19028 NoDaTextile_EMP-Addendum complete

From:Minnich, Carolyn
To:"Corbitt, Chris L."
Cc:"Franchina, Dave ([e-mail])"; "[e-mail]"; Sullivan, Mike
Subject:RE: [External] Finalized EMP Amendment letter for NoDa Textile BF Site - Phase 2
Date:Thursday, February 01, 2018 9:38:00 AM
Attachments:19028 NoDa EMP and Addendum 20180201.pdfimage003.pngimage001.png
Thank you the addendum is acceptable. The attached document is the complete EMP from 2016 and
Addendum together. Please provide to the GC. I will update on Laserfiche. If you have questions or
comments, please contact me.

Carolyn Minnich
Brownfields Project Manager
Division of Waste Management
Department of Environmental Quality

704 661 0330 office/mobile
[e-mail]

1646 Mail Service Center
Raleigh, NC 27699-1646

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Corbitt, Chris L. [mailto:[e-mail]]
Sent: Tuesday, January 30, 2018 2:32 PM
To: Minnich, Carolyn <[e-mail]>
Cc: 'Franchina, Dave ([e-mail])' <[e-mail]>;
'[e-mail]' <[e-mail]>; Sullivan,
Mike <[e-mail]>
Subject: [External] Finalized EMP Amendment letter for NoDa Textile BF Site - Phase 2

CAUTION: External email. Do not click links or open attachments unless verified. Send all suspicious email as an
attachment to [e-mail].

Carolyn,
Attached is the finalized version of the EMP Amendments letter for the NoDa Textile BF site, Phase
2. Please let me know if you need anything else.
Thanks,
Chris

Christopher L. Corbitt, PG
Senior Geologist  I  Environmental Services
Terracon Consultants, Inc
2701 Westport Road  I Charlotte, NC 28208 
P 704-509-1777 I F 704-509-1888 I M 704-301-3089
[e-mail] I www.terracon.com
P Please consider the environment before printing this e-mail.

Terracon provides environmental, facilities, geotechnical, and materials consulting engineering services delivered
with responsiveness, resourcefulness, and reliability.
Private and confidential as detailed here (www.terracon.com/disclaimer). If you cannot access hyperlink,
please e-mail sender.
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Approved EMP, February 12, 2015
NORTH CAROLINA BROWNFIELDS PROGRAM
ENVIRONMENTAL MANAGEMENT PLAN
This form is to be used to prepare an Environmental Management Plan (EMP) for projects in the
North Carolina Brownfields Program at the direction of a project manager for the program.
Prospective Developers and/or their consultants must complete and submit this form and all
pertinent attachments to their project manager prior to any site earthmoving or other
development related activities. For the resultant EMP to be valid for use, it must be completed,
reviewed by the program, and signed by all signers at the bottom. Consult your project manager
if you have questions.
GENERAL INFORMATION
Date: February 15, 2016
Brownfields Assigned Project Name: NoDa Textile Brownfields Site
Brownfields Project Number: 19028-15-060
Brownfields Property Address: 430 East 36th Street, Charlotte, Mecklenburg County
Brownfields Property Area (acres): 5.816 acres
Is Brownfields Property Subject to RCRA Permit?☐ Yes ☒ No
If yes enter Permit No.: Not Applicable
Is Brownfields Property Subject to a Solid Waste Permit?☐ Yes ☒ No
If yes, enter Permit No.: Not Applicable
COMMUNICATIONS
Prospective Developer (PD):Crescent NoDa, LLC
Phone Numbers: Office:980.321.6194 Mobile:[phone]
Email:[e-mail]
Primary PD Contact:Ms. Katie Maloomian
Phone Numbers: Office:980.321.6194 Mobile:[phone]
Email:[e-mail]
Environmental Consultant:Mr. Chris Corbitt at Terracon Consultants, Inc.
Phone Numbers: Office:704.509.1777 Mobile:[phone]
Email:[e-mail]
Brownfields Program Project Manager:Ms. Carolyn Minnich
Office:704.661.0330
Email:[e-mail]
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Approved EMP, February 12, 2015
Other DENR Program Contacts (if applicable, i.e., UST Section, Inactive Hazardous Site Branch,
Hazardous Waste, Solid Waste):Not Applicable
NOTIFICATIONS TO THE BROWNFIELDS PROGRAM
Advance Notification Times to Brownfields Project Manager: Check each box to accept minimum notice
periods (in calendar days) for each type of on-site task:
On-site assessment or remedial activities:Within 10 days ☒
Construction or grading start:Within 10 days ☒
Discovery of stained soil, odors, USTs, buried drums or waste, landfill, or other signs of previously
unknown contamination:Within 48 hours ☒
Implementation of emergency actions (e.g. dewatering, flood, or soil erosion control
measures in area of contamination, venting of explosive environments):
Within 48 hours ☒
Installation of Mitigation systems:Within 10 days ☒
Other notifications as required by local, state or federal agencies to implement
redevelopment activities: (as applicable):Within 30 days ☒
REDEVELOPMENT PLANS
1)Type of Redevelopment (check all that apply):
☒ Residential ☒ Recreational ☐ Institutional ☒ Commercial ☒ Office ☒Retail ☐ Industrial
☒ Other, specify:Hotel and parking
2) Summary of Redevelopment Plans (attach conceptual or detailed plans as available): See
Appendix A.
a)Do plans include demolition of structure(s)?:☒ Yes ☐ No ☐ Unknown
b) Do plans include removal of building foundation slab(s) or pavement:
☒ Yes ☐ No ☐ Unknown
c)Provide brief summary of redevelopment plans, including demolition, removal of building
slabs/pavement and other structures:Two existing on-site buildings will be demolished and their
slabs removed prior to redevelopment of the site. Most of the site will be graded during
redevelopment. A new building will be located in the southwestern portion of the property.
Redevelopment plans include a first-floor retail level with residential above and adjacent to the
retail level. The proposed building includes 344 apartment units ranging from 5 to 7 stories. A
partially enclosed basement area is planned in the westernmost portion of the building with the
remaining structures built on-grade. Redevelopment plans also include a parking area to the east
of the building and a multi-level parking deck adjoining the building to the north. Two open
courtyard areas will be located at the center of the main building. New access roads and pavement
will be constructed along the perimeter. Redevelopment plans are included as Appendix A.
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Approved EMP, February 12, 2015
3)Which category of risk-based screening level is used or is anticipated to be specified in the
Brownfields Agreement?
☒ Residential ☐Non-residential or Industrial/Commercial
Note: If children frequent the property, residential screening levels shall be cited in the Brownfields
Agreement for comparison purposes.
4) Schedule for Redevelopment (attach construction schedule):Actual schedule has not been
prepared. We will provide the schedule as it becomes available.
a)Phase I start date and anticipated duration (specify activities during each phase):TBD
b)If applicable, Phase 2 start date and anticipated duration (specify activities during each
phase): An additional building is planned for some point in the future. The date is unknown at
this time. The building will likely include ground floor retail with office, hotel, or multi-family
residential space above.
c)Additional phases planned? If yes, specify activities if known:
Yes ☐ Not in the foreseeable future ☒
Decision pending☐
d)Provide the planned date of occupancy for new buildings:TBD
CONTAMINATED MEDIA
Contaminated Media (attach tabulated data summaries for each impacted media and figure(s) with
sample locations): Tabulated data and figures are provided in Appendix B.
Part 1. Soil:☒ Yes ☐ No ☐ Suspected
Part 2. Groundwater:☒ Yes ☐ No ☐ Suspected
Part 3. Surface Water:☐ Yes ☒ No ☐ Suspected
Part 4. Sediment:☐ Yes ☒ No ☐ Suspected
Part 5. Soil Vapor:☐ Yes ☐ No ☒ Suspected
Part 6. Sub-Slab Soil Vapor:☐ Yes ☐ No ☒ Suspected
Part 7. Indoor Air:☐ Yes ☐ No ☒ Suspected
PART 1. SOIL – Please fill out the information below, using detailed site plans, if available, or estimate
using known areas of contaminated soil and a conceptual redevelopment plan. Provide a figure
overlaying new construction onto figure showing contaminated soil and groundwater locations.
1)Known or suspected contaminants in soil (list specific compounds): Based on review of the historical
information, the eastern portion of site was developed as a fire extinguisher manufacturing company
in the early 1900s. By the early 1930s, New England Waste Company occupied the site as a re-user of
waste cotton products provided from nearby textile mills. Newco Fibre, another textile-related
company occupied the site from the mid-1960s to the early 2000s. Ultimate Gym and the Chop Shop,
a concert venue, have occupied the remaining two buildings on the site since 2006.
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Approved EMP, February 12, 2015
Volatile Organic Compounds (VOCs):
During the Limited Site Investigation at the site, soil samples obtained for chemical analysis were
collected at depths ranging from 6 to 24 feet below ground surface. Methylene Chloride (boring B-
12) and tetrachloroethene (boring B-4) were detected in soils above their respective Protection of
Groundwater PSRGs; however, no volatile compounds were detected above the Residential and
Industrial PSRGs.
Semi-Volatile Organic Compounds (SVOCs):
Based on past assessment activities by Terracon and others, various polynuclear aromatic
hydrocarbons (PAHs) were detected in soils in the eastern (beneath former Newco Fibre building, now
demolished), western (parking area) and central (beneath Ultimate Gym building) portions of the site.
A figure depicting the locations of the borings is attached to this EMP. PAH constituents detected at
low concentrations in the soils that exceeded their respective Preliminary Residential Health Based
Remediation Goals established by the North Carolina Department of Environmental Quality (NCDEQ)
included benzo(a)anthracene, benzo(b)fluoranthene, indeno(1,2,3-cd)pyrene, and benzo(a)pyrene.
Other PAHs were detected at the site but the concentrations are below current regulatory standards.
Metals:
Previous on-site soil samples collected by Hart & Hickman (H&H) contained arsenic above current NC
DEQ Preliminary Soil Remediation Goals (PSRGs). Soil sampling results and sample locations are
provided in Appendix B.
2)Depth of known or suspected contaminants (feet):
Volatile Organic Compounds:
Methylene Chloride (boring B-12) and tetrachloroethene (boring B-4) were detected above their
respective Protection of Groundwater PSRGs at depths of 13-14 and 18-20 feet below ground surface
(bgs) but below residential standards;
Semi-Volatile Organic Compounds:
Semi-volatile compounds were detected above their respective Protection of Groundwater and
Residential PSRGs at depths of 19-20 and 15-16 feet bgs in borings B-10 and B-13, respectively.
Additionally, benzo[a]pyrene was present at a concentration higher than the Industrial PSRG at a
depth of 19-20 feet bgs in boring B-10. A previous assessment of the parcel by H&H in 2007 detected
SVOCs in shallower soils (1.5-2.5 feet bgs) at concentrations above PSRGs.
Metals:
H&H detected arsenic above residential standards in soils at the site at depths ranging from 1.5 to 2.5
feet bgs.
3)Area of soil disturbed by redevelopment (square feet):Approximately 5.5 acres based on the 50%
design plan.
4)Depths of soil to be excavated (feet):Grading/excavation activities are generally limited to the
upper 2 feet (maximum of 2.3 feet according to the cut and fill diagram provided in Appendix A).
5)Estimated volume of soil (cubic yards) to be excavated (attach grading plan):The estimated
volume of excavation/cut material is 664 cubic yards. A grading plan and a cut and fill diagram are
included in Appendix A.
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Approved EMP, February 12, 2015
6)Estimated volume of excavated soil (cubic yards) anticipated to be impacted by contaminants:
Excavated soil is not anticipated to be impacted by contaminants exceeding applicable soil screening
levels.
7)Estimated volume of contaminated soil expected to be disposed offsite, if applicable:Disposal of
impacted soils at off-site locations is not anticipated at this time; however, if impacted soils are
encountered that require disposal at an off-site location, these activities will be initiated in accordance
with disposal facility requirements and NCDEQ regulations.
IMPORTED FILL SOIL
1)Will fill soil be imported to the site?☒ Yes ☐ No ☐Unknown
2)If yes, what is the estimated volume of fill soil to be imported?The estimated volume of fill soil
that will be imported to the site is 33,260 cubic yards.
3)If yes, what is the depth of fill soil to be used at the property?The depth of the fill soil varies
throughout the site. From 0 up to 14 feet of fill soil is planned according to the cut and fill diagram in
Appendix A. Most of the imported fill materials will be placed in the northern portions of the site.
4)PRIOR TO ITS PLACEMENT AT THE BROWNFIELDS PROPERTY. Provide plan to analyze fill soil to
demonstrate that it meets acceptable standards and can be considered clean for use at the
Brownfields property (Check all that apply), or attach existing data:A borrow site for the required
fill soil has been identified. The borrow site is located at 1301 East Morehead Street in Charlotte,
North Carolina. Soil samples were collected and submitted for laboratory analysis for this borrow
site by GeoScience Group and soils from the borrow site have been approved for use at Brownfields
Project Number 19032-15-060 (Central Avenue Apartments). The laboratory analytical reports are
included in Appendix B of this EMP. For the purpose of characterization of borrow fill, the same
laboratory analytical data will be used to fulfill the requirements for the NoDa Textile Brownfields
site.
☐ Volatile organic compounds (VOCs) by EPA Method 8260
☐ Semi-volatile organic compounds (SVOCs) by EPA Method 8270
☐ Metals RCRA List (8) (arsenic, barium, cadmium, chromium (speciated), mercury, lead,
selenium and silver)
☐ Metals – Hazardous Substance List -14 (antimony, arsenic, beryllium, cadmium, chromium
(speciated according to IHSB protocol), copper, lead, manganese, mercury, nickel, selenium,
silver, thallium, and zinc)
☐ Metals – EPA Priority Pollutant List – 13 (arsenic, beryllium, cadmium, chromium (speciated
according to IHSB protocol), copper, mercury, nickel, lead, antimony, selenium, silver,
thallium, and zinc)
☐ Other Constituents and Analytical Method:Click here to enter text.
☒ Known borrow material (DESCRIBE SOURCE AND ATTACH SAMPLING PROFILE):See
description above.
