-Bromophenyl phenyl ether 110.6 166.9 0 66.2 50 - 1256.6
4-Chloro-3-methylphenol 102.3 166.9 0 61.3 45 - 1306.6
4-Chloroaniline 86.3 166.9 0 51.7 20 - 1206.6
4-Chlorophenyl phenyl ether 111.5 166.9 0 66.8 50 - 1206.6
4-Nitroaniline 80.25 166.9 0 48.1 50 - 127 S 6.6
4-Nitrophenol 95.63 166.9 0 57.3 40 - 14713
Acenaphthene 92.05 166.9 0 55.2 50 - 1203.3
Acenaphthylene 101.3 166.9 0 60.7 50 - 1203.3
Acetophenone 86.88 166.9 0 52.1 50 - 1206.6
Anthracene 100.2 166.9 0 60.1 50 - 1233.3
Atrazine 116.8 166.9 0 70.0 29 - 1486.6
Benz(a)anthracene 107.9 166.9 0 64.7 50 - 1313.3
Benzaldehyde 64.89 166.9 2.378 37.5 22 - 1296.6
Benzo(a)pyrene 100.2 166.9 0 60.0 50 - 1303.3
Benzo(b)fluoranthene 119.3 166.9 0 71.5 50 - 1373.3
Benzo(g,h,i)perylene 114.7 166.9 0 68.7 50 - 1303.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:HS14070861-21MS Units:ug/Kg Analysis Date:23-Jul-2014 18:32
Run ID:SV-4_238295 SeqNo:2945431 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Benzo(k)fluoranthene 89.59 166.9 0 53.7 50 - 1433.3
Bis(2-chloroethoxy)methane 90.12 166.9 0 54.0 50 - 1206.6
Bis(2-chloroethyl)ether 93.11 166.9 0 55.8 45 - 1276.6
Bis(2-chloroisopropyl)ether 97.34 166.9 0 58.3 50 - 1206.6
Bis(2-ethylhexyl)phthalate 100.7 166.9 5.387 57.1 21 - 1486.6
Butyl benzyl phthalate 94.39 166.9 0 56.6 50 - 1366.6
Caprolactam 72.56 166.9 0 43.5 50 - 135 S 6.6
Carbazole 101.9 166.9 0 61.0 50 - 1436.6
Chrysene 109.1 166.9 0 65.4 50 - 1303.3
Dibenz(a,h)anthracene 118.1 166.9 0 70.8 50 - 1303.3
Dibenzofuran 101.1 166.9 0 60.6 50 - 1253.3
Diethyl phthalate 96.03 166.9 0 57.5 50 - 1256.6
Dimethyl phthalate 102.5 166.9 0 61.4 50 - 1256.6
Di-n-butyl phthalate 100.6 166.9 4.503 57.6 50 - 1406.6
Di-n-octyl phthalate 92.88 166.9 0 55.7 50 - 1406.6
Fluoranthene 111 166.9 0 66.5 50 - 1313.3
Fluorene 108.3 166.9 0 64.9 50 - 1253.3
Hexachlorobenzene 119.4 166.9 0 71.5 50 - 1246.6
Hexachlorobutadiene 116 166.9 0 69.5 50 - 1256.6
Hexachlorocyclopentadiene 92.22 166.9 0 55.3 45 - 1356.6
Hexachloroethane 88.71 166.9 0 53.2 45 - 1256.6
Indeno(1,2,3-cd)pyrene 125.7 166.9 0 75.3 45 - 1393.3
Isophorone 91.23 166.9 0 54.7 45 - 1306.6
Naphthalene 104.6 166.9 0 62.7 50 - 1253.3
Nitrobenzene 88.42 166.9 0 53.0 50 - 1256.6
N-Nitrosodi-n-propylamine 88.59 166.9 0 53.1 45 - 1206.6
N-Nitrosodiphenylamine 98.04 166.9 0 58.7 50 - 1306.6
Pentachlorophenol 69.44 166.9 0 41.6 23 - 1366.6
Phenanthrene 110.2 166.9 0 66.0 50 - 1253.3
Phenol 90.47 166.9 0 54.2 45 - 1306.6
Pyrene 100.7 166.9 0 60.3 45 - 1303.3
118.8 166.9 0 71.2 36 - 1266.6Surr: 2,4,6-Tribromophenol
100.5 166.9 0 60.2 43 - 1256.6Surr: 2-Fluorobiphenyl
75.71 166.9 0 45.4 37 - 1256.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:HS14070861-21MS Units:ug/Kg Analysis Date:23-Jul-2014 18:32
Run ID:SV-4_238295 SeqNo:2945431 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
110.1 166.9 0 66.0 32 - 1256.6Surr: 4-Terphenyl-d14
85.72 166.9 0 51.4 37 - 1256.6Surr: Nitrobenzene-d5
85.58 166.9 0 51.3 40 - 1256.6Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:HS14070861-21MSD Units:ug/Kg Analysis Date:23-Jul-2014 18:53
Run ID:SV-4_238295 SeqNo:2945432 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,1´-Biphenyl 123.1 166.5 94.9 74.0 50 - 120 94.9 25.9 306.6
2,4,5-Trichlorophenol 129.9 166.5 104.6 78.0 45 - 127 104.6 21.5 306.6
2,4,6-Trichlorophenol 138.8 166.5 105.2 83.3 45 - 130 105.2 27.5 306.6
2,4-Dichlorophenol 130.6 166.5 104.4 78.5 45 - 125 104.4 22.3 306.6
2,4-Dimethylphenol 115.4 166.5 92.07 69.3 45 - 120 92.07 22.5 306.6
2,4-Dinitrophenol 29.26 166.5 34.44 17.6 10 - 126 34.44 16.3 3013
2,4-Dinitrotoluene 142 166.5 109.4 85.3 50 - 130 109.4 25.9 306.6
2,6-Dinitrotoluene 139.7 166.5 115.9 83.9 50 - 125 115.9 18.6 306.6
2-Chloronaphthalene 129.6 166.5 107.6 77.8 50 - 145 107.6 18.6 306.6
2-Chlorophenol 120.3 166.5 95.5 72.3 45 - 120 95.5 23 306.6
2-Methylnaphthalene 128.8 166.5 102.9 77.4 50 - 120 102.9 22.4 303.3
2-Methylphenol 113.3 166.5 90.68 68.1 45 - 120 90.68 22.2 306.6
2-Nitroaniline 134.9 166.5 105.8 81.0 45 - 138 105.8 24.2 306.6
2-Nitrophenol 126.5 166.5 100.8 76.0 45 - 125 100.8 22.6 306.6
3&4-Methylphenol 114.5 166.5 90.1 68.8 45 - 120 90.1 23.9 306.6
3,3´-Dichlorobenzidine 111.5 166.5 85.14 67.0 15 - 120 85.14 26.8 306.6
3-Nitroaniline 107.4 166.5 86.85 64.5 40 - 120 86.85 21.1 306.6
4,6-Dinitro-2-methylphenol 67.75 166.5 63.68 40.7 15 - 135 63.68 6.2 306.6
4-Bromophenyl phenyl ether 137 166.5 110.6 82.3 50 - 125 110.6 21.4 306.6
4-Chloro-3-methylphenol 130.1 166.5 102.3 78.1 45 - 130 102.3 23.9 306.6
4-Chloroaniline 110.1 166.5 86.3 66.1 20 - 120 86.3 24.2 306.6
4-Chlorophenyl phenyl ether 142.8 166.5 111.5 85.7 50 - 120 111.5 24.6 306.6
4-Nitroaniline 103.1 166.5 80.25 61.9 50 - 127 80.25 24.9 306.6
4-Nitrophenol 109.8 166.5 95.63 66.0 40 - 147 95.63 13.8 3013
Acenaphthene 117.8 166.5 92.05 70.7 50 - 120 92.05 24.5 303.3
Acenaphthylene 129.3 166.5 101.3 77.7 50 - 120 101.3 24.2 303.3
Acetophenone 108.8 166.5 86.88 65.3 50 - 120 86.88 22.4 306.6
Anthracene 129.1 166.5 100.2 77.6 50 - 123 100.2 25.2 303.3
Atrazine 142.1 166.5 116.8 85.4 29 - 148 116.8 19.6 306.6
Benz(a)anthracene 132.8 166.5 107.9 79.8 50 - 131 107.9 20.7 303.3
Benzaldehyde 62.94 166.5 64.89 36.4 22 - 129 64.89 3.06 306.6
Benzo(a)pyrene 124.1 166.5 100.2 74.5 50 - 130 100.2 21.4 303.3
Benzo(b)fluoranthene 140.5 166.5 119.3 84.4 50 - 137 119.3 16.3 303.3
Benzo(g,h,i)perylene 143.5 166.5 114.7 86.2 50 - 130 114.7 22.3 303.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:HS14070861-21MSD Units:ug/Kg Analysis Date:23-Jul-2014 18:53
Run ID:SV-4_238295 SeqNo:2945432 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Benzo(k)fluoranthene 114.9 166.5 89.59 69.0 50 - 143 89.59 24.7 303.3
Bis(2-chloroethoxy)methane 110.8 166.5 90.12 66.6 50 - 120 90.12 20.6 306.6
Bis(2-chloroethyl)ether 112.7 166.5 93.11 67.7 45 - 127 93.11 19 306.6
Bis(2-chloroisopropyl)ether 119.7 166.5 97.34 71.9 50 - 120 97.34 20.6 306.6
Bis(2-ethylhexyl)phthalate 129.1 166.5 100.7 74.3 21 - 148 100.7 24.7 306.6
Butyl benzyl phthalate 117.5 166.5 94.39 70.6 50 - 136 94.39 21.8 306.6
Caprolactam 71.08 166.5 72.56 42.7 50 - 135 72.56 2.05 30 S 6.6
Carbazole 124.7 166.5 101.9 74.9 50 - 143 101.9 20.1 306.6
Chrysene 134 166.5 109.1 80.5 50 - 130 109.1 20.5 303.3
Dibenz(a,h)anthracene 146 166.5 118.1 87.7 50 - 130 118.1 21.1 303.3
Dibenzofuran 130.5 166.5 101.1 78.4 50 - 125 101.1 25.4 303.3
Diethyl phthalate 126.9 166.5 96.03 76.2 50 - 125 96.03 27.7 306.6
Dimethyl phthalate 130.8 166.5 102.5 78.5 50 - 125 102.5 24.2 306.6
Di-n-butyl phthalate 123.9 166.5 100.6 71.7 50 - 140 100.6 20.8 306.6
Di-n-octyl phthalate 115.4 166.5 92.88 69.3 50 - 140 92.88 21.7 306.6
Fluoranthene 134.2 166.5 111 80.6 50 - 131 111 18.8 303.3
Fluorene 134.7 166.5 108.3 80.9 50 - 125 108.3 21.7 303.3
Hexachlorobenzene 147.2 166.5 119.4 88.4 50 - 124 119.4 20.9 306.6
Hexachlorobutadiene 152.7 166.5 116 91.7 50 - 125 116 27.3 306.6
Hexachlorocyclopentadiene 110 166.5 92.22 66.1 45 - 135 92.22 17.6 306.6
Hexachloroethane 110 166.5 88.71 66.1 45 - 125 88.71 21.4 306.6
Indeno(1,2,3-cd)pyrene 149.5 166.5 125.7 89.8 45 - 139 125.7 17.3 303.3
Isophorone 113.7 166.5 91.23 68.3 45 - 130 91.23 21.9 306.6
Naphthalene 132.4 166.5 104.6 79.5 50 - 125 104.6 23.5 303.3
Nitrobenzene 107.9 166.5 88.42 64.8 50 - 125 88.42 19.8 306.6
N-Nitrosodi-n-propylamine 109.1 166.5 88.59 65.5 45 - 120 88.59 20.8 306.6
N-Nitrosodiphenylamine 118.5 166.5 98.04 71.2 50 - 130 98.04 18.9 306.6
Pentachlorophenol 75.58 166.5 69.44 45.4 23 - 136 69.44 8.46 306.6
Phenanthrene 127.3 166.5 110.2 76.4 50 - 125 110.2 14.4 303.3
Phenol 110.5 166.5 90.47 66.4 45 - 130 90.47 19.9 306.6
Pyrene 123.9 166.5 100.7 74.4 45 - 130 100.7 20.7 303.3
151.8 166.5 118.8 91.2 36 - 126 118.8 24.4 306.6Surr: 2,4,6-Tribromophenol
128.4 166.5 100.5 77.1 43 - 125 100.5 24.3 306.6Surr: 2-Fluorobiphenyl
97.28 166.5 75.71 58.4 37 - 125 75.71 24.9 306.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84405a Instrument: SV-4 Method: SW8270
Sample ID:HS14070861-21MSD Units:ug/Kg Analysis Date:23-Jul-2014 18:53
Run ID:SV-4_238295 SeqNo:2945432 PrepDate:23-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
133.8 166.5 110.1 80.4 32 - 125 110.1 19.5 306.6Surr: 4-Terphenyl-d14
108.8 166.5 85.72 65.3 37 - 125 85.72 23.7 306.6Surr: Nitrobenzene-d5
104 166.5 85.58 62.5 40 - 125 85.58 19.4 306.6Surr: Phenol-d6
The following samples were anayzed in this batch:HS14070721-26
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:MBLK-84441 Units:ug/Kg Analysis Date:24-Jul-2014 14:18
Run ID:SV-4_238412 SeqNo:2948325 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,1´-Biphenyl U 6.6
2,4,5-Trichlorophenol U 6.6
2,4,6-Trichlorophenol U 6.6
2,4-Dichlorophenol U 6.6
2,4-Dimethylphenol U 6.6
2,4-Dinitrophenol U 13
2,4-Dinitrotoluene U 6.6
2,6-Dinitrotoluene U 6.6
2-Chloronaphthalene U 6.6
2-Chlorophenol U 6.6
2-Methylnaphthalene U 3.3
2-Methylphenol U 6.6
2-Nitroaniline U 6.6
2-Nitrophenol U 6.6
3&4-Methylphenol U 6.6
3,3´-Dichlorobenzidine U 6.6
3-Nitroaniline U 6.6
4,6-Dinitro-2-methylphenol U 6.6
4-Bromophenyl phenyl ether U 6.6
4-Chloro-3-methylphenol U 6.6
4-Chloroaniline U 6.6
4-Chlorophenyl phenyl ether U 6.6
4-Nitroaniline U 6.6
4-Nitrophenol U 13
Acenaphthene U 3.3
Acenaphthylene U 3.3
Acetophenone U 6.6
Anthracene U 3.3
Atrazine U 6.6
Benz(a)anthracene U 3.3
Benzaldehyde U 6.6
Benzo(a)pyrene U 3.3
Benzo(b)fluoranthene U 3.3
Benzo(g,h,i)perylene U 3.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:MBLK-84441 Units:ug/Kg Analysis Date:24-Jul-2014 14:18
Run ID:SV-4_238412 SeqNo:2948325 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Benzo(k)fluoranthene U 3.3
Bis(2-chloroethoxy)methane U 6.6
Bis(2-chloroethyl)ether U 6.6
Bis(2-chloroisopropyl)ether U 6.6
Bis(2-ethylhexyl)phthalate U 6.6
Butyl benzyl phthalate U 6.6
Caprolactam U 6.6
Carbazole U 6.6
Chrysene U 3.3
Dibenz(a,h)anthracene U 3.3
Dibenzofuran U 3.3
Diethyl phthalate U 6.6
Dimethyl phthalate U 6.6
Di-n-butyl phthalate U 6.6
Di-n-octyl phthalate U 6.6
Fluoranthene U 3.3
Fluorene U 3.3
Hexachlorobenzene U 6.6
Hexachlorobutadiene U 6.6
Hexachlorocyclopentadiene U 6.6
Hexachloroethane U 6.6
Indeno(1,2,3-cd)pyrene U 3.3
Isophorone U 6.6
Naphthalene U 3.3
Nitrobenzene U 6.6
N-Nitrosodi-n-propylamine U 6.6
N-Nitrosodiphenylamine U 6.6
Pentachlorophenol U 6.6
Phenanthrene U 3.3
Phenol U 6.6
Pyrene U 3.3
113.4 167 0 67.9 36 - 1266.6Surr: 2,4,6-Tribromophenol
