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Home My WebLink About13002_Historic Biltmore Village II_Brownfield Assessment Report_20091016SOIL, GROUNDWATER, AND SOIL GAS ASSESSMENT REPORT 1 FAIRVIEW ROAD PROPERTY ASHEVILLE, NORTH CAROLINA S&ME Project No. 1411-09-040A NCDENR Brownfields Project No. 130002-09-11 Prepared for: Historic Biltmore Village II, LLC c/o Mr. Joseph Tanneberger Hill Partners, Inc. 101 W. Worthington Avenue Suite 204 Charlotte, North Carolina 28203 Prepared by: 44 Buck Shoals Road, Suite C-3 Arden, North Carolina 28704 October 16, 2009 i TABLE OF CONTENTS 1. BACKGROUND ........................................................................................................ 1 1.1 Property Information...........................................................................................1 1.2 Site History.........................................................................................................1 1.3 Project History....................................................................................................1 1.3.1 Brownfields Property Application......................................................1 1.3.2 Phase I Environmental Site Assessment (March 2009)......................1 1.3.3 Brownfields Area Reconnaissance and Receptor Survey (March 2009) .............................................................................................................3 1.3.4 Work Plan for Additional Assessment................................................3 1.3.5 Quality Assurance Project Plan ..........................................................3 2. MATERIAL AND METHODS................................................................................4 2.1 Soil Sampling and Analyses...............................................................................4 2.1.1 Sample Collection...............................................................................4 2.1.2 Sample Analyses.................................................................................4 2.2 Groundwater Sampling and Analyses.................................................................5 2.2.1 Existing Monitoring Wells..................................................................5 2.2.2 Temporary Monitoring Well Installation............................................5 2.2.3 Sample Collection...............................................................................5 2.2.4 Sample Analyses.................................................................................6 2.3 Soil Gas Sampling and Analyses........................................................................6 2.3.1 Soil Gas Probe Installation..................................................................6 2.3.2 Sample Collection...............................................................................6 2.3.3 Sample Analyses.................................................................................6 2.4 Analytical Laboratory.........................................................................................6 2.5 Decontamination Procedures..............................................................................7 2.6 Investigative Derived Wastes .............................................................................7 2.7 Regulatory Standards and Screening Thresholds ............................................... 7 3. RESULTS AND DISCUSSIONS..............................................................................8 3.1 Site Hydrogeology..............................................................................................8 3.2 Analytical Data Quality Review.........................................................................8 3.3 Quality Control Data...........................................................................................9 3.3.1 Trip Blanks..........................................................................................9 3.3.2 Field Blank..........................................................................................9 3.3.3 Duplicate Samples ..............................................................................9 3.4 Drum Storage and Former Vertical AST Area.................................................11 3.4.1 Soil Quality.......................................................................................11 3.4.2 Groundwater Quality ........................................................................12 3.4.3 Regulatory Standard/Goal Comparison............................................12 3.5 Former Petroleum Tank....................................................................................13 3.5.1 Soil Quality.......................................................................................13 3.5.2 Groundwater Quality ........................................................................13 3.5.3 Regulatory Standard/Goal Comparison............................................14 3.6 Fuel Loading Rack............................................................................................ 14 3.6.1 Soil Quality.......................................................................................14 ii 3.6.2 Regulatory Standard/Goal Comparison............................................15 3.7 Underground Petroleum Product Line..............................................................15 3.7.1 Soil Quality.......................................................................................15 3.7.2 Regulatory Standard/Goal Comparison............................................16 3.8 Horizontal AST Area........................................................................................16 3.8.1 Soil Quality.......................................................................................16 3.8.2 Regulatory Standard/Goal Comparison............................................17 3.9 Vertical AST Area............................................................................................ 18 3.9.1 Soil Quality.......................................................................................18 3.9.2 Regulatory Standard/Goal Comparison............................................18 3.10 Elevated 55-Gallon Drum.................................................................................19 3.10.1 Soil Quality.......................................................................................19 3.10.2 Regulatory Standard/Goal Comparison............................................19 3.11 Coal Storage Area............................................................................................. 20 3.11.1 Soil Quality.......................................................................................20 3.12 Regulatory Standard/Goal Comparison............................................................21 3.13 Existing Monitoring Wells................................................................................21 3.13.1 Groundwater Quality ........................................................................22 3.14 Soil Gas Assessment.........................................................................................22 3.14.1 Soil Gas Quality................................................................................22 3.14.2 Regulatory Screening Comparison...................................................23 4. RECOMMENDATIONS ........................................................................................23 4.1 Petroleum Storage and Dispenser Equipment...................................................23 4.2 Near-Surface Contaminated Soil......................................................................23 4.3 Existing Building/Soil Gas ...............................................................................24 4.4 Groundwater .....................................................................................................24 5. SOLE USE STATEMENT......................................................................................25 6. LIMITATIONS........................................................................................................25 7. REFERENCES ........................................................................................................ 25 TABLES Table 1 Well Construction and Groundwater Elevation Data Table 2 Summary of Additional Field Data Table 3 Summary of Quality Control Analytical Data Table 4 Summary of Soil Analytical Data Table 5 Summary of Groundwater Analytical Data Table 6 Summary of Soil Gas Analytical Data FIGURES Figure 1 Project Location Map Figure 2 Site Plan Figure 3 Potentiometric Map Figure 4 Soil Analytical Results Map Figure 5 Groundwater and Soil Gas Results Map iii APPENDICES Appendix I Well Construction Logs Appendix II Clean Canister Certification Report Appendix III Regulatory Standards and Benchmarks Appendix IV Soil Laboratory Report Appendix V Groundwater Laboratory Report Appendix VI Soil Gas Laboratory Report Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 1 1. BACKGROUND 1.1 Property Information The subject property is located near the intersection of London Road and Fairview Road in the City of Asheville, Buncombe County, North Carolina. Figure 1 shows the approximate location of the site. The parcel is currently owned by Rankin Patterson Oil Co., Inc. and is currently being used as an office for Rankin-Patterson Oil Company. Three structures including an office building and two utility buildings are located on the property. The site contains seven large petroleum above ground storage tanks (ASTs) and two smaller ASTs that are remnants of the former retail petroleum distribution business known as Rankin-Patterson Oil Company. The petroleum distribution business has not operated on the property since 2008. The property is identified as 1 Fairview Road and is being considered for purchase by Historic Biltmore Village II, LLC (HBVII). HBVII is ultimately considering redevelopment of the subject property as a parking lot to support the Brownfields site identified as 9 Reed Street and other businesses in the Historical Biltmore Village. However, HBVII would also like to have the option to keep the existing building for lease space. 1.2 Site History Based on a review of Sanborn Fire Insurance maps, as early as 1907, the subject property was operated as an ice factory and a coal yard. The property was soon after operated as Biltmore Milling Co., a facility for processing corn. From at least 1945 until 1977, the property was operated as Biltmore Coal & Lumber. Biltmore Coal & Lumber sold lumber and packaged and sold coal. Beginning in around 1954, Biltmore Coal & Lumber began storing fuel oil for retail sales. In 1977, the property was purchased by Rankin- Patterson Oil Company. The existing petroleum storage tanks were reconfigured and additional storage tanks were added. The facility stored and sold petroleum materials until 2008. However, the storage tanks used at the facility remain onsite. 1.3 Project History The following is a summary of the assessment activities that have been conducted in association with the subject property: 1.3.1 Brownfields Property Application On January 12, 2009, a Brownfields Property Application to enter into a Brownfields Agreement was submitted to the Brownfields Program of the North Carolina Department of Environment and Natural Resources (NCDENR) Division of Waste Management. On February 20, 2009, the subject site was determined to be eligible to enter into the Brownfields Program by NCDENR to work towards obtaining a Brownfields Agreement. 1.3.2 Phase I Environmental Site Assessment (March 2009) In March 2009, under contract with Land-of-Sky Regional Council, S&ME completed a Phase I Environmental Site Assessment (ESA) on the subject property. The Phase I ESA Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 2 was performed in accordance with the All Appropriate Inquiry Rule set forth in 40 C.F.R. Part 312 and the American Society for Testing and Materials (ASTM) Practice entitled E 1527-05, Standard Practice for Environmental Assessments: Phase I Environmental Site Assessment Process. The Phase I ESA identified the following recognized environmental conditions (RECs): • As many as three (3) 20,000 gallon vertical ASTs were used to store #2 fuel oil and kerosene since at least 1954. • Three (3) 20,000 horizontal ASTs were used to store gasoline and diesel fuel since at least 1982. • Staining and discoloration of the soil/gravel was observed within the secondary containment area of the fuel loading rack. • One (1) 10,000 vertical AST was used to store varsol since at least 1988. • One (1) 550 gallon horizontal AST was used to store gasoline since at least 1988. • One (1) 550 gallon horizontal AST was used to diesel fuel since at least 1988 until about 2006. • A gasoline tank was identified near the former office building on the 1950 Sanborn fire insurance map. • Approximately 3,000 gallons of fuel oil were spilled at the facility in 2003. • One (1) 55 gallon AST was and remains located on the subject property. • For approximately 20 years, the concrete pad located in the southeastern corner of the property was used for empty drum and pump storage. • A pile of suspected used oil-dry was observed near the utility building near the northwest corner of the property. • The subject property was operated as a coal yard for at least 37 years. Based on a review of the 1951, 1965, and 1975 aerial photographs of the site, mounds of coal were visible on the western portion of the property. • Petroleum-impacted groundwater and free product have been confirmed to be associated with the release of fuel oil from an underground piping system at the Asheville Oil Company, the adjoining property to the north of the subject property. Based on the available groundwater flow maps for the Asheville Oil Company site, contaminated groundwater and/or free product is likely to have migrated or to migrate toward the subject property. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 3 • Petroleum-impacted groundwater and free product have been confirmed to be associated with the release from an underground storage tank (UST) system at the Biltmore Food Store property, located south and topographically upgradient from the subject property. Free product has historically been detected in the five recovery wells on the property and in the telephone manhole vault located northwest of the property under Fairview Road. Based on the topography of the Biltmore Food Store, contaminated groundwater and/or free product is expected to have migrated or to migrate towards the subject property. The Site Plan showing the layout of the features on the property is included as Figure 2. 1.3.3 Brownfields Area Reconnaissance and Receptor Survey (March 2009) In April 2009, under contract with Land-of-Sky Regional Council, S&ME completed the Brownfields Area Reconnaissance and Receptor Survey for the subject property. The survey was performed in general accordance with S&ME Proposal No. ENV-051-09 dated March 19, 2009, to identify the presence of subsurface structures, underground utilities, water bodies, and water wells in the vicinity of the subject property. 1.3.4 Work Plan for Additional Assessment On June 22, 2009, S&ME submitted the Work Plan for Soil and Groundwater Assessment to Ms. Tracy Wahl, Brownfields Project Manger with NCDENR. The Work Plan proposed assessment activities at the site assuming that the existing structure would be demolished and the property would be used as a parking lot. Prior to receiving comments regarding the Work Plan from Ms. Wahl, on June 24, 2009, Mr. Joe Tanneberger with HBVII contacted Mr. David Loftis of S&ME by telephone. In the conversation, Mr. Tanneberger stated that HBVII wanted the option to use the existing structure for lease space. Based on this request, Ms. Wahl requested that the Work Plan be modified to include at least two soil gas samples from outside of the building footprint. No sub-slab samples were requested by Ms. Wahl, since the onsite structure rests on a crawlspace foundation. On July 21, 2009, S&ME submitted the revised Work Plan to Ms. Wahl. On July 28, 2009, Ms. Wahl approved the Work Plan via an electronic message provided to Mr. Loftis. 1.3.5 Quality Assurance Project Plan S&ME completed the Quality Assurance Project Plan (QAPP) on August 26, 2009, and submitted the QAPP to Ms. Wanda Jennings, EPA Region 4 Brownfields Coordinator. On September 3, 2009, S&ME received comments regarding the QAPP via electronic mail from Ms. Jennings. S&ME addressed Ms. Jennings’ comments and submitted the final version of the QAPP to Ms. Jennings on September 4, 2009. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 4 2. MATERIAL AND METHODS Unless specially noted, all field activities were performed in accordance with the following documents: • S&ME, Inc. Work Plan for Limited Soil, Groundwater, and Soil Gas Assessment. July 21, 2009. • S&ME, Inc. Quality Assurance Project Plan. September 3, 2009. 2.1 Soil Sampling and Analyses 2.1.1 Sample Collection Soil samples were collected using a stainless steel hand auger or direct push techniques using a Geoprobe®. Where a concrete slab or asphalt pavement was present, the near surface soil samples were collected from the first soil encountered beneath the concrete slab or pavement system. For samples in locations were no concrete or pavement cap was present, the near surface samples were collected from approximately one foot below land surface (bls). Subsurface soil samples were collected approximately 1.5 feet above the measured water table approximately 6 feet bls. Contrary to the Work Plan and the QAPP, the sample depth for subsurface soil samples was not selected based on field screening for organic vapors using an Organic Vapor Analyzer (OVA) because the unsaturated soil zone was only 6 ft. in thickness. 2.1.2 Sample Analyses Soil samples collected in association with potential petroleum-related releases at the (1) vertical and horizontal ASTs, (2) former gasoline tank, (3) fuel loading rack, and (4) buried fuel product lines were analyzed for the following parameters: • Volatile organic compounds (VOCs) by SW846 Method 8260B, and • Semi-volatile organic compounds (SVOCs) by SW846 Method 8270C Soil samples collected in association with the former drum and pump storage area were analyzed for the following parameters: • VOCs by SW846 Method 8260B, • SVOCs by SW846 Method 8270C, and • Oil & grease (O&G) with silica gel cleanup by SW846 Method 9071. Soil samples collected in association with the portion of the property used to store coal were analyzed for the following parameters: • SVOCs by SW 846 Method 8270C, and Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 5 • NCDENR Hazardous Substance List (HSL) metals by SW 846 Methods 6010B and 7471 (mercury). The HSL metals list includes antimony, arsenic, beryllium, cadmium, chromium, copper, lead, manganese, mercury, nickel, selenium, silver, thallium, and zinc. 2.2 Groundwater Sampling and Analyses Shallow groundwater samples were collected and analyzed to characterize the quality of the shallow groundwater at the site. 2.2.1 Existing Monitoring Wells Monitoring wells MW-1, MW-2, MW-3, and MW-4 were installed in 2003 by Mountain Environmental Services, Inc. (Mountain) in response to the 2003 release of heating oil at the facility. All of the existing monitoring wells, except MW-3, were located in the field. S&ME searched for MW-3 using a metal detector and digging with a shovel and rake in locations suspected to contain MW-3 based on figures in Mountain assessment reports for the property. Nevertheless, this well was not located. The well construction details for the existing monitoring wells are included in Table 1. The monitoring well construction logs prepared by Mountain are included in Appendix I. The locations of the temporary wells are shown on Figure 3. 2.2.2 Temporary Monitoring Well Installation Three (3) temporary monitoring wells (1Fair-TW1, 1Fair-TW2, and 1Fair-TW3) were installed by Probe Technology, Inc. of Concord, North Carolina, in the shallow aquifer using direct push technology. The wells consisted of 1-inch diameter, flush-thread, polyvinylchloride (PVC) pipe inserted into an approximate 2.25-in. diameter hole. The lower portion of the pipe consisted of manufactured well screen with 0.010-inch slots. The annulus around the well screen was filled with #2 filter sand to a depth of 1 feet. above the top of the wells screen. Hydrated bentonite chips were placed around the remaining annulus of the well casing up to the ground surface. The well construction details for the temporary wells are included in Table 1. The temporary well construction logs for included in Appendix I. After the temporary wells were sampled, the wells were properly abandoned by a North Carolina-licensed well driller. 2.2.3 Sample Collection Before purging and sampling of the monitoring wells, the water level and depth at each temporary and permanent monitoring well was measured and recorded to provide an approximation of instantaneous groundwater flow direction. The measured water level data are presented in Table 1. Each well was developed and purged for sampling using a variable speed, electric, peristaltic pump. Each well was considered purged when three (3) to five (5) well volumes had been evacuated from the well. New silicone tubing (at the pump head) and polyethylene tubing (downwell) was used to purge each well. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 6 Once the wells had been purged, a groundwater sample was collected using a disposable bailer and immediately dispensed into laboratory-prepared containers. 2.2.4 Sample Analyses The collected groundwater samples were analyzed for: • VOCs by SW846 Method 8260B, and • SVOCs by SW846 Method 8270C 2.3 Soil Gas Sampling and Analyses Soil gas samples were collected and analyzed to evaluate the potential for petroleum vapors to exist in the building crawlspace. 2.3.1 Soil Gas Probe Installation On September 8, 2009, two (2) soil gas probes (1Fair-SG1 and 1Fair-SG2) were installed by Probe Technology, Inc. in the unsaturated zone using direct push technology. The soil gas probes consisted of 0.75-inch diameter, flush-thread, PVC pipe inserted into an approximate 2.25-inch diameter hole that was 6 feet deep. The lower portion of the gas probes consisted of 2-inch of manufactured well screen with 0.010-in slots. Each boring was backfilled with 1 foot of #2 filter sand and the remaining 5 feet of the hole was grouted to the ground surface with a bentonite mix. Each soil gas probe was then sealed with an air-tight cap. The soil gas probes were allowed to sit overnight before sampling. 2.3.2 Sample Collection Each soil gas probe was evacuated for approximately 30 seconds using a peristaltic pump. A six (6) liter (L) pre-evacuated, certified-clean Summa Canister© and regulator was attached to each probe using ¼-inch inside diameter (I.D.) Teflon™ tubing. Clean certification and flowrate calibration were performed by the laboratory. The laboratory reports indicating that the Summa Canister© were clean is provided Appendix II. “Laboratory-certified clean” is defined for use herein as the non-detection of all analytes in the VOC Method TO-15 suite without elevated detection limits. The samples were collected over an eight (8) hour continuous period. Canister vacuum readings were documented before sampling to demonstrate that each canister was not leaking prior to sampling. The canister vacuum readings were documented after sampling to demonstrate that each flow controller collected the sample as designed. Canister vacuum readings are presented on Table 2. 2.3.3 Sample Analyses The collected gas samples were analyzed for VOCs by EPA Method TO-15. 2.4 Analytical Laboratory All sample analyses were performed in accordance with the United States Environmental Protection Agency by Pace Analytical Services, Inc. (Pace) The soil and groundwater samples were analyzed by the Pace lab in Huntersville, North Carolina and the air samples were analyzed by the Pace lab in Minneapolis, Minnesota. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 7 2.5 Decontamination Procedures Prior to use and after each sampling event, all small sampling equipment was decontaminated and cleaned to prevent cross-contamination. The equipment decontamination procedure consisted of a potable water rinse to remove visible dirt and debris followed by an Alconox® wash, another potable water rinse, a deionized water rinse, an isopropyl alcohol wash, and final deionized water rinse followed by air drying of the equipment. The larger equipment, including Geoprobe® rods and Macro-Core samplers and the rig itself, were cleaned with a high-pressure, hot water steam cleaner. The equipment was rinsed once with the steam cleaner and then scrubbed to remove any remaining loose debris, followed by another wash with the steam cleaner and then air-dried. The large equipment decon rinsate was contained within a bermed area and pumped into EPA approved containers and labeled as to their contents. 2.6 Investigative Derived Wastes In accordance with the approved QAPP, soil cuttings generated during the collection of soil samples in association with former coal storage area were placed into a labeled and sealed 55-gallon drum that was staged onsite. Due to the relatively low concentrations of arsenic (11.8 mg/kg or less) and the small quantity of soil (approximately one cubic foot or less), with NCDENR approval, S&ME recommends that the soil be spread in the areas that will be capped with by the parking lot pavement system. In accordance with Section 12 of the UST Section Guidelines for the Investigation and Remediation of Contamination from Non-UST Petroleum Releases dated July 1, 2009 (http://www.wastenotnc.org/ust/docs/Non-USTGuid053107.pdf) and Section 6.1.2 page 62 in the Guidelines for Assessment and Corrective Action for UST Releases dated July 15, 2008 (http://www.wastenotnc.org/ust/docs/aca_body.pdf), the soil cuttings generated during the collection of soil samples from all other locations (i.e petroleum sources) were spread on the ground following sample collection. Liquid waste generated during decontamination activities was placed into labeled and sealed 55-gallon drums that were staged onsite. The water should be sampled and analyzed for parameters required by the selected disposal facility. Disposable supplies such as gloves, bailers, string, and tubing were placed in a garbage bag and placed in the trash bin at S&ME’s office. Garbage from the trash bin is land filled at the Buncombe County Landfill. 2.7 Regulatory Standards and Screening Thresholds In accordance with the NCDENR North Carolina Brownfields Program, the parameter- specific values used standard and screening thresholds are: Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 8 Soil • UST Section Guidelines for the Investigation and Remediation of Contamination from Non-UST Petroleum Releases (http://www.wastenotnc.org/ust/docs/Non-USTGuid053107.pdf) • NCDENR Inactive Hazardous Sites Branch (IHSB) Health-Based Soil Remediation Goals (SRGs) (http://www.wastenotnc.org/soiltable.pdf ) and • IHSB Protection of Groundwater SRGs (http://www.wastenotnc.org/SFHOME/PGWSRG_Table.pdf) Groundwater • Groundwater Quality Standards for Class GA groundwater provided in Subchapter 2L Section .0200 North Carolina Administrative Code (NCAC) (http://h2o.enr.state.nc.us/admin/rules/documents/15ANCAC2Lbooklet.p df) Soil Gas • NCDENR Inactive Hazardous Sites Branch (IHSB) Vapor Intrusion Screening Levels for Soil (provided by Tracy Wahl with NCDENR on October 2, 2009) • NCDENR IHSB Industrial/Commercial Vapor Intrusion Screening Tables (provided by Tracy Wahl with NCDENR on October 2, 2009) Appendix III contains tables and excerpts of the applicable standards and thresholds contained above. 3. RESULTS AND DISCUSSIONS 3.1 Site Hydrogeology A groundwater elevation contour map (see Figure 3) was prepared from groundwater elevation data (see Table 1) obtained from three (3) temporary wells and three (3) existing permanent monitoring wells. Based on the measured groundwater level data, the instantaneous groundwater flow direction for the shallow aquifer appeared to be to the north-northeast towards Sweeten Creek, which borders the property to the west and east. The shallow groundwater likely discharges into Sweeten Creek. 3.2 Analytical Data Quality Review The laboratory analytical reports for the groundwater, soil, and soil gas samples are included in Appendices IV, V, and VI, respectively. The analytical data were reviewed qualitatively to ensure that analyte concentrations in the dataset were of known quality. Data qualifiers assigned by the laboratory were reviewed to verify that rejected or unsupportable data were note included in the dataset. Quality control data provided in the laboratory reports were also reviewed. No rejected or otherwise unacceptable quality data were used in the dataset. Accordingly, it was Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 9 concluded that the data acquired to develop the assessment report were of sufficient quality to make decisions regarding analyte nature and extent with confidence. 3.3 Quality Control Data 3.3.1 Trip Blanks One (1) trip blank water sample was placed in each sample cooler containing soil and groundwater samples. Each sample was analyzed for VOCs by SW846 Method 8260B. No target compounds were detected in the trip blank samples (see Table 3). The results of the trip blank analysis indicated that the collected soil and groundwater samples were not subject to cross contamination during shipment. Equipment rinsate samples were collected by containerizing deionized water that was poured through the hand auger bucket and Macro-Core sampler following the decontamination procedures outlined in Section 2.5. The collected equipment rinsate samples were analyzed for VOCs and SVOCs by SW846 Method 8260B and 8270C, respectively. The results of the rinsate sample analyses did not detect any VOCs and SVOCs target compound in exceedance of the method detection limit (see Table 3). The laboratory results indicated that the decontamination procedures were sufficient to remove residual contaminants from the sampling equipment. 3.3.2 Field Blank One (1) field blank was collected during groundwater sample collection activities. The field blank sample was collected by filling laboratory-prepared containers with deionized water following the same general procedures as used for collection of the groundwater samples. The field blank sample was analyzed for VOCs and SVOCs by SW846 Method 8260B and 8270C, respectively. No target compounds were detected in exceedance of the laboratory reporting limits (see Table 3). The laboratory results indicated that the groundwater sample collection procedures did not contaminate or otherwise compromise the integrity of the groundwater samples. 3.3.3 Duplicate Samples Duplicate samples were analyzed in association with the collected soil, groundwater, and soil gas samples. Relative percent difference (RPD), a measure of precision, was used to compare analytical results between sample and duplicate pair. RPD is calculated by: RPD (%) = [X1-X2] / Xave * 100 where: X1 = concentration of sample X2 = concentration of duplicate pair Xave = ((X1 + X2) / 2) Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 10 During the RPD calculations, for concentrations of analytes not detected by the laboratory method, the concentrations were set equal to the laboratory reporting limit. Soil Duplicate soil samples were submitted for samples 1Fair-TW1-SS1-09-09 and 1Fair- TW3-SS2-09-09 and analyzed for the same parameters as the original samples. For ease of readings and reporting, sample names were abbreviated. For example, sample 1Fair- TW1-SS1-09-09 is referred to as TW1-SS1. The laboratory results for the duplicate soil samples are provided in Table 4. The laboratory results for the detected compounds in soil sample TW1-SS1 and its blind duplicate (Duplicate 3) had RPDs between 0.6% and 145.3%. The laboratory results for the detected compounds in soil sample TW3-SS2 and its blind duplicate (Duplicate 2) did not detect target compounds in exceedance of the laboratory reporting limits. The RPDs for several compounds in association with the Duplicate 3 analysis exceeded the 30% threshold established in the QAPP. However, a review of the laboratory data quality information provided along with the analytical reports found no data were flagged as rejected. Based on this observation, S&ME believes that the acquired data should be accepted. For duplicate samples, where % RPD was calculated as a quality metric and the resulting value was outside of the acceptable tolerance specified in the project QAPP, samples exhibiting the higher concentration were used in the data analysis. Groundwater A duplicate groundwater sample (Duplicate) was submitted for groundwater sample TW- 3 and analyzed for the same parameters as the original sample. The laboratory results for the duplicate groundwater sample are provided in Table 5. The laboratory results for the detected compounds in groundwater sample TW-3 and its blind duplicate (Duplicate) had RPDs between 3.6% and 45.4%. The RPDs for several compounds in association with the Duplicate analysis exceeded the 30% threshold established in the QAPP. However, a review of the laboratory data quality information provided along with the analytical reports found no data were flagged as rejected. Based on this observation, S&ME believes that the acquired data should be accepted. For duplicate samples, where % RPD was calculated as a quality metric and the resulting value was outside of the acceptable tolerance specified in the project QAPP, samples exhibiting the higher concentration were used in the data analysis. Soil Gas A duplicate soil gas sample (DUP1) was submitted for soil gas sample SG2 and analyzed for the same parameters as the original sample. The laboratory results for the duplicate soil gas sample are provided in Table 6. The laboratory results for the detected compounds in soil gas sample SG2 and its blind duplicate (DUP1) had RPDs between 49% and 198%. The RPDs for all detected compounds exceed 30% threshold established in the QAPP. Based on a review of the Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 11 laboratory data and our sampling procedures, S&ME believes that a loose connection or a leaky valve was present in association with canister used to collect the soil gas sample SG2. The laboratory data for SG2 is believed to reflect the concentrations present in the ambient air and not the subsurface soils. Therefore, it is our opinion that the data for sample DUP1 should be used to evaluate the soil gas conditions at probe SG2. 3.4 Drum Storage and Former Vertical AST Area From at least 1954 until around 1988, three (3) vertical AST’s were located on the concrete pad located on the southeast corner of the subject site. The tanks were used to store #2 fuel oil and kerosene. For approximately 20 years (since 1988), the concrete pad has been used for empty drum and pump storage. During our site reconnaissance, S&ME observed at least 24 drums labeled as 10W40 oil, cutting lubricant, antifreeze, and gear compound. Several piles of oil-dry were noted on the concrete. The presence of oil-dry suggests that spills have occurred in the area. 3.4.1 Soil Quality Temporary monitoring well TW-1 was installed within the concrete pad. One (1) soil sample (TW1-SS1) was collected for laboratory analyses during completion of the well soil boring. The soil sample was collected from a depth interval of 1.5 feet to 3.5 feet, immediately below the concrete slab and sub-grade stone. The sample was collected to evaluate the effects of suspected petroleum releases would have on the soil below the concrete slab. A duplicate sample (DUP3) of TW1-SS1 was also collected. The collected samples were submitted for analyses for VOCs, SVOCs, and O&G with silica gel cleanup. The following results were obtained (see Table 4 and Figure 4): VOCs • Ten (10) VOCs were detected in sample TW1-SS1. • Ten (10) VOCs were detected in sample DUP3. • There were no elevated detection limit issues in samples TW1-SS1 and DUP3, except the detection limits for benzene, 0.249 mg/kg and 0.255 mg/kg , respectively, exceeded the NCDENR IHSB Protection of Groundwater SRG (0.00562 mg/kg). SVOCs • Two (2) SVOCs, 1-methylnaphthalene and 2-methylnaphthalene were detected in sample TW1-SS1. • No other SVOCs were detected in sample TW1-SS1. • Elevated detection limits were noted in sample TW1-SS1 since several of the target compounds had detection limits greater than the NCDENR IHSB Protection of Groundwater SRGs. • Three (3) SVOCs, 1-methylnaphthalene, 2-methylnaphthalene, and naphthalene, were detected in sample DUP3. • No other SVOCs were detected in sample DUP3. • There were no elevated detection limits issues in sample DUP3, except the detection limit for benzo(a)anthracene (0.431 mg/kg) exceeded the NCDENR Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 12 IHSB Protection of Groundwater and NCDENR IHSB Health-Based SRGs of 0.343 mg/kg and 0.15 mg/kg, respectively. Oil & Grease • O&G was detected at a concentration of 141 milligrams per kilograms (mg/kg) in sample TW1-SS1. • O&G was detected at a concentration of 118 mg/kg in sample DUP3. • There were no elevated detection limits issues in samples TW1-SS1 and DUP3. 3.4.2 Groundwater Quality Temporary monitoring well TW-1 was installed to assess groundwater impacts from suspected petroleum releases on the concrete slab. The collected sample was submitted for analyses for VOCs and SVOCs. The following results were obtained (see Table 5 and Figure 5): VOCs • One (1) VOC was detected; methyl-tert butyl ether (MTBE) at a concentration of 3.3 micrograms per liter (μg/L). • No other VOCs were detected. • There were no elevated detection limit issues. SVOCs • One (1) SVOC was detected; 1-methylnapthalene at a concentration of 12.6 μg/L. • No other SVOCs were detected. • There were no elevated detection limit issues. 3.4.3 Regulatory Standard/Goal Comparison Soil • VOCs, n-butylbenzene, naphthalene, n-propylbenzene, and 1,2,4- trimethylbenzene, were detected in sample TW1-SS1 at concentrations exceeding NCDENR IHSB Protection of Groundwater SRGs. • 1,2,4-Trimethylbenzene was detected in sample TW1-SS1 at a concentration exceeding the NCDENR IHSB Health-Based SRGs. • VOCs, n-butylbenzene, sec-butylbenzene, naphthalene, n-propylbenzene, and 1,2,4-trimethylbenzene, were detected in sample DUP3 at concentrations exceeding NCDENR IHSB Protection of Groundwater SRGs. • 1,2,4-Trimethylbenzene was detected in sample DUP3 at a concentration exceeding the NCDENR IHSB Health-Based SRGs. • 2-Methylnaphthalene, an SVOC, was detected at concentration exceeding the NCDENR IHSB Protection of Groundwater SRGs in sample TW1-SS1. • 2-Methylnaphthalene and naphthalene were detected at concentrations exceeding the NCDENR IHSB Protection of Groundwater SRGs in sample DUP3. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 13 • No exceedances of the NCDENR Action Limit of 250 mg/kg for O&G were detected. Groundwater • No exceedances of the NCAC 2L groundwater quality standards were detected 3.5 Former Petroleum Tank A gasoline tank was depicted south of the building onsite on the 1950 Sanborn Fire Insurance map, although the tank did not appear on later Sanborn maps The Sanborn maps did not distinguish between above-ground and underground tanks. The approximate location of the gasoline tank shown on the 1950 Sanborn map is depicted on Figure 2. Based on the gap in Sanborn map coverage, from 1925 to 1949 and 1951 to 1954, it is possible that this tank may have been located on the subject property for up to 27 years. 3.5.1 Soil Quality Temporary monitoring well TW-2 was installed in the suspected location of the former gasoline tank based on the 1950 Sanborn map. Two (2) soil samples were collected for laboratory analyses during completion of the well soil boring. One (1) soil sample (TW2-SS1) was collected from a depth interval 1.5 feet to 2.0 feet, immediately beneath the pavement system, to assess possible impacts to the near surface soils assuming that the tank was an AST. A second soil sample was collected from a depth interval 4.0 feet to 4.5 feet (immediately above the capillary zone) to assess impacts to the subsurface soils assuming that the tank was an UST. The collected soil samples were analyzed for VOCs and SVOCs. The following results were obtained (see Table 4 and Figure 4): VOCs • No VOCs, except benzene in soil sample TW2-SS1, were detected at concentrations in exceedance of the laboratory reporting limits. • There were no elevated detection limit issues, except the detection limit for benzene (0.215 mg/kg) in soil sample TW2-SS1 exceeded the NCDENR IHSB Protection of Groundwater SRGs (0.00562 mg/kg). SVOCs • No SVOCs were detected at concentrations in exceedance of the laboratory reporting limits. • There were no elevated detection limit issues, except the detection limit for benzo(a)anthracene in soil samples TW2-SS1 (0.400 mg/kg) and TW2-SS2 (0.355 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater and NCDENR IHSB Health-Based SRGs of 0.343 mg/kg and 0.15 mg/kg, respectively. 3.5.2 Groundwater Quality Temporary monitoring well TW-2 was installed to assess groundwater impacts from suspected petroleum releases from the former petroleum storage tank identified in the Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 14 1950 Sanborn map. The collected sample was submitted for analyses for VOCs and SVOCs. The following results were obtained (see Table 5 and Figure 5): VOCs • Seven (7) VOCs were detected in the sample. • There were no elevated detection limit issues. SVOCs • No SVOCs were detected in exceedance of the laboratory reporting limits. • There were no elevated detection limit issues. 3.5.3 Regulatory Standard/Goal Comparison Soil • Benzene was detected at 0.0063 mg/kg, which exceeded the NCDENR IHSB Protection of Groundwater SRG of 0.00562 mg/kg. Groundwater • One compound, benzene (4.9 μg/L), was detected at a concentration greater than its corresponding NCAC 2L groundwater quality standard (1 μg/L). 3.6 Fuel Loading Rack During the site reconnaissance for S&ME’s Phase I ESA, staining and discoloration of the soil/gravel was observed within the secondary containment area of the fuel loading rack. Observations made during our site reconnaissance suggested that pipe fittings leaked and spilled during fuel loading. The Site Manager stated that minor spills occurred at the loading rack when residual product spilled from the “arm” after use. 3.6.1 Soil Quality Temporary monitoring well TW-3 was installed adjacent to the fuel loading rack secondary containment area. The well was placed in an area contained oil dry residue. Two (2) soil samples were collected for laboratory analyses during completion of the well soil boring. One (1) soil sample (TW3-SS1) was collected from a depth interval 1.5 feet to 2.0 feet, immediately beneath the pavement system, to assess impacts to the near- surface soils as a result of spills at the fuel loading rack. A second soil sample (TW3- SS2) was collected from a depth interval of 3.5 feet to 4.5 feet (immediately above the capillary zone) to provide additional data regarding the vertical extent of contamination. A duplicate sample (DUP2) of TW3-SS2 was also collected. The collected soil samples were analyzed for VOCs and SVOCs. The following results were obtained (see Table 4 and Figure 4): VOCs • Two (2) VOCs (di-isopropyl ether and MTBE) were detected in the near- surface shallow soil sample (TW3-SS1). • No other VOCs were detected in sample TW3-SS1. • No VOCs were detected in the subsurface soil sample (TW3-SS2) at concentrations in exceedance of the laboratory reporting limits. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 15 • No VOCs were detected in the duplicate sample (DUP2) of TW3-SS2 in exceedance of the laboratory reporting limits. • There were no elevated detection limit issues, except the detection limits for benzene in sample TW3-SS2 (0.202 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater SRG for benzene (0.00562 mg/kg). SVOCs • Six (6) SVOCs were detected in the sample TW3-SS1. • No SVOCs were detected in sample TW3-SS2 at concentrations in exceedance of the laboratory reporting limits. • No SVOCs were detected in the duplicate sample (DUP2) of TW3-SS2 in exceedance of the laboratory reporting limits. • There were no elevated detection limit issues except the detection limit for benzo(a)anthracene in soil samples TW3-SS1 (0.369 mg/kg), TW3-SS2 (0.388 mg/kg), and DUP2 (0.400 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater and NCDENR IHSB Health-Based SRGs of 0.343 mg/kg and 0.15 mg/kg, respectively. 3.6.2 Regulatory Standard/Goal Comparison Soil • SVOCs, 2-methylnaphthalene and naphthalene, were detected in sample TW3-SS1 at concentrations exceeding the NCDENR IHSB Protection of Groundwater SRGs but less than NCDENR IHSB Health-Based SRGs. • There were no exceedances of the NCDENR IHSB Protection of Groundwater and the NCDENR IHSB Health-Based SRGs in samples TW3-SS1 and DUP 2. 3.7 Underground Petroleum Product Line Underground product lines exist beneath the paved area between the current AST area and the fuel loading rack. Priority Underground Locating Service, LLC., the private utility locating contractor, identified two (2) underground product lines connecting the storage tank area to the fuel loading rack. According to Priority Underground Locating Service, LLC, the product lines are approximately 2 feet bls. The approximate location of the product lines are indicated on Figure 4. 3.7.1 Soil Quality Two (2) soil borings (SB1 and SB2) were completed at locations between the two (2) product lines. One (1) soil sample was collected from each of the two (2) borings for laboratory analyses to assess whether the soil has been impacted by a release(s) of petroleum at the ground surface or at the product line. The soil samples were collected from a depth interval of 3.5 feet to 4.0 feet, approximately 1.5 feet below the product lines elevation. The collected soil samples were analyzed for VOCs and SVOCs. The following results were obtained (see Table 4 and Figure 4): VOCs Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 16 • Seven (7) VOCs were detected in sample (SB1) collected from soil boring SB1. • Eleven (11) VOCs were detected in sample (SB2) collected from soil boring SB2 (SB2). • There were no elevated detection limit issues, except the detection limit for benzene in soil sample SB2 (0.233 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater SRG (0.00562 mg/kg) for benzene. SVOCs • Three (3) SVOCs were detected in sample SB1. • Three (3) SVOCs were detected in sample SB2. • There were no elevation detection limit issues except the detection limit for benzo(a)anthracene in soil samples SB1 (0.391 mg/kg) and SB2 (0.375 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater SRG (0.343 mg/kg) and NCDENR IHSB Health-Based SRG (0.15 mg/kg). 3.7.2 Regulatory Standard/Goal Comparison Soil • VOCs, benzene and naphthalene, were detected in sample SB1 at concentrations exceeding the NCDENR IHSB Protection of Groundwater SRGs but less than NCDENR IHSB Health-Based SRGs. • VOCs, naphthalene, n-propylbenzene, 1,2,4-trimethylbenzene, and xylene, were detected in sample SB2 at concentrations that exceeded the NCDENR IHSB Protection of Groundwater SRGs. • The concentration of 1,2,4-trimethylbenzene in sample SB2 also exceeded the NCDENR IHSB Health-Based SRGs. • SVOCs, 2-Methylnaphthalene and naphthalene, concentrations that exceeded the NCDENR IHSB Protection of Groundwater SRGs but were less than NCDENR IHSB Health-Based SRGs were detected in samples SB1 and SB2. 3.8 Horizontal AST Area A secondary containment area is located on the northwest side of the building. This secondary containment area served as spill protection for three horizontal ASTs; one (1) 20,000 gallon premium gasoline, one (1) 20,000 gallon gasoline, and one (1) 20,000 gallon diesel. 3.8.1 Soil Quality Two (2) soil borings (SB3 and SB4) were performed to collect near-surface soil samples from within the containment area to assess the impacts of potential releases from the AST system. One (1) soil sample was collected from each boring from a depth interval of 0.5 feet to 1 feet bls. S&ME observed significant staining and petroleum odors from the soil sample collected from soil boring SB3. S&ME observed a slight petroleum odor from the soil sample collected from soil boring SB4. Both soil samples were analyzed for VOCs and SVOCs. The following results were obtained (see Table 4 and Figure 4): VOCs • Eleven (11) VOCs were detected in soil sample SB3. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 17 • Six (6) VOCs were detected in soil sample SB4. • There were no elevated detection limit issues, except the detection limit for benzene in soil sample SB3 (0.520 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater SRG (0.00562 mg/kg) for benzene. SVOCs • Three (3) SVOCs, 1-methylnaphthalene, 2-methylnaphthalene and naphthalene, were detected in soil sample SB3. • Nine (9) SVOCs were detected in soil sample SB4. • There were no elevated detection limit issues, except for benzo(a)anthracene in soil sample SB3 where the detection limit of 8.610 mg/kg exceeded the NCDENR IHSB Protection of Groundwater and NCDENR IHSB Health- Based SRGs of 0.343 mg/kg and 0.15 mg/kg, respectively. 3.8.2 Regulatory Standard/Goal Comparison Soil • Eight (8) of the following VOCs in soil sample SB3 exhibited concentrations that exceeded the NCDENR IHSB Protection of Groundwater SRGs: o n-butylbenzene, o sec-butylbenzene, o isopropylbenzene, o naphthalene, o n-propylbenzene, o 1,2,4-trimethylbenzene, o 1,3,5with benzene, and o naphthalene. • The concentrations of naphthalene and 1,2,4-trimethylbenzene in soil sample SB3 were greater than the NCDENR IHSB Health-Based SRG. • The concentrations of benzene, naphthalene, and xylene in soil sample SB4 were greater than the NCDENR IHSB Protection of Groundwater SRGs. • Benzene in soil sample SB4 was detected at a concentration that exceeded the NCDENR IHSB Health-Based SRG. • SVOCs, 2-Methylnaphthalene and naphthalene, were detected in soil sample SB3 at concentrations that exceeded the NCDENR IHSB Protection of Groundwater SRGs. (Note: 1-methylnaphthalene does not have a corresponding NCDENR IHSB Protection of Groundwater SRG) • 1-Methylnaphthalene and naphthalene were detected in soil sample SB3 at concentrations greater than the NCDENR IHSB Health-Based SRGs. • Benzo(a)anthracene and naphthalene were detected in soil sample SB4 at concentrations exceeding the NCDENR IHSB Protection of Groundwater SRGs and NCDENR IHSB Health-Based SRGs. • 2-Methylnaphthalene was detected in soil sample SB4 at a concentration greater than the NCDENR IHSB Protection of Groundwater SRGs. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 18 3.9 Vertical AST Area A second containment area is located on the northwest side of the building. This secondary containment area served as spill protection for four (4) large vertical ASTs and two (2) small horizontal ASTs. The vertical ASTs included one (1) 10,000 gallon varsol, one (1) 20,000 gallon kerosene, and two (2) 20,000 gallon #2 fuel oil tanks. The horizontal tanks included one (1) 550 gallon gasoline and one (1) 550 gallon overflow tanks. 3.9.1 Soil Quality Two (2) near surface soil samples within the vertical AST containment area were collected to assess impacts that spills from the ASTs had on the near-surface soils. During completion of the hand auger borings, S&ME discovered that this secondary containment area was covered with a concrete slab overlain with gravel. One (1) soil sample (SB4) was collected from within the secondary containment area from soil located above the concrete slab and slightly mixed with the gravel layer (see Figure 4). The collected sample had significant petroleum odors and staining. S&ME attempted the collected of soil sample SB5 in a similar fashion from four (4) locations within the containment area. The presence of the concrete slab and the lack of soil above the slab did not permit collection of a sample from within the secondary containment area. Therefore, soil boring SB6 was performed immediately outside of the containment area. Soil sample SB-6 was collected from this boring at a depth interval of 2 feet bls to 3 feet bls, in a soil layer below a layer of stone. Soil samples SB5 and SB6 were analyzed for VOCs and SVOCs. The following results were obtained (see Table 4 and Figure 4): VOCs • Eight (8) VOCs and ten (10) VOCs were detected in samples SB5 and SB6, respectively. • There were no elevated detection limit issues, except the detection limit for benzene in soil samples SB5 (1.060 mg/kg) and SB6 (0.233 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater SRG (0.00562 mg/kg) for benzene. SVOCs • No SVOCs were detected in soil sample SB5 at concentration greater than the laboratory reporting limits. • There were no elevation detection limit issues except the detection limit for benzo(a)anthracene in soil samples SB5 (0.351 mg/kg) and SB6 (7.760 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater SRG (0.343 mg/kg) and the NCDENR IHSB Health-Based SRG (0.15 mg/kg). 3.9.2 Regulatory Standard/Goal Comparison • VOCs, naphthalene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, and xylene, were detected at concentrations greater than the NCDENR IHSB Protection of Groundwater SRGs in soil sample SB5. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 19 • The detected concentration of 1,2,4-trimethylbenzene in soil sample SB5 also exceeded the NCDENR IHSB Health-Based SRG. • VOCs, n-butylbenzene, isopropylbenzene, naphthalene, n-propylbenzene, and 1,2,4-trimethylbenzene, were detected at concentrations greater than the NCDENR IHSB Protection of Groundwater SRGs in soil sample SB6. • The detected concentration of 1,2,4-trimethylbenzene in soil sample SB6 also exceeded the NCDENR IHSB Health-Based SRG. • 2-Methylnaphthalene was detected in soil sample SB6 at a concentration that exceeded the NCDENR IHSB Protection of Groundwater SRGs. 3.10 Elevated 55-Gallon Drum Two (2) storage tanks on stands were noted adjacent to one of the utility buildings during the site reconnaissance. One (1) of the tanks is a 55 gallon drum with a drain spout. A rubber hose with a fueling nozzle appears to have been formerly connected to the spout. Significant corrosion was noted along the weld that secures the top to the drum. The second tank appeared to be in fair condition with no signs of corrosion. 3.10.1 Soil Quality One (1) soil boring (SB7) was performed to collect a near-surface soil sample beneath the drum. One (1) soil sample (SB7) was collected from a depth interval of 1 feet to 2 feet from the soil boring to assess for the presence of petroleum contaminated soil beneath the drum. The collected soil sample was analyzed for VOCs and SVOCs. The following results were obtained (see Table 4 and Figure 4): VOCs • Ten (10) VOCs were detected in soil sample SB7. • There were no elevated detection issues. SVOCs • Four (4) SVOCs, benzoic acid, 1-methylnaphthalene, 2-methylnaphtahlene, and naphthalene, were detected in sample SB7. The benzoic acid, 1- methylnaphthalene, and naphthalene concentrations were reported as estimated values. • There were no elevation detection limit issues except the detection limit for benzo(a)anthracene (7.870 mg/kg) exceeded the NCDENR IHSB Protection of Groundwater SRG (0.343 mg/kg) and NCDENR IHSB Health-Based SRG (0.15 mg/kg). 3.10.2 Regulatory Standard/Goal Comparison • The detected VOCs did not exceed the NCDENR IHSB Protection of Groundwater and NCDENR IHSB Health-Based SRGs. • SVOC 2-methylnaphthalene exceeded the NCDENR IHSB Protection of Groundwater SRG. • The estimated concentration of naphthalene wass greater than the NCDENR IHSB Protection of Groundwater SRG. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 20 3.11 Coal Storage Area The subject property was operated as a coal yard for at least 37 years. Based on a review of the 1951, 1965, and 1975 aerial photographs of the site, mounds of coal were visible on the western portion of the property. This information suggested that the coal was historically stored in piles that were not covered. Leachate from coal can contain metals, such as, but not limited to, arsenic, aluminum, cadmium, chromium, copper, iron, lead, nickel, manganese, and mercury. These metals can leach into the soil and cause impacts to both soil and groundwater. 3.11.1 Soil Quality Soil samples SB8, SB9, SB10, and SB11 were collected from four (4) soil borings identified as SB8, SB9, SB10, and SB11 on Figure 4. One (1) soil sample was collected from each boring from a depth interval of 1.5 feet bls to 2.0 feet bls, immediately below the pavement system. The collected soil samples were analyzed for HSL Metals and SVOCs. Background soil sample BK1 was collected from soil boring BK1 shown on Figure 4 and was analyzed for HSL Metals. A duplicate soil sample of BK1 (DUP1) was collected. The following results were obtained (see Table 4 and Figure 4): HSL Metals • Nine (9) target metals (arsenic, beryllium, chromium, copper, lead, manganese, mercury, nickel, and zinc) were detected were detected in sample SB8. • Eleven target metals (antimony, arsenic, beryllium, cadmium, chromium, copper, lead, manganese, mercury, nickel, and zinc) were detected in sample SB9. • Ten (10) target metals (arsenic, beryllium, chromium, copper, lead, manganese, mercury, nickel, selenium, and zinc) were detected in sample SB10. • Twelve target metals (antimony, arsenic, beryllium, cadmium, chromium, copper, lead, manganese, mercury, nickel, selenium, and zinc) were detected in sample SB11. • Nine (9) target metals (arsenic, beryllium, chromium, copper, lead, manganese, mercury, nickel, and zinc) were detected in background samples BK1 and duplicate (DUP1). • There were no elevated detection limit issues. SVOCs • No SVOCs were detected in soil sample SB8. • Two (2) SVOCs, 2-methylnaphthalene and naphthalene, were detected in soil sample SB9. • One (1) SVOC, naphthalene, was detected in soil sample SB10. • 2-methylnaphthalene and naphthalene were detected in soil sample SB11. • There were no elevated detection issues except the detection limits for benzo(a)anthracene in soil samples SB8 (0.394 mg/kg), SB9 (0.380 mg/kg), SB10 (0.439 mg/kg), and SB11 (0.373 mg/kg) exceeded the NCDENR IHSB Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 21 Protection of Groundwater SRG (0.343 mg/kg) and NCDENR IHSB Health- Based SRG (0.15 mg/kg). 3.12 Regulatory Standard/Goal Comparison • In soil sample SB8, chromium, manganese, and mercury were detected at concentrations greater than the NCDENR IHSB Protection of Groundwater SRGs and the concentrations detected in background soil sample BK1. • Manganese and mercury were detected in soil sample SB9 at concentrations that exceeded the NCDENR IHSB Protection of Groundwater SRGs. The mercury concentration also exceeded the mercury concentration detected in background soil sample BK1. • Mercury was detected in soil sample SB10 at a concentration greater than the NCDENR IHSB Protection of Groundwater SRGs and significantly greater than the mercury concentration detected in background soil sample BK1. • Manganese and mercury were detected in soil sample SB11 at concentrations exceeding the NCDENR IHSB Protection of Groundwater SRGs. The mercury concentration also exceeded the mercury concentration detected in background soil sample BK1. • Arsenic was detected in soil samples SB9 (11.8 mg/kg), SB10 (10 mg/kg), and SB11 (7.1 mg/kg) at concentrations greater than the NCDENR IHSB Health-Based SRG of 4.4 mg/kg and the arsenic concentration detected in background soil sample BK1. According to the U.S. Geological Survey (USGS) Professional Paper 1648 Geochemical Landscapes of Conterminous United States-New Map Presentations for 22 Elements (http://pubs.usgs.gov/pp/p1648/p1648.pdf), arsenic has been documented in western North Carolina at concentrations from approximately 4.0 mg/kg to 7.0 mg/kg. The detected arsenic concentrations exceeded the range determined by the USGS paper. 3.13 Existing Monitoring Wells Approximately 3,000 gallons of fuel was spilled at the facility in 2003. The spill occurred when a worker for a petroleum delivery mistakenly left a valve open, which allowed the overflow tank to fill with product and eventually overflow. The spill was reported when free product was observed flowing in Sweeten Creek. From 2003 until 2007, free product recovery activities such as Aggressive Fluid Vapor Recovery and hand bailing were performed. Approximately 128 tons of contaminated soil was hauled offsite for disposal in 2003. The soil was excavated from within the secondary containment area and during the installation of three interceptor trenches. Assessment activities related to the soil suggested that other sources of contamination other than the 2003 spill may exist. Soil assessment activities were not performed due to the presence of concrete in the subsurface in the immediate vicinity of the secondary containment area. A fingerprinting evaluation performed on groundwater samples collected in November 2005 suggested that the petroleum in the samples originated from another source other Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 22 than the 2003 spill. Specifically, the source was considered to be an old diesel fuel or #2 fuel oil release and a gasoline release. Based on this information, NCDENR considered the 2003 spill to be remediated and issued a Notice of No Further Action in 2008 for the incident. However, the notice indicated that groundwater at the facility remained contaminated. 3.13.1 Groundwater Quality Free product was measured in monitoring well MW-4 using a disposal bailer at a thickness of approximately 1-in. Due to the presence of free product, a groundwater sample was not collected from monitoring well MW-4. Groundwater samples were collected from monitoring wells MW-1 and MW-2 to evaluate the groundwater quality in association with the 2003 release of heating oil. The collected groundwater samples were analyzed for VOCs and SVOCs. The following results were obtained (see Table 5 and Figure 5): VOCs • Two (2) VOCs, di-isopropyl ether and MTBE, were detected in the groundwater samples collected from MW-1 and MW-2. • No other VOCs were detected. • There were no elevated detection limit issues. SVOCs • No SVOCs were detected in the collected groundwater samples in exceedance of the laboratory reporting limits. • There were no elevated detection limit issues. 3.14 Soil Gas Assessment As was previously stated, HBVII wanted the option to use the existing onsite building for lease space. Due to the documented and suspected historical releases of petroleum materials at the site, NCDENR requested that two (2) soil gas samples be collected to evaluate the potential for petroleum vapors to be present in the building crawlspace. 3.14.1 Soil Gas Quality Soil gas samples were collected from locations SG1 and SG2 (see Figure 5), and a duplicate sample (DUP1) was collected from gas probe SG2. The collected gas samples were analyzed for VOCs and the following results were obtained (see Table 6 and Figure 5): VOCs • Seven (7) VOCs were detected in soil gas sample SG1. • Nine (9) VOCs were detected in soil gas sample SG2. • Eleven VOCs were detected in soil gas sample DUP1. • Elevated detection limits for several compounds were noted in soil gas samples SG1 and DUP1. • The detected concentrations in soil gas sample SG2 were significantly lower than the concentrations detected in its duplicate samples (DUP1). As noted in Section Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 23 3.3.3, the data from sample DUP1 were used to evaluate the soil gas conditions in the vicinity of probe SG2. 3.14.2 Regulatory Screening Comparison VOCs • Benzene, ethylbenzene, n-hexane, 1,3,4-trimethylbenzene, and m&p xylenes were detected in soil gas sample SG1 at concentrations that exceeded the NCDENR IHSB Industrial/Commercial Vapor Intrusion Screening levels. • None of the detected VOCs in sample SG2 were reported at concentrations greater than the NCDENR IHSB Industrial/Commercial Vapor Intrusion Screening levels. • Benzene, ethylbenzene, n-hexane, 1,2,4-trimethylbenzene, 1,3,4- trimethylbenzene, and m&p xylenes were detected in soil gas sample DUP1 at concentrations that exceeded the NCDENR IHSB Industrial/Commercial Vapor Intrusion Screening levels. 4. RECOMMENDATIONS It is our understanding that Historic Biltmore Village II, LLC is considering using the existing building as lease space and the open portion of the property as parking for the Biltmore Village area. The following summarizes our recommendations based on the data reported herein and the indicated intended use of the property. The recommendations following are strictly presented in association with the findings of our assessment of the soil, groundwater, soil gas at the site. 4.1 Petroleum Storage and Dispenser Equipment • The tanks, product lines, and fuel loading rack equipment should be removed and properly disposed of offsite by a contractor with the training and experience to perform such tasks. • Prior to removal of the tanks and product lines, the residual product and sludge should be removed and disposed of at a permitted facility. • All derived wastes generated during cleaning of the tanks, product lines, and fuel loading racks should be disposed of properly at a permitted facility. • Petroleum-contaminated soil that is encountered and excavated as part of the equipment removal activities should be properly characterized for offsite disposal and, then properly disposed of off-site. 4.2 Near-Surface Contaminated Soil Areas with petroleum contaminated soil should be covered (i.e., impervious via paving or buildings) and/or remained covered to protect human receptors from exposure and to reduce recharge that will facilitate the contamination of groundwater. If construction activities for the redevelopment warrant removal of the petroleum-contaminated soil, petroleum-stained concrete and/or -asphalt pavement, the materials should be properly Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 24 characterized and transported to an appropriate, permitted off-site disposal facility. Construction workers that will be excavating and loading the contaminated soil should be properly trained and informed according to applicable Occupational Health and Safety Administration (OSHA) regulations. 