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Approved EMP, February 12, 2015
MANAGING ON-SITE SOIL
1)If soil in known or suspected areas of contamination is anticipated to be excavated from the
Brownfield Property, relocated on the Brownfields Property, or otherwise disturbed during site
grading or other redevelopment activities, please provide a grading plan that clearly illustrates
areas of cut and fill (approximate areas and volumes are acceptable, if only preliminary data
available).Current plans do not involve excavation or moving of impacted soil. A grading plan is
provided in Appendix A.
2)HAZARDOUS WASTE DETERMINATION – Does the soil contain a LISTED WASTE as defined in the
North Carolina Hazardous Waste Section under 40 CFR Part 261.31-261.35?☐ Yes ☒ No
8)If yes, explain why below, including the level of knowledge regarding processes generating the
waste (include pertinent analytical results as needed).Not Applicable
If yes, do the soils exceed the “Contained-Out” levels in Attachment 1 of the North Carolina
Contained-In Policy? ☐ Yes ☒ No Not Applicable
NOTE: IF SOIL MEETS THE DEFINITION OF A LISTED HAZARDOUS WASTE AND EXCEEDS THE CONTAINED-
OUT LEVELS IN ATTACHMENT 1 TO THE NORTH CAROLINA CONTAINED-IN POLICY THE SOIL MAY NOT
BE RE-USED ON SITE AND MUST BE DISPOSED OF IN ACCORDANCE WITH NCDEQ HAZARDOUS WASTE
SECTION RULES AND REGULATIONS.
3)☐ Hazardous Waste Determination – Does the soil contain a CHARACTERISTIC WASTE?
☐ Yes ☒ No
If yes, mark reason(s) why below (and include pertinent analytical results). If no, explain rationale:
Historical analytical results from the site did not identify soils that were considered to be hazardous waste.
Recent soil sampling activities at the site did not detect constituents of concern that are deemed
hazardous by characteristic using the Rule of 20 (Arsenic, cadmium, and hexavalent chromium).
☐ Ignitability
☐ Corrosivity
☐ Reactivity
☐ Toxicity
☐ TCLP results
☐ Rule of 20 results (20 times total analytical results for an individual hazardous
constituent on TCLP list cannot, by test method, exceed regulatory TCLP standard)
NOTE: IF SOIL MEETS THE DEFINITION OF A CHARACTERISTIC HAZARDOUS WASTE, THE SOIL MAY NOT
BE RE-USED ON SITE AND MUST BE DISPOSED OF IN ACCORDANCE WITH DENR HAZARDOUS WASTE
SECTION RULES AND REGULATIONS.
4)Screening criteria by which soil disposition decisions will be made (e.g., left in place, capped in place
with low permeability barrier, removed to on-site location and capped, removed offsite):
☒ Preliminary Health-Based Residential SRGs dated September 2015
☐ Preliminary Health-Based Industrial/Commercial SRGs INSERT DATE.
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Approved EMP, February 12, 2015
☐ Site-specific risk-based cleanup level, or acceptable concentrations determined via
calculated cumulative risk. Enter details of methods used for determination/explanation:
Click here to enter text.
5) Check the following action(s) to be taken during excavation and management of said soils:
☐ Manage fugitive dust from site:
☐ Yes ☒ No
If yes, describe method; If no, explain rationale: Monitoring of fugitive dust for constituents of
concern (VOCs and SVOCs) will not be conducted at the site. These types of constituents of concern
typically do not adhere to airborne particulate matter. Unlike metals, VOCs and SVOCs will generally
vaporize into the air. Soils that are dry and have the potential to migrate through air from the site will be
managed in accordance with typical construction practices. This usually takes the form of a light
application of water periodically to moisten soils and reduce airborne dust.
☒ Field Screening:
☒ Yes ☐ No
If yes, describe method; If no, explain rationale: When chemical odors are detected during
grading/excavation activities at the site, the soils will be screened with a photo-ionization detector (PID)
to identify relative concentrations and evaluate the need for sampling and laboratory analysis.
☒ Soil Sample Collection:
☒ Yes ☐ No
If yes, describe method (e.g., in-situ grab, composite, stockpile, etc.); If no, explain rationale:
If during grading, impacted soils are discovered, procedures for screening and sampling the soils
will be implemented as described in Part 9 “Contingency for encountering unknown tanks, drums,
or other waste materials”.
☐ Stockpile impacted soil in accordance with NCDEQ IHSB protocol in the current version of
the “Guidelines for Assessment and Cleanup”, and providing erosion control, prohibiting
contact between surface water/precipitation and contaminated soil, and preventing
contaminated runoff. Explain any variances:
Click here to enter text.
☒ Analyze potentially impacted soil for the following chemical analytes:
☒ Volatile organic compounds (VOCs) by EPA Method 8260
☒ Semi-volatile organic compounds (SVOCs) by EPA Method 8270
☒ Metals RCRA List (8) (arsenic, barium, cadmium, chromium (speciated), mercury,
lead, selenium and silver)
☐ Metals –Hazardous Substance List -14 (antimony, arsenic, beryllium, cadmium,
chromium (speciated according to IHSB protocol), copper, lead, manganese, mercury,
nickel, selenium, silver, thallium, and zinc)
☐ Metals – EPA Priority Pollutant List – 13 (arsenic, beryllium, cadmium, chromium
(speciated according to IHSB protocol), copper, mercury, nickel, lead, antimony,
selenium, silver, thallium, and zinc)
☐ Other Constituent(s) and Analytical Method(s):Click here to enter text.
☒ Proposed Measures to Obtain Pre-Approval for Reuse of Impacted Soil within the
Brownfields Property Boundary
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Approved EMP, February 12, 2015
☒ Provide documentation of analytical report(s) to Brownfields Project Manager
☒ Provide documentation of final location, thickness and depth of relocated soil on
site map to Brownfields Project Manager once known
☐ Use geotextile to mark depth of fill material (provide description of material)
☒ Manage soil under impervious cap ☒ or clean fill ☒
Describe cap or fill:To be determined but likely placed beneath structures or pavement
areas, if necessary (provide location diagram).
☒ Confer with NC BF Project Manager if Brownfield Plat must be revised (or re-
recorded if actions are Post-Recordation).
☐ Other:Click here to enter text.
☒ Final grade sampling of exposed soil (i.e., soil that will not be under buildings or permanent
hardscape): [if not checked provide rationale for not needing]Based on initial development plans
for the site, exposed soils (not under structures or hardscapes) will be mostly limited to
landscaped areas along the northern and eastern perimeter of the site where significantly
impacted soils are not anticipated. If contaminated soils are encountered in areas of exposed
soils, these soils will be managed in accordance with contingency procedures discussed in Part 9
of this EMP. Because of limited knowledge regarding site conditions, final grade sampling will be
conducted to ensure that the property is safe for its intended reuse.
Provide diagram of soil sampling locations, number of samples, and denote Chemical Analytical
Program with check boxes below (Check all that apply):
☒ Volatile organic compounds (VOCs) by EPA Method 8260
☒ Semi-volatile organic compounds (SVOCs) by EPA Method 8270
☒ Metals RCRA List (8) (arsenic, barium, cadmium, chromium (speciated), mercury,
lead, selenium and silver)
☐ Metals –Hazardous Substance List -14 (antimony, arsenic, beryllium, cadmium,
chromium (speciated according to IHSB protocol), copper, lead, manganese, mercury,
nickel, selenium, silver, thallium, and zinc)
☐ Metals – EPA Priority Pollutant List – 13 (arsenic, beryllium, cadmium, chromium
(speciated according to IHSB protocol), copper, mercury, nickel, lead, antimony,
selenium, silver, thallium, and zinc)
☐ Pesticides
☐ PCBs
☐ Other Constituents & Analytical Method: Click here to enter text.
OFF-SITE TRANSPORT & DISPOSITION OF EXCAVATED SOIL
NOTE: Unless soil will be transported offsite for disposal in a permitted facility under applicable
regulations, no contaminated or potentially contaminated soil may leave the site without approval from
the brownfields program. Failure to obtain approval may violate a brownfields agreement, endangering
liability protections and making said action subject to enforcement. Justifications provided below must
be approved by the Program in writing prior to completing transport activities.
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Approved EMP, February 12, 2015
☐ Transport and dispose of impacted soil offsite (documentation of final disposition must be sent to
Brownfields Project Manager)
☒ Landfill – analytical program determined by landfill: Off-site disposal of impacted soils is not
anticipated at this time; however, if grading specifications are not met, off-site disposal options
will be considered.
☒ Landfarm or other treatment facility:Off-site disposal of impacted soils is not anticipated at
this time; however, if grading specifications are not met, off-site disposal options will be
considered.
☐ Use as Beneficial Fill Offsite – provide justification:Click here to enter text.
☐ Use as Beneficial Fill at another Suitable Brownfields Site – (Note: a determination that a
site is a “Suitable Brownfields site will require, at a minimum, that similar concentrations of the same
or similar contaminants already exist at both sites, use of impacted soil as beneficial soil will not
increase the potential for risk to human health and the environment at that site, and that notarized
documentation of the acceptance of such soil from the property owner of the receiving site is provided
to Brownfields. Provide justification:Click here to enter text.
MANAGEMENT OF UTILITY TRENCHES
☐ Install liner between native impacted soils and base of utility trench before filling with clean fill
(Preferred)
☒ Last out, first in principle for impacted soils (if soil can safely be reused onsite and is not a hazardous
waste), i.e., impacted soils are placed back at approximately the depths they were removed from such
that impacted soil is not placed at a greater depth than the original depth from which it was excavated.
During initial site grading activities, certain uncapped areas of the site and soils beneath areas capped by
existing concrete building pads are assumed to be potentially impacted by COCs (based on known
contaminants and concentrations); thus, workers should use appropriate safety apparel.
Soils will at times need to be disturbed for the construction of utilities or other structures. With respect
to subsurface utility construction at the site, the general rule will be to remove and stockpile soils so that
a “last out, first in” process occurs. During excavation, soils in the upper 2 feet should be stockpiled and
segregated as the first materials removed. These soils/fill materials will be the last returned to the
excavation during backfilling. Utility trenches will be backfilled with clean soils.
Soils will typically “bulk” or expand in volume when disturbed by excavation. The contractor will compact
these materials into place according to the compaction requirements of the construction design. If no
specifications for compacted fill exist, the contractor will tamp the materials in place using the mechanical
excavator or equivalent. Utilities or structures will replace a certain volume of soils in these areas,
resulting in excess soils as excavation spoils.
After the initial grading of the site, the worker and contractor should plan from onset of construction to
maintain a cap comprised of either (a) clean fill, or (b) other barrier approved by the NC DEQ for areas
that will not be capped with a building, asphalt, or concrete surface. If excess contaminant impacted
soils/fill are produced from excavation as spoils which cannot be restored to original depths through the
process of “first out, last in”, they must be handled with special care. The worker or contractor will work
with the Brownfields Project Manager to ensure that, if the soils are contaminated, they are either
properly re-used on-site or disposed of off-site.
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Approved EMP, February 12, 2015
☐ Evaluate whether necessary to install barriers in conduits to prevent soil vapor transport, and/or
degradation of conduit materials due to direct impact with contaminants? Result: Yes □ No □
If no, include rationale here.To be determined based on future development plans.
If yes, provide specifications on barrier materials
Other comments regarding managing impacted soil in utility trenches:Concerns and methods for
environmental handling of soils do not preclude nor modify any of the Occupational Safety and Health
Administration (OSHA) requirements for worker safety incumbent upon contractors for regular site safety
and trenching/excavation activities. OSHA requirements will dictate adjustments of the soil management
methods where necessary.
PART 2. GROUNDWATER – Please fill out the information below and attach figure showing
distribution of groundwater contaminants at site
What is the depth to groundwater at the Brownfields Property?During the 2015 Limited Site
Investigations (LSI), groundwater was encountered at two soil boring locations (B-1 and B-8) at 16 and
21.7 feet bgs, respectively. Groundwater was not encountered at 11 additional soil borings where depths
ranged from 9 to 32 feet bgs. Terracon also performed a preliminary geotechnical engineering
investigation in 2015 and observed groundwater in 4 test borings at depths ranging from 18.5 to 23.5 feet
bgs.
Is groundwater known to be contaminated by ☒ onsite ☐ offsite ☐ both ☒ or unknown sources?
Describe source(s):Two groundwater samples were collected at the site in 2015. Sample B-1 was
obtained near the northwestern corner of the site parcel and Sample B-8 was collected in the east-central
portion of the site. Based on the analytical results, groundwater has been impacted by VOCs and SVOCs.
Tetrachloroethene was detected in groundwater sample B-1 (94.1 µg/L) in the down-gradient portion of
the site at a concentration that exceeds the NCAC 2L Standard. Trichloroethene, cis-1,2-dichloroethene
and toluene were also detected in sample B-1 at concentrations below their respective 2L Standards. No
PAH constituents or other SVOCs were detected in sample B-1. Anthracene (0.54J µg/L) and
benzo(a)fluoranthene (1.0J µg/L) were detected in sample B-8 in an up-gradient portion of the site near
the former Johnston Mill property. Various petroleum constituents and chloroform were also detected
in sample B-8 at concentrations below 2L Standards. A previous assessment of the parcel by H&H in 2007
detected chromium, lead, and selenium above 2L Standards in borings SB-10 (chromium and lead) and
TW-1 (selenium). The source(s) of the detected constituents in the groundwater is unknown at this time
but is likely attributed to historical operations on the site or adjacent properties. Groundwater analytical
data and sampling locations are provided in Appendix B.
What is the direction of groundwater flow at the Brownfields Property?Only limited information on
lateral groundwater flow patterns at the site is available. Based on topography, groundwater flow is
apparently to the west.
Will groundwater likely be encountered during planned redevelopment activities?☐ Yes ☒ No
If yes, describe these activities:Groundwater was measured at the site between 16 and 23.5 feet bgs.
The majority of the redevelopment activities will be completed as slab-on-grade and shallow utility
excavations; thus, construction activities will not encounter groundwater. The southwestern portion of
the proposed building will have a basement but it is currently unknown if the basement excavation will
encounter groundwater.
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Approved EMP, February 12, 2015
In the event that contaminated groundwater is encountered during redevelopment activities (even if
no is checked above), list activities for contingent management of groundwater (e.g., dewatering of
groundwater from excavations or foundations, containerizing, offsite disposal, discharge to sanitary
sewer, or sampling procedures):Excavations in areas where groundwater is encountered should be
allowed to re-infiltrate for approximately 24 hours (if it does not affect the construction schedule) or
remove the groundwater so that construction activities may proceed. The retrieved water will be
containerized so that the water can be sampled for disposal characterization before it is allowed to leave
the site. Based on the types of contaminants documented on the site, water samples will be analyzed for
VOCs and SVOCs. If containerized water is determined to be above regulatory standards, the Brownfields
Project Manager will be contacted and the water will be disposed in accordance with regulatory
requirements.