133 167 0 79.6 43 - 1256.6Surr: 2-Fluorobiphenyl
137.2 167 0 82.2 37 - 1256.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:MBLK-84441 Units:ug/Kg Analysis Date:24-Jul-2014 14:18
Run ID:SV-4_238412 SeqNo:2948325 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
137.5 167 0 82.3 32 - 1256.6Surr: 4-Terphenyl-d14
143.5 167 0 85.9 37 - 1256.6Surr: Nitrobenzene-d5
123.4 167 0 73.9 40 - 1256.6Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:LCS-84441 Units:ug/Kg Analysis Date:24-Jul-2014 14:38
Run ID:SV-4_238412 SeqNo:2948326 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,1´-Biphenyl 124.4 167 0 74.5 50 - 1206.6
2,4,5-Trichlorophenol 158.1 167 0 94.7 45 - 1276.6
2,4,6-Trichlorophenol 156.8 167 0 93.9 45 - 1306.6
2,4-Dichlorophenol 140.2 167 0 83.9 45 - 1256.6
2,4-Dimethylphenol 125.6 167 0 75.2 45 - 1206.6
2,4-Dinitrophenol 136 167 0 81.4 10 - 12613
2,4-Dinitrotoluene 158.2 167 0 94.7 50 - 1306.6
2,6-Dinitrotoluene 155.2 167 0 92.9 50 - 1256.6
2-Chloronaphthalene 130.2 167 0 77.9 50 - 1456.6
2-Chlorophenol 126.7 167 0 75.8 45 - 1206.6
2-Methylnaphthalene 128.1 167 0 76.7 50 - 1203.3
2-Methylphenol 141.6 167 0 84.8 45 - 1206.6
2-Nitroaniline 196.9 167 0 118 45 - 1386.6
2-Nitrophenol 133.1 167 0 79.7 45 - 1256.6
3&4-Methylphenol 135.8 167 0 81.3 45 - 1206.6
3,3´-Dichlorobenzidine 116.2 167 0 69.6 15 - 1206.6
3-Nitroaniline 149.3 167 0 89.4 40 - 1206.6
4,6-Dinitro-2-methylphenol 145.2 167 0 87.0 15 - 1356.6
4-Bromophenyl phenyl ether 144.5 167 0 86.5 50 - 1256.6
4-Chloro-3-methylphenol 157.5 167 0 94.3 45 - 1306.6
4-Chloroaniline 136 167 0 81.5 20 - 1206.6
4-Chlorophenyl phenyl ether 154.8 167 0 92.7 50 - 1206.6
4-Nitroaniline 143.5 167 0 85.9 50 - 1276.6
4-Nitrophenol 197.1 167 0 118 40 - 14713
Acenaphthene 119.9 167 0 71.8 50 - 1203.3
Acenaphthylene 131.5 167 0 78.8 50 - 1203.3
Acetophenone 124.8 167 0 74.7 50 - 1206.6
Anthracene 141.4 167 0 84.7 50 - 1233.3
Atrazine 157.6 167 0 94.4 29 - 1486.6
Benz(a)anthracene 140.2 167 0 84.0 50 - 1313.3
Benzaldehyde 38.29 167 0 22.9 22 - 1296.6
Benzo(a)pyrene 138.5 167 0 82.9 50 - 1303.3
Benzo(b)fluoranthene 145.5 167 0 87.1 50 - 1373.3
Benzo(g,h,i)perylene 143 167 0 85.6 50 - 1303.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:LCS-84441 Units:ug/Kg Analysis Date:24-Jul-2014 14:38
Run ID:SV-4_238412 SeqNo:2948326 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Benzo(k)fluoranthene 140 167 0 83.8 50 - 1433.3
Bis(2-chloroethoxy)methane 133 167 0 79.6 50 - 1206.6
Bis(2-chloroethyl)ether 129.4 167 0 77.5 45 - 1276.6
Bis(2-chloroisopropyl)ether 128.1 167 0 76.7 50 - 1206.6
Bis(2-ethylhexyl)phthalate 130.5 167 0 78.2 21 - 1486.6
Butyl benzyl phthalate 124.5 167 0 74.6 50 - 1366.6
Caprolactam 139.2 167 0 83.4 50 - 1356.6
Carbazole 142.7 167 0 85.4 50 - 1436.6
Chrysene 140.8 167 0 84.3 50 - 1303.3
Dibenz(a,h)anthracene 140.8 167 0 84.3 50 - 1303.3
Dibenzofuran 137 167 0 82.0 50 - 1253.3
Diethyl phthalate 135.8 167 0 81.3 50 - 1256.6
Dimethyl phthalate 146.2 167 0 87.6 50 - 1256.6
Di-n-butyl phthalate 138.7 167 0 83.0 50 - 1406.6
Di-n-octyl phthalate 129.9 167 0 77.8 50 - 1406.6
Fluoranthene 149.4 167 0 89.5 50 - 1313.3
Fluorene 142.9 167 0 85.6 50 - 1253.3
Hexachlorobenzene 145.7 167 0 87.3 50 - 1246.6
Hexachlorobutadiene 170.9 167 0 102 50 - 1256.6
Hexachlorocyclopentadiene 157.4 167 0 94.2 45 - 1356.6
Hexachloroethane 131 167 0 78.5 45 - 1256.6
Indeno(1,2,3-cd)pyrene 162.2 167 0 97.1 45 - 1393.3
Isophorone 152.4 167 0 91.3 45 - 1306.6
Naphthalene 135.1 167 0 80.9 50 - 1253.3
Nitrobenzene 143.8 167 0 86.1 50 - 1256.6
N-Nitrosodi-n-propylamine 151 167 0 90.4 45 - 1206.6
N-Nitrosodiphenylamine 128.8 167 0 77.1 50 - 1306.6
Pentachlorophenol 146.6 167 0 87.8 23 - 1366.6
Phenanthrene 145.2 167 0 86.9 50 - 1253.3
Phenol 141.7 167 0 84.9 45 - 1306.6
Pyrene 133.8 167 0 80.1 45 - 1303.3
152.7 167 0 91.4 36 - 1266.6Surr: 2,4,6-Tribromophenol
133.7 167 0 80.0 43 - 1256.6Surr: 2-Fluorobiphenyl
126.2 167 0 75.6 37 - 1256.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:LCS-84441 Units:ug/Kg Analysis Date:24-Jul-2014 14:38
Run ID:SV-4_238412 SeqNo:2948326 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
136.3 167 0 81.6 32 - 1256.6Surr: 4-Terphenyl-d14
149.6 167 0 89.6 37 - 1256.6Surr: Nitrobenzene-d5
130.5 167 0 78.1 40 - 1256.6Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:HS14070721-07MS Units:ug/Kg Analysis Date:24-Jul-2014 15:18
Run ID:SV-4_238412 SeqNo:2948328 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:B-18A (1-2)
1,1´-Biphenyl 128.6 166.9 0 77.0 50 - 1206.6
2,4,5-Trichlorophenol 156.4 166.9 0 93.7 45 - 1276.6
2,4,6-Trichlorophenol 157.6 166.9 0 94.4 45 - 1306.6
2,4-Dichlorophenol 147.5 166.9 0 88.4 45 - 1256.6
2,4-Dimethylphenol 131.3 166.9 0 78.7 45 - 1206.6
2,4-Dinitrophenol 133 166.9 0 79.7 10 - 12613
2,4-Dinitrotoluene 154.2 166.9 0 92.4 50 - 1306.6
2,6-Dinitrotoluene 154.8 166.9 0 92.7 50 - 1256.6
2-Chloronaphthalene 138.1 166.9 0 82.8 50 - 1456.6
2-Chlorophenol 122.2 166.9 0 73.2 45 - 1206.6
2-Methylnaphthalene 134.4 166.9 0 80.5 50 - 1203.3
2-Methylphenol 140.2 166.9 0 84.0 45 - 1206.6
2-Nitroaniline 194.2 166.9 0 116 45 - 1386.6
2-Nitrophenol 133.5 166.9 0 80.0 45 - 1256.6
3&4-Methylphenol 130.9 166.9 0 78.4 45 - 1206.6
3,3´-Dichlorobenzidine 65.84 166.9 0 39.5 15 - 1206.6
3-Nitroaniline 127.6 166.9 0 76.4 40 - 1206.6
4,6-Dinitro-2-methylphenol 147.7 166.9 0 88.5 15 - 1356.6
4-Bromophenyl phenyl ether 136.7 166.9 0 81.9 50 - 1256.6
4-Chloro-3-methylphenol 157.5 166.9 0 94.4 45 - 1306.6
4-Chloroaniline 107.9 166.9 0 64.6 20 - 1206.6
4-Chlorophenyl phenyl ether 149.3 166.9 0 89.4 50 - 1206.6
4-Nitroaniline 140.4 166.9 0 84.1 50 - 1276.6
4-Nitrophenol 192 166.9 0 115 40 - 14713
Acenaphthene 118.6 166.9 0 71.0 50 - 1203.3
Acenaphthylene 132.6 166.9 0 79.5 50 - 1203.3
Acetophenone 128.3 166.9 0 76.9 50 - 1206.6
Anthracene 138.6 166.9 0 83.0 50 - 1233.3
Atrazine 157.9 166.9 0 94.6 29 - 1486.6
Benz(a)anthracene 142.3 166.9 0 85.3 50 - 1313.3
Benzaldehyde 43.71 166.9 0 26.2 22 - 1296.6
Benzo(a)pyrene 146.4 166.9 0 87.7 50 - 1303.3
Benzo(b)fluoranthene 159.5 166.9 0 95.6 50 - 1373.3
Benzo(g,h,i)perylene 151.1 166.9 0 90.5 50 - 1303.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:HS14070721-07MS Units:ug/Kg Analysis Date:24-Jul-2014 15:18
Run ID:SV-4_238412 SeqNo:2948328 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:B-18A (1-2)
Benzo(k)fluoranthene 141.1 166.9 0 84.5 50 - 1433.3
Bis(2-chloroethoxy)methane 134.4 166.9 0 80.5 50 - 1206.6
Bis(2-chloroethyl)ether 128.6 166.9 0 77.1 45 - 1276.6
Bis(2-chloroisopropyl)ether 124.3 166.9 0 74.5 50 - 1206.6
Bis(2-ethylhexyl)phthalate 133.2 166.9 1.86 78.7 21 - 1486.6
Butyl benzyl phthalate 127.8 166.9 0 76.6 50 - 1366.6
Caprolactam 153.8 166.9 10.52 85.8 50 - 1356.6
Carbazole 154.2 166.9 0 92.4 50 - 1436.6
Chrysene 144 166.9 0 86.3 50 - 1303.3
Dibenz(a,h)anthracene 150.5 166.9 0 90.2 50 - 1303.3
Dibenzofuran 137.8 166.9 0 82.5 50 - 1253.3
Diethyl phthalate 132.4 166.9 0 79.3 50 - 1256.6
Dimethyl phthalate 141.1 166.9 0 84.6 50 - 1256.6
Di-n-butyl phthalate 142.9 166.9 0 85.6 50 - 1406.6
Di-n-octyl phthalate 140.7 166.9 0 84.3 50 - 1406.6
Fluoranthene 152.5 166.9 0 91.4 50 - 1313.3
Fluorene 140.1 166.9 0 83.9 50 - 1253.3
Hexachlorobenzene 141.1 166.9 0 84.5 50 - 1246.6
Hexachlorobutadiene 174.9 166.9 0 105 50 - 1256.6
Hexachlorocyclopentadiene 156.3 166.9 0 93.6 45 - 1356.6
Hexachloroethane 126 166.9 0 75.5 45 - 1256.6
Indeno(1,2,3-cd)pyrene 165.8 166.9 0 99.4 45 - 1393.3
Isophorone 152.3 166.9 0 91.2 45 - 1306.6
Naphthalene 140.5 166.9 0 84.2 50 - 1253.3
Nitrobenzene 150.2 166.9 0 90.0 50 - 1256.6
N-Nitrosodi-n-propylamine 146.3 166.9 0 87.7 45 - 1206.6
N-Nitrosodiphenylamine 126.2 166.9 0 75.6 50 - 1306.6
Pentachlorophenol 149.9 166.9 0 89.8 23 - 1366.6
Phenanthrene 143.5 166.9 0 86.0 50 - 1253.3
Phenol 136.4 166.9 0 81.7 45 - 1306.6
Pyrene 136.3 166.9 0 81.6 45 - 1303.3
154.9 166.9 0 92.8 36 - 1266.6Surr: 2,4,6-Tribromophenol
139.1 166.9 0 83.3 43 - 1256.6Surr: 2-Fluorobiphenyl
123.3 166.9 0 73.9 37 - 1256.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:HS14070721-07MS Units:ug/Kg Analysis Date:24-Jul-2014 15:18
Run ID:SV-4_238412 SeqNo:2948328 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:B-18A (1-2)
144.5 166.9 0 86.6 32 - 1256.6Surr: 4-Terphenyl-d14
153.2 166.9 0 91.8 37 - 1256.6Surr: Nitrobenzene-d5
130.3 166.9 0 78.1 40 - 1256.6Surr: Phenol-d6
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:HS14070721-07MSD Units:ug/Kg Analysis Date:24-Jul-2014 15:39
Run ID:SV-4_238412 SeqNo:2948329 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:B-18A (1-2)
1,1´-Biphenyl 122.6 166.8 128.6 73.5 50 - 120 128.6 4.79 306.6
2,4,5-Trichlorophenol 150.6 166.8 156.4 90.3 45 - 127 156.4 3.77 306.6
2,4,6-Trichlorophenol 152 166.8 157.6 91.1 45 - 130 157.6 3.57 306.6
2,4-Dichlorophenol 139.2 166.8 147.5 83.4 45 - 125 147.5 5.81 306.6
2,4-Dimethylphenol 123.2 166.8 131.3 73.9 45 - 120 131.3 6.31 306.6
2,4-Dinitrophenol 113.2 166.8 133 67.9 10 - 126 133 16 3013
2,4-Dinitrotoluene 149.5 166.8 154.2 89.6 50 - 130 154.2 3.1 306.6
2,6-Dinitrotoluene 145.3 166.8 154.8 87.1 50 - 125 154.8 6.35 306.6
2-Chloronaphthalene 135.6 166.8 138.1 81.3 50 - 145 138.1 1.8 306.6
2-Chlorophenol 124.9 166.8 122.2 74.8 45 - 120 122.2 2.14 306.6
2-Methylnaphthalene 125.5 166.8 134.4 75.2 50 - 120 134.4 6.82 303.3
2-Methylphenol 137.3 166.8 140.2 82.3 45 - 120 140.2 2.09 306.6
2-Nitroaniline 185.8 166.8 194.2 111 45 - 138 194.2 4.41 306.6
2-Nitrophenol 127.7 166.8 133.5 76.6 45 - 125 133.5 4.4 306.6
3&4-Methylphenol 132 166.8 130.9 79.1 45 - 120 130.9 0.84 306.6
3,3´-Dichlorobenzidine 104.2 166.8 65.84 62.4 15 - 120 65.84 45.1 30 R 6.6
3-Nitroaniline 141.6 166.8 127.6 84.9 40 - 120 127.6 10.5 306.6
4,6-Dinitro-2-methylphenol 135.2 166.8 147.7 81.0 15 - 135 147.7 8.86 306.6
4-Bromophenyl phenyl ether 133.5 166.8 136.7 80.0 50 - 125 136.7 2.4 306.6
4-Chloro-3-methylphenol 148.2 166.8 157.5 88.8 45 - 130 157.5 6.1 306.6
4-Chloroaniline 122.9 166.8 107.9 73.7 20 - 120 107.9 13 306.6
4-Chlorophenyl phenyl ether 146.5 166.8 149.3 87.8 50 - 120 149.3 1.84 306.6
4-Nitroaniline 136 166.8 140.4 81.5 50 - 127 140.4 3.21 306.6
4-Nitrophenol 176.1 166.8 192 106 40 - 147 192 8.65 3013
Acenaphthene 116.4 166.8 118.6 69.8 50 - 120 118.6 1.84 303.3
Acenaphthylene 126.9 166.8 132.6 76.1 50 - 120 132.6 4.4 303.3
Acetophenone 124.5 166.8 128.3 74.6 50 - 120 128.3 3.02 306.6