4.3 Existing Building/Soil Gas Based on the results of the soil gas samples collected adjacent to the existing building, the potential exists for the crawlspace to currently contain petroleum vapors that could be harmful to occupants of the building. Accordingly, an appropriate (i.e., NCDENR- approvable) soil gas/vapor intrusion mitigation system should be designed and specified to obviate this potential issue. 4.4 Groundwater Free product was detected in monitoring well MW-4 at a thickness of approximately 1-in. Data provided in Mountain’s March 2007 Product Recovery and Monitoring Report dated January 24, 2008, indicated that free product has historically been present in well MW-4 at thicknesses ranging from a sheen to 1.53 ft. While monitoring well MW-3 could not be located during our assessment, free product had historically been detected in this well at thicknesses ranging from a sheen to 0.55 ft. Free product was not detected in MW-3 and MW-4 during the final free product measurement event conducted in April 2007. It is our understanding, based on a review of the NCDENR documents related to the 2003 #2 fuel oil spill, that the incident was closed because the free product had been removed and the remaining dissolved contaminants appear to be from a source other than the 2003 spill. However, free product has reappeared in MW-4 and is likely associated with the 2003 spill. This suggests that the NFA issued by NCDENR on this event may be open for reconsideration. The data collected as part of this Brownfields assessment indicated that groundwater contamination exists beneath the fuel loading rack. Based on the distribution of groundwater contaminants at the site, the loading rack appeared to be source of petroleum-contaminated groundwater. The release appeared to be gasoline, based on the presence of MTBE and elevated concentrations of benzene in the groundwater sample. The source of this contamination was removed when operation of the petroleum distribution facility stopped in 2008. S&ME recommends that monitored natural attenuation (MNA) be employed as the approach for remediation of the groundwater in the vicinity of the fuel loading rack. Groundwater will not be used on the site for any purpose; therefore, the presence of the petroleum-contaminated groundwater will not impact future occupants of the property. Minimal groundwater contamination (benzene-4.9 μg/L) was noted in the vicinity of the former gasoline tank shown on the 1950 Sanborn map. S&ME recommends that MNA be employed to remediate this area of contamination. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 25 5. SOLE USE STATEMENT All materials and information used for this project were obtained by S&ME. This report is provided for the sole use of Historic Biltmore Village II, LLC, United States Environmental Protection Agency, and the North Carolina Department of Environment and Natural Resources for this project. Use of this report by any parties other than Historic Biltmore Village II, LLC, United States Environmental Protection Agency, and the North Carolina Department of Environment and Natural Resources will be at such party's sole risk. S&ME disclaims liability for any use of or reliance on this report by third parties. 6. LIMITATIONS The assessment described herein represents the environmental conditions of the property at the date the soil, groundwater, soil gas, were collected for laboratory analyses. The assessment data do not represent the future environmental conditions of the property and should not be construed in this manner. 7. REFERENCES Mountain Environmental Services. 2003. Comprehensive Site Assessment Report. December 30, 2003. Mountain Environmental Services. 2007. March 2007 Product Recovery and Monitoring Report. January 24, 2008. NCDENR-UST Section. 2008. Notice of No Further Action. February 21, 2008. (related to the 2003 spill) S&ME, Inc. 2009. Brownfields Area Reconnaissance and Receptor Survey. April 29, 2009. S&ME, Inc. 2009. Phase I Environmental Site Assessment. May 8, 2009. S&ME, Inc. 2009. Work Plan for Soil and Groundwater Assessment. July 21, 2009. S&ME, Inc. 2009. Quality Assurance Project Plan Soil and Groundwater Assessment. September 3, 2009. North Carolina Department of Environment of Natural Resources, Division of Waste Management, Underground Storage Tank Section. 2007. UST Section Guidelines for the Investigation and Remediation of Contamination from Non-UST Petroleum Releases. July 1, 2007. (http://www.wastenotnc.org/ust/docs/Non-USTGuid053107.pdf) North Carolina Department of Environment of Natural Resources, Division of Waste Management, Underground Storage Tank Section. 2008. Guidelines for Assessment and Corrective Action for UST Releases. July 15, 2008. (http://www.wastenotnc.org/ust/docs/aca_body.pdf) Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 26 U.S. Geological Survey. 2001. Geochemical Landscapes of Conterminous United States-New Map Presentations for 22 Elements. November 2001. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 TABLES Well IDInstallation DateWell Diameter (inches)Total Depth (ft below TOC)TOC Elevation1 (ft above datum)Ground Surface Elevation1 (ft above datum)Top of Screen Elevation (ft above datum)Bottom of Screen Elevation (ft above datum)Depth to Water from TOC (feet)9/9/2009 Free Product Thickness (feet)Groundwater Elevation (ft above datum)MW-1211/6/2003 2 8.44 99.39 100.00 96.95 90.95 5.86 0.00 93.53MW-2211/6/2003 2 9.20 99.72 100.19 96.52 90.52 7.46 0.00 92.26MW-3211/6/2003 2MW-4211/6/2003 2 12.33 102.54 99.95 96.21 90.21 11.35 0.10 91.19TW-19/8/200931 10.95 103.10 102.04 99.15 92.15 8.60 0.00 94.50TW-29/8/200931 10.17 102.37 101.18 100.20 92.20 8.18 0.00 94.19TW-39/8/200931 14.60 102.02 100.27 97.42 87.42 8.01 0.00 94.01Notes: TOC = Top of casing ft = feet 1Elevations provided based on relative datum established onsite 2Wells were installed by Mountain Environmental Services, Inc. 3Wells were abandoned by a NC Licensed Well Driller on September 24, 2009. Depth to groundwater measurements taken on 9-9-09 Corrected groundwater elevations were calculated using a specific gravity of 0.85 for heating oilWell Could Not Be LocatedS&ME Project No. 1411-09-040ATable 1Well Construction and Groundwater Elevation Data1 Fairview RoadAsheville, North Carolina Sample ID SG1 SG1 DUP1 Sample Date 9/9/2009 9/9/2009 9/9/2009 Canister Vacuum Readings Start -30 in. Hg -26 in.Hg -26 in.Hg Finish -14 in.Hg 0 in.Hg 0 in.Hg Notes: in.Hg = Inches of mercury 1Sample IDs actually use the following nomenclature; Example: Sample SG1 is acutally called 1Fair-SG1-09-09 in the laboratory reports. S&ME Project No. 1411-09-040A Table 2 Summary of Additional Field Data 1 Fairview Road Asheville, North Carolina Sample ID1Trip Blank 1 Trip Blank 2 Trip Blank 1 Trip Blank 2 Equipment Rinsate 1 Equipment Rinsate 1 Field BlankSample Date9/8/2008 9/8/2009 9/9/2009 9/9/2009 9/8/2009 9/8/2009 9/9/2009Sample Time----9:23 12:25 10:00Commentsw/ soil samples w/ soil samplesw/ groundwater samplesw/ groundwater sampleshand auger Macro-Core samplerVOCs (Method 8260)ND ND ND ND ND ND ND -SVOCs (Method 8270)NA NA NA NA ND ND ND -Notes: Concentrations reported in micrograms per liter (μg/L) Only detected analytes are reported in the table 1Sample IDs actually use the following nomenclature; Example: Sample Trip Blank 1 is acutally called 1Fair-TripBlank1-09-09 in the laboratory reports. ND = Not detected NA = Not analyzed NSE = No standard estabilished Concentrations in bold exceed the NCAC 2L Groundwater Quality Standards NCAC 2L Standards = North Carolina Groundwater Quality Standards - = Not applicableS&ME Project No. 1411-09-040ANCAC 2L StandardsTable 3Summary of Quality Control Analytical Data1 Fairview RoadAsheville, North Carolina Sample ID1SB1 SB2 SB3 SB4 SB5 SB6 SB7Sample Date9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009Sample Time12:15 12:20 9:20 9:25 9:30 11:00 11:10Sample Depth (ft bls)3.5 - 4 3.5 - 4 0.5 - 1 0.5 - 1 0.5 - 1 2 - 3 1 - 2VOCs (Method 8260)-Benzene0.251<0.233 <0.5201.350<1.060 <0.233 <0.0043 0.00562 1.1n-Butylbenzene <0.231 1.99019.200<0.356 <1.0604.3300.0357 4.31 NGEsec-Butylbenzene <0.231 0.39918.000<0.356 <1.060 2.870 0.0342 3.33 NGEEthylbenzene 0.431 3.580 4.560 <0.981 1.780 0.443 0.0121 4.57 5.7Isopropylbenzene 0.246 0.7006.950<0.356 <1.0601.6800.0152 1.68 NGEp-Isopropyltoluene <0.213 0.962 16.300 <0.356 2.640 4.450 0.0520 NSE NGENaphthalene1.580 2.350 22.100 2.950 3.700 5.8000.0121 0.585 3.9n-Propylbenzene 0.8512.780 10.700<0.356 1.4802.8400.0309 1.71 NGEToluene <0.213 0.270 1.160 7.120 1.140 <0.233 <0.0043 7.27 9301,2,4-Trimethylbenzene 0.25020.900 86.0001.92026.900 25.5000.159 7.49 131,3,5-Trimethylbenzene <0.213 5.47010.5000.5029.2402.860 0.0465 7.33 NGEXylene (total) 0.6968.700 8.470 8.260 14.9001.890 0.0849 4.96 120SVOCs (Method 8270)Anthracene <0.391 <0.375 <8.610 0.426 <0.351 <7.760 <7.870 995 3,400Benzo(a)anthracene <0.391 <0.375 <8.6100.628<0.351 <7.760 <7.870 0.343 0.15Benzoic Acid <1.950 <1.880 <43.000 <1.860 <1.75 <38.800 25.000 (J) 113 48,000Chrysene <0.391 <0.375 <8.610 0.607 <0.351 <7.760 <7.870 38.2 15Fluoranthene <0.391 <0.375 <8.610 0.494 <0.351 <7.760 <7.870 276 4601-Methylnaphthalene 8.840 1.28024.6006.590 <0.351 <7.760 6.840 (J) NSE 222-Methylnaphthalene15.800 2.350 32.500 9.310<0.3518.480 8.6601.72 62Naphthalene15.700 2.210 19.200 7.170<0.351 <7.7603.220 (J)0.585 3.9Phenanthrene <0.391 <0.375 <8.610 2.850 <0.351 <7.760 <7.870 59.6 NGEPyrene <0.391 <0.375 <8.610 0.743 <0.351 <7.760 <7.870 286 340Notes: Concentrations reported in milligrams per kilogram Only detected analytes are reported in the table 1Sample IDs actually use the following nomenclature; Example: Sample SB1 is acutally called 1Fair-SB1-09-09 in the laboratory reports VOCs = Volatile organic compounds SVOCs = Semi-volatile organic compounds ft bls = feet below land surface (J) = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit IHSB SRGs = Inactive Hazardous Sites Branch Health-Based Soil Remediation Goals NGE = No SRG established Concentrations in bold exceed exceed the corresponding Protection of Groundwater or Health-Based SRGsS&ME Project No. 1411-09-040AIHSB Protection of Groundwater SRGsIHSB SRGsTable 4Summary of Soil Analytical Data1 Fairview RoadAsheville, North Carolina 1 of 3 Sample ID1SB-8 SB-9 SB-10 SB-11 BK1 DUP1Sample Date9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009Sample Time11:40 11:30 11:25 11:20 11:55 (BK1)Sample Depth (ft bls)1.5' - 2' 1.5' - 2' 1.5' - 2' 1.5' - 2' 2.5 - 3 2.5 - 3Metals (Method 6010/7471)-Antimony <3.4 0.75 <0.59 1.3 <2.7 <2.3 5.42 6.2Arsenic 4.211.8 10 7.13.2 3.4 26.2 4.4Beryllium 1.1 0.36 0.23 2.1 0.61 0.59 3.38 32Cadmium <0.68 0.93 <0.12 0.25 <0.55 <0.46 0.95 14Chromium58.411.0 3.4 5.5 20.2 20.0 27.2 24,000*Copper 27.6 18.5 7.0 38.0 47.6 41.6 704 620Lead 11.0 34.7 13.0 24.9 65.6 103 270 400Manganese499 88.617.493.8 274 27765.2 360Mercury0.091 0.094 0.41 0.075 0.069 0.0490.015 1.3Nickel 12.4 6.4 3.0 10.2 14.1 12.9 56.4 320Selenium <6.8 <0.99 3.1 1.4 <5.5 <4.6 12.2 78Zinc 50.7 196 33.8 56.5 115 125 550 4,600SVOCs (Method 8270)Dibenzofuran <0.394 <0.380 <0.439 1.010 NA NA 4.66 NGE1-Methylnaphthalene <0.394 1.450 1.050 3.750 NA NA NSE 222-Methylnaphthalene <0.3941.7701.4104.580NA NA 1.72 62Naphthalene <0.3941.270 0.901 3.250NA NA 0.585 3.9Phenanthrene <0.394 0.662 <0.439 1.400 NA NA 59.6 NGEPyrene <0.394 0.450 <0.439 0.518 NA NA 286 340Notes: Concentrations reported in milligrams per kilogram Only detected analytes are reported in the table 1Sample IDs actually use the following nomenclature; Example: Sample SB8 is acutally called 1Fair-SB8-09-09 in the laboratory reports VOCs = Volatile organic compounds SVOCs = Semi-volatile organic compounds NA = Not analyzed ft bls = feet below land surface IHSB SRGs = Inactive Hazardous Sites Branch Health-Based Soil Remediation Goals NGE = No SRG established Concentrations in bold exceed exceed the corresponding Protection of Groundwater or Health-Based SRGs * Chromium IIIS&ME Project No. 1411-09-040AIHSB SRGsIHSB Protection of Groundwater SRGsTable 4Summary of Soil Analytical Data1 Fairview RoadAsheville, North Carolina 2 of 3 Sample ID1TW1-SS1 DUP3 TW2-SS1 TW2-SS2 TW3-SS1 TW3-SS2 DUP2Sample Date9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009 9/8/2009Sample Time13:05 (TW1-SS1) 13:15 13:20 12:40 12:45 (TW3-SS2)Sample Depth (ft bls)2.5' - 3.5' 2.5' - 3.5' 1.5' - 2.0' 4.0' - 4.5' 1.5' - 2.0' 3.5' - 4.5' 3.5' - 4.5'Oil & Grease (Method 9071)141 118 NA NA NA NA NA--250 250VOCs (Method 8260)Benzene <0.249 <0.2550.0063<0.215 <0.004 <0.202 <0.220 0.00562 1.1 - -n-Butylbenzene4.560 6.140<0.0049 <0.215 <0.004 <0.202 <0.220 4.31 NGE - -sec-Butylbenzene 3.0304.170<0.0049 <0.215 <0.004 <0.202 <0.220 3.33 NGE - -tert-Butylbenzene <0.249 <0.366 <0.0049 <0.215 <0.004 <0.202 <0.220 3.36 NGEDiisopropyl ether <0.249 <0.255 <0.0049 <0.215 0.0045 <0.202 <0.220 0.373 NGE - -Ethylbenzene 0.474 0.605 <0.0049 <0.215 <0.004 <0.202 <0.220 4.57 5.7 - -Isopropylbenzene 1.100 1.650 <0.0049 <0.215 <0.004 <0.202 <0.220 1.68 NGE - -p-Isopropyltoluene 5.800 4.670 <0.0049 <0.215 <0.004 <0.202 <0.220 NSE NGE - -Methyl tert-butyl ether <0.249 <0.255 <0.0049 <0.215 0.0106 <0.202 <0.220 0.916 39 - -Naphthalene5.250 5.140<0.0049 <0.215 <0.004 <0.202 <0.220 0.585 3.9 - -n-Propylbenzene2.000 2.700<0.0049 <0.215 <0.004 <0.202 <0.220 1.71 NGE - -1,2,4-Trimethylbenzene17.500 17.400<0.0049 <0.215 <0.004 <0.202 <0.220 7.49 13 - -1,3,5-Trimethylbenzene 4.940 7.320 <0.0049 <0.215 <0.004 <0.202 <0.220 7.33 NGE - -Xylene (total) 1.670 2.240 <0.0098 <0.429 <0.008 <0.403 <0.439 4.96 120 - -SVOCs (Method 8270)--Benzo(a)anthracene <8.460 <0.431 <0.400 <0.355 <0.369 <0.388 <0.400 0.343 0.15 - -Dibenzofuran <8.460 <0.431 <0.400 <0.355 0.699 <0.388 <0.400 4.66 NGE - -1-Methylnaphthalene 16.000 5.820 <0.400 <0.355 2.200 <0.388 <0.400 NSE 22 - -2-Methylnaphthalene12.200 8.830<0.400 <0.3553.060<0.388 <0.400 1.72 62 - -Naphthalene <8.4601.340<0.400 <0.3552.140<0.388 <0.400 0.585 3.9 - -Phenanthrene <8.460 1.660 <0.400 <0.355 1.140 <0.388 <0.400 59.6 NGE - -Pyrene <8.460 <0.431 <0.400 <0.355 0.640 <0.388 <0.400 286 340 - -Notes: Concentrations reported in milligrams per kilogram Only detected analytes are reported in the table 1Sample IDs actually use the following nomenclature; Example: Sample SB8 is acutally called 1Fair-SB8-09-09 in the laboratory reports VOCs = Volatile organic compounds SVOCs = Semi-volatile organic compounds NA = Not analyzed ft bls = feet below land surface IHSB SRGs = Inactive Hazardous Sites Branch Health-Based Soil Remediation Goals NCDENR Non-UST Action Levels = NC Department of Environment and Natural Resources, Division of Waste Manangement, UST Sectiion, Non-UST Action Levels NCDENR UST Action Levels = NC Department of Environment and Natural Resources, Division of Waste Manangement, UST Sectiion, UST Action Levels NGE = No SRG established Concentrations in bold exceed exceed the corresponding Protection of Groundwater or Health-Based SRGs, NCDENR UST Action Limit, or Non-UST Action LimitNCDENR UST Action LevelsS&ME Project No. 1411-09-040AIHSB SRGsIHSB Protection of Groundwater SRGsTable 4Summary of Soil Analytical Data1 Fairview RoadAsheville, North CarolinaNCDENR Non-UST Action Levels 3 of 3 Sample ID1TW-1 TW-2TW-3 Duplicate MW-1 MW-2Sample Date9/9/2009 9/9/2009 9/9/2009 9/9/2009 9/9/2009 9/9/2009Sample Time9:10 10:2011:15 (TW3)12:05 13:30VOCs (Method 8260)Benzene<14.9 1,870 1,220<1 <1 1Diisopropyl ether<1 2.5450 28432.2 19.8 70Ethylbenzene <1 3.4 282 220 <1 <1 550MTBE 3.3 4.9219138 6 3 200Naphthalene <1 8.985.2 82.2<1 <1 21Toluene <1 2.2 45.7 31.7 <1 <1 1000Xylene (total) <3 3.5831.2 578<3 <3 530SVOCs (Method 8270)1-Methylnaphthalene <12.3 <11.8 <13 15.6 <12 <12.8 NSE2-Methylnaphthalene 12.6 <11.818.4 27.5<12 <12.8 14Notes: Concentrations reported in micrograms per liter (μg/L) Only detected analytes are reported in the table 1Sample IDs actually use the following nomenclature; Example: Sample TW-1 is acutally called 1Fair-TW1-09-09 in the laboratory reports. NSE = No standard established Concentrations in bold exceed the NCAC 2L Groundwater Quality Standards NCAC 2L Standards = North Carolina Groundwater Quality StandardsS&ME Project No. 1411-09-040ANCAC 2L StandardsTable 5Summary of Groundwater Analytical Data1 Fairview RoadAsheville, North Carolina Sample ID1SG1SG22DUP1Sample Date9/9/2009 9/9/2009 9/9/2009Sample Time15:42 15:55 (SG2)VOCs (Method TO-15)Benzene3,52022.32,180160 31Cyclohexane38,000 825 49,700 NSE NSEEthylbenzene17,00031.92,810490 974-Ethyltoluene 24,900 45.9 3,470 NSE NSEn-Heptane <3990 <11.1 2,810 NSE NSEn-Hexane12,60039.13,2406,200 1,500Propylene <1680 <4.7 111 NSE NSEToluene <3710 51.3 <85 44,000 10,0001,2,4-Trimethylbenzene <12000 <33.52,31062 151,3,5-Trimethylbenzene14,50036.32,2105.2 13m&p-Xylene36,60064.95,180620* 150*o-Xylene <4240 33.6852620* 150*Notes: Concentrations reported in micrograms per cubic meter (μg/m3) VOCs = Volatile organic compounds by Method TO-15 Only detected analytes are reported in the table IIHSB = NCDENR Inactive Hazardous Sites Branch 1Sample IDs actually use the following nomenclature; Example: Sample SG1 is actually called 1Fair-SG1-09-09 in the laboratory report. 2The data for SG2 was not used in the analysis based on the QC analysis described in Section 3.3.3. 3IHSB Industrial/Commercial Vapor Instrusion Screening Levels for Soil Gas. Provided by Ms. Tracy Wahl with the NCDENR North Carolina Brownfields Program on October 2, 2009. 4IHSB Residential Vapor Instrusion Screening Levels for Soil Gas. Provided by Ms. Tracy Wahl with the NCDENR North Carolina Brownfields Program on October 2, 2009. *Screening values for xylene provided by Ms. Hana Assefa with the NCDENR IHSB on October 2, 2009. NSE = No screening value established Concentrations in bold exceed the IHSB Industrial/Commercial Soil Gas Screening LevelsIHSB Industrial/Commercial Soil Gas Screening Levels3IHSB Residential Soil Gas Screening Levels4S&ME Project No. 1411-09-040ATable 6Summary of Soil Gas Analytical Data1 Fairview RoadAsheville, North Carolina Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 FIGURES SCALE:As shownProject Location MapFIGURE NO.CHECKED BY: WHW1 Fairview RoadSource of Street Map: http://www.mapquest.com/ DRAWN BY:DRLAsheville, North CarolinaDATE:4/17/2009JOB NO.1411-09-040A1SUBJECT SITE A = 20,000 gal gasoline (premium) B = 20,000 gal gasoline C = 20,000 gal undyed diesel D = 10,000 gal varsol E = 20,000 gal kerosene F = 20,000 gal #2 fuel oil G = 20,000 gal #2 fuel oil H = 550 gal diesel (former) I = 550 gal gasoline J = 550 gal overflow tankNote: Property boundaries approximated for visualizationSCALE:As shownFIGURE NO.purposes only on a 2006 aerial photograph.CHECKED BYWHWSource of Aerial Photograph: Buncombe County GISDRAWN BY:DRLProperty Information SystemDATE:4/17/2009JOB NO.1411-09-040A2Site Plan1 Fairview RoadAsheville, North Carolina2APPROXIMATE SITE BOUNDARYSWEETEN CREEKDrum/pump storage & location of 3 former vertical 20,000 gallon ASTsLoading RackABCDEFGIHGasoline DispenserFormer Diesel DispenserFormer Motor Oil Drum Storage100 gallon AST55 gallon ASTMound of Used Oil DryJFormer gasoline tank based on 1950 Sanborn map. Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 APPENDIX I (WELL CONSTRUCTION LOGS) LEGENDDESCRIPTION STRATA ELEVATION(ft.)WELL DETAILS DEPTH(ft.)Diameter: Type: Interval: SEAL DRILLING CONTRACTOR: DRILLING METHOD: DATE DRILLED: LATITUDE: LONGITUDE: TOP OF CASING ELEVATION: DATUM: LOGGED BY: 0.010"PVC 3.0 - 10.0 1" PVC -1.06 - 3.0 CONCRETE SCREEN Gray Clayey FineSAND Saprolite: FP TSC TDSYMBOL2.00 3.00 10.00 WELL CONSTRUCTION DETAILS DEPTH(ft.)Bentonite0.0 - 2.0 Type: Interval: Type: Interval: TOP OF CASING GROUND SURFACEBENTONITE SEAL FILTER PACKTOP OF SCREENBOTTOM OF SCREEN TOTAL DEPTHCEMENT GROUT FILTER PACK BENTONITE CEMENT GROUT CUTTINGS / BACKFILL STATIC WATER LEVEL LEGEND 0 5 10 COMPLETION REPORT OF WELL No. TW-1 TOC GSBS FPTSCBSC TDCG MONITORING WELL WELL LOGS.GPJ S&ME.GDT 9/30/09Sheet 1 of 1 GS #2 Sand 2.0 - 10.0 FILTERPACK N. Currie 2 ¼" Macro-Core 9/8/09 Diameter: Type: Interval: 0.00 MSL S. Spinner RISER CASING GROUT Diameter: Type: Interval: Type: Interval: PROTECTIVE CASING COMPLETION REPORT OF WELL No. TW-1 PROJECT: PROJECT NO: PROJECT LOCATION: 1 Fairview Road Property1411-09-040A Asheville, North Carolina Sheet 1 of 1 7.54 feet BLS measured on 9/09/09. WATER LEVEL: LEGENDDESCRIPTION STRATA ELEVATION(ft.)WELL DETAILS DEPTH(ft.)Diameter: Type: Interval: SEAL DRILLING CONTRACTOR: DRILLING METHOD: DATE DRILLED: LATITUDE: LONGITUDE: TOP OF CASING ELEVATION: DATUM: LOGGED BY: 0.010"PVC 3.0 - 11.0 1" PVC -1.19 - 3.0 CONCRETE SCREEN Gray Clayey FineSAND Saprolite: FP TSC TDSYMBOL2.00 3.00 11.00 WELL CONSTRUCTION DETAILS DEPTH(ft.)Bentonite0.0 - 2.0 Type: Interval: Type: Interval: TOP OF CASING GROUND SURFACEBENTONITE SEAL FILTER PACKTOP OF SCREENBOTTOM OF SCREEN TOTAL DEPTHCEMENT GROUT FILTER PACK BENTONITE CEMENT GROUT CUTTINGS / BACKFILL STATIC WATER LEVEL LEGEND 0 5 10 COMPLETION REPORT OF WELL No. TW-2 TOC GSBS FPTSCBSC TDCG MONITORING WELL WELL LOGS.GPJ S&ME.GDT 9/30/09Sheet 1 of 1 GS #2 Sand 2.0 - 11.0 FILTERPACK N. Currie 2 ¼" Macro-Core 9/8/09 Diameter: Type: Interval: 0.00 MSL S. Spinner RISER CASING GROUT Diameter: Type: Interval: Type: Interval: PROTECTIVE CASING COMPLETION REPORT OF WELL No. TW-2 PROJECT: PROJECT NO: PROJECT LOCATION: 1 Fairview Road Property1411-09-040A Asheville, North Carolina Sheet 1 of 1 6.99 feet BLS measured on 9/09/09. WATER LEVEL: LEGENDDESCRIPTION STRATA ELEVATION(ft.)WELL DETAILS DEPTH(ft.)Diameter: Type: Interval: SEAL DRILLING CONTRACTOR: DRILLING METHOD: DATE DRILLED: LATITUDE: LONGITUDE: TOP OF CASING ELEVATION: DATUM: LOGGED BY: 0.010"PVC 3.0 - 13.0 1" PVC -1.75 - 3.0 CONCRETE SCREEN Gray Clayey FineSAND Saprolite: FP TSC TDSYMBOL2.00 3.00 13.00 WELL CONSTRUCTION DETAILS DEPTH(ft.)Bentonite0.0 - 2.0 Type: Interval: Type: Interval: TOP OF CASING GROUND SURFACEBENTONITE SEAL FILTER PACKTOP OF SCREENBOTTOM OF SCREEN TOTAL DEPTHCEMENT GROUT FILTER PACK BENTONITE CEMENT GROUT CUTTINGS / BACKFILL STATIC WATER LEVEL LEGEND 0 5 10 COMPLETION REPORT OF WELL No. TW-3 TOC GSBS FPTSCBSC TDCG MONITORING WELL WELL LOGS.GPJ S&ME.GDT 9/30/09Sheet 1 of 1 GS #2 Sand 2.0 - 13.0 FILTERPACK N. Currie 2 ¼" Macro-Core 9/8/09 Diameter: Type: Interval: 0.00 MSL S. Spinner RISER CASING GROUT Diameter: Type: Interval: Type: Interval: PROTECTIVE CASING COMPLETION REPORT OF WELL No. TW-3 PROJECT: PROJECT NO: PROJECT LOCATION: 1 Fairview Road Property1411-09-040A Asheville, North Carolina Sheet 1 of 1 6.26 feet BLS measured on 9/09/09. WATER LEVEL: Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 APPENDIX II (CLEAN CANISTER CERTIFICATION REPORT) Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 APPENDIX III (REGULATORY STANDARDS AND BENCHMARKS) UST SECTION GUIDELINES FOR THE INVESTIGATION AND REMEDIATION OF CONTAMINATION FROM NON-UST PETROLEUM RELEASES STATE of NORTH CAROLINA DEPARTMENT of ENVIRONMENT and NATURAL RESOURCES DIVISION of WASTE MANAGEMENT UST SECTION Effective July 1, 2007 12 5.0 Cleanup Requirements for Contaminated Soil The goal of soil restoration is to ensure that groundwater contamination does not occur or continue to occur. Table 1 outlines the required analytical methods for contaminated soil. In response to the need for a simple method for contaminant identification and to lower the cost of analysis, for the present time the UST Section will continue to allow the use of the TPH method analyses for suspected or known petroleum contamination. The TPH Action Levels are as follows: Analytical Method Action Level EPA Method 8015B 10 ppm TPH EPA Method 8015B 40 ppm TPH EPA Method 9071B (Oil & Grease) 250 ppm Oil & Grease In the event petroleum contaminated soil is located near the groundwater, the regional office for the UST Section may require analyses in addition to or in lieu of TPH. These additional requirements are outlined in Table 2, however you should contact the appropriate regional office to determine if they are necessary. Soil cleanup levels have been established for some commonly encountered compounds. The soil- to-groundwater maximum soil contaminant concentrations were established to protect groundwater from the leaching of contaminants in soil. Contaminated soil must be cleaned up to the soil-to-groundwater maximum contaminant concentrations. Contaminated soil clean- up levels are provided in Table 3. The most recent version of these cleanup levels may be downloaded from the Internet from the following web site address http://www.wastenotnc.org/ust/docs/tblmscc.pdf. The equations used by the Department to calculate the soil-to-groundwater maximum soil contaminant concentrations are provided in Figure 3. The soil organic carbon-water partition coefficients, soil-water partition coefficients and Henry’s Law Constants used to calculate the soil-to-groundwater maximum contaminant concentrations for organic and inorganic compounds were obtained from the following references: ß EPA, 1996. Soil Screening Guidance: Technical Background Document. (EPA/540/R95/128); ß EPA, 1986. Superfund Public Health Evaluation Manual. Office of Emergency and Remedial Response (EPA/540/1-86/060); ß Agency for Toxic Substances and Disease Registry, “Toxicological Profile for [individual chemical]. ” U.S. Public Health Service; ß Montgomery, J.H., 1996. Groundwater Chemicals Desk Reference. CRC Press, Inc.; ß Sims, R.C., J.L. Sims and S.G. Hansen, 1991. Soil Transport and Fate Database, Version 2.0. EPA Robert S. Kerr Environmental Laboratory; and ß Baes, C.F., III, R.D. Sharp, A.L. Sjoreen, and R.W. Shor, 1984. A Review and Analysis of Parameters for Assessing Transport of Environmentally Released Radionuclides through Agriculture. Oak Ridge National Laboratory; ß Other appropriate, published, peer-reviewed and scientifically valid data. INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 1 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Acephate* 30560-19-1 4.80E+01 N Acetaldehyde* 75-07-0 1.10E+05 1.10E+01 C Acetochlor 34256-82-1 2.40E+02 N Acetone 67-64-1 3 1.10E+05 1.20E+04 N Acetone Cyanohydrin 75-86-5 1.10E+05 4.00E+01 N Acetonitrile 75-05-8 1.30E+05 1.70E+02 N Acetophenone 98-86-2 3 2.30E+03 1.60E+03 N Acrolein 107-02-8 2.50E+04 3.20E-02 N Acrylamide* 79-06-1 1.10E-01 C Acrylic Acid 79-10-7 6.00E+03 N Acrylonitrile* 107-13-1 1.10E+04 2.40E-01 C Adiponitrile 111-69-3 1.70E+06 N Alachlor* 15972-60-8 2.40E+01 C ALAR 1596-84-5 1.80E+03 N Aldicarb 116-06-3 1.20E+01 N Aldicarb Sulfone 1646-88-4 1.20E+01 N Aldrin* 309-00-2 2.90E-02 C Ally 74223-64-6 3.00E+03 N Allyl Alcohol 107-18-6 6.20E+01 N Allyl Chloride 107-05-1 1.50E+03 3.60E-01 N Aluminum 7429-90-5 1.50E+04 N Aluminum Phosphide 20859-73-8 6.20E+00 N Amdro 67485-29-4 3.60E+00 N Ametryn 834-12-8 1.10E+02 N Aminophenol, m- 591-27-5 9.80E+02 N Aminophenol, p- 123-30-8 2.40E+02 N Amitraz 33089-61-1 3.00E+01 N Ammonia 7664-41-7 2.80E+07 N Ammonium Perchlorate 7790-98-9 1.10E+01 N Ammonium Sulfamate 7773-06-0 3.20E+03 N Aniline* 62-53-3 8.50E+01 C Antimony (metallic) 7440-36-0 6.20E+00 N Antimony Pentoxide 1314-60-9 7.80E+00 N Antimony Potassium Tartrate 304-61-0 1.40E+01 N Antimony Tetroxide 1332-81-6 6.20E+00 N Antimony Trioxide 1309-64-4 6.20E+00 N Apollo 74115-24-5 1.60E+02 N Aramite* 140-57-8 1.90E+01 C Arsenic, Inorganic* 7440-38-2 2 4.40E+00 N Arsine 7784-42-1 1.40E+04 N Assure 76578-14-8 1.10E+02 N Asulam 3337-71-1 6.20E+02 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 2 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Atrazine* 1912-24-9 2.10E+00 C Avermectin B1 65195-55-3 4.80E+00 N Azobenzene 103-33-3 4.90E+00 C Barium 7440-39-3 3.00E+03 N Baygon 114-26-1 4.80E+01 N Bayleton 43121-43-3 3.60E+02 N Baythroid 68359-37-5 3.00E+02 N Benefin 1861-40-1 3.60E+03 N Benomyl 17804-35-2 6.20E+02 N Bentazon 25057-89-0 3.60E+02 N Benzaldehyde 100-52-7 3 1.90E+03 1.60E+03 N Benzene* 71-43-2 2.00E+03 1.10E+00 C Benzenethiol 108-98-5 1.40E+03 1.60E-01 N Benzidine 92-87-5 5.00E-04 C,M Benzoic Acid 65-85-0 4.80E+04 N Benzotrichloride 98-07-7 1.60E+02 4.90E-02 C Benzyl Alcohol 100-51-6 6.20E+03 N Benzyl Chloride 100-44-7 6.40E+01 3.80E+00 C Beryllium and compounds 7440-41-7 3.20E+01 N Bidrin 141-66-2 1.20E+00 N Bifenox 42576-02-3 1.10E+02 N Biphenthrin 82657-04-3 1.80E+02 N Biphenyl, 1,1'- 92-52-4 2.60E+02 2.60E+02 Csat Bis(2-chloroethoxy)methane 111-91-1 3.60E+01 N Bis(2-chloroethyl)ether 111-44-4 3.30E+03 1.90E-01 C Bis(2-chloro-1-methylethyl) ether 108-60-1 5.70E+02 3.50E+00 C Bis(2-ethylhexyl)phthalate* 117-81-7 3.50E+01 C Bis(chloromethyl)ether 542-88-1 2.80E+03 2.70E-04 C Bisphenol A 80-05-7 6.20E+02 N Boron And Borates Only 7440-42-8 3.20E+03 N Boron Trifluoride 7637-07-2 2.00E+05 N Bromate* 15541-45-4 9.10E-01 C Bromodichloromethane* 75-27-4 9.90E+02 1.00E+01 C Bromoform* 75-25-2 6.10E+01 C Bromomethane 74-83-9 3.60E+03 1.60E+00 N Bromophos 2104-96-3 6.20E+01 N Bromoxynil 1689-84-5 2.40E+02 N Bromoxynil Octanoate 1689-99-2 2.40E+02 N Butadiene, 1,3-* 106-99-0 6.90E+02 7.70E-02 C Butanol, N- 71-36-3 1.20E+03 N Butyl Benzyl Phthlate 85-68-7 2.60E+02 C Butylate 2008-41-5 6.20E+02 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 3 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Butylphthalyl Butylglycolate 85-70-1 1.20E+04 N Cacodylic Acid 75-60-5 2.40E+02 N Cadmium (Diet) 7440-43-9 1.40E+01 N Caprolactam 105-60-2 6.20E+03 N Captafol* 2425-06-1 3.20E+00 C Captan* 133-06-2 2.10E+02 C Carbaryl 63-25-2 1.20E+03 N Carbazole 86-74-8 2.40E+01 C Carbofuran 1563-66-2 6.20E+01 N Carbon Disulfide 75-15-0 3 2.60E+02 1.30E+02 N Carbon Tetrachloride* 56-23-5 4.80E+02 2.50E-01 C Carbosulfan 55285-14-8 1.20E+02 N Carboxin 5234-68-4 1.20E+03 N Chloral Hydrate 302-17-0 1.20E+03 N Chloramben 133-90-4 1.80E+02 N Chloranil 118-75-2 1.20E+00 C Chlordane* 57-74-9 1.60E+00 C Chlordecone (Kepone) 143-50-0 3.00E-02 C Chlorimuron, Ethyl- 90982-32-4 2.40E+02 N Chlorine 7782-50-5 1.50E+03 N Chlorine Dioxide 10049-04-4 4.60E+02 N Chlorite (Sodium Salt) 7758-19-2 4.60E+02 N Chloro-1,1-difluoroethane, 1- 75-68-3 1.20E+03 1.20E+03 Csat Chloro-1,3-butadiene, 2- 126-99-8 8.20E+02 1.70E+00 N Chloro-2-methylaniline HCl, 4- 3165-93-3 1.10E+00 C Chloro-2-methylaniline, 4- 95-69-2 1.80E+00 C Chloroacetic Acid 79-11-8 2.40E+01 N Chloroacetophenone, 2- 532-27-4 8.60E+03 N Chloroaniline, p- 106-47-8 4.80E+01 N Chlorobenzene 108-90-7 8.60E+02 9.00E+00 C Chlorobenzilate* 510-15-6 4.40E+00 C Chlorobenzotrifluoride, 4- 98-56-6 5.50E+02 4.20E+01 N Chlorobutane, 1- 109-69-3 3 7.90E+02 6.20E+02 N Chlorodifluoromethane 75-45-6 1.70E+03 1.70E+03 Csat Chloroform 67-66-3 2.70E+03 3.00E-01 C Chloromethane* 74-87-3 1.40E+03 1.70E+00 C Chloronaphthalene, Beta- 91-58-7 2.10E+02 2.10E+02 Csat Chlorophenol, 2- 95-57-8 7.90E+04 7.80E+01 N Chlorothalonil* 1897-45-6 1.60E+02 C Chlorotoluene, o- 95-49-8 3 1.00E+03 3.20E+02 N Chlorotoluene, p- 106-43-4 2.90E+02 2.90E+02 Csat Chlorpropham 101-21-3 2.40E+03 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 4 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Chlorpyrifos 2921-88-2 3.60E+01 N Chlorpyrifos Methyl 5598-13-0 1.20E+02 N Chlorsulfuron 64902-72-3 6.20E+02 N Chlorthiophos 60238-56-4 9.80E+00 N Chromium (III) (Insoluble Salts) 16065-83-1 2.40E+04 N Chromium VI (particulates) 18540-29-9 4.60E+01 N Copper 7440-50-8 6.20E+02 N Cresol, m- 108-39-4 6.20E+02 N Cresol, o- 95-48-7 6.20E+02 N Cresol, p- 106-44-5 6.20E+01 N Crotonaldehyde, trans- 123-73-9 2.40E+04 3.40E-01 C Cumene 98-82-8 3.10E+02 3.10E+02 Csat Cyanazine* 21725-46-2 5.80E-01 C Cyanides Calcium Cyanide 592-01-8 6.20E+02 N Copper Cyanide 544-92-3 7.80E+01 N Cyanide (CN-) 57-12-5 3.20E+02 N Cyanogen 460-19-5 6.20E+02 N Cyanogen Bromide 506-68-3 1.40E+03 N Cyanogen Chloride 506-77-4 7.80E+02 N Hydrogen Cyanide 74-90-8 3.20E+02 N Potassium Cyanide 151-50-8 7.80E+02 N Potassium Silver Cyanide 506-61-6 3.20E+03 N Silver Cyanide 506-64-9 1.60E+03 N Sodium Cyanide 143-33-9 6.20E+02 N Thiocyanate 463-56-9 5.60E+03 3.20E+00 N Zinc Cyanide 557-21-1 7.80E+02 N Cyclohexane 110-82-7 1.20E+02 1.20E+02 Csat Cyclohexane, 1,2,3,4,5-pentabromo-6-chloro- 87-84-3 2.10E+01 C Cyclohexanone 108-94-1 6.20E+04 N Cyclohexylamine 108-91-8 2.40E+03 N Cyhalothrin/karate 68085-85-8 6.20E+01 N Cypermethrin 52315-07-8 1.20E+02 N Cyromazine 66215-27-8 9.20E+01 N Dacthal 1861-32-1 1.20E+02 N Dalapon 75-99-0 3.60E+02 N DDD 72-54-8 2.00E+00 C DDE, p,p'- 72-55-9 1.40E+00 C DDT* 50-29-3 1.70E+00 C Decabromodiphenyl Ether 1163-19-5 8.60E+01 N Demeton 8065-48-3 4.80E-01 N Di(2-ethylhexyl)adipate* 103-23-1 4.00E+02 C October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 5 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Diallate 2303-16-4 8.00E+00 C Diazinon 333-41-5 1.10E+01 N Dibromo-3-chloropropane, 1,2- 96-12-8 1.10E+03 5.60E-03 C Dibromobenzene, 1,4- 106-37-6 1.20E+02 N Dibromochloromethane* 124-48-1 8.50E+02 5.80E+00 C Dibromoethane, 1,2- 106-93-4 1.40E+03 3.40E-02 C Dibromomethane (Methylene Bromide) 74-95-3 3.00E+03 1.60E+02 N Dibutyl Phthalate 84-74-2 1.20E+03 N Dibutyltin Compounds NA 3.60E+00 N Dicamba 1918-00-9 3.60E+02 N Dichloro-2-butene, 1,4- 764-41-0 6.10E+02 3.20E-03 C Dichloroacetic Acid* 79-43-6 9.70E+00 N Dichlorobenzene, 1,2- 95-50-1 2.20E+02 2.20E+02 Csat Dichlorobenzene, 1,4- 106-46-7 2.60E+00 C Dichlorobenzidine, 3,3'- 91-94-1 1.10E+00 C Dichlorodifluoromethane 75-71-8 8.50E+02 3.80E+01 N Dichloroethane, 1,1-* 75-34-3 1.80E+03 3.40E+00 C Dichloroethane, 1,2- 107-06-2 1.90E+03 4.50E-01 C Dichloroethylene, 1,1- 75-35-4 1.20E+03 5.00E+01 N Dichloroethylene, 1,2- (Mixed Isomers) 540-59-0 1.40E+03 1.40E+02 N Dichloroethylene, 1,2-cis- 156-59-2 1.40E+03 1.60E+02 N Dichloroethylene, 1,2-trans- 156-60-5 1.50E+03 2.20E+01 N Dichlorophenol, 2,4- 120-83-2 3.60E+01 N Dichlorophenoxy Acetic Acid, 2,4- 94-75-7 1.40E+02 N Dichlorophenoxy)butyric Acid, 4-(2,4- 94-82-6 9.80E+01 N Dichloropropane, 1,2-* 78-87-5 1.50E+03 9.30E-01 C Dichloropropane, 1,3- 142-28-9 3 1.60E+03 3.20E+02 N Dichloropropanol, 2,3- 616-23-9 3.60E+01 N Dichloropropene, 1,3-* 542-75-6 1.70E+03 1.70E+00 C Dichlorvos* 62-73-7 1.70E+00 C Dicyclopentadiene 77-73-6 5.90E+02 5.80E+00 N Dieldrin* 60-57-1 3.00E-02 C Diethyl Phthalate 84-66-2 9.80E+03 N Diethylformamide 617-84-5 1.20E+01 N Diethylstilbestrol 56-53-1 1.40E-03 C Difenzoquat 43222-48-6 9.80E+02 N Diflubenzuron 35367-38-5 2.40E+02 N Difluoroethane, 1,1- 75-37-6 1.50E+03 1.50E+03 Csat Diisopropyl Methylphosphonate 1445-75-6 4.30E+02 4.30E+02 Csat Dimethipin 55290-64-7 2.40E+02 N Dimethoate 60-51-5 2.40E+00 N Dimethoxybenzidine, 3,3'- 119-90-4 3.50E+01 C October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 6 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Dimethyl methylphosphonate* 756-79-6 2.90E+02 C Dimethylaniline HCl, 2,4- 21436-96-4 8.40E-01 C Dimethylaniline, 2,4- 95-68-1 6.50E-01 C Dimethylaniline, N,N- 121-69-7 8.20E+02 3.20E+01 N Dimethylformamide 68-12-2 1.20E+03 N Dimethylphenol, 2,4- 105-67-9 2.40E+02 N Dimethylphenol, 2,6- 576-26-1 7.40E+00 N Dimethylphenol, 3,4- 95-65-8 1.20E+01 N Dimethylterephthalate 120-61-6 6.10E+00 6.10E+00 Csat Dinitro-o-cyclohexyl Phenol, 4,6- 131-89-5 2.40E+01 N Dinitrobenzene, 1,2- 528-29-0 1.20E+00 N Dinitrobenzene, 1,3- 99-65-0 1.20E+00 N Dinitrobenzene, 1,4- 100-25-4 1.20E+00 N Dinitrophenol, 2,4- 51-28-5 2.40E+01 N Dinitrotoluene Mixture, 2,4/2,6-* 25321-14-6 7.10E-01 C Dinitrotoluene, 2,4- 121-14-2 2.40E+01 N Dinitrotoluene, 2,6- 606-20-2 1.20E+01 N Dinitrotoluene, 2-Amino-4,6- 35572-78-2 3.00E+01 N Dinitrotoluene, 4-Amino-2,6- 19406-51-0 3.00E+01 N Dinoseb 88-85-7 1.20E+01 N Dioxane, 1,4- 123-91-1 4.40E+01 C Dioxins 4 Hexachlorodibenzo-p-dioxin 34465-46-8 4.50E-05 C Hexachlorodibenzo-p-dioxin, Mixture NA 9.40E-05 C HpCDD, 2,3,7,8- 37871-00-4 4.50E-04 C OCDD 3268-87-9 1.50E-02 C PeCDD, 2,3,7,8- 36088-22-9 4.50E-06 C TCDD, 2,3,7,8-* 1746-01-6 4.50E-06 C Diphenamid 957-51-7 3.60E+02 N Diphenylamine 122-39-4 3.00E+02 N Diphenylhydrazine, 1,2- 122-66-7 6.10E-01 C Diquat 85-00-7 2.60E+01 N Direct Black 38 1937-37-7 6.60E-02 C Direct Blue 6 2602-46-2 6.60E-02 C Direct Brown 95 16071-86-6 7.20E-02 C Disulfoton 298-04-4 4.80E-01 N Dithiane, 1,4- 505-29-3 1.20E+02 N Diuron 330-54-1 2.40E+01 N Dodine 2439-10-3 4.80E+01 N Endosulfan 115-29-7 7.40E+01 N Endothall 145-73-3 2.40E+02 N Endrin 72-20-8 3.60E+00 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 7 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Epichlorohydrin 106-89-8 8.40E+03 3.60E+00 N Epoxybutane, 1,2- 106-88-7 1.20E+04 3.00E+01 N EPTC3 759-94-4 6.20E+02 4.00E+02 N Ethephon 16672-87-0 6.20E+01 N Ethion 563-12-2 6.20E+00 N Ethoxyethanol Acetate, 2- 111-15-9 3.60E+03 N Ethoxyethanol, 2- 110-80-5 4.80E+04 N Ethyl Acetate 141-78-6 1.10E+04 1.10E+04 Csat Ethyl Acrylate 140-88-5 2.60E+03 1.30E+01 C Ethyl Chloride 75-00-3 2.20E+03 2.20E+03 Csat Ethyl Ether3 60-29-7 8.20E+03 3.20E+03 N Ethyl Methacrylate 97-63-2 1.20E+03 1.20E+03 Csat Ethyl-p-nitrophenyl Phosphonate 2104-64-5 1.20E-01 N Ethylbenzene3 100-41-4 5.50E+02 5.70E+00 C Ethylene Cyanohydrin 109-78-4 3.60E+02 N Ethylene Diamine 107-15-3 1.10E+03 N Ethylene Glycol 107-21-1 2.40E+04 N Ethylene Glycol Monobutyl Ether 111-76-2 6.20E+03 N Ethylene Oxide 75-21-8 1.10E+05 1.60E-01 C Ethylene Thiourea 96-45-7 9.80E-01 N Ethylphthalyl Ethyl Glycolate 84-72-0 3.60E+04 N Express 101200-48-0 9.80E+01 N Fenamiphos 22224-92-6 3.00E+00 N Fenpropathrin 39515-41-8 3.00E+02 N Fluometuron 2164-17-2 1.60E+02 N Fluorine (Soluble Fluoride) 7782-41-4 9.40E+02 N Fluridone 59756-60-4 9.80E+02 N Flurprimidol 56425-91-3 2.40E+02 N Flutolanil 66332-96-5 7.40E+02 N Fluvalinate 69409-94-5 1.20E+02 N Folpet* 133-07-3 1.40E+02 C Fomesafen 72178-02-0 2.60E+00 C Fonofos 944-22-9 2.40E+01 N Formaldehyde 50-00-0 2.40E+03 N Formic Acid 64-18-6 2.40E+04 N Fosetyl-AL 39148-24-8 3.60E+04 N Furans 4 Furan 110-00-9 6.80E+03 1.60E+01 N HpCDF, 2,3,7,8- 38998-75-3 3.70E-04 C HxCDF, 2,3,7,8- 55684-94-1 3.70E-05 C OCDF 39001-02-0 1.20E-02 C PeCDF, 1,2,3,7,8- 57117-41-6 1.20E-04 C October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 8 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 PeCDF, 2,3,4,7,8- 57117-31-4 1.20E-05 C TCDF, 2,3,7,8- 51207-31-9 3.70E-05 C Furazolidone 67-45-8 1.30E-01 C Furfural 98-01-1 3.60E+01 N Furium 531-82-8 3.20E-01 C Furmecyclox 60568-05-0 1.60E+01 C Glufosinate, Ammonium 77182-82-2 4.80E+00 N Glycidyl 765-34-4 4.80E+00 N Glyphosate 1071-83-6 1.20E+03 N Goal 42874-03-3 3.60E+01 N Haloxyfop, Methyl 69806-40-2 6.20E-01 N Harmony 79277-27-3 1.60E+02 N Heptachlor* 76-44-8 1.10E-01 C Heptachlor Epoxide* 1024-57-3 5.30E-02 C Hexabromobenzene 87-82-1 2.40E+01 N Hexachlorobenzene* 118-74-1 3.00E-01 C Hexachlorobutadiene* 87-68-3 6.20E+00 C Hexachlorocyclohexane, Alpha- 319-84-6 7.70E-02 C Hexachlorocyclohexane, Beta- 319-85-7 2.70E-01 C Hexachlorocyclohexane, Gamma- (Lindane)* 58-89-9 5.20E-01 C Hexachlorocyclohexane, Technical 608-73-1 2.70E-01 C Hexachlorocyclopentadiene 77-47-4 7.40E+01 N Hexachloroethane 67-72-1 1.20E+01 N Hexachlorophene 70-30-4 3.60E+00 N Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX)* 121-82-4 5.50E+00 C Hexamethylene Diisocyanate, 1,6- 822-06-0 4.10E+03 7.40E-01 N Hexane, N-3 110-54-3 1.40E+02 1.10E+02 N Hexanedioic Acid 124-04-9 2.40E+04 N Hexazinone 51235-04-2 4.00E+02 N Hydrazine 302-01-2 2.10E-01 C Hydrazine Sulfate 10034-93-2 2.10E-01 C Hydrogen Chloride 7647-01-0 5.60E+06 N Hydrogen Sulfide 7783-06-4 5.60E+05 N Imazalil 35554-44-0 1.60E+02 N Imazaquin 81335-37-7 3.00E+03 N Iprodione 36734-19-7 4.80E+02 N Iron 7439-89-6 1.10E+04 N Isobutyl Alcohol3 78-83-1 9.60E+03 4.60E+03 N Isophorone* 78-59-1 5.10E+02 C Isopropalin 33820-53-0 1.80E+02 N Isopropyl Methyl Phosphonic Acid 1832-54-8 1.20E+03 N Isoxaben 82558-50-7 6.20E+02 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 9 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Kerb 23950-58-5 9.20E+02 N Lactofen 77501-63-4 2.40E+01 N Lead Compounds Lead and Compounds 7439-92-1 5 4.00E+02 Tetraethyl Lead 78-00-2 1.20E-03 N Linuron 330-55-2 2.40E+01 N Lithium Perchlorate 7791-03-9 1.10E+01 N Londax 83055-99-6 2.40E+03 N Malathion 121-75-5 2.40E+02 N Maleic Anhydride 108-31-6 1.20E+03 N Maleic Hydrazide 123-33-1 6.20E+03 N Malononitrile 109-77-3 1.20E+00 N Mancozeb 8018-01-7 3.60E+02 N Maneb 12427-38-2 6.20E+01 N Manganese (Water) 7439-96-5 3.60E+02 N MCPA 94-74-6 6.20E+00 N MCPB 94-81-5 1.20E+02 N MCPP 93-65-2 1.20E+01 N Mephosfolan 950-10-7 1.10E+00 N Mepiquat Chloride 24307-26-4 3.60E+02 N Mercury Compounds Mercuric Chloride 7487-94-7 4.60E+00 N Mercuric Sulfide 1344-48-5 4.60E+00 N Mercury (elemental) 7439-97-6 3 3.10E+00 1.30E+00 N Mercury, Inorganic Salts NA 4.60E+00 N Methyl Mercury 22967-92-6 1.60E+00 N Phenylmercuric Acetate 62-38-4 9.80E-01 N Merphos 150-50-5 3.60E-01 N Merphos Oxide 78-48-8 3.60E-01 N Metalaxyl 57837-19-1 7.40E+02 N Methacrylonitrile 126-98-7 4.50E+03 6.40E-01 N Methamidophos 10265-92-6 6.20E-01 N Methanol 67-56-1 6.20E+03 N Methidathion 950-37-8 1.20E+01 N Methomyl 16752-77-5 3.00E+02 N Methoxy-5-nitroaniline, 2- 99-59-2 9.90E+00 C Methoxychlor 72-43-5 6.20E+01 N Methoxyethanol Acetate, 2- 110-49-6 2.40E+01 N Methoxyethanol, 2- 109-86-4 3.60E+01 N Methyl Acetate 79-20-9 3 2.90E+04 1.60E+04 N Methyl Acrylate 96-33-3 6.90E+03 4.60E+02 N Methyl Ethyl Ketone (2-Butanone) 78-93-3 3 2.80E+04 5.60E+03 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 10 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 108-10-1 3 3.20E+03 1.10E+03 N Methyl Methacrylate 80-62-6 3 2.50E+03 9.40E+02 N Methyl Parathion 298-00-0 3.00E+00 N Methyl Styrene (Mixed Isomers) 25013-15-4 4.50E+02 3.80E+01 N Methyl tert-Butyl Ether (MTBE)* 1634-04-4 3 6.90E+03 3.90E+01 C Methyl-5-Nitroaniline, 2- 99-55-8 1.50E+01 C Methylaniline Hydrochloride, 2- 636-21-5 3.70E+00 C Methylarsonic acid 124-58-3 1.20E+02 N Methylene Chloride* 75-09-2 3.50E+03 1.10E+01 C Methylene-bis(2-chloroaniline), 4,4'-* 101-14-4 M 1.20E+00 C Methylene-bis(N,N-dimethyl) Aniline, 4,4'- 101-61-1 1.10E+01 C Methylenebisbenzenamine, 4,4'- 101-77-9 3.00E-01 C Methylenediphenyl Diisocyanate 101-68-8 1.70E-05 N Methylstyrene, Alpha- 98-83-9 4.50E+02 4.50E+02 Csat Metolachlor 51218-45-2 1.80E+03 N Metribuzin 21087-64-9 3.00E+02 N Mirex* 2385-85-5 2.70E-02 C Molinate 2212-67-1 2.40E+01 N Molybdenum 7439-98-7 7.80E+01 N Monochloramine 10599-90-3 1.60E+03 N Monomethylaniline 100-61-8 2.40E+01 N N,N'-Diphenyl-1,4-benzenediamine 74-31-7 3.60E+00 N Naled 300-76-5 2.40E+01 N Napropamide 15299-99-7 1.20E+03 N Nickel Refinery Dust NA 1.40E+04 C Nickel Soluble Salts 7440-02-0 3.20E+02 N Nickel Subsulfide 12035-72-2 6.90E+03 C Nitrate 14797-55-8 2.60E+04 N Nitrite 14797-65-0 1.60E+03 N Nitrobenzene 98-95-3 2.60E+03 6.20E+00 N Nitrofurantoin 67-20-9 8.60E+02 N Nitrofurazone 59-87-0 3.70E-01 C Nitroglycerin 55-63-0 1.20E+00 N Nitroguanidine 556-88-7 1.20E+03 N Nitromethane* 75-52-5 1.70E+04 4.70E+00 C Nitropropane, 2- 79-46-9 4.30E+03 1.20E-02 C Nitroso-di-N-butylamine, N- 924-16-3 1.30E+04 9.30E-02 C Nitroso-di-N-propylamine, N- 621-64-7 6.90E-02 C Nitroso-N-ethylurea, N- 759-73-9 4.30E-03 C,M Nitrosodiethanolamine, N- 1116-54-7 1.70E-01 C Nitrosodiethylamine, N- 55-18-5 7.70E-04 C,M Nitrosodimethylamine, N-* 62-75-9 2.30E-03 C,M October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 11 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Nitrosodiphenylamine, N- 86-30-6 9.90E+01 C Nitrosomethylethylamine, N- 10595-95-6 2.20E-02 C Nitrosopyrrolidine, N- 930-55-2 2.30E-01 C Nitrotoluene, o- 88-72-2 1.30E+03 2.90E+00 C Nitrotoluene, p-* 99-99-0 3.00E+01 C Norflurazon 27314-13-2 4.80E+02 N Nustar 85509-19-9 8.60E+00 N Octabromodiphenyl Ether 32536-52-0 3.60E+01 N Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetra (HMX) 2691-41-0 7.6E+02 N Octamethylpyrophosphoramide 152-16-9 2.40E+01 N Oryzalin 19044-88-3 6.20E+02 N Oxadiazon 19666-30-9 6.20E+01 N Oxamyl 23135-22-0 3.00E+02 N Paclobutrazol 76738-62-0 1.60E+02 N Polynuclear Aromatic Hydrocarbons (PAHs) 7 Acenaphthene 83-32-9 6.80E+02 N Anthracene 120-12-7 3.40E+03 N Benz[a]anthracene 56-55-3 1.50E-01 C,M Benzo[a]pyrene 50-32-8 1.50E-02 C,M Benzo[b]fluoranthene 205-99-2 1.50E-01 C,M Benzo[k]fluoranthene 207-08-9 1.50E+00 C,M Chrysene 218-01-9 1.50E+01 C,M Dibenz[a,h]anthracene 53-70-3 1.50E-02 C,M Fluoranthene 206-44-0 4.60E+02 N Fluorene 86-73-7 4.60E+02 N Indeno[1,2,3-cd]pyrene 193-39-5 1.50E-01 C,M Methylnaphthalene, 1- 90-12-0 3 4.60E+02 2.20E+01 C Methylnaphthalene, 2- 91-57-6 3 4.40E+02 6.20E+01 N Naphthalene* 91-20-3 3.90E+00 C Pyrene 129-00-0 3.40E+02 N Paraquat Dichloride 1910-42-5 5.40E+01 N Parathion 56-38-2 7.40E+01 N Polychlorinated Biphenyls (PCBs) 7 1.00E+00 6 Pebulate 1114-71-2 6.20E+02 N Pendimethalin 40487-42-1 4.80E+02 N Pentabromodiphenyl Ether 32534-81-9 2.40E+01 N Pentachlorobenzene 608-93-5 9.80E+00 N Pentachloronitrobenzene* 82-68-8 1.90E+00 C Pentachlorophenol* 87-86-5 3.00E+00 C Perchlorate and Perchlorate Salts 14797-73-0 1.10E+01 N Permethrin 52645-53-1 6.20E+02 N Phenmedipham 13684-63-4 3.00E+03 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 12 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Phenol 108-95-2 3.60E+03 N Phenylenediamine, m- 108-45-2 7.40E+01 N Phenylenediamine, o- 95-54-5 1.00E+01 C Phenylenediamine, p- 106-50-3 2.40E+03 N Phenylphenol, 2- 90-43-7 2.50E+02 N Phorate 298-02-2 2.40E+00 N Phosgene 75-44-5 8.70E+04 8.00E-02 N Phosmet 732-11-6 2.40E+02 N Phosphine 7803-51-2 4.60E+00 N Phosphoric Acid 7664-38-2 2.80E+06 N Phosphorus, White 7723-14-0 3.20E-01 N Phthalic Acid, P- 100-21-0 1.20E-04 N Phthalic Anhydride 85-44-9 2.40E-04 N Picloram 1918-02-1 8.60E+02 N Pirimiphos, Methyl 29232-93-7 1.20E+02 N Polybrominated Biphenyls* 59536-65-1 1.60E-02 C Polymeric Methylene Diphenyl Diisocyanate (PMDI) 9016-87-9 1.70E+05 N Potassium Perchlorate 7778-74-7 1.10E+01 N Prochloraz* 67747-09-5 3.20E+00 C Profluralin 26399-36-0 7.40E+01 N Prometon 1610-18-0 1.80E+02 N Prometryn 7287-19-6 4.80E+01 N Propachlor 1918-16-7 1.60E+02 N Propanil 709-98-8 6.20E+01 N Propargite 2312-35-8 2.40E+02 N Propargyl Alcohol 107-19-7 2.40E+01 N Propazine 139-40-2 2.40E+02 N Propham 122-42-9 2.40E+02 N Propiconazole 60207-90-1 1.60E+02 N Propylene Glycol 57-55-6 2.40E+05 N Propylene Glycol Dinitrate 6423-43-4 1.40E+03 1.20E+01 N Propylene Glycol Monoethyl Ether 1569-02-4 8.60E+03 N Propylene Glycol Monomethyl Ether 107-98-2 8.60E+03 N Propylene Oxide* 75-56-9 6.80E+04 1.90E+00 C Pursuit 81335-77-5 3.00E+03 N Pydrin 51630-58-1 3.00E+02 N Pyridine 110-86-1 3.00E+05 1.60E+01 N Quinalphos 13593-03-8 6.20E+00 N Quinoline 91-22-5 1.60E-01 C Refractory Ceramic Fibers NA 8.60E+06 N Resmethrin 10453-86-8 3.60E+02 N Ronnel 299-84-3 6.20E+02 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 13 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Rotenone 83-79-4 4.80E+01 N Savey 78587-05-0 3.00E+02 N Selenious Acid 7783-00-8 7.80E+01 N Selenium 7782-49-2 7.80E+01 N Selenourea 630-10-4 6.20E+01 N Sethoxydim 74051-80-2 1.10E+03 N Silver 7440-22-4 7.80E+01 N Simazine* 122-34-9 4.00E+00 C Sodium Acifluorfen 62476-59-9 1.60E+02 N Sodium Azide 26628-22-8 6.20E+01 N Sodium Diethyldithiocarbamate 148-18-5 1.80E+00 C Sodium Fluoroacetate 62-74-8 2.40E-01 N Sodium Metavanadate 13718-26-8 1.60E+01 N Sodium Perchlorate 7601-89-0 1.10E+01 N Stirofos (Tetrachlorovinphos)* 961-11-5 2.00E+01 C Strontium, Stable 7440-24-6 9.40E+03 N Strychnine 57-24-9 3.60E+00 N Styrene 100-42-5 1.00E+03 1.00E+03 Csat Systhane 88671-89-0 3.00E+02 N TCMTB 21564-17-0 3.60E+02 N Tebuthiuron 34014-18-1 8.60E+02 N Temephos 3383-96-8 2.40E+02 N Terbacil 5902-51-2 1.60E+02 N Terbufos 13071-79-9 3.00E-01 N Terbutryn 886-50-0 1.20E+01 N Tetrachlorobenzene, 1,2,4,5- 95-94-3 3.60E+00 N Tetrachloroethane, 1,1,1,2- 630-20-6 7.50E+02 2.00E+00 C Tetrachloroethane, 1,1,2,2- 79-34-5 2.10E+03 5.90E-01 C Tetrachloroethylene 127-18-4 1.80E+02 5.70E-01 C Tetrachlorophenol, 2,3,4,6- 58-90-2 3.60E+02 N Tetrachlorotoluene, p- alpha, alpha, alpha- 5216-25-1 2.40E-02 C Tetraethyl Dithiopyrophosphate 3689-24-5 6.20E+00 N Tetrafluoroethane, 1,1,1,2- 811-97-2 8.20E+02 8.20E+02 Csat Tetryl (Trinitrophenylmethylnitramine) 479-45-8 4.80E+01 N Thallium (I) Nitrate 10102-45-1 1.40E+00 N Thallium (Soluble Salts) 7440-28-0 1.00E+00 N Thallium Acetate 563-68-8 1.40E+00 N Thallium Carbonate 6533-73-9 1.30E+00 N Thallium Chloride 7791-12-0 1.30E+00 N Thallium Sulfate 7446-18-6 1.30E+00 N Thiobencarb 28249-77-6 1.20E+02 N Thiofanox 39196-18-4 3.60E+00 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 14 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Thiophanate, Methyl 23564-05-8 9.80E+02 N Thiram 137-26-8 6.20E+01 N Tin 7440-31-5 9.40E+03 N Toluene 108-88-3 9.30E+02 9.30E+02 Csat Toluene diisocyanate mixture (TDI) 26471-62-5 2.10E+03 1.10E+01 N Toluene-2,4-diamine 95-80-7 1.30E-01 C Toluene-2,5-diamine 95-70-5 7.40E+03 N Toluene-2,6-diamine 823-40-5 3.60E+02 N Toluidine, o- (Methylaniline, 2-) 95-53-4 2.70E+00 C Toluidine, p- 106-49-0 2.60E+00 C Toxaphene 8001-35-2 4.40E-01 C Tralomethrin 66841-25-6 9.20E+01 N Triallate 2303-17-5 1.60E+02 N Triasulfuron 82097-50-5 1.20E+02 N Tribromobenzene, 1,2,4- 615-54-3 6.20E+01 N Tributyltin Compounds NA 3.60E+00 N Tributyltin Oxide 56-35-9 3.60E+00 N Trichloro-1,2,2-trifluoroethane, 1,1,2- 76-13-1 9.40E+02 9.40E+02 Csat Trichloroaniline HCl, 2,4,6- 33663-50-2 1.70E+01 C Trichloroaniline, 2,4,6- 634-93-5 1.40E+01 C Trichlorobenzene, 1,2,4-* 120-82-1 3 2.20E+02 1.74E+01 N Trichloroethane, 1,1,1- 71-55-6 6.80E+02 6.80E+02 Csat Trichloroethane, 1,1,2-* 79-00-5 5.60E+02 1.10E+00 C Trichloroethylene 79-01-6 7.50E+02 2.80E+00 C Trichlorofluoromethane 75-69-4 1.30E+03 1.60E+02 N Trichlorophenol, 2,4,5- 95-95-4 1.20E+03 N Trichlorophenol, 2,4,6-* 88-06-2 1.20E+01 N Trichlorophenoxy) Propionic Acid, 2(2,4,5- 93-72-1 9.80E+01 N Trichlorophenoxyacetic Acid, 2,4,5- 93-76-5 1.20E+02 N Trichloropropane, 1,1,2- 598-77-6 1.40E+03 7.80E+01 N Trichloropropane, 1,2,3- 96-18-4 1.60E+03 9.10E-02 C Tridiphane 58138-08-2 3.60E+01 N Triethylamine 121-44-8 5.50E+04 3.40E+01 N Trifluralin* 1582-09-8 6.30E+01 C Trimethyl Phosphate 512-56-1 1.30E+01 N Trimethylbenzene, 1,2,4- 95-63-6 2.50E+02 1.30E+01 N Trinitrobenzene, 1,3,5- 99-35-4 4.40E+02 N Trinitrotoluene, 2,4,6-* 118-96-7 1.90E+01 C Tri-n-butyltin 688-73-3 3.60E+00 N Uranium (Soluble Salts) NA 4.60E+01 N Vanadium Pentoxide 1314-62-1 1.40E+02 N Vanadium Sulfate 36907-42-3 3.20E+02 N October 2008 INACTIVE HAZARDOUS SITES BRANCH HEALTH-BASED SOIL REMEDIATION GOALS1 These health-based remediation goals must be used in conjunction with either the REC or State-Lead Guidance documents and apply only at sites with signed administrative agreements with the Division of Waste Management. In addition to these health-based goals, soils must also meet protection of groundwater remediation goals. If sensitive environments are present at a site, the branch may require the adjustment of remediation goals and/or the proposed remedial alternative. Page 15 of 16 See Csat RG (ppm) footnote Contaminant CASRN Foot note (mg/kg) (mg/kg) 8 Vanadium and Compounds NA 7.80E+01 N Vanadium, Metallic 7440-62-2 1.10E+02 N Vanadyl Sulfate 27774-13-6 3.20E+02 N Vernolate 1929-77-7 1.20E+01 N Vinclozolin 50471-44-8 3.00E+02 N Vinyl Acetate 108-05-4 2.80E+03 2.00E+02 N Vinyl Bromide 593-60-2 1.70E+03 1.10E-01 C Vinyl Chloride 75-01-4 4.00E+03 6.00E-02 C,M Warfarin 81-81-2 3.60E+00 N Xylene, Mixture 1330-20-7 3 3.00E+02 1.20E+02 N Xylene, P- 106-42-3 4.50E+02 4.50E+02 Csat Xylene, m- 108-38-3 4.40E+02 4.40E+02 Csat Xylene, o- 95-47-6 3.00E+02 3.00E+02 Csat Zinc (Metallic) 7440-66-6 4.60E+03 N Zinc Phosphide 1314-84-7 4.60E+00 N Zineb 12122-67-7 6.20E+02 N * - Contaminant exhibits both carcinogenic and non-carcinogenic effects. The lower of the carcinogenic remediation goal at 1.0E-06 risk or the non-carcinogenic remediation goal at a hazard quotient of 0.2 is listed. 1 - Adapted from the 2008 USEPA Regional Screening Tables. Cleanup below method detection limits using analytical methods prescribed in the guidelines, is not required. 2 - The arsenic value is the non-carcinogenic value because the carcinogenic value is below the laboratory method detection limit (MDL). 3 - When adjusting the remediation goals for a chemical as described in appendix E of the REC guidelines, its Soil Saturation Concentration (Csat) must not be exceeded unless protection of groundwater concentration have been met. 4 - Remediation goals for dioxins and furans can also be calculated as a toxic equivalency concentration (TEQ) by using the toxicity equivalence factor (TEF) methodology. (See TEF table for dioxins and furans.) 5 - The RG is based on USEPA guidance on lead cleanup levels. The value cannot be adjusted. 6 - Remediation goals for carcinogenic PAHs can also be calculated as a toxic equivalency concentration (TEQ) by using the toxicity equivalence factor (TEF) methodology. (See TEF table for carcinogenic PAHs.) 7 - The RG is based on USEPA policy for cleanup of PCBs at Superfund Sites. The Branch is currently reviewing the PCB remediation goal policy and may issue further guidance at a later date. 8 - C - The RG is based on the carcinogenic endpoint and corresponds to an excess lifetime cancer risk of 1 in 1,000,000. N - The RG is based on the non-carcinogenic endpoint and corresponds to a hazard quotient of 0.2. M - Contaminant is a mutagen. Csat – Soil Saturation Concentration. NA- Not available. October 2008 Page 16 of 16 INACTIVE HAZARDOUS SITES BRANCH Toxic Equivalent Factor Tables for Calculation of Soil Remediation Goals Toxic Equivalent Factor (TEF) Table for Dioxins and Furans CHEMICAL CASRN TEF* Dioxins and Furans 4 CDDs 2,3,7,8-TetraCDD 1 1,2,3,7,8-PentaCDD 1 1,2,3,4,7,8-HexaCDD 0.1 1,2,3,6,7,8-HexaCDD 0.1 1,2,3,7,8,9-HexaCDD 0.1 1,2,3,4,6,7,8-HeptaCDD 0.01 1,2,3,4,6,7,8,9-OctaCDD 0.0003 CDFs 2,3,7,8-TetraCDF 0.1 1,2,3,7,8-PentaCDF 0.03 2,3,4,7,8-PentaCDF 0.3 1,2,3,4,7,8-HexaCDF 0.1 1,2,3,6,7,8-HexaCDF 0.1 1,2,3,7,8,9-HexaCDF 0.1 2,3,4,6,7,8-HexaCDF 0.1 1,2,3,4,6,7,8-HeptaCDF 0.01 1,2,3,4,7,8,9-HeptaCDF 0.01 1,2,3,4,6,7,8,9-OctaCDF 0.0003 Toxic Equivalent Factor (TEF) Table for Carcinogenic Polyaromatic Hydrocarbons (PAHs) CHEMICAL CASRN TEF* Polynuclear aromatic hydrocarbons 6 Benzo[a]pyrene 50328 1.0 Benzo[b]fluoranthene 205992 0.1 Benzo[k]fluoranthene 207089 0.01 Benz[a]anthracene 56553 0.1 Chrysene 218019 0.001 Dibenz[a,h]anthracene 53703 1.0 Indeno(1,2,3-cd)pyrene 193395 0.1 *These toxic equivalent factors (TEF) are to be used as per footnotes 4 and 6 on the previous page. October 2008 GUIDELINES FOR SITE CHECKS, TANK CLOSURE, AND INITIAL RESPONSE AND ABATEMENT FOR UST RELEASES UST Section North Carolina Department of Environment and Natural Resources Division of Waste Management March 1, 2007 Version Change 3, Effective December 1, 2008 4 4.0 UST Site Check Guidelines for Regulated UST Systems 4.1 Regulatory Authority A site check is required if a release from a regulated UST system has been suspected or confirmed by the presence, at the site or nearby, of the regulated substance as free product, dissolved product, or vapor in soils, sewer and utility lines, surface water, groundwater, etc; by unusual operating conditions; or by leak detection and/or tightness testing results, in accordance with 15A NCAC 2N .0601 and .0603 and .0701- .0704. A site check is required if a spill or overfill is known to have occurred at the site. A site check is also required if the UST system is suspected to be the source of an off-site impact, in accordance with 15A NCAC 2N .0602. 4.2 Site Check Description The site check assessment procedure requires sampling where contamination is observed or is most likely to be present at the site. The scope of assessment therefore includes the soil surrounding the entire UST system and the groundwater. The sampling procedure requires the same sampling protocol required for UST closure. The sampling protocol must consider the nature of the stored substance, the type of initial alarm or cause for suspicion, the type of backfill, the depth to groundwater, and any other factors appropriate for identifying the presence and source of the release. Site check activities are required of owners and operators of UST systems in any of the circumstances described below: 1) Evidence of a release is present at the UST site or is found offsite and may be related to a release at the UST site. Such evidence includes, but is not limited to, the discovery of the presence of regulated substances (such as dissolved product, free product, or vapors) in soils, basements, sewer or utility lines, and nearby surface water and groundwater; 2) Tightness test results for the UST system do not indicate that a leak exists, but environmental contamination indicates that a release from the UST system may have occurred; 3) The applied method of leak detection indicates a suspected release and a follow-up tightness test confirms that result; 4) A spill or overfill of a regulated substance has occurred. If State Trust Fund reimbursement is anticipated, please refer to the current version of the Reasonable Rate Document for information about allowed reimbursement. 4.3 Site Check Requirements When conducting a site check, the procedures below must be included: 5 1) Soil samples must be collected around the perimeter of a single UST or around the perimeter of a set of USTs in a single pit, according to the sampling procedure described in item #1 of 5.3.B, Removal of UST(s) underlain by a concrete pad. Samples must be collected within 3 feet of the UST(s) at a depth equal to the depth of the tank bottom(s) or no deeper than 2 feet below the depth of the tank bottom into the native soil. 2) One sample must be collected at the fill port of each UST (or under any catchment basin at the fill port) to document overfills. 3) Soil samples must also be collected underneath associated product lines, dispensers, containment sumps, turbine pumps or turbine containment sumps, and other areas where contamination is suspected or observed, as described in 5.3.F. Note that it may not be necessary to collect samples from around the entire system, as indicated in items 1-3 above, if the area of the suspected release is localized. Note also that if the UST system contains an ethanol-gasoline blend, the UST Section will determine if the assessment required in items 1-3 is adequate. 4) All soil samples must be analyzed by approved methods as specified in Table 1, p. 31. 5) If required by the UST Section, a permanent monitoring well, constructed according to Title 15A NCAC 2C, Well Construction Standards, must be installed as close as possible to and within 5 feet of the (part of the) UST system with the (suspected) release in a downgradient direction, and a groundwater sample must be collected and analyzed as specified in Tables 2 and 6. 6) If the results of the site check indicate that no soil contamination equals or exceeds 10 mg/kg TPH for petroleum (or exceeds the soil-to-groundwater MSCC, or the MDL if no MSCC is established, for regulated hazardous substances), no groundwater contamination exceeds the groundwater quality standard established in 15A NCAC 2L .0202, and no free product is present, then the results must be reported to the UST Section in a Site Check Report (Appendix A, p. 48). The Site Check Report must be submitted to the branch of the UST Section which requested it (to Permits and Inspections Branch, if required by a UST inspector, or to the appropriate regional office of the Corrective Action Branch, if required by an incident manager). The Site Check Report must be received by the UST Section within 30 days of the receipt of the Notice of Regulatory Requirements or the Notice of Violation. If it was necessary to remove all or part of the UST system to allow access for site check sampling, then the required UST closure report elements (UST-12 Format with UST-2 Form, Appendix A, p. 60) should be submitted as part of the Site Check Report. The reporting requirements are described in Section 8.0, and the outline of the format is presented in Appendix A, p. 48. No further action will be required. 7) If the results of the site check indicate that soil contamination equals or exceeds 10 mg/kg TPH for petroleum (or exceeds the soil-to-groundwater MSCCs, or the MDL if no MSCC is established, for regulated hazardous substances), groundwater contamination exceeds the 2L Change 2 6 standards, or free product is present, then the initial response and abatement actions must be performed. A flowchart illustrating the requirements for releases discovered during site checks is presented as Figure 1 on p. 41. Initial response actions which are required include submittal of a 24-Hour Release and Reporting Form (Appendix A, p. 54) to the UST Section within 24 hours following discovery of the release; action to stop the release; and identification and mitigation of hazards from exposure to pollutants. Initial abatement actions include determination of the source of the release (if not previously identified); investigation and removal of free product; submittal of a 20-Day Report (Appendix A, p. 56) to the UST Section within 20 days following discovery of the release; and excavation of contaminated soil to the maximum extent possible, followed by confirmation sampling as described in Section 9.1 and in Table 1, p. 31. The final results of the initial abatement actions for a petroleum release must be reported in an Initial Abatement Action Report (Appendix A, p. 66), which must be submitted to the UST Section within 90 days following discovery of the release. (The final results of the initial abatement actions for a hazardous substance release must be reported in a 45-Day Report, the requirements for which are addressed in the current version of the Guidelines for Assessment and Corrective Action for UST Releases; the 45-Day Report must be submitted within 45 days following discovery of the release.) The 24-Hour Report, the 20-Day-Report, and the Initial Abatement Action Report (or the 45- Day Report, for a hazardous substance release) must be submitted to the branch of the UST Section which requested it (to Permits and Inspections Branch, if required by a UST inspector, or to the appropriate regional office of the Corrective Action Branch, if required by an incident manager). If it was necessary to remove all or part of the UST system to allow access for site check sampling and/or excavation, then the required UST closure report elements (UST-12 Format with UST-2 Form, Appendix A, p. 60) should be submitted as part of the Initial Abatement Action Report. The reporting requirements are described in Section 8.0, and the outline of the format is presented in Appendix A, p. 66. 8) If the Initial Abatement Action Report for a petroleum release shows that post-excavation soil contaminant concentrations do not exceed the lower of the soil-to-groundwater or residential maximum soil contaminant concentrations (MSCCs) and reports that neither groundwater nor bedrock has been encountered in the excavation, then no further action will be required. However, if the Initial Abatement Action Report indicates that soil contaminant concentrations exceed the lower of the soil-to-groundwater or residential MSCCs or reports that groundwater or bedrock has been encountered in the excavation, then the responsible party must perform further assessment and submit a Limited Site Assessment Report within 120 days of the discovery of the release. The Limited Site Assessment Report format is presented in the Guidelines for Assessment and Corrective for UST Releases, current version. 