PART 3. SURFACE WATER – Please fill out the information below.
Attach a map showing the location of surface water at the Brownfields Property.At the present time,
there are no surface water bodies on the site parcel. Redevelopment of the site should include a
stormwater management plan (designed by the civil engineer for the project) to control the accumulation
of stormwater on the construction site. Erosion control methods should be implemented in accordance
with an erosion control plan to prevent stormwater from leaving the site.
Is surface water at the property known to be contaminated:☐ Yes ☒ No
Will workers or the public be in contact with surface water during planned redevelopment activities?
☒ Yes ☐ No Potentially, stormwater can accumulate in excavations and utility trenches during
construction activities following precipitation events.In the event stormwater management is required,
the applicable excavation activities should cease pending removal and characterization of the water.
In the event that contaminated surface water is encountered during redevelopment activities, or clean
surface water enters open excavations, list activities for management of such events (e.g. flooding,
contaminated surface water run-off, stormwater impacts):Excavations and trenches in areas where
potentially impacted soils could be encountered and near parcel boundaries shall be graded, bermed, or
provided with an equivalent barrier where necessary to help prevent stormwater from entering
excavations and stormwater run-off from leaving the site boundaries. Stormwater or water from an
unidentified source that collects in excavation areas will be removed so that construction activities may
proceed. The retrieved water will be containerized or diverted to an on-site stormwater management
basin where the water will be sampled for disposal characterization before it is allowed to leave the site.
Based on the types of contaminants documented on the site, water samples will be analyzed for VOCs,
SVOCs, and metals. If containerized water is determined to be above regulatory standards, the
Brownfields Project Manager will be contacted and the water will be disposed in accordance with
regulatory requirements.
PART 4. SEDIMENT – Please fill out the information below.
Is sediment at the property known to be contaminated:☐ Yes ☒ No
12
Approved EMP, February 12, 2015
Will workers or the public be in contact with sediment during planned redevelopment activities?
☐ Yes ☒ No
If yes, attach a map showing location of known contaminated sediment at the property.
In the event that contaminated sediment is encountered during redevelopment activities, list activities
for management of such events (stream bed disturbance):Not Applicable. There are no known current
or historical natural drainage features on the site.
PART 5. SOIL VAPOR – Please fill out the information below.
Do concentrations of volatile organic compounds at the Brownfields property exceed the following
vapor intrusion screening levels in the following media:
IHSB Residential Screening Levels:
Soil Vapor:☐ Yes ☐ No ☒ Unknown
Groundwater:☒ Yes ☐ No ☐ Unknown
IHSB Industrial/Commercial Screening Levels:
Soil Vapor:☐ Yes ☐ No ☒ Unknown
Groundwater:☒ Yes ☐ No ☐ Unknown
Attach a map (Appendix C) showing the location of soil vapor contaminants exceeding site screening
levels.
If applicable, at what depth(s) is soil vapor known to be contaminated?Soil vapor is not currently known
to be contaminated at the site. No soil vapor samples have been collected at the site. Tetrachloroethylene
was detected in groundwater at the site at levels exceeding regulatory standards indicating the potential
presence of VOC-impacted soil vapor. A soil vapor assessment plan is currently being developed to further
evaluate soil vapor.
Will workers encounter contaminated soil vapor during planned redevelopment activities?
☐ Yes ☐ No ☒ Unknown
In the event that contaminated soil vapor is encountered during redevelopment activities (trenches,
manways, basements or other subsurface work, list activities for management of such contact:Volatile
organic compounds (VOCs), including chlorinated compounds, have been identified in localized areas
within soils and the groundwater beneath the site. Soil Vapor Intrusion Barriers (SVIBs) could be installed
during construction to prevent VOCs or gases from collecting beneath and in the on-site buildings. The
SVIB acts as an engineered barrier that mitigates the potential inhalation exposure pathway. The
anticipated SVIB design and construction specifications have not been prepared at this time. Terracon, if
necessary, will review and provide comments pertaining to the design and specifications prior to
installation of the vapor barrier. Terracon will also monitor the installation and testing of the SVIB to
provide assurance that the system has been installed in accordance with the design and specifications.
13
Approved EMP, February 12, 2015
PART 6. SUB-SLAB SOIL VAPOR -please fill out the information below if existing buildings or
foundations will be retained in the redevelopment.
Are sub-slab soil vapor data available for the Brownfields Property?☐ Yes ☒ No ☐ Unknown
If data indicate that sub-slab soil vapor concentrations exceed screening levels, attach a map (Appendix
C) showing the location of these exceedances.Not applicable. Vapors will be evaluated, as discussed in
Part 5.
At what depth(s) is sub-slab soil vapor known to be contaminated?☐ 0-6 inches ☐ Other, If other
describe:Not applicable.
Will workers encounter contaminated sub-slab soil vapor during planned redevelopment activities?
☐ Yes ☐ No ☒ Unknown
In the event that contaminated soil vapor is encountered during redevelopment activities, list activities
for management of such contact:Volatile organic compounds (VOCs), including chlorinated compounds,
have been identified in localized areas within soils and the groundwater beneath the site. Vapors will be
evaluated, as discussed in Part 5. Soil Vapor Intrusion Barriers (SVIBs) could be installed during
construction to prevent VOCs or gases from collecting beneath and in the on-site buildings. The SVIB acts
as an engineered barrier that mitigates the potential inhalation exposure pathway. The anticipated SVIB
design and construction specifications have not been prepared at this time. The vapor barrier installer
shall conduct the installation of the SVIB in accordance with Occupational Safety and Health
Administration (OSHA) requirements for worker safety incumbent upon contractor’s site safety plan.
PART 7. INDOOR AIR – Please fill out the information below.
Are indoor air data available for the Brownfields Property?☐ Yes ☒ No ☐ Unknown, a vapor
assessment will be conducted, as discussed in Part 5.
If yes, attach a map showing the location where indoor air contaminants exceed site screening levels.
If the structures where indoor air has been documented to exceed risk-based screening levels will not
be demolished as part of redevelopment activities, will workers encounter contaminated indoor air
during planned redevelopment activities?
☐ Yes ☐ No ☒ Unknown
In the event that contaminated indoor air is encountered during redevelopment activities, list activities
for management of such contact:Not Applicable
PART 8. Vapor Mitigation System – Please fill out the information below.
Is a vapor intrusion mitigation system proposed for this Brownfields Property?
☐ Yes ☐ No ☒ Unknown
14
Approved EMP, February 12, 2015
If yes, provide the date the plan was submitted to the Brownfields Program.
Attach the plan.
Has the vapor mitigation plan been approved by the NC Brownfields Program?
☐ Yes ☒ No ☐ Unknown
Has the vapor mitigation plan been signed and sealed by a North Carolina professional engineer?☐
Yes ☒ No The anticipated SVIB design and construction specifications have not been prepared at this
time. Terracon, if necessary, will review and provide comments pertaining to the design and specifications
prior to installation of the vapor barrier. Terracon will also monitor the installation and testing of the SVIB
to provide assurance that the system has been installed in accordance with the design and specifications.
What are the components of the vapor intrusion mitigation system?
☐ Sub-slab depressurization system
☐ Sub-membrane depressurization system
☐ Block-wall depressurization system
☐ Drain tile depressurization system
☐ Passive mitigation methods
☒ Vapor barriers
☐ Perforated piping vented to exterior
☐ Other method:Click here to enter text.
PART 9. CONTINGENCY FOR ENCOUNTERING UNKNOWN TANKS, DRUMS, OR OTHER WASTE
MATERIALS
Please provide a contingency plan in the event unknown tanks, drums, fuel lines, landfills, or other
waste materials are encountered during site activities.
There is a possibility that materials of unknown type (tanks, drums or impacted soils) could be present on
the site. The worker and contractor must be able to recognize when conditions change at the site. Field
staff must be able to identify if a new discovery of changed chemical conditions has occurred, and if so, if
it is significant. If there is question of the significance of a new discovery or changed condition, the
environmental manager (Chris Corbitt) or equivalent qualified environmental professional should make
the determination. The worker or contractor should be alert during earthwork for the following
indications that will trigger the possible identification of a new condition not addressed by previous
investigations and evaluation.
1)During soil disturbance, the worker or contractor should observe soils for unique color changes
that are unlike surrounding soils. The soils identified during previous environmental
investigations were reportedly varied in color and composition, ranging from red to yellow/tan to
grey. When observing soils, some may be more saturated than others depending on recent
rainfall and the depth of soil disturbance (near the water table). Moist soils tend to appear darker.
The worker or contractor should closely observe dark, moist soils for evidence of saturation by
fluids other than water. Although no free phase petroleum products or other chemicals were
noted in prior site investigation reports, oddly colored soils or soils saturated by apparent
petroleum products or other chemicals are indicative of a changed condition.
15
Approved EMP, February 12, 2015
2)Secondly, soils impacted by petroleum constituents or chlorinated compounds as noted during
prior site investigations could produce chemical or solvent odors associated with on-site impacts.
Soils may often have a “musty” or “rotting” odor if found mixed with vegetation or dark organic
soils. Strong fuel, solvent or chemical odors in soils are indicative of a changed condition.
3) Prior assessment reports did not identify any current underground storage tanks (USTs) but given
the site history, the presence of USTs is a possibility. One UST used to store heating oil was
reportedly removed in the 1970s or 1980s. Although we do not anticipate encountering drums,
underground storage tanks, or other debris, the worker and contractor should be cognizant of
man-made containers or remnants of containers of any material. The presence of whole or
crushed drums or containers in excess of one gallon in the soils in combination with odor or
unique color changes may be indicative of a changed condition.
If a changed condition is noted at the site, the suspect soils should be isolated as soon as possible from
contact and disturbance by rain and wind until screening identification can be made. Construction
flagging tape attached to stakes can be used to prevent accidental movement of the soils by earthwork
operations. Cover the soils with plastic sheeting and weight the covering with planks, sandbags, or
equivalent. The soils should be screened for volatile and semi-volatile organic compounds. The screening
will be provided by the on-site environmental manager or other qualified environmental professional.
The owner or contractor may alternatively go directly to laboratory testing for identification purposes.
Screening tests can be conducted on the site and can produce preliminary results quickly. The field test
does not produce a precise measurement of the amount of contaminant found in the soils, but indicates
that contaminants are likely present and warrants further caution and actual measurement. If preliminary
screening activities indicate a changed condition may be present, it may be necessary to conduct
laboratory testing to determine if contaminants present in the soil actually pose a significant risk.
Laboratory testing requires time that varies depending on the type of test needed. In general, laboratory
testing for chlorinated compounds and petroleum hydrocarbons can take on the order of 5 to 7 business
days unless special arrangements are made with the laboratory for more expensive “RUSH” results.
During this time, the impacted soils should be further isolated from worker and public exposure. Special
handling and care must be taken in sampling and transporting soils for the laboratory tests to be accurate.
The workers in physical contact with suspect impacted soil should have training consistent with 29 OSHA
1910.120.
For small volumes, the soil can be placed temporarily in steel open-top drums with bolt-on lids. After
sealing, the drum should be clearly labeled with pertinent information such as “Do Not Disturb”, sample
number, date, and name of sampler. The drums should be placed in an on-site area protected from
general traffic. For larger volumes, it can be effective to place the soils into commercial roll-off dumpsters
which have been previously washed and cleaned of residues or soils can be stockpiled on plastic sheeting.
The containers will not have free-draining bottoms and stockpiles shall be graded, bermed, or provided
with an equivalent barrier where necessary to help prevent water run-off. The tops of the containers or
stockpiles will then be covered with plastic sheeting and secured against wind and rain. The commercial
containers or stockpiles should be placarded with information similar to the notation on drums.
Check the following activities that will be conducted prior to commencing earth-moving activities at
the site:
☒ Review of historic maps (Sanborn Maps, facility maps)
0 Conduct geophysical surveys to evaluate the location of suspect UST, fuel lines, utility lines, etc.
D Interviews with employees/former employees/facility managers/neighbors
Notification to State Brownfields Project Manager, UST Section, Fire Department, and/or other officials,
as necessary and appropriate, is required when new potential source(s) of contamination are
discovered. See Notification Section on Page 1 for notification requirements.
POST-REDEVELOPMENT REPORTING
In accordance with the site's Brownfield Agreement, provide a report within the designated schedule
to the State Brownfields Project Manager.
181 Check box to acknowledge consent to provide a redevelopment summary report in compliance with
the site's Brownfields Agreement.
APPROVAL SIGNATURES
Prospective Developer Date
Benjamin l. Collins, Vice President of Crescent Communities, LLC, the Manager of Crescent MF
EMC JV Member, LLC, the Manager of EMC Crescent MF Venture LLC, the Sole Member and Manager
of Crescent NoDa, LLC.
Consultant Date
Christopher L. Corbitt, Senior Project Manager, Terracon Consultants, Inc.
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Approved EMP, February 12, 2015
I
Appendix A:
Redevelopment and Grading Plans
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PH. [phone] terracon.com
2020 STARITA RD, SUITE E CHARLOTTE, NC
FIGURE
X
CUT AND FILL DIAGRAM AND HISTORICAL SAMPLE LOCATIONS
NODA TEXTILE BROWNFIELDS SITE430 EAST 36TH STREETCHARLOTTE, NC
71157713A
CZ
CLC
01/25/2016
Project No.:
Drawn By:
Checked By:
Date: N:\Projects\2015\71157713A\Figures\MXD\EMP_Grading_and_Hist_Samples.mxd³
0 100 20050Feet1 inch = 70 feet
Legend
SiteParcel
Parcel Boundaries
!(Soil Sample Location
#0 Groundwater Sample Location
Existing Buildings
Proposed Building Footprint
Proposed Subgrade Parking Area
Proposed Slab on Grade Area (Retail/Residential)
Proposed Basement Area (Retail/Residential)
Proposed Pavement
Notes:- C = Cut- F = Fill- Sample locations are approximate and based on historical reports.- Locations of building footprints, site features, and cut and fill diagram are approximate.- Parcel data obtained from Mecklenbrug County GIS website.- Construction details provided by Crescent Communities.- Cut and Fill Diagram provided by Summit Contracting Group, Inc.
