21052_Little Rock Rd_Assessment Report_20180328

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Brownfields Assessment Report Little Rock Road
6108, 6120, 6128 Wilkinson Boulevard and
3000, 3012 Little Rock Road
Charlotte, North Carolina H&H Job No. RKI-008
Table of Contents

Section Page No.
1.0 Introduction ............................................................................................................................ 1
2.0 Background Information....................................................................................................... 3
3.0 Brownfields Assessment Activities ....................................................................................... 6
3.1 Utility Clearance and Geophysical Survey ........................................................................... 6
3.2 Soil Assessment .................................................................................................................... 7
3.3 Groundwater Assessment ..................................................................................................... 8
3.4 Quality Assurance/Quality Control .................................................................................... 11
4.0 Brownfields Assessment Results ......................................................................................... 13
4.1 Soil Analytical Results ....................................................................................................... 13
4.2 Groundwater Flow .............................................................................................................. 14
4.3 Groundwater Analytical Results ......................................................................................... 14
5.0 Summary and Conclusions.................................................................................................. 16

List of Figures
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Shallow Groundwater Potentiometric Map

List of Appendices
Appendix A Well Construction Permits
Appendix B Boring Logs

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Appendix C Well Construction Records
Appendix D Groundwater Sampling Records
Appendix E Laboratory Analytical Reports

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Brownfields Assessment Work Plan Little Rock Road
6108, 6120, 6128 Wilkinson Boulevard and
3000, 3012 Little Rock Road
Charlotte, North Carolina H&H Job No. RKI-008

1.0 Introduction

Hart & Hickman, PC (H&H) is pleased to present this Brownfields Assessment Report for the
Little Rock Road Brownfields Site located at 6108, 6120, and 6128 Wilkinson Boulevard and 3000
and 3012 Little Rock Road in Charlotte, Mecklenburg County, North Carolina (Brownfields
Project # 21052-17-060). A Site location map is included as Figure 1.

The subject Site is comprised of seven parcels totaling approximately 5.89 acres. The Site contains
four vacant commercial buildings, two occupied commercial buildings, one canopy structure, and
two open carports. The commercial building located at 6128 Wilkinson Boulevard is currently
occupied by a hair salon, and the commercial building located at 3000-B Little Rock Road is
currently occupied by an automotive service and repair facility. The remainder of the Site is
vacant. The Site has historically been used for residential and various commercial purposes
including retail gasoline distribution, vehicle rental, automotive salvage, automotive sales and
service, prefabricated building sales, hair salon, and general office space. The Site is planned to
be redeveloped for office, hotel, retail and/or restaurant uses.

The Site received eligibility into the North Carolina Department of Environmental Quality (DEQ)
Brownfields Program via a Letter of Eligibility dated December 22, 2017. The Prospective
Developer, RK Investments Charlotte LLC, subsequently elected to participate in the Brownfields
Program Redevelopment Now option. As part of this process, a data gap meeting was held with
the DEQ Brownfields project manager, Mr. Brad Atkinson, via telephone on January 10, 2018 to
discuss the Site history, proposed redevelopment plans, previous assessment results, data gaps,
and the proposed schedule for completing the Brownfields Agreement. H&H performed the

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Brownfields assessment activities presented in this report in accordance with a DEQ-approved
Brownfields Assessment Work Plan (Work Plan) dated January 30, 2018 and follow up
discussions with the Brownfields project manager.

The Brownfields assessment activities were conducted to further evaluate potential risks associated
with future Site development. The assessment activities included collection of soil and
groundwater samples from the Site. A summary of Site history and previous assessment activities
is included in Section 2.0, and the methods and results of the Brownfields assessment activities
are presented in Sections 3.0 and 4.0.

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2.0 Background Information

The Site was undeveloped wooded land in the earliest historical resource reviewed, a 1938 aerial
photograph. By 1951, the southeastern portion of the Site was developed for commercial purposes
and the northeastern portion of the Site was developed with a residence. The Woodward Warren
Company, a commercial refrigeration sales and service company, occupied the southeastern
portion of the Site between at least 1956 and 1963. By 1964, the southeastern portion of the Site
had transitioned into a gas station and automotive service facility. This portion of the Site was
occupied by various gas station operators between 1964 and 1988. The southeastern portion of
the Site has primarily been vacant since 1988, with periodic use for prefabricated building sales.

By 1962, the northern portion of the Site transitioned into an automotive salvage yard and later to
a used car dealership and automotive service and repair facility. Most recently, the northern
portion of the Site contained a vehicle rental facility, an automotive sales and service operation,
and various office tenants. Currently, automotive service and repair operations are conducted in
the far northern portion of the property (addressed at 3000-B Little Rock Road).

The southwestern portion of the Site was developed in 1974 with a commercial retail/office
building. Various commercial tenants have occupied the southwestern portion of the Site,
including a hair salon and landscape design company. Currently, a hair salon operates in the
southwest portion of the Site (addressed at 6128 Wilkinson Boulevard).

The former retail gas station and automotive repair facility located in the southeastern portion of
the Site (6100-6108 Wilkinson Boulevard) was formerly known as the Little Rock Crown Service
Station (1964) and Little Rock Phillips 66 Service Station (1969) (a.k.a. former Airport
Automotive) and operated from approximately 1964 through 1988. Soil and groundwater impacts
were identified at the subject Site as a result of the former Site gas station and automotive repair
operations. According to our review of previous reports, the following underground storage tanks
(USTs) were formerly present on the subject Site:

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• (3) 6,000-gallon gasoline USTs
• (1) 4,000-gallon diesel UST
• (1) 250-gallon heating oil UST
• (1) 250-gallon waste oil UST
• (2) approximately 1,000-gallon orphan gasoline USTs

Soil and groundwater impacts were initially discovered at the Site during the removal of a 4,000-
gallon diesel UST in December 1990 (Incident No. 6951). Subsequently, one 250-gallon heating
oil UST and three 6,000-gallon gasoline USTs were removed from the Site in March 1992. Free
phase product was observed in the tank basin at the time of removal and later free phase product
was observed in monitoring wells at the Site. Reportedly, approximately 900 gallons of product
and petroleum-impacted groundwater were removed from the tank basin and approximately 200
cubic yards of petroleum-impacted soil were removed for off-Site disposal at that time. Free phase
product recovery efforts were conducted at the Site between 1992 and 2015 and included hand
bailing, absorbent socks, and periodic aggressive fluid-vapor recovery (AFVR) events.

Based on the observance of free phase product and the presence of six water supply wells within
a 1,000 ft radius of the subject Site, DEQ classified the release incident as high risk. Municipal
water connections were provided to the six properties in 2003 and 2004 and DEQ subsequently
lowered the incident risk classification from high to intermediate risk.

Source area soil remedial activities were conducted including the excavation and off-Site disposal
of approximately 1,038 tons of petroleum-impacted soil from the former southern pump island in
January 2014, and approximately 1,040 tons of petroleum-impacted soil at the former eastern
pump island in August 2014. Excavation confirmation sample results indicated that two of the ten
soil samples contained petroleum-related compounds at concentrations above the DEQ Inactive
Hazardous Sites Branch (IHSB) Commercial/Industrial Health Based Preliminary Soil
Remediation Goals (PSRGs). The two soil samples with compounds above Commercial/Industrial
PSRGs were collected from the base of the excavation at the former southern pump island at depths
of 15 ft and 17 ft below ground surface (bgs). Based on the depth of the base samples, it is unlikely
that workers would disturb the petroleum-impacted soil during future redevelopment activities.

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A well network comprised of 20 monitoring wells and one recovery well were installed at the Site
between 1992 and 2015. H&H reviewed the most recent groundwater monitoring report for the
former Airport Automotive facility dated March 11, 2016. According to the report, benzene and
1,2-dichloroethane are present at concentrations exceeding DEQ Gross Contamination Levels
(GCLs) in the southeastern portion of the Site. Additionally, a background monitoring well located
near Little Rock Road indicates the southeastern portion of the Site has been impacted from a
release incident associated with the east adjacent and hydraulically upgradient Airport Express gas
station (Incident No. 36360). Free phase product has not been observed in monitoring wells at the
Site since October 2015.

Because extensive historical assessment activities have been conducted in the southern portion of
the Site associated with the former gas station, the Brownfields assessment activities reported
herein focused on the northern portion of the Site.

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3.0 Brownfields Assessment Activities

The assessment activities were performed in general accordance with DEQ – IHSB Guidelines for
Assessment and Cleanup dated October 2015, and most recent version of the US Environmental
Protection Agency (EPA) Region IV Science and Ecosystem Support (SESD) Field Branches
Quality System and Technical Procedures guidance.

As required by Mecklenburg County, H&H obtained a Subsurface Investigation Permit (SIP No.
70002495) from LUESA prior to installing temporary monitoring wells at the Site. Additionally,
H&H obtained a Monitoring Well Construction Permit (Permit No. WM0300948) from DEQ
Division of Water Resources prior to installing temporary monitoring wells at the Site. Copies of
the well construction permits are provided in Appendix A.

H&H conducted the Brownfields assessment activities at the Site on February 15 - 16, 2018. A
discussion of the methods, analytical results, and conclusions of the Brownfields assessment
activities are provided in the following sections.

3.1 Utility Clearance and Geophysical Survey

Prior to conducting the Brownfields assessment activities, H&H contacted North Carolina 811
One-Call, the public utility locating service, to mark subsurface utilities at the Site. H&H also
contracted a private utility locator, Sweetwater Utility Locating LLC (Sweetwater), to screen the
proposed boring locations for subgrade utilities using ground-penetrating radar (GPR) and
electromagnetic methods.

Sweetwater also performed a GPR survey to confirm the presence of a UST associated with an
apparent fill port observed along the west rear side of the former vehicle rental property building
(3012 Little Rock Road). The results of the GPR survey confirmed the presence and orientation
of the UST (see Figure 2). Sweetwater utilized a probe rod to determine that the top of the UST

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is approximately 1.5 ft bgs. The UST measures approximately 5.5 ft in length and approximately
4 ft in diameter. Therefore, the volume of the UST is estimated to be approximately 500-gallons.
Based on the location and estimated volume of the UST, the tank is likely a non-regulated heating
oil UST used to provide heat to the former vehicle rental building. The location of the UST is
presented on Figure 2.

3.2 Soil Assessment

H&H contracted with South Atlantic Environmental Drilling and Construction Company, Inc.
(SAEDACCO) of Fort Mill, South Carolina to perform subsurface drilling activities utilizing a
track-mounted GeoProbe® 7822DT direct push technology (DPT) drill rig. To assess the potential
for soil impact, H&H advanced five soil borings (HHSB-1 through HHSB-5) at the Site.

A summary of the soil boring locations is presented below:

• Soil borings HHSB-1, HHSB-3, and HHSB-4 were advanced in the vicinity of historical
automotive repair operations in the northeast portion of the Site.

• Soil borings HHSB-2 and HHSB-5 were advanced in the vicinity of historical automotive
salvage operations in the northern and east-central portions of the Site.

Soil borings HHSB-3 and HHSB-5 were advanced in areas of observed surface staining. The
locations of the soil borings are indicated on Figure 2.

Additionally, two background soil samples were be collected to assess naturally occurring
concentrations of metals in soil at the Site. The locations of the background soil borings were
determined in the field and were collected from areas that did not appear to have been impacted
from historical operations. The background soil borings were advanced in the undeveloped
wooded portion of the Site near the western Site boundary (see Figure 2).

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Soil samples were collected using either a decontaminated stainless-steel hand auger or by DPT
utilizing a decontaminated 5 ft long Macro-Core® sampler with disposable acetate liners.
Following collection, soil samples were described for lithologic purposes, inspected for the
presence of staining and odors, and field-screened for the presence of organic vapors with a
calibrated photo-ionization detector (PID). Based upon field screening results, H&H collected one
soil sample from each boring location for laboratory analysis. If there was field evidence of
potential impacts, then the sample exhibiting the greatest potential for impact was submitted for
laboratory analysis. If no evidence of potential impact was observed, then the soil sample for
laboratory analysis was collected from within the upper five ft of soil column which is the area
most likely to be disturbed during future redevelopment activities and/or most likely to pose a
direct contact exposure concern. Boring logs with lithologic descriptions and field screening
results are provided in Appendix B.

Upon collection, the soil samples were placed directly into dedicated laboratory-supplied sample
containers, labeled with the sample identification, date, and requested analysis, and placed in a
laboratory supplied cooler with ice. The samples were shipped via overnight courier to
TestAmerica Laboratories, Inc. (Test America) under chain-of-custody protocol for analysis of
volatile organic compounds (VOCs) by EPA Method 8260, semi-VOCs (SVOCs) by EPA Method
8270, and the Resource Conservation and Recovery Act (RCRA) metals by EPA Methods
6020/7471 plus hexavalent chromium by EPA Method 7196. The RCRA metals include arsenic,
barium, cadmium, chromium, lead, mercury, selenium, and silver. The background soil samples
were analyzed for RCRA metals plus hexavalent chromium by EPA Methods 6020/7471/7196
only.

3.3 Groundwater Assessment

To evaluate the potential for vapor intrusion into future Site buildings associated with groundwater
impacts and to evaluate groundwater conditions in the northern portion of the Site, three temporary
monitoring wells (HHTMW-1 through HHTMW-3) were installed and sampled for laboratory
analysis. Additionally, three existing permanent monitoring wells (labelled MW-3 through MW-

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5) in the northern portion of the Site were sampled for laboratory analysis. The temporary
monitoring wells and existing monitoring well locations are depicted on Figure 2, the soil boring
logs are presented in Appendix B, the well construction records are presented in Appendix C, and
groundwater sampling records are presented in Appendix D.

A summary of the temporary and existing monitoring well locations is presented below:

• Temporary well HHTMW-1 was installed west and topographically downgradient of the
UST to assess the potential for groundwater impacts from the former vehicle rental
property building UST.

• HHTMW-2 was installed in the north-central portion of the Site to assess the potential for
groundwater impacts associated with historical automotive operations.

• HHTMW-3 was installed west and topographically downgradient of the former automotive
salvage operations in the HHSB-2 soil boring.

• Existing monitoring well MW-3 is located east of the canopy structure in the vicinity of
historical automotive salvage and repair operations.

• Existing monitoring well MW-4 is located west and topographically downgradient of the
former automotive salvage building located in the east-central portion of the Site.

• Existing monitoring well MW-5 is located in the northwest portion of the Site, west and
topographically downgradient of historical and current automotive repair operations.

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The temporary monitoring wells were advanced with a track-mounted GeoProbe® 7822DT drill
rig utilizing DPT and hollow-stem auger (HSA) methods. The temporary monitoring wells were
constructed using 1-inch diameter PVC riser with a 10-ft section of PVC screen set to bracket the
shallow unconsolidated aquifer. At each temporary well, a sand filter pack was placed from the
bottom of the boring to approximately two ft above the top of the well screen and a hydrated
bentonite seal was placed from the top of the sand filter pack to the ground surface. Temporary
well riser pipe was secured with a locked expansion plug.

Upon installation, the temporary monitoring wells were allowed to equilibrate to static conditions
and a decontaminated electronic water level indicator was used to measure the depth to the water
table relative to the top of casing elevations in the temporary and existing monitoring wells. The
measured depths to water in the wells ranged from approximately 22 ft bgs in the northern portion
of the Site to approximately 18 ft bgs in the east-central portion of the Site.

Prior to sampling, H&H developed the temporary monitoring wells by removing at least three well
volumes using a peristaltic pump. After a minimum of three well volumes were purged,
development was considered complete when field parameters of pH, conductivity, and oxidation
reduction potential (ORP) stabilized and the water was visually clear.

Following development, H&H collected groundwater samples from the temporary and existing
monitoring wells for laboratory analysis on February 16, 2018 using low flow/low stress purging
techniques with a peristaltic pump and dedicated polyethylene tubing. The intake point of the
pump tubing was placed in the approximate mid-portion of the submerged portion of the well
screen. A water quality meter was utilized to collect measurements of pH, temperature, dissolved
oxygen, ORP, turbidity, and specific conductivity at 3 to 5-minute intervals during the purging
process. Purging was considered complete when field parameters stabilized, and turbidity was
less than 10 nephelometric turbidity units (NTUs). Final sample turbidity readings are presented
on Table 2 and were all less than the 10 NTU. Groundwater sampling records are provided in
Appendix D.

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The groundwater samples were collected directly into laboratory supplied sample containers using
the “soda straw” method to minimize volatile loss during sampling. The sample containers were
labeled with the sample identification, date, and requested analysis, placed in a laboratory supplied
cooler with ice, and shipped via overnight courier under standard chain-of-custody protocol to
TestAmerica for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and
RCRA metals by EPA Methods 6020/7471 plus hexavalent chromium by EPA Method 7196. The
temporary monitoring well and existing monitoring well locations were estimated using a sub-
meter GPS unit.

As requested by DEQ Brownfields, existing monitoring well MW-3 was gauged with an oil/water
interface probe to determine the potential presence of free product in the well. The presence of
free product was not detected in MW-3 during the gauging activities at the Site.

3.4 Quality Assurance/Quality Control

H&H utilized standard quality assurance/quality control (QA/QC) processes during the
Brownfields assessment activities. Non-dedicated sampling equipment, including DPT tooling,
the water level meter, and the hand auger, were decontaminated using Liquinox® detergent and
deionized water prior to and between each sampling location. H&H and SAEDACCO wore nitrile
gloves while handling samples, and the groundwater samples were collected using dedicated
tubing. Soil and groundwater samples were collected in laboratory-provided containers and placed
on ice immediately after collection.

For field and laboratory QA/QC purposes, H&H collected one duplicate soil sample from boring
HHSB-3 and one duplicate water sample from existing monitoring well MW-3. The duplicate
samples were analyzed for the same compounds as the parent samples. The results of analysis of
the duplicate samples are provided in Tables 2 and 3 and indicate good analytical repeatability for
the duplicate samples.

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Two laboratory-supplied trip blanks accompanied field personnel during groundwater sample
collection activities and the VOC sample containers during shipment. The trip blanks were
analyzed for VOCs by EPA Method 8260. There were no VOC detections in the trip blanks.

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4.0 Brownfields Assessment Results

The results of analysis of the groundwater samples are summarized in Table 2, and the results of
analysis of the soil samples are summarized in Table 3. Laboratory analytical data reports and
chain-of-custody records are included as Appendix E.

4.1 Soil Analytical Results

In Table 3, the soil laboratory analytical results are compared to the DEQ IHSB Residential and
Industrial/Commercial PSRGs dated February 2018. However, based upon the anticipated future
use of the Site for commercial purposes, the discussion below focuses on comparison of the data
to the Industrial/Commercial PSRGs. Metals concentrations were first compared to Site specific
background levels before comparison to the PSRGs.

VOCs
Analytical results indicate that no VOCs were detected in any of the soil samples at concentrations
exceeding Residential or Industrial/Commercial PSRGs.

SVOCs
Analytical results indicate that no SVOCs were detected in any of the soil samples at
concentrations exceeding laboratory reporting limits.

Metals
The results of the metals analyses indicate that concentrations of arsenic were detected above
laboratory reporting limits in each soil sample at concentrations ranging from 1.48 mg/kg to 4.13
mg/kg and generally within the range of Site-specific background concentrations (1.53 mg/kg to
1.91 mg/kg). One sample, HHSB-4, collected from north-central portion of the Site contained
arsenic at a concentration 4.13 mg/kg, which is above the Industrial/Commercial PSRG of 3 mg/kg
and slightly exceeds the background range. No other metals were detected above background and
Industrial/Commercial PSRGs.

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4.2 Groundwater Flow

The temporary and existing monitoring well top of casing elevations were determined using survey
methods to the nearest 0.01 ft and were referenced to an assumed datum of 100.00 ft at the
HHTMW-1 top of casing. A summary of temporary well construction, the existing monitoring
well construction data obtained from the well tags, and groundwater elevation data is presented on
Table 1.

A shallow unconsolidated aquifer potentiometric map generated from water table elevations is
provided as Figure 3. As indicated on the figure, the general direction of shallow groundwater
flow in the northern portion of the Site is to the west which is consistent with area topography.
Depth to groundwater ranges from approximately 22 ft bgs in the far northern portion of the Site
to approximately 18 ft bgs in the east-central portion of the Site.

4.3 Groundwater Analytical Results

Laboratory analytical results were compared to the 15A North Carolina Administrative Code
02L.0202 Groundwater Quality Standards (2L Standards) and the DEQ DWM Groundwater Vapor
Intrusion Screening Levels (VISLs).

VOCs
Analytical results indicate that no VOCs were detected at concentrations exceeding 2L Standards
in any of the groundwater samples.

VOCs
Analytical results indicate that no SVOCs were detected in any of the groundwater samples at
concentrations exceeding laboratory reporting limits.

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Metals
Analytical results indicate the metal chromium (total) was detected in one sample (MW-5) at a
concentration of 12.3 µg/L, which slightly exceeds the 2L Standard of 10 µg/L. Hexavalent
chromium was not detected in the MW-5 sample. Additionally, the results indicate that elevated
concentrations of barium were detected in temporary well HHTMW-1 (2,190 µg/L) and existing
monitoring well MW-3 (1,740 µg/L) and its associated duplicate sample (1,780 µg/L) at
concentrations exceeding the 2L Standard of 700 µg/L. HHTMW-1 and MW-3 are located in the
far northeastern portion of the Site.

As discussed in Section 3.3 above, field measurements of temperature, pH, conductivity, ORP,
and turbidity were collected during the groundwater sampling event. Turbidity of the HHTMW-
1 and MW-3 samples was less than 10 NTU indicating that the elevated concentrations of barium
are not likely associated with suspended sediment in the samples. However, the pH of the
HHTMW-1 and MW-3 samples was low and in the range of 4.5 pH standard units (SU) versus the
pH of the other samples collected at the Site (ranging from 5.9 SU to 6.6 SU). In addition,
dissolved oxygen concentrations were generally lower in samples HHTMW-1 (0.93 mg/L) and
MW-3 (0.39 mg/L) as compared to the other Site wells (ranging from 1.40 mg/L to 6.41 mg/L).
The presence of lower pH and lower dissolved oxygen concentrations can lead to mobilization of
naturally occurring metals such as barium in aquifer sediment. Although the source of the elevated
barium in groundwater in the northeastern portion of the Site is not conclusively known, it is
possible that naturally occurring low pH and low dissolved oxygen conditions may be present in
this area of Site and may be contributing to the elevated barium concentrations in samples
HHTMW-1 and MW-3. No other metals were detected at concentrations above 2L Standards.

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5.0 Summary and Conclusions

H&H completed Brownfields assessment activities at the Little Rock Road Brownfields property
located 6108, 6120, and 6128 Wilkinson Boulevard and 3000 and 3012 Little Rock Road in
Charlotte, Mecklenburg County, North Carolina. The Brownfields assessment activities were
conducted to evaluate potential risks associated with future Site development. Because extensive
historical assessment activities have been conducted in association with a former gas station in the
southern portion of the Site, the Brownfields assessment activities focused on the northern portion
of the Site. The Brownfields assessment activities included the collection of soil and groundwater
samples for laboratory analysis. Based on the results of the assessment activities, H&H concludes
the following:

Soil
• The analytical results of the soil samples indicate no VOCs or SVOCs were detected above
Residential PSRGs. One metal, arsenic, was detected in each sample at concentrations
above the Residential PSRG, but generally within the range of Site specific background
levels (except HHSB-4). Arsenic was detected in one sample, HHSB-4 (4.13 mg/kg),
located in the north-central portion of the Site, at a concentration slightly above background
and the Industrial/Commercial PSRG of 3 mg/kg.

Groundwater
• Shallow groundwater flow in the northern portion of the Site is to the west which is
consistent with Site topography. Depth to groundwater ranges from approximately 22 ft
bgs in the far northern portion of the Site to approximately 18 ft bgs in the east-central
portion of the Site.

• The results of the groundwater assessment indicate that no VOCs or SVOCs were detected
in groundwater from the monitoring wells in the northern portion of the Site. The metal
chromium (total) was detected in one sample located in the far northern portion of the Site
at a concentration slightly above the 2L Standard. In addition, elevated concentrations of

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barium were detected in two groundwater samples collected in the far northeastern portion
of the Site at concentrations above the 2L Standard. Although the source of the barium is
not known, it is possible that naturally occurring low pH conditions and low dissolved
oxygen conditions may be present in this area of Site, which mobilized naturally occurring
barium in the shallow unconsolidated aquifer.

• Based on the lack of VOCs detected above vapor intrusion screening levels in groundwater
from wells in the northern portion of the Site, vapor intrusion is not a significant concern
for future buildings in the northern portion of the Site.

Figures
TITLE
PROJECT
SITE LOCATION MAP
LITTLE ROCK ROAD BROWNFIELDS SITE
WILKINSON BOULEVARD & LITTLE ROCK ROAD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
1-30-2018 0
1RKI-008
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
DERITA, NORTH CAROLINA 1996
SITE
LITTLE ROCK ROADMW-3 MW-3A
RW-1
MW-6
MW-8
MW-5
MW-8A
7
4
12
5
118
SW-2
SW-1 SW-4
SW-3
BOTTOM-1
BOTTOM-2
BASE-1
SW-1
SW-2
BASE-2
MW-10D
MW-11A
MW-21
MW-8B
MW-3B
MW-18
MW-16DMW-17
MW-12
MW-9
MW-19
MW-15A
MW-20
MW-22D
MW-6A
MW-5
MW-3
HHSB-1/
HHTMW-1
HHSB-3MW-4
HHSB-4
HHTMW-2HHSB-2/
HHTMW-3
HHSB-5
BKG-2
BKG-1
REVISION NO. 0
JOB NO. RKI-008
DATE: 3-27-18
FIGURE NO. 2
LITTLE ROCK ROAD BROWNFIELDS SITE
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
PROPOSED BUILDING FOOTPRINT
UNDERGROUND STORAGE TANK
MONITORING WELL LOCATION
ABANDONED MONITORING WELL
LOCATION
TEMPORARY MONITORING WELL
TEMPORARY MONITORING WELL/
SOIL BORING LOCATION (H&H; 2/2018)
SOIL BORING LOCATION (H&H; 2/2018)
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
WILKINSON BOULEVARD
AIRPORT EXPRESS
FORMER VEHICLE RENTAL
(VACANT)
FORMER OFFICE/ USED CAR SALES
(VACANT)
AUTO SERVICE & REPAIR
FORMER AUTO SERVICE & REPAIR
(VACANT)
CANOPY
FORMER GAS STATION
HAIR
SALON
S:\AAA-Master Projects\RK Investments (RKI)\RKI-008 RK Investments Little Rock Road\Figures\Site Map.dwg, FIG 2, 3/27/2018 3:06:50 PM, zbarlow
LITTLE ROCK ROADMW-3 MW-3A
RW-1
MW-6
MW-8
MW-5
MW-8A7273 747572737475MW-10D
MW-11A
MW-21
MW-8B
MW-3B
MW-18
MW-16DMW-17
MW-12
MW-9
MW-19
MW-15A
MW-20
MW-22D
MW-6A
MW-5
MW-3
HHTMW-1
MW-4
HHTMW-2HHTMW-3
(76.00)
(73.70)(70.06)
(75.10)
(71.83)
(70.60)71REVISION NO. 0
JOB NO. RKI-008
DATE: 2-27-18
FIGURE NO. 3
LITTLE ROCK ROAD BROWNFIELDS SITE
CHARLOTTE, NORTH CAROLINA
SHALLOW GROUNDWATER
POTENTIOMETRIC MAP
LEGEND
SITE PROPERTY BOUNDARY
MONITORING WELL LOCATION
ABANDONED MONITORING WELL
LOCATION
TEMPORARY MONITORING WELL
GROUNDWATER ELEVATION (FT)
GROUNDWATER ELEVATION CONTOUR
(FT)
INFERRED GROUNDWATER FLOW
DIRECTION
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
WILKINSON BOULEVARD
75
(76.00)
NOTES:
1. TOP OF CASING ELEVATIONS WERE MEASURED ON
2/19/18. HHTMW-1 WAS ASSIGNED AN ASSUMED TOP
OF CASING ELEVATION OF 100.00 FT.
2. HHTMW-1 THROUGH HHTMW-3, AND MW-3 THROUGH
MW-5 GAUGED ON 2/19/18.S:\AAA-Master Projects\RK Investments (RKI)\RKI-008 RK Investments Little Rock Road\Figures\Shallow GW Gradient Map.dwg, FIG 3, 2/27/2018 11:03:23 AM, zbarlow
Tables
Table 1
Summary of Well Construction and Groundwater Elevation Data
Little Rock Road
Charlotte, North Carolina
H&H Job No. RKI-008
Well ID
Well
Diameter
(inches)
TOC
Elevation
(feet)
Total Depth
(feet below
TOC)
Screen Length
(feet)
Static Depth to
Groundwater
(feet below TOC)
Groundwater
Elevation
(feet below TOC)
HHTMW-1 1 100.00 28 10 24.00 76.00
HHTMW-2 1 97.19 28 10 23.49 73.70
HHTMW-3 1 92.78 29 10 22.72 70.06
MW-3**2 97.04 32 20 21.94 75.10
MW-4**2 89.75 35 20 17.92 71.83MW-5**2 92.78 35 20 22.18 70.60
Notes:
TMW = temporary monitoring well; MW = permanent monitoring well; TOC = top of casing
Depth to groundwater measurements collected on February 19, 2018
Elevations are approximate and are referenced to an arbitrary datum of 100 ft at HHTMW-1
**Monitoring well installed by others in October 2012; well construction information obtained from well tag
S:\AAA-Master Projects\RK Investments (RKI)\RKI-008 RK Investments Little Rock Road\Tables\Analytical Data Tables
5/17/2017
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2
Summary of Groundwater Analytical Results
Little Rock Road
Charlotte, North Carolina
H&H Job No. RKI-008
Area of Concern
Underground Storage
Tank
Historical Automotive
Repair Downgradient Downgradient
Sample ID HHTMW-1 HHTMW-2 HHTMW-3 MW-4 MW-5 Trip Blank 1 Trip Blank 2
Date 2/16/2018 2/16/2018 2/16/2018 2/16/2018 2/16/2018 2/16/2018 2/16/2018 ----
VOCs (8260) µg/LChloroform 70 8.1 36 1.68 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00Methyl tert-Butyl Ether (MTBE)20 4,500 20,000 1.29 1.29 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00 <1.00
SVOCs (8270) µg/L ------BRL BRL BRL BRL BRL BRL BRL
Metals (6020/7471) µg/L
Arsenic 10 NS NS <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0
Barium 700 NS NS 2,190 62.4 7.08 1,740 1,780 22.2 52.1Cadmium2NSNS<1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0Total Chromium 10 NS NS <2.0 <2.0 7.08 <2.0 <2.0 9.0 12.3Hexavalent Chromium NS NS NS <10 <10 <10 <10 <10 <10 <10
Trivalent Chromium**NS NS NS <2.0 <2.0 7.08 <2.0 <2.0 9.0 12.3Lead15NSNS5.98 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0Mercury1NSNS<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0Selenium20NSNS<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0Silver20NSNS<2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.0
Turbidity (NTU)------7.67 7.00 3.11 6.96 2.74
pH (SU)------4.51 5.95 6.57 5.94 5.85
Dissolved Oxygen ------0.93 4.67 6.41 1.40 3.01
Notes:
1) North Carolina 15A NCAC 02L Groundwater Standards (2L Standards) (April 2013)2) North Carolina Department of Environmental Quality (DEQ) - Division of Waste Management (DWM) Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) (October 2017)3) DEQ DWM Non-Residential Vapor Intrusion GWSLs (February 2018)** Total Chromium - Hexavalent Chromium = Trivalent Chromium
Only compounds detected in at least one sample shown aboveConcentrations are reported in micrograms per liter (µg/L)
Laboratory analytical methods are shown in parenthesesBold values exceed a 2L Standard (April 2013)
-- = Not Applicable; NS = Not Specified; VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds
BRL = below laboratory reporting limit; NTU = Nephelometric Turbidity Unit; SU = pH Standard Unit
North Carolina 2L
Groundwater
Standards (1)MW-3 / DUPLICATE-1
4.62
0.39
1.98
Historical Automotive Salvage/RepairNon-Residential
Vapor Intrusion
Groundwater
Screening
Levels (3)
Residential Vapor
Intrusion
Groundwater
Screening
Levels (2)
S:\AAA-Master Projects\RK Investments (RKI)\RKI-008 RK Investments Little Rock Road\Tables\Analytical Data Tables3/27/2018
Table 2 (Page 1 of 1)
Hart & Hickman, PC
Table 3
Summary of Soil Analytical Results
Little Rock Road
Charlotte, North Carolina
H&H Job No. RKI-008
Area of Concern
Historical
Automotive
Repair
Historical
Automotive
Salvage
Historical
Automotive
Repair
Surface
Staining
Sample ID BKG-1 BKG-2 HHSB-1 HHSB-2 HHSB-4 HHSB-5
Date 2/16/2018 2/16/2018 02/15/2018 02/15/2018 02/16/2018 02/16/2018
Depth (ft bgs)1-2 1-2 1-2 1-2 1-2 0-1
VOCs (8260) mg/kgAcetone 12,000 140,000 NA NA <0.0435 0.0574 0.0529 0.0671 <0.0432 0.07161,2,4-Trimethylbenzene 63 370 NA NA <0.00174 <0.00184 0.00311 <0.00161 <0.00173 <0.00182
SVOCs (8270) mg/kg ----NA NA BRL BRL BRL BRL BRL BRL
Metals (6020/7471/7196) mg/kg
Arsenic 0.68 3.0 1.91 1.53 1.48 2.68 2.77 2.64 4.13 2.79
Barium 3,100 47,000 99.9 15.2 5.03 28.2 35.5 53.1 26.6 42.7
Cadmium 14 200 <0.517 <0.534 <0.592 <0.596 <0.566 <0.557 <0.554 <0.490
Chromium (Total)NS NS 24.1 24.5 9.40 F1 24.8 20.2 30.6 30.2 21.0
Hexavalent Chromium 0.31 6.5 <5.98 <5.59 <6.15 <6.13 <6.62 <6.15 <6.36 <5.83
Trivalent Chromium**23,000 350,000 24.1 24.5 9.40 F1 24.8 20.2 30.6 30.2 21.0Lead40080017.9 6.61 5.21 9.44 21.9 12.6 11.6 23.5
Mercury 2.3 9.7 <0.117 <0.112 <0.126 <0.121 <0.132 <0.121 <0.127 <0.114
Selenium 78 1,200 <0.517 <0.534 <0.592 <0.596 0.815 <0.557 1.33 <0.490
Silver 78 1,200 <0.517 <0.534 <0.592 <0.596 <0.566 <0.557 <0.554 <0.490
Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB)
Health Based Preliminary Soil Remediation Goals (PSRGs) (February 2018)
** = Total Chromium - Hexavalent Chromium = Trivalent Chromium
Soil concentrations are reported in milligrams per kilogram (mg/kg)
Laboratory analytical methods are shown in parentheses
F1 = laboratory matrix spike and/or matrix spike duplicate recovery was outside acceptable threshold
VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds
NA = not analyzed; NS = not specified; BRL = below laboratory reporting limit; ft bgs = feet below ground surface; -- = not applicable
0-1
02/15/2018
Industrial/
Commercial
PSRGs (1)
(mg/kg)
Residential
PSRGs (1)
(mg/kg)
Screening Criteria Site Specific Background
HHSB-3 / DUPLICATE-2
Surface Staining
S:\AAA-Master Projects\RK Investments (RKI)\RKI-008 RK Investments Little Rock Road\Tables\Analytical Data Tables
3/27/2018
Table 3 (Page 1 of 1)Hart & Hickman, PC
Appendix A
Well Construction Permits
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________ 
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

