15019 Norfolk BF Post Const Rpt 20180329

State of North Carolina | Environmental Quality | Waste Management
1646 Mail Service Center | 217 West Jones Street | Raleigh, NC 27699-1646
919 707 8200 T

June 20, 2018

Sent Via E-mail

Matt Bramblett, PE
Hart & Hickman, PC
2923 South Tryon Street, Suite 100 Charlotte, NC 28203
[e-mail]

Subject: Post Construction Sampling and Impacts Map Letter Report
Former Norfolk Southern Intermodal Facility Charlotte, Mecklenburg County
Brownfields Project Number 15019-11-60

Dear Mr. Bramblett,
On March 29, 2018, the Department of Environmental Quality (DEQ) Brownfields Program
received the Post Construction Sampling and Impacts Map (Rev1) for the above referenced
Brownfields Property. DEQ Brownfields reviewed this document, and determined that comments
made by DEQ Brownfields to previous versions of this document have been incorporated as
requested. The post construction sampling requirement is complete and to the satisfaction of DEQ Brownfields.

Be advised that this response from the Brownfields Program does not waive any applicable
requirement for future submittals as may be required by the Brownfields Agreement. If you have
questions about this correspondence or require additional information, please feel free to contact me by phone at 704/661-0330 or by email at [e-mail].

Sincerely, Carolyn Minnich
Carolyn Minnich
Brownfields Project Manager

ec: Wolfe, David [e-mail] Pierotti, Doug [e-mail]

Via Email
March 29, 2018
NCDEQ
Division of Waste Management
Brownfields Program
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Ms. Carolyn Minnich

Re: Post-Construction Sampling and Impacts Map (Rev 1)
Former Norfolk Southern Intermodal Facility Brownfields Project No. 15019-11-60
Charlotte, North Carolina
H&H Project No. CAT-105

Dear Carolyn:

1.0 Introduction

On behalf of the City of Charlotte (City), Hart & Hickman, PC (H&H) is submitting this letter
report to summarize post-construction soil sampling activities and to provide a post-construction
soil and groundwater impacts map for the Former Norfolk Southern Intermodal Facility site in
accordance with the Brownfields Agreement (BFA). A Site Location Map is included as Figure
1.
The site is in the final stages of redevelopment as part of the Charlotte Area Transit System (CATS)
Light Rail Blue Line Extension (BLE). As we observed during our December 12, 2017 site visit,
the mass grading is complete and the surface construction is nearly complete. The contractor is
now completing paving and landscaping. The purpose of this report is to document post-
construction sampling activities and update the Brownfields map to show where impacts remain.
A general summary of the environmental activities conducted at the site is provided below.

Ms. Carolyn Minnich
March 29, 2018
Page 2

S:\AAA-Master Projects\Charlotte Area Transit System (CAT)\CAT-105 NSIF BF Closeout\Report\NSIF BF Post Construction Report.docx
2.0 Soil Sampling Methodology

On January 3, 2018, the North Carolina Department of Environmental Quality (DEQ) approved
H&H’s scope of work for post-construction soil sampling via email. On January 9, H&H
completed the soil sampling by advancing a decontaminated stainless steel hand auger at three
locations not under hardscape (BFSS-1, BFSS-2, and BFSS-3) on the northern, central and
southern parts of the Brownfields property, respectively. Sample locations are depicted on Figure
2. The northern location is a grassy area near the stormwater management pond; the central
location is in the landscaped area in front of the new maintenance building; and the southern
location is a grassy area adjacent to the Parkwood Station platforms.

Each hand auger location was advanced to two feet below ground surface (bgs) to assess
shallow/surface soil. Soils were observed for the presence of staining and odors, and field
screened for the presence of organic vapors with a calibrated photo-ionization detector (PID).
There were no obvious soil impacts based on field screening. Boring logs with lithologic
descriptions and field screening results are included in Appendix A. H&H collected a shallow
soil sample from 0-1 feet bgs from each location.

The soil samples were collected in laboratory-supplied containers, properly labeled, and placed
in an iced cooler. Samples were delivered to Prism Laboratories, Inc. (Prism) in Charlotte, North
Carolina for analysis under standard chain-of-custody protocol. Soil samples were analyzed for
volatile organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds
(SVOCs) by EPA Method 8270, and RCRA metals by EPA Methods 6020/7471. The laboratory
analytical data report is provided in Appendix B. After sampling, hand auger locations were
backfilled with hydrated bentonite.

3.0 Soil Analytical Results

The most important factor is that the soil results be acceptable for non-residential (i.e., industrial
uses). Therefore, the results were compared to DEQ Inactive Hazardous Site Branch (IHSB)
Ms. Carolyn Minnich
March 29, 2018
Page 3

S:\AAA-Master Projects\Charlotte Area Transit System (CAT)\CAT-105 NSIF BF Closeout\Report\NSIF BF Post Construction Report.docx
Preliminary Industrial Health-Based Soil Remediation Goals (PSRGs) dated February 2018.
Metal results were also compared to two times the average regional background metal
concentrations (2x background). Soil analytical results are summarized on Table 1. Background
concentrations were obtained from published sources as also documented on Table 1.

The VOC compound acetone was detected in all three soil samples; however, concentrations did
not exceed the Industrial PSRGs. Acetone is a common laboratory-introduced contaminant. No
other VOCs were detected in the soil samples.

Two of the three soil sample locations (BFSS-1 and BFSS-3) had detectable concentrations of
certain SVOCs. No SVOC concentrations exceeded the Industrial PSRGs. The SVOCs detected
were 2-methylnaphthalene, benzo(a)anthracene, benzo(a)pyrene benzo(b)fluoranthene,
benzo(g,h,i)perylene, benzo(k)fluoranthene, chrysene, fluoranthene, indeno(1,2,3-cd)pyrene,
naphthalene, phenanthrene, and pyrene.

Arsenic, barium, cadmium, chromium, lead, mercury, selenium, and silver concentrations were
detected in all three soil samples. Most of the metals detected appeared to be naturally occurring.
However, the arsenic concentration in BFSS-1 of 13 mg/kg was detected at a concentration
greater than 2x background and also above the Industrial PSRG of 3.0 mg/kg.

Based on the elevated arsenic concentration in BFSS-1, H&H further evaluated the detection
using the NC DEQ risk assessment calculator dated February 2018. The risk-calculator indicated
that the arsenic and other detected compounds in BFSS-1 could cause a risk to non-residential
workers of 4.3 * 10-6 for carcinogenic effects and produce a hazard quotient of 0.029. The risk
calculator indicates that these calculated risks are acceptable in comparison to the thresholds of
10-4 for carcinogenic effects and 1 for the hazard quotient. The location of BFSS-1 is in a
controlled area along the rail corridor that is not accessible to the public. The risk calculation
results are provided in Appendix C.

Table 1 (Page 1 of 1)
Summary of Soil Analytical Data
Norfolk Southern Intermodal Facility
Charlotte, North Carolina
H&H Job No. CAT-105
S:\AAA-Master Projects\Charlotte Area Transit System (CAT)\CAT-105 NSIF BF Closeout\Data Tables - Final.xlsx
3/29/2018
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Sample ID BFSS-1 BFSS-2 BFSS-3
Depth (ft bgs)0-1 0-1 0-1
Sample Date
Protection of
Groundwater
PSRGs1
Residential
PSRGs1
Industrial
PSRGs2
Background
Metals Range3
Background
Metals
Mean3 1/16/2018 1/16/2018 1/16/2018
Units (mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)(mg/kg)
VOCs (8260B)
Acetone 25 12,000 140,000 ----0.022 J 0.089 0.032
SVOCs (8270C)
2-Methylnaphthalene 3.1 48.0 600 ----0.15 J <0.068 <0.066
Benzo(a)anthracene 0.35 1.1 21 ----<0.051 <0.055 0.16 J
Benzo(a)pyrene 0.12 0.11 2.1 ----<0.042 <0.046 0.24 J
Benzo(b)fluoranthene 1.2 0.42 21 ----0.14 J <0.049 0.41 J
Benzo(g,h,i)perylene 15,600 NE NE ----<0.043 <0.046 0.13 J
Benzo(k)fluoranthene 12 11 210 ----<0.051 <0.056 0.15 J
Chrysene 36 110 2,100 ----<0.049 <0.053 0.23 J
Fluoranthene 670 480 6,000 ----0.14 J <0.054 0.19 J
Indeno(1,2,3-cd)pyrene 3.9 1.1 21 ----<0.045 <0.049 0.15 J
Naphthalene 0.39 4.10 18 ----0.13 J <0.068 <0.067
Phenanthrene 134 NR NE ----0.15 J <0.055 <0.054
Pyrene 440 360 4,500 ----0.13 J <0.056 0.21 J
RCRA Metals (6020A/7471A)4
Arsenic 5.8 0.68 3.0 1.0-18 4.8 13 2.2 1.5 J
Barium 580 3,100 47,000 50-1000 356 130 150 110
Cadmium 3 14 200 1.0-10 4.3 0.11 J 0.081 J 0.046 J
Chromium 360,000 23,000 350,000 7-300 65 82 110 39
Lead NE 400 800 ND-50 16 13 13 6.4
Mercury 1.0 2.3 9.7 0.03-0.52 0.121 0.037 0.015 J 0.0023 J
Selenium 2.1 78 1,200 <1.0-0.8 0.42 2.0 2.4 1.2 J
Silver 3.4 78 1,200 ND-5.0 NE 0.047 J 0.065 J 0.046 J
Notes:
1) NC Department of Environmental Quality Inactive Hazardous Sites Branch (IHSB) Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs) - February 20182) DEQ IHSB Preliminary Industrial Soil Remediation Goal - February 2018
3) Background concentrations for metals • Elements in North American Soils, 2nd Edition, James Dragun and Chekiri Khaled, 20054) Mercury analyzed by EPA Method 7471AOnly those compounds detected in at least one sample shown aboveBold indicates an exceedance of the industrial PSRG or DEQ UST Action Level; however, risk calculator indicates acceptable risk
Underlined indicates an excedance of the Protection of Groundwater PSRGGrey shading indicates metal concentration exceeds 2x the Background Metals MeanVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; mg/kg = milligrams per kilogramNE = Not Established; -- = Not applicable; J = laboratory estimated value
Screening Criteria
TITLE
PROJECT
SITE LOCATION MAP
NORFOLK SOUTHERN INTERMODAL FACILITY
BROWNFIELDS PROJECT NO. 15019-11-60CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
01/29/2018 0
1CAT-105
0 2000 4000N
APPROXIMATE
SCALE IN FEET
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
Charlotte East, 2013
SITE
BFSS-2
BFSS-3
BFSS-1
BFSS-1
BFSS-2
BFSS-3
BFSS-1
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
HISTORICAL ON-SITE FACILITIES
DRAINAGE DITCH
POLE-MOUNTED TRANSFORMER
RAILROAD TRACK
STREAM
(SUGAR CREEK AND TRIBUTARIES)
FENCE LINE
AREA MANAGED AS IMPACTED SOIL
CONTAMINATED SOIL REUSED AS
BACKFILL & CAPPED WITH CLEAN SOIL
DPT LOCATIONS
POST-CONFIRMATION SOIL SAMPLE
LOCATION
JOB NO. CAT-105
REVISION NO. 0DATE: 2-23-18
FIGURE NO. 2
NORFOLK SOUTHERN INTERMODAL FACILITY
BROWNFIELDS PROJECT NO. 15019-11-60
CHARLOTTE, NORTH CAROLINA
SITE & SAMPLE LOCATION MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.AREAS NOT SHOWN AS IMPACTED WERE FIELD SCREENED
FOR EVIDENCE OF ENVIRONMENTAL IMPACTS DURING SITE
WORK.
2.POST CONSTRUCTION SOIL SAMPLES COLLECTED 1/9/18.
CONSOLIDATED PIPE
& SUPPLY CO.
N. B
R
E
V
A
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D
S
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RAIL CAR STORAGE YARD
FORMER GUARD HOUSE/OFFICE
FORMER PROPANE AST
FORMER OFFICE TRAILER
FORMER CONCRETE TRACTOR
TRAILER STORAGE AREA
WATER QUALITY AREA
MAINTENANCE BUILDING
ENRANCE
OPERATIONS FACILITY & PARKING
FORMER VEGETABLE OIL REFINERY
FORMER TINSMITH SHOP
FORMER MURRAY CONSTRUCTION
FORMER VEGETABLE OIL REFINERY
WASTEWATER BASIN
FORMER J. KING HARRISON CO.
FORMER HARPER CRAWFORD BAGGING
COMPANY & COTTON WAREHOUSE (1920s-1950s)
FORMER COTTON
WAREHOUSES
FORMER STORAGE TRAILERS
HIGHLAND MILLS, INC.
PARKING LOT
FORMER TRAILCO TRAILER REPAIR
FORMER H&M
TRUCK REPAIR
FORMER TSI
CRANE REPAIR
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TMW-7
TMW-5
DPT-2/
TMW-1
TMW-4
TMW-11
TMW-9
TMW-3
TMW-2
TMW-10
DPT-35
DPT-40
DPT-44
TMW-12
TMW-13
BFSS-1
BFSS-1
BFSS-2
BFSS-3
BFSS-1
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
HISTORICAL ON-SITE FACILITIES
DRAINAGE DITCH
POLE-MOUNTED TRANSFORMER
RAILROAD TRACK
STREAM
(SUGAR CREEK AND TRIBUTARIES)
FENCE LINE
AREA MANAGED AS IMPACTED SOIL
CONTAMINATED SOIL REUSED AS
BACKFILL & CAPPED WITH CLEAN SOIL
DPT LOCATIONS
TEMPORARY MONITORING WELL
LOCATION >NC 2L STANDARDS
SOIL SAMPLE LOCATION >NC DEQ IHSB
INDUSTRIAL SOIL REMEDIATION GOALS
GROUNDWATER IMPACTS >NC 2L
STANDARDS
SOIL & GROUNDWATER IMPACTS >NCDEQ
IHSB INDUSTRIAL SOIL REMEDIATION
GOALS & NC 2L STANDARDS
JOB NO. CAT-105
REVISION NO. 0DATE: 3-7-18
FIGURE NO. 3
NORFOLK SOUTHERN INTERMODAL FACILITY
BROWNFIELDS PROJECT NO. 15019-11-60
CHARLOTTE, NORTH CAROLINA
POST-CONSTRUCTION SOIL
AND GROUNDWATER IMPACTS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
TMW-7
NOTES:
1.PER THE ENVIRONMENTAL MANAGEMENT PLAN, AREAS NOT SHOWN AS IMPACTED WERE FIELD SCREENED FOR
EVIDENCE OF ENVIRONMENTAL IMPACTS DURING SITE WORK.
2.ONLY DPT & TMW SAMPLE LOCATIONS EXCEEDING THE NC 2L GROUNDWATER STANDARDS OR NC DEQ IHSB
INDUSTRIAL SOIL REMEDIATION GOALS (SRGs) DATED FEBRUARY 2018 ARE SHOWN.
3.PRELIMINARY SRGs DISPLAYED FOR NON-CARCINOGENS ARE FOR A HAZARD QUOTIENT EQUAL TO 0.2.
SCREENING LEVELS DISPLAYED FOR CARCINOGENS ARE FOR A 1.0E-06 LIFETIME INCREMENTAL CANCER RISK.
DEQ FEBRUARY 2018 RISK CALCULATOR INDICATES ACCEPTABLE RISK FOR BFSS-1 ARSENIC RESULTS.
4.PARCELS ASSOCIATED WITH NSIF BROWNFIELD ARE: PIN #08301142, PIN #08301141, PIN #08301151, PIN #08301146,
PIN #08301148, PIN #08301147, PIN #08301144, PIN #08301149.
5.THE AREAS & TYPES OF CONTAMINATION DEPICTED HEREON ARE APPROXIMATIONS DERIVED FROM THE BEST
AVAILABLE INFORMATION AT THE TIME OF FILING.
6.FOR LAND USE RESTRICTIONS, REFER TO SURVEY PLAT DATED 09/23/14.
7.FOR MORE INFORMATION REGARDING BROWNFIELDS PROJECT NO. 15019-11-60, REFER TO FILES LOCATED AT
MECKLENBURG COUNTY REGISTER OF DEEDS.
GROUNDWATER IMPACT LOCATIONS
GROUNDWATER
CONTAMINANT
SAMPLE
LOCATION
DATE OF
SAMPLING CONCENTRATION EXCEEDING STANDARD (μg/L)2L STANDARD
(μg/L)
CHROMIUM TMW-7 8/15/14 11 10
MANGANESE TMW-1 8/13/14 280 50
MANGANESE TMW-2 8/13/14 1,000 50
MANGANESE TMW-3 8/13/14 450 50
MANGANESE TMW-4 8/14/14 70 50
MANGANESE TMW-7 8/15/14 290 50
MANGANESE TMW-9 8/15/14 650 50
MANGANESE TMW-10 8/18/14 1,200 50
MANGANESE TMW-11 8/18/14 540 50
MANGANESE TMW-12 10/2/14 85 50
TETRACHLOROETHENE TMW-4 8/14/14 0.86 0.7
TETRACHLOROETHENE TMW-5 8/15/14 0.71 0.7
TETRACHLOROETHENE TMW-9 8/15/14 67 0.7
TETRACHLOROETHENE TMW-11 8/18/14 0.73 0.7
TETRACHLOROETHENE TMW-12 10/2/14 3.0 0.7
TETRACHLOROETHENE TMW-13 10/3/14 9.0 0.7
TRICHLOROETHENE TMW-3 8/13/14 6.6 3
TRICHLOROETHENE TMW-4 8/14/14 8.1 3
TRICHLOROETHENE TMW-13 10/3/14 3.9 3
SITE
DUNL
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FORMER TSI
CRANE REPAIR
FORMER H&M
TRUCK REPAIR
FORMER TRAILCO TRAILER REPAIR
HIGHLAND MILLS, INC.
PARKING LOT
FORMER STORAGE TRAILERS
FORMER COTTON
WAREHOUSES
FORMER HARPER CRAWFORD BAGGING
COMPANY & COTTON WAREHOUSE (1920s-1950s)
FORMER J. KING HARRISON CO.
FORMER VEGETABLE OIL REFINERY
WASTEWATER BASIN
FORMER MURRAY CONSTRUCTION
FORMER TINSMITH SHOP
FORMER VEGETABLE OIL REFINERY
OPERATIONS FACILITY & PARKING
ENRANCE
MAINTENANCE BUILDING
FORMER CONCRETE TRACTOR
TRAILER STORAGE AREA
FORMER OFFICE TRAILER
FORMER PROPANE AST
FORMER GUARD HOUSE/OFFICE
RAIL CAR STORAGE YARD
N. B
R
E
V
A
R
D
S
T
R
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T
CONSOLIDATED PIPE
& SUPPLY CO.
WATER QUALITY AREA
PARKWOOD STATION
25TH STREET STATION
DPT-2/
TMW-1
SOIL IMPACT LOCATIONS
SOIL CONTAMINANT SAMPLE
LOCATION DEPTH (FT)DATE OF
SAMPLING
CONCENTRATION
EXCEEDING SCREENING
LEVEL (mg/kg)
INDUSTRIAL SCREENING
LEVEL3 (mg/kg)
ARSENIC DPT-2 4-6 8/12/14 15 3.0
ARSENIC DPT-35 8-10 9/30/14 9.2 3.0
ARSENIC DPT-40 4-6 10/2/14 6.0 3.0
ARSENIC DPT-44 8-10 10/2/14 5.5 3.0
ARSENIC BFSS-1 0-1 1/9/18 13 3.0
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APPENDIX A
SOIL BORING LOGS