APARTMENTCOMPLEX
APARTMENTCOMPLEX
FORMER REFINERY
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1130+00PHASE 1PHASE 2T
TTPHASE 1PHASE 2PHASE 1PHASE 21.2%717.48708.00START CURB717.48717.12717.48BP717.10RIM 716.70BP 717.10RIM 716.70BP 717.00714.50RIM 715.90717.48717.48FFE 717.50BP716.20RIM 714.60BP 716.203.00%RIM 715.90717.48717.40717.48717.48RIM715.90RIM 706.30706.38COURTYARD A(SEE COURTYARDLAYOUT PLAN THIS SET)COURTYARD B(SEE COURTYARDLAYOUT PLAN THIS SET)35TH STREET36TH STREETLYNX BLUE LINE EXTENSION - 36TH STREET STATIONPARKING STRUCTUREEXISTING RAILROADEXISTING RAILROADREMNANT PIECE OFRAILROAD TRACK5.0%714.50716.50716.00716.40BP 716.201.5%716.80717.30714.00717.00718.002% MAX717.122% MAX2% MAX716.40717.12717.12716.70717.12716.402% MAX2.30%716.402.60%717.12717.12717.20717.40716.70717.12716.702% MAX717.48717.20717.40717.40717.40717.48717.30717.30717.302%MAX3%717.283%
1%1%1%2%MAX717.28717.303.3%716.50716.50RIM 716.302%MAX716.50RIM 716.30TW 716.50712711710710TW 715.17TW 713.84TW 712.50SWALE706.38706.15706.38706.38RIM 704.98BC 705.25RIM 705.50TC 706.00BC 705.803.9%RAILROAD R/WPROPERTYBOUNDARYFUTURE LIGHT RAILSTATION STAIRTHE YARDSAT NODAPROPERTYBOUNDARYFUTURE RAILROADTRACK CENTERLINERIM 706.00717.48RIM 717.39717.25717.46RIM 717.392% MAX2% MAXLEGEND:717.26SPOT ELEVATIONHARDSCAPE DRAINGRATE ELEVATIONTOP OF WALLTWBOTTOM OF WALLBWBREAK POINTBPSLOPELANDSCAPE DRAINHARDSCAPE DRAINTOP OF STAIRTSBOTTOM OF STAIRBS1%RIM717.26PRELIMINARYNOT FOR CONSTRUCTIONCHARLOTTE, NC 28205
CRESCENT NoDa10/01/201510550-00CRESCENT COMMUNITIES
SHEET TITLE
SCALE (U.N.O.)
JOB NAME
LOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABC DEFGHJK123456789101112131415‹/RUG$HFN6DUJHQWLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck Sargent1. PRICING - 10.01.150'15'15'30'60'OVERALL GRADING PLANC5.01" = 30'
PRELIMINARYNOT FOR CONSTRUCTIONCHARLOTTE, NC 28205
CRESCENT NoDa10/01/201510550-00CRESCENT COMMUNITIES
SHEET TITLE
SCALE (U.N.O.)
JOB NAME
LOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABC DEFGHJK123456789101112131415‹/RUG$HFN6DUJHQWLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck Sargent1. PRICING - 10.01.15GRADING NOTES:1.) REFER TO LAYOUT PLAN FOR RELATED NOTES.2.) ALL CONTOURS AND SPOT ELEVATIONS REFLECT FINISHED GRADE.3.) ALL FILL TO BE COMPACTED TO 98% A.A.S.H.O. STANDARD COMPACTION UNLESS OTHERWISE NOTED.4.) THE PROPOSED CONTOURS SHOWN IN DRIVES, PARKING LOTS AND SIDEWALKS ARE FINISHED ELEVATIONSINCLUDING ASPHALT. REFER TO PAVEMENT CROSS-SECTION DATA TO ESTABLISH CORRECT SUB-BASE OR AGGREGATEBASE COURSE ELEVATIONS.5.) LIMITS OF CLEARING SHOWN ON EROSION CONTROL PLANS ARE BASED ON CUT AND FILL SLOPES OR OTHERGRADING REQUIREMENTS.6.) ANY GRADING BEYOND THE LIMITS OF CONSTRUCTION SHOWN ON THE EROSION CONTROL PLAN IS SUBJECT TO AFINE.7.) STABILIZATION IS THE BEST FORM OF EROSION CONTROL. TEMPORARY SEEDING IS NECESSARY TO ACHIEVEEROSION CONTROL ON DENUDED AREAS AND ESPECIALLY WHEN THE CONSTRUCTION SEQUENCE REQUIRES IT. ALLGRADED SLOPES ARE TO BE SEEDED OR LANDSCAPED: WITHIN 7 CALENDAR DAYS FROM THE LAST LAND-DISTRUBINGACTIVITY FOR ALL PERIMETER DIKES, SWALES, PERIMETER SLOPES, AND ALL SLOPES STEEPER THAN 3 HORIZONTAL TO 1VERTICAL (3:1); AND AS SOON AS PRACTICABLE BUT IN ANY EVENT WITHIN 14 CALENDAR DAYS FROM LASTLAND-DISTURBING ACTIVITY FOR ALL OTHER DISTURBED AREAS.8.) CONTRACTOR SHALL INSTALL EROSION CONTROL MEASURES AS INDICATED ON EROSION CONTROL PLANS. NOEROSION CONTROL DEVICE MEASURE MAY BE REMOVED UNTIL THE SITE IS STABILIZED.9.) ON-SITE BURIAL PITS REQUIRE AN ON-SITE DEMOLITION LANDFILL PERMIT FROM THE ZONING ADMINISTRATOR.10.) SLOPES SHALL BE GRADED NO STEEPER THAN 2:1. FILL SLOPES GREATER THAN 10' REQUIRE ADEQUATETERRACING (CLDSM #30.16).11.) THE CITY ENGINEERING DEPARTMENT SHALL BE NOTIFIED 24 HOURS IN ADVANCE OF THE COMMENCEMENT OFCONSTRUCTION ACTIVITY.12.) NON-STANDARD ITEMS (IE: PAVERS, IRRIGATION SYSTEMS, ETC.) IN THE RIGHT-OF-WAY REQUIRE A RIGHT-OF-WAYENCROACHMENT AGREEMENT WITH THE CHARLOTTE DEPARTMENT OF TRANSPORTATION/NORTH CAROLINADEPARTMENT OF TRANSPORTATION BEFORE INSTALLATION.13.) PRIOR TO PLAT RECORDATION, OFFSITE R/W AND/OR CONSTRUCTION EASEMENTS ARE REQUIRED TO BE OBTAINEDACCORDING TO THE GUIDELINES OF THE "OFFSITE R/W ACQUISITION PROCESS". THESE NEEDED R/W ANDCONSTRUCTION LIMITS ARE CLEARLY SHOWN ON THE ROADWAY IMPROVEMENT PLAN.14.) THE DEVELOPER SHALL CONTACT THE CHARLOTTE DEPARTMENT OF TRANSPORTATION TO IDENTIFY ANYCONFLICTS WITH TRAFFIC SIGNALIZATION EQUIPMENT. 60-90 DAYS WILL BE REQUIRED TO COORDINATE RELOCATION.DEVELOPER SHALL BE RESPONSIBLE FOR ALL RELATED RELOCATION COST AND/OR ANY REPAIR COST CAUSED BY THECONTRACTOR/DEVELOPER.15.) IN ORDER TO ENSURE PROPER DRAINAGE, MAINTAIN MINIMUM 0.5% SLOPE ON ALL CURB.16.) STORM DRAIN PIPE TO FOLLOW THE APPROVED CITY OF CHARLOTTE STANDARDS AND SPECIFICATIONS. RCPSTORM DRAINAGE PIPE INSTALLED WITHIN EXISTING OR PROPOSED PUBLIC RIGHT-OF-WAY MUST BE APPROVED BY THECITY'S INSPECTOR PRIOR TO ANY BACKFILL BEING PLACED. BACKFILL MATERIAL MUST BE APPROVED BY THE CITYINSPECTOR PRIOR TO PLACEMENT OF THE MATERIAL WITHIN THE PUBLIC RIGHT-OF-WAY. THE CITY INSPECTOR MUSTBE PRESENT DURING THE BACKFILLING OPERATION AS WELL.A) BACKFILL MATERIAL USED TO INSTALL RCP PIPE WITHIN THE STREET RIGHT-OF-WAY SHALL BE SELECT MATERIAL,CLASS II-IV, AS DEFINED BY SECTION 1016-3 OF THE NCDOT STANDARD SPECIFICATIONS FOR ROADS AND STRUCTURES.UPON SUBMITTAL OF WRITTEN CERTIFICATION OF MATERIAL SUITABILITY BY A LICENSED GEOTECHNICAL ENGINEER,NCDOT CLASS I SELECT MATERIAL MAY BE USED. ALL BACKFILL MATERIAL SHALL BE APPROVED BY THE CITYINSPECTOR PRIOR TO PLACEMENT OF THE MATERIAL WITHIN THE STREET RIGHT-OF-WAY.17.) GRADING CONTRACTORS SHALL NOTIFY AND COOPERATE WITH ALL UTILITY COMPANIES OR FIRMS HAVINGFACILITIES ON OR ADJACENT TO THE SITE BEFORE DISTURBING, ALTERING, REMOVING, RELOCATING, ADJUSTING ORCONNECTING TO SAID FACILITIES. CONTRACTORS SHALL PAY ALL COSTS IN CONNECTION WITH THE ALTERATION OF ORRELOCATION OF THE FACILITIES. CONTRACTORS SHALL RAISE OR LOWER TOPS OF EXISTING MANHOLES AS REQUIREDTO MATCH FINISHED GRADES.18.) GRADING CONTRACTOR SHALL COOPERATE AND WORK WITH ALL OTHER CONTRACTORS PERFORMING WORK ONTHIS PROJECT TO INSURE PROPER AND TIMELY COMPLETION OF THIS PROJECT.19.) THE GRADING CONTRACTOR SHALL USE WHATEVER MEASURES ARE REQUIRED TO PREVENT SILT ANDCONSTRUCTION DEBRIS FROM FLOWING ONTO ADJACENT PROPERTIES. CONTRACTOR SHALL COMPLY WITH ALL LOCAL,STATE, AND FEDERAL EROSION SEDIMENT AND SILTATION ORDINANCES. CONTRACTOR SHALL REMOVE ALLTEMPORARY EROSION CONTROL STRUCTURES UPON COMPLETION OF PERMANENT DRAINAGE FACILITIES AND NOTBEFORE ALL AREAS DRAINING INTO THESE STRUCTURES ARE SUFFICIENTLY STABILIZED.20.) FOR ANY WORK ON THE STATE OR CITY RIGHT-OF-WAY, THE GRADING CONTRACTOR SHALL: A) NOT STOREMATERIAL, EXCESS DIRT OR EQUIPMENT IN THE RIGHT-OF-WAY IN CASE OF MULTILANE HIGHWAYS. THE PAVEMENTSHALL BE KEPT FREE FROM ANY MUD OR EXCAVATION WASTE FROM TRUCKS OR OTHER EQUIPMENT. ON COMPLETIONOF THE WORK ALL EXCESS MATERIAL SHALL BE REMOVED FROM THE RIGHT-OF-WAY; B) PROVIDE ALL NECESSARY ANDADEQUATE SAFETY PRECAUTIONS SUCH AS SIGNS, FLAGS, LIGHT BARRICADES AND FLAGMEN AS REQUIRED BY THELOCAL AUTHORITIES AND IN ACCORDANCE WITH THE MANUAL ON UNIFORM TRAFFIC CONTROL DEVICES. THE GRADINGCONTRACTOR SHALL BE SOLELY RESPONSIBLE FOR AND HOLD HARMLESS THE CITY OF CHARLOTTE, THE STATE OFNORTH CAROLINA, THE ARCHITECT/ENGINEER, AND THE OWNER FROM ANY CLAIMS FOR DAMAGE DONE TO EXISTINGPRIVATE PROPERTY, PUBLIC UTILITIES, OR TO THE TRAVELING PUBLIC; C) COMPLETE WORK TO THE SATISFACTION OFTHE CHARLOTTE MECKLENBURG UTILITIES DEPARTMENT (CMUD) AND OBTAIN A LETTER FROM THE DEPARTMENTSTATING THAT THE WORK IS ACCEPTABLE.21.) GRADING CONTRACTOR SHALL TAKE ALL AVAILABLE PRECAUTIONS TO CONTROL DUST. CONTRACTOR SHALLCONTROL DUST BY SPRINKLING, OR BY OTHER METHODS AS DIRECTED BY ENGINEER AND/OR OWNER'SREPRESENTATIVE AT NO ADDITIONAL COST TO OWNER.22.) GRADING CONTRACTOR TO COMPLY WITH ALL STATE AND LOCAL SEDIMENT CONTROL AND AIR POLLUTIONORDINANCES OR RULES.23.) BEFORE ANY MACHINE WORK IS DONE, CONTRACTOR SHALL STAKE OUT AND MARK THE ITEMS ESTABLISHED BYTHE SITE PLAN. CONTROL POINTS SHALL BE PRESERVED AT ALL TIMES DURING THE COURSE OF THE PROJECT. LACKOF PROPER WORKING POINTS AND GRADE STAKES MAY REQUIRE CESSATION OF OPERATIONS UNTIL SUCH POINTS ANDGRADES HAVE BEEN PLACED TO THE OWNER'S SATISFACTION.24.) "AS-BUILT" DRAWINGS AND PLANS OF THE STORM DRAINAGE