Anthracene 130.4 166.8 138.6 78.2 50 - 123 138.6 6.08 303.3
Atrazine 147.9 166.8 157.9 88.7 29 - 148 157.9 6.49 306.6
Benz(a)anthracene 130.4 166.8 142.3 78.1 50 - 131 142.3 8.76 303.3
Benzaldehyde 40.45 166.8 43.71 24.2 22 - 129 43.71 7.75 306.6
Benzo(a)pyrene 131 166.8 146.4 78.5 50 - 130 146.4 11.1 303.3
Benzo(b)fluoranthene 155.2 166.8 159.5 93.0 50 - 137 159.5 2.76 303.3
Benzo(g,h,i)perylene 133.5 166.8 151.1 80.0 50 - 130 151.1 12.3 303.3
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:HS14070721-07MSD Units:ug/Kg Analysis Date:24-Jul-2014 15:39
Run ID:SV-4_238412 SeqNo:2948329 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:B-18A (1-2)
Benzo(k)fluoranthene 118 166.8 141.1 70.8 50 - 143 141.1 17.8 303.3
Bis(2-chloroethoxy)methane 131.7 166.8 134.4 79.0 50 - 120 134.4 2.01 306.6
Bis(2-chloroethyl)ether 128 166.8 128.6 76.7 45 - 127 128.6 0.492 306.6
Bis(2-chloroisopropyl)ether 126.5 166.8 124.3 75.8 50 - 120 124.3 1.78 306.6
Bis(2-ethylhexyl)phthalate 126.3 166.8 133.2 74.6 21 - 148 133.2 5.34 306.6
Butyl benzyl phthalate 115.5 166.8 127.8 69.2 50 - 136 127.8 10.1 306.6
Caprolactam 145.5 166.8 153.8 80.9 50 - 135 153.8 5.53 306.6
Carbazole 142 166.8 154.2 85.1 50 - 143 154.2 8.25 306.6
Chrysene 135.6 166.8 144 81.3 50 - 130 144 6.05 303.3
Dibenz(a,h)anthracene 134.7 166.8 150.5 80.7 50 - 130 150.5 11.1 303.3
Dibenzofuran 131.8 166.8 137.8 79.0 50 - 125 137.8 4.46 303.3
Diethyl phthalate 128.2 166.8 132.4 76.8 50 - 125 132.4 3.23 306.6
Dimethyl phthalate 134.4 166.8 141.1 80.5 50 - 125 141.1 4.89 306.6
Di-n-butyl phthalate 128.3 166.8 142.9 76.9 50 - 140 142.9 10.7 306.6
Di-n-octyl phthalate 123.4 166.8 140.7 74.0 50 - 140 140.7 13.1 306.6
Fluoranthene 139.1 166.8 152.5 83.4 50 - 131 152.5 9.2 303.3
Fluorene 137.2 166.8 140.1 82.2 50 - 125 140.1 2.09 303.3
Hexachlorobenzene 139 166.8 141.1 83.3 50 - 124 141.1 1.44 306.6
Hexachlorobutadiene 163.9 166.8 174.9 98.2 50 - 125 174.9 6.5 306.6
Hexachlorocyclopentadiene 158 166.8 156.3 94.7 45 - 135 156.3 1.09 306.6
Hexachloroethane 129.6 166.8 126 77.7 45 - 125 126 2.85 306.6
Indeno(1,2,3-cd)pyrene 145.7 166.8 165.8 87.3 45 - 139 165.8 12.9 303.3
Isophorone 144 166.8 152.3 86.3 45 - 130 152.3 5.6 306.6
Naphthalene 132.1 166.8 140.5 79.2 50 - 125 140.5 6.22 303.3
Nitrobenzene 140.5 166.8 150.2 84.2 50 - 125 150.2 6.71 306.6
N-Nitrosodi-n-propylamine 148.3 166.8 146.3 88.9 45 - 120 146.3 1.3 306.6
N-Nitrosodiphenylamine 120.9 166.8 126.2 72.4 50 - 130 126.2 4.35 306.6
Pentachlorophenol 139.5 166.8 149.9 83.6 23 - 136 149.9 7.19 306.6
Phenanthrene 134.3 166.8 143.5 80.5 50 - 125 143.5 6.66 303.3
Phenol 138.6 166.8 136.4 83.1 45 - 130 136.4 1.6 306.6
Pyrene 126 166.8 136.3 75.5 45 - 130 136.3 7.82 303.3
152.8 166.8 154.9 91.6 36 - 126 154.9 1.32 306.6Surr: 2,4,6-Tribromophenol
132.4 166.8 139.1 79.4 43 - 125 139.1 4.92 306.6Surr: 2-Fluorobiphenyl
123.3 166.8 123.3 73.9 37 - 125 123.3 0.0216 306.6Surr: 2-Fluorophenol
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: 84441 Instrument: SV-4 Method: SW8270
Sample ID:HS14070721-07MSD Units:ug/Kg Analysis Date:24-Jul-2014 15:39
Run ID:SV-4_238412 SeqNo:2948329 PrepDate:24-Jul-2014 DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:B-18A (1-2)
132.2 166.8 144.5 79.2 32 - 125 144.5 8.94 306.6Surr: 4-Terphenyl-d14
149.5 166.8 153.2 89.6 37 - 125 153.2 2.42 306.6Surr: Nitrobenzene-d5
129.8 166.8 130.3 77.8 40 - 125 130.3 0.392 306.6Surr: Phenol-d6
The following samples were anayzed in this batch:HS14070721-07 HS14070721-08 HS14070721-09 HS14070721-10
HS14070721-11 HS14070721-12 HS14070721-13 HS14070721-14
HS14070721-15 HS14070721-19 HS14070721-20 HS14070721-23
HS14070721-24 HS14070721-25
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:VBLKS1-072214 Units:ug/Kg Analysis Date:22-Jul-2014 13:06
Run ID:VOA5_237862 SeqNo:2935033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,1,1-Trichloroethane U 5.0
1,1,2,2-Tetrachloroethane U 5.0
1,1,2-Trichlor-1,2,2-trifluoroethane U 5.0
1,1,2-Trichloroethane U 5.0
1,1-Dichloroethane U 5.0
1,1-Dichloroethene U 5.0
1,2,4-Trichlorobenzene U 5.0
1,2-Dibromo-3-chloropropane U 5.0
1,2-Dibromoethane U 5.0
1,2-Dichlorobenzene U 5.0
1,2-Dichloroethane U 5.0
1,2-Dichloropropane U 5.0
1,3-Dichlorobenzene U 5.0
1,4-Dichlorobenzene U 5.0
2-Butanone U 10
2-Hexanone U 10
4-Methyl-2-pentanone U 10
Acetone U 20
Benzene U 5.0
Bromodichloromethane U 5.0
Bromoform U 5.0
Bromomethane U 10
Carbon disulfide U 10
Carbon tetrachloride U 5.0
Chlorobenzene U 5.0
Chloroethane U 10
Chloroform U 5.0
Chloromethane U 10
cis-1,2-Dichloroethene U 5.0
cis-1,3-Dichloropropene U 5.0
Cyclohexane U 5.0
Dibromochloromethane U 5.0
Dichlorodifluoromethane U 5.0
Dichloromethane U 10
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:VBLKS1-072214 Units:ug/Kg Analysis Date:22-Jul-2014 13:06
Run ID:VOA5_237862 SeqNo:2935033 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ethylbenzene U 5.0
Isopropylbenzene U 5.0
m,p-Xylene U 10
Methyl acetate U 5.0
Methyl tert-butyl ether U 5.0
Methylcyclohexane U 5.0
o-Xylene U 5.0
Styrene U 5.0
Tetrachloroethene U 5.0
Toluene U 5.0
trans-1,2-Dichloroethene U 5.0
trans-1,3-Dichloropropene U 5.0
Trichloroethene U 5.0
Trichlorofluoromethane U 5.0
Vinyl chloride U 2.0
Xylenes, Total U 10
47.23 50 0 94.5 70 - 1285.0Surr: 1,2-Dichloroethane-d4
47.5 50 0 95.0 73 - 1265.0Surr: 4-Bromofluorobenzene
47.36 50 0 94.7 71 - 1285.0Surr: Dibromofluoromethane
50.31 50 0 101 73 - 1275.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:VLCSS1-072214 Units:ug/Kg Analysis Date:22-Jul-2014 12:19
Run ID:VOA5_237862 SeqNo:2935032 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,1,1-Trichloroethane 47.47 50 0 94.9 79 - 1245.0
1,1,2,2-Tetrachloroethane 45.03 50 0 90.1 75 - 1235.0
1,1,2-Trichlor-1,2,2-trifluoroethane 48.38 50 0 96.8 79 - 1255.0
1,1,2-Trichloroethane 45.66 50 0 91.3 79 - 1205.0
1,1-Dichloroethane 48.1 50 0 96.2 75 - 1245.0
1,1-Dichloroethene 47.99 50 0 96.0 80 - 1225.0
1,2,4-Trichlorobenzene 44.78 50 0 89.6 74 - 1285.0
1,2-Dibromo-3-chloropropane 44.64 50 0 89.3 66 - 1295.0
1,2-Dibromoethane 44.7 50 0 89.4 70 - 1205.0
1,2-Dichlorobenzene 45.12 50 0 90.2 75 - 1205.0
1,2-Dichloroethane 46.18 50 0 92.4 73 - 1215.0
1,2-Dichloropropane 46.06 50 0 92.1 76 - 1205.0
1,3-Dichlorobenzene 45.28 50 0 90.6 70 - 1255.0
1,4-Dichlorobenzene 45.46 50 0 90.9 77 - 1205.0
2-Butanone 89.12 100 0 89.1 65 - 13010
2-Hexanone 92.83 100 0 92.8 65 - 13310
4-Methyl-2-pentanone 91.19 100 0 91.2 69 - 13010
Acetone 103.3 100 0 103 53 - 14220
Benzene 46.38 50 0 92.8 79 - 1205.0
Bromodichloromethane 45.71 50 0 91.4 79 - 1215.0
Bromoform 44.04 50 0 88.1 74 - 1225.0
Bromomethane 49.86 50 0 99.7 68 - 13110
Carbon disulfide 95.97 100 0 96.0 80 - 12410
Carbon tetrachloride 46.71 50 0 93.4 74 - 1265.0
Chlorobenzene 45 50 0 90.0 79 - 1205.0
Chloroethane 45.79 50 0 91.6 76 - 12610
Chloroform 45.99 50 0 92.0 78 - 1205.0
Chloromethane 46.42 50 0 92.8 69 - 12910
cis-1,2-Dichloroethene 46 50 0 92.0 80 - 1205.0
cis-1,3-Dichloropropene 47.37 50 0 94.7 77 - 1235.0
Cyclohexane 49.07 50 0 98.1 74 - 1265.0
Dibromochloromethane 45.54 50 0 91.1 78 - 1225.0
Dichlorodifluoromethane 46.06 50 0 92.1 57 - 1405.0
Dichloromethane 46.87 50 0 93.7 62 - 13010
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:VLCSS1-072214 Units:ug/Kg Analysis Date:22-Jul-2014 12:19
Run ID:VOA5_237862 SeqNo:2935032 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ethylbenzene 46.28 50 0 92.6 80 - 1225.0
Isopropylbenzene 46.09 50 0 92.2 72 - 1275.0
m,p-Xylene 91.69 100 0 91.7 79 - 12210
Methyl acetate 45.17 50 0 90.3 69 - 1235.0
Methyl tert-butyl ether 49.05 50 0 98.1 76 - 1215.0
Methylcyclohexane 46.41 50 0 92.8 77 - 1265.0
o-Xylene 45.25 50 0 90.5 80 - 1235.0
Styrene 46.08 50 0 92.2 78 - 1245.0
Tetrachloroethene 50.8 50 0 102 73 - 1295.0
Toluene 45.63 50 0 91.3 79 - 1205.0
trans-1,2-Dichloroethene 47.21 50 0 94.4 79 - 1225.0
trans-1,3-Dichloropropene 47.81 50 0 95.6 77 - 1205.0
Trichloroethene 47.4 50 0 94.8 80 - 1215.0
Trichlorofluoromethane 48.91 50 0 97.8 75 - 1265.0
Vinyl chloride 49.83 50 0 99.7 76 - 1262.0
Xylenes, Total 136.9 150 0 91.3 80 - 12010
49.83 50 0 99.7 70 - 1285.0Surr: 1,2-Dichloroethane-d4
48.85 50 0 97.7 73 - 1265.0Surr: 4-Bromofluorobenzene
49.39 50 0 98.8 71 - 1285.0Surr: Dibromofluoromethane
49.49 50 0 99.0 73 - 1275.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:HS14070721-07MS Units:ug/Kg Analysis Date:22-Jul-2014 13:52
Run ID:VOA5_237862 SeqNo:2935035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:B-18A (1-2)
1,1,1-Trichloroethane 49.92 50 0 99.8 79 - 1245.0
1,1,2,2-Tetrachloroethane 47.73 50 0 95.5 75 - 1235.0
1,1,2-Trichlor-1,2,2-trifluoroethane 51.92 50 0 104 79 - 1255.0
1,1,2-Trichloroethane 47.02 50 0 94.0 79 - 1205.0
1,1-Dichloroethane 49.13 50 0 98.3 75 - 1245.0
1,1-Dichloroethene 50.29 50 0 101 80 - 1225.0
1,2,4-Trichlorobenzene 42.33 50 0 84.7 74 - 1285.0
1,2-Dibromo-3-chloropropane 43.16 50 0 86.3 66 - 1295.0
1,2-Dibromoethane 47.26 50 0 94.5 70 - 1205.0
1,2-Dichlorobenzene 45.62 50 0 91.2 75 - 1205.0
1,2-Dichloroethane 47.68 50 0 95.4 73 - 1215.0
1,2-Dichloropropane 47.23 50 0 94.5 76 - 1205.0
1,3-Dichlorobenzene 45.25 50 0 90.5 70 - 1255.0
1,4-Dichlorobenzene 45.47 50 0 90.9 77 - 1205.0
2-Butanone 86.94 100 0 86.9 65 - 13010
2-Hexanone 91.67 100 0 91.7 65 - 13310
4-Methyl-2-pentanone 94.88 100 0 94.9 69 - 13010
Acetone 89.8 100 0 89.8 53 - 14220
Benzene 48.12 50 0 96.2 79 - 1205.0
Bromodichloromethane 47.38 50 0 94.8 79 - 1215.0
Bromoform 45.76 50 0 91.5 74 - 1225.0
Bromomethane 52.23 50 0 104 68 - 13110
Carbon disulfide 99.16 100 0 99.2 80 - 12410
Carbon tetrachloride 48.23 50 0 96.5 74 - 1265.0
Chlorobenzene 46.94 50 0 93.9 79 - 1205.0
Chloroethane 49.09 50 0 98.2 76 - 12610
Chloroform 48.07 50 0 96.1 78 - 1205.0
Chloromethane 48.06 50 0 96.1 69 - 12910
cis-1,2-Dichloroethene 47.6 50 0 95.2 80 - 1205.0
cis-1,3-Dichloropropene 48.74 50 0 97.5 77 - 1235.0
Cyclohexane 50.7 50 0 101 74 - 1265.0
Dibromochloromethane 47.22 50 0 94.4 78 - 1225.0
Dichlorodifluoromethane 49.05 50 0 98.1 57 - 1405.0
Dichloromethane 57.18 50 0 114 62 - 13010
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:HS14070721-07MS Units:ug/Kg Analysis Date:22-Jul-2014 13:52
Run ID:VOA5_237862 SeqNo:2935035 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:B-18A (1-2)
Ethylbenzene 48.27 50 0 96.5 80 - 1225.0
Isopropylbenzene 47.58 50 0 95.2 72 - 1275.0
m,p-Xylene 95.76 100 0 95.8 79 - 12210