NOTES: Hole precleared on 1/9/18 using hand auger.
generated using LogitEasy.com
Client:
Project:
Address:
Charlotte Area Transit Systems
CAT-105
N Brevard Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BFSS-1
1 of 1
Drilling Start Date: 01-09-2018
Drilling End Date: 01-09-2018
Drilling Company:
Drilling Method: Hand Auger
Drilling Equipment:
Driller:
Logged By:Kenneth Windsand
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR (0') ORGANIC SOIL (OL)
(0.25') Sandy SILT (ML); trace clay, stiff, dry, tan brown, with rock fragments
(1.25') Sandy SILT (ML); trace clay, stiff, dry, tan brown, mixed with black sandy silt
(2') Boring terminated
2.8
6.8
BFSS-1(0'-1')
0
1
2
3
4
5
NOTES: Hole precleared on 1/09/2018 using hand auger.
generated using LogitEasy.com
Client:
Project:
Address:
Charlotte Area Transit Systems
CAT-105
N Brevard Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BFSS-2
1 of 1
Drilling Start Date: 01-09-2018
Drilling End Date: 01-09-2018
Drilling Company:
Drilling Method: Hand Auger
Drilling Equipment:
Driller:
Logged By:Kenneth Windsand
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 12:32 (0') Lean CLAY (CL); trace fine-medium sand, some silt, mostly clay, medium plasticity,
medium stiff, moist, brown gray, with rock fragments
(1.25') Silty GRAVEL (GM); mostly fine-coarse grained gravel, few fine-medium sand,
little silt, poorly graded, medium dense, moist, gray
(2') Boring terminated
2.5
6.2
BFSS-2(0'-1')
0
1
2
3
4
5
NOTES: Hole precleared on 01/09/2018 using hand auger.
generated using LogitEasy.com
Client:
Project:
Address:
Charlotte Area Transit Systems
CAT-105
N Brevard Street, Charlotte, NC
BORING LOG
Boring No.
Page:
BFSS-3
1 of 1
Drilling Start Date: 01-09-2018
Drilling End Date: 01-09-2018
Drilling Company:
Drilling Method: Hand Auger
Drilling Equipment:
Driller:
Logged By:Kenneth Windsand
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR 12:43 (0') SILT (ML); trace fine-medium sand, mostly silt, some clay, soft, moist, red orange
(0.5') Sandy SILT (ML); trace clay, medium stiff, moist, tan brown
(1.25') Lean CLAY (CL); some silt, mostly clay, medium plasticity, medium stiff, moist,
red brown, with gray black fine to medium sands
(2') Boring terminated
0.2
0.8
BFSS-3(0'-1')
0
1
2
3
4
5

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APPENDIX B
ANALYTICAL LABORATORY REPORT