SYSTEM, MUST BE SUBMITTED PRIOR TO FINALINSPECTION TO THE CITY/COUNTY ENGINEERING DEPARTMENT IN ACCORDANCE WITH THE CITY/COUNTY SUBDIVISIONORDINANCE.25.) CONTRACTOR SHALL REPAIR OR REPLACE IN-KIND ANY DAMAGE THAT OCCURS AS RESULT OF HIS WORK.26.) APPROVAL OF THIS PLAN IS NOT AN AUTHORIZATION TO GRADE ADJACENT PROPERTIES. WHEN FIELD CONDITIONSWARRANT OFF-SITE GRADING, PERMISSION MUST BE OBTAINED FROM THE AFFECTED PROPERTY OWNERS.27.) THE PURPOSE OF THE STORM DRAINAGE EASEMENT (SDE) IS TO PROVIDE STORM WATER CONVEYANCE. BUILDINGSARE NOT PERMITTED IN THE EASEMENT AREA. ANY OTHER OBJECTS WHICH IMPEDE STORM WATER FLOW OR SYSTEMMAINTENANCE ARE ALSO PROHIBITED.28.) PE SEALED SHOP DRAWINGS FOR RETAINING WALL MUST BE SUBMITTED TO CITY ENGINEER PRIOR TOCONSTRUCTION.29.) PRIOR TO INSTALLATION, PE SEALED SHOP DRAWINGS FOR UNDERGROUND DETENTION SYSTEMS MUST BEFURNISHED TO CITY OF CHARLOTTE ENGINEERING FOR APPROVAL.30.) CERTIFICATION AND STREET CUT PERMITS ARE REQUIRED FOR UTILITY CUTS ON CITY STREETS. ALLOW 7 DAYSPROCESSING FOR PERMIT. FOR INFORMATION CONTACT CHARLOTTE DEPARTMENT OF TRANSPORTATION (704-336-4025)OR VISIT HTTP://WWW.CHARMECK.ORG/DEPARTMENTS/TRANSPORTATION/STREET+MAINTENANCE/HOME.HTMLSITE ACCESSIBILITY NOTES1. ALL BUILDINGS WITHIN THE BOUNDARY OF THlS SITE, UNLESS OTHERWISESTATED AS EXEMPT, SHALL HAVE "ACCESSIBLE ROUTES" AS REQUIRED THATCONFORM TO THE REQUIREMENTS OF "THE AMERICANS WITH DISABILITIESACT", FAIR HOUSING STANDARDS, ICC ANSI A 117.1-209 AND GOVERNING STATEHANDICAP CODE STANDARDS.- THESE STANDARDS FOR ACCESSIBILITY INCLUDE, BUT ARE NOT LIMITEDTO:MAXIMUM WALK SLOPE - 5%MAXIMUM RAMP SLOPE - 8.33% WITH RAILINGMAXIMUM CROSS SLOPE - 2%2. ALL WALKS TO BE BROOM FINISHED CONCRETE UNLESS OTHERWISESPECIFIED ON THESE DRAWINGSMAXIMUM ACCESSIBLE ROUTE LENGTH (NC) - 200'3. THE PAVEMENT SLOPE WITHIN ACCESSIBLE PARKING SPACES SHALL NOTEXCEED 2% IN ALL DIRECTIONS.4. CONTRACTOR TO CONTACT THE APPROPRIATE AUTHORITY FOR ANYVARYING SITE CONDITIONS OR DISCREPANCIES AFFECTING SITE ACCESSIBILITYREQUIREMENTS.ADDITIONAL ACCESSIBLE ROUTE NOTES FOR ACCESSIBILITY COMPLIANCE WITHICC/ANSI A117.1-2009, AND 2010 ADA STANDARDS.1. PROTRUDING OBJECTS ON CIRCULATION PATHS WITHIN COMMON USEAREAS TO COMPLY WITH ANSI 2009 SECTION 307, INCLUDING:A.) PROTRUSION LIMITS: OBJECTS WITH LEADING EDGES MORE THAN 27"AND NOT MORE THAN 80" ABOVE THE FLOOR MAY PROTRUDE 4"MAXIMUM HORIZONTALLY INTO THE CIRCULATION PATH. EXCEPTIONSINCLUDE HANDRAILS, DOOR CLOSER, AND DOOR STOPS.B.) POST MOUNTED OBJECTS: OBJECTS ON POSTS OR PYLONS SHALL BEPERMITTED TO OVERHANG 4" MAXIMUM WHERE MORE THAN 27" AND NOTMORE THAN 80" ABOVE THE FLOOR. OBJECTS ON MULTIPLE POSTS ORPYLONS WHERE THE CLEAR DISTANCE BETWEEN THE POSTS OR PYLONSIS GREATER THAN 42" SHALL HAVE THE LOWEST EDGE OF SUCH OBJECTEITHER 27" MAXIMUM OR 80" MINIMUM ABOVE THE FLOOR.C.) REDUCED VERTICAL CLEARANCE: GUARDRAILS OR OTHER BARRIERSSHALL BE PROVIDED WHERE OBJECT PROTRUSION IS BEYOND THELIMITS ALLOWED BY SECTIONS 307.2 AND 307.3, AND WHERE THEVERTICAL CLEARANCE IS LESS THAN 80" ABOVE THE FLOOR. THELEADING EDGE OF SUCH GUARDRAIL OR BARRIER SHALL BE 27"MAXIMUM ABOVE THE FLOOR.2. PROTRUDING OBJECTS ON CIRCULATIONS PATHS WITHIN PUBLIC USE AREASTO COMPLY WITHIN 2010 ADA CODE, SECTION 307, INCLUDING:A.) 2010 ADA SECTION 307.2: OBJECTS PROJECTING FROM WALLSB.) 2010 ADA SECTION 307.4: MINIMUM CLEAR HEADROOM3. FLOOR AND GROUND SURFACES IN COMMON USE AREAS SHALL BE STABLE,FIRM AND SLIP-RESISTANT AND SHALL COMPLY WITHIN ANSI 2009 SECTIONS3O2.4. FLOOR AND GROUND SURFACES ALONG ACCESSIBLE ROUTES AND INACCESSIBLE ROOMS AND SPACES WITHIN PUBLIC USE AREAS SHALL BE STABLE,FIRM, AND SLIP-RESISTANT AND SHALL COMPLY WITH 2010 ADA SECTION 302.5. CHANGES IN LEVEL IN COMMON USE AREAS SHALL COMPLY WITH ANSI 2009.6. CHANGES IN LEVEL ALONG ACCESSIBLE ROUTES AND IN ACCESSIBLE ROOMSAND SPACES WITH PUBLIC USE AREAS SHALL COMPLY WITHIN 2010 ADASECTION 303.7. IF TREES OR OTHER PLANTINGS OVERHANG ALONG THE CIRCULATIONROUTES AT THE SIDEWALK WITHOUT PROTECTION AT 27" A.F.F. OR LOWER,ASSURE THEY DO NOT EXTEND GREATER THAN 4" INTO THE CIRCULATIONROUTE AT A HEIGHT OF 80" ABOVE GRADE OR LOWER (1986 ANSI, SECTION4.4.1).8. THE CONTROLS AT ANY ADDITIONAL COMMON USE ELEMENTS SUCH AS GATEHARDWARE, FIRE PIT, POOL SHOWER, ETC. WHICH ARE INTENDED TO BE USEDBY THE RESIDENTS AND THEIR GUESTS ARE LOCATED ON AN ACCESSIBLEROUTE, WITHIN THE REQUIRED REACH RANGE OF 15"-48" A.F.F. AND AREOPERABLE WITHIN ONE HAND USING 5LB MAXIMUM PRESSURE WITHOUT TIGHTGRASPING, PINCHING, OR TWISTING OF THE WRIST (1986 ANSI, SECTION 4.25AND ANSI 2009, SECTION 308).ADA DOOR and/or GATE POINTS OF ACCESSPLANSCALE: 1/2" = 1'-0"5'-0"5'-0"2% MAX SLOPE2% MAX SLOPE ADJACENT PAVINGAREA, REFER TOPAVING PLANADJACENT PAVINGOR LANDSCAPEAREA, REFER TOPAVING PLANFACE OFBUILDINGOR FENCEDOOR OR GATE1'-6"REQUIRED CLEARANCEON PULL SIDEOR LATCH SIDE OF DOOR OR GATEGRADING NOTES
C5.1AS SHOWN
N26°51'10"W 403.33'T
T
TUP
UP
MECH
088
ELEC
082
MECH
087
ELEC
081
ELEC
080
MECH
086
STAIR 04
094
CORR.
073
CORR.
072
STAIR 02
092
G1
A261
C1
A261
C1
A261
G1
A262
G1
A262
STORAGE 1
001
STORAGE 2
002
STORAGE 3
003
STORAGE 4
004
STORAGE 5
005
FACILITIES/STORAGE
074
SEE PARKING DECK PLAN
SHEET AP100
STAIR 05
095
A121
B1
STAIR 03
093
A313
A12
A314
A11
A316
A12
A3
A4
A5
A6 A7
T2
066
T3
065
T3
064
B1
059
B1
057
B2
054
A1
056
B1
058
A1
060
A1
052
A2
055
A2
053
A2
051
B2
048 A5
046
A5
044
A3
049
A1
050
TRASH/REC
076
A341
A12
B2
036
S1
038
A1
040
B2
042
MECH
085
MECH
089
DOG WASH
007
WORKSHOP
006
A1
A262
A1
A262
A122
A9
19
A217
E9
A217
H3
A217
F3
ELEVATOR
LOBBY
098
A217
A6
AB
C D SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:53:46 PMCHARLOTTE, NC 28205BASEMENT LEVEL FLOOR PLANCRESCENT NoDa10/01/2015
10550-00
A100CRESCENT COMMUNITIESA. DO NOT SCALE DRAWINGS, DIMENSIONS GOVERN.
B. ALL PARTITIONS ARE DIMENSIONED TO FACE OF
CONCRETE OR CENTERLINE OF OPENING UNLESS
NOTED OTHERWISE. ALL DIMENSIONS SHOWN ON
THE DRAWINGS ARE TO BE CONSIDERED CRITICAL.
IT SHALL BE THE RESPONSIBILITY OF THE
CONTRACTOR TO INFORM THE ARCHITECT OF ANY
DEVIATION IN THE PLACEMENT OF WORK PRIOR TO
INSTALLATION.
C. BUILDING DIMENSIONS ARE TYPICAL FOR ALL
LEVELS UNLESS NOTED OTHERWISE.
D. DOUBLE STUD CONSTRUCTION TO BE USED AT ALL
DOOR OPENINGS.
E. ALL FLOOR AND WALL PENETRATIONS IN RATED
ASSEMBLIES SHALL BE SEALED WITH APPROVED,
CURRENT, FIRESTOP ASSEMBLIES APPROPRIATE
FOR THE RATED WALL ASSEMBLY.
F. FURNISH CLASS A, B, C FIRE EXTINGUISHERS ON
BRACKETS AS INDICATED ON THE DRAWINGS
G. SLOPE ALL CONCRETE PARKING AREAS TO DRAIN.
H. PROVIDE SPECIFIED CLEAR SEALER AT ALL
EXPOSED CONCRETE.
I. GROUT ALL CMU PARTITIONS TO THE TOP OF
STRUCTURE.
J. GROUT ALL HOLLOW METAL FRAMES IN CONCRETE
PARTITIONS.
K. DOORS IN PARKING STRUCTURES TO BE PT-0.
REFER TO FINISH SCHEDULE.
L. PROVIDE MAXIMUM ¾” THRESHOLDS AT EXTERIOR
DOORS. WARP SLABS AS REQUIRED, TYP.
M. PROVIDE 114” CLEARANCE AT VAN ACCESSIBLE
PARKING SPACES WITH CLEAR PATH OF TRAVEL TO
DECK ENTRANCE. PROVIDE 98” CLEARANCE AT
ACCESSIBLE PARKING SPACES. COORDINATE
LIGHTING AND FIRE PROTECTION SYSTEMS IN
PARKING STRUCTURE TO MAINTAIN REQUIRED
HEIGHT CLEARANCES.
N. ALL UNIT DEMISING WALLS SHALL BE TYPE P-20
UNLESS NOTED OTHERWISE.
O. ALL CORRIDOR WALLS SHALL BE TYPE P-10 WITH
FIRE RETARDANT TREATED WOOD UNLESS NOTED
OTHERWISE. USE TYPE P-19 WHERE LOAD BEARING
– SEE STRUCTURAL.
P. FURNISH FIRE EXTINGUISHERS IN FULLY RECESSED
CABINETS IN ALL COMMON AREAS AND
CORRIDORS.
Q. PROVIDE GYP. BOARD CONTROL JOINTS @ 30’-0” ON
CENTER MAXIMUM OR AS INDICATED ON INTERIOR
ELEVATIONS.
R. REFER TO LIFE SAFETY DRAWINGS FOR FIRE
RATED PARTITION LOCATIONS AND INFORMATION.
S. ALL WOOD FRAMING AND BLOCKING BELOW THE
PODIUM TO BE FIRE RETARDANT TREATED.
T. SEE A201-A203 FOR BUILDING ELEVATIONS AND
A211 & A212 FOR SECTIONS.2040FT01 50% PRICING 10.1.15
2 City Comments 10.9.15
3 PRICING ADD. 1 10.9.15
3
N26°51'10"W 403.33'S U
A A S HT O 2 0 0 1 (U S)
T
T
T
TUP
UP
UP
UP
D WR EF
A202
G1
A201
B1
11
12
13
14
15
16
17
S
R
Q
3
2
1
A.4 B.4
A B C D
P
4
E
6
7
8
9
10
A215
A8
A2
F8
A216 F9
F3
A9
A3
F3
RETAIL AREA 1
2481 S.F.
RETAIL AREA 2
1193 S.F.
RETAIL AREA 3
1019 S.F.
RETAIL AREA 4
1179 S.F.
A1
5
MECH
187
ELEC
181 MECH
189
STOR.
174
ELEC
180
MECH
186
MECH
185
CORR.
172
STAIR 01
191
STAIR 02
192
STAIR 04
194
ELEC
179
ELECTRICAL
112
BOOSTER PUMP
111
FIRE PUMP
110
G1
A261
C1
A261
C1
A261
G1
A262
G1
A262
GREASE
SHAFT
ABOVE
105.64°
FITNESS CENTER
104
SEE PARKING DECK PLAN
SHEET AP101
CENTRAL TRASH
175
RETAIL CORR.