44 Figure 4 Flowchart of Requirements for Non-Regulated Petroleum UST System Releases PERFORM INITIAL ABATEMENT ACTIONS Submit 24-hour Release and Report Form within 24 hours of discovery of release Submit 20-Day Report within 20 days of confirmation of release Excavate contaminated soil to maximum extent possible (mandatory) See Section 7.0 Perform and submit Limited Site Assessment Report within 120 days of discovery of release. (Refer to Guidelines for Assessment and Corrective Action) Submit Initial Abatement Action (including Excavation, Post- Excavation Soil Contamination Assessment) Report within 90 days of discovery of release No further action If soil >lowest MSCCs, bedrock is encountered in excavation, or groundwater is encountered and is >2L If soil <lowest MSCCs, bedrock is not encountered in excavation, and groundwater is not encountered (or is encountered but is <2L) Collect/analyze post-excavation soil samples; and, if groundwater is encountered in the excavation, install a monitoring well and sample/analyze groundwater. ID & mitigate fire, explosion, vapor hazards ID & mitigate hazards from exposure to pollutants (supply alternate water) Determine source or presence of release if previous activities have failed to do so. Act to prevent further release On discovery of evidence of a release (vapors, staining, FP sheen), sample soil to confirm. If release is confirmed, remove UST and collect and analyze additional soil (and groundwater samples) using regulated closure assessment procedure and analytical methods (TPH). If soil >10 mg/kg TPH or groundwater or bedrock is encountered (and groundwater is>2L) If soil <10 mg/kg TPH and groundwater and bedrock are not encountered (or groundwater is <2L) No further action PERFORM INITIAL RESPONSE ACTIONS Investigate/ begin to recover FP within 14 days 26 (f) Groundwater quality standards specified in Paragraphs (g) and (h) of this Rule and interim maximum allowable concentrations established pursuant to Paragraph (c) of this Rule shall be reviewed on a triennial basis. Appropriate modifications to established standards shall be made in accordance with the procedure prescribed in Paragraph (d) of this Rule where modifications are considered appropriate based on data published subsequent to the previous review. (g) Class GA Standards. Where not otherwise indicated, the standard refers to the total concentration in milligrams per liter of any constituent in a dissolved, colloidal or particulate form which is mobile in groundwater. This does not apply to sediment or other particulate matter which is preserved in a groundwater sample as a result of well construction or sampling procedures. (1) acetone: 0.7 (2) acenaphthene: 0.08 (3) acenaphthylene: 0.21 (4) acrylamide (propenamide): 0.000008 (5) anthracene: 2.1 (6) arsenic: 0.05 (7) atrazine and chlorotriazine metabolites: 0.0030 (8) barium: 2.0 (9) benzene: 0.001 (10) benzo(a)anthracene (benz(a)anthracene): 0.0000479 (11) benzo(b)fluoranthene: 4.79 x 10- 5 (12) benzo(k)fluoranthene: 4.79 x 10- 4 (13) benzo(g,h,i,)perylene: 0.21 (14) benzo(a)pyrene: 4.79 x 10-6 (15) boron: 0.315 (16) bromodichloromethane: 0.00056 (17) bromoform (tribromomethane): 0.00443 (18) n-butylbenzene: 0.07 (19) sec-butylbenzene: 0.07 (20) tert-butylbenzene: 0.07 (21) butylbenzyl phthalate: 0.10 (22) cadmium: 0.00175 (23) caprolactam: 3.5 (24) carbofuran: 0.035 (25) carbon disulfide: 0.7 (26) carbon tetrachloride: 0.000269 (27) chlordane: 1.0 x 10-4 (28) chloride: 250.0 (29) chlorobenzene: 0.05 (30) chloroethane: 2.80 (31) chloroform (trichloromethane): 0.07 27 (32) chloromethane (methyl chloride): 2.6 x 10-3 (33) 2-chlorophenol: 0.00036 (34) 2-chlorotoluene: 0.14 (35) chromium: 0.05 (36) chrysene: 0.00479 (37) cis-1,2-dichloroethene: 0.07 (38) coliform organisms (total): 1 per 100 milliliters (39) color: 15 color units (40) copper: 1.0 (41) cyanide (free cyanide): 0.07 (42) 2, 4-D (2,4-dichlorophenoxy acetic acid): 0.07 (43) dibenz(a,h)anthracene: 4.7 x 10-6 (44) 1,2-dibromo-3-chloropropane: 2.5 x 10-5 (45) dichlorodifluoromethane (Freon-12; Halon): 1.4 (46) p,p’-dichlorodiphenyl dichloroethane (DDD): 1.4 x 10-4 (47) p,p’-dichlorodiphenyltrichloroethane (DDT): 1.0 x 10-4 (48) 1,1-dichloroethane: 0.07 (49) 1,2-dichloroethane (ethylene dichloride): 0.00038 (50) 1,1-dichloroethylene (vinylidene chloride): 0.007 (51) 1,2-dichloropropane: 0.00051 (52) 1,3-dichloropropene (cis and trans isomers): 0.00019 (53) dieldrin: 2.2 x 10-6 (54) di-n-butyl (or dibutyl) phthalate (DBP): 0.7 (55) diethylphthalate (DEP): 5.0 (56) di(2-ethylhexyl) phthalate (DEHP): 0.0025 (57) 2,4-dimethylphenol (m-xylenol): 0.14 (58) di-n-octyl phthalate: 0.14 (59) p-dioxane (1,4-diethylene dioxide): 0.007 (60) dioxin: 2.2 x 10-10 (61) diphenyl (1,1– diphenyl): 0.35 (62) dissolved solids (total): 500 (63) disulfoton: 2.8 x 10-4 (64) diundecyl phthalate (Santicizer 711): 0.14 (65) endosulfan II (beta-endosulfan): 0.0420 (66) endrin: 0.002 (67) endrin (total endrin: includes endrin, endrin aldehyde, and endrin ketone): 2.1 x 10-3 (68) epichlorohydrin (1-chloro-2,3-epoxypropane): 0.00354 (69) ethylbenzene: 0.550 (70) ethylene dibromide (EDB; 1,2-dibromoethane): 4.0 x 10-7 (71) ethylene glycol: 14.0 28 (72) fluoranthene: 0.28 (73) fluorene: 0.28 (74) fluoride: 2.0 (75) foaming agents: 0.5 (76) gross alpha (adjusted)particle activity (excluding radium-226 and uranium): 15 pCi/l (77) heptachlor: 7.8 x 10-6 (78) heptachlor epoxide: 3.8 x 10-6 (79) heptane: 0.42 (80) hexachlorobenzene (perchlorobenzene): 0.00002 (81) hexachlorocyclohexane isomers (total hexachlorocyclohexane: includes alpha,beta,delta,gamma, and epsilon isomers): 1.9 x 10-5 (82) n-hexane: 0.42 (83) indeno(1,2,3-cd)pyrene: 4.79 x 10-5 (84) iron: 0.3 (85) isophorone: 0.0368 (86) isopropylbenzene: 0.070 (87) isopropyl ether (diisopropyl ether): 0.070 (88) lead: 0.015 (89) lindane: 2.0 x 10-4 (90) manganese: 0.05 (91) mercury: 0.00105 (92) metadichlorobenzene (1,3-dichlorobenzene): 0.170 (93) methanol: 3.5 (94) methoxychlor: 0.035 (95) methylene chloride (dichloromethane): 0.0046 (96) methyl ethyl ketone (MEK; 2-butanone): 4.20 (97) 2-methylnaphthalene: 0.0140 (98) 3-methylphenol (m-cresol): 0.0350 (99) 4-methylphenol (p-cresol): 3.5 x 10-3 (100) methyl tert-butyl ether (MTBE): 0.2 (101) naphthalene: 0.021 (102) nickel: 0.1 (103) nitrate: (as N) 10.0 (104) nitrite: (as N) 1.0 (105) N-nitrosodimethylamine: 7.0 x 10-7 (106) orthodichlorobenzene (1,2-dichlorobenzene): 0.024 (107) oxamyl: 0.175 (108) paradichlorobenzene (1,4-dichlorobenzene): 0.0014 (109) pentachlorophenol: 0.00029 (110) petroleum aliphatic carbon fraction class C5 - C8: 0.42 29 (111) petroleum aliphatic carbon fraction class C9 - C18: 4.20 (112) petroleum aliphatic carbon fraction class C19 - C36: 42.0 (113) petroleum aromatics carbon fraction class C9 – C22: 0.210 (114) pH: 6.5 - 8.5 (115) phenanthrene: 0.21 (116) phenol: 0.30 (117) phorate: 1.4 x 10-3 (118) n-propylbenzene: 0.070 (119) pyrene: 0.21 (120) selenium: 0.05 (121) silver: 0.0175 (122) simazine: 0.004 (123) styrene (ethenylbenzene): 0.1 (124) sulfate: 250.0 (125) tetrachloroethylene (perchloroethylene; PCE): 0.0007 (126) 2,3,4,6-tetrachlorophenol: 0.210 (127) toluene (methylbenzene): 1.0 (128) toxaphene: 3.1 x 10-5 (129) 2, 4, 5,-TP (Silvex): 0.05 (130) trans-1,2-dichloroethene: 0.10 (131) 1,1,1-trichloroethane (methyl chloroform): 0.2 (132) trichloroethylene (TCE): 0.0028 (133) trichlorofluoromethane: 2.1 (134) 1,1,2-trichloro-1,2,2-trifluoroethane (CFC-113): 210.0 (135) 1,2,3- trichloropropane: 5.0 x 10-6 (136) 1,2,4-trimethylbenzene: 0.350 (137) 1,3,5-trimethylbenzene: 0.350 (138) vinyl chloride (chloroethylene): 1.5 x 10-5 (139) xylenes (o-, m-, and p-): 0.53 (140) zinc: 1.05 (h) Class GSA Standards. The standards for this class shall be the same as those for Class GA except as follows: (1) chloride: allowable increase not to exceed 100 percent of the natural quality concentration. (2) total dissolved solids: 1000 mg/l. (i) Class GC Waters. (1) The concentrations of substances which, at the time of classification exceed the standards applicable to Class GA or GSA groundwaters shall not be caused to increase, nor shall the concentrations of other substances be caused to exceed the GA or GSA standards as a 30 result of further disposal of contaminants to or beneath the surface of the land within the boundary of the area classified GC. (2) The concentrations of substances which, at the time of classification, exceed the standards applicable to GA or GSA groundwaters shall not be caused to migrate as a result of activities within the boundary of the GC classification, so as to violate the groundwater or surface water quality standards in adjoining waters of a different class. (3) Concentrations of specific substances, which exceed the established standard at the time of classification, shall be listed in Section .0300 of this Subchapter. History Note: Authority G.S. 143-214.1; 143B-282(a)(2); Eff. June 10, 1979; Amended Eff. November 1, 1994; October 1, 1993; September 1, 1992; August 1, 1989; Temporary Amendment Eff. June 30, 2002; Amended Eff. August 1, 2002; Temporary Amendment Expired February 9, 2003; Amended Eff. April 1, 2005. SECTION .0300 - ASSIGNMENT OF UNDERGROUND WATER CLASSIFICATIONS 15A NCAC 02L .0301 CLASSIFICATIONS: GENERAL (a) Schedule of Classifications. The classifications are based on the quality, occurrence and existing or contemplated best usage of the groundwaters as established in Section .0200 of this Subchapter and are assigned statewide except where supplemented or supplanted by specific classification assignments by major river basins. (b) Classifications and Water Quality Standards. The classifications and standards assigned to the groundwaters are denoted by the letters GA, GSA, or GC. These classifications refer to the classifications and standards established by Rule .0201 of this Subchapter. History Note: Authority G.S. 143-214.1; 143B-282(2); Eff. December 30, 1983; Amended Eff. August 1, 1989. 15A NCAC 02L .0302 STATEWIDE IHSB INDUSTRIAL /COMMERCIAL VAPOR INTRUSION SCREENING TABLES. BASED ON SEPTEMBER 2008 USEPA REGIONAL TABLE AMBIENT AIR CONCENTRATIONS.1 Carcinogenic Target Risk (TR) = 1E-06Carcinogenic Target Risk (TR) = 1E-05Noncancer Hazard Index (HI) = 0.2Noncancer Hazard Index (HI) = 0.2Cgw (ug/l)= Ctarget,ia(ug/m3) X 10-03m3/L X 1H X 1/alpha Where H is Dimensionless Henrys Law Constant 2Acceptable Indoor Air Concentration ug/m3BasisAcceptable Soil Gas Concentration ug/m3 Acceptable Groundwater Concentration (Cgw) ug/lBasisAcetaldehyde 75-07-0 5.6E+00 C 7.8E+01 2.9E+03 NAcetone 67-64-1 2.8E+04 N 2.8E+05 1.8E+07 NAcetonitrile 75-05-8 5.2E+01 N 5.2E+02 3.7E+04 NAldrin 309-00-2 2.5E-03 C 2.5E-01 1.4E+01 CAniline 62-53-3 8.8E-01 N 8.8E+00 1.1E+04 NBenzene 71-43-2 1.6E+00 C 1.6E+02 7.0E+01 CBenzyl Chloride 100-44-7 8.8E-01 N 8.8E+00 5.2E+01 NBis(2-chloroethyl)ether 111-44-4 3.7E-02 C 3.7E+00 5.3E+02 CBis(2-chloro-1-methylethyl) ether 108-60-1 1.2E+00 C 1.2E+02 2.6E+03 CBis(chloromethyl)ether 542-88-1 2.0E-04 C 2.0E-02 2.4E-01 CBromoform 75-25-2 1.1E+01 C 1.1E+03 5.0E+03 CButadiene, 1,3- 106-99-0 4.1E-01 C 1.8E+01 5.9E-01 NCarbon Disulfide 75-15-0 6.2E+02 N 6.2E+03 1.1E+03 NCarbon Tetrachloride 56-23-5 8.2E-01 C 8.2E+01 7.5E+00 CChlordane 12789-03-6 1.2E-01 C 6.2E+00 3.1E+02 NChloro-1,3-butadiene, 2- 126-99-8 6.2E+00 N 6.2E+01 2.7E+00 NChlorobenzene 108-90-7 4.4E+01 N 4.4E+02 3.4E+02 NChlorodifluoromethane 75-45-6 4.4E+04 N 4.4E+05 2.6E+04 NChloroform 67-66-3 5.3E-01 C 5.3E+01 3.5E+01 CCumene 98-82-8 3.6E+02 N 3.6E+03 7.7E+02 N Hydrogen Cyanide 74-90-8 2.6E+00 N 2.6E+01 4.8E+02 NDibromo-3-chloropropane, 1,2- 96-12-8 2.0E-03 C 2.0E-01 3.3E+00 CDichlorobenzene, 1,2- 95-50-1 1.8E+02 N 1.8E+03 2.3E+03 NDichlorobenzene, 1,4- 106-46-7 1.1E+00 C 1.1E+02 1.1E+02 CDichlorodifluoromethane 75-71-8 2.2E-01 N 2.2E+00 1.6E-02 NDichloroethane, 1,1- 75-34-3 7.7E+00 C 7.7E+02 3.3E+02 CDichloroethane, 1,2- 107-06-2 4.7E-01 C 4.7E+01 9.8E+01 CDichloroethylene, 1,1- 75-35-4 1.8E+02 N 1.8E+03 1.6E+02 NDichloroethylene, 1,2-trans- 156-60-5 5.2E+01 N 5.2E+02 1.4E+02 NDichloropropane, 1,2- 78-87-5 1.2E+00 C 3.6E+01 3.0E+01 NDichloropropene, 1,3- 542-75-6 3.1E+00 C 1.8E+02 1.2E+02 NDieldrin 60-57-1 2.7E-03 C 2.7E-01 6.6E+01 CEpichlorohydrin 106-89-8 8.8E-01 N 8.8E+00 7.3E+02 NEthylbenzene 100-41-4 4.9E+00 C 4.9E+02 1.5E+02 CEthylene Oxide 75-21-8 1.4E-01 C 2.8E-01 4.6E+00 NHeptachlor 76-44-8 9.4E-03 C 1.9E-02 1.6E-01 NHeptachlor Epoxide 1024-57-3 4.7E-03 C 9.4E-03 1.1E+00 NHexachlorobenzene 118-74-1 2.7E-02 C 5.4E-02 7.7E-02 NAcceptable Soil Gas Concentration = Acceptable Indoor Air Concentration At Carcinogenic Target Risk (TR) = 1E-05 and Noncancer Hazard Index (HI) =0.2 X 10 Where Alpha =0.1ContaminantAnalyte CAS No. 1. This table is subject to periodic revision. Verify this is the most current copy before use.2. Questions about this table should be directed to the appropriate project manager or risk assessor.Page 1 of 2 IHSB INDUSTRIAL /COMMERCIAL VAPOR INTRUSION SCREENING TABLES. BASED ON SEPTEMBER 2008 USEPA REGIONAL TABLE AMBIENT AIR CONCENTRATIONS.1 Carcinogenic Target Risk (TR) = 1E-06Carcinogenic Target Risk (TR) = 1E-05Noncancer Hazard Index (HI) = 0.2Noncancer Hazard Index (HI) = 0.2Cgw (ug/l)= Ctarget,ia(ug/m3) X 10-03m3/L X 1H X 1/alpha Where H is Dimensionless Henrys Law Constant 2Acceptable Indoor Air Concentration ug/m3BasisAcceptable Soil Gas Concentration ug/m3 Acceptable Groundwater Concentration (Cgw) ug/lBasisAcceptable Soil Gas Concentration = Acceptable Indoor Air Concentration At Carcinogenic Target Risk (TR) = 1E-05 and Noncancer Hazard Index (HI) =0.2 X 10 Where Alpha =0.1ContaminantAnalyte CAS No.Hexachlorocyclohexane, Gamma- (Lindane) 58-89-9 4.0E-02 C 8.0E-02 3.8E+01 NHexachlorocyclopentadiene 77-47-4 1.8E-01 N 1.8E+00 1.6E-01 NHexachloroethane 67-72-1 3.1E+00 C 3.1E+02 1.9E+02 CHexane, N- 110-54-3 6.2E+02 N 6.2E+03 8.4E+00 NMethacrylonitrile 126-98-7 6.2E-01 N 6.2E+00 6.2E+01 NMethyl Ethyl Ketone (2-Butanone) 78-93-3 4.4E+03 N 4.4E+04 1.9E+06 NMethyl Isobutyl Ketone (4-methyl-2-pentanone) 108-10-1 2.6E+03 N 2.6E+04 4.6E+05 NMethyl Methacrylate 80-62-6 6.2E+02 N 6.2E+03 4.4E+04 NMethylene Chloride 75-09-2 2.6E+01 C 2.6E+03 2.0E+03 C Mercury (elemental) 7439-97-6 2.6E-01 N 2.6E+00 5.5E-01 NNitrobenzene 98-95-3 1.8E+00 N 1.8E+01 1.8E+03 NNitropropane, 2- 79-46-9 4.5E-03 C 4.5E-01 9.2E+00 CNitroso-di-N-butylamine, N- 924-16-3 7.7E-03 C 7.7E-01 1.4E+02 CPhenol 108-95-2 1.8E+02 N 1.8E+03 1.3E+07 N Benzo[b]fluoranthene 205-99-2 1.1E-01 C 1.1E+01 4.1E+04 C Chrysene 218-01-9 1.1E+00 C 1.1E+02 5.2E+04 C Naphthalene 91-20-3 3.6E-01 C 2.6E+01 1.4E+02 NStyrene 100-42-5 8.8E+02 N 8.8E+03 8.0E+03 NTetrachloroethane, 1,1,1,2- 630-20-6 1.7E+00 C 1.7E+02 1.7E+02 CTetrachloroethane, 1,1,2,2- 79-34-5 2.1E-01 C 2.1E+01 1.4E+02 CTetrachloroethylene 127-18-4 2.1E+00 C 2.1E+02 2.9E+01 CToluene 108-88-3 4.4E+03 N 4.4E+04 1.6E+04 NTrichloro-1,2,2-trifluoroethane, 1,1,2- 76-13-1 2.6E+04 N 2.6E+05 1.2E+03 NTrichlorobenzene, 1,2,4- 120-82-1 3.6E+00 N 3.6E+01 6.2E+01 NTrichloroethane, 1,1,1- 71-55-6 4.4E+03 N 4.4E+04 6.3E+03 NTrichloroethane, 1,1,2- 79-00-5 7.7E-01 C 7.7E+01 2.3E+02 CTrichloroethylene 79-01-6 6.1E+00 C 6.1E+02 1.5E+02 CTrichlorofluoromethane 75-69-4 6.2E+02 N 6.2E+03 1.6E+02 NTrichloropropene, 1,2,3- 96-19-5 8.8E-01 N 8.8E+00 1.2E+00 NTriethylamine 121-44-8 6.2E+00 N 6.2E+01 1.0E+03 NTrimethylbenzene, 1,2,4- 95-63-6 6.2E+00 N 6.2E+01 2.5E+01 NTrimethylbenzene, 1,3,5- 108-67-8 5.2E+00 N 5.2E+01 1.4E+01 NVinyl Acetate 108-05-4 1.8E+02 N 1.8E+03 8.4E+03 NVinyl Chloride 75-01-4 2.8E+00 C 2.8E+02 1.0E+02 C 1. This table is subject to periodic revision. Verify this is the most current copy before use.2. Questions about this table should be directed to the appropriate project manager or risk assessor.Page 2 of 2 IHSB RESIDENTIAL VAPOR INTRUSION SCREENING LEVELS FOR AIR, SOIL GAS, AND GROUNDWATER BASED ON THE SEPTEMBER 2008 USEPA REGIONAL TABLE AMBIENT AIR CONCENTRATIONS 1Carcinogenic Target Risk (TR) = 1E-06Carcinogenic Target Risk (TR) = 1E-05Noncancer Hazard Index (HI) = 0.2Noncancer Hazard Index (HI) = 0.2Cgw (ug/l)= Ctarget,ia(ug/m3) X 10-03m3/L X 1H X 1/alpha Where H is Dimensionless Henrys Law Constant 2Acceptable Indoor Air Concentration ug/m3 Basis Acceptable Soil Gas Concentration ug/m3 Acceptable Groundwater Concentration (Cgw) ug/l BasisAcetaldehyde 75-07-0 1.1E+00 C 1.9E+01 7.0E+02 NAcetone 67-64-1 6.4E+03 N 6.4E+04 4.0E+06 NAcetonitrile 75-05-8 1.3E+01 N 1.3E+02 9.0E+03 NAcrolein 107-02-8 4.2E-03 N 4.2E-02 8.4E-01 NAcrylonitrile 107-13-1 3.6E-02 C 3.6E+00 6.4E+01 CAldrin 309-00-2 5.0E-04 C 5.0E-02 2.8E+00 CAniline 62-53-3 2.0E-01 N 2.0E+00 2.4E+03 NBenzene 71-43-2 3.1E-01 C 3.1E+01 1.3E+01CBenzyl Chloride 100-44-7 2.0E-01 N 2.0E+00 1.2E+01NBis(2-chloroethyl)ether 111-44-4 7.4E-03 C 7.4E-01 1.1E+02CBis(2-chloro-1-methylethyl) ether 108-60-1 2.4E-01 C 2.4E+01 5.2E+02CBis(chloromethyl)ether 542-88-1 3.9E-05 C 3.9E-03 4.6E-02CBromoform 75-25-2 2.2E+00 C 2.2E+02 1.0E+03CButadiene, 1,3- 106-99-0 8.1E-02 C 4.2E+00 1.4E-01CCarbon Disulfide 75-15-0 1.5E+02 N 1.5E+03 2.5E+02NCarbon Tetrachloride 56-23-5 1.6E-01 C 1.6E+01 1.5E+00CChlordane 12789-03-6 2.4E-02 C 1.5E+00 7.3E+01NChloro-1,3-butadiene, 2- 126-99-8 1.5E+00 N 1.5E+01 6.3E-01NChlorobenzene 108-90-7 1.0E+01 N 1.0E+02 8.0E+01NChlorodifluoromethane 75-45-6 1.0E+04 N 1.0E+05 6.1E+03NChloroform 67-66-3 1.1E-01 C 1.1E+01 7.3E+00CCumene 98-82-8 1.1E-01 N 8.4E+02 1.8E+02N Hydrogen Cyanide 74-90-8 1.1E-01 N 6.2E+00 1.1E+02NDibromo-3-chloropropane, 1,2- 96-12-8 1.6E-04 C 1.6E-02 2.7E-01CDibromoethane, 1,2- 106-93-4 4.1E-03 C 4.1E-01 1.5E+00CDichlorobenzene, 1,2- 95-50-1 4.2E+01 N 4.2E+02 5.4E+02NDichlorobenzene, 1,4- 106-46-7 2.2E-01 C 2.2E+01 2.2E+01CDichlorodifluoromethane 75-71-8 4.2E+01 N 4.2E+02 3.0E+00NDichloroethane, 1,1- 75-34-3 1.5E+00 C 1.5E+02 6.5E+01CDichloroethane, 1,2- 107-06-2 9.4E-02 C 9.4E+00 2.0E+01CDichloroethylene, 1,1- 75-35-4 4.2E+01 N 4.2E+02 3.8E+01NDichloroethylene, 1,2-trans- 156-60-5 1.3E+01 N 1.3E+02 3.3E+01NDichloropropane, 1,2- 78-87-5 2.4E-01 C 8.4E+00 7.0E+00NDichloropropene, 1,3- 542-75-6 6.1E-01 C 4.2E+01 2.8E+01NDieldrin 60-57-1 5.3E-04 C 5.3E-02 1.3E+01CEpichlorohydrin 106-89-8 2.0E-01 N 2.0E+00 1.7E+02NEthylbenzene 100-41-4 9.7E-01 C 9.7E+01 3.0E+01CEthylene Oxide 75-21-8 2.8E-02 C 2.8E+00 4.6E+01CHeptachlor 76-44-8 1.9E-03 C 1.9E-01 1.6E+00CHeptachlor Epoxide 1024-57-3 9.4E-04 C 9.4E-02 1.1E+01CHexachlorobenzene 118-74-1 5.3E-03 C 5.3E-01 7.6E-01CAcceptable Soil Gas Concentration = Acceptable Indoor Air Concentration At Carcinogenic Target Risk (TR) =1E-05and Noncancer Hazard Index (HI)=0.2 x 10 Where Alpha =0.1 ContaminantAnalyte CAS No. 1. This table is subject to periodic revision. Verify this is the most current copy before use.2. Questions about this table should be directed to the appropriate project manager or risk assessor.Page 1 of 2 IHSB RESIDENTIAL VAPOR INTRUSION SCREENING LEVELS FOR AIR, SOIL GAS, AND GROUNDWATER BASED ON THE SEPTEMBER 2008 USEPA REGIONAL TABLE AMBIENT AIR CONCENTRATIONS 1Carcinogenic Target Risk (TR) = 1E-06Carcinogenic Target Risk (TR) = 1E-05Noncancer Hazard Index (HI) = 0.2Noncancer Hazard Index (HI) = 0.2Cgw (ug/l)= Ctarget,ia(ug/m3) X 10-03m3/L X 1H X 1/alpha Where H is Dimensionless Henrys Law Constant 2Acceptable Indoor Air Concentration ug/m3 Basis Acceptable Soil Gas Concentration ug/m3 Acceptable Groundwater Concentration (Cgw) ug/l BasisAcceptable Soil Gas Concentration = Acceptable Indoor Air Concentration At Carcinogenic Target Risk (TR) =1E-05and Noncancer Hazard Index (HI)=0.2 x 10 Where Alpha =0.1 ContaminantAnalyte CAS No.Hexachlorocyclohexane, Gamma- (Lindane) 58-89-9 7.8E-03 C 7.8E-01 3.7E+02CHexachlorocyclopentadiene 77-47-4 4.2E-02 N 4.2E-01 3.8E-02NHexachloroethane 67-72-1 6.1E-01 C 6.1E+01 3.8E+01CHexane, N- 110-54-3 1.5E+02 N 1.5E+03 2.0E+00NMethacrylonitrile 126-98-7 1.5E-01 N 1.5E+00 1.5E+01NMethyl Ethyl Ketone (2-Butanone) 78-93-3 1.0E+03 N 1.0E+04 4.5E+05NMethyl Isobutyl Ketone (4-methyl-2-pentanone) 108-10-1 6.2E+02 N 6.2E+03 1.1E+05NMethyl Methacrylate 80-62-6 1.5E+02 N 1.5E+03 1.0E+04NMethyl tert-Butyl Ether (MTBE) 1634-04-4 9.4E+00 C 9.4E+02 3.9E+03CMethylene Chloride 75-09-2 5.2E+00 C 5.2E+02 4.0E+02C Mercury (elemental) 7439-97-6 6.2E-02 N 6.2E-01 1.3E-01NNitrobenzene 98-95-3 4.2E-01 N 4.2E+00 4.3E+02NNitropropane, 2- 79-46-9 9.0E-04 C 9.0E-02 1.8E+00CNitroso-di-N-butylamine, N- 924-16-3 1.5E-03 C 1.5E-01 2.8E+01CPhenol 108-95-2 4.2E+01 N 4.2E+02 3.0E+06N Benzo[b]fluoranthene 205-99-2 8.7E-03 C 8.7E-01 3.2E+03C Chrysene 218-01-9 8.7E-02 C 8.7E+00 4.1E+03C Naphthalene 91-20-3 7.2E-02 C 6.2E+00 3.4E+01NStyrene 100-42-5 2.0E+02 N 2.0E+03 1.8E+03NTetrachloroethane, 1,1,1,2- 630-20-6 3.3E-01 C 3.3E+01 3.3E+01CTetrachloroethane, 1,1,2,2- 79-34-5 4.2E-02 C 4.2E+00 2.8E+01CTetrachloroethylene 127-18-4 4.1E-01 C 4.1E+01 5.7E+00CToluene 108-88-3 1.0E+03 N 1.0E+04 3.9E+03NTrichloro-1,2,2-trifluoroethane, 1,1,2- 76-13-1 6.2E+03 N 6.2E+04 2.8E+02NTrichlorobenzene, 1,2,4- 120-82-1 8.4E-01 N 8.4E+00 1.4E+01NTrichloroethane, 1,1,1- 71-55-6 1.0E+03 N 1.0E+04 1.5E+03NTrichloroethane, 1,1,2- 79-00-5 1.5E-01 C 1.5E+01 4.4E+01CTrichloroethylene 79-01-6 1.2E+00 C 1.2E+02 3.0E+01CTrichlorofluoromethane 75-69-4 1.5E+02 N 1.5E+03 3.7E+01NTrichloropropene, 1,2,3- 96-19-5 2.0E-01 N 2.0E+00 2.8E-01NTrimethylbenzene, 1,2,4- 95-63-6 1.5E+00 N 1.5E+01 5.8E+00NTrimethylbenzene, 1,3,5- 108-67-8 1.3E+00 N 1.3E+01 3.5E+00NVinyl Acetate 108-05-4 4.2E+01 N 4.2E+02 2.0E+03NVinyl Chloride 75-01-4 1.6E-01 C 1.1E+00 5.9E+00C 1. This table is subject to periodic revision. Verify this is the most current copy before use.2. Questions about this table should be directed to the appropriate project manager or risk assessor.Page 2 of 2 Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 APPENDIX IV (SOIL LABORATORY RERORT) October 14, 2009 LIMS USE: FR - SCOTT SPINNER LIMS OBJECT ID: 9252614 9252614 Project: Pace Project No.: RE: Mr. Scott SpinnerS&ME44 Buck Shoals RoadArden, NC 28704 1 FAIRVIEW RD 1411-09-040A Dear Mr. Spinner: Enclosed are the analytical results for sample(s) received by the laboratory on September 08, 2009. The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Charlotte Certification IDsWest Virginia Certification #: 357Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012 North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784South Carolina Certification #: 990060001South Carolina Drinking Water Cert. #: 990060003Tennessee Certification #: 04010 Asheville Certification IDsWest Virginia Certification #: 356Florida/NELAP Certification #: E87648Louisiana/LELAP Certification #: 03095Massachusetts Certification #: M-NC030New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9Connecticut Certification #: PH-0106 North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Tennessee Certification #: 2980Virginia Certification #: 00072North Carolina Drinking Water Certification #: 37712 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 9252614001 1 FAIR -SB3-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CALH 9252614002 1 FAIR -SB4-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614003 1 FAIR -SB5-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614004 1 FAIR -SB6-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CALH 9252614005 1 FAIR -SB7-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CALH 9252614006 1 FAIR -SB11-09-09 ASTM D2974-87 1 PASI-CTNM EPA 6010 13 PASI-ASHB EPA 7471 1 PASI-ASAJ EPA 8270 75 PASI-CBET 9252614007 1 FAIR -SB10-09-09 ASTM D2974-87 1 PASI-CTNM EPA 6010 13 PASI-ASHB EPA 7471 1 PASI-ASAJ EPA 8270 75 PASI-CBET 9252614008 1 FAIR -SB9-09-09 ASTM D2974-87 1 PASI-CTNM EPA 6010 13 PASI-ASHB EPA 7471 1 PASI-ASAJ EPA 8270 75 PASI-CBET 9252614009 1 FAIR -SB8-09-09 ASTM D2974-87 1 PASI-CTNM EPA 6010 13 PASI-ASHB EPA 7471 1 PASI-ASAJ EPA 8270 75 PASI-CBET 9252614010 1 FAIR -BK1-09-09 ASTM D2974-87 1 PASI-CTNM EPA 6010 13 PASI-ASHB EPA 7471 1 PASI-ASAJ 9252614011 1 FAIR -DUP1-09-09 ASTM D2974-87 1 PASI-CTNM EPA 6010 13 PASI-ASHB EPA 7471 1 PASI-ASAJ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 9252614012 1 FAIR -SB1-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CALH, BET 9252614013 1 FAIR -SB2-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614015 1 FAIR -TW3-SS1-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614016 1 FAIR -TW3-SS2-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614017 1 FAIR -DUP2-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614018 1 FAIR -TW1-SS1-09-09 9071B ASE 1 PASI-CEAJ ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614019 1 FAIR -DUP3-09-09 9071B ASE 1 PASI-CEAJ ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614020 1 FAIR -TW2-SS1-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614021 1 FAIR -TW2-SS2-09-09 ASTM D2974-87 1 PASI-CTNM EPA 8260 71 PASI-CDLK EPA 8270 75 PASI-CBET 9252614022 1 FAIR -TRIP BLANK 1-09-09 EPA 8260 63 PASI-CAW 9252614023 1 FAIR -TRIP BLANK 2-09-09 EPA 8260 63 PASI-CAW 9252614024 1 FAIR -EQUIP RINSATE 1-09-09 EPA 8260 63 PASI-CAW EPA 8270 75 PASI-CBET 9252614025 1 FAIR -EQUIP RINSATE 2-09-09 EPA 8260 63 PASI-CAW EPA 8270 75 PASI-CBET REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB3-09-09 Lab ID:9252614001 Collected:09/08/09 09:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 20 10/02/09 22:00 83-32-909/09/09 00:008610 Acenaphthylene ND ug/kg 20 10/02/09 22:00 208-96-809/09/09 00:008610 Aniline ND ug/kg 20 10/02/09 22:00 62-53-309/09/09 00:008610 Anthracene ND ug/kg 20 10/02/09 22:00 120-12-709/09/09 00:008610 Benzo(a)anthracene ND ug/kg 20 10/02/09 22:00 56-55-309/09/09 00:008610 Benzo(a)pyrene ND ug/kg 20 10/02/09 22:00 50-32-809/09/09 00:008610 Benzo(b)fluoranthene ND ug/kg 20 10/02/09 22:00 205-99-209/09/09 00:008610 Benzo(g,h,i)perylene ND ug/kg 20 10/02/09 22:00 191-24-209/09/09 00:008610 Benzo(k)fluoranthene ND ug/kg 20 10/02/09 22:00 207-08-909/09/09 00:008610 Benzoic Acid ND ug/kg 20 10/02/09 22:00 65-85-009/09/09 00:0043000 Benzyl alcohol ND ug/kg 20 10/02/09 22:00 100-51-609/09/09 00:0017200 4-Bromophenylphenyl ether ND ug/kg 20 10/02/09 22:00 101-55-309/09/09 00:008610 Butylbenzylphthalate ND ug/kg 20 10/02/09 22:00 85-68-709/09/09 00:008610 4-Chloro-3-methylphenol ND ug/kg 20 10/02/09 22:00 59-50-709/09/09 00:0017200 4-Chloroaniline ND ug/kg 20 10/02/09 22:00 106-47-809/09/09 00:0043000 bis(2-Chloroethoxy)methane ND ug/kg 20 10/02/09 22:00 111-91-109/09/09 00:008610 bis(2-Chloroethyl) ether ND ug/kg 20 10/02/09 22:00 111-44-409/09/09 00:008610 bis(2-Chloroisopropyl) ether ND ug/kg 20 10/02/09 22:00 108-60-109/09/09 00:008610 2-Chloronaphthalene ND ug/kg 20 10/02/09 22:00 91-58-709/09/09 00:008610 2-Chlorophenol ND ug/kg 20 10/02/09 22:00 95-57-809/09/09 00:008610 4-Chlorophenylphenyl ether ND ug/kg 20 10/02/09 22:00 7005-72-309/09/09 00:008610 Chrysene ND ug/kg 20 10/02/09 22:00 218-01-909/09/09 00:008610 Dibenz(a,h)anthracene ND ug/kg 20 10/02/09 22:00 53-70-309/09/09 00:008610 Dibenzofuran ND ug/kg 20 10/02/09 22:00 132-64-909/09/09 00:008610 1,2-Dichlorobenzene ND ug/kg 20 10/02/09 22:00 95-50-109/09/09 00:008610 1,3-Dichlorobenzene ND ug/kg 20 10/02/09 22:00 541-73-109/09/09 00:008610 1,4-Dichlorobenzene ND ug/kg 20 10/02/09 22:00 106-46-709/09/09 00:008610 3,3'-Dichlorobenzidine ND ug/kg 20 10/02/09 22:00 91-94-109/09/09 00:0043000 2,4-Dichlorophenol ND ug/kg 20 10/02/09 22:00 120-83-209/09/09 00:008610 Diethylphthalate ND ug/kg 20 10/02/09 22:00 84-66-209/09/09 00:008610 2,4-Dimethylphenol ND ug/kg 20 10/02/09 22:00 105-67-909/09/09 00:008610 Dimethylphthalate ND ug/kg 20 10/02/09 22:00 131-11-309/09/09 00:008610 Di-n-butylphthalate ND ug/kg 20 10/02/09 22:00 84-74-209/09/09 00:008610 4,6-Dinitro-2-methylphenol ND ug/kg 20 10/02/09 22:00 534-52-109/09/09 00:0017200 2,4-Dinitrophenol ND ug/kg 20 10/02/09 22:00 51-28-509/09/09 00:0043000 2,4-Dinitrotoluene ND ug/kg 20 10/02/09 22:00 121-14-209/09/09 00:008610 2,6-Dinitrotoluene ND ug/kg 20 10/02/09 22:00 606-20-209/09/09 00:008610 Di-n-octylphthalate ND ug/kg 20 10/02/09 22:00 117-84-009/09/09 00:008610 1,2-Diphenylhydrazine ND ug/kg 20 10/02/09 22:00 122-66-709/09/09 00:008610 bis(2-Ethylhexyl)phthalate ND ug/kg 20 10/02/09 22:00 117-81-709/09/09 00:008610 Fluoranthene ND ug/kg 20 10/02/09 22:00 206-44-009/09/09 00:008610 Fluorene ND ug/kg 20 10/02/09 22:00 86-73-709/09/09 00:008610 Hexachloro-1,3-butadiene ND ug/kg 20 10/02/09 22:00 87-68-309/09/09 00:008610 Hexachlorobenzene ND ug/kg 20 10/02/09 22:00 118-74-109/09/09 00:008610 Hexachlorocyclopentadiene ND ug/kg 20 10/02/09 22:00 77-47-409/09/09 00:008610 Hexachloroethane ND ug/kg 20 10/02/09 22:00 67-72-109/09/09 00:008610 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 5 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB3-09-09 Lab ID:9252614001 Collected:09/08/09 09:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 20 10/02/09 22:00 193-39-509/09/09 00:008610 Isophorone ND ug/kg 20 10/02/09 22:00 78-59-109/09/09 00:008610 1-Methylnaphthalene 24600 ug/kg 20 10/02/09 22:00 90-12-009/09/09 00:008610 2-Methylnaphthalene 32500 ug/kg 20 10/02/09 22:00 91-57-609/09/09 00:008610 2-Methylphenol(o-Cresol)ND ug/kg 20 10/02/09 22:00 95-48-709/09/09 00:008610 3&4-Methylphenol(m&p Cresol)ND ug/kg 20 10/02/09 22:0009/09/09 00:008610 Naphthalene 19200 ug/kg 20 10/02/09 22:00 91-20-309/09/09 00:008610 2-Nitroaniline ND ug/kg 20 10/02/09 22:00 88-74-409/09/09 00:0043000 3-Nitroaniline ND ug/kg 20 10/02/09 22:00 99-09-209/09/09 00:0043000 4-Nitroaniline ND ug/kg 20 10/02/09 22:00 100-01-609/09/09 00:0017200 Nitrobenzene ND ug/kg 20 10/02/09 22:00 98-95-309/09/09 00:008610 2-Nitrophenol ND ug/kg 20 10/02/09 22:00 88-75-509/09/09 00:008610 4-Nitrophenol ND ug/kg 20 10/02/09 22:00 100-02-709/09/09 00:0043000 N-Nitrosodimethylamine ND ug/kg 20 10/02/09 22:00 62-75-909/09/09 00:008610 N-Nitroso-di-n-propylamine ND ug/kg 20 10/02/09 22:00 621-64-709/09/09 00:008610 N-Nitrosodiphenylamine ND ug/kg 20 10/02/09 22:00 86-30-609/09/09 00:008610 Pentachlorophenol ND ug/kg 20 10/02/09 22:00 87-86-509/09/09 00:0043000 Phenanthrene ND ug/kg 20 10/02/09 22:00 85-01-809/09/09 00:008610 Phenol ND ug/kg 20 10/02/09 22:00 108-95-209/09/09 00:008610 Pyrene ND ug/kg 20 10/02/09 22:00 129-00-009/09/09 00:008610 1,2,4-Trichlorobenzene ND ug/kg 20 10/02/09 22:00 120-82-109/09/09 00:008610 2,4,5-Trichlorophenol ND ug/kg 20 10/02/09 22:00 95-95-409/09/09 00:008610 2,4,6-Trichlorophenol ND ug/kg 20 10/02/09 22:00 88-06-209/09/09 00:008610 Nitrobenzene-d5 (S)0 %20 10/02/09 22:00 4165-60-0 IS,S409/09/09 00:0030-150 2-Fluorobiphenyl (S)0 %20 10/02/09 22:00 321-60-8 S409/09/09 00:0046-120 Terphenyl-d14 (S)0 %20 10/02/09 22:00 1718-51-0 S409/09/09 00:0038-108 Phenol-d6 (S)0 %20 10/02/09 22:00 13127-88-3 S409/09/09 00:0035-120 2-Fluorophenol (S)0 %20 10/02/09 22:00 367-12-4 S409/09/09 00:0024-120 2,4,6-Tribromophenol (S)0 %20 10/02/09 22:00 118-79-6 S409/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 100 09/10/09 15:15 67-64-110400 Benzene ND ug/kg 100 09/10/09 15:15 71-43-2520 Bromobenzene ND ug/kg 100 09/10/09 15:15 108-86-1520 Bromochloromethane ND ug/kg 100 09/10/09 15:15 74-97-5520 Bromodichloromethane ND ug/kg 100 09/10/09 15:15 75-27-4520 Bromoform ND ug/kg 100 09/10/09 15:15 75-25-2520 Bromomethane ND ug/kg 100 09/10/09 15:15 74-83-91040 2-Butanone (MEK)ND ug/kg 100 09/10/09 15:15 78-93-310400 n-Butylbenzene 19200 ug/kg 100 09/10/09 15:15 104-51-8520 sec-Butylbenzene 18000 ug/kg 100 09/10/09 15:15 135-98-8520 tert-Butylbenzene ND ug/kg 100 09/10/09 15:15 98-06-6520 Carbon tetrachloride ND ug/kg 100 09/10/09 15:15 56-23-5520 Chlorobenzene ND ug/kg 100 09/10/09 15:15 108-90-7520 Chloroethane ND ug/kg 100 09/10/09 15:15 75-00-31040 Chloroform ND ug/kg 100 09/10/09 15:15 67-66-3520 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 6 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB3-09-09 Lab ID:9252614001 Collected:09/08/09 09:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 100 09/10/09 15:15 74-87-31040 2-Chlorotoluene ND ug/kg 100 09/10/09 15:15 95-49-8520 4-Chlorotoluene ND ug/kg 100 09/10/09 15:15 106-43-4520 1,2-Dibromo-3-chloropropane ND ug/kg 100 09/10/09 15:15 96-12-8520 Dibromochloromethane ND ug/kg 100 09/10/09 15:15 124-48-1520 1,2-Dibromoethane (EDB)ND ug/kg 100 09/10/09 15:15 106-93-4520 Dibromomethane ND ug/kg 100 09/10/09 15:15 74-95-3520 1,2-Dichlorobenzene ND ug/kg 100 09/10/09 15:15 95-50-1520 1,3-Dichlorobenzene ND ug/kg 100 09/10/09 15:15 541-73-1520 1,4-Dichlorobenzene ND ug/kg 100 09/10/09 15:15 106-46-7520 Dichlorodifluoromethane ND ug/kg 100 09/10/09 15:15 75-71-81040 1,1-Dichloroethane ND ug/kg 100 09/10/09 15:15 75-34-3520 1,2-Dichloroethane ND ug/kg 100 09/10/09 15:15 107-06-2520 1,1-Dichloroethene ND ug/kg 100 09/10/09 15:15 75-35-4520 cis-1,2-Dichloroethene ND ug/kg 100 09/10/09 15:15 156-59-2520 trans-1,2-Dichloroethene ND ug/kg 100 09/10/09 15:15 156-60-5520 1,2-Dichloropropane ND ug/kg 100 09/10/09 15:15 78-87-5520 1,3-Dichloropropane ND ug/kg 100 09/10/09 15:15 142-28-9520 2,2-Dichloropropane ND ug/kg 100 09/10/09 15:15 594-20-7520 1,1-Dichloropropene ND ug/kg 100 09/10/09 15:15 563-58-6520 cis-1,3-Dichloropropene ND ug/kg 100 09/10/09 15:15 10061-01-5520 trans-1,3-Dichloropropene ND ug/kg 100 09/10/09 15:15 10061-02-6520 Diisopropyl ether ND ug/kg 100 09/10/09 15:15 108-20-3520 Ethylbenzene 4560 ug/kg 100 09/10/09 15:15 100-41-4520 Hexachloro-1,3-butadiene ND ug/kg 100 09/10/09 15:15 87-68-3520 2-Hexanone ND ug/kg 100 09/10/09 15:15 591-78-65200 Isopropylbenzene (Cumene)6950 ug/kg 100 09/10/09 15:15 98-82-8520 p-Isopropyltoluene 16300 ug/kg 100 09/10/09 15:15 99-87-6520 Methylene Chloride ND ug/kg 100 09/10/09 15:15 75-09-22080 4-Methyl-2-pentanone (MIBK)ND ug/kg 100 09/10/09 15:15 108-10-15200 Methyl-tert-butyl ether ND ug/kg 100 09/10/09 15:15 1634-04-4520 Naphthalene 22100 ug/kg 1000 09/11/09 10:54 91-20-35200 n-Propylbenzene 10700 ug/kg 100 09/10/09 15:15 103-65-1520 Styrene ND ug/kg 100 09/10/09 15:15 100-42-5520 1,1,1,2-Tetrachloroethane ND ug/kg 100 09/10/09 15:15 630-20-6520 1,1,2,2-Tetrachloroethane ND ug/kg 100 09/10/09 15:15 79-34-5520 Tetrachloroethene ND ug/kg 100 09/10/09 15:15 127-18-4520 Toluene 1160 ug/kg 100 09/10/09 15:15 108-88-3520 1,2,3-Trichlorobenzene ND ug/kg 100 09/10/09 15:15 87-61-6520 1,2,4-Trichlorobenzene ND ug/kg 100 09/10/09 15:15 120-82-1520 1,1,1-Trichloroethane ND ug/kg 100 09/10/09 15:15 71-55-6520 1,1,2-Trichloroethane ND ug/kg 100 09/10/09 15:15 79-00-5520 Trichloroethene ND ug/kg 100 09/10/09 15:15 79-01-6520 Trichlorofluoromethane ND ug/kg 100 09/10/09 15:15 75-69-4520 1,2,3-Trichloropropane ND ug/kg 100 09/10/09 15:15 96-18-4520 1,2,4-Trimethylbenzene 86000 ug/kg 1000 09/11/09 10:54 95-63-65200 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 7 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB3-09-09 Lab ID:9252614001 Collected:09/08/09 09:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene 10500 ug/kg 100 09/10/09 15:15 108-67-8520 Vinyl acetate ND ug/kg 100 09/10/09 15:15 108-05-45200 Vinyl chloride ND ug/kg 100 09/10/09 15:15 75-01-41040 Xylene (Total)8470 ug/kg 100 09/10/09 15:15 1330-20-71040 m&p-Xylene 7200 ug/kg 100 09/10/09 15:15 1330-20-71040 o-Xylene 1270 ug/kg 100 09/10/09 15:15 95-47-6520 Dibromofluoromethane (S)103 %100 09/10/09 15:15 1868-53-779-116 Toluene-d8 (S)103 %100 09/10/09 15:15 2037-26-588-110 4-Bromofluorobenzene (S)107 %100 09/10/09 15:15 460-00-474-115 1,2-Dichloroethane-d4 (S)105 %100 09/10/09 15:15 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 23.3 %1 09/09/09 13:380.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 8 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB4-09-09 Lab ID:9252614002 Collected:09/08/09 09:25 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/22/09 23:18 83-32-909/09/09 00:00373 Acenaphthylene ND ug/kg 1 09/22/09 23:18 208-96-809/09/09 00:00373 Aniline ND ug/kg 1 09/22/09 23:18 62-53-309/09/09 00:00373 Anthracene 426 ug/kg 1 09/22/09 23:18 120-12-709/09/09 00:00373 Benzo(a)anthracene 628 ug/kg 1 09/22/09 23:18 56-55-309/09/09 00:00373 Benzo(a)pyrene ND ug/kg 1 09/22/09 23:18 50-32-809/09/09 00:00373 Benzo(b)fluoranthene ND ug/kg 1 09/22/09 23:18 205-99-209/09/09 00:00373 Benzo(g,h,i)perylene ND ug/kg 1 09/22/09 23:18 191-24-209/09/09 00:00373 Benzo(k)fluoranthene ND ug/kg 1 09/22/09 23:18 207-08-909/09/09 00:00373 Benzoic Acid ND ug/kg 1 09/22/09 23:18 65-85-009/09/09 00:001860 Benzyl alcohol ND ug/kg 1 09/22/09 23:18 100-51-609/09/09 00:00745 4-Bromophenylphenyl ether ND ug/kg 1 09/22/09 23:18 101-55-309/09/09 00:00373 Butylbenzylphthalate ND ug/kg 1 09/22/09 23:18 85-68-709/09/09 00:00373 4-Chloro-3-methylphenol ND ug/kg 1 09/22/09 23:18 59-50-709/09/09 00:00745 4-Chloroaniline ND ug/kg 1 09/22/09 23:18 106-47-809/09/09 00:001860 bis(2-Chloroethoxy)methane ND ug/kg 1 09/22/09 23:18 111-91-109/09/09 00:00373 bis(2-Chloroethyl) ether ND ug/kg 1 09/22/09 23:18 111-44-409/09/09 00:00373 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/22/09 23:18 108-60-109/09/09 00:00373 2-Chloronaphthalene ND ug/kg 1 09/22/09 23:18 91-58-709/09/09 00:00373 2-Chlorophenol ND ug/kg 1 09/22/09 23:18 95-57-809/09/09 00:00373 4-Chlorophenylphenyl ether ND ug/kg 1 09/22/09 23:18 7005-72-309/09/09 00:00373 Chrysene 607 ug/kg 1 09/22/09 23:18 218-01-909/09/09 00:00373 Dibenz(a,h)anthracene ND ug/kg 1 09/22/09 23:18 53-70-309/09/09 00:00373 Dibenzofuran ND ug/kg 1 09/22/09 23:18 132-64-909/09/09 00:00373 1,2-Dichlorobenzene ND ug/kg 1 09/22/09 23:18 95-50-109/09/09 00:00373 1,3-Dichlorobenzene ND ug/kg 1 09/22/09 23:18 541-73-109/09/09 00:00373 1,4-Dichlorobenzene ND ug/kg 1 09/22/09 23:18 106-46-709/09/09 00:00373 3,3'-Dichlorobenzidine ND ug/kg 1 09/22/09 23:18 91-94-109/09/09 00:001860 2,4-Dichlorophenol ND ug/kg 1 09/22/09 23:18 120-83-209/09/09 00:00373 Diethylphthalate ND ug/kg 1 09/22/09 23:18 84-66-209/09/09 00:00373 2,4-Dimethylphenol ND ug/kg 1 09/22/09 23:18 105-67-909/09/09 00:00373 Dimethylphthalate ND ug/kg 1 09/22/09 23:18 131-11-309/09/09 00:00373 Di-n-butylphthalate ND ug/kg 1 09/22/09 23:18 84-74-209/09/09 00:00373 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/22/09 23:18 534-52-109/09/09 00:00745 2,4-Dinitrophenol ND ug/kg 1 09/22/09 23:18 51-28-509/09/09 00:001860 2,4-Dinitrotoluene ND ug/kg 1 09/22/09 23:18 121-14-209/09/09 00:00373 2,6-Dinitrotoluene ND ug/kg 1 09/22/09 23:18 606-20-209/09/09 00:00373 Di-n-octylphthalate ND ug/kg 1 09/22/09 23:18 117-84-009/09/09 00:00373 1,2-Diphenylhydrazine ND ug/kg 1 09/22/09 23:18 122-66-709/09/09 00:00373 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/22/09 23:18 117-81-709/09/09 00:00373 Fluoranthene 494 ug/kg 1 09/22/09 23:18 206-44-009/09/09 00:00373 Fluorene ND ug/kg 1 09/22/09 23:18 86-73-709/09/09 00:00373 Hexachloro-1,3-butadiene ND ug/kg 1 09/22/09 23:18 87-68-309/09/09 00:00373 Hexachlorobenzene ND ug/kg 1 09/22/09 23:18 118-74-109/09/09 00:00373 Hexachlorocyclopentadiene ND ug/kg 1 09/22/09 23:18 77-47-409/09/09 00:00373 Hexachloroethane ND ug/kg 1 09/22/09 23:18 67-72-109/09/09 00:00373 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 9 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB4-09-09 Lab ID:9252614002 Collected:09/08/09 09:25 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/22/09 23:18 193-39-509/09/09 00:00373 Isophorone ND ug/kg 1 09/22/09 23:18 78-59-109/09/09 00:00373 1-Methylnaphthalene 6590 ug/kg 1 09/22/09 23:18 90-12-009/09/09 00:00373 2-Methylnaphthalene 9310 ug/kg 1 09/22/09 23:18 91-57-609/09/09 00:00373 2-Methylphenol(o-Cresol)ND ug/kg 1 09/22/09 23:18 95-48-709/09/09 00:00373 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/22/09 23:1809/09/09 00:00373 Naphthalene 7170 ug/kg 1 09/22/09 23:18 91-20-309/09/09 00:00373 2-Nitroaniline ND ug/kg 1 09/22/09 23:18 88-74-409/09/09 00:001860 3-Nitroaniline ND ug/kg 1 09/22/09 23:18 99-09-209/09/09 00:001860 4-Nitroaniline ND ug/kg 1 09/22/09 23:18 100-01-609/09/09 00:00745 Nitrobenzene ND ug/kg 1 09/22/09 23:18 98-95-309/09/09 00:00373 2-Nitrophenol ND ug/kg 1 09/22/09 23:18 88-75-509/09/09 00:00373 4-Nitrophenol ND ug/kg 1 09/22/09 23:18 100-02-709/09/09 00:001860 N-Nitrosodimethylamine ND ug/kg 1 09/22/09 23:18 62-75-909/09/09 00:00373 N-Nitroso-di-n-propylamine ND ug/kg 1 09/22/09 23:18 621-64-709/09/09 00:00373 N-Nitrosodiphenylamine ND ug/kg 1 09/22/09 23:18 86-30-609/09/09 00:00373 Pentachlorophenol ND ug/kg 1 09/22/09 23:18 87-86-509/09/09 00:001860 Phenanthrene 2850 ug/kg 1 09/22/09 23:18 85-01-809/09/09 00:00373 Phenol ND ug/kg 1 09/22/09 23:18 108-95-209/09/09 00:00373 Pyrene 743 ug/kg 1 09/22/09 23:18 129-00-009/09/09 00:00373 1,2,4-Trichlorobenzene ND ug/kg 1 09/22/09 23:18 120-82-109/09/09 00:00373 2,4,5-Trichlorophenol ND ug/kg 1 09/22/09 23:18 95-95-409/09/09 00:00373 2,4,6-Trichlorophenol ND ug/kg 1 09/22/09 23:18 88-06-209/09/09 00:00373 Nitrobenzene-d5 (S)55 %1 09/22/09 23:18 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)59 %1 09/22/09 23:18 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)105 %1 09/22/09 23:18 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)26 %1 09/22/09 23:18 13127-88-3 1g09/09/09 00:0035-120 2-Fluorophenol (S)31 %1 09/22/09 23:18 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)47 %1 09/22/09 23:18 118-79-609/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/10/09 15:33 67-64-17130 Benzene 1350 ug/kg 50 09/10/09 15:33 71-43-2356 Bromobenzene ND ug/kg 50 09/10/09 15:33 108-86-1356 Bromochloromethane ND ug/kg 50 09/10/09 15:33 74-97-5356 Bromodichloromethane ND ug/kg 50 09/10/09 15:33 75-27-4356 Bromoform ND ug/kg 50 09/10/09 15:33 75-25-2356 Bromomethane ND ug/kg 50 09/10/09 15:33 74-83-9713 2-Butanone (MEK)ND ug/kg 50 09/10/09 15:33 78-93-37130 n-Butylbenzene ND ug/kg 50 09/10/09 15:33 104-51-8356 sec-Butylbenzene ND ug/kg 50 09/10/09 15:33 135-98-8356 tert-Butylbenzene ND ug/kg 50 09/10/09 15:33 98-06-6356 Carbon tetrachloride ND ug/kg 50 09/10/09 15:33 56-23-5356 Chlorobenzene ND ug/kg 50 09/10/09 15:33 108-90-7356 Chloroethane ND ug/kg 50 09/10/09 15:33 75-00-3713 Chloroform ND ug/kg 50 09/10/09 15:33 67-66-3356 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 10 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB4-09-09 Lab ID:9252614002 Collected:09/08/09 09:25 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 50 09/10/09 15:33 74-87-3713 2-Chlorotoluene ND ug/kg 50 09/10/09 15:33 95-49-8356 4-Chlorotoluene ND ug/kg 50 09/10/09 15:33 106-43-4356 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/10/09 15:33 96-12-8356 Dibromochloromethane ND ug/kg 50 09/10/09 15:33 124-48-1356 1,2-Dibromoethane (EDB)ND ug/kg 50 09/10/09 15:33 106-93-4356 Dibromomethane ND ug/kg 50 09/10/09 15:33 74-95-3356 1,2-Dichlorobenzene ND ug/kg 50 09/10/09 15:33 95-50-1356 1,3-Dichlorobenzene ND ug/kg 50 09/10/09 15:33 541-73-1356 1,4-Dichlorobenzene ND ug/kg 50 09/10/09 15:33 106-46-7356 Dichlorodifluoromethane ND ug/kg 50 09/10/09 15:33 75-71-8713 1,1-Dichloroethane ND ug/kg 50 09/10/09 15:33 75-34-3356 1,2-Dichloroethane ND ug/kg 50 09/10/09 15:33 107-06-2356 1,1-Dichloroethene ND ug/kg 50 09/10/09 15:33 75-35-4356 cis-1,2-Dichloroethene ND ug/kg 50 09/10/09 15:33 156-59-2356 trans-1,2-Dichloroethene ND ug/kg 50 09/10/09 15:33 156-60-5356 1,2-Dichloropropane ND ug/kg 50 09/10/09 15:33 78-87-5356 1,3-Dichloropropane ND ug/kg 50 09/10/09 15:33 142-28-9356 2,2-Dichloropropane ND ug/kg 50 09/10/09 15:33 594-20-7356 1,1-Dichloropropene ND ug/kg 50 09/10/09 15:33 563-58-6356 cis-1,3-Dichloropropene ND ug/kg 50 09/10/09 15:33 10061-01-5356 trans-1,3-Dichloropropene ND ug/kg 50 09/10/09 15:33 10061-02-6356 Diisopropyl ether ND ug/kg 50 09/10/09 15:33 108-20-3356 Ethylbenzene 981 ug/kg 50 09/10/09 15:33 100-41-4356 Hexachloro-1,3-butadiene ND ug/kg 50 09/10/09 15:33 87-68-3356 2-Hexanone ND ug/kg 50 09/10/09 15:33 591-78-63560 Isopropylbenzene (Cumene)ND ug/kg 50 09/10/09 15:33 98-82-8356 p-Isopropyltoluene ND ug/kg 50 09/10/09 15:33 99-87-6356 Methylene Chloride ND ug/kg 50 09/10/09 15:33 75-09-21430 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/10/09 15:33 108-10-13560 Methyl-tert-butyl ether ND ug/kg 50 09/10/09 15:33 1634-04-4356 Naphthalene 2950 ug/kg 50 09/10/09 15:33 91-20-3356 n-Propylbenzene ND ug/kg 50 09/10/09 15:33 103-65-1356 Styrene ND ug/kg 50 09/10/09 15:33 100-42-5356 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/10/09 15:33 630-20-6356 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/10/09 15:33 79-34-5356 Tetrachloroethene ND ug/kg 50 09/10/09 15:33 127-18-4356 Toluene 7120 ug/kg 50 09/10/09 15:33 108-88-3356 1,2,3-Trichlorobenzene ND ug/kg 50 09/10/09 15:33 87-61-6356 1,2,4-Trichlorobenzene ND ug/kg 50 09/10/09 15:33 120-82-1356 1,1,1-Trichloroethane ND ug/kg 50 09/10/09 15:33 71-55-6356 1,1,2-Trichloroethane ND ug/kg 50 09/10/09 15:33 79-00-5356 Trichloroethene ND ug/kg 50 09/10/09 15:33 79-01-6356 Trichlorofluoromethane ND ug/kg 50 09/10/09 15:33 75-69-4356 1,2,3-Trichloropropane ND ug/kg 50 09/10/09 15:33 96-18-4356 1,2,4-Trimethylbenzene 1920 ug/kg 50 09/10/09 15:33 95-63-6356 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 11 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB4-09-09 Lab ID:9252614002 Collected:09/08/09 09:25 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene 502 ug/kg 50 09/10/09 15:33 108-67-8356 Vinyl acetate ND ug/kg 50 09/10/09 15:33 108-05-43560 Vinyl chloride ND ug/kg 50 09/10/09 15:33 75-01-4713 Xylene (Total)8260 ug/kg 50 09/10/09 15:33 1330-20-7713 m&p-Xylene 5430 ug/kg 50 09/10/09 15:33 1330-20-7713 o-Xylene 2830 ug/kg 50 09/10/09 15:33 95-47-6356 Dibromofluoromethane (S)98 %50 09/10/09 15:33 1868-53-779-116 Toluene-d8 (S)101 %50 09/10/09 15:33 2037-26-588-110 4-Bromofluorobenzene (S)97 %50 09/10/09 15:33 460-00-474-115 1,2-Dichloroethane-d4 (S)93 %50 09/10/09 15:33 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 11.4 %1 09/09/09 13:380.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 12 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB5-09-09 Lab ID:9252614003 Collected:09/08/09 09:30 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/22/09 23:42 83-32-909/09/09 00:00351 Acenaphthylene ND ug/kg 1 09/22/09 23:42 208-96-809/09/09 00:00351 Aniline ND ug/kg 1 09/22/09 23:42 62-53-309/09/09 00:00351 Anthracene ND ug/kg 1 09/22/09 23:42 120-12-709/09/09 00:00351 Benzo(a)anthracene ND ug/kg 1 09/22/09 23:42 56-55-309/09/09 00:00351 Benzo(a)pyrene ND ug/kg 1 09/22/09 23:42 50-32-809/09/09 00:00351 Benzo(b)fluoranthene ND ug/kg 1 09/22/09 23:42 205-99-209/09/09 00:00351 Benzo(g,h,i)perylene ND ug/kg 1 09/22/09 23:42 191-24-209/09/09 00:00351 Benzo(k)fluoranthene ND ug/kg 1 09/22/09 23:42 207-08-909/09/09 00:00351 Benzoic Acid ND ug/kg 1 09/22/09 23:42 65-85-009/09/09 00:001750 Benzyl alcohol ND ug/kg 1 09/22/09 23:42 100-51-609/09/09 00:00701 4-Bromophenylphenyl ether ND ug/kg 1 09/22/09 23:42 101-55-309/09/09 00:00351 Butylbenzylphthalate ND ug/kg 1 09/22/09 23:42 85-68-709/09/09 00:00351 4-Chloro-3-methylphenol ND ug/kg 1 09/22/09 23:42 59-50-709/09/09 00:00701 4-Chloroaniline ND ug/kg 1 09/22/09 23:42 106-47-809/09/09 00:001750 bis(2-Chloroethoxy)methane ND ug/kg 1 09/22/09 23:42 111-91-109/09/09 00:00351 bis(2-Chloroethyl) ether ND ug/kg 1 09/22/09 23:42 111-44-409/09/09 00:00351 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/22/09 23:42 108-60-109/09/09 00:00351 2-Chloronaphthalene ND ug/kg 1 09/22/09 23:42 91-58-709/09/09 00:00351 2-Chlorophenol ND ug/kg 1 09/22/09 23:42 95-57-809/09/09 00:00351 4-Chlorophenylphenyl ether ND ug/kg 1 09/22/09 23:42 7005-72-309/09/09 00:00351 Chrysene ND ug/kg 1 09/22/09 23:42 218-01-909/09/09 00:00351 Dibenz(a,h)anthracene ND ug/kg 1 09/22/09 23:42 53-70-309/09/09 00:00351 Dibenzofuran ND ug/kg 1 09/22/09 23:42 132-64-909/09/09 00:00351 1,2-Dichlorobenzene ND ug/kg 1 09/22/09 23:42 95-50-109/09/09 00:00351 1,3-Dichlorobenzene ND ug/kg 1 09/22/09 23:42 541-73-109/09/09 00:00351 1,4-Dichlorobenzene ND ug/kg 1 09/22/09 23:42 106-46-709/09/09 00:00351 3,3'-Dichlorobenzidine ND ug/kg 1 09/22/09 23:42 91-94-109/09/09 00:001750 2,4-Dichlorophenol ND ug/kg 1 09/22/09 23:42 120-83-209/09/09 00:00351 Diethylphthalate ND ug/kg 1 09/22/09 23:42 84-66-209/09/09 00:00351 2,4-Dimethylphenol ND ug/kg 1 09/22/09 23:42 105-67-909/09/09 00:00351 Dimethylphthalate ND ug/kg 1 09/22/09 23:42 131-11-309/09/09 00:00351 Di-n-butylphthalate ND ug/kg 1 09/22/09 23:42 84-74-209/09/09 00:00351 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/22/09 23:42 534-52-109/09/09 00:00701 2,4-Dinitrophenol ND ug/kg 1 09/22/09 23:42 51-28-509/09/09 00:001750 2,4-Dinitrotoluene ND ug/kg 1 09/22/09 23:42 121-14-209/09/09 00:00351 2,6-Dinitrotoluene ND ug/kg 1 09/22/09 23:42 606-20-209/09/09 00:00351 Di-n-octylphthalate ND ug/kg 1 09/22/09 23:42 117-84-009/09/09 00:00351 1,2-Diphenylhydrazine ND ug/kg 1 09/22/09 23:42 122-66-709/09/09 00:00351 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/22/09 23:42 117-81-709/09/09 00:00351 Fluoranthene ND ug/kg 1 09/22/09 23:42 206-44-009/09/09 00:00351 Fluorene ND ug/kg 1 09/22/09 23:42 86-73-709/09/09 00:00351 Hexachloro-1,3-butadiene ND ug/kg 1 09/22/09 23:42 87-68-309/09/09 00:00351 Hexachlorobenzene ND ug/kg 1 09/22/09 23:42 118-74-109/09/09 00:00351 Hexachlorocyclopentadiene ND ug/kg 1 09/22/09 23:42 77-47-409/09/09 00:00351 Hexachloroethane ND ug/kg 1 09/22/09 23:42 67-72-109/09/09 00:00351 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 13 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB5-09-09 Lab ID:9252614003 Collected:09/08/09 09:30 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/22/09 23:42 193-39-509/09/09 00:00351 Isophorone ND ug/kg 1 09/22/09 23:42 78-59-109/09/09 00:00351 1-Methylnaphthalene ND ug/kg 1 09/22/09 23:42 90-12-009/09/09 00:00351 2-Methylnaphthalene ND ug/kg 1 09/22/09 23:42 91-57-609/09/09 00:00351 2-Methylphenol(o-Cresol)ND ug/kg 1 09/22/09 23:42 95-48-709/09/09 00:00351 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/22/09 23:4209/09/09 00:00351 Naphthalene ND ug/kg 1 09/22/09 23:42 91-20-309/09/09 00:00351 2-Nitroaniline ND ug/kg 1 09/22/09 23:42 88-74-409/09/09 00:001750 3-Nitroaniline ND ug/kg 1 09/22/09 23:42 99-09-209/09/09 00:001750 4-Nitroaniline ND ug/kg 1 09/22/09 23:42 100-01-609/09/09 00:00701 Nitrobenzene ND ug/kg 1 09/22/09 23:42 98-95-309/09/09 00:00351 2-Nitrophenol ND ug/kg 1 09/22/09 23:42 88-75-509/09/09 00:00351 4-Nitrophenol ND ug/kg 1 09/22/09 23:42 100-02-709/09/09 00:001750 N-Nitrosodimethylamine ND ug/kg 1 09/22/09 23:42 62-75-909/09/09 00:00351 N-Nitroso-di-n-propylamine ND ug/kg 1 09/22/09 23:42 621-64-709/09/09 00:00351 N-Nitrosodiphenylamine ND ug/kg 1 09/22/09 23:42 86-30-609/09/09 00:00351 Pentachlorophenol ND ug/kg 1 09/22/09 23:42 87-86-509/09/09 00:001750 Phenanthrene ND ug/kg 1 09/22/09 23:42 85-01-809/09/09 00:00351 Phenol ND ug/kg 1 09/22/09 23:42 108-95-209/09/09 00:00351 Pyrene ND ug/kg 1 09/22/09 23:42 129-00-009/09/09 00:00351 1,2,4-Trichlorobenzene ND ug/kg 1 09/22/09 23:42 120-82-109/09/09 00:00351 2,4,5-Trichlorophenol ND ug/kg 1 09/22/09 23:42 95-95-409/09/09 00:00351 2,4,6-Trichlorophenol ND ug/kg 1 09/22/09 23:42 88-06-209/09/09 00:00351 Nitrobenzene-d5 (S)48 %1 09/22/09 23:42 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)48 %1 09/22/09 23:42 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)59 %1 09/22/09 23:42 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)37 %1 09/22/09 23:42 13127-88-309/09/09 00:0035-120 2-Fluorophenol (S)35 %1 09/22/09 23:42 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)52 %1 09/22/09 23:42 118-79-609/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 250 09/10/09 16:10 67-64-121100 Benzene ND ug/kg 250 09/10/09 16:10 71-43-21060 Bromobenzene ND ug/kg 250 09/10/09 16:10 108-86-11060 Bromochloromethane ND ug/kg 250 09/10/09 16:10 74-97-51060 Bromodichloromethane ND ug/kg 250 09/10/09 16:10 75-27-41060 Bromoform ND ug/kg 250 09/10/09 16:10 75-25-21060 Bromomethane ND ug/kg 250 09/10/09 16:10 74-83-92110 2-Butanone (MEK)ND ug/kg 250 09/10/09 16:10 78-93-321100 n-Butylbenzene ND ug/kg 250 09/10/09 16:10 104-51-81060 sec-Butylbenzene ND ug/kg 250 09/10/09 16:10 135-98-81060 tert-Butylbenzene ND ug/kg 250 09/10/09 16:10 98-06-61060 Carbon tetrachloride ND ug/kg 250 09/10/09 16:10 56-23-51060 Chlorobenzene ND ug/kg 250 09/10/09 16:10 108-90-71060 Chloroethane ND ug/kg 250 09/10/09 16:10 75-00-32110 Chloroform ND ug/kg 250 09/10/09 16:10 67-66-31060 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 14 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB5-09-09 Lab ID:9252614003 Collected:09/08/09 09:30 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 250 09/10/09 16:10 74-87-32110 2-Chlorotoluene ND ug/kg 250 09/10/09 16:10 95-49-81060 4-Chlorotoluene ND ug/kg 250 09/10/09 16:10 106-43-41060 1,2-Dibromo-3-chloropropane ND ug/kg 250 09/10/09 16:10 96-12-81060 Dibromochloromethane ND ug/kg 250 09/10/09 16:10 124-48-11060 1,2-Dibromoethane (EDB)ND ug/kg 250 09/10/09 16:10 106-93-41060 Dibromomethane ND ug/kg 250 09/10/09 16:10 74-95-31060 1,2-Dichlorobenzene ND ug/kg 250 09/10/09 16:10 95-50-11060 1,3-Dichlorobenzene ND ug/kg 250 09/10/09 16:10 541-73-11060 1,4-Dichlorobenzene ND ug/kg 250 09/10/09 16:10 106-46-71060 Dichlorodifluoromethane ND ug/kg 250 09/10/09 16:10 75-71-82110 1,1-Dichloroethane ND ug/kg 250 09/10/09 16:10 75-34-31060 1,2-Dichloroethane ND ug/kg 250 09/10/09 16:10 107-06-21060 1,1-Dichloroethene ND ug/kg 250 09/10/09 16:10 75-35-41060 cis-1,2-Dichloroethene ND ug/kg 250 09/10/09 16:10 156-59-21060 trans-1,2-Dichloroethene ND ug/kg 250 09/10/09 16:10 156-60-51060 1,2-Dichloropropane ND ug/kg 250 09/10/09 16:10 78-87-51060 1,3-Dichloropropane ND ug/kg 250 09/10/09 16:10 142-28-91060 2,2-Dichloropropane ND ug/kg 250 09/10/09 16:10 594-20-71060 1,1-Dichloropropene ND ug/kg 250 09/10/09 16:10 563-58-61060 cis-1,3-Dichloropropene ND ug/kg 250 09/10/09 16:10 10061-01-51060 trans-1,3-Dichloropropene ND ug/kg 250 09/10/09 16:10 10061-02-61060 Diisopropyl ether ND ug/kg 250 09/10/09 16:10 108-20-31060 Ethylbenzene 1780 ug/kg 250 09/10/09 16:10 100-41-41060 Hexachloro-1,3-butadiene ND ug/kg 250 09/10/09 16:10 87-68-31060 2-Hexanone ND ug/kg 250 09/10/09 16:10 591-78-610600 Isopropylbenzene (Cumene)ND ug/kg 250 09/10/09 16:10 98-82-81060 p-Isopropyltoluene 2640 ug/kg 250 09/10/09 16:10 99-87-61060 Methylene Chloride ND ug/kg 250 09/10/09 16:10 75-09-24220 4-Methyl-2-pentanone (MIBK)ND ug/kg 250 09/10/09 16:10 108-10-110600 Methyl-tert-butyl ether ND ug/kg 250 09/10/09 16:10 1634-04-41060 Naphthalene 3700 ug/kg 250 09/10/09 16:10 91-20-31060 n-Propylbenzene 1480 ug/kg 250 09/10/09 16:10 103-65-11060 Styrene ND ug/kg 250 09/10/09 16:10 100-42-51060 1,1,1,2-Tetrachloroethane ND ug/kg 250 09/10/09 16:10 630-20-61060 1,1,2,2-Tetrachloroethane ND ug/kg 250 09/10/09 16:10 79-34-51060 Tetrachloroethene ND ug/kg 250 09/10/09 16:10 127-18-41060 Toluene 1140 ug/kg 250 09/10/09 16:10 108-88-31060 1,2,3-Trichlorobenzene ND ug/kg 250 09/10/09 16:10 87-61-61060 1,2,4-Trichlorobenzene ND ug/kg 250 09/10/09 16:10 120-82-11060 1,1,1-Trichloroethane ND ug/kg 250 09/10/09 16:10 71-55-61060 1,1,2-Trichloroethane ND ug/kg 250 09/10/09 16:10 79-00-51060 Trichloroethene ND ug/kg 250 09/10/09 16:10 79-01-61060 Trichlorofluoromethane ND ug/kg 250 09/10/09 16:10 75-69-41060 1,2,3-Trichloropropane ND ug/kg 250 09/10/09 16:10 96-18-41060 1,2,4-Trimethylbenzene 26900 ug/kg 250 09/10/09 16:10 95-63-61060 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 15 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB5-09-09 Lab ID:9252614003 Collected:09/08/09 09:30 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene 9240 ug/kg 250 09/10/09 16:10 108-67-81060 Vinyl acetate ND ug/kg 250 09/10/09 16:10 108-05-410600 Vinyl chloride ND ug/kg 250 09/10/09 16:10 75-01-42110 Xylene (Total)14900 ug/kg 250 09/10/09 16:10 1330-20-72110 m&p-Xylene 12700 ug/kg 250 09/10/09 16:10 1330-20-72110 o-Xylene 2220 ug/kg 250 09/10/09 16:10 95-47-61060 Dibromofluoromethane (S)102 %250 09/10/09 16:10 1868-53-779-116 Toluene-d8 (S)101 %250 09/10/09 16:10 2037-26-588-110 4-Bromofluorobenzene (S)99 %250 09/10/09 16:10 460-00-474-115 1,2-Dichloroethane-d4 (S)107 %250 09/10/09 16:10 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 5.9 %1 09/09/09 13:390.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 16 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB6-09-09 Lab ID:9252614004 Collected:09/08/09 11:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 20 10/02/09 22:26 83-32-909/09/09 00:007760 Acenaphthylene ND ug/kg 20 10/02/09 22:26 208-96-809/09/09 00:007760 Aniline ND ug/kg 20 10/02/09 22:26 62-53-309/09/09 00:007760 Anthracene ND ug/kg 20 10/02/09 22:26 120-12-709/09/09 00:007760 Benzo(a)anthracene ND ug/kg 20 10/02/09 22:26 56-55-309/09/09 00:007760 Benzo(a)pyrene ND ug/kg 20 10/02/09 22:26 50-32-809/09/09 00:007760 Benzo(b)fluoranthene ND ug/kg 20 10/02/09 22:26 205-99-209/09/09 00:007760 Benzo(g,h,i)perylene ND ug/kg 20 10/02/09 22:26 191-24-209/09/09 00:007760 Benzo(k)fluoranthene ND ug/kg 20 10/02/09 22:26 207-08-909/09/09 00:007760 Benzoic Acid ND ug/kg 20 10/02/09 22:26 65-85-009/09/09 00:0038800 Benzyl alcohol ND ug/kg 20 10/02/09 22:26 100-51-609/09/09 00:0015500 4-Bromophenylphenyl ether ND ug/kg 20 10/02/09 22:26 101-55-309/09/09 00:007760 Butylbenzylphthalate ND ug/kg 20 10/02/09 22:26 85-68-709/09/09 00:007760 4-Chloro-3-methylphenol ND ug/kg 20 10/02/09 22:26 59-50-709/09/09 00:0015500 4-Chloroaniline ND ug/kg 20 10/02/09 22:26 106-47-809/09/09 00:0038800 bis(2-Chloroethoxy)methane ND ug/kg 20 10/02/09 22:26 111-91-109/09/09 00:007760 bis(2-Chloroethyl) ether ND ug/kg 20 10/02/09 22:26 111-44-409/09/09 00:007760 bis(2-Chloroisopropyl) ether ND ug/kg 20 10/02/09 22:26 108-60-109/09/09 00:007760 2-Chloronaphthalene ND ug/kg 20 10/02/09 22:26 91-58-709/09/09 00:007760 2-Chlorophenol ND ug/kg 20 10/02/09 22:26 95-57-809/09/09 00:007760 4-Chlorophenylphenyl ether ND ug/kg 20 10/02/09 22:26 7005-72-309/09/09 00:007760 Chrysene ND ug/kg 20 10/02/09 22:26 218-01-909/09/09 00:007760 Dibenz(a,h)anthracene ND ug/kg 20 10/02/09 22:26 53-70-309/09/09 00:007760 Dibenzofuran ND ug/kg 20 10/02/09 22:26 132-64-909/09/09 00:007760 1,2-Dichlorobenzene ND ug/kg 20 10/02/09 22:26 95-50-109/09/09 00:007760 1,3-Dichlorobenzene ND ug/kg 20 10/02/09 22:26 541-73-109/09/09 00:007760 1,4-Dichlorobenzene ND ug/kg 20 10/02/09 22:26 106-46-709/09/09 00:007760 3,3'-Dichlorobenzidine ND ug/kg 20 10/02/09 22:26 91-94-109/09/09 00:0038800 2,4-Dichlorophenol ND ug/kg 20 10/02/09 22:26 120-83-209/09/09 00:007760 Diethylphthalate ND ug/kg 20 10/02/09 22:26 84-66-209/09/09 00:007760 2,4-Dimethylphenol ND ug/kg 20 10/02/09 22:26 105-67-909/09/09 00:007760 Dimethylphthalate ND ug/kg 20 10/02/09 22:26 131-11-309/09/09 00:007760 Di-n-butylphthalate ND ug/kg 20 10/02/09 22:26 84-74-209/09/09 00:007760 4,6-Dinitro-2-methylphenol ND ug/kg 20 10/02/09 22:26 534-52-109/09/09 00:0015500 2,4-Dinitrophenol ND ug/kg 20 10/02/09 22:26 51-28-509/09/09 00:0038800 2,4-Dinitrotoluene ND ug/kg 20 10/02/09 22:26 121-14-209/09/09 00:007760 2,6-Dinitrotoluene ND ug/kg 20 10/02/09 22:26 606-20-209/09/09 00:007760 Di-n-octylphthalate ND ug/kg 20 10/02/09 22:26 117-84-009/09/09 00:007760 1,2-Diphenylhydrazine ND ug/kg 20 10/02/09 22:26 122-66-709/09/09 00:007760 bis(2-Ethylhexyl)phthalate ND ug/kg 20 10/02/09 22:26 117-81-709/09/09 00:007760 Fluoranthene ND ug/kg 20 10/02/09 22:26 206-44-009/09/09 00:007760 Fluorene ND ug/kg 20 10/02/09 22:26 86-73-709/09/09 00:007760 Hexachloro-1,3-butadiene ND ug/kg 20 10/02/09 22:26 87-68-309/09/09 00:007760 Hexachlorobenzene ND ug/kg 20 10/02/09 22:26 118-74-109/09/09 00:007760 Hexachlorocyclopentadiene ND ug/kg 20 10/02/09 22:26 77-47-409/09/09 00:007760 Hexachloroethane ND ug/kg 20 10/02/09 22:26 67-72-109/09/09 00:007760 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 17 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB6-09-09 Lab ID:9252614004 Collected:09/08/09 11:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 20 10/02/09 22:26 193-39-509/09/09 00:007760 Isophorone ND ug/kg 20 10/02/09 22:26 78-59-109/09/09 00:007760 1-Methylnaphthalene ND ug/kg 20 10/02/09 22:26 90-12-009/09/09 00:007760 2-Methylnaphthalene 8480 ug/kg 20 10/02/09 22:26 91-57-609/09/09 00:007760 2-Methylphenol(o-Cresol)ND ug/kg 20 10/02/09 22:26 95-48-709/09/09 00:007760 3&4-Methylphenol(m&p Cresol)ND ug/kg 20 10/02/09 22:2609/09/09 00:007760 Naphthalene ND ug/kg 20 10/02/09 22:26 91-20-309/09/09 00:007760 2-Nitroaniline ND ug/kg 20 10/02/09 22:26 88-74-409/09/09 00:0038800 3-Nitroaniline ND ug/kg 20 10/02/09 22:26 99-09-209/09/09 00:0038800 4-Nitroaniline ND ug/kg 20 10/02/09 22:26 100-01-609/09/09 00:0015500 Nitrobenzene ND ug/kg 20 10/02/09 22:26 98-95-309/09/09 00:007760 2-Nitrophenol ND ug/kg 20 10/02/09 22:26 88-75-509/09/09 00:007760 4-Nitrophenol ND ug/kg 20 10/02/09 22:26 100-02-709/09/09 00:0038800 N-Nitrosodimethylamine ND ug/kg 20 10/02/09 22:26 62-75-909/09/09 00:007760 N-Nitroso-di-n-propylamine ND ug/kg 20 10/02/09 22:26 621-64-709/09/09 00:007760 N-Nitrosodiphenylamine ND ug/kg 20 10/02/09 22:26 86-30-609/09/09 00:007760 Pentachlorophenol ND ug/kg 20 10/02/09 22:26 87-86-509/09/09 00:0038800 Phenanthrene ND ug/kg 20 10/02/09 22:26 85-01-809/09/09 00:007760 Phenol ND ug/kg 20 10/02/09 22:26 108-95-209/09/09 00:007760 Pyrene ND ug/kg 20 10/02/09 22:26 129-00-009/09/09 00:007760 1,2,4-Trichlorobenzene ND ug/kg 20 10/02/09 22:26 120-82-109/09/09 00:007760 2,4,5-Trichlorophenol ND ug/kg 20 10/02/09 22:26 95-95-409/09/09 00:007760 2,4,6-Trichlorophenol ND ug/kg 20 10/02/09 22:26 88-06-209/09/09 00:007760 Nitrobenzene-d5 (S)0 %20 10/02/09 22:26 4165-60-0 IS,S409/09/09 00:0030-150 2-Fluorobiphenyl (S)0 %20 10/02/09 22:26 321-60-8 S409/09/09 00:0046-120 Terphenyl-d14 (S)0 %20 10/02/09 22:26 1718-51-0 S409/09/09 00:0038-108 Phenol-d6 (S)0 %20 10/02/09 22:26 13127-88-3 S409/09/09 00:0035-120 2-Fluorophenol (S)0 %20 10/02/09 22:26 367-12-4 S409/09/09 00:0024-120 2,4,6-Tribromophenol (S)0 %20 10/02/09 22:26 118-79-6 S409/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/11/09 18:15 67-64-14660 Benzene ND ug/kg 50 09/11/09 18:15 71-43-2233 Bromobenzene ND ug/kg 50 09/11/09 18:15 108-86-1233 Bromochloromethane ND ug/kg 50 09/11/09 18:15 74-97-5233 Bromodichloromethane ND ug/kg 50 09/11/09 18:15 75-27-4233 Bromoform ND ug/kg 50 09/11/09 18:15 75-25-2233 Bromomethane ND ug/kg 50 09/11/09 18:15 74-83-9466 2-Butanone (MEK)ND ug/kg 50 09/11/09 18:15 78-93-34660 n-Butylbenzene 4330 ug/kg 50 09/11/09 18:15 104-51-8233 sec-Butylbenzene 2870 ug/kg 50 09/11/09 18:15 135-98-8233 tert-Butylbenzene ND ug/kg 50 09/11/09 18:15 98-06-6233 Carbon tetrachloride ND ug/kg 50 09/11/09 18:15 56-23-5233 Chlorobenzene ND ug/kg 50 09/11/09 18:15 108-90-7233 Chloroethane ND ug/kg 50 09/11/09 18:15 75-00-3466 Chloroform ND ug/kg 50 09/11/09 18:15 67-66-3233 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 18 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB6-09-09 Lab ID:9252614004 Collected:09/08/09 11:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 50 09/11/09 18:15 74-87-3466 2-Chlorotoluene ND ug/kg 50 09/11/09 18:15 95-49-8233 4-Chlorotoluene ND ug/kg 50 09/11/09 18:15 106-43-4233 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/11/09 18:15 96-12-8233 Dibromochloromethane ND ug/kg 50 09/11/09 18:15 124-48-1233 1,2-Dibromoethane (EDB)ND ug/kg 50 09/11/09 18:15 106-93-4233 Dibromomethane ND ug/kg 50 09/11/09 18:15 74-95-3233 1,2-Dichlorobenzene ND ug/kg 50 09/11/09 18:15 95-50-1233 1,3-Dichlorobenzene ND ug/kg 50 09/11/09 18:15 541-73-1233 1,4-Dichlorobenzene ND ug/kg 50 09/11/09 18:15 106-46-7233 Dichlorodifluoromethane ND ug/kg 50 09/11/09 18:15 75-71-8466 1,1-Dichloroethane ND ug/kg 50 09/11/09 18:15 75-34-3233 1,2-Dichloroethane ND ug/kg 50 09/11/09 18:15 107-06-2233 1,1-Dichloroethene ND ug/kg 50 09/11/09 18:15 75-35-4233 cis-1,2-Dichloroethene ND ug/kg 50 09/11/09 18:15 156-59-2233 trans-1,2-Dichloroethene ND ug/kg 50 09/11/09 18:15 156-60-5233 1,2-Dichloropropane ND ug/kg 50 09/11/09 18:15 78-87-5233 1,3-Dichloropropane ND ug/kg 50 09/11/09 18:15 142-28-9233 2,2-Dichloropropane ND ug/kg 50 09/11/09 18:15 594-20-7233 1,1-Dichloropropene ND ug/kg 50 09/11/09 18:15 563-58-6233 cis-1,3-Dichloropropene ND ug/kg 50 09/11/09 18:15 10061-01-5233 trans-1,3-Dichloropropene ND ug/kg 50 09/11/09 18:15 10061-02-6233 Diisopropyl ether ND ug/kg 50 09/11/09 18:15 108-20-3233 Ethylbenzene 443 ug/kg 50 09/11/09 18:15 100-41-4233 Hexachloro-1,3-butadiene ND ug/kg 50 09/11/09 18:15 87-68-3233 2-Hexanone ND ug/kg 50 09/11/09 18:15 591-78-62330 Isopropylbenzene (Cumene)1680 ug/kg 50 09/11/09 18:15 98-82-8233 p-Isopropyltoluene 4450 ug/kg 50 09/11/09 18:15 99-87-6233 Methylene Chloride ND ug/kg 50 09/11/09 18:15 75-09-2933 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/11/09 18:15 108-10-12330 Methyl-tert-butyl ether ND ug/kg 50 09/11/09 18:15 1634-04-4233 Naphthalene 5800 ug/kg 50 09/11/09 18:15 91-20-3233 n-Propylbenzene 2840 ug/kg 50 09/11/09 18:15 103-65-1233 Styrene ND ug/kg 50 09/11/09 18:15 100-42-5233 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/11/09 18:15 630-20-6233 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/11/09 18:15 79-34-5233 Tetrachloroethene ND ug/kg 50 09/11/09 18:15 127-18-4233 Toluene ND ug/kg 50 09/11/09 18:15 108-88-3233 1,2,3-Trichlorobenzene ND ug/kg 50 09/11/09 18:15 87-61-6233 1,2,4-Trichlorobenzene ND ug/kg 50 09/11/09 18:15 120-82-1233 1,1,1-Trichloroethane ND ug/kg 50 09/11/09 18:15 71-55-6233 1,1,2-Trichloroethane ND ug/kg 50 09/11/09 18:15 79-00-5233 Trichloroethene ND ug/kg 50 09/11/09 18:15 79-01-6233 Trichlorofluoromethane ND ug/kg 50 09/11/09 18:15 75-69-4233 1,2,3-Trichloropropane ND ug/kg 50 09/11/09 18:15 96-18-4233 1,2,4-Trimethylbenzene 25500 ug/kg 250 09/14/09 14:49 95-63-61170 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 19 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB6-09-09 Lab ID:9252614004 Collected:09/08/09 11:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene 2860 ug/kg 50 09/11/09 18:15 108-67-8233 Vinyl acetate ND ug/kg 50 09/11/09 18:15 108-05-42330 Vinyl chloride ND ug/kg 50 09/11/09 18:15 75-01-4466 Xylene (Total)1890 ug/kg 50 09/11/09 18:15 1330-20-7466 m&p-Xylene 1190 ug/kg 50 09/11/09 18:15 1330-20-7466 o-Xylene 697 ug/kg 50 09/11/09 18:15 95-47-6233 Dibromofluoromethane (S)101 %50 09/11/09 18:15 1868-53-779-116 Toluene-d8 (S)101 %50 09/11/09 18:15 2037-26-588-110 4-Bromofluorobenzene (S)101 %50 09/11/09 18:15 460-00-474-115 1,2-Dichloroethane-d4 (S)102 %50 09/11/09 18:15 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 14.9 %1 09/09/09 13:410.