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
01/16/2018
Hart & Hickman (Charlotte)
Ken Windsand
2923 South Tryon St. Ste 100
Charlotte, NC 28203
Project: CAT-105 NSIF Brownfields Sampling
Lab Submittal Date: 01/09/2018
Prism Work Order: 8010088
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Not Detected at the MDLU
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 36
Sample Receipt Summary
01/16/2018
Prism Work Order: 8010088
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
8010088-01 01/09/18BFSS-1 (0-1)01/09/18Solid
8010088-02 01/09/18BFSS-2 (0-1)01/09/18Solid
8010088-03 01/09/18BFSS-3 (0-1)01/09/18Solid
Samples were received in good condition at 2.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 36
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8010088
01/16/2018
Summary of Detections
0.15 J mg/kg dry8010088-01 BFSS-1 (0-1)2-Methylnaphthalene 8270D
0.14 J mg/kg dry8010088-01 BFSS-1 (0-1)Benzo(b)fluoranthene 8270D
0.14 J mg/kg dry8010088-01 BFSS-1 (0-1)Fluoranthene 8270D
0.13 J mg/kg dry8010088-01 BFSS-1 (0-1)Naphthalene 8270D
0.15 J mg/kg dry8010088-01 BFSS-1 (0-1)Phenanthrene 8270D
0.13 J mg/kg dry8010088-01 BFSS-1 (0-1)Pyrene 8270D
0.037 mg/kg dry8010088-01 BFSS-1 (0-1)Mercury 7471B
13 mg/kg dry8010088-01 BFSS-1 (0-1)Arsenic 6020B
130 mg/kg dry8010088-01 BFSS-1 (0-1)Barium 6020B
0.11 J mg/kg dry8010088-01 BFSS-1 (0-1)Cadmium 6020B
82 mg/kg dry8010088-01 BFSS-1 (0-1)Chromium 6020B
13 mg/kg dry8010088-01 BFSS-1 (0-1)Lead 6020B
2.0 mg/kg dry8010088-01 BFSS-1 (0-1)Selenium 6020B
0.047 LH, J mg/kg dry8010088-01 BFSS-1 (0-1)Silver 6020B
0.022 J mg/kg dry8010088-01 BFSS-1 (0-1)Acetone 8260B
0.015 J mg/kg dry8010088-02 BFSS-2 (0-1)Mercury 7471B
2.2 mg/kg dry8010088-02 BFSS-2 (0-1)Arsenic 6020B
150 mg/kg dry8010088-02 BFSS-2 (0-1)Barium 6020B
0.081 J mg/kg dry8010088-02 BFSS-2 (0-1)Cadmium 6020B
110 mg/kg dry8010088-02 BFSS-2 (0-1)Chromium 6020B
13 mg/kg dry8010088-02 BFSS-2 (0-1)Lead 6020B
2.4 mg/kg dry8010088-02 BFSS-2 (0-1)Selenium 6020B
0.065 LH, J mg/kg dry8010088-02 BFSS-2 (0-1)Silver 6020B
0.089 mg/kg dry8010088-02 BFSS-2 (0-1)Acetone 8260B
0.16 J mg/kg dry8010088-03 BFSS-3 (0-1)Benzo(a)anthracene 8270D
0.24 J mg/kg dry8010088-03 BFSS-3 (0-1)Benzo(a)pyrene 8270D
0.41 J mg/kg dry8010088-03 BFSS-3 (0-1)Benzo(b)fluoranthene 8270D
0.13 J mg/kg dry8010088-03 BFSS-3 (0-1)Benzo(g,h,i)perylene 8270D
0.15 J mg/kg dry8010088-03 BFSS-3 (0-1)Benzo(k)fluoranthene 8270D
0.23 J mg/kg dry8010088-03 BFSS-3 (0-1)Chrysene 8270D
0.19 J mg/kg dry8010088-03 BFSS-3 (0-1)Fluoranthene 8270D
0.15 J mg/kg dry8010088-03 BFSS-3 (0-1)Indeno(1,2,3-cd)pyrene 8270D
0.21 J mg/kg dry8010088-03 BFSS-3 (0-1)Pyrene 8270D
0.0023 J mg/kg dry8010088-03 BFSS-3 (0-1)Mercury 7471B
1.5 J mg/kg dry8010088-03 BFSS-3 (0-1)Arsenic 6020B
110 mg/kg dry8010088-03 BFSS-3 (0-1)Barium 6020B
0.046 J mg/kg dry8010088-03 BFSS-3 (0-1)Cadmium 6020B
39 mg/kg dry8010088-03 BFSS-3 (0-1)Chromium 6020B
6.4 mg/kg dry8010088-03 BFSS-3 (0-1)Lead 6020B
1.2 J mg/kg dry8010088-03 BFSS-3 (0-1)Selenium 6020B
0.046 LH, J mg/kg dry8010088-03 BFSS-3 (0-1)Silver 6020B
0.032 mg/kg dry8010088-03 BFSS-3 (0-1)Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 36
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-01
Prism Work Order: 8010088
Time Collected: 01/09/18 10:15
Time Submitted: 01/09/18 13:35
BFSS-1 (0-1)
General Chemistry Parameters
*SM2540 G P8A013210.100 1/10/18 15:45 TJY% by
Weight
0.100% Solids 84.2
Semivolatile Organic Compounds by GC/MS
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0321,1’-Biphenyl 0.032 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0612,3,4,6-Tetrachlorophenol 0.061 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0742,4,5-Trichlorophenol 0.074 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0732,4,6-Trichlorophenol 0.073 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0762,4-Dichlorophenol 0.076 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0602,4-Dimethylphenol 0.060 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0552,4-Dinitrophenol 0.055 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0482,4-Dinitrotoluene 0.048 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0522,6-Dinitrotoluene 0.052 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0572-Chloronaphthalene 0.057 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0562-Chlorophenol 0.056 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0632-Methylnaphthalene 0.15 J
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0502-Methylphenol 0.050 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0712-Nitroaniline 0.071 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0712-Nitrophenol 0.071 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0773,3’-Dichlorobenzidine 0.077 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0483/4-Methylphenol 0.048 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0673-Nitroaniline 0.067 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol 0.059 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0674-Bromophenyl phenyl ether 0.067 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0554-Chloro-3-methylphenol 0.055 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0474-Chloroaniline 0.047 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether 0.051 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0714-Nitroaniline 0.071 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.0604-Nitrophenol 0.060 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.053Acenaphthene0.053 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.057Acenaphthylene0.057 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.065Acetophenone0.065 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.063Anthracene0.063 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.061Atrazine0.061 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.034Benzaldehyde0.034 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.051Benzo(a)anthracene 0.051 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.042Benzo(a)pyrene 0.042 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.045Benzo(b)fluoranthene 0.14 J
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.043Benzo(g,h,i)perylene 0.043 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.051Benzo(k)fluoranthene 0.051 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.068bis(2-Chloroethoxy)methane 0.068 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.055Bis(2-Chloroethyl)ether 0.055 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.067Bis(2-chloroisopropyl)ether 0.067 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-01
Prism Work Order: 8010088
Time Collected: 01/09/18 10:15
Time Submitted: 01/09/18 13:35
BFSS-1 (0-1)
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate 0.058 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.056Butyl benzyl phthalate 0.056 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.059Caprolactam0.059 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.060Carbazole0.060 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.049Chrysene0.049 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene 0.048 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.060Dibenzofuran0.060 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.054Diethyl phthalate 0.054 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.052Dimethyl phthalate 0.052 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.056Di-n-butyl phthalate 0.056 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.048Di-n-octyl phthalate 0.048 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.050Fluoranthene0.14 J
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.056Fluorene0.056 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.062Hexachlorobenzene0.062 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.070Hexachlorobutadiene0.070 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.070Hexachlorocyclopentadiene0.070 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.066Hexachloroethane0.066 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene 0.045 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.053Isophorone0.053 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.063Naphthalene0.13 J
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.056Nitrobenzene0.056 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine 0.062 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.060N-Nitrosodiphenylamine 0.060 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.046Pentachlorophenol0.046 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.051Phenanthrene0.15 J
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.058Phenol0.058 U
8270D P8A014710.39 1/13/18 3:59 JMVmg/kg dry 0.052Pyrene0.13 J
Surrogate Recovery Control Limits
37-13167 %2,4,6-Tribromophenol
47-13068 %2-Fluorobiphenyl
44-11761 %2-Fluorophenol
45-12159 %Nitrobenzene-d5
37-12762 %Phenol-d5
38-13569 %Terphenyl-d14
Total Metals
7471B P8A013310.022 1/11/18 14:03 JABmg/kg dry 0.0021Mercury0.037
6020B P8A0126101.8 1/12/18 16:11 EGCmg/kg dry 0.16Arsenic13
6020B P8A012610121/12/18 16:11 EGCmg/kg dry 0.073Barium130
6020B P8A0126100.30 1/12/18 16:11 EGCmg/kg dry 0.023Cadmium0.11 J
6020B P8A0126100.60 1/12/18 16:11 EGCmg/kg dry 0.034Chromium82
6020B P8A0126100.30 1/12/18 16:11 EGCmg/kg dry 0.068Lead13
6020B P8A0126101.2 1/12/18 16:11 EGCmg/kg dry 0.25Selenium2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-01
Prism Work Order: 8010088
Time Collected: 01/09/18 10:15
Time Submitted: 01/09/18 13:35
BFSS-1 (0-1)
6020B P8A0126100.30 1/12/18 16:11 EGCmg/kg dry 0.023Silver0.047 LH, J
Volatile Organic Compounds by GC/MS
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000271,1,1-Trichloroethane 0.00027 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000381,1,2,2-Tetrachloroethane 0.00038 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.000421,1,2-Trichloro-1,2,2-trifluoroethane 0.00042 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000501,1,2-Trichloroethane 0.00050 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000161,1-Dichloroethane 0.00016 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000251,1-Dichloroethylene 0.00025 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene 0.00032 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.000421,2,4-Trichlorobenzene 0.00042 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000421,2-Dibromo-3-chloropropane 0.00042 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000231,2-Dibromoethane 0.00023 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.000261,2-Dichlorobenzene 0.00026 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000341,2-Dichloroethane 0.00034 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.000351,2-Dichloropropane 0.00035 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.000371,3-Dichlorobenzene 0.00037 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.000221,4-Dichlorobenzene 0.00022 U
8260B P8A018810.11 1/15/18 15:22 ANGmg/kg dry 0.0111,4-Dioxane 0.011 U
8260B P8A018810.023 1/15/18 15:22 ANGmg/kg dry 0.0014Acetone0.022 J
8260B P8A018810.0034 1/15/18 15:22 ANGmg/kg dry 0.00033Benzene0.00033 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00031Bromochloromethane0.00031 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00031Bromodichloromethane0.00031 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00064Bromoform0.00064 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00069Bromomethane0.00069 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00028Carbon disulfide 0.00028 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00028Carbon Tetrachloride 0.00028 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00030Chlorobenzene0.00030 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00047Chloroethane0.00047 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00041Chloroform0.00041 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00038Chloromethane0.00038 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene 0.00024 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene 0.00019 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00037Cyclohexane0.00037 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00023Dibromochloromethane0.00023 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00026Dichlorodifluoromethane0.00026 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00022Ethylbenzene0.00022 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00033Isopropylbenzene (Cumene)0.00033 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00052m,p-Xylenes 0.00052 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00085Methyl Acetate 0.00085 U
8260B P8A018810.056 1/15/18 15:22 ANGmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)0.00051 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00048Methylcyclohexane0.00048 U
8260B P8A018810.023 1/15/18 15:22 ANGmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)0.00051 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00048Methyl Isobutyl Ketone 0.00048 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-01
Prism Work Order: 8010088
Time Collected: 01/09/18 10:15
Time Submitted: 01/09/18 13:35
BFSS-1 (0-1)
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00032Methylene Chloride 0.00032 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether 0.00018 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00023o-Xylene 0.00023 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00034Styrene0.00034 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00027Tetrachloroethylene0.00027 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00032Toluene0.00032 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene 0.00034 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene 0.00030 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00036Trichloroethylene0.00036 U
8260B P8A018810.0056 1/15/18 15:22 ANGmg/kg dry 0.00036Trichlorofluoromethane0.00036 U
8260B P8A018810.011 1/15/18 15:22 ANGmg/kg dry 0.00027Vinyl chloride 0.00027 U
8260B P8A018810.017 1/15/18 15:22 ANGmg/kg dry 0.0011Xylenes, total 0.0011 U
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12986 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-02
Prism Work Order: 8010088
Time Collected: 01/09/18 11:00
Time Submitted: 01/09/18 13:35
BFSS-2 (0-1)
General Chemistry Parameters
*SM2540 G P8A013210.100 1/10/18 15:45 TJY% by
Weight
0.100% Solids 77.9
Semivolatile Organic Compounds by GC/MS