Agent
2/8/2018
70002495
RK Investments Charlotte, LLC
704-366-8689
3800 Pomfret Lane
Charlotte NC 28211
Hart and Hickman, PC
Brett Lawerence
7048874601
2923 South Tryon Street
Charlotte NC 28203
Little Rock Road Brownfields
05536936
3012 LITTLE ROCK RD
CHARLOTTE NC 28214
Appendix B
Boring Logs
NOTES: Hole precleared to 5 ft using hand auger, DPT to 10 ft, and HSA 28 ft.
generated using LogitEasy.com
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
WELL LOG
Well No.
Page:
HHSB-1/HHTMW-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/15/18 9:30
2/15/18 10:00
SAEDACCO
DPT/HSA
Geoprobe 7822DT
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
28.0
8.25
HA/DPT
23.0
24.0
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
28.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips/Bent. Chips
No. 2 Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
GR
GR
GR
GR
GR
DP
12:46
12:46
12:47
12:48
12:48
0.50
1.00
1.00
1.00
1.00
4.00
(0') Concrete
(0.5') Lean CLAY with sand (CL); few fine-medium sand, some silt, medium plasticity,
soft, reddish-brown, with white and gray brown mottling, slightly moist
(3') SILT with sand (MH); few fine-medium sand, some clay, medium plasticity,
soft, reddish-brown, with grayish brown and white modeling, slightly moist
(7') SILT (MH); some clay, medium plasticity, medium stiff, light
reddish-brown, with tan to white and brown modeling, slightly moist
(14') SILT (MH); some clay, medium stiff, moist, dark reddish-brown
(20') SILT (MH); some clay, soft, wet, light grayish brown
(25') SILT (MH); some clay, soft, saturated, Light grayish brown
(28') Boring terminated
1.8
1.3
1.1
2.5
3.4
3.3
3.9
4.1
6.8
3.9
3.8
5.9
4.0
4.8
4.8
4.8
4.3
HHSB-1
0
5
10
15
20
25
30
NOTES: Hole precleared to 5 ft using hand auger, DPT to 15 ft, and HSA 28 ft.
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
WELL LOG
Well No.
Page:
HHTMW-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/15/2018 11:35
2/15/2018 13:05
SAEDACCO
DPT/HSA
Geoprobe 7822DT
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
28.0
8.25
DPT
17.0
23.5
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
28.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips/Bent. Chips
No. 2 sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
GR
GR
GR
GR
GR
DP
DP
12:07
12:08
12:08
12:08
12:09
12:09
1.00
1.00
1.00
1.00
1.00
5.00
4.00
(0') Clayey GRAVEL (GC); dense, moist, dark reddish-gray, gravel parking lot fill
(0.5') Lean CLAY with sand (CL); few fine-medium sand, medium plasticity, medium
stiff, moist, dark reddish-brown
(1.5') Lean CLAY with sand (CL); few medium sand, some silt, medium plasticity,
medium stiff, reddish-brown, slightly moist
(6') Elastic SILT (MH); some clay, low plasticity, stiff, dry, reddish-black
(8') As Above: dark reddish-brown, slightly moist
(11') Lean CLAY (CL); medium plasticity, soft, moist, dark reddish-brown, with white
and black mottling
(14.5') Lean CLAY (CL); some silt, medium plasticity, very soft, wet, light
reddish-brown
(19') Lean CLAY with sand (CL); trace fine-medium sand, some silt, medium
plasticity, very soft, saturated, light grayish brown
(28') Boring terminated
1.3
1.9
2.0
1.7
2.1
2.9
3.9
4.0
2.2
3.3
3.2
2.5
1.4
2.4
2.3
1.9
0
5
10
15
20
25
30
NOTES: Hole precleared to 5 ft using hand auger, DPT to 15 ft, and HSA to 29 ft bgs.
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
WELL LOG
Well No.
Page:
HHSB-2/HHTMW-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/15/18 14:40
2/15/18 15:25
SAEDACCO
DPT/HSA
Geoprobe 7822DT
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
29.0
8.25
HA/DPT
19.0
23.5
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
27.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips/Bent. Chips
No. 2 Sand
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
30
GR
GR
GR
GR
GR
DP
DP
1.00
1.00
1.00
1.00
1.00
5.00
5.00
(0') Sandy lean CLAY (CL); trace coarse gravel, little medium sand, some silt,
medium plasticity, medium stiff, moist, reddish-brown, with some dark brown organic
matter and leaves
(1') Lean CLAY (CL); trace fine-medium sand, some silt, medium plasticity, soft,
reddish-brown, slightly moist
(5') As Above: very stiff, with white mottling
(8') SILT (MH); some clay, medium stiff, moist, dark reddish-brown, white and black
mottling
(13') SILT (ML); trace fine-coarse gravel, few fine-medium sand, few clay, soft, moist,
Light grayish yellow brown
(19') Lean CLAY (CL); little silt, medium plasticity, very soft, wet, light grayish brown
(25') Fat CLAY (CH); few silt, high plasticity, very soft, wet, light grayish brown
(29') Boring terminated
7.5
12.1
12.9
13.8
13.2
15.2
18.2
12.1
14.9
6.7
16.1
25.6
18.4
8.9
11.2
9.5
HHSB-2 &SB-DUP
0
5
10
15
20
25
30
NOTES: Hole precleared to 5.0 ft bgs using hand auger, DPT to 10 ft bgs.
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
BORING LOG
Boring No.
Page:
HHSB-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/15/2018 16:40
2/15/2018 16:50
SAEDACCO
HA/DPT
Geoprobe 7822 DT
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
10.0
3.25
HA/DPT
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
GR
GR
GR
GR
GR
DP
1.00
1.00
1.00
1.00
1.00
5.00
(0') Lean CLAY with gravel (CL); few fine-coarse gravel, few fine-medium sand, some
silt, medium plasticity, medium stiff, moist, very dark reddish-brown, dark grayish black
staining
(0.33') Asphalt
(0.66') Lean CLAY with sand (CL); trace fine-coarse gravel, few fine-medium sand,
some silt, medium plasticity, medium stiff, reddish-brown, slightly moist
(4') SILT (MH); some clay, low plasticity, stiff, dry, reddish-brown
(6') As Above: medium stiff, slightly moist
(7.5') SILT (MH); some clay, low plasticity, soft, moist, dark reddish-brown, with black
and white mottling
(10') Boring terminated
12.8
11.2
7.8
5.9
7.6
7.1
8.1
7.4
HHSB-3 (0.5-1.0)
0
5
10
15
NOTES:
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
BORING LOG
Boring No.
Page:
HHSB-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/16/2018 9:05
2/16/2018 9:20
SAEDACCO
HA/DPT
Geoprobe 7822 DT
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
10.0
3.25
HA/DPT
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
GR
DP
GR
GR
GR
GR
09:28
09:28
09:28
09:28
09:29
09:29
1.00
5.00
1.00
1.00
1.00
1.00
(0') Asphalt
(0.5') SILT with sand (MH); few fine-coarse gravel, few fine-medium sand, some clay,
stiff, dark reddish-brown, slightly moist
(2.5') As Above: reddish brown
(5') Elastic SILT (MH); some clay, stiff, reddish-brown, with white mottling, slightly moist
(10') Boring terminated
2.3
1.9
1.4
1.1
2.5
3.9
3.3
4.2
HHSB-4 (1-2)
0
5
10
15
NOTES:
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
BORING LOG
Boring No.
Page:
HHSB-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/16/2018 8:15
2/16/2018 8:35
SAEDACCO
HA/DPT
Geoprobe 7822 DT
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
10.0
3.25
HA/DPT
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
GR
GR
GR
GR
GR
DP
1.00
1.00
1.00
1.00
1.00
5.00
(0') SILT (MH); little fine-coarse gravel, few medium sand, some clay, stiff, dark
reddish-brown
(1') As Above: medium brown to orange
(4') Lean CLAY with sand (CL); little fine-medium sand, some silt, medium plasticity,
stiff, dry, reddish-brown
(8.5') As Above: slightly moist
(10') Boring terminated
0.3
0.3
0.2
0.8
4.4
4.6
4.8
4.4
HHSB-5 (0-1)
0
5
10
15
NOTES:
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
BORING LOG
Boring No.
Page:
BKG-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/16/18 10:15
2/16/18 10:30
SAEDACCO
Other
Hand Auger
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR
GR
13:07
13:10
1.00
1.00 (0') ORGANIC SOIL (OH); trace fine-medium sand, few silt, mostly clay, high plasticity,
soft, moist, light reddish brown
(1') As Above: few roots
(2') Boring terminated
16.5
7.8 BKG-1
0
1
2
3
4
5
NOTES:
Client:
Project:
Address:
RK Investments
RKI.008
3000 Little Rock Road, Charlotte, NC
BORING LOG
Boring No.
Page:
BKG-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/16/18 10:45
2/16/18 11:00
SAEDACCO
Other
Hand Auger
Daniel Gaspari
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
2.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
GR
GR
13:18
13:18
1.00
1.00
(0') ORGANIC SOIL (OH); trace fine-medium sand, mostly clay, high plasticity, soft,
moist, light reddish brown, black mottling composed of organic matter, some roots
(1') As Above: no black organic matter, few roots
(2') Boring terminated
11.6
31.2
BKG-2
0
1
2
3
4
5
Appendix C
Well Construction Records
Appendix D
Groundwater Sampling Records
Appendix E
Laboratory Analytical Reports
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-146552-1
TestAmerica Sample Delivery Group: RKI.008
Client Project/Site: Little Rock Road Brownfields
Revision: 1
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Brett Lawrence
Authorized for release by:
2/26/2018 5:58:33 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Little Rock Road Brownfields
TestAmerica Job ID: 490-146552-1
SDG: RKI.008
Page 2 of 64 TestAmerica Nashville2/26/2018 (Rev. 1)
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .57
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .60
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .61
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .62
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Sample Summary
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-146552-1 MW-3 Water 02/16/18 12:50 02/17/18 09:25
490-146552-2 MW-4 Water 02/16/18 14:30 02/17/18 09:25
490-146552-3 MW-5 Water 02/16/18 16:40 02/17/18 09:25
490-146552-4 HHTMW-1 Water 02/16/18 19:10 02/17/18 09:25
490-146552-5 HHTMW-2 Water 02/16/18 18:25 02/17/18 09:25
490-146552-6 HHTMW-3 Water 02/16/18 15:40 02/17/18 09:25
490-146552-7 Duplicate-1 Water 02/16/18 13:30 02/17/18 09:25
490-146552-8 Trip Blank 1 Water 02/16/18 00:01 02/17/18 09:25
490-146552-9 Trip Blank 2 Water 02/16/18 00:01 02/17/18 09:25
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146552-1
Project/Site: Little Rock Road Brownfields SDG: RKI.008
Job ID: 490-146552-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-146552-1
REVISED REPORT: Revised to change the semple ID of 490-146552-7 from MW-6 to Duplicate-1 at the client's request. This report
replaces the one generated on 02/23/18 @ 1242.
Comments
No additional comments.
Receipt
The samples were received on 2/17/2018 9:25 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 2 coolers at receipt time were 3.1º C and 4.7º C.
GC/MS VOA
Method 8260B: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for analytical batch 490-496192
recovered outside control limits for the following analytes: Bromomethane and Dichlorodifluoromethane. These analytes were biased
high in the LCS and were not detected in the associated samples; therefore, the data have been reported.
Method 8260B: The method blank for analytical batch 490-496192 contained 1,2,3-Trichlorobenzene above the reporting limit (RL). None
of the samples associated with this method blank contained the target compound; therefore, re-extraction and/or re-analysis of samples
were not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: The laboratory control sample (LCS) and / or laboratory control sample duplicate (LCSD) for preparation batch
490-496205 and analytical batch 490-496272 recovered outside control limits for the following analytes: 4,6-Dinitro-2-methylphenol,
Acenaphthylene, Benzo[b]fluoranthene, Carbazole, Fluoranthene, Phenanthrene, Pentachlorophenol and n-Nitrosodiphenylamine(as
diphenylamine). These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have
been reported.
Method 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-496205 and analytical batch 490-496272.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
Method 7196A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 490-496732 were outside control limits.
Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was
within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Qualifiers
GC/MS VOA
Qualifier Description
4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
Qualifier
F2 MS/MSD RPD exceeds control limits
*LCS or LCSD is outside acceptance limits.
GC/MS Semi VOA
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
General Chemistry
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-1Client Sample ID: MW-3
Matrix: WaterDate Collected: 02/16/18 12:50
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 21:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 21:38 1BenzeneND
1.00 ug/L 02/17/18 21:38 1BromobenzeneND
1.00 ug/L 02/17/18 21:38 1BromochloromethaneND
1.00 ug/L 02/17/18 21:38 1BromodichloromethaneND
1.00 ug/L 02/17/18 21:38 1BromoformND
1.00 ug/L 02/17/18 21:38 1BromomethaneND *
50.0 ug/L 02/17/18 21:38 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 21:38 1Carbon disulfide ND
1.00 ug/L 02/17/18 21:38 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 21:38 1ChlorobenzeneND
1.00 ug/L 02/17/18 21:38 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 21:38 1ChloroethaneND
1.00 ug/L 02/17/18 21:38 1ChloroformND
1.00 ug/L 02/17/18 21:38 1ChloromethaneND
1.00 ug/L 02/17/18 21:38 12-Chlorotoluene ND
1.00 ug/L 02/17/18 21:38 14-Chlorotoluene ND
1.00 ug/L 02/17/18 21:38 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 21:38 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 21:38 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 21:38 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 21:38 1DibromomethaneND
1.00 ug/L 02/17/18 21:38 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 21:38 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 21:38 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 21:38 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 21:38 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 21:38 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 21:38 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 21:38 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 21:38 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 21:38 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 21:38 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 21:38 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 21:38 1Diisopropyl ether ND
1.00 ug/L 02/17/18 21:38 1EthylbenzeneND
2.00 ug/L 02/17/18 21:38 1HexachlorobutadieneND
10.0 ug/L 02/17/18 21:38 12-Hexanone ND
1.00 ug/L 02/17/18 21:38 1IsopropylbenzeneND
5.00 ug/L 02/17/18 21:38 1Methylene Chloride ND
10.0 ug/L 02/17/18 21:38 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 21:38 1Methyl tert-butyl ether ND
5.00 ug/L 02/17/18 21:38 1NaphthaleneND
1.00 ug/L 02/17/18 21:38 1n-Butylbenzene ND
1.00 ug/L 02/17/18 21:38 1N-Propylbenzene ND
1.00 ug/L 02/17/18 21:38 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 21:38 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 21:38 1StyreneND
1.00 ug/L 02/17/18 21:38 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-1Client Sample ID: MW-3
Matrix: WaterDate Collected: 02/16/18 12:50
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 21:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 21:38 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 21:38 1TetrachloroetheneND
1.00 ug/L 02/17/18 21:38 1TolueneND
1.00 ug/L 02/17/18 21:38 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 21:38 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 21:38 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 21:38 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 21:38 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 21:38 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 21:38 1TrichloroetheneND
1.00 ug/L 02/17/18 21:38 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 21:38 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 21:38 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 21:38 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 21:38 1Vinyl chloride ND
3.00 ug/L 02/17/18 21:38 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)100 70-130 02/17/18 21:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)100 02/17/18 21:38 170-130
1,2-Dichloroethane-d4 (Surr)104 02/17/18 21:38 170-130
Toluene-d8 (Surr)92 02/17/18 21:38 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1AcenaphthyleneND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1AnthraceneND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1Benzo[a]anthracene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1Benzo[a]pyrene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1Benzo[b]fluoranthene ND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1Benzo[g,h,i]perylene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1Benzo[k]fluoranthene ND *
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Bis(2-chloroethoxy)methane ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Bis(2-chloroethyl)ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1bis (2-chloroisopropyl) ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Bis(2-ethylhexyl) phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 14-Bromophenyl phenyl ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Butyl benzyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1CarbazoleND *
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 14-Chloroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 14-Chloro-3-methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12-Chloronaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12-Chlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 14-Chlorophenyl phenyl ether ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1ChryseneND
17.2 ug/L 02/17/18 16:28 02/19/18 16:26 1CresolsND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1Dibenz(a,h)anthracene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1DibenzofuranND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-1Client Sample ID: MW-3
Matrix: WaterDate Collected: 02/16/18 12:50
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 11,3-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 11,4-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 13,3'-Dichlorobenzidine ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12,4-Dichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Diethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12,4-Dimethylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Dimethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Di-n-butyl phthalate ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:26 14,6-Dinitro-2-methylphenol ND *
21.6 ug/L 02/17/18 16:28 02/19/18 16:26 12,4-Dinitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12,4-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12,6-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1Di-n-octyl phthalate ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1FluorantheneND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1FluoreneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1HexachlorobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1HexachlorobutadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1HexachlorocyclopentadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1HexachloroethaneND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1Indeno[1,2,3-cd]pyrene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1IsophoroneND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 11-Methylnaphthalene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 12-Methylnaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12-Methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 13 & 4 Methylphenol ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1NaphthaleneND
21.6 ug/L 02/17/18 16:28 02/19/18 16:26 12-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:26 13-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:26 14-Nitroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1NitrobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12-Nitrophenol ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:26 14-Nitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1N-Nitrosodi-n-propylamine ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1n-Nitrosodiphenylamine(as
diphenylamine)
ND *
21.6 ug/L 02/17/18 16:28 02/19/18 16:26 1PentachlorophenolND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1PhenanthreneND *
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 1PhenolND
1.72 ug/L 02/17/18 16:28 02/19/18 16:26 1PyreneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 11,2,4-Trichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12,4,5-Trichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:26 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)40 29-120 02/17/18 16:28 02/19/18 16:26 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)35 02/17/18 16:28 02/19/18 16:26 110-120
Nitrobenzene-d5 (Surr)40 02/17/18 16:28 02/19/18 16:26 127-120
Phenol-d5 (Surr)25 02/17/18 16:28 02/19/18 16:26 110-120
Terphenyl-d14 (Surr)52 02/17/18 16:28 02/19/18 16:26 113-120
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-1Client Sample ID: MW-3
Matrix: WaterDate Collected: 02/16/18 12:50
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)50 10-120 02/17/18 16:28 02/19/18 16:26 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00200 mg/L 02/19/18 15:26 02/20/18 12:22 1Barium1.74
0.00100 mg/L 02/19/18 15:26 02/20/18 12:22 1CadmiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:22 1ChromiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:22 1LeadND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:22 1SeleniumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:22 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 19:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND F1 0.0100 mg/L 02/17/18 10:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-2Client Sample ID: MW-4
Matrix: WaterDate Collected: 02/16/18 14:30
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 22:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 22:05 1BenzeneND
1.00 ug/L 02/17/18 22:05 1BromobenzeneND
1.00 ug/L 02/17/18 22:05 1BromochloromethaneND
1.00 ug/L 02/17/18 22:05 1BromodichloromethaneND
1.00 ug/L 02/17/18 22:05 1BromoformND
1.00 ug/L 02/17/18 22:05 1BromomethaneND *
50.0 ug/L 02/17/18 22:05 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 22:05 1Carbon disulfide ND
1.00 ug/L 02/17/18 22:05 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 22:05 1ChlorobenzeneND
1.00 ug/L 02/17/18 22:05 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 22:05 1ChloroethaneND
1.00 ug/L 02/17/18 22:05 1ChloroformND
1.00 ug/L 02/17/18 22:05 1ChloromethaneND
1.00 ug/L 02/17/18 22:05 12-Chlorotoluene ND
1.00 ug/L 02/17/18 22:05 14-Chlorotoluene ND
1.00 ug/L 02/17/18 22:05 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 22:05 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 22:05 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 22:05 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 22:05 1DibromomethaneND
1.00 ug/L 02/17/18 22:05 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:05 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:05 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:05 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 22:05 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 22:05 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 22:05 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 22:05 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 22:05 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 22:05 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 22:05 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 22:05 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 22:05 1Diisopropyl ether ND
1.00 ug/L 02/17/18 22:05 1EthylbenzeneND
2.00 ug/L 02/17/18 22:05 1HexachlorobutadieneND
10.0 ug/L 02/17/18 22:05 12-Hexanone ND
1.00 ug/L 02/17/18 22:05 1IsopropylbenzeneND
5.00 ug/L 02/17/18 22:05 1Methylene Chloride ND
10.0 ug/L 02/17/18 22:05 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 22:05 1Methyl tert-butyl ether ND
5.00 ug/L 02/17/18 22:05 1NaphthaleneND
1.00 ug/L 02/17/18 22:05 1n-Butylbenzene ND
1.00 ug/L 02/17/18 22:05 1N-Propylbenzene ND
1.00 ug/L 02/17/18 22:05 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 22:05 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 22:05 1StyreneND
1.00 ug/L 02/17/18 22:05 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-2Client Sample ID: MW-4
Matrix: WaterDate Collected: 02/16/18 14:30
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 22:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 22:05 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 22:05 1TetrachloroetheneND
1.00 ug/L 02/17/18 22:05 1TolueneND
1.00 ug/L 02/17/18 22:05 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 22:05 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 22:05 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 22:05 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 22:05 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 22:05 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 22:05 1TrichloroetheneND
1.00 ug/L 02/17/18 22:05 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 22:05 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 22:05 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 22:05 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 22:05 1Vinyl chloride ND
3.00 ug/L 02/17/18 22:05 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)102 70-130 02/17/18 22:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)102 02/17/18 22:05 170-130
1,2-Dichloroethane-d4 (Surr)104 02/17/18 22:05 170-130
Toluene-d8 (Surr)92 02/17/18 22:05 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1AcenaphthyleneND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1AnthraceneND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1Benzo[a]anthracene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1Benzo[a]pyrene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1Benzo[b]fluoranthene ND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1Benzo[g,h,i]perylene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1Benzo[k]fluoranthene ND *
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Bis(2-chloroethoxy)methane ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Bis(2-chloroethyl)ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1bis (2-chloroisopropyl) ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Bis(2-ethylhexyl) phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 14-Bromophenyl phenyl ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Butyl benzyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1CarbazoleND *
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 14-Chloroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 14-Chloro-3-methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12-Chloronaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12-Chlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 14-Chlorophenyl phenyl ether ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1ChryseneND
17.2 ug/L 02/17/18 16:28 02/19/18 16:47 1CresolsND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1Dibenz(a,h)anthracene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1DibenzofuranND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-2Client Sample ID: MW-4
Matrix: WaterDate Collected: 02/16/18 14:30
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 11,3-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 11,4-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 13,3'-Dichlorobenzidine ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12,4-Dichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Diethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12,4-Dimethylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Dimethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Di-n-butyl phthalate ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:47 14,6-Dinitro-2-methylphenol ND *
21.6 ug/L 02/17/18 16:28 02/19/18 16:47 12,4-Dinitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12,4-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12,6-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1Di-n-octyl phthalate ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1FluorantheneND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1FluoreneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1HexachlorobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1HexachlorobutadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1HexachlorocyclopentadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1HexachloroethaneND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1Indeno[1,2,3-cd]pyrene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1IsophoroneND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 11-Methylnaphthalene ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 12-Methylnaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12-Methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 13 & 4 Methylphenol ND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1NaphthaleneND
21.6 ug/L 02/17/18 16:28 02/19/18 16:47 12-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:47 13-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:47 14-Nitroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1NitrobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12-Nitrophenol ND
21.6 ug/L 02/17/18 16:28 02/19/18 16:47 14-Nitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1N-Nitrosodi-n-propylamine ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1n-Nitrosodiphenylamine(as
diphenylamine)
ND *
21.6 ug/L 02/17/18 16:28 02/19/18 16:47 1PentachlorophenolND *
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1PhenanthreneND *
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 1PhenolND
1.72 ug/L 02/17/18 16:28 02/19/18 16:47 1PyreneND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 11,2,4-Trichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12,4,5-Trichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 16:47 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)51 29-120 02/17/18 16:28 02/19/18 16:47 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)46 02/17/18 16:28 02/19/18 16:47 110-120
Nitrobenzene-d5 (Surr)56 02/17/18 16:28 02/19/18 16:47 127-120
Phenol-d5 (Surr)33 02/17/18 16:28 02/19/18 16:47 110-120
Terphenyl-d14 (Surr)62 02/17/18 16:28 02/19/18 16:47 113-120
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-2Client Sample ID: MW-4
Matrix: WaterDate Collected: 02/16/18 14:30
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)62 10-120 02/17/18 16:28 02/19/18 16:47 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00200 mg/L 02/19/18 15:26 02/20/18 12:07 1Barium0.0222
0.00100 mg/L 02/19/18 15:26 02/20/18 12:07 1CadmiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:07 1Chromium0.00900
0.00200 mg/L 02/19/18 15:26 02/20/18 12:07 1LeadND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:07 1SeleniumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:07 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 19:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 0.0100 mg/L 02/17/18 10:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-3Client Sample ID: MW-5
Matrix: WaterDate Collected: 02/16/18 16:40
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 22:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 22:31 1BenzeneND
1.00 ug/L 02/17/18 22:31 1BromobenzeneND
1.00 ug/L 02/17/18 22:31 1BromochloromethaneND
1.00 ug/L 02/17/18 22:31 1BromodichloromethaneND
1.00 ug/L 02/17/18 22:31 1BromoformND
1.00 ug/L 02/17/18 22:31 1BromomethaneND *
50.0 ug/L 02/17/18 22:31 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 22:31 1Carbon disulfide ND
1.00 ug/L 02/17/18 22:31 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 22:31 1ChlorobenzeneND
1.00 ug/L 02/17/18 22:31 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 22:31 1ChloroethaneND
1.00 ug/L 02/17/18 22:31 1ChloroformND
1.00 ug/L 02/17/18 22:31 1ChloromethaneND
1.00 ug/L 02/17/18 22:31 12-Chlorotoluene ND
1.00 ug/L 02/17/18 22:31 14-Chlorotoluene ND
1.00 ug/L 02/17/18 22:31 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 22:31 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 22:31 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 22:31 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 22:31 1DibromomethaneND
1.00 ug/L 02/17/18 22:31 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:31 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:31 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:31 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 22:31 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 22:31 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 22:31 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 22:31 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 22:31 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 22:31 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 22:31 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 22:31 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 22:31 1Diisopropyl ether ND
1.00 ug/L 02/17/18 22:31 1EthylbenzeneND
2.00 ug/L 02/17/18 22:31 1HexachlorobutadieneND
10.0 ug/L 02/17/18 22:31 12-Hexanone ND
1.00 ug/L 02/17/18 22:31 1IsopropylbenzeneND
5.00 ug/L 02/17/18 22:31 1Methylene Chloride ND
10.0 ug/L 02/17/18 22:31 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 22:31 1Methyl tert-butyl ether ND
5.00 ug/L 02/17/18 22:31 1NaphthaleneND
1.00 ug/L 02/17/18 22:31 1n-Butylbenzene ND
1.00 ug/L 02/17/18 22:31 1N-Propylbenzene ND
1.00 ug/L 02/17/18 22:31 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 22:31 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 22:31 1StyreneND
1.00 ug/L 02/17/18 22:31 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-3Client Sample ID: MW-5
Matrix: WaterDate Collected: 02/16/18 16:40
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 22:31 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 22:31 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 22:31 1TetrachloroetheneND
1.00 ug/L 02/17/18 22:31 1TolueneND
1.00 ug/L 02/17/18 22:31 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 22:31 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 22:31 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 22:31 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 22:31 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 22:31 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 22:31 1TrichloroetheneND
1.00 ug/L 02/17/18 22:31 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 22:31 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 22:31 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 22:31 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 22:31 1Vinyl chloride ND
3.00 ug/L 02/17/18 22:31 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)103 70-130 02/17/18 22:31 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)95 02/17/18 22:31 170-130
1,2-Dichloroethane-d4 (Surr)102 02/17/18 22:31 170-130
Toluene-d8 (Surr)105 02/17/18 22:31 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1AcenaphthyleneND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1AnthraceneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1Benzo[a]anthracene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1Benzo[a]pyrene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1Benzo[b]fluoranthene ND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1Benzo[g,h,i]perylene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1Benzo[k]fluoranthene ND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Bis(2-chloroethoxy)methane ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Bis(2-chloroethyl)ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1bis (2-chloroisopropyl) ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Bis(2-ethylhexyl) phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 14-Bromophenyl phenyl ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Butyl benzyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1CarbazoleND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 14-Chloroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 14-Chloro-3-methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12-Chloronaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12-Chlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 14-Chlorophenyl phenyl ether ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1ChryseneND