Methyl acetate 47.01 50 0 94.0 69 - 1235.0
Methyl tert-butyl ether 49.38 50 0 98.8 76 - 1215.0
Methylcyclohexane 47.07 50 0 94.1 77 - 1265.0
o-Xylene 47.49 50 0 95.0 80 - 1235.0
Styrene 47.67 50 0 95.3 78 - 1245.0
Tetrachloroethene 38.79 50 0 77.6 73 - 1295.0
Toluene 47.78 50 0 95.6 79 - 1205.0
trans-1,2-Dichloroethene 49.47 50 0 98.9 79 - 1225.0
trans-1,3-Dichloropropene 48.75 50 0 97.5 77 - 1205.0
Trichloroethene 47.67 50 0 95.3 80 - 1215.0
Trichlorofluoromethane 51.89 50 0 104 75 - 1265.0
Vinyl chloride 52.25 50 0 104 76 - 1262.0
Xylenes, Total 143.2 150 0 95.5 80 - 12010
49.38 50 0 98.8 70 - 1285.0Surr: 1,2-Dichloroethane-d4
49.09 50 0 98.2 73 - 1265.0Surr: 4-Bromofluorobenzene
49.3 50 0 98.6 71 - 1285.0Surr: Dibromofluoromethane
48.71 50 0 97.4 73 - 1275.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:HS14070721-07MSD Units:ug/Kg Analysis Date:22-Jul-2014 14:16
Run ID:VOA5_237862 SeqNo:2935036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:B-18A (1-2)
1,1,1-Trichloroethane 47.29 50 49.92 94.6 79 - 124 49.92 5.41 305.0
1,1,2,2-Tetrachloroethane 44.14 50 47.73 88.3 75 - 123 47.73 7.83 305.0
1,1,2-Trichlor-1,2,2-trifluoroethane 50.21 50 51.92 100 79 - 125 51.92 3.34 305.0
1,1,2-Trichloroethane 43.55 50 47.02 87.1 79 - 120 47.02 7.66 305.0
1,1-Dichloroethane 45.97 50 49.13 91.9 75 - 124 49.13 6.65 305.0
1,1-Dichloroethene 47.27 50 50.29 94.5 80 - 122 50.29 6.2 305.0
1,2,4-Trichlorobenzene 41.17 50 42.33 82.3 74 - 128 42.33 2.8 305.0
1,2-Dibromo-3-chloropropane 40.9 50 43.16 81.8 66 - 129 43.16 5.38 305.0
1,2-Dibromoethane 43.53 50 47.26 87.1 70 - 120 47.26 8.22 305.0
1,2-Dichlorobenzene 43.05 50 45.62 86.1 75 - 120 45.62 5.8 305.0
1,2-Dichloroethane 43.97 50 47.68 87.9 73 - 121 47.68 8.1 305.0
1,2-Dichloropropane 44.94 50 47.23 89.9 76 - 120 47.23 4.99 305.0
1,3-Dichlorobenzene 43.49 50 45.25 87.0 70 - 125 45.25 3.97 305.0
1,4-Dichlorobenzene 43.45 50 45.47 86.9 77 - 120 45.47 4.54 305.0
2-Butanone 79.02 100 86.94 79.0 65 - 130 86.94 9.54 3010
2-Hexanone 85.27 100 91.67 85.3 65 - 133 91.67 7.24 3010
4-Methyl-2-pentanone 86.79 100 94.88 86.8 69 - 130 94.88 8.91 3010
Acetone 84.43 100 89.8 84.4 53 - 142 89.8 6.16 3020
Benzene 45.65 50 48.12 91.3 79 - 120 48.12 5.26 305.0
Bromodichloromethane 44.65 50 47.38 89.3 79 - 121 47.38 5.92 305.0
Bromoform 42.4 50 45.76 84.8 74 - 122 45.76 7.63 305.0
Bromomethane 48.55 50 52.23 97.1 68 - 131 52.23 7.31 3010
Carbon disulfide 92.68 100 99.16 92.7 80 - 124 99.16 6.76 3010
Carbon tetrachloride 47.9 50 48.23 95.8 74 - 126 48.23 0.677 305.0
Chlorobenzene 44.96 50 46.94 89.9 79 - 120 46.94 4.31 305.0
Chloroethane 45.84 50 49.09 91.7 76 - 126 49.09 6.85 3010
Chloroform 45.07 50 48.07 90.1 78 - 120 48.07 6.45 305.0
Chloromethane 44.36 50 48.06 88.7 69 - 129 48.06 8 3010
cis-1,2-Dichloroethene 44.4 50 47.6 88.8 80 - 120 47.6 6.95 305.0
cis-1,3-Dichloropropene 45.86 50 48.74 91.7 77 - 123 48.74 6.1 305.0
Cyclohexane 49.64 50 50.7 99.3 74 - 126 50.7 2.12 305.0
Dibromochloromethane 44.41 50 47.22 88.8 78 - 122 47.22 6.13 305.0
Dichlorodifluoromethane 46.98 50 49.05 94.0 57 - 140 49.05 4.32 305.0
Dichloromethane 53.17 50 57.18 106 62 - 130 57.18 7.26 3010
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R237862 Instrument: VOA5 Method: SW8260
Sample ID:HS14070721-07MSD Units:ug/Kg Analysis Date:22-Jul-2014 14:16
Run ID:VOA5_237862 SeqNo:2935036 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:B-18A (1-2)
Ethylbenzene 46.45 50 48.27 92.9 80 - 122 48.27 3.85 305.0
Isopropylbenzene 46.59 50 47.58 93.2 72 - 127 47.58 2.1 305.0
m,p-Xylene 92.55 100 95.76 92.5 79 - 122 95.76 3.41 3010
Methyl acetate 45.01 50 47.01 90.0 69 - 123 47.01 4.33 305.0
Methyl tert-butyl ether 45.93 50 49.38 91.9 76 - 121 49.38 7.23 305.0
Methylcyclohexane 46.82 50 47.07 93.6 77 - 126 47.07 0.538 305.0
o-Xylene 46.04 50 47.49 92.1 80 - 123 47.49 3.12 305.0
Styrene 45.72 50 47.67 91.4 78 - 124 47.67 4.17 305.0
Tetrachloroethene 38.17 50 38.79 76.3 73 - 129 38.79 1.61 305.0
Toluene 46.06 50 47.78 92.1 79 - 120 47.78 3.67 305.0
trans-1,2-Dichloroethene 46.51 50 49.47 93.0 79 - 122 49.47 6.16 305.0
trans-1,3-Dichloropropene 45.45 50 48.75 90.9 77 - 120 48.75 7.01 305.0
Trichloroethene 45.06 50 47.67 90.1 80 - 121 47.67 5.64 305.0
Trichlorofluoromethane 48.99 50 51.89 98.0 75 - 126 51.89 5.75 305.0
Vinyl chloride 48.32 50 52.25 96.6 76 - 126 52.25 7.82 302.0
Xylenes, Total 138.6 150 143.2 92.4 79 - 123 143.2 3.31 3010
48.49 50 49.38 97.0 70 - 128 49.38 1.81 305.0Surr: 1,2-Dichloroethane-d4
48.32 50 49.09 96.6 73 - 126 49.09 1.59 305.0Surr: 4-Bromofluorobenzene
48.73 50 49.3 97.5 71 - 128 49.3 1.15 305.0Surr: Dibromofluoromethane
48.72 50 48.71 97.4 73 - 127 48.71 0.0236 305.0Surr: Toluene-d8
The following samples were anayzed in this batch:HS14070721-07 HS14070721-08 HS14070721-09 HS14070721-10
HS14070721-11
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:VBLKW-140725 Units:ug/L Analysis Date:25-Jul-2014 12:10
Run ID:VOA4_238123 SeqNo:2941900 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
1,1,1-Trichloroethane U 1.0
1,1,2,2-Tetrachloroethane U 1.0
1,1,2-Trichlor-1,2,2-trifluoroethane U 1.0
1,1,2-Trichloroethane U 1.0
1,1-Dichloroethane U 1.0
1,1-Dichloroethene U 1.0
1,2,4-Trichlorobenzene U 1.0
1,2-Dibromo-3-chloropropane U 1.0
1,2-Dibromoethane U 1.0
1,2-Dichlorobenzene U 1.0
1,2-Dichloroethane U 1.0
1,2-Dichloropropane U 1.0
1,3-Dichlorobenzene U 1.0
1,4-Dichlorobenzene U 1.0
2-Butanone U 2.0
2-Hexanone U 2.0
4-Methyl-2-pentanone U 2.0
Acetone U 2.0
Benzene U 1.0
Bromodichloromethane U 1.0
Bromoform U 1.0
Bromomethane U 1.0
Carbon disulfide U 2.0
Carbon tetrachloride U 1.0
Chlorobenzene U 1.0
Chloroethane U 1.0
Chloroform U 1.0
Chloromethane U 1.0
cis-1,2-Dichloroethene U 1.0
cis-1,3-Dichloropropene U 1.0
Cyclohexane U 1.0
Dibromochloromethane U 1.0
Dichlorodifluoromethane U 1.0
Dichloromethane U 2.0
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:VBLKW-140725 Units:ug/L Analysis Date:25-Jul-2014 12:10
Run ID:VOA4_238123 SeqNo:2941900 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MBLK
Client ID:
Ethylbenzene U 1.0
Isopropylbenzene U 1.0
m,p-Xylene U 2.0
Methyl acetate U 1.0
Methyl tert-butyl ether U 1.0
Methylcyclohexane U 1.0
o-Xylene U 1.0
Styrene U 1.0
Tetrachloroethene U 1.0
Toluene U 1.0
trans-1,2-Dichloroethene U 1.0
trans-1,3-Dichloropropene U 1.0
Trichloroethene U 1.0
Trichlorofluoromethane U 1.0
Vinyl chloride U 1.0
Xylenes, Total U 3.0
50.73 50 0 101 71 - 1251.0Surr: 1,2-Dichloroethane-d4
48.72 50 0 97.4 70 - 1251.0Surr: 4-Bromofluorobenzene
47.74 50 0 95.5 74 - 1251.0Surr: Dibromofluoromethane
49.97 50 0 99.9 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:VLCSW-140725 Units:ug/L Analysis Date:25-Jul-2014 11:20
Run ID:VOA4_238123 SeqNo:2941899 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
1,1,1-Trichloroethane 51.07 50 0 102 75 - 1301.0
1,1,2,2-Tetrachloroethane 50.91 50 0 102 74 - 1231.0
1,1,2-Trichlor-1,2,2-trifluoroethane 54.12 50 0 108 70 - 1301.0
1,1,2-Trichloroethane 50.89 50 0 102 80 - 1201.0
1,1-Dichloroethane 52.95 50 0 106 80 - 1201.0
1,1-Dichloroethene 51.75 50 0 103 75 - 1301.0
1,2,4-Trichlorobenzene 50.85 50 0 102 77 - 1201.0
1,2-Dibromo-3-chloropropane 48.4 50 0 96.8 68 - 1251.0
1,2-Dibromoethane 50.2 50 0 100 80 - 1201.0
1,2-Dichlorobenzene 50.99 50 0 102 80 - 1201.0
1,2-Dichloroethane 52.06 50 0 104 79 - 1201.0
1,2-Dichloropropane 51.8 50 0 104 80 - 1201.0
1,3-Dichlorobenzene 50.61 50 0 101 80 - 1201.0
1,4-Dichlorobenzene 50.63 50 0 101 80 - 1201.0
2-Butanone 105.3 100 0 105 60 - 1402.0
2-Hexanone 99.83 100 0 99.8 60 - 1312.0
4-Methyl-2-pentanone 97.42 100 0 97.4 60 - 1352.0
Acetone 111.7 100 0 112 60 - 1402.0
Benzene 50.5 50 0 101 80 - 1201.0
Bromodichloromethane 49.12 50 0 98.2 75 - 1201.0
Bromoform 45.84 50 0 91.7 70 - 1301.0
Bromomethane 44 50 0 88.0 63 - 1391.0
Carbon disulfide 93.98 100 0 94.0 75 - 1252.0
Carbon tetrachloride 49.94 50 0 99.9 75 - 1251.0
Chlorobenzene 50.51 50 0 101 80 - 1201.0
Chloroethane 53.25 50 0 107 70 - 1301.0
Chloroform 52.48 50 0 105 70 - 1301.0
Chloromethane 50.04 50 0 100 65 - 1301.0
cis-1,2-Dichloroethene 51.48 50 0 103 75 - 1251.0
cis-1,3-Dichloropropene 52.24 50 0 104 79 - 1251.0
Cyclohexane 54 50 0 108 75 - 1251.0
Dibromochloromethane 48.13 50 0 96.3 70 - 1301.0
Dichlorodifluoromethane 51.42 50 0 103 60 - 1401.0
Dichloromethane 51.32 50 0 103 65 - 1332.0
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:VLCSW-140725 Units:ug/L Analysis Date:25-Jul-2014 11:20
Run ID:VOA4_238123 SeqNo:2941899 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
LCS
Client ID:
Ethylbenzene 49.8 50 0 99.6 80 - 1201.0
Isopropylbenzene 49.56 50 0 99.1 80 - 1201.0
m,p-Xylene 99.52 100 0 99.5 80 - 1202.0
Methyl acetate 52.41 50 0 105 76 - 1221.0
Methyl tert-butyl ether 50.8 50 0 102 70 - 1251.0
Methylcyclohexane 51.63 50 0 103 70 - 1221.0
o-Xylene 49.89 50 0 99.8 80 - 1201.0
Styrene 50.07 50 0 100 78 - 1221.0
Tetrachloroethene 44.71 50 0 89.4 75 - 1301.0
Toluene 50.64 50 0 101 80 - 1211.0
trans-1,2-Dichloroethene 51.54 50 0 103 75 - 1251.0
trans-1,3-Dichloropropene 48.61 50 0 97.2 76 - 1251.0
Trichloroethene 49.63 50 0 99.3 75 - 1251.0
Trichlorofluoromethane 52.54 50 0 105 72 - 1321.0
Vinyl chloride 52.7 50 0 105 70 - 1351.0
Xylenes, Total 149.4 150 0 99.6 80 - 1243.0
49.34 50 0 98.7 71 - 1251.0Surr: 1,2-Dichloroethane-d4
48.97 50 0 97.9 70 - 1251.0Surr: 4-Bromofluorobenzene
49.3 50 0 98.6 74 - 1251.0Surr: Dibromofluoromethane
49.16 50 0 98.3 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:HS14070715-01MS Units:ug/L Analysis Date:25-Jul-2014 19:52
Run ID:VOA4_238123 SeqNo:2941918 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
1,1,1-Trichloroethane 51.78 50 0 104 75 - 1301.0
1,1,2,2-Tetrachloroethane 49.46 50 0 98.9 74 - 1231.0
1,1,2-Trichlor-1,2,2-trifluoroethane 54.77 50 0 110 70 - 1301.0
1,1,2-Trichloroethane 49.44 50 0 98.9 80 - 1201.0
1,1-Dichloroethane 52.11 50 0 104 80 - 1201.0
1,1-Dichloroethene 52.56 50 0 105 75 - 1301.0
1,2,4-Trichlorobenzene 41.7 50 0 83.4 77 - 1201.0
1,2-Dibromo-3-chloropropane 45.32 50 0 90.6 68 - 1251.0
1,2-Dibromoethane 48.86 50 0 97.7 80 - 1201.0
1,2-Dichlorobenzene 46.79 50 0 93.6 80 - 1201.0
1,2-Dichloroethane 51.53 50 0 103 79 - 1201.0
1,2-Dichloropropane 50.38 50 0 101 80 - 1201.0
1,3-Dichlorobenzene 46.28 50 0 92.6 80 - 1201.0
1,4-Dichlorobenzene 46.08 50 0 92.2 80 - 1201.0
2-Butanone 105.7 100 0 106 60 - 1402.0
2-Hexanone 99.97 100 0 100.