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0351,1’-Biphenyl 0.035 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0662,3,4,6-Tetrachlorophenol 0.066 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0802,4,5-Trichlorophenol 0.080 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0792,4,6-Trichlorophenol 0.079 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0822,4-Dichlorophenol 0.082 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0652,4-Dimethylphenol 0.065 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0592,4-Dinitrophenol 0.059 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0512,4-Dinitrotoluene 0.051 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0562,6-Dinitrotoluene 0.056 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0612-Chloronaphthalene 0.061 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0602-Chlorophenol 0.060 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0682-Methylnaphthalene 0.068 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0542-Methylphenol 0.054 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0772-Nitroaniline 0.077 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0772-Nitrophenol 0.077 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0843,3’-Dichlorobenzidine 0.084 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0523/4-Methylphenol 0.052 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0733-Nitroaniline 0.073 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0644,6-Dinitro-2-methylphenol 0.064 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0734-Bromophenyl phenyl ether 0.073 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0594-Chloro-3-methylphenol 0.059 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0514-Chloroaniline 0.051 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether 0.055 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0774-Nitroaniline 0.077 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.0654-Nitrophenol 0.065 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.058Acenaphthene0.058 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.061Acenaphthylene0.061 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.071Acetophenone0.071 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.068Anthracene0.068 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.066Atrazine0.066 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.037Benzaldehyde0.037 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.055Benzo(a)anthracene 0.055 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.046Benzo(a)pyrene 0.046 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.049Benzo(b)fluoranthene 0.049 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.046Benzo(g,h,i)perylene 0.046 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.056Benzo(k)fluoranthene 0.056 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.074bis(2-Chloroethoxy)methane 0.074 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether 0.060 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether 0.072 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-02
Prism Work Order: 8010088
Time Collected: 01/09/18 11:00
Time Submitted: 01/09/18 13:35
BFSS-2 (0-1)
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate 0.063 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.060Butyl benzyl phthalate 0.060 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.064Caprolactam0.064 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.065Carbazole0.065 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.053Chrysene0.053 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene 0.052 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.064Dibenzofuran0.064 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.058Diethyl phthalate 0.058 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.056Dimethyl phthalate 0.056 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.060Di-n-butyl phthalate 0.060 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.052Di-n-octyl phthalate 0.052 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.054Fluoranthene0.054 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.061Fluorene0.061 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.067Hexachlorobenzene0.067 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.076Hexachlorobutadiene0.076 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.076Hexachlorocyclopentadiene0.076 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.071Hexachloroethane0.071 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene 0.049 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.057Isophorone0.057 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.068Naphthalene0.068 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.060Nitrobenzene0.060 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.067N-Nitroso-di-n-propylamine 0.067 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.064N-Nitrosodiphenylamine 0.064 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.050Pentachlorophenol0.050 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.055Phenanthrene0.055 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.062Phenol0.062 U
8270D P8A014710.42 1/13/18 4:43 JMVmg/kg dry 0.056Pyrene0.056 U
Surrogate Recovery Control Limits
37-13169 %2,4,6-Tribromophenol
47-13067 %2-Fluorobiphenyl
44-11762 %2-Fluorophenol
45-12162 %Nitrobenzene-d5
37-12762 %Phenol-d5
38-13567 %Terphenyl-d14
Total Metals
7471B P8A013310.024 1/11/18 14:16 JABmg/kg dry 0.0023Mercury0.015 J
6020B P8A0126102.0 1/12/18 16:34 EGCmg/kg dry 0.18Arsenic2.2
6020B P8A012610131/12/18 16:34 EGCmg/kg dry 0.080Barium150
6020B P8A0126100.33 1/12/18 16:34 EGCmg/kg dry 0.025Cadmium0.081 J
6020B P8A0126100.66 1/12/18 16:34 EGCmg/kg dry 0.037Chromium110
6020B P8A0126100.33 1/12/18 16:34 EGCmg/kg dry 0.075Lead13
6020B P8A0126101.3 1/12/18 16:34 EGCmg/kg dry 0.27Selenium2.4
6020B P8A0126100.33 1/12/18 16:34 EGCmg/kg dry 0.025Silver0.065 LH, J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-02
Prism Work Order: 8010088
Time Collected: 01/09/18 11:00
Time Submitted: 01/09/18 13:35
BFSS-2 (0-1)
Volatile Organic Compounds by GC/MS
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000261,1,1-Trichloroethane 0.00026 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000371,1,2,2-Tetrachloroethane 0.00037 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.000401,1,2-Trichloro-1,2,2-trifluoroethane 0.00040 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000481,1,2-Trichloroethane 0.00048 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000151,1-Dichloroethane 0.00015 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000241,1-Dichloroethylene 0.00024 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.000311,2,3-Trichlorobenzene 0.00031 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.000401,2,4-Trichlorobenzene 0.00040 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000401,2-Dibromo-3-chloropropane 0.00040 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000221,2-Dibromoethane 0.00022 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.000251,2-Dichlorobenzene 0.00025 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000321,2-Dichloroethane 0.00032 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.000341,2-Dichloropropane 0.00034 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.000361,3-Dichlorobenzene 0.00036 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.000211,4-Dichlorobenzene 0.00021 U
8260B P8A018810.11 1/15/18 15:50 ANGmg/kg dry 0.0111,4-Dioxane 0.011 U
8260B P8A018810.022 1/15/18 15:50 ANGmg/kg dry 0.0013Acetone0.089
8260B P8A018810.0032 1/15/18 15:50 ANGmg/kg dry 0.00031Benzene0.00031 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00030Bromochloromethane0.00030 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00030Bromodichloromethane0.00030 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00061Bromoform0.00061 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00067Bromomethane0.00067 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00027Carbon disulfide 0.00027 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00027Carbon Tetrachloride 0.00027 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00029Chlorobenzene0.00029 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00045Chloroethane0.00045 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00039Chloroform0.00039 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00036Chloromethane0.00036 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00023cis-1,2-Dichloroethylene 0.00023 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00018cis-1,3-Dichloropropylene 0.00018 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00035Cyclohexane0.00035 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00022Dibromochloromethane0.00022 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00025Dichlorodifluoromethane0.00025 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00021Ethylbenzene0.00021 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00032Isopropylbenzene (Cumene)0.00032 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00050m,p-Xylenes 0.00050 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00082Methyl Acetate 0.00082 U
8260B P8A018810.054 1/15/18 15:50 ANGmg/kg dry 0.00049Methyl Butyl Ketone (2-Hexanone)0.00049 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00046Methylcyclohexane0.00046 U
8260B P8A018810.022 1/15/18 15:50 ANGmg/kg dry 0.00049Methyl Ethyl Ketone (2-Butanone)0.00049 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00046Methyl Isobutyl Ketone 0.00046 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00030Methylene Chloride 0.00030 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-02
Prism Work Order: 8010088
Time Collected: 01/09/18 11:00
Time Submitted: 01/09/18 13:35
BFSS-2 (0-1)
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00017Methyl-tert-Butyl Ether 0.00017 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00022o-Xylene 0.00022 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00033Styrene0.00033 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00026Tetrachloroethylene0.00026 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00031Toluene0.00031 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00032trans-1,2-Dichloroethylene 0.00032 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00028trans-1,3-Dichloropropylene 0.00028 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00035Trichloroethylene0.00035 U
8260B P8A018810.0054 1/15/18 15:50 ANGmg/kg dry 0.00035Trichlorofluoromethane0.00035 U
8260B P8A018810.011 1/15/18 15:50 ANGmg/kg dry 0.00026Vinyl chloride 0.00026 U
8260B P8A018810.016 1/15/18 15:50 ANGmg/kg dry 0.0010Xylenes, total 0.0010 U
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12986 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-03
Prism Work Order: 8010088
Time Collected: 01/09/18 11:45
Time Submitted: 01/09/18 13:35
BFSS-3 (0-1)
General Chemistry Parameters
*SM2540 G P8A013210.100 1/10/18 15:45 TJY% by
Weight
0.100% Solids 79.5
Semivolatile Organic Compounds by GC/MS
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0341,1’-Biphenyl 0.034 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0642,3,4,6-Tetrachlorophenol 0.064 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0782,4,5-Trichlorophenol 0.078 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0782,4,6-Trichlorophenol 0.078 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0802,4-Dichlorophenol 0.080 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0642,4-Dimethylphenol 0.064 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0582,4-Dinitrophenol 0.058 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0502,4-Dinitrotoluene 0.050 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0552,6-Dinitrotoluene 0.055 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0602-Chloronaphthalene 0.060 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0592-Chlorophenol 0.059 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0662-Methylnaphthalene 0.066 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0532-Methylphenol 0.053 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0752-Nitroaniline 0.075 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0762-Nitrophenol 0.076 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0823,3’-Dichlorobenzidine 0.082 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0513/4-Methylphenol 0.051 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0713-Nitroaniline 0.071 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol 0.062 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0714-Bromophenyl phenyl ether 0.071 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0584-Chloro-3-methylphenol 0.058 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0504-Chloroaniline 0.050 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether 0.054 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0764-Nitroaniline 0.076 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.0644-Nitrophenol 0.064 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.056Acenaphthene0.056 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.060Acenaphthylene0.060 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.069Acetophenone0.069 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.067Anthracene0.067 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.064Atrazine0.064 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.036Benzaldehyde0.036 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.054Benzo(a)anthracene 0.16 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.045Benzo(a)pyrene 0.24 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.048Benzo(b)fluoranthene 0.41 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.046Benzo(g,h,i)perylene 0.13 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.054Benzo(k)fluoranthene 0.15 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.072bis(2-Chloroethoxy)methane 0.072 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.059Bis(2-Chloroethyl)ether 0.059 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.071Bis(2-chloroisopropyl)ether 0.071 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-03
Prism Work Order: 8010088
Time Collected: 01/09/18 11:45
Time Submitted: 01/09/18 13:35
BFSS-3 (0-1)
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.062Bis(2-Ethylhexyl)phthalate 0.062 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.059Butyl benzyl phthalate 0.059 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.063Caprolactam0.063 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.064Carbazole0.064 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.052Chrysene0.23 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene 0.051 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.063Dibenzofuran0.063 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.057Diethyl phthalate 0.057 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.055Dimethyl phthalate 0.055 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.059Di-n-butyl phthalate 0.059 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.051Di-n-octyl phthalate 0.051 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.053Fluoranthene0.19 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.060Fluorene0.060 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.066Hexachlorobenzene0.066 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.075Hexachlorobutadiene0.075 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.074Hexachlorocyclopentadiene0.074 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.070Hexachloroethane0.070 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene 0.15 J