103.1
NOTE 1
STAIR 03
193
A312
A12
A313
A9
A314
A8
A315
A8
A316
D9
A2
A3
A4
A5
A6 A7
A217
A9
A340
A10
T2 Mezzanine
066T3 Mezzanine
065
T3 Mezzanine
064
B1
159
B1
157
B2
154
A1
156
B1
158
A1
160
B2
136
A5c ADA
138
S1
124
B2
142
A5
144
A5
146
B2
148
A1
150
A2
155
A2
153
A2
151
A3
149
A1
147
B1
145
B1
143
A1
141
A3
139
B2c ADA
120
S1
137
A1
135 B1
133
B1
131
S1
118
S1
116
B1
114
B2
126
S1
128
S1
130
S1
132
S1
134
A1
152
MAIL & RAIL
101
LEASING
100
ELEC/DATA
177
LOADING
113
18
CLUB ROOM
102
MECH
184
STAIR 05
195
TRASH/REC
176
A317
A12
A341
F12
A1
140
A1
122
MECH
183
RETAIL AREA 5
1744 S.F.
A1
A262
A1
A262
POOL EQUIP.
109
18" MIN.18" MIN.1 8 " M IN .
WOMENS
108
MENS
106
MANAGER
100.5
WORK ROOM
100.2
R.R.
100.1
PACKAGES
100.3
BREAK
100.4
CORR.
171.1
JAN.
108.1
CORR.
171
19
A217
E9
A217
H3
A217
F3
ELEVATOR
LOBBY
199
ELEVATOR
LOBBY
198
A217
A6
A6313
A317
A6
A217 A1
GROUP FITNESS
104.1
A608H5
AB
C D SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:53:54 PMCHARLOTTE, NC 28205LEVEL 1 FLOOR PLANCRESCENT NoDa10/01/2015
10550-00
A101CRESCENT COMMUNITIES1. PROVIDE TWO (2) HOUR RATING AT UNDERSIDE OF
ENTRANCE DRIVE BRIDGE.
2. JANITOR CLOSET MOP SINK: FIAT MSB-2424
A SEE GENERAL NOTES A100 TYP.
B ALL STAIRS TO BE METAL PAN STAIRS.
C CONTRACTOR SHALL MAKE WRITTEN REQUEST TO
OWNER FOR ANY AND ALL CONSTRUCTION
EASEMENTS THAT THE CONSTRACTOR DEEMS
NECESSARY PRIOR TO BEGINNING WORK
D TWO HOUR SHAFT AROUND TRASH CHUTE
E ALL UNIT DEMISING WALLS SHALL BE 1WD56G UNLESS
NOTED OTHERWISE.
F ALL CORRIDOR WALLS SHALL BE 1WD456 UNLESS
NOTED OTHERWISE.
G SLOPE ALL BALCONIES AT 2% FROM BUILDING
H PROVIDE TRAFFIC COATING AT ALL RESIDENTIAL
BALCONIES
I SEE ENLARGED PLANS FOR ADDITIONAL WALL TYPES
2040FT01 50% PRICING 10.1.15
2 PRICING ADD. 1 10.9.15
2
2
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
FP07
67' - 0"
ROOF
(+798')
78' - 2"
321 4 6 7 8 9 10
5
G1
A261
G1
A261
C1
A261
C1
A261
LAPSIDING TYPE- 1
6" EXPOSURE
ALUMINUM STORE
FRONT
CORRUGATED MTL -
TYPE 2
CORRUGATED MTL -
TYPE 1
CONCRETE/ METAL
CANOPY
PANEL AND CHANNEL
ALUMINUM
STOREFRONT
CORRUGATED
MTL. TYPE 1
LAPSIDING
TYPE 2
8" REVEAL
SIGNAGE -
METAL PANEL
PBPC
LAPSIDING
TYPE 1
8" REVEAL
T.O.
PARAPET 2
83' - 6"
PANEL AND
CHANNEL
PANEL AND CHANNEL
A211
F3
A211
A6
PERFORATED RAILING PERFORATED RAILINGVERTICAL PICKET RAILING
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
FP07
67' - 0"
A B C D EA1
CORRUGATED MTL.
TYPE 1
LAPSIDING TYPE 1
6" REVEAL
PANEL AND CHANNEL
CORRUGATED MTL.
TYPE 2
ALUMINUM
STOREFRONT
PANEL AND
CHANNEL
BRICK
BRICK
PANEL AND CHANNEL ALUMINUM
STOREFRONT
LAPSIDING TYPE 1;
6" REVEAL
A2
SIGNAGE - METAL
PANEL
A1
A262
A1
A262
T.O.
PARAPET 2
83' - 6"
A212
E5
A212
A5
A213
A4
PERFORATED RAILING
VERTICAL PICKET RAILING
BR-1 - BRICK - COLOR 1 -
MODULAR
CR-1 - CORRUGATED
METAL - TYPE 1
FC-1 - FIBER CEMENT
LAP SIDING - COLOR 1
FC-2 - FIBER CEMENT LAP
SIDING - COLOR 2
FCP-1 - FIBER CEMENT PANELIZED
CLADDING SYSTEM (PANEL AND
CHANNEL)
CR-2 - CORRUGATED
METAL - TYPE 2 - COLOR 1
FC-3 - FIBER CEMENT LAP
SIDING - COLOR 3
CR-3 - CORRUGATED
METAL - TYPE 2 - COLOR 2 SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONSEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
MATERIAL KEYNOTES GENERAL NOTES SHEET SPECIFIC NOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:54:38 PMCHARLOTTE, NC 28205EXTERIOR ELEVATIONSCRESCENT NoDa10/01/2015
10550-00
A201CRESCENT COMMUNITIESSCALE: 1/16" = 1'-0"
EAST ELEVATIONF4
SCALE: 1/16" = 1'-0"
SOUTH ELEVATIONB1 1632FT01. A STANDALONE MOCK-UP ILLUSTRATING ALL OF THE MAJOR EXTERIOR BUILDING
COMPONENTS WILL BE REQUIRED. THIS INCLUDES, EXTERIOR FINISHES, WINDOW
AND FLASHING ETC. A MOCK-UP DRAWINGS WILL BE PROVIDED BY ARCHITECT. THE
MOCK-UP SHALL REMAIN IN PLACE DURING THE DURATION OF CONSTRUCTION, BUT IS
NOT PERMANENT. MOCK-UP APPROVAL IS AT THE DISCRETION OF THE ARCHITECT
AND OWNER.
2. ELEVATIONS DEPICT MATERIAL TYPE ONLY, FINAL COLOR SECTIONS AND
LOCATIONS WILL BE REFINED BY ARCHITECT FOR 100% CD.
1 50% PRICING 10.1.15
2 City Comments 10.9.15
3 PRICING ADD. 1 10.9.15
3
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
A.4B.4
G1
A262
G1
A262
CORRUGATED
METAL TYPE 1
ALUMINUM
STOREFRONT
BRIDGE FROM
PARKING DECK
ALUMINUM FINS
CHAIN LINK
FENCE LAPSIDING TYPE
1; 6" REVEAL
P2P3P4P5P6P7P8 A6A7
A1
A262
A1
A262
T.O.
PARAPET 1
60' - 6"
LAPSIDING TYPE
1; 6" REVEAL
PANEL AND
CHANNEL
A214
A7
A214
A1
VERTICAL PICKET RAILING
PERFORATED RAILING
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
G1
A261
G1
A261
C1
A261
C1
A261
PANEL AND
CHANNEL
LAPSIDING TYPE 1;
6" REVEAL
CORRUGATED MTL
TYPE 1
CORRUGATED
MTL. TYPE 2
ACM METAL
CANOPY
CANOPY
GROUND LEVEL
ENTRY/EXIT PARKING
DECK
PA PB PCA3A4A5
PANEL AND
CHANNEL
19
T.O.
PARAPET 1
60' - 6"
A214
F7
A214
F1
A213
E6
VERTICAL PICKET RAILING
BR-1 - BRICK - COLOR 1 -
MODULAR
CR-1 - CORRUGATED
METAL - TYPE 1
FC-1 - FIBER CEMENT
LAP SIDING - COLOR 1
FC-2 - FIBER CEMENT LAP
SIDING - COLOR 2
FCP-1 - FIBER CEMENT PANELIZED
CLADDING SYSTEM (PANEL AND
CHANNEL)
CR-2 - CORRUGATED
METAL - TYPE 2 - COLOR 1
FC-3 - FIBER CEMENT LAP
SIDING - COLOR 3
CR-3 - CORRUGATED
METAL - TYPE 2 - COLOR 2 SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONSEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
MATERIAL KEYNOTES GENERAL NOTES SHEET SPECIFIC NOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:54:41 PMCHARLOTTE, NC 28205EXTERIOR ELEVATIONSCRESCENT NoDa10/01/2015
10550-00
A202CRESCENT COMMUNITIESSCALE: 1/16" = 1'-0"
NORTH ELEVATIONG1
SCALE: 1/16" = 1'-0"
WEST ELEVATIONB4 1632FT01. A STANDALONE MOCK-UP ILLUSTRATING ALL OF THE MAJOR
EXTERIOR BUILDING COMPONENTS WILL BE REQUIRED. THIS
INCLUDES, EXTERIOR FINISHES, WINDOW AND FLASHING ETC. A
MOCK-UP DRAWINGS WILL BE PROVIDED BY ARCHITECT. THE
MOCK-UP SHALL REMAIN IN PLACE DURING THE DURATION OF
CONSTRUCTION, BUT IS NOT PERMANENT. MOCK-UP APPROVAL IS
AT THE DISCRETION OF THE ARCHITECT AND OWNER.
2. ELEVATIONS DEPICT MATERIAL TYPE ONLY, FINAL COLOR
SECTIONS AND LOCATIONS WILL BE REFINED BY ARCHITECT FOR
100% CD.
1 50% PRICING 10.1.15
2 City Comments 10.9.15
3 PRICING ADD. 1 10.9.15
3
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
FP07
67' - 0"
ROOF
(+798')
78' - 2"
P1P2P3P4P5P6P7P8
4' - 1 1/2"2' - 3"43' - 9"36' - 0"36' - 0"36' - 0"36' - 0"36' - 0"43' - 9"
TYP.D7
AP001
3' - 3"5' - 3"6' - 2"5' - 0"5' - 11"5' - 3"5' - 11"5' - 3"5' - 11"5' - 3"5' - 11"SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
1/16" = 1'-0"C:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/1/2015 1:53:50 PMCHARLOTTE, NC 28205PARKING DECK ELEVATIONSCRESCENT NoDa10/01/2015
10550-00
AP201CRESCENT COMMUNITIESSCALE: 1/16" = 1'-0"
PARKING DECK ELEVATION - NORTHA1 1632FT0
STORAGE 1 STORAGE 2 STORAGE 3 STORAGE 4 STORAGE 5T2T3T3B1B1B2 A1 B1 A1A1A2A2A2B2A5 A5A3A1B2S1A1B2A3A4A5A6A7A819SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABCDEFGHJK123456789101112131415© 2013 Lord Aeck SargentLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck SargentS1-01
STORAGE 3 STORAGE 4 STORAGE 5B2 A1 B1 A1A5 A5B2S1A1B24321678910A.4B.4CDE11121314151617518SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABCDEFGHJK123456789101112131415© 2013 Lord Aeck SargentLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck SargentS1-02
SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONSEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTIONLord, Aeck & Sargent, Inc.
Architect
M2 Strucural, LLC
Structural Engineer
Charlotte Mechanical
Mechanical/ Plumbing
LandDesign
Civil Engineer/ Landscape Design
1175 Peachtree Street NE
Suite 2400
Atlanta, GA 30361
[phone]
[phone] - Fax
887 West Marietta St.
Suite T-103
Atlanta, GA 30318
404-829-2612
14301 S Lakes Drive
Suite E
Charlotte, NC 28273
704-847-1198
704-847-4377 - Fax
223 North Graham Street
Charlotte, NC 28202
704-333-0325
704-332-3246 - Fax
LAS Project No.
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
MATERIAL KEYNOTES GENERAL NOTES SHEET SPECIFIC NOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
Power Design, Inc
Electrical
11600 Ninth Street North
St. Petersburg, FL, 33716
727-568-7953
727-210-0508 - Fax
Vignette Interior Design
Interior Designer
1514 South Church Street
Suite 107
Charlotte, NC 28203
704-315-2929
C:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/1/2015 4:31:58 PMCHARLOTTE, NC 28205COVER SHEETCRESCENT NoDa10/01/2015
10550-00
G001CRESCENT COMMUNITIESCRESCENT COMMUNITIES
CRESCENT NoDa
10550-00
10/01/2015
50% PRICING
1 50% PRICING 10.1.15
1
SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
3" = 1'-0"C:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:55:20 PMCHARLOTTE, NC 28205UNIT AND AREA MATRIXCRESCENT NoDa10/01/2015
10550-00
G031CRESCENT COMMUNITIES1 50% PRICING 10.1.15
2 PRICING ADD. 1 10.9.15
2
EXISTING
FENCE (TYP)
EX. GRAVEL
EX. PAVEMENT/
CONCRETE/GRAVEL (TYP)
EX. PAVEMENT/
CONCRETE/GRAVEL (TYP)
EXISTING FIRE
HYDRANT (TYP)
EXISTING OVERHEAD
UTILITY (TYP)
EXISTING STORM
DRAINAGE (TYP)
EXISTING FENCE (TYP)
ABANDONED RAILROAD
TRACKS (TYP)
EXISTING GAS (TYP)
EXISTING
RETAINING WALL
AND FENCE
EXISTING UTILITY
POLE/FIRE HYDRANT (TYP)
EXISTING SANITARYSEWER (TYP)
EXISTING RAILROAD
TRACKS (TYP)
EXISTING
UNDERGROUND
ELECTRIC (TYP)
PROPERTY
BOUNDARY (TYP)
PROPERTY
BOUNDARY (TYP)
FUTURE LIGHT RAIL
STATION PER BLE PLANS
(UNDER CONSTRUCTION)
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
FUTURE RAILROAD
TRACK CENTERLINE
PER BLE PLANS
FUTURE LIGHT
RAIL STATION PER
BLE PLANS
15'15'30'60'
EXISTING STORM
DRAINAGE (TYP)
NOTES
1.THE CONTRACTOR IS CAUTIONED THAT THE LOCATION AND/OR
ELEVATION OF EXISTING UTILITIES AS SHOWN ON THESE PLANS
ARE BASED ON RECORDS OF THE VARIOUS UTILITY COMPANIES,
PREVIOUS DESIGN DOCUMENTS, AND WHERE POSSIBLE,
MEASUREMENTS TAKEN IN THE FIELD. THE INFORMATION IS NOT
TO BE RELIED ON AS BEING EXACT OR COMPLETE. THE LOCATION
OF EXISTING UTILITIES MUST BE VERIFIED IN THE FIELD BY THE
CONTRACTOR PRIOR TO CONSTRUCTION.