17.2 ug/L 02/17/18 16:28 02/19/18 17:09 1CresolsND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1Dibenz(a,h)anthracene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1DibenzofuranND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-3Client Sample ID: MW-5
Matrix: WaterDate Collected: 02/16/18 16:40
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 11,3-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 11,4-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 13,3'-Dichlorobenzidine ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12,4-Dichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Diethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12,4-Dimethylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Dimethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Di-n-butyl phthalate ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:09 14,6-Dinitro-2-methylphenol ND *
21.6 ug/L 02/17/18 16:28 02/19/18 17:09 12,4-Dinitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12,4-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12,6-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1Di-n-octyl phthalate ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1FluorantheneND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1FluoreneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1HexachlorobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1HexachlorobutadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1HexachlorocyclopentadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1HexachloroethaneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1Indeno[1,2,3-cd]pyrene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1IsophoroneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 11-Methylnaphthalene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 12-Methylnaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12-Methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 13 & 4 Methylphenol ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1NaphthaleneND
21.6 ug/L 02/17/18 16:28 02/19/18 17:09 12-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:09 13-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:09 14-Nitroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1NitrobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12-Nitrophenol ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:09 14-Nitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1N-Nitrosodi-n-propylamine ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1n-Nitrosodiphenylamine(as
diphenylamine)
ND *
21.6 ug/L 02/17/18 16:28 02/19/18 17:09 1PentachlorophenolND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1PhenanthreneND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 1PhenolND
1.72 ug/L 02/17/18 16:28 02/19/18 17:09 1PyreneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 11,2,4-Trichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12,4,5-Trichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:09 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)65 29-120 02/17/18 16:28 02/19/18 17:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)59 02/17/18 16:28 02/19/18 17:09 110-120
Nitrobenzene-d5 (Surr)68 02/17/18 16:28 02/19/18 17:09 127-120
Phenol-d5 (Surr)41 02/17/18 16:28 02/19/18 17:09 110-120
Terphenyl-d14 (Surr)76 02/17/18 16:28 02/19/18 17:09 113-120
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-3Client Sample ID: MW-5
Matrix: WaterDate Collected: 02/16/18 16:40
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)76 10-120 02/17/18 16:28 02/19/18 17:09 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:25 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00200 mg/L 02/19/18 15:26 02/20/18 12:25 1Barium0.0521
0.00100 mg/L 02/19/18 15:26 02/20/18 12:25 1CadmiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:25 1Chromium0.0123
0.00200 mg/L 02/19/18 15:26 02/20/18 12:25 1LeadND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:25 1SeleniumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:25 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 19:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 0.0100 mg/L 02/17/18 10:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-4Client Sample ID: HHTMW-1
Matrix: WaterDate Collected: 02/16/18 19:10
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 22:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 22:58 1BenzeneND
1.00 ug/L 02/17/18 22:58 1BromobenzeneND
1.00 ug/L 02/17/18 22:58 1BromochloromethaneND
1.00 ug/L 02/17/18 22:58 1BromodichloromethaneND
1.00 ug/L 02/17/18 22:58 1BromoformND
1.00 ug/L 02/17/18 22:58 1BromomethaneND *
50.0 ug/L 02/17/18 22:58 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 22:58 1Carbon disulfide ND
1.00 ug/L 02/17/18 22:58 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 22:58 1ChlorobenzeneND
1.00 ug/L 02/17/18 22:58 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 22:58 1ChloroethaneND
1.00 ug/L 02/17/18 22:58 1Chloroform1.68
1.00 ug/L 02/17/18 22:58 1ChloromethaneND
1.00 ug/L 02/17/18 22:58 12-Chlorotoluene ND
1.00 ug/L 02/17/18 22:58 14-Chlorotoluene ND
1.00 ug/L 02/17/18 22:58 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 22:58 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 22:58 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 22:58 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 22:58 1DibromomethaneND
1.00 ug/L 02/17/18 22:58 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:58 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:58 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 22:58 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 22:58 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 22:58 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 22:58 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 22:58 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 22:58 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 22:58 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 22:58 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 22:58 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 22:58 1Diisopropyl ether ND
1.00 ug/L 02/17/18 22:58 1EthylbenzeneND
2.00 ug/L 02/17/18 22:58 1HexachlorobutadieneND
10.0 ug/L 02/17/18 22:58 12-Hexanone ND
1.00 ug/L 02/17/18 22:58 1IsopropylbenzeneND
5.00 ug/L 02/17/18 22:58 1Methylene Chloride ND
10.0 ug/L 02/17/18 22:58 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 22:58 1Methyl tert-butyl ether 1.29
5.00 ug/L 02/17/18 22:58 1NaphthaleneND
1.00 ug/L 02/17/18 22:58 1n-Butylbenzene ND
1.00 ug/L 02/17/18 22:58 1N-Propylbenzene ND
1.00 ug/L 02/17/18 22:58 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 22:58 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 22:58 1StyreneND
1.00 ug/L 02/17/18 22:58 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-4Client Sample ID: HHTMW-1
Matrix: WaterDate Collected: 02/16/18 19:10
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 22:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 22:58 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 22:58 1TetrachloroetheneND
1.00 ug/L 02/17/18 22:58 1TolueneND
1.00 ug/L 02/17/18 22:58 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 22:58 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 22:58 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 22:58 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 22:58 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 22:58 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 22:58 1TrichloroetheneND
1.00 ug/L 02/17/18 22:58 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 22:58 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 22:58 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 22:58 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 22:58 1Vinyl chloride ND
3.00 ug/L 02/17/18 22:58 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)98 70-130 02/17/18 22:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)96 02/17/18 22:58 170-130
1,2-Dichloroethane-d4 (Surr)100 02/17/18 22:58 170-130
Toluene-d8 (Surr)92 02/17/18 22:58 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1AcenaphthyleneND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1AnthraceneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1Benzo[a]anthracene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1Benzo[a]pyrene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1Benzo[b]fluoranthene ND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1Benzo[g,h,i]perylene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1Benzo[k]fluoranthene ND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Bis(2-chloroethoxy)methane ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Bis(2-chloroethyl)ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1bis (2-chloroisopropyl) ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Bis(2-ethylhexyl) phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 14-Bromophenyl phenyl ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Butyl benzyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1CarbazoleND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 14-Chloroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 14-Chloro-3-methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12-Chloronaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12-Chlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 14-Chlorophenyl phenyl ether ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1ChryseneND
17.2 ug/L 02/17/18 16:28 02/19/18 17:30 1CresolsND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1Dibenz(a,h)anthracene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1DibenzofuranND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-4Client Sample ID: HHTMW-1
Matrix: WaterDate Collected: 02/16/18 19:10
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 11,3-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 11,4-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 13,3'-Dichlorobenzidine ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12,4-Dichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Diethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12,4-Dimethylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Dimethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Di-n-butyl phthalate ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:30 14,6-Dinitro-2-methylphenol ND *
21.6 ug/L 02/17/18 16:28 02/19/18 17:30 12,4-Dinitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12,4-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12,6-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1Di-n-octyl phthalate ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1FluorantheneND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1FluoreneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1HexachlorobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1HexachlorobutadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1HexachlorocyclopentadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1HexachloroethaneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1Indeno[1,2,3-cd]pyrene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1IsophoroneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 11-Methylnaphthalene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 12-Methylnaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12-Methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 13 & 4 Methylphenol ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1NaphthaleneND
21.6 ug/L 02/17/18 16:28 02/19/18 17:30 12-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:30 13-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:30 14-Nitroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1NitrobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12-Nitrophenol ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:30 14-Nitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1N-Nitrosodi-n-propylamine ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1n-Nitrosodiphenylamine(as
diphenylamine)
ND *
21.6 ug/L 02/17/18 16:28 02/19/18 17:30 1PentachlorophenolND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1PhenanthreneND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 1PhenolND
1.72 ug/L 02/17/18 16:28 02/19/18 17:30 1PyreneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 11,2,4-Trichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12,4,5-Trichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:30 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)57 29-120 02/17/18 16:28 02/19/18 17:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)49 02/17/18 16:28 02/19/18 17:30 110-120
Nitrobenzene-d5 (Surr)57 02/17/18 16:28 02/19/18 17:30 127-120
Phenol-d5 (Surr)36 02/17/18 16:28 02/19/18 17:30 110-120
Terphenyl-d14 (Surr)63 02/17/18 16:28 02/19/18 17:30 113-120
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-4Client Sample ID: HHTMW-1
Matrix: WaterDate Collected: 02/16/18 19:10
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)65 10-120 02/17/18 16:28 02/19/18 17:30 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00200 mg/L 02/19/18 15:26 02/20/18 12:34 1Barium2.19
0.00100 mg/L 02/19/18 15:26 02/20/18 12:34 1CadmiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:34 1ChromiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:34 1Lead0.00598
0.00200 mg/L 02/19/18 15:26 02/20/18 12:34 1SeleniumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:34 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 19:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 0.0100 mg/L 02/17/18 10:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-5Client Sample ID: HHTMW-2
Matrix: WaterDate Collected: 02/16/18 18:25
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 23:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 23:24 1BenzeneND
1.00 ug/L 02/17/18 23:24 1BromobenzeneND
1.00 ug/L 02/17/18 23:24 1BromochloromethaneND
1.00 ug/L 02/17/18 23:24 1BromodichloromethaneND
1.00 ug/L 02/17/18 23:24 1BromoformND
1.00 ug/L 02/17/18 23:24 1BromomethaneND *
50.0 ug/L 02/17/18 23:24 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 23:24 1Carbon disulfide ND
1.00 ug/L 02/17/18 23:24 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 23:24 1ChlorobenzeneND
1.00 ug/L 02/17/18 23:24 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 23:24 1ChloroethaneND
1.00 ug/L 02/17/18 23:24 1ChloroformND
1.00 ug/L 02/17/18 23:24 1ChloromethaneND
1.00 ug/L 02/17/18 23:24 12-Chlorotoluene ND
1.00 ug/L 02/17/18 23:24 14-Chlorotoluene ND
1.00 ug/L 02/17/18 23:24 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 23:24 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 23:24 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 23:24 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 23:24 1DibromomethaneND
1.00 ug/L 02/17/18 23:24 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 23:24 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 23:24 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 23:24 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 23:24 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 23:24 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 23:24 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 23:24 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 23:24 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 23:24 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 23:24 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 23:24 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 23:24 1Diisopropyl ether ND
1.00 ug/L 02/17/18 23:24 1EthylbenzeneND
2.00 ug/L 02/17/18 23:24 1HexachlorobutadieneND
10.0 ug/L 02/17/18 23:24 12-Hexanone ND
1.00 ug/L 02/17/18 23:24 1IsopropylbenzeneND
5.00 ug/L 02/17/18 23:24 1Methylene Chloride ND
10.0 ug/L 02/17/18 23:24 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 23:24 1Methyl tert-butyl ether 1.29
5.00 ug/L 02/17/18 23:24 1NaphthaleneND
1.00 ug/L 02/17/18 23:24 1n-Butylbenzene ND
1.00 ug/L 02/17/18 23:24 1N-Propylbenzene ND
1.00 ug/L 02/17/18 23:24 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 23:24 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 23:24 1StyreneND
1.00 ug/L 02/17/18 23:24 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-5Client Sample ID: HHTMW-2
Matrix: WaterDate Collected: 02/16/18 18:25
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 23:24 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 23:24 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 23:24 1TetrachloroetheneND
1.00 ug/L 02/17/18 23:24 1TolueneND
1.00 ug/L 02/17/18 23:24 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 23:24 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 23:24 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 23:24 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 23:24 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 23:24 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 23:24 1TrichloroetheneND
1.00 ug/L 02/17/18 23:24 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 23:24 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 23:24 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 23:24 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 23:24 1Vinyl chloride ND
3.00 ug/L 02/17/18 23:24 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)104 70-130 02/17/18 23:24 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)104 02/17/18 23:24 170-130
1,2-Dichloroethane-d4 (Surr)109 02/17/18 23:24 170-130
Toluene-d8 (Surr)97 02/17/18 23:24 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1AcenaphthyleneND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1AnthraceneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1Benzo[a]anthracene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1Benzo[a]pyrene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1Benzo[b]fluoranthene ND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1Benzo[g,h,i]perylene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1Benzo[k]fluoranthene ND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Bis(2-chloroethoxy)methane ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Bis(2-chloroethyl)ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1bis (2-chloroisopropyl) ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Bis(2-ethylhexyl) phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 14-Bromophenyl phenyl ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Butyl benzyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1CarbazoleND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 14-Chloroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 14-Chloro-3-methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12-Chloronaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12-Chlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 14-Chlorophenyl phenyl ether ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1ChryseneND
17.2 ug/L 02/17/18 16:28 02/19/18 17:52 1CresolsND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1Dibenz(a,h)anthracene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1DibenzofuranND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-5Client Sample ID: HHTMW-2
Matrix: WaterDate Collected: 02/16/18 18:25
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 11,3-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 11,4-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 13,3'-Dichlorobenzidine ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12,4-Dichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Diethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12,4-Dimethylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Dimethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Di-n-butyl phthalate ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:52 14,6-Dinitro-2-methylphenol ND *
21.6 ug/L 02/17/18 16:28 02/19/18 17:52 12,4-Dinitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12,4-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12,6-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1Di-n-octyl phthalate ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1FluorantheneND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1FluoreneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1HexachlorobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1HexachlorobutadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1HexachlorocyclopentadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1HexachloroethaneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1Indeno[1,2,3-cd]pyrene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1IsophoroneND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 11-Methylnaphthalene ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 12-Methylnaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12-Methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 13 & 4 Methylphenol ND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1NaphthaleneND
21.6 ug/L 02/17/18 16:28 02/19/18 17:52 12-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:52 13-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:52 14-Nitroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1NitrobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12-Nitrophenol ND
21.6 ug/L 02/17/18 16:28 02/19/18 17:52 14-Nitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1N-Nitrosodi-n-propylamine ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1n-Nitrosodiphenylamine(as
diphenylamine)
ND *
21.6 ug/L 02/17/18 16:28 02/19/18 17:52 1PentachlorophenolND *
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1PhenanthreneND *
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 1PhenolND
1.72 ug/L 02/17/18 16:28 02/19/18 17:52 1PyreneND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 11,2,4-Trichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12,4,5-Trichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 17:52 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)51 29-120 02/17/18 16:28 02/19/18 17:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)45 02/17/18 16:28 02/19/18 17:52 110-120
Nitrobenzene-d5 (Surr)55 02/17/18 16:28 02/19/18 17:52 127-120
Phenol-d5 (Surr)33 02/17/18 16:28 02/19/18 17:52 110-120
Terphenyl-d14 (Surr)60 02/17/18 16:28 02/19/18 17:52 113-120
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-5Client Sample ID: HHTMW-2
Matrix: WaterDate Collected: 02/16/18 18:25
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)61 10-120 02/17/18 16:28 02/19/18 17:52 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00200 mg/L 02/19/18 15:26 02/20/18 12:37 1Barium0.0624
0.00100 mg/L 02/19/18 15:26 02/20/18 12:37 1CadmiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:37 1ChromiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:37 1LeadND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:37 1SeleniumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:37 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 20:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 0.0100 mg/L 02/17/18 10:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-6Client Sample ID: HHTMW-3
Matrix: WaterDate Collected: 02/16/18 15:40
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 23:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 23:51 1BenzeneND
1.00 ug/L 02/17/18 23:51 1BromobenzeneND
1.00 ug/L 02/17/18 23:51 1BromochloromethaneND
1.00 ug/L 02/17/18 23:51 1BromodichloromethaneND
1.00 ug/L 02/17/18 23:51 1BromoformND
1.00 ug/L 02/17/18 23:51 1BromomethaneND *
50.0 ug/L 02/17/18 23:51 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 23:51 1Carbon disulfide ND
1.00 ug/L 02/17/18 23:51 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 23:51 1ChlorobenzeneND
1.00 ug/L 02/17/18 23:51 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 23:51 1ChloroethaneND
1.00 ug/L 02/17/18 23:51 1ChloroformND
1.00 ug/L 02/17/18 23:51 1ChloromethaneND
1.00 ug/L 02/17/18 23:51 12-Chlorotoluene ND
1.00 ug/L 02/17/18 23:51 14-Chlorotoluene ND
1.00 ug/L 02/17/18 23:51 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 23:51 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 23:51 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 23:51 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 23:51 1DibromomethaneND
1.00 ug/L 02/17/18 23:51 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 23:51 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 23:51 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 23:51 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 23:51 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 23:51 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 23:51 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 23:51 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 23:51 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 23:51 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 23:51 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 23:51 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 23:51 1Diisopropyl ether ND
1.00 ug/L 02/17/18 23:51 1EthylbenzeneND
2.00 ug/L 02/17/18 23:51 1HexachlorobutadieneND
10.0 ug/L 02/17/18 23:51 12-Hexanone ND
1.00 ug/L 02/17/18 23:51 1IsopropylbenzeneND
5.00 ug/L 02/17/18 23:51 1Methylene Chloride ND
10.0 ug/L 02/17/18 23:51 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 23:51 1Methyl tert-butyl ether ND
5.00 ug/L 02/17/18 23:51 1NaphthaleneND
1.00 ug/L 02/17/18 23:51 1n-Butylbenzene ND
1.00 ug/L 02/17/18 23:51 1N-Propylbenzene ND
1.00 ug/L 02/17/18 23:51 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 23:51 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 23:51 1StyreneND
1.00 ug/L 02/17/18 23:51 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-6Client Sample ID: HHTMW-3
Matrix: WaterDate Collected: 02/16/18 15:40
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 23:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 23:51 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 23:51 1TetrachloroetheneND
1.00 ug/L 02/17/18 23:51 1TolueneND
1.00 ug/L 02/17/18 23:51 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 23:51 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 23:51 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 23:51 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 23:51 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 23:51 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 23:51 1TrichloroetheneND
1.00 ug/L 02/17/18 23:51 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 23:51 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 23:51 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 23:51 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 23:51 1Vinyl chloride ND
3.00 ug/L 02/17/18 23:51 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)104 70-130 02/17/18 23:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)106 02/17/18 23:51 170-130
1,2-Dichloroethane-d4 (Surr)106 02/17/18 23:51 170-130
Toluene-d8 (Surr)99 02/17/18 23:51 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1AcenaphthyleneND *
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1AnthraceneND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1Benzo[a]anthracene ND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1Benzo[a]pyrene ND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1Benzo[b]fluoranthene ND *
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1Benzo[g,h,i]perylene ND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1Benzo[k]fluoranthene ND *
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Bis(2-chloroethoxy)methane ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Bis(2-chloroethyl)ether ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1bis (2-chloroisopropyl) ether ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Bis(2-ethylhexyl) phthalate ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 14-Bromophenyl phenyl ether ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Butyl benzyl phthalate ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1CarbazoleND *
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 14-Chloroaniline ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 14-Chloro-3-methylphenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12-Chloronaphthalene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12-Chlorophenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 14-Chlorophenyl phenyl ether ND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1ChryseneND
17.5 ug/L 02/17/18 16:28 02/19/18 18:13 1CresolsND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1Dibenz(a,h)anthracene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1DibenzofuranND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-6Client Sample ID: HHTMW-3
Matrix: WaterDate Collected: 02/16/18 15:40
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 11,3-Dichlorobenzene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 11,4-Dichlorobenzene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 13,3'-Dichlorobenzidine ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12,4-Dichlorophenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Diethyl phthalate ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12,4-Dimethylphenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Dimethyl phthalate ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Di-n-butyl phthalate ND
21.9 ug/L 02/17/18 16:28 02/19/18 18:13 14,6-Dinitro-2-methylphenol ND *
21.9 ug/L 02/17/18 16:28 02/19/18 18:13 12,4-Dinitrophenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12,4-Dinitrotoluene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12,6-Dinitrotoluene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1Di-n-octyl phthalate ND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1FluorantheneND *
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1FluoreneND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1HexachlorobenzeneND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1HexachlorobutadieneND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1HexachlorocyclopentadieneND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1HexachloroethaneND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1Indeno[1,2,3-cd]pyrene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1IsophoroneND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 11-Methylnaphthalene ND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 12-Methylnaphthalene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12-Methylphenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 13 & 4 Methylphenol ND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1NaphthaleneND
21.9 ug/L 02/17/18 16:28 02/19/18 18:13 12-Nitroaniline ND
21.9 ug/L 02/17/18 16:28 02/19/18 18:13 13-Nitroaniline ND
21.9 ug/L 02/17/18 16:28 02/19/18 18:13 14-Nitroaniline ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1NitrobenzeneND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12-Nitrophenol ND
21.9 ug/L 02/17/18 16:28 02/19/18 18:13 14-Nitrophenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1N-Nitrosodi-n-propylamine ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1n-Nitrosodiphenylamine(as
diphenylamine)
ND *
21.9 ug/L 02/17/18 16:28 02/19/18 18:13 1PentachlorophenolND *
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1PhenanthreneND *
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 1PhenolND
1.75 ug/L 02/17/18 16:28 02/19/18 18:13 1PyreneND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 11,2,4-Trichlorobenzene ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12,4,5-Trichlorophenol ND
8.77 ug/L 02/17/18 16:28 02/19/18 18:13 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)52 29-120 02/17/18 16:28 02/19/18 18:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)43 02/17/18 16:28 02/19/18 18:13 110-120
Nitrobenzene-d5 (Surr)55 02/17/18 16:28 02/19/18 18:13 127-120
Phenol-d5 (Surr)31 02/17/18 16:28 02/19/18 18:13 110-120
Terphenyl-d14 (Surr)55 02/17/18 16:28 02/19/18 18:13 113-120
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-6Client Sample ID: HHTMW-3
Matrix: WaterDate Collected: 02/16/18 15:40
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)57 10-120 02/17/18 16:28 02/19/18 18:13 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00200 mg/L 02/19/18 15:26 02/20/18 12:40 1Barium0.0343
0.00100 mg/L 02/19/18 15:26 02/20/18 12:40 1CadmiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:40 1Chromium0.00708
0.00200 mg/L 02/19/18 15:26 02/20/18 12:40 1LeadND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:40 1SeleniumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:40 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 20:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 0.0100 mg/L 02/17/18 10:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-7Client Sample ID: Duplicate-1
Matrix: WaterDate Collected: 02/16/18 13:30
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/18/18 00:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/18/18 00:18 1BenzeneND
1.00 ug/L 02/18/18 00:18 1BromobenzeneND
1.00 ug/L 02/18/18 00:18 1BromochloromethaneND
1.00 ug/L 02/18/18 00:18 1BromodichloromethaneND
1.00 ug/L 02/18/18 00:18 1BromoformND
1.00 ug/L 02/18/18 00:18 1BromomethaneND *
50.0 ug/L 02/18/18 00:18 12-Butanone (MEK)ND
1.00 ug/L 02/18/18 00:18 1Carbon disulfide ND
1.00 ug/L 02/18/18 00:18 1Carbon tetrachloride ND
1.00 ug/L 02/18/18 00:18 1ChlorobenzeneND
1.00 ug/L 02/18/18 00:18 1ChlorodibromomethaneND
1.00 ug/L 02/18/18 00:18 1ChloroethaneND
1.00 ug/L 02/18/18 00:18 1ChloroformND
1.00 ug/L 02/18/18 00:18 1ChloromethaneND
1.00 ug/L 02/18/18 00:18 12-Chlorotoluene ND
1.00 ug/L 02/18/18 00:18 14-Chlorotoluene ND
1.00 ug/L 02/18/18 00:18 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/18/18 00:18 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/18/18 00:18 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/18/18 00:18 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/18/18 00:18 1DibromomethaneND
1.00 ug/L 02/18/18 00:18 11,2-Dichlorobenzene ND
1.00 ug/L 02/18/18 00:18 11,3-Dichlorobenzene ND
1.00 ug/L 02/18/18 00:18 11,4-Dichlorobenzene ND
1.00 ug/L 02/18/18 00:18 1DichlorodifluoromethaneND *
1.00 ug/L 02/18/18 00:18 11,1-Dichloroethane ND
1.00 ug/L 02/18/18 00:18 11,2-Dichloroethane ND
1.00 ug/L 02/18/18 00:18 11,1-Dichloroethene ND
1.00 ug/L 02/18/18 00:18 11,2-Dichloroethene, Total ND
1.00 ug/L 02/18/18 00:18 11,2-Dichloropropane ND
1.00 ug/L 02/18/18 00:18 11,3-Dichloropropane ND
1.00 ug/L 02/18/18 00:18 12,2-Dichloropropane ND
1.00 ug/L 02/18/18 00:18 11,1-Dichloropropene ND
2.00 ug/L 02/18/18 00:18 1Diisopropyl ether ND
1.00 ug/L 02/18/18 00:18 1EthylbenzeneND
2.00 ug/L 02/18/18 00:18 1HexachlorobutadieneND
10.0 ug/L 02/18/18 00:18 12-Hexanone ND
1.00 ug/L 02/18/18 00:18 1IsopropylbenzeneND
5.00 ug/L 02/18/18 00:18 1Methylene Chloride ND
10.0 ug/L 02/18/18 00:18 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/18/18 00:18 1Methyl tert-butyl ether ND
5.00 ug/L 02/18/18 00:18 1NaphthaleneND