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.056Isophorone0.056 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.067Naphthalene0.067 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.059Nitrobenzene0.059 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine 0.065 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.063N-Nitrosodiphenylamine 0.063 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.049Pentachlorophenol0.049 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.054Phenanthrene0.054 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.061Phenol0.061 U
8270D P8A014710.42 1/13/18 4:21 JMVmg/kg dry 0.055Pyrene0.21 J
Surrogate Recovery Control Limits
37-13176 %2,4,6-Tribromophenol
47-13070 %2-Fluorobiphenyl
44-11764 %2-Fluorophenol
45-12160 %Nitrobenzene-d5
37-12765 %Phenol-d5
38-13573 %Terphenyl-d14
Total Metals
7471B P8A013310.024 1/11/18 14:21 JABmg/kg dry 0.0023Mercury0.0023 J
6020B P8A0126101.9 1/12/18 16:42 EGCmg/kg dry 0.17Arsenic1.5 J
6020B P8A012610131/12/18 16:42 EGCmg/kg dry 0.078Barium110
6020B P8A0126100.32 1/12/18 16:42 EGCmg/kg dry 0.024Cadmium0.046 J
6020B P8A0126100.64 1/12/18 16:42 EGCmg/kg dry 0.036Chromium39
6020B P8A0126100.32 1/12/18 16:42 EGCmg/kg dry 0.073Lead6.4
6020B P8A0126101.3 1/12/18 16:42 EGCmg/kg dry 0.26Selenium1.2 J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-03
Prism Work Order: 8010088
Time Collected: 01/09/18 11:45
Time Submitted: 01/09/18 13:35
BFSS-3 (0-1)
6020B P8A0126100.32 1/12/18 16:42 EGCmg/kg dry 0.024Silver0.046 LH, J
Volatile Organic Compounds by GC/MS
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000271,1,1-Trichloroethane 0.00027 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000381,1,2,2-Tetrachloroethane 0.00038 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.000421,1,2-Trichloro-1,2,2-trifluoroethane 0.00042 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000501,1,2-Trichloroethane 0.00050 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000161,1-Dichloroethane 0.00016 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000251,1-Dichloroethylene 0.00025 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene 0.00032 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.000421,2,4-Trichlorobenzene 0.00042 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000421,2-Dibromo-3-chloropropane 0.00042 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000231,2-Dibromoethane 0.00023 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.000271,2-Dichlorobenzene 0.00027 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000341,2-Dichloroethane 0.00034 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.000351,2-Dichloropropane 0.00035 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.000381,3-Dichlorobenzene 0.00038 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.000221,4-Dichlorobenzene 0.00022 U
8260B P8A018810.11 1/15/18 16:17 ANGmg/kg dry 0.0111,4-Dioxane 0.011 U
8260B P8A018810.023 1/15/18 16:17 ANGmg/kg dry 0.0014Acetone0.032
8260B P8A018810.0034 1/15/18 16:17 ANGmg/kg dry 0.00033Benzene0.00033 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00031Bromochloromethane0.00031 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00032Bromodichloromethane0.00032 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00064Bromoform0.00064 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00070Bromomethane0.00070 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00028Carbon disulfide 0.00028 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00028Carbon Tetrachloride 0.00028 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00030Chlorobenzene0.00030 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00047Chloroethane0.00047 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00041Chloroform0.00041 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00038Chloromethane0.00038 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene 0.00024 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene 0.00019 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00037Cyclohexane0.00037 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00023Dibromochloromethane0.00023 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00026Dichlorodifluoromethane0.00026 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00022Ethylbenzene0.00022 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00034Isopropylbenzene (Cumene)0.00034 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00052m,p-Xylenes 0.00052 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00086Methyl Acetate 0.00086 U
8260B P8A018810.057 1/15/18 16:17 ANGmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)0.00051 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00048Methylcyclohexane0.00048 U
8260B P8A018810.023 1/15/18 16:17 ANGmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)0.00051 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00048Methyl Isobutyl Ketone 0.00048 U
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 36
Laboratory Report
01/16/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Sample Matrix: Solid
Client Sample ID:
Prism Sample ID: 8010088-03
Prism Work Order: 8010088
Time Collected: 01/09/18 11:45
Time Submitted: 01/09/18 13:35
BFSS-3 (0-1)
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00032Methylene Chloride 0.00032 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether 0.00018 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00023o-Xylene 0.00023 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00034Styrene0.00034 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00027Tetrachloroethylene0.00027 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00033Toluene0.00033 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene 0.00034 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene 0.00030 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00037Trichloroethylene0.00037 U
8260B P8A018810.0057 1/15/18 16:17 ANGmg/kg dry 0.00037Trichlorofluoromethane0.00037 U
8260B P8A018810.011 1/15/18 16:17 ANGmg/kg dry 0.00027Vinyl chloride 0.00027 U
8260B P8A018810.017 1/15/18 16:17 ANGmg/kg dry 0.0011Xylenes, total 0.0011 U
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12986 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8A0188 - 5035
Blank (P8A0188-BLK1)Prepared & Analyzed: 01/15/18
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wetBRL0.010
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.010
1,2,4-Trichlorobenzene mg/kg wetBRL0.010
1,2-Dibromo-3-chloropropane mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.010
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.010
1,4-Dichlorobenzene mg/kg wetBRL0.010
1,4-Dioxane mg/kg wetBRL0.10
Acetone mg/kg wetBRL0.020
Benzene mg/kg wetBRL0.0030
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon disulfide mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.010
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Cyclohexane mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.010
Ethylbenzene mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.010
m,p-Xylenes mg/kg wetBRL0.010
Methyl Acetate mg/kg wetBRL0.0050
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methylcyclohexane mg/kg wetBRL0.0050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.020
Methyl Isobutyl Ketone mg/kg wetBRL0.010
Methylene Chloride mg/kg wetBRL0.010
Methyl-tert-Butyl Ether mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.010
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8A0188 - 5035
Blank (P8A0188-BLK1)Prepared & Analyzed: 01/15/18
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl chloride mg/kg wetBRL0.010
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9647.9
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10049.8
ug/L 50.00 76-129Surrogate: Toluene-d8 8743.3
LCS (P8A0188-BS1)Prepared & Analyzed: 01/15/18
1,1,1-Trichloroethane mg/kg wet0.0489 0.0050 0.05000 67-13198
1,1,2,2-Tetrachloroethane mg/kg wet0.0436 0.0050 0.05000 56-12687
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0524 0.010 0.05000 70-130105
1,1,2-Trichloroethane mg/kg wet0.0459 0.0050 0.05000 70-13392
1,1-Dichloroethane mg/kg wet0.0489 0.0050 0.05000 74-12798
1,1-Dichloroethylene mg/kg wet0.0446 0.0050 0.05000 67-14989
1,2,3-Trichlorobenzene mg/kg wet0.0398 0.010 0.05000 68-13080
1,2,4-Trichlorobenzene mg/kg wet0.0399 0.010 0.05000 66-12580
1,2-Dibromo-3-chloropropane mg/kg wet0.0453 0.0050 0.05000 55-15791
1,2-Dibromoethane mg/kg wet0.0469 0.0050 0.05000 70-13294
1,2-Dichlorobenzene mg/kg wet0.0422 0.010 0.05000 72-12384
1,2-Dichloroethane mg/kg wet0.0533 0.0050 0.05000 68-128107
1,2-Dichloropropane mg/kg wet0.0520 0.0050 0.05000 73-130104
1,3-Dichlorobenzene mg/kg wet0.0425 0.010 0.05000 71-12085
1,4-Dichlorobenzene mg/kg wet0.0422 0.010 0.05000 71-12384
1,4-Dioxane mg/kg wet0.585 0.10 0.5000 70-130117
Acetone mg/kg wet0.101 0.020 0.1000 29-198101
Benzene mg/kg wet0.0516 0.0030 0.05000 74-127103
Bromochloromethane mg/kg wet0.0524 0.0050 0.05000 72-134105
Bromodichloromethane mg/kg wet0.0538 0.0050 0.05000 75-122108
Bromoform mg/kg wet0.0482 0.0050 0.05000 66-13596
Bromomethane mg/kg wet0.0482 0.010 0.05000 20-18096
Carbon disulfide mg/kg wet0.0515 0.010 0.05000 61-129103
Carbon Tetrachloride mg/kg wet0.0522 0.0050 0.05000 64-143104
Chlorobenzene mg/kg wet0.0473 0.0050 0.05000 74-11895
Chloroethane mg/kg wet0.0429 0.010 0.05000 33-14986
Chloroform mg/kg wet0.0507 0.0050 0.05000 73-127101
Chloromethane mg/kg wet0.0389 0.010 0.05000 45-14378
cis-1,2-Dichloroethylene mg/kg wet0.0518 0.0050 0.05000 76-134104
cis-1,3-Dichloropropylene mg/kg wet0.0546 0.0050 0.05000 71-125109
Cyclohexane mg/kg wet0.0504 0.0050 0.05000 70-130101
Dibromochloromethane mg/kg wet0.0462 0.0050 0.05000 73-12292
Dichlorodifluoromethane mg/kg wet0.0234 0.010 0.05000 26-14647
Ethylbenzene mg/kg wet0.0468 0.0050 0.05000 74-12894
Isopropylbenzene (Cumene)mg/kg wet0.0425 0.010 0.05000 68-12685
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8A0188 - 5035
LCS (P8A0188-BS1)Prepared & Analyzed: 01/15/18
m,p-Xylenes mg/kg wet0.0950 0.010 0.1000 75-12495
Methyl Acetate mg/kg wet0.0518 0.0050 0.05000 70-130104
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0468 0.050 0.05000 J61-15794
Methylcyclohexane mg/kg wet0.0518 0.0050 0.05000 70-130104
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0518 0.020 0.05000 63-149104
Methyl Isobutyl Ketone mg/kg wet0.0555 0.010 0.05000 57-162111
Methylene Chloride mg/kg wet0.0462 0.010 0.05000 74-12992
Methyl-tert-Butyl Ether mg/kg wet0.0497 0.0050 0.05000 70-13099
o-Xylene mg/kg wet0.0471 0.0050 0.05000 74-12694
Styrene mg/kg wet0.0494 0.0050 0.05000 77-12199
Tetrachloroethylene mg/kg wet0.0516 0.010 0.05000 68-130103
Toluene mg/kg wet0.0544 0.0050 0.05000 71-129109
trans-1,2-Dichloroethylene mg/kg wet0.0499 0.0050 0.05000 73-132100
trans-1,3-Dichloropropylene mg/kg wet0.0575 0.0050 0.05000 68-123115
Trichloroethylene mg/kg wet0.0521 0.0050 0.05000 75-133104
Trichlorofluoromethane mg/kg wet0.0622 0.0050 0.05000 44-146124
Vinyl chloride mg/kg wet0.0445 0.010 0.05000 48-14789
Xylenes, total mg/kg wet0.142 0.015 0.1500 74-12695
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9346.6
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 76-129Surrogate: Toluene-d8 8643.0
LCS Dup (P8A0188-BSD1)Prepared & Analyzed: 01/15/18
1,1,1-Trichloroethane mg/kg wet0.0520 0.0050 0.05000 2067-131104 6
1,1,2,2-Tetrachloroethane mg/kg wet0.0433 0.0050 0.05000 2056-12687 0.8
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg wet0.0542 0.010 0.05000 2070-130108 3
1,1,2-Trichloroethane mg/kg wet0.0477 0.0050 0.05000 2070-13395 4
1,1-Dichloroethane mg/kg wet0.0519 0.0050 0.05000 2074-127104 6
1,1-Dichloroethylene mg/kg wet0.0537 0.0050 0.05000 2067-149107 19
1,2,3-Trichlorobenzene mg/kg wet0.0418 0.010 0.05000 2068-13084 5
1,2,4-Trichlorobenzene mg/kg wet0.0414 0.010 0.05000 2066-12583 4
1,2-Dibromo-3-chloropropane mg/kg wet0.0442 0.0050 0.05000 2055-15788 2
1,2-Dibromoethane mg/kg wet0.0469 0.0050 0.05000 2070-13294 0.02
1,2-Dichlorobenzene mg/kg wet0.0439 0.010 0.05000 2072-12388 4
1,2-Dichloroethane mg/kg wet0.0546 0.0050 0.05000 2068-128109 2
1,2-Dichloropropane mg/kg wet0.0546 0.0050 0.05000 2073-130109 5
1,3-Dichlorobenzene mg/kg wet0.0440 0.010 0.05000 2071-12088 4
1,4-Dichlorobenzene mg/kg wet0.0441 0.010 0.05000 2071-12388 4
1,4-Dioxane mg/kg wet0.584 0.10 0.5000 2070-130117 0.2
Acetone mg/kg wet0.0942 0.020 0.1000 2029-19894 7
Benzene mg/kg wet0.0539 0.0030 0.05000 2074-127108 4
Bromochloromethane mg/kg wet0.0547 0.0050 0.05000 2072-134109 4
Bromodichloromethane mg/kg wet0.0562 0.0050 0.05000 2075-122112 4
Bromoform mg/kg wet0.0488 0.0050 0.05000 2066-13598 1
Bromomethane mg/kg wet0.0509 0.010 0.05000 2020-180102 5
Carbon disulfide mg/kg wet0.0534 0.010 0.05000 2061-129107 4
Carbon Tetrachloride mg/kg wet0.0567 0.0050 0.05000 2064-143113 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8A0188 - 5035
LCS Dup (P8A0188-BSD1)Prepared & Analyzed: 01/15/18
Chlorobenzene mg/kg wet0.0496 0.0050 0.05000 2074-11899 5
Chloroethane mg/kg wet0.0459 0.010 0.05000 2033-14992 7
Chloroform mg/kg wet0.0536 0.0050 0.05000 2073-127107 5
Chloromethane mg/kg wet0.0403 0.010 0.05000 2045-14381 3
cis-1,2-Dichloroethylene mg/kg wet0.0544 0.0050 0.05000 2076-134109 5
cis-1,3-Dichloropropylene mg/kg wet0.0566 0.0050 0.05000 2071-125113 4
Cyclohexane mg/kg wet0.0541 0.0050 0.05000 2070-130108 7
Dibromochloromethane mg/kg wet0.0478 0.0050 0.05000 2073-12296 3
Dichlorodifluoromethane mg/kg wet0.0243 0.010 0.05000 2026-14649 4
Ethylbenzene mg/kg wet0.0498 0.0050 0.05000 2074-128100 6
Isopropylbenzene (Cumene)mg/kg wet0.0452 0.010 0.05000 2068-12690 6
m,p-Xylenes mg/kg wet0.100 0.010 0.1000 2075-124100 6
Methyl Acetate mg/kg wet0.0489 0.0050 0.05000 2070-13098 6
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0459 0.050 0.05000 20 J61-15792 2
Methylcyclohexane mg/kg wet0.0545 0.0050 0.05000 2070-130109 5
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0490 0.020 0.05000 2063-14998 6
Methyl Isobutyl Ketone mg/kg wet0.0540 0.010 0.05000 2057-162108 3
Methylene Chloride mg/kg wet0.0478 0.010 0.05000 2074-12996 4
Methyl-tert-Butyl Ether mg/kg wet0.0491 0.0050 0.05000 2070-13098 1
o-Xylene mg/kg wet0.0498 0.0050 0.05000 2074-126100 6
Styrene mg/kg wet0.0518 0.0050 0.05000 2077-121104 5
Tetrachloroethylene mg/kg wet0.0541 0.010 0.05000 2068-130108 5
Toluene mg/kg wet0.0564 0.0050 0.05000 2071-129113 4
trans-1,2-Dichloroethylene mg/kg wet0.0519 0.0050 0.05000 2073-132104 4
trans-1,3-Dichloropropylene mg/kg wet0.0587 0.0050 0.05000 2068-123117 2
Trichloroethylene mg/kg wet0.0547 0.0050 0.05000 2075-133109 5
Trichlorofluoromethane mg/kg wet0.0641 0.0050 0.05000 2044-146128 3
Vinyl chloride mg/kg wet0.0462 0.010 0.05000 2048-14792 4
Xylenes, total mg/kg wet0.150 0.015 0.1500 2074-126100 6
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9246.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.5