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 20 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB7-09-09 Lab ID:9252614005 Collected:09/08/09 11:10 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 20 10/02/09 22:52 83-32-909/09/09 00:007870 Acenaphthylene ND ug/kg 20 10/02/09 22:52 208-96-809/09/09 00:007870 Aniline ND ug/kg 20 10/02/09 22:52 62-53-309/09/09 00:007870 Anthracene ND ug/kg 20 10/02/09 22:52 120-12-709/09/09 00:007870 Benzo(a)anthracene ND ug/kg 20 10/02/09 22:52 56-55-309/09/09 00:007870 Benzo(a)pyrene ND ug/kg 20 10/02/09 22:52 50-32-809/09/09 00:007870 Benzo(b)fluoranthene ND ug/kg 20 10/02/09 22:52 205-99-209/09/09 00:007870 Benzo(g,h,i)perylene ND ug/kg 20 10/02/09 22:52 191-24-209/09/09 00:007870 Benzo(k)fluoranthene ND ug/kg 20 10/02/09 22:52 207-08-909/09/09 00:007870 Benzoic Acid 25000J ug/kg 20 10/02/09 22:52 65-85-009/09/09 00:0039400 Benzyl alcohol ND ug/kg 20 10/02/09 22:52 100-51-609/09/09 00:0015700 4-Bromophenylphenyl ether ND ug/kg 20 10/02/09 22:52 101-55-309/09/09 00:007870 Butylbenzylphthalate ND ug/kg 20 10/02/09 22:52 85-68-709/09/09 00:007870 4-Chloro-3-methylphenol ND ug/kg 20 10/02/09 22:52 59-50-709/09/09 00:0015700 4-Chloroaniline ND ug/kg 20 10/02/09 22:52 106-47-809/09/09 00:0039400 bis(2-Chloroethoxy)methane ND ug/kg 20 10/02/09 22:52 111-91-109/09/09 00:007870 bis(2-Chloroethyl) ether ND ug/kg 20 10/02/09 22:52 111-44-409/09/09 00:007870 bis(2-Chloroisopropyl) ether ND ug/kg 20 10/02/09 22:52 108-60-109/09/09 00:007870 2-Chloronaphthalene ND ug/kg 20 10/02/09 22:52 91-58-709/09/09 00:007870 2-Chlorophenol ND ug/kg 20 10/02/09 22:52 95-57-809/09/09 00:007870 4-Chlorophenylphenyl ether ND ug/kg 20 10/02/09 22:52 7005-72-309/09/09 00:007870 Chrysene ND ug/kg 20 10/02/09 22:52 218-01-909/09/09 00:007870 Dibenz(a,h)anthracene ND ug/kg 20 10/02/09 22:52 53-70-309/09/09 00:007870 Dibenzofuran ND ug/kg 20 10/02/09 22:52 132-64-909/09/09 00:007870 1,2-Dichlorobenzene ND ug/kg 20 10/02/09 22:52 95-50-109/09/09 00:007870 1,3-Dichlorobenzene ND ug/kg 20 10/02/09 22:52 541-73-109/09/09 00:007870 1,4-Dichlorobenzene ND ug/kg 20 10/02/09 22:52 106-46-709/09/09 00:007870 3,3'-Dichlorobenzidine ND ug/kg 20 10/02/09 22:52 91-94-109/09/09 00:0039400 2,4-Dichlorophenol ND ug/kg 20 10/02/09 22:52 120-83-209/09/09 00:007870 Diethylphthalate ND ug/kg 20 10/02/09 22:52 84-66-209/09/09 00:007870 2,4-Dimethylphenol ND ug/kg 20 10/02/09 22:52 105-67-909/09/09 00:007870 Dimethylphthalate ND ug/kg 20 10/02/09 22:52 131-11-309/09/09 00:007870 Di-n-butylphthalate ND ug/kg 20 10/02/09 22:52 84-74-209/09/09 00:007870 4,6-Dinitro-2-methylphenol ND ug/kg 20 10/02/09 22:52 534-52-109/09/09 00:0015700 2,4-Dinitrophenol ND ug/kg 20 10/02/09 22:52 51-28-509/09/09 00:0039400 2,4-Dinitrotoluene ND ug/kg 20 10/02/09 22:52 121-14-209/09/09 00:007870 2,6-Dinitrotoluene ND ug/kg 20 10/02/09 22:52 606-20-209/09/09 00:007870 Di-n-octylphthalate ND ug/kg 20 10/02/09 22:52 117-84-009/09/09 00:007870 1,2-Diphenylhydrazine ND ug/kg 20 10/02/09 22:52 122-66-709/09/09 00:007870 bis(2-Ethylhexyl)phthalate ND ug/kg 20 10/02/09 22:52 117-81-709/09/09 00:007870 Fluoranthene ND ug/kg 20 10/02/09 22:52 206-44-009/09/09 00:007870 Fluorene ND ug/kg 20 10/02/09 22:52 86-73-709/09/09 00:007870 Hexachloro-1,3-butadiene ND ug/kg 20 10/02/09 22:52 87-68-309/09/09 00:007870 Hexachlorobenzene ND ug/kg 20 10/02/09 22:52 118-74-109/09/09 00:007870 Hexachlorocyclopentadiene ND ug/kg 20 10/02/09 22:52 77-47-409/09/09 00:007870 Hexachloroethane ND ug/kg 20 10/02/09 22:52 67-72-109/09/09 00:007870 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 21 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB7-09-09 Lab ID:9252614005 Collected:09/08/09 11:10 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 20 10/02/09 22:52 193-39-509/09/09 00:007870 Isophorone ND ug/kg 20 10/02/09 22:52 78-59-109/09/09 00:007870 1-Methylnaphthalene 6840J ug/kg 20 10/02/09 22:52 90-12-009/09/09 00:007870 2-Methylnaphthalene 8660 ug/kg 20 10/02/09 22:52 91-57-609/09/09 00:007870 2-Methylphenol(o-Cresol)ND ug/kg 20 10/02/09 22:52 95-48-709/09/09 00:007870 3&4-Methylphenol(m&p Cresol)ND ug/kg 20 10/02/09 22:5209/09/09 00:007870 Naphthalene 3220J ug/kg 20 10/02/09 22:52 91-20-309/09/09 00:007870 2-Nitroaniline ND ug/kg 20 10/02/09 22:52 88-74-409/09/09 00:0039400 3-Nitroaniline ND ug/kg 20 10/02/09 22:52 99-09-209/09/09 00:0039400 4-Nitroaniline ND ug/kg 20 10/02/09 22:52 100-01-609/09/09 00:0015700 Nitrobenzene ND ug/kg 20 10/02/09 22:52 98-95-309/09/09 00:007870 2-Nitrophenol ND ug/kg 20 10/02/09 22:52 88-75-509/09/09 00:007870 4-Nitrophenol ND ug/kg 20 10/02/09 22:52 100-02-709/09/09 00:0039400 N-Nitrosodimethylamine ND ug/kg 20 10/02/09 22:52 62-75-909/09/09 00:007870 N-Nitroso-di-n-propylamine ND ug/kg 20 10/02/09 22:52 621-64-709/09/09 00:007870 N-Nitrosodiphenylamine ND ug/kg 20 10/02/09 22:52 86-30-609/09/09 00:007870 Pentachlorophenol ND ug/kg 20 10/02/09 22:52 87-86-509/09/09 00:0039400 Phenanthrene ND ug/kg 20 10/02/09 22:52 85-01-809/09/09 00:007870 Phenol ND ug/kg 20 10/02/09 22:52 108-95-209/09/09 00:007870 Pyrene ND ug/kg 20 10/02/09 22:52 129-00-009/09/09 00:007870 1,2,4-Trichlorobenzene ND ug/kg 20 10/02/09 22:52 120-82-109/09/09 00:007870 2,4,5-Trichlorophenol ND ug/kg 20 10/02/09 22:52 95-95-409/09/09 00:007870 2,4,6-Trichlorophenol ND ug/kg 20 10/02/09 22:52 88-06-209/09/09 00:007870 Nitrobenzene-d5 (S)0 %20 10/02/09 22:52 4165-60-0 D3,IS,S409/09/09 00:0030-150 2-Fluorobiphenyl (S)0 %20 10/02/09 22:52 321-60-8 S409/09/09 00:0046-120 Terphenyl-d14 (S)0 %20 10/02/09 22:52 1718-51-0 S409/09/09 00:0038-108 Phenol-d6 (S)0 %20 10/02/09 22:52 13127-88-3 S409/09/09 00:0035-120 2-Fluorophenol (S)0 %20 10/02/09 22:52 367-12-4 S409/09/09 00:0024-120 2,4,6-Tribromophenol (S)0 %20 10/02/09 22:52 118-79-6 S409/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 1 09/11/09 14:53 67-64-185.2 Benzene ND ug/kg 1 09/11/09 14:53 71-43-24.3 Bromobenzene ND ug/kg 1 09/11/09 14:53 108-86-14.3 Bromochloromethane ND ug/kg 1 09/11/09 14:53 74-97-54.3 Bromodichloromethane ND ug/kg 1 09/11/09 14:53 75-27-44.3 Bromoform ND ug/kg 1 09/11/09 14:53 75-25-24.3 Bromomethane ND ug/kg 1 09/11/09 14:53 74-83-98.5 2-Butanone (MEK)ND ug/kg 1 09/11/09 14:53 78-93-385.2 n-Butylbenzene 35.7 ug/kg 1 09/11/09 14:53 104-51-84.3 sec-Butylbenzene 34.2 ug/kg 1 09/11/09 14:53 135-98-84.3 tert-Butylbenzene ND ug/kg 1 09/11/09 14:53 98-06-64.3 Carbon tetrachloride ND ug/kg 1 09/11/09 14:53 56-23-54.3 Chlorobenzene ND ug/kg 1 09/11/09 14:53 108-90-74.3 Chloroethane ND ug/kg 1 09/11/09 14:53 75-00-38.5 Chloroform ND ug/kg 1 09/11/09 14:53 67-66-34.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 22 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB7-09-09 Lab ID:9252614005 Collected:09/08/09 11:10 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 1 09/11/09 14:53 74-87-38.5 2-Chlorotoluene ND ug/kg 1 09/11/09 14:53 95-49-84.3 4-Chlorotoluene ND ug/kg 1 09/11/09 14:53 106-43-44.3 1,2-Dibromo-3-chloropropane ND ug/kg 1 09/11/09 14:53 96-12-84.3 Dibromochloromethane ND ug/kg 1 09/11/09 14:53 124-48-14.3 1,2-Dibromoethane (EDB)ND ug/kg 1 09/11/09 14:53 106-93-44.3 Dibromomethane ND ug/kg 1 09/11/09 14:53 74-95-34.3 1,2-Dichlorobenzene ND ug/kg 1 09/11/09 14:53 95-50-14.3 1,3-Dichlorobenzene ND ug/kg 1 09/11/09 14:53 541-73-14.3 1,4-Dichlorobenzene ND ug/kg 1 09/11/09 14:53 106-46-74.3 Dichlorodifluoromethane ND ug/kg 1 09/11/09 14:53 75-71-88.5 1,1-Dichloroethane ND ug/kg 1 09/11/09 14:53 75-34-34.3 1,2-Dichloroethane ND ug/kg 1 09/11/09 14:53 107-06-24.3 1,1-Dichloroethene ND ug/kg 1 09/11/09 14:53 75-35-44.3 cis-1,2-Dichloroethene ND ug/kg 1 09/11/09 14:53 156-59-24.3 trans-1,2-Dichloroethene ND ug/kg 1 09/11/09 14:53 156-60-54.3 1,2-Dichloropropane ND ug/kg 1 09/11/09 14:53 78-87-54.3 1,3-Dichloropropane ND ug/kg 1 09/11/09 14:53 142-28-94.3 2,2-Dichloropropane ND ug/kg 1 09/11/09 14:53 594-20-74.3 1,1-Dichloropropene ND ug/kg 1 09/11/09 14:53 563-58-64.3 cis-1,3-Dichloropropene ND ug/kg 1 09/11/09 14:53 10061-01-54.3 trans-1,3-Dichloropropene ND ug/kg 1 09/11/09 14:53 10061-02-64.3 Diisopropyl ether ND ug/kg 1 09/11/09 14:53 108-20-34.3 Ethylbenzene 12.1 ug/kg 1 09/11/09 14:53 100-41-44.3 Hexachloro-1,3-butadiene ND ug/kg 1 09/11/09 14:53 87-68-34.3 2-Hexanone ND ug/kg 1 09/11/09 14:53 591-78-642.6 Isopropylbenzene (Cumene)15.2 ug/kg 1 09/11/09 14:53 98-82-84.3 p-Isopropyltoluene 52.0 ug/kg 1 09/11/09 14:53 99-87-64.3 Methylene Chloride ND ug/kg 1 09/11/09 14:53 75-09-217.0 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 09/11/09 14:53 108-10-142.6 Methyl-tert-butyl ether ND ug/kg 1 09/11/09 14:53 1634-04-44.3 Naphthalene 12.1 ug/kg 1 09/11/09 14:53 91-20-34.3 n-Propylbenzene 30.9 ug/kg 1 09/11/09 14:53 103-65-14.3 Styrene ND ug/kg 1 09/11/09 14:53 100-42-54.3 1,1,1,2-Tetrachloroethane ND ug/kg 1 09/11/09 14:53 630-20-64.3 1,1,2,2-Tetrachloroethane ND ug/kg 1 09/11/09 14:53 79-34-54.3 Tetrachloroethene ND ug/kg 1 09/11/09 14:53 127-18-44.3 Toluene ND ug/kg 1 09/11/09 14:53 108-88-34.3 1,2,3-Trichlorobenzene ND ug/kg 1 09/11/09 14:53 87-61-64.3 1,2,4-Trichlorobenzene ND ug/kg 1 09/11/09 14:53 120-82-14.3 1,1,1-Trichloroethane ND ug/kg 1 09/11/09 14:53 71-55-64.3 1,1,2-Trichloroethane ND ug/kg 1 09/11/09 14:53 79-00-54.3 Trichloroethene ND ug/kg 1 09/11/09 14:53 79-01-64.3 Trichlorofluoromethane ND ug/kg 1 09/11/09 14:53 75-69-44.3 1,2,3-Trichloropropane ND ug/kg 1 09/11/09 14:53 96-18-44.3 1,2,4-Trimethylbenzene 159 ug/kg 1 09/11/09 14:53 95-63-64.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 23 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB7-09-09 Lab ID:9252614005 Collected:09/08/09 11:10 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene 46.5 ug/kg 1 09/11/09 14:53 108-67-84.3 Vinyl acetate ND ug/kg 1 09/11/09 14:53 108-05-442.6 Vinyl chloride ND ug/kg 1 09/11/09 14:53 75-01-48.5 Xylene (Total)84.9 ug/kg 1 09/11/09 14:53 1330-20-78.5 m&p-Xylene 80.0 ug/kg 1 09/11/09 14:53 1330-20-78.5 o-Xylene 4.8 ug/kg 1 09/11/09 14:53 95-47-64.3 Dibromofluoromethane (S)99 %1 09/11/09 14:53 1868-53-779-116 Toluene-d8 (S)100 %1 09/11/09 14:53 2037-26-588-110 4-Bromofluorobenzene (S)94 %1 09/11/09 14:53 460-00-474-115 1,2-Dichloroethane-d4 (S)100 %1 09/11/09 14:53 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 16.1 %1 09/09/09 13:420.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 24 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB11-09-09 Lab ID:9252614006 Collected:09/08/09 11:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony 1.3 mg/kg 1 09/10/09 20:09 7440-36-0 M0,R109/09/09 15:000.53 Arsenic 7.1 mg/kg 1 09/10/09 20:09 7440-38-2 R109/09/09 15:000.53 Beryllium 2.1 mg/kg 1 09/10/09 20:09 7440-41-7 R109/09/09 15:000.11 Cadmium 0.25 mg/kg 1 09/10/09 20:09 7440-43-9 R109/09/09 15:000.11 Chromium 5.5 mg/kg 1 09/10/09 20:09 7440-47-3 R109/09/09 15:000.53 Copper 38.0 mg/kg 1 09/10/09 20:09 7440-50-8 M009/09/09 15:000.53 Lead 24.9 mg/kg 1 09/10/09 20:09 7439-92-1 M0,R109/09/09 15:000.53 Manganese 93.8 mg/kg 1 09/10/09 20:09 7439-96-5 M0,R109/09/09 15:000.53 Nickel 10.2 mg/kg 1 09/10/09 20:09 7440-02-0 M0,R109/09/09 15:000.53 Selenium 1.4 mg/kg 1 09/10/09 20:09 7782-49-2 R109/09/09 15:001.1 Silver ND mg/kg 1 09/10/09 20:09 7440-22-4 R109/09/09 15:000.53 Thallium ND mg/kg 1 09/10/09 20:09 7440-28-0 M0,R109/09/09 15:001.1 Zinc 56.5 mg/kg 1 09/10/09 20:09 7440-66-6 M009/09/09 15:001.1 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.075 mg/kg 1 09/11/09 14:08 7439-97-609/11/09 10:160.0048 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/23/09 00:55 83-32-909/09/09 00:00373 Acenaphthylene ND ug/kg 1 09/23/09 00:55 208-96-809/09/09 00:00373 Aniline ND ug/kg 1 09/23/09 00:55 62-53-309/09/09 00:00373 Anthracene ND ug/kg 1 09/23/09 00:55 120-12-709/09/09 00:00373 Benzo(a)anthracene ND ug/kg 1 09/23/09 00:55 56-55-309/09/09 00:00373 Benzo(a)pyrene ND ug/kg 1 09/23/09 00:55 50-32-809/09/09 00:00373 Benzo(b)fluoranthene ND ug/kg 1 09/23/09 00:55 205-99-209/09/09 00:00373 Benzo(g,h,i)perylene ND ug/kg 1 09/23/09 00:55 191-24-209/09/09 00:00373 Benzo(k)fluoranthene ND ug/kg 1 09/23/09 00:55 207-08-909/09/09 00:00373 Benzoic Acid ND ug/kg 1 09/23/09 00:55 65-85-009/09/09 00:001870 Benzyl alcohol ND ug/kg 1 09/23/09 00:55 100-51-609/09/09 00:00746 4-Bromophenylphenyl ether ND ug/kg 1 09/23/09 00:55 101-55-309/09/09 00:00373 Butylbenzylphthalate ND ug/kg 1 09/23/09 00:55 85-68-709/09/09 00:00373 4-Chloro-3-methylphenol ND ug/kg 1 09/23/09 00:55 59-50-709/09/09 00:00746 4-Chloroaniline ND ug/kg 1 09/23/09 00:55 106-47-809/09/09 00:001870 bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/09 00:55 111-91-109/09/09 00:00373 bis(2-Chloroethyl) ether ND ug/kg 1 09/23/09 00:55 111-44-409/09/09 00:00373 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/09 00:55 108-60-109/09/09 00:00373 2-Chloronaphthalene ND ug/kg 1 09/23/09 00:55 91-58-709/09/09 00:00373 2-Chlorophenol ND ug/kg 1 09/23/09 00:55 95-57-809/09/09 00:00373 4-Chlorophenylphenyl ether ND ug/kg 1 09/23/09 00:55 7005-72-309/09/09 00:00373 Chrysene ND ug/kg 1 09/23/09 00:55 218-01-909/09/09 00:00373 Dibenz(a,h)anthracene ND ug/kg 1 09/23/09 00:55 53-70-309/09/09 00:00373 Dibenzofuran 1010 ug/kg 1 09/23/09 00:55 132-64-909/09/09 00:00373 1,2-Dichlorobenzene ND ug/kg 1 09/23/09 00:55 95-50-109/09/09 00:00373 1,3-Dichlorobenzene ND ug/kg 1 09/23/09 00:55 541-73-109/09/09 00:00373 1,4-Dichlorobenzene ND ug/kg 1 09/23/09 00:55 106-46-709/09/09 00:00373 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 25 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB11-09-09 Lab ID:9252614006 Collected:09/08/09 11:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 3,3'-Dichlorobenzidine ND ug/kg 1 09/23/09 00:55 91-94-109/09/09 00:001870 2,4-Dichlorophenol ND ug/kg 1 09/23/09 00:55 120-83-209/09/09 00:00373 Diethylphthalate ND ug/kg 1 09/23/09 00:55 84-66-209/09/09 00:00373 2,4-Dimethylphenol ND ug/kg 1 09/23/09 00:55 105-67-909/09/09 00:00373 Dimethylphthalate ND ug/kg 1 09/23/09 00:55 131-11-309/09/09 00:00373 Di-n-butylphthalate ND ug/kg 1 09/23/09 00:55 84-74-209/09/09 00:00373 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/09 00:55 534-52-109/09/09 00:00746 2,4-Dinitrophenol ND ug/kg 1 09/23/09 00:55 51-28-509/09/09 00:001870 2,4-Dinitrotoluene ND ug/kg 1 09/23/09 00:55 121-14-209/09/09 00:00373 2,6-Dinitrotoluene ND ug/kg 1 09/23/09 00:55 606-20-209/09/09 00:00373 Di-n-octylphthalate ND ug/kg 1 09/23/09 00:55 117-84-009/09/09 00:00373 1,2-Diphenylhydrazine ND ug/kg 1 09/23/09 00:55 122-66-709/09/09 00:00373 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/09 00:55 117-81-709/09/09 00:00373 Fluoranthene ND ug/kg 1 09/23/09 00:55 206-44-009/09/09 00:00373 Fluorene ND ug/kg 1 09/23/09 00:55 86-73-709/09/09 00:00373 Hexachloro-1,3-butadiene ND ug/kg 1 09/23/09 00:55 87-68-309/09/09 00:00373 Hexachlorobenzene ND ug/kg 1 09/23/09 00:55 118-74-109/09/09 00:00373 Hexachlorocyclopentadiene ND ug/kg 1 09/23/09 00:55 77-47-409/09/09 00:00373 Hexachloroethane ND ug/kg 1 09/23/09 00:55 67-72-109/09/09 00:00373 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/09 00:55 193-39-509/09/09 00:00373 Isophorone ND ug/kg 1 09/23/09 00:55 78-59-109/09/09 00:00373 1-Methylnaphthalene 3750 ug/kg 1 09/23/09 00:55 90-12-009/09/09 00:00373 2-Methylnaphthalene 4580 ug/kg 1 09/23/09 00:55 91-57-609/09/09 00:00373 2-Methylphenol(o-Cresol)ND ug/kg 1 09/23/09 00:55 95-48-709/09/09 00:00373 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/23/09 00:5509/09/09 00:00373 Naphthalene 3250 ug/kg 1 09/23/09 00:55 91-20-309/09/09 00:00373 2-Nitroaniline ND ug/kg 1 09/23/09 00:55 88-74-409/09/09 00:001870 3-Nitroaniline ND ug/kg 1 09/23/09 00:55 99-09-209/09/09 00:001870 4-Nitroaniline ND ug/kg 1 09/23/09 00:55 100-01-609/09/09 00:00746 Nitrobenzene ND ug/kg 1 09/23/09 00:55 98-95-309/09/09 00:00373 2-Nitrophenol ND ug/kg 1 09/23/09 00:55 88-75-509/09/09 00:00373 4-Nitrophenol ND ug/kg 1 09/23/09 00:55 100-02-709/09/09 00:001870 N-Nitrosodimethylamine ND ug/kg 1 09/23/09 00:55 62-75-909/09/09 00:00373 N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/09 00:55 621-64-709/09/09 00:00373 N-Nitrosodiphenylamine ND ug/kg 1 09/23/09 00:55 86-30-609/09/09 00:00373 Pentachlorophenol ND ug/kg 1 09/23/09 00:55 87-86-509/09/09 00:001870 Phenanthrene 1400 ug/kg 1 09/23/09 00:55 85-01-809/09/09 00:00373 Phenol ND ug/kg 1 09/23/09 00:55 108-95-209/09/09 00:00373 Pyrene 518 ug/kg 1 09/23/09 00:55 129-00-009/09/09 00:00373 1,2,4-Trichlorobenzene ND ug/kg 1 09/23/09 00:55 120-82-109/09/09 00:00373 2,4,5-Trichlorophenol ND ug/kg 1 09/23/09 00:55 95-95-409/09/09 00:00373 2,4,6-Trichlorophenol ND ug/kg 1 09/23/09 00:55 88-06-209/09/09 00:00373 Nitrobenzene-d5 (S)40 %1 09/23/09 00:55 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)47 %1 09/23/09 00:55 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)107 %1 09/23/09 00:55 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)36 %1 09/23/09 00:55 13127-88-309/09/09 00:0035-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 26 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB11-09-09 Lab ID:9252614006 Collected:09/08/09 11:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 2-Fluorophenol (S)25 %1 09/23/09 00:55 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)56 %1 09/23/09 00:55 118-79-609/09/09 00:0044-136 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 11.6 %1 09/09/09 13:430.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 27 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB10-09-09 Lab ID:9252614007 Collected:09/08/09 11:25 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony ND mg/kg 1 09/10/09 20:33 7440-36-009/09/09 15:000.59 Arsenic 10 mg/kg 1 09/10/09 20:33 7440-38-209/09/09 15:000.59 Beryllium 0.23 mg/kg 1 09/10/09 20:33 7440-41-709/09/09 15:000.12 Cadmium ND mg/kg 1 09/10/09 20:33 7440-43-909/09/09 15:000.12 Chromium 3.4 mg/kg 1 09/10/09 20:33 7440-47-309/09/09 15:000.59 Copper 7.0 mg/kg 1 09/10/09 20:33 7440-50-809/09/09 15:000.59 Lead 13.0 mg/kg 1 09/10/09 20:33 7439-92-109/09/09 15:000.59 Manganese 17.4 mg/kg 1 09/10/09 20:33 7439-96-509/09/09 15:000.59 Nickel 3.0 mg/kg 1 09/10/09 20:33 7440-02-009/09/09 15:000.59 Selenium 3.1 mg/kg 1 09/10/09 20:33 7782-49-209/09/09 15:001.2 Silver ND mg/kg 1 09/10/09 20:33 7440-22-409/09/09 15:000.59 Thallium ND mg/kg 1 09/10/09 20:33 7440-28-009/09/09 15:001.2 Zinc 33.8 mg/kg 1 09/10/09 20:33 7440-66-609/09/09 15:001.2 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.41 mg/kg 5 09/14/09 16:30 7439-97-609/11/09 10:160.031 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/23/09 01:19 83-32-909/09/09 00:00439 Acenaphthylene ND ug/kg 1 09/23/09 01:19 208-96-809/09/09 00:00439 Aniline ND ug/kg 1 09/23/09 01:19 62-53-309/09/09 00:00439 Anthracene ND ug/kg 1 09/23/09 01:19 120-12-709/09/09 00:00439 Benzo(a)anthracene ND ug/kg 1 09/23/09 01:19 56-55-309/09/09 00:00439 Benzo(a)pyrene ND ug/kg 1 09/23/09 01:19 50-32-809/09/09 00:00439 Benzo(b)fluoranthene ND ug/kg 1 09/23/09 01:19 205-99-209/09/09 00:00439 Benzo(g,h,i)perylene ND ug/kg 1 09/23/09 01:19 191-24-209/09/09 00:00439 Benzo(k)fluoranthene ND ug/kg 1 09/23/09 01:19 207-08-909/09/09 00:00439 Benzoic Acid ND ug/kg 1 09/23/09 01:19 65-85-009/09/09 00:002200 Benzyl alcohol ND ug/kg 1 09/23/09 01:19 100-51-609/09/09 00:00879 4-Bromophenylphenyl ether ND ug/kg 1 09/23/09 01:19 101-55-309/09/09 00:00439 Butylbenzylphthalate ND ug/kg 1 09/23/09 01:19 85-68-709/09/09 00:00439 4-Chloro-3-methylphenol ND ug/kg 1 09/23/09 01:19 59-50-709/09/09 00:00879 4-Chloroaniline ND ug/kg 1 09/23/09 01:19 106-47-809/09/09 00:002200 bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/09 01:19 111-91-109/09/09 00:00439 bis(2-Chloroethyl) ether ND ug/kg 1 09/23/09 01:19 111-44-409/09/09 00:00439 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/09 01:19 108-60-109/09/09 00:00439 2-Chloronaphthalene ND ug/kg 1 09/23/09 01:19 91-58-709/09/09 00:00439 2-Chlorophenol ND ug/kg 1 09/23/09 01:19 95-57-809/09/09 00:00439 4-Chlorophenylphenyl ether ND ug/kg 1 09/23/09 01:19 7005-72-309/09/09 00:00439 Chrysene ND ug/kg 1 09/23/09 01:19 218-01-909/09/09 00:00439 Dibenz(a,h)anthracene ND ug/kg 1 09/23/09 01:19 53-70-309/09/09 00:00439 Dibenzofuran ND ug/kg 1 09/23/09 01:19 132-64-909/09/09 00:00439 1,2-Dichlorobenzene ND ug/kg 1 09/23/09 01:19 95-50-109/09/09 00:00439 1,3-Dichlorobenzene ND ug/kg 1 09/23/09 01:19 541-73-109/09/09 00:00439 1,4-Dichlorobenzene ND ug/kg 1 09/23/09 01:19 106-46-709/09/09 00:00439 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 28 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB10-09-09 Lab ID:9252614007 Collected:09/08/09 11:25 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 3,3'-Dichlorobenzidine ND ug/kg 1 09/23/09 01:19 91-94-109/09/09 00:002200 2,4-Dichlorophenol ND ug/kg 1 09/23/09 01:19 120-83-209/09/09 00:00439 Diethylphthalate ND ug/kg 1 09/23/09 01:19 84-66-209/09/09 00:00439 2,4-Dimethylphenol ND ug/kg 1 09/23/09 01:19 105-67-909/09/09 00:00439 Dimethylphthalate ND ug/kg 1 09/23/09 01:19 131-11-309/09/09 00:00439 Di-n-butylphthalate ND ug/kg 1 09/23/09 01:19 84-74-209/09/09 00:00439 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/09 01:19 534-52-109/09/09 00:00879 2,4-Dinitrophenol ND ug/kg 1 09/23/09 01:19 51-28-509/09/09 00:002200 2,4-Dinitrotoluene ND ug/kg 1 09/23/09 01:19 121-14-209/09/09 00:00439 2,6-Dinitrotoluene ND ug/kg 1 09/23/09 01:19 606-20-209/09/09 00:00439 Di-n-octylphthalate ND ug/kg 1 09/23/09 01:19 117-84-009/09/09 00:00439 1,2-Diphenylhydrazine ND ug/kg 1 09/23/09 01:19 122-66-709/09/09 00:00439 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/09 01:19 117-81-709/09/09 00:00439 Fluoranthene ND ug/kg 1 09/23/09 01:19 206-44-009/09/09 00:00439 Fluorene ND ug/kg 1 09/23/09 01:19 86-73-709/09/09 00:00439 Hexachloro-1,3-butadiene ND ug/kg 1 09/23/09 01:19 87-68-309/09/09 00:00439 Hexachlorobenzene ND ug/kg 1 09/23/09 01:19 118-74-109/09/09 00:00439 Hexachlorocyclopentadiene ND ug/kg 1 09/23/09 01:19 77-47-409/09/09 00:00439 Hexachloroethane ND ug/kg 1 09/23/09 01:19 67-72-109/09/09 00:00439 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/09 01:19 193-39-509/09/09 00:00439 Isophorone ND ug/kg 1 09/23/09 01:19 78-59-109/09/09 00:00439 1-Methylnaphthalene 1050 ug/kg 1 09/23/09 01:19 90-12-009/09/09 00:00439 2-Methylnaphthalene 1410 ug/kg 1 09/23/09 01:19 91-57-609/09/09 00:00439 2-Methylphenol(o-Cresol)ND ug/kg 1 09/23/09 01:19 95-48-709/09/09 00:00439 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/23/09 01:1909/09/09 00:00439 Naphthalene 901 ug/kg 1 09/23/09 01:19 91-20-309/09/09 00:00439 2-Nitroaniline ND ug/kg 1 09/23/09 01:19 88-74-409/09/09 00:002200 3-Nitroaniline ND ug/kg 1 09/23/09 01:19 99-09-209/09/09 00:002200 4-Nitroaniline ND ug/kg 1 09/23/09 01:19 100-01-609/09/09 00:00879 Nitrobenzene ND ug/kg 1 09/23/09 01:19 98-95-309/09/09 00:00439 2-Nitrophenol ND ug/kg 1 09/23/09 01:19 88-75-509/09/09 00:00439 4-Nitrophenol ND ug/kg 1 09/23/09 01:19 100-02-709/09/09 00:002200 N-Nitrosodimethylamine ND ug/kg 1 09/23/09 01:19 62-75-909/09/09 00:00439 N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/09 01:19 621-64-709/09/09 00:00439 N-Nitrosodiphenylamine ND ug/kg 1 09/23/09 01:19 86-30-609/09/09 00:00439 Pentachlorophenol ND ug/kg 1 09/23/09 01:19 87-86-509/09/09 00:002200 Phenanthrene ND ug/kg 1 09/23/09 01:19 85-01-809/09/09 00:00439 Phenol ND ug/kg 1 09/23/09 01:19 108-95-209/09/09 00:00439 Pyrene ND ug/kg 1 09/23/09 01:19 129-00-009/09/09 00:00439 1,2,4-Trichlorobenzene ND ug/kg 1 09/23/09 01:19 120-82-109/09/09 00:00439 2,4,5-Trichlorophenol ND ug/kg 1 09/23/09 01:19 95-95-409/09/09 00:00439 2,4,6-Trichlorophenol ND ug/kg 1 09/23/09 01:19 88-06-209/09/09 00:00439 Nitrobenzene-d5 (S)40 %1 09/23/09 01:19 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)48 %1 09/23/09 01:19 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)104 %1 09/23/09 01:19 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)35 %1 09/23/09 01:19 13127-88-309/09/09 00:0035-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 29 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB10-09-09 Lab ID:9252614007 Collected:09/08/09 11:25 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 2-Fluorophenol (S)33 %1 09/23/09 01:19 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)44 %1 09/23/09 01:19 118-79-609/09/09 00:0044-136 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 24.9 %1 09/09/09 13:430.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 30 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB9-09-09 Lab ID:9252614008 Collected:09/08/09 11:30 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony 0.75 mg/kg 1 09/10/09 20:37 7440-36-009/09/09 15:000.50 Arsenic 11.8 mg/kg 1 09/10/09 20:37 7440-38-209/09/09 15:000.50 Beryllium 0.36 mg/kg 1 09/10/09 20:37 7440-41-709/09/09 15:000.099 Cadmium 0.93 mg/kg 1 09/10/09 20:37 7440-43-909/09/09 15:000.099 Chromium 11.0 mg/kg 1 09/10/09 20:37 7440-47-309/09/09 15:000.50 Copper 18.5 mg/kg 1 09/10/09 20:37 7440-50-809/09/09 15:000.50 Lead 34.7 mg/kg 1 09/10/09 20:37 7439-92-109/09/09 15:000.50 Manganese 88.6 mg/kg 1 09/10/09 20:37 7439-96-509/09/09 15:000.50 Nickel 6.4 mg/kg 1 09/10/09 20:37 7440-02-009/09/09 15:000.50 Selenium ND mg/kg 1 09/10/09 20:37 7782-49-209/09/09 15:000.99 Silver ND mg/kg 1 09/10/09 20:37 7440-22-409/09/09 15:000.50 Thallium ND mg/kg 1 09/10/09 20:37 7440-28-009/09/09 15:000.99 Zinc 196 mg/kg 1 09/10/09 20:37 7440-66-609/09/09 15:000.99 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.094 mg/kg 1 09/14/09 16:33 7439-97-609/11/09 10:160.0047 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/23/09 01:43 83-32-909/09/09 00:00380 Acenaphthylene ND ug/kg 1 09/23/09 01:43 208-96-809/09/09 00:00380 Aniline ND ug/kg 1 09/23/09 01:43 62-53-309/09/09 00:00380 Anthracene ND ug/kg 1 09/23/09 01:43 120-12-709/09/09 00:00380 Benzo(a)anthracene ND ug/kg 1 09/23/09 01:43 56-55-309/09/09 00:00380 Benzo(a)pyrene ND ug/kg 1 09/23/09 01:43 50-32-809/09/09 00:00380 Benzo(b)fluoranthene ND ug/kg 1 09/23/09 01:43 205-99-209/09/09 00:00380 Benzo(g,h,i)perylene ND ug/kg 1 09/23/09 01:43 191-24-209/09/09 00:00380 Benzo(k)fluoranthene ND ug/kg 1 09/23/09 01:43 207-08-909/09/09 00:00380 Benzoic Acid ND ug/kg 1 09/23/09 01:43 65-85-009/09/09 00:001900 Benzyl alcohol ND ug/kg 1 09/23/09 01:43 100-51-609/09/09 00:00761 4-Bromophenylphenyl ether ND ug/kg 1 09/23/09 01:43 101-55-309/09/09 00:00380 Butylbenzylphthalate ND ug/kg 1 09/23/09 01:43 85-68-709/09/09 00:00380 4-Chloro-3-methylphenol ND ug/kg 1 09/23/09 01:43 59-50-709/09/09 00:00761 4-Chloroaniline ND ug/kg 1 09/23/09 01:43 106-47-809/09/09 00:001900 bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/09 01:43 111-91-109/09/09 00:00380 bis(2-Chloroethyl) ether ND ug/kg 1 09/23/09 01:43 111-44-409/09/09 00:00380 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/09 01:43 108-60-109/09/09 00:00380 2-Chloronaphthalene ND ug/kg 1 09/23/09 01:43 91-58-709/09/09 00:00380 2-Chlorophenol ND ug/kg 1 09/23/09 01:43 95-57-809/09/09 00:00380 4-Chlorophenylphenyl ether ND ug/kg 1 09/23/09 01:43 7005-72-309/09/09 00:00380 Chrysene ND ug/kg 1 09/23/09 01:43 218-01-909/09/09 00:00380 Dibenz(a,h)anthracene ND ug/kg 1 09/23/09 01:43 53-70-309/09/09 00:00380 Dibenzofuran ND ug/kg 1 09/23/09 01:43 132-64-909/09/09 00:00380 1,2-Dichlorobenzene ND ug/kg 1 09/23/09 01:43 95-50-109/09/09 00:00380 1,3-Dichlorobenzene ND ug/kg 1 09/23/09 01:43 541-73-109/09/09 00:00380 1,4-Dichlorobenzene ND ug/kg 1 09/23/09 01:43 106-46-709/09/09 00:00380 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 31 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB9-09-09 Lab ID:9252614008 Collected:09/08/09 11:30 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 3,3'-Dichlorobenzidine ND ug/kg 1 09/23/09 01:43 91-94-109/09/09 00:001900 2,4-Dichlorophenol ND ug/kg 1 09/23/09 01:43 120-83-209/09/09 00:00380 Diethylphthalate ND ug/kg 1 09/23/09 01:43 84-66-209/09/09 00:00380 2,4-Dimethylphenol ND ug/kg 1 09/23/09 01:43 105-67-909/09/09 00:00380 Dimethylphthalate ND ug/kg 1 09/23/09 01:43 131-11-309/09/09 00:00380 Di-n-butylphthalate ND ug/kg 1 09/23/09 01:43 84-74-209/09/09 00:00380 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/09 01:43 534-52-109/09/09 00:00761 2,4-Dinitrophenol ND ug/kg 1 09/23/09 01:43 51-28-509/09/09 00:001900 2,4-Dinitrotoluene ND ug/kg 1 09/23/09 01:43 121-14-209/09/09 00:00380 2,6-Dinitrotoluene ND ug/kg 1 09/23/09 01:43 606-20-209/09/09 00:00380 Di-n-octylphthalate ND ug/kg 1 09/23/09 01:43 117-84-009/09/09 00:00380 1,2-Diphenylhydrazine ND ug/kg 1 09/23/09 01:43 122-66-709/09/09 00:00380 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/09 01:43 117-81-709/09/09 00:00380 Fluoranthene ND ug/kg 1 09/23/09 01:43 206-44-009/09/09 00:00380 Fluorene ND ug/kg 1 09/23/09 01:43 86-73-709/09/09 00:00380 Hexachloro-1,3-butadiene ND ug/kg 1 09/23/09 01:43 87-68-309/09/09 00:00380 Hexachlorobenzene ND ug/kg 1 09/23/09 01:43 118-74-109/09/09 00:00380 Hexachlorocyclopentadiene ND ug/kg 1 09/23/09 01:43 77-47-409/09/09 00:00380 Hexachloroethane ND ug/kg 1 09/23/09 01:43 67-72-109/09/09 00:00380 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/09 01:43 193-39-509/09/09 00:00380 Isophorone ND ug/kg 1 09/23/09 01:43 78-59-109/09/09 00:00380 1-Methylnaphthalene 1450 ug/kg 1 09/23/09 01:43 90-12-009/09/09 00:00380 2-Methylnaphthalene 1770 ug/kg 1 09/23/09 01:43 91-57-609/09/09 00:00380 2-Methylphenol(o-Cresol)ND ug/kg 1 09/23/09 01:43 95-48-709/09/09 00:00380 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/23/09 01:4309/09/09 00:00380 Naphthalene 1270 ug/kg 1 09/23/09 01:43 91-20-309/09/09 00:00380 2-Nitroaniline ND ug/kg 1 09/23/09 01:43 88-74-409/09/09 00:001900 3-Nitroaniline ND ug/kg 1 09/23/09 01:43 99-09-209/09/09 00:001900 4-Nitroaniline ND ug/kg 1 09/23/09 01:43 100-01-609/09/09 00:00761 Nitrobenzene ND ug/kg 1 09/23/09 01:43 98-95-309/09/09 00:00380 2-Nitrophenol ND ug/kg 1 09/23/09 01:43 88-75-509/09/09 00:00380 4-Nitrophenol ND ug/kg 1 09/23/09 01:43 100-02-709/09/09 00:001900 N-Nitrosodimethylamine ND ug/kg 1 09/23/09 01:43 62-75-909/09/09 00:00380 N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/09 01:43 621-64-709/09/09 00:00380 N-Nitrosodiphenylamine ND ug/kg 1 09/23/09 01:43 86-30-609/09/09 00:00380 Pentachlorophenol ND ug/kg 1 09/23/09 01:43 87-86-509/09/09 00:001900 Phenanthrene 662 ug/kg 1 09/23/09 01:43 85-01-809/09/09 00:00380 Phenol ND ug/kg 1 09/23/09 01:43 108-95-209/09/09 00:00380 Pyrene 450 ug/kg 1 09/23/09 01:43 129-00-009/09/09 00:00380 1,2,4-Trichlorobenzene ND ug/kg 1 09/23/09 01:43 120-82-109/09/09 00:00380 2,4,5-Trichlorophenol ND ug/kg 1 09/23/09 01:43 95-95-409/09/09 00:00380 2,4,6-Trichlorophenol ND ug/kg 1 09/23/09 01:43 88-06-209/09/09 00:00380 Nitrobenzene-d5 (S)55 %1 09/23/09 01:43 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)65 %1 09/23/09 01:43 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)97 %1 09/23/09 01:43 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)46 %1 09/23/09 01:43 13127-88-309/09/09 00:0035-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 32 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB9-09-09 Lab ID:9252614008 Collected:09/08/09 11:30 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 2-Fluorophenol (S)42 %1 09/23/09 01:43 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)51 %1 09/23/09 01:43 118-79-609/09/09 00:0044-136 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 13.3 %1 09/09/09 13:430.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 33 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB8-09-09 Lab ID:9252614009 Collected:09/08/09 11:40 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony ND mg/kg 10 09/11/09 11:45 7440-36-009/09/09 15:003.4 Arsenic 4.2 mg/kg 10 09/11/09 11:45 7440-38-209/09/09 15:003.4 Beryllium 1.1 mg/kg 10 09/11/09 11:45 7440-41-709/09/09 15:000.68 Cadmium ND mg/kg 10 09/11/09 11:45 7440-43-909/09/09 15:000.68 Chromium 58.4 mg/kg 10 09/11/09 11:45 7440-47-309/09/09 15:003.4 Copper 27.6 mg/kg 10 09/11/09 11:45 7440-50-809/09/09 15:003.4 Lead 11.0 mg/kg 10 09/11/09 11:45 7439-92-109/09/09 15:003.4 Manganese 499 mg/kg 10 09/11/09 11:45 7439-96-509/09/09 15:003.4 Nickel 12.4 mg/kg 10 09/11/09 11:45 7440-02-009/09/09 15:003.4 Selenium ND mg/kg 10 09/11/09 11:45 7782-49-209/09/09 15:006.8 Silver ND mg/kg 10 09/11/09 11:45 7440-22-409/09/09 15:003.4 Thallium ND mg/kg 10 09/11/09 11:45 7440-28-009/09/09 15:006.8 Zinc 50.7 mg/kg 10 09/11/09 11:45 7440-66-609/09/09 15:006.8 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.091 mg/kg 1 09/14/09 16:35 7439-97-609/11/09 10:160.0060 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/23/09 02:08 83-32-909/09/09 00:00394 Acenaphthylene ND ug/kg 1 09/23/09 02:08 208-96-809/09/09 00:00394 Aniline ND ug/kg 1 09/23/09 02:08 62-53-309/09/09 00:00394 Anthracene ND ug/kg 1 09/23/09 02:08 120-12-709/09/09 00:00394 Benzo(a)anthracene ND ug/kg 1 09/23/09 02:08 56-55-309/09/09 00:00394 Benzo(a)pyrene ND ug/kg 1 09/23/09 02:08 50-32-809/09/09 00:00394 Benzo(b)fluoranthene ND ug/kg 1 09/23/09 02:08 205-99-209/09/09 00:00394 Benzo(g,h,i)perylene ND ug/kg 1 09/23/09 02:08 191-24-209/09/09 00:00394 Benzo(k)fluoranthene ND ug/kg 1 09/23/09 02:08 207-08-909/09/09 00:00394 Benzoic Acid ND ug/kg 1 09/23/09 02:08 65-85-009/09/09 00:001970 Benzyl alcohol ND ug/kg 1 09/23/09 02:08 100-51-609/09/09 00:00788 4-Bromophenylphenyl ether ND ug/kg 1 09/23/09 02:08 101-55-309/09/09 00:00394 Butylbenzylphthalate ND ug/kg 1 09/23/09 02:08 85-68-709/09/09 00:00394 4-Chloro-3-methylphenol ND ug/kg 1 09/23/09 02:08 59-50-709/09/09 00:00788 4-Chloroaniline ND ug/kg 1 09/23/09 02:08 106-47-809/09/09 00:001970 bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/09 02:08 111-91-109/09/09 00:00394 bis(2-Chloroethyl) ether ND ug/kg 1 09/23/09 02:08 111-44-409/09/09 00:00394 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/09 02:08 108-60-109/09/09 00:00394 2-Chloronaphthalene ND ug/kg 1 09/23/09 02:08 91-58-709/09/09 00:00394 2-Chlorophenol ND ug/kg 1 09/23/09 02:08 95-57-809/09/09 00:00394 4-Chlorophenylphenyl ether ND ug/kg 1 09/23/09 02:08 7005-72-309/09/09 00:00394 Chrysene ND ug/kg 1 09/23/09 02:08 218-01-909/09/09 00:00394 Dibenz(a,h)anthracene ND ug/kg 1 09/23/09 02:08 53-70-309/09/09 00:00394 Dibenzofuran ND ug/kg 1 09/23/09 02:08 132-64-909/09/09 00:00394 1,2-Dichlorobenzene ND ug/kg 1 09/23/09 02:08 95-50-109/09/09 00:00394 1,3-Dichlorobenzene ND ug/kg 1 09/23/09 02:08 541-73-109/09/09 00:00394 1,4-Dichlorobenzene ND ug/kg 1 09/23/09 02:08 106-46-709/09/09 00:00394 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 34 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB8-09-09 Lab ID:9252614009 Collected:09/08/09 11:40 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 3,3'-Dichlorobenzidine ND ug/kg 1 09/23/09 02:08 91-94-109/09/09 00:001970 2,4-Dichlorophenol ND ug/kg 1 09/23/09 02:08 120-83-209/09/09 00:00394 Diethylphthalate ND ug/kg 1 09/23/09 02:08 84-66-209/09/09 00:00394 2,4-Dimethylphenol ND ug/kg 1 09/23/09 02:08 105-67-909/09/09 00:00394 Dimethylphthalate ND ug/kg 1 09/23/09 02:08 131-11-309/09/09 00:00394 Di-n-butylphthalate ND ug/kg 1 09/23/09 02:08 84-74-209/09/09 00:00394 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/09 02:08 534-52-109/09/09 00:00788 2,4-Dinitrophenol ND ug/kg 1 09/23/09 02:08 51-28-509/09/09 00:001970 2,4-Dinitrotoluene ND ug/kg 1 09/23/09 02:08 121-14-209/09/09 00:00394 2,6-Dinitrotoluene ND ug/kg 1 09/23/09 02:08 606-20-209/09/09 00:00394 Di-n-octylphthalate ND ug/kg 1 09/23/09 02:08 117-84-009/09/09 00:00394 1,2-Diphenylhydrazine ND ug/kg 1 09/23/09 02:08 122-66-709/09/09 00:00394 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/09 02:08 117-81-709/09/09 00:00394 Fluoranthene ND ug/kg 1 09/23/09 02:08 206-44-009/09/09 00:00394 Fluorene ND ug/kg 1 09/23/09 02:08 86-73-709/09/09 00:00394 Hexachloro-1,3-butadiene ND ug/kg 1 09/23/09 02:08 87-68-309/09/09 00:00394 Hexachlorobenzene ND ug/kg 1 09/23/09 02:08 118-74-109/09/09 00:00394 Hexachlorocyclopentadiene ND ug/kg 1 09/23/09 02:08 77-47-409/09/09 00:00394 Hexachloroethane ND ug/kg 1 09/23/09 02:08 67-72-109/09/09 00:00394 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/09 02:08 193-39-509/09/09 00:00394 Isophorone ND ug/kg 1 09/23/09 02:08 78-59-109/09/09 00:00394 1-Methylnaphthalene ND ug/kg 1 09/23/09 02:08 90-12-009/09/09 00:00394 2-Methylnaphthalene ND ug/kg 1 09/23/09 02:08 91-57-609/09/09 00:00394 2-Methylphenol(o-Cresol)ND ug/kg 1 09/23/09 02:08 95-48-709/09/09 00:00394 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/23/09 02:0809/09/09 00:00394 Naphthalene ND ug/kg 1 09/23/09 02:08 91-20-309/09/09 00:00394 2-Nitroaniline ND ug/kg 1 09/23/09 02:08 88-74-409/09/09 00:001970 3-Nitroaniline ND ug/kg 1 09/23/09 02:08 99-09-209/09/09 00:001970 4-Nitroaniline ND ug/kg 1 09/23/09 02:08 100-01-609/09/09 00:00788 Nitrobenzene ND ug/kg 1 09/23/09 02:08 98-95-309/09/09 00:00394 2-Nitrophenol ND ug/kg 1 09/23/09 02:08 88-75-509/09/09 00:00394 4-Nitrophenol ND ug/kg 1 09/23/09 02:08 100-02-709/09/09 00:001970 N-Nitrosodimethylamine ND ug/kg 1 09/23/09 02:08 62-75-909/09/09 00:00394 N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/09 02:08 621-64-709/09/09 00:00394 N-Nitrosodiphenylamine ND ug/kg 1 09/23/09 02:08 86-30-609/09/09 00:00394 Pentachlorophenol ND ug/kg 1 09/23/09 02:08 87-86-509/09/09 00:001970 Phenanthrene ND ug/kg 1 09/23/09 02:08 85-01-809/09/09 00:00394 Phenol ND ug/kg 1 09/23/09 02:08 108-95-209/09/09 00:00394 Pyrene ND ug/kg 1 09/23/09 02:08 129-00-009/09/09 00:00394 1,2,4-Trichlorobenzene ND ug/kg 1 09/23/09 02:08 120-82-109/09/09 00:00394 2,4,5-Trichlorophenol ND ug/kg 1 09/23/09 02:08 95-95-409/09/09 00:00394 2,4,6-Trichlorophenol ND ug/kg 1 09/23/09 02:08 88-06-209/09/09 00:00394 Nitrobenzene-d5 (S)47 %1 09/23/09 02:08 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)61 %1 09/23/09 02:08 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)99 %1 09/23/09 02:08 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)43 %1 09/23/09 02:08 13127-88-309/09/09 00:0035-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 35 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB8-09-09 Lab ID:9252614009 Collected:09/08/09 11:40 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 2-Fluorophenol (S)37 %1 09/23/09 02:08 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)59 %1 09/23/09 02:08 118-79-609/09/09 00:0044-136 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 16.2 %1 09/09/09 13:430.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 36 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -BK1-09-09 Lab ID:9252614010 Collected:09/08/09 11:55 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony ND mg/kg 5 09/11/09 11:49 7440-36-009/09/09 15:002.7 Arsenic 3.2 mg/kg 5 09/11/09 11:49 7440-38-209/09/09 15:002.7 Beryllium 0.61 mg/kg 5 09/11/09 11:49 7440-41-709/09/09 15:000.55 Cadmium ND mg/kg 5 09/11/09 11:49 7440-43-909/09/09 15:000.55 Chromium 20.2 mg/kg 5 09/11/09 11:49 7440-47-309/09/09 15:002.7 Copper 47.6 mg/kg 5 09/11/09 11:49 7440-50-809/09/09 15:002.7 Lead 65.6 mg/kg 5 09/11/09 11:49 7439-92-109/09/09 15:002.7 Manganese 274 mg/kg 5 09/11/09 11:49 7439-96-509/09/09 15:002.7 Nickel 14.1 mg/kg 5 09/11/09 11:49 7440-02-009/09/09 15:002.7 Selenium ND mg/kg 5 09/11/09 11:49 7782-49-209/09/09 15:005.5 Silver ND mg/kg 5 09/11/09 11:49 7440-22-409/09/09 15:002.7 Thallium ND mg/kg 5 09/11/09 11:49 7440-28-009/09/09 15:005.5 Zinc 115 mg/kg 5 09/11/09 11:49 7440-66-609/09/09 15:005.5 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.069 mg/kg 1 09/14/09 16:48 7439-97-609/11/09 10:160.0062 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 19.7 %1 09/09/09 13:440.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 37 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP1-09-09 Lab ID:9252614011 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Antimony ND mg/kg 5 09/11/09 11:52 7440-36-009/09/09 15:002.3 Arsenic 3.4 mg/kg 5 09/11/09 11:52 7440-38-209/09/09 15:002.3 Beryllium 0.59 mg/kg 5 09/11/09 11:52 7440-41-709/09/09 15:000.46 Cadmium ND mg/kg 5 09/11/09 11:52 7440-43-909/09/09 15:000.46 Chromium 20.0 mg/kg 5 09/11/09 11:52 7440-47-309/09/09 15:002.3 Copper 41.6 mg/kg 5 09/11/09 11:52 7440-50-809/09/09 15:002.3 Lead 103 mg/kg 5 09/11/09 11:52 7439-92-109/09/09 15:002.3 Manganese 277 mg/kg 5 09/11/09 11:52 7439-96-509/09/09 15:002.3 Nickel 12.9 mg/kg 5 09/11/09 11:52 7440-02-009/09/09 15:002.3 Selenium ND mg/kg 5 09/11/09 11:52 7782-49-209/09/09 15:004.6 Silver ND mg/kg 5 09/11/09 11:52 7440-22-409/09/09 15:002.3 Thallium ND mg/kg 5 09/11/09 11:52 7440-28-009/09/09 15:004.6 Zinc 125 mg/kg 5 09/11/09 11:52 7440-66-609/09/09 15:004.6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 0.049 mg/kg 1 09/14/09 16:51 7439-97-609/11/09 10:160.0052 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 9.6 %1 09/09/09 13:440.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 38 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB1-09-09 Lab ID:9252614012 Collected:09/08/09 12:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/23/09 02:32 83-32-909/09/09 00:00391 Acenaphthylene ND ug/kg 1 09/23/09 02:32 208-96-809/09/09 00:00391 Aniline ND ug/kg 1 09/23/09 02:32 62-53-309/09/09 00:00391 Anthracene ND ug/kg 1 09/23/09 02:32 120-12-709/09/09 00:00391 Benzo(a)anthracene ND ug/kg 1 09/23/09 02:32 56-55-309/09/09 00:00391 Benzo(a)pyrene ND ug/kg 1 09/23/09 02:32 50-32-809/09/09 00:00391 Benzo(b)fluoranthene ND ug/kg 1 09/23/09 02:32 205-99-209/09/09 00:00391 Benzo(g,h,i)perylene ND ug/kg 1 09/23/09 02:32 191-24-209/09/09 00:00391 Benzo(k)fluoranthene ND ug/kg 1 09/23/09 02:32 207-08-909/09/09 00:00391 Benzoic Acid ND ug/kg 1 09/23/09 02:32 65-85-009/09/09 00:001950 Benzyl alcohol ND ug/kg 1 09/23/09 02:32 100-51-609/09/09 00:00781 4-Bromophenylphenyl ether ND ug/kg 1 09/23/09 02:32 101-55-309/09/09 00:00391 Butylbenzylphthalate ND ug/kg 1 09/23/09 02:32 85-68-709/09/09 00:00391 4-Chloro-3-methylphenol ND ug/kg 1 09/23/09 02:32 59-50-709/09/09 00:00781 4-Chloroaniline ND ug/kg 1 09/23/09 02:32 106-47-809/09/09 00:001950 bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/09 02:32 111-91-109/09/09 00:00391 bis(2-Chloroethyl) ether ND ug/kg 1 09/23/09 02:32 111-44-409/09/09 00:00391 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/09 02:32 108-60-109/09/09 00:00391 2-Chloronaphthalene ND ug/kg 1 09/23/09 02:32 91-58-709/09/09 00:00391 2-Chlorophenol ND ug/kg 1 09/23/09 02:32 95-57-809/09/09 00:00391 4-Chlorophenylphenyl ether ND ug/kg 1 09/23/09 02:32 7005-72-309/09/09 00:00391 Chrysene ND ug/kg 1 09/23/09 02:32 218-01-909/09/09 00:00391 Dibenz(a,h)anthracene ND ug/kg 1 09/23/09 02:32 53-70-309/09/09 00:00391 Dibenzofuran ND ug/kg 1 09/23/09 02:32 132-64-909/09/09 00:00391 1,2-Dichlorobenzene ND ug/kg 1 09/23/09 02:32 95-50-109/09/09 00:00391 1,3-Dichlorobenzene ND ug/kg 1 09/23/09 02:32 541-73-109/09/09 00:00391 1,4-Dichlorobenzene ND ug/kg 1 09/23/09 02:32 106-46-709/09/09 00:00391 3,3'-Dichlorobenzidine ND ug/kg 1 09/23/09 02:32 91-94-109/09/09 00:001950 2,4-Dichlorophenol ND ug/kg 1 09/23/09 02:32 120-83-209/09/09 00:00391 Diethylphthalate ND ug/kg 1 09/23/09 02:32 84-66-209/09/09 00:00391 2,4-Dimethylphenol ND ug/kg 1 09/23/09 02:32 105-67-909/09/09 00:00391 Dimethylphthalate ND ug/kg 1 09/23/09 02:32 131-11-309/09/09 00:00391 Di-n-butylphthalate ND ug/kg 1 09/23/09 02:32 84-74-209/09/09 00:00391 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/09 02:32 534-52-109/09/09 00:00781 2,4-Dinitrophenol ND ug/kg 1 09/23/09 02:32 51-28-509/09/09 00:001950 2,4-Dinitrotoluene ND ug/kg 1 09/23/09 02:32 121-14-209/09/09 00:00391 2,6-Dinitrotoluene ND ug/kg 1 09/23/09 02:32 606-20-209/09/09 00:00391 Di-n-octylphthalate ND ug/kg 1 09/23/09 02:32 117-84-009/09/09 00:00391 1,2-Diphenylhydrazine ND ug/kg 1 09/23/09 02:32 122-66-709/09/09 00:00391 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/09 02:32 117-81-709/09/09 00:00391 Fluoranthene ND ug/kg 1 09/23/09 02:32 206-44-009/09/09 00:00391 Fluorene ND ug/kg 1 09/23/09 02:32 86-73-709/09/09 00:00391 Hexachloro-1,3-butadiene ND ug/kg 1 09/23/09 02:32 87-68-309/09/09 00:00391 Hexachlorobenzene ND ug/kg 1 09/23/09 02:32 118-74-109/09/09 00:00391 Hexachlorocyclopentadiene ND ug/kg 1 09/23/09 02:32 77-47-409/09/09 00:00391 Hexachloroethane ND ug/kg 1 09/23/09 02:32 67-72-109/09/09 00:00391 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 39 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB1-09-09 Lab ID:9252614012 Collected:09/08/09 12:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/09 02:32 193-39-509/09/09 00:00391 Isophorone ND ug/kg 1 09/23/09 02:32 78-59-109/09/09 00:00391 1-Methylnaphthalene 8840 ug/kg 20 10/02/09 23:18 90-12-009/09/09 00:007810 2-Methylnaphthalene 15800 ug/kg 20 10/02/09 23:18 91-57-609/09/09 00:007810 2-Methylphenol(o-Cresol)ND ug/kg 1 09/23/09 02:32 95-48-709/09/09 00:00391 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/23/09 02:3209/09/09 00:00391 Naphthalene 15700 ug/kg 20 10/02/09 23:18 91-20-309/09/09 00:007810 2-Nitroaniline ND ug/kg 1 09/23/09 02:32 88-74-409/09/09 00:001950 3-Nitroaniline ND ug/kg 1 09/23/09 02:32 99-09-209/09/09 00:001950 4-Nitroaniline ND ug/kg 1 09/23/09 02:32 100-01-609/09/09 00:00781 Nitrobenzene ND ug/kg 1 09/23/09 02:32 98-95-309/09/09 00:00391 2-Nitrophenol ND ug/kg 1 09/23/09 02:32 88-75-509/09/09 00:00391 4-Nitrophenol ND ug/kg 1 09/23/09 02:32 100-02-709/09/09 00:001950 N-Nitrosodimethylamine ND ug/kg 1 09/23/09 02:32 62-75-909/09/09 00:00391 N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/09 02:32 621-64-709/09/09 00:00391 N-Nitrosodiphenylamine ND ug/kg 1 09/23/09 02:32 86-30-609/09/09 00:00391 Pentachlorophenol ND ug/kg 1 09/23/09 02:32 87-86-509/09/09 00:001950 Phenanthrene ND ug/kg 1 09/23/09 02:32 85-01-809/09/09 00:00391 Phenol ND ug/kg 1 09/23/09 02:32 108-95-209/09/09 00:00391 Pyrene ND ug/kg 1 09/23/09 02:32 129-00-009/09/09 00:00391 1,2,4-Trichlorobenzene ND ug/kg 1 09/23/09 02:32 120-82-109/09/09 00:00391 2,4,5-Trichlorophenol ND ug/kg 1 09/23/09 02:32 95-95-409/09/09 00:00391 2,4,6-Trichlorophenol ND ug/kg 1 09/23/09 02:32 88-06-209/09/09 00:00391 Nitrobenzene-d5 (S)38 %1 09/23/09 02:32 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)48 %1 09/23/09 02:32 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)93 %1 09/23/09 02:32 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)31 %1 09/23/09 02:32 13127-88-3 1g,S009/09/09 00:0035-120 2-Fluorophenol (S)31 %1 09/23/09 02:32 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)48 %1 09/23/09 02:32 118-79-609/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/10/09 15:51 67-64-14270 Benzene 251 ug/kg 50 09/10/09 15:51 71-43-2213 Bromobenzene ND ug/kg 50 09/10/09 15:51 108-86-1213 Bromochloromethane ND ug/kg 50 09/10/09 15:51 74-97-5213 Bromodichloromethane ND ug/kg 50 09/10/09 15:51 75-27-4213 Bromoform ND ug/kg 50 09/10/09 15:51 75-25-2213 Bromomethane ND ug/kg 50 09/10/09 15:51 74-83-9427 2-Butanone (MEK)ND ug/kg 50 09/10/09 15:51 78-93-34270 n-Butylbenzene ND ug/kg 50 09/10/09 15:51 104-51-8213 sec-Butylbenzene ND ug/kg 50 09/10/09 15:51 135-98-8213 tert-Butylbenzene ND ug/kg 50 09/10/09 15:51 98-06-6213 Carbon tetrachloride ND ug/kg 50 09/10/09 15:51 56-23-5213 Chlorobenzene ND ug/kg 50 09/10/09 15:51 108-90-7213 Chloroethane ND ug/kg 50 09/10/09 15:51 75-00-3427 Chloroform ND ug/kg 50 09/10/09 15:51 67-66-3213 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 40 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB1-09-09 Lab ID:9252614012 Collected:09/08/09 12:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 50 09/10/09 15:51 74-87-3427 2-Chlorotoluene ND ug/kg 50 09/10/09 15:51 95-49-8213 4-Chlorotoluene ND ug/kg 50 09/10/09 15:51 106-43-4213 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/10/09 15:51 96-12-8213 Dibromochloromethane ND ug/kg 50 09/10/09 15:51 124-48-1213 1,2-Dibromoethane (EDB)ND ug/kg 50 09/10/09 15:51 106-93-4213 Dibromomethane ND ug/kg 50 09/10/09 15:51 74-95-3213 1,2-Dichlorobenzene ND ug/kg 50 09/10/09 15:51 95-50-1213 1,3-Dichlorobenzene ND ug/kg 50 09/10/09 15:51 541-73-1213 1,4-Dichlorobenzene ND ug/kg 50 09/10/09 15:51 106-46-7213 Dichlorodifluoromethane ND ug/kg 50 09/10/09 15:51 75-71-8427 1,1-Dichloroethane ND ug/kg 50 09/10/09 15:51 75-34-3213 1,2-Dichloroethane ND ug/kg 50 09/10/09 15:51 107-06-2213 1,1-Dichloroethene ND ug/kg 50 09/10/09 15:51 75-35-4213 cis-1,2-Dichloroethene ND ug/kg 50 09/10/09 15:51 156-59-2213 trans-1,2-Dichloroethene ND ug/kg 50 09/10/09 15:51 156-60-5213 1,2-Dichloropropane ND ug/kg 50 09/10/09 15:51 78-87-5213 1,3-Dichloropropane ND ug/kg 50 09/10/09 15:51 142-28-9213 2,2-Dichloropropane ND ug/kg 50 09/10/09 15:51 594-20-7213 1,1-Dichloropropene ND ug/kg 50 09/10/09 15:51 563-58-6213 cis-1,3-Dichloropropene ND ug/kg 50 09/10/09 15:51 10061-01-5213 trans-1,3-Dichloropropene ND ug/kg 50 09/10/09 15:51 10061-02-6213 Diisopropyl ether ND ug/kg 50 09/10/09 15:51 108-20-3213 Ethylbenzene 431 ug/kg 50 09/10/09 15:51 100-41-4213 Hexachloro-1,3-butadiene ND ug/kg 50 09/10/09 15:51 87-68-3213 2-Hexanone ND ug/kg 50 09/10/09 15:51 591-78-62130 Isopropylbenzene (Cumene)246 ug/kg 50 09/10/09 15:51 98-82-8213 p-Isopropyltoluene ND ug/kg 50 09/10/09 15:51 99-87-6213 Methylene Chloride ND ug/kg 50 09/10/09 15:51 75-09-2854 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/10/09 15:51 108-10-12130 Methyl-tert-butyl ether ND ug/kg 50 09/10/09 15:51 1634-04-4213 Naphthalene 1580 ug/kg 50 09/10/09 15:51 91-20-3213 n-Propylbenzene 851 ug/kg 50 09/10/09 15:51 103-65-1213 Styrene ND ug/kg 50 09/10/09 15:51 100-42-5213 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/10/09 15:51 630-20-6213 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/10/09 15:51 79-34-5213 Tetrachloroethene ND ug/kg 50 09/10/09 15:51 127-18-4213 Toluene ND ug/kg 50 09/10/09 15:51 108-88-3213 1,2,3-Trichlorobenzene ND ug/kg 50 09/10/09 15:51 87-61-6213 1,2,4-Trichlorobenzene ND ug/kg 50 09/10/09 15:51 120-82-1213 1,1,1-Trichloroethane ND ug/kg 50 09/10/09 15:51 71-55-6213 1,1,2-Trichloroethane ND ug/kg 50 09/10/09 15:51 79-00-5213 Trichloroethene ND ug/kg 50 09/10/09 15:51 79-01-6213 Trichlorofluoromethane ND ug/kg 50 09/10/09 15:51 75-69-4213 1,2,3-Trichloropropane ND ug/kg 50 09/10/09 15:51 96-18-4213 1,2,4-Trimethylbenzene 250 ug/kg 50 09/10/09 15:51 95-63-6213 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 41 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB1-09-09 Lab ID:9252614012 Collected:09/08/09 12:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene ND ug/kg 50 09/10/09 15:51 108-67-8213 Vinyl acetate ND ug/kg 50 09/10/09 15:51 108-05-42130 Vinyl chloride ND ug/kg 50 09/10/09 15:51 75-01-4427 Xylene (Total)696 ug/kg 50 09/10/09 15:51 1330-20-7427 m&p-Xylene 616 ug/kg 50 09/10/09 15:51 1330-20-7427 o-Xylene ND ug/kg 50 09/10/09 15:51 95-47-6213 Dibromofluoromethane (S)97 %50 09/10/09 15:51 1868-53-7 D379-116 Toluene-d8 (S)101 %50 09/10/09 15:51 2037-26-588-110 4-Bromofluorobenzene (S)98 %50 09/10/09 15:51 460-00-474-115 1,2-Dichloroethane-d4 (S)95 %50 09/10/09 15:51 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 15.5 %1 09/09/09 13:440.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 42 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB2-09-09 Lab ID:9252614013 Collected:09/08/09 12:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/23/09 02:56 83-32-909/09/09 00:00375 Acenaphthylene ND ug/kg 1 09/23/09 02:56 208-96-809/09/09 00:00375 Aniline ND ug/kg 1 09/23/09 02:56 62-53-309/09/09 00:00375 Anthracene ND ug/kg 1 09/23/09 02:56 120-12-709/09/09 00:00375 Benzo(a)anthracene ND ug/kg 1 09/23/09 02:56 56-55-309/09/09 00:00375 Benzo(a)pyrene ND ug/kg 1 09/23/09 02:56 50-32-809/09/09 00:00375 Benzo(b)fluoranthene ND ug/kg 1 09/23/09 02:56 205-99-209/09/09 00:00375 Benzo(g,h,i)perylene ND ug/kg 1 09/23/09 02:56 191-24-209/09/09 00:00375 Benzo(k)fluoranthene ND ug/kg 1 09/23/09 02:56 207-08-909/09/09 00:00375 Benzoic Acid ND ug/kg 1 09/23/09 02:56 65-85-009/09/09 00:001880 Benzyl alcohol ND ug/kg 1 09/23/09 02:56 100-51-609/09/09 00:00751 4-Bromophenylphenyl ether ND ug/kg 1 09/23/09 02:56 101-55-309/09/09 00:00375 Butylbenzylphthalate ND ug/kg 1 09/23/09 02:56 85-68-709/09/09 00:00375 4-Chloro-3-methylphenol ND ug/kg 1 09/23/09 02:56 59-50-709/09/09 00:00751 4-Chloroaniline ND ug/kg 1 09/23/09 02:56 106-47-809/09/09 00:001880 bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/09 02:56 111-91-109/09/09 00:00375 bis(2-Chloroethyl) ether ND ug/kg 1 09/23/09 02:56 111-44-409/09/09 00:00375 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/09 02:56 108-60-109/09/09 00:00375 2-Chloronaphthalene ND ug/kg 1 09/23/09 02:56 91-58-709/09/09 00:00375 2-Chlorophenol ND ug/kg 1 09/23/09 02:56 95-57-809/09/09 00:00375 4-Chlorophenylphenyl ether ND ug/kg 1 09/23/09 02:56 7005-72-309/09/09 00:00375 Chrysene ND ug/kg 1 09/23/09 02:56 218-01-909/09/09 00:00375 Dibenz(a,h)anthracene ND ug/kg 1 09/23/09 02:56 53-70-309/09/09 00:00375 Dibenzofuran ND ug/kg 1 09/23/09 02:56 132-64-909/09/09 00:00375 1,2-Dichlorobenzene ND ug/kg 1 09/23/09 02:56 95-50-109/09/09 00:00375 1,3-Dichlorobenzene ND ug/kg 1 09/23/09 02:56 541-73-109/09/09 00:00375 1,4-Dichlorobenzene ND ug/kg 1 09/23/09 02:56 106-46-709/09/09 00:00375 3,3'-Dichlorobenzidine ND ug/kg 1 09/23/09 02:56 91-94-109/09/09 00:001880 2,4-Dichlorophenol ND ug/kg 1 09/23/09 02:56 120-83-209/09/09 00:00375 Diethylphthalate ND ug/kg 1 09/23/09 02:56 84-66-209/09/09 00:00375 2,4-Dimethylphenol ND ug/kg 1 09/23/09 02:56 105-67-909/09/09 00:00375 Dimethylphthalate ND ug/kg 1 09/23/09 02:56 131-11-309/09/09 00:00375 Di-n-butylphthalate ND ug/kg 1 09/23/09 02:56 84-74-209/09/09 00:00375 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/09 02:56 534-52-109/09/09 00:00751 2,4-Dinitrophenol ND ug/kg 1 09/23/09 02:56 51-28-509/09/09 00:001880 2,4-Dinitrotoluene ND ug/kg 1 09/23/09 02:56 121-14-209/09/09 00:00375 2,6-Dinitrotoluene ND ug/kg 1 09/23/09 02:56 606-20-209/09/09 00:00375 Di-n-octylphthalate ND ug/kg 1 09/23/09 02:56 117-84-009/09/09 00:00375 1,2-Diphenylhydrazine ND ug/kg 1 09/23/09 02:56 122-66-709/09/09 00:00375 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/09 02:56 117-81-709/09/09 00:00375 Fluoranthene ND ug/kg 1 09/23/09 02:56 206-44-009/09/09 00:00375 Fluorene ND ug/kg 1 09/23/09 02:56 86-73-709/09/09 00:00375 Hexachloro-1,3-butadiene ND ug/kg 1 09/23/09 02:56 87-68-309/09/09 00:00375 Hexachlorobenzene ND ug/kg 1 09/23/09 02:56 118-74-109/09/09 00:00375 Hexachlorocyclopentadiene ND ug/kg 1 09/23/09 02:56 77-47-409/09/09 00:00375 Hexachloroethane ND ug/kg 1 09/23/09 02:56 67-72-109/09/09 00:00375 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 43 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB2-09-09 Lab ID:9252614013 Collected:09/08/09 12:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/09 02:56 193-39-509/09/09 00:00375 Isophorone ND ug/kg 1 09/23/09 02:56 78-59-109/09/09 00:00375 1-Methylnaphthalene 1280 ug/kg 1 09/23/09 02:56 90-12-009/09/09 00:00375 2-Methylnaphthalene 2350 ug/kg 1 09/23/09 02:56 91-57-609/09/09 00:00375 2-Methylphenol(o-Cresol)ND ug/kg 1 09/23/09 02:56 95-48-709/09/09 00:00375 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/23/09 02:5609/09/09 00:00375 Naphthalene 2210 ug/kg 1 09/23/09 02:56 91-20-309/09/09 00:00375 2-Nitroaniline ND ug/kg 1 09/23/09 02:56 88-74-409/09/09 00:001880 3-Nitroaniline ND ug/kg 1 09/23/09 02:56 99-09-209/09/09 00:001880 4-Nitroaniline ND ug/kg 1 09/23/09 02:56 100-01-609/09/09 00:00751 Nitrobenzene ND ug/kg 1 09/23/09 02:56 98-95-309/09/09 00:00375 2-Nitrophenol ND ug/kg 1 09/23/09 02:56 88-75-509/09/09 00:00375 4-Nitrophenol ND ug/kg 1 09/23/09 02:56 100-02-709/09/09 00:001880 N-Nitrosodimethylamine ND ug/kg 1 09/23/09 02:56 62-75-909/09/09 00:00375 N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/09 02:56 621-64-709/09/09 00:00375 N-Nitrosodiphenylamine ND ug/kg 1 09/23/09 02:56 86-30-609/09/09 00:00375 Pentachlorophenol ND ug/kg 1 09/23/09 02:56 87-86-509/09/09 00:001880 Phenanthrene ND ug/kg 1 09/23/09 02:56 85-01-809/09/09 00:00375 Phenol ND ug/kg 1 09/23/09 02:56 108-95-209/09/09 00:00375 Pyrene ND ug/kg 1 09/23/09 02:56 129-00-009/09/09 00:00375 1,2,4-Trichlorobenzene ND ug/kg 1 09/23/09 02:56 120-82-109/09/09 00:00375 2,4,5-Trichlorophenol ND ug/kg 1 09/23/09 02:56 95-95-409/09/09 00:00375 2,4,6-Trichlorophenol ND ug/kg 1 09/23/09 02:56 88-06-209/09/09 00:00375 Nitrobenzene-d5 (S)44 %1 09/23/09 02:56 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)49 %1 09/23/09 02:56 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)89 %1 09/23/09 02:56 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)35 %1 09/23/09 02:56 13127-88-309/09/09 00:0035-120 2-Fluorophenol (S)29 %1 09/23/09 02:56 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)52 %1 09/23/09 02:56 118-79-609/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/11/09 17:57 67-64-14670 Benzene ND ug/kg 50 09/11/09 17:57 71-43-2233 Bromobenzene ND ug/kg 50 09/11/09 17:57 108-86-1233 Bromochloromethane ND ug/kg 50 09/11/09 17:57 74-97-5233 Bromodichloromethane ND ug/kg 50 09/11/09 17:57 75-27-4233 Bromoform ND ug/kg 50 09/11/09 17:57 75-25-2233 Bromomethane ND ug/kg 50 09/11/09 17:57 74-83-9467 2-Butanone (MEK)ND ug/kg 50 09/11/09 17:57 78-93-34670 n-Butylbenzene 1990 ug/kg 50 09/11/09 17:57 104-51-8233 sec-Butylbenzene 399 ug/kg 50 09/11/09 17:57 135-98-8233 tert-Butylbenzene ND ug/kg 50 09/11/09 17:57 98-06-6233 Carbon tetrachloride ND ug/kg 50 09/11/09 17:57 56-23-5233 Chlorobenzene ND ug/kg 50 09/11/09 17:57 108-90-7233 Chloroethane ND ug/kg 50 09/11/09 17:57 75-00-3467 Chloroform ND ug/kg 50 09/11/09 17:57 67-66-3233 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 44 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB2-09-09 Lab ID:9252614013 Collected:09/08/09 12:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 50 09/11/09 17:57 74-87-3467 2-Chlorotoluene ND ug/kg 50 09/11/09 17:57 95-49-8233 4-Chlorotoluene ND ug/kg 50 09/11/09 17:57 106-43-4233 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/11/09 17:57 96-12-8233 Dibromochloromethane ND ug/kg 50 09/11/09 17:57 124-48-1233 1,2-Dibromoethane (EDB)ND ug/kg 50 09/11/09 17:57 106-93-4233 Dibromomethane ND ug/kg 50 09/11/09 17:57 74-95-3233 1,2-Dichlorobenzene ND ug/kg 50 09/11/09 17:57 95-50-1233 1,3-Dichlorobenzene ND ug/kg 50 09/11/09 17:57 541-73-1233 1,4-Dichlorobenzene ND ug/kg 50 09/11/09 17:57 106-46-7233 Dichlorodifluoromethane ND ug/kg 50 09/11/09 17:57 75-71-8467 1,1-Dichloroethane ND ug/kg 50 09/11/09 17:57 75-34-3233 1,2-Dichloroethane ND ug/kg 50 09/11/09 17:57 107-06-2233 1,1-Dichloroethene ND ug/kg 50 09/11/09 17:57 75-35-4233 cis-1,2-Dichloroethene ND ug/kg 50 09/11/09 17:57 156-59-2233 trans-1,2-Dichloroethene ND ug/kg 50 09/11/09 17:57 156-60-5233 1,2-Dichloropropane ND ug/kg 50 09/11/09 17:57 78-87-5233 1,3-Dichloropropane ND ug/kg 50 09/11/09 17:57 142-28-9233 2,2-Dichloropropane ND ug/kg 50 09/11/09 17:57 594-20-7233 1,1-Dichloropropene ND ug/kg 50 09/11/09 17:57 563-58-6233 cis-1,3-Dichloropropene ND ug/kg 50 09/11/09 17:57 10061-01-5233 trans-1,3-Dichloropropene ND ug/kg 50 09/11/09 17:57 10061-02-6233 Diisopropyl ether ND ug/kg 50 09/11/09 17:57 108-20-3233 Ethylbenzene 3580 ug/kg 50 09/11/09 17:57 100-41-4233 Hexachloro-1,3-butadiene ND ug/kg 50 09/11/09 17:57 87-68-3233 2-Hexanone ND ug/kg 50 09/11/09 17:57 591-78-62330 Isopropylbenzene (Cumene)700 ug/kg 50 09/11/09 17:57 98-82-8233 p-Isopropyltoluene 962 ug/kg 50 09/11/09 17:57 99-87-6233 Methylene Chloride ND ug/kg 50 09/11/09 17:57 75-09-2934 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/11/09 17:57 108-10-12330 Methyl-tert-butyl ether ND ug/kg 50 09/11/09 17:57 1634-04-4233 Naphthalene 2350 ug/kg 50 09/11/09 17:57 91-20-3233 n-Propylbenzene 2780 ug/kg 50 09/11/09 17:57 103-65-1233 Styrene ND ug/kg 50 09/11/09 17:57 100-42-5233 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/11/09 17:57 630-20-6233 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/11/09 17:57 79-34-5233 Tetrachloroethene ND ug/kg 50 09/11/09 17:57 127-18-4233 Toluene 270 ug/kg 50 09/11/09 17:57 108-88-3233 1,2,3-Trichlorobenzene ND ug/kg 50 09/11/09 17:57 87-61-6233 1,2,4-Trichlorobenzene ND ug/kg 50 09/11/09 17:57 120-82-1233 1,1,1-Trichloroethane ND ug/kg 50 09/11/09 17:57 71-55-6233 1,1,2-Trichloroethane ND ug/kg 50 09/11/09 17:57 79-00-5233 Trichloroethene ND ug/kg 50 09/11/09 17:57 79-01-6233 Trichlorofluoromethane ND ug/kg 50 09/11/09 17:57 75-69-4233 1,2,3-Trichloropropane ND ug/kg 50 09/11/09 17:57 96-18-4233 1,2,4-Trimethylbenzene 20900 ug/kg 250 09/14/09 15:08 95-63-61170 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 45 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -SB2-09-09 Lab ID:9252614013 Collected:09/08/09 12:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene 5470 ug/kg 50 09/11/09 17:57 108-67-8233 Vinyl acetate ND ug/kg 50 09/11/09 17:57 108-05-42330 Vinyl chloride ND ug/kg 50 09/11/09 17:57 75-01-4467 Xylene (Total)8700 ug/kg 50 09/11/09 17:57 1330-20-7467 m&p-Xylene 8470 ug/kg 50 09/11/09 17:57 1330-20-7467 o-Xylene 238 ug/kg 50 09/11/09 17:57 95-47-6233 Dibromofluoromethane (S)97 %50 09/11/09 17:57 1868-53-779-116 Toluene-d8 (S)99 %50 09/11/09 17:57 2037-26-588-110 4-Bromofluorobenzene (S)97 %50 09/11/09 17:57 460-00-474-115 1,2-Dichloroethane-d4 (S)96 %50 09/11/09 17:57 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 12.1 %1 09/09/09 13:440.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 46 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS1-09-09 Lab ID:9252614015 Collected:09/08/09 12:40 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/23/09 03:20 83-32-909/09/09 00:00369 Acenaphthylene ND ug/kg 1 09/23/09 03:20 208-96-809/09/09 00:00369 Aniline ND ug/kg 1 09/23/09 03:20 62-53-309/09/09 00:00369 Anthracene ND ug/kg 1 09/23/09 03:20 120-12-709/09/09 00:00369 Benzo(a)anthracene ND ug/kg 1 09/23/09 03:20 56-55-309/09/09 00:00369 Benzo(a)pyrene ND ug/kg 1 09/23/09 03:20 50-32-809/09/09 00:00369 Benzo(b)fluoranthene ND ug/kg 1 09/23/09 03:20 205-99-209/09/09 00:00369 Benzo(g,h,i)perylene ND ug/kg 1 09/23/09 03:20 191-24-209/09/09 00:00369 Benzo(k)fluoranthene ND ug/kg 1 09/23/09 03:20 207-08-909/09/09 00:00369 Benzoic Acid ND ug/kg 1 09/23/09 03:20 65-85-009/09/09 00:001850 Benzyl alcohol ND ug/kg 1 09/23/09 03:20 100-51-609/09/09 00:00739 4-Bromophenylphenyl ether ND ug/kg 1 09/23/09 03:20 101-55-309/09/09 00:00369 Butylbenzylphthalate ND ug/kg 1 09/23/09 03:20 85-68-709/09/09 00:00369 4-Chloro-3-methylphenol ND ug/kg 1 09/23/09 03:20 59-50-709/09/09 00:00739 4-Chloroaniline ND ug/kg 1 09/23/09 03:20 106-47-809/09/09 00:001850 bis(2-Chloroethoxy)methane ND ug/kg 1 09/23/09 03:20 111-91-109/09/09 00:00369 bis(2-Chloroethyl) ether ND ug/kg 1 09/23/09 03:20 111-44-409/09/09 00:00369 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/23/09 03:20 108-60-109/09/09 00:00369 2-Chloronaphthalene ND ug/kg 1 09/23/09 03:20 91-58-709/09/09 00:00369 2-Chlorophenol ND ug/kg 1 09/23/09 03:20 95-57-809/09/09 00:00369 4-Chlorophenylphenyl ether ND ug/kg 1 09/23/09 03:20 7005-72-309/09/09 00:00369 Chrysene ND ug/kg 1 09/23/09 03:20 218-01-909/09/09 00:00369 Dibenz(a,h)anthracene ND ug/kg 1 09/23/09 03:20 53-70-309/09/09 00:00369 Dibenzofuran 699 ug/kg 1 09/23/09 03:20 132-64-909/09/09 00:00369 1,2-Dichlorobenzene ND ug/kg 1 09/23/09 03:20 95-50-109/09/09 00:00369 1,3-Dichlorobenzene ND ug/kg 1 09/23/09 03:20 541-73-109/09/09 00:00369 1,4-Dichlorobenzene ND ug/kg 1 09/23/09 03:20 106-46-709/09/09 00:00369 3,3'-Dichlorobenzidine ND ug/kg 1 09/23/09 03:20 91-94-109/09/09 00:001850 2,4-Dichlorophenol ND ug/kg 1 09/23/09 03:20 120-83-209/09/09 00:00369 Diethylphthalate ND ug/kg 1 09/23/09 03:20 84-66-209/09/09 00:00369 2,4-Dimethylphenol ND ug/kg 1 09/23/09 03:20 105-67-909/09/09 00:00369 Dimethylphthalate ND ug/kg 1 09/23/09 03:20 131-11-309/09/09 00:00369 Di-n-butylphthalate ND ug/kg 1 09/23/09 03:20 84-74-209/09/09 00:00369 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/23/09 03:20 534-52-109/09/09 00:00739 2,4-Dinitrophenol ND ug/kg 1 09/23/09 03:20 51-28-509/09/09 00:001850 2,4-Dinitrotoluene ND ug/kg 1 09/23/09 03:20 121-14-209/09/09 00:00369 2,6-Dinitrotoluene ND ug/kg 1 09/23/09 03:20 606-20-209/09/09 00:00369 Di-n-octylphthalate ND ug/kg 1 09/23/09 03:20 117-84-009/09/09 00:00369 1,2-Diphenylhydrazine ND ug/kg 1 09/23/09 03:20 122-66-709/09/09 00:00369 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/23/09 03:20 117-81-709/09/09 00:00369 Fluoranthene ND ug/kg 1 09/23/09 03:20 206-44-009/09/09 00:00369 Fluorene ND ug/kg 1 09/23/09 03:20 86-73-709/09/09 00:00369 Hexachloro-1,3-butadiene ND ug/kg 1 09/23/09 03:20 87-68-309/09/09 00:00369 Hexachlorobenzene ND ug/kg 1 09/23/09 03:20 118-74-109/09/09 00:00369 Hexachlorocyclopentadiene ND ug/kg 1 09/23/09 03:20 77-47-409/09/09 00:00369 Hexachloroethane ND ug/kg 1 09/23/09 03:20 67-72-109/09/09 00:00369 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 47 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS1-09-09 Lab ID:9252614015 Collected:09/08/09 12:40 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/09 03:20 193-39-509/09/09 00:00369 Isophorone ND ug/kg 1 09/23/09 03:20 78-59-109/09/09 00:00369 1-Methylnaphthalene 2200 ug/kg 1 09/23/09 03:20 90-12-009/09/09 00:00369 2-Methylnaphthalene 3060 ug/kg 1 09/23/09 03:20 91-57-609/09/09 00:00369 2-Methylphenol(o-Cresol)ND ug/kg 1 09/23/09 03:20 95-48-709/09/09 00:00369 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/23/09 03:2009/09/09 00:00369 Naphthalene 2140 ug/kg 1 09/23/09 03:20 91-20-309/09/09 00:00369 2-Nitroaniline ND ug/kg 1 09/23/09 03:20 88-74-409/09/09 00:001850 3-Nitroaniline ND ug/kg 1 09/23/09 03:20 99-09-209/09/09 00:001850 4-Nitroaniline ND ug/kg 1 09/23/09 03:20 100-01-609/09/09 00:00739 Nitrobenzene ND ug/kg 1 09/23/09 03:20 98-95-309/09/09 00:00369 2-Nitrophenol ND ug/kg 1 09/23/09 03:20 88-75-509/09/09 00:00369 4-Nitrophenol ND ug/kg 1 09/23/09 03:20 100-02-709/09/09 00:001850 N-Nitrosodimethylamine ND ug/kg 1 09/23/09 03:20 62-75-909/09/09 00:00369 N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/09 03:20 621-64-709/09/09 00:00369 N-Nitrosodiphenylamine ND ug/kg 1 09/23/09 03:20 86-30-609/09/09 00:00369 Pentachlorophenol ND ug/kg 1 09/23/09 03:20 87-86-509/09/09 00:001850 Phenanthrene 1140 ug/kg 1 09/23/09 03:20 85-01-809/09/09 00:00369 Phenol ND ug/kg 1 09/23/09 03:20 108-95-209/09/09 00:00369 Pyrene 640 ug/kg 1 09/23/09 03:20 129-00-009/09/09 00:00369 1,2,4-Trichlorobenzene ND ug/kg 1 09/23/09 03:20 120-82-109/09/09 00:00369 2,4,5-Trichlorophenol ND ug/kg 1 09/23/09 03:20 95-95-409/09/09 00:00369 2,4,6-Trichlorophenol ND ug/kg 1 09/23/09 03:20 88-06-209/09/09 00:00369 Nitrobenzene-d5 (S)34 %1 09/23/09 03:20 4165-60-009/09/09 00:0030-150 2-Fluorobiphenyl (S)48 %1 09/23/09 03:20 321-60-809/09/09 00:0046-120 Terphenyl-d14 (S)86 %1 09/23/09 03:20 1718-51-009/09/09 00:0038-108 Phenol-d6 (S)39 %1 09/23/09 03:20 13127-88-309/09/09 00:0035-120 2-Fluorophenol (S)28 %1 09/23/09 03:20 367-12-409/09/09 00:0024-120 2,4,6-Tribromophenol (S)46 %1 09/23/09 03:20 118-79-609/09/09 00:0044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 1 09/11/09 15:12 67-64-179.5 Benzene ND ug/kg 1 09/11/09 15:12 71-43-24.0 Bromobenzene ND ug/kg 1 09/11/09 15:12 108-86-14.0 Bromochloromethane ND ug/kg 1 09/11/09 15:12 74-97-54.0 Bromodichloromethane ND ug/kg 1 09/11/09 15:12 75-27-44.0 Bromoform ND ug/kg 1 09/11/09 15:12 75-25-24.0 Bromomethane ND ug/kg 1 09/11/09 15:12 74-83-98.0 2-Butanone (MEK)ND ug/kg 1 09/11/09 15:12 78-93-379.5 n-Butylbenzene ND ug/kg 1 09/11/09 15:12 104-51-84.0 sec-Butylbenzene ND ug/kg 1 09/11/09 15:12 135-98-84.0 tert-Butylbenzene ND ug/kg 1 09/11/09 15:12 98-06-64.0 Carbon tetrachloride ND ug/kg 1 09/11/09 15:12 56-23-54.0 Chlorobenzene ND ug/kg 1 09/11/09 15:12 108-90-74.0 Chloroethane ND ug/kg 1 09/11/09 15:12 75-00-38.0 Chloroform ND ug/kg 1 09/11/09 15:12 67-66-34.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 48 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS1-09-09 Lab ID:9252614015 Collected:09/08/09 12:40 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 1 09/11/09 15:12 74-87-38.0 2-Chlorotoluene ND ug/kg 1 09/11/09 15:12 95-49-84.0 4-Chlorotoluene ND ug/kg 1 09/11/09 15:12 106-43-44.0 1,2-Dibromo-3-chloropropane ND ug/kg 1 09/11/09 15:12 96-12-84.0 Dibromochloromethane ND ug/kg 1 09/11/09 15:12 124-48-14.0 1,2-Dibromoethane (EDB)ND ug/kg 1 09/11/09 15:12 106-93-44.0 Dibromomethane ND ug/kg 1 09/11/09 15:12 74-95-34.0 1,2-Dichlorobenzene ND ug/kg 1 09/11/09 15:12 95-50-14.0 1,3-Dichlorobenzene ND ug/kg 1 09/11/09 15:12 541-73-14.0 1,4-Dichlorobenzene ND ug/kg 1 09/11/09 15:12 106-46-74.0 Dichlorodifluoromethane ND ug/kg 1 09/11/09 15:12 75-71-88.0 1,1-Dichloroethane ND ug/kg 1 09/11/09 15:12 75-34-34.0 1,2-Dichloroethane ND ug/kg 1 09/11/09 15:12 107-06-24.0 1,1-Dichloroethene ND ug/kg 1 09/11/09 15:12 75-35-44.0 cis-1,2-Dichloroethene ND ug/kg 1 09/11/09 15:12 156-59-24.0 trans-1,2-Dichloroethene ND ug/kg 1 09/11/09 15:12 156-60-54.0 1,2-Dichloropropane ND ug/kg 1 09/11/09 15:12 78-87-54.0 1,3-Dichloropropane ND ug/kg 1 09/11/09 15:12 142-28-94.0 2,2-Dichloropropane ND ug/kg 1 09/11/09 15:12 594-20-74.0 1,1-Dichloropropene ND ug/kg 1 09/11/09 15:12 563-58-64.0 cis-1,3-Dichloropropene ND ug/kg 1 09/11/09 15:12 10061-01-54.0 trans-1,3-Dichloropropene ND ug/kg 1 09/11/09 15:12 10061-02-64.0 Diisopropyl ether 4.5 ug/kg 1 09/11/09 15:12 108-20-34.0 Ethylbenzene ND ug/kg 1 09/11/09 15:12 100-41-44.0 Hexachloro-1,3-butadiene ND ug/kg 1 09/11/09 15:12 87-68-34.0 2-Hexanone ND ug/kg 1 09/11/09 15:12 591-78-639.8 Isopropylbenzene (Cumene)ND ug/kg 1 09/11/09 15:12 98-82-84.0 p-Isopropyltoluene ND ug/kg 1 09/11/09 15:12 99-87-64.0 Methylene Chloride ND ug/kg 1 09/11/09 15:12 75-09-215.9 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 09/11/09 15:12 108-10-139.8 Methyl-tert-butyl ether 10.6 ug/kg 1 09/11/09 15:12 1634-04-44.0 Naphthalene ND ug/kg 1 09/11/09 15:12 91-20-34.0 n-Propylbenzene ND ug/kg 1 09/11/09 15:12 103-65-14.0 Styrene ND ug/kg 1 09/11/09 15:12 100-42-54.0 1,1,1,2-Tetrachloroethane ND ug/kg 1 09/11/09 15:12 630-20-64.0 1,1,2,2-Tetrachloroethane ND ug/kg 1 09/11/09 15:12 79-34-54.0 Tetrachloroethene ND ug/kg 1 09/11/09 15:12 127-18-44.0 Toluene ND ug/kg 1 09/11/09 15:12 108-88-34.0 1,2,3-Trichlorobenzene ND ug/kg 1 09/11/09 15:12 87-61-64.0 1,2,4-Trichlorobenzene ND ug/kg 1 09/11/09 15:12 120-82-14.0 1,1,1-Trichloroethane ND ug/kg 1 09/11/09 15:12 71-55-64.0 1,1,2-Trichloroethane ND ug/kg 1 09/11/09 15:12 79-00-54.0 Trichloroethene ND ug/kg 1 09/11/09 15:12 79-01-64.0 Trichlorofluoromethane ND ug/kg 1 09/11/09 15:12 75-69-44.0 1,2,3-Trichloropropane ND ug/kg 1 09/11/09 15:12 96-18-44.0 1,2,4-Trimethylbenzene ND ug/kg 1 09/11/09 15:12 95-63-64.