1.00 ug/L 02/18/18 00:18 1n-Butylbenzene ND
1.00 ug/L 02/18/18 00:18 1N-Propylbenzene ND
1.00 ug/L 02/18/18 00:18 1p-Isopropyltoluene ND
1.00 ug/L 02/18/18 00:18 1sec-Butylbenzene ND
1.00 ug/L 02/18/18 00:18 1StyreneND
1.00 ug/L 02/18/18 00:18 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-7Client Sample ID: Duplicate-1
Matrix: WaterDate Collected: 02/16/18 13:30
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/18/18 00:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/18/18 00:18 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/18/18 00:18 1TetrachloroetheneND
1.00 ug/L 02/18/18 00:18 1TolueneND
1.00 ug/L 02/18/18 00:18 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/18/18 00:18 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/18/18 00:18 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/18/18 00:18 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/18/18 00:18 11,1,1-Trichloroethane ND
1.00 ug/L 02/18/18 00:18 11,1,2-Trichloroethane ND
1.00 ug/L 02/18/18 00:18 1TrichloroetheneND
1.00 ug/L 02/18/18 00:18 1TrichlorofluoromethaneND
1.00 ug/L 02/18/18 00:18 11,2,3-Trichloropropane ND
1.00 ug/L 02/18/18 00:18 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/18/18 00:18 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/18/18 00:18 1Vinyl chloride ND
3.00 ug/L 02/18/18 00:18 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)98 70-130 02/18/18 00:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)95 02/18/18 00:18 170-130
1,2-Dichloroethane-d4 (Surr)103 02/18/18 00:18 170-130
Toluene-d8 (Surr)96 02/18/18 00:18 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1AcenaphthyleneND *
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1AnthraceneND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1Benzo[a]anthracene ND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1Benzo[a]pyrene ND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1Benzo[b]fluoranthene ND *
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1Benzo[g,h,i]perylene ND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1Benzo[k]fluoranthene ND *
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Bis(2-chloroethoxy)methane ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Bis(2-chloroethyl)ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1bis (2-chloroisopropyl) ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Bis(2-ethylhexyl) phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 14-Bromophenyl phenyl ether ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Butyl benzyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1CarbazoleND *
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 14-Chloroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 14-Chloro-3-methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12-Chloronaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12-Chlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 14-Chlorophenyl phenyl ether ND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1ChryseneND
17.2 ug/L 02/17/18 16:28 02/19/18 18:34 1CresolsND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1Dibenz(a,h)anthracene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1DibenzofuranND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-7Client Sample ID: Duplicate-1
Matrix: WaterDate Collected: 02/16/18 13:30
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 11,3-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 11,4-Dichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 13,3'-Dichlorobenzidine ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12,4-Dichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Diethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12,4-Dimethylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Dimethyl phthalate ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Di-n-butyl phthalate ND
21.6 ug/L 02/17/18 16:28 02/19/18 18:34 14,6-Dinitro-2-methylphenol ND *
21.6 ug/L 02/17/18 16:28 02/19/18 18:34 12,4-Dinitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12,4-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12,6-Dinitrotoluene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1Di-n-octyl phthalate ND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1FluorantheneND *
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1FluoreneND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1HexachlorobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1HexachlorobutadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1HexachlorocyclopentadieneND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1HexachloroethaneND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1Indeno[1,2,3-cd]pyrene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1IsophoroneND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 11-Methylnaphthalene ND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 12-Methylnaphthalene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12-Methylphenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 13 & 4 Methylphenol ND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1NaphthaleneND
21.6 ug/L 02/17/18 16:28 02/19/18 18:34 12-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 18:34 13-Nitroaniline ND
21.6 ug/L 02/17/18 16:28 02/19/18 18:34 14-Nitroaniline ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1NitrobenzeneND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12-Nitrophenol ND
21.6 ug/L 02/17/18 16:28 02/19/18 18:34 14-Nitrophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1N-Nitrosodi-n-propylamine ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1n-Nitrosodiphenylamine(as
diphenylamine)
ND *
21.6 ug/L 02/17/18 16:28 02/19/18 18:34 1PentachlorophenolND *
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1PhenanthreneND *
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 1PhenolND
1.72 ug/L 02/17/18 16:28 02/19/18 18:34 1PyreneND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 11,2,4-Trichlorobenzene ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12,4,5-Trichlorophenol ND
8.62 ug/L 02/17/18 16:28 02/19/18 18:34 12,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)61 29-120 02/17/18 16:28 02/19/18 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)55 02/17/18 16:28 02/19/18 18:34 110-120
Nitrobenzene-d5 (Surr)65 02/17/18 16:28 02/19/18 18:34 127-120
Phenol-d5 (Surr)40 02/17/18 16:28 02/19/18 18:34 110-120
Terphenyl-d14 (Surr)72 02/17/18 16:28 02/19/18 18:34 113-120
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-7Client Sample ID: Duplicate-1
Matrix: WaterDate Collected: 02/16/18 13:30
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)73 10-120 02/17/18 16:28 02/19/18 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00200 mg/L 02/19/18 15:26 02/20/18 12:43 1Barium1.78
0.00100 mg/L 02/19/18 15:26 02/20/18 12:43 1CadmiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:43 1ChromiumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:43 1LeadND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:43 1SeleniumND
0.00200 mg/L 02/19/18 15:26 02/20/18 12:43 1SilverND
Method: 7470A - Mercury (CVAA)
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 20:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 0.0100 mg/L 02/17/18 10:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-8Client Sample ID: Trip Blank 1
Matrix: WaterDate Collected: 02/16/18 00:01
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 18:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 18:06 1BenzeneND
1.00 ug/L 02/17/18 18:06 1BromobenzeneND
1.00 ug/L 02/17/18 18:06 1BromochloromethaneND
1.00 ug/L 02/17/18 18:06 1BromodichloromethaneND
1.00 ug/L 02/17/18 18:06 1BromoformND
1.00 ug/L 02/17/18 18:06 1BromomethaneND *
50.0 ug/L 02/17/18 18:06 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 18:06 1Carbon disulfide ND
1.00 ug/L 02/17/18 18:06 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 18:06 1ChlorobenzeneND
1.00 ug/L 02/17/18 18:06 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 18:06 1ChloroethaneND
1.00 ug/L 02/17/18 18:06 1ChloroformND
1.00 ug/L 02/17/18 18:06 1ChloromethaneND
1.00 ug/L 02/17/18 18:06 12-Chlorotoluene ND
1.00 ug/L 02/17/18 18:06 14-Chlorotoluene ND
1.00 ug/L 02/17/18 18:06 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 18:06 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 18:06 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 18:06 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 18:06 1DibromomethaneND
1.00 ug/L 02/17/18 18:06 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 18:06 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 18:06 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 18:06 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 18:06 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 18:06 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 18:06 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 18:06 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 18:06 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 18:06 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 18:06 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 18:06 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 18:06 1Diisopropyl ether ND
1.00 ug/L 02/17/18 18:06 1EthylbenzeneND
2.00 ug/L 02/17/18 18:06 1HexachlorobutadieneND
10.0 ug/L 02/17/18 18:06 12-Hexanone ND
1.00 ug/L 02/17/18 18:06 1IsopropylbenzeneND
5.00 ug/L 02/17/18 18:06 1Methylene Chloride ND
10.0 ug/L 02/17/18 18:06 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 18:06 1Methyl tert-butyl ether ND
5.00 ug/L 02/17/18 18:06 1NaphthaleneND
1.00 ug/L 02/17/18 18:06 1n-Butylbenzene ND
1.00 ug/L 02/17/18 18:06 1N-Propylbenzene ND
1.00 ug/L 02/17/18 18:06 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 18:06 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 18:06 1StyreneND
1.00 ug/L 02/17/18 18:06 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-8Client Sample ID: Trip Blank 1
Matrix: WaterDate Collected: 02/16/18 00:01
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 18:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 18:06 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 18:06 1TetrachloroetheneND
1.00 ug/L 02/17/18 18:06 1TolueneND
1.00 ug/L 02/17/18 18:06 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 18:06 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 18:06 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 18:06 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 18:06 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 18:06 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 18:06 1TrichloroetheneND
1.00 ug/L 02/17/18 18:06 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 18:06 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 18:06 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 18:06 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 18:06 1Vinyl chloride ND
3.00 ug/L 02/17/18 18:06 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)102 70-130 02/17/18 18:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)99 02/17/18 18:06 170-130
1,2-Dichloroethane-d4 (Surr)97 02/17/18 18:06 170-130
Toluene-d8 (Surr)105 02/17/18 18:06 170-130
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-9Client Sample ID: Trip Blank 2
Matrix: WaterDate Collected: 02/16/18 00:01
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 02/17/18 18:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 18:32 1BenzeneND
1.00 ug/L 02/17/18 18:32 1BromobenzeneND
1.00 ug/L 02/17/18 18:32 1BromochloromethaneND
1.00 ug/L 02/17/18 18:32 1BromodichloromethaneND
1.00 ug/L 02/17/18 18:32 1BromoformND
1.00 ug/L 02/17/18 18:32 1BromomethaneND *
50.0 ug/L 02/17/18 18:32 12-Butanone (MEK)ND
1.00 ug/L 02/17/18 18:32 1Carbon disulfide ND
1.00 ug/L 02/17/18 18:32 1Carbon tetrachloride ND
1.00 ug/L 02/17/18 18:32 1ChlorobenzeneND
1.00 ug/L 02/17/18 18:32 1ChlorodibromomethaneND
1.00 ug/L 02/17/18 18:32 1ChloroethaneND
1.00 ug/L 02/17/18 18:32 1ChloroformND
1.00 ug/L 02/17/18 18:32 1ChloromethaneND
1.00 ug/L 02/17/18 18:32 12-Chlorotoluene ND
1.00 ug/L 02/17/18 18:32 14-Chlorotoluene ND
1.00 ug/L 02/17/18 18:32 1cis-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 18:32 1cis-1,3-Dichloropropene ND
10.0 ug/L 02/17/18 18:32 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 02/17/18 18:32 11,2-Dibromoethane (EDB)ND
1.00 ug/L 02/17/18 18:32 1DibromomethaneND
1.00 ug/L 02/17/18 18:32 11,2-Dichlorobenzene ND
1.00 ug/L 02/17/18 18:32 11,3-Dichlorobenzene ND
1.00 ug/L 02/17/18 18:32 11,4-Dichlorobenzene ND
1.00 ug/L 02/17/18 18:32 1DichlorodifluoromethaneND *
1.00 ug/L 02/17/18 18:32 11,1-Dichloroethane ND
1.00 ug/L 02/17/18 18:32 11,2-Dichloroethane ND
1.00 ug/L 02/17/18 18:32 11,1-Dichloroethene ND
1.00 ug/L 02/17/18 18:32 11,2-Dichloroethene, Total ND
1.00 ug/L 02/17/18 18:32 11,2-Dichloropropane ND
1.00 ug/L 02/17/18 18:32 11,3-Dichloropropane ND
1.00 ug/L 02/17/18 18:32 12,2-Dichloropropane ND
1.00 ug/L 02/17/18 18:32 11,1-Dichloropropene ND
2.00 ug/L 02/17/18 18:32 1Diisopropyl ether ND
1.00 ug/L 02/17/18 18:32 1EthylbenzeneND
2.00 ug/L 02/17/18 18:32 1HexachlorobutadieneND
10.0 ug/L 02/17/18 18:32 12-Hexanone ND
1.00 ug/L 02/17/18 18:32 1IsopropylbenzeneND
5.00 ug/L 02/17/18 18:32 1Methylene Chloride ND
10.0 ug/L 02/17/18 18:32 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 02/17/18 18:32 1Methyl tert-butyl ether ND
5.00 ug/L 02/17/18 18:32 1NaphthaleneND
1.00 ug/L 02/17/18 18:32 1n-Butylbenzene ND
1.00 ug/L 02/17/18 18:32 1N-Propylbenzene ND
1.00 ug/L 02/17/18 18:32 1p-Isopropyltoluene ND
1.00 ug/L 02/17/18 18:32 1sec-Butylbenzene ND
1.00 ug/L 02/17/18 18:32 1StyreneND
1.00 ug/L 02/17/18 18:32 1tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Lab Sample ID: 490-146552-9Client Sample ID: Trip Blank 2
Matrix: WaterDate Collected: 02/16/18 00:01
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 02/17/18 18:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1.00 ug/L 02/17/18 18:32 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 02/17/18 18:32 1TetrachloroetheneND
1.00 ug/L 02/17/18 18:32 1TolueneND
1.00 ug/L 02/17/18 18:32 1trans-1,2-Dichloroethene ND
1.00 ug/L 02/17/18 18:32 1trans-1,3-Dichloropropene ND
1.00 ug/L 02/17/18 18:32 11,2,3-Trichlorobenzene ND
1.00 ug/L 02/17/18 18:32 11,2,4-Trichlorobenzene ND
1.00 ug/L 02/17/18 18:32 11,1,1-Trichloroethane ND
1.00 ug/L 02/17/18 18:32 11,1,2-Trichloroethane ND
1.00 ug/L 02/17/18 18:32 1TrichloroetheneND
1.00 ug/L 02/17/18 18:32 1TrichlorofluoromethaneND
1.00 ug/L 02/17/18 18:32 11,2,3-Trichloropropane ND
1.00 ug/L 02/17/18 18:32 11,2,4-Trimethylbenzene ND
1.00 ug/L 02/17/18 18:32 11,3,5-Trimethylbenzene ND
1.00 ug/L 02/17/18 18:32 1Vinyl chloride ND
3.00 ug/L 02/17/18 18:32 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)103 70-130 02/17/18 18:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)101 02/17/18 18:32 170-130
1,2-Dichloroethane-d4 (Surr)104 02/17/18 18:32 170-130
Toluene-d8 (Surr)95 02/17/18 18:32 170-130
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Page 37 of 64 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-496192/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
RL MDL
Acetone ND 25.0 ug/L 02/17/18 16:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1.00 ug/L 02/17/18 16:46 1Benzene
ND 1.00 ug/L 02/17/18 16:46 1Bromobenzene
ND 1.00 ug/L 02/17/18 16:46 1Bromochloromethane
ND 1.00 ug/L 02/17/18 16:46 1Bromodichloromethane
ND 1.00 ug/L 02/17/18 16:46 1Bromoform
ND 1.00 ug/L 02/17/18 16:46 1Bromomethane
ND 50.0 ug/L 02/17/18 16:46 12-Butanone (MEK)
ND 1.00 ug/L 02/17/18 16:46 1Carbon disulfide
ND 1.00 ug/L 02/17/18 16:46 1Carbon tetrachloride
ND 1.00 ug/L 02/17/18 16:46 1Chlorobenzene
ND 1.00 ug/L 02/17/18 16:46 1Chlorodibromomethane
ND 1.00 ug/L 02/17/18 16:46 1Chloroethane
ND 1.00 ug/L 02/17/18 16:46 1Chloroform
ND 1.00 ug/L 02/17/18 16:46 1Chloromethane
ND 1.00 ug/L 02/17/18 16:46 12-Chlorotoluene
ND 1.00 ug/L 02/17/18 16:46 14-Chlorotoluene
ND 1.00 ug/L 02/17/18 16:46 1cis-1,2-Dichloroethene
ND 1.00 ug/L 02/17/18 16:46 1cis-1,3-Dichloropropene
ND 10.0 ug/L 02/17/18 16:46 11,2-Dibromo-3-Chloropropane
ND 1.00 ug/L 02/17/18 16:46 11,2-Dibromoethane (EDB)
ND 1.00 ug/L 02/17/18 16:46 1Dibromomethane
ND 1.00 ug/L 02/17/18 16:46 11,2-Dichlorobenzene
ND 1.00 ug/L 02/17/18 16:46 11,3-Dichlorobenzene
ND 1.00 ug/L 02/17/18 16:46 11,4-Dichlorobenzene
ND 1.00 ug/L 02/17/18 16:46 1Dichlorodifluoromethane
ND 1.00 ug/L 02/17/18 16:46 11,1-Dichloroethane
ND 1.00 ug/L 02/17/18 16:46 11,2-Dichloroethane
ND 1.00 ug/L 02/17/18 16:46 11,1-Dichloroethene
ND 1.00 ug/L 02/17/18 16:46 11,2-Dichloroethene, Total
ND 1.00 ug/L 02/17/18 16:46 11,2-Dichloropropane
ND 1.00 ug/L 02/17/18 16:46 11,3-Dichloropropane
ND 1.00 ug/L 02/17/18 16:46 12,2-Dichloropropane
ND 1.00 ug/L 02/17/18 16:46 11,1-Dichloropropene
ND 2.00 ug/L 02/17/18 16:46 1Diisopropyl ether
ND 1.00 ug/L 02/17/18 16:46 1Ethylbenzene
ND 2.00 ug/L 02/17/18 16:46 1Hexachlorobutadiene
ND 10.0 ug/L 02/17/18 16:46 12-Hexanone
ND 1.00 ug/L 02/17/18 16:46 1Isopropylbenzene
ND 5.00 ug/L 02/17/18 16:46 1Methylene Chloride
ND 10.0 ug/L 02/17/18 16:46 14-Methyl-2-pentanone (MIBK)
ND 1.00 ug/L 02/17/18 16:46 1Methyl tert-butyl ether
ND 5.00 ug/L 02/17/18 16:46 1Naphthalene
ND 1.00 ug/L 02/17/18 16:46 1n-Butylbenzene
ND 1.00 ug/L 02/17/18 16:46 1N-Propylbenzene
ND 1.00 ug/L 02/17/18 16:46 1p-Isopropyltoluene
ND 1.00 ug/L 02/17/18 16:46 1sec-Butylbenzene
ND 1.00 ug/L 02/17/18 16:46 1Styrene
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Page 38 of 64 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-496192/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
RL MDL
tert-Butylbenzene ND 1.00 ug/L 02/17/18 16:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 1.00 ug/L 02/17/18 16:46 11,1,1,2-Tetrachloroethane
ND 1.00 ug/L 02/17/18 16:46 11,1,2,2-Tetrachloroethane
ND 1.00 ug/L 02/17/18 16:46 1Tetrachloroethene
ND 1.00 ug/L 02/17/18 16:46 1Toluene
ND 1.00 ug/L 02/17/18 16:46 1trans-1,2-Dichloroethene
ND 1.00 ug/L 02/17/18 16:46 1trans-1,3-Dichloropropene
2.234 1.00 ug/L 02/17/18 16:46 11,2,3-Trichlorobenzene
ND 1.00 ug/L 02/17/18 16:46 11,2,4-Trichlorobenzene
ND 1.00 ug/L 02/17/18 16:46 11,1,1-Trichloroethane
ND 1.00 ug/L 02/17/18 16:46 11,1,2-Trichloroethane
ND 1.00 ug/L 02/17/18 16:46 1Trichloroethene
ND 1.00 ug/L 02/17/18 16:46 1Trichlorofluoromethane
ND 1.00 ug/L 02/17/18 16:46 11,2,3-Trichloropropane
ND 1.00 ug/L 02/17/18 16:46 11,2,4-Trimethylbenzene
ND 1.00 ug/L 02/17/18 16:46 11,3,5-Trimethylbenzene
ND 1.00 ug/L 02/17/18 16:46 1Vinyl chloride
ND 3.00 ug/L 02/17/18 16:46 1Xylenes, Total
4-Bromofluorobenzene (Surr)102 70-130 02/17/18 16:46 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
103 02/17/18 16:46 1Dibromofluoromethane (Surr)70-130
103 02/17/18 16:46 11,2-Dichloroethane-d4 (Surr)70-130
99 02/17/18 16:46 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496192/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
Acetone 100 125.4 ug/L 125 39-150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 20.0 22.50 ug/L 112 70-130
Bromobenzene 20.0 18.46 ug/L 92 70-130
Bromochloromethane 20.0 23.37 ug/L 117 70-130
Bromodichloromethane 20.0 22.19 ug/L 111 70-130
Bromoform 20.0 18.77 ug/L 94 70-137
Bromomethane 20.0 35.21 * ug/L 176 53-150
2-Butanone (MEK)100 116.2 ug/L 116 55-143
Carbon disulfide 20.0 23.90 ug/L 120 64-135
Carbon tetrachloride 20.0 23.58 ug/L 118 70-147
Chlorobenzene 20.0 21.16 ug/L 106 70-130
Chlorodibromomethane 20.0 20.68 ug/L 103 70-133
Chloroethane 20.0 23.74 ug/L 119 60-138
Chloroform 20.0 22.39 ug/L 112 70-130
Chloromethane 20.0 23.79 ug/L 119 33-150
2-Chlorotoluene 20.0 19.75 ug/L 99 70-130
4-Chlorotoluene 20.0 20.89 ug/L 104 70-130
cis-1,2-Dichloroethene 20.0 22.59 ug/L 113 70-130
TestAmerica Nashville
Page 39 of 64 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496192/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
cis-1,3-Dichloropropene 20.0 21.94 ug/L 110 70-133
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 20.0 18.58 ug/L 93 45-138
1,2-Dibromoethane (EDB)20.0 22.15 ug/L 111 70-130
Dibromomethane 20.0 22.45 ug/L 112 70-130
1,2-Dichlorobenzene 20.0 21.42 ug/L 107 70-130
1,3-Dichlorobenzene 20.0 21.02 ug/L 105 70-130
1,4-Dichlorobenzene 20.0 21.19 ug/L 106 70-130
Dichlorodifluoromethane 20.0 28.48 ug/L 142 48-150
1,1-Dichloroethane 20.0 21.98 ug/L 110 70-130
1,2-Dichloroethane 20.0 22.55 ug/L 113 70-130
1,1-Dichloroethene 20.0 24.27 ug/L 121 70-132
1,2-Dichloroethene, Total 40.0 46.33 ug/L 116 70-130
1,2-Dichloropropane 20.0 21.40 ug/L 107 70-130
1,3-Dichloropropane 20.0 22.05 ug/L 110 70-130
2,2-Dichloropropane 20.0 22.90 ug/L 115 60-143
1,1-Dichloropropene 20.0 23.40 ug/L 117 70-130
Diisopropyl ether 20.0 23.40 ug/L 117 66-142
Ethylbenzene 20.0 20.90 ug/L 104 70-130
Hexachlorobutadiene 20.0 19.27 ug/L 96 70-138
2-Hexanone 100 107.4 ug/L 107 54-142
Isopropylbenzene 20.0 19.87 ug/L 99 70-131
Methylene Chloride 20.0 22.97 ug/L 115 70-130
4-Methyl-2-pentanone (MIBK)100 105.9 ug/L 106 60-137
Methyl tert-butyl ether 20.0 23.14 ug/L 116 70-130
Naphthalene 20.0 22.10 ug/L 110 54-150
n-Butylbenzene 20.0 19.32 ug/L 97 68-137
N-Propylbenzene 20.0 19.41 ug/L 97 70-134
p-Isopropyltoluene 20.0 19.78 ug/L 99 66-130
sec-Butylbenzene 20.0 20.17 ug/L 101 70-135
Styrene 20.0 20.48 ug/L 102 70-130
tert-Butylbenzene 20.0 20.44 ug/L 102 70-130
1,1,1,2-Tetrachloroethane 20.0 21.30 ug/L 106 70-130
1,1,2,2-Tetrachloroethane 20.0 20.24 ug/L 101 69-131
Tetrachloroethene 20.0 21.92 ug/L 110 70-130
Toluene 20.0 21.82 ug/L 109 70-130
trans-1,2-Dichloroethene 20.0 23.74 ug/L 119 70-130
trans-1,3-Dichloropropene 20.0 21.83 ug/L 109 63-142
1,2,3-Trichlorobenzene 20.0 22.67 ug/L 113 46-150
1,2,4-Trichlorobenzene 20.0 20.49 ug/L 102 58-147
1,1,1-Trichloroethane 20.0 23.74 ug/L 119 70-135
1,1,2-Trichloroethane 20.0 22.07 ug/L 110 70-130
Trichloroethene 20.0 23.32 ug/L 117 70-130
Trichlorofluoromethane 20.0 24.06 ug/L 120 59-150
1,2,3-Trichloropropane 20.0 19.61 ug/L 98 70-131
1,2,4-Trimethylbenzene 20.0 20.49 ug/L 102 70-130
1,3,5-Trimethylbenzene 20.0 20.23 ug/L 101 70-130
Vinyl chloride 20.0 25.42 ug/L 127 57-137
Xylenes, Total 40.0 40.68 ug/L 102 70-132
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496192/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
4-Bromofluorobenzene (Surr)70 -130
Surrogate
96
LCS LCS
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
1031,2-Dichloroethane-d4 (Surr)70 -130
99Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496192/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
Acetone 100 108.8 ug/L 109 39-150 14 23
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 20.0 22.91 ug/L 115 70-130 2 12
Bromobenzene 20.0 20.07 ug/L 100 70-130 8 16
Bromochloromethane 20.0 22.66 ug/L 113 70-130 3 16
Bromodichloromethane 20.0 23.04 ug/L 115 70-130 4 14
Bromoform 20.0 17.15 ug/L 86 70-137 9 14
Bromomethane 20.0 36.94 * ug/L 185 53-150 5 19
2-Butanone (MEK)100 115.3 ug/L 115 55-143 1 19
Carbon disulfide 20.0 25.01 ug/L 125 64-135 5 16
Carbon tetrachloride 20.0 24.30 ug/L 121 70-147 3 16
Chlorobenzene 20.0 20.98 ug/L 105 70-130 1 12
Chlorodibromomethane 20.0 20.57 ug/L 103 70-133 0 13
Chloroethane 20.0 25.87 ug/L 129 60-138 9 15
Chloroform 20.0 23.21 ug/L 116 70-130 4 14
Chloromethane 20.0 25.40 ug/L 127 33-150 7 20
2-Chlorotoluene 20.0 21.47 ug/L 107 70-130 8 15
4-Chlorotoluene 20.0 21.74 ug/L 109 70-130 4 15
cis-1,2-Dichloroethene 20.0 23.67 ug/L 118 70-130 5 15
cis-1,3-Dichloropropene 20.0 22.10 ug/L 110 70-133 1 15
1,2-Dibromo-3-Chloropropane 20.0 18.88 ug/L 94 45-138 2 19
1,2-Dibromoethane (EDB)20.0 20.98 ug/L 105 70-130 5 13
Dibromomethane 20.0 22.99 ug/L 115 70-130 2 14
1,2-Dichlorobenzene 20.0 21.44 ug/L 107 70-130 0 12
1,3-Dichlorobenzene 20.0 21.47 ug/L 107 70-130 2 13
1,4-Dichlorobenzene 20.0 21.62 ug/L 108 70-130 2 12
Dichlorodifluoromethane 20.0 30.96 * ug/L 155 48-150 8 16
1,1-Dichloroethane 20.0 22.48 ug/L 112 70-130 2 17
1,2-Dichloroethane 20.0 21.80 ug/L 109 70-130 3 13
1,1-Dichloroethene 20.0 25.42 ug/L 127 70-132 5 20
1,2-Dichloroethene, Total 40.0 49.15 ug/L 123 70-130 6 14
1,2-Dichloropropane 20.0 23.28 ug/L 116 70-130 8 15
1,3-Dichloropropane 20.0 21.34 ug/L 107 70-130 3 12
2,2-Dichloropropane 20.0 23.47 ug/L 117 60-143 2 20
1,1-Dichloropropene 20.0 23.46 ug/L 117 70-130 0 16
Diisopropyl ether 20.0 24.28 ug/L 121 66-142 4 14
Ethylbenzene 20.0 20.94 ug/L 105 70-130 0 12
Hexachlorobutadiene 20.0 19.60 ug/L 98 70-138 2 16
2-Hexanone 100 98.39 ug/L 98 54-142 9 17
TestAmerica Nashville
Page 41 of 64 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496192/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
Isopropylbenzene 20.0 19.09 ug/L 95 70-131 4 13
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 20.0 23.63 ug/L 118 70-130 3 15
4-Methyl-2-pentanone (MIBK)100 102.8 ug/L 103 60-137 3 21
Methyl tert-butyl ether 20.0 23.62 ug/L 118 70-130 2 16
Naphthalene 20.0 22.74 ug/L 114 54-150 3 15
n-Butylbenzene 20.0 20.45 ug/L 102 68-137 6 14
N-Propylbenzene 20.0 21.29 ug/L 106 70-134 9 14
p-Isopropyltoluene 20.0 20.83 ug/L 104 66-130 5 13
sec-Butylbenzene 20.0 20.76 ug/L 104 70-135 3 14
Styrene 20.0 20.34 ug/L 102 70-130 1 12
tert-Butylbenzene 20.0 20.65 ug/L 103 70-130 1 14
1,1,1,2-Tetrachloroethane 20.0 21.24 ug/L 106 70-130 0 13
1,1,2,2-Tetrachloroethane 20.0 21.30 ug/L 106 69-131 5 15
Tetrachloroethene 20.0 22.18 ug/L 111 70-130 1 17
Toluene 20.0 22.24 ug/L 111 70-130 2 13
trans-1,2-Dichloroethene 20.0 25.48 ug/L 127 70-130 7 15
trans-1,3-Dichloropropene 20.0 21.53 ug/L 108 63-142 1 13
1,2,3-Trichlorobenzene 20.0 24.68 ug/L 123 46-150 8 16
1,2,4-Trichlorobenzene 20.0 21.00 ug/L 105 58-147 2 15
1,1,1-Trichloroethane 20.0 23.72 ug/L 119 70-135 0 15
1,1,2-Trichloroethane 20.0 21.14 ug/L 106 70-130 4 13
Trichloroethene 20.0 23.71 ug/L 119 70-130 2 14
Trichlorofluoromethane 20.0 26.06 ug/L 130 59-150 8 22
1,2,3-Trichloropropane 20.0 21.62 ug/L 108 70-131 10 14
1,2,4-Trimethylbenzene 20.0 21.22 ug/L 106 70-130 4 13
1,3,5-Trimethylbenzene 20.0 19.43 ug/L 97 70-130 4 14
Vinyl chloride 20.0 26.08 ug/L 130 57-137 3 15
Xylenes, Total 40.0 41.15 ug/L 103 70-132 1 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
97
LCSD LCSD
Qualifier Limits%Recovery
104Dibromofluoromethane (Surr)70 -130
1031,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix SpikeLab Sample ID: 490-146544-B-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
Acetone ND 100 94.10 ug/L 94 39-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene ND 20.0 21.40 ug/L 107 55-147
Bromobenzene ND 20.0 16.73 ug/L 84 60-133
Bromochloromethane ND 20.0 22.20 ug/L 111 59-132
Bromodichloromethane ND 20.0 21.68 ug/L 108 70-140
Bromoform ND 20.0 15.27 ug/L 76 53-150
Bromomethane ND *20.0 28.08 ug/L 140 30-150
2-Butanone (MEK)ND 100 103.4 ug/L 103 50-143
TestAmerica Nashville
Page 42 of 64 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-146544-B-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
Carbon disulfide ND 20.0 20.05 ug/L 100 35-150
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Carbon tetrachloride ND 20.0 23.14 ug/L 116 56-150
Chlorobenzene ND 20.0 19.50 ug/L 98 70-130
Chlorodibromomethane ND 20.0 18.90 ug/L 94 66-140
Chloroethane ND 20.0 22.07 ug/L 110 58-141
Chloroform ND 20.0 22.69 ug/L 110 66-138
Chloromethane ND 20.0 22.72 ug/L 114 10-150
2-Chlorotoluene ND 20.0 18.75 ug/L 94 67-138
4-Chlorotoluene ND 20.0 18.62 ug/L 93 69-138
cis-1,2-Dichloroethene 9.15 20.0 29.91 ug/L 104 68-131
cis-1,3-Dichloropropene ND 20.0 19.37 ug/L 97 70-133
1,2-Dibromo-3-Chloropropane ND 20.0 13.57 ug/L 68 38-138
1,2-Dibromoethane (EDB)ND 20.0 19.13 ug/L 96 65-137
Dibromomethane ND 20.0 21.21 ug/L 106 70-130
1,2-Dichlorobenzene ND 20.0 19.71 ug/L 99 70-130
1,3-Dichlorobenzene ND 20.0 19.61 ug/L 98 68-131
1,4-Dichlorobenzene ND 20.0 19.53 ug/L 98 70-130
Dichlorodifluoromethane ND *20.0 24.42 ug/L 122 10-150
1,1-Dichloroethane ND 20.0 21.55 ug/L 108 61-139
1,2-Dichloroethane ND 20.0 20.44 ug/L 102 64-136
1,1-Dichloroethene ND 20.0 23.42 ug/L 117 54-150
1,2-Dichloroethene, Total 9.15 40.0 52.41 ug/L 108 60-134
1,2-Dichloropropane ND 20.0 21.20 ug/L 106 67-130
1,3-Dichloropropane ND 20.0 19.79 ug/L 99 70-130
2,2-Dichloropropane ND 20.0 19.00 ug/L 95 50-146
1,1-Dichloropropene ND 20.0 22.53 ug/L 113 54-150
Diisopropyl ether ND 20.0 21.63 ug/L 108 56-142
Ethylbenzene ND 20.0 20.63 ug/L 103 65-139
Hexachlorobutadiene ND 20.0 16.46 ug/L 82 61-141
2-Hexanone ND 100 93.70 ug/L 94 44-150
Isopropylbenzene ND 20.0 18.77 ug/L 94 70-137
Methylene Chloride ND 20.0 21.02 ug/L 105 64-130
4-Methyl-2-pentanone (MIBK)ND 100 96.13 ug/L 96 50-140
Methyl tert-butyl ether ND 20.0 20.89 ug/L 104 55-141
Naphthalene ND F2 20.0 10.75 ug/L 54 32-150
n-Butylbenzene ND 20.0 19.27 ug/L 96 61-141
N-Propylbenzene ND 20.0 18.42 ug/L 92 53-150
p-Isopropyltoluene ND 20.0 19.51 ug/L 98 66-137
sec-Butylbenzene ND 20.0 19.82 ug/L 99 55-136
Styrene ND 20.0 18.33 ug/L 92 70-130
tert-Butylbenzene ND 20.0 19.55 ug/L 98 70-138
1,1,1,2-Tetrachloroethane ND 20.0 19.67 ug/L 98 70-131
1,1,2,2-Tetrachloroethane ND 20.0 17.00 ug/L 85 56-145
Tetrachloroethene 2.96 20.0 23.70 ug/L 104 57-138
Toluene ND 20.0 20.48 ug/L 101 64-136
trans-1,2-Dichloroethene ND 20.0 22.50 ug/L 112 59-143
trans-1,3-Dichloropropene ND 20.0 19.09 ug/L 95 63-142
1,2,3-Trichlorobenzene ND F2 20.0 10.35 ug/L 52 36-150
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-146544-B-3 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
1,2,4-Trichlorobenzene ND F2 20.0 13.14 ug/L 66 47-147
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,1,1-Trichloroethane ND 20.0 22.44 ug/L 112 68-144
1,1,2-Trichloroethane ND 20.0 19.41 ug/L 97 70-130
Trichloroethene 118 F2 20.0 136.3 4 ug/L 94 63-135
Trichlorofluoromethane ND 20.0 23.94 ug/L 120 44-150
1,2,3-Trichloropropane ND 20.0 16.62 ug/L 83 65-131
1,2,4-Trimethylbenzene ND 20.0 19.47 ug/L 97 64-136
1,3,5-Trimethylbenzene ND 20.0 17.66 ug/L 88 69-139
Vinyl chloride ND 20.0 22.38 ug/L 112 57-150
Xylenes, Total ND 40.0 38.38 ug/L 96 69-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
86
MS MS
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1041,2-Dichloroethane-d4 (Surr)70 -130
95Toluene-d8 (Surr)70 -130
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-146544-C-3 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
Acetone ND 100 92.01 ug/L 92 39-150 2 28
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Benzene ND 20.0 21.16 ug/L 106 55-147 1 22
Bromobenzene ND 20.0 17.81 ug/L 89 60-133 6 18
Bromochloromethane ND 20.0 21.10 ug/L 106 59-132 5 21
Bromodichloromethane ND 20.0 18.92 ug/L 95 70-140 14 196
Bromoform ND 20.0 16.60 ug/L 83 53-150 8 20
Bromomethane ND *20.0 30.07 ug/L 150 30-150 7 44
2-Butanone (MEK)ND 100 101.0 ug/L 101 50-143 2 28
Carbon disulfide ND 20.0 19.61 ug/L 98 35-150 2 34
Carbon tetrachloride ND 20.0 22.31 ug/L 112 56-150 4 18
Chlorobenzene ND 20.0 19.80 ug/L 99 70-130 2 15
Chlorodibromomethane ND 20.0 18.98 ug/L 95 66-140 0 19
Chloroethane ND 20.0 21.73 ug/L 109 58-141 2 31
Chloroform ND 20.0 21.48 ug/L 104 66-138 5 21
Chloromethane ND 20.0 22.06 ug/L 110 10-150 3 43
2-Chlorotoluene ND 20.0 19.26 ug/L 96 67-138 3 17
4-Chlorotoluene ND 20.0 19.28 ug/L 96 69-138 4 15
cis-1,2-Dichloroethene 9.15 20.0 28.03 ug/L 94 68-131 6 21
cis-1,3-Dichloropropene ND 20.0 18.97 ug/L 95 70-133 2 19
1,2-Dibromo-3-Chloropropane ND 20.0 14.81 ug/L 74 38-138 9 26
1,2-Dibromoethane (EDB)ND 20.0 20.22 ug/L 101 65-137 6 21
Dibromomethane ND 20.0 19.51 ug/L 98 70-130 8 19
1,2-Dichlorobenzene ND 20.0 19.91 ug/L 100 70-130 1 15
1,3-Dichlorobenzene ND 20.0 19.19 ug/L 96 68-131 2 14
1,4-Dichlorobenzene ND 20.0 19.84 ug/L 99 70-130 2 14
Dichlorodifluoromethane ND *20.0 23.80 ug/L 119 10-150 3 50
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-146544-C-3 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496192
1,1-Dichloroethane ND 20.0 20.98 ug/L 105 61-139 3 23
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
1,2-Dichloroethane ND 20.0 20.22 ug/L 101 64-136 1 22
1,1-Dichloroethene ND 20.0 22.44 ug/L 112 54-150 4 24
1,2-Dichloroethene, Total 9.15 40.0 49.94 ug/L 102 60-134 5 22
1,2-Dichloropropane ND 20.0 19.59 ug/L 98 67-130 8 19
1,3-Dichloropropane ND 20.0 19.89 ug/L 99 70-130 0 17
2,2-Dichloropropane ND 20.0 18.10 ug/L 91 50-146 5 20
1,1-Dichloropropene ND 20.0 21.63 ug/L 108 54-150 4 24
Diisopropyl ether ND 20.0 20.50 ug/L 103 56-142 5 22
Ethylbenzene ND 20.0 20.03 ug/L 100 65-139 3 18
Hexachlorobutadiene ND 20.0 18.36 ug/L 92 61-141 11 26
2-Hexanone ND 100 94.29 ug/L 94 44-150 1 21
Isopropylbenzene ND 20.0 21.00 ug/L 105 70-137 11 17
Methylene Chloride ND 20.0 20.26 ug/L 101 64-130 4 22
4-Methyl-2-pentanone (MIBK)ND 100 95.88 ug/L 96 50-140 0 24
Methyl tert-butyl ether ND 20.0 20.33 ug/L 102 55-141 3 24
Naphthalene ND F2 20.0 18.86 F2 ug/L 94 32-150 55 40
n-Butylbenzene ND 20.0 19.85 ug/L 99 61-141 3 17
N-Propylbenzene ND 20.0 19.77 ug/L 99 53-150 7 18
p-Isopropyltoluene ND 20.0 19.93 ug/L 100 66-137 2 16
sec-Butylbenzene ND 20.0 20.31 ug/L 102 55-136 2 50
Styrene ND 20.0 20.09 ug/L 100 70-130 9 16
tert-Butylbenzene ND 20.0 20.10 ug/L 100 70-138 3 17
1,1,1,2-Tetrachloroethane ND 20.0 18.78 ug/L 94 70-131 5 16
1,1,2,2-Tetrachloroethane ND 20.0 18.49 ug/L 92 56-145 8 19
Tetrachloroethene 2.96 20.0 24.64 ug/L 108 57-138 4 17
Toluene ND 20.0 20.93 ug/L 104 64-136 2 18
trans-1,2-Dichloroethene ND 20.0 21.91 ug/L 110 59-143 3 25
trans-1,3-Dichloropropene ND 20.0 18.70 ug/L 94 63-142 2 18
1,2,3-Trichlorobenzene ND F2 20.0 19.45 F2 ug/L 97 36-150 61 43
1,2,4-Trichlorobenzene ND F2 20.0 18.23 F2 ug/L 91 47-147 32 24
1,1,1-Trichloroethane ND 20.0 22.13 ug/L 111 68-144 1 17
1,1,2-Trichloroethane ND 20.0 20.10 ug/L 101 70-130 4 18
Trichloroethene 118 F2 20.0 114.2 4 F2 ug/L -17 63-135 18 17
Trichlorofluoromethane ND 20.0 22.66 ug/L 113 44-150 6 32
1,2,3-Trichloropropane ND 20.0 18.84 ug/L 94 65-131 12 19
1,2,4-Trimethylbenzene ND 20.0 19.13 ug/L 96 64-136 2 18
1,3,5-Trimethylbenzene ND 20.0 18.60 ug/L 93 69-139 5 17
Vinyl chloride ND 20.0 22.99 ug/L 115 57-150 3 37
Xylenes, Total ND 40.0 40.31 ug/L 101 69-132 5 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
96
MSD MSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1031,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
TestAmerica Nashville
Page 45 of 64 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-496205/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496272 Prep Batch: 496205
RL MDL
Acenaphthene ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Acenaphthylene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Anthracene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Benzo[a]anthracene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Benzo[a]pyrene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Benzo[b]fluoranthene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Benzo[g,h,i]perylene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Benzo[k]fluoranthene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Bis(2-chloroethoxy)methane
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Bis(2-chloroethyl)ether
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1bis (2-chloroisopropyl) ether
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Bis(2-ethylhexyl) phthalate
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 14-Bromophenyl phenyl ether
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Butyl benzyl phthalate
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Carbazole
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 14-Chloroaniline
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 14-Chloro-3-methylphenol
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12-Chloronaphthalene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12-Chlorophenol
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 14-Chlorophenyl phenyl ether
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Chrysene