ug/L 50.00 76-129Surrogate: Toluene-d8 8743.5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8A0188 - 5035
Matrix Spike (P8A0188-MS1)Prepared & Analyzed: 01/15/18 Source: 8010088-01
1,1,1-Trichloroethane mg/kg dry0.0508 0.0061 0.06056 BRL 52-13984
1,1,2,2-Tetrachloroethane mg/kg dry0.0227 0.0061 0.06056 BRL M39-13538
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg dry0.0560 0.012 0.06056 BRL 70-13092
1,1,2-Trichloroethane mg/kg dry0.0294 0.0061 0.06056 BRL 44-14049
1,1-Dichloroethane mg/kg dry0.0436 0.0061 0.06056 BRL 59-13772
1,1-Dichloroethylene mg/kg dry0.0464 0.0061 0.06056 BRL 54-16277
1,2,3-Trichlorobenzene mg/kg dry0.00956 0.012 0.06056 BRL M, J34-12016
1,2,4-Trichlorobenzene mg/kg dry0.00923 0.012 0.06056 BRL M, J35-11615
1,2-Dibromo-3-chloropropane mg/kg dry0.0208 0.0061 0.06056 BRL 27-13234
1,2-Dibromoethane mg/kg dry0.0215 0.0061 0.06056 BRL M49-13236
1,2-Dichlorobenzene mg/kg dry0.0171 0.012 0.06056 BRL M42-13028
1,2-Dichloroethane mg/kg dry0.0344 0.0061 0.06056 BRL 51-13157
1,2-Dichloropropane mg/kg dry0.0405 0.0061 0.06056 BRL 55-13867
1,3-Dichlorobenzene mg/kg dry0.0161 0.012 0.06056 BRL M41-12927
1,4-Dichlorobenzene mg/kg dry0.0142 0.012 0.06056 BRL M44-13424
1,4-Dioxane mg/kg dry0.756 0.12 0.6056 BRL 70-130125
Acetone mg/kg dry0.0689 0.024 0.1211 0.0220 34-14339
Benzene mg/kg dry0.0427 0.0036 0.06056 BRL 60-13571
Bromochloromethane mg/kg dry0.0326 0.0061 0.06056 BRL M55-13654
Bromodichloromethane mg/kg dry0.0359 0.0061 0.06056 BRL 55-12759
Bromoform mg/kg dry0.0181 0.0061 0.06056 BRL M40-13630
Bromomethane mg/kg dry0.0295 0.012 0.06056 BRL 30-13749
Carbon disulfide mg/kg dry0.0378 0.012 0.06056 BRL 49-13962
Carbon Tetrachloride mg/kg dry0.0496 0.0061 0.06056 BRL 48-15382
Chlorobenzene mg/kg dry0.0269 0.0061 0.06056 BRL M57-12544
Chloroethane mg/kg dry0.0383 0.012 0.06056 BRL 16-17763
Chloroform mg/kg dry0.0424 0.0061 0.06056 BRL 56-13770
Chloromethane mg/kg dry0.0337 0.012 0.06056 BRL 40-14556
cis-1,2-Dichloroethylene mg/kg dry0.0342 0.0061 0.06056 BRL M58-14056
cis-1,3-Dichloropropylene mg/kg dry0.0255 0.0061 0.06056 BRL 42-13542
Cyclohexane mg/kg dry0.0467 0.0061 0.06056 BRL 70-13077
Dibromochloromethane mg/kg dry0.0239 0.0061 0.06056 BRL M49-12740
Dichlorodifluoromethane mg/kg dry0.0289 0.012 0.06056 BRL 25-15148
Ethylbenzene mg/kg dry0.0328 0.0061 0.06056 BRL 44-14454
Isopropylbenzene (Cumene)mg/kg dry0.0305 0.012 0.06056 BRL 41-14050
m,p-Xylenes mg/kg dry0.0654 0.012 0.1211 BRL 36-14854
Methyl Acetate mg/kg dry0.0304 0.0061 0.06056 BRL M70-13050
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0184 0.061 0.06056 BRL M, J30-14730
Methylcyclohexane mg/kg dry0.0422 0.0061 0.06056 BRL 70-13070
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0305 0.024 0.06056 BRL 24-16050
Methyl Isobutyl Ketone mg/kg dry0.0326 0.012 0.06056 BRL 25-16354
Methylene Chloride mg/kg dry0.0500 0.012 0.06056 BRL 53-14483
Methyl-tert-Butyl Ether mg/kg dry0.0376 0.0061 0.06056 BRL 49-13562
o-Xylene mg/kg dry0.0335 0.0061 0.06056 BRL 43-14355
Styrene mg/kg dry0.0234 0.0061 0.06056 BRL M42-13239
Tetrachloroethylene mg/kg dry0.0409 0.012 0.06056 BRL 47-14268
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8A0188 - 5035
Matrix Spike (P8A0188-MS1)Prepared & Analyzed: 01/15/18 Source: 8010088-01
Toluene mg/kg dry0.0408 0.0061 0.06056 BRL 57-13567
trans-1,2-Dichloroethylene mg/kg dry0.0348 0.0061 0.06056 BRL 58-14158
trans-1,3-Dichloropropylene mg/kg dry0.0193 0.0061 0.06056 BRL M41-12432
Trichloroethylene mg/kg dry0.0384 0.0061 0.06056 BRL 38-16463
Trichlorofluoromethane mg/kg dry0.0534 0.0061 0.06056 BRL 30-15788
Vinyl chloride mg/kg dry0.0449 0.012 0.06056 BRL 40-15674
Xylenes, total mg/kg dry0.0989 0.018 0.1817 BRL 36-14854
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.6
ug/L 50.00 76-129Surrogate: Toluene-d8 8643.0
Matrix Spike Dup (P8A0188-MSD1)Prepared: 01/15/18 Analyzed: 01/16/18 Source: 8010088-01
1,1,1-Trichloroethane mg/kg dry0.0503 0.0061 0.06106 BRL 2152-13982 1
1,1,2,2-Tetrachloroethane mg/kg dry0.0247 0.0061 0.06106 BRL 2239-13540 8
1,1,2-Trichloro-1,2,2-trifluoroethane mg/kg dry0.0546 0.012 0.06106 BRL 2070-13089 2
1,1,2-Trichloroethane mg/kg dry0.0320 0.0061 0.06106 BRL 2144-14052 9
1,1-Dichloroethane mg/kg dry0.0435 0.0061 0.06106 BRL 2159-13771 0.1
1,1-Dichloroethylene mg/kg dry0.0437 0.0061 0.06106 BRL 2254-16272 6
1,2,3-Trichlorobenzene mg/kg dry0.0107 0.012 0.06106 BRL 41 M, J34-12017 11
1,2,4-Trichlorobenzene mg/kg dry0.0105 0.012 0.06106 BRL 62 M, J35-11617 13
1,2-Dibromo-3-chloropropane mg/kg dry0.0226 0.0061 0.06106 BRL 2527-13237 8
1,2-Dibromoethane mg/kg dry0.0232 0.0061 0.06106 BRL 15 M49-13238 7
1,2-Dichlorobenzene mg/kg dry0.0186 0.012 0.06106 BRL 21 M42-13031 8
1,2-Dichloroethane mg/kg dry0.0360 0.0061 0.06106 BRL 1351-13159 4
1,2-Dichloropropane mg/kg dry0.0412 0.0061 0.06106 BRL 1655-13868 2
1,3-Dichlorobenzene mg/kg dry0.0170 0.012 0.06106 BRL 24 M41-12928 6
1,4-Dichlorobenzene mg/kg dry0.0154 0.012 0.06106 BRL 21 M44-13425 8
1,4-Dioxane mg/kg dry0.638 0.12 0.6106 BRL 2070-130105 17
Acetone mg/kg dry0.0709 0.024 0.1221 0.0220 4934-14340 3
Benzene mg/kg dry0.0424 0.0037 0.06106 BRL 2060-13569 0.9
Bromochloromethane mg/kg dry0.0336 0.0061 0.06106 BRL 1855-13655 3
Bromodichloromethane mg/kg dry0.0385 0.0061 0.06106 BRL 1755-12763 7
Bromoform mg/kg dry0.0211 0.0061 0.06106 BRL 35 M40-13635 15
Bromomethane mg/kg dry0.0334 0.012 0.06106 BRL 3030-13755 12
Carbon disulfide mg/kg dry0.0382 0.012 0.06106 BRL 2649-13963 1
Carbon Tetrachloride mg/kg dry0.0503 0.0061 0.06106 BRL 2348-15382 1
Chlorobenzene mg/kg dry0.0280 0.0061 0.06106 BRL 14 M57-12546 4
Chloroethane mg/kg dry0.0383 0.012 0.06106 BRL 4716-17763 0.2
Chloroform mg/kg dry0.0430 0.0061 0.06106 BRL 1856-13770 1
Chloromethane mg/kg dry0.0343 0.012 0.06106 BRL 2640-14556 2
cis-1,2-Dichloroethylene mg/kg dry0.0347 0.0061 0.06106 BRL 28 M58-14057 2
cis-1,3-Dichloropropylene mg/kg dry0.0268 0.0061 0.06106 BRL 3242-13544 5
Cyclohexane mg/kg dry0.0463 0.0061 0.06106 BRL 2070-13076 0.8
Dibromochloromethane mg/kg dry0.0271 0.0061 0.06106 BRL 24 M49-12744 13
Dichlorodifluoromethane mg/kg dry0.0286 0.012 0.06106 BRL 3725-15147 1
Ethylbenzene mg/kg dry0.0337 0.0061 0.06106 BRL 1944-14455 3
Isopropylbenzene (Cumene)mg/kg dry0.0312 0.012 0.06106 BRL 2741-14051 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8A0188 - 5035
Matrix Spike Dup (P8A0188-MSD1)Prepared: 01/15/18 Analyzed: 01/16/18 Source: 8010088-01
m,p-Xylenes mg/kg dry0.0665 0.012 0.1221 BRL 2036-14854 2
Methyl Acetate mg/kg dry0.0334 0.0061 0.06106 BRL 20 M70-13055 10
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0201 0.061 0.06106 BRL 42 M, J30-14733 8
Methylcyclohexane mg/kg dry0.0415 0.0061 0.06106 BRL 20 M70-13068 2
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0327 0.024 0.06106 BRL 4224-16053 7
Methyl Isobutyl Ketone mg/kg dry0.0353 0.012 0.06106 BRL 4425-16358 8
Methylene Chloride mg/kg dry0.0506 0.012 0.06106 BRL 1453-14483 1
Methyl-tert-Butyl Ether mg/kg dry0.0391 0.0061 0.06106 BRL 2249-13564 4
o-Xylene mg/kg dry0.0343 0.0061 0.06106 BRL 1743-14356 2
Styrene mg/kg dry0.0252 0.0061 0.06106 BRL 28 M42-13241 8
Tetrachloroethylene mg/kg dry0.0406 0.012 0.06106 BRL 2647-14266 0.9
Toluene mg/kg dry0.0411 0.0061 0.06106 BRL 2257-13567 0.8
trans-1,2-Dichloroethylene mg/kg dry0.0347 0.0061 0.06106 BRL 18 M58-14157 0.4
trans-1,3-Dichloropropylene mg/kg dry0.0208 0.0061 0.06106 BRL 20 M41-12434 8
Trichloroethylene mg/kg dry0.0382 0.0061 0.06106 BRL 1838-16463 0.3
Trichlorofluoromethane mg/kg dry0.0543 0.0061 0.06106 BRL 2730-15789 2
Vinyl chloride mg/kg dry0.0437 0.012 0.06106 BRL 3540-15672 3
Xylenes, total mg/kg dry0.101 0.018 0.1832 BRL 2036-14855 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9949.6
ug/L 50.00 76-129Surrogate: Toluene-d8 8542.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
Blank (P8A0147-BLK1)Prepared: 01/11/18 Analyzed: 01/12/18
1,1’-Biphenyl mg/kg wetBRL0.33
2,3,4,6-Tetrachlorophenol mg/kg wetBRL0.33
2,4,5-Trichlorophenol mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitroaniline mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
3-Nitroaniline mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitroaniline mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Acetophenone mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Atrazine mg/kg wetBRL0.33
Benzaldehyde mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Caprolactam mg/kg wetBRL0.33
Carbazole mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
Blank (P8A0147-BLK1)Prepared: 01/11/18 Analyzed: 01/12/18
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 782.59
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 741.24
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 712.38
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 661.10
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 702.34
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 791.31
LCS (P8A0147-BS1)Prepared: 01/11/18 Analyzed: 01/12/18
2,4,5-Trichlorophenol mg/kg wet1.16 0.33 1.667 41-12470
2,4,6-Trichlorophenol mg/kg wet1.14 0.33 1.667 39-12669
2,4-Dichlorophenol mg/kg wet0.982 0.33 1.667 40-12259
2,4-Dimethylphenol mg/kg wet1.18 0.33 1.667 30-12771
2,4-Dinitrophenol mg/kg wet0.960 0.33 1.667 27-12958
2,4-Dinitrotoluene mg/kg wet1.14 0.33 1.667 48-12668
2,6-Dinitrotoluene mg/kg wet1.17 0.33 1.667 46-12470
2-Chloronaphthalene mg/kg wet1.07 0.33 1.667 41-11464
2-Chlorophenol mg/kg wet1.03 0.33 1.667 34-12162
2-Methylnaphthalene mg/kg wet0.957 0.33 1.667 38-12257
2-Methylphenol mg/kg wet1.12 0.33 1.667 32-12267
2-Nitroaniline mg/kg wet1.10 0.33 1.667 44-12766
2-Nitrophenol mg/kg wet0.884 0.33 1.667 36-12353
3,3’-Dichlorobenzidine mg/kg wet1.19 0.33 1.667 22-12171
3/4-Methylphenol mg/kg wet1.05 0.33 1.667 34-11963
3-Nitroaniline mg/kg wet1.14 0.33 1.667 33-11968
4,6-Dinitro-2-methylphenol mg/kg wet1.13 0.33 1.667 29-13268
4-Bromophenyl phenyl ether mg/kg wet1.08 0.33 1.667 46-12465
4-Chloro-3-methylphenol mg/kg wet1.03 0.33 1.667 45-12262
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
LCS (P8A0147-BS1)Prepared: 01/11/18 Analyzed: 01/12/18
4-Chloroaniline mg/kg wet1.02 0.33 1.667 17-10661
4-Chlorophenyl phenyl ether mg/kg wet1.14 0.33 1.667 45-12168
4-Nitroaniline mg/kg wet1.08 0.33 1.667 63-14765
4-Nitrophenol mg/kg wet1.15 0.33 1.667 30-13269
Acenaphthene mg/kg wet1.12 0.33 1.667 40-12367
Acenaphthylene mg/kg wet1.18 0.33 1.667 32-13271
Acetophenone mg/kg wet0.997 0.33 1.667 33-11560
Anthracene mg/kg wet1.25 0.33 1.667 47-12375
Benzo(a)anthracene mg/kg wet1.19 0.33 1.667 49-12671
Benzo(a)pyrene mg/kg wet1.22 0.33 1.667 45-12973
Benzo(b)fluoranthene mg/kg wet1.21 0.33 1.667 45-13273
Benzo(g,h,i)perylene mg/kg wet1.16 0.33 1.667 43-13470
Benzo(k)fluoranthene mg/kg wet1.18 0.33 1.667 47-13271
bis(2-Chloroethoxy)methane mg/kg wet0.942 0.33 1.667 36-12157
Bis(2-Chloroethyl)ether mg/kg wet0.885 0.33 1.667 31-12053
Bis(2-chloroisopropyl)ether mg/kg wet0.936 0.33 1.667 33-13156
Bis(2-Ethylhexyl)phthalate mg/kg wet1.20 0.33 1.667 51-13372
Butyl benzyl phthalate mg/kg wet1.12 0.33 1.667 48-13267
Carbazole mg/kg wet1.18 0.33 1.667 50-12371
Chrysene mg/kg wet1.12 0.33 1.667 50-12467
Dibenzo(a,h)anthracene mg/kg wet0.618 0.33 1.667 L45-13437
Dibenzofuran mg/kg wet1.11 0.33 1.667 44-12066
Diethyl phthalate mg/kg wet1.11 0.33 1.667 50-12466
Dimethyl phthalate mg/kg wet1.09 0.33 1.667 48-12466
Di-n-butyl phthalate mg/kg wet1.17 0.33 1.667 51-12870
Di-n-octyl phthalate mg/kg wet1.19 0.33 1.667 45-14072
Fluoranthene mg/kg wet1.21 0.33 1.667 50-12772
Fluorene mg/kg wet1.18 0.33 1.667 43-12571
Hexachlorobenzene mg/kg wet1.14 0.33 1.667 45-12269
Hexachlorobutadiene mg/kg wet0.864 0.33 1.667 32-12352
Hexachlorocyclopentadiene mg/kg wet0.853 0.33 1.667 32-11751
Hexachloroethane mg/kg wet0.803 0.33 1.667 28-11748
Indeno(1,2,3-cd)pyrene mg/kg wet1.24 0.33 1.667 45-13374
Isophorone mg/kg wet0.954 0.33 1.667 30-12257
Naphthalene mg/kg wet0.917 0.33 1.667 35-12355
Nitrobenzene mg/kg wet0.820 0.33 1.667 34-12249
N-Nitroso-di-n-propylamine mg/kg wet1.05 0.33 1.667 36-12063
N-Nitrosodiphenylamine mg/kg wet1.41 0.33 1.667 38-12784
Pentachlorophenol mg/kg wet1.31 0.33 1.667 25-13379
Phenanthrene mg/kg wet1.23 0.33 1.667 50-12174
Phenol mg/kg wet1.10 0.33 1.667 34-12166
Pyrene mg/kg wet1.19 0.33 1.667 47-12771
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 752.48
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 701.16
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 642.13
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 560.930
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
LCS (P8A0147-BS1)Prepared: 01/11/18 Analyzed: 01/12/18
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 642.13
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 711.18
LCS (P8A0147-BS2)Prepared: 01/11/18 Analyzed: 01/12/18
1,1’-Biphenyl mg/kg wet1.01 0.33 1.667 40-11760
2,3,4,6-Tetrachlorophenol mg/kg wet1.42 0.33 1.667 44-12585
Atrazine mg/kg wet1.17 0.33 1.667 47-12770
Benzaldehyde mg/kg wet0.889 0.33 1.667 35-11553
Caprolactam mg/kg wet1.10 0.33 1.667 46-11766
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 722.41
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 661.10
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 642.12
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 590.986
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 622.08
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 691.15
LCS Dup (P8A0147-BSD1)Prepared: 01/11/18 Analyzed: 01/12/18
2,4,5-Trichlorophenol mg/kg wet1.00 0.33 1.667 2041-12460 15
2,4,6-Trichlorophenol mg/kg wet1.11 0.33 1.667 2039-12666 3
2,4-Dichlorophenol mg/kg wet0.945 0.33 1.667 2040-12257 4
2,4-Dimethylphenol mg/kg wet1.14 0.33 1.667 2030-12769 3
2,4-Dinitrophenol mg/kg wet0.956 0.33 1.667 2027-12957 0.3
2,4-Dinitrotoluene mg/kg wet1.15 0.33 1.667 2048-12669 1
2,6-Dinitrotoluene mg/kg wet1.20 0.33 1.667 2046-12472 3
2-Chloronaphthalene mg/kg wet1.05 0.33 1.667 2041-11463 2
2-Chlorophenol mg/kg wet0.997 0.33 1.667 2034-12160 4
2-Methylnaphthalene mg/kg wet0.927 0.33 1.667 2038-12256 3
2-Methylphenol mg/kg wet1.09 0.33 1.667 2032-12266 2
2-Nitroaniline mg/kg wet1.11 0.33 1.667 2044-12767 0.8
2-Nitrophenol mg/kg wet0.867 0.33 1.667 2036-12352 2
3,3’-Dichlorobenzidine mg/kg wet1.20 0.33 1.667 2022-12172 0.8
3/4-Methylphenol mg/kg wet1.05 0.33 1.667 2034-11963 0.3
3-Nitroaniline mg/kg wet1.15 0.33 1.667 2033-11969 0.6
4,6-Dinitro-2-methylphenol mg/kg wet1.14 0.33 1.667 2029-13269 2
4-Bromophenyl phenyl ether mg/kg wet1.09 0.33 1.667 2046-12465 0.4
4-Chloro-3-methylphenol mg/kg wet1.02 0.33 1.667 2045-12261 1
4-Chloroaniline mg/kg wet0.988 0.33 1.667 2017-10659 3
4-Chlorophenyl phenyl ether mg/kg wet1.13 0.33 1.667 2045-12168 0.3
4-Nitroaniline mg/kg wet1.11 0.33 1.667 2063-14766 2
4-Nitrophenol mg/kg wet1.16 0.33 1.667 2030-13270 0.9
Acenaphthene mg/kg wet1.10 0.33 1.667 2040-12366 2
Acenaphthylene mg/kg wet1.18 0.33 1.667 2032-13270 0.6
Acetophenone mg/kg wet0.972 0.33 1.667 2033-11558 2
Anthracene mg/kg wet1.25 0.33 1.667 2047-12375 0.3
Benzo(a)anthracene mg/kg wet1.21 0.33 1.667 2049-12673 2