0 60 - 1312.0
4-Methyl-2-pentanone 99.61 100 0 99.6 60 - 1352.0
Acetone 116.7 100 0 117 60 - 1402.0
Benzene 50.79 50 0 102 80 - 1201.0
Bromodichloromethane 47.86 50 0 95.7 75 - 1201.0
Bromoform 44.55 50 0 89.1 70 - 1301.0
Bromomethane 35.28 50 0 70.6 63 - 1391.0
Carbon disulfide 96.51 100 0 96.5 75 - 1252.0
Carbon tetrachloride 50.66 50 0 101 79 - 1201.0
Chlorobenzene 48.8 50 0 97.6 80 - 1201.0
Chloroethane 55.55 50 0 111 70 - 1301.0
Chloroform 52.26 50 0 105 70 - 1301.0
Chloromethane 50 50 0 100 65 - 1301.0
cis-1,2-Dichloroethene 50.67 50 0 101 75 - 1251.0
cis-1,3-Dichloropropene 47.14 50 0 94.3 79 - 1251.0
Cyclohexane 53.07 50 0 106 75 - 1251.0
Dibromochloromethane 46.78 50 0 93.6 70 - 1301.0
Dichlorodifluoromethane 52.13 50 0 104 60 - 1401.0
Dichloromethane 50.79 50 0 102 65 - 1332.0
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:HS14070715-01MS Units:ug/L Analysis Date:25-Jul-2014 19:52
Run ID:VOA4_238123 SeqNo:2941918 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MS
Client ID:
Ethylbenzene 47.95 50 0 95.9 80 - 1201.0
Isopropylbenzene 47.72 50 0 95.4 80 - 1201.0
m,p-Xylene 96.47 100 0 96.5 80 - 1202.0
Methyl acetate 46.93 50 0 93.9 76 - 1221.0
Methyl tert-butyl ether 47.57 50 0 95.1 70 - 1251.0
Methylcyclohexane 47.34 50 0 94.7 70 - 1221.0
o-Xylene 48.14 50 0 96.3 80 - 1201.0
Styrene 47.16 50 0 94.3 78 - 1221.0
Tetrachloroethene 43.36 50 0 86.7 75 - 1301.0
Toluene 50.04 50 0 100 80 - 1211.0
trans-1,2-Dichloroethene 52.21 50 0 104 75 - 1251.0
trans-1,3-Dichloropropene 44.3 50 0 88.6 76 - 1251.0
Trichloroethene 49.38 50 0 98.8 75 - 1251.0
Trichlorofluoromethane 55.22 50 0 110 72 - 1321.0
Vinyl chloride 54.41 50 0 109 70 - 1351.0
Xylenes, Total 144.6 150 0 96.4 80 - 1243.0
50.6 50 0 101 71 - 1251.0Surr: 1,2-Dichloroethane-d4
49.23 50 0 98.5 70 - 1251.0Surr: 4-Bromofluorobenzene
50.18 50 0 100 74 - 1251.0Surr: Dibromofluoromethane
49.34 50 0 98.7 75 - 1251.0Surr: Toluene-d8
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:HS14070715-01MSD Units:ug/L Analysis Date:25-Jul-2014 20:18
Run ID:VOA4_238123 SeqNo:2941919 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
1,1,1-Trichloroethane 53.25 50 51.78 106 75 - 130 51.78 2.8 201.0
1,1,2,2-Tetrachloroethane 50.72 50 49.46 101 74 - 123 49.46 2.51 201.0
1,1,2-Trichlor-1,2,2-trifluoroethane 55.72 50 54.77 111 70 - 130 54.77 1.72 201.0
1,1,2-Trichloroethane 50.32 50 49.44 101 80 - 120 49.44 1.76 201.0
1,1-Dichloroethane 53.51 50 52.11 107 80 - 120 52.11 2.66 201.0
1,1-Dichloroethene 54.89 50 52.56 110 75 - 130 52.56 4.35 201.0
1,2,4-Trichlorobenzene 42.54 50 41.7 85.1 77 - 120 41.7 2 201.0
1,2-Dibromo-3-chloropropane 47.59 50 45.32 95.2 68 - 125 45.32 4.9 201.0
1,2-Dibromoethane 50.15 50 48.86 100 80 - 120 48.86 2.62 201.0
1,2-Dichlorobenzene 48.1 50 46.79 96.2 80 - 120 46.79 2.75 201.0
1,2-Dichloroethane 51.95 50 51.53 104 79 - 120 51.53 0.808 201.0
1,2-Dichloropropane 51.66 50 50.38 103 80 - 120 50.38 2.51 201.0
1,3-Dichlorobenzene 47.51 50 46.28 95.0 80 - 120 46.28 2.63 201.0
1,4-Dichlorobenzene 47.64 50 46.08 95.3 80 - 120 46.08 3.34 201.0
2-Butanone 106 100 105.7 106 60 - 140 105.7 0.201 202.0
2-Hexanone 100.5 100 99.97 100 60 - 131 99.97 0.496 202.0
4-Methyl-2-pentanone 101.3 100 99.61 101 60 - 135 99.61 1.65 202.0
Acetone 116.9 100 116.7 117 60 - 140 116.7 0.19 202.0
Benzene 51.48 50 50.79 103 80 - 120 50.79 1.35 201.0
Bromodichloromethane 49.17 50 47.86 98.3 75 - 120 47.86 2.69 201.0
Bromoform 46.33 50 44.55 92.7 70 - 130 44.55 3.92 201.0
Bromomethane 43.22 50 35.28 86.4 63 - 139 35.28 20.2 20 R 1.0
Carbon disulfide 99.12 100 96.51 99.1 75 - 125 96.51 2.66 202.0
Carbon tetrachloride 51.55 50 50.66 103 75 - 125 50.66 1.75 201.0
Chlorobenzene 49.54 50 48.8 99.1 80 - 120 48.8 1.5 201.0
Chloroethane 56.52 50 55.55 113 70 - 130 55.55 1.73 201.0
Chloroform 52.9 50 52.26 106 70 - 130 52.26 1.22 201.0
Chloromethane 51.33 50 50 103 65 - 130 50 2.62 201.0
cis-1,2-Dichloroethene 51.79 50 50.67 104 75 - 125 50.67 2.19 201.0
cis-1,3-Dichloropropene 49.39 50 47.14 98.8 79 - 125 47.14 4.67 201.0
Cyclohexane 54.49 50 53.07 109 75 - 125 53.07 2.65 201.0
Dibromochloromethane 47.51 50 46.78 95.0 70 - 130 46.78 1.54 201.0
Dichlorodifluoromethane 53.1 50 52.13 106 60 - 140 52.13 1.85 201.0
Dichloromethane 51.08 50 50.79 102 65 - 133 50.79 0.585 202.0
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238123 Instrument: VOA4 Method: SW8260
Sample ID:HS14070715-01MSD Units:ug/L Analysis Date:25-Jul-2014 20:18
Run ID:VOA4_238123 SeqNo:2941919 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
MSD
Client ID:
Ethylbenzene 49.46 50 47.95 98.9 80 - 120 47.95 3.1 201.0
Isopropylbenzene 48.2 50 47.72 96.4 80 - 120 47.72 1.01 201.0
m,p-Xylene 98.59 100 96.47 98.6 80 - 120 96.47 2.17 202.0
Methyl acetate 45.52 50 46.93 91.0 76 - 122 46.93 3.05 201.0
Methyl tert-butyl ether 50.05 50 47.57 100 70 - 125 47.57 5.09 201.0
Methylcyclohexane 47.14 50 47.34 94.3 70 - 122 47.34 0.43 201.0
o-Xylene 48.76 50 48.14 97.5 80 - 120 48.14 1.29 201.0
Styrene 47.68 50 47.16 95.4 78 - 122 47.16 1.09 201.0
Tetrachloroethene 44.05 50 43.36 88.1 75 - 130 43.36 1.56 201.0
Toluene 51.05 50 50.04 102 80 - 121 50.04 2 201.0
trans-1,2-Dichloroethene 52.96 50 52.21 106 75 - 125 52.21 1.42 201.0
trans-1,3-Dichloropropene 46.26 50 44.3 92.5 76 - 125 44.3 4.33 201.0
Trichloroethene 50.36 50 49.38 101 75 - 125 49.38 1.97 201.0
Trichlorofluoromethane 56.41 50 55.22 113 72 - 132 55.22 2.14 201.0
Vinyl chloride 55.98 50 54.41 112 70 - 135 54.41 2.84 201.0
Xylenes, Total 147.3 150 144.6 98.2 80 - 124 144.6 1.88 203.0
49.09 50 50.6 98.2 71 - 125 50.6 3.04 201.0Surr: 1,2-Dichloroethane-d4
48.83 50 49.23 97.7 70 - 125 49.23 0.813 201.0Surr: 4-Bromofluorobenzene
49.31 50 50.18 98.6 74 - 125 50.18 1.74 201.0Surr: Dibromofluoromethane
48.63 50 49.34 97.3 75 - 125 49.34 1.45 201.0Surr: Toluene-d8
The following samples were anayzed in this batch:HS14070721-02 HS14070721-04 HS14070721-05
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Client:
Project:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
WorkOrder: HS14070721 QC BATCH REPORT
Batch ID: R238044 Instrument: Balance1 Method: SW3550
Sample ID:HS14070721-26DUP Units:wt%Analysis Date:24-Jul-2014 14:50
Run ID:Balance1_238044 SeqNo:2940101 PrepDate:DF:1
Analyte SPK ValPQLResult
SPK Ref
Value %REC
Control
Limit
RPD Ref
Value %RPD
RPD
Limit Qual
DUP
Client ID:B-14B (4.5-5.5)
Percent Moisture 13.19 14.79 14.79 11.4 200.0100
The following samples were anayzed in this batch:HS14070721-07 HS14070721-08 HS14070721-09 HS14070721-10
HS14070721-11 HS14070721-12 HS14070721-13 HS14070721-14
HS14070721-15 HS14070721-19 HS14070721-20 HS14070721-21
HS14070721-22 HS14070721-23 HS14070721-24 HS14070721-25
HS14070721-26
ALS Group USA, Corp Date: 06-Aug-14
Note: See Qualifiers Page for a list of qualifiers and their explanation.
QUALIFIERS,
ACRONYMS, UNITS
Client:
Project:
WorkOrder:
Golder Associates, Inc.
Eaton Phase II Goldsboro NC 13384340
HS14070721
Qualifier Description
*Value exceeds Regulatory Limit
a Not accredited
B Analyte detected in the associated Method Blank above the Reporting Limit
E Value above quantitation range
H Analyzed outside of Holding Time
J Analyte detected below quantitation limit
M Manually integrated, see raw data for justification
n Not offered for accreditation
ND Not Detected at the Reporting Limit
O Sample amount is > 4 times amount spiked
P Dual Column results percent difference > 40%
R RPD above laboratory control limit
S Spike Recovery outside laboratory control limits
U Analyzed but not detected above the MDL/SDL
Acronym Description
DCS Detectability Check Study
DUP Method Duplicate
LCS Laboratory Control Sample
LCSD Laboratory Control Sample Duplicate
MBLK Method Blank
MDL Method Detection Limit
MQL Method Quantitation Limit
MS Matrix Spike
MSD Matrix Spike Duplicate
PDS Post Digestion Spike
PQL Practical Quantitaion Limit
SD Serial Dilution
SDL Sample Detection Limit
TRRP Texas Risk Reduction Program
Unit Reported Description
µg/Kg-dry Micrograms per Kilogram- Dry weight corrected
µg/L Micrograms per Liter
Date
mg/Kg-dry Milligrams per Kilogram- Dry weight corrected
mg/L Milligrams per Liter
wt%
ALS Group USA, Corp Date: 06-Aug-14
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Agency Number Expire Date
Arkansas AR - 2014 27-Mar-2015
Dept of Defense L2231 Rev 3-20-2014 22-Dec-2015
Illinois 003403 09-May-2015
Kentucky KY 2014-2015 30-Apr-2015
North Carolina 624 - 2014 31-Dec-2014
North Dakota R-193 2025 30-Apr-2015
Oklahoma 2013-024 31-Aug-2014
Texas TX104704231-14-13 30-Apr-2015
06-Aug-14Date: ALS Group USA, Corp
KMR
15-Jul-2014 17:00Date/Time Received:
HS14070721
Golder NC
Work Order:
Client Name:
Sample Receipt Checklist
Received by:
Shipping container/cooler in good condition?
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
Container/Temp Blank temperature in compliance?
Temperature(s)/Thermometer(s):
Cooler(s)/Kit(s):
Date/Time sample(s) sent to storage:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
pH adjusted?
pH adjusted by:
Login Notes:
No Not Present
Yes No Not Present
Yes No Not Present
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
Yes No
3.2c/3.2c 0.1c/0.1c C/U 1
4290 4215
Yes No No VOA vials submitted
Yes No N/A
Yes No N/A
Checklist completed by:Michael E. Schepcoff DateeSignatureDateeSignature
22-Jul-2014
FedExWater and Soil Carrier name:Matrices:
Reviewed by:Dane J. Wacasey
Client Contacted:Date Contacted:Person Contacted:
Contacted By:Regarding:
Comments:
Corrective Action:
0
Yes
ALS Group USA, Corp 06-Aug-14Date:
August 05, 2014 Service Request No:J1405454
Dane Wacasey
ALS Group USA, Corp.
10450 Stancliff Road
Suite 210
Houston, TX 77099-4338
All analyses were performed according to our laboratory’s quality assurance program. The test
results meet requirements of the NELAP standards except as noted in the case narrative report.
All results are intended to be considered in their entirety, and ALS Environmental is not responsible
for use of less than the complete report. Results apply only to the items
submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the
report. In accordance to the NELAC 2003 Standard, a statement on the estimated uncertainty of
measurement of any quantitative analysis will be supplied upon request.
For your reference, these analyses have been assigned our service request number
Enclosed are the results of the sample(s) submitted to our laboratory
Laboratory Results for: HS14070721
Dear Dane,
July 23, 2014
J1405454.
Please contact me if you have any questions. My extension is 4407. You may also contact me via
email at [e-mail].
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
Brian Weigel
dba ALS Environmental
ALS Group USA, Corp.
ADDRESS
FAXPHONE
9143 Philips Highway, Suite 200, Jacksonville, FL 32256
[phone]+1 904 739 2277 |
Page 1 of 17
CLIENT ID: MW-10 Lab ID: J1405454-001
Analyte Results Flag MDL PQL Units Method
Barium, Total Recoverable 88.0 0.5 2.0 ug/L 6020A
Chromium, Total Recoverable 0.8 J 0.2 1.0 ug/L 6020A
Lead, Total Recoverable 0.30 J 0.12 0.50 ug/L 6020A
CLIENT ID: MW-12 Lab ID: J1405454-002
Analyte Results Flag MDL PQL Units Method
Arsenic, Total Recoverable 2.2 0.5 1.0 ug/L 6020A
Barium, Total Recoverable 34.0 0.5 2.0 ug/L 6020A
Chromium, Total Recoverable 0.6 J 0.2 1.0 ug/L 6020A
Lead, Total Recoverable 0.19 J 0.12 0.50 ug/L 6020A
CLIENT ID: MW-12 DUP Lab ID: J1405454-003
Analyte Results Flag MDL PQL Units Method
Arsenic, Total Recoverable 1.6 0.5 1.0 ug/L 6020A
Barium, Total Recoverable 34.3 0.5 2.0 ug/L 6020A
Chromium, Total Recoverable 0.6 J 0.2 1.0 ug/L 6020A
Lead, Total Recoverable 0.19 J 0.12 0.50 ug/L 6020A
SAMPLE DETECTION SUMMARY
Page 2 of 17
CASE NARRATIVE
J1405454
Date Received:
Service Request:
Water
HS14070721
ALS Environmental - US
Sample Matrix:
Project:
Client:
7/23/14
NARRATIVE
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical
results for samples designated for Tier II data deliverables, including results of QC samples analyzed from this delivery group.
When appropriate to the procedure, method blank results have been reported with each analytical test. Analytical procedures
performed by the lab are validated in accordance with NELAC standards. Parameters that are included in the NELAC Fields of
Testing but are not included in the lab’s NELAC accreditation are identified in the discussion of each analytical procedure.
Sample Receipt
Three water samples  were received for analysis at ALS Environmental on 07/23/2014. The samples were received in good
condition and consistent with the accompanying chain of custody form. Samples are refrigerated at <6°C upon receipt at the lab
except for aqueous samples designated for metals analyses, which are stored at room temperature.
Metals Analyses:
No issues noted.
9143 Philips Highway, Suite 200, Jacksonville, FL 32256 | 904-739-2277 | www.alsglobal.com
Approved by Date 8/5/2014
Page 3 of 17
State Certifications, Accreditations, and Licenses
Agency Number Expire Date
Florida Department of Health E82502 6/30/2015
North Carolina Department of Environment and Natural Resources 527 12/31/2014
Virginia Environmental Accreditation Program 460191 12/14/2014
Louisiana Department of Environmental Quality 02086 6/30/2015
Georgia Department of Natural Resources 958 6/30/2015
Kentucky Division of Waste Management 63 6/30/2015
South Carolina Department of Health and Environmental Control 96021001 6/30/2015
Texas Commision on Environmental Quality T104704197-13-5 5/31/2015
Maine Department of Health and Human Services 2011006 2/3/2015
Department of Defense 66206 11/1/2014
Pennsylvania Department of Environmental Protection 68-04835 8/31/2014
9143 Philips Highway, Suite 200, Jacksonville, FL 32256 | 904-739-2277 | www.alsglobal.com
Page 4 of 17
+ Possible Tedlar bag artifact.