ND 20.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Cresols
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Dibenz(a,h)anthracene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Dibenzofuran
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 11,2-Dichlorobenzene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 11,3-Dichlorobenzene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 11,4-Dichlorobenzene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 13,3'-Dichlorobenzidine
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12,4-Dichlorophenol
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Diethyl phthalate
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12,4-Dimethylphenol
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Dimethyl phthalate
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Di-n-butyl phthalate
ND 25.0 ug/L 02/17/18 16:28 02/19/18 15:21 14,6-Dinitro-2-methylphenol
ND 25.0 ug/L 02/17/18 16:28 02/19/18 15:21 12,4-Dinitrophenol
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12,4-Dinitrotoluene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12,6-Dinitrotoluene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Di-n-octyl phthalate
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Fluoranthene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Fluorene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Hexachlorobenzene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Hexachlorobutadiene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Hexachlorocyclopentadiene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Hexachloroethane
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Indeno[1,2,3-cd]pyrene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Isophorone
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 11-Methylnaphthalene
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 12-Methylnaphthalene
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-496205/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496272 Prep Batch: 496205
RL MDL
2-Methylphenol ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 13 & 4 Methylphenol
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Naphthalene
ND 25.0 ug/L 02/17/18 16:28 02/19/18 15:21 12-Nitroaniline
ND 25.0 ug/L 02/17/18 16:28 02/19/18 15:21 13-Nitroaniline
ND 25.0 ug/L 02/17/18 16:28 02/19/18 15:21 14-Nitroaniline
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Nitrobenzene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12-Nitrophenol
ND 25.0 ug/L 02/17/18 16:28 02/19/18 15:21 14-Nitrophenol
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1N-Nitrosodi-n-propylamine
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 25.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Pentachlorophenol
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Phenanthrene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 1Phenol
ND 2.00 ug/L 02/17/18 16:28 02/19/18 15:21 1Pyrene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 11,2,4-Trichlorobenzene
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12,4,5-Trichlorophenol
ND 10.0 ug/L 02/17/18 16:28 02/19/18 15:21 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)59 29-120 02/19/18 15:21 1
MB MB
Surrogate
02/17/18 16:28
Dil FacPrepared AnalyzedQualifier Limits%Recovery
55 02/17/18 16:28 02/19/18 15:21 12-Fluorophenol (Surr)10-120
62 02/17/18 16:28 02/19/18 15:21 1Nitrobenzene-d5 (Surr)27-120
39 02/17/18 16:28 02/19/18 15:21 1Phenol-d5 (Surr)10-120
65 02/17/18 16:28 02/19/18 15:21 1Terphenyl-d14 (Surr)13-120
67 02/17/18 16:28 02/19/18 15:21 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496205/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496272 Prep Batch: 496205
Acenaphthene 40.0 50.62 ug/L 127 36-129
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 40.0 51.72 * ug/L 129 36-120
Anthracene 40.0 49.89 ug/L 125 42-130
Benzo[a]anthracene 40.0 51.39 ug/L 128 41-131
Benzo[a]pyrene 40.0 49.68 ug/L 124 45-131
Benzo[b]fluoranthene 40.0 53.69 * ug/L 134 43-132
Benzo[g,h,i]perylene 40.0 52.24 ug/L 131 38-138
Benzo[k]fluoranthene 40.0 51.50 ug/L 129 44-129
Bis(2-chloroethoxy)methane 40.0 47.12 ug/L 118 35-127
Bis(2-chloroethyl)ether 40.0 41.39 ug/L 103 27-132
bis (2-chloroisopropyl) ether 40.0 40.93 ug/L 102 24-136
Bis(2-ethylhexyl) phthalate 40.0 47.82 ug/L 120 41-147
4-Bromophenyl phenyl ether 40.0 49.32 ug/L 123 36-135
Butyl benzyl phthalate 40.0 49.55 ug/L 124 34-146
Carbazole 40.0 54.76 * ug/L 137 42-130
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496205/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496272 Prep Batch: 496205
4-Chloroaniline 40.0 33.80 ug/L 85 27-131
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Chloro-3-methylphenol 40.0 49.74 ug/L 124 10-150
2-Chloronaphthalene 40.0 48.75 ug/L 122 32-127
2-Chlorophenol 40.0 45.84 ug/L 115 10-150
4-Chlorophenyl phenyl ether 40.0 49.12 ug/L 123 36-131
Chrysene 40.0 51.77 ug/L 129 39-130
Cresols 80.0 83.38 ug/L 104 10-132
Dibenz(a,h)anthracene 40.0 54.43 ug/L 136 43-140
Dibenzofuran 40.0 49.90 ug/L 125 35-127
1,2-Dichlorobenzene 40.0 36.40 ug/L 91 27-120
1,3-Dichlorobenzene 40.0 33.55 ug/L 84 22-120
1,4-Dichlorobenzene 40.0 34.71 ug/L 87 24-120
3,3'-Dichlorobenzidine 40.0 50.34 ug/L 126 46-143
2,4-Dichlorophenol 40.0 49.49 ug/L 124 10-150
Diethyl phthalate 40.0 52.16 ug/L 130 31-136
2,4-Dimethylphenol 40.0 31.85 ug/L 80 10-150
Dimethyl phthalate 40.0 50.98 ug/L 127 34-134
Di-n-butyl phthalate 40.0 53.25 ug/L 133 42-140
4,6-Dinitro-2-methylphenol 80.0 133.4 * ug/L 167 10-150
2,4-Dinitrophenol 80.0 115.9 ug/L 145 10-150
2,4-Dinitrotoluene 40.0 53.30 ug/L 133 36-138
2,6-Dinitrotoluene 40.0 51.23 ug/L 128 41-137
Di-n-octyl phthalate 40.0 47.80 ug/L 119 42-142
Fluoranthene 40.0 53.54 * ug/L 134 31-132
Fluorene 40.0 51.43 ug/L 129 37-130
Hexachlorobenzene 40.0 51.80 ug/L 129 36-140
Hexachlorobutadiene 40.0 38.53 ug/L 96 18-136
Hexachlorocyclopentadiene 40.0 15.49 ug/L 39 17-128
Hexachloroethane 40.0 32.25 ug/L 81 23-120
Indeno[1,2,3-cd]pyrene 40.0 52.84 ug/L 132 40-136
Isophorone 40.0 24.42 ug/L 61 39-120
1-Methylnaphthalene 40.0 43.76 ug/L 109 36-131
2-Methylnaphthalene 40.0 42.49 ug/L 106 31-120
2-Methylphenol 40.0 42.34 ug/L 106 10-133
3 & 4 Methylphenol 40.0 41.04 ug/L 103 10-135
Naphthalene 40.0 42.68 ug/L 107 32-120
2-Nitroaniline 40.0 53.94 ug/L 135 35-147
3-Nitroaniline 40.0 49.50 ug/L 124 36-128
4-Nitroaniline 40.0 52.17 ug/L 130 38-139
Nitrobenzene 40.0 47.42 ug/L 119 10-150
2-Nitrophenol 40.0 48.60 ug/L 122 10-150
4-Nitrophenol 80.0 79.37 ug/L 99 10-110
N-Nitrosodi-n-propylamine 40.0 41.63 ug/L 104 32-136
n-Nitrosodiphenylamine(as
diphenylamine)
34.0 50.38 * ug/L 148 44-123
Pentachlorophenol 80.0 143.9 * ug/L 180 10-150
Phenanthrene 40.0 51.63 * ug/L 129 39-126
Phenol 40.0 30.16 ug/L 75 10-110
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496205/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496272 Prep Batch: 496205
Pyrene 40.0 50.15 ug/L 125 37-129
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,2,4-Trichlorobenzene 40.0 39.84 ug/L 100 24-127
2,4,5-Trichlorophenol 40.0 55.45 ug/L 139 10-150
2,4,6-Trichlorophenol 40.0 55.81 ug/L 140 10-150
2-Fluorobiphenyl (Surr)29 -120
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
472-Fluorophenol (Surr)10 -120
60Nitrobenzene-d5 (Surr)27 -120
36Phenol-d5 (Surr)10 -120
59Terphenyl-d14 (Surr)13 -120
692,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496205/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496272 Prep Batch: 496205
Acenaphthene 40.0 46.71 ug/L 117 36-129 8 50
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 40.0 47.79 ug/L 119 36-120 8 50
Anthracene 40.0 47.23 ug/L 118 42-130 5 50
Benzo[a]anthracene 40.0 49.28 ug/L 123 41-131 4 50
Benzo[a]pyrene 40.0 48.07 ug/L 120 45-131 3 50
Benzo[b]fluoranthene 40.0 48.55 ug/L 121 43-132 10 50
Benzo[g,h,i]perylene 40.0 50.83 ug/L 127 38-138 3 50
Benzo[k]fluoranthene 40.0 52.44 * ug/L 131 44-129 2 50
Bis(2-chloroethoxy)methane 40.0 45.36 ug/L 113 35-127 4 50
Bis(2-chloroethyl)ether 40.0 41.29 ug/L 103 27-132 0 50
bis (2-chloroisopropyl) ether 40.0 40.80 ug/L 102 24-136 0 50
Bis(2-ethylhexyl) phthalate 40.0 45.89 ug/L 115 41-147 4 47
4-Bromophenyl phenyl ether 40.0 46.52 ug/L 116 36-135 6 50
Butyl benzyl phthalate 40.0 47.27 ug/L 118 34-146 5 50
Carbazole 40.0 52.44 * ug/L 131 42-130 4 50
4-Chloroaniline 40.0 32.50 ug/L 81 27-131 4 34
4-Chloro-3-methylphenol 40.0 47.37 ug/L 118 10-150 5 50
2-Chloronaphthalene 40.0 45.78 ug/L 114 32-127 6 50
2-Chlorophenol 40.0 47.04 ug/L 118 10-150 3 49
4-Chlorophenyl phenyl ether 40.0 45.37 ug/L 113 36-131 8 50
Chrysene 40.0 49.26 ug/L 123 39-130 5 50
Cresols 80.0 83.65 ug/L 105 10-132 0 50
Dibenz(a,h)anthracene 40.0 52.35 ug/L 131 43-140 4 50
Dibenzofuran 40.0 46.52 ug/L 116 35-127 7 50
1,2-Dichlorobenzene 40.0 36.03 ug/L 90 27-120 1 50
1,3-Dichlorobenzene 40.0 32.67 ug/L 82 22-120 3 50
1,4-Dichlorobenzene 40.0 34.41 ug/L 86 24-120 1 50
3,3'-Dichlorobenzidine 40.0 48.11 ug/L 120 46-143 5 50
2,4-Dichlorophenol 40.0 48.43 ug/L 121 10-150 2 50
Diethyl phthalate 40.0 47.17 ug/L 118 31-136 10 50
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496205/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496272 Prep Batch: 496205
2,4-Dimethylphenol 40.0 33.75 ug/L 84 10-150 6 50
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Dimethyl phthalate 40.0 46.87 ug/L 117 34-134 8 50
Di-n-butyl phthalate 40.0 50.39 ug/L 126 42-140 6 50
4,6-Dinitro-2-methylphenol 80.0 128.9 * ug/L 161 10-150 3 50
2,4-Dinitrophenol 80.0 112.5 ug/L 141 10-150 3 50
2,4-Dinitrotoluene 40.0 49.65 ug/L 124 36-138 7 50
2,6-Dinitrotoluene 40.0 47.40 ug/L 118 41-137 8 50
Di-n-octyl phthalate 40.0 44.68 ug/L 112 42-142 7 49
Fluoranthene 40.0 50.75 ug/L 127 31-132 5 50
Fluorene 40.0 46.81 ug/L 117 37-130 9 50
Hexachlorobenzene 40.0 49.03 ug/L 123 36-140 5 50
Hexachlorobutadiene 40.0 36.34 ug/L 91 18-136 6 50
Hexachlorocyclopentadiene 40.0 13.95 ug/L 35 17-128 10 50
Hexachloroethane 40.0 30.93 ug/L 77 23-120 4 50
Indeno[1,2,3-cd]pyrene 40.0 50.71 ug/L 127 40-136 4 50
Isophorone 40.0 22.59 ug/L 56 39-120 8 50
1-Methylnaphthalene 40.0 42.45 ug/L 106 36-131 3 50
2-Methylnaphthalene 40.0 40.69 ug/L 102 31-120 4 50
2-Methylphenol 40.0 42.58 ug/L 106 10-133 1 45
3 & 4 Methylphenol 40.0 41.07 ug/L 103 10-135 0 46
Naphthalene 40.0 42.24 ug/L 106 32-120 1 50
2-Nitroaniline 40.0 50.07 ug/L 125 35-147 7 50
3-Nitroaniline 40.0 45.54 ug/L 114 36-128 8 27
4-Nitroaniline 40.0 48.27 ug/L 121 38-139 8 42
Nitrobenzene 40.0 47.23 ug/L 118 10-150 0 50
2-Nitrophenol 40.0 47.11 ug/L 118 10-150 3 50
4-Nitrophenol 80.0 74.31 ug/L 93 10-110 7 40
N-Nitrosodi-n-propylamine 40.0 41.45 ug/L 104 32-136 0 50
n-Nitrosodiphenylamine(as
diphenylamine)
34.0 47.32 * ug/L 139 44-123 6 50
Pentachlorophenol 80.0 139.1 * ug/L 174 10-150 3 50
Phenanthrene 40.0 48.84 ug/L 122 39-126 6 50
Phenol 40.0 30.32 ug/L 76 10-110 1 36
Pyrene 40.0 47.35 ug/L 118 37-129 6 50
1,2,4-Trichlorobenzene 40.0 39.05 ug/L 98 24-127 2 50
2,4,5-Trichlorophenol 40.0 51.63 ug/L 129 10-150 7 50
2,4,6-Trichlorophenol 40.0 50.96 ug/L 127 10-150 9 50
2-Fluorobiphenyl (Surr)29 -120
Surrogate
56
LCSD LCSD
Qualifier Limits%Recovery
472-Fluorophenol (Surr)10 -120
59Nitrobenzene-d5 (Surr)27 -120
36Phenol-d5 (Surr)10 -120
57Terphenyl-d14 (Surr)13 -120
642,4,6-Tribromophenol (Surr)10 -120
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-496453/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496453
RL MDL
Arsenic ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:01 1Barium
ND 0.00100 mg/L 02/19/18 15:26 02/20/18 12:01 1Cadmium
ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:01 1Chromium
ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:01 1Lead
ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:01 1Selenium
ND 0.00200 mg/L 02/19/18 15:26 02/20/18 12:01 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496453/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496453
Arsenic 0.100 0.09604 mg/L 96 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 0.100 0.09277 mg/L 93 80-120
Cadmium 0.100 0.1003 mg/L 100 80-120
Chromium 0.100 0.09788 mg/L 98 80-120
Lead 0.100 0.09780 mg/L 98 80-120
Selenium 0.100 0.09006 mg/L 90 80-120
Silver 0.100 0.1040 mg/L 104 80-120
Client Sample ID: MW-4Lab Sample ID: 490-146552-2 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496453
Arsenic ND 0.100 0.09808 mg/L 98 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 0.0222 0.100 0.1205 mg/L 98 75-125
Cadmium ND 0.100 0.1003 mg/L 100 75-125
Chromium 0.00900 0.100 0.1035 mg/L 95 75-125
Lead ND 0.100 0.09917 mg/L 99 75-125
Selenium ND 0.100 0.09462 mg/L 94 75-125
Silver ND 0.100 0.1031 mg/L 103 75-125
Client Sample ID: MW-4Lab Sample ID: 490-146552-2 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496453
Arsenic ND 0.100 0.09990 mg/L 100 75-125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 0.0222 0.100 0.1172 mg/L 95 75-125 3 20
Cadmium ND 0.100 0.09962 mg/L 100 75-125 1 20
Chromium 0.00900 0.100 0.1040 mg/L 95 75-125 0 20
Lead ND 0.100 0.09974 mg/L 99 75-125 1 20
Selenium ND 0.100 0.09384 mg/L 93 75-125 1 20
Silver ND 0.100 0.1043 mg/L 104 75-125 1 20
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-496741/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496802 Prep Batch: 496741
RL MDL
Mercury ND 0.000200 mg/L 02/20/18 15:50 02/20/18 19:13 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496741/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496802 Prep Batch: 496741
Mercury 0.00100 0.0009825 mg/L 98 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Matrix SpikeLab Sample ID: 490-146532-A-1-F MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496802 Prep Batch: 496741
Mercury ND 0.00100 0.0009035 mg/L 90 75-125
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-146532-A-1-G MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496802 Prep Batch: 496741
Mercury ND 0.00100 0.0008842 mg/L 88 75-125 2 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 490-496732/2
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496732
RL MDL
Chromium, hex ND 0.0100 mg/L 02/17/18 10:53 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496732/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496732
Chromium, hex 0.100 0.09200 mg/L 92 85-115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: MW-3Lab Sample ID: 490-146552-1 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496732
Chromium, hex ND F1 0.100 0.08400 F1 mg/L 84 85-115
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method: 7196A - Chromium, Hexavalent (Continued)
Client Sample ID: MW-3Lab Sample ID: 490-146552-1 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496732
Chromium, hex ND F1 0.100 0.08400 F1 mg/L 84 85-115 0 20
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: MW-3Lab Sample ID: 490-146552-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 496732
Chromium, hex ND F1 ND mg/L NC 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
GC/MS VOA
Analysis Batch: 496192
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-146552-1 MW-3 Total/NA
Water 8260B490-146552-2 MW-4 Total/NA
Water 8260B490-146552-3 MW-5 Total/NA
Water 8260B490-146552-4 HHTMW-1 Total/NA
Water 8260B490-146552-5 HHTMW-2 Total/NA
Water 8260B490-146552-6 HHTMW-3 Total/NA
Water 8260B490-146552-7 Duplicate-1 Total/NA
Water 8260B490-146552-8 Trip Blank 1 Total/NA
Water 8260B490-146552-9 Trip Blank 2 Total/NA
Water 8260BMB 490-496192/6 Method Blank Total/NA
Water 8260BLCS 490-496192/3 Lab Control Sample Total/NA
Water 8260BLCSD 490-496192/4 Lab Control Sample Dup Total/NA
Water 8260B490-146544-B-3 MS Matrix Spike Total/NA
Water 8260B490-146544-C-3 MSD Matrix Spike Duplicate Total/NA
GC/MS Semi VOA
Prep Batch: 496205
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C490-146552-1 MW-3 Total/NA
Water 3510C490-146552-2 MW-4 Total/NA
Water 3510C490-146552-3 MW-5 Total/NA
Water 3510C490-146552-4 HHTMW-1 Total/NA
Water 3510C490-146552-5 HHTMW-2 Total/NA
Water 3510C490-146552-6 HHTMW-3 Total/NA
Water 3510C490-146552-7 Duplicate-1 Total/NA
Water 3510CMB 490-496205/1-A Method Blank Total/NA
Water 3510CLCS 490-496205/2-A Lab Control Sample Total/NA
Water 3510CLCSD 490-496205/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 496272
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8270D 496205490-146552-1 MW-3 Total/NA
Water 8270D 496205490-146552-2 MW-4 Total/NA
Water 8270D 496205490-146552-3 MW-5 Total/NA
Water 8270D 496205490-146552-4 HHTMW-1 Total/NA
Water 8270D 496205490-146552-5 HHTMW-2 Total/NA
Water 8270D 496205490-146552-6 HHTMW-3 Total/NA
Water 8270D 496205490-146552-7 Duplicate-1 Total/NA
Water 8270D 496205MB 490-496205/1-A Method Blank Total/NA
Water 8270D 496205LCS 490-496205/2-A Lab Control Sample Total/NA
Water 8270D 496205LCSD 490-496205/3-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 496453
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-146552-1 MW-3 Total/NA
Water 3010A490-146552-2 MW-4 Total/NA
Water 3010A490-146552-3 MW-5 Total/NA
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Metals (Continued)
Prep Batch: 496453 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3010A490-146552-4 HHTMW-1 Total/NA
Water 3010A490-146552-5 HHTMW-2 Total/NA
Water 3010A490-146552-6 HHTMW-3 Total/NA
Water 3010A490-146552-7 Duplicate-1 Total/NA
Water 3010AMB 490-496453/1-A Method Blank Total/NA
Water 3010ALCS 490-496453/2-A Lab Control Sample Total/NA
Water 3010A490-146552-2 MS MW-4 Total/NA
Water 3010A490-146552-2 MSD MW-4 Total/NA
Analysis Batch: 496726
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 496453490-146552-1 MW-3 Total/NA
Water 6020B 496453490-146552-2 MW-4 Total/NA
Water 6020B 496453490-146552-3 MW-5 Total/NA
Water 6020B 496453490-146552-4 HHTMW-1 Total/NA
Water 6020B 496453490-146552-5 HHTMW-2 Total/NA
Water 6020B 496453490-146552-6 HHTMW-3 Total/NA
Water 6020B 496453490-146552-7 Duplicate-1 Total/NA
Water 6020B 496453MB 490-496453/1-A Method Blank Total/NA
Water 6020B 496453LCS 490-496453/2-A Lab Control Sample Total/NA
Water 6020B 496453490-146552-2 MS MW-4 Total/NA
Water 6020B 496453490-146552-2 MSD MW-4 Total/NA
Prep Batch: 496741
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A490-146552-1 MW-3 Total/NA
Water 7470A490-146552-2 MW-4 Total/NA
Water 7470A490-146552-3 MW-5 Total/NA
Water 7470A490-146552-4 HHTMW-1 Total/NA
Water 7470A490-146552-5 HHTMW-2 Total/NA
Water 7470A490-146552-6 HHTMW-3 Total/NA
Water 7470A490-146552-7 Duplicate-1 Total/NA
Water 7470AMB 490-496741/1-A Method Blank Total/NA
Water 7470ALCS 490-496741/2-A Lab Control Sample Total/NA
Water 7470A490-146532-A-1-F MS Matrix Spike Total/NA
Water 7470A490-146532-A-1-G MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 496802
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 496741MB 490-496741/1-A Method Blank Total/NA
Water 7470A 496741LCS 490-496741/2-A Lab Control Sample Total/NA
Water 7470A 496741490-146532-A-1-F MS Matrix Spike Total/NA
Water 7470A 496741490-146532-A-1-G MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 496822
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 496741490-146552-1 MW-3 Total/NA
Water 7470A 496741490-146552-2 MW-4 Total/NA
Water 7470A 496741490-146552-3 MW-5 Total/NA
Water 7470A 496741490-146552-4 HHTMW-1 Total/NA
Water 7470A 496741490-146552-5 HHTMW-2 Total/NA
TestAmerica Nashville
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QC Association Summary
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Metals (Continued)
Analysis Batch: 496822 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7470A 496741490-146552-6 HHTMW-3 Total/NA
Water 7470A 496741490-146552-7 Duplicate-1 Total/NA
General Chemistry
Analysis Batch: 496732
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 7196A490-146552-1 MW-3 Total/NA
Water 7196A490-146552-2 MW-4 Total/NA
Water 7196A490-146552-3 MW-5 Total/NA
Water 7196A490-146552-4 HHTMW-1 Total/NA
Water 7196A490-146552-5 HHTMW-2 Total/NA
Water 7196A490-146552-6 HHTMW-3 Total/NA
Water 7196A490-146552-7 Duplicate-1 Total/NA
Water 7196AMB 490-496732/2 Method Blank Total/NA
Water 7196ALCS 490-496732/3 Lab Control Sample Total/NA
Water 7196A490-146552-1 MS MW-3 Total/NA
Water 7196A490-146552-1 MSD MW-3 Total/NA
Water 7196A490-146552-1 DU MW-3 Total/NA
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146552-1
Project/Site: Little Rock Road Brownfields SDG: RKI.008
Client Sample ID: MW-3 Lab Sample ID: 490-146552-1
Matrix: WaterDate Collected: 02/16/18 12:50
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 21:381 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 496205 02/17/18 16:28 JKG TAL NSHTotal/NA 290 mL 1 mL
Analysis 8270D 1 496272 02/19/18 16:26 T1C TAL NSHTotal/NA
Prep 3010A 496453 02/19/18 15:26 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 496726 02/20/18 12:22 BLG TAL NSHTotal/NA
Prep 7470A 496741 02/20/18 15:50 RDH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 496822 02/20/18 19:49 RDH TAL NSHTotal/NA
Analysis 7196A 1 496732 02/17/18 10:53 SOG TAL NSHTotal/NA 10 mL 10 mL
Client Sample ID: MW-4 Lab Sample ID: 490-146552-2
Matrix: WaterDate Collected: 02/16/18 14:30
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 22:051 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 496205 02/17/18 16:28 JKG TAL NSHTotal/NA 290 mL 1 mL
Analysis 8270D 1 496272 02/19/18 16:47 T1C TAL NSHTotal/NA
Prep 3010A 496453 02/19/18 15:26 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 496726 02/20/18 12:07 BLG TAL NSHTotal/NA
Prep 7470A 496741 02/20/18 15:50 RDH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 496822 02/20/18 19:52 RDH TAL NSHTotal/NA
Analysis 7196A 1 496732 02/17/18 10:53 SOG TAL NSHTotal/NA 10 mL 10 mL
Client Sample ID: MW-5 Lab Sample ID: 490-146552-3
Matrix: WaterDate Collected: 02/16/18 16:40
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 22:311 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 496205 02/17/18 16:28 JKG TAL NSHTotal/NA 290 mL 1 mL
Analysis 8270D 1 496272 02/19/18 17:09 T1C TAL NSHTotal/NA
Prep 3010A 496453 02/19/18 15:26 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 496726 02/20/18 12:25 BLG TAL NSHTotal/NA
Prep 7470A 496741 02/20/18 15:50 RDH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 496822 02/20/18 19:55 RDH TAL NSHTotal/NA
Analysis 7196A 1 496732 02/17/18 10:53 SOG TAL NSHTotal/NA 10 mL 10 mL
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146552-1
Project/Site: Little Rock Road Brownfields SDG: RKI.008
Client Sample ID: HHTMW-1 Lab Sample ID: 490-146552-4
Matrix: WaterDate Collected: 02/16/18 19:10
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 22:581 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 496205 02/17/18 16:28 JKG TAL NSHTotal/NA 290 mL 1 mL
Analysis 8270D 1 496272 02/19/18 17:30 T1C TAL NSHTotal/NA
Prep 3010A 496453 02/19/18 15:26 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 496726 02/20/18 12:34 BLG TAL NSHTotal/NA
Prep 7470A 496741 02/20/18 15:50 RDH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 496822 02/20/18 19:57 RDH TAL NSHTotal/NA
Analysis 7196A 1 496732 02/17/18 10:53 SOG TAL NSHTotal/NA 10 mL 10 mL
Client Sample ID: HHTMW-2 Lab Sample ID: 490-146552-5
Matrix: WaterDate Collected: 02/16/18 18:25
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 23:241 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 496205 02/17/18 16:28 JKG TAL NSHTotal/NA 290 mL 1 mL
Analysis 8270D 1 496272 02/19/18 17:52 T1C TAL NSHTotal/NA
Prep 3010A 496453 02/19/18 15:26 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 496726 02/20/18 12:37 BLG TAL NSHTotal/NA
Prep 7470A 496741 02/20/18 15:50 RDH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 496822 02/20/18 20:00 RDH TAL NSHTotal/NA
Analysis 7196A 1 496732 02/17/18 10:53 SOG TAL NSHTotal/NA 10 mL 10 mL
Client Sample ID: HHTMW-3 Lab Sample ID: 490-146552-6
Matrix: WaterDate Collected: 02/16/18 15:40
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 23:511 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 496205 02/17/18 16:28 JKG TAL NSHTotal/NA 285 mL 1 mL
Analysis 8270D 1 496272 02/19/18 18:13 T1C TAL NSHTotal/NA
Prep 3010A 496453 02/19/18 15:26 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 496726 02/20/18 12:40 BLG TAL NSHTotal/NA
Prep 7470A 496741 02/20/18 15:50 RDH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 496822 02/20/18 20:03 RDH TAL NSHTotal/NA
Analysis 7196A 1 496732 02/17/18 10:53 SOG TAL NSHTotal/NA 10 mL 10 mL
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146552-1
Project/Site: Little Rock Road Brownfields SDG: RKI.008
Client Sample ID: Duplicate-1 Lab Sample ID: 490-146552-7
Matrix: WaterDate Collected: 02/16/18 13:30
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/18/18 00:181 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3510C 496205 02/17/18 16:28 JKG TAL NSHTotal/NA 290 mL 1 mL
Analysis 8270D 1 496272 02/19/18 18:34 T1C TAL NSHTotal/NA
Prep 3010A 496453 02/19/18 15:26 RDF TAL NSHTotal/NA 50 mL 50 mL
Analysis 6020B 1 496726 02/20/18 12:43 BLG TAL NSHTotal/NA
Prep 7470A 496741 02/20/18 15:50 RDH TAL NSHTotal/NA 30 mL 30 mL
Analysis 7470A 1 496822 02/20/18 20:06 RDH TAL NSHTotal/NA
Analysis 7196A 1 496732 02/17/18 10:53 SOG TAL NSHTotal/NA 10 mL 10 mL
Client Sample ID: Trip Blank 1 Lab Sample ID: 490-146552-8
Matrix: WaterDate Collected: 02/16/18 00:01
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 18:061 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Trip Blank 2 Lab Sample ID: 490-146552-9
Matrix: WaterDate Collected: 02/16/18 00:01
Date Received: 02/17/18 09:25
Analysis 8260B S1S02/17/18 18:321 TAL NSH496192
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-146552-1Client: Hart & Hickman, PC
SDG: RKI.008Project/Site: Little Rock Road Brownfields
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467470AMercury (CVAA)TAL NSH
SW8467196AChromium, Hexavalent TAL NSH
Protocol References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Accreditation/Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146552-1
Project/Site: Little Rock Road Brownfields SDG: RKI.008
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
South Carolina 84009 (001)4State Program 02-28-18 *
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but are not accredited/certified under this accreditation/certification:
8270D 3510C Water 3,3'-Dichlorobenzidine
8270D 3510C Water Carbazole
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
7196A Water Chromium, hex
8260B Water 1,2-Dichloroethene, Total
8270D 3510C Water 1-Methylnaphthalene
TestAmerica Nashville
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
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Page 64 of 64 2/26/2018 (Rev. 1)
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-146593-1
TestAmerica Sample Delivery Group: RKI-008
Client Project/Site: Little Rock Road Brownfield
Revision: 1
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Brett Lawrence
Authorized for release by:
2/26/2018 5:56:20 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Little Rock Road Brownfield
TestAmerica Job ID: 490-146593-1
SDG: RKI-008
Page 2 of 55 TestAmerica Nashville2/26/2018 (Rev. 1)
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .45
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .49
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .53
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54
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Sample Summary
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-146593-1 HHSB-1 (1-2)Solid 02/15/18 10:05 02/17/18 09:25
490-146593-2 HHSB-2 (1-2)Solid 02/15/18 15:35 02/17/18 09:25
490-146593-3 HHSB-3 (0-1)Solid 02/15/18 16:50 02/17/18 09:25
490-146593-4 Duplicate-2 Solid 02/15/18 16:45 02/17/18 09:25
490-146593-5 HHSB-4 (1-2)Solid 02/16/18 09:30 02/17/18 09:25
490-146593-6 HHSB-5 (0-1)Solid 02/16/18 09:00 02/17/18 09:25
490-146593-7 BKG-1 (1-2)Solid 02/16/18 10:30 02/17/18 09:25
490-146593-8 BKG-2 (1-2)Solid 02/16/18 11:00 02/17/18 09:25
TestAmerica Nashville
Page 3 of 55 2/26/2018 (Rev. 1)
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146593-1
Project/Site: Little Rock Road Brownfield SDG: RKI-008
Job ID: 490-146593-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-146593-1
REVISED REPORT: Revised to change the semple ID of 490-146552-7 from HHSB-3 (1-2) to Duplicate-2 at the client's request. This report
replaces the one generated on 02/22/18 @ 1427.
Comments
No additional comments.
Receipt
The samples were received on 2/17/2018 9:25 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.8º C.
GC/MS VOA
Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-496298.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 490-496428 and analytical batch 490-496518.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Qualifiers
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-1Client Sample ID: HHSB-1 (1-2)
Matrix: SolidDate Collected: 02/15/18 10:05
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0435 mg/Kg ☼02/15/18 09:05 02/19/18 13:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Benzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Bromobenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Bromochloromethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Bromodichloromethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Bromoform ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼Bromomethane ND
0.0435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼2-Butanone (MEK)ND
0.00435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Carbon disulfide ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Carbon tetrachloride ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Chlorobenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Chlorodibromomethane ND
0.00435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Chloroethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Chloroform ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Chloromethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼2-Chlorotoluene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼4-Chlorotoluene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼cis-1,2-Dichloroethene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼cis-1,3-Dichloropropene ND
0.00435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼1,2-Dibromo-3-Chloropropane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2-Dibromoethane (EDB)ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Dibromomethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2-Dichlorobenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,3-Dichlorobenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼1,4-Dichlorobenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Dichlorodifluoromethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,1-Dichloroethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2-Dichloroethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼1,1-Dichloroethene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2-Dichloroethene, Total ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2-Dichloropropane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,3-Dichloropropane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼2,2-Dichloropropane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼1,1-Dichloropropene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Diisopropyl ether ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Ethylbenzene ND
0.00435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Hexachlorobutadiene ND
0.0435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼2-Hexanone ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Isopropylbenzene ND
0.00869 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Methylene Chloride ND
0.0435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼4-Methyl-2-pentanone (MIBK)ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Methyl tert-butyl ether ND
0.00435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼Naphthalene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼n-Butylbenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼N-Propylbenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼p-Isopropyltoluene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼sec-Butylbenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Styrene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-1Client Sample ID: HHSB-1 (1-2)
Matrix: SolidDate Collected: 02/15/18 10:05
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00174 mg/Kg ☼02/15/18 09:05 02/19/18 13:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,1,2,2-Tetrachloroethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼Tetrachloroethene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Toluene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼trans-1,2-Dichloroethene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼trans-1,3-Dichloropropene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼1,2,3-Trichlorobenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2,4-Trichlorobenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,1,1-Trichloroethane ND
0.00435 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,1,2-Trichloroethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Trichloroethene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼Trichlorofluoromethane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2,3-Trichloropropane ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,2,4-Trimethylbenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼1,3,5-Trimethylbenzene ND
0.00174 mg/Kg 02/15/18 09:05 02/19/18 13:53 1☼Vinyl chloride ND
0.00521 mg/Kg 02/15/18 09:05 02/19/18 13:53 1
☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)90 70-130 02/15/18 09:05 02/19/18 13:53 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)114 02/15/18 09:05 02/19/18 13:53 170-130
1,2-Dichloroethane-d4 (Surr)98 02/15/18 09:05 02/19/18 13:53 170-130
Toluene-d8 (Surr)94 02/15/18 09:05 02/19/18 13:53 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0828 mg/Kg ☼02/19/18 14:03 02/20/18 13:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Acenaphthylene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Anthracene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼Benzo[a]anthracene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Benzo[a]pyrene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Benzo[b]fluoranthene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Benzo[g,h,i]perylene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼Benzo[k]fluoranthene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Bis(2-chloroethoxy)methane ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Bis(2-chloroethyl)ether ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼bis (2-chloroisopropyl) ether ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Bis(2-ethylhexyl) phthalate ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼4-Bromophenyl phenyl ether ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Butyl benzyl phthalate ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Carbazole ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼4-Chloroaniline ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼4-Chloro-3-methylphenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2-Chloronaphthalene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2-Chlorophenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼4-Chlorophenyl phenyl ether ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼Chrysene ND
0.823 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Cresols ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Dibenz(a,h)anthracene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-1Client Sample ID: HHSB-1 (1-2)
Matrix: SolidDate Collected: 02/15/18 10:05