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 49 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS1-09-09 Lab ID:9252614015 Collected:09/08/09 12:40 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene ND ug/kg 1 09/11/09 15:12 108-67-84.0 Vinyl acetate ND ug/kg 1 09/11/09 15:12 108-05-439.8 Vinyl chloride ND ug/kg 1 09/11/09 15:12 75-01-48.0 Xylene (Total)ND ug/kg 1 09/11/09 15:12 1330-20-78.0 m&p-Xylene ND ug/kg 1 09/11/09 15:12 1330-20-78.0 o-Xylene ND ug/kg 1 09/11/09 15:12 95-47-64.0 Dibromofluoromethane (S)100 %1 09/11/09 15:12 1868-53-779-116 Toluene-d8 (S)100 %1 09/11/09 15:12 2037-26-588-110 4-Bromofluorobenzene (S)99 %1 09/11/09 15:12 460-00-474-115 1,2-Dichloroethane-d4 (S)99 %1 09/11/09 15:12 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 10.7 %1 09/09/09 13:450.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 50 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS2-09-09 Lab ID:9252614016 Collected:09/08/09 12:45 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/19/09 02:22 83-32-909/10/09 14:30388 Acenaphthylene ND ug/kg 1 09/19/09 02:22 208-96-809/10/09 14:30388 Aniline ND ug/kg 1 09/19/09 02:22 62-53-309/10/09 14:30388 Anthracene ND ug/kg 1 09/19/09 02:22 120-12-709/10/09 14:30388 Benzo(a)anthracene ND ug/kg 1 09/19/09 02:22 56-55-309/10/09 14:30388 Benzo(a)pyrene ND ug/kg 1 09/19/09 02:22 50-32-809/10/09 14:30388 Benzo(b)fluoranthene ND ug/kg 1 09/19/09 02:22 205-99-209/10/09 14:30388 Benzo(g,h,i)perylene ND ug/kg 1 09/19/09 02:22 191-24-209/10/09 14:30388 Benzo(k)fluoranthene ND ug/kg 1 09/19/09 02:22 207-08-909/10/09 14:30388 Benzoic Acid ND ug/kg 1 09/19/09 02:22 65-85-009/10/09 14:301940 Benzyl alcohol ND ug/kg 1 09/19/09 02:22 100-51-609/10/09 14:30776 4-Bromophenylphenyl ether ND ug/kg 1 09/19/09 02:22 101-55-309/10/09 14:30388 Butylbenzylphthalate ND ug/kg 1 09/19/09 02:22 85-68-709/10/09 14:30388 4-Chloro-3-methylphenol ND ug/kg 1 09/19/09 02:22 59-50-709/10/09 14:30776 4-Chloroaniline ND ug/kg 1 09/19/09 02:22 106-47-809/10/09 14:301940 bis(2-Chloroethoxy)methane ND ug/kg 1 09/19/09 02:22 111-91-109/10/09 14:30388 bis(2-Chloroethyl) ether ND ug/kg 1 09/19/09 02:22 111-44-409/10/09 14:30388 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/19/09 02:22 108-60-109/10/09 14:30388 2-Chloronaphthalene ND ug/kg 1 09/19/09 02:22 91-58-709/10/09 14:30388 2-Chlorophenol ND ug/kg 1 09/19/09 02:22 95-57-809/10/09 14:30388 4-Chlorophenylphenyl ether ND ug/kg 1 09/19/09 02:22 7005-72-309/10/09 14:30388 Chrysene ND ug/kg 1 09/19/09 02:22 218-01-909/10/09 14:30388 Dibenz(a,h)anthracene ND ug/kg 1 09/19/09 02:22 53-70-309/10/09 14:30388 Dibenzofuran ND ug/kg 1 09/19/09 02:22 132-64-909/10/09 14:30388 1,2-Dichlorobenzene ND ug/kg 1 09/19/09 02:22 95-50-109/10/09 14:30388 1,3-Dichlorobenzene ND ug/kg 1 09/19/09 02:22 541-73-109/10/09 14:30388 1,4-Dichlorobenzene ND ug/kg 1 09/19/09 02:22 106-46-709/10/09 14:30388 3,3'-Dichlorobenzidine ND ug/kg 1 09/19/09 02:22 91-94-109/10/09 14:301940 2,4-Dichlorophenol ND ug/kg 1 09/19/09 02:22 120-83-209/10/09 14:30388 Diethylphthalate ND ug/kg 1 09/19/09 02:22 84-66-209/10/09 14:30388 2,4-Dimethylphenol ND ug/kg 1 09/19/09 02:22 105-67-909/10/09 14:30388 Dimethylphthalate ND ug/kg 1 09/19/09 02:22 131-11-309/10/09 14:30388 Di-n-butylphthalate ND ug/kg 1 09/19/09 02:22 84-74-209/10/09 14:30388 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/09 02:22 534-52-109/10/09 14:30776 2,4-Dinitrophenol ND ug/kg 1 09/19/09 02:22 51-28-509/10/09 14:301940 2,4-Dinitrotoluene ND ug/kg 1 09/19/09 02:22 121-14-209/10/09 14:30388 2,6-Dinitrotoluene ND ug/kg 1 09/19/09 02:22 606-20-209/10/09 14:30388 Di-n-octylphthalate ND ug/kg 1 09/19/09 02:22 117-84-009/10/09 14:30388 1,2-Diphenylhydrazine ND ug/kg 1 09/19/09 02:22 122-66-709/10/09 14:30388 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/09 02:22 117-81-709/10/09 14:30388 Fluoranthene ND ug/kg 1 09/19/09 02:22 206-44-009/10/09 14:30388 Fluorene ND ug/kg 1 09/19/09 02:22 86-73-709/10/09 14:30388 Hexachloro-1,3-butadiene ND ug/kg 1 09/19/09 02:22 87-68-309/10/09 14:30388 Hexachlorobenzene ND ug/kg 1 09/19/09 02:22 118-74-109/10/09 14:30388 Hexachlorocyclopentadiene ND ug/kg 1 09/19/09 02:22 77-47-409/10/09 14:30388 Hexachloroethane ND ug/kg 1 09/19/09 02:22 67-72-109/10/09 14:30388 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 51 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS2-09-09 Lab ID:9252614016 Collected:09/08/09 12:45 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/09 02:22 193-39-509/10/09 14:30388 Isophorone ND ug/kg 1 09/19/09 02:22 78-59-109/10/09 14:30388 1-Methylnaphthalene ND ug/kg 1 09/19/09 02:22 90-12-009/10/09 14:30388 2-Methylnaphthalene ND ug/kg 1 09/19/09 02:22 91-57-609/10/09 14:30388 2-Methylphenol(o-Cresol)ND ug/kg 1 09/19/09 02:22 95-48-709/10/09 14:30388 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/19/09 02:2209/10/09 14:30388 Naphthalene ND ug/kg 1 09/19/09 02:22 91-20-309/10/09 14:30388 2-Nitroaniline ND ug/kg 1 09/19/09 02:22 88-74-409/10/09 14:301940 3-Nitroaniline ND ug/kg 1 09/19/09 02:22 99-09-209/10/09 14:301940 4-Nitroaniline ND ug/kg 1 09/19/09 02:22 100-01-609/10/09 14:30776 Nitrobenzene ND ug/kg 1 09/19/09 02:22 98-95-309/10/09 14:30388 2-Nitrophenol ND ug/kg 1 09/19/09 02:22 88-75-509/10/09 14:30388 4-Nitrophenol ND ug/kg 1 09/19/09 02:22 100-02-709/10/09 14:301940 N-Nitrosodimethylamine ND ug/kg 1 09/19/09 02:22 62-75-909/10/09 14:30388 N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/09 02:22 621-64-709/10/09 14:30388 N-Nitrosodiphenylamine ND ug/kg 1 09/19/09 02:22 86-30-609/10/09 14:30388 Pentachlorophenol ND ug/kg 1 09/19/09 02:22 87-86-509/10/09 14:301940 Phenanthrene ND ug/kg 1 09/19/09 02:22 85-01-809/10/09 14:30388 Phenol ND ug/kg 1 09/19/09 02:22 108-95-209/10/09 14:30388 Pyrene ND ug/kg 1 09/19/09 02:22 129-00-009/10/09 14:30388 1,2,4-Trichlorobenzene ND ug/kg 1 09/19/09 02:22 120-82-109/10/09 14:30388 2,4,5-Trichlorophenol ND ug/kg 1 09/19/09 02:22 95-95-409/10/09 14:30388 2,4,6-Trichlorophenol ND ug/kg 1 09/19/09 02:22 88-06-209/10/09 14:30388 Nitrobenzene-d5 (S)47 %1 09/19/09 02:22 4165-60-009/10/09 14:3030-150 2-Fluorobiphenyl (S)46 %1 09/19/09 02:22 321-60-809/10/09 14:3046-120 Terphenyl-d14 (S)57 %1 09/19/09 02:22 1718-51-009/10/09 14:3038-108 Phenol-d6 (S)32 %1 09/19/09 02:22 13127-88-3 1g09/10/09 14:3035-120 2-Fluorophenol (S)33 %1 09/19/09 02:22 367-12-409/10/09 14:3024-120 2,4,6-Tribromophenol (S)54 %1 09/19/09 02:22 118-79-609/10/09 14:3044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/11/09 19:10 67-64-14030 Benzene ND ug/kg 50 09/11/09 19:10 71-43-2202 Bromobenzene ND ug/kg 50 09/11/09 19:10 108-86-1202 Bromochloromethane ND ug/kg 50 09/11/09 19:10 74-97-5202 Bromodichloromethane ND ug/kg 50 09/11/09 19:10 75-27-4202 Bromoform ND ug/kg 50 09/11/09 19:10 75-25-2202 Bromomethane ND ug/kg 50 09/11/09 19:10 74-83-9403 2-Butanone (MEK)ND ug/kg 50 09/11/09 19:10 78-93-34030 n-Butylbenzene ND ug/kg 50 09/11/09 19:10 104-51-8202 sec-Butylbenzene ND ug/kg 50 09/11/09 19:10 135-98-8202 tert-Butylbenzene ND ug/kg 50 09/11/09 19:10 98-06-6202 Carbon tetrachloride ND ug/kg 50 09/11/09 19:10 56-23-5202 Chlorobenzene ND ug/kg 50 09/11/09 19:10 108-90-7202 Chloroethane ND ug/kg 50 09/11/09 19:10 75-00-3403 Chloroform ND ug/kg 50 09/11/09 19:10 67-66-3202 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 52 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS2-09-09 Lab ID:9252614016 Collected:09/08/09 12:45 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 50 09/11/09 19:10 74-87-3403 2-Chlorotoluene ND ug/kg 50 09/11/09 19:10 95-49-8202 4-Chlorotoluene ND ug/kg 50 09/11/09 19:10 106-43-4202 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/11/09 19:10 96-12-8202 Dibromochloromethane ND ug/kg 50 09/11/09 19:10 124-48-1202 1,2-Dibromoethane (EDB)ND ug/kg 50 09/11/09 19:10 106-93-4202 Dibromomethane ND ug/kg 50 09/11/09 19:10 74-95-3202 1,2-Dichlorobenzene ND ug/kg 50 09/11/09 19:10 95-50-1202 1,3-Dichlorobenzene ND ug/kg 50 09/11/09 19:10 541-73-1202 1,4-Dichlorobenzene ND ug/kg 50 09/11/09 19:10 106-46-7202 Dichlorodifluoromethane ND ug/kg 50 09/11/09 19:10 75-71-8403 1,1-Dichloroethane ND ug/kg 50 09/11/09 19:10 75-34-3202 1,2-Dichloroethane ND ug/kg 50 09/11/09 19:10 107-06-2202 1,1-Dichloroethene ND ug/kg 50 09/11/09 19:10 75-35-4202 cis-1,2-Dichloroethene ND ug/kg 50 09/11/09 19:10 156-59-2202 trans-1,2-Dichloroethene ND ug/kg 50 09/11/09 19:10 156-60-5202 1,2-Dichloropropane ND ug/kg 50 09/11/09 19:10 78-87-5202 1,3-Dichloropropane ND ug/kg 50 09/11/09 19:10 142-28-9202 2,2-Dichloropropane ND ug/kg 50 09/11/09 19:10 594-20-7202 1,1-Dichloropropene ND ug/kg 50 09/11/09 19:10 563-58-6202 cis-1,3-Dichloropropene ND ug/kg 50 09/11/09 19:10 10061-01-5202 trans-1,3-Dichloropropene ND ug/kg 50 09/11/09 19:10 10061-02-6202 Diisopropyl ether ND ug/kg 50 09/11/09 19:10 108-20-3202 Ethylbenzene ND ug/kg 50 09/11/09 19:10 100-41-4202 Hexachloro-1,3-butadiene ND ug/kg 50 09/11/09 19:10 87-68-3202 2-Hexanone ND ug/kg 50 09/11/09 19:10 591-78-62020 Isopropylbenzene (Cumene)ND ug/kg 50 09/11/09 19:10 98-82-8202 p-Isopropyltoluene ND ug/kg 50 09/11/09 19:10 99-87-6202 Methylene Chloride ND ug/kg 50 09/11/09 19:10 75-09-2806 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/11/09 19:10 108-10-12020 Methyl-tert-butyl ether ND ug/kg 50 09/11/09 19:10 1634-04-4202 Naphthalene ND ug/kg 50 09/11/09 19:10 91-20-3202 n-Propylbenzene ND ug/kg 50 09/11/09 19:10 103-65-1202 Styrene ND ug/kg 50 09/11/09 19:10 100-42-5202 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/11/09 19:10 630-20-6202 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/11/09 19:10 79-34-5202 Tetrachloroethene ND ug/kg 50 09/11/09 19:10 127-18-4202 Toluene ND ug/kg 50 09/11/09 19:10 108-88-3202 1,2,3-Trichlorobenzene ND ug/kg 50 09/11/09 19:10 87-61-6202 1,2,4-Trichlorobenzene ND ug/kg 50 09/11/09 19:10 120-82-1202 1,1,1-Trichloroethane ND ug/kg 50 09/11/09 19:10 71-55-6202 1,1,2-Trichloroethane ND ug/kg 50 09/11/09 19:10 79-00-5202 Trichloroethene ND ug/kg 50 09/11/09 19:10 79-01-6202 Trichlorofluoromethane ND ug/kg 50 09/11/09 19:10 75-69-4202 1,2,3-Trichloropropane ND ug/kg 50 09/11/09 19:10 96-18-4202 1,2,4-Trimethylbenzene ND ug/kg 50 09/11/09 19:10 95-63-6202 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 53 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW3-SS2-09-09 Lab ID:9252614016 Collected:09/08/09 12:45 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene ND ug/kg 50 09/11/09 19:10 108-67-8202 Vinyl acetate ND ug/kg 50 09/11/09 19:10 108-05-42020 Vinyl chloride ND ug/kg 50 09/11/09 19:10 75-01-4403 Xylene (Total)ND ug/kg 50 09/11/09 19:10 1330-20-7403 m&p-Xylene ND ug/kg 50 09/11/09 19:10 1330-20-7403 o-Xylene ND ug/kg 50 09/11/09 19:10 95-47-6202 Dibromofluoromethane (S)99 %50 09/11/09 19:10 1868-53-7 D379-116 Toluene-d8 (S)100 %50 09/11/09 19:10 2037-26-588-110 4-Bromofluorobenzene (S)101 %50 09/11/09 19:10 460-00-474-115 1,2-Dichloroethane-d4 (S)97 %50 09/11/09 19:10 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 14.9 %1 09/09/09 13:450.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 54 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP2-09-09 Lab ID:9252614017 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/19/09 02:45 83-32-909/10/09 14:30400 Acenaphthylene ND ug/kg 1 09/19/09 02:45 208-96-809/10/09 14:30400 Aniline ND ug/kg 1 09/19/09 02:45 62-53-309/10/09 14:30400 Anthracene ND ug/kg 1 09/19/09 02:45 120-12-709/10/09 14:30400 Benzo(a)anthracene ND ug/kg 1 09/19/09 02:45 56-55-309/10/09 14:30400 Benzo(a)pyrene ND ug/kg 1 09/19/09 02:45 50-32-809/10/09 14:30400 Benzo(b)fluoranthene ND ug/kg 1 09/19/09 02:45 205-99-209/10/09 14:30400 Benzo(g,h,i)perylene ND ug/kg 1 09/19/09 02:45 191-24-209/10/09 14:30400 Benzo(k)fluoranthene ND ug/kg 1 09/19/09 02:45 207-08-909/10/09 14:30400 Benzoic Acid ND ug/kg 1 09/19/09 02:45 65-85-009/10/09 14:302000 Benzyl alcohol ND ug/kg 1 09/19/09 02:45 100-51-609/10/09 14:30799 4-Bromophenylphenyl ether ND ug/kg 1 09/19/09 02:45 101-55-309/10/09 14:30400 Butylbenzylphthalate ND ug/kg 1 09/19/09 02:45 85-68-709/10/09 14:30400 4-Chloro-3-methylphenol ND ug/kg 1 09/19/09 02:45 59-50-709/10/09 14:30799 4-Chloroaniline ND ug/kg 1 09/19/09 02:45 106-47-809/10/09 14:302000 bis(2-Chloroethoxy)methane ND ug/kg 1 09/19/09 02:45 111-91-109/10/09 14:30400 bis(2-Chloroethyl) ether ND ug/kg 1 09/19/09 02:45 111-44-409/10/09 14:30400 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/19/09 02:45 108-60-109/10/09 14:30400 2-Chloronaphthalene ND ug/kg 1 09/19/09 02:45 91-58-709/10/09 14:30400 2-Chlorophenol ND ug/kg 1 09/19/09 02:45 95-57-809/10/09 14:30400 4-Chlorophenylphenyl ether ND ug/kg 1 09/19/09 02:45 7005-72-309/10/09 14:30400 Chrysene ND ug/kg 1 09/19/09 02:45 218-01-909/10/09 14:30400 Dibenz(a,h)anthracene ND ug/kg 1 09/19/09 02:45 53-70-309/10/09 14:30400 Dibenzofuran ND ug/kg 1 09/19/09 02:45 132-64-909/10/09 14:30400 1,2-Dichlorobenzene ND ug/kg 1 09/19/09 02:45 95-50-109/10/09 14:30400 1,3-Dichlorobenzene ND ug/kg 1 09/19/09 02:45 541-73-109/10/09 14:30400 1,4-Dichlorobenzene ND ug/kg 1 09/19/09 02:45 106-46-709/10/09 14:30400 3,3'-Dichlorobenzidine ND ug/kg 1 09/19/09 02:45 91-94-109/10/09 14:302000 2,4-Dichlorophenol ND ug/kg 1 09/19/09 02:45 120-83-209/10/09 14:30400 Diethylphthalate ND ug/kg 1 09/19/09 02:45 84-66-209/10/09 14:30400 2,4-Dimethylphenol ND ug/kg 1 09/19/09 02:45 105-67-909/10/09 14:30400 Dimethylphthalate ND ug/kg 1 09/19/09 02:45 131-11-309/10/09 14:30400 Di-n-butylphthalate ND ug/kg 1 09/19/09 02:45 84-74-209/10/09 14:30400 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/09 02:45 534-52-109/10/09 14:30799 2,4-Dinitrophenol ND ug/kg 1 09/19/09 02:45 51-28-509/10/09 14:302000 2,4-Dinitrotoluene ND ug/kg 1 09/19/09 02:45 121-14-209/10/09 14:30400 2,6-Dinitrotoluene ND ug/kg 1 09/19/09 02:45 606-20-209/10/09 14:30400 Di-n-octylphthalate ND ug/kg 1 09/19/09 02:45 117-84-009/10/09 14:30400 1,2-Diphenylhydrazine ND ug/kg 1 09/19/09 02:45 122-66-709/10/09 14:30400 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/09 02:45 117-81-709/10/09 14:30400 Fluoranthene ND ug/kg 1 09/19/09 02:45 206-44-009/10/09 14:30400 Fluorene ND ug/kg 1 09/19/09 02:45 86-73-709/10/09 14:30400 Hexachloro-1,3-butadiene ND ug/kg 1 09/19/09 02:45 87-68-309/10/09 14:30400 Hexachlorobenzene ND ug/kg 1 09/19/09 02:45 118-74-109/10/09 14:30400 Hexachlorocyclopentadiene ND ug/kg 1 09/19/09 02:45 77-47-409/10/09 14:30400 Hexachloroethane ND ug/kg 1 09/19/09 02:45 67-72-109/10/09 14:30400 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 55 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP2-09-09 Lab ID:9252614017 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/09 02:45 193-39-509/10/09 14:30400 Isophorone ND ug/kg 1 09/19/09 02:45 78-59-109/10/09 14:30400 1-Methylnaphthalene ND ug/kg 1 09/19/09 02:45 90-12-009/10/09 14:30400 2-Methylnaphthalene ND ug/kg 1 09/19/09 02:45 91-57-609/10/09 14:30400 2-Methylphenol(o-Cresol)ND ug/kg 1 09/19/09 02:45 95-48-709/10/09 14:30400 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/19/09 02:4509/10/09 14:30400 Naphthalene ND ug/kg 1 09/19/09 02:45 91-20-309/10/09 14:30400 2-Nitroaniline ND ug/kg 1 09/19/09 02:45 88-74-409/10/09 14:302000 3-Nitroaniline ND ug/kg 1 09/19/09 02:45 99-09-209/10/09 14:302000 4-Nitroaniline ND ug/kg 1 09/19/09 02:45 100-01-609/10/09 14:30799 Nitrobenzene ND ug/kg 1 09/19/09 02:45 98-95-309/10/09 14:30400 2-Nitrophenol ND ug/kg 1 09/19/09 02:45 88-75-509/10/09 14:30400 4-Nitrophenol ND ug/kg 1 09/19/09 02:45 100-02-709/10/09 14:302000 N-Nitrosodimethylamine ND ug/kg 1 09/19/09 02:45 62-75-909/10/09 14:30400 N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/09 02:45 621-64-709/10/09 14:30400 N-Nitrosodiphenylamine ND ug/kg 1 09/19/09 02:45 86-30-609/10/09 14:30400 Pentachlorophenol ND ug/kg 1 09/19/09 02:45 87-86-509/10/09 14:302000 Phenanthrene ND ug/kg 1 09/19/09 02:45 85-01-809/10/09 14:30400 Phenol ND ug/kg 1 09/19/09 02:45 108-95-209/10/09 14:30400 Pyrene ND ug/kg 1 09/19/09 02:45 129-00-009/10/09 14:30400 1,2,4-Trichlorobenzene ND ug/kg 1 09/19/09 02:45 120-82-109/10/09 14:30400 2,4,5-Trichlorophenol ND ug/kg 1 09/19/09 02:45 95-95-409/10/09 14:30400 2,4,6-Trichlorophenol ND ug/kg 1 09/19/09 02:45 88-06-209/10/09 14:30400 Nitrobenzene-d5 (S)32 %1 09/19/09 02:45 4165-60-009/10/09 14:3030-150 2-Fluorobiphenyl (S)55 %1 09/19/09 02:45 321-60-809/10/09 14:3046-120 Terphenyl-d14 (S)63 %1 09/19/09 02:45 1718-51-009/10/09 14:3038-108 Phenol-d6 (S)30 %1 09/19/09 02:45 13127-88-3 1g09/10/09 14:3035-120 2-Fluorophenol (S)29 %1 09/19/09 02:45 367-12-409/10/09 14:3024-120 2,4,6-Tribromophenol (S)46 %1 09/19/09 02:45 118-79-609/10/09 14:3044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/11/09 19:29 67-64-14390 Benzene ND ug/kg 50 09/11/09 19:29 71-43-2220 Bromobenzene ND ug/kg 50 09/11/09 19:29 108-86-1220 Bromochloromethane ND ug/kg 50 09/11/09 19:29 74-97-5220 Bromodichloromethane ND ug/kg 50 09/11/09 19:29 75-27-4220 Bromoform ND ug/kg 50 09/11/09 19:29 75-25-2220 Bromomethane ND ug/kg 50 09/11/09 19:29 74-83-9439 2-Butanone (MEK)ND ug/kg 50 09/11/09 19:29 78-93-34390 n-Butylbenzene ND ug/kg 50 09/11/09 19:29 104-51-8220 sec-Butylbenzene ND ug/kg 50 09/11/09 19:29 135-98-8220 tert-Butylbenzene ND ug/kg 50 09/11/09 19:29 98-06-6220 Carbon tetrachloride ND ug/kg 50 09/11/09 19:29 56-23-5220 Chlorobenzene ND ug/kg 50 09/11/09 19:29 108-90-7220 Chloroethane ND ug/kg 50 09/11/09 19:29 75-00-3439 Chloroform ND ug/kg 50 09/11/09 19:29 67-66-3220 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 56 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP2-09-09 Lab ID:9252614017 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 50 09/11/09 19:29 74-87-3439 2-Chlorotoluene ND ug/kg 50 09/11/09 19:29 95-49-8220 4-Chlorotoluene ND ug/kg 50 09/11/09 19:29 106-43-4220 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/11/09 19:29 96-12-8220 Dibromochloromethane ND ug/kg 50 09/11/09 19:29 124-48-1220 1,2-Dibromoethane (EDB)ND ug/kg 50 09/11/09 19:29 106-93-4220 Dibromomethane ND ug/kg 50 09/11/09 19:29 74-95-3220 1,2-Dichlorobenzene ND ug/kg 50 09/11/09 19:29 95-50-1220 1,3-Dichlorobenzene ND ug/kg 50 09/11/09 19:29 541-73-1220 1,4-Dichlorobenzene ND ug/kg 50 09/11/09 19:29 106-46-7220 Dichlorodifluoromethane ND ug/kg 50 09/11/09 19:29 75-71-8439 1,1-Dichloroethane ND ug/kg 50 09/11/09 19:29 75-34-3220 1,2-Dichloroethane ND ug/kg 50 09/11/09 19:29 107-06-2220 1,1-Dichloroethene ND ug/kg 50 09/11/09 19:29 75-35-4220 cis-1,2-Dichloroethene ND ug/kg 50 09/11/09 19:29 156-59-2220 trans-1,2-Dichloroethene ND ug/kg 50 09/11/09 19:29 156-60-5220 1,2-Dichloropropane ND ug/kg 50 09/11/09 19:29 78-87-5220 1,3-Dichloropropane ND ug/kg 50 09/11/09 19:29 142-28-9220 2,2-Dichloropropane ND ug/kg 50 09/11/09 19:29 594-20-7220 1,1-Dichloropropene ND ug/kg 50 09/11/09 19:29 563-58-6220 cis-1,3-Dichloropropene ND ug/kg 50 09/11/09 19:29 10061-01-5220 trans-1,3-Dichloropropene ND ug/kg 50 09/11/09 19:29 10061-02-6220 Diisopropyl ether ND ug/kg 50 09/11/09 19:29 108-20-3220 Ethylbenzene ND ug/kg 50 09/11/09 19:29 100-41-4220 Hexachloro-1,3-butadiene ND ug/kg 50 09/11/09 19:29 87-68-3220 2-Hexanone ND ug/kg 50 09/11/09 19:29 591-78-62200 Isopropylbenzene (Cumene)ND ug/kg 50 09/11/09 19:29 98-82-8220 p-Isopropyltoluene ND ug/kg 50 09/11/09 19:29 99-87-6220 Methylene Chloride ND ug/kg 50 09/11/09 19:29 75-09-2879 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/11/09 19:29 108-10-12200 Methyl-tert-butyl ether ND ug/kg 50 09/11/09 19:29 1634-04-4220 Naphthalene ND ug/kg 50 09/11/09 19:29 91-20-3220 n-Propylbenzene ND ug/kg 50 09/11/09 19:29 103-65-1220 Styrene ND ug/kg 50 09/11/09 19:29 100-42-5220 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/11/09 19:29 630-20-6220 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/11/09 19:29 79-34-5220 Tetrachloroethene ND ug/kg 50 09/11/09 19:29 127-18-4220 Toluene ND ug/kg 50 09/11/09 19:29 108-88-3220 1,2,3-Trichlorobenzene ND ug/kg 50 09/11/09 19:29 87-61-6220 1,2,4-Trichlorobenzene ND ug/kg 50 09/11/09 19:29 120-82-1220 1,1,1-Trichloroethane ND ug/kg 50 09/11/09 19:29 71-55-6220 1,1,2-Trichloroethane ND ug/kg 50 09/11/09 19:29 79-00-5220 Trichloroethene ND ug/kg 50 09/11/09 19:29 79-01-6220 Trichlorofluoromethane ND ug/kg 50 09/11/09 19:29 75-69-4220 1,2,3-Trichloropropane ND ug/kg 50 09/11/09 19:29 96-18-4220 1,2,4-Trimethylbenzene ND ug/kg 50 09/11/09 19:29 95-63-6220 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 57 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP2-09-09 Lab ID:9252614017 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene ND ug/kg 50 09/11/09 19:29 108-67-8220 Vinyl acetate ND ug/kg 50 09/11/09 19:29 108-05-42200 Vinyl chloride ND ug/kg 50 09/11/09 19:29 75-01-4439 Xylene (Total)ND ug/kg 50 09/11/09 19:29 1330-20-7439 m&p-Xylene ND ug/kg 50 09/11/09 19:29 1330-20-7439 o-Xylene ND ug/kg 50 09/11/09 19:29 95-47-6220 Dibromofluoromethane (S)98 %50 09/11/09 19:29 1868-53-7 D379-116 Toluene-d8 (S)101 %50 09/11/09 19:29 2037-26-588-110 4-Bromofluorobenzene (S)99 %50 09/11/09 19:29 460-00-474-115 1,2-Dichloroethane-d4 (S)94 %50 09/11/09 19:29 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 17.4 %1 09/09/09 13:450.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 58 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW1-SS1-09-09 Lab ID:9252614018 Collected:09/08/09 13:05 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 9071 SGT-HEM, TPH Analytical Method: 9071B ASE Preparation Method: 9071B ASE Total Petroleum Hydrocarbons 141 mg/kg 1 09/15/09 17:5709/09/09 09:1589.8 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 20 09/22/09 21:47 83-32-909/10/09 14:308460 Acenaphthylene ND ug/kg 20 09/22/09 21:47 208-96-809/10/09 14:308460 Aniline ND ug/kg 20 09/22/09 21:47 62-53-309/10/09 14:308460 Anthracene ND ug/kg 20 09/22/09 21:47 120-12-709/10/09 14:308460 Benzo(a)anthracene ND ug/kg 20 09/22/09 21:47 56-55-309/10/09 14:308460 Benzo(a)pyrene ND ug/kg 20 09/22/09 21:47 50-32-809/10/09 14:308460 Benzo(b)fluoranthene ND ug/kg 20 09/22/09 21:47 205-99-209/10/09 14:308460 Benzo(g,h,i)perylene ND ug/kg 20 09/22/09 21:47 191-24-209/10/09 14:308460 Benzo(k)fluoranthene ND ug/kg 20 09/22/09 21:47 207-08-909/10/09 14:308460 Benzoic Acid ND ug/kg 20 09/22/09 21:47 65-85-009/10/09 14:3042300 Benzyl alcohol ND ug/kg 20 09/22/09 21:47 100-51-609/10/09 14:3016900 4-Bromophenylphenyl ether ND ug/kg 20 09/22/09 21:47 101-55-309/10/09 14:308460 Butylbenzylphthalate ND ug/kg 20 09/22/09 21:47 85-68-709/10/09 14:308460 4-Chloro-3-methylphenol ND ug/kg 20 09/22/09 21:47 59-50-709/10/09 14:3016900 4-Chloroaniline ND ug/kg 20 09/22/09 21:47 106-47-809/10/09 14:3042300 bis(2-Chloroethoxy)methane ND ug/kg 20 09/22/09 21:47 111-91-109/10/09 14:308460 bis(2-Chloroethyl) ether ND ug/kg 20 09/22/09 21:47 111-44-409/10/09 14:308460 bis(2-Chloroisopropyl) ether ND ug/kg 20 09/22/09 21:47 108-60-109/10/09 14:308460 2-Chloronaphthalene ND ug/kg 20 09/22/09 21:47 91-58-709/10/09 14:308460 2-Chlorophenol ND ug/kg 20 09/22/09 21:47 95-57-809/10/09 14:308460 4-Chlorophenylphenyl ether ND ug/kg 20 09/22/09 21:47 7005-72-309/10/09 14:308460 Chrysene ND ug/kg 20 09/22/09 21:47 218-01-909/10/09 14:308460 Dibenz(a,h)anthracene ND ug/kg 20 09/22/09 21:47 53-70-309/10/09 14:308460 Dibenzofuran ND ug/kg 20 09/22/09 21:47 132-64-909/10/09 14:308460 1,2-Dichlorobenzene ND ug/kg 20 09/22/09 21:47 95-50-109/10/09 14:308460 1,3-Dichlorobenzene ND ug/kg 20 09/22/09 21:47 541-73-109/10/09 14:308460 1,4-Dichlorobenzene ND ug/kg 20 09/22/09 21:47 106-46-709/10/09 14:308460 3,3'-Dichlorobenzidine ND ug/kg 20 09/22/09 21:47 91-94-109/10/09 14:3042300 2,4-Dichlorophenol ND ug/kg 20 09/22/09 21:47 120-83-209/10/09 14:308460 Diethylphthalate ND ug/kg 20 09/22/09 21:47 84-66-209/10/09 14:308460 2,4-Dimethylphenol ND ug/kg 20 09/22/09 21:47 105-67-909/10/09 14:308460 Dimethylphthalate ND ug/kg 20 09/22/09 21:47 131-11-309/10/09 14:308460 Di-n-butylphthalate ND ug/kg 20 09/22/09 21:47 84-74-209/10/09 14:308460 4,6-Dinitro-2-methylphenol ND ug/kg 20 09/22/09 21:47 534-52-109/10/09 14:3016900 2,4-Dinitrophenol ND ug/kg 20 09/22/09 21:47 51-28-509/10/09 14:3042300 2,4-Dinitrotoluene ND ug/kg 20 09/22/09 21:47 121-14-209/10/09 14:308460 2,6-Dinitrotoluene ND ug/kg 20 09/22/09 21:47 606-20-209/10/09 14:308460 Di-n-octylphthalate ND ug/kg 20 09/22/09 21:47 117-84-009/10/09 14:308460 1,2-Diphenylhydrazine ND ug/kg 20 09/22/09 21:47 122-66-709/10/09 14:308460 bis(2-Ethylhexyl)phthalate ND ug/kg 20 09/22/09 21:47 117-81-709/10/09 14:308460 Fluoranthene ND ug/kg 20 09/22/09 21:47 206-44-009/10/09 14:308460 Fluorene ND ug/kg 20 09/22/09 21:47 86-73-709/10/09 14:308460 Hexachloro-1,3-butadiene ND ug/kg 20 09/22/09 21:47 87-68-309/10/09 14:308460 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 59 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW1-SS1-09-09 Lab ID:9252614018 Collected:09/08/09 13:05 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Hexachlorobenzene ND ug/kg 20 09/22/09 21:47 118-74-109/10/09 14:308460 Hexachlorocyclopentadiene ND ug/kg 20 09/22/09 21:47 77-47-409/10/09 14:308460 Hexachloroethane ND ug/kg 20 09/22/09 21:47 67-72-109/10/09 14:308460 Indeno(1,2,3-cd)pyrene ND ug/kg 20 09/22/09 21:47 193-39-509/10/09 14:308460 Isophorone ND ug/kg 20 09/22/09 21:47 78-59-109/10/09 14:308460 1-Methylnaphthalene 16000 ug/kg 20 09/22/09 21:47 90-12-009/10/09 14:308460 2-Methylnaphthalene 12200 ug/kg 20 09/22/09 21:47 91-57-609/10/09 14:308460 2-Methylphenol(o-Cresol)ND ug/kg 20 09/22/09 21:47 95-48-709/10/09 14:308460 3&4-Methylphenol(m&p Cresol)ND ug/kg 20 09/22/09 21:4709/10/09 14:308460 Naphthalene ND ug/kg 20 09/22/09 21:47 91-20-309/10/09 14:308460 2-Nitroaniline ND ug/kg 20 09/22/09 21:47 88-74-409/10/09 14:3042300 3-Nitroaniline ND ug/kg 20 09/22/09 21:47 99-09-209/10/09 14:3042300 4-Nitroaniline ND ug/kg 20 09/22/09 21:47 100-01-609/10/09 14:3016900 Nitrobenzene ND ug/kg 20 09/22/09 21:47 98-95-309/10/09 14:308460 2-Nitrophenol ND ug/kg 20 09/22/09 21:47 88-75-509/10/09 14:308460 4-Nitrophenol ND ug/kg 20 09/22/09 21:47 100-02-709/10/09 14:3042300 N-Nitrosodimethylamine ND ug/kg 20 09/22/09 21:47 62-75-909/10/09 14:308460 N-Nitroso-di-n-propylamine ND ug/kg 20 09/22/09 21:47 621-64-709/10/09 14:308460 N-Nitrosodiphenylamine ND ug/kg 20 09/22/09 21:47 86-30-609/10/09 14:308460 Pentachlorophenol ND ug/kg 20 09/22/09 21:47 87-86-509/10/09 14:3042300 Phenanthrene ND ug/kg 20 09/22/09 21:47 85-01-809/10/09 14:308460 Phenol ND ug/kg 20 09/22/09 21:47 108-95-209/10/09 14:308460 Pyrene ND ug/kg 20 09/22/09 21:47 129-00-009/10/09 14:308460 1,2,4-Trichlorobenzene ND ug/kg 20 09/22/09 21:47 120-82-109/10/09 14:308460 2,4,5-Trichlorophenol ND ug/kg 20 09/22/09 21:47 95-95-409/10/09 14:308460 2,4,6-Trichlorophenol ND ug/kg 20 09/22/09 21:47 88-06-209/10/09 14:308460 Nitrobenzene-d5 (S)0 %20 09/22/09 21:47 4165-60-0 3g,D309/10/09 14:3030-150 2-Fluorobiphenyl (S)0 %20 09/22/09 21:47 321-60-809/10/09 14:3046-120 Terphenyl-d14 (S)0 %20 09/22/09 21:47 1718-51-009/10/09 14:3038-108 Phenol-d6 (S)0 %20 09/22/09 21:47 13127-88-309/10/09 14:3035-120 2-Fluorophenol (S)0 %20 09/22/09 21:47 367-12-409/10/09 14:3024-120 2,4,6-Tribromophenol (S)0 %20 09/22/09 21:47 118-79-609/10/09 14:3044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/11/09 18:34 67-64-14980 Benzene ND ug/kg 50 09/11/09 18:34 71-43-2249 Bromobenzene ND ug/kg 50 09/11/09 18:34 108-86-1249 Bromochloromethane ND ug/kg 50 09/11/09 18:34 74-97-5249 Bromodichloromethane ND ug/kg 50 09/11/09 18:34 75-27-4249 Bromoform ND ug/kg 50 09/11/09 18:34 75-25-2249 Bromomethane ND ug/kg 50 09/11/09 18:34 74-83-9498 2-Butanone (MEK)ND ug/kg 50 09/11/09 18:34 78-93-34980 n-Butylbenzene 4560 ug/kg 50 09/11/09 18:34 104-51-8249 sec-Butylbenzene 3030 ug/kg 50 09/11/09 18:34 135-98-8249 tert-Butylbenzene ND ug/kg 50 09/11/09 18:34 98-06-6249 Carbon tetrachloride ND ug/kg 50 09/11/09 18:34 56-23-5249 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 60 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW1-SS1-09-09 Lab ID:9252614018 Collected:09/08/09 13:05 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chlorobenzene ND ug/kg 50 09/11/09 18:34 108-90-7249 Chloroethane ND ug/kg 50 09/11/09 18:34 75-00-3498 Chloroform ND ug/kg 50 09/11/09 18:34 67-66-3249 Chloromethane ND ug/kg 50 09/11/09 18:34 74-87-3498 2-Chlorotoluene ND ug/kg 50 09/11/09 18:34 95-49-8249 4-Chlorotoluene ND ug/kg 50 09/11/09 18:34 106-43-4249 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/11/09 18:34 96-12-8249 Dibromochloromethane ND ug/kg 50 09/11/09 18:34 124-48-1249 1,2-Dibromoethane (EDB)ND ug/kg 50 09/11/09 18:34 106-93-4249 Dibromomethane ND ug/kg 50 09/11/09 18:34 74-95-3249 1,2-Dichlorobenzene ND ug/kg 50 09/11/09 18:34 95-50-1249 1,3-Dichlorobenzene ND ug/kg 50 09/11/09 18:34 541-73-1249 1,4-Dichlorobenzene ND ug/kg 50 09/11/09 18:34 106-46-7249 Dichlorodifluoromethane ND ug/kg 50 09/11/09 18:34 75-71-8498 1,1-Dichloroethane ND ug/kg 50 09/11/09 18:34 75-34-3249 1,2-Dichloroethane ND ug/kg 50 09/11/09 18:34 107-06-2249 1,1-Dichloroethene ND ug/kg 50 09/11/09 18:34 75-35-4249 cis-1,2-Dichloroethene ND ug/kg 50 09/11/09 18:34 156-59-2249 trans-1,2-Dichloroethene ND ug/kg 50 09/11/09 18:34 156-60-5249 1,2-Dichloropropane ND ug/kg 50 09/11/09 18:34 78-87-5249 1,3-Dichloropropane ND ug/kg 50 09/11/09 18:34 142-28-9249 2,2-Dichloropropane ND ug/kg 50 09/11/09 18:34 594-20-7249 1,1-Dichloropropene ND ug/kg 50 09/11/09 18:34 563-58-6249 cis-1,3-Dichloropropene ND ug/kg 50 09/11/09 18:34 10061-01-5249 trans-1,3-Dichloropropene ND ug/kg 50 09/11/09 18:34 10061-02-6249 Diisopropyl ether ND ug/kg 50 09/11/09 18:34 108-20-3249 Ethylbenzene 474 ug/kg 50 09/11/09 18:34 100-41-4249 Hexachloro-1,3-butadiene ND ug/kg 50 09/11/09 18:34 87-68-3249 2-Hexanone ND ug/kg 50 09/11/09 18:34 591-78-62490 Isopropylbenzene (Cumene)1100 ug/kg 50 09/11/09 18:34 98-82-8249 p-Isopropyltoluene 5800 ug/kg 50 09/11/09 18:34 99-87-6249 Methylene Chloride ND ug/kg 50 09/11/09 18:34 75-09-2996 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/11/09 18:34 108-10-12490 Methyl-tert-butyl ether ND ug/kg 50 09/11/09 18:34 1634-04-4249 Naphthalene 5250 ug/kg 50 09/11/09 18:34 91-20-3249 n-Propylbenzene 2000 ug/kg 50 09/11/09 18:34 103-65-1249 Styrene ND ug/kg 50 09/11/09 18:34 100-42-5249 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/11/09 18:34 630-20-6249 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/11/09 18:34 79-34-5249 Tetrachloroethene ND ug/kg 50 09/11/09 18:34 127-18-4249 Toluene ND ug/kg 50 09/11/09 18:34 108-88-3249 1,2,3-Trichlorobenzene ND ug/kg 50 09/11/09 18:34 87-61-6249 1,2,4-Trichlorobenzene ND ug/kg 50 09/11/09 18:34 120-82-1249 1,1,1-Trichloroethane ND ug/kg 50 09/11/09 18:34 71-55-6249 1,1,2-Trichloroethane ND ug/kg 50 09/11/09 18:34 79-00-5249 Trichloroethene ND ug/kg 50 09/11/09 18:34 79-01-6249 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 61 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW1-SS1-09-09 Lab ID:9252614018 Collected:09/08/09 13:05 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Trichlorofluoromethane ND ug/kg 50 09/11/09 18:34 75-69-4249 1,2,3-Trichloropropane ND ug/kg 50 09/11/09 18:34 96-18-4249 1,2,4-Trimethylbenzene 17500 ug/kg 100 09/14/09 14:31 95-63-6498 1,3,5-Trimethylbenzene 4940 ug/kg 50 09/11/09 18:34 108-67-8249 Vinyl acetate ND ug/kg 50 09/11/09 18:34 108-05-42490 Vinyl chloride ND ug/kg 50 09/11/09 18:34 75-01-4498 Xylene (Total)1670 ug/kg 50 09/11/09 18:34 1330-20-7498 m&p-Xylene 980 ug/kg 50 09/11/09 18:34 1330-20-7498 o-Xylene 691 ug/kg 50 09/11/09 18:34 95-47-6249 Dibromofluoromethane (S)101 %50 09/11/09 18:34 1868-53-779-116 Toluene-d8 (S)101 %50 09/11/09 18:34 2037-26-588-110 4-Bromofluorobenzene (S)100 %50 09/11/09 18:34 460-00-474-115 1,2-Dichloroethane-d4 (S)98 %50 09/11/09 18:34 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 22.0 %1 09/09/09 13:450.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 62 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP3-09-09 Lab ID:9252614019 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 9071 SGT-HEM, TPH Analytical Method: 9071B ASE Preparation Method: 9071B ASE Total Petroleum Hydrocarbons 118 mg/kg 1 09/15/09 17:5709/09/09 09:1591.4 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/19/09 03:29 83-32-909/10/09 14:30431 Acenaphthylene ND ug/kg 1 09/19/09 03:29 208-96-809/10/09 14:30431 Aniline ND ug/kg 1 09/19/09 03:29 62-53-309/10/09 14:30431 Anthracene ND ug/kg 1 09/19/09 03:29 120-12-709/10/09 14:30431 Benzo(a)anthracene ND ug/kg 1 09/19/09 03:29 56-55-309/10/09 14:30431 Benzo(a)pyrene ND ug/kg 1 09/19/09 03:29 50-32-809/10/09 14:30431 Benzo(b)fluoranthene ND ug/kg 1 09/19/09 03:29 205-99-209/10/09 14:30431 Benzo(g,h,i)perylene ND ug/kg 1 09/19/09 03:29 191-24-209/10/09 14:30431 Benzo(k)fluoranthene ND ug/kg 1 09/19/09 03:29 207-08-909/10/09 14:30431 Benzoic Acid ND ug/kg 1 09/19/09 03:29 65-85-009/10/09 14:302150 Benzyl alcohol ND ug/kg 1 09/19/09 03:29 100-51-609/10/09 14:30862 4-Bromophenylphenyl ether ND ug/kg 1 09/19/09 03:29 101-55-309/10/09 14:30431 Butylbenzylphthalate ND ug/kg 1 09/19/09 03:29 85-68-709/10/09 14:30431 4-Chloro-3-methylphenol ND ug/kg 1 09/19/09 03:29 59-50-709/10/09 14:30862 4-Chloroaniline ND ug/kg 1 09/19/09 03:29 106-47-809/10/09 14:302150 bis(2-Chloroethoxy)methane ND ug/kg 1 09/19/09 03:29 111-91-109/10/09 14:30431 bis(2-Chloroethyl) ether ND ug/kg 1 09/19/09 03:29 111-44-409/10/09 14:30431 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/19/09 03:29 108-60-109/10/09 14:30431 2-Chloronaphthalene ND ug/kg 1 09/19/09 03:29 91-58-709/10/09 14:30431 2-Chlorophenol ND ug/kg 1 09/19/09 03:29 95-57-809/10/09 14:30431 4-Chlorophenylphenyl ether ND ug/kg 1 09/19/09 03:29 7005-72-309/10/09 14:30431 Chrysene ND ug/kg 1 09/19/09 03:29 218-01-909/10/09 14:30431 Dibenz(a,h)anthracene ND ug/kg 1 09/19/09 03:29 53-70-309/10/09 14:30431 Dibenzofuran ND ug/kg 1 09/19/09 03:29 132-64-909/10/09 14:30431 1,2-Dichlorobenzene ND ug/kg 1 09/19/09 03:29 95-50-109/10/09 14:30431 1,3-Dichlorobenzene ND ug/kg 1 09/19/09 03:29 541-73-109/10/09 14:30431 1,4-Dichlorobenzene ND ug/kg 1 09/19/09 03:29 106-46-709/10/09 14:30431 3,3'-Dichlorobenzidine ND ug/kg 1 09/19/09 03:29 91-94-109/10/09 14:302150 2,4-Dichlorophenol ND ug/kg 1 09/19/09 03:29 120-83-209/10/09 14:30431 Diethylphthalate ND ug/kg 1 09/19/09 03:29 84-66-209/10/09 14:30431 2,4-Dimethylphenol ND ug/kg 1 09/19/09 03:29 105-67-909/10/09 14:30431 Dimethylphthalate ND ug/kg 1 09/19/09 03:29 131-11-309/10/09 14:30431 Di-n-butylphthalate ND ug/kg 1 09/19/09 03:29 84-74-209/10/09 14:30431 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/09 03:29 534-52-109/10/09 14:30862 2,4-Dinitrophenol ND ug/kg 1 09/19/09 03:29 51-28-509/10/09 14:302150 2,4-Dinitrotoluene ND ug/kg 1 09/19/09 03:29 121-14-209/10/09 14:30431 2,6-Dinitrotoluene ND ug/kg 1 09/19/09 03:29 606-20-209/10/09 14:30431 Di-n-octylphthalate ND ug/kg 1 09/19/09 03:29 117-84-009/10/09 14:30431 1,2-Diphenylhydrazine ND ug/kg 1 09/19/09 03:29 122-66-709/10/09 14:30431 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/09 03:29 117-81-709/10/09 14:30431 Fluoranthene ND ug/kg 1 09/19/09 03:29 206-44-009/10/09 14:30431 Fluorene 968 ug/kg 1 09/19/09 03:29 86-73-709/10/09 14:30431 Hexachloro-1,3-butadiene ND ug/kg 1 09/19/09 03:29 87-68-309/10/09 14:30431 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 63 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP3-09-09 Lab ID:9252614019 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Hexachlorobenzene ND ug/kg 1 09/19/09 03:29 118-74-109/10/09 14:30431 Hexachlorocyclopentadiene ND ug/kg 1 09/19/09 03:29 77-47-409/10/09 14:30431 Hexachloroethane ND ug/kg 1 09/19/09 03:29 67-72-109/10/09 14:30431 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/09 03:29 193-39-509/10/09 14:30431 Isophorone ND ug/kg 1 09/19/09 03:29 78-59-109/10/09 14:30431 1-Methylnaphthalene 5820 ug/kg 1 09/19/09 03:29 90-12-009/10/09 14:30431 2-Methylnaphthalene 8830 ug/kg 1 09/19/09 03:29 91-57-609/10/09 14:30431 2-Methylphenol(o-Cresol)ND ug/kg 1 09/19/09 03:29 95-48-709/10/09 14:30431 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/19/09 03:2909/10/09 14:30431 Naphthalene 1340 ug/kg 1 09/19/09 03:29 91-20-309/10/09 14:30431 2-Nitroaniline ND ug/kg 1 09/19/09 03:29 88-74-409/10/09 14:302150 3-Nitroaniline ND ug/kg 1 09/19/09 03:29 99-09-209/10/09 14:302150 4-Nitroaniline ND ug/kg 1 09/19/09 03:29 100-01-609/10/09 14:30862 Nitrobenzene ND ug/kg 1 09/19/09 03:29 98-95-309/10/09 14:30431 2-Nitrophenol ND ug/kg 1 09/19/09 03:29 88-75-509/10/09 14:30431 4-Nitrophenol ND ug/kg 1 09/19/09 03:29 100-02-709/10/09 14:302150 N-Nitrosodimethylamine ND ug/kg 1 09/19/09 03:29 62-75-909/10/09 14:30431 N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/09 03:29 621-64-709/10/09 14:30431 N-Nitrosodiphenylamine ND ug/kg 1 09/19/09 03:29 86-30-609/10/09 14:30431 Pentachlorophenol ND ug/kg 1 09/19/09 03:29 87-86-509/10/09 14:302150 Phenanthrene 1660 ug/kg 1 09/19/09 03:29 85-01-809/10/09 14:30431 Phenol ND ug/kg 1 09/19/09 03:29 108-95-209/10/09 14:30431 Pyrene ND ug/kg 1 09/19/09 03:29 129-00-009/10/09 14:30431 1,2,4-Trichlorobenzene ND ug/kg 1 09/19/09 03:29 120-82-109/10/09 14:30431 2,4,5-Trichlorophenol ND ug/kg 1 09/19/09 03:29 95-95-409/10/09 14:30431 2,4,6-Trichlorophenol ND ug/kg 1 09/19/09 03:29 88-06-209/10/09 14:30431 Nitrobenzene-d5 (S)49 %1 09/19/09 03:29 4165-60-009/10/09 14:3030-150 2-Fluorobiphenyl (S)64 %1 09/19/09 03:29 321-60-809/10/09 14:3046-120 Terphenyl-d14 (S)80 %1 09/19/09 03:29 1718-51-009/10/09 14:3038-108 Phenol-d6 (S)61 %1 09/19/09 03:29 13127-88-309/10/09 14:3035-120 2-Fluorophenol (S)49 %1 09/19/09 03:29 367-12-409/10/09 14:3024-120 2,4,6-Tribromophenol (S)66 %1 09/19/09 03:29 118-79-609/10/09 14:3044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/11/09 18:52 67-64-15100 Benzene ND ug/kg 50 09/11/09 18:52 71-43-2255 Bromobenzene ND ug/kg 50 09/11/09 18:52 108-86-1255 Bromochloromethane ND ug/kg 50 09/11/09 18:52 74-97-5255 Bromodichloromethane ND ug/kg 50 09/11/09 18:52 75-27-4255 Bromoform ND ug/kg 50 09/11/09 18:52 75-25-2255 Bromomethane ND ug/kg 50 09/11/09 18:52 74-83-9510 2-Butanone (MEK)ND ug/kg 50 09/11/09 18:52 78-93-35100 n-Butylbenzene 6140 ug/kg 50 09/11/09 18:52 104-51-8255 sec-Butylbenzene 4170 ug/kg 50 09/11/09 18:52 135-98-8255 tert-Butylbenzene 366 ug/kg 50 09/11/09 18:52 98-06-6255 Carbon tetrachloride ND ug/kg 50 09/11/09 18:52 56-23-5255 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 64 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP3-09-09 Lab ID:9252614019 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chlorobenzene ND ug/kg 50 09/11/09 18:52 108-90-7255 Chloroethane ND ug/kg 50 09/11/09 18:52 75-00-3510 Chloroform ND ug/kg 50 09/11/09 18:52 67-66-3255 Chloromethane ND ug/kg 50 09/11/09 18:52 74-87-3510 2-Chlorotoluene ND ug/kg 50 09/11/09 18:52 95-49-8255 4-Chlorotoluene ND ug/kg 50 09/11/09 18:52 106-43-4255 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/11/09 18:52 96-12-8255 Dibromochloromethane ND ug/kg 50 09/11/09 18:52 124-48-1255 1,2-Dibromoethane (EDB)ND ug/kg 50 09/11/09 18:52 106-93-4255 Dibromomethane ND ug/kg 50 09/11/09 18:52 74-95-3255 1,2-Dichlorobenzene ND ug/kg 50 09/11/09 18:52 95-50-1255 1,3-Dichlorobenzene ND ug/kg 50 09/11/09 18:52 541-73-1255 1,4-Dichlorobenzene ND ug/kg 50 09/11/09 18:52 106-46-7255 Dichlorodifluoromethane ND ug/kg 50 09/11/09 18:52 75-71-8510 1,1-Dichloroethane ND ug/kg 50 09/11/09 18:52 75-34-3255 1,2-Dichloroethane ND ug/kg 50 09/11/09 18:52 107-06-2255 1,1-Dichloroethene ND ug/kg 50 09/11/09 18:52 75-35-4255 cis-1,2-Dichloroethene ND ug/kg 50 09/11/09 18:52 156-59-2255 trans-1,2-Dichloroethene ND ug/kg 50 09/11/09 18:52 156-60-5255 1,2-Dichloropropane ND ug/kg 50 09/11/09 18:52 78-87-5255 1,3-Dichloropropane ND ug/kg 50 09/11/09 18:52 142-28-9255 2,2-Dichloropropane ND ug/kg 50 09/11/09 18:52 594-20-7255 1,1-Dichloropropene ND ug/kg 50 09/11/09 18:52 563-58-6255 cis-1,3-Dichloropropene ND ug/kg 50 09/11/09 18:52 10061-01-5255 trans-1,3-Dichloropropene ND ug/kg 50 09/11/09 18:52 10061-02-6255 Diisopropyl ether ND ug/kg 50 09/11/09 18:52 108-20-3255 Ethylbenzene 605 ug/kg 50 09/11/09 18:52 100-41-4255 Hexachloro-1,3-butadiene ND ug/kg 50 09/11/09 18:52 87-68-3255 2-Hexanone ND ug/kg 50 09/11/09 18:52 591-78-62550 Isopropylbenzene (Cumene)1650 ug/kg 50 09/11/09 18:52 98-82-8255 p-Isopropyltoluene 4670 ug/kg 50 09/11/09 18:52 99-87-6255 Methylene Chloride ND ug/kg 50 09/11/09 18:52 75-09-21020 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/11/09 18:52 108-10-12550 Methyl-tert-butyl ether ND ug/kg 50 09/11/09 18:52 1634-04-4255 Naphthalene 5140 ug/kg 50 09/11/09 18:52 91-20-3255 n-Propylbenzene 2700 ug/kg 50 09/11/09 18:52 103-65-1255 Styrene ND ug/kg 50 09/11/09 18:52 100-42-5255 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/11/09 18:52 630-20-6255 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/11/09 18:52 79-34-5255 Tetrachloroethene ND ug/kg 50 09/11/09 18:52 127-18-4255 Toluene ND ug/kg 50 09/11/09 18:52 108-88-3255 1,2,3-Trichlorobenzene ND ug/kg 50 09/11/09 18:52 87-61-6255 1,2,4-Trichlorobenzene ND ug/kg 50 09/11/09 18:52 120-82-1255 1,1,1-Trichloroethane ND ug/kg 50 09/11/09 18:52 71-55-6255 1,1,2-Trichloroethane ND ug/kg 50 09/11/09 18:52 79-00-5255 Trichloroethene ND ug/kg 50 09/11/09 18:52 79-01-6255 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 65 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -DUP3-09-09 Lab ID:9252614019 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Trichlorofluoromethane ND ug/kg 50 09/11/09 18:52 75-69-4255 1,2,3-Trichloropropane ND ug/kg 50 09/11/09 18:52 96-18-4255 1,2,4-Trimethylbenzene 17400 ug/kg 250 09/14/09 15:26 95-63-61280 1,3,5-Trimethylbenzene 7320 ug/kg 50 09/11/09 18:52 108-67-8255 Vinyl acetate ND ug/kg 50 09/11/09 18:52 108-05-42550 Vinyl chloride ND ug/kg 50 09/11/09 18:52 75-01-4510 Xylene (Total)2240 ug/kg 50 09/11/09 18:52 1330-20-7510 m&p-Xylene 1200 ug/kg 50 09/11/09 18:52 1330-20-7510 o-Xylene 1030 ug/kg 50 09/11/09 18:52 95-47-6255 Dibromofluoromethane (S)101 %50 09/11/09 18:52 1868-53-779-116 Toluene-d8 (S)101 %50 09/11/09 18:52 2037-26-588-110 4-Bromofluorobenzene (S)105 %50 09/11/09 18:52 460-00-474-115 1,2-Dichloroethane-d4 (S)103 %50 09/11/09 18:52 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 23.4 %1 09/09/09 13:470.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 66 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS1-09-09 Lab ID:9252614020 Collected:09/08/09 13:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/19/09 03:51 83-32-909/10/09 14:30400 Acenaphthylene ND ug/kg 1 09/19/09 03:51 208-96-809/10/09 14:30400 Aniline ND ug/kg 1 09/19/09 03:51 62-53-309/10/09 14:30400 Anthracene ND ug/kg 1 09/19/09 03:51 120-12-709/10/09 14:30400 Benzo(a)anthracene ND ug/kg 1 09/19/09 03:51 56-55-309/10/09 14:30400 Benzo(a)pyrene ND ug/kg 1 09/19/09 03:51 50-32-809/10/09 14:30400 Benzo(b)fluoranthene ND ug/kg 1 09/19/09 03:51 205-99-209/10/09 14:30400 Benzo(g,h,i)perylene ND ug/kg 1 09/19/09 03:51 191-24-209/10/09 14:30400 Benzo(k)fluoranthene ND ug/kg 1 09/19/09 03:51 207-08-909/10/09 14:30400 Benzoic Acid ND ug/kg 1 09/19/09 03:51 65-85-009/10/09 14:302000 Benzyl alcohol ND ug/kg 1 09/19/09 03:51 100-51-609/10/09 14:30801 4-Bromophenylphenyl ether ND ug/kg 1 09/19/09 03:51 101-55-309/10/09 14:30400 Butylbenzylphthalate ND ug/kg 1 09/19/09 03:51 85-68-709/10/09 14:30400 4-Chloro-3-methylphenol ND ug/kg 1 09/19/09 03:51 59-50-709/10/09 14:30801 4-Chloroaniline ND ug/kg 1 09/19/09 03:51 106-47-809/10/09 14:302000 bis(2-Chloroethoxy)methane ND ug/kg 1 09/19/09 03:51 111-91-109/10/09 14:30400 bis(2-Chloroethyl) ether ND ug/kg 1 09/19/09 03:51 111-44-409/10/09 14:30400 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/19/09 03:51 108-60-109/10/09 14:30400 2-Chloronaphthalene ND ug/kg 1 09/19/09 03:51 91-58-709/10/09 14:30400 2-Chlorophenol ND ug/kg 1 09/19/09 03:51 95-57-809/10/09 14:30400 4-Chlorophenylphenyl ether ND ug/kg 1 09/19/09 03:51 7005-72-309/10/09 14:30400 Chrysene ND ug/kg 1 09/19/09 03:51 218-01-909/10/09 14:30400 Dibenz(a,h)anthracene ND ug/kg 1 09/19/09 03:51 53-70-309/10/09 14:30400 Dibenzofuran ND ug/kg 1 09/19/09 03:51 132-64-909/10/09 14:30400 1,2-Dichlorobenzene ND ug/kg 1 09/19/09 03:51 95-50-109/10/09 14:30400 1,3-Dichlorobenzene ND ug/kg 1 09/19/09 03:51 541-73-109/10/09 14:30400 1,4-Dichlorobenzene ND ug/kg 1 09/19/09 03:51 106-46-709/10/09 14:30400 3,3'-Dichlorobenzidine ND ug/kg 1 09/19/09 03:51 91-94-109/10/09 14:302000 2,4-Dichlorophenol ND ug/kg 1 09/19/09 03:51 120-83-209/10/09 14:30400 Diethylphthalate ND ug/kg 1 09/19/09 03:51 84-66-209/10/09 14:30400 2,4-Dimethylphenol ND ug/kg 1 09/19/09 03:51 105-67-909/10/09 14:30400 Dimethylphthalate ND ug/kg 1 09/19/09 03:51 131-11-309/10/09 14:30400 Di-n-butylphthalate ND ug/kg 1 09/19/09 03:51 84-74-209/10/09 14:30400 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/09 03:51 534-52-109/10/09 14:30801 2,4-Dinitrophenol ND ug/kg 1 09/19/09 03:51 51-28-509/10/09 14:302000 2,4-Dinitrotoluene ND ug/kg 1 09/19/09 03:51 121-14-209/10/09 14:30400 2,6-Dinitrotoluene ND ug/kg 1 09/19/09 03:51 606-20-209/10/09 14:30400 Di-n-octylphthalate ND ug/kg 1 09/19/09 03:51 117-84-009/10/09 14:30400 1,2-Diphenylhydrazine ND ug/kg 1 09/19/09 03:51 122-66-709/10/09 14:30400 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/09 03:51 117-81-709/10/09 14:30400 Fluoranthene ND ug/kg 1 09/19/09 03:51 206-44-009/10/09 14:30400 Fluorene ND ug/kg 1 09/19/09 03:51 86-73-709/10/09 14:30400 Hexachloro-1,3-butadiene ND ug/kg 1 09/19/09 03:51 87-68-309/10/09 14:30400 Hexachlorobenzene ND ug/kg 1 09/19/09 03:51 118-74-109/10/09 14:30400 Hexachlorocyclopentadiene ND ug/kg 1 09/19/09 03:51 77-47-409/10/09 14:30400 Hexachloroethane ND ug/kg 1 09/19/09 03:51 67-72-109/10/09 14:30400 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 67 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS1-09-09 Lab ID:9252614020 Collected:09/08/09 13:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/09 03:51 193-39-509/10/09 14:30400 Isophorone ND ug/kg 1 09/19/09 03:51 78-59-109/10/09 14:30400 1-Methylnaphthalene ND ug/kg 1 09/19/09 03:51 90-12-009/10/09 14:30400 2-Methylnaphthalene ND ug/kg 1 09/19/09 03:51 91-57-609/10/09 14:30400 2-Methylphenol(o-Cresol)ND ug/kg 1 09/19/09 03:51 95-48-709/10/09 14:30400 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/19/09 03:5109/10/09 14:30400 Naphthalene ND ug/kg 1 09/19/09 03:51 91-20-309/10/09 14:30400 2-Nitroaniline ND ug/kg 1 09/19/09 03:51 88-74-409/10/09 14:302000 3-Nitroaniline ND ug/kg 1 09/19/09 03:51 99-09-209/10/09 14:302000 4-Nitroaniline ND ug/kg 1 09/19/09 03:51 100-01-609/10/09 14:30801 Nitrobenzene ND ug/kg 1 09/19/09 03:51 98-95-309/10/09 14:30400 2-Nitrophenol ND ug/kg 1 09/19/09 03:51 88-75-509/10/09 14:30400 4-Nitrophenol ND ug/kg 1 09/19/09 03:51 100-02-709/10/09 14:302000 N-Nitrosodimethylamine ND ug/kg 1 09/19/09 03:51 62-75-909/10/09 14:30400 N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/09 03:51 621-64-709/10/09 14:30400 N-Nitrosodiphenylamine ND ug/kg 1 09/19/09 03:51 86-30-609/10/09 14:30400 Pentachlorophenol ND ug/kg 1 09/19/09 03:51 87-86-509/10/09 14:302000 Phenanthrene ND ug/kg 1 09/19/09 03:51 85-01-809/10/09 14:30400 Phenol ND ug/kg 1 09/19/09 03:51 108-95-209/10/09 14:30400 Pyrene ND ug/kg 1 09/19/09 03:51 129-00-009/10/09 14:30400 1,2,4-Trichlorobenzene ND ug/kg 1 09/19/09 03:51 120-82-109/10/09 14:30400 2,4,5-Trichlorophenol ND ug/kg 1 09/19/09 03:51 95-95-409/10/09 14:30400 2,4,6-Trichlorophenol ND ug/kg 1 09/19/09 03:51 88-06-209/10/09 14:30400 Nitrobenzene-d5 (S)43 %1 09/19/09 03:51 4165-60-009/10/09 14:3030-150 2-Fluorobiphenyl (S)50 %1 09/19/09 03:51 321-60-809/10/09 14:3046-120 Terphenyl-d14 (S)93 %1 09/19/09 03:51 1718-51-009/10/09 14:3038-108 Phenol-d6 (S)43 %1 09/19/09 03:51 13127-88-309/10/09 14:3035-120 2-Fluorophenol (S)40 %1 09/19/09 03:51 367-12-409/10/09 14:3024-120 2,4,6-Tribromophenol (S)51 %1 09/19/09 03:51 118-79-609/10/09 14:3044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 1 09/11/09 15:30 67-64-198.1 Benzene 6.3 ug/kg 1 09/11/09 15:30 71-43-24.9 Bromobenzene ND ug/kg 1 09/11/09 15:30 108-86-14.9 Bromochloromethane ND ug/kg 1 09/11/09 15:30 74-97-54.9 Bromodichloromethane ND ug/kg 1 09/11/09 15:30 75-27-44.9 Bromoform ND ug/kg 1 09/11/09 15:30 75-25-24.9 Bromomethane ND ug/kg 1 09/11/09 15:30 74-83-99.8 2-Butanone (MEK)ND ug/kg 1 09/11/09 15:30 78-93-398.1 n-Butylbenzene ND ug/kg 1 09/11/09 15:30 104-51-84.9 sec-Butylbenzene ND ug/kg 1 09/11/09 15:30 135-98-84.9 tert-Butylbenzene ND ug/kg 1 09/11/09 15:30 98-06-64.9 Carbon tetrachloride ND ug/kg 1 09/11/09 15:30 56-23-54.9 Chlorobenzene ND ug/kg 1 09/11/09 15:30 108-90-74.9 Chloroethane ND ug/kg 1 09/11/09 15:30 75-00-39.8 Chloroform ND ug/kg 1 09/11/09 15:30 67-66-34.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 68 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS1-09-09 Lab ID:9252614020 Collected:09/08/09 13:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 1 09/11/09 15:30 74-87-39.8 2-Chlorotoluene ND ug/kg 1 09/11/09 15:30 95-49-84.9 4-Chlorotoluene ND ug/kg 1 09/11/09 15:30 106-43-44.9 1,2-Dibromo-3-chloropropane ND ug/kg 1 09/11/09 15:30 96-12-84.9 Dibromochloromethane ND ug/kg 1 09/11/09 15:30 124-48-14.9 1,2-Dibromoethane (EDB)ND ug/kg 1 09/11/09 15:30 106-93-44.9 Dibromomethane ND ug/kg 1 09/11/09 15:30 74-95-34.9 1,2-Dichlorobenzene ND ug/kg 1 09/11/09 15:30 95-50-14.9 1,3-Dichlorobenzene ND ug/kg 1 09/11/09 15:30 541-73-14.9 1,4-Dichlorobenzene ND ug/kg 1 09/11/09 15:30 106-46-74.9 Dichlorodifluoromethane ND ug/kg 1 09/11/09 15:30 75-71-89.8 1,1-Dichloroethane ND ug/kg 1 09/11/09 15:30 75-34-34.9 1,2-Dichloroethane ND ug/kg 1 09/11/09 15:30 107-06-24.9 1,1-Dichloroethene ND ug/kg 1 09/11/09 15:30 75-35-44.9 cis-1,2-Dichloroethene ND ug/kg 1 09/11/09 15:30 156-59-24.9 trans-1,2-Dichloroethene ND ug/kg 1 09/11/09 15:30 156-60-54.9 1,2-Dichloropropane ND ug/kg 1 09/11/09 15:30 78-87-54.9 1,3-Dichloropropane ND ug/kg 1 09/11/09 15:30 142-28-94.9 2,2-Dichloropropane ND ug/kg 1 09/11/09 15:30 594-20-74.9 1,1-Dichloropropene ND ug/kg 1 09/11/09 15:30 563-58-64.9 cis-1,3-Dichloropropene ND ug/kg 1 09/11/09 15:30 10061-01-54.9 trans-1,3-Dichloropropene ND ug/kg 1 09/11/09 15:30 10061-02-64.9 Diisopropyl ether ND ug/kg 1 09/11/09 15:30 108-20-34.9 Ethylbenzene ND ug/kg 1 09/11/09 15:30 100-41-44.9 Hexachloro-1,3-butadiene ND ug/kg 1 09/11/09 15:30 87-68-34.9 2-Hexanone ND ug/kg 1 09/11/09 15:30 591-78-649.1 Isopropylbenzene (Cumene)ND ug/kg 1 09/11/09 15:30 98-82-84.9 p-Isopropyltoluene ND ug/kg 1 09/11/09 15:30 99-87-64.9 Methylene Chloride ND ug/kg 1 09/11/09 15:30 75-09-219.6 4-Methyl-2-pentanone (MIBK)ND ug/kg 1 09/11/09 15:30 108-10-149.1 Methyl-tert-butyl ether ND ug/kg 1 09/11/09 15:30 1634-04-44.9 Naphthalene ND ug/kg 1 09/11/09 15:30 91-20-34.9 n-Propylbenzene ND ug/kg 1 09/11/09 15:30 103-65-14.9 Styrene ND ug/kg 1 09/11/09 15:30 100-42-54.9 1,1,1,2-Tetrachloroethane ND ug/kg 1 09/11/09 15:30 630-20-64.9 1,1,2,2-Tetrachloroethane ND ug/kg 1 09/11/09 15:30 79-34-54.9 Tetrachloroethene ND ug/kg 1 09/11/09 15:30 127-18-44.9 Toluene ND ug/kg 1 09/11/09 15:30 108-88-34.9 1,2,3-Trichlorobenzene ND ug/kg 1 09/11/09 15:30 87-61-64.9 1,2,4-Trichlorobenzene ND ug/kg 1 09/11/09 15:30 120-82-14.9 1,1,1-Trichloroethane ND ug/kg 1 09/11/09 15:30 71-55-64.9 1,1,2-Trichloroethane ND ug/kg 1 09/11/09 15:30 79-00-54.9 Trichloroethene ND ug/kg 1 09/11/09 15:30 79-01-64.9 Trichlorofluoromethane ND ug/kg 1 09/11/09 15:30 75-69-44.9 1,2,3-Trichloropropane ND ug/kg 1 09/11/09 15:30 96-18-44.9 1,2,4-Trimethylbenzene ND ug/kg 1 09/11/09 15:30 95-63-64.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 69 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS1-09-09 Lab ID:9252614020 Collected:09/08/09 13:15 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene ND ug/kg 1 09/11/09 15:30 108-67-84.9 Vinyl acetate ND ug/kg 1 09/11/09 15:30 108-05-449.1 Vinyl chloride ND ug/kg 1 09/11/09 15:30 75-01-49.8 Xylene (Total)ND ug/kg 1 09/11/09 15:30 1330-20-79.8 m&p-Xylene ND ug/kg 1 09/11/09 15:30 1330-20-79.8 o-Xylene ND ug/kg 1 09/11/09 15:30 95-47-64.9 Dibromofluoromethane (S)99 %1 09/11/09 15:30 1868-53-779-116 Toluene-d8 (S)99 %1 09/11/09 15:30 2037-26-588-110 4-Bromofluorobenzene (S)97 %1 09/11/09 15:30 460-00-474-115 1,2-Dichloroethane-d4 (S)96 %1 09/11/09 15:30 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 17.6 %1 09/09/09 13:470.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 70 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS2-09-09 Lab ID:9252614021 Collected:09/08/09 13:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Acenaphthene ND ug/kg 1 09/19/09 04:13 83-32-909/10/09 14:30355 Acenaphthylene ND ug/kg 1 09/19/09 04:13 208-96-809/10/09 14:30355 Aniline ND ug/kg 1 09/19/09 04:13 62-53-309/10/09 14:30355 Anthracene ND ug/kg 1 09/19/09 04:13 120-12-709/10/09 14:30355 Benzo(a)anthracene ND ug/kg 1 09/19/09 04:13 56-55-309/10/09 14:30355 Benzo(a)pyrene ND ug/kg 1 09/19/09 04:13 50-32-809/10/09 14:30355 Benzo(b)fluoranthene ND ug/kg 1 09/19/09 04:13 205-99-209/10/09 14:30355 Benzo(g,h,i)perylene ND ug/kg 1 09/19/09 04:13 191-24-209/10/09 14:30355 Benzo(k)fluoranthene ND ug/kg 1 09/19/09 04:13 207-08-909/10/09 14:30355 Benzoic Acid ND ug/kg 1 09/19/09 04:13 65-85-009/10/09 14:301770 Benzyl alcohol ND ug/kg 1 09/19/09 04:13 100-51-609/10/09 14:30709 4-Bromophenylphenyl ether ND ug/kg 1 09/19/09 04:13 101-55-309/10/09 14:30355 Butylbenzylphthalate ND ug/kg 1 09/19/09 04:13 85-68-709/10/09 14:30355 4-Chloro-3-methylphenol ND ug/kg 1 09/19/09 04:13 59-50-709/10/09 14:30709 4-Chloroaniline ND ug/kg 1 09/19/09 04:13 106-47-809/10/09 14:301770 bis(2-Chloroethoxy)methane ND ug/kg 1 09/19/09 04:13 111-91-109/10/09 14:30355 bis(2-Chloroethyl) ether ND ug/kg 1 09/19/09 04:13 111-44-409/10/09 14:30355 bis(2-Chloroisopropyl) ether ND ug/kg 1 09/19/09 04:13 108-60-109/10/09 14:30355 2-Chloronaphthalene ND ug/kg 1 09/19/09 04:13 91-58-709/10/09 14:30355 2-Chlorophenol ND ug/kg 1 09/19/09 04:13 95-57-809/10/09 14:30355 4-Chlorophenylphenyl ether ND ug/kg 1 09/19/09 04:13 7005-72-309/10/09 14:30355 Chrysene ND ug/kg 1 09/19/09 04:13 218-01-909/10/09 14:30355 Dibenz(a,h)anthracene ND ug/kg 1 09/19/09 04:13 53-70-309/10/09 14:30355 Dibenzofuran ND ug/kg 1 09/19/09 04:13 132-64-909/10/09 14:30355 1,2-Dichlorobenzene ND ug/kg 1 09/19/09 04:13 95-50-109/10/09 14:30355 1,3-Dichlorobenzene ND ug/kg 1 09/19/09 04:13 541-73-109/10/09 14:30355 1,4-Dichlorobenzene ND ug/kg 1 09/19/09 04:13 106-46-709/10/09 14:30355 3,3'-Dichlorobenzidine ND ug/kg 1 09/19/09 04:13 91-94-109/10/09 14:301770 2,4-Dichlorophenol ND ug/kg 1 09/19/09 04:13 120-83-209/10/09 14:30355 Diethylphthalate ND ug/kg 1 09/19/09 04:13 84-66-209/10/09 14:30355 2,4-Dimethylphenol ND ug/kg 1 09/19/09 04:13 105-67-909/10/09 14:30355 Dimethylphthalate ND ug/kg 1 09/19/09 04:13 131-11-309/10/09 14:30355 Di-n-butylphthalate ND ug/kg 1 09/19/09 04:13 84-74-209/10/09 14:30355 4,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/09 04:13 534-52-109/10/09 14:30709 2,4-Dinitrophenol ND ug/kg 1 09/19/09 04:13 51-28-509/10/09 14:301770 2,4-Dinitrotoluene ND ug/kg 1 09/19/09 04:13 121-14-209/10/09 14:30355 2,6-Dinitrotoluene ND ug/kg 1 09/19/09 04:13 606-20-209/10/09 14:30355 Di-n-octylphthalate ND ug/kg 1 09/19/09 04:13 117-84-009/10/09 14:30355 1,2-Diphenylhydrazine ND ug/kg 1 09/19/09 04:13 122-66-709/10/09 14:30355 bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/09 04:13 117-81-709/10/09 14:30355 Fluoranthene ND ug/kg 1 09/19/09 04:13 206-44-009/10/09 14:30355 Fluorene ND ug/kg 1 09/19/09 04:13 86-73-709/10/09 14:30355 Hexachloro-1,3-butadiene ND ug/kg 1 09/19/09 04:13 87-68-309/10/09 14:30355 Hexachlorobenzene ND ug/kg 1 09/19/09 04:13 118-74-109/10/09 14:30355 Hexachlorocyclopentadiene ND ug/kg 1 09/19/09 04:13 77-47-409/10/09 14:30355 Hexachloroethane ND ug/kg 1 09/19/09 04:13 67-72-109/10/09 14:30355 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 71 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS2-09-09 Lab ID:9252614021 Collected:09/08/09 13:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546 Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/09 04:13 193-39-509/10/09 14:30355 Isophorone ND ug/kg 1 09/19/09 04:13 78-59-109/10/09 14:30355 1-Methylnaphthalene ND ug/kg 1 09/19/09 04:13 90-12-009/10/09 14:30355 2-Methylnaphthalene ND ug/kg 1 09/19/09 04:13 91-57-609/10/09 14:30355 2-Methylphenol(o-Cresol)ND ug/kg 1 09/19/09 04:13 95-48-709/10/09 14:30355 3&4-Methylphenol(m&p Cresol)ND ug/kg 1 09/19/09 04:1309/10/09 14:30355 Naphthalene ND ug/kg 1 09/19/09 04:13 91-20-309/10/09 14:30355 2-Nitroaniline ND ug/kg 1 09/19/09 04:13 88-74-409/10/09 14:301770 3-Nitroaniline ND ug/kg 1 09/19/09 04:13 99-09-209/10/09 14:301770 4-Nitroaniline ND ug/kg 1 09/19/09 04:13 100-01-609/10/09 14:30709 Nitrobenzene ND ug/kg 1 09/19/09 04:13 98-95-309/10/09 14:30355 2-Nitrophenol ND ug/kg 1 09/19/09 04:13 88-75-509/10/09 14:30355 4-Nitrophenol ND ug/kg 1 09/19/09 04:13 100-02-709/10/09 14:301770 N-Nitrosodimethylamine ND ug/kg 1 09/19/09 04:13 62-75-909/10/09 14:30355 N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/09 04:13 621-64-709/10/09 14:30355 N-Nitrosodiphenylamine ND ug/kg 1 09/19/09 04:13 86-30-609/10/09 14:30355 Pentachlorophenol ND ug/kg 1 09/19/09 04:13 87-86-509/10/09 14:301770 Phenanthrene ND ug/kg 1 09/19/09 04:13 85-01-809/10/09 14:30355 Phenol ND ug/kg 1 09/19/09 04:13 108-95-209/10/09 14:30355 Pyrene ND ug/kg 1 09/19/09 04:13 129-00-009/10/09 14:30355 1,2,4-Trichlorobenzene ND ug/kg 1 09/19/09 04:13 120-82-109/10/09 14:30355 2,4,5-Trichlorophenol ND ug/kg 1 09/19/09 04:13 95-95-409/10/09 14:30355 2,4,6-Trichlorophenol ND ug/kg 1 09/19/09 04:13 88-06-209/10/09 14:30355 Nitrobenzene-d5 (S)32 %1 09/19/09 04:13 4165-60-009/10/09 14:3030-150 2-Fluorobiphenyl (S)49 %1 09/19/09 04:13 321-60-809/10/09 14:3046-120 Terphenyl-d14 (S)49 %1 09/19/09 04:13 1718-51-009/10/09 14:3038-108 Phenol-d6 (S)33 %1 09/19/09 04:13 13127-88-3 1g09/10/09 14:3035-120 2-Fluorophenol (S)34 %1 09/19/09 04:13 367-12-409/10/09 14:3024-120 2,4,6-Tribromophenol (S)44 %1 09/19/09 04:13 118-79-609/10/09 14:3044-136 8260/5035A Volatile Organics Analytical Method: EPA 8260 Acetone ND ug/kg 50 09/14/09 13:17 67-64-14290 Benzene ND ug/kg 50 09/14/09 13:17 71-43-2215 Bromobenzene ND ug/kg 50 09/14/09 13:17 108-86-1215 Bromochloromethane ND ug/kg 50 09/14/09 13:17 74-97-5215 Bromodichloromethane ND ug/kg 50 09/14/09 13:17 75-27-4215 Bromoform ND ug/kg 50 09/14/09 13:17 75-25-2215 Bromomethane ND ug/kg 50 09/14/09 13:17 74-83-9429 2-Butanone (MEK)ND ug/kg 50 09/14/09 13:17 78-93-34290 n-Butylbenzene ND ug/kg 50 09/14/09 13:17 104-51-8215 sec-Butylbenzene ND ug/kg 50 09/14/09 13:17 135-98-8215 tert-Butylbenzene ND ug/kg 50 09/14/09 13:17 98-06-6215 Carbon tetrachloride ND ug/kg 50 09/14/09 13:17 56-23-5215 Chlorobenzene ND ug/kg 50 09/14/09 13:17 108-90-7215 Chloroethane ND ug/kg 50 09/14/09 13:17 75-00-3429 Chloroform ND ug/kg 50 09/14/09 13:17 67-66-3215 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 72 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS2-09-09 Lab ID:9252614021 Collected:09/08/09 13:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 Chloromethane ND ug/kg 50 09/14/09 13:17 74-87-3429 2-Chlorotoluene ND ug/kg 50 09/14/09 13:17 95-49-8215 4-Chlorotoluene ND ug/kg 50 09/14/09 13:17 106-43-4215 1,2-Dibromo-3-chloropropane ND ug/kg 50 09/14/09 13:17 96-12-8215 Dibromochloromethane ND ug/kg 50 09/14/09 13:17 124-48-1215 1,2-Dibromoethane (EDB)ND ug/kg 50 09/14/09 13:17 106-93-4215 Dibromomethane ND ug/kg 50 09/14/09 13:17 74-95-3215 1,2-Dichlorobenzene ND ug/kg 50 09/14/09 13:17 95-50-1215 1,3-Dichlorobenzene ND ug/kg 50 09/14/09 13:17 541-73-1215 1,4-Dichlorobenzene ND ug/kg 50 09/14/09 13:17 106-46-7215 Dichlorodifluoromethane ND ug/kg 50 09/14/09 13:17 75-71-8429 1,1-Dichloroethane ND ug/kg 50 09/14/09 13:17 75-34-3215 1,2-Dichloroethane ND ug/kg 50 09/14/09 13:17 107-06-2215 1,1-Dichloroethene ND ug/kg 50 09/14/09 13:17 75-35-4215 cis-1,2-Dichloroethene ND ug/kg 50 09/14/09 13:17 156-59-2215 trans-1,2-Dichloroethene ND ug/kg 50 09/14/09 13:17 156-60-5215 1,2-Dichloropropane ND ug/kg 50 09/14/09 13:17 78-87-5215 1,3-Dichloropropane ND ug/kg 50 09/14/09 13:17 142-28-9215 2,2-Dichloropropane ND ug/kg 50 09/14/09 13:17 594-20-7215 1,1-Dichloropropene ND ug/kg 50 09/14/09 13:17 563-58-6215 cis-1,3-Dichloropropene ND ug/kg 50 09/14/09 13:17 10061-01-5215 trans-1,3-Dichloropropene ND ug/kg 50 09/14/09 13:17 10061-02-6215 Diisopropyl ether ND ug/kg 50 09/14/09 13:17 108-20-3215 Ethylbenzene ND ug/kg 50 09/14/09 13:17 100-41-4215 Hexachloro-1,3-butadiene ND ug/kg 50 09/14/09 13:17 87-68-3215 2-Hexanone ND ug/kg 50 09/14/09 13:17 591-78-62150 Isopropylbenzene (Cumene)ND ug/kg 50 09/14/09 13:17 98-82-8215 p-Isopropyltoluene ND ug/kg 50 09/14/09 13:17 99-87-6215 Methylene Chloride ND ug/kg 50 09/14/09 13:17 75-09-2859 4-Methyl-2-pentanone (MIBK)ND ug/kg 50 09/14/09 13:17 108-10-12150 Methyl-tert-butyl ether ND ug/kg 50 09/14/09 13:17 1634-04-4215 Naphthalene ND ug/kg 50 09/14/09 13:17 91-20-3215 n-Propylbenzene ND ug/kg 50 09/14/09 13:17 103-65-1215 Styrene ND ug/kg 50 09/14/09 13:17 100-42-5215 1,1,1,2-Tetrachloroethane ND ug/kg 50 09/14/09 13:17 630-20-6215 1,1,2,2-Tetrachloroethane ND ug/kg 50 09/14/09 13:17 79-34-5215 Tetrachloroethene ND ug/kg 50 09/14/09 13:17 127-18-4215 Toluene ND ug/kg 50 09/14/09 13:17 108-88-3215 1,2,3-Trichlorobenzene ND ug/kg 50 09/14/09 13:17 87-61-6215 1,2,4-Trichlorobenzene ND ug/kg 50 09/14/09 13:17 120-82-1215 1,1,1-Trichloroethane ND ug/kg 50 09/14/09 13:17 71-55-6215 1,1,2-Trichloroethane ND ug/kg 50 09/14/09 13:17 79-00-5215 Trichloroethene ND ug/kg 50 09/14/09 13:17 79-01-6215 Trichlorofluoromethane ND ug/kg 50 09/14/09 13:17 75-69-4215 1,2,3-Trichloropropane ND ug/kg 50 09/14/09 13:17 96-18-4215 1,2,4-Trimethylbenzene ND ug/kg 50 09/14/09 13:17 95-63-6215 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 73 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TW2-SS2-09-09 Lab ID:9252614021 Collected:09/08/09 13:20 Received:09/08/09 14:35 Matrix:Solid Results reported on a "dry-weight" basis Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260/5035A Volatile Organics Analytical Method: EPA 8260 1,3,5-Trimethylbenzene ND ug/kg 50 09/14/09 13:17 108-67-8215 Vinyl acetate ND ug/kg 50 09/14/09 13:17 108-05-42150 Vinyl chloride ND ug/kg 50 09/14/09 13:17 75-01-4429 Xylene (Total)ND ug/kg 50 09/14/09 13:17 1330-20-7429 m&p-Xylene ND ug/kg 50 09/14/09 13:17 1330-20-7429 o-Xylene ND ug/kg 50 09/14/09 13:17 95-47-6215 Dibromofluoromethane (S)96 %50 09/14/09 13:17 1868-53-7 D379-116 Toluene-d8 (S)102 %50 09/14/09 13:17 2037-26-588-110 4-Bromofluorobenzene (S)98 %50 09/14/09 13:17 460-00-474-115 1,2-Dichloroethane-d4 (S)96 %50 09/14/09 13:17 17060-07-069-121 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 7.0 %1 09/09/09 13:470.10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 74 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TRIP BLANK 1-09- 09 Lab ID:9252614022 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 02:14 67-64-125.0 Benzene ND ug/L 1 09/13/09 02:14 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 02:14 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 02:14 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 02:14 75-27-41.0 Bromoform ND ug/L 1 09/13/09 02:14 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 02:14 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 02:14 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 02:14 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 02:14 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 02:14 75-00-31.0 Chloroform ND ug/L 1 09/13/09 02:14 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 02:14 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 02:14 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 02:14 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 02:14 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 02:14 124-48-11.0 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 02:14 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 02:14 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 02:14 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 02:14 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 02:14 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 02:14 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 02:14 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 02:14 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 02:14 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 02:14 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 02:14 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 02:14 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 02:14 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 02:14 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 02:14 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 02:14 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 02:14 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 02:14 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 02:14 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 02:14 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 02:14 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 02:14 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 02:14 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 02:14 108-10-15.0 Methyl-tert-butyl ether ND ug/L 1 09/13/09 02:14 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 02:14 91-20-31.0 Styrene ND ug/L 1 09/13/09 02:14 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 02:14 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 02:14 79-34-51.