A TIC is a suspected aldol-condensation product
B Analyte found in the associated method blank as well as in the sample.
BC Reported results are not blank corrected.
BH The back section of the tube yielded higher results than the front.
BT Results indicated possible breakthrough; back section >=10% front section.
C Result identification confirmed.
D Compound identified in an analysis at a secondary dilution factor
D Spike was diluted out
DE Reported results are corrected for desorption efficiency.
E Estimated value. Concentration above calibration range
E The percent difference for the serial dilution was greater than 10%, indicating a possible
matrix interference in the sample.
H1 Sample analysis performed past holding time. See case narrative.
H2 Initial analysis within holding time. Reanalysis for the required dilution was past holding
time.
H3 Sample was received and analyzed past holding time.
H4 Sample was extracted past required extraction holding time, but analyzed within analysis
holding time. See case narrative.
I Internal standard not within the specified limits. See case narrative.
J Estimated Value. Concentration found below MRL.
K A deflection in the QC ion may indicate interference with the quantitation of this ion. The
concentration of this analyte should be considered as an estimate.
K Analyte was detected above the method reporting limit prior to normalization.
L1 Laboratory control sample recovery outside the specified limits; results may be biased
high.
L2 Laboratory control sample recovery outside the specified limits; results may be biased low.
L3 Laboratory control sample recovery outside the specified limits.
M Matrix interference; results may be biased high.
M The duplicate injection precision not met.
M1 Matrix interference due to coelution with a non-target compound; results may be biased
high.
N Presumptive evidence of a compound for TICs that have been identified based on a mass
spectral library search.
N The Matrix Spike sample recovery is not within control limits. See case narrative.
P Indicates chlorodiphenyl ether interference present at the retention time of the target
compound.
P Pesticide/Aroclor target analyte > 40% difference for detected concentrations between GC
columns
Q Indicates as estimated value because the P and P + 2 theoretical abundance ratio does not
meet method criteria.
R Duplicate Precision not met.
R1 Duplicate precision not within the specified limits; however, the results are below the
MRL and considered estimated.
S Surrogate recovery not within specified limits.
Data Qualifiers
Lab Standard
Page 5 of 17
S The reported value was determined by the Method of Standard Additions (MSA).
T Analyte is a tentatively identified compound, result is estimated.
U Compound was analyzed for, but was not detected (ND).
V1 The continuing calibration verification standard was outside (biased high) the specified
limits for this compound.
V2 The continuing calibration verification standard was outside (biased low) the specified
limits for this compound.
W Result quantified, but the corresponding peak was detected outside the generated retention
time window.
W The post-digestion spike for furnace AA analysis is out of control limits, while sample
absorbance is less than 50% of spike absorbance.
X See case narrative.
Y Recovery outside limits
Y The chromatogram resembles a petroleum product but does not match the calibration
standard.
Z The chromatogram does not resemble a petroleum product.
i The MRL/MDL has been elevated due to a matrix interference.
Data Qualifiers
Lab Standard
Page 6 of 17
ASTM American Society for Testing and Materials
A2LA American Association for Laboratory Accreditation
CARB California Air Resources Board
CAS Number Chemical Abstract Service registry Number
CFC Chlorofluorocarbon
CFU Colony-Forming Unit
DEC Department of Environmental Conservation
DEQ Department of Environmental Quality
DHS Department of Health Services
DOE Department of Ecology
DOH Department of Health
EPA U. S. Environmental Protection Agency
ELAP Environmental Laboratory Accreditation Program
GC Gas Chromatography
GC/MS Gas Chromatography/Mass Spectrometry
LUFT Leaking Underground Fuel Tank
M Modified
MCL Maximum Contaminant Level is the highest permissible concentration of a
substance allowed in drinking water as established by the USEPA.
MDL Method Detection Limit
MPN Most Probable Number
MRL Method Reporting Limit
NA Not Applicable
NC Not Calculated
NCASI National Council of the Paper Industry for Air and Stream Improvement
ND Not Detected
NIOSH National Institute for Occupational Safety and Health
PQL Practical Quantitation Limit
RCRA Resource Conservation and Recovery Act
SIM Selected Ion Monitoring
TPH Total Petroleum Hydrocarbons
tr Trace level is the concentration of an analyte that is less than the PQL but
greater than or equal to the MDL.
Acronyms
ALS Laboratory Group
Page 7 of 17
MW-10J1405454-001 7/15/2014 1600
MW-12J1405454-002 7/15/2014 1400
MW-12 DUPJ1405454-003 7/15/2014 0000
Client:ALS Environmental - US Service Request:J1405454
Project:HS14070721
SAMPLE CROSS-REFERENCE
SAMPLE #CLIENT SAMPLE ID DATE TIME
Printed 8/5/2014 11:47:10 PM Sample Summary
Page 8 of 17
Client:
07/23/14 15:43
J1405454
Date Received:
Date Collected:
Service Request:
Water
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 16:00
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name Q
Date
Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:MW-10
Lab Code:J1405454-001
Arsenic, Total Recoverable 07/31/14 21:57 07/25/1410.51.0 U0.56020A ug/L
Barium, Total Recoverable 07/31/14 21:57 07/25/1410.52.088.06020A ug/L
Cadmium, Total Recoverable 07/31/14 21:57 07/25/1410.100.40 U0.106020A ug/L
Chromium, Total Recoverable 07/31/14 21:57 07/25/1410.21.0 J0.86020A ug/L
Lead, Total Recoverable 07/31/14 21:57 07/25/1410.120.50 J0.306020A ug/L
Mercury, Total 07/31/14 15:08 07/30/1410.020.10 U0.027470A ug/L
Selenium, Total Recoverable 07/31/14 21:57 07/25/1411.12.0 U1.16020A ug/L
Silver, Total Recoverable 07/31/14 21:57 07/25/1410.060.50 U0.066020A ug/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 11:47:16 PM 14-0000298132 rev 00Superset Reference:Page 9 of 17
Client:
07/23/14 15:43
J1405454
Date Received:
Date Collected:
Service Request:
Water
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 14:00
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name Q
Date
Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:MW-12
Lab Code:J1405454-002
Arsenic, Total Recoverable 07/31/14 22:02 07/25/1410.51.02.26020A ug/L
Barium, Total Recoverable 07/31/14 22:02 07/25/1410.52.034.06020A ug/L
Cadmium, Total Recoverable 07/31/14 22:02 07/25/1410.100.40 U0.106020A ug/L
Chromium, Total Recoverable 07/31/14 22:02 07/25/1410.21.0 J0.66020A ug/L
Lead, Total Recoverable 07/31/14 22:02 07/25/1410.120.50 J0.196020A ug/L
Mercury, Total 07/31/14 15:09 07/30/1410.020.10 U0.027470A ug/L
Selenium, Total Recoverable 07/31/14 22:02 07/25/1411.12.0 U1.16020A ug/L
Silver, Total Recoverable 07/31/14 22:02 07/25/1410.060.50 U0.066020A ug/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 11:47:16 PM 14-0000298132 rev 00Superset Reference:Page 10 of 17
Client:
07/23/14 15:43
J1405454
Date Received:
Date Collected:
Service Request:
Water
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 00:00
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name Q
Date
Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:MW-12 DUP
Lab Code:J1405454-003
Arsenic, Total Recoverable 07/31/14 22:07 07/25/1410.51.01.66020A ug/L
Barium, Total Recoverable 07/31/14 22:07 07/25/1410.52.034.36020A ug/L
Cadmium, Total Recoverable 07/31/14 22:07 07/25/1410.100.40 U0.106020A ug/L
Chromium, Total Recoverable 07/31/14 22:07 07/25/1410.21.0 J0.66020A ug/L
Lead, Total Recoverable 07/31/14 22:07 07/25/1410.120.50 J0.196020A ug/L
Mercury, Total 07/31/14 15:13 07/30/1410.020.10 U0.027470A ug/L
Selenium, Total Recoverable 07/31/14 22:07 07/25/1411.12.0 U1.16020A ug/L
Silver, Total Recoverable 07/31/14 22:07 07/25/1410.060.50 U0.066020A ug/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 11:47:16 PM 14-0000298132 rev 00Superset Reference:Page 11 of 17
Client:
NA
J1405454
Date Received:
Date Collected:
Service Request:
Water
HS14070721
ALS Environmental - US
Sample Matrix:
Project:NA
Inorganic Parameters
Basis:NA
Analysis
MethodAnalyte Name Q
Date
Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:Method Blank
Lab Code:J1405454-MB
Arsenic, Total Recoverable 07/31/14 21:22 07/25/1410.51.0 U0.56020A ug/L
Barium, Total Recoverable 07/31/14 21:22 07/25/1410.52.0 U0.56020A ug/L
Cadmium, Total Recoverable 07/31/14 21:22 07/25/1410.100.40 U0.106020A ug/L
Chromium, Total Recoverable 07/31/14 21:22 07/25/1410.21.0 U0.26020A ug/L
Lead, Total Recoverable 07/31/14 21:22 07/25/1410.120.50 U0.126020A ug/L
Mercury, Total 07/31/14 14:32 07/30/1410.020.10 U0.027470A ug/L
Selenium, Total Recoverable 07/31/14 21:22 07/25/1411.12.0 U1.16020A ug/L
Silver, Total Recoverable 07/31/14 21:22 07/25/1410.060.50 U0.066020A ug/L
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 11:47:16 PM 14-0000298132 rev 00Superset Reference:Page 12 of 17
QA/QC Report
ug/L
J1405457-005 Basis:Lab Code:
Units:Sample Name:Batch QC
Inorganic Parameters
Duplicate Matrix Spike Summary
NA
Client:
Project:
Sample Matrix:
ALS Environmental - US
HS14070721
Water
Service Request:
Date Analyzed:
Date Received:
J1405454
07/31/14
N/A
Date Collected:N/A
EPA 3005A
6020A
Prep Method:
Analysis Method:
Analyte Name
RPD
LimitRPDResult
Sample
Result
Spike
Amount % Rec
Matrix Spike
J1405457-005MS J1405457-005DMS
Duplicate Matrix Spike
% Rec
Spike
AmountResult
% Rec
Limits
ALS Group USA, Corp.
dba ALS Environmental
07/25/14Date Extracted:
Arsenic, Total Recoverable 0.5 U 51.1 50.0 102 50.7 50.0 101 75-125 <1 20
Barium, Total Recoverable 0.5 U 105 100 105 102 100 102 75-125 3 20
Cadmium, Total Recoverable 0.10 U 21.6 20.0 108 20.9 20.0 105 75-125 3 20
Chromium, Total Recoverable 0.2 U 52.4 50.0 105 51.1 50.0 102 75-125 3 20
Lead, Total Recoverable 0.12 U 26.0 25.0 104 25.5 25.0 102 75-125 2 20
Selenium, Total Recoverable 1.1 U 102 100 102 100 100 100 75-125 1 20
Silver, Total Recoverable 0.06 U 26.6 25.0 106 26.1 25.0 104 75-125 2 20
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 8/5/2014 11:47:17 PM 14-0000298132 rev 00Superset Reference:Page 13 of 17
Analyte Name
J1405454
Date Analyzed:
Service Request:
Water
HS14070721
ALS Environmental - US
Sample Matrix:
Project:
Client:
Lab Control Sample Summary
Inorganic Parameters
NA
ug/L
Basis:
Units:
Lab Control Sample
J1405454-LCS
7/31/14
Spike AmountResult % Rec % Rec LimitsAnalytical Method
dba ALS Environmental
ALS Group USA, Corp.
QA/QC Report
Arsenic, Total Recoverable 80-120102 50.051.16020A
Barium, Total Recoverable 80-120104 1001046020A
Cadmium, Total Recoverable 80-120106 20.021.26020A
Chromium, Total Recoverable 80-120103 50.051.66020A
Lead, Total Recoverable 80-120103 25.025.86020A
Mercury, Total 80-12099 1.251.247470A
Selenium, Total Recoverable 80-120101 1001016020A
Silver, Total Recoverable 80-120106 25.026.56020A
14-0000298132 rev 00Superset Reference:Printed 8/5/2014 11:47:16 PM Page 14 of 17
Page 15 of 17
Page 16 of 17
Page 17 of 17
August 05, 2014 Service Request No:J1405489
Dane Wacasey
ALS Group USA, Corp.
10450 Stancliff Road
Suite 210
Houston, TX 77099-4338
All analyses were performed according to our laboratory’s quality assurance program. The test
results meet requirements of the NELAP standards except as noted in the case narrative report.
All results are intended to be considered in their entirety, and ALS Environmental is not responsible
for use of less than the complete report. Results apply only to the items
submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the
report. In accordance to the NELAC 2003 Standard, a statement on the estimated uncertainty of
measurement of any quantitative analysis will be supplied upon request.
For your reference, these analyses have been assigned our service request number
Enclosed are the results of the sample(s) submitted to our laboratory
Laboratory Results for: HS14070721
Dear Dane,
July 23, 2014
J1405489.
Please contact me if you have any questions. My extension is 4407. You may also contact me via
email at [e-mail].
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
Brian Weigel
dba ALS Environmental
ALS Group USA, Corp.
ADDRESS
FAXPHONE
9143 Philips Highway, Suite 200, Jacksonville, FL 32256
[phone]+1 904 739 2277 |
Page 1 of 48
CLIENT ID: B-18A (1-2)Lab ID: J1405489-001
Analyte Results Flag MDL PQL Units Method
Solids, Total 96 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 2.3 J 0.3 3.0 mg/Kg 6020A
CLIENT ID: B-18B (4.5-5.5)Lab ID: J1405489-002
Analyte Results Flag MDL PQL Units Method
Solids, Total 89 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 1.0 J 0.3 3.7 mg/Kg 6020A
CLIENT ID: B-18B (4.5-5.5) DUP Lab ID: J1405489-003
Analyte Results Flag MDL PQL Units Method
Solids, Total 96 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 1.2 J 0.3 4.1 mg/Kg 6020A
CLIENT ID: B-17A (1-2)Lab ID: J1405489-004
Analyte Results Flag MDL PQL Units Method
Solids, Total 79 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.5 J 0.3 2.3 mg/Kg 6020A
CLIENT ID: B-17B (4.5-5.5)Lab ID: J1405489-005
Analyte Results Flag MDL PQL Units Method
Solids, Total 96 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.7 J 0.3 3.3 mg/Kg 6020A
CLIENT ID: B-19A (1-2)Lab ID: J1405489-006
Analyte Results Flag MDL PQL Units Method
Solids, Total 96 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.7 J 0.3 3.6 mg/Kg 6020A
CLIENT ID: B-19B (4.5-5.5)Lab ID: J1405489-007
Analyte Results Flag MDL PQL Units Method
Solids, Total 95 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.7 J 0.3 4.2 mg/Kg 6020A
CLIENT ID: B-20A (1-2)Lab ID: J1405489-008
Analyte Results Flag MDL PQL Units Method
Solids, Total 97 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.5 J 0.3 4.8 mg/Kg 6020A
CLIENT ID: B-20B (4.5-5.5)Lab ID: J1405489-009
Analyte Results Flag MDL PQL Units Method
Solids, Total 94 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.8 J 0.3 4.8 mg/Kg 6020A
CLIENT ID: B-9A (3.5-4.0)Lab ID: J1405489-010
Analyte Results Flag MDL PQL Units Method
Solids, Total 83 0.10 0.10 Percent 160.3
SAMPLE DETECTION SUMMARY
Page 2 of 48
CLIENT ID: B-9A (3.5-4.0)Lab ID: J1405489-010
Analyte Results Flag MDL PQL Units Method
Arsenic, Total Recoverable 0.4 J 0.3 4.8 mg/Kg 6020A
CLIENT ID: B-10A (1-2)Lab ID: J1405489-011
Analyte Results Flag MDL PQL Units Method
Solids, Total 75 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.5 J 0.3 3.5 mg/Kg 6020A
CLIENT ID: B-10B (4-5)Lab ID: J1405489-012
Analyte Results Flag MDL PQL Units Method
Solids, Total 83 0.10 0.10 Percent 160.3
CLIENT ID: B-14A (1-2)Lab ID: J1405489-013
Analyte Results Flag MDL PQL Units Method
Solids, Total 87 0.10 0.10 Percent 160.3
Arsenic, Total Recoverable 0.5 J 0.4 5.7 mg/Kg 6020A
CLIENT ID: B-14B (4.5-5.5)Lab ID: J1405489-014
Analyte Results Flag MDL PQL Units Method
Solids, Total 85 0.10 0.10 Percent 160.3
CLIENT ID: B-15 (3-4)Lab ID: J1405489-015
Analyte Results Flag MDL PQL Units Method
Solids, Total 84 0.10 0.10 Percent 160.3
CLIENT ID: B-16 (3-4)Lab ID: J1405489-016
Analyte Results Flag MDL PQL Units Method
Solids, Total 87 0.10 0.10 Percent 160.3
SAMPLE DETECTION SUMMARY
Page 3 of 48
CASE NARRATIVE
J1405489
Date Received:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:
Client:
07/23/14 - 07/24/14
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical
results for samples designated for Tier II data deliverables, including results of QC samples analyzed from this delivery group.