Benzo(a)pyrene mg/kg wet1.20 0.33 1.667 2045-12972 1
Benzo(b)fluoranthene mg/kg wet1.21 0.33 1.667 2045-13273 0.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
LCS Dup (P8A0147-BSD1)Prepared: 01/11/18 Analyzed: 01/12/18
Benzo(g,h,i)perylene mg/kg wet1.15 0.33 1.667 2043-13469 0.5
Benzo(k)fluoranthene mg/kg wet1.20 0.33 1.667 2047-13272 2
bis(2-Chloroethoxy)methane mg/kg wet0.931 0.33 1.667 2036-12156 1
Bis(2-Chloroethyl)ether mg/kg wet0.862 0.33 1.667 2031-12052 3
Bis(2-chloroisopropyl)ether mg/kg wet0.895 0.33 1.667 2033-13154 4
Bis(2-Ethylhexyl)phthalate mg/kg wet1.20 0.33 1.667 2051-13372 0.3
Butyl benzyl phthalate mg/kg wet1.15 0.33 1.667 2048-13269 2
Carbazole mg/kg wet1.18 0.33 1.667 2050-12371 0.7
Chrysene mg/kg wet1.14 0.33 1.667 2050-12469 2
Dibenzo(a,h)anthracene mg/kg wet0.623 0.33 1.667 20 L45-13437 0.7
Dibenzofuran mg/kg wet1.09 0.33 1.667 2044-12066 1
Diethyl phthalate mg/kg wet1.13 0.33 1.667 2050-12468 2
Dimethyl phthalate mg/kg wet1.11 0.33 1.667 2048-12466 1
Di-n-butyl phthalate mg/kg wet1.19 0.33 1.667 2051-12871 2
Di-n-octyl phthalate mg/kg wet1.21 0.33 1.667 2045-14073 2
Fluoranthene mg/kg wet1.21 0.33 1.667 2050-12773 0.2
Fluorene mg/kg wet1.18 0.33 1.667 2043-12571 0.06
Hexachlorobenzene mg/kg wet1.14 0.33 1.667 2045-12268 0.3
Hexachlorobutadiene mg/kg wet0.816 0.33 1.667 2032-12349 6
Hexachlorocyclopentadiene mg/kg wet0.841 0.33 1.667 2032-11750 1
Hexachloroethane mg/kg wet0.773 0.33 1.667 2028-11746 4
Indeno(1,2,3-cd)pyrene mg/kg wet1.25 0.33 1.667 2045-13375 1
Isophorone mg/kg wet0.940 0.33 1.667 2030-12256 1
Naphthalene mg/kg wet0.880 0.33 1.667 2035-12353 4
Nitrobenzene mg/kg wet0.780 0.33 1.667 2034-12247 5
N-Nitroso-di-n-propylamine mg/kg wet1.04 0.33 1.667 2036-12062 2
N-Nitrosodiphenylamine mg/kg wet1.39 0.33 1.667 2038-12783 2
Pentachlorophenol mg/kg wet1.33 0.33 1.667 2025-13380 1
Phenanthrene mg/kg wet1.23 0.33 1.667 2050-12174 0.05
Phenol mg/kg wet0.989 0.33 1.667 2034-12159 11
Pyrene mg/kg wet1.19 0.33 1.667 2047-12772 0.4
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 742.46
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 671.12
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 622.07
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 530.884
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 622.07
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 701.17
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
LCS Dup (P8A0147-BSD2)Prepared: 01/11/18 Analyzed: 01/12/18
1,1’-Biphenyl mg/kg wet1.16 0.33 1.667 2040-11770 14
2,3,4,6-Tetrachlorophenol mg/kg wet1.61 0.33 1.667 2044-12597 12
Atrazine mg/kg wet1.31 0.33 1.667 2047-12779 11
Benzaldehyde mg/kg wet1.06 0.33 1.667 2035-11564 17
Caprolactam mg/kg wet1.27 0.33 1.667 2046-11776 14
mg/kg wet 3.333 37-131Surrogate: 2,4,6-Tribromophenol 772.58
mg/kg wet 1.667 47-130Surrogate: 2-Fluorobiphenyl 751.25
mg/kg wet 3.333 44-117Surrogate: 2-Fluorophenol 722.39
mg/kg wet 1.667 45-121Surrogate: Nitrobenzene-d5 671.12
mg/kg wet 3.333 37-127Surrogate: Phenol-d5 712.38
mg/kg wet 1.667 38-135Surrogate: Terphenyl-d14 761.27
Matrix Spike (P8A0147-MS1)Prepared: 01/11/18 Analyzed: 01/12/18 Source: 8010088-01
2,4,5-Trichlorophenol mg/kg dry1.07 0.39 1.978 BRL 41-12454
2,4,6-Trichlorophenol mg/kg dry1.18 0.39 1.978 BRL 39-12660
2,4-Dichlorophenol mg/kg dry1.00 0.39 1.978 BRL 40-12251
2,4-Dimethylphenol mg/kg dry1.12 0.39 1.978 BRL 30-12756
2,4-Dinitrophenol mg/kg dry0.746 0.39 1.978 BRL 27-12938
2,4-Dinitrotoluene mg/kg dry1.17 0.39 1.978 BRL 48-12659
2,6-Dinitrotoluene mg/kg dry1.21 0.39 1.978 BRL 46-12461
2-Chloronaphthalene mg/kg dry1.09 0.39 1.978 BRL 41-11455
2-Chlorophenol mg/kg dry1.01 0.39 1.978 BRL 34-12151
2-Methylnaphthalene mg/kg dry1.06 0.39 1.978 0.150 38-12246
2-Methylphenol mg/kg dry1.08 0.39 1.978 BRL 32-12255
2-Nitroaniline mg/kg dry1.14 0.39 1.978 BRL 44-12758
2-Nitrophenol mg/kg dry0.923 0.39 1.978 BRL 36-12347
3,3’-Dichlorobenzidine mg/kg dry1.06 0.39 1.978 BRL 22-12154
3/4-Methylphenol mg/kg dry1.05 0.39 1.978 BRL 34-11953
3-Nitroaniline mg/kg dry1.15 0.39 1.978 BRL 33-11958
4,6-Dinitro-2-methylphenol mg/kg dry1.07 0.39 1.978 BRL 29-13254
4-Bromophenyl phenyl ether mg/kg dry1.13 0.39 1.978 BRL 46-12457
4-Chloro-3-methylphenol mg/kg dry1.08 0.39 1.978 BRL 45-12255
4-Chloroaniline mg/kg dry1.02 0.39 1.978 BRL 17-10651
4-Chlorophenyl phenyl ether mg/kg dry1.17 0.39 1.978 BRL 45-12159
4-Nitroaniline mg/kg dry1.08 0.39 1.978 BRL M63-14755
4-Nitrophenol mg/kg dry1.24 0.39 1.978 BRL 30-13263
Acenaphthene mg/kg dry1.14 0.39 1.978 BRL 40-12358
Acenaphthylene mg/kg dry1.22 0.39 1.978 BRL 32-13262
Acetophenone mg/kg dry1.00 0.39 1.978 BRL 33-11551
Anthracene mg/kg dry1.29 0.39 1.978 BRL 47-12365
Benzo(a)anthracene mg/kg dry1.25 0.39 1.978 BRL 49-12663
Benzo(a)pyrene mg/kg dry1.23 0.39 1.978 BRL 45-12962
Benzo(b)fluoranthene mg/kg dry1.27 0.39 1.978 0.145 45-13257
Benzo(g,h,i)perylene mg/kg dry1.19 0.39 1.978 BRL 43-13460
Benzo(k)fluoranthene mg/kg dry1.21 0.39 1.978 BRL 47-13261
bis(2-Chloroethoxy)methane mg/kg dry0.953 0.39 1.978 BRL 36-12148
Bis(2-Chloroethyl)ether mg/kg dry0.912 0.39 1.978 BRL 31-12046
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
Matrix Spike (P8A0147-MS1)Prepared: 01/11/18 Analyzed: 01/12/18 Source: 8010088-01
Bis(2-chloroisopropyl)ether mg/kg dry0.898 0.39 1.978 BRL 33-13145
Bis(2-Ethylhexyl)phthalate mg/kg dry1.24 0.39 1.978 BRL 51-13363
Butyl benzyl phthalate mg/kg dry1.20 0.39 1.978 BRL 48-13261
Carbazole mg/kg dry1.22 0.39 1.978 BRL 50-12362
Chrysene mg/kg dry1.19 0.39 1.978 BRL 50-12460
Dibenzo(a,h)anthracene mg/kg dry0.630 0.39 1.978 BRL M45-13432
Dibenzofuran mg/kg dry1.14 0.39 1.978 BRL 44-12058
Diethyl phthalate mg/kg dry1.15 0.39 1.978 BRL 50-12458
Dimethyl phthalate mg/kg dry1.12 0.39 1.978 BRL 48-12457
Di-n-butyl phthalate mg/kg dry1.22 0.39 1.978 BRL 51-12862
Di-n-octyl phthalate mg/kg dry1.23 0.39 1.978 BRL 45-14062
Fluoranthene mg/kg dry1.29 0.39 1.978 0.139 50-12758
Fluorene mg/kg dry1.21 0.39 1.978 BRL 43-12561
Hexachlorobenzene mg/kg dry1.15 0.39 1.978 BRL 45-12258
Hexachlorobutadiene mg/kg dry0.857 0.39 1.978 BRL 32-12343
Hexachlorocyclopentadiene mg/kg dry0.709 0.39 1.978 BRL 32-11736
Hexachloroethane mg/kg dry0.767 0.39 1.978 BRL 28-11739
Indeno(1,2,3-cd)pyrene mg/kg dry1.29 0.39 1.978 BRL 45-13365
Isophorone mg/kg dry0.960 0.39 1.978 BRL 30-12249
Naphthalene mg/kg dry0.967 0.39 1.978 0.126 35-12343
Nitrobenzene mg/kg dry0.824 0.39 1.978 BRL 34-12242
N-Nitroso-di-n-propylamine mg/kg dry1.04 0.39 1.978 BRL 36-12052
N-Nitrosodiphenylamine mg/kg dry1.43 0.39 1.978 BRL 38-12772
Pentachlorophenol mg/kg dry1.48 0.39 1.978 BRL 25-13375
Phenanthrene mg/kg dry1.33 0.39 1.978 0.148 50-12160
Phenol mg/kg dry1.08 0.39 1.978 BRL 34-12155
Pyrene mg/kg dry1.30 0.39 1.978 0.128 47-12759
mg/kg dry 3.955 37-131Surrogate: 2,4,6-Tribromophenol 612.43
mg/kg dry 1.978 47-130Surrogate: 2-Fluorobiphenyl 601.18
mg/kg dry 3.955 44-117Surrogate: 2-Fluorophenol 522.05
mg/kg dry 1.978 45-121Surrogate: Nitrobenzene-d5 470.924
mg/kg dry 3.955 37-127Surrogate: Phenol-d5 532.11
mg/kg dry 1.978 38-135Surrogate: Terphenyl-d14 611.21
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
Matrix Spike Dup (P8A0147-MSD1)Prepared: 01/11/18 Analyzed: 01/12/18 Source: 8010088-01
2,4,5-Trichlorophenol mg/kg dry1.26 0.39 1.974 BRL 2041-12464 17
2,4,6-Trichlorophenol mg/kg dry1.23 0.39 1.974 BRL 2039-12662 4
2,4-Dichlorophenol mg/kg dry1.07 0.39 1.974 BRL 2040-12254 6
2,4-Dimethylphenol mg/kg dry1.16 0.39 1.974 BRL 2030-12759 4
2,4-Dinitrophenol mg/kg dry0.753 0.39 1.974 BRL 2027-12938 0.9
2,4-Dinitrotoluene mg/kg dry1.23 0.39 1.974 BRL 2048-12662 4
2,6-Dinitrotoluene mg/kg dry1.28 0.39 1.974 BRL 2046-12465 5
2-Chloronaphthalene mg/kg dry1.14 0.39 1.974 BRL 2041-11458 4
2-Chlorophenol mg/kg dry1.12 0.39 1.974 BRL 2034-12157 11
2-Methylnaphthalene mg/kg dry1.07 0.39 1.974 0.150 2038-12246 0.8
2-Methylphenol mg/kg dry1.19 0.39 1.974 BRL 2032-12260 10
2-Nitroaniline mg/kg dry1.23 0.39 1.974 BRL 2044-12762 8
2-Nitrophenol mg/kg dry0.983 0.39 1.974 BRL 2036-12350 6
3,3’-Dichlorobenzidine mg/kg dry1.13 0.39 1.974 BRL 2022-12157 6
3/4-Methylphenol mg/kg dry1.13 0.39 1.974 BRL 2034-11957 8
3-Nitroaniline mg/kg dry1.22 0.39 1.974 BRL 2033-11962 6
4,6-Dinitro-2-methylphenol mg/kg dry1.09 0.39 1.974 BRL 2029-13255 3
4-Bromophenyl phenyl ether mg/kg dry1.19 0.39 1.974 BRL 2046-12460 5
4-Chloro-3-methylphenol mg/kg dry1.13 0.39 1.974 BRL 2045-12257 5
4-Chloroaniline mg/kg dry1.05 0.39 1.974 BRL 2017-10653 3
4-Chlorophenyl phenyl ether mg/kg dry1.22 0.39 1.974 BRL 2045-12162 4
4-Nitroaniline mg/kg dry1.16 0.39 1.974 BRL 20 M63-14759 7
4-Nitrophenol mg/kg dry1.33 0.39 1.974 BRL 2030-13267 7
Acenaphthene mg/kg dry1.19 0.39 1.974 BRL 2040-12360 4
Acenaphthylene mg/kg dry1.27 0.39 1.974 BRL 2032-13264 4
Acetophenone mg/kg dry1.13 0.39 1.974 BRL 2033-11557 12
Anthracene mg/kg dry1.36 0.39 1.974 BRL 2047-12369 5
Benzo(a)anthracene mg/kg dry1.33 0.39 1.974 BRL 2049-12667 6
Benzo(a)pyrene mg/kg dry1.32 0.39 1.974 BRL 2045-12967 7
Benzo(b)fluoranthene mg/kg dry1.35 0.39 1.974 0.145 2045-13261 6
Benzo(g,h,i)perylene mg/kg dry1.26 0.39 1.974 BRL 2043-13464 6
Benzo(k)fluoranthene mg/kg dry1.27 0.39 1.974 BRL 2047-13264 5
bis(2-Chloroethoxy)methane mg/kg dry1.03 0.39 1.974 BRL 2036-12152 8
Bis(2-Chloroethyl)ether mg/kg dry0.991 0.39 1.974 BRL 2031-12050 8
Bis(2-chloroisopropyl)ether mg/kg dry0.993 0.39 1.974 BRL 2033-13150 10
Bis(2-Ethylhexyl)phthalate mg/kg dry1.30 0.39 1.974 BRL 2051-13366 4
Butyl benzyl phthalate mg/kg dry1.27 0.39 1.974 BRL 2048-13264 6
Carbazole mg/kg dry1.28 0.39 1.974 BRL 2050-12365 5
Chrysene mg/kg dry1.21 0.39 1.974 BRL 2050-12462 2
Dibenzo(a,h)anthracene mg/kg dry0.677 0.39 1.974 BRL 20 M45-13434 7
Dibenzofuran mg/kg dry1.19 0.39 1.974 BRL 2044-12060 4
Diethyl phthalate mg/kg dry1.19 0.39 1.974 BRL 2050-12460 4
Dimethyl phthalate mg/kg dry1.19 0.39 1.974 BRL 2048-12460 6
Di-n-butyl phthalate mg/kg dry1.29 0.39 1.974 BRL 2051-12865 5
Di-n-octyl phthalate mg/kg dry1.34 0.39 1.974 BRL 2045-14068 8
Fluoranthene mg/kg dry1.36 0.39 1.974 0.139 2050-12762 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8A0147 - 3546
Matrix Spike Dup (P8A0147-MSD1)Prepared: 01/11/18 Analyzed: 01/12/18 Source: 8010088-01
Fluorene mg/kg dry1.27 0.39 1.974 BRL 2043-12564 4
Hexachlorobenzene mg/kg dry1.21 0.39 1.974 BRL 2045-12261 5
Hexachlorobutadiene mg/kg dry0.914 0.39 1.974 BRL 2032-12346 6
Hexachlorocyclopentadiene mg/kg dry0.642 0.39 1.974 BRL 2032-11733 10
Hexachloroethane mg/kg dry0.835 0.39 1.974 BRL 2028-11742 9
Indeno(1,2,3-cd)pyrene mg/kg dry1.37 0.39 1.974 BRL 2045-13369 6
Isophorone mg/kg dry1.02 0.39 1.974 BRL 2030-12252 6
Naphthalene mg/kg dry1.02 0.39 1.974 0.126 2035-12345 6
Nitrobenzene mg/kg dry0.878 0.39 1.974 BRL 2034-12244 6
N-Nitroso-di-n-propylamine mg/kg dry1.14 0.39 1.974 BRL 2036-12058 9
N-Nitrosodiphenylamine mg/kg dry1.49 0.39 1.974 BRL 2038-12775 4
Pentachlorophenol mg/kg dry1.53 0.39 1.974 BRL 2025-13378 4
Phenanthrene mg/kg dry1.38 0.39 1.974 0.148 2050-12163 4
Phenol mg/kg dry1.12 0.39 1.974 BRL 2034-12157 3
Pyrene mg/kg dry1.35 0.39 1.974 0.128 2047-12762 3
mg/kg dry 3.949 37-131Surrogate: 2,4,6-Tribromophenol 632.49
mg/kg dry 1.974 47-130Surrogate: 2-Fluorobiphenyl 601.19
mg/kg dry 3.949 44-117Surrogate: 2-Fluorophenol 572.23
mg/kg dry 1.974 45-121Surrogate: Nitrobenzene-d5 490.975
mg/kg dry 3.949 37-127Surrogate: Phenol-d5 582.28
mg/kg dry 1.974 38-135Surrogate: Terphenyl-d14 621.23
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8A0126 - 3050B
Blank (P8A0126-BLK1)Prepared: 01/11/18 Analyzed: 01/12/18
Arsenic mg/kg wetBRL1.5
Barium mg/kg wet0.0980 10 J
Cadmium mg/kg wet0.0248 0.25 J
Chromium mg/kg wet0.0298 0.50 J
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL1.0
Silver mg/kg wet0.0335 0.25 J
LCS (P8A0126-BS1)Prepared: 01/11/18 Analyzed: 01/12/18
Arsenic mg/kg wet27.3 1.5 25.00 80-120109
Barium mg/kg wet27.5 10 25.00 80-120110
Cadmium mg/kg wet28.6 0.25 25.00 80-120115
Chromium mg/kg wet27.7 0.50 25.00 80-120111
Lead mg/kg wet28.9 0.25 25.00 80-120116
Selenium mg/kg wet27.0 1.0 25.00 80-120108
Silver mg/kg wet12.2 0.25 10.00 LH80-120122
Matrix Spike (P8A0126-MS1)Prepared: 01/11/18 Analyzed: 01/12/18 Source: 8010088-01
Arsenic mg/kg dry37.8 1.7 29.10 13.2 75-12584
Barium mg/kg dry16412 29.09 126 M75-125131
Cadmium mg/kg dry30.5 0.29 29.09 0.107 75-125105
Chromium mg/kg dry1200.58 29.10 81.8 M75-125130
Lead mg/kg dry43.0 0.29 29.10 13.1 75-125103
Selenium mg/kg dry30.7 1.2 29.09 1.98 75-12599
Silver mg/kg dry12.8 0.29 11.64 0.0474 75-125110
Matrix Spike Dup (P8A0126-MSD1)Prepared: 01/11/18 Analyzed: 01/12/18 Source: 8010088-01
Arsenic mg/kg dry40.5 1.8 29.98 13.2 2075-12591 7
Barium mg/kg dry16412 29.97 126 20 M75-125127 0.08
Cadmium mg/kg dry32.8 0.30 29.97 0.107 2075-125109 7
Chromium mg/kg dry1250.60 29.98 81.8 20 M75-125146 5
Lead mg/kg dry44.4 0.30 29.98 13.1 2075-125104 3
Selenium mg/kg dry31.9 1.2 29.97 1.98 2075-125100 4
Silver mg/kg dry13.8 0.30 11.99 0.0474 2075-125114 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 36
1/16/18
Level II QC Report
2923 South Tryon St. Ste 100
Project: CAT-105 NSIF Brownfields
Sampling
Hart & Hickman (Charlotte)
Charlotte, NC 28203
Attn: Ken Windsand
Prism Work Order: 8010088
Time Submitted: 1/9/2018 1:35:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8A0126 - 3050B
Post Spike (P8A0126-PS1)Prepared: 01/11/18 Analyzed: 01/12/18 Source: 8010088-01
Arsenic ug/L144 100.0 44.6 80-12099
Barium ug/L512 100.0 425 80-12087
Cadmium ug/L101 100.0 0.362 80-120101
Chromium ug/L367 100.0 276 80-12091
Lead ug/L147 100.0 44.1 80-120103
Selenium ug/L107 100.0 6.69 80-120100
Silver ug/L108 100.0 0.160 80-120108
Batch P8A0133 - 7471B
Blank (P8A0133-BLK1)Prepared & Analyzed: 01/11/18
Mercury mg/kg wetBRL0.020
LCS (P8A0133-BS1)Prepared & Analyzed: 01/11/18
Mercury mg/kg wet0.443 0.020 0.4167 80-120106
Matrix Spike (P8A0133-MS1)Prepared & Analyzed: 01/11/18 Source: 8010088-01
Mercury mg/kg dry0.450 0.023 0.4865 0.0373 80-12085
Matrix Spike Dup (P8A0133-MSD1)Prepared & Analyzed: 01/11/18 Source: 8010088-01
Mercury mg/kg dry0.486 0.023 0.4865 0.0373 2080-12092 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 36
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P8A01328010088-01 01/10/18 15:4530 30g g
P8A01328010088-02 01/10/18 15:4530 30g g
P8A01328010088-03 01/10/18 15:4530 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P8A01478010088-01 01/11/18 15:3630 1g mL
P8A01478010088-02 01/11/18 15:3630 1g mL
P8A01478010088-03 01/11/18 15:3630 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P8A01268010088-01 01/11/18 8:501.98 50g mL
P8A01268010088-02 01/11/18 8:501.95 50g mL
P8A01268010088-03 01/11/18 8:501.96 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P8A01338010088-01 01/11/18 11:150.65 50g mL
P8A01338010088-02 01/11/18 11:150.63 50g mL
P8A01338010088-03 01/11/18 11:150.63 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P8A01888010088-01 01/15/18 8:505.27 5g mL
P8A01888010088-02 01/15/18 8:505.93 5g mL
P8A01888010088-03 01/15/18 8:505.55 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 36
Page 36 of 36