2.SHOULD UNCHARTED, OR INCORRECTLY CHARTED PIPING OR
OTHER UTILITIES BE ENCOUNTERED DURING CONSTRUCTION,
CONSULT PROJECT ENGINEER AND UTILITY OWNER FOR
IMMEDIATE ACTION.
3.PRIOR TO THE COMMENCEMENT OF CONSTRUCTION, THE
CONTRACTOR SHALL COORDINATE HIS/HER ACTIVITIES WITH ALL
UTILITY COMPANIES SERVING THIS AREA. THE CONTRACTOR IS
TO COORDINATE FULLY WITH THE UTILITY COMPANIES ON THE
EXACT LOCATION OF ALL UNDERGROUND UTILITIES PRIOR TO
DEMOLITION, CONSTRUCTION, AND EXCAVATION.
4.CONTRACTOR SHALL VERIFY AND PROTECT ALL PUBLIC UTILITIES.
ANY WORK ASSOCIATED WITH SAID UTILITIES TO BE
COORDINATED WITH APPROPRIATE UTILITY COMPANY.
EXISITING CONDITIONS SURVEY
SURVEY PROVIDED BY LDSI. LIGHT RAIL BLUE LINE AND 36TH STREET GRADING AND
LAYOUT INFORMATION PROVIDED BY CATS AND HAS BEEN INCORPORATED INTO THE BASE
INFORMATION. THESE PLANS HAVE BEEN DESIGNED BASED ON THE ABOVE COMBINATION
OF SURVEY AND LIGHT RAIL BLUE LINE DESIGN DATA. CONTRACTOR SHALL VERIFY THAT
THE LOCATION OF ALL BLE STRUCTURES AND UTILITIES, AS WELL AS OTHER
SURROUNDING UTILITIES, ARE CONSISTENT WITH DESIGN DATA SHOWN. IF DISCREPANCIES
ARE DISCOVERED, THE CONTRACTOR SHALL IMMEDIATELY NOTIFY CIVIL ENGINEER OF
RECORD.
EX. CONCRETE
INV: 696.23
INV: 696.19
EXISTING CONCRETE
RETAINING WALL
EXISTING BROKEN
CONCRETE RETAINING WALL
EX. GRAVEL
EX. GRAVEL
EX. CONCRETE
INV: 699.24
15" RCP
INV: 699.24
INV: 706.32
STMH RIM: 706.02
INV IN: 700.62
INV OUT: 699.40
STMH RIM: 708.09
INV CL: 703.05
INV: 692.56
INV: 698.60
STMH RIM: 703.95INV IN: 700.85
INV OUT: 693.10
18" RCP
24"
R
C
P18" CMP
EX. CONCRETE
15" RCP 15" RCP
INV: 703.0136" RCPABANDONED RAILROAD
TRACKS (TYP)
EXISTING RAILROAD
TRACKS (TYP)
APPROXIMATE
LOCATION OF TCE
PER DB 28247 PG 545 APPROXIMATE
LOCATION OF TCEPER DB 28247 PG 545
APPROXIMATE
LOCATION OF TCE
PER DB 28247 PG 545
APPROXIMATE
LOCATION OF TCEPER DB 29562 PG 94
APPROXIMATE
LOCATION OF TCE
PER DB 29562 PG 9418" RCPEX. LIGHT
POLE (TYP)
EX. OVERHEAD
UTILITY (TYP)
PERMANENT
EASEMENT PER
DB 28247 PG545
CURB PER CATS BLE
DESIGN PLANS (TYP)
SANITARY SEWER PER CATS
BLE DESIGN PLANS (TYP)
SIDEWALK PER CATS
BLE DESIGN PLANS (TYP)
42" RCP
15" RCP15" RCP42" RCP42" RCP42" STEEL36" RCP15" RCP8" PVC8" PVC8" PVC
8" PVC 8" PVC
8" P
V
C
BLE SSMH
RIM: 707.20
INV IN: 701.29
INV OUT: 701.09
BLE SSMH
RIM: 703.20
INV IN: 698.24
INV OUT: 698.04
BLE SSMHRIM: 696.40
INV IN: 692.07
INV OUT: 691.87
BLE SSMHRIM: 697.40
INV IN: 692.60
INV OUT: 691.40
BLE SSMH
RIM: 708.90INV IN: UNKNOWN
INV OUT: 696.82
WATER LINE PER CATSBLE DESIGN PLANS (TYP)12" DIP
WATER12" DIP WATER5.THE CONTRACTOR SHALL IMMEDIATELY REPORT TO THE OWNER
AND ENGINEER ANY DISCREPANCIES FOUND BETWEEN ACTUAL
FIELD CONDITIONS AND CONSTRUCTION DOCUMENTS AND SHALL
WAIT FOR INSTRUCTIONS PRIOR TO PROCEEDING.
6.PRIOR TO BEGINNING CONSTRUCTION THE CONTRACTOR IS
RESPONSIBLE TO VERIFY THAT ALL REQUIRED PERMITS AND
APPROVALS HAVE BEEN OBTAINED FROM ALL REGULATORY
AUTHORITIES AND SHALL BE THOROUGHLY FAMILIAR WITH
CONDITIONS OF SAID PERMITS AND INSPECTION REQUIREMENTS.
7.THE CONTRACTOR SHALL CONTACT ALL OWNERS OF EASEMENTS,
UTILITIES AND RIGHT-OF-WAYS, PUBLIC OR PRIVATE, PRIOR TO
WORKING IN THESE AREAS.
8.THE CONTRACTOR SHALL BE RESPONSIBLE FOR DAMAGE TO ANY
EXISTING ITEM AND/OR MATERIAL INSIDE OR OUTSIDE THE
CONSTRUCTION LIMITS.
9.LANDDESIGN SHALL NOT BE IN CONTROL OR CHARGE OF, AND
SHALL NOT BE RESPONSIBLE FOR ACTUAL CONSTRUCTION
MEANS, METHODS, TECHNIQUES, PROCEDURES, OR SAFETY
PRECAUTIONS IN CONNECTION WITH THE WORK, OR FOR THE
ACTS OR OMISSIONS OF CONTRACTORS OR ANY OTHER PERSONS
NOT UNDER THE EMPLOYMENT OF LANDDESIGN.
PROJECT INFORMATION
- ZONING: TOD
- JURISDICTION: CHARLOTTE
- DISTRICT: CENTRAL CATAWBA
- WITHIN DISTRESSED BUSINESS DISTRICT: YES NO
- WITHIN TRANSIT ORIENTED DISTRICT: YES NO
CHARLOTTE, NC 28205CRESCENT NoDa10/01/2015
10550-00CRESCENT COMMUNITIESSHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
‹/RUG$HFN6DUJHQW
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
1. PRICING - 10.01.15
EX. WOODEN
RETAINING WALL EXISTING CONDITIONSC1.1 1" = 30'
EXISTING FENCE TO
BE REMOVED
EX. PAVEMENT/
CONCRETE/GRAVEL TO BE
REMOVED (TYP)
EX. PAVEMENT/ CONCRETE/GRAVEL
TO BE REMOVED (TYP)
EX. PAVEMENT/ CONCRETE/GRAVEL
TO BE REMOVED (TYP)
EXISTING FENCE TOBE REMOVED
EXISTING UTILITY
POLE/FIRE HYDRANT
TO BE REMOVED (TYP)
EXISTING OVERHEAD
UTILITY TO BE REMOVED
EXISTING STORM
DRAINAGE TO BE
REMOVED OR RELOCATED
EXISTING FENCE
TO BE REMOVED
EXISTING RAILROAD
TRACKS TO BE REMOVED
EXISTING GAS TO
BE REMOVED (TYP)
EXISTING FENCE
TO BE REMOVED
EXISTING UTILITY
POLE/FIRE HYDRANT
TO BE REMOVED (TYP)
EXISTING SANITARY SEWER
TO BE REMOVED (TYP)
EXISTING RAILROAD
TRACKS TO BE REMOVED
EXISTING UNDERGROUNDELECTRIC TO BE
REMOVED (TYP)
EXISTING STORM
DRAINAGE TO BE
REMOVED
PROPERTY
BOUNDARY (TYP)
PROPERTY
BOUNDARY (TYP)
FUTURE LIGHT
RAIL STATION
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
FUTURE RAILROAD
TRACK CENTERLINE
FUTURE LIGHT
RAIL STATION
15'15'30'60'
EXISTING STORM
DRAINAGE TO BEREMOVED
EXISTING GAS MAIN
EXISTING SANITARY SEWER
EXISTING WATER MAIN
EXISTING STORM DRAINAGE
LEGEND
EXISTING ELECTRIC
EXISTING UNDERGROUND TELEPHONE
EXISTING FENCE
DEMOLITION NOTES
1.EXISTING UTILITIES (ELECTRIC, CABLE, TELEPHONE, GAS, ETC.) TO BE
REMOVED/RELOCATED SHALL BE DONE BY OTHERS AND PAID FOR BY
CONTRACTOR UNLESS PREVIOUS NEGOTIATIONS HAVE BEEN MADE
WITH OWNER. ALL OTHER UTILITIES (WATER, SEWER, STORM AND
IRRIGATION) SHALL BE REMOVED BY CONTRACTOR.
2.DEMOLITION WORK SHALL NOT COMMENCE UNTIL DEMOLITION PERMIT
HAS BEEN ISSUED.
3.CONTRACTOR SHALL SUBMIT DEMOLITION SCHEDULE TO OWNER PRIOR
TO PROCEEDING WITH DEMOLITION ACTIVITIES.
4.EXTENT OF SITE CLEARING IS SHOWN ON EROSION CONTROL PLANS.
5.CONDUCT SITE DEMOLITION OPERATIONS TO ENSURE MINIMUM
INTERFERENCE WITH ROADS, STREETS, WALKS, AND OTHER ADJACENT
OCCUPIED OR USED FACILITIES. DO NOT CLOSE OR OBSTRUCT
STREETS, WALKS OR OTHER OCCUPIED OR USED FACILITIES WITHOUT
PERMISSION FROM AUTHORITIES HAVING JURISDICTION.
6.ALL PROPERTY AFFECTED BY THIS WORK SHALL BE RESTORED TO A
CONDITION EQUAL TO OR BETTER THAN THE EXISTING UNLESS
OTHERWISE SPECIFICALLY EXEMPTED BY THESE PLANS.
7.REMOVE WASTE MATERIALS AND UNSUITABLE AND EXCESS TOPSOIL
FROM PROPERTY AND DISPOSE OF OFF-SITE IN A LEGAL MANNER.
(PERMIT REQUIRED FOR OFF-SITE DISPOSAL)
8.LOCATE EXISTING ABOVE GROUND AND UNDERGROUND UTILITIES IN
AREAS OF WORK. IF UTILITIES ARE TO REMAIN IN PLACE, PROVIDE
ADEQUATE MEANS OF SUPPORT AND PROTECTION DURING DEMOLITION
OPERATION.
9.SHOULD UNCHARTED, OR INCORRECTLY CHARTED PIPING OR OTHER
UTILITIES BE ENCOUNTERED DURING DEMOLITION, CONSULT PROJECT
ENGINEER AND UTILITY OWNER FOR IMMEDIATE ACTION.
10.DEMOLISH AND COMPLETELY REMOVE FROM SITE MATERIAL INDICATED
ON PLAN OR NOTED "TO BE REMOVED".
11.PROTECT STRUCTURES, UTILITIES, SIDEWALKS, PAVEMENTS, AND
OTHER FACILITIES FROM DAMAGE CAUSED BY SETTLEMENT, LATERAL
MOVEMENT, UNDERMINING, WASHOUT AND OTHER HAZARDS CREATED
BY THE DEMOLITION OPERATION.
12.CONTRACTOR SHALL MAINTAIN POSITIVE STORM DRAINAGE DURING
CONSTRUCTION TO INSURE NO DAMAGE TO ADJACENT PROPERTIES
OCCURS DURING STORM EVENTS.
13.THE CONTRACTOR IS CAUTIONED THAT THE LOCATION AND/OR
ELEVATION OF EXISTING UTILITIES AS SHOWN ON THESE PLANS ARE
BASED ON RECORDS OF THE VARIOUS UTILITY COMPANIES, PREVIOUS
DESIGN DOCUMENTS, AND WHERE POSSIBLE, MEASUREMENTS TAKEN
IN THE FIELD. THE INFORMATION IS NOT TO BE RELIED ON AS BEING
EXACT OR COMPLETE. THE LOCATION OF EXISTING UTILITIES MUST BE
VERIFIED IN THE FIELD BY THE CONTRACTOR PRIOR TO CONSTRUCTION.
14.ALL DEMOLITION AND CONSTRUCTION SHALL COMPLY WITH
APPLICABLE BUILDING CODES AND LOCAL RESTRICTIONS. THE
CONTRACTOR MUST COMPLY WITH ALL OF THE CONTRACTOR
REGISTRATION REQUIREMENTS OF ALL GOVERNING AUTHORITIES.
15.PRIOR TO THE COMMENCEMENT OF DEMOLITION, THE CONTRACTOR
WILL COORDINATE HIS ACTIVITIES WITH ALL UTILITY COMPANIES
SERVING THIS AREA. THE CONTRACTOR IS TO COORDINATE FULLY WITH
THE UTILITY COMPANIES ON THE EXACT LOCATION OF ALL
UNDERGROUND UTILITIES PRIOR TO DEMOLITION, CONSTRUCTION, AND
EXCAVATION.
16.ALL PAVING REMOVAL AND DEMOLITION SHALL BE PERFORMED AS
SHOWN ON THE PLANS OR AS DIRECTED BY THE ENGINEER OR OWNER.
17.RELOCATION OR REMOVAL OF OVERHEAD OR UNDERGROUND UTILITIES
SHALL BE COORDINATED WITH THE APPROPRIATE UTILITY COMPANY.
18.ALL PROPOSED PAVEMENT CUTS SHALL BE SAW CUT ONLY.
19.CONTRACTOR SHALL PROVIDE A MINIMUM OF 72 HOURS ADVANCE
NOTICE TO THE OWNER PRIOR TO STARTING DEMOLITION ACTIVITIES.