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.412 mg/Kg ☼02/19/18 14:03 02/20/18 13:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼1,3-Dichlorobenzene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼1,4-Dichlorobenzene ND
0.828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼3,3'-Dichlorobenzidine ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2,4-Dichlorophenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Diethyl phthalate ND
0.828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼2,4-Dimethylphenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Dimethyl phthalate ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Di-n-butyl phthalate ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼4,6-Dinitro-2-methylphenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2,4-Dinitrophenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼2,4-Dinitrotoluene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2,6-Dinitrotoluene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Di-n-octyl phthalate ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Fluoranthene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼Fluorene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Hexachlorobenzene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Hexachlorobutadiene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Hexachlorocyclopentadiene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Hexachloroethane ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼Indeno[1,2,3-cd]pyrene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Isophorone ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼1-Methylnaphthalene ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2-Methylnaphthalene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼2-Methylphenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼3 & 4 Methylphenol ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Naphthalene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2-Nitroaniline ND
0.828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼3-Nitroaniline ND
0.828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼4-Nitroaniline ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Nitrobenzene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2-Nitrophenol ND
0.828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼4-Nitrophenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼N-Nitrosodi-n-propylamine ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Pentachlorophenol ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Phenanthrene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼Phenol ND
0.0828 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼Pyrene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼1,2,4-Trichlorobenzene ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1
☼2,4,5-Trichlorophenol ND
0.412 mg/Kg 02/19/18 14:03 02/20/18 13:58 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)53 29-120 02/19/18 14:03 02/20/18 13:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)46 02/19/18 14:03 02/20/18 13:58 110-120
Nitrobenzene-d5 (Surr)46 02/19/18 14:03 02/20/18 13:58 127-120
Phenol-d5 (Surr)46 02/19/18 14:03 02/20/18 13:58 110-120
Terphenyl-d14 (Surr)74 02/19/18 14:03 02/20/18 13:58 113-120
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-1Client Sample ID: HHSB-1 (1-2)
Matrix: SolidDate Collected: 02/15/18 10:05
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)63 10-120 02/19/18 14:03 02/20/18 13:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.48 0.592 mg/Kg ☼02/19/18 09:17 02/20/18 10:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.592 mg/Kg 02/19/18 09:17 02/20/18 10:18 1
☼Barium 5.03
0.592 mg/Kg 02/19/18 09:17 02/20/18 10:18 1☼Cadmium ND
0.592 mg/Kg 02/19/18 09:17 02/20/18 10:18 1
☼Chromium 9.40 F1
0.592 mg/Kg 02/19/18 09:17 02/20/18 10:18 1
☼Lead 5.21
0.592 mg/Kg 02/19/18 09:17 02/20/18 10:18 1
☼Selenium ND
0.592 mg/Kg 02/19/18 09:17 02/20/18 10:18 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.126 mg/Kg ☼02/20/18 10:01 02/20/18 15:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 6.15 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 79.7 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-2Client Sample ID: HHSB-2 (1-2)
Matrix: SolidDate Collected: 02/15/18 15:35
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0574 0.0460 mg/Kg ☼02/15/18 14:35 02/19/18 14:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Benzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Bromobenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Bromochloromethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Bromodichloromethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Bromoform ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼Bromomethane ND
0.0460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼2-Butanone (MEK)ND
0.00460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Carbon disulfide ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Carbon tetrachloride ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Chlorobenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Chlorodibromomethane ND
0.00460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Chloroethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Chloroform ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Chloromethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼2-Chlorotoluene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼4-Chlorotoluene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼cis-1,2-Dichloroethene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼cis-1,3-Dichloropropene ND
0.00460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼1,2-Dibromo-3-Chloropropane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2-Dibromoethane (EDB)ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Dibromomethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2-Dichlorobenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,3-Dichlorobenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼1,4-Dichlorobenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Dichlorodifluoromethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,1-Dichloroethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2-Dichloroethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼1,1-Dichloroethene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2-Dichloroethene, Total ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2-Dichloropropane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,3-Dichloropropane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼2,2-Dichloropropane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼1,1-Dichloropropene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Diisopropyl ether ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Ethylbenzene ND
0.00460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Hexachlorobutadiene ND
0.0460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼2-Hexanone ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Isopropylbenzene ND
0.00921 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Methylene Chloride ND
0.0460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼4-Methyl-2-pentanone (MIBK)ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Methyl tert-butyl ether ND
0.00460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼Naphthalene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼n-Butylbenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼N-Propylbenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼p-Isopropyltoluene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼sec-Butylbenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Styrene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼tert-Butylbenzene ND
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-2Client Sample ID: HHSB-2 (1-2)
Matrix: SolidDate Collected: 02/15/18 15:35
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00184 mg/Kg ☼02/15/18 14:35 02/19/18 14:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,1,2,2-Tetrachloroethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼Tetrachloroethene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Toluene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼trans-1,2-Dichloroethene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼trans-1,3-Dichloropropene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼1,2,3-Trichlorobenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2,4-Trichlorobenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,1,1-Trichloroethane ND
0.00460 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,1,2-Trichloroethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Trichloroethene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼Trichlorofluoromethane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2,3-Trichloropropane ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,2,4-Trimethylbenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼1,3,5-Trimethylbenzene ND
0.00184 mg/Kg 02/15/18 14:35 02/19/18 14:20 1☼Vinyl chloride ND
0.00552 mg/Kg 02/15/18 14:35 02/19/18 14:20 1
☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)90 70-130 02/15/18 14:35 02/19/18 14:20 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)114 02/15/18 14:35 02/19/18 14:20 170-130
1,2-Dichloroethane-d4 (Surr)101 02/15/18 14:35 02/19/18 14:20 170-130
Toluene-d8 (Surr)95 02/15/18 14:35 02/19/18 14:20 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0806 mg/Kg ☼02/19/18 14:03 02/20/18 14:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Acenaphthylene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Anthracene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼Benzo[a]anthracene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Benzo[a]pyrene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Benzo[b]fluoranthene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Benzo[g,h,i]perylene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼Benzo[k]fluoranthene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Bis(2-chloroethoxy)methane ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Bis(2-chloroethyl)ether ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼bis (2-chloroisopropyl) ether ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Bis(2-ethylhexyl) phthalate ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼4-Bromophenyl phenyl ether ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Butyl benzyl phthalate ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Carbazole ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼4-Chloroaniline ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼4-Chloro-3-methylphenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2-Chloronaphthalene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2-Chlorophenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼4-Chlorophenyl phenyl ether ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼Chrysene ND
0.802 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Cresols ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Dibenz(a,h)anthracene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-2Client Sample ID: HHSB-2 (1-2)
Matrix: SolidDate Collected: 02/15/18 15:35
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.401 mg/Kg ☼02/19/18 14:03 02/20/18 14:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼1,3-Dichlorobenzene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼1,4-Dichlorobenzene ND
0.806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼3,3'-Dichlorobenzidine ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2,4-Dichlorophenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Diethyl phthalate ND
0.806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼2,4-Dimethylphenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Dimethyl phthalate ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Di-n-butyl phthalate ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼4,6-Dinitro-2-methylphenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2,4-Dinitrophenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼2,4-Dinitrotoluene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2,6-Dinitrotoluene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Di-n-octyl phthalate ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Fluoranthene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼Fluorene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Hexachlorobenzene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Hexachlorobutadiene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Hexachlorocyclopentadiene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Hexachloroethane ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼Indeno[1,2,3-cd]pyrene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Isophorone ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼1-Methylnaphthalene ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2-Methylnaphthalene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼2-Methylphenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼3 & 4 Methylphenol ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Naphthalene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2-Nitroaniline ND
0.806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼3-Nitroaniline ND
0.806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼4-Nitroaniline ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Nitrobenzene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2-Nitrophenol ND
0.806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼4-Nitrophenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼N-Nitrosodi-n-propylamine ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Pentachlorophenol ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Phenanthrene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼Phenol ND
0.0806 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼Pyrene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼1,2,4-Trichlorobenzene ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1
☼2,4,5-Trichlorophenol ND
0.401 mg/Kg 02/19/18 14:03 02/20/18 14:18 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)76 29-120 02/19/18 14:03 02/20/18 14:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)71 02/19/18 14:03 02/20/18 14:18 110-120
Nitrobenzene-d5 (Surr)72 02/19/18 14:03 02/20/18 14:18 127-120
Phenol-d5 (Surr)72 02/19/18 14:03 02/20/18 14:18 110-120
Terphenyl-d14 (Surr)94 02/19/18 14:03 02/20/18 14:18 113-120
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-2Client Sample ID: HHSB-2 (1-2)
Matrix: SolidDate Collected: 02/15/18 15:35
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)79 10-120 02/19/18 14:03 02/20/18 14:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 2.68 0.596 mg/Kg ☼02/19/18 09:17 02/20/18 10:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.596 mg/Kg 02/19/18 09:17 02/20/18 10:33 1
☼Barium 28.2
0.596 mg/Kg 02/19/18 09:17 02/20/18 10:33 1☼Cadmium ND
0.596 mg/Kg 02/19/18 09:17 02/20/18 10:33 1
☼Chromium 24.8
0.596 mg/Kg 02/19/18 09:17 02/20/18 10:33 1
☼Lead 9.44
0.596 mg/Kg 02/19/18 09:17 02/20/18 10:33 1
☼Selenium ND
0.596 mg/Kg 02/19/18 09:17 02/20/18 10:33 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.121 mg/Kg ☼02/20/18 10:01 02/20/18 15:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 6.13 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 80.6 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Nashville
Page 13 of 55 2/26/2018 (Rev. 1)
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-3Client Sample ID: HHSB-3 (0-1)
Matrix: SolidDate Collected: 02/15/18 16:50
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0529 0.0520 mg/Kg ☼02/15/18 15:50 02/19/18 14:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Benzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Bromobenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Bromochloromethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Bromodichloromethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Bromoform ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼Bromomethane ND
0.0520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼2-Butanone (MEK)ND
0.00520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Carbon disulfide ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Carbon tetrachloride ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Chlorobenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Chlorodibromomethane ND
0.00520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Chloroethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Chloroform ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Chloromethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼2-Chlorotoluene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼4-Chlorotoluene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼cis-1,2-Dichloroethene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼cis-1,3-Dichloropropene ND
0.00520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼1,2-Dibromo-3-Chloropropane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2-Dibromoethane (EDB)ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Dibromomethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2-Dichlorobenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,3-Dichlorobenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼1,4-Dichlorobenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Dichlorodifluoromethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,1-Dichloroethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2-Dichloroethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼1,1-Dichloroethene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2-Dichloroethene, Total ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2-Dichloropropane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,3-Dichloropropane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼2,2-Dichloropropane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼1,1-Dichloropropene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Diisopropyl ether ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Ethylbenzene ND
0.00520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Hexachlorobutadiene ND
0.0520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼2-Hexanone ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Isopropylbenzene ND
0.0104 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Methylene Chloride ND
0.0520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼4-Methyl-2-pentanone (MIBK)ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Methyl tert-butyl ether ND
0.00520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼Naphthalene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼n-Butylbenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼N-Propylbenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼p-Isopropyltoluene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼sec-Butylbenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Styrene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-3Client Sample ID: HHSB-3 (0-1)
Matrix: SolidDate Collected: 02/15/18 16:50
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00208 mg/Kg ☼02/15/18 15:50 02/19/18 14:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,1,2,2-Tetrachloroethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼Tetrachloroethene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Toluene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼trans-1,2-Dichloroethene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼trans-1,3-Dichloropropene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼1,2,3-Trichlorobenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2,4-Trichlorobenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,1,1-Trichloroethane ND
0.00520 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,1,2-Trichloroethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Trichloroethene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼Trichlorofluoromethane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2,3-Trichloropropane ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,2,4-Trimethylbenzene 0.00311
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼1,3,5-Trimethylbenzene ND
0.00208 mg/Kg 02/15/18 15:50 02/19/18 14:48 1☼Vinyl chloride ND
0.00624 mg/Kg 02/15/18 15:50 02/19/18 14:48 1
☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)114 70-130 02/15/18 15:50 02/19/18 14:48 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)113 02/15/18 15:50 02/19/18 14:48 170-130
1,2-Dichloroethane-d4 (Surr)97 02/15/18 15:50 02/19/18 14:48 170-130
Toluene-d8 (Surr)101 02/15/18 15:50 02/19/18 14:48 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0886 mg/Kg ☼02/19/18 14:03 02/20/18 14:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Acenaphthylene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Anthracene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼Benzo[a]anthracene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Benzo[a]pyrene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Benzo[b]fluoranthene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Benzo[g,h,i]perylene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼Benzo[k]fluoranthene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Bis(2-chloroethoxy)methane ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Bis(2-chloroethyl)ether ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼bis (2-chloroisopropyl) ether ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Bis(2-ethylhexyl) phthalate ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼4-Bromophenyl phenyl ether ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Butyl benzyl phthalate ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Carbazole ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼4-Chloroaniline ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼4-Chloro-3-methylphenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2-Chloronaphthalene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2-Chlorophenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼4-Chlorophenyl phenyl ether ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼Chrysene ND
0.880 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Cresols ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Dibenz(a,h)anthracene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-3Client Sample ID: HHSB-3 (0-1)
Matrix: SolidDate Collected: 02/15/18 16:50
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.440 mg/Kg ☼02/19/18 14:03 02/20/18 14:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼1,3-Dichlorobenzene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼1,4-Dichlorobenzene ND
0.886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼3,3'-Dichlorobenzidine ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2,4-Dichlorophenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Diethyl phthalate ND
0.886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼2,4-Dimethylphenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Dimethyl phthalate ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Di-n-butyl phthalate ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼4,6-Dinitro-2-methylphenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2,4-Dinitrophenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼2,4-Dinitrotoluene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2,6-Dinitrotoluene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Di-n-octyl phthalate ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Fluoranthene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼Fluorene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Hexachlorobenzene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Hexachlorobutadiene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Hexachlorocyclopentadiene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Hexachloroethane ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼Indeno[1,2,3-cd]pyrene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Isophorone ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼1-Methylnaphthalene ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2-Methylnaphthalene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼2-Methylphenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼3 & 4 Methylphenol ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Naphthalene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2-Nitroaniline ND
0.886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼3-Nitroaniline ND
0.886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼4-Nitroaniline ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Nitrobenzene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2-Nitrophenol ND
0.886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼4-Nitrophenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼N-Nitrosodi-n-propylamine ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Pentachlorophenol ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Phenanthrene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼Phenol ND
0.0886 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼Pyrene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼1,2,4-Trichlorobenzene ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1
☼2,4,5-Trichlorophenol ND
0.440 mg/Kg 02/19/18 14:03 02/20/18 14:39 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)66 29-120 02/19/18 14:03 02/20/18 14:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)54 02/19/18 14:03 02/20/18 14:39 110-120
Nitrobenzene-d5 (Surr)57 02/19/18 14:03 02/20/18 14:39 127-120
Phenol-d5 (Surr)61 02/19/18 14:03 02/20/18 14:39 110-120
Terphenyl-d14 (Surr)91 02/19/18 14:03 02/20/18 14:39 113-120
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-3Client Sample ID: HHSB-3 (0-1)
Matrix: SolidDate Collected: 02/15/18 16:50
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)82 10-120 02/19/18 14:03 02/20/18 14:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 2.77 0.566 mg/Kg ☼02/19/18 09:17 02/20/18 10:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.566 mg/Kg 02/19/18 09:17 02/20/18 10:37 1
☼Barium 35.5
0.566 mg/Kg 02/19/18 09:17 02/20/18 10:37 1☼Cadmium ND
0.566 mg/Kg 02/19/18 09:17 02/20/18 10:37 1
☼Chromium 20.2
0.566 mg/Kg 02/19/18 09:17 02/20/18 10:37 1
☼Lead 21.9
0.566 mg/Kg 02/19/18 09:17 02/20/18 10:37 1
☼Selenium 0.815
0.566 mg/Kg 02/19/18 09:17 02/20/18 10:37 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.132 mg/Kg ☼02/20/18 10:01 02/20/18 15:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 6.62 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 74.9 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-4Client Sample ID: Duplicate-2
Matrix: SolidDate Collected: 02/15/18 16:45
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0671 0.0402 mg/Kg ☼02/15/18 15:45 02/19/18 15:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Benzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Bromobenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Bromochloromethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Bromodichloromethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Bromoform ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼Bromomethane ND
0.0402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼2-Butanone (MEK)ND
0.00402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Carbon disulfide ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Carbon tetrachloride ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Chlorobenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Chlorodibromomethane ND
0.00402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Chloroethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Chloroform ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Chloromethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼2-Chlorotoluene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼4-Chlorotoluene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼cis-1,2-Dichloroethene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼cis-1,3-Dichloropropene ND
0.00402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼1,2-Dibromo-3-Chloropropane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2-Dibromoethane (EDB)ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Dibromomethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2-Dichlorobenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,3-Dichlorobenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼1,4-Dichlorobenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Dichlorodifluoromethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,1-Dichloroethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2-Dichloroethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼1,1-Dichloroethene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2-Dichloroethene, Total ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2-Dichloropropane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,3-Dichloropropane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼2,2-Dichloropropane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼1,1-Dichloropropene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Diisopropyl ether ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Ethylbenzene ND
0.00402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Hexachlorobutadiene ND
0.0402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼2-Hexanone ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Isopropylbenzene ND
0.00803 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Methylene Chloride ND
0.0402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼4-Methyl-2-pentanone (MIBK)ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Methyl tert-butyl ether ND
0.00402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼Naphthalene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼n-Butylbenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼N-Propylbenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼p-Isopropyltoluene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼sec-Butylbenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Styrene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼tert-Butylbenzene ND
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-4Client Sample ID: Duplicate-2
Matrix: SolidDate Collected: 02/15/18 16:45
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00161 mg/Kg ☼02/15/18 15:45 02/19/18 15:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,1,2,2-Tetrachloroethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼Tetrachloroethene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Toluene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼trans-1,2-Dichloroethene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼trans-1,3-Dichloropropene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼1,2,3-Trichlorobenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2,4-Trichlorobenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,1,1-Trichloroethane ND
0.00402 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,1,2-Trichloroethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Trichloroethene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼Trichlorofluoromethane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2,3-Trichloropropane ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,2,4-Trimethylbenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼1,3,5-Trimethylbenzene ND
0.00161 mg/Kg 02/15/18 15:45 02/19/18 15:16 1☼Vinyl chloride ND
0.00482 mg/Kg 02/15/18 15:45 02/19/18 15:16 1
☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)92 70-130 02/15/18 15:45 02/19/18 15:16 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)113 02/15/18 15:45 02/19/18 15:16 170-130
1,2-Dichloroethane-d4 (Surr)100 02/15/18 15:45 02/19/18 15:16 170-130
Toluene-d8 (Surr)96 02/15/18 15:45 02/19/18 15:16 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0814 mg/Kg ☼02/19/18 14:03 02/20/18 14:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Acenaphthylene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Anthracene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼Benzo[a]anthracene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Benzo[a]pyrene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Benzo[b]fluoranthene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Benzo[g,h,i]perylene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼Benzo[k]fluoranthene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Bis(2-chloroethoxy)methane ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Bis(2-chloroethyl)ether ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼bis (2-chloroisopropyl) ether ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Bis(2-ethylhexyl) phthalate ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼4-Bromophenyl phenyl ether ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Butyl benzyl phthalate ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Carbazole ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼4-Chloroaniline ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼4-Chloro-3-methylphenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2-Chloronaphthalene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2-Chlorophenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼4-Chlorophenyl phenyl ether ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼Chrysene ND
0.809 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Cresols ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Dibenz(a,h)anthracene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-4Client Sample ID: Duplicate-2
Matrix: SolidDate Collected: 02/15/18 16:45
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.405 mg/Kg ☼02/19/18 14:03 02/20/18 14:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼1,3-Dichlorobenzene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼1,4-Dichlorobenzene ND
0.814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼3,3'-Dichlorobenzidine ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2,4-Dichlorophenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Diethyl phthalate ND
0.814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼2,4-Dimethylphenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Dimethyl phthalate ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Di-n-butyl phthalate ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼4,6-Dinitro-2-methylphenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2,4-Dinitrophenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼2,4-Dinitrotoluene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2,6-Dinitrotoluene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Di-n-octyl phthalate ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Fluoranthene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼Fluorene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Hexachlorobenzene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Hexachlorobutadiene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Hexachlorocyclopentadiene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Hexachloroethane ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼Indeno[1,2,3-cd]pyrene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Isophorone ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼1-Methylnaphthalene ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2-Methylnaphthalene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼2-Methylphenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼3 & 4 Methylphenol ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Naphthalene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2-Nitroaniline ND