When appropriate to the procedure, method blank results have been reported with each analytical test. Analytical procedures
performed by the lab are validated in accordance with NELAC standards. Parameters that are included in the NELAC Fields of
Testing but are not included in the lab’s NELAC accreditation are identified in the discussion of each analytical procedure.
Sample Receipt
Sixteen soil samples  were received for analysis at ALS Environmental on 07/23-07/24/14. The samples were received in good
condition and consistent with the accompanying chain of custody form. Samples are refrigerated at <6°C upon receipt at the lab
except for aqueous samples designated for metals analyses, which are stored at room temperature.
Metals Analyses:
No issues noted.
General Chemistry Analyses:
No issues noted.
9143 Philips Highway, Suite 200, Jacksonville, FL 32256 | 904-739-2277 | www.alsglobal.com
Approved by Date 8/5/2014
Page 4 of 48
State Certifications, Accreditations, and Licenses
Agency Number Expire Date
Florida Department of Health E82502 6/30/2015
North Carolina Department of Environment and Natural Resources 527 12/31/2014
Virginia Environmental Accreditation Program 460191 12/14/2014
Louisiana Department of Environmental Quality 02086 6/30/2015
Georgia Department of Natural Resources 958 6/30/2015
Kentucky Division of Waste Management 63 6/30/2015
South Carolina Department of Health and Environmental Control 96021001 6/30/2015
Texas Commision on Environmental Quality T104704197-13-5 5/31/2015
Maine Department of Health and Human Services 2011006 2/3/2015
Department of Defense 66206 11/1/2014
Pennsylvania Department of Environmental Protection 68-04835 8/31/2014
9143 Philips Highway, Suite 200, Jacksonville, FL 32256 | 904-739-2277 | www.alsglobal.com
Page 5 of 48
+ Possible Tedlar bag artifact.
A TIC is a suspected aldol-condensation product
B Analyte found in the associated method blank as well as in the sample.
BC Reported results are not blank corrected.
BH The back section of the tube yielded higher results than the front.
BT Results indicated possible breakthrough; back section >=10% front section.
C Result identification confirmed.
D Compound identified in an analysis at a secondary dilution factor
D Spike was diluted out
DE Reported results are corrected for desorption efficiency.
E Estimated value. Concentration above calibration range
E The percent difference for the serial dilution was greater than 10%, indicating a possible
matrix interference in the sample.
H1 Sample analysis performed past holding time. See case narrative.
H2 Initial analysis within holding time. Reanalysis for the required dilution was past holding
time.
H3 Sample was received and analyzed past holding time.
H4 Sample was extracted past required extraction holding time, but analyzed within analysis
holding time. See case narrative.
I Internal standard not within the specified limits. See case narrative.
J Estimated Value. Concentration found below MRL.
K A deflection in the QC ion may indicate interference with the quantitation of this ion. The
concentration of this analyte should be considered as an estimate.
K Analyte was detected above the method reporting limit prior to normalization.
L1 Laboratory control sample recovery outside the specified limits; results may be biased
high.
L2 Laboratory control sample recovery outside the specified limits; results may be biased low.
L3 Laboratory control sample recovery outside the specified limits.
M Matrix interference; results may be biased high.
M The duplicate injection precision not met.
M1 Matrix interference due to coelution with a non-target compound; results may be biased
high.
N Presumptive evidence of a compound for TICs that have been identified based on a mass
spectral library search.
N The Matrix Spike sample recovery is not within control limits. See case narrative.
P Indicates chlorodiphenyl ether interference present at the retention time of the target
compound.
P Pesticide/Aroclor target analyte > 40% difference for detected concentrations between GC
columns
Q Indicates as estimated value because the P and P + 2 theoretical abundance ratio does not
meet method criteria.
R Duplicate Precision not met.
R1 Duplicate precision not within the specified limits; however, the results are below the
MRL and considered estimated.
S Surrogate recovery not within specified limits.
Data Qualifiers
Lab Standard
Page 6 of 48
S The reported value was determined by the Method of Standard Additions (MSA).
T Analyte is a tentatively identified compound, result is estimated.
U Compound was analyzed for, but was not detected (ND).
V1 The continuing calibration verification standard was outside (biased high) the specified
limits for this compound.
V2 The continuing calibration verification standard was outside (biased low) the specified
limits for this compound.
W Result quantified, but the corresponding peak was detected outside the generated retention
time window.
W The post-digestion spike for furnace AA analysis is out of control limits, while sample
absorbance is less than 50% of spike absorbance.
X See case narrative.
Y Recovery outside limits
Y The chromatogram resembles a petroleum product but does not match the calibration
standard.
Z The chromatogram does not resemble a petroleum product.
i The MRL/MDL has been elevated due to a matrix interference.
Data Qualifiers
Lab Standard
Page 7 of 48
ASTM American Society for Testing and Materials
A2LA American Association for Laboratory Accreditation
CARB California Air Resources Board
CAS Number Chemical Abstract Service registry Number
CFC Chlorofluorocarbon
CFU Colony-Forming Unit
DEC Department of Environmental Conservation
DEQ Department of Environmental Quality
DHS Department of Health Services
DOE Department of Ecology
DOH Department of Health
EPA U. S. Environmental Protection Agency
ELAP Environmental Laboratory Accreditation Program
GC Gas Chromatography
GC/MS Gas Chromatography/Mass Spectrometry
LUFT Leaking Underground Fuel Tank
M Modified
MCL Maximum Contaminant Level is the highest permissible concentration of a
substance allowed in drinking water as established by the USEPA.
MDL Method Detection Limit
MPN Most Probable Number
MRL Method Reporting Limit
NA Not Applicable
NC Not Calculated
NCASI National Council of the Paper Industry for Air and Stream Improvement
ND Not Detected
NIOSH National Institute for Occupational Safety and Health
PQL Practical Quantitation Limit
RCRA Resource Conservation and Recovery Act
SIM Selected Ion Monitoring
TPH Total Petroleum Hydrocarbons
tr Trace level is the concentration of an analyte that is less than the PQL but
greater than or equal to the MDL.
Acronyms
ALS Laboratory Group
Page 8 of 48
B-18A (1-2)J1405489-001 7/14/2014 1350
B-18B (4.5-5.5)J1405489-002 7/14/2014 1410
B-18B (4.5-5.5) DUPJ1405489-003 7/14/2014 1410
B-17A (1-2)J1405489-004 7/14/2014 1745
B-17B (4.5-5.5)J1405489-005 7/14/2014 1755
B-19A (1-2)J1405489-006 7/14/2014 1653
B-19B (4.5-5.5)J1405489-007 7/14/2014 1706
B-20A (1-2)J1405489-008 7/14/2014 1530
B-20B (4.5-5.5)J1405489-009 7/14/2014 1550
B-9A (3.5-4.0)J1405489-010 7/15/2014 0835
B-10A (1-2)J1405489-011 7/15/2014 1000
B-10B (4-5)J1405489-012 7/15/2014 1005
B-14A (1-2)J1405489-013 7/14/2014 0905
B-14B (4.5-5.5)J1405489-014 7/14/2014 0910
B-15 (3-4)J1405489-015 7/14/2014 0855
B-16 (3-4)J1405489-016 7/14/2014 0830
Client:ALS Environmental - US Service Request:J1405489
Project:HS14070721
SAMPLE CROSS-REFERENCE
SAMPLE #CLIENT SAMPLE ID DATE TIME
Printed 8/5/2014 10:18:50 PM Sample Summary
Page 9 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 13:50
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-18A (1-2)
Lab Code:J1405489-001
Arsenic, Total Recoverable 07/31/14 00:17 07/30/14100.33.0 J2.36020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:56 PM 14-0000297392 rev 00Superset Reference:Page 10 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 13:50
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-18A (1-2)
Lab Code:J1405489-001
Solids, Total 07/25/14 10:3310.100.1096160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:00 PM 14-0000297392 rev 00Superset Reference:Page 11 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 14:10
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-18B (4.5-5.5)
Lab Code:J1405489-002
Arsenic, Total Recoverable 07/31/14 00:42 07/30/14100.33.7 J1.06020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 12 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 14:10
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-18B (4.5-5.5)
Lab Code:J1405489-002
Solids, Total 07/25/14 10:3310.100.1089160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:00 PM 14-0000297392 rev 00Superset Reference:Page 13 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 14:10
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-18B (4.5-5.5) DUP
Lab Code:J1405489-003
Arsenic, Total Recoverable 07/31/14 00:47 07/30/14100.34.1 J1.26020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 14 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 14:10
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-18B (4.5-5.5) DUP
Lab Code:J1405489-003
Solids, Total 07/25/14 10:3310.100.1096160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:00 PM 14-0000297392 rev 00Superset Reference:Page 15 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 17:45
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-17A (1-2)
Lab Code:J1405489-004
Arsenic, Total Recoverable 07/31/14 01:02 07/30/14100.32.3 J0.56020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 16 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 17:45
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-17A (1-2)
Lab Code:J1405489-004
Solids, Total 07/25/14 10:3310.100.1079160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 17 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 17:55
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-17B (4.5-5.5)
Lab Code:J1405489-005
Arsenic, Total Recoverable 07/31/14 01:07 07/30/14100.33.3 J0.76020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 18 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 17:55
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-17B (4.5-5.5)
Lab Code:J1405489-005
Solids, Total 07/25/14 10:3310.100.1096160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 19 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 16:53
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-19A (1-2)
Lab Code:J1405489-006
Arsenic, Total Recoverable 07/31/14 01:12 07/30/14100.33.6 J0.76020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 20 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 16:53
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-19A (1-2)
Lab Code:J1405489-006
Solids, Total 07/25/14 10:3310.100.1096160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 21 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 17:06
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-19B (4.5-5.5)
Lab Code:J1405489-007
Arsenic, Total Recoverable 07/31/14 01:17 07/30/14100.34.2 J0.76020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 22 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 17:06
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-19B (4.5-5.5)
Lab Code:J1405489-007
Solids, Total 07/25/14 10:3310.100.1095160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 23 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 15:30
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-20A (1-2)
Lab Code:J1405489-008
Arsenic, Total Recoverable 07/31/14 01:22 07/30/14100.34.8 J0.56020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 24 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 15:30
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-20A (1-2)
Lab Code:J1405489-008
Solids, Total 07/25/14 10:3310.100.1097160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 25 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 15:50
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-20B (4.5-5.5)
Lab Code:J1405489-009
Arsenic, Total Recoverable 07/31/14 01:27 07/30/14100.34.8 J0.86020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 26 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 15:50
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-20B (4.5-5.5)
Lab Code:J1405489-009
Solids, Total 07/25/14 10:3310.100.1094160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 27 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 08:35
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-9A (3.5-4.0)
Lab Code:J1405489-010
Arsenic, Total Recoverable 07/31/14 01:32 07/30/14100.34.8 J0.46020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 28 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 08:35
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-9A (3.5-4.0)
Lab Code:J1405489-010
Solids, Total 07/25/14 10:3310.100.1083160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 29 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 10:00
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-10A (1-2)
Lab Code:J1405489-011
Arsenic, Total Recoverable 07/31/14 01:37 07/30/14100.33.5 J0.56020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 30 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 10:00
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-10A (1-2)
Lab Code:J1405489-011
Solids, Total 07/25/14 10:3310.100.1075160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 31 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 10:05
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-10B (4-5)
Lab Code:J1405489-012
Arsenic, Total Recoverable 07/31/14 01:42 07/30/14100.33.7 U0.36020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:57 PM 14-0000297392 rev 00Superset Reference:Page 32 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/15/14 10:05
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-10B (4-5)
Lab Code:J1405489-012
Solids, Total 07/25/14 10:3310.100.1083160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 33 of 48
Client:
07/24/14 09:10
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 09:05
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-14A (1-2)
Lab Code:J1405489-013
Arsenic, Total Recoverable 07/31/14 01:47 07/30/14100.45.7 J0.56020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:58 PM 14-0000297392 rev 00Superset Reference:Page 34 of 48
Client:
07/24/14 09:10
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 09:05
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-14A (1-2)
Lab Code:J1405489-013
Solids, Total 07/25/14 10:3310.100.1087160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 35 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 09:10
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-14B (4.5-5.5)
Lab Code:J1405489-014
Arsenic, Total Recoverable 07/31/14 02:02 07/30/14100.33.6 U0.36020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:58 PM 14-0000297392 rev 00Superset Reference:Page 36 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 09:10
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-14B (4.5-5.5)
Lab Code:J1405489-014
Solids, Total 07/25/14 10:3310.100.1085160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 37 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 08:55
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-15 (3-4)
Lab Code:J1405489-015
Arsenic, Total Recoverable 07/31/14 02:08 07/30/14100.34.6 U0.36020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:58 PM 14-0000297392 rev 00Superset Reference:Page 38 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 08:55
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-15 (3-4)
Lab Code:J1405489-015
Solids, Total 07/25/14 10:3310.100.1084160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 39 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 08:30
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:B-16 (3-4)
Lab Code:J1405489-016
Arsenic, Total Recoverable 07/31/14 02:13 07/30/14100.34.4 U0.36020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:58 PM 14-0000297392 rev 00Superset Reference:Page 40 of 48
Client:
07/23/14 09:00
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:07/14/14 08:30
General Chemistry Parameters
Basis:As Received
Analysis MethodAnalyte Name QDate AnalyzedDil.MDLPQLResultUnits
Sample Name:B-16 (3-4)
Lab Code:J1405489-016
Solids, Total 07/25/14 10:3310.100.1087160.3 Modified Percent
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 41 of 48
Client:
NA
J1405489
Date Received:
Date Collected:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:NA
Inorganic Parameters
Basis:Dry
Analysis
MethodAnalyte Name QDate Analyzed
Date
ExtractedDil.MDLPQLResultUnits
Sample Name:Method Blank
Lab Code:J1405489-MB
Arsenic, Total Recoverable 07/31/14 00:07 07/30/14100.35.0 U0.36020A mg/Kg
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 8/5/2014 10:18:58 PM 14-0000297392 rev 00Superset Reference:Page 42 of 48
QA/QC Report
mg/Kg
J1405489-001 Basis:Lab Code:
Units:Sample Name:B-18A (1-2)
Inorganic Parameters
Duplicate Matrix Spike Summary
Dry
Client:
Project:
Sample Matrix:
ALS Environmental - US
HS14070721
Soil
Service Request:
Date Analyzed:
Date Received:
J1405489
07/31/14
07/23/14
Date Collected:07/14/14
EPA 3050B
6020A
Prep Method:
Analysis Method:
Analyte Name
RPD
LimitRPDResult
Sample
Result
Spike
Amount % Rec
Matrix Spike
J1405489-001MS J1405489-001DMS
Duplicate Matrix Spike
% Rec
Spike
AmountResult
% Rec
Limits
ALS Group USA, Corp.
dba ALS Environmental
07/30/14Date Extracted:
Arsenic, Total Recoverable 2.3 J 14.4 15.4 79 14.4 14.9 82 75-125 <1 20
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 8/5/2014 10:18:56 PM 14-0000297392 rev 00Superset Reference:Page 43 of 48
Sample Name
J1405489
Date Analyzed:
Service Request:
Soil
HS14070721
ALS Environmental - US
Sample Matrix:
Project:
Client:
Lab Control Sample Summary
Arsenic, Total Recoverable
Analysis Method:
Prep Method:
6020A
EPA 3050B Dry
mg/Kg
Basis:
Units:
Analysis Lot:404331
07/31/14
Spike
AmountResult % Rec
% Rec
Limits
07/30/14Date Extracted:
Lab Code
dba ALS Environmental
ALS Group USA, Corp.