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 75 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TRIP BLANK 1-09- 09 Lab ID:9252614022 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1 09/13/09 02:14 127-18-41.0 Toluene ND ug/L 1 09/13/09 02:14 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 02:14 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 02:14 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 02:14 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 02:14 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 02:14 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 02:14 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 02:14 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 02:14 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 02:14 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 02:14 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 02:14 95-47-61.0 4-Bromofluorobenzene (S)98 %1 09/13/09 02:14 460-00-487-109 Dibromofluoromethane (S)100 %1 09/13/09 02:14 1868-53-785-115 1,2-Dichloroethane-d4 (S)100 %1 09/13/09 02:14 17060-07-079-120 Toluene-d8 (S)100 %1 09/13/09 02:14 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 76 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TRIP BLANK 2-09- 09 Lab ID:9252614023 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 02:33 67-64-125.0 Benzene ND ug/L 1 09/13/09 02:33 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 02:33 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 02:33 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 02:33 75-27-41.0 Bromoform ND ug/L 1 09/13/09 02:33 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 02:33 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 02:33 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 02:33 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 02:33 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 02:33 75-00-31.0 Chloroform ND ug/L 1 09/13/09 02:33 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 02:33 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 02:33 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 02:33 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 02:33 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 02:33 124-48-11.0 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 02:33 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 02:33 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 02:33 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 02:33 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 02:33 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 02:33 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 02:33 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 02:33 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 02:33 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 02:33 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 02:33 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 02:33 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 02:33 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 02:33 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 02:33 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 02:33 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 02:33 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 02:33 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 02:33 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 02:33 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 02:33 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 02:33 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 02:33 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 02:33 108-10-15.0 Methyl-tert-butyl ether ND ug/L 1 09/13/09 02:33 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 02:33 91-20-31.0 Styrene ND ug/L 1 09/13/09 02:33 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 02:33 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 02:33 79-34-51.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 77 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -TRIP BLANK 2-09- 09 Lab ID:9252614023 Collected:09/08/09 00:00 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Tetrachloroethene ND ug/L 1 09/13/09 02:33 127-18-41.0 Toluene ND ug/L 1 09/13/09 02:33 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 02:33 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 02:33 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 02:33 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 02:33 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 02:33 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 02:33 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 02:33 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 02:33 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 02:33 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 02:33 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 02:33 95-47-61.0 4-Bromofluorobenzene (S)99 %1 09/13/09 02:33 460-00-487-109 Dibromofluoromethane (S)99 %1 09/13/09 02:33 1868-53-785-115 1,2-Dichloroethane-d4 (S)99 %1 09/13/09 02:33 17060-07-079-120 Toluene-d8 (S)99 %1 09/13/09 02:33 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 78 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 1- 09-09 Lab ID:9252614024 Collected:09/08/09 09:23 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 01:10 83-32-909/15/09 09:0010.9 Acenaphthylene ND ug/L 1 09/18/09 01:10 208-96-809/15/09 09:0010.9 Aniline ND ug/L 1 09/18/09 01:10 62-53-309/15/09 09:0010.9 Anthracene ND ug/L 1 09/18/09 01:10 120-12-709/15/09 09:0010.9 Benzo(a)anthracene ND ug/L 1 09/18/09 01:10 56-55-309/15/09 09:0010.9 Benzo(a)pyrene ND ug/L 1 09/18/09 01:10 50-32-809/15/09 09:0010.9 Benzo(b)fluoranthene ND ug/L 1 09/18/09 01:10 205-99-209/15/09 09:0010.9 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 01:10 191-24-209/15/09 09:0010.9 Benzo(k)fluoranthene ND ug/L 1 09/18/09 01:10 207-08-909/15/09 09:0010.9 Benzoic Acid ND ug/L 1 09/18/09 01:10 65-85-009/15/09 09:0054.3 Benzyl alcohol ND ug/L 1 09/18/09 01:10 100-51-609/15/09 09:0021.7 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 01:10 101-55-309/15/09 09:0010.9 Butylbenzylphthalate ND ug/L 1 09/18/09 01:10 85-68-709/15/09 09:0010.9 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 01:10 59-50-709/15/09 09:0021.7 4-Chloroaniline ND ug/L 1 09/18/09 01:10 106-47-809/15/09 09:0054.3 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 01:10 111-91-109/15/09 09:0010.9 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 01:10 111-44-409/15/09 09:0010.9 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 01:10 108-60-109/15/09 09:0010.9 2-Chloronaphthalene ND ug/L 1 09/18/09 01:10 91-58-709/15/09 09:0010.9 2-Chlorophenol ND ug/L 1 09/18/09 01:10 95-57-809/15/09 09:0010.9 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 01:10 7005-72-309/15/09 09:0010.9 Chrysene ND ug/L 1 09/18/09 01:10 218-01-909/15/09 09:0010.9 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 01:10 53-70-309/15/09 09:0010.9 Dibenzofuran ND ug/L 1 09/18/09 01:10 132-64-909/15/09 09:0010.9 1,2-Dichlorobenzene ND ug/L 1 09/18/09 01:10 95-50-109/15/09 09:0010.9 1,3-Dichlorobenzene ND ug/L 1 09/18/09 01:10 541-73-109/15/09 09:0010.9 1,4-Dichlorobenzene ND ug/L 1 09/18/09 01:10 106-46-709/15/09 09:0010.9 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 01:10 91-94-109/15/09 09:0054.3 2,4-Dichlorophenol ND ug/L 1 09/18/09 01:10 120-83-209/15/09 09:0010.9 Diethylphthalate ND ug/L 1 09/18/09 01:10 84-66-209/15/09 09:0010.9 2,4-Dimethylphenol ND ug/L 1 09/18/09 01:10 105-67-909/15/09 09:0010.9 Dimethylphthalate ND ug/L 1 09/18/09 01:10 131-11-309/15/09 09:0010.9 Di-n-butylphthalate ND ug/L 1 09/18/09 01:10 84-74-209/15/09 09:0010.9 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 01:10 534-52-109/15/09 09:0021.7 2,4-Dinitrophenol ND ug/L 1 09/18/09 01:10 51-28-509/15/09 09:0054.3 2,4-Dinitrotoluene ND ug/L 1 09/18/09 01:10 121-14-209/15/09 09:0010.9 2,6-Dinitrotoluene ND ug/L 1 09/18/09 01:10 606-20-209/15/09 09:0010.9 Di-n-octylphthalate ND ug/L 1 09/18/09 01:10 117-84-009/15/09 09:0010.9 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 01:10 122-66-709/15/09 09:0010.9 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 01:10 117-81-709/15/09 09:0010.9 Fluoranthene ND ug/L 1 09/18/09 01:10 206-44-009/15/09 09:0010.9 Fluorene ND ug/L 1 09/18/09 01:10 86-73-709/15/09 09:0010.9 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 01:10 87-68-309/15/09 09:0010.9 Hexachlorobenzene ND ug/L 1 09/18/09 01:10 118-74-109/15/09 09:0010.9 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 01:10 77-47-409/15/09 09:0010.9 Hexachloroethane ND ug/L 1 09/18/09 01:10 67-72-109/15/09 09:0010.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 79 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 1- 09-09 Lab ID:9252614024 Collected:09/08/09 09:23 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 01:10 193-39-509/15/09 09:0010.9 Isophorone ND ug/L 1 09/18/09 01:10 78-59-109/15/09 09:0010.9 1-Methylnaphthalene ND ug/L 1 09/18/09 01:10 90-12-009/15/09 09:0010.9 2-Methylnaphthalene ND ug/L 1 09/18/09 01:10 91-57-609/15/09 09:0010.9 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 01:10 95-48-709/15/09 09:0010.9 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 01:1009/15/09 09:0010.9 Naphthalene ND ug/L 1 09/18/09 01:10 91-20-309/15/09 09:0010.9 2-Nitroaniline ND ug/L 1 09/18/09 01:10 88-74-409/15/09 09:0054.3 3-Nitroaniline ND ug/L 1 09/18/09 01:10 99-09-209/15/09 09:0054.3 4-Nitroaniline ND ug/L 1 09/18/09 01:10 100-01-609/15/09 09:0054.3 Nitrobenzene ND ug/L 1 09/18/09 01:10 98-95-309/15/09 09:0010.9 2-Nitrophenol ND ug/L 1 09/18/09 01:10 88-75-509/15/09 09:0010.9 4-Nitrophenol ND ug/L 1 09/18/09 01:10 100-02-709/15/09 09:0054.3 N-Nitrosodimethylamine ND ug/L 1 09/18/09 01:10 62-75-909/15/09 09:0010.9 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 01:10 621-64-709/15/09 09:0010.9 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 01:10 86-30-609/15/09 09:0010.9 Pentachlorophenol ND ug/L 1 09/18/09 01:10 87-86-509/15/09 09:0054.3 Phenanthrene ND ug/L 1 09/18/09 01:10 85-01-809/15/09 09:0010.9 Phenol ND ug/L 1 09/18/09 01:10 108-95-209/15/09 09:0010.9 Pyrene ND ug/L 1 09/18/09 01:10 129-00-009/15/09 09:0010.9 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 01:10 120-82-109/15/09 09:0010.9 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 01:10 95-95-409/15/09 09:0010.9 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 01:10 88-06-209/15/09 09:0010.9 Nitrobenzene-d5 (S)47 %1 09/18/09 01:10 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)55 %1 09/18/09 01:10 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)80 %1 09/18/09 01:10 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)27 %1 09/18/09 01:10 13127-88-309/15/09 09:0025-150 2-Fluorophenol (S)30 %1 09/18/09 01:10 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)50 %1 09/18/09 01:10 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 03:31 67-64-125.0 Benzene ND ug/L 1 09/13/09 03:31 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 03:31 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 03:31 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 03:31 75-27-41.0 Bromoform ND ug/L 1 09/13/09 03:31 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 03:31 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 03:31 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 03:31 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 03:31 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 03:31 75-00-31.0 Chloroform ND ug/L 1 09/13/09 03:31 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 03:31 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 03:31 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 03:31 106-43-41.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 80 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 1- 09-09 Lab ID:9252614024 Collected:09/08/09 09:23 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 03:31 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 03:31 124-48-11.0 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 03:31 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 03:31 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 03:31 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 03:31 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 03:31 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 03:31 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 03:31 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 03:31 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 03:31 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 03:31 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 03:31 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 03:31 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 03:31 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 03:31 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 03:31 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 03:31 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 03:31 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 03:31 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 03:31 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 03:31 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 03:31 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 03:31 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 03:31 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 03:31 108-10-15.0 Methyl-tert-butyl ether ND ug/L 1 09/13/09 03:31 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 03:31 91-20-31.0 Styrene ND ug/L 1 09/13/09 03:31 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 03:31 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 03:31 79-34-51.0 Tetrachloroethene ND ug/L 1 09/13/09 03:31 127-18-41.0 Toluene ND ug/L 1 09/13/09 03:31 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 03:31 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 03:31 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 03:31 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 03:31 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 03:31 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 03:31 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 03:31 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 03:31 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 03:31 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 03:31 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 03:31 95-47-61.0 4-Bromofluorobenzene (S)99 %1 09/13/09 03:31 460-00-487-109 Dibromofluoromethane (S)100 %1 09/13/09 03:31 1868-53-785-115 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 81 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 1- 09-09 Lab ID:9252614024 Collected:09/08/09 09:23 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dichloroethane-d4 (S)99 %1 09/13/09 03:31 17060-07-079-120 Toluene-d8 (S)100 %1 09/13/09 03:31 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 82 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 2- 09-09 Lab ID:9252614025 Collected:09/08/09 12:25 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 01:32 83-32-909/15/09 09:0011.1 Acenaphthylene ND ug/L 1 09/18/09 01:32 208-96-809/15/09 09:0011.1 Aniline ND ug/L 1 09/18/09 01:32 62-53-309/15/09 09:0011.1 Anthracene ND ug/L 1 09/18/09 01:32 120-12-709/15/09 09:0011.1 Benzo(a)anthracene ND ug/L 1 09/18/09 01:32 56-55-309/15/09 09:0011.1 Benzo(a)pyrene ND ug/L 1 09/18/09 01:32 50-32-809/15/09 09:0011.1 Benzo(b)fluoranthene ND ug/L 1 09/18/09 01:32 205-99-209/15/09 09:0011.1 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 01:32 191-24-209/15/09 09:0011.1 Benzo(k)fluoranthene ND ug/L 1 09/18/09 01:32 207-08-909/15/09 09:0011.1 Benzoic Acid ND ug/L 1 09/18/09 01:32 65-85-009/15/09 09:0055.6 Benzyl alcohol ND ug/L 1 09/18/09 01:32 100-51-609/15/09 09:0022.2 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 01:32 101-55-309/15/09 09:0011.1 Butylbenzylphthalate ND ug/L 1 09/18/09 01:32 85-68-709/15/09 09:0011.1 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 01:32 59-50-709/15/09 09:0022.2 4-Chloroaniline ND ug/L 1 09/18/09 01:32 106-47-809/15/09 09:0055.6 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 01:32 111-91-109/15/09 09:0011.1 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 01:32 111-44-409/15/09 09:0011.1 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 01:32 108-60-109/15/09 09:0011.1 2-Chloronaphthalene ND ug/L 1 09/18/09 01:32 91-58-709/15/09 09:0011.1 2-Chlorophenol ND ug/L 1 09/18/09 01:32 95-57-809/15/09 09:0011.1 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 01:32 7005-72-309/15/09 09:0011.1 Chrysene ND ug/L 1 09/18/09 01:32 218-01-909/15/09 09:0011.1 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 01:32 53-70-309/15/09 09:0011.1 Dibenzofuran ND ug/L 1 09/18/09 01:32 132-64-909/15/09 09:0011.1 1,2-Dichlorobenzene ND ug/L 1 09/18/09 01:32 95-50-109/15/09 09:0011.1 1,3-Dichlorobenzene ND ug/L 1 09/18/09 01:32 541-73-109/15/09 09:0011.1 1,4-Dichlorobenzene ND ug/L 1 09/18/09 01:32 106-46-709/15/09 09:0011.1 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 01:32 91-94-109/15/09 09:0055.6 2,4-Dichlorophenol ND ug/L 1 09/18/09 01:32 120-83-209/15/09 09:0011.1 Diethylphthalate ND ug/L 1 09/18/09 01:32 84-66-209/15/09 09:0011.1 2,4-Dimethylphenol ND ug/L 1 09/18/09 01:32 105-67-909/15/09 09:0011.1 Dimethylphthalate ND ug/L 1 09/18/09 01:32 131-11-309/15/09 09:0011.1 Di-n-butylphthalate ND ug/L 1 09/18/09 01:32 84-74-209/15/09 09:0011.1 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 01:32 534-52-109/15/09 09:0022.2 2,4-Dinitrophenol ND ug/L 1 09/18/09 01:32 51-28-509/15/09 09:0055.6 2,4-Dinitrotoluene ND ug/L 1 09/18/09 01:32 121-14-209/15/09 09:0011.1 2,6-Dinitrotoluene ND ug/L 1 09/18/09 01:32 606-20-209/15/09 09:0011.1 Di-n-octylphthalate ND ug/L 1 09/18/09 01:32 117-84-009/15/09 09:0011.1 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 01:32 122-66-709/15/09 09:0011.1 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 01:32 117-81-709/15/09 09:0011.1 Fluoranthene ND ug/L 1 09/18/09 01:32 206-44-009/15/09 09:0011.1 Fluorene ND ug/L 1 09/18/09 01:32 86-73-709/15/09 09:0011.1 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 01:32 87-68-309/15/09 09:0011.1 Hexachlorobenzene ND ug/L 1 09/18/09 01:32 118-74-109/15/09 09:0011.1 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 01:32 77-47-409/15/09 09:0011.1 Hexachloroethane ND ug/L 1 09/18/09 01:32 67-72-109/15/09 09:0011.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 83 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 2- 09-09 Lab ID:9252614025 Collected:09/08/09 12:25 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 01:32 193-39-509/15/09 09:0011.1 Isophorone ND ug/L 1 09/18/09 01:32 78-59-109/15/09 09:0011.1 1-Methylnaphthalene ND ug/L 1 09/18/09 01:32 90-12-009/15/09 09:0011.1 2-Methylnaphthalene ND ug/L 1 09/18/09 01:32 91-57-609/15/09 09:0011.1 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 01:32 95-48-709/15/09 09:0011.1 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 01:3209/15/09 09:0011.1 Naphthalene ND ug/L 1 09/18/09 01:32 91-20-309/15/09 09:0011.1 2-Nitroaniline ND ug/L 1 09/18/09 01:32 88-74-409/15/09 09:0055.6 3-Nitroaniline ND ug/L 1 09/18/09 01:32 99-09-209/15/09 09:0055.6 4-Nitroaniline ND ug/L 1 09/18/09 01:32 100-01-609/15/09 09:0055.6 Nitrobenzene ND ug/L 1 09/18/09 01:32 98-95-309/15/09 09:0011.1 2-Nitrophenol ND ug/L 1 09/18/09 01:32 88-75-509/15/09 09:0011.1 4-Nitrophenol ND ug/L 1 09/18/09 01:32 100-02-709/15/09 09:0055.6 N-Nitrosodimethylamine ND ug/L 1 09/18/09 01:32 62-75-909/15/09 09:0011.1 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 01:32 621-64-709/15/09 09:0011.1 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 01:32 86-30-609/15/09 09:0011.1 Pentachlorophenol ND ug/L 1 09/18/09 01:32 87-86-509/15/09 09:0055.6 Phenanthrene ND ug/L 1 09/18/09 01:32 85-01-809/15/09 09:0011.1 Phenol ND ug/L 1 09/18/09 01:32 108-95-209/15/09 09:0011.1 Pyrene ND ug/L 1 09/18/09 01:32 129-00-009/15/09 09:0011.1 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 01:32 120-82-109/15/09 09:0011.1 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 01:32 95-95-409/15/09 09:0011.1 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 01:32 88-06-209/15/09 09:0011.1 Nitrobenzene-d5 (S)47 %1 09/18/09 01:32 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)51 %1 09/18/09 01:32 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)75 %1 09/18/09 01:32 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)26 %1 09/18/09 01:32 13127-88-309/15/09 09:0025-150 2-Fluorophenol (S)31 %1 09/18/09 01:32 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)52 %1 09/18/09 01:32 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 03:50 67-64-125.0 Benzene ND ug/L 1 09/13/09 03:50 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 03:50 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 03:50 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 03:50 75-27-41.0 Bromoform ND ug/L 1 09/13/09 03:50 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 03:50 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 03:50 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 03:50 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 03:50 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 03:50 75-00-31.0 Chloroform ND ug/L 1 09/13/09 03:50 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 03:50 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 03:50 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 03:50 106-43-41.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 84 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 2- 09-09 Lab ID:9252614025 Collected:09/08/09 12:25 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 03:50 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 03:50 124-48-11.0 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 03:50 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 03:50 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 03:50 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 03:50 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 03:50 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 03:50 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 03:50 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 03:50 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 03:50 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 03:50 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 03:50 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 03:50 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 03:50 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 03:50 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 03:50 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 03:50 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 03:50 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 03:50 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 03:50 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 03:50 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 03:50 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 03:50 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 03:50 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 03:50 108-10-15.0 Methyl-tert-butyl ether ND ug/L 1 09/13/09 03:50 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 03:50 91-20-31.0 Styrene ND ug/L 1 09/13/09 03:50 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 03:50 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 03:50 79-34-51.0 Tetrachloroethene ND ug/L 1 09/13/09 03:50 127-18-41.0 Toluene ND ug/L 1 09/13/09 03:50 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 03:50 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 03:50 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 03:50 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 03:50 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 03:50 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 03:50 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 03:50 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 03:50 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 03:50 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 03:50 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 03:50 95-47-61.0 4-Bromofluorobenzene (S)98 %1 09/13/09 03:50 460-00-487-109 Dibromofluoromethane (S)101 %1 09/13/09 03:50 1868-53-785-115 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 85 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR -EQUIP RINSATE 2- 09-09 Lab ID:9252614025 Collected:09/08/09 12:25 Received:09/08/09 14:35 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dichloroethane-d4 (S)100 %1 09/13/09 03:50 17060-07-079-120 Toluene-d8 (S)100 %1 09/13/09 03:50 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 86 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/7988 EPA 3510 EPA 8270 8270 Water MSSV Associated Lab Samples:9252614024, 9252614025 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335996 Associated Lab Samples:9252614024, 9252614025 Matrix:Water Analyzed 1,2,4-Trichlorobenzene ug/L ND 10.0 09/17/09 17:04 1,2-Dichlorobenzene ug/L ND 10.0 09/17/09 17:04 1,2-Diphenylhydrazine ug/L ND 10.0 09/17/09 17:04 1,3-Dichlorobenzene ug/L ND 10.0 09/17/09 17:04 1,4-Dichlorobenzene ug/L ND 10.0 09/17/09 17:04 1-Methylnaphthalene ug/L ND 10.0 09/17/09 17:04 2,4,5-Trichlorophenol ug/L ND 10.0 09/17/09 17:04 2,4,6-Trichlorophenol ug/L ND 10.0 09/17/09 17:04 2,4-Dichlorophenol ug/L ND 10.0 09/17/09 17:04 2,4-Dimethylphenol ug/L ND 10.0 09/17/09 17:04 2,4-Dinitrophenol ug/L ND 50.0 09/17/09 17:04 2,4-Dinitrotoluene ug/L ND 10.0 09/17/09 17:04 2,6-Dinitrotoluene ug/L ND 10.0 09/17/09 17:04 2-Chloronaphthalene ug/L ND 10.0 09/17/09 17:04 2-Chlorophenol ug/L ND 10.0 09/17/09 17:04 2-Methylnaphthalene ug/L ND 10.0 09/17/09 17:04 2-Methylphenol(o-Cresol)ug/L ND 10.0 09/17/09 17:04 2-Nitroaniline ug/L ND 50.0 09/17/09 17:04 2-Nitrophenol ug/L ND 10.0 09/17/09 17:04 3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/17/09 17:04 3,3'-Dichlorobenzidine ug/L ND 50.0 09/17/09 17:04 3-Nitroaniline ug/L ND 50.0 09/17/09 17:04 4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/17/09 17:04 4-Bromophenylphenyl ether ug/L ND 10.0 09/17/09 17:04 4-Chloro-3-methylphenol ug/L ND 20.0 09/17/09 17:04 4-Chloroaniline ug/L ND 50.0 09/17/09 17:04 4-Chlorophenylphenyl ether ug/L ND 10.0 09/17/09 17:04 4-Nitroaniline ug/L ND 50.0 09/17/09 17:04 4-Nitrophenol ug/L ND 50.0 09/17/09 17:04 Acenaphthene ug/L ND 10.0 09/17/09 17:04 Acenaphthylene ug/L ND 10.0 09/17/09 17:04 Aniline ug/L ND 10.0 09/17/09 17:04 Anthracene ug/L ND 10.0 09/17/09 17:04 Benzo(a)anthracene ug/L ND 10.0 09/17/09 17:04 Benzo(a)pyrene ug/L ND 10.0 09/17/09 17:04 Benzo(b)fluoranthene ug/L ND 10.0 09/17/09 17:04 Benzo(g,h,i)perylene ug/L ND 10.0 09/17/09 17:04 Benzo(k)fluoranthene ug/L ND 10.0 09/17/09 17:04 Benzoic Acid ug/L ND 50.0 09/17/09 17:04 Benzyl alcohol ug/L ND 20.0 09/17/09 17:04 bis(2-Chloroethoxy)methane ug/L ND 10.0 09/17/09 17:04 bis(2-Chloroethyl) ether ug/L ND 10.0 09/17/09 17:04 bis(2-Chloroisopropyl) ether ug/L ND 10.0 09/17/09 17:04 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 87 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335996 Associated Lab Samples:9252614024, 9252614025 Matrix:Water Analyzed bis(2-Ethylhexyl)phthalate ug/L ND 10.0 09/17/09 17:04 Butylbenzylphthalate ug/L ND 10.0 09/17/09 17:04 Chrysene ug/L ND 10.0 09/17/09 17:04 Di-n-butylphthalate ug/L ND 10.0 09/17/09 17:04 Di-n-octylphthalate ug/L ND 10.0 09/17/09 17:04 Dibenz(a,h)anthracene ug/L ND 10.0 09/17/09 17:04 Dibenzofuran ug/L ND 10.0 09/17/09 17:04 Diethylphthalate ug/L ND 10.0 09/17/09 17:04 Dimethylphthalate ug/L ND 10.0 09/17/09 17:04 Fluoranthene ug/L ND 10.0 09/17/09 17:04 Fluorene ug/L ND 10.0 09/17/09 17:04 Hexachloro-1,3-butadiene ug/L ND 10.0 09/17/09 17:04 Hexachlorobenzene ug/L ND 10.0 09/17/09 17:04 Hexachlorocyclopentadiene ug/L ND 10.0 09/17/09 17:04 Hexachloroethane ug/L ND 10.0 09/17/09 17:04 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/17/09 17:04 Isophorone ug/L ND 10.0 09/17/09 17:04 N-Nitroso-di-n-propylamine ug/L ND 10.0 09/17/09 17:04 N-Nitrosodimethylamine ug/L ND 10.0 09/17/09 17:04 N-Nitrosodiphenylamine ug/L ND 10.0 09/17/09 17:04 Naphthalene ug/L ND 10.0 09/17/09 17:04 Nitrobenzene ug/L ND 10.0 09/17/09 17:04 Pentachlorophenol ug/L ND 50.0 09/17/09 17:04 Phenanthrene ug/L ND 10.0 09/17/09 17:04 Phenol ug/L ND 10.0 09/17/09 17:04 Pyrene ug/L ND 10.0 09/17/09 17:04 2,4,6-Tribromophenol (S)%53 25-150 09/17/09 17:04 2-Fluorobiphenyl (S)%51 30-150 09/17/09 17:04 2-Fluorophenol (S)%31 25-150 09/17/09 17:04 Nitrobenzene-d5 (S)%49 30-150 09/17/09 17:04 Phenol-d6 (S)%33 25-150 09/17/09 17:04 Terphenyl-d14 (S)%61 30-150 09/17/09 17:04 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335997LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/L 11.925 48 19-120 1,2-Dichlorobenzene ug/L 10.625 42 19-120 1,2-Diphenylhydrazine ug/L 20.925 84 50-150 1,3-Dichlorobenzene ug/L 9.7J25 39 15-120 1,4-Dichlorobenzene ug/L 10.825 43 15-120 1-Methylnaphthalene ug/L 14.025 56 21-120 2,4,5-Trichlorophenol ug/L 17.425 70 23-113 2,4,6-Trichlorophenol ug/L 20.125 80 21-113 2,4-Dichlorophenol ug/L 17.325 69 12-127 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 88 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335997LABORATORY CONTROL SAMPLE: LCSSpike 2,4-Dimethylphenol ug/L 18.225 73 24-120 2,4-Dinitrophenol ug/L 10.3J25 41 10-127 2,4-Dinitrotoluene ug/L 19.225 77 36-115 2,6-Dinitrotoluene ug/L 19.625 78 37-114 2-Chloronaphthalene ug/L 16.925 68 36-101 2-Chlorophenol ug/L 20.125 80 24-120 2-Methylnaphthalene ug/L 19.025 76 19-120 2-Methylphenol(o-Cresol)ug/L 16.525 66 25-120 2-Nitroaniline ug/L 20.3J25 81 30-109 2-Nitrophenol ug/L 18.925 75 24-120 3&4-Methylphenol(m&p Cresol)ug/L 15.325 61 24-120 3,3'-Dichlorobenzidine ug/L 20.7J25 83 14-120 3-Nitroaniline ug/L 24.8J25 99 23-133 4,6-Dinitro-2-methylphenol ug/L 11.6J25 46 10-128 4-Bromophenylphenyl ether ug/L 21.425 86 35-113 4-Chloro-3-methylphenol ug/L 19J25 76 32-107 4-Chloroaniline ug/L 25J25 100 12-150 4-Chlorophenylphenyl ether ug/L 20.125 81 36-110 4-Nitroaniline ug/L 23J25 92 12-150 4-Nitrophenol ug/L 17.9J25 72 10-120 Acenaphthene ug/L 18.425 74 27-102 Acenaphthylene ug/L 19.425 78 25-105 Aniline ug/L 15.325 61 10-150 Anthracene ug/L 20.525 82 30-113 Benzo(a)anthracene ug/L 19.325 77 27-113 Benzo(a)pyrene ug/L 19.225 77 27-119 Benzo(b)fluoranthene ug/L 15.925 64 22-114 Benzo(g,h,i)perylene ug/L 15.725 63 10-129 Benzo(k)fluoranthene ug/L 20.225 81 24-111 Benzoic Acid ug/L ND L0252324-120 Benzyl alcohol ug/L 24.125 96 24-120 bis(2-Chloroethoxy)methane ug/L 22.425 90 32-120 bis(2-Chloroethyl) ether ug/L 24.825 99 29-120 bis(2-Chloroisopropyl) ether ug/L 23.625 94 22-120 bis(2-Ethylhexyl)phthalate ug/L 21.325 85 29-125 Butylbenzylphthalate ug/L 21.525 86 33-120 Chrysene ug/L 19.325 77 23-112 Di-n-butylphthalate ug/L 21.825 87 38-116 Di-n-octylphthalate ug/L 22.825 91 32-122 Dibenz(a,h)anthracene ug/L 18.325 73 10-129 Dibenzofuran ug/L 18.025 72 37-107 Diethylphthalate ug/L 22.225 89 40-111 Dimethylphthalate ug/L 21.125 84 39-108 Fluoranthene ug/L 20.325 81 27-112 Fluorene ug/L 18.725 75 29-107 Hexachloro-1,3-butadiene ug/L 9.3J25 37 10-113 Hexachlorobenzene ug/L 19.025 76 29-119 Hexachlorocyclopentadiene ug/L 7.5J25 30 10-113 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 89 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335997LABORATORY CONTROL SAMPLE: LCSSpike Hexachloroethane ug/L 7.8J25 31 10-120 Indeno(1,2,3-cd)pyrene ug/L 18.225 73 14-123 Isophorone ug/L 18.725 75 23-150 N-Nitroso-di-n-propylamine ug/L 23.425 94 31-104 N-Nitrosodimethylamine ug/L 16.325 65 10-120 N-Nitrosodiphenylamine ug/L 25.325 101 27-139 Naphthalene ug/L 15.125 60 17-120 Nitrobenzene ug/L 18.025 72 27-120 Pentachlorophenol ug/L 12.9J25 51 10-135 Phenanthrene ug/L 19.525 78 28-111 Phenol ug/L 7.4J25 30 10-120 Pyrene ug/L 17.925 71 27-113 2,4,6-Tribromophenol (S)%76 25-150 2-Fluorobiphenyl (S)%73 30-150 2-Fluorophenol (S)%48 25-150 Nitrobenzene-d5 (S)%71 30-150 Phenol-d6 (S)%29 25-150 Terphenyl-d14 (S)%71 30-150 Parameter Units MS Result % Rec Limits Qual% RecConc. 335998MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252704001 335999 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,2,4-Trichlorobenzene ug/L R11114513-12058 32119ND50.0 68.9 1,4-Dichlorobenzene ug/L R11114419-12059 35119ND49.3 70.1 2,4-Dinitrotoluene ug/L R11115441-10969 31119ND59.6 81.6 2-Chlorophenol ug/L R11115933-12077 33119ND65.9 91.9 4-Chloro-3-methylphenol ug/L 111 58 30-10872 27119ND64.8 85.2 4-Nitrophenol ug/L 111 51 10-12066119ND56.8J 78.8J Acenaphthene ug/L 111 59 27-10172 28119ND65.1 86.2 N-Nitroso-di-n-propylamine ug/L 111 78 34-12086 16119ND87.0 102 Pentachlorophenol ug/L 111 59 10-13865119ND65.3J 77.9J Phenol ug/L R11114010-12055 38119ND44.8 65.6 Pyrene ug/L 111 71 31-11079 17119ND79.4 93.9 2,4,6-Tribromophenol (S)%66 25-15080 2-Fluorobiphenyl (S)%57 30-15073 2-Fluorophenol (S)%40 25-15051 Nitrobenzene-d5 (S)%50 30-15064 Phenol-d6 (S)%36 25-15048 Terphenyl-d14 (S)%71 30-15077 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 90 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/7940 EPA 3546 EPA 8270 8270 Solid MSSV Microwave Associated Lab Samples:9252614001, 9252614002, 9252614003, 9252614004, 9252614005, 9252614006, 9252614007, 9252614008,9252614009, 9252614012, 9252614013, 9252614015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:333609 Associated Lab Samples:9252614001, 9252614002, 9252614003, 9252614004, 9252614005, 9252614006, 9252614007, 9252614008,9252614009, 9252614012, 9252614013, 9252614015 Matrix:Solid Analyzed 1,2,4-Trichlorobenzene ug/kg ND 330 09/14/09 23:45 1,2-Dichlorobenzene ug/kg ND 330 09/14/09 23:45 1,2-Diphenylhydrazine ug/kg ND 330 09/14/09 23:45 1,3-Dichlorobenzene ug/kg ND 330 09/14/09 23:45 1,4-Dichlorobenzene ug/kg ND 330 09/14/09 23:45 1-Methylnaphthalene ug/kg ND 330 09/14/09 23:45 2,4,5-Trichlorophenol ug/kg ND 330 09/14/09 23:45 2,4,6-Trichlorophenol ug/kg ND 330 09/14/09 23:45 2,4-Dichlorophenol ug/kg ND 330 09/14/09 23:45 2,4-Dimethylphenol ug/kg ND 330 09/14/09 23:45 2,4-Dinitrophenol ug/kg ND 1650 09/14/09 23:45 2,4-Dinitrotoluene ug/kg ND 330 09/14/09 23:45 2,6-Dinitrotoluene ug/kg ND 330 09/14/09 23:45 2-Chloronaphthalene ug/kg ND 330 09/14/09 23:45 2-Chlorophenol ug/kg ND 330 09/14/09 23:45 2-Methylnaphthalene ug/kg ND 330 09/14/09 23:45 2-Methylphenol(o-Cresol)ug/kg ND 330 09/14/09 23:45 2-Nitroaniline ug/kg ND 1650 09/14/09 23:45 2-Nitrophenol ug/kg ND 330 09/14/09 23:45 3&4-Methylphenol(m&p Cresol)ug/kg ND 330 09/14/09 23:45 3,3'-Dichlorobenzidine ug/kg ND 1650 09/14/09 23:45 3-Nitroaniline ug/kg ND 1650 09/14/09 23:45 4,6-Dinitro-2-methylphenol ug/kg ND 660 09/14/09 23:45 4-Bromophenylphenyl ether ug/kg ND 330 09/14/09 23:45 4-Chloro-3-methylphenol ug/kg ND 660 09/14/09 23:45 4-Chloroaniline ug/kg ND 1650 09/14/09 23:45 4-Chlorophenylphenyl ether ug/kg ND 330 09/14/09 23:45 4-Nitroaniline ug/kg ND 660 09/14/09 23:45 4-Nitrophenol ug/kg ND 1650 09/14/09 23:45 Acenaphthene ug/kg ND 330 09/14/09 23:45 Acenaphthylene ug/kg ND 330 09/14/09 23:45 Aniline ug/kg ND 330 09/14/09 23:45 Anthracene ug/kg ND 330 09/14/09 23:45 Benzo(a)anthracene ug/kg ND 330 09/14/09 23:45 Benzo(a)pyrene ug/kg ND 330 09/14/09 23:45 Benzo(b)fluoranthene ug/kg ND 330 09/14/09 23:45 Benzo(g,h,i)perylene ug/kg ND 330 09/14/09 23:45 Benzo(k)fluoranthene ug/kg ND 330 09/14/09 23:45 Benzoic Acid ug/kg ND 1650 09/14/09 23:45 Benzyl alcohol ug/kg ND 660 09/14/09 23:45 bis(2-Chloroethoxy)methane ug/kg ND 330 09/14/09 23:45 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 91 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:333609 Associated Lab Samples:9252614001, 9252614002, 9252614003, 9252614004, 9252614005, 9252614006, 9252614007, 9252614008,9252614009, 9252614012, 9252614013, 9252614015 Matrix:Solid Analyzed bis(2-Chloroethyl) ether ug/kg ND 330 09/14/09 23:45 bis(2-Chloroisopropyl) ether ug/kg ND 330 09/14/09 23:45 bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/14/09 23:45 Butylbenzylphthalate ug/kg ND 330 09/14/09 23:45 Chrysene ug/kg ND 330 09/14/09 23:45 Di-n-butylphthalate ug/kg ND 330 09/14/09 23:45 Di-n-octylphthalate ug/kg ND 330 09/14/09 23:45 Dibenz(a,h)anthracene ug/kg ND 330 09/14/09 23:45 Dibenzofuran ug/kg ND 330 09/14/09 23:45 Diethylphthalate ug/kg ND 330 09/14/09 23:45 Dimethylphthalate ug/kg ND 330 09/14/09 23:45 Fluoranthene ug/kg ND 330 09/14/09 23:45 Fluorene ug/kg ND 330 09/14/09 23:45 Hexachloro-1,3-butadiene ug/kg ND 330 09/14/09 23:45 Hexachlorobenzene ug/kg ND 330 09/14/09 23:45 Hexachlorocyclopentadiene ug/kg ND 330 09/14/09 23:45 Hexachloroethane ug/kg ND 330 09/14/09 23:45 Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/14/09 23:45 Isophorone ug/kg ND 330 09/14/09 23:45 N-Nitroso-di-n-propylamine ug/kg ND 330 09/14/09 23:45 N-Nitrosodimethylamine ug/kg ND 330 09/14/09 23:45 N-Nitrosodiphenylamine ug/kg ND 330 09/14/09 23:45 Naphthalene ug/kg ND 330 09/14/09 23:45 Nitrobenzene ug/kg ND 330 09/14/09 23:45 Pentachlorophenol ug/kg ND 1650 09/14/09 23:45 Phenanthrene ug/kg ND 330 09/14/09 23:45 Phenol ug/kg ND 330 09/14/09 23:45 Pyrene ug/kg ND 330 09/14/09 23:45 2,4,6-Tribromophenol (S)%47 44-136 09/14/09 23:45 2-Fluorobiphenyl (S)%51 46-120 09/14/09 23:45 2-Fluorophenol (S)%34 24-120 09/14/09 23:45 Nitrobenzene-d5 (S)%44 30-150 09/14/09 23:45 Phenol-d6 (S)%38 35-120 09/14/09 23:45 Terphenyl-d14 (S)%50 38-108 09/14/09 23:45 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333610LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/kg 10301670 62 50-150 1,2-Dichlorobenzene ug/kg 9071670 54 50-150 1,2-Diphenylhydrazine ug/kg 9871670 59 43-130 1,3-Dichlorobenzene ug/kg 9721670 58 50-150 1,4-Dichlorobenzene ug/kg 10401670 62 50-150 1-Methylnaphthalene ug/kg 11101670 66 50-150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 92 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333610LABORATORY CONTROL SAMPLE: LCSSpike 2,4,5-Trichlorophenol ug/kg 10701670 64 50-150 2,4,6-Trichlorophenol ug/kg 9781670 59 50-150 2,4-Dichlorophenol ug/kg 8811670 53 50-150 2,4-Dimethylphenol ug/kg 9791670 59 50-150 2,4-Dinitrophenol ug/kg 907J1670 54 20-111 2,4-Dinitrotoluene ug/kg 10101670 60 50-150 2,6-Dinitrotoluene ug/kg 8371670 50 50-150 2-Chloronaphthalene ug/kg 9641670 58 50-150 2-Chlorophenol ug/kg 9511670 57 50-150 2-Methylnaphthalene ug/kg 10401670 62 50-150 2-Methylphenol(o-Cresol)ug/kg 9281670 56 50-150 2-Nitroaniline ug/kg 1060J1670 63 50-150 2-Nitrophenol ug/kg 8761670 53 50-150 3&4-Methylphenol(m&p Cresol)ug/kg 10501670 63 50-150 3,3'-Dichlorobenzidine ug/kg 886J1670 53 50-150 3-Nitroaniline ug/kg 939J1670 56 50-150 4,6-Dinitro-2-methylphenol ug/kg 9811670 59 15-136 4-Bromophenylphenyl ether ug/kg 9571670 57 50-150 4-Chloro-3-methylphenol ug/kg 13101670 79 50-150 4-Chloroaniline ug/kg 1210J1670 72 50-150 4-Chlorophenylphenyl ether ug/kg 9751670 59 50-150 4-Nitroaniline ug/kg 9571670 57 50-150 4-Nitrophenol ug/kg 1330J1670 80 33-105 Acenaphthene ug/kg 9231670 55 50-150 Acenaphthylene ug/kg 8771670 53 50-150 Aniline ug/kg 11701670 70 50-150 Anthracene ug/kg 8681670 52 50-150 Benzo(a)anthracene ug/kg 9811670 59 50-150 Benzo(a)pyrene ug/kg 10901670 66 50-150 Benzo(b)fluoranthene ug/kg 10901670 65 50-150 Benzo(g,h,i)perylene ug/kg 8761670 53 24-117 Benzo(k)fluoranthene ug/kg 11501670 69 50-150 Benzoic Acid ug/kg 452J1670 27 15-104 Benzyl alcohol ug/kg 9501670 57 50-150 bis(2-Chloroethoxy)methane ug/kg 8851670 53 50-150 bis(2-Chloroethyl) ether ug/kg 15201670 91 50-150 bis(2-Chloroisopropyl) ether ug/kg 9071670 54 50-150 bis(2-Ethylhexyl)phthalate ug/kg 9481670 57 50-150 Butylbenzylphthalate ug/kg 8981670 54 50-150 Chrysene ug/kg 10201670 61 50-150 Di-n-butylphthalate ug/kg 10301670 62 50-150 Di-n-octylphthalate ug/kg 9711670 58 50-150 Dibenz(a,h)anthracene ug/kg 8691670 52 17-128 Dibenzofuran ug/kg 8541670 51 50-150 Diethylphthalate ug/kg 8841670 53 50-150 Dimethylphthalate ug/kg 10001670 60 50-150 Fluoranthene ug/kg 10701670 64 50-150 Fluorene ug/kg 9001670 54 50-150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 93 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333610LABORATORY CONTROL SAMPLE: LCSSpike Hexachloro-1,3-butadiene ug/kg 9671670 58 50-150 Hexachlorobenzene ug/kg 10201670 61 50-150 Hexachlorocyclopentadiene ug/kg 8551670 51 15-114 Hexachloroethane ug/kg 8851670 53 50-150 Indeno(1,2,3-cd)pyrene ug/kg 8971670 54 19-128 Isophorone ug/kg 10301670 62 50-150 N-Nitroso-di-n-propylamine ug/kg 9501670 57 50-150 N-Nitrosodimethylamine ug/kg 8621670 52 50-150 N-Nitrosodiphenylamine ug/kg 9771670 59 50-150 Naphthalene ug/kg 10201670 61 50-150 Nitrobenzene ug/kg 10601670 63 50-150 Pentachlorophenol ug/kg 960J1670 58 15-130 Phenanthrene ug/kg 9221670 55 50-150 Phenol ug/kg 8391670 50 42-120 Pyrene ug/kg 9701670 58 50-150 2,4,6-Tribromophenol (S)%53 44-136 2-Fluorobiphenyl (S)%55 46-120 2-Fluorophenol (S)%36 24-120 Nitrobenzene-d5 (S)%47 30-150 Phenol-d6 (S)%39 35-120 Terphenyl-d14 (S)%58 38-108 Parameter Units MS Result % Rec Limits Qual% RecConc. 333613MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252614006 333614 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,2,4-Trichlorobenzene ug/kg 1890 54 50-15067 201890ND10201250 1,4-Dichlorobenzene ug/kg 1890 52 50-15057 91890ND9781070 2,4-Dinitrotoluene ug/kg M018904450-15055 231890ND8281040 2-Chlorophenol ug/kg 1890 50 50-15051 11890ND947953 4-Chloro-3-methylphenol ug/kg R118905250-15082 451890ND9791550 4-Nitrophenol ug/kg 1890 57 50-150791890ND1080J1490J Acenaphthene ug/kg 1890 51 50-15058 121890ND9651090 N-Nitroso-di-n-propylamine ug/kg 1890 54 50-15063 151890ND10201180 Pentachlorophenol ug/kg M018904550-150691890ND844J1290J Phenol ug/kg 1890 59 50-15059 01890ND11101110 2,4,6-Tribromophenol (S)%47 44-13648 2-Fluorobiphenyl (S)%62 46-12058 2-Fluorophenol (S)%25 24-12027 Nitrobenzene-d5 (S)%50 30-15060 Phenol-d6 (S)%1g2735-12039 Terphenyl-d14 (S)%85 38-10896 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 94 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/5044 EPA 3050 EPA 6010 6010 MET Associated Lab Samples:9252614006, 9252614007, 9252614008, 9252614009, 9252614010, 9252614011 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:333485 Associated Lab Samples:9252614006, 9252614007, 9252614008, 9252614009, 9252614010, 9252614011 Matrix:Solid Analyzed Antimony mg/kg ND 0.50 09/10/09 18:44 Arsenic mg/kg ND 0.50 09/10/09 18:44 Beryllium mg/kg ND 0.10 09/10/09 18:44 Cadmium mg/kg ND 0.10 09/10/09 18:44 Chromium mg/kg ND 0.50 09/10/09 18:44 Copper mg/kg ND 0.50 09/10/09 18:44 Lead mg/kg ND 0.50 09/10/09 18:44 Manganese mg/kg ND 0.50 09/10/09 18:44 Nickel mg/kg ND 0.50 09/10/09 18:44 Selenium mg/kg ND 1.0 09/10/09 18:44 Silver mg/kg ND 0.50 09/10/09 18:44 Thallium mg/kg ND 1.0 09/10/09 18:44 Zinc mg/kg ND 1.0 09/10/09 18:44 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333486LABORATORY CONTROL SAMPLE: LCSSpike Antimony mg/kg 51.950 104 80-120 Arsenic mg/kg 48.850 98 80-120 Beryllium mg/kg 50.350 101 80-120 Cadmium mg/kg 49.350 99 80-120 Chromium mg/kg 50.250 100 80-120 Copper mg/kg 49.350 99 80-120 Lead mg/kg 50.050 100 80-120 Manganese mg/kg 51.050 102 80-120 Nickel mg/kg 50.050 100 80-120 Selenium mg/kg 48.550 97 80-120 Silver mg/kg 25.625 102 80-120 Thallium mg/kg 47.750 95 80-120 Zinc mg/kg 50.550 101 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 333487MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252614006 333488 MSD Result MSD % Rec RPD MSDMS Spike Conc. Antimony mg/kg M0,R136.8 74 75-12585 4048.71.3 28.3 42.7 Arsenic mg/kg R136.8 75 75-12584 3348.77.1 34.4 48.1 Beryllium mg/kg R136.8 78 75-12583 3348.72.1 30.6 42.6 Cadmium mg/kg R136.8 76 75-12582 3548.70.25 28.3 40.2 Chromium mg/kg R136.8 78 75-12584 3148.75.5 34.2 46.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 95 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units MS Result % Rec Limits Qual% RecConc. 333487MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252614006 333488 MSD Result MSD % Rec RPD MSDMS Spike Conc. Copper mg/kg M036.8 60 75-12570 1948.738.0 60.1 72.3 Lead mg/kg M0,R136.8 37 75-12567 4048.724.9 38.3 57.3 Manganese mg/kg M0,R136.8 68 75-125146 3348.793.8 119 165 Nickel mg/kg M0,R136.8 68 75-12576 2948.710.2 35.2 47.2 Selenium mg/kg R136.8 79 75-12585 3548.71.4 30.4 43.1 Silver mg/kg R118.3 82 75-12588 3424.4ND 15.3 21.6 Thallium mg/kg M0,R136.8 60 75-12563 3348.7ND 21.9 30.6 Zinc mg/kg M036.8 415 75-125394 1748.756.5 209 248 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 96 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/8247 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:9252614021 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:334872 Associated Lab Samples:9252614021 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/11/09 10:18 1,1,1-Trichloroethane ug/kg ND 5.0 09/11/09 10:18 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/11/09 10:18 1,1,2-Trichloroethane ug/kg ND 5.0 09/11/09 10:18 1,1-Dichloroethane ug/kg ND 5.0 09/11/09 10:18 1,1-Dichloroethene ug/kg ND 5.0 09/11/09 10:18 1,1-Dichloropropene ug/kg ND 5.0 09/11/09 10:18 1,2,3-Trichlorobenzene ug/kg ND 5.0 09/11/09 10:18 1,2,3-Trichloropropane ug/kg ND 5.0 09/11/09 10:18 1,2,4-Trichlorobenzene ug/kg ND 5.0 09/11/09 10:18 1,2,4-Trimethylbenzene ug/kg ND 5.0 09/11/09 10:18 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/11/09 10:18 1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/11/09 10:18 1,2-Dichlorobenzene ug/kg ND 5.0 09/11/09 10:18 1,2-Dichloroethane ug/kg ND 5.0 09/11/09 10:18 1,2-Dichloropropane ug/kg ND 5.0 09/11/09 10:18 1,3,5-Trimethylbenzene ug/kg ND 5.0 09/11/09 10:18 1,3-Dichlorobenzene ug/kg ND 5.0 09/11/09 10:18 1,3-Dichloropropane ug/kg ND 5.0 09/11/09 10:18 1,4-Dichlorobenzene ug/kg ND 5.0 09/11/09 10:18 2,2-Dichloropropane ug/kg ND 5.0 09/11/09 10:18 2-Butanone (MEK)ug/kg ND 100 09/11/09 10:18 2-Chlorotoluene ug/kg ND 5.0 09/11/09 10:18 2-Hexanone ug/kg ND 50.0 09/11/09 10:18 4-Chlorotoluene ug/kg ND 5.0 09/11/09 10:18 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/11/09 10:18 Acetone ug/kg ND 100 09/11/09 10:18 Benzene ug/kg ND 5.0 09/11/09 10:18 Bromobenzene ug/kg ND 5.0 09/11/09 10:18 Bromochloromethane ug/kg ND 5.0 09/11/09 10:18 Bromodichloromethane ug/kg ND 5.0 09/11/09 10:18 Bromoform ug/kg ND 5.0 09/11/09 10:18 Bromomethane ug/kg ND 10.0 09/11/09 10:18 Carbon tetrachloride ug/kg ND 5.0 09/11/09 10:18 Chlorobenzene ug/kg ND 5.0 09/11/09 10:18 Chloroethane ug/kg ND 10.0 09/11/09 10:18 Chloroform ug/kg ND 5.0 09/11/09 10:18 Chloromethane ug/kg ND 10.0 09/11/09 10:18 cis-1,2-Dichloroethene ug/kg ND 5.0 09/11/09 10:18 cis-1,3-Dichloropropene ug/kg ND 5.0 09/11/09 10:18 Dibromochloromethane ug/kg ND 5.0 09/11/09 10:18 Dibromomethane ug/kg ND 5.0 09/11/09 10:18 Dichlorodifluoromethane ug/kg ND 10.0 09/11/09 10:18 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 97 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:334872 Associated Lab Samples:9252614021 Matrix:Solid Analyzed Diisopropyl ether ug/kg ND 5.0 09/11/09 10:18 Ethylbenzene ug/kg ND 5.0 09/11/09 10:18 Hexachloro-1,3-butadiene ug/kg ND 5.0 09/11/09 10:18 Isopropylbenzene (Cumene)ug/kg ND 5.0 09/11/09 10:18 m&p-Xylene ug/kg ND 10.0 09/11/09 10:18 Methyl-tert-butyl ether ug/kg ND 5.0 09/11/09 10:18 Methylene Chloride ug/kg ND 20.0 09/11/09 10:18 n-Butylbenzene ug/kg ND 5.0 09/11/09 10:18 n-Propylbenzene ug/kg ND 5.0 09/11/09 10:18 Naphthalene ug/kg ND 5.0 09/11/09 10:18 o-Xylene ug/kg ND 5.0 09/11/09 10:18 p-Isopropyltoluene ug/kg ND 5.0 09/11/09 10:18 sec-Butylbenzene ug/kg ND 5.0 09/11/09 10:18 Styrene ug/kg ND 5.0 09/11/09 10:18 tert-Butylbenzene ug/kg ND 5.0 09/11/09 10:18 Tetrachloroethene ug/kg ND 5.0 09/11/09 10:18 Toluene ug/kg ND 5.0 09/11/09 10:18 trans-1,2-Dichloroethene ug/kg ND 5.0 09/11/09 10:18 trans-1,3-Dichloropropene ug/kg ND 5.0 09/11/09 10:18 Trichloroethene ug/kg ND 5.0 09/11/09 10:18 Trichlorofluoromethane ug/kg ND 5.0 09/11/09 10:18 Vinyl acetate ug/kg ND 50.0 09/11/09 10:18 Vinyl chloride ug/kg ND 10.0 09/11/09 10:18 Xylene (Total)ug/kg ND 10.0 09/11/09 10:18 1,2-Dichloroethane-d4 (S)%94 69-121 09/11/09 10:18 4-Bromofluorobenzene (S)%98 74-115 09/11/09 10:18 Dibromofluoromethane (S)%100 79-116 09/11/09 10:18 Toluene-d8 (S)%102 88-110 09/11/09 10:18 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334873LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 51.450 103 75-137 1,1,1-Trichloroethane ug/kg 49.150 98 70-140 1,1,2,2-Tetrachloroethane ug/kg 48.750 97 74-133 1,1,2-Trichloroethane ug/kg 49.750 99 79-129 1,1-Dichloroethane ug/kg 49.450 99 72-139 1,1-Dichloroethene ug/kg 52.950 106 69-154 1,1-Dichloropropene ug/kg 53.550 107 74-138 1,2,3-Trichlorobenzene ug/kg 54.450 109 71-150 1,2,3-Trichloropropane ug/kg 49.050 98 74-135 1,2,4-Trichlorobenzene ug/kg 61.050 122 68-150 1,2,4-Trimethylbenzene ug/kg 53.450 107 70-130 1,2-Dibromo-3-chloropropane ug/kg 47.850 96 65-146 1,2-Dibromoethane (EDB)ug/kg 51.650 103 77-136 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 98 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334873LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dichlorobenzene ug/kg 51.650 103 75-141 1,2-Dichloroethane ug/kg 49.450 99 74-134 1,2-Dichloropropane ug/kg 52.050 104 77-138 1,3,5-Trimethylbenzene ug/kg 52.550 105 65-128 1,3-Dichlorobenzene ug/kg 53.350 107 76-133 1,3-Dichloropropane ug/kg 49.850 100 79-132 1,4-Dichlorobenzene ug/kg 53.550 107 75-137 2,2-Dichloropropane ug/kg 52.550 105 73-137 2-Butanone (MEK)ug/kg 92.1J100 92 61-138 2-Chlorotoluene ug/kg 49.650 99 73-138 2-Hexanone ug/kg 95.0100 95 58-159 4-Chlorotoluene ug/kg 54.450 109 75-136 4-Methyl-2-pentanone (MIBK)ug/kg 94.8100 95 74-139 Acetone ug/kg 94.6J100 95 58-150 Benzene ug/kg 49.150 98 71-140 Bromobenzene ug/kg 50.750 101 72-144 Bromochloromethane ug/kg 50.450 101 78-133 Bromodichloromethane ug/kg 47.650 95 78-133 Bromoform ug/kg 50.650 101 74-132 Bromomethane ug/kg 87.750 175 63-184 Carbon tetrachloride ug/kg 59.250 118 73-143 Chlorobenzene ug/kg 50.850 102 77-137 Chloroethane ug/kg 59.350 119 68-146 Chloroform ug/kg 49.450 99 75-137 Chloromethane ug/kg 57.650 115 54-143 cis-1,2-Dichloroethene ug/kg 51.350 103 71-143 cis-1,3-Dichloropropene ug/kg 53.450 107 76-133 Dibromochloromethane ug/kg 48.650 97 77-131 Dibromomethane ug/kg 49.550 99 63-184 Dichlorodifluoromethane ug/kg 64.950 130 36-173 Diisopropyl ether ug/kg 47.850 96 68-144 Ethylbenzene ug/kg 52.150 104 69-141 Hexachloro-1,3-butadiene ug/kg 52.350 105 70-152 Isopropylbenzene (Cumene)ug/kg 54.750 109 77-143 m&p-Xylene ug/kg 107100 107 72-138 Methyl-tert-butyl ether ug/kg 48.250 96 2-138 Methylene Chloride ug/kg 50.050 100 69-136 n-Butylbenzene ug/kg 56.050 112 65-128 n-Propylbenzene ug/kg 54.350 109 72-139 Naphthalene ug/kg 52.650 105 61-138 o-Xylene ug/kg 53.250 106 74-137 p-Isopropyltoluene ug/kg 54.550 109 66-128 sec-Butylbenzene ug/kg 54.050 108 72-140 Styrene ug/kg 52.350 105 76-137 tert-Butylbenzene ug/kg 52.050 104 68-141 Tetrachloroethene ug/kg 54.850 110 72-136 Toluene ug/kg 49.450 99 69-139 trans-1,2-Dichloroethene ug/kg 49.750 99 72-144 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 99 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334873LABORATORY CONTROL SAMPLE: LCSSpike trans-1,3-Dichloropropene ug/kg 53.950 108 73-135 Trichloroethene ug/kg 52.250 104 75-136 Trichlorofluoromethane ug/kg 56.850 114 69-144 Vinyl acetate ug/kg 288 L310028850-150 Vinyl chloride ug/kg 60.250 120 61-145 Xylene (Total)ug/kg 160150 107 73-138 1,2-Dichloroethane-d4 (S)%94 69-121 4-Bromofluorobenzene (S)%103 74-115 Dibromofluoromethane (S)%99 79-116 Toluene-d8 (S)%100 88-110 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 100 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/8230 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:9252614001, 9252614002, 9252614003, 9252614012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:333518 Associated Lab Samples:9252614001, 9252614002, 9252614003, 9252614012 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/09/09 12:36 1,1,1-Trichloroethane ug/kg ND 5.0 09/09/09 12:36 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/09/09 12:36 1,1,2-Trichloroethane ug/kg ND 5.0 09/09/09 12:36 1,1-Dichloroethane ug/kg ND 5.0 09/09/09 12:36 1,1-Dichloroethene ug/kg ND 5.0 09/09/09 12:36 1,1-Dichloropropene ug/kg ND 5.0 09/09/09 12:36 1,2,3-Trichlorobenzene ug/kg ND 5.0 09/09/09 12:36 1,2,3-Trichloropropane ug/kg ND 5.0 09/09/09 12:36 1,2,4-Trichlorobenzene ug/kg ND 5.0 09/09/09 12:36 1,2,4-Trimethylbenzene ug/kg ND 5.0 09/09/09 12:36 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/09/09 12:36 1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/09/09 12:36 1,2-Dichlorobenzene ug/kg ND 5.0 09/09/09 12:36 1,2-Dichloroethane ug/kg ND 5.0 09/09/09 12:36 1,2-Dichloropropane ug/kg ND 5.0 09/09/09 12:36 1,3,5-Trimethylbenzene ug/kg ND 5.0 09/09/09 12:36 1,3-Dichlorobenzene ug/kg ND 5.0 09/09/09 12:36 1,3-Dichloropropane ug/kg ND 5.0 09/09/09 12:36 1,4-Dichlorobenzene ug/kg ND 5.0 09/09/09 12:36 2,2-Dichloropropane ug/kg ND 5.0 09/09/09 12:36 2-Butanone (MEK)ug/kg ND 100 09/09/09 12:36 2-Chlorotoluene ug/kg ND 5.0 09/09/09 12:36 2-Hexanone ug/kg ND 50.0 09/09/09 12:36 4-Chlorotoluene ug/kg ND 5.0 09/09/09 12:36 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/09/09 12:36 Acetone ug/kg ND 100 09/09/09 12:36 Benzene ug/kg ND 5.0 09/09/09 12:36 Bromobenzene ug/kg ND 5.0 09/09/09 12:36 Bromochloromethane ug/kg ND 5.0 09/09/09 12:36 Bromodichloromethane ug/kg ND 5.0 09/09/09 12:36 Bromoform ug/kg ND 5.0 09/09/09 12:36 Bromomethane ug/kg ND 10.0 09/09/09 12:36 Carbon tetrachloride ug/kg ND 5.0 09/09/09 12:36 Chlorobenzene ug/kg ND 5.0 09/09/09 12:36 Chloroethane ug/kg ND 10.0 09/09/09 12:36 Chloroform ug/kg ND 5.0 09/09/09 12:36 Chloromethane ug/kg ND 10.0 09/09/09 12:36 cis-1,2-Dichloroethene ug/kg ND 5.0 09/09/09 12:36 cis-1,3-Dichloropropene ug/kg ND 5.0 09/09/09 12:36 Dibromochloromethane ug/kg ND 5.0 09/09/09 12:36 Dibromomethane ug/kg ND 5.0 09/09/09 12:36 Dichlorodifluoromethane ug/kg ND 10.0 09/09/09 12:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 101 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:333518 Associated Lab Samples:9252614001, 9252614002, 9252614003, 9252614012 Matrix:Solid Analyzed Diisopropyl ether ug/kg ND 5.0 09/09/09 12:36 Ethylbenzene ug/kg ND 5.0 09/09/09 12:36 Hexachloro-1,3-butadiene ug/kg ND 5.0 09/09/09 12:36 Isopropylbenzene (Cumene)ug/kg ND 5.0 09/09/09 12:36 m&p-Xylene ug/kg ND 10.0 09/09/09 12:36 Methyl-tert-butyl ether ug/kg ND 5.0 09/09/09 12:36 Methylene Chloride ug/kg ND 20.0 09/09/09 12:36 n-Butylbenzene ug/kg ND 5.0 09/09/09 12:36 n-Propylbenzene ug/kg ND 5.0 09/09/09 12:36 Naphthalene ug/kg ND 5.0 09/09/09 12:36 o-Xylene ug/kg ND 5.0 09/09/09 12:36 p-Isopropyltoluene ug/kg ND 5.0 09/09/09 12:36 sec-Butylbenzene ug/kg ND 5.0 09/09/09 12:36 Styrene ug/kg ND 5.0 09/09/09 12:36 tert-Butylbenzene ug/kg ND 5.0 09/09/09 12:36 Tetrachloroethene ug/kg ND 5.0 09/09/09 12:36 Toluene ug/kg ND 5.0 09/09/09 12:36 trans-1,2-Dichloroethene ug/kg ND 5.0 09/09/09 12:36 trans-1,3-Dichloropropene ug/kg ND 5.0 09/09/09 12:36 Trichloroethene ug/kg ND 5.0 09/09/09 12:36 Trichlorofluoromethane ug/kg ND 5.0 09/09/09 12:36 Vinyl acetate ug/kg ND 50.0 09/09/09 12:36 Vinyl chloride ug/kg ND 10.0 09/09/09 12:36 Xylene (Total)ug/kg ND 10.0 09/09/09 12:36 1,2-Dichloroethane-d4 (S)%100 69-121 09/09/09 12:36 4-Bromofluorobenzene (S)%98 74-115 09/09/09 12:36 Dibromofluoromethane (S)%101 79-116 09/09/09 12:36 Toluene-d8 (S)%102 88-110 09/09/09 12:36 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333519LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 52.150 104 75-137 1,1,1-Trichloroethane ug/kg 50.650 101 70-140 1,1,2,2-Tetrachloroethane ug/kg 49.850 100 74-133 1,1,2-Trichloroethane ug/kg 50.150 100 79-129 1,1-Dichloroethane ug/kg 50.450 101 72-139 1,1-Dichloroethene ug/kg 53.550 107 69-154 1,1-Dichloropropene ug/kg 54.450 109 74-138 1,2,3-Trichlorobenzene ug/kg 54.650 109 71-150 1,2,3-Trichloropropane ug/kg 50.150 100 74-135 1,2,4-Trichlorobenzene ug/kg 60.450 121 68-150 1,2,4-Trimethylbenzene ug/kg 54.550 109 70-130 1,2-Dibromo-3-chloropropane ug/kg 47.250 94 65-146 1,2-Dibromoethane (EDB)ug/kg 51.850 104 77-136 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 102 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333519LABORATORY CONTROL SAMPLE: LCSSpike 1,2-Dichlorobenzene ug/kg 53.550 107 75-141 1,2-Dichloroethane ug/kg 51.650 103 74-134 1,2-Dichloropropane ug/kg 53.450 107 77-138 1,3,5-Trimethylbenzene ug/kg 54.550 109 65-128 1,3-Dichlorobenzene ug/kg 54.850 110 76-133 1,3-Dichloropropane ug/kg 50.550 101 79-132 1,4-Dichlorobenzene ug/kg 54.850 110 75-137 2,2-Dichloropropane ug/kg 54.750 109 73-137 2-Butanone (MEK)ug/kg 90.8J100 91 61-138 2-Chlorotoluene ug/kg 51.850 104 73-138 2-Hexanone ug/kg 90.4100 90 58-159 4-Chlorotoluene ug/kg 55.550 111 75-136 4-Methyl-2-pentanone (MIBK)ug/kg 95.5100 95 74-139 Acetone ug/kg 89.5J100 89 58-150 Benzene ug/kg 50.550 101 71-140 Bromobenzene ug/kg 52.850 106 72-144 Bromochloromethane ug/kg 50.250 100 78-133 Bromodichloromethane ug/kg 49.650 99 78-133 Bromoform ug/kg 50.650 101 74-132 Bromomethane ug/kg 91.250 182 63-184 Carbon tetrachloride ug/kg 54.350 109 73-143 Chlorobenzene ug/kg 51.350 103 77-137 Chloroethane ug/kg 59.350 119 68-146 Chloroform ug/kg 50.350 101 75-137 Chloromethane ug/kg 56.750 113 54-143 cis-1,2-Dichloroethene ug/kg 52.150 104 71-143 cis-1,3-Dichloropropene ug/kg 54.350 109 76-133 Dibromochloromethane ug/kg 49.650 99 77-131 Dibromomethane ug/kg 52.050 104 63-184 Dichlorodifluoromethane ug/kg 57.550 115 36-173 Diisopropyl ether ug/kg 48.250 96 68-144 Ethylbenzene ug/kg 52.850 106 69-141 Hexachloro-1,3-butadiene ug/kg 53.150 106 70-152 Isopropylbenzene (Cumene)ug/kg 54.650 109 77-143 m&p-Xylene ug/kg 109100 109 72-138 Methyl-tert-butyl ether ug/kg 48.350 97 2-138 Methylene Chloride ug/kg 48.150 96 69-136 n-Butylbenzene ug/kg 57.250 114 65-128 n-Propylbenzene ug/kg 56.350 113 72-139 Naphthalene ug/kg 49.550 99 61-138 o-Xylene ug/kg 53.350 107 74-137 p-Isopropyltoluene ug/kg 56.450 113 66-128 sec-Butylbenzene ug/kg 55.550 111 72-140 Styrene ug/kg 52.650 105 76-137 tert-Butylbenzene ug/kg 53.650 107 68-141 Tetrachloroethene ug/kg 54.250 108 72-136 Toluene ug/kg 50.150 100 69-139 trans-1,2-Dichloroethene ug/kg 50.050 100 72-144 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 103 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333519LABORATORY CONTROL SAMPLE: LCSSpike trans-1,3-Dichloropropene ug/kg 54.750 109 73-135 Trichloroethene ug/kg 53.150 106 75-136 Trichlorofluoromethane ug/kg 56.650 113 69-144 Vinyl acetate ug/kg 291 L310029150-150 Vinyl chloride ug/kg 58.850 118 61-145 Xylene (Total)ug/kg 162150 108 73-138 1,2-Dichloroethane-d4 (S)%94 69-121 4-Bromofluorobenzene (S)%101 74-115 Dibromofluoromethane (S)%98 79-116 Toluene-d8 (S)%100 88-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 334139MATRIX SPIKE SAMPLE: MSSpike Result 9252590001 1,1-Dichloroethene ug/kg 50.152.4 96 33-158ND Benzene ug/kg 44.152.4 84 46-143ND Chlorobenzene ug/kg 45.952.4 87 29-159ND Toluene ug/kg 45.052.4 86 38-145ND Trichloroethene ug/kg 47.952.4 91 70-130ND 1,2-Dichloroethane-d4 (S)%96 69-121 4-Bromofluorobenzene (S)%98 74-115 Dibromofluoromethane (S)%98 79-116 Toluene-d8 (S)%100 88-110 Parameter Units Dup Result QualifiersRPDResult 9252579005 334138SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/kg ND 1,1,1-Trichloroethane ug/kg ND 1,1,2,2-Tetrachloroethane ug/kg ND 1,1,2-Trichloroethane ug/kg ND 1,1-Dichloroethane ug/kg ND 1,1-Dichloroethene ug/kg ND 1,1-Dichloropropene ug/kg ND 1,2,3-Trichlorobenzene ug/kg ND 1,2,3-Trichloropropane ug/kg ND 1,2,4-Trichlorobenzene ug/kg ND 1,2,4-Trimethylbenzene ug/kg ND 1,2-Dibromo-3-chloropropane ug/kg ND 1,2-Dibromoethane (EDB)ug/kg ND 1,2-Dichlorobenzene ug/kg ND 1,2-Dichloroethane ug/kg ND 1,2-Dichloropropane ug/kg ND 1,3,5-Trimethylbenzene ug/kg ND 1,3-Dichlorobenzene ug/kg ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 104 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Dup Result QualifiersRPDResult 9252579005 334138SAMPLE DUPLICATE: 1,3-Dichloropropane ug/kg ND 1,4-Dichlorobenzene ug/kg ND 2,2-Dichloropropane ug/kg ND 2-Butanone (MEK)ug/kg ND 2-Chlorotoluene ug/kg ND 2-Hexanone ug/kg ND 4-Chlorotoluene ug/kg ND 4-Methyl-2-pentanone (MIBK)ug/kg ND Acetone ug/kg 16.1J Benzene ug/kg ND Bromobenzene ug/kg ND Bromochloromethane ug/kg ND Bromodichloromethane ug/kg ND Bromoform ug/kg ND Bromomethane ug/kg ND Carbon tetrachloride ug/kg ND Chlorobenzene ug/kg ND Chloroethane ug/kg ND Chloroform ug/kg ND Chloromethane ug/kg ND cis-1,2-Dichloroethene ug/kg ND cis-1,3-Dichloropropene ug/kg ND Dibromochloromethane ug/kg ND Dibromomethane ug/kg ND Dichlorodifluoromethane ug/kg ND Diisopropyl ether ug/kg ND Ethylbenzene ug/kg ND Hexachloro-1,3-butadiene ug/kg ND Isopropylbenzene (Cumene)ug/kg ND m&p-Xylene ug/kg ND Methyl-tert-butyl ether ug/kg ND Methylene Chloride ug/kg ND n-Butylbenzene ug/kg ND n-Propylbenzene ug/kg ND Naphthalene ug/kg ND o-Xylene ug/kg ND p-Isopropyltoluene ug/kg ND sec-Butylbenzene ug/kg ND Styrene ug/kg 15.1 C8 tert-Butylbenzene ug/kg ND Tetrachloroethene ug/kg ND Toluene ug/kg ND trans-1,2-Dichloroethene ug/kg ND trans-1,3-Dichloropropene ug/kg ND Trichloroethene ug/kg ND Trichlorofluoromethane ug/kg ND Vinyl acetate ug/kg ND Vinyl chloride ug/kg ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 105 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Dup Result QualifiersRPDResult 9252579005 334138SAMPLE DUPLICATE: Xylene (Total)ug/kg ND 1,2-Dichloroethane-d4 (S)%97 4-Bromofluorobenzene (S)%94 Dibromofluoromethane (S)%98 Toluene-d8 (S)%99 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 106 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: MERP/2368 EPA 7471 EPA 7471 7471 Mercury Associated Lab Samples:9252614006, 9252614007, 9252614008, 9252614009, 9252614010, 9252614011 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:334170 Associated Lab Samples:9252614006, 9252614007, 9252614008, 9252614009, 9252614010, 9252614011 Matrix:Solid Analyzed Mercury mg/kg ND 0.0050 09/11/09 13:43 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334171LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.063.067 94 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 334172MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252614006 334173 MSD Result MSD % Rec RPD MSDMS Spike Conc. Mercury mg/kg .064 -2 75-125-33 37.0760.075 0.074 0.051 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 107 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/2699 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:9252614004, 9252614005, 9252614006, 9252614007, 9252614008, 9252614009, 9252614010, 9252614011,9252614012, 9252614013, 9252614015, 9252614016, 9252614017, 9252614018, 9252614019, 9252614020,9252614021 Parameter Units Dup Result QualifiersRPDResult 9252614004 333324SAMPLE DUPLICATE: Percent Moisture %14.9 014.9 Parameter Units Dup Result QualifiersRPDResult 9252618001 333343SAMPLE DUPLICATE: Percent Moisture %29.7 129.