0.814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼3-Nitroaniline ND
0.814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼4-Nitroaniline ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Nitrobenzene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2-Nitrophenol ND
0.814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼4-Nitrophenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼N-Nitrosodi-n-propylamine ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Pentachlorophenol ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Phenanthrene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼Phenol ND
0.0814 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼Pyrene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼1,2,4-Trichlorobenzene ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1
☼2,4,5-Trichlorophenol ND
0.405 mg/Kg 02/19/18 14:03 02/20/18 14:59 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)67 29-120 02/19/18 14:03 02/20/18 14:59 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)64 02/19/18 14:03 02/20/18 14:59 110-120
Nitrobenzene-d5 (Surr)65 02/19/18 14:03 02/20/18 14:59 127-120
Phenol-d5 (Surr)65 02/19/18 14:03 02/20/18 14:59 110-120
Terphenyl-d14 (Surr)87 02/19/18 14:03 02/20/18 14:59 113-120
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-4Client Sample ID: Duplicate-2
Matrix: SolidDate Collected: 02/15/18 16:45
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)78 10-120 02/19/18 14:03 02/20/18 14:59 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 2.64 0.557 mg/Kg ☼02/19/18 09:17 02/20/18 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.557 mg/Kg 02/19/18 09:17 02/20/18 10:46 1
☼Barium 53.1
0.557 mg/Kg 02/19/18 09:17 02/20/18 10:46 1☼Cadmium ND
0.557 mg/Kg 02/19/18 09:17 02/20/18 10:46 1
☼Chromium 30.6
0.557 mg/Kg 02/19/18 09:17 02/20/18 10:46 1
☼Lead 12.6
0.557 mg/Kg 02/19/18 09:17 02/20/18 10:46 1
☼Selenium ND
0.557 mg/Kg 02/19/18 09:17 02/20/18 10:46 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.121 mg/Kg ☼02/20/18 10:01 02/20/18 15:50 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 6.15 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 81.6 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-5Client Sample ID: HHSB-4 (1-2)
Matrix: SolidDate Collected: 02/16/18 09:30
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0432 mg/Kg ☼02/16/18 08:30 02/19/18 15:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Benzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Bromobenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Bromochloromethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Bromodichloromethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Bromoform ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼Bromomethane ND
0.0432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼2-Butanone (MEK)ND
0.00432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Carbon disulfide ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Carbon tetrachloride ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Chlorobenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Chlorodibromomethane ND
0.00432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Chloroethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Chloroform ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Chloromethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼2-Chlorotoluene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼4-Chlorotoluene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼cis-1,2-Dichloroethene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼cis-1,3-Dichloropropene ND
0.00432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼1,2-Dibromo-3-Chloropropane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2-Dibromoethane (EDB)ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Dibromomethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2-Dichlorobenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,3-Dichlorobenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼1,4-Dichlorobenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Dichlorodifluoromethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,1-Dichloroethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2-Dichloroethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼1,1-Dichloroethene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2-Dichloroethene, Total ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2-Dichloropropane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,3-Dichloropropane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼2,2-Dichloropropane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼1,1-Dichloropropene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Diisopropyl ether ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Ethylbenzene ND
0.00432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Hexachlorobutadiene ND
0.0432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼2-Hexanone ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Isopropylbenzene ND
0.00865 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Methylene Chloride ND
0.0432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼4-Methyl-2-pentanone (MIBK)ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Methyl tert-butyl ether ND
0.00432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼Naphthalene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼n-Butylbenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼N-Propylbenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼p-Isopropyltoluene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼sec-Butylbenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Styrene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-5Client Sample ID: HHSB-4 (1-2)
Matrix: SolidDate Collected: 02/16/18 09:30
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00173 mg/Kg ☼02/16/18 08:30 02/19/18 15:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,1,2,2-Tetrachloroethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼Tetrachloroethene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Toluene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼trans-1,2-Dichloroethene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼trans-1,3-Dichloropropene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼1,2,3-Trichlorobenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2,4-Trichlorobenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,1,1-Trichloroethane ND
0.00432 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,1,2-Trichloroethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Trichloroethene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼Trichlorofluoromethane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2,3-Trichloropropane ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,2,4-Trimethylbenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼1,3,5-Trimethylbenzene ND
0.00173 mg/Kg 02/16/18 08:30 02/19/18 15:44 1☼Vinyl chloride ND
0.00519 mg/Kg 02/16/18 08:30 02/19/18 15:44 1
☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)90 70-130 02/16/18 08:30 02/19/18 15:44 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)117 02/16/18 08:30 02/19/18 15:44 170-130
1,2-Dichloroethane-d4 (Surr)100 02/16/18 08:30 02/19/18 15:44 170-130
Toluene-d8 (Surr)96 02/16/18 08:30 02/19/18 15:44 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0842 mg/Kg ☼02/19/18 14:03 02/21/18 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Acenaphthylene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Anthracene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼Benzo[a]anthracene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Benzo[a]pyrene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Benzo[b]fluoranthene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Benzo[g,h,i]perylene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼Benzo[k]fluoranthene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Bis(2-chloroethoxy)methane ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Bis(2-chloroethyl)ether ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼bis (2-chloroisopropyl) ether ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Bis(2-ethylhexyl) phthalate ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼4-Bromophenyl phenyl ether ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Butyl benzyl phthalate ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Carbazole ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼4-Chloroaniline ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼4-Chloro-3-methylphenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2-Chloronaphthalene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2-Chlorophenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼4-Chlorophenyl phenyl ether ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼Chrysene ND
0.837 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Cresols ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Dibenz(a,h)anthracene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-5Client Sample ID: HHSB-4 (1-2)
Matrix: SolidDate Collected: 02/16/18 09:30
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.419 mg/Kg ☼02/19/18 14:03 02/21/18 10:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼1,3-Dichlorobenzene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼1,4-Dichlorobenzene ND
0.842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼3,3'-Dichlorobenzidine ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2,4-Dichlorophenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Diethyl phthalate ND
0.842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼2,4-Dimethylphenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Dimethyl phthalate ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Di-n-butyl phthalate ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼4,6-Dinitro-2-methylphenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2,4-Dinitrophenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼2,4-Dinitrotoluene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2,6-Dinitrotoluene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Di-n-octyl phthalate ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Fluoranthene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼Fluorene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Hexachlorobenzene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Hexachlorobutadiene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Hexachlorocyclopentadiene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Hexachloroethane ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼Indeno[1,2,3-cd]pyrene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Isophorone ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼1-Methylnaphthalene ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2-Methylnaphthalene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼2-Methylphenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼3 & 4 Methylphenol ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Naphthalene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2-Nitroaniline ND
0.842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼3-Nitroaniline ND
0.842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼4-Nitroaniline ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Nitrobenzene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2-Nitrophenol ND
0.842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼4-Nitrophenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼N-Nitrosodi-n-propylamine ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Pentachlorophenol ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Phenanthrene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼Phenol ND
0.0842 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼Pyrene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼1,2,4-Trichlorobenzene ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1
☼2,4,5-Trichlorophenol ND
0.419 mg/Kg 02/19/18 14:03 02/21/18 10:45 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)67 29-120 02/19/18 14:03 02/21/18 10:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)71 02/19/18 14:03 02/21/18 10:45 110-120
Nitrobenzene-d5 (Surr)69 02/19/18 14:03 02/21/18 10:45 127-120
Phenol-d5 (Surr)77 02/19/18 14:03 02/21/18 10:45 110-120
Terphenyl-d14 (Surr)82 02/19/18 14:03 02/21/18 10:45 113-120
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-5Client Sample ID: HHSB-4 (1-2)
Matrix: SolidDate Collected: 02/16/18 09:30
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)99 10-120 02/19/18 14:03 02/21/18 10:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 4.13 0.554 mg/Kg ☼02/19/18 09:17 02/20/18 10:49 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.554 mg/Kg 02/19/18 09:17 02/20/18 10:49 1
☼Barium 26.6
0.554 mg/Kg 02/19/18 09:17 02/20/18 10:49 1☼Cadmium ND
0.554 mg/Kg 02/19/18 09:17 02/20/18 10:49 1
☼Chromium 30.2
0.554 mg/Kg 02/19/18 09:17 02/20/18 10:49 1
☼Lead 11.6
0.554 mg/Kg 02/19/18 09:17 02/20/18 10:49 1
☼Selenium 1.33
0.554 mg/Kg 02/19/18 09:17 02/20/18 10:49 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.127 mg/Kg ☼02/20/18 10:01 02/20/18 15:53 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 6.36 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 77.9 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-6Client Sample ID: HHSB-5 (0-1)
Matrix: SolidDate Collected: 02/16/18 09:00
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0716 0.0454 mg/Kg ☼02/16/18 08:00 02/19/18 16:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Benzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Bromobenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Bromochloromethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Bromodichloromethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Bromoform ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼Bromomethane ND
0.0454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼2-Butanone (MEK)ND
0.00454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Carbon disulfide ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Carbon tetrachloride ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Chlorobenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Chlorodibromomethane ND
0.00454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Chloroethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Chloroform ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Chloromethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼2-Chlorotoluene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼4-Chlorotoluene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼cis-1,2-Dichloroethene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼cis-1,3-Dichloropropene ND
0.00454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼1,2-Dibromo-3-Chloropropane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2-Dibromoethane (EDB)ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Dibromomethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2-Dichlorobenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,3-Dichlorobenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼1,4-Dichlorobenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Dichlorodifluoromethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,1-Dichloroethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2-Dichloroethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼1,1-Dichloroethene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2-Dichloroethene, Total ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2-Dichloropropane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,3-Dichloropropane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼2,2-Dichloropropane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼1,1-Dichloropropene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Diisopropyl ether ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Ethylbenzene ND
0.00454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Hexachlorobutadiene ND
0.0454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼2-Hexanone ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Isopropylbenzene ND
0.00908 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Methylene Chloride ND
0.0454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼4-Methyl-2-pentanone (MIBK)ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Methyl tert-butyl ether ND
0.00454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼Naphthalene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼n-Butylbenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼N-Propylbenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼p-Isopropyltoluene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼sec-Butylbenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Styrene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-6Client Sample ID: HHSB-5 (0-1)
Matrix: SolidDate Collected: 02/16/18 09:00
Date Received: 02/17/18 09:25
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00182 mg/Kg ☼02/16/18 08:00 02/19/18 16:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,1,2,2-Tetrachloroethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼Tetrachloroethene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Toluene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼trans-1,2-Dichloroethene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼trans-1,3-Dichloropropene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼1,2,3-Trichlorobenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2,4-Trichlorobenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,1,1-Trichloroethane ND
0.00454 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,1,2-Trichloroethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Trichloroethene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼Trichlorofluoromethane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2,3-Trichloropropane ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,2,4-Trimethylbenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼1,3,5-Trimethylbenzene ND
0.00182 mg/Kg 02/16/18 08:00 02/19/18 16:11 1☼Vinyl chloride ND
0.00545 mg/Kg 02/16/18 08:00 02/19/18 16:11 1
☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)97 70-130 02/16/18 08:00 02/19/18 16:11 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Dibromofluoromethane (Surr)114 02/16/18 08:00 02/19/18 16:11 170-130
1,2-Dichloroethane-d4 (Surr)96 02/16/18 08:00 02/19/18 16:11 170-130
Toluene-d8 (Surr)99 02/16/18 08:00 02/19/18 16:11 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0769 mg/Kg ☼02/19/18 14:03 02/20/18 15:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Acenaphthylene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Anthracene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼Benzo[a]anthracene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Benzo[a]pyrene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Benzo[b]fluoranthene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Benzo[g,h,i]perylene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼Benzo[k]fluoranthene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Bis(2-chloroethoxy)methane ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Bis(2-chloroethyl)ether ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼bis (2-chloroisopropyl) ether ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Bis(2-ethylhexyl) phthalate ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼4-Bromophenyl phenyl ether ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Butyl benzyl phthalate ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Carbazole ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼4-Chloroaniline ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼4-Chloro-3-methylphenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2-Chloronaphthalene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2-Chlorophenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼4-Chlorophenyl phenyl ether ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼Chrysene ND
0.764 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Cresols ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Dibenz(a,h)anthracene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-6Client Sample ID: HHSB-5 (0-1)
Matrix: SolidDate Collected: 02/16/18 09:00
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.382 mg/Kg ☼02/19/18 14:03 02/20/18 15:40 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼1,3-Dichlorobenzene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼1,4-Dichlorobenzene ND
0.769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼3,3'-Dichlorobenzidine ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2,4-Dichlorophenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Diethyl phthalate ND
0.769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼2,4-Dimethylphenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Dimethyl phthalate ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Di-n-butyl phthalate ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼4,6-Dinitro-2-methylphenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2,4-Dinitrophenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼2,4-Dinitrotoluene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2,6-Dinitrotoluene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Di-n-octyl phthalate ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Fluoranthene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼Fluorene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Hexachlorobenzene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Hexachlorobutadiene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Hexachlorocyclopentadiene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Hexachloroethane ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼Indeno[1,2,3-cd]pyrene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Isophorone ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼1-Methylnaphthalene ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2-Methylnaphthalene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼2-Methylphenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼3 & 4 Methylphenol ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Naphthalene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2-Nitroaniline ND
0.769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼3-Nitroaniline ND
0.769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼4-Nitroaniline ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Nitrobenzene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2-Nitrophenol ND
0.769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼4-Nitrophenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼N-Nitrosodi-n-propylamine ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Pentachlorophenol ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Phenanthrene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼Phenol ND
0.0769 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼Pyrene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼1,2,4-Trichlorobenzene ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1
☼2,4,5-Trichlorophenol ND
0.382 mg/Kg 02/19/18 14:03 02/20/18 15:40 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)68 29-120 02/19/18 14:03 02/20/18 15:40 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
2-Fluorophenol (Surr)61 02/19/18 14:03 02/20/18 15:40 110-120
Nitrobenzene-d5 (Surr)62 02/19/18 14:03 02/20/18 15:40 127-120
Phenol-d5 (Surr)61 02/19/18 14:03 02/20/18 15:40 110-120
Terphenyl-d14 (Surr)86 02/19/18 14:03 02/20/18 15:40 113-120
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-6Client Sample ID: HHSB-5 (0-1)
Matrix: SolidDate Collected: 02/16/18 09:00
Date Received: 02/17/18 09:25
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)76 10-120 02/19/18 14:03 02/20/18 15:40 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 2.79 0.490 mg/Kg ☼02/19/18 09:17 02/20/18 10:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.490 mg/Kg 02/19/18 09:17 02/20/18 10:52 1
☼Barium 42.7
0.490 mg/Kg 02/19/18 09:17 02/20/18 10:52 1☼Cadmium ND
0.490 mg/Kg 02/19/18 09:17 02/20/18 10:52 1
☼Chromium 21.0
0.490 mg/Kg 02/19/18 09:17 02/20/18 10:52 1
☼Lead 23.5
0.490 mg/Kg 02/19/18 09:17 02/20/18 10:52 1
☼Selenium ND
0.490 mg/Kg 02/19/18 09:17 02/20/18 10:52 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.114 mg/Kg ☼02/20/18 10:01 02/20/18 15:56 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 5.83 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 85.1 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Nashville
Page 29 of 55 2/26/2018 (Rev. 1)
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-7Client Sample ID: BKG-1 (1-2)
Matrix: SolidDate Collected: 02/16/18 10:30
Date Received: 02/17/18 09:25
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.91 0.517 mg/Kg ☼02/19/18 09:17 02/20/18 10:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.517 mg/Kg 02/19/18 09:17 02/20/18 10:55 1
☼Barium 99.9
0.517 mg/Kg 02/19/18 09:17 02/20/18 10:55 1
☼Cadmium ND
0.517 mg/Kg 02/19/18 09:17 02/20/18 10:55 1
☼Chromium 24.1
0.517 mg/Kg 02/19/18 09:17 02/20/18 10:55 1
☼Lead 17.9
0.517 mg/Kg 02/19/18 09:17 02/20/18 10:55 1
☼Selenium ND
0.517 mg/Kg 02/19/18 09:17 02/20/18 10:55 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.117 mg/Kg ☼02/20/18 10:11 02/20/18 15:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 5.98 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 81.9 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Nashville
Page 30 of 55 2/26/2018 (Rev. 1)
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Client Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Lab Sample ID: 490-146593-8Client Sample ID: BKG-2 (1-2)
Matrix: SolidDate Collected: 02/16/18 11:00
Date Received: 02/17/18 09:25
Method: 6020B - Metals (ICP/MS)
RL MDL
Arsenic 1.53 0.534 mg/Kg ☼02/19/18 09:17 02/20/18 10:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.534 mg/Kg 02/19/18 09:17 02/20/18 10:58 1
☼Barium 15.2
0.534 mg/Kg 02/19/18 09:17 02/20/18 10:58 1
☼Cadmium ND
0.534 mg/Kg 02/19/18 09:17 02/20/18 10:58 1
☼Chromium 24.5
0.534 mg/Kg 02/19/18 09:17 02/20/18 10:58 1
☼Lead 6.61
0.534 mg/Kg 02/19/18 09:17 02/20/18 10:58 1
☼Selenium ND
0.534 mg/Kg 02/19/18 09:17 02/20/18 10:58 1☼Silver ND
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.112 mg/Kg ☼02/20/18 10:11 02/20/18 16:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
General Chemistry
RL MDL
Chromium, hex ND 5.59 mg/Kg ☼02/20/18 09:07 02/20/18 15:11 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
RL RL
Percent Solids 86.7 0.1 %02/20/18 12:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Nashville
Page 31 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-496298/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496298
RL MDL
Acetone ND 0.0500 mg/Kg 02/19/18 12:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.00200 mg/Kg 02/19/18 12:57 1Benzene
ND 0.00200 mg/Kg 02/19/18 12:57 1Bromobenzene
ND 0.00200 mg/Kg 02/19/18 12:57 1Bromochloromethane
ND 0.00200 mg/Kg 02/19/18 12:57 1Bromodichloromethane
ND 0.00200 mg/Kg 02/19/18 12:57 1Bromoform
ND 0.00200 mg/Kg 02/19/18 12:57 1Bromomethane
ND 0.0500 mg/Kg 02/19/18 12:57 12-Butanone (MEK)
ND 0.00500 mg/Kg 02/19/18 12:57 1Carbon disulfide
ND 0.00200 mg/Kg 02/19/18 12:57 1Carbon tetrachloride
ND 0.00200 mg/Kg 02/19/18 12:57 1Chlorobenzene
ND 0.00200 mg/Kg 02/19/18 12:57 1Chlorodibromomethane
ND 0.00500 mg/Kg 02/19/18 12:57 1Chloroethane
ND 0.00200 mg/Kg 02/19/18 12:57 1Chloroform
ND 0.00200 mg/Kg 02/19/18 12:57 1Chloromethane
ND 0.00200 mg/Kg 02/19/18 12:57 12-Chlorotoluene
ND 0.00200 mg/Kg 02/19/18 12:57 14-Chlorotoluene
ND 0.00200 mg/Kg 02/19/18 12:57 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 02/19/18 12:57 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 02/19/18 12:57 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 02/19/18 12:57 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 02/19/18 12:57 1Dibromomethane
ND 0.00200 mg/Kg 02/19/18 12:57 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 02/19/18 12:57 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 02/19/18 12:57 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 02/19/18 12:57 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 02/19/18 12:57 11,1-Dichloroethane
ND 0.00200 mg/Kg 02/19/18 12:57 11,2-Dichloroethane
ND 0.00200 mg/Kg 02/19/18 12:57 11,1-Dichloroethene
ND 0.00200 mg/Kg 02/19/18 12:57 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 02/19/18 12:57 11,2-Dichloropropane
ND 0.00200 mg/Kg 02/19/18 12:57 11,3-Dichloropropane
ND 0.00200 mg/Kg 02/19/18 12:57 12,2-Dichloropropane
ND 0.00200 mg/Kg 02/19/18 12:57 11,1-Dichloropropene
ND 0.00200 mg/Kg 02/19/18 12:57 1Diisopropyl ether
ND 0.00200 mg/Kg 02/19/18 12:57 1Ethylbenzene
ND 0.00500 mg/Kg 02/19/18 12:57 1Hexachlorobutadiene
ND 0.0500 mg/Kg 02/19/18 12:57 12-Hexanone
ND 0.00200 mg/Kg 02/19/18 12:57 1Isopropylbenzene
ND 0.0100 mg/Kg 02/19/18 12:57 1Methylene Chloride
ND 0.0500 mg/Kg 02/19/18 12:57 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 02/19/18 12:57 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 02/19/18 12:57 1Naphthalene
ND 0.00200 mg/Kg 02/19/18 12:57 1n-Butylbenzene
ND 0.00200 mg/Kg 02/19/18 12:57 1N-Propylbenzene
ND 0.00200 mg/Kg 02/19/18 12:57 1p-Isopropyltoluene
ND 0.00200 mg/Kg 02/19/18 12:57 1sec-Butylbenzene
ND 0.00200 mg/Kg 02/19/18 12:57 1Styrene
TestAmerica Nashville
Page 32 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-496298/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496298
RL MDL
tert-Butylbenzene ND 0.00200 mg/Kg 02/19/18 12:57 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.00200 mg/Kg 02/19/18 12:57 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 02/19/18 12:57 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 02/19/18 12:57 1Tetrachloroethene
ND 0.00200 mg/Kg 02/19/18 12:57 1Toluene
ND 0.00200 mg/Kg 02/19/18 12:57 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 02/19/18 12:57 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 02/19/18 12:57 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 02/19/18 12:57 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 02/19/18 12:57 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 02/19/18 12:57 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 02/19/18 12:57 1Trichloroethene
ND 0.00200 mg/Kg 02/19/18 12:57 1Trichlorofluoromethane
ND 0.00200 mg/Kg 02/19/18 12:57 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 02/19/18 12:57 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 02/19/18 12:57 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 02/19/18 12:57 1Vinyl chloride
ND 0.00600 mg/Kg 02/19/18 12:57 1Xylenes, Total
4-Bromofluorobenzene (Surr)87 70-130 02/19/18 12:57 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
112 02/19/18 12:57 1Dibromofluoromethane (Surr)70-130
93 02/19/18 12:57 11,2-Dichloroethane-d4 (Surr)70-130
93 02/19/18 12:57 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496298/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496298
Acetone 0.250 0.2017 mg/Kg 81 45-145
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.04711 mg/Kg 94 70-130
Bromobenzene 0.0500 0.04175 mg/Kg 83 67-130
Bromochloromethane 0.0500 0.05382 mg/Kg 108 70-133
Bromodichloromethane 0.0500 0.05134 mg/Kg 103 70-130
Bromoform 0.0500 0.05440 mg/Kg 109 59-137
Bromomethane 0.0500 0.05460 mg/Kg 109 32-150
2-Butanone (MEK)0.250 0.2212 mg/Kg 88 50-149
Carbon disulfide 0.0500 0.04734 mg/Kg 95 66-138
Carbon tetrachloride 0.0500 0.05730 mg/Kg 115 70-131
Chlorobenzene 0.0500 0.05061 mg/Kg 101 70-130
Chlorodibromomethane 0.0500 0.05488 mg/Kg 110 70-130
Chloroethane 0.0500 0.04908 mg/Kg 98 37-150
Chloroform 0.0500 0.04912 mg/Kg 98 70-130
Chloromethane 0.0500 0.03939 mg/Kg 79 53-150
2-Chlorotoluene 0.0500 0.04621 mg/Kg 92 70-132
4-Chlorotoluene 0.0500 0.04702 mg/Kg 94 67-135
cis-1,2-Dichloroethene 0.0500 0.05186 mg/Kg 104 70-132
TestAmerica Nashville
Page 33 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496298/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496298
cis-1,3-Dichloropropene 0.0500 0.04816 mg/Kg 96 70-130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.05950 mg/Kg 119 47-144
1,2-Dibromoethane (EDB)0.0500 0.04960 mg/Kg 99 69-130
Dibromomethane 0.0500 0.04931 mg/Kg 99 70-130
1,2-Dichlorobenzene 0.0500 0.05612 mg/Kg 112 70-134
1,3-Dichlorobenzene 0.0500 0.05235 mg/Kg 105 69-137
1,4-Dichlorobenzene 0.0500 0.05011 mg/Kg 100 66-134
Dichlorodifluoromethane 0.0500 0.05355 mg/Kg 107 32-150
1,1-Dichloroethane 0.0500 0.04509 mg/Kg 90 70-130
1,2-Dichloroethane 0.0500 0.04405 mg/Kg 88 65-134
1,1-Dichloroethene 0.0500 0.05336 mg/Kg 107 70-131
1,2-Dichloroethene, Total 0.100 0.09634 mg/Kg 96 70-130
1,2-Dichloropropane 0.0500 0.04312 mg/Kg 86 70-130
1,3-Dichloropropane 0.0500 0.04312 mg/Kg 86 70-130
2,2-Dichloropropane 0.0500 0.05085 mg/Kg 102 57-150
1,1-Dichloropropene 0.0500 0.04748 mg/Kg 95 70-130
Diisopropyl ether 0.0500 0.03667 mg/Kg 73 68-134
Ethylbenzene 0.0500 0.04637 mg/Kg 93 70-130
Hexachlorobutadiene 0.0500 0.05713 mg/Kg 114 64-137
2-Hexanone 0.250 0.1923 mg/Kg 77 47-148
Isopropylbenzene 0.0500 0.05143 mg/Kg 103 70-130
Methylene Chloride 0.0500 0.04451 mg/Kg 89 69-130
4-Methyl-2-pentanone (MIBK)0.250 0.1898 mg/Kg 76 48-150
Methyl tert-butyl ether 0.0500 0.04341 mg/Kg 87 54-145
Naphthalene 0.0500 0.05597 mg/Kg 112 55-149
n-Butylbenzene 0.0500 0.05462 mg/Kg 109 57-150
N-Propylbenzene 0.0500 0.04736 mg/Kg 95 62-150
p-Isopropyltoluene 0.0500 0.05049 mg/Kg 101 66-147
sec-Butylbenzene 0.0500 0.04963 mg/Kg 99 68-147
Styrene 0.0500 0.04989 mg/Kg 100 70-131
tert-Butylbenzene 0.0500 0.05253 mg/Kg 105 70-138
1,1,1,2-Tetrachloroethane 0.0500 0.05381 mg/Kg 108 70-130
1,1,2,2-Tetrachloroethane 0.0500 0.04121 mg/Kg 82 61-134
Tetrachloroethene 0.0500 0.05712 mg/Kg 114 70-130
Toluene 0.0500 0.04785 mg/Kg 96 70-130
trans-1,2-Dichloroethene 0.0500 0.04448 mg/Kg 89 70-130
trans-1,3-Dichloropropene 0.0500 0.04595 mg/Kg 92 67-130
1,2,3-Trichlorobenzene 0.0500 0.06040 mg/Kg 121 57-146
1,2,4-Trichlorobenzene 0.0500 0.06310 mg/Kg 126 47-150
1,1,1-Trichloroethane 0.0500 0.05420 mg/Kg 108 70-130
1,1,2-Trichloroethane 0.0500 0.04806 mg/Kg 96 70-130
Trichloroethene 0.0500 0.05834 mg/Kg 117 70-130
Trichlorofluoromethane 0.0500 0.05669 mg/Kg 113 53-150
1,2,3-Trichloropropane 0.0500 0.04341 mg/Kg 87 60-139
1,2,4-Trimethylbenzene 0.0500 0.04805 mg/Kg 96 70-140
1,3,5-Trimethylbenzene 0.0500 0.04772 mg/Kg 95 69-141
Vinyl chloride 0.0500 0.04431 mg/Kg 89 63-150
Xylenes, Total 0.100 0.09688 mg/Kg 97 70-130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496298/3
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496298
4-Bromofluorobenzene (Surr)70 -130
Surrogate
90
LCS LCS
Qualifier Limits%Recovery
108Dibromofluoromethane (Surr)70 -130
911,2-Dichloroethane-d4 (Surr)70 -130
95Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496298/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496298
Acetone 0.250 0.1929 mg/Kg 77 45-145 4 38
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.04827 mg/Kg 97 70-130 2 37
Bromobenzene 0.0500 0.04044 mg/Kg 81 67-130 3 40
Bromochloromethane 0.0500 0.05539 mg/Kg 111 70-133 3 15
Bromodichloromethane 0.0500 0.05167 mg/Kg 103 70-130 1 20
Bromoform 0.0500 0.05501 mg/Kg 110 59-137 1 17
Bromomethane 0.0500 0.05861 mg/Kg 117 32-150 7 45
2-Butanone (MEK)0.250 0.2154 mg/Kg 86 50-149 3 39
Carbon disulfide 0.0500 0.04823 mg/Kg 96 66-138 2 41
Carbon tetrachloride 0.0500 0.05959 mg/Kg 119 70-131 4 41
Chlorobenzene 0.0500 0.05196 mg/Kg 104 70-130 3 40
Chlorodibromomethane 0.0500 0.05447 mg/Kg 109 70-130 1 14
Chloroethane 0.0500 0.04774 mg/Kg 95 37-150 3 50