20.CONTRACTOR SHALL VERIFY AND PROTECT ALL PUBLIC UTILITIES. ANY
WORK ASSOCIATED WITH SAID UTILITIES TO BE COORDINATED WITH
APPROPRIATE UTILITY COMPANY.
21.THE CONTRACTOR SHALL IMMEDIATELY REPORT TO THE OWNER AND
ENGINEER ANY DISCREPANCIES FOUND BETWEEN ACTUAL FIELD
CONDITIONS AND CONSTRUCTION DOCUMENTS AND SHALL WAIT FOR
INSTRUCTIONS PRIOR TO PROCEEDING.
22.PRIOR TO BEGINNING CONSTRUCTION THE CONTRACTOR IS
RESPONSIBLE TO VERIFY THAT ALL REQUIRED PERMITS AND
APPROVALS HAVE BEEN OBTAINED FROM ALL REGULATORY
AUTHORITIES AND SHALL BE THOROUGHLY FAMILIAR WITH CONDITIONS
OF SAID PERMITS AND INSPECTION REQUIREMENTS.
23.THE GENERAL CONTRACTOR SHALL CONTACT ALL OWNERS OF
EASEMENTS, UTILITIES AND RIGHT-OF-WAYS, PUBLIC OR PRIVATE,
PRIOR TO WORKING IN THESE AREAS.
24.THE CONTRACTOR SHALL BE RESPONSIBLE FOR DAMAGE TO ANY
EXISTING ITEM AND/OR MATERIAL INSIDE OR OUTSIDE THE
CONSTRUCTION LIMITS.
25.CONTRACTOR SHALL MAINTAIN THE SITE IN A MANNER SO THAT
WORKMEN AND PUBLIC ARE PROTECTED FROM INJURY.
26.LANDDESIGN SHALL NOT BE IN CONTROL OR CHARGE OF, AND SHALL
NOT BE RESPONSIBLE FOR ACTUAL CONSTRUCTION MEANS, METHODS,
TECHNIQUES, PROCEDURES, OR SAFETY PRECAUTIONS IN CONNECTION
WITH THE WORK, OR FOR THE ACTS OR OMISSIONS OF CONTRACTORS
OR ANY OTHER PERSONS NOT UNDER THE EMPLOYMENT OF
LANDDESIGN.
EXISTING ASPHALT/CONCRETETO BE REMOVED
EXISTING UTILITY TO BE REMOVED
EXISTING BLDG TO BE REMOVED
CHARLOTTE, NC 28205CRESCENT NoDa10/01/2015
10550-00CRESCENT COMMUNITIESSHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
‹/RUG$HFN6DUJHQW
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
1. PRICING - 10.01.15
EXISTING CONCRETE/RETAINAING WALL TO
BE REMOVED DEMOLITION PLANC2.0 1" = 30'27. CONTRACTOR SHALL NOT ENTER RAIL
ROAD R/W AT ANY TIME WITHOUT A PERMIT
OR AUTHORIZATION FROM THE
RESPONSIBLE PARTIES.
R/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WAPAPBBLLLLLRTTRTRRTLWFTVMTVMTVMTVM
1130+00PHASE 1PHASE 2T
TTPHASE 1PHASE 2PHASE 1PHASE 2R/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WAPAPBBLLLLLRTTRTRRTLWFTVMTVMTVMTVM
1130+0012.00'12.00'30.00'18.00'18.00'8.00'6.00'6.00'
7.50'
TYP.23.50' TYP.5.00'22.00'9.50'6.00'6.50'8.00'15.00'8.00'TYP.8.00'30.44'23.07'
10.26'16.00'7.00'12.00'7.00'11.50'
6.00'8.00
'
5.80'6.00'5.16'22.00'6.00'11.00'11.00'8.50'P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.COURTYARD A(SEE COURTYARDLAYOUT PLAN THIS SET)COURTYARD B(SEE COURTYARDLAYOUT PLAN THIS SET)35TH STREETLYNX BLUE LINE EXTENSION - 36TH STREET STATION(UNDER CONSTRUCTION)PARKING STRUCTUREEXISTING RAILROADEXISTING RAILROADNODA PLAZA(SEE PLAZA LAYOUTPLAN THIS SET)REMNANT PIECE OFRAILROAD TRACK16' SETBACK16' SETBACK16' SETBACK61.00'R25.00'5.50'5.50'6.00'40.00'30.00'30.00'65.00'21.63'34.76'33.49'47.19'24.00'11.50'19.00'R40.00'P.A.P.A.P.A.P.A.12.00'12.00'
R18.00'TRASHSERVICE/LOADING24.00'8.00
'
8.00'R14.50'R13.00'R18.50'R17.00'R25.00'R
2
5
.
0
0
'R61.00'R39.00'R50.00'R36.00'R14.00'R10.50'R13.50'72.00'7.00'72.00'2.00'20.00
'20.00'25.00'BUILDINGABOVEP.A.P.A.P.A.P.A.14.00'1.50
'2.00'2.00
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'14.54'LCLC4.50'TYP.4.50'TYP.8.00'1'-0" SIDEWALK EASEMENTFUTURECOMMERCIALPAD36TH STREET(UNDER CONSTRUCTION)P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.0'15'15'30'60'PRELIMINARYNOT FOR CONSTRUCTIONCHARLOTTE, NC 28205
CRESCENT NoDa10/01/201510550-00CRESCENT COMMUNITIES
SHEET TITLE
SCALE (U.N.O.)
JOB NAME
LOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABC DEFGHJK123456789101112131415‹/RUG$HFN6DUJHQWLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck Sargent1. PRICING - 10.01.15DEVELOPMENT SUMMARY:1.TAX PARCEL ID NUMBER:- #083031032.SITE JURISDICTION:- CITY OF CHARLOTTE3.EXISTING ZONING & USES:- TRANSIT ORIENTED DEVELOPMENT DISTRICT: MIXED-USE ORIENTED OPTIONAL (TOD-MO)4.PROPOSED USES:- MULTI-FAMILY APARTMENTS- RETAIL5.TOTAL SITE SF (ACREAGE):“6)“$&6.DIMENSIONAL REQUIREMENTS:- 16' SETBACK - 36TH STREET - MEASURED FROM FUTURE BACK OF CURB- 15' STREET SIDE YARD SETBACK TO SOUTH - EXISTING NCRR R.O.W (RESERVED FOR FUTURE CROSS CHARLOTTE TRAIL)- 54' BUILDING SIDE YARD SETBACK TO SOUTH - EXISTING NCRR R.O.W.- SIDE YARD SETBACK TO NORTH - NONE REQUIRED- 10' REAR YARD SETBACK - ADJACENT TO THE YARDS AT NODA7.TOTAL RESIDENTIAL UNITS:- 345 UNITSPARKING REQUIREMENTS:1A.VEHICULAR PARKING REQUIRED:- RETAIL:MAXIMUM OF ONE SPACE PER 250 SQ. FT.- RESIDENTIAL: MIN. OF 1 SPACE/UNIT, MAX. OF 1.6 SPACES/UNIT1B.VEHICULAR PARKING PROVIDED:- RETAIL: 100 SPACES WITHIN DECK- RESIDENTIAL: 446 SPACES WITHIN DECK- ON STREET: 5 ON-STREET PARALLEL SPACES ON PRIVATE ST. - TOTAL SPACES = 551 SPACES2A.BICYCLE PARKING REQUIRED:- RETAIL:- LONG TERM:2 SPACES REQUIRED- SHORT TERM:5% OF AUTO PARKING (6 SPACE REQUIRED)- RESIDENTIAL:- LONG TERM: NONE REQUIRED- SHORT TERM:1 SPACE PER 20 UNITS (17 SPACES REQUIRED)2B.BICYCLE PARKING PROVIDED:- 10 SPACES- 24 SPACES WITHIN DECK (LONG TERM)- TOTAL SPACES = 34 SPACESGENERAL NOTES:1. SITE SURVEY INFORMATION PROVIDED BY:LDSI, INC.508 WEST 5TH ST.CHARLOTTE, NC 28202704.337.8329VICINITY MAPNTSSITENORTH DAV
IDSON
STE. 36TH STNORTH TRYON
STLYNX BLUE LINENCRRLAYOUT NOTES:1.AT TIME OF STAKING, CONTRACTOR TO CONTACT LANDSCAPE ARCHITECT FOR DIGITAL SITE PLAN FILE FOR COORDINATIONOF STAKING.2.SHOULD ANY DISCREPANCIES OR ERRORS BETWEEN COORDINATE POINTS AND DIMENSIONS OR OMISSIONS OF CRITICALSTAKING INFORMATION BE DISCOVERED, CONTACT THE LANDSCAPE ARCHITECT IMMEDIATELY FOR A COORDINATEDSOLUTION.3.ALL DIMENSIONS AND RADII ARE TO THE BACK OF CURB UNLESS OTHERWISE NOTED.4.ALL SIDEWALKS SHALL BE FIELD STAKED FOR APPROVAL BY THE LANDSCAPE ARCHITECT.5.LAND DEVELOPMENT ENGINEER TO BE GIVEN 24 HOURS NOTICE PRIOR TO START OF CONSTRUCTION.6.ALL CONSTRUCTION SHALL COMPLY WITH CHARLOTTE/MECKLENBURG LAND DEVELOPMENT STANDARDS ANDSPECIFICATIONS.7.ALL PATCH WORK WITHIN LIMIT OF CONSTRUCTION SHALL BE CONSISTENT WITH ASSOCIATED ASPHALT PAVEMENT DETAIL.8.ELECTRICAL, TELEPHONE, AND CABLE LINES AND POLES TO BE ELIMINATED OR RELOCATED, SHALL BE COORDINATED WITHDUKE POWER, AT&T, AND TIME WARNER.9.ALL TRAFFIC SIGNS AND MARKINGS TO BE INSTALLED AND COMPLY WITH CURRENT CLDSM AND MUTCD STANDARDS ANDSPECIFICATIONS.10.REFER TO CIVIL DRAWINGS FOR ADDITIONAL INFORMATION.11.RIGHT -OF-WAY ENCROACHMENT AGREEMENT IS REQUIRED FOR THE INSTALLATION OF ALL NON-STANDARD ITEMS(IRRIGATION SYSTEMS, DECORATIVE CONCRETE PAVEMENT, BRICK PAVERS, ETC.) WITHIN A PROPOSED/EXISTING CITYMAINTAINED STREET RIGHT OF WAY BY A PRIVATE INDIVIDUAL, GROUP, BUSINESS, OR HOMEOWNER'S/BUSINESSASSOCIATION.12.PER SECTION 18-175(e) OF THE CITY CODE AND SECTION 10.0 OF THE CITY'S POST CONSTRUCTION CONTROLS EASEMENTS(PCCEs) MUST BE RECORDED PRIOR TO THE ISSUANCE OF THE CERTIFICATE OF OCCUPANCY.13.REFER TO ELECTRICAL PLANS FOR FINAL SITE LIGHTING LOCATIONS.8.TOTAL STORIES:- 7 STORIES ON PODIUM/5 STORIES PLUS BASEMENT LEVEL9.BUILDING HEIGHT:- MID-RISE RESIDENTIAL = 55'-10"- MID-RISE RESIDENTIAL ON PODIUM = 78'-2" (MAX HEIGHT ALLOWED = 85'-0"10.PROPOSED GROSS FLOOR AREA:- 290,500 SF11.REQUIRED URBAN OPEN SPACE:- NONE REQUIRED13.PROPOSED URBAN OPEN SPACE:- PUBLIC URBAN OPEN SPACE PROVIDED = +/- 36,580 SF- PRIVATE OPEN SPACE PROVIDED:+ POOL COURTYARD = +/- 7,000 SF+ AMENITY COURTYARD = +/- 5,420 SF+ ROOF DECK AMENITY SPACE = +/- 4,210 SF14.OFF STREET SERVICE*:- RETAIL/RESIDENTIAL LOADING SPACES:0 SPACES (NONE REQUIRED)- RECYCLING STATION REQUIRED:1 STATIONS @ 144 SF PER 80- RECYCLING STATION PROVIDED: 5 STATIONS @ 144 SF = 720 SF TOTAL- SOLID WASTE REQUIRED:SPACE FOR 8 CU. YD. COMPACTOR PER 90 UNITS- SOLID WASTE PROVIDED:SPACE FOR AN EQUIVALENT TO (4) 8 CU. YD. COMPACTORS*ALL SOLID WASTE AND RECYCLING SERVICES TO BE PROVIDED BY A PRIVATE COMPANY.THE YARDSAT NODAOVERALL LAYOUT PLANC3.01" = 30'35 TH ST
R/WR/WR/WR/WR/WR/W X X XR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WBLTAPAPBBLLLLLRTTRTRRTLWFTVMTVMTVMTVM 1122+00 (-LRTNB-)1123+00
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1127+00 (-LRTNB
-
)
1128+00
1129+00
1125+00
1130+00R/WR/WR/WR/WR/WR/W X X XR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WBLTAPAPBBLLLLLRTTRTRRTLWFTVMTVMTVMTVM 1122+00 (-LRTNB-)1123+00
1126+00
1127+00 (-LRTNB
-
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1130+00PHASE 1PHASE 2T
TTPHASE 1PHASE 2PHASE 1PHASE 21.2%717.48708.00START CURB717.48717.12717.48BP717.10RIM 716.70BP 717.10RIM 716.70BP 717.00714.50RIM 715.90717.48717.48FFE 717.50BP716.20RIM 714.60BP 716.203.00%RIM 715.90717.48717.40717.48717.48RIM715.90RIM 706.30706.38COURTYARD A(SEE COURTYARDLAYOUT PLAN THIS SET)COURTYARD B(SEE COURTYARDLAYOUT PLAN THIS SET)35TH STREET36TH STREETLYNX BLUE LINE EXTENSION - 36TH STREET STATIONPARKING STRUCTUREEXISTING RAILROADEXISTING RAILROADREMNANT PIECE OFRAILROAD TRACK5.0%714.50716.50716.00716.40BP 716.201.5%716.80717.30714.00717.00718.002% MAX717.122% MAX2% MAX716.40717.12717.12716.70717.12716.402% MAX2.30%716.402.60%717.12717.12717.20717.40716.70717.12716.702% MAX717.48717.20717.40717.40717.40717.48717.30717.30717.302%MAX3%717.283%
1%1%