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 108 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/8245 EPA 8260 EPA 8260 8260 MSV 5035A Volatile Organics Associated Lab Samples:9252614004, 9252614005, 9252614013, 9252614015, 9252614016, 9252614017, 9252614018, 9252614019,9252614020 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:334866 Associated Lab Samples:9252614004, 9252614005, 9252614013, 9252614015, 9252614016, 9252614017, 9252614018, 9252614019,9252614020 Matrix:Solid Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/11/09 10:36 1,1,1-Trichloroethane ug/kg ND 5.0 09/11/09 10:36 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/11/09 10:36 1,1,2-Trichloroethane ug/kg ND 5.0 09/11/09 10:36 1,1-Dichloroethane ug/kg ND 5.0 09/11/09 10:36 1,1-Dichloroethene ug/kg ND 5.0 09/11/09 10:36 1,1-Dichloropropene ug/kg ND 5.0 09/11/09 10:36 1,2,3-Trichlorobenzene ug/kg ND 5.0 09/11/09 10:36 1,2,3-Trichloropropane ug/kg ND 5.0 09/11/09 10:36 1,2,4-Trichlorobenzene ug/kg ND 5.0 09/11/09 10:36 1,2,4-Trimethylbenzene ug/kg ND 5.0 09/11/09 10:36 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/11/09 10:36 1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/11/09 10:36 1,2-Dichlorobenzene ug/kg ND 5.0 09/11/09 10:36 1,2-Dichloroethane ug/kg ND 5.0 09/11/09 10:36 1,2-Dichloropropane ug/kg ND 5.0 09/11/09 10:36 1,3,5-Trimethylbenzene ug/kg ND 5.0 09/11/09 10:36 1,3-Dichlorobenzene ug/kg ND 5.0 09/11/09 10:36 1,3-Dichloropropane ug/kg ND 5.0 09/11/09 10:36 1,4-Dichlorobenzene ug/kg ND 5.0 09/11/09 10:36 2,2-Dichloropropane ug/kg ND 5.0 09/11/09 10:36 2-Butanone (MEK)ug/kg ND 100 09/11/09 10:36 2-Chlorotoluene ug/kg ND 5.0 09/11/09 10:36 2-Hexanone ug/kg ND 50.0 09/11/09 10:36 4-Chlorotoluene ug/kg ND 5.0 09/11/09 10:36 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/11/09 10:36 Acetone ug/kg ND 100 09/11/09 10:36 Benzene ug/kg ND 5.0 09/11/09 10:36 Bromobenzene ug/kg ND 5.0 09/11/09 10:36 Bromochloromethane ug/kg ND 5.0 09/11/09 10:36 Bromodichloromethane ug/kg ND 5.0 09/11/09 10:36 Bromoform ug/kg ND 5.0 09/11/09 10:36 Bromomethane ug/kg ND 10.0 09/11/09 10:36 Carbon tetrachloride ug/kg ND 5.0 09/11/09 10:36 Chlorobenzene ug/kg ND 5.0 09/11/09 10:36 Chloroethane ug/kg ND 10.0 09/11/09 10:36 Chloroform ug/kg ND 5.0 09/11/09 10:36 Chloromethane ug/kg ND 10.0 09/11/09 10:36 cis-1,2-Dichloroethene ug/kg ND 5.0 09/11/09 10:36 cis-1,3-Dichloropropene ug/kg ND 5.0 09/11/09 10:36 Dibromochloromethane ug/kg ND 5.0 09/11/09 10:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 109 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:334866 Associated Lab Samples:9252614004, 9252614005, 9252614013, 9252614015, 9252614016, 9252614017, 9252614018, 9252614019,9252614020 Matrix:Solid Analyzed Dibromomethane ug/kg ND 5.0 09/11/09 10:36 Dichlorodifluoromethane ug/kg ND 10.0 09/11/09 10:36 Diisopropyl ether ug/kg ND 5.0 09/11/09 10:36 Ethylbenzene ug/kg ND 5.0 09/11/09 10:36 Hexachloro-1,3-butadiene ug/kg ND 5.0 09/11/09 10:36 Isopropylbenzene (Cumene)ug/kg ND 5.0 09/11/09 10:36 m&p-Xylene ug/kg ND 10.0 09/11/09 10:36 Methyl-tert-butyl ether ug/kg ND 5.0 09/11/09 10:36 Methylene Chloride ug/kg ND 20.0 09/11/09 10:36 n-Butylbenzene ug/kg ND 5.0 09/11/09 10:36 n-Propylbenzene ug/kg ND 5.0 09/11/09 10:36 Naphthalene ug/kg ND 5.0 09/11/09 10:36 o-Xylene ug/kg ND 5.0 09/11/09 10:36 p-Isopropyltoluene ug/kg ND 5.0 09/11/09 10:36 sec-Butylbenzene ug/kg ND 5.0 09/11/09 10:36 Styrene ug/kg ND 5.0 09/11/09 10:36 tert-Butylbenzene ug/kg ND 5.0 09/11/09 10:36 Tetrachloroethene ug/kg ND 5.0 09/11/09 10:36 Toluene ug/kg ND 5.0 09/11/09 10:36 trans-1,2-Dichloroethene ug/kg ND 5.0 09/11/09 10:36 trans-1,3-Dichloropropene ug/kg ND 5.0 09/11/09 10:36 Trichloroethene ug/kg ND 5.0 09/11/09 10:36 Trichlorofluoromethane ug/kg ND 5.0 09/11/09 10:36 Vinyl acetate ug/kg ND 50.0 09/11/09 10:36 Vinyl chloride ug/kg ND 10.0 09/11/09 10:36 Xylene (Total)ug/kg ND 10.0 09/11/09 10:36 1,2-Dichloroethane-d4 (S)%95 69-121 09/11/09 10:36 4-Bromofluorobenzene (S)%98 74-115 09/11/09 10:36 Dibromofluoromethane (S)%98 79-116 09/11/09 10:36 Toluene-d8 (S)%101 88-110 09/11/09 10:36 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334867LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 55.250 110 75-137 1,1,1-Trichloroethane ug/kg 52.050 104 70-140 1,1,2,2-Tetrachloroethane ug/kg 54.550 109 74-133 1,1,2-Trichloroethane ug/kg 53.350 107 79-129 1,1-Dichloroethane ug/kg 53.150 106 72-139 1,1-Dichloroethene ug/kg 56.250 112 69-154 1,1-Dichloropropene ug/kg 57.450 115 74-138 1,2,3-Trichlorobenzene ug/kg 62.050 124 71-150 1,2,3-Trichloropropane ug/kg 54.750 109 74-135 1,2,4-Trichlorobenzene ug/kg 67.050 134 68-150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 110 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334867LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trimethylbenzene ug/kg 57.450 115 70-130 1,2-Dibromo-3-chloropropane ug/kg 49.850 100 65-146 1,2-Dibromoethane (EDB)ug/kg 56.350 113 77-136 1,2-Dichlorobenzene ug/kg 56.550 113 75-141 1,2-Dichloroethane ug/kg 52.750 105 74-134 1,2-Dichloropropane ug/kg 54.650 109 77-138 1,3,5-Trimethylbenzene ug/kg 57.050 114 65-128 1,3-Dichlorobenzene ug/kg 58.150 116 76-133 1,3-Dichloropropane ug/kg 54.050 108 79-132 1,4-Dichlorobenzene ug/kg 57.550 115 75-137 2,2-Dichloropropane ug/kg 57.350 115 73-137 2-Butanone (MEK)ug/kg 99.1J100 99 61-138 2-Chlorotoluene ug/kg 53.350 107 73-138 2-Hexanone ug/kg 102100 102 58-159 4-Chlorotoluene ug/kg 58.650 117 75-136 4-Methyl-2-pentanone (MIBK)ug/kg 102100 102 74-139 Acetone ug/kg 98.9J100 99 58-150 Benzene ug/kg 52.450 105 71-140 Bromobenzene ug/kg 54.750 109 72-144 Bromochloromethane ug/kg 54.250 108 78-133 Bromodichloromethane ug/kg 50.950 102 78-133 Bromoform ug/kg 54.450 109 74-132 Bromomethane ug/kg 94.8 L35019063-184 Carbon tetrachloride ug/kg 62.750 125 73-143 Chlorobenzene ug/kg 54.950 110 77-137 Chloroethane ug/kg 63.450 127 68-146 Chloroform ug/kg 51.850 104 75-137 Chloromethane ug/kg 63.350 127 54-143 cis-1,2-Dichloroethene ug/kg 54.550 109 71-143 cis-1,3-Dichloropropene ug/kg 56.850 114 76-133 Dibromochloromethane ug/kg 52.650 105 77-131 Dibromomethane ug/kg 54.450 109 63-184 Dichlorodifluoromethane ug/kg 69.250 138 36-173 Diisopropyl ether ug/kg 50.150 100 68-144 Ethylbenzene ug/kg 56.650 113 69-141 Hexachloro-1,3-butadiene ug/kg 56.450 113 70-152 Isopropylbenzene (Cumene)ug/kg 59.250 118 77-143 m&p-Xylene ug/kg 116100 116 72-138 Methyl-tert-butyl ether ug/kg 51.250 102 2-138 Methylene Chloride ug/kg 53.450 107 69-136 n-Butylbenzene ug/kg 61.350 123 65-128 n-Propylbenzene ug/kg 58.550 117 72-139 Naphthalene ug/kg 59.050 118 61-138 o-Xylene ug/kg 56.950 114 74-137 p-Isopropyltoluene ug/kg 59.350 119 66-128 sec-Butylbenzene ug/kg 58.550 117 72-140 Styrene ug/kg 56.050 112 76-137 tert-Butylbenzene ug/kg 56.150 112 68-141 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 111 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334867LABORATORY CONTROL SAMPLE: LCSSpike Tetrachloroethene ug/kg 58.950 118 72-136 Toluene ug/kg 52.850 106 69-139 trans-1,2-Dichloroethene ug/kg 52.850 106 72-144 trans-1,3-Dichloropropene ug/kg 57.550 115 73-135 Trichloroethene ug/kg 56.250 112 75-136 Trichlorofluoromethane ug/kg 61.150 122 69-144 Vinyl acetate ug/kg 326 L310032650-150 Vinyl chloride ug/kg 66.450 133 61-145 Xylene (Total)ug/kg 173150 115 73-138 1,2-Dichloroethane-d4 (S)%92 69-121 4-Bromofluorobenzene (S)%103 74-115 Dibromofluoromethane (S)%98 79-116 Toluene-d8 (S)%100 88-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 335287MATRIX SPIKE SAMPLE: MSSpike Result 9252614015 1,1-Dichloroethene ug/kg 43.342.3 102 33-158ND Benzene ug/kg 39.642.3 91 46-143ND Chlorobenzene ug/kg 33.142.3 78 29-159ND Toluene ug/kg 37.042.3 85 38-145ND Trichloroethene ug/kg 37.042.3 87 70-130ND 1,2-Dichloroethane-d4 (S)%102 69-121 4-Bromofluorobenzene (S)%95 74-115 Dibromofluoromethane (S)%100 79-116 Toluene-d8 (S)%99 88-110 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 335760MATRIX SPIKE SAMPLE: MSSpike Result 9252614020 1,1-Dichloroethene ug/kg 45.645.9 99 33-158ND Benzene ug/kg 45.645.9 86 46-1436.3 Chlorobenzene ug/kg 32.045.9 70 29-159ND Toluene ug/kg 36.245.9 73 38-145ND Trichloroethene ug/kg 38.145.9 83 70-130ND 1,2-Dichloroethane-d4 (S)%109 69-121 4-Bromofluorobenzene (S)%96 74-115 Dibromofluoromethane (S)%101 79-116 Toluene-d8 (S)%98 88-110 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 112 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/7947 EPA 3546 EPA 8270 8270 Solid MSSV Microwave Associated Lab Samples:9252614016, 9252614017, 9252614018, 9252614019, 9252614020, 9252614021 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:334354 Associated Lab Samples:9252614016, 9252614017, 9252614018, 9252614019, 9252614020, 9252614021 Matrix:Solid Analyzed 1,2,4-Trichlorobenzene ug/kg ND 330 09/15/09 00:28 1,2-Dichlorobenzene ug/kg ND 330 09/15/09 00:28 1,2-Diphenylhydrazine ug/kg ND 330 09/15/09 00:28 1,3-Dichlorobenzene ug/kg ND 330 09/15/09 00:28 1,4-Dichlorobenzene ug/kg ND 330 09/15/09 00:28 1-Methylnaphthalene ug/kg ND 330 09/15/09 00:28 2,4,5-Trichlorophenol ug/kg ND 330 09/15/09 00:28 2,4,6-Trichlorophenol ug/kg ND 330 09/15/09 00:28 2,4-Dichlorophenol ug/kg ND 330 09/15/09 00:28 2,4-Dimethylphenol ug/kg ND 330 09/15/09 00:28 2,4-Dinitrophenol ug/kg ND 1650 09/15/09 00:28 2,4-Dinitrotoluene ug/kg ND 330 09/15/09 00:28 2,6-Dinitrotoluene ug/kg ND 330 09/15/09 00:28 2-Chloronaphthalene ug/kg ND 330 09/15/09 00:28 2-Chlorophenol ug/kg ND 330 09/15/09 00:28 2-Methylnaphthalene ug/kg ND 330 09/15/09 00:28 2-Methylphenol(o-Cresol)ug/kg ND 330 09/15/09 00:28 2-Nitroaniline ug/kg ND 1650 09/15/09 00:28 2-Nitrophenol ug/kg ND 330 09/15/09 00:28 3&4-Methylphenol(m&p Cresol)ug/kg ND 330 09/15/09 00:28 3,3'-Dichlorobenzidine ug/kg ND 1650 09/15/09 00:28 3-Nitroaniline ug/kg ND 1650 09/15/09 00:28 4,6-Dinitro-2-methylphenol ug/kg ND 660 09/15/09 00:28 4-Bromophenylphenyl ether ug/kg ND 330 09/15/09 00:28 4-Chloro-3-methylphenol ug/kg ND 660 09/15/09 00:28 4-Chloroaniline ug/kg ND 1650 09/15/09 00:28 4-Chlorophenylphenyl ether ug/kg ND 330 09/15/09 00:28 4-Nitroaniline ug/kg ND 660 09/15/09 00:28 4-Nitrophenol ug/kg ND 1650 09/15/09 00:28 Acenaphthene ug/kg ND 330 09/15/09 00:28 Acenaphthylene ug/kg ND 330 09/15/09 00:28 Aniline ug/kg ND 330 09/15/09 00:28 Anthracene ug/kg ND 330 09/15/09 00:28 Benzo(a)anthracene ug/kg ND 330 09/15/09 00:28 Benzo(a)pyrene ug/kg ND 330 09/15/09 00:28 Benzo(b)fluoranthene ug/kg ND 330 09/15/09 00:28 Benzo(g,h,i)perylene ug/kg ND 330 09/15/09 00:28 Benzo(k)fluoranthene ug/kg ND 330 09/15/09 00:28 Benzoic Acid ug/kg ND 1650 09/15/09 00:28 Benzyl alcohol ug/kg ND 660 09/15/09 00:28 bis(2-Chloroethoxy)methane ug/kg ND 330 09/15/09 00:28 bis(2-Chloroethyl) ether ug/kg ND 330 09/15/09 00:28 bis(2-Chloroisopropyl) ether ug/kg ND 330 09/15/09 00:28 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 113 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:334354 Associated Lab Samples:9252614016, 9252614017, 9252614018, 9252614019, 9252614020, 9252614021 Matrix:Solid Analyzed bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/15/09 00:28 Butylbenzylphthalate ug/kg ND 330 09/15/09 00:28 Chrysene ug/kg ND 330 09/15/09 00:28 Di-n-butylphthalate ug/kg ND 330 09/15/09 00:28 Di-n-octylphthalate ug/kg ND 330 09/15/09 00:28 Dibenz(a,h)anthracene ug/kg ND 330 09/15/09 00:28 Dibenzofuran ug/kg ND 330 09/15/09 00:28 Diethylphthalate ug/kg ND 330 09/15/09 00:28 Dimethylphthalate ug/kg ND 330 09/15/09 00:28 Fluoranthene ug/kg ND 330 09/15/09 00:28 Fluorene ug/kg ND 330 09/15/09 00:28 Hexachloro-1,3-butadiene ug/kg ND 330 09/15/09 00:28 Hexachlorobenzene ug/kg ND 330 09/15/09 00:28 Hexachlorocyclopentadiene ug/kg ND 330 09/15/09 00:28 Hexachloroethane ug/kg ND 330 09/15/09 00:28 Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/15/09 00:28 Isophorone ug/kg ND 330 09/15/09 00:28 N-Nitroso-di-n-propylamine ug/kg ND 330 09/15/09 00:28 N-Nitrosodimethylamine ug/kg ND 330 09/15/09 00:28 N-Nitrosodiphenylamine ug/kg ND 330 09/15/09 00:28 Naphthalene ug/kg ND 330 09/15/09 00:28 Nitrobenzene ug/kg ND 330 09/15/09 00:28 Pentachlorophenol ug/kg ND 1650 09/15/09 00:28 Phenanthrene ug/kg ND 330 09/15/09 00:28 Phenol ug/kg ND 330 09/15/09 00:28 Pyrene ug/kg ND 330 09/15/09 00:28 2,4,6-Tribromophenol (S)%60 44-136 09/15/09 00:28 2-Fluorobiphenyl (S)%62 46-120 09/15/09 00:28 2-Fluorophenol (S)%39 24-120 09/15/09 00:28 Nitrobenzene-d5 (S)%50 30-150 09/15/09 00:28 Phenol-d6 (S)%43 35-120 09/15/09 00:28 Terphenyl-d14 (S)%54 38-108 09/15/09 00:28 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334355LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/kg 8821670 53 50-150 1,2-Dichlorobenzene ug/kg 10201670 61 50-150 1,2-Diphenylhydrazine ug/kg 10201670 61 43-130 1,3-Dichlorobenzene ug/kg 11301670 68 50-150 1,4-Dichlorobenzene ug/kg 12101670 72 50-150 1-Methylnaphthalene ug/kg 12501670 75 50-150 2,4,5-Trichlorophenol ug/kg 8751670 53 50-150 2,4,6-Trichlorophenol ug/kg 8641670 52 50-150 2,4-Dichlorophenol ug/kg 11301670 68 50-150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 114 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334355LABORATORY CONTROL SAMPLE: LCSSpike 2,4-Dimethylphenol ug/kg 9041670 54 50-150 2,4-Dinitrophenol ug/kg 1150J1670 69 20-111 2,4-Dinitrotoluene ug/kg 9971670 60 50-150 2,6-Dinitrotoluene ug/kg 9911670 59 50-150 2-Chloronaphthalene ug/kg 9401670 56 50-150 2-Chlorophenol ug/kg 10701670 64 50-150 2-Methylnaphthalene ug/kg 11701670 70 50-150 2-Methylphenol(o-Cresol)ug/kg 9391670 56 50-150 2-Nitroaniline ug/kg 1010J1670 60 50-150 2-Nitrophenol ug/kg 9251670 56 50-150 3&4-Methylphenol(m&p Cresol)ug/kg 8921670 53 50-150 3,3'-Dichlorobenzidine ug/kg 1040J1670 62 50-150 3-Nitroaniline ug/kg 945J1670 57 50-150 4,6-Dinitro-2-methylphenol ug/kg 9241670 55 15-136 4-Bromophenylphenyl ether ug/kg 9121670 55 50-150 4-Chloro-3-methylphenol ug/kg 11401670 68 50-150 4-Chloroaniline ug/kg 1100J1670 66 50-150 4-Chlorophenylphenyl ether ug/kg 10501670 63 50-150 4-Nitroaniline ug/kg 9031670 54 50-150 4-Nitrophenol ug/kg 1240J1670 75 33-105 Acenaphthene ug/kg 9651670 58 50-150 Acenaphthylene ug/kg 9311670 56 50-150 Aniline ug/kg 10301670 62 50-150 Anthracene ug/kg 13701670 82 50-150 Benzo(a)anthracene ug/kg 13201670 79 50-150 Benzo(a)pyrene ug/kg 9441670 57 50-150 Benzo(b)fluoranthene ug/kg 9631670 58 50-150 Benzo(g,h,i)perylene ug/kg 8491670 51 24-117 Benzo(k)fluoranthene ug/kg 10101670 61 50-150 Benzoic Acid ug/kg 274J1670 16 15-104 Benzyl alcohol ug/kg 9431670 57 50-150 bis(2-Chloroethoxy)methane ug/kg 10801670 65 50-150 bis(2-Chloroethyl) ether ug/kg 12901670 78 50-150 bis(2-Chloroisopropyl) ether ug/kg 9951670 60 50-150 bis(2-Ethylhexyl)phthalate ug/kg 13201670 79 50-150 Butylbenzylphthalate ug/kg 11901670 72 50-150 Chrysene ug/kg 13901670 83 50-150 Di-n-butylphthalate ug/kg 9841670 59 50-150 Di-n-octylphthalate ug/kg 11801670 71 50-150 Dibenz(a,h)anthracene ug/kg 11301670 68 17-128 Dibenzofuran ug/kg 8681670 52 50-150 Diethylphthalate ug/kg 10101670 61 50-150 Dimethylphthalate ug/kg 10401670 62 50-150 Fluoranthene ug/kg 10801670 65 50-150 Fluorene ug/kg 10101670 60 50-150 Hexachloro-1,3-butadiene ug/kg 8431670 51 50-150 Hexachlorobenzene ug/kg 9011670 54 50-150 Hexachlorocyclopentadiene ug/kg 11001670 66 15-114 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 115 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 334355LABORATORY CONTROL SAMPLE: LCSSpike Hexachloroethane ug/kg 8981670 54 50-150 Indeno(1,2,3-cd)pyrene ug/kg 8901670 53 19-128 Isophorone ug/kg 9321670 56 50-150 N-Nitroso-di-n-propylamine ug/kg 8871670 53 50-150 N-Nitrosodimethylamine ug/kg 8921670 54 50-150 N-Nitrosodiphenylamine ug/kg 8671670 52 50-150 Naphthalene ug/kg 9741670 58 50-150 Nitrobenzene ug/kg 11001670 66 50-150 Pentachlorophenol ug/kg 929J1670 56 15-130 Phenanthrene ug/kg 13401670 81 50-150 Phenol ug/kg 9141670 55 42-120 Pyrene ug/kg 11201670 67 50-150 2,4,6-Tribromophenol (S)%55 44-136 2-Fluorobiphenyl (S)%56 46-120 2-Fluorophenol (S)%29 24-120 Nitrobenzene-d5 (S)%58 30-150 Phenol-d6 (S)%36 35-120 Terphenyl-d14 (S)%54 38-108 Parameter Units MS Result % Rec Limits Qual% RecConc. 334356MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252614018 334357 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,2,4-Trichlorobenzene ug/kg 2140 0 50-15002140NDNDND 1,4-Dichlorobenzene ug/kg 2140 0 50-15002140NDNDND 2,4-Dinitrotoluene ug/kg 2140 0 50-15002140NDNDND 2-Chlorophenol ug/kg 2140 0 50-15002140NDNDND 4-Chloro-3-methylphenol ug/kg 2140 0 50-15002140NDNDND 4-Nitrophenol ug/kg 2140 0 50-15002140NDNDND Acenaphthene ug/kg 2140 0 50-15002140NDNDND N-Nitroso-di-n-propylamine ug/kg 2140 0 50-15002140NDNDND Pentachlorophenol ug/kg 2140 0 50-15002140NDNDND Phenol ug/kg 2g,D32140050-15002140NDNDND Pyrene ug/kg 2140 0 50-15002140NDNDND 2,4,6-Tribromophenol (S)%0 44-1360 2-Fluorobiphenyl (S)%0 46-1200 2-Fluorophenol (S)%0 24-1200 Nitrobenzene-d5 (S)%3g,D3030-1500 Phenol-d6 (S)%0 35-1200 Terphenyl-d14 (S)%0 38-1080 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 116 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/8261 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:9252614022, 9252614023, 9252614024, 9252614025 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335656 Associated Lab Samples:9252614022, 9252614023, 9252614024, 9252614025 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/13/09 01:36 1,1,1-Trichloroethane ug/L ND 1.0 09/13/09 01:36 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/13/09 01:36 1,1,2-Trichloroethane ug/L ND 1.0 09/13/09 01:36 1,1-Dichloroethane ug/L ND 1.0 09/13/09 01:36 1,1-Dichloroethene ug/L ND 1.0 09/13/09 01:36 1,1-Dichloropropene ug/L ND 1.0 09/13/09 01:36 1,2,3-Trichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,2,3-Trichloropropane ug/L ND 1.0 09/13/09 01:36 1,2,4-Trichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,2-Dibromo-3-chloropropane ug/L ND 3.0 09/13/09 01:36 1,2-Dibromoethane (EDB)ug/L ND 1.0 09/13/09 01:36 1,2-Dichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,2-Dichloroethane ug/L ND 1.0 09/13/09 01:36 1,2-Dichloropropane ug/L ND 1.0 09/13/09 01:36 1,3-Dichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,3-Dichloropropane ug/L ND 1.0 09/13/09 01:36 1,4-Dichlorobenzene ug/L ND 1.0 09/13/09 01:36 2,2-Dichloropropane ug/L ND 1.0 09/13/09 01:36 2-Butanone (MEK)ug/L ND 5.0 09/13/09 01:36 2-Chlorotoluene ug/L ND 1.0 09/13/09 01:36 2-Hexanone ug/L ND 5.0 09/13/09 01:36 4-Chlorotoluene ug/L ND 1.0 09/13/09 01:36 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/13/09 01:36 Acetone ug/L ND 25.0 09/13/09 01:36 Benzene ug/L ND 1.0 09/13/09 01:36 Bromobenzene ug/L ND 1.0 09/13/09 01:36 Bromochloromethane ug/L ND 1.0 09/13/09 01:36 Bromodichloromethane ug/L ND 1.0 09/13/09 01:36 Bromoform ug/L ND 1.0 09/13/09 01:36 Bromomethane ug/L ND 5.0 09/13/09 01:36 Carbon tetrachloride ug/L ND 1.0 09/13/09 01:36 Chlorobenzene ug/L ND 1.0 09/13/09 01:36 Chloroethane ug/L ND 1.0 09/13/09 01:36 Chloroform ug/L ND 1.0 09/13/09 01:36 Chloromethane ug/L ND 1.0 09/13/09 01:36 cis-1,2-Dichloroethene ug/L ND 1.0 09/13/09 01:36 cis-1,3-Dichloropropene ug/L ND 1.0 09/13/09 01:36 Dibromochloromethane ug/L ND 1.0 09/13/09 01:36 Dibromomethane ug/L ND 1.0 09/13/09 01:36 Dichlorodifluoromethane ug/L ND 1.0 09/13/09 01:36 Diisopropyl ether ug/L ND 1.0 09/13/09 01:36 Ethylbenzene ug/L ND 1.0 09/13/09 01:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 117 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335656 Associated Lab Samples:9252614022, 9252614023, 9252614024, 9252614025 Matrix:Water Analyzed Hexachloro-1,3-butadiene ug/L ND 1.0 09/13/09 01:36 m&p-Xylene ug/L ND 2.0 09/13/09 01:36 Methyl-tert-butyl ether ug/L ND 1.0 09/13/09 01:36 Methylene Chloride ug/L ND 2.0 09/13/09 01:36 Naphthalene ug/L ND 1.0 09/13/09 01:36 o-Xylene ug/L ND 1.0 09/13/09 01:36 p-Isopropyltoluene ug/L ND 1.0 09/13/09 01:36 Styrene ug/L ND 1.0 09/13/09 01:36 Tetrachloroethene ug/L ND 1.0 09/13/09 01:36 Toluene ug/L ND 1.0 09/13/09 01:36 trans-1,2-Dichloroethene ug/L ND 1.0 09/13/09 01:36 trans-1,3-Dichloropropene ug/L ND 1.0 09/13/09 01:36 Trichloroethene ug/L ND 1.0 09/13/09 01:36 Trichlorofluoromethane ug/L ND 1.0 09/13/09 01:36 Vinyl acetate ug/L ND 2.0 09/13/09 01:36 Vinyl chloride ug/L ND 1.0 09/13/09 01:36 1,2-Dichloroethane-d4 (S)%99 79-120 09/13/09 01:36 4-Bromofluorobenzene (S)%99 87-109 09/13/09 01:36 Dibromofluoromethane (S)%101 85-115 09/13/09 01:36 Toluene-d8 (S)%98 70-120 09/13/09 01:36 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335657LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 48.350 97 83-125 1,1,1-Trichloroethane ug/L 45.750 91 80-129 1,1,2,2-Tetrachloroethane ug/L 46.050 92 73-127 1,1,2-Trichloroethane ug/L 49.750 99 77-123 1,1-Dichloroethane ug/L 47.650 95 76-129 1,1-Dichloroethene ug/L 49.450 99 78-146 1,1-Dichloropropene ug/L 48.550 97 79-134 1,2,3-Trichlorobenzene ug/L 47.750 95 70-150 1,2,3-Trichloropropane ug/L 46.450 93 72-125 1,2,4-Trichlorobenzene ug/L 47.250 94 68-127 1,2-Dibromo-3-chloropropane ug/L 49.150 98 65-128 1,2-Dibromoethane (EDB)ug/L 50.250 100 81-125 1,2-Dichlorobenzene ug/L 48.250 96 82-126 1,2-Dichloroethane ug/L 49.050 98 72-126 1,2-Dichloropropane ug/L 49.950 100 80-127 1,3-Dichlorobenzene ug/L 46.850 94 82-124 1,3-Dichloropropane ug/L 48.850 98 79-124 1,4-Dichlorobenzene ug/L 46.050 92 79-125 2,2-Dichloropropane ug/L 42.550 85 58-140 2-Butanone (MEK)ug/L 95.0100 95 50-134 2-Chlorotoluene ug/L 45.950 92 81-126 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 118 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335657LABORATORY CONTROL SAMPLE: LCSSpike 2-Hexanone ug/L 92.7100 93 58-138 4-Chlorotoluene ug/L 47.950 96 82-126 4-Methyl-2-pentanone (MIBK)ug/L 95.8100 96 70-131 Acetone ug/L 103100 103 50-146 Benzene ug/L 46.650 93 78-128 Bromobenzene ug/L 48.350 97 81-127 Bromochloromethane ug/L 46.550 93 73-124 Bromodichloromethane ug/L 44.950 90 81-125 Bromoform ug/L 45.650 91 71-125 Bromomethane ug/L 63.350 127 50-150 Carbon tetrachloride ug/L 46.150 92 81-137 Chlorobenzene ug/L 46.750 93 82-126 Chloroethane ug/L 51.550 103 69-140 Chloroform ug/L 44.850 90 77-129 Chloromethane ug/L 44.350 89 54-139 cis-1,2-Dichloroethene ug/L 48.750 97 76-133 cis-1,3-Dichloropropene ug/L 49.050 98 76-127 Dibromochloromethane ug/L 44.550 89 77-125 Dibromomethane ug/L 47.550 95 77-125 Dichlorodifluoromethane ug/L 53.050 106 50-150 Diisopropyl ether ug/L 48.650 97 74-131 Ethylbenzene ug/L 47.450 95 80-127 Hexachloro-1,3-butadiene ug/L 43.850 88 78-145 m&p-Xylene ug/L 98.0100 98 82-127 Methyl-tert-butyl ether ug/L 50.250 100 71-130 Methylene Chloride ug/L 46.450 93 67-133 Naphthalene ug/L 50.350 101 52-136 o-Xylene ug/L 48.750 97 83-124 p-Isopropyltoluene ug/L 48.350 97 73-122 Styrene ug/L 48.250 96 80-130 Tetrachloroethene ug/L 46.450 93 78-128 Toluene ug/L 46.250 92 76-126 trans-1,2-Dichloroethene ug/L 44.750 89 78-134 trans-1,3-Dichloropropene ug/L 50.350 101 75-125 Trichloroethene ug/L 48.150 96 79-127 Trichlorofluoromethane ug/L 48.450 97 76-148 Vinyl acetate ug/L 82.4100 82 50-150 Vinyl chloride ug/L 51.850 104 67-143 1,2-Dichloroethane-d4 (S)%99 79-120 4-Bromofluorobenzene (S)%99 87-109 Dibromofluoromethane (S)%102 85-115 Toluene-d8 (S)%99 70-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 119 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A Parameter Units MS Result % Rec Limits Qual% RecConc. 335658MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252704001 335659 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1-Dichloroethene ug/L 50 100 60-150105 550ND49.8 52.3 Benzene ug/L 50 92 74-13696 450ND45.8 47.9 Chlorobenzene ug/L 50 90 79-13594 450ND45.2 47.0 Toluene ug/L 50 91 73-13195 450ND45.8 47.5 Trichloroethene ug/L 50 92 73-13196 450ND46.2 48.1 1,2-Dichloroethane-d4 (S)%98 79-12098 4-Bromofluorobenzene (S)%98 87-109101 Dibromofluoromethane (S)%100 85-115100 Toluene-d8 (S)%99 70-120100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 120 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: GCSV/6192 9071B ASE 9071B ASE 9071B SGT-HEM, TPH Gravimetric Associated Lab Samples:9252614018, 9252614019 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:333442 Associated Lab Samples:9252614018, 9252614019 Matrix:Solid Analyzed Total Petroleum Hydrocarbons mg/kg ND 70.0 09/15/09 17:56 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 333443LABORATORY CONTROL SAMPLE: LCSSpike Total Petroleum Hydrocarbons mg/kg 620667 93 78-114 Parameter Units MS Result % Rec Limits Qual% RecConc. 333444MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252614018 333445 MSD Result MSD % Rec RPD MSDMS Spike Conc. Total Petroleum Hydrocarbons mg/kg 855 89 78-11493 4855141906940 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 121 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/2698 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:9252614001, 9252614002, 9252614003 Parameter Units Dup Result QualifiersRPDResult 9252574002 333322SAMPLE DUPLICATE: Percent Moisture %29.3 430.5 Parameter Units Dup Result QualifiersRPDResult 9252614003 333323SAMPLE DUPLICATE: Percent Moisture %6.8 145.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 122 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Pace Project No.: Project: 9252614 1 FAIRVIEW RD 1411-09-040A DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the 2 remaining acidsurrogates.1g Matrix spike recoveries not evaluated against control limits due to sample dilution.2g Surrogate recoveries not evaluated against control limits due to sample dilution.3g Result may be biased high due to carryover from previously analyzed sample.C8 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 The internal standard response is below criteria. Results may be biased high.IS Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.L3 Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0 RPD value was outside control limits.R1 Surrogate recovery outside laboratory control limits.S0 Surrogate recovery not evaluated against control limits due to sample dilution.S4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 10/14/2009 03:17 PM Page 123 of 123 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 APPENDIX V (GROUNDWATER LABORATORY REPORT) September 24, 2009 LIMS USE: FR - SCOTT SPINNER LIMS OBJECT ID: 9252704 9252704 Project: Pace Project No.: RE: Mr. Scott SpinnerS&ME44 Buck Shoals RoadArden, NC 28704 1 FAIRVIEW ROAD 1411-09-040A Dear Mr. Spinner: Enclosed are the analytical results for sample(s) received by the laboratory on September 09, 2009. The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Brandon Helton for Kevin Herringkevin.herring@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Charlotte Certification IDsWest Virginia Certification #: 357Virginia Certification #: 00213Tennessee Certification #: 04010South Carolina Drinking Water Cert. #: 990060003South Carolina Certification #: 990060001Pennsylvania Certification #: 68-00784Connecticut Certification #: PH-0104 North Carolina Field Services Certification #: 5342North Carolina Drinking Water Certification #: 37706New Jersey Certification #: NC012Louisiana/LELAP Certification #: 04034Kentucky UST Certification #: 84Florida/NELAP Certification #: E87627North Carolina Wastewater Certification #: 12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 9252704001 1 FAIR-TW1-09-09 EPA 8260 63 PASI-CAW EPA 8270 75 PASI-CBET 9252704002 1 FAIR-TW2-09-09 EPA 8260 63 PASI-CMCK EPA 8270 75 PASI-CBET 9252704003 1 FAIR-TW3-09-09 EPA 8260 63 PASI-CMCK EPA 8270 75 PASI-CBET 9252704004 1 FAIR-DUPLICATE-09-09 EPA 8260 63 PASI-CMCK EPA 8270 75 PASI-CBET 9252704005 1 FAIR-MW1-09-09 EPA 8260 63 PASI-CAW EPA 8270 75 PASI-CBET 9252704006 1 FAIR-MW2-09-09 EPA 8260 63 PASI-CAW EPA 8270 75 PASI-CBET 9252704007 1 FAIR-FIELDBLANK-09-09 EPA 8260 63 PASI-CAW 9252704008 1 FAIR-TRIPBLANK1-09-09 EPA 8260 63 PASI-CAW 9252704009 1 FAIR-TRIPBLANK2-09-09 EPA 8260 63 PASI-CAW REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW1-09-09 Lab ID:9252704001 Collected:09/09/09 09:10 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 01:54 83-32-909/15/09 09:0012.3 Acenaphthylene ND ug/L 1 09/18/09 01:54 208-96-809/15/09 09:0012.3 Aniline ND ug/L 1 09/18/09 01:54 62-53-309/15/09 09:0012.3 Anthracene ND ug/L 1 09/18/09 01:54 120-12-709/15/09 09:0012.3 Benzo(a)anthracene ND ug/L 1 09/18/09 01:54 56-55-309/15/09 09:0012.3 Benzo(a)pyrene ND ug/L 1 09/18/09 01:54 50-32-809/15/09 09:0012.3 Benzo(b)fluoranthene ND ug/L 1 09/18/09 01:54 205-99-209/15/09 09:0012.3 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 01:54 191-24-209/15/09 09:0012.3 Benzo(k)fluoranthene ND ug/L 1 09/18/09 01:54 207-08-909/15/09 09:0012.3 Benzoic Acid ND ug/L 1 09/18/09 01:54 65-85-009/15/09 09:0061.7 Benzyl alcohol ND ug/L 1 09/18/09 01:54 100-51-609/15/09 09:0024.7 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 01:54 101-55-309/15/09 09:0012.3 Butylbenzylphthalate ND ug/L 1 09/18/09 01:54 85-68-709/15/09 09:0012.3 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 01:54 59-50-709/15/09 09:0024.7 4-Chloroaniline ND ug/L 1 09/18/09 01:54 106-47-809/15/09 09:0061.7 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 01:54 111-91-109/15/09 09:0012.3 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 01:54 111-44-409/15/09 09:0012.3 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 01:54 108-60-109/15/09 09:0012.3 2-Chloronaphthalene ND ug/L 1 09/18/09 01:54 91-58-709/15/09 09:0012.3 2-Chlorophenol ND ug/L 1 09/18/09 01:54 95-57-809/15/09 09:0012.3 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 01:54 7005-72-309/15/09 09:0012.3 Chrysene ND ug/L 1 09/18/09 01:54 218-01-909/15/09 09:0012.3 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 01:54 53-70-309/15/09 09:0012.3 Dibenzofuran ND ug/L 1 09/18/09 01:54 132-64-909/15/09 09:0012.3 1,2-Dichlorobenzene ND ug/L 1 09/18/09 01:54 95-50-109/15/09 09:0012.3 1,3-Dichlorobenzene ND ug/L 1 09/18/09 01:54 541-73-109/15/09 09:0012.3 1,4-Dichlorobenzene ND ug/L 1 09/18/09 01:54 106-46-709/15/09 09:0012.3 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 01:54 91-94-109/15/09 09:0061.7 2,4-Dichlorophenol ND ug/L 1 09/18/09 01:54 120-83-209/15/09 09:0012.3 Diethylphthalate ND ug/L 1 09/18/09 01:54 84-66-209/15/09 09:0012.3 2,4-Dimethylphenol ND ug/L 1 09/18/09 01:54 105-67-909/15/09 09:0012.3 Dimethylphthalate ND ug/L 1 09/18/09 01:54 131-11-309/15/09 09:0012.3 Di-n-butylphthalate ND ug/L 1 09/18/09 01:54 84-74-209/15/09 09:0012.3 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 01:54 534-52-109/15/09 09:0024.7 2,4-Dinitrophenol ND ug/L 1 09/18/09 01:54 51-28-509/15/09 09:0061.7 2,4-Dinitrotoluene ND ug/L 1 09/18/09 01:54 121-14-209/15/09 09:0012.3 2,6-Dinitrotoluene ND ug/L 1 09/18/09 01:54 606-20-209/15/09 09:0012.3 Di-n-octylphthalate ND ug/L 1 09/18/09 01:54 117-84-009/15/09 09:0012.3 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 01:54 122-66-709/15/09 09:0012.3 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 01:54 117-81-709/15/09 09:0012.3 Fluoranthene ND ug/L 1 09/18/09 01:54 206-44-009/15/09 09:0012.3 Fluorene ND ug/L 1 09/18/09 01:54 86-73-709/15/09 09:0012.3 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 01:54 87-68-309/15/09 09:0012.3 Hexachlorobenzene ND ug/L 1 09/18/09 01:54 118-74-109/15/09 09:0012.3 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 01:54 77-47-409/15/09 09:0012.3 Hexachloroethane ND ug/L 1 09/18/09 01:54 67-72-109/15/09 09:0012.3 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 01:54 193-39-509/15/09 09:0012.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 4 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW1-09-09 Lab ID:9252704001 Collected:09/09/09 09:10 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Isophorone ND ug/L 1 09/18/09 01:54 78-59-109/15/09 09:0012.3 1-Methylnaphthalene ND ug/L 1 09/18/09 01:54 90-12-009/15/09 09:0012.3 2-Methylnaphthalene 12.6 ug/L 1 09/18/09 01:54 91-57-609/15/09 09:0012.3 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 01:54 95-48-709/15/09 09:0012.3 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 01:5409/15/09 09:0012.3 Naphthalene ND ug/L 1 09/18/09 01:54 91-20-309/15/09 09:0012.3 2-Nitroaniline ND ug/L 1 09/18/09 01:54 88-74-409/15/09 09:0061.7 3-Nitroaniline ND ug/L 1 09/18/09 01:54 99-09-209/15/09 09:0061.7 4-Nitroaniline ND ug/L 1 09/18/09 01:54 100-01-609/15/09 09:0061.7 Nitrobenzene ND ug/L 1 09/18/09 01:54 98-95-309/15/09 09:0012.3 2-Nitrophenol ND ug/L 1 09/18/09 01:54 88-75-509/15/09 09:0012.3 4-Nitrophenol ND ug/L 1 09/18/09 01:54 100-02-709/15/09 09:0061.7 N-Nitrosodimethylamine ND ug/L 1 09/18/09 01:54 62-75-909/15/09 09:0012.3 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 01:54 621-64-709/15/09 09:0012.3 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 01:54 86-30-609/15/09 09:0012.3 Pentachlorophenol ND ug/L 1 09/18/09 01:54 87-86-509/15/09 09:0061.7 Phenanthrene ND ug/L 1 09/18/09 01:54 85-01-809/15/09 09:0012.3 Phenol ND ug/L 1 09/18/09 01:54 108-95-209/15/09 09:0012.3 Pyrene ND ug/L 1 09/18/09 01:54 129-00-009/15/09 09:0012.3 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 01:54 120-82-109/15/09 09:0012.3 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 01:54 95-95-409/15/09 09:0012.3 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 01:54 88-06-209/15/09 09:0012.3 Nitrobenzene-d5 (S)64 %1 09/18/09 01:54 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)53 %1 09/18/09 01:54 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)60 %1 09/18/09 01:54 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)30 %1 09/18/09 01:54 13127-88-309/15/09 09:0025-150 2-Fluorophenol (S)27 %1 09/18/09 01:54 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)64 %1 09/18/09 01:54 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 04:29 67-64-125.0 Benzene ND ug/L 1 09/13/09 04:29 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 04:29 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 04:29 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 04:29 75-27-41.0 Bromoform ND ug/L 1 09/13/09 04:29 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 04:29 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 04:29 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 04:29 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 04:29 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 04:29 75-00-31.0 Chloroform ND ug/L 1 09/13/09 04:29 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 04:29 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 04:29 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 04:29 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 04:29 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 04:29 124-48-11.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 5 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW1-09-09 Lab ID:9252704001 Collected:09/09/09 09:10 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 04:29 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 04:29 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 04:29 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 04:29 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 04:29 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 04:29 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 04:29 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 04:29 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 04:29 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 04:29 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 04:29 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 04:29 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 04:29 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 04:29 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 04:29 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 04:29 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 04:29 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 04:29 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 04:29 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 04:29 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 04:29 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 04:29 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 04:29 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 04:29 108-10-15.0 Methyl-tert-butyl ether 3.3 ug/L 1 09/13/09 04:29 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 04:29 91-20-31.0 Styrene ND ug/L 1 09/13/09 04:29 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 04:29 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 04:29 79-34-51.0 Tetrachloroethene ND ug/L 1 09/13/09 04:29 127-18-41.0 Toluene ND ug/L 1 09/13/09 04:29 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 04:29 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 04:29 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 04:29 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 04:29 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 04:29 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 04:29 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 04:29 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 04:29 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 04:29 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 04:29 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 04:29 95-47-61.0 4-Bromofluorobenzene (S)98 %1 09/13/09 04:29 460-00-487-109 Dibromofluoromethane (S)100 %1 09/13/09 04:29 1868-53-785-115 1,2-Dichloroethane-d4 (S)99 %1 09/13/09 04:29 17060-07-079-120 Toluene-d8 (S)98 %1 09/13/09 04:29 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 6 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW2-09-09 Lab ID:9252704002 Collected:09/09/09 10:20 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 02:17 83-32-909/15/09 09:0011.8 Acenaphthylene ND ug/L 1 09/18/09 02:17 208-96-809/15/09 09:0011.8 Aniline ND ug/L 1 09/18/09 02:17 62-53-309/15/09 09:0011.8 Anthracene ND ug/L 1 09/18/09 02:17 120-12-709/15/09 09:0011.8 Benzo(a)anthracene ND ug/L 1 09/18/09 02:17 56-55-309/15/09 09:0011.8 Benzo(a)pyrene ND ug/L 1 09/18/09 02:17 50-32-809/15/09 09:0011.8 Benzo(b)fluoranthene ND ug/L 1 09/18/09 02:17 205-99-209/15/09 09:0011.8 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 02:17 191-24-209/15/09 09:0011.8 Benzo(k)fluoranthene ND ug/L 1 09/18/09 02:17 207-08-909/15/09 09:0011.8 Benzoic Acid ND ug/L 1 09/18/09 02:17 65-85-009/15/09 09:0058.8 Benzyl alcohol ND ug/L 1 09/18/09 02:17 100-51-609/15/09 09:0023.5 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 02:17 101-55-309/15/09 09:0011.8 Butylbenzylphthalate ND ug/L 1 09/18/09 02:17 85-68-709/15/09 09:0011.8 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 02:17 59-50-709/15/09 09:0023.5 4-Chloroaniline ND ug/L 1 09/18/09 02:17 106-47-809/15/09 09:0058.8 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 02:17 111-91-109/15/09 09:0011.8 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 02:17 111-44-409/15/09 09:0011.8 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 02:17 108-60-109/15/09 09:0011.8 2-Chloronaphthalene ND ug/L 1 09/18/09 02:17 91-58-709/15/09 09:0011.8 2-Chlorophenol ND ug/L 1 09/18/09 02:17 95-57-809/15/09 09:0011.8 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 02:17 7005-72-309/15/09 09:0011.8 Chrysene ND ug/L 1 09/18/09 02:17 218-01-909/15/09 09:0011.8 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 02:17 53-70-309/15/09 09:0011.8 Dibenzofuran ND ug/L 1 09/18/09 02:17 132-64-909/15/09 09:0011.8 1,2-Dichlorobenzene ND ug/L 1 09/18/09 02:17 95-50-109/15/09 09:0011.8 1,3-Dichlorobenzene ND ug/L 1 09/18/09 02:17 541-73-109/15/09 09:0011.8 1,4-Dichlorobenzene ND ug/L 1 09/18/09 02:17 106-46-709/15/09 09:0011.8 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 02:17 91-94-109/15/09 09:0058.8 2,4-Dichlorophenol ND ug/L 1 09/18/09 02:17 120-83-209/15/09 09:0011.8 Diethylphthalate ND ug/L 1 09/18/09 02:17 84-66-209/15/09 09:0011.8 2,4-Dimethylphenol ND ug/L 1 09/18/09 02:17 105-67-909/15/09 09:0011.8 Dimethylphthalate ND ug/L 1 09/18/09 02:17 131-11-309/15/09 09:0011.8 Di-n-butylphthalate ND ug/L 1 09/18/09 02:17 84-74-209/15/09 09:0011.8 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 02:17 534-52-109/15/09 09:0023.5 2,4-Dinitrophenol ND ug/L 1 09/18/09 02:17 51-28-509/15/09 09:0058.8 2,4-Dinitrotoluene ND ug/L 1 09/18/09 02:17 121-14-209/15/09 09:0011.8 2,6-Dinitrotoluene ND ug/L 1 09/18/09 02:17 606-20-209/15/09 09:0011.8 Di-n-octylphthalate ND ug/L 1 09/18/09 02:17 117-84-009/15/09 09:0011.8 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 02:17 122-66-709/15/09 09:0011.8 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 02:17 117-81-709/15/09 09:0011.8 Fluoranthene ND ug/L 1 09/18/09 02:17 206-44-009/15/09 09:0011.8 Fluorene ND ug/L 1 09/18/09 02:17 86-73-709/15/09 09:0011.8 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 02:17 87-68-309/15/09 09:0011.8 Hexachlorobenzene ND ug/L 1 09/18/09 02:17 118-74-109/15/09 09:0011.8 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 02:17 77-47-409/15/09 09:0011.8 Hexachloroethane ND ug/L 1 09/18/09 02:17 67-72-109/15/09 09:0011.8 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 02:17 193-39-509/15/09 09:0011.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 7 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW2-09-09 Lab ID:9252704002 Collected:09/09/09 10:20 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Isophorone ND ug/L 1 09/18/09 02:17 78-59-109/15/09 09:0011.8 1-Methylnaphthalene ND ug/L 1 09/18/09 02:17 90-12-009/15/09 09:0011.8 2-Methylnaphthalene ND ug/L 1 09/18/09 02:17 91-57-609/15/09 09:0011.8 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 02:17 95-48-709/15/09 09:0011.8 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 02:1709/15/09 09:0011.8 Naphthalene ND ug/L 1 09/18/09 02:17 91-20-309/15/09 09:0011.8 2-Nitroaniline ND ug/L 1 09/18/09 02:17 88-74-409/15/09 09:0058.8 3-Nitroaniline ND ug/L 1 09/18/09 02:17 99-09-209/15/09 09:0058.8 4-Nitroaniline ND ug/L 1 09/18/09 02:17 100-01-609/15/09 09:0058.8 Nitrobenzene ND ug/L 1 09/18/09 02:17 98-95-309/15/09 09:0011.8 2-Nitrophenol ND ug/L 1 09/18/09 02:17 88-75-509/15/09 09:0011.8 4-Nitrophenol ND ug/L 1 09/18/09 02:17 100-02-709/15/09 09:0058.8 N-Nitrosodimethylamine ND ug/L 1 09/18/09 02:17 62-75-909/15/09 09:0011.8 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 02:17 621-64-709/15/09 09:0011.8 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 02:17 86-30-609/15/09 09:0011.8 Pentachlorophenol ND ug/L 1 09/18/09 02:17 87-86-509/15/09 09:0058.8 Phenanthrene ND ug/L 1 09/18/09 02:17 85-01-809/15/09 09:0011.8 Phenol ND ug/L 1 09/18/09 02:17 108-95-209/15/09 09:0011.8 Pyrene ND ug/L 1 09/18/09 02:17 129-00-009/15/09 09:0011.8 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 02:17 120-82-109/15/09 09:0011.8 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 02:17 95-95-409/15/09 09:0011.8 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 02:17 88-06-209/15/09 09:0011.8 Nitrobenzene-d5 (S)60 %1 09/18/09 02:17 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)66 %1 09/18/09 02:17 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)94 %1 09/18/09 02:17 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)28 %1 09/18/09 02:17 13127-88-309/15/09 09:0025-150 2-Fluorophenol (S)36 %1 09/18/09 02:17 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)58 %1 09/18/09 02:17 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/21/09 06:20 67-64-125.0 Benzene 4.9 ug/L 1 09/21/09 06:20 71-43-21.0 Bromobenzene ND ug/L 1 09/21/09 06:20 108-86-11.0 Bromochloromethane ND ug/L 1 09/21/09 06:20 74-97-51.0 Bromodichloromethane ND ug/L 1 09/21/09 06:20 75-27-41.0 Bromoform ND ug/L 1 09/21/09 06:20 75-25-21.0 Bromomethane ND ug/L 1 09/21/09 06:20 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/21/09 06:20 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/21/09 06:20 56-23-51.0 Chlorobenzene ND ug/L 1 09/21/09 06:20 108-90-71.0 Chloroethane ND ug/L 1 09/21/09 06:20 75-00-31.0 Chloroform ND ug/L 1 09/21/09 06:20 67-66-31.0 Chloromethane ND ug/L 1 09/21/09 06:20 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/21/09 06:20 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/21/09 06:20 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/21/09 06:20 96-12-83.0 Dibromochloromethane ND ug/L 1 09/21/09 06:20 124-48-11.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 8 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW2-09-09 Lab ID:9252704002 Collected:09/09/09 10:20 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 09/21/09 06:20 106-93-41.0 Dibromomethane ND ug/L 1 09/21/09 06:20 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/21/09 06:20 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/21/09 06:20 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/21/09 06:20 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/21/09 06:20 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/21/09 06:20 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/21/09 06:20 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/21/09 06:20 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/21/09 06:20 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/21/09 06:20 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/21/09 06:20 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/21/09 06:20 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/21/09 06:20 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/21/09 06:20 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/21/09 06:20 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/21/09 06:20 10061-02-61.0 Diisopropyl ether 2.5 ug/L 1 09/21/09 06:20 108-20-31.0 Ethylbenzene 3.4 ug/L 1 09/21/09 06:20 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/21/09 06:20 87-68-31.0 2-Hexanone ND ug/L 1 09/21/09 06:20 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/21/09 06:20 99-87-61.0 Methylene Chloride ND ug/L 1 09/21/09 06:20 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/21/09 06:20 108-10-15.0 Methyl-tert-butyl ether 4.9 ug/L 1 09/21/09 06:20 1634-04-41.0 Naphthalene 8.9 ug/L 1 09/21/09 06:20 91-20-31.0 Styrene ND ug/L 1 09/21/09 06:20 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/21/09 06:20 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/21/09 06:20 79-34-51.0 Tetrachloroethene ND ug/L 1 09/21/09 06:20 127-18-41.0 Toluene 2.2 ug/L 1 09/21/09 06:20 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/21/09 06:20 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/21/09 06:20 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/21/09 06:20 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/21/09 06:20 79-00-51.0 Trichloroethene ND ug/L 1 09/21/09 06:20 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/21/09 06:20 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/21/09 06:20 96-18-41.0 Vinyl acetate ND ug/L 1 09/21/09 06:20 108-05-42.0 Vinyl chloride ND ug/L 1 09/21/09 06:20 75-01-41.0 m&p-Xylene 3.5 ug/L 1 09/21/09 06:20 1330-20-72.0 o-Xylene ND ug/L 1 09/21/09 06:20 95-47-61.0 4-Bromofluorobenzene (S)100 %1 09/21/09 06:20 460-00-487-109 Dibromofluoromethane (S)102 %1 09/21/09 06:20 1868-53-785-115 1,2-Dichloroethane-d4 (S)111 %1 09/21/09 06:20 17060-07-079-120 Toluene-d8 (S)98 %1 09/21/09 06:20 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 9 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW3-09-09 Lab ID:9252704003 Collected:09/09/09 11:15 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 02:39 83-32-909/15/09 09:0013.0 Acenaphthylene ND ug/L 1 09/18/09 02:39 208-96-809/15/09 09:0013.0 Aniline ND ug/L 1 09/18/09 02:39 62-53-309/15/09 09:0013.0 Anthracene ND ug/L 1 09/18/09 02:39 120-12-709/15/09 09:0013.0 Benzo(a)anthracene ND ug/L 1 09/18/09 02:39 56-55-309/15/09 09:0013.0 Benzo(a)pyrene ND ug/L 1 09/18/09 02:39 50-32-809/15/09 09:0013.0 Benzo(b)fluoranthene ND ug/L 1 09/18/09 02:39 205-99-209/15/09 09:0013.0 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 02:39 191-24-209/15/09 09:0013.0 Benzo(k)fluoranthene ND ug/L 1 09/18/09 02:39 207-08-909/15/09 09:0013.0 Benzoic Acid ND ug/L 1 09/18/09 02:39 65-85-009/15/09 09:0064.9 Benzyl alcohol ND ug/L 1 09/18/09 02:39 100-51-609/15/09 09:0026.0 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 02:39 101-55-309/15/09 09:0013.0 Butylbenzylphthalate ND ug/L 1 09/18/09 02:39 85-68-709/15/09 09:0013.0 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 02:39 59-50-709/15/09 09:0026.0 4-Chloroaniline ND ug/L 1 09/18/09 02:39 106-47-809/15/09 09:0064.9 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 02:39 111-91-109/15/09 09:0013.0 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 02:39 111-44-409/15/09 09:0013.0 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 02:39 108-60-109/15/09 09:0013.0 2-Chloronaphthalene ND ug/L 1 09/18/09 02:39 91-58-709/15/09 09:0013.0 2-Chlorophenol ND ug/L 1 09/18/09 02:39 95-57-809/15/09 09:0013.0 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 02:39 7005-72-309/15/09 09:0013.0 Chrysene ND ug/L 1 09/18/09 02:39 218-01-909/15/09 09:0013.0 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 02:39 53-70-309/15/09 09:0013.0 Dibenzofuran ND ug/L 1 09/18/09 02:39 132-64-909/15/09 09:0013.0 1,2-Dichlorobenzene ND ug/L 1 09/18/09 02:39 95-50-109/15/09 09:0013.0 1,3-Dichlorobenzene ND ug/L 1 09/18/09 02:39 541-73-109/15/09 09:0013.0 1,4-Dichlorobenzene ND ug/L 1 09/18/09 02:39 106-46-709/15/09 09:0013.0 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 02:39 91-94-109/15/09 09:0064.9 2,4-Dichlorophenol ND ug/L 1 09/18/09 02:39 120-83-209/15/09 09:0013.0 Diethylphthalate ND ug/L 1 09/18/09 02:39 84-66-209/15/09 09:0013.0 2,4-Dimethylphenol ND ug/L 1 09/18/09 02:39 105-67-909/15/09 09:0013.0 Dimethylphthalate ND ug/L 1 09/18/09 02:39 131-11-309/15/09 09:0013.0 Di-n-butylphthalate ND ug/L 1 09/18/09 02:39 84-74-209/15/09 09:0013.0 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 02:39 534-52-109/15/09 09:0026.0 2,4-Dinitrophenol ND ug/L 1 09/18/09 02:39 51-28-509/15/09 09:0064.9 2,4-Dinitrotoluene ND ug/L 1 09/18/09 02:39 121-14-209/15/09 09:0013.0 2,6-Dinitrotoluene ND ug/L 1 09/18/09 02:39 606-20-209/15/09 09:0013.0 Di-n-octylphthalate ND ug/L 1 09/18/09 02:39 117-84-009/15/09 09:0013.0 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 02:39 122-66-709/15/09 09:0013.0 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 02:39 117-81-709/15/09 09:0013.0 Fluoranthene ND ug/L 1 09/18/09 02:39 206-44-009/15/09 09:0013.0 Fluorene ND ug/L 1 09/18/09 02:39 86-73-709/15/09 09:0013.0 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 02:39 87-68-309/15/09 09:0013.0 Hexachlorobenzene ND ug/L 1 09/18/09 02:39 118-74-109/15/09 09:0013.0 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 02:39 77-47-409/15/09 09:0013.0 Hexachloroethane ND ug/L 1 09/18/09 02:39 67-72-109/15/09 09:0013.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 02:39 193-39-509/15/09 09:0013.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 10 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW3-09-09 Lab ID:9252704003 Collected:09/09/09 11:15 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Isophorone ND ug/L 1 09/18/09 02:39 78-59-109/15/09 09:0013.0 1-Methylnaphthalene ND ug/L 1 09/18/09 02:39 90-12-009/15/09 09:0013.0 2-Methylnaphthalene 18.4 ug/L 1 09/18/09 02:39 91-57-609/15/09 09:0013.0 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 02:39 95-48-709/15/09 09:0013.0 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 02:3909/15/09 09:0013.0 Naphthalene ND ug/L 1 09/18/09 02:39 91-20-309/15/09 09:0013.0 2-Nitroaniline ND ug/L 1 09/18/09 02:39 88-74-409/15/09 09:0064.9 3-Nitroaniline ND ug/L 1 09/18/09 02:39 99-09-209/15/09 09:0064.9 4-Nitroaniline ND ug/L 1 09/18/09 02:39 100-01-609/15/09 09:0064.9 Nitrobenzene ND ug/L 1 09/18/09 02:39 98-95-309/15/09 09:0013.0 2-Nitrophenol ND ug/L 1 09/18/09 02:39 88-75-509/15/09 09:0013.0 4-Nitrophenol ND ug/L 1 09/18/09 02:39 100-02-709/15/09 09:0064.9 N-Nitrosodimethylamine ND ug/L 1 09/18/09 02:39 62-75-909/15/09 09:0013.0 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 02:39 621-64-709/15/09 09:0013.0 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 02:39 86-30-609/15/09 09:0013.0 Pentachlorophenol ND ug/L 1 09/18/09 02:39 87-86-509/15/09 09:0064.9 Phenanthrene ND ug/L 1 09/18/09 02:39 85-01-809/15/09 09:0013.0 Phenol ND ug/L 1 09/18/09 02:39 108-95-209/15/09 09:0013.0 Pyrene ND ug/L 1 09/18/09 02:39 129-00-009/15/09 09:0013.0 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 02:39 120-82-109/15/09 09:0013.0 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 02:39 95-95-409/15/09 09:0013.0 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 02:39 88-06-209/15/09 09:0013.0 Nitrobenzene-d5 (S)49 %1 09/18/09 02:39 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)57 %1 09/18/09 02:39 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)68 %1 09/18/09 02:39 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)26 %1 09/18/09 02:39 13127-88-309/15/09 09:0025-150 2-Fluorophenol (S)33 %1 09/18/09 02:39 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)46 %1 09/18/09 02:39 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 10 09/21/09 07:34 67-64-1250 Benzene 1870 ug/L 10 09/21/09 07:34 71-43-210.0 Bromobenzene ND ug/L 10 09/21/09 07:34 108-86-110.0 Bromochloromethane ND ug/L 10 09/21/09 07:34 74-97-510.0 Bromodichloromethane ND ug/L 10 09/21/09 07:34 75-27-410.0 Bromoform ND ug/L 10 09/21/09 07:34 75-25-210.0 Bromomethane ND ug/L 10 09/21/09 07:34 74-83-950.0 2-Butanone (MEK)ND ug/L 10 09/21/09 07:34 78-93-350.0 Carbon tetrachloride ND ug/L 10 09/21/09 07:34 56-23-510.0 Chlorobenzene ND ug/L 10 09/21/09 07:34 108-90-710.0 Chloroethane ND ug/L 10 09/21/09 07:34 75-00-310.0 Chloroform ND ug/L 10 09/21/09 07:34 67-66-310.0 Chloromethane ND ug/L 10 09/21/09 07:34 74-87-310.0 2-Chlorotoluene ND ug/L 10 09/21/09 07:34 95-49-810.0 4-Chlorotoluene ND ug/L 10 09/21/09 07:34 106-43-410.0 1,2-Dibromo-3-chloropropane ND ug/L 10 09/21/09 07:34 96-12-830.0 Dibromochloromethane ND ug/L 10 09/21/09 07:34 124-48-110.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 11 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TW3-09-09 Lab ID:9252704003 Collected:09/09/09 11:15 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 10 09/21/09 07:34 106-93-410.0 Dibromomethane ND ug/L 10 09/21/09 07:34 74-95-310.0 1,2-Dichlorobenzene ND ug/L 10 09/21/09 07:34 95-50-110.0 1,3-Dichlorobenzene ND ug/L 10 09/21/09 07:34 541-73-110.0 1,4-Dichlorobenzene ND ug/L 10 09/21/09 07:34 106-46-710.0 Dichlorodifluoromethane ND ug/L 10 09/21/09 07:34 75-71-810.0 1,1-Dichloroethane ND ug/L 10 09/21/09 07:34 75-34-310.0 1,2-Dichloroethane ND ug/L 10 09/21/09 07:34 107-06-210.0 1,1-Dichloroethene ND ug/L 10 09/21/09 07:34 75-35-410.0 cis-1,2-Dichloroethene ND ug/L 10 09/21/09 07:34 156-59-210.0 trans-1,2-Dichloroethene ND ug/L 10 09/21/09 07:34 156-60-510.0 1,2-Dichloropropane ND ug/L 10 09/21/09 07:34 78-87-510.0 1,3-Dichloropropane ND ug/L 10 09/21/09 07:34 142-28-910.0 2,2-Dichloropropane ND ug/L 10 09/21/09 07:34 594-20-710.0 1,1-Dichloropropene ND ug/L 10 09/21/09 07:34 563-58-610.0 cis-1,3-Dichloropropene ND ug/L 10 09/21/09 07:34 10061-01-510.0 trans-1,3-Dichloropropene ND ug/L 10 09/21/09 07:34 10061-02-610.0 Diisopropyl ether 450 ug/L 10 09/21/09 07:34 108-20-310.0 Ethylbenzene 282 ug/L 10 09/21/09 07:34 100-41-410.0 Hexachloro-1,3-butadiene ND ug/L 10 09/21/09 07:34 87-68-310.0 2-Hexanone ND ug/L 10 09/21/09 07:34 591-78-650.0 p-Isopropyltoluene ND ug/L 10 09/21/09 07:34 99-87-610.0 Methylene Chloride ND ug/L 10 09/21/09 07:34 75-09-220.0 4-Methyl-2-pentanone (MIBK)ND ug/L 10 09/21/09 07:34 108-10-150.0 Methyl-tert-butyl ether 219 ug/L 10 09/21/09 07:34 1634-04-410.0 Naphthalene 85.2 ug/L 10 09/21/09 07:34 91-20-310.0 Styrene ND ug/L 10 09/21/09 07:34 100-42-510.0 1,1,1,2-Tetrachloroethane ND ug/L 10 09/21/09 07:34 630-20-610.0 1,1,2,2-Tetrachloroethane ND ug/L 10 09/21/09 07:34 79-34-510.0 Tetrachloroethene ND ug/L 10 09/21/09 07:34 127-18-410.0 Toluene 45.7 ug/L 10 09/21/09 07:34 108-88-310.0 1,2,3-Trichlorobenzene ND ug/L 10 09/21/09 07:34 87-61-610.0 1,2,4-Trichlorobenzene ND ug/L 10 09/21/09 07:34 120-82-110.0 1,1,1-Trichloroethane ND ug/L 10 09/21/09 07:34 71-55-610.0 1,1,2-Trichloroethane ND ug/L 10 09/21/09 07:34 79-00-510.0 Trichloroethene ND ug/L 10 09/21/09 07:34 79-01-610.0 Trichlorofluoromethane ND ug/L 10 09/21/09 07:34 75-69-410.0 1,2,3-Trichloropropane ND ug/L 10 09/21/09 07:34 96-18-410.0 Vinyl acetate ND ug/L 10 09/21/09 07:34 108-05-420.0 Vinyl chloride ND ug/L 10 09/21/09 07:34 75-01-410.0 m&p-Xylene 818 ug/L 10 09/21/09 07:34 1330-20-720.0 o-Xylene 13.2 ug/L 10 09/21/09 07:34 95-47-610.0 4-Bromofluorobenzene (S)99 %10 09/21/09 07:34 460-00-487-109 Dibromofluoromethane (S)99 %10 09/21/09 07:34 1868-53-785-115 1,2-Dichloroethane-d4 (S)104 %10 09/21/09 07:34 17060-07-079-120 Toluene-d8 (S)98 %10 09/21/09 07:34 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 12 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-DUPLICATE-09-09 Lab ID:9252704004 Collected:09/09/09 00:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 03:01 83-32-909/15/09 09:0011.6 Acenaphthylene ND ug/L 1 09/18/09 03:01 208-96-809/15/09 09:0011.6 Aniline ND ug/L 1 09/18/09 03:01 62-53-309/15/09 09:0011.6 Anthracene ND ug/L 1 09/18/09 03:01 120-12-709/15/09 09:0011.6 Benzo(a)anthracene ND ug/L 1 09/18/09 03:01 56-55-309/15/09 09:0011.6 Benzo(a)pyrene ND ug/L 1 09/18/09 03:01 50-32-809/15/09 09:0011.6 Benzo(b)fluoranthene ND ug/L 1 09/18/09 03:01 205-99-209/15/09 09:0011.6 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 03:01 191-24-209/15/09 09:0011.6 Benzo(k)fluoranthene ND ug/L 1 09/18/09 03:01 207-08-909/15/09 09:0011.6 Benzoic Acid ND ug/L 1 09/18/09 03:01 65-85-009/15/09 09:0058.1 Benzyl alcohol ND ug/L 1 09/18/09 03:01 100-51-609/15/09 09:0023.3 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 03:01 101-55-309/15/09 09:0011.6 Butylbenzylphthalate ND ug/L 1 09/18/09 03:01 85-68-709/15/09 09:0011.6 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 03:01 59-50-709/15/09 09:0023.3 4-Chloroaniline ND ug/L 1 09/18/09 03:01 106-47-809/15/09 09:0058.1 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 03:01 111-91-109/15/09 09:0011.6 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 03:01 111-44-409/15/09 09:0011.6 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 03:01 108-60-109/15/09 09:0011.6 2-Chloronaphthalene ND ug/L 1 09/18/09 03:01 91-58-709/15/09 09:0011.6 2-Chlorophenol ND ug/L 1 09/18/09 03:01 95-57-809/15/09 09:0011.6 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 03:01 7005-72-309/15/09 09:0011.6 Chrysene ND ug/L 1 09/18/09 03:01 218-01-909/15/09 09:0011.6 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 03:01 53-70-309/15/09 09:0011.6 Dibenzofuran ND ug/L 1 09/18/09 03:01 132-64-909/15/09 09:0011.6 1,2-Dichlorobenzene ND ug/L 1 09/18/09 03:01 95-50-109/15/09 09:0011.6 1,3-Dichlorobenzene ND ug/L 1 09/18/09 03:01 541-73-109/15/09 09:0011.6 1,4-Dichlorobenzene ND ug/L 1 09/18/09 03:01 106-46-709/15/09 09:0011.6 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 03:01 91-94-109/15/09 09:0058.1 2,4-Dichlorophenol ND ug/L 1 09/18/09 03:01 120-83-209/15/09 09:0011.6 Diethylphthalate ND ug/L 1 09/18/09 03:01 84-66-209/15/09 09:0011.6 2,4-Dimethylphenol ND ug/L 1 09/18/09 03:01 105-67-909/15/09 09:0011.6 Dimethylphthalate ND ug/L 1 09/18/09 03:01 131-11-309/15/09 09:0011.6 Di-n-butylphthalate ND ug/L 1 09/18/09 03:01 84-74-209/15/09 09:0011.6 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 03:01 534-52-109/15/09 09:0023.3 2,4-Dinitrophenol ND ug/L 1 09/18/09 03:01 51-28-509/15/09 09:0058.1 2,4-Dinitrotoluene ND ug/L 1 09/18/09 03:01 121-14-209/15/09 09:0011.6 2,6-Dinitrotoluene ND ug/L 1 09/18/09 03:01 606-20-209/15/09 09:0011.6 Di-n-octylphthalate ND ug/L 1 09/18/09 03:01 117-84-009/15/09 09:0011.6 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 03:01 122-66-709/15/09 09:0011.6 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 03:01 117-81-709/15/09 09:0011.6 Fluoranthene ND ug/L 1 09/18/09 03:01 206-44-009/15/09 09:0011.6 Fluorene ND ug/L 1 09/18/09 03:01 86-73-709/15/09 09:0011.6 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 03:01 87-68-309/15/09 09:0011.6 Hexachlorobenzene ND ug/L 1 09/18/09 03:01 118-74-109/15/09 09:0011.6 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 03:01 77-47-409/15/09 09:0011.6 Hexachloroethane ND ug/L 1 09/18/09 03:01 67-72-109/15/09 09:0011.6 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 03:01 193-39-509/15/09 09:0011.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 13 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-DUPLICATE-09-09 Lab ID:9252704004 Collected:09/09/09 00:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Isophorone ND ug/L 1 09/18/09 03:01 78-59-109/15/09 09:0011.6 1-Methylnaphthalene 15.6 ug/L 1 09/18/09 03:01 90-12-009/15/09 09:0011.6 2-Methylnaphthalene 27.5 ug/L 1 09/18/09 03:01 91-57-609/15/09 09:0011.6 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 03:01 95-48-709/15/09 09:0011.6 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 03:0109/15/09 09:0011.6 Naphthalene ND ug/L 1 09/18/09 03:01 91-20-309/15/09 09:0011.6 2-Nitroaniline ND ug/L 1 09/18/09 03:01 88-74-409/15/09 09:0058.1 3-Nitroaniline ND ug/L 1 09/18/09 03:01 99-09-209/15/09 09:0058.1 4-Nitroaniline ND ug/L 1 09/18/09 03:01 100-01-609/15/09 09:0058.1 Nitrobenzene ND ug/L 1 09/18/09 03:01 98-95-309/15/09 09:0011.6 2-Nitrophenol ND ug/L 1 09/18/09 03:01 88-75-509/15/09 09:0011.6 4-Nitrophenol ND ug/L 1 09/18/09 03:01 100-02-709/15/09 09:0058.1 N-Nitrosodimethylamine ND ug/L 1 09/18/09 03:01 62-75-909/15/09 09:0011.6 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 03:01 621-64-709/15/09 09:0011.6 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 03:01 86-30-609/15/09 09:0011.6 Pentachlorophenol ND ug/L 1 09/18/09 03:01 87-86-509/15/09 09:0058.1 Phenanthrene ND ug/L 1 09/18/09 03:01 85-01-809/15/09 09:0011.6 Phenol ND ug/L 1 09/18/09 03:01 108-95-209/15/09 09:0011.6 Pyrene ND ug/L 1 09/18/09 03:01 129-00-009/15/09 09:0011.6 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 03:01 120-82-109/15/09 09:0011.6 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 03:01 95-95-409/15/09 09:0011.6 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 03:01 88-06-209/15/09 09:0011.6 Nitrobenzene-d5 (S)57 %1 09/18/09 03:01 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)65 %1 09/18/09 03:01 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)95 %1 09/18/09 03:01 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)29 %1 09/18/09 03:01 13127-88-309/15/09 09:0025-150 2-Fluorophenol (S)37 %1 09/18/09 03:01 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)74 %1 09/18/09 03:01 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 10 09/21/09 08:01 67-64-1250 Benzene 1220 ug/L 10 09/21/09 08:01 71-43-210.0 Bromobenzene ND ug/L 10 09/21/09 08:01 108-86-110.0 Bromochloromethane ND ug/L 10 09/21/09 08:01 74-97-510.0 Bromodichloromethane ND ug/L 10 09/21/09 08:01 75-27-410.0 Bromoform ND ug/L 10 09/21/09 08:01 75-25-210.0 Bromomethane ND ug/L 10 09/21/09 08:01 74-83-950.0 2-Butanone (MEK)ND ug/L 10 09/21/09 08:01 78-93-350.0 Carbon tetrachloride ND ug/L 10 09/21/09 08:01 56-23-510.0 Chlorobenzene ND ug/L 10 09/21/09 08:01 108-90-710.0 Chloroethane ND ug/L 10 09/21/09 08:01 75-00-310.0 Chloroform ND ug/L 10 09/21/09 08:01 67-66-310.0 Chloromethane ND ug/L 10 09/21/09 08:01 74-87-310.0 2-Chlorotoluene ND ug/L 10 09/21/09 08:01 95-49-810.0 4-Chlorotoluene ND ug/L 10 09/21/09 08:01 106-43-410.0 1,2-Dibromo-3-chloropropane ND ug/L 10 09/21/09 08:01 96-12-830.0 Dibromochloromethane ND ug/L 10 09/21/09 08:01 124-48-110.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 14 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-DUPLICATE-09-09 Lab ID:9252704004 Collected:09/09/09 00:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 10 09/21/09 08:01 106-93-410.0 Dibromomethane ND ug/L 10 09/21/09 08:01 74-95-310.0 1,2-Dichlorobenzene ND ug/L 10 09/21/09 08:01 95-50-110.0 1,3-Dichlorobenzene ND ug/L 10 09/21/09 08:01 541-73-110.0 1,4-Dichlorobenzene ND ug/L 10 09/21/09 08:01 106-46-710.0 Dichlorodifluoromethane ND ug/L 10 09/21/09 08:01 75-71-810.0 1,1-Dichloroethane ND ug/L 10 09/21/09 08:01 75-34-310.0 1,2-Dichloroethane ND ug/L 10 09/21/09 08:01 107-06-210.0 1,1-Dichloroethene ND ug/L 10 09/21/09 08:01 75-35-410.0 cis-1,2-Dichloroethene ND ug/L 10 09/21/09 08:01 156-59-210.0 trans-1,2-Dichloroethene ND ug/L 10 09/21/09 08:01 156-60-510.0 1,2-Dichloropropane ND ug/L 10 09/21/09 08:01 78-87-510.0 1,3-Dichloropropane ND ug/L 10 09/21/09 08:01 142-28-910.0 2,2-Dichloropropane ND ug/L 10 09/21/09 08:01 594-20-710.0 1,1-Dichloropropene ND ug/L 10 09/21/09 08:01 563-58-610.0 cis-1,3-Dichloropropene ND ug/L 10 09/21/09 08:01 10061-01-510.0 trans-1,3-Dichloropropene ND ug/L 10 09/21/09 08:01 10061-02-610.0 Diisopropyl ether 284 ug/L 10 09/21/09 08:01 108-20-310.0 Ethylbenzene 220 ug/L 10 09/21/09 08:01 100-41-410.0 Hexachloro-1,3-butadiene ND ug/L 10 09/21/09 08:01 87-68-310.0 2-Hexanone ND ug/L 10 09/21/09 08:01 591-78-650.0 p-Isopropyltoluene ND ug/L 10 09/21/09 08:01 99-87-610.0 Methylene Chloride ND ug/L 10 09/21/09 08:01 75-09-220.0 4-Methyl-2-pentanone (MIBK)ND ug/L 10 09/21/09 08:01 108-10-150.0 Methyl-tert-butyl ether 138 ug/L 10 09/21/09 08:01 1634-04-410.0 Naphthalene 82.2 ug/L 10 09/21/09 08:01 91-20-310.0 Styrene ND ug/L 10 09/21/09 08:01 100-42-510.0 1,1,1,2-Tetrachloroethane ND ug/L 10 09/21/09 08:01 630-20-610.0 1,1,2,2-Tetrachloroethane ND ug/L 10 09/21/09 08:01 79-34-510.0 Tetrachloroethene ND ug/L 10 09/21/09 08:01 127-18-410.0 Toluene 31.7 ug/L 10 09/21/09 08:01 108-88-310.0 1,2,3-Trichlorobenzene ND ug/L 10 09/21/09 08:01 87-61-610.0 1,2,4-Trichlorobenzene ND ug/L 10 09/21/09 08:01 120-82-110.0 1,1,1-Trichloroethane ND ug/L 10 09/21/09 08:01 71-55-610.0 1,1,2-Trichloroethane ND ug/L 10 09/21/09 08:01 79-00-510.0 Trichloroethene ND ug/L 10 09/21/09 08:01 79-01-610.0 Trichlorofluoromethane ND ug/L 10 09/21/09 08:01 75-69-410.0 1,2,3-Trichloropropane ND ug/L 10 09/21/09 08:01 96-18-410.0 Vinyl acetate ND ug/L 10 09/21/09 08:01 108-05-420.0 Vinyl chloride ND ug/L 10 09/21/09 08:01 75-01-410.0 m&p-Xylene 578 ug/L 10 09/21/09 08:01 1330-20-720.0 o-Xylene ND ug/L 10 09/21/09 08:01 95-47-610.0 4-Bromofluorobenzene (S)100 %10 09/21/09 08:01 460-00-487-109 Dibromofluoromethane (S)101 %10 09/21/09 08:01 1868-53-785-115 1,2-Dichloroethane-d4 (S)105 %10 09/21/09 08:01 17060-07-079-120 Toluene-d8 (S)98 %10 09/21/09 08:01 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 15 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-MW1-09-09 Lab ID:9252704005 Collected:09/09/09 12:05 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 03:23 83-32-909/15/09 09:0012.0 Acenaphthylene ND ug/L 1 09/18/09 03:23 208-96-809/15/09 09:0012.0 Aniline ND ug/L 1 09/18/09 03:23 62-53-309/15/09 09:0012.0 Anthracene ND ug/L 1 09/18/09 03:23 120-12-709/15/09 09:0012.0 Benzo(a)anthracene ND ug/L 1 09/18/09 03:23 56-55-309/15/09 09:0012.0 Benzo(a)pyrene ND ug/L 1 09/18/09 03:23 50-32-809/15/09 09:0012.0 Benzo(b)fluoranthene ND ug/L 1 09/18/09 03:23 205-99-209/15/09 09:0012.0 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 03:23 191-24-209/15/09 09:0012.0 Benzo(k)fluoranthene ND ug/L 1 09/18/09 03:23 207-08-909/15/09 09:0012.0 Benzoic Acid ND ug/L 1 09/18/09 03:23 65-85-009/15/09 09:0060.2 Benzyl alcohol ND ug/L 1 09/18/09 03:23 100-51-609/15/09 09:0024.1 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 03:23 101-55-309/15/09 09:0012.0 Butylbenzylphthalate ND ug/L 1 09/18/09 03:23 85-68-709/15/09 09:0012.0 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 03:23 59-50-709/15/09 09:0024.1 4-Chloroaniline ND ug/L 1 09/18/09 03:23 106-47-809/15/09 09:0060.2 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 03:23 111-91-109/15/09 09:0012.0 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 03:23 111-44-409/15/09 09:0012.0 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 03:23 108-60-109/15/09 09:0012.0 2-Chloronaphthalene ND ug/L 1 09/18/09 03:23 91-58-709/15/09 09:0012.0 2-Chlorophenol ND ug/L 1 09/18/09 03:23 95-57-809/15/09 09:0012.0 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 03:23 7005-72-309/15/09 09:0012.0 Chrysene ND ug/L 1 09/18/09 03:23 218-01-909/15/09 09:0012.0 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 03:23 53-70-309/15/09 09:0012.0 Dibenzofuran ND ug/L 1 09/18/09 03:23 132-64-909/15/09 09:0012.0 1,2-Dichlorobenzene ND ug/L 1 09/18/09 03:23 95-50-109/15/09 09:0012.0 1,3-Dichlorobenzene ND ug/L 1 09/18/09 03:23 541-73-109/15/09 09:0012.0 1,4-Dichlorobenzene ND ug/L 1 09/18/09 03:23 106-46-709/15/09 09:0012.0 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 03:23 91-94-109/15/09 09:0060.2 2,4-Dichlorophenol ND ug/L 1 09/18/09 03:23 120-83-209/15/09 09:0012.0 Diethylphthalate ND ug/L 1 09/18/09 03:23 84-66-209/15/09 09:0012.0 2,4-Dimethylphenol ND ug/L 1 09/18/09 03:23 105-67-909/15/09 09:0012.0 Dimethylphthalate ND ug/L 1 09/18/09 03:23 131-11-309/15/09 09:0012.0 Di-n-butylphthalate ND ug/L 1 09/18/09 03:23 84-74-209/15/09 09:0012.0 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 03:23 534-52-109/15/09 09:0024.1 2,4-Dinitrophenol ND ug/L 1 09/18/09 03:23 51-28-509/15/09 09:0060.2 2,4-Dinitrotoluene ND ug/L 1 09/18/09 03:23 121-14-209/15/09 09:0012.0 2,6-Dinitrotoluene ND ug/L 1 09/18/09 03:23 606-20-209/15/09 09:0012.0 Di-n-octylphthalate ND ug/L 1 09/18/09 03:23 117-84-009/15/09 09:0012.0 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 03:23 122-66-709/15/09 09:0012.0 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 03:23 117-81-709/15/09 09:0012.0 Fluoranthene ND ug/L 1 09/18/09 03:23 206-44-009/15/09 09:0012.0 Fluorene ND ug/L 1 09/18/09 03:23 86-73-709/15/09 09:0012.0 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 03:23 87-68-309/15/09 09:0012.0 Hexachlorobenzene ND ug/L 1 09/18/09 03:23 118-74-109/15/09 09:0012.0 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 03:23 77-47-409/15/09 09:0012.0 Hexachloroethane ND ug/L 1 09/18/09 03:23 67-72-109/15/09 09:0012.0 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 03:23 193-39-509/15/09 09:0012.