QA/QC Report
Lab Control Sample 80-12097 25.024.3J1405489-LCS
14-0000297392 rev 00Superset Reference:Printed 8/5/2014 10:18:58 PM Page 44 of 48
ALS Group USA, Corp.
QA/QC Report
Client:
Project
Sample Matrix:Soil
HS14070721
ALS Environmental - US Service Request:J1405489
07/15/14Date Collected:
Date Received:07/23/14
07/25/14Date Analyzed:
Replicate Sample Summary
General Chemistry Parameters
B-9A (3.5-4.0)Percent
Basis:
Units:
J1405489-010 As ReceivedLab Code:
Sample Name:
RPD LimitPQL MDLAnalysis Method RPD
Duplicate
Sample
J1405489-
010DUP
Result Average
Sample
ResultAnalyte Name
dba ALS Environmental
Solids, Total <1 0.10 0.10 83 83 83.2 20160.3 Modified
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 8/5/2014 10:19:01 PM 14-0000297392 rev 00Superset Reference:Page 45 of 48
ALS Group USA, Corp.
QA/QC Report
Client:
Project
Sample Matrix:Soil
HS14070721
ALS Environmental - US Service Request:J1405489
07/14/14Date Collected:
Date Received:07/23/14
07/25/14Date Analyzed:
Replicate Sample Summary
General Chemistry Parameters
B-16 (3-4)Percent
Basis:
Units:
J1405489-016 As ReceivedLab Code:
Sample Name:
RPD LimitPQL MDLAnalysis Method RPD
Duplicate
Sample
J1405489-
016DUP
Result Average
Sample
ResultAnalyte Name
dba ALS Environmental
Solids, Total <1 0.10 0.10 87 86 86.4 20160.3 Modified
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 8/5/2014 10:19:02 PM 14-0000297392 rev 00Superset Reference:Page 46 of 48
Page 47 of 48
Page 48 of 48

ATTACHMENT 3
MONITORING WELL LOGS
Project:MW-9
Drilling Subcontractor:Date/time of Well Installation:7/1/2014
Driller:Kevin White
Logged By:D. Reedy 14.0 ft
Flush mount
O.D. of Outer Protective Casing N/A
0.0 bgs
2 ft. X 2 ft
cement/bentonite grout
cement/bentonite grout
6 inch diameter
1.0 ft bgs
Bentonite
3.0 ft bgs
4.0 ft bgs
WATER LEVEL MEASUREMENTS
Date
Depth from TOC
Time
PVC
No. 2 sand
Monitoring Well No.:
Approx. Stickup
Type of Backfill
Type of Surface Seal
Type of Screen
Size of Filter Sand
Depth to Bottom of Well From Top
of Monitoring Well Pipe:
MONITORING WELL INSTALLATION SKETCH
Depth or Height (ft) From Ground
Surface
2 inch
0.01
14.0 feet bgs
Mid Atlantic Drilling - MADD
Eaton - Goldsboro, NC
Diameter of Borehole
Type of Seal
Dimensions of Concrete Pad
I.D. of screen
Size of Screen Opening
Project:MW-10
Drilling Subcontractor:Date/time of Well Installation:7/1/2014
Driller:Kevin White
Logged By:D. Reedy 14.0 ft
Flush mount
O.D. of Outer Protective Casing N/A
0.0 bgs
2 ft. X 2 ft
cement/bentonite grout
cement/bentonite grout
6 inch diameter
1.0 ft bgs
Bentonite
3.0 ft bgs
4.0 ft bgs
WATER LEVEL MEASUREMENTS
Date
Depth from TOC
Time
MONITORING WELL INSTALLATION SKETCH
Eaton - Goldsboro, NC Monitoring Well No.:
Mid Atlantic Drilling - MADD
Depth to Bottom of Well From Top
of Monitoring Well Pipe:
Depth or Height (ft) From Ground
Surface
Approx. Stickup
Dimensions of Concrete Pad
Type of Surface Seal
Type of Backfill
Diameter of Borehole
Type of Seal
I.D. of screen 2 inch
Size of Screen Opening 0.01
PVCType of Screen
Size of Filter Sand No. 2 sand
14.0 feet bgs
Project:MW-11
Drilling Subcontractor:Date/time of Well Installation:7/1/2014
Driller:Kevin White
Logged By:D. Reedy 14.0 ft
Flush mount
O.D. of Outer Protective Casing N/A
0.0 bgs
2 ft. X 2 ft
cement/bentonite grout
cement/bentonite grout
6 inch diameter
1.0 ft bgs
Bentonite
3.0 ft bgs
4.0 ft bgs
WATER LEVEL MEASUREMENTS
Date
Depth from TOC
Time
MONITORING WELL INSTALLATION SKETCH
Eaton - Goldsboro, NC Monitoring Well No.:
Mid Atlantic Drilling - MADD
Depth to Bottom of Well From Top
of Monitoring Well Pipe:
Depth or Height (ft) From Ground
Surface
Approx. Stickup
Dimensions of Concrete Pad
Type of Surface Seal
Type of Backfill
Diameter of Borehole
Type of Seal
I.D. of screen 2 inch
Size of Screen Opening 0.01
PVCType of Screen
Size of Filter Sand No. 2 sand
14.0 feet bgs
Project:MW-12
Drilling Subcontractor:Date/time of Well Installation:7/1/2014
Driller:Kevin White
Logged By:D. Reedy 14.0 ft
Flush mount
O.D. of Outer Protective Casing N/A
0.0 bgs
2 ft. X 2 ft
cement/bentonite grout
cement/bentonite grout
6 inch diameter
1.0 ft bgs
Bentonite
3.0 ft bgs
4.0 ft bgs
WATER LEVEL MEASUREMENTS
Date
Depth from TOC
Time
MONITORING WELL INSTALLATION SKETCH
Eaton - Goldsboro, NC Monitoring Well No.:
Mid Atlantic Drilling - MADD
Depth to Bottom of Well From Top
of Monitoring Well Pipe:
Depth or Height (ft) From Ground
Surface
Approx. Stickup
Dimensions of Concrete Pad
Type of Surface Seal
Type of Backfill
Diameter of Borehole
Type of Seal
I.D. of screen 2 inch
Size of Screen Opening 0.01
PVCType of Screen
Size of Filter Sand No. 2 sand
14.0 feet bgs
Project:MW-13
Drilling Subcontractor:Date/time of Well Installation:7/1/2014
Driller:Kevin White
Logged By:D. Reedy 14.0 ft
Flush mount
O.D. of Outer Protective Casing N/A
0.0 bgs
2 ft. X 2 ft
cement/bentonite grout
cement/bentonite grout
6 inch diameter
1.0 ft bgs
Bentonite
3.0 ft bgs
4.0 ft bgs
WATER LEVEL MEASUREMENTS
Date
Depth from TOC
Time
MONITORING WELL INSTALLATION SKETCH
Eaton - Goldsboro, NC Monitoring Well No.:
Mid Atlantic Drilling - MADD
Depth to Bottom of Well From Top
of Monitoring Well Pipe:
Depth or Height (ft) From Ground
Surface
Approx. Stickup
Dimensions of Concrete Pad
Type of Surface Seal
Type of Backfill
Diameter of Borehole
Type of Seal
I.D. of screen 2 inch
Size of Screen Opening 0.01
PVCType of Screen
Size of Filter Sand No. 2 sand
14.0 feet bgs

ATTACHMENT 4
GROUNDWATER SAMPLE COLLECTION FORMS
DATE:
Project Name:Project No./Phase No.:
Well ID:MW-9 Sampler(s):
Well Diameter:2.0 inches Int. Depth to Water:4.89 feet
Depth to Bottom:14.00 feet Water Column Thickness:9.11 feet
Well Volume:0.0 gallons 3x Well Volume:4.4603 gallons
Well Location:
Equipment:
Time pH Cond.Turb.Dis O2 Temp.ORP DTW Rate
(S.U.)(mS/cm)(NTU)(mg/L)(°C)(millivolts)(feet)
16:15 5.51 0.185 164.60 1.61 24.93 130.6 4.89 300 ml/min
16:20 5.49 0.182 147.10 1.64 24.94 142.1 4.90 300 ml/min
16:25 5.48 0.177 47.90 1.59 24.86 53.2 4.90 300 ml/min
16:30 5.47 0.177 47.00 1.51 24.82 46.7 4.91 300 ml/min
16:35 5.47 0.172 21.30 1.47 24.77 160.7 4.93 300 ml/min
16:40 5.47 0.172 20.30 1.46 24.78 161.3 4.93 300 ml/min
16:45 5.50 0.171 14.60 1.41 23.75 149.4 4.94 300 ml/min
16:50 5.47 0.172 12.30 1.40 24.77 155.1 4.95 300 ml/min
17:00
Comments (weather conditions, color, type of sample, purge-water management, etc.):
2.8 Gallons
Signature:Date:
QA/QC Sign Off:Date:
7/15/2014
GROUNDWATER SAMPLING LOG
13384340.0005
R. Lovett
located along the northern side of the building near the main entrance.
Total volume purged:
YSI 556, Solinst water level, Mini Rae PID, and Peristaltic Pump
SAMPLED
Eaton - Goldsboro, NC
DATE:
Project Name:Project No./Phase No.:
Well ID:MW-10 Sampler(s):
Well Diameter:2.0 inches Int. Depth to Water:4.94 feet
Depth to Bottom:14.00 feet Water Column Thickness:9.06 feet
Well Volume:0.0 gallons 3x Well Volume:4.4358 gallons
Well Location:
Equipment:
Time pH Cond.Turb.Dis O2 Temp.ORP DTW Rate
(S.U.)(mS/cm)(NTU)(mg/L)(°C)(millivolts)(feet)
15:30 5.58 0.223 9.80 1.37 24.16 82.9 0.00 300 ml/min
15:35 5.50 0.221 4.50 1.28 13.96 90.9 5.00 300 ml/min
15:40 5.46 0.219 0.90 1.23 23.80 89.8 5.01 300 ml/min
15:45 5.44 0.218 0.90 1.20 23.83 86.4 5.00 300 ml/min
15:50 5.43 0.218 0.90 1.20 23.86 86.4 5.01 300 ml/min
15:55 5.44 0.219 0.90 1.20 23.84 86.4 5.02 300 ml/min
16:00 5.43 0.218 0.90 1.20 23.86 86.5 5.02 300 ml/min
16:00
Comments (weather conditions, color, type of sample, purge-water management, etc.):
2.4 Gallons
Signature:Date:
7/15/2014
GROUNDWATER SAMPLING LOG
13384340.0005
R. Lovett
located along the eastern side of the building
YSI 556, Solinst water level, Mini Rae PID, and Peristaltic Pump
SAMPLED
Total volume purged:
QA/QC Sign Off:Date:
Eaton - Goldsboro, NC
DATE:
Project Name:Project No./Phase No.:
Well ID:MW-11 Sampler(s):
Well Diameter:2.0 inches Int. Depth to Water:4.8 feet
Depth to Bottom:14.00 feet Water Column Thickness:9.2 feet
Well Volume:0.0 gallons 3x Well Volume:4.50432 gallons
Well Location:
Equipment:
Time pH Cond.Turb.Dis O2 Temp.ORP DTW Rate
(S.U.)(mS/cm)(NTU)(mg/L)(°C)(millivolts)(feet)
14:30 5.34 0.104 2.40 2.01 23.42 22.5 0.00 300 ml/min
14:35 5.32 0.099 2.20 0.90 22.62 22.9 4.85 300 ml/min
14:40 5.37 0.086 1.30 0.79 22.18 39.6 4.86 300 ml/min
14:45 5.24 0.084 1.50 0.72 21.99 38.8 4.87 300 ml/min
14:50 5.35 0.077 27.60 0.70 21.84 37.1 4.89 300 ml/min
14:55 5.42 0.075 39.60 0.70 21.75 34.1 4.90 300 ml/min
15:00 5.44 0.075 48.10 0.68 21.71 47.9 4.90 300 ml/min
15:05 5.50 0.073 31.30 0.07 21.71 40.3 4.92 300 ml/min
15:05
Comments (weather conditions, color, type of sample, purge-water management, etc.):
2.8 Gallons
Signature:Date:
7/15/2014
GROUNDWATER SAMPLING LOG
Eaton - Goldsboro, NC 13384340.0005
R. Lovett
located along the southeastern corner of the building
YSI 556, Solinst water level, Mini Rae PID, and Peristaltic Pump
SAMPLED
Total volume purged:
QA/QC Sign Off:Date:
DATE:
Project Name:Project No./Phase No.:
Well ID:MW-12 Sampler(s):
Well Diameter:2.0 inches Int. Depth to Water:4.52 feet
Depth to Bottom:14.00 feet Water Column Thickness:9.48 feet
Well Volume:0.0 gallons 3x Well Volume:4.641408 gallons
Well Location:
Equipment:
Time pH Cond.Turb.Dis O2 Temp.ORP DTW Rate
(S.U.)(mS/cm)(NTU)(mg/L)(°C)(millivolts)(feet)
13:20 5.31 0.088 79.00 1.52 26.55 57.0 0.00 300 ml/min
13:25 5.13 0.084 22.80 0.59 24.63 42.1 4.60 300 ml/min
13:30 5.13 0.081 17.30 0.47 24.64 34.9 4.62 300 ml/min
13:35 5.14 0.081 27.10 0.49 24.52 42.1 4.66 300 ml/min
13:40 5.11 0.084 15.10 0.48 24.36 17.1 4.67 300 ml/min
13:45 5.09 0.084 15.00 0.48 24.27 17.6 4.68 300 ml/min
13:50 5.07 0.084 13.20 0.46 24.22 17.8 4.69 300 ml/min
13:55 5.08 0.084 12.10 0.46 24.13 17.8 4.70 300 ml/min
14:00
Comments (weather conditions, color, type of sample, purge-water management, etc.):
2.8 Gallons
Signature:Date:
7/15/2014
GROUNDWATER SAMPLING LOG
Eaton - Goldsboro, NC 13384340.0005
R. Lovett
located in the middle of the southern building exterior wall
YSI 556, Solinst water level, Mini Rae PID, and Peristaltic Pump
SAMPLED
Total volume purged:
QA/QC Sign Off:Date:
DATE:
Project Name:Project No./Phase No.:
Well ID:MW-13 Sampler(s):
Well Diameter:2.0 inches Int. Depth to Water:4.49 feet
Depth to Bottom:14.00 feet Water Column Thickness:9.51 feet
Well Volume:0.0 gallons 3x Well Volume:4.656096 gallons
Well Location:
Equipment:
Time pH Cond.Turb.Dis O2 Temp.ORP DTW Rate
(S.U.)(mS/cm)(NTU)(mg/L)(°C)(millivolts)(feet)
12:15 6.39 0.197 6.70 1.97 23.47 8.9 0.00 300 ml/min
12:20 6.00 0.162 4.20 1.51 23.12 12.8 4.62 300 ml/min
12:25 5.73 0.140 3.60 0.92 22.65 19.2 4.62 300 ml/min
12:30 5.18 0.105 2.10 0.52 22.34 29.2 4.68 300 ml/min
12:35 5.12 0.104 1.20 0.54 22.22 31.5 4.68 300 ml/min
12:40 5.08 0.102 5.20 0.50 22.02 36.8 4.68 300 ml/min
12:45 5.07 0.101 6.50 0.48 22.07 40.1 4.70 300 ml/min
12:50 5.06 0.101 10.00 0.41 22.68 40.2 4.70 300 ml/min
13:00
Comments (weather conditions, color, type of sample, purge-water management, etc.):
3.6 Gallons
Signature:Date:
7/15/2014
GROUNDWATER SAMPLING LOG
Eaton - Goldsboro, NC 13384340.0005
R. Lovett
located along the southwestern portion of the building near trash compactor.
YSI 556, Solinst water level, Mini Rae PID, and Peristaltic Pump
SAMPLED
Total volume purged:
QA/QC Sign Off:Date:

Golder, Golder Associates and the GA globe design are trademarks of Golder Associates Corporation

Golder Associates Inc.
5B Oak Branch Drive
Greensboro, NC 27407 USA
Tel: [phone]
Fax: [phone]