\\hhfs01.harthickman.local\masterfiles\AAA-Master Projects\Charlotte Area Transit System (CAT)\CAT-105 NSIF BF Closeout\Report\NSIF BF Post Construction Report.docx

APPENDIX C
RISK CALCULATION RESULTS
DEQ Risk Calculator - Primary - Non-Residential Worker Soil Combined Pathways
Version Date: February 2018
Basis: November 2017 EPA RSL Table
Site ID: 15019-11-60
Exposure Unit ID: BFSS-1
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:
Ingestion
Concentration (mg/kg)
Dermal
Concentration (mg/kg)
Inhalation
Concentration (mg/kg)*
Ingestion
Carcinogenic Risk
Dermal
Carcinogenic Risk
Inhalation
Carcinogenic Risk
Calculated
Carcinogenic Risk
Ingestion
Hazard Quotient
Dermal
Hazard Quotient
Inhalation
Hazard Quotient
Calculated Non-
Carcinogenic Hazard Quotient67-64-1 Acetone 0.022 0.022 0.022 2.1E-08 1.1E-08 3.2E-087440-38-2 Arsenic, Inorganic 13 13 13 3.6E-06 7.6E-07 7.7E-11 4.3E-06 2.2E-02 4.7E-03 3.3E-06 2.7E-02
7440-39-3 Barium 130 130 130 5.6E-04 1.0E-06 5.6E-047440-43-9 Cadmium (Diet)0.11 0.11 0.11 2.7E-13 2.7E-13 9.4E-05 1.6E-05 4.2E-08 1.1E-0416065-83-1 Chromium(III), Insoluble Salts 82 82 82 4.7E-05 4.7E-057439-92-1 ~Lead and Compounds 13 13 13 <SL**<SL**<SL**
7439-97-6 ~Mercury (elemental)0.037 0.037 0.037 7.6E-04 7.6E-04205-99-2 ~Benzo[b]fluoranthene 0.14 0.14 0.14 4.3E-09 2.4E-09 1.2E-14 6.6E-09206-44-0 ~Fluoranthene 0.14 0.14 0.14 3.0E-06 1.6E-06 4.6E-0691-57-6 ~Methylnaphthalene, 2-0.15 0.15 0.15 3.2E-05 1.8E-05 5.0E-05
91-20-3 ~Naphthalene 0.13 0.13 0.13 7.3E-09 7.3E-09 5.6E-06 3.1E-06 2.0E-04 2.1E-04
129-00-0 ~Pyrene 0.13 0.13 0.13 3.7E-06 2.0E-06 5.8E-067782-49-2 Selenium 2 2 2 3.4E-04 3.8E-10 3.4E-047440-22-4 Silver 0.047 0.047 0.047 8.0E-06 8.0E-06
Cumulative:4.3E-06 2.9E-02
Output Form 2C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 800
mg/kg for commercial/industrial soil.
North Carolina DEQ Risk Calculator