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 16 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-MW1-09-09 Lab ID:9252704005 Collected:09/09/09 12:05 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Isophorone ND ug/L 1 09/18/09 03:23 78-59-109/15/09 09:0012.0 1-Methylnaphthalene ND ug/L 1 09/18/09 03:23 90-12-009/15/09 09:0012.0 2-Methylnaphthalene ND ug/L 1 09/18/09 03:23 91-57-609/15/09 09:0012.0 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 03:23 95-48-709/15/09 09:0012.0 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 03:2309/15/09 09:0012.0 Naphthalene ND ug/L 1 09/18/09 03:23 91-20-309/15/09 09:0012.0 2-Nitroaniline ND ug/L 1 09/18/09 03:23 88-74-409/15/09 09:0060.2 3-Nitroaniline ND ug/L 1 09/18/09 03:23 99-09-209/15/09 09:0060.2 4-Nitroaniline ND ug/L 1 09/18/09 03:23 100-01-609/15/09 09:0060.2 Nitrobenzene ND ug/L 1 09/18/09 03:23 98-95-309/15/09 09:0012.0 2-Nitrophenol ND ug/L 1 09/18/09 03:23 88-75-509/15/09 09:0012.0 4-Nitrophenol ND ug/L 1 09/18/09 03:23 100-02-709/15/09 09:0060.2 N-Nitrosodimethylamine ND ug/L 1 09/18/09 03:23 62-75-909/15/09 09:0012.0 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 03:23 621-64-709/15/09 09:0012.0 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 03:23 86-30-609/15/09 09:0012.0 Pentachlorophenol ND ug/L 1 09/18/09 03:23 87-86-509/15/09 09:0060.2 Phenanthrene ND ug/L 1 09/18/09 03:23 85-01-809/15/09 09:0012.0 Phenol ND ug/L 1 09/18/09 03:23 108-95-209/15/09 09:0012.0 Pyrene ND ug/L 1 09/18/09 03:23 129-00-009/15/09 09:0012.0 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 03:23 120-82-109/15/09 09:0012.0 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 03:23 95-95-409/15/09 09:0012.0 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 03:23 88-06-209/15/09 09:0012.0 Nitrobenzene-d5 (S)50 %1 09/18/09 03:23 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)54 %1 09/18/09 03:23 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)71 %1 09/18/09 03:23 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)22 %1 09/18/09 03:23 13127-88-3 1g09/15/09 09:0025-150 2-Fluorophenol (S)33 %1 09/18/09 03:23 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)48 %1 09/18/09 03:23 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 05:46 67-64-125.0 Benzene ND ug/L 1 09/13/09 05:46 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 05:46 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 05:46 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 05:46 75-27-41.0 Bromoform ND ug/L 1 09/13/09 05:46 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 05:46 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 05:46 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 05:46 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 05:46 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 05:46 75-00-31.0 Chloroform ND ug/L 1 09/13/09 05:46 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 05:46 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 05:46 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 05:46 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 05:46 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 05:46 124-48-11.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 17 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-MW1-09-09 Lab ID:9252704005 Collected:09/09/09 12:05 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 05:46 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 05:46 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 05:46 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 05:46 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 05:46 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 05:46 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 05:46 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 05:46 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 05:46 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 05:46 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 05:46 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 05:46 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 05:46 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 05:46 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 05:46 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 05:46 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 05:46 10061-02-61.0 Diisopropyl ether 32.2 ug/L 1 09/13/09 05:46 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 05:46 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 05:46 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 05:46 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 05:46 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 05:46 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 05:46 108-10-15.0 Methyl-tert-butyl ether 6.0 ug/L 1 09/13/09 05:46 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 05:46 91-20-31.0 Styrene ND ug/L 1 09/13/09 05:46 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 05:46 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 05:46 79-34-51.0 Tetrachloroethene ND ug/L 1 09/13/09 05:46 127-18-41.0 Toluene ND ug/L 1 09/13/09 05:46 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 05:46 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 05:46 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 05:46 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 05:46 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 05:46 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 05:46 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 05:46 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 05:46 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 05:46 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 05:46 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 05:46 95-47-61.0 4-Bromofluorobenzene (S)100 %1 09/13/09 05:46 460-00-487-109 Dibromofluoromethane (S)100 %1 09/13/09 05:46 1868-53-785-115 1,2-Dichloroethane-d4 (S)100 %1 09/13/09 05:46 17060-07-079-120 Toluene-d8 (S)100 %1 09/13/09 05:46 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 18 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-MW2-09-09 Lab ID:9252704006 Collected:09/09/09 13:30 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 1 09/18/09 03:45 83-32-909/15/09 09:0012.8 Acenaphthylene ND ug/L 1 09/18/09 03:45 208-96-809/15/09 09:0012.8 Aniline ND ug/L 1 09/18/09 03:45 62-53-309/15/09 09:0012.8 Anthracene ND ug/L 1 09/18/09 03:45 120-12-709/15/09 09:0012.8 Benzo(a)anthracene ND ug/L 1 09/18/09 03:45 56-55-309/15/09 09:0012.8 Benzo(a)pyrene ND ug/L 1 09/18/09 03:45 50-32-809/15/09 09:0012.8 Benzo(b)fluoranthene ND ug/L 1 09/18/09 03:45 205-99-209/15/09 09:0012.8 Benzo(g,h,i)perylene ND ug/L 1 09/18/09 03:45 191-24-209/15/09 09:0012.8 Benzo(k)fluoranthene ND ug/L 1 09/18/09 03:45 207-08-909/15/09 09:0012.8 Benzoic Acid ND ug/L 1 09/18/09 03:45 65-85-009/15/09 09:0064.1 Benzyl alcohol ND ug/L 1 09/18/09 03:45 100-51-609/15/09 09:0025.6 4-Bromophenylphenyl ether ND ug/L 1 09/18/09 03:45 101-55-309/15/09 09:0012.8 Butylbenzylphthalate ND ug/L 1 09/18/09 03:45 85-68-709/15/09 09:0012.8 4-Chloro-3-methylphenol ND ug/L 1 09/18/09 03:45 59-50-709/15/09 09:0025.6 4-Chloroaniline ND ug/L 1 09/18/09 03:45 106-47-809/15/09 09:0064.1 bis(2-Chloroethoxy)methane ND ug/L 1 09/18/09 03:45 111-91-109/15/09 09:0012.8 bis(2-Chloroethyl) ether ND ug/L 1 09/18/09 03:45 111-44-409/15/09 09:0012.8 bis(2-Chloroisopropyl) ether ND ug/L 1 09/18/09 03:45 108-60-109/15/09 09:0012.8 2-Chloronaphthalene ND ug/L 1 09/18/09 03:45 91-58-709/15/09 09:0012.8 2-Chlorophenol ND ug/L 1 09/18/09 03:45 95-57-809/15/09 09:0012.8 4-Chlorophenylphenyl ether ND ug/L 1 09/18/09 03:45 7005-72-309/15/09 09:0012.8 Chrysene ND ug/L 1 09/18/09 03:45 218-01-909/15/09 09:0012.8 Dibenz(a,h)anthracene ND ug/L 1 09/18/09 03:45 53-70-309/15/09 09:0012.8 Dibenzofuran ND ug/L 1 09/18/09 03:45 132-64-909/15/09 09:0012.8 1,2-Dichlorobenzene ND ug/L 1 09/18/09 03:45 95-50-109/15/09 09:0012.8 1,3-Dichlorobenzene ND ug/L 1 09/18/09 03:45 541-73-109/15/09 09:0012.8 1,4-Dichlorobenzene ND ug/L 1 09/18/09 03:45 106-46-709/15/09 09:0012.8 3,3'-Dichlorobenzidine ND ug/L 1 09/18/09 03:45 91-94-109/15/09 09:0064.1 2,4-Dichlorophenol ND ug/L 1 09/18/09 03:45 120-83-209/15/09 09:0012.8 Diethylphthalate ND ug/L 1 09/18/09 03:45 84-66-209/15/09 09:0012.8 2,4-Dimethylphenol ND ug/L 1 09/18/09 03:45 105-67-909/15/09 09:0012.8 Dimethylphthalate ND ug/L 1 09/18/09 03:45 131-11-309/15/09 09:0012.8 Di-n-butylphthalate ND ug/L 1 09/18/09 03:45 84-74-209/15/09 09:0012.8 4,6-Dinitro-2-methylphenol ND ug/L 1 09/18/09 03:45 534-52-109/15/09 09:0025.6 2,4-Dinitrophenol ND ug/L 1 09/18/09 03:45 51-28-509/15/09 09:0064.1 2,4-Dinitrotoluene ND ug/L 1 09/18/09 03:45 121-14-209/15/09 09:0012.8 2,6-Dinitrotoluene ND ug/L 1 09/18/09 03:45 606-20-209/15/09 09:0012.8 Di-n-octylphthalate ND ug/L 1 09/18/09 03:45 117-84-009/15/09 09:0012.8 1,2-Diphenylhydrazine ND ug/L 1 09/18/09 03:45 122-66-709/15/09 09:0012.8 bis(2-Ethylhexyl)phthalate ND ug/L 1 09/18/09 03:45 117-81-709/15/09 09:0012.8 Fluoranthene ND ug/L 1 09/18/09 03:45 206-44-009/15/09 09:0012.8 Fluorene ND ug/L 1 09/18/09 03:45 86-73-709/15/09 09:0012.8 Hexachloro-1,3-butadiene ND ug/L 1 09/18/09 03:45 87-68-309/15/09 09:0012.8 Hexachlorobenzene ND ug/L 1 09/18/09 03:45 118-74-109/15/09 09:0012.8 Hexachlorocyclopentadiene ND ug/L 1 09/18/09 03:45 77-47-409/15/09 09:0012.8 Hexachloroethane ND ug/L 1 09/18/09 03:45 67-72-109/15/09 09:0012.8 Indeno(1,2,3-cd)pyrene ND ug/L 1 09/18/09 03:45 193-39-509/15/09 09:0012.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 19 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-MW2-09-09 Lab ID:9252704006 Collected:09/09/09 13:30 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Isophorone ND ug/L 1 09/18/09 03:45 78-59-109/15/09 09:0012.8 1-Methylnaphthalene ND ug/L 1 09/18/09 03:45 90-12-009/15/09 09:0012.8 2-Methylnaphthalene ND ug/L 1 09/18/09 03:45 91-57-609/15/09 09:0012.8 2-Methylphenol(o-Cresol)ND ug/L 1 09/18/09 03:45 95-48-709/15/09 09:0012.8 3&4-Methylphenol(m&p Cresol)ND ug/L 1 09/18/09 03:4509/15/09 09:0012.8 Naphthalene ND ug/L 1 09/18/09 03:45 91-20-309/15/09 09:0012.8 2-Nitroaniline ND ug/L 1 09/18/09 03:45 88-74-409/15/09 09:0064.1 3-Nitroaniline ND ug/L 1 09/18/09 03:45 99-09-209/15/09 09:0064.1 4-Nitroaniline ND ug/L 1 09/18/09 03:45 100-01-609/15/09 09:0064.1 Nitrobenzene ND ug/L 1 09/18/09 03:45 98-95-309/15/09 09:0012.8 2-Nitrophenol ND ug/L 1 09/18/09 03:45 88-75-509/15/09 09:0012.8 4-Nitrophenol ND ug/L 1 09/18/09 03:45 100-02-709/15/09 09:0064.1 N-Nitrosodimethylamine ND ug/L 1 09/18/09 03:45 62-75-909/15/09 09:0012.8 N-Nitroso-di-n-propylamine ND ug/L 1 09/18/09 03:45 621-64-709/15/09 09:0012.8 N-Nitrosodiphenylamine ND ug/L 1 09/18/09 03:45 86-30-609/15/09 09:0012.8 Pentachlorophenol ND ug/L 1 09/18/09 03:45 87-86-509/15/09 09:0064.1 Phenanthrene ND ug/L 1 09/18/09 03:45 85-01-809/15/09 09:0012.8 Phenol ND ug/L 1 09/18/09 03:45 108-95-209/15/09 09:0012.8 Pyrene ND ug/L 1 09/18/09 03:45 129-00-009/15/09 09:0012.8 1,2,4-Trichlorobenzene ND ug/L 1 09/18/09 03:45 120-82-109/15/09 09:0012.8 2,4,5-Trichlorophenol ND ug/L 1 09/18/09 03:45 95-95-409/15/09 09:0012.8 2,4,6-Trichlorophenol ND ug/L 1 09/18/09 03:45 88-06-209/15/09 09:0012.8 Nitrobenzene-d5 (S)45 %1 09/18/09 03:45 4165-60-009/15/09 09:0030-150 2-Fluorobiphenyl (S)49 %1 09/18/09 03:45 321-60-809/15/09 09:0030-150 Terphenyl-d14 (S)72 %1 09/18/09 03:45 1718-51-009/15/09 09:0030-150 Phenol-d6 (S)25 %1 09/18/09 03:45 13127-88-309/15/09 09:0025-150 2-Fluorophenol (S)33 %1 09/18/09 03:45 367-12-409/15/09 09:0025-150 2,4,6-Tribromophenol (S)57 %1 09/18/09 03:45 118-79-609/15/09 09:0025-150 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/16/09 18:56 67-64-125.0 Benzene ND ug/L 1 09/16/09 18:56 71-43-21.0 Bromobenzene ND ug/L 1 09/16/09 18:56 108-86-11.0 Bromochloromethane ND ug/L 1 09/16/09 18:56 74-97-51.0 Bromodichloromethane ND ug/L 1 09/16/09 18:56 75-27-41.0 Bromoform ND ug/L 1 09/16/09 18:56 75-25-21.0 Bromomethane ND ug/L 1 09/16/09 18:56 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/16/09 18:56 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/16/09 18:56 56-23-51.0 Chlorobenzene ND ug/L 1 09/16/09 18:56 108-90-71.0 Chloroethane ND ug/L 1 09/16/09 18:56 75-00-31.0 Chloroform ND ug/L 1 09/16/09 18:56 67-66-31.0 Chloromethane ND ug/L 1 09/16/09 18:56 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/16/09 18:56 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/16/09 18:56 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/16/09 18:56 96-12-83.0 Dibromochloromethane ND ug/L 1 09/16/09 18:56 124-48-11.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 20 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-MW2-09-09 Lab ID:9252704006 Collected:09/09/09 13:30 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 1,2-Dibromoethane (EDB)ND ug/L 1 09/16/09 18:56 106-93-41.0 Dibromomethane ND ug/L 1 09/16/09 18:56 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/16/09 18:56 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/16/09 18:56 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/16/09 18:56 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/16/09 18:56 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/16/09 18:56 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/16/09 18:56 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/16/09 18:56 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/16/09 18:56 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/16/09 18:56 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/16/09 18:56 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/16/09 18:56 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/16/09 18:56 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/16/09 18:56 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/16/09 18:56 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/16/09 18:56 10061-02-61.0 Diisopropyl ether 19.8 ug/L 1 09/16/09 18:56 108-20-31.0 Ethylbenzene ND ug/L 1 09/16/09 18:56 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/16/09 18:56 87-68-31.0 2-Hexanone ND ug/L 1 09/16/09 18:56 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/16/09 18:56 99-87-61.0 Methylene Chloride ND ug/L 1 09/16/09 18:56 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/16/09 18:56 108-10-15.0 Methyl-tert-butyl ether 3.0 ug/L 1 09/16/09 18:56 1634-04-41.0 Naphthalene ND ug/L 1 09/16/09 18:56 91-20-31.0 Styrene ND ug/L 1 09/16/09 18:56 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/16/09 18:56 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/16/09 18:56 79-34-51.0 Tetrachloroethene ND ug/L 1 09/16/09 18:56 127-18-41.0 Toluene ND ug/L 1 09/16/09 18:56 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/16/09 18:56 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/16/09 18:56 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/16/09 18:56 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/16/09 18:56 79-00-51.0 Trichloroethene ND ug/L 1 09/16/09 18:56 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/16/09 18:56 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/16/09 18:56 96-18-41.0 Vinyl acetate ND ug/L 1 09/16/09 18:56 108-05-42.0 Vinyl chloride ND ug/L 1 09/16/09 18:56 75-01-41.0 m&p-Xylene ND ug/L 1 09/16/09 18:56 1330-20-72.0 o-Xylene ND ug/L 1 09/16/09 18:56 95-47-61.0 4-Bromofluorobenzene (S)100 %1 09/16/09 18:56 460-00-487-109 Dibromofluoromethane (S)103 %1 09/16/09 18:56 1868-53-785-115 1,2-Dichloroethane-d4 (S)102 %1 09/16/09 18:56 17060-07-079-120 Toluene-d8 (S)99 %1 09/16/09 18:56 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 21 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-FIELDBLANK-09-09 Lab ID:9252704007 Collected:09/09/09 10:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 06:24 67-64-125.0 Benzene ND ug/L 1 09/13/09 06:24 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 06:24 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 06:24 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 06:24 75-27-41.0 Bromoform ND ug/L 1 09/13/09 06:24 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 06:24 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 06:24 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 06:24 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 06:24 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 06:24 75-00-31.0 Chloroform ND ug/L 1 09/13/09 06:24 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 06:24 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 06:24 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 06:24 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 06:24 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 06:24 124-48-11.0 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 06:24 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 06:24 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 06:24 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 06:24 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 06:24 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 06:24 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 06:24 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 06:24 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 06:24 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 06:24 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 06:24 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 06:24 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 06:24 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 06:24 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 06:24 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 06:24 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 06:24 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 06:24 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 06:24 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 06:24 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 06:24 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 06:24 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 06:24 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 06:24 108-10-15.0 Methyl-tert-butyl ether ND ug/L 1 09/13/09 06:24 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 06:24 91-20-31.0 Styrene ND ug/L 1 09/13/09 06:24 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 06:24 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 06:24 79-34-51.0 Tetrachloroethene ND ug/L 1 09/13/09 06:24 127-18-41.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 22 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-FIELDBLANK-09-09 Lab ID:9252704007 Collected:09/09/09 10:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1 09/13/09 06:24 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 06:24 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 06:24 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 06:24 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 06:24 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 06:24 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 06:24 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 06:24 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 06:24 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 06:24 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 06:24 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 06:24 95-47-61.0 4-Bromofluorobenzene (S)97 %1 09/13/09 06:24 460-00-487-109 Dibromofluoromethane (S)100 %1 09/13/09 06:24 1868-53-785-115 1,2-Dichloroethane-d4 (S)100 %1 09/13/09 06:24 17060-07-079-120 Toluene-d8 (S)100 %1 09/13/09 06:24 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 23 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TRIPBLANK1-09-09 Lab ID:9252704008 Collected:09/09/09 00:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 02:53 67-64-125.0 Benzene ND ug/L 1 09/13/09 02:53 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 02:53 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 02:53 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 02:53 75-27-41.0 Bromoform ND ug/L 1 09/13/09 02:53 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 02:53 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 02:53 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 02:53 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 02:53 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 02:53 75-00-31.0 Chloroform ND ug/L 1 09/13/09 02:53 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 02:53 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 02:53 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 02:53 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 02:53 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 02:53 124-48-11.0 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 02:53 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 02:53 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 02:53 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 02:53 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 02:53 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 02:53 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 02:53 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 02:53 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 02:53 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 02:53 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 02:53 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 02:53 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 02:53 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 02:53 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 02:53 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 02:53 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 02:53 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 02:53 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 02:53 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 02:53 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 02:53 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 02:53 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 02:53 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 02:53 108-10-15.0 Methyl-tert-butyl ether ND ug/L 1 09/13/09 02:53 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 02:53 91-20-31.0 Styrene ND ug/L 1 09/13/09 02:53 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 02:53 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 02:53 79-34-51.0 Tetrachloroethene ND ug/L 1 09/13/09 02:53 127-18-41.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 24 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TRIPBLANK1-09-09 Lab ID:9252704008 Collected:09/09/09 00:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1 09/13/09 02:53 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 02:53 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 02:53 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 02:53 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 02:53 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 02:53 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 02:53 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 02:53 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 02:53 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 02:53 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 02:53 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 02:53 95-47-61.0 4-Bromofluorobenzene (S)100 %1 09/13/09 02:53 460-00-487-109 Dibromofluoromethane (S)101 %1 09/13/09 02:53 1868-53-785-115 1,2-Dichloroethane-d4 (S)101 %1 09/13/09 02:53 17060-07-079-120 Toluene-d8 (S)100 %1 09/13/09 02:53 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 25 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TRIPBLANK2-09-09 Lab ID:9252704009 Collected:09/09/09 00:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Acetone ND ug/L 1 09/13/09 03:12 67-64-125.0 Benzene ND ug/L 1 09/13/09 03:12 71-43-21.0 Bromobenzene ND ug/L 1 09/13/09 03:12 108-86-11.0 Bromochloromethane ND ug/L 1 09/13/09 03:12 74-97-51.0 Bromodichloromethane ND ug/L 1 09/13/09 03:12 75-27-41.0 Bromoform ND ug/L 1 09/13/09 03:12 75-25-21.0 Bromomethane ND ug/L 1 09/13/09 03:12 74-83-95.0 2-Butanone (MEK)ND ug/L 1 09/13/09 03:12 78-93-35.0 Carbon tetrachloride ND ug/L 1 09/13/09 03:12 56-23-51.0 Chlorobenzene ND ug/L 1 09/13/09 03:12 108-90-71.0 Chloroethane ND ug/L 1 09/13/09 03:12 75-00-31.0 Chloroform ND ug/L 1 09/13/09 03:12 67-66-31.0 Chloromethane ND ug/L 1 09/13/09 03:12 74-87-31.0 2-Chlorotoluene ND ug/L 1 09/13/09 03:12 95-49-81.0 4-Chlorotoluene ND ug/L 1 09/13/09 03:12 106-43-41.0 1,2-Dibromo-3-chloropropane ND ug/L 1 09/13/09 03:12 96-12-83.0 Dibromochloromethane ND ug/L 1 09/13/09 03:12 124-48-11.0 1,2-Dibromoethane (EDB)ND ug/L 1 09/13/09 03:12 106-93-41.0 Dibromomethane ND ug/L 1 09/13/09 03:12 74-95-31.0 1,2-Dichlorobenzene ND ug/L 1 09/13/09 03:12 95-50-11.0 1,3-Dichlorobenzene ND ug/L 1 09/13/09 03:12 541-73-11.0 1,4-Dichlorobenzene ND ug/L 1 09/13/09 03:12 106-46-71.0 Dichlorodifluoromethane ND ug/L 1 09/13/09 03:12 75-71-81.0 1,1-Dichloroethane ND ug/L 1 09/13/09 03:12 75-34-31.0 1,2-Dichloroethane ND ug/L 1 09/13/09 03:12 107-06-21.0 1,1-Dichloroethene ND ug/L 1 09/13/09 03:12 75-35-41.0 cis-1,2-Dichloroethene ND ug/L 1 09/13/09 03:12 156-59-21.0 trans-1,2-Dichloroethene ND ug/L 1 09/13/09 03:12 156-60-51.0 1,2-Dichloropropane ND ug/L 1 09/13/09 03:12 78-87-51.0 1,3-Dichloropropane ND ug/L 1 09/13/09 03:12 142-28-91.0 2,2-Dichloropropane ND ug/L 1 09/13/09 03:12 594-20-71.0 1,1-Dichloropropene ND ug/L 1 09/13/09 03:12 563-58-61.0 cis-1,3-Dichloropropene ND ug/L 1 09/13/09 03:12 10061-01-51.0 trans-1,3-Dichloropropene ND ug/L 1 09/13/09 03:12 10061-02-61.0 Diisopropyl ether ND ug/L 1 09/13/09 03:12 108-20-31.0 Ethylbenzene ND ug/L 1 09/13/09 03:12 100-41-41.0 Hexachloro-1,3-butadiene ND ug/L 1 09/13/09 03:12 87-68-31.0 2-Hexanone ND ug/L 1 09/13/09 03:12 591-78-65.0 p-Isopropyltoluene ND ug/L 1 09/13/09 03:12 99-87-61.0 Methylene Chloride ND ug/L 1 09/13/09 03:12 75-09-22.0 4-Methyl-2-pentanone (MIBK)ND ug/L 1 09/13/09 03:12 108-10-15.0 Methyl-tert-butyl ether ND ug/L 1 09/13/09 03:12 1634-04-41.0 Naphthalene ND ug/L 1 09/13/09 03:12 91-20-31.0 Styrene ND ug/L 1 09/13/09 03:12 100-42-51.0 1,1,1,2-Tetrachloroethane ND ug/L 1 09/13/09 03:12 630-20-61.0 1,1,2,2-Tetrachloroethane ND ug/L 1 09/13/09 03:12 79-34-51.0 Tetrachloroethene ND ug/L 1 09/13/09 03:12 127-18-41.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 26 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Sample:1 FAIR-TRIPBLANK2-09-09 Lab ID:9252704009 Collected:09/09/09 00:00 Received:09/09/09 15:10 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit 8260 MSV Low Level Analytical Method: EPA 8260 Toluene ND ug/L 1 09/13/09 03:12 108-88-31.0 1,2,3-Trichlorobenzene ND ug/L 1 09/13/09 03:12 87-61-61.0 1,2,4-Trichlorobenzene ND ug/L 1 09/13/09 03:12 120-82-11.0 1,1,1-Trichloroethane ND ug/L 1 09/13/09 03:12 71-55-61.0 1,1,2-Trichloroethane ND ug/L 1 09/13/09 03:12 79-00-51.0 Trichloroethene ND ug/L 1 09/13/09 03:12 79-01-61.0 Trichlorofluoromethane ND ug/L 1 09/13/09 03:12 75-69-41.0 1,2,3-Trichloropropane ND ug/L 1 09/13/09 03:12 96-18-41.0 Vinyl acetate ND ug/L 1 09/13/09 03:12 108-05-42.0 Vinyl chloride ND ug/L 1 09/13/09 03:12 75-01-41.0 m&p-Xylene ND ug/L 1 09/13/09 03:12 1330-20-72.0 o-Xylene ND ug/L 1 09/13/09 03:12 95-47-61.0 4-Bromofluorobenzene (S)98 %1 09/13/09 03:12 460-00-487-109 Dibromofluoromethane (S)101 %1 09/13/09 03:12 1868-53-785-115 1,2-Dichloroethane-d4 (S)100 %1 09/13/09 03:12 17060-07-079-120 Toluene-d8 (S)98 %1 09/13/09 03:12 2037-26-570-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 27 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: OEXT/7988 EPA 3510 EPA 8270 8270 Water MSSV Associated Lab Samples:9252704001, 9252704002, 9252704003, 9252704004, 9252704005, 9252704006 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335996 Associated Lab Samples:9252704001, 9252704002, 9252704003, 9252704004, 9252704005, 9252704006 Matrix:Water Analyzed 1,2,4-Trichlorobenzene ug/L ND 10.0 09/17/09 17:04 1,2-Dichlorobenzene ug/L ND 10.0 09/17/09 17:04 1,2-Diphenylhydrazine ug/L ND 10.0 09/17/09 17:04 1,3-Dichlorobenzene ug/L ND 10.0 09/17/09 17:04 1,4-Dichlorobenzene ug/L ND 10.0 09/17/09 17:04 1-Methylnaphthalene ug/L ND 10.0 09/17/09 17:04 2,4,5-Trichlorophenol ug/L ND 10.0 09/17/09 17:04 2,4,6-Trichlorophenol ug/L ND 10.0 09/17/09 17:04 2,4-Dichlorophenol ug/L ND 10.0 09/17/09 17:04 2,4-Dimethylphenol ug/L ND 10.0 09/17/09 17:04 2,4-Dinitrophenol ug/L ND 50.0 09/17/09 17:04 2,4-Dinitrotoluene ug/L ND 10.0 09/17/09 17:04 2,6-Dinitrotoluene ug/L ND 10.0 09/17/09 17:04 2-Chloronaphthalene ug/L ND 10.0 09/17/09 17:04 2-Chlorophenol ug/L ND 10.0 09/17/09 17:04 2-Methylnaphthalene ug/L ND 10.0 09/17/09 17:04 2-Methylphenol(o-Cresol)ug/L ND 10.0 09/17/09 17:04 2-Nitroaniline ug/L ND 50.0 09/17/09 17:04 2-Nitrophenol ug/L ND 10.0 09/17/09 17:04 3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/17/09 17:04 3,3'-Dichlorobenzidine ug/L ND 50.0 09/17/09 17:04 3-Nitroaniline ug/L ND 50.0 09/17/09 17:04 4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/17/09 17:04 4-Bromophenylphenyl ether ug/L ND 10.0 09/17/09 17:04 4-Chloro-3-methylphenol ug/L ND 20.0 09/17/09 17:04 4-Chloroaniline ug/L ND 50.0 09/17/09 17:04 4-Chlorophenylphenyl ether ug/L ND 10.0 09/17/09 17:04 4-Nitroaniline ug/L ND 50.0 09/17/09 17:04 4-Nitrophenol ug/L ND 50.0 09/17/09 17:04 Acenaphthene ug/L ND 10.0 09/17/09 17:04 Acenaphthylene ug/L ND 10.0 09/17/09 17:04 Aniline ug/L ND 10.0 09/17/09 17:04 Anthracene ug/L ND 10.0 09/17/09 17:04 Benzo(a)anthracene ug/L ND 10.0 09/17/09 17:04 Benzo(a)pyrene ug/L ND 10.0 09/17/09 17:04 Benzo(b)fluoranthene ug/L ND 10.0 09/17/09 17:04 Benzo(g,h,i)perylene ug/L ND 10.0 09/17/09 17:04 Benzo(k)fluoranthene ug/L ND 10.0 09/17/09 17:04 Benzoic Acid ug/L ND 50.0 09/17/09 17:04 Benzyl alcohol ug/L ND 20.0 09/17/09 17:04 bis(2-Chloroethoxy)methane ug/L ND 10.0 09/17/09 17:04 bis(2-Chloroethyl) ether ug/L ND 10.0 09/17/09 17:04 bis(2-Chloroisopropyl) ether ug/L ND 10.0 09/17/09 17:04 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 28 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335996 Associated Lab Samples:9252704001, 9252704002, 9252704003, 9252704004, 9252704005, 9252704006 Matrix:Water Analyzed bis(2-Ethylhexyl)phthalate ug/L ND 10.0 09/17/09 17:04 Butylbenzylphthalate ug/L ND 10.0 09/17/09 17:04 Chrysene ug/L ND 10.0 09/17/09 17:04 Di-n-butylphthalate ug/L ND 10.0 09/17/09 17:04 Di-n-octylphthalate ug/L ND 10.0 09/17/09 17:04 Dibenz(a,h)anthracene ug/L ND 10.0 09/17/09 17:04 Dibenzofuran ug/L ND 10.0 09/17/09 17:04 Diethylphthalate ug/L ND 10.0 09/17/09 17:04 Dimethylphthalate ug/L ND 10.0 09/17/09 17:04 Fluoranthene ug/L ND 10.0 09/17/09 17:04 Fluorene ug/L ND 10.0 09/17/09 17:04 Hexachloro-1,3-butadiene ug/L ND 10.0 09/17/09 17:04 Hexachlorobenzene ug/L ND 10.0 09/17/09 17:04 Hexachlorocyclopentadiene ug/L ND 10.0 09/17/09 17:04 Hexachloroethane ug/L ND 10.0 09/17/09 17:04 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/17/09 17:04 Isophorone ug/L ND 10.0 09/17/09 17:04 N-Nitroso-di-n-propylamine ug/L ND 10.0 09/17/09 17:04 N-Nitrosodimethylamine ug/L ND 10.0 09/17/09 17:04 N-Nitrosodiphenylamine ug/L ND 10.0 09/17/09 17:04 Naphthalene ug/L ND 10.0 09/17/09 17:04 Nitrobenzene ug/L ND 10.0 09/17/09 17:04 Pentachlorophenol ug/L ND 50.0 09/17/09 17:04 Phenanthrene ug/L ND 10.0 09/17/09 17:04 Phenol ug/L ND 10.0 09/17/09 17:04 Pyrene ug/L ND 10.0 09/17/09 17:04 2,4,6-Tribromophenol (S)%53 25-150 09/17/09 17:04 2-Fluorobiphenyl (S)%51 30-150 09/17/09 17:04 2-Fluorophenol (S)%31 25-150 09/17/09 17:04 Nitrobenzene-d5 (S)%49 30-150 09/17/09 17:04 Phenol-d6 (S)%33 25-150 09/17/09 17:04 Terphenyl-d14 (S)%61 30-150 09/17/09 17:04 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335997LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/L 11.925 48 19-120 1,2-Dichlorobenzene ug/L 10.625 42 19-120 1,2-Diphenylhydrazine ug/L 20.925 84 50-150 1,3-Dichlorobenzene ug/L 9.7J25 39 15-120 1,4-Dichlorobenzene ug/L 10.825 43 15-120 1-Methylnaphthalene ug/L 14.025 56 21-120 2,4,5-Trichlorophenol ug/L 17.425 70 23-113 2,4,6-Trichlorophenol ug/L 20.125 80 21-113 2,4-Dichlorophenol ug/L 17.325 69 12-127 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 29 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335997LABORATORY CONTROL SAMPLE: LCSSpike 2,4-Dimethylphenol ug/L 18.225 73 24-120 2,4-Dinitrophenol ug/L 10.3J25 41 10-127 2,4-Dinitrotoluene ug/L 19.225 77 36-115 2,6-Dinitrotoluene ug/L 19.625 78 37-114 2-Chloronaphthalene ug/L 16.925 68 36-101 2-Chlorophenol ug/L 20.125 80 24-120 2-Methylnaphthalene ug/L 19.025 76 19-120 2-Methylphenol(o-Cresol)ug/L 16.525 66 25-120 2-Nitroaniline ug/L 20.3J25 81 30-109 2-Nitrophenol ug/L 18.925 75 24-120 3&4-Methylphenol(m&p Cresol)ug/L 15.325 61 24-120 3,3'-Dichlorobenzidine ug/L 20.7J25 83 14-120 3-Nitroaniline ug/L 24.8J25 99 23-133 4,6-Dinitro-2-methylphenol ug/L 11.6J25 46 10-128 4-Bromophenylphenyl ether ug/L 21.425 86 35-113 4-Chloro-3-methylphenol ug/L 19J25 76 32-107 4-Chloroaniline ug/L 25J25 100 12-150 4-Chlorophenylphenyl ether ug/L 20.125 81 36-110 4-Nitroaniline ug/L 23J25 92 12-150 4-Nitrophenol ug/L 17.9J25 72 10-120 Acenaphthene ug/L 18.425 74 27-102 Acenaphthylene ug/L 19.425 78 25-105 Aniline ug/L 15.325 61 10-150 Anthracene ug/L 20.525 82 30-113 Benzo(a)anthracene ug/L 19.325 77 27-113 Benzo(a)pyrene ug/L 19.225 77 27-119 Benzo(b)fluoranthene ug/L 15.925 64 22-114 Benzo(g,h,i)perylene ug/L 15.725 63 10-129 Benzo(k)fluoranthene ug/L 20.225 81 24-111 Benzoic Acid ug/L ND L0252324-120 Benzyl alcohol ug/L 24.125 96 24-120 bis(2-Chloroethoxy)methane ug/L 22.425 90 32-120 bis(2-Chloroethyl) ether ug/L 24.825 99 29-120 bis(2-Chloroisopropyl) ether ug/L 23.625 94 22-120 bis(2-Ethylhexyl)phthalate ug/L 21.325 85 29-125 Butylbenzylphthalate ug/L 21.525 86 33-120 Chrysene ug/L 19.325 77 23-112 Di-n-butylphthalate ug/L 21.825 87 38-116 Di-n-octylphthalate ug/L 22.825 91 32-122 Dibenz(a,h)anthracene ug/L 18.325 73 10-129 Dibenzofuran ug/L 18.025 72 37-107 Diethylphthalate ug/L 22.225 89 40-111 Dimethylphthalate ug/L 21.125 84 39-108 Fluoranthene ug/L 20.325 81 27-112 Fluorene ug/L 18.725 75 29-107 Hexachloro-1,3-butadiene ug/L 9.3J25 37 10-113 Hexachlorobenzene ug/L 19.025 76 29-119 Hexachlorocyclopentadiene ug/L 7.5J25 30 10-113 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 30 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335997LABORATORY CONTROL SAMPLE: LCSSpike Hexachloroethane ug/L 7.8J25 31 10-120 Indeno(1,2,3-cd)pyrene ug/L 18.225 73 14-123 Isophorone ug/L 18.725 75 23-150 N-Nitroso-di-n-propylamine ug/L 23.425 94 31-104 N-Nitrosodimethylamine ug/L 16.325 65 10-120 N-Nitrosodiphenylamine ug/L 25.325 101 27-139 Naphthalene ug/L 15.125 60 17-120 Nitrobenzene ug/L 18.025 72 27-120 Pentachlorophenol ug/L 12.9J25 51 10-135 Phenanthrene ug/L 19.525 78 28-111 Phenol ug/L 7.4J25 30 10-120 Pyrene ug/L 17.925 71 27-113 2,4,6-Tribromophenol (S)%76 25-150 2-Fluorobiphenyl (S)%73 30-150 2-Fluorophenol (S)%48 25-150 Nitrobenzene-d5 (S)%71 30-150 Phenol-d6 (S)%29 25-150 Terphenyl-d14 (S)%71 30-150 Parameter Units MS Result % Rec Limits Qual% RecConc. 335998MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252704001 335999 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,2,4-Trichlorobenzene ug/L R11114513-12058 32119ND50.0 68.9 1,4-Dichlorobenzene ug/L R11114419-12059 35119ND49.3 70.1 2,4-Dinitrotoluene ug/L R11115441-10969 31119ND59.6 81.6 2-Chlorophenol ug/L R11115933-12077 33119ND65.9 91.9 4-Chloro-3-methylphenol ug/L 111 58 30-10872 27119ND64.8 85.2 4-Nitrophenol ug/L 111 51 10-12066119ND56.8J 78.8J Acenaphthene ug/L 111 59 27-10172 28119ND65.1 86.2 N-Nitroso-di-n-propylamine ug/L 111 78 34-12086 16119ND87.0 102 Pentachlorophenol ug/L 111 59 10-13865119ND65.3J 77.9J Phenol ug/L R11114010-12055 38119ND44.8 65.6 Pyrene ug/L 111 71 31-11079 17119ND79.4 93.9 2,4,6-Tribromophenol (S)%66 25-15080 2-Fluorobiphenyl (S)%57 30-15073 2-Fluorophenol (S)%40 25-15051 Nitrobenzene-d5 (S)%50 30-15064 Phenol-d6 (S)%36 25-15048 Terphenyl-d14 (S)%71 30-15077 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 31 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/8261 EPA 8260 EPA 8260 8260 MSV Low Level Associated Lab Samples:9252704001, 9252704002, 9252704003, 9252704004, 9252704005, 9252704006, 9252704007, 9252704008,9252704009 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335656 Associated Lab Samples:9252704001, 9252704002, 9252704003, 9252704004, 9252704005, 9252704006, 9252704007, 9252704008,9252704009 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/13/09 01:36 1,1,1-Trichloroethane ug/L ND 1.0 09/13/09 01:36 1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/13/09 01:36 1,1,2-Trichloroethane ug/L ND 1.0 09/13/09 01:36 1,1-Dichloroethane ug/L ND 1.0 09/13/09 01:36 1,1-Dichloroethene ug/L ND 1.0 09/13/09 01:36 1,1-Dichloropropene ug/L ND 1.0 09/13/09 01:36 1,2,3-Trichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,2,3-Trichloropropane ug/L ND 1.0 09/13/09 01:36 1,2,4-Trichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,2-Dibromo-3-chloropropane ug/L ND 3.0 09/13/09 01:36 1,2-Dibromoethane (EDB)ug/L ND 1.0 09/13/09 01:36 1,2-Dichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,2-Dichloroethane ug/L ND 1.0 09/13/09 01:36 1,2-Dichloropropane ug/L ND 1.0 09/13/09 01:36 1,3-Dichlorobenzene ug/L ND 1.0 09/13/09 01:36 1,3-Dichloropropane ug/L ND 1.0 09/13/09 01:36 1,4-Dichlorobenzene ug/L ND 1.0 09/13/09 01:36 2,2-Dichloropropane ug/L ND 1.0 09/13/09 01:36 2-Butanone (MEK)ug/L ND 5.0 09/13/09 01:36 2-Chlorotoluene ug/L ND 1.0 09/13/09 01:36 2-Hexanone ug/L ND 5.0 09/13/09 01:36 4-Chlorotoluene ug/L ND 1.0 09/13/09 01:36 4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/13/09 01:36 Acetone ug/L ND 25.0 09/13/09 01:36 Benzene ug/L ND 1.0 09/13/09 01:36 Bromobenzene ug/L ND 1.0 09/13/09 01:36 Bromochloromethane ug/L ND 1.0 09/13/09 01:36 Bromodichloromethane ug/L ND 1.0 09/13/09 01:36 Bromoform ug/L ND 1.0 09/13/09 01:36 Bromomethane ug/L ND 5.0 09/13/09 01:36 Carbon tetrachloride ug/L ND 1.0 09/13/09 01:36 Chlorobenzene ug/L ND 1.0 09/13/09 01:36 Chloroethane ug/L ND 1.0 09/13/09 01:36 Chloroform ug/L ND 1.0 09/13/09 01:36 Chloromethane ug/L ND 1.0 09/13/09 01:36 cis-1,2-Dichloroethene ug/L ND 1.0 09/13/09 01:36 cis-1,3-Dichloropropene ug/L ND 1.0 09/13/09 01:36 Dibromochloromethane ug/L ND 1.0 09/13/09 01:36 Dibromomethane ug/L ND 1.0 09/13/09 01:36 Dichlorodifluoromethane ug/L ND 1.0 09/13/09 01:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 32 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:335656 Associated Lab Samples:9252704001, 9252704002, 9252704003, 9252704004, 9252704005, 9252704006, 9252704007, 9252704008,9252704009 Matrix:Water Analyzed Diisopropyl ether ug/L ND 1.0 09/13/09 01:36 Ethylbenzene ug/L ND 1.0 09/13/09 01:36 Hexachloro-1,3-butadiene ug/L ND 1.0 09/13/09 01:36 m&p-Xylene ug/L ND 2.0 09/13/09 01:36 Methyl-tert-butyl ether ug/L ND 1.0 09/13/09 01:36 Methylene Chloride ug/L ND 2.0 09/13/09 01:36 Naphthalene ug/L ND 1.0 09/13/09 01:36 o-Xylene ug/L ND 1.0 09/13/09 01:36 p-Isopropyltoluene ug/L ND 1.0 09/13/09 01:36 Styrene ug/L ND 1.0 09/13/09 01:36 Tetrachloroethene ug/L ND 1.0 09/13/09 01:36 Toluene ug/L ND 1.0 09/13/09 01:36 trans-1,2-Dichloroethene ug/L ND 1.0 09/13/09 01:36 trans-1,3-Dichloropropene ug/L ND 1.0 09/13/09 01:36 Trichloroethene ug/L ND 1.0 09/13/09 01:36 Trichlorofluoromethane ug/L ND 1.0 09/13/09 01:36 Vinyl acetate ug/L ND 2.0 09/13/09 01:36 Vinyl chloride ug/L ND 1.0 09/13/09 01:36 1,2-Dichloroethane-d4 (S)%99 79-120 09/13/09 01:36 4-Bromofluorobenzene (S)%99 87-109 09/13/09 01:36 Dibromofluoromethane (S)%101 85-115 09/13/09 01:36 Toluene-d8 (S)%98 70-120 09/13/09 01:36 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335657LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 48.350 97 83-125 1,1,1-Trichloroethane ug/L 45.750 91 80-129 1,1,2,2-Tetrachloroethane ug/L 46.050 92 73-127 1,1,2-Trichloroethane ug/L 49.750 99 77-123 1,1-Dichloroethane ug/L 47.650 95 76-129 1,1-Dichloroethene ug/L 49.450 99 78-146 1,1-Dichloropropene ug/L 48.550 97 79-134 1,2,3-Trichlorobenzene ug/L 47.750 95 70-150 1,2,3-Trichloropropane ug/L 46.450 93 72-125 1,2,4-Trichlorobenzene ug/L 47.250 94 68-127 1,2-Dibromo-3-chloropropane ug/L 49.150 98 65-128 1,2-Dibromoethane (EDB)ug/L 50.250 100 81-125 1,2-Dichlorobenzene ug/L 48.250 96 82-126 1,2-Dichloroethane ug/L 49.050 98 72-126 1,2-Dichloropropane ug/L 49.950 100 80-127 1,3-Dichlorobenzene ug/L 46.850 94 82-124 1,3-Dichloropropane ug/L 48.850 98 79-124 1,4-Dichlorobenzene ug/L 46.050 92 79-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 33 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 335657LABORATORY CONTROL SAMPLE: LCSSpike 2,2-Dichloropropane ug/L 42.550 85 58-140 2-Butanone (MEK)ug/L 95.0100 95 50-134 2-Chlorotoluene ug/L 45.950 92 81-126 2-Hexanone ug/L 92.7100 93 58-138 4-Chlorotoluene ug/L 47.950 96 82-126 4-Methyl-2-pentanone (MIBK)ug/L 95.8100 96 70-131 Acetone ug/L 103100 103 50-146 Benzene ug/L 46.650 93 78-128 Bromobenzene ug/L 48.350 97 81-127 Bromochloromethane ug/L 46.550 93 73-124 Bromodichloromethane ug/L 44.950 90 81-125 Bromoform ug/L 45.650 91 71-125 Bromomethane ug/L 63.350 127 50-150 Carbon tetrachloride ug/L 46.150 92 81-137 Chlorobenzene ug/L 46.750 93 82-126 Chloroethane ug/L 51.550 103 69-140 Chloroform ug/L 44.850 90 77-129 Chloromethane ug/L 44.350 89 54-139 cis-1,2-Dichloroethene ug/L 48.750 97 76-133 cis-1,3-Dichloropropene ug/L 49.050 98 76-127 Dibromochloromethane ug/L 44.550 89 77-125 Dibromomethane ug/L 47.550 95 77-125 Dichlorodifluoromethane ug/L 53.050 106 50-150 Diisopropyl ether ug/L 48.650 97 74-131 Ethylbenzene ug/L 47.450 95 80-127 Hexachloro-1,3-butadiene ug/L 43.850 88 78-145 m&p-Xylene ug/L 98.0100 98 82-127 Methyl-tert-butyl ether ug/L 50.250 100 71-130 Methylene Chloride ug/L 46.450 93 67-133 Naphthalene ug/L 50.350 101 52-136 o-Xylene ug/L 48.750 97 83-124 p-Isopropyltoluene ug/L 48.350 97 73-122 Styrene ug/L 48.250 96 80-130 Tetrachloroethene ug/L 46.450 93 78-128 Toluene ug/L 46.250 92 76-126 trans-1,2-Dichloroethene ug/L 44.750 89 78-134 trans-1,3-Dichloropropene ug/L 50.350 101 75-125 Trichloroethene ug/L 48.150 96 79-127 Trichlorofluoromethane ug/L 48.450 97 76-148 Vinyl acetate ug/L 82.4100 82 50-150 Vinyl chloride ug/L 51.850 104 67-143 1,2-Dichloroethane-d4 (S)%99 79-120 4-Bromofluorobenzene (S)%99 87-109 Dibromofluoromethane (S)%102 85-115 Toluene-d8 (S)%99 70-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 34 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A Parameter Units MS Result % Rec Limits Qual% RecConc. 335658MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 9252704001 335659 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1-Dichloroethene ug/L 50 100 60-150105 550ND49.8 52.3 Benzene ug/L 50 92 74-13696 450ND45.8 47.9 Chlorobenzene ug/L 50 90 79-13594 450ND45.2 47.0 Toluene ug/L 50 91 73-13195 450ND45.8 47.5 Trichloroethene ug/L 50 92 73-13196 450ND46.2 48.1 1,2-Dichloroethane-d4 (S)%98 79-12098 4-Bromofluorobenzene (S)%98 87-109101 Dibromofluoromethane (S)%100 85-115100 Toluene-d8 (S)%99 70-120100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 35 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Pace Project No.: Project: 9252704 1 FAIRVIEW ROAD 1411-09-040A DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. LABORATORIES Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the 2 remaining acidsurrogates.1g Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0 RPD value was outside control limits.R1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/24/2009 02:51 PM Page 36 of 36 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Soil, Groundwater, and Soil Gas Assessment ReportS&ME Project No. 1411-09-040A 1 Fairview Road Property - Asheville, NC October 16, 2009 APPENDIX VI (SOIL GAS LABORATORY RERPORT) September 29, 2009 LIMS USE: FR - DAVID LOFTIS LIMS OBJECT ID: 9252830 9252830 Project: Pace Project No.: RE: Mr. David LoftisS&ME44 Buck Shoals RoadArden, NC 28704 1 FAIRVIEW RD 1411-09-040A Dear Mr. Loftis: Enclosed are the analytical results for sample(s) received by the laboratory on September 10, 2009. The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of the report. Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All Microbiological analyses were performed at the laboratory where the samples were received. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Minnesota Certification IDsWisconsin Certification #: 999407970Alaska Certification #: UST-078Tennessee Certification #: 02818Pennsylvania Certification #: 68-00563Oregon Certification #: MN200001North Dakota Certification #: R-036North Carolina Certification #: 530New York Certification #: 11647New Jersey Certification #: MN-002Montana Certification #: MT CERT0092Minnesota Certification #: 027-053-137 Maine Certification #: 2007029Louisiana Certification #: 03086Louisiana Certification #: LA080009Kansas Certification #: E-10167Iowa Certification #: 368Illinois Certification #: 200011Florida/NELAP Certification #: E87605California Certification #: 01155CAArizona Certification #: AZ-0014Washington Certification #: C754 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 SAMPLE ANALYTE COUNT Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 9252830001 1 FAIR - SG1-09-09 TO-15 57 PASI-MLCW 9252830002 1 FAIR - SG2-09-09 TO-15 57 PASI-MLCW 9252830003 1 FAIR - DUP1-09-09 TO-15 57 PASI-MLCW REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR - SG1-09-09 Lab ID:9252830001 Collected:09/09/09 15:42 Received:09/10/09 13:28 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone ND ug/m3 4812.8 09/26/09 06:45 67-64-12310 Benzene 3520 ug/m3 4812.8 09/26/09 06:45 71-43-23130 Bromodichloromethane ND ug/m3 4812.8 09/26/09 06:45 75-27-46740 Bromoform ND ug/m3 4812.8 09/26/09 06:45 75-25-210100 Bromomethane ND ug/m3 4812.8 09/26/09 06:45 74-83-93800 1,3-Butadiene ND ug/m3 4812.8 09/26/09 06:45 106-99-02170 2-Butanone (MEK)ND ug/m3 4812.8 09/26/09 06:45 78-93-32890 Carbon disulfide ND ug/m3 4812.8 09/26/09 06:45 75-15-03030 Carbon tetrachloride ND ug/m3 4812.8 09/26/09 06:45 56-23-56260 Chlorobenzene ND ug/m3 4812.8 09/26/09 06:45 108-90-74520 Chloroethane ND ug/m3 4812.8 09/26/09 06:45 75-00-32600 Chloroform ND ug/m3 4812.8 09/26/09 06:45 67-66-34760 Chloromethane ND ug/m3 4812.8 09/26/09 06:45 74-87-32020 Cyclohexane 38000 ug/m3 4812.8 09/26/09 06:45 110-82-73270 Dibromochloromethane ND ug/m3 4812.8 09/26/09 06:45 124-48-18180 1,2-Dibromoethane (EDB)ND ug/m3 4812.8 09/26/09 06:45 106-93-47700 1,2-Dichlorobenzene ND ug/m3 4812.8 09/26/09 06:45 95-50-15780 1,3-Dichlorobenzene ND ug/m3 4812.8 09/26/09 06:45 541-73-15780 1,4-Dichlorobenzene ND ug/m3 4812.8 09/26/09 06:45 106-46-75780 Dichlorodifluoromethane ND ug/m3 4812.8 09/26/09 06:45 75-71-8 D34810 1,1-Dichloroethane ND ug/m3 4812.8 09/26/09 06:45 75-34-33950 1,2-Dichloroethane ND ug/m3 4812.8 09/26/09 06:45 107-06-23950 1,1-Dichloroethene ND ug/m3 4812.8 09/26/09 06:45 75-35-43900 cis-1,2-Dichloroethene ND ug/m3 4812.8 09/26/09 06:45 156-59-23900 trans-1,2-Dichloroethene ND ug/m3 4812.8 09/26/09 06:45 156-60-53900 1,2-Dichloropropane ND ug/m3 4812.8 09/26/09 06:45 78-87-54520 cis-1,3-Dichloropropene ND ug/m3 4812.8 09/26/09 06:45 10061-01-54430 trans-1,3-Dichloropropene ND ug/m3 4812.8 09/26/09 06:45 10061-02-64430 Dichlorotetrafluoroethane ND ug/m3 4812.8 09/26/09 06:45 76-14-26740 Ethyl acetate ND ug/m3 4812.8 09/26/09 06:45 141-78-63510 Ethylbenzene 17000 ug/m3 4812.8 09/26/09 06:45 100-41-44240 4-Ethyltoluene 24900 ug/m3 4812.8 09/26/09 06:45 622-96-812000 n-Heptane ND ug/m3 4812.8 09/26/09 06:45 142-82-53990 Hexachloro-1,3-butadiene ND ug/m3 4812.8 09/26/09 06:45 87-68-310600 n-Hexane 12600 ug/m3 4812.8 09/26/09 06:45 110-54-33470 2-Hexanone ND ug/m3 4812.8 09/26/09 06:45 591-78-63990 Methylene Chloride ND ug/m3 4812.8 09/26/09 06:45 75-09-23420 4-Methyl-2-pentanone (MIBK)ND ug/m3 4812.8 09/26/09 06:45 108-10-13990 Methyl-tert-butyl ether ND ug/m3 4812.8 09/26/09 06:45 1634-04-43510 Propylene ND ug/m3 4812.8 09/26/09 06:45 115-07-11680 Styrene ND ug/m3 4812.8 09/26/09 06:45 100-42-54190 1,1,2,2-Tetrachloroethane ND ug/m3 4812.8 09/26/09 06:45 79-34-56740 Tetrachloroethene ND ug/m3 4812.8 09/26/09 06:45 127-18-46740 Tetrahydrofuran ND ug/m3 4812.8 09/26/09 06:45 109-99-92890 Toluene ND ug/m3 4812.8 09/26/09 06:45 108-88-33710 1,2,4-Trichlorobenzene ND ug/m3 4812.8 09/26/09 06:45 120-82-14760 1,1,1-Trichloroethane ND ug/m3 4812.8 09/26/09 06:45 71-55-65290 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 4 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR - SG1-09-09 Lab ID:9252830001 Collected:09/09/09 15:42 Received:09/10/09 13:28 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 1,1,2-Trichloroethane ND ug/m3 4812.8 09/26/09 06:45 79-00-55290 Trichloroethene ND ug/m3 4812.8 09/26/09 06:45 79-01-65290 Trichlorofluoromethane ND ug/m3 4812.8 09/26/09 06:45 75-69-45290 1,1,2-Trichlorotrifluoroethane ND ug/m3 4812.8 09/26/09 06:45 76-13-17700 1,2,4-Trimethylbenzene ND ug/m3 4812.8 09/26/09 06:45 95-63-612000 1,3,5-Trimethylbenzene 14500 ug/m3 4812.8 09/26/09 06:45 108-67-812000 Vinyl acetate ND ug/m3 4812.8 09/26/09 06:45 108-05-43420 Vinyl chloride ND ug/m3 4812.8 09/26/09 06:45 75-01-42500 m&p-Xylene 36600 ug/m3 4812.8 09/26/09 06:45 1330-20-78470 o-Xylene ND ug/m3 4812.8 09/26/09 06:45 95-47-64240 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 5 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR - SG2-09-09 Lab ID:9252830002 Collected:09/09/09 15:55 Received:09/10/09 13:28 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone ND ug/m3 13.4 09/26/09 04:48 67-64-16.4 Benzene 22.3 ug/m3 13.4 09/26/09 04:48 71-43-28.7 Bromodichloromethane ND ug/m3 13.4 09/26/09 04:48 75-27-418.8 Bromoform ND ug/m3 13.4 09/26/09 04:48 75-25-228.1 Bromomethane ND ug/m3 13.4 09/26/09 04:48 74-83-910.6 1,3-Butadiene ND ug/m3 13.4 09/26/09 04:48 106-99-06.0 2-Butanone (MEK)ND ug/m3 13.4 09/26/09 04:48 78-93-38.0 Carbon disulfide ND ug/m3 13.4 09/26/09 04:48 75-15-08.4 Carbon tetrachloride ND ug/m3 13.4 09/26/09 04:48 56-23-517.4 Chlorobenzene ND ug/m3 13.4 09/26/09 04:48 108-90-712.6 Chloroethane ND ug/m3 13.4 09/26/09 04:48 75-00-37.2 Chloroform ND ug/m3 13.4 09/26/09 04:48 67-66-313.3 Chloromethane ND ug/m3 13.4 09/26/09 04:48 74-87-35.6 Cyclohexane 825 ug/m3 13.4 09/26/09 04:48 110-82-79.1 Dibromochloromethane ND ug/m3 13.4 09/26/09 04:48 124-48-122.8 1,2-Dibromoethane (EDB)ND ug/m3 13.4 09/26/09 04:48 106-93-421.4 1,2-Dichlorobenzene ND ug/m3 13.4 09/26/09 04:48 95-50-116.1 1,3-Dichlorobenzene ND ug/m3 13.4 09/26/09 04:48 541-73-116.1 1,4-Dichlorobenzene ND ug/m3 13.4 09/26/09 04:48 106-46-716.1 Dichlorodifluoromethane ND ug/m3 13.4 09/26/09 04:48 75-71-8 D313.4 1,1-Dichloroethane ND ug/m3 13.4 09/26/09 04:48 75-34-311.0 1,2-Dichloroethane ND ug/m3 13.4 09/26/09 04:48 107-06-211.0 1,1-Dichloroethene ND ug/m3 13.4 09/26/09 04:48 75-35-410.9 cis-1,2-Dichloroethene ND ug/m3 13.4 09/26/09 04:48 156-59-210.9 trans-1,2-Dichloroethene ND ug/m3 13.4 09/26/09 04:48 156-60-510.9 1,2-Dichloropropane ND ug/m3 13.4 09/26/09 04:48 78-87-512.6 cis-1,3-Dichloropropene ND ug/m3 13.4 09/26/09 04:48 10061-01-512.3 trans-1,3-Dichloropropene ND ug/m3 13.4 09/26/09 04:48 10061-02-612.3 Dichlorotetrafluoroethane ND ug/m3 13.4 09/26/09 04:48 76-14-218.8 Ethyl acetate ND ug/m3 13.4 09/26/09 04:48 141-78-69.8 Ethylbenzene 31.9 ug/m3 13.4 09/26/09 04:48 100-41-411.8 4-Ethyltoluene 45.9 ug/m3 13.4 09/26/09 04:48 622-96-833.5 n-Heptane ND ug/m3 13.4 09/26/09 04:48 142-82-511.1 Hexachloro-1,3-butadiene ND ug/m3 13.4 09/26/09 04:48 87-68-329.5 n-Hexane 39.1 ug/m3 13.4 09/26/09 04:48 110-54-39.6 2-Hexanone ND ug/m3 13.4 09/26/09 04:48 591-78-611.1 Methylene Chloride ND ug/m3 13.4 09/26/09 04:48 75-09-29.5 4-Methyl-2-pentanone (MIBK)ND ug/m3 13.4 09/26/09 04:48 108-10-111.1 Methyl-tert-butyl ether ND ug/m3 13.4 09/26/09 04:48 1634-04-49.8 Propylene ND ug/m3 13.4 09/26/09 04:48 115-07-14.7 Styrene ND ug/m3 13.4 09/26/09 04:48 100-42-511.7 1,1,2,2-Tetrachloroethane ND ug/m3 13.4 09/26/09 04:48 79-34-518.8 Tetrachloroethene ND ug/m3 13.4 09/26/09 04:48 127-18-418.8 Tetrahydrofuran ND ug/m3 13.4 09/26/09 04:48 109-99-98.0 Toluene 51.3 ug/m3 13.4 09/26/09 04:48 108-88-310.3 1,2,4-Trichlorobenzene ND ug/m3 13.4 09/26/09 04:48 120-82-113.3 1,1,1-Trichloroethane ND ug/m3 13.4 09/26/09 04:48 71-55-614.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 6 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR - SG2-09-09 Lab ID:9252830002 Collected:09/09/09 15:55 Received:09/10/09 13:28 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 1,1,2-Trichloroethane ND ug/m3 13.4 09/26/09 04:48 79-00-514.7 Trichloroethene ND ug/m3 13.4 09/26/09 04:48 79-01-614.7 Trichlorofluoromethane ND ug/m3 13.4 09/26/09 04:48 75-69-414.7 1,1,2-Trichlorotrifluoroethane ND ug/m3 13.4 09/26/09 04:48 76-13-121.4 1,2,4-Trimethylbenzene ND ug/m3 13.4 09/26/09 04:48 95-63-633.5 1,3,5-Trimethylbenzene 36.3 ug/m3 13.4 09/26/09 04:48 108-67-833.5 Vinyl acetate ND ug/m3 13.4 09/26/09 04:48 108-05-49.5 Vinyl chloride ND ug/m3 13.4 09/26/09 04:48 75-01-47.0 m&p-Xylene 64.9 ug/m3 13.4 09/26/09 04:48 1330-20-723.6 o-Xylene 33.6 ug/m3 13.4 09/26/09 04:48 95-47-611.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 7 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR - DUP1-09-09 Lab ID:9252830003 Collected:09/09/09 00:00 Received:09/10/09 13:28 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 Acetone ND ug/m3 110.4 09/26/09 05:17 67-64-153.0 Benzene 2180 ug/m3 110.4 09/26/09 05:17 71-43-271.8 Bromodichloromethane ND ug/m3 110.4 09/26/09 05:17 75-27-4155 Bromoform ND ug/m3 110.4 09/26/09 05:17 75-25-2232 Bromomethane ND ug/m3 110.4 09/26/09 05:17 74-83-987.2 1,3-Butadiene ND ug/m3 110.4 09/26/09 05:17 106-99-049.7 2-Butanone (MEK)ND ug/m3 110.4 09/26/09 05:17 78-93-366.2 Carbon disulfide ND ug/m3 110.4 09/26/09 05:17 75-15-069.6 Carbon tetrachloride ND ug/m3 110.4 09/26/09 05:17 56-23-5144 Chlorobenzene ND ug/m3 110.4 09/26/09 05:17 108-90-7104 Chloroethane ND ug/m3 110.4 09/26/09 05:17 75-00-359.6 Chloroform ND ug/m3 110.4 09/26/09 05:17 67-66-3109 Chloromethane ND ug/m3 110.4 09/26/09 05:17 74-87-346.4 Cyclohexane 49700 ug/m3 110.4 09/26/09 05:17 110-82-7 E75.1 Dibromochloromethane ND ug/m3 110.4 09/26/09 05:17 124-48-1188 1,2-Dibromoethane (EDB)ND ug/m3 110.4 09/26/09 05:17 106-93-4177 1,2-Dichlorobenzene ND ug/m3 110.4 09/26/09 05:17 95-50-1132 1,3-Dichlorobenzene ND ug/m3 110.4 09/26/09 05:17 541-73-1132 1,4-Dichlorobenzene ND ug/m3 110.4 09/26/09 05:17 106-46-7132 Dichlorodifluoromethane ND ug/m3 110.4 09/26/09 05:17 75-71-8110 1,1-Dichloroethane ND ug/m3 110.4 09/26/09 05:17 75-34-390.5 1,2-Dichloroethane ND ug/m3 110.4 09/26/09 05:17 107-06-290.5 1,1-Dichloroethene ND ug/m3 110.4 09/26/09 05:17 75-35-489.4 cis-1,2-Dichloroethene ND ug/m3 110.4 09/26/09 05:17 156-59-289.4 trans-1,2-Dichloroethene ND ug/m3 110.4 09/26/09 05:17 156-60-589.4 1,2-Dichloropropane ND ug/m3 110.4 09/26/09 05:17 78-87-5104 cis-1,3-Dichloropropene ND ug/m3 110.4 09/26/09 05:17 10061-01-5102 trans-1,3-Dichloropropene ND ug/m3 110.4 09/26/09 05:17 10061-02-6102 Dichlorotetrafluoroethane ND ug/m3 110.4 09/26/09 05:17 76-14-2155 Ethyl acetate ND ug/m3 110.4 09/26/09 05:17 141-78-680.6 Ethylbenzene 2810 ug/m3 110.4 09/26/09 05:17 100-41-497.2 4-Ethyltoluene 3470 ug/m3 110.4 09/26/09 05:17 622-96-8276 n-Heptane 2810 ug/m3 110.4 09/26/09 05:17 142-82-591.6 Hexachloro-1,3-butadiene ND ug/m3 110.4 09/26/09 05:17 87-68-3243 n-Hexane 3240 ug/m3 110.4 09/26/09 05:17 110-54-379.5 2-Hexanone ND ug/m3 110.4 09/26/09 05:17 591-78-691.6 Methylene Chloride ND ug/m3 110.4 09/26/09 05:17 75-09-278.4 4-Methyl-2-pentanone (MIBK)ND ug/m3 110.4 09/26/09 05:17 108-10-191.6 Methyl-tert-butyl ether ND ug/m3 110.4 09/26/09 05:17 1634-04-480.6 Propylene 111 ug/m3 110.4 09/26/09 05:17 115-07-138.6 Styrene ND ug/m3 110.4 09/26/09 05:17 100-42-596.0 1,1,2,2-Tetrachloroethane ND ug/m3 110.4 09/26/09 05:17 79-34-5155 Tetrachloroethene ND ug/m3 110.4 09/26/09 05:17 127-18-4155 Tetrahydrofuran ND ug/m3 110.4 09/26/09 05:17 109-99-966.2 Toluene ND ug/m3 110.4 09/26/09 05:17 108-88-385.0 1,2,4-Trichlorobenzene ND ug/m3 110.4 09/26/09 05:17 120-82-1109 1,1,1-Trichloroethane ND ug/m3 110.4 09/26/09 05:17 71-55-6121 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 8 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Sample:1 FAIR - DUP1-09-09 Lab ID:9252830003 Collected:09/09/09 00:00 Received:09/10/09 13:28 Matrix:Air Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit TO15 MSV AIR Analytical Method: TO-15 1,1,2-Trichloroethane ND ug/m3 110.4 09/26/09 05:17 79-00-5121 Trichloroethene ND ug/m3 110.4 09/26/09 05:17 79-01-6121 Trichlorofluoromethane ND ug/m3 110.4 09/26/09 05:17 75-69-4121 1,1,2-Trichlorotrifluoroethane ND ug/m3 110.4 09/26/09 05:17 76-13-1177 1,2,4-Trimethylbenzene 2310 ug/m3 110.4 09/26/09 05:17 95-63-6276 1,3,5-Trimethylbenzene 2210 ug/m3 110.4 09/26/09 05:17 108-67-8276 Vinyl acetate ND ug/m3 110.4 09/26/09 05:17 108-05-478.4 Vinyl chloride ND ug/m3 110.4 09/26/09 05:17 75-01-457.4 m&p-Xylene 5180 ug/m3 110.4 09/26/09 05:17 1330-20-7194 o-Xylene 852 ug/m3 110.4 09/26/09 05:17 95-47-697.2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 9 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A QC Batch: QC Batch Method: Analysis Method: Analysis Description: AIR/9162 TO-15 TO-15 TO15 MSV AIR Low Level Associated Lab Samples:9252830001, 9252830002, 9252830003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:686858 Associated Lab Samples:9252830001, 9252830002, 9252830003 Matrix:Air Analyzed 1,1,1-Trichloroethane ug/m3 ND 1.1 09/25/09 17:04 1,1,2,2-Tetrachloroethane ug/m3 ND 1.4 09/25/09 17:04 1,1,2-Trichloroethane ug/m3 ND 1.1 09/25/09 17:04 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 09/25/09 17:04 1,1-Dichloroethane ug/m3 ND 0.82 09/25/09 17:04 1,1-Dichloroethene ug/m3 ND 0.81 09/25/09 17:04 1,2,4-Trichlorobenzene ug/m3 ND 0.99 09/25/09 17:04 1,2,4-Trimethylbenzene ug/m3 ND 2.5 09/25/09 17:04 1,2-Dibromoethane (EDB)ug/m3 ND 1.6 09/25/09 17:04 1,2-Dichlorobenzene ug/m3 ND 1.2 09/25/09 17:04 1,2-Dichloroethane ug/m3 ND 0.82 09/25/09 17:04 1,2-Dichloropropane ug/m3 ND 0.94 09/25/09 17:04 1,3,5-Trimethylbenzene ug/m3 ND 2.5 09/25/09 17:04 1,3-Butadiene ug/m3 ND 0.45 09/25/09 17:04 1,3-Dichlorobenzene ug/m3 ND 1.2 09/25/09 17:04 1,4-Dichlorobenzene ug/m3 ND 1.2 09/25/09 17:04 2-Butanone (MEK)ug/m3 ND 0.60 09/25/09 17:04 2-Hexanone ug/m3 ND 0.83 09/25/09 17:04 4-Ethyltoluene ug/m3 ND 2.5 09/25/09 17:04 4-Methyl-2-pentanone (MIBK)ug/m3 ND 0.83 09/25/09 17:04 Acetone ug/m3 ND 0.48 09/25/09 17:04 Benzene ug/m3 ND 0.65 09/25/09 17:04 Bromodichloromethane ug/m3 ND 1.4 09/25/09 17:04 Bromoform ug/m3 ND 2.1 09/25/09 17:04 Bromomethane ug/m3 ND 0.79 09/25/09 17:04 Carbon disulfide ug/m3 ND 0.63 09/25/09 17:04 Carbon tetrachloride ug/m3 ND 1.3 09/25/09 17:04 Chlorobenzene ug/m3 ND 0.94 09/25/09 17:04 Chloroethane ug/m3 ND 0.54 09/25/09 17:04 Chloroform ug/m3 ND 0.99 09/25/09 17:04 Chloromethane ug/m3 ND 0.42 09/25/09 17:04 cis-1,2-Dichloroethene ug/m3 ND 0.81 09/25/09 17:04 cis-1,3-Dichloropropene ug/m3 ND 0.92 09/25/09 17:04 Cyclohexane ug/m3 ND 0.68 09/25/09 17:04 Dibromochloromethane ug/m3 ND 1.7 09/25/09 17:04 Dichlorodifluoromethane ug/m3 ND 1.0 09/25/09 17:04 Dichlorotetrafluoroethane ug/m3 ND 1.4 09/25/09 17:04 Ethyl acetate ug/m3 ND 0.73 09/25/09 17:04 Ethylbenzene ug/m3 ND 0.88 09/25/09 17:04 Hexachloro-1,3-butadiene ug/m3 ND 2.2 09/25/09 17:04 m&p-Xylene ug/m3 ND 1.8 09/25/09 17:04 Methyl-tert-butyl ether ug/m3 ND 0.73 09/25/09 17:04 Methylene Chloride ug/m3 ND 0.71 09/25/09 17:04 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 10 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:686858 Associated Lab Samples:9252830001, 9252830002, 9252830003 Matrix:Air Analyzed n-Heptane ug/m3 ND 0.83 09/25/09 17:04 n-Hexane ug/m3 ND 0.72 09/25/09 17:04 o-Xylene ug/m3 ND 0.88 09/25/09 17:04 Propylene ug/m3 ND 0.35 09/25/09 17:04 Styrene ug/m3 ND 0.87 09/25/09 17:04 Tetrachloroethene ug/m3 ND 1.4 09/25/09 17:04 Tetrahydrofuran ug/m3 ND 0.60 09/25/09 17:04 Toluene ug/m3 ND 0.77 09/25/09 17:04 trans-1,2-Dichloroethene ug/m3 ND 0.81 09/25/09 17:04 trans-1,3-Dichloropropene ug/m3 ND 0.92 09/25/09 17:04 Trichloroethene ug/m3 ND 1.1 09/25/09 17:04 Trichlorofluoromethane ug/m3 ND 1.1 09/25/09 17:04 Vinyl acetate ug/m3 ND 0.71 09/25/09 17:04 Vinyl chloride ug/m3 ND 0.52 09/25/09 17:04 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 686859LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1-Trichloroethane ug/m3 51.263 81 55-127 1,1,2,2-Tetrachloroethane ug/m3 60.269.8 86 58-128 1,1,2-Trichloroethane ug/m3 45.855.5 83 58-126 1,1,2-Trichlorotrifluoroethane ug/m3 61.977.9 80 49-134 1,1-Dichloroethane ug/m3 37.941.1 92 52-129 1,1-Dichloroethene ug/m3 43.540.3 108 50-130 1,2,4-Trichlorobenzene ug/m3 53.375.4 71 30-150 1,2,4-Trimethylbenzene ug/m3 46.550 93 53-144 1,2-Dibromoethane (EDB)ug/m3 65.578.1 84 57-137 1,2-Dichlorobenzene ug/m3 49.861.1 81 65-140 1,2-Dichloroethane ug/m3 48.444.9 108 54-125 1,2-Dichloropropane ug/m3 61.150.8 120 60-125 1,3,5-Trimethylbenzene ug/m3 45.150 90 54-139 1,3-Butadiene ug/m3 23.722.5 105 54-125 1,3-Dichlorobenzene ug/m3 51.961.1 85 62-140 1,4-Dichlorobenzene ug/m3 48.261.1 79 61-139 2-Butanone (MEK)ug/m3 26.030 87 47-138 2-Hexanone ug/m3 31.041.6 74 40-143 4-Ethyltoluene ug/m3 41.050 82 57-139 4-Methyl-2-pentanone (MIBK)ug/m3 31.041.6 75 54-132 Acetone ug/m3 14.524.1 60 44-147 Benzene ug/m3 35.632.8 108 60-125 Bromodichloromethane ug/m3 58.168.1 85 53-130 Bromoform ug/m3 107105 102 55-125 Bromomethane ug/m3 43.239.9 108 53-132 Carbon disulfide ug/m3 28.231.7 89 57-150 Carbon tetrachloride ug/m3 60.464 95 53-125 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 11 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 686859LABORATORY CONTROL SAMPLE: LCSSpike Chlorobenzene ug/m3 55.246.8 118 50-136 Chloroethane ug/m3 28.126.8 105 55-130 Chloroform ug/m3 53.949.6 109 56-125 Chloromethane ug/m3 24.321 116 49-127 cis-1,2-Dichloroethene ug/m3 44.540.3 110 58-127 cis-1,3-Dichloropropene ug/m3 45.748.5 94 62-135 Cyclohexane ug/m3 40.735.7 114 56-135 Dibromochloromethane ug/m3 71.886.6 83 48-132 Dichlorodifluoromethane ug/m3 42.050.3 84 54-130 Dichlorotetrafluoroethane ug/m3 64.071.1 90 50-125 Ethyl acetate ug/m3 41.136.6 112 70-141 Ethylbenzene ug/m3 44.248.7 91 57-135 Hexachloro-1,3-butadiene ug/m3 70.1108 65 30-150 m&p-Xylene ug/m3 88.892.7 96 61-135 Methyl-tert-butyl ether ug/m3 39.036.6 106 56-130 Methylene Chloride ug/m3 18.934.6 55 49-127 n-Heptane ug/m3 43.241.7 104 57-133 n-Hexane ug/m3 36.435.8 102 55-135 o-Xylene ug/m3 40.744.1 92 60-134 Propylene ug/m3 15.217.5 87 63-147 Styrene ug/m3 35.143.3 81 58-142 Tetrachloroethene ug/m3 80.271.7 112 61-132 Tetrahydrofuran ug/m3 17.522.5 78 67-134 Toluene ug/m3 44.038.3 115 56-132 trans-1,2-Dichloroethene ug/m3 45.941.9 109 52-131 trans-1,3-Dichloropropene ug/m3 38.546.1 83 62-131 Trichloroethene ug/m3 73.554.6 134 68-150 Trichlorofluoromethane ug/m3 60.657.1 106 52-142 Vinyl acetate ug/m3 34.635.8 97 53-136 Vinyl chloride ug/m3 26.326 101 57-132 Parameter Units Dup Result QualifiersRPDResult 10112542003 687891SAMPLE DUPLICATE: 1,1,1-Trichloroethane ug/m3 ND 1,1,2,2-Tetrachloroethane ug/m3 ND 1,1,2-Trichloroethane ug/m3 ND 1,1,2-Trichlorotrifluoroethane ug/m3 ND 1,1-Dichloroethane ug/m3 ND 1,1-Dichloroethene ug/m3 ND 1,2,4-Trichlorobenzene ug/m3 ND 1,2,4-Trimethylbenzene ug/m3 ND 1,2-Dibromoethane (EDB)ug/m3 ND 1,2-Dichlorobenzene ug/m3 ND 1,2-Dichloroethane ug/m3 ND 1,2-Dichloropropane ug/m3 ND 1,3,5-Trimethylbenzene ug/m3 ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 12 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A Parameter Units Dup Result QualifiersRPDResult 10112542003 687891SAMPLE DUPLICATE: 1,3-Butadiene ug/m3 ND 1,3-Dichlorobenzene ug/m3 ND 1,4-Dichlorobenzene ug/m3 ND 2-Butanone (MEK)ug/m3 2.9 6 2-Hexanone ug/m3 ND 4-Ethyltoluene ug/m3 6.0 2 4-Methyl-2-pentanone (MIBK)ug/m3 2.0 2 Acetone ug/m3 22.5 8 Benzene ug/m3 1.4 7 Bromodichloromethane ug/m3 ND Bromoform ug/m3 ND Bromomethane ug/m3 ND Carbon disulfide ug/m3 1.3 1 Carbon tetrachloride ug/m3 ND Chlorobenzene ug/m3 ND Chloroethane ug/m3 ND Chloroform ug/m3 ND Chloromethane ug/m3 2.0 6 cis-1,2-Dichloroethene ug/m3 ND cis-1,3-Dichloropropene ug/m3 ND Cyclohexane ug/m3 ND Dibromochloromethane ug/m3 ND Dichlorodifluoromethane ug/m3 2.2 5 Dichlorotetrafluoroethane ug/m3 ND Ethyl acetate ug/m3 ND Ethylbenzene ug/m3 1.9 1 Hexachloro-1,3-butadiene ug/m3 ND m&p-Xylene ug/m3 4.0 2 Methyl-tert-butyl ether ug/m3 ND Methylene Chloride ug/m3 ND n-Heptane ug/m3 ND n-Hexane ug/m3 1.1 2 o-Xylene ug/m3 2.3 0 Propylene ug/m3 ND Styrene ug/m3 ND Tetrachloroethene ug/m3 ND Tetrahydrofuran ug/m3 ND Toluene ug/m3 10.2 6 trans-1,2-Dichloroethene ug/m3 ND trans-1,3-Dichloropropene ug/m3 ND Trichloroethene ug/m3 ND Trichlorofluoromethane ug/m3 1.7 5 Vinyl acetate ug/m3 3.1 17 Vinyl chloride ug/m3 ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 13 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALIFIERS Pace Project No.: Project: 9252830 1 FAIRVIEW RD 1411-09-040A DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes. U - Indicates the compound was analyzed for, but not detected. LABORATORIES Pace Analytical Services - MinneapolisPASI-M SAMPLE QUALIFIERS Sample: 9252830001 The sample was analyzed by serial dilution.[1] Sample: 9252830003 The sample was analyzed by serial dilution.[1] ANALYTE QUALIFIERS Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 Analyte concentration exceeded the calibration range. The reported result is estimated.E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Date: 09/29/2009 07:34 AM Page 14 of 14 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176