Chloroform 0.0500 0.05030 mg/Kg 101 70-130 2 15
Chloromethane 0.0500 0.04036 mg/Kg 81 53-150 2 47
2-Chlorotoluene 0.0500 0.04534 mg/Kg 91 70-132 2 41
4-Chlorotoluene 0.0500 0.04575 mg/Kg 92 67-135 3 41
cis-1,2-Dichloroethene 0.0500 0.05361 mg/Kg 107 70-132 3 18
cis-1,3-Dichloropropene 0.0500 0.04975 mg/Kg 100 70-130 3 42
1,2-Dibromo-3-Chloropropane 0.0500 0.05819 mg/Kg 116 47-144 2 38
1,2-Dibromoethane (EDB)0.0500 0.04985 mg/Kg 100 69-130 0 17
Dibromomethane 0.0500 0.05059 mg/Kg 101 70-130 3 19
1,2-Dichlorobenzene 0.0500 0.05608 mg/Kg 112 70-134 0 40
1,3-Dichlorobenzene 0.0500 0.05221 mg/Kg 104 69-137 0 41
1,4-Dichlorobenzene 0.0500 0.05261 mg/Kg 105 66-134 5 41
Dichlorodifluoromethane 0.0500 0.05501 mg/Kg 110 32-150 3 50
1,1-Dichloroethane 0.0500 0.04592 mg/Kg 92 70-130 2 42
1,2-Dichloroethane 0.0500 0.04479 mg/Kg 90 65-134 2 16
1,1-Dichloroethene 0.0500 0.05347 mg/Kg 107 70-131 0 43
1,2-Dichloroethene, Total 0.100 0.09895 mg/Kg 99 70-130 3 41
1,2-Dichloropropane 0.0500 0.04414 mg/Kg 88 70-130 2 15
1,3-Dichloropropane 0.0500 0.04209 mg/Kg 84 70-130 2 15
2,2-Dichloropropane 0.0500 0.05176 mg/Kg 104 57-150 2 42
1,1-Dichloropropene 0.0500 0.04875 mg/Kg 98 70-130 3 41
Diisopropyl ether 0.0500 0.03761 mg/Kg 75 68-134 3 36
Ethylbenzene 0.0500 0.04768 mg/Kg 95 70-130 3 38
Hexachlorobutadiene 0.0500 0.05770 mg/Kg 115 64-137 1 44
2-Hexanone 0.250 0.1848 mg/Kg 74 47-148 4 38
TestAmerica Nashville
Page 35 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496298/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496298
Isopropylbenzene 0.0500 0.05249 mg/Kg 105 70-130 2 39
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 0.0500 0.04532 mg/Kg 91 69-130 2 19
4-Methyl-2-pentanone (MIBK)0.250 0.1885 mg/Kg 75 48-150 1 41
Methyl tert-butyl ether 0.0500 0.04354 mg/Kg 87 54-145 0 36
Naphthalene 0.0500 0.05480 mg/Kg 110 55-149 2 37
n-Butylbenzene 0.0500 0.05447 mg/Kg 109 57-150 0 39
N-Propylbenzene 0.0500 0.04678 mg/Kg 94 62-150 1 38
p-Isopropyltoluene 0.0500 0.05060 mg/Kg 101 66-147 0 38
sec-Butylbenzene 0.0500 0.04901 mg/Kg 98 68-147 1 38
Styrene 0.0500 0.05120 mg/Kg 102 70-131 3 40
tert-Butylbenzene 0.0500 0.05200 mg/Kg 104 70-138 1 38
1,1,1,2-Tetrachloroethane 0.0500 0.05491 mg/Kg 110 70-130 2 41
1,1,2,2-Tetrachloroethane 0.0500 0.04045 mg/Kg 81 61-134 2 16
Tetrachloroethene 0.0500 0.05881 mg/Kg 118 70-130 3 41
Toluene 0.0500 0.04885 mg/Kg 98 70-130 2 40
trans-1,2-Dichloroethene 0.0500 0.04534 mg/Kg 91 70-130 2 41
trans-1,3-Dichloropropene 0.0500 0.04722 mg/Kg 94 67-130 3 41
1,2,3-Trichlorobenzene 0.0500 0.05851 mg/Kg 117 57-146 3 42
1,2,4-Trichlorobenzene 0.0500 0.06154 mg/Kg 123 47-150 2 43
1,1,1-Trichloroethane 0.0500 0.05521 mg/Kg 110 70-130 2 41
1,1,2-Trichloroethane 0.0500 0.04938 mg/Kg 99 70-130 3 17
Trichloroethene 0.0500 0.06031 mg/Kg 121 70-130 3 41
Trichlorofluoromethane 0.0500 0.05786 mg/Kg 116 53-150 2 49
1,2,3-Trichloropropane 0.0500 0.04184 mg/Kg 84 60-139 4 16
1,2,4-Trimethylbenzene 0.0500 0.04772 mg/Kg 95 70-140 1 38
1,3,5-Trimethylbenzene 0.0500 0.04732 mg/Kg 95 69-141 1 38
Vinyl chloride 0.0500 0.04598 mg/Kg 92 63-150 4 46
Xylenes, Total 0.100 0.09908 mg/Kg 99 70-130 2 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
87
LCSD LCSD
Qualifier Limits%Recovery
110Dibromofluoromethane (Surr)70 -130
911,2-Dichloroethane-d4 (Surr)70 -130
96Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-496428/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
RL MDL
Acenaphthene ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Acenaphthylene
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Anthracene
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Benzo[a]anthracene
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Benzo[a]pyrene
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Benzo[b]fluoranthene
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-496428/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
RL MDL
Benzo[g,h,i]perylene ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Benzo[k]fluoranthene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Bis(2-chloroethoxy)methane
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Bis(2-chloroethyl)ether
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1bis (2-chloroisopropyl) ether
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Bis(2-ethylhexyl) phthalate
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 14-Bromophenyl phenyl ether
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Butyl benzyl phthalate
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Carbazole
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 14-Chloroaniline
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 14-Chloro-3-methylphenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12-Chloronaphthalene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12-Chlorophenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 14-Chlorophenyl phenyl ether
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Chrysene
ND 0.666 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Cresols
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Dibenz(a,h)anthracene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Dibenzofuran
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 11,2-Dichlorobenzene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 11,3-Dichlorobenzene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 11,4-Dichlorobenzene
ND 0.670 mg/Kg 02/19/18 14:01 02/20/18 12:17 13,3'-Dichlorobenzidine
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12,4-Dichlorophenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Diethyl phthalate
ND 0.670 mg/Kg 02/19/18 14:01 02/20/18 12:17 12,4-Dimethylphenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Dimethyl phthalate
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Di-n-butyl phthalate
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 14,6-Dinitro-2-methylphenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12,4-Dinitrophenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12,4-Dinitrotoluene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12,6-Dinitrotoluene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Di-n-octyl phthalate
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Fluoranthene
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Fluorene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Hexachlorobenzene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Hexachlorobutadiene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Hexachlorocyclopentadiene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Hexachloroethane
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Indeno[1,2,3-cd]pyrene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Isophorone
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 11-Methylnaphthalene
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 12-Methylnaphthalene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12-Methylphenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 13 & 4 Methylphenol
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Naphthalene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12-Nitroaniline
ND 0.670 mg/Kg 02/19/18 14:01 02/20/18 12:17 13-Nitroaniline
ND 0.670 mg/Kg 02/19/18 14:01 02/20/18 12:17 14-Nitroaniline
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-496428/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
RL MDL
Nitrobenzene ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12-Nitrophenol
ND 0.670 mg/Kg 02/19/18 14:01 02/20/18 12:17 14-Nitrophenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1N-Nitrosodi-n-propylamine
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Pentachlorophenol
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Phenanthrene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Phenol
ND 0.0670 mg/Kg 02/19/18 14:01 02/20/18 12:17 1Pyrene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 11,2,4-Trichlorobenzene
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12,4,5-Trichlorophenol
ND 0.333 mg/Kg 02/19/18 14:01 02/20/18 12:17 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)73 29-120 02/20/18 12:17 1
MB MB
Surrogate
02/19/18 14:01
Dil FacPrepared AnalyzedQualifier Limits%Recovery
58 02/19/18 14:01 02/20/18 12:17 12-Fluorophenol (Surr)10-120
70 02/19/18 14:01 02/20/18 12:17 1Nitrobenzene-d5 (Surr)27-120
60 02/19/18 14:01 02/20/18 12:17 1Phenol-d5 (Surr)10-120
90 02/19/18 14:01 02/20/18 12:17 1Terphenyl-d14 (Surr)13-120
53 02/19/18 14:01 02/20/18 12:17 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496428/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
Acenaphthene 1.67 1.101 mg/Kg 66 36-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.221 mg/Kg 73 38-120
Anthracene 1.67 1.205 mg/Kg 72 46-124
Benzo[a]anthracene 1.67 1.193 mg/Kg 72 45-120
Benzo[a]pyrene 1.67 1.251 mg/Kg 75 45-120
Benzo[b]fluoranthene 1.67 1.166 mg/Kg 70 42-120
Benzo[g,h,i]perylene 1.67 1.297 mg/Kg 78 38-120
Benzo[k]fluoranthene 1.67 1.294 mg/Kg 78 42-120
Bis(2-chloroethoxy)methane 1.67 1.020 mg/Kg 61 32-120
Bis(2-chloroethyl)ether 1.67 0.9899 mg/Kg 59 31-120
bis (2-chloroisopropyl) ether 1.67 0.8531 mg/Kg 51 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.349 mg/Kg 81 43-120
4-Bromophenyl phenyl ether 1.67 1.185 mg/Kg 71 40-120
Butyl benzyl phthalate 1.67 1.268 mg/Kg 76 43-133
Carbazole 1.67 1.188 mg/Kg 71 44-120
4-Chloroaniline 1.67 1.028 mg/Kg 62 35-120
4-Chloro-3-methylphenol 1.67 1.133 mg/Kg 68 38-120
2-Chloronaphthalene 1.67 1.099 mg/Kg 66 34-120
2-Chlorophenol 1.67 0.9654 mg/Kg 58 32-120
4-Chlorophenyl phenyl ether 1.67 1.134 mg/Kg 68 42-120
Chrysene 1.67 1.178 mg/Kg 71 43-120
TestAmerica Nashville
Page 38 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496428/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
Cresols 3.33 1.998 mg/Kg 60 36-129
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Dibenz(a,h)anthracene 1.67 1.374 mg/Kg 82 32-128
Dibenzofuran 1.67 1.135 mg/Kg 68 41-120
1,2-Dichlorobenzene 1.67 0.9782 mg/Kg 59 33-120
1,3-Dichlorobenzene 1.67 0.9372 mg/Kg 56 32-120
1,4-Dichlorobenzene 1.67 0.9421 mg/Kg 57 32-120
3,3'-Dichlorobenzidine 1.67 1.299 mg/Kg 78 39-120
2,4-Dichlorophenol 1.67 1.018 mg/Kg 61 32-120
Diethyl phthalate 1.67 1.206 mg/Kg 72 41-122
2,4-Dimethylphenol 1.67 1.004 mg/Kg 60 32-120
Dimethyl phthalate 1.67 1.157 mg/Kg 69 55-120
Di-n-butyl phthalate 1.67 1.251 mg/Kg 75 46-127
4,6-Dinitro-2-methylphenol 3.33 2.466 mg/Kg 74 27-134
2,4-Dinitrophenol 3.33 1.827 mg/Kg 55 10-142
2,4-Dinitrotoluene 1.67 1.171 mg/Kg 70 43-120
2,6-Dinitrotoluene 1.67 1.164 mg/Kg 70 43-120
Di-n-octyl phthalate 1.67 1.319 mg/Kg 79 40-130
Fluoranthene 1.67 1.197 mg/Kg 72 46-120
Fluorene 1.67 1.179 mg/Kg 71 42-120
Hexachlorobenzene 1.67 1.206 mg/Kg 72 44-120
Hexachlorobutadiene 1.67 1.044 mg/Kg 63 31-120
Hexachlorocyclopentadiene 1.67 1.016 mg/Kg 61 24-120
Hexachloroethane 1.67 0.9940 mg/Kg 60 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.305 mg/Kg 78 41-121
Isophorone 1.67 1.022 mg/Kg 61 33-120
1-Methylnaphthalene 1.67 0.9736 mg/Kg 58 32-120
2-Methylnaphthalene 1.67 1.008 mg/Kg 60 28-120
2-Methylphenol 1.67 0.9760 mg/Kg 59 36-120
3 & 4 Methylphenol 1.67 1.022 mg/Kg 61 37-120
Naphthalene 1.67 0.9870 mg/Kg 59 32-120
2-Nitroaniline 1.67 1.166 mg/Kg 70 40-120
3-Nitroaniline 1.67 1.170 mg/Kg 70 42-120
4-Nitroaniline 1.67 1.080 mg/Kg 65 43-120
Nitrobenzene 1.67 1.025 mg/Kg 61 26-120
2-Nitrophenol 1.67 1.017 mg/Kg 61 29-120
4-Nitrophenol 3.33 2.392 mg/Kg 72 32-136
N-Nitrosodi-n-propylamine 1.67 0.9988 mg/Kg 60 35-120
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.204 mg/Kg 85 52-140
Pentachlorophenol 3.33 1.894 mg/Kg 57 44-134
Phenanthrene 1.67 1.201 mg/Kg 72 45-120
Phenol 1.67 1.063 mg/Kg 64 30-120
Pyrene 1.67 1.298 mg/Kg 78 43-120
1,2,4-Trichlorobenzene 1.67 0.9691 mg/Kg 58 29-120
2,4,5-Trichlorophenol 1.67 1.062 mg/Kg 64 39-120
2,4,6-Trichlorophenol 1.67 1.125 mg/Kg 67 39-120
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Page 39 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496428/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
2-Fluorobiphenyl (Surr)29 -120
Surrogate
58
LCS LCS
Qualifier Limits%Recovery
512-Fluorophenol (Surr)10 -120
52Nitrobenzene-d5 (Surr)27 -120
52Phenol-d5 (Surr)10 -120
70Terphenyl-d14 (Surr)13 -120
632,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496428/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
Acenaphthene 1.67 1.364 mg/Kg 82 36-120 21 50
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 1.67 1.511 mg/Kg 91 38-120 21 50
Anthracene 1.67 1.454 mg/Kg 87 46-124 19 49
Benzo[a]anthracene 1.67 1.469 mg/Kg 88 45-120 21 50
Benzo[a]pyrene 1.67 1.532 mg/Kg 92 45-120 20 50
Benzo[b]fluoranthene 1.67 1.401 mg/Kg 84 42-120 18 50
Benzo[g,h,i]perylene 1.67 1.595 mg/Kg 96 38-120 21 50
Benzo[k]fluoranthene 1.67 1.575 mg/Kg 95 42-120 20 45
Bis(2-chloroethoxy)methane 1.67 1.289 mg/Kg 77 32-120 23 50
Bis(2-chloroethyl)ether 1.67 1.264 mg/Kg 76 31-120 24 50
bis (2-chloroisopropyl) ether 1.67 1.126 mg/Kg 68 32-120 28 50
Bis(2-ethylhexyl) phthalate 1.67 1.645 mg/Kg 99 43-120 20 50
4-Bromophenyl phenyl ether 1.67 1.428 mg/Kg 86 40-120 19 37
Butyl benzyl phthalate 1.67 1.506 mg/Kg 90 43-133 17 50
Carbazole 1.67 1.432 mg/Kg 86 44-120 19 46
4-Chloroaniline 1.67 1.275 mg/Kg 76 35-120 21 50
4-Chloro-3-methylphenol 1.67 1.386 mg/Kg 83 38-120 20 49
2-Chloronaphthalene 1.67 1.371 mg/Kg 82 34-120 22 50
2-Chlorophenol 1.67 1.282 mg/Kg 77 32-120 28 50
4-Chlorophenyl phenyl ether 1.67 1.371 mg/Kg 82 42-120 19 50
Chrysene 1.67 1.462 mg/Kg 88 43-120 22 49
Cresols 3.33 2.606 mg/Kg 78 36-129 26 50
Dibenz(a,h)anthracene 1.67 1.615 mg/Kg 97 32-128 16 50
Dibenzofuran 1.67 1.379 mg/Kg 83 41-120 19 50
1,2-Dichlorobenzene 1.67 1.258 mg/Kg 75 33-120 25 50
1,3-Dichlorobenzene 1.67 1.264 mg/Kg 76 32-120 30 50
1,4-Dichlorobenzene 1.67 1.262 mg/Kg 76 32-120 29 50
3,3'-Dichlorobenzidine 1.67 1.619 mg/Kg 97 39-120 22 50
2,4-Dichlorophenol 1.67 1.295 mg/Kg 78 32-120 24 50
Diethyl phthalate 1.67 1.442 mg/Kg 86 41-122 18 45
2,4-Dimethylphenol 1.67 1.285 mg/Kg 77 32-120 25 50
Dimethyl phthalate 1.67 1.414 mg/Kg 85 55-120 20 46
Di-n-butyl phthalate 1.67 1.507 mg/Kg 90 46-127 19 49
4,6-Dinitro-2-methylphenol 3.33 2.994 mg/Kg 90 27-134 19 50
2,4-Dinitrophenol 3.33 2.249 mg/Kg 67 10-142 21 50
2,4-Dinitrotoluene 1.67 1.387 mg/Kg 83 43-120 17 50
TestAmerica Nashville
Page 40 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496428/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496518 Prep Batch: 496428
2,6-Dinitrotoluene 1.67 1.371 mg/Kg 82 43-120 16 50
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Di-n-octyl phthalate 1.67 1.543 mg/Kg 93 40-130 16 50
Fluoranthene 1.67 1.453 mg/Kg 87 46-120 19 50
Fluorene 1.67 1.409 mg/Kg 85 42-120 18 50
Hexachlorobenzene 1.67 1.456 mg/Kg 87 44-120 19 50
Hexachlorobutadiene 1.67 1.374 mg/Kg 82 31-120 27 50
Hexachlorocyclopentadiene 1.67 1.372 mg/Kg 82 24-120 30 50
Hexachloroethane 1.67 1.318 mg/Kg 79 33-120 28 50
Indeno[1,2,3-cd]pyrene 1.67 1.624 mg/Kg 97 41-121 22 50
Isophorone 1.67 1.250 mg/Kg 75 33-120 20 50
1-Methylnaphthalene 1.67 1.231 mg/Kg 74 32-120 23 50
2-Methylnaphthalene 1.67 1.245 mg/Kg 75 28-120 21 50
2-Methylphenol 1.67 1.292 mg/Kg 78 36-120 28 50
3 & 4 Methylphenol 1.67 1.314 mg/Kg 79 37-120 25 50
Naphthalene 1.67 1.275 mg/Kg 77 32-120 25 50
2-Nitroaniline 1.67 1.411 mg/Kg 85 40-120 19 50
3-Nitroaniline 1.67 1.365 mg/Kg 82 42-120 15 49
4-Nitroaniline 1.67 1.280 mg/Kg 77 43-120 17 49
Nitrobenzene 1.67 1.353 mg/Kg 81 26-120 28 50
2-Nitrophenol 1.67 1.303 mg/Kg 78 29-120 25 50
4-Nitrophenol 3.33 2.899 mg/Kg 87 32-136 19 45
N-Nitrosodi-n-propylamine 1.67 1.241 mg/Kg 74 35-120 22 50
n-Nitrosodiphenylamine(as
diphenylamine)
1.42 1.470 mg/Kg 104 52-140 20 50
Pentachlorophenol 3.33 2.582 mg/Kg 77 44-134 31 50
Phenanthrene 1.67 1.450 mg/Kg 87 45-120 19 50
Phenol 1.67 1.390 mg/Kg 83 30-120 27 50
Pyrene 1.67 1.507 mg/Kg 90 43-120 15 50
1,2,4-Trichlorobenzene 1.67 1.288 mg/Kg 77 29-120 28 50
2,4,5-Trichlorophenol 1.67 1.353 mg/Kg 81 39-120 24 50
2,4,6-Trichlorophenol 1.67 1.350 mg/Kg 81 39-120 18 50
2-Fluorobiphenyl (Surr)29 -120
Surrogate
73
LCSD LCSD
Qualifier Limits%Recovery
692-Fluorophenol (Surr)10 -120
68Nitrobenzene-d5 (Surr)27 -120
67Phenol-d5 (Surr)10 -120
83Terphenyl-d14 (Surr)13 -120
782,4,6-Tribromophenol (Surr)10 -120
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-496285/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496285
RL MDL
Arsenic ND 0.481 mg/Kg 02/19/18 09:17 02/20/18 10:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
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Page 41 of 55 2/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 6020B - Metals (ICP/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-496285/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496285
RL MDL
Barium ND 0.481 mg/Kg 02/19/18 09:17 02/20/18 10:09 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.481 mg/Kg 02/19/18 09:17 02/20/18 10:09 1Cadmium
ND 0.481 mg/Kg 02/19/18 09:17 02/20/18 10:09 1Chromium
ND 0.481 mg/Kg 02/19/18 09:17 02/20/18 10:09 1Lead
ND 0.481 mg/Kg 02/19/18 09:17 02/20/18 10:09 1Selenium
ND 0.481 mg/Kg 02/19/18 09:17 02/20/18 10:09 1Silver
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496285/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496285
Arsenic 17.5 17.45 mg/Kg 99 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Barium 17.5 17.16 mg/Kg 98 80-120
Cadmium 17.5 17.33 mg/Kg 99 80-120
Chromium 17.5 16.89 mg/Kg 96 80-120
Lead 17.5 17.23 mg/Kg 98 80-120
Selenium 17.5 16.91 mg/Kg 96 80-120
Silver 17.5 18.21 mg/Kg 104 80-120
Client Sample ID: HHSB-1 (1-2)Lab Sample ID: 490-146593-1 MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496285
Arsenic 1.48 24.6 24.14 mg/Kg 92 75-125☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Barium 5.03 24.6 28.51 mg/Kg 95 75-125☼
Cadmium ND 24.6 24.15 mg/Kg 98 75-125☼
Chromium 9.40 F1 24.6 22.03 F1 mg/Kg 51 75-125☼
Lead 5.21 24.6 30.33 mg/Kg 102 75-125☼
Selenium ND 24.6 21.74 mg/Kg 86 75-125☼
Silver ND 24.6 25.77 mg/Kg 105 75-125☼
Client Sample ID: HHSB-1 (1-2)Lab Sample ID: 490-146593-1 MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496726 Prep Batch: 496285
Arsenic 1.48 24.6 22.72 mg/Kg 86 75-125 6 20
☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Barium 5.03 24.6 26.16 mg/Kg 86 75-125 9 20
☼
Cadmium ND 24.6 22.96 mg/Kg 93 75-125 5 20
☼
Chromium 9.40 F1 24.6 21.14 F1 mg/Kg 48 75-125 4 20☼
Lead 5.21 24.6 27.81 mg/Kg 92 75-125 9 20
☼
Selenium ND 24.6 20.67 mg/Kg 82 75-125 5 20
☼
Silver ND 24.6 24.87 mg/Kg 101 75-125 4 20
☼
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-496568/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496773 Prep Batch: 496568
RL MDL
Mercury ND 0.0988 mg/Kg 02/20/18 10:01 02/20/18 14:01 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-496568/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496773 Prep Batch: 496568
Mercury 0.167 0.1479 mg/Kg 89 80-120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-496568/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496773 Prep Batch: 496568
Mercury 0.162 0.1524 mg/Kg 94 80-120 3 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Method: 7196A - Chromium, Hexavalent
Client Sample ID: Method BlankLab Sample ID: MB 490-496532/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496728 Prep Batch: 496532
RL MDL
Chromium, hex ND 4.99 mg/Kg 02/10/18 14:15 02/20/18 15:11 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCSI 490-496532/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496728 Prep Batch: 496532
Chromium, hex 64.6 65.97 mg/Kg 102 80-120
Analyte
LCSI LCSI
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Lab Control SampleLab Sample ID: LCSS 490-496532/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496728 Prep Batch: 496532
Chromium, hex 39.9 39.32 mg/Kg 98 80-120
Analyte
LCSS LCSS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: HHSB-1 (1-2)Lab Sample ID: 490-146593-1 MSI
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496728 Prep Batch: 496532
Chromium, hex ND 79.8 74.08 mg/Kg 93 75-125☼
Analyte
MSI MSI
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method: 7196A - Chromium, Hexavalent (Continued)
Client Sample ID: HHSB-1 (1-2)Lab Sample ID: 490-146593-1 MSS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496728 Prep Batch: 496532
Chromium, hex ND 47.8 47.52 mg/Kg 99 75-125☼
Analyte
MSS MSS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: HHSB-1 (1-2)Lab Sample ID: 490-146593-1 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496728 Prep Batch: 496532
Chromium, hex ND ND mg/Kg NC 20
☼
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: Moisture - Percent Moisture
Client Sample ID: DuplicateLab Sample ID: 490-146592-G-34 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496682
Percent Solids 74.0 75.7 %20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Client Sample ID: DuplicateLab Sample ID: 490-146624-E-4 DU
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 496682
Percent Solids 83.5 84.4 %20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
GC/MS VOA
Analysis Batch: 496298
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B 496324490-146593-1 HHSB-1 (1-2)Total/NA
Solid 8260B 496324490-146593-2 HHSB-2 (1-2)Total/NA
Solid 8260B 496324490-146593-3 HHSB-3 (0-1)Total/NA
Solid 8260B 496324490-146593-4 Duplicate-2 Total/NA
Solid 8260B 496324490-146593-5 HHSB-4 (1-2)Total/NA
Solid 8260B 496324490-146593-6 HHSB-5 (0-1)Total/NA
Solid 8260BMB 490-496298/7 Method Blank Total/NA
Solid 8260BLCS 490-496298/3 Lab Control Sample Total/NA
Solid 8260BLCSD 490-496298/4 Lab Control Sample Dup Total/NA
Prep Batch: 496324
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035490-146593-1 HHSB-1 (1-2)Total/NA
Solid 5035490-146593-2 HHSB-2 (1-2)Total/NA
Solid 5035490-146593-3 HHSB-3 (0-1)Total/NA
Solid 5035490-146593-4 Duplicate-2 Total/NA
Solid 5035490-146593-5 HHSB-4 (1-2)Total/NA
Solid 5035490-146593-6 HHSB-5 (0-1)Total/NA
GC/MS Semi VOA
Prep Batch: 496428
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550C490-146593-1 HHSB-1 (1-2)Total/NA
Solid 3550C490-146593-2 HHSB-2 (1-2)Total/NA
Solid 3550C490-146593-3 HHSB-3 (0-1)Total/NA
Solid 3550C490-146593-4 Duplicate-2 Total/NA
Solid 3550C490-146593-5 HHSB-4 (1-2)Total/NA
Solid 3550C490-146593-6 HHSB-5 (0-1)Total/NA
Solid 3550CMB 490-496428/1-A Method Blank Total/NA
Solid 3550CLCS 490-496428/2-A Lab Control Sample Total/NA
Solid 3550CLCSD 490-496428/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 496518
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 496428490-146593-1 HHSB-1 (1-2)Total/NA
Solid 8270D 496428490-146593-2 HHSB-2 (1-2)Total/NA
Solid 8270D 496428490-146593-3 HHSB-3 (0-1)Total/NA
Solid 8270D 496428490-146593-4 Duplicate-2 Total/NA
Solid 8270D 496428490-146593-6 HHSB-5 (0-1)Total/NA
Solid 8270D 496428MB 490-496428/1-A Method Blank Total/NA
Solid 8270D 496428LCS 490-496428/2-A Lab Control Sample Total/NA
Solid 8270D 496428LCSD 490-496428/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 496813
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 496428490-146593-5 HHSB-4 (1-2)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Metals
Prep Batch: 496285
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3051A490-146593-1 HHSB-1 (1-2)Total/NA
Solid 3051A490-146593-2 HHSB-2 (1-2)Total/NA
Solid 3051A490-146593-3 HHSB-3 (0-1)Total/NA
Solid 3051A490-146593-4 Duplicate-2 Total/NA
Solid 3051A490-146593-5 HHSB-4 (1-2)Total/NA
Solid 3051A490-146593-6 HHSB-5 (0-1)Total/NA
Solid 3051A490-146593-7 BKG-1 (1-2)Total/NA
Solid 3051A490-146593-8 BKG-2 (1-2)Total/NA
Solid 3051AMB 490-496285/1-A Method Blank Total/NA
Solid 3051ALCS 490-496285/2-A Lab Control Sample Total/NA
Solid 3051A490-146593-1 MS HHSB-1 (1-2)Total/NA
Solid 3051A490-146593-1 MSD HHSB-1 (1-2)Total/NA
Prep Batch: 496568
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B490-146593-1 HHSB-1 (1-2)Total/NA
Solid 7471B490-146593-2 HHSB-2 (1-2)Total/NA
Solid 7471B490-146593-3 HHSB-3 (0-1)Total/NA
Solid 7471B490-146593-4 Duplicate-2 Total/NA
Solid 7471B490-146593-5 HHSB-4 (1-2)Total/NA
Solid 7471B490-146593-6 HHSB-5 (0-1)Total/NA
Solid 7471B490-146593-7 BKG-1 (1-2)Total/NA
Solid 7471B490-146593-8 BKG-2 (1-2)Total/NA
Solid 7471BMB 490-496568/1-A Method Blank Total/NA
Solid 7471BLCS 490-496568/2-A Lab Control Sample Total/NA
Solid 7471BLCSD 490-496568/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 496726
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6020B 496285490-146593-1 HHSB-1 (1-2)Total/NA
Solid 6020B 496285490-146593-2 HHSB-2 (1-2)Total/NA
Solid 6020B 496285490-146593-3 HHSB-3 (0-1)Total/NA
Solid 6020B 496285490-146593-4 Duplicate-2 Total/NA
Solid 6020B 496285490-146593-5 HHSB-4 (1-2)Total/NA
Solid 6020B 496285490-146593-6 HHSB-5 (0-1)Total/NA
Solid 6020B 496285490-146593-7 BKG-1 (1-2)Total/NA
Solid 6020B 496285490-146593-8 BKG-2 (1-2)Total/NA
Solid 6020B 496285MB 490-496285/1-A Method Blank Total/NA
Solid 6020B 496285LCS 490-496285/2-A Lab Control Sample Total/NA
Solid 6020B 496285490-146593-1 MS HHSB-1 (1-2)Total/NA
Solid 6020B 496285490-146593-1 MSD HHSB-1 (1-2)Total/NA
Analysis Batch: 496773
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 496568490-146593-1 HHSB-1 (1-2)Total/NA
Solid 7471B 496568490-146593-2 HHSB-2 (1-2)Total/NA
Solid 7471B 496568490-146593-3 HHSB-3 (0-1)Total/NA
Solid 7471B 496568490-146593-4 Duplicate-2 Total/NA
Solid 7471B 496568490-146593-5 HHSB-4 (1-2)Total/NA
Solid 7471B 496568490-146593-6 HHSB-5 (0-1)Total/NA
Solid 7471B 496568490-146593-7 BKG-1 (1-2)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Metals (Continued)
Analysis Batch: 496773 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7471B 496568490-146593-8 BKG-2 (1-2)Total/NA
Solid 7471B 496568MB 490-496568/1-A Method Blank Total/NA
Solid 7471B 496568LCS 490-496568/2-A Lab Control Sample Total/NA
Solid 7471B 496568LCSD 490-496568/3-A Lab Control Sample Dup Total/NA
General Chemistry
Prep Batch: 496532
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A490-146593-1 HHSB-1 (1-2)Total/NA
Solid 3060A490-146593-2 HHSB-2 (1-2)Total/NA
Solid 3060A490-146593-3 HHSB-3 (0-1)Total/NA
Solid 3060A490-146593-4 Duplicate-2 Total/NA
Solid 3060A490-146593-5 HHSB-4 (1-2)Total/NA
Solid 3060A490-146593-6 HHSB-5 (0-1)Total/NA
Solid 3060A490-146593-7 BKG-1 (1-2)Total/NA
Solid 3060A490-146593-8 BKG-2 (1-2)Total/NA
Solid 3060AMB 490-496532/1-A Method Blank Total/NA
Solid 3060ALCSI 490-496532/3-A Lab Control Sample Total/NA
Solid 3060ALCSS 490-496532/2-A Lab Control Sample Total/NA
Solid 3060A490-146593-1 MSI HHSB-1 (1-2)Total/NA
Solid 3060A490-146593-1 MSS HHSB-1 (1-2)Total/NA
Solid 3060A490-146593-1 DU HHSB-1 (1-2)Total/NA
Analysis Batch: 496682
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture490-146593-1 HHSB-1 (1-2)Total/NA
Solid Moisture490-146593-2 HHSB-2 (1-2)Total/NA
Solid Moisture490-146593-3 HHSB-3 (0-1)Total/NA
Solid Moisture490-146593-4 Duplicate-2 Total/NA
Solid Moisture490-146593-5 HHSB-4 (1-2)Total/NA
Solid Moisture490-146593-6 HHSB-5 (0-1)Total/NA
Solid Moisture490-146593-7 BKG-1 (1-2)Total/NA
Solid Moisture490-146593-8 BKG-2 (1-2)Total/NA
Solid Moisture490-146592-G-34 DU Duplicate Total/NA
Solid Moisture490-146624-E-4 DU Duplicate Total/NA
Analysis Batch: 496728
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 496532490-146593-1 HHSB-1 (1-2)Total/NA
Solid 7196A 496532490-146593-2 HHSB-2 (1-2)Total/NA
Solid 7196A 496532490-146593-3 HHSB-3 (0-1)Total/NA
Solid 7196A 496532490-146593-4 Duplicate-2 Total/NA
Solid 7196A 496532490-146593-5 HHSB-4 (1-2)Total/NA
Solid 7196A 496532490-146593-6 HHSB-5 (0-1)Total/NA
Solid 7196A 496532490-146593-7 BKG-1 (1-2)Total/NA
Solid 7196A 496532490-146593-8 BKG-2 (1-2)Total/NA
Solid 7196A 496532MB 490-496532/1-A Method Blank Total/NA
Solid 7196A 496532LCSI 490-496532/3-A Lab Control Sample Total/NA
Solid 7196A 496532LCSS 490-496532/2-A Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
General Chemistry (Continued)
Analysis Batch: 496728 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7196A 496532490-146593-1 MSI HHSB-1 (1-2)Total/NA
Solid 7196A 496532490-146593-1 MSS HHSB-1 (1-2)Total/NA
Solid 7196A 496532490-146593-1 DU HHSB-1 (1-2)Total/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146593-1
Project/Site: Little Rock Road Brownfield SDG: RKI-008
Client Sample ID: HHSB-1 (1-2)Lab Sample ID: 490-146593-1
Matrix: SolidDate Collected: 02/15/18 10:05
Date Received: 02/17/18 09:25
Prep 5035 JLP02/15/18 09:05 TAL NSH496324
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 7.217 g 5.0 mL
Analysis 8260B 1 496298 02/19/18 13:53 RP TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 496428 02/19/18 14:03 AMD TAL NSHTotal/NA 30.45 g 1.00 mL
Analysis 8270D 1 496518 02/20/18 13:58 KME TAL NSHTotal/NA
Prep 3051A 496285 02/19/18 09:17 WJE TAL NSHTotal/NA 0.53 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:18 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:01 RDH TAL NSHTotal/NA 0.598 g 100 mL
Analysis 7471B 1 496773 02/20/18 15:42 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.5478 g 500 mL
Analysis 7196A 1 496728 02/20/18 15:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Client Sample ID: HHSB-2 (1-2)Lab Sample ID: 490-146593-2
Matrix: SolidDate Collected: 02/15/18 15:35
Date Received: 02/17/18 09:25
Prep 5035 JLP02/15/18 14:35 TAL NSH496324
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.735 g 5.0 mL
Analysis 8260B 1 496298 02/19/18 14:20 RP TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 496428 02/19/18 14:03 AMD TAL NSHTotal/NA 30.91 g 1.00 mL
Analysis 8270D 1 496518 02/20/18 14:18 KME TAL NSHTotal/NA
Prep 3051A 496285 02/19/18 09:17 WJE TAL NSHTotal/NA 0.52 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:33 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:01 RDH TAL NSHTotal/NA 0.616 g 100 mL
Analysis 7471B 1 496773 02/20/18 15:45 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.5269 g 500 mL
Analysis 7196A 1 496728 02/20/18 15:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Client Sample ID: HHSB-3 (0-1)Lab Sample ID: 490-146593-3
Matrix: SolidDate Collected: 02/15/18 16:50
Date Received: 02/17/18 09:25
Prep 5035 JLP02/15/18 15:50 TAL NSH496324
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.417 g 5.0 mL
Analysis 8260B 1 496298 02/19/18 14:48 RP TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 496428 02/19/18 14:03 AMD TAL NSHTotal/NA 30.31 g 1.00 mL
Analysis 8270D 1 496518 02/20/18 14:39 KME TAL NSHTotal/NA
Prep 3051A 496285 02/19/18 09:17 WJE TAL NSHTotal/NA 0.59 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:37 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:01 RDH TAL NSHTotal/NA 0.606 g 100 mL
Analysis 7471B 1 496773 02/20/18 15:48 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.5210 g 500 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146593-1
Project/Site: Little Rock Road Brownfield SDG: RKI-008
Client Sample ID: HHSB-3 (0-1)Lab Sample ID: 490-146593-3
Matrix: SolidDate Collected: 02/15/18 16:50
Date Received: 02/17/18 09:25
Analysis 7196A BMC02/20/18 15:111 TAL NSH496728
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Client Sample ID: Duplicate-2 Lab Sample ID: 490-146593-4
Matrix: SolidDate Collected: 02/15/18 16:45
Date Received: 02/17/18 09:25
Prep 5035 JLP02/15/18 15:45 TAL NSH496324
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 7.631 g 5.0 mL
Analysis 8260B 1 496298 02/19/18 15:16 RP TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 496428 02/19/18 14:03 AMD TAL NSHTotal/NA 30.28 g 1.00 mL
Analysis 8270D 1 496518 02/20/18 14:59 KME TAL NSHTotal/NA
Prep 3051A 496285 02/19/18 09:17 WJE TAL NSHTotal/NA 0.55 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:46 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:01 RDH TAL NSHTotal/NA 0.610 g 100 mL
Analysis 7471B 1 496773 02/20/18 15:50 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.4910 g 500 mL
Analysis 7196A 1 496728 02/20/18 15:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Client Sample ID: HHSB-4 (1-2)Lab Sample ID: 490-146593-5
Matrix: SolidDate Collected: 02/16/18 09:30
Date Received: 02/17/18 09:25
Prep 5035 JLP02/16/18 08:30 TAL NSH496324
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 7.426 g 5.0 mL
Analysis 8260B 1 496298 02/19/18 15:44 RP TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 496428 02/19/18 14:03 AMD TAL NSHTotal/NA 30.65 g 1.00 mL
Analysis 8270D 1 496813 02/21/18 10:45 KME TAL NSHTotal/NA
Prep 3051A 496285 02/19/18 09:17 WJE TAL NSHTotal/NA 0.58 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:49 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:01 RDH TAL NSHTotal/NA 0.608 g 100 mL
Analysis 7471B 1 496773 02/20/18 15:53 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.5237 g 500 mL
Analysis 7196A 1 496728 02/20/18 15:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Client Sample ID: HHSB-5 (0-1)Lab Sample ID: 490-146593-6
Matrix: SolidDate Collected: 02/16/18 09:00
Date Received: 02/17/18 09:25
Prep 5035 JLP02/16/18 08:00 TAL NSH496324
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.473 g 5.0 mL
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146593-1
Project/Site: Little Rock Road Brownfield SDG: RKI-008
Client Sample ID: HHSB-5 (0-1)Lab Sample ID: 490-146593-6
Matrix: SolidDate Collected: 02/16/18 09:00
Date Received: 02/17/18 09:25
Analysis 8260B RP02/19/18 16:111 TAL NSH496298
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 g 5 mL
Prep 3550C 496428 02/19/18 14:03 AMD TAL NSHTotal/NA 30.74 g 1.00 mL
Analysis 8270D 1 496518 02/20/18 15:40 KME TAL NSHTotal/NA
Prep 3051A 496285 02/19/18 09:17 WJE TAL NSHTotal/NA 0.60 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:52 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:01 RDH TAL NSHTotal/NA 0.618 g 100 mL
Analysis 7471B 1 496773 02/20/18 15:56 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.5199 g 500 mL
Analysis 7196A 1 496728 02/20/18 15:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Client Sample ID: BKG-1 (1-2)Lab Sample ID: 490-146593-7
Matrix: SolidDate Collected: 02/16/18 10:30
Date Received: 02/17/18 09:25
Prep 3051A WJE02/19/18 09:17 TAL NSH496285
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 0.59 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:55 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:11 RDH TAL NSHTotal/NA 0.624 g 100 mL
Analysis 7471B 1 496773 02/20/18 15:59 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.5501 g 500 mL
Analysis 7196A 1 496728 02/20/18 15:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Client Sample ID: BKG-2 (1-2)Lab Sample ID: 490-146593-8
Matrix: SolidDate Collected: 02/16/18 11:00
Date Received: 02/17/18 09:25
Prep 3051A WJE02/19/18 09:17 TAL NSH496285
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 0.54 g 100 mL
Analysis 6020B 1 496726 02/20/18 10:58 BLG TAL NSHTotal/NA
Prep 7471B 496568 02/20/18 10:11 RDH TAL NSHTotal/NA 0.619 g 100 mL
Analysis 7471B 1 496773 02/20/18 16:01 RDH TAL NSHTotal/NA
Prep 3060A 496532 02/20/18 09:07 BMC TAL NSHTotal/NA 2.5775 g 500 mL
Analysis 7196A 1 496728 02/20/18 15:11 BMC TAL NSHTotal/NA 50 mL 50 mL
Analysis Moisture 1 496682 02/20/18 12:34 BAA TAL NSHTotal/NA
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-146593-1Client: Hart & Hickman, PC
SDG: RKI-008Project/Site: Little Rock Road Brownfield
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8466020BMetals (ICP/MS)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
SW8467196AChromium, Hexavalent TAL NSH
EPAMoisturePercent Moisture TAL NSH
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Accreditation/Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-146593-1
Project/Site: Little Rock Road Brownfield SDG: RKI-008
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-18
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
Moisture Solid Percent Solids
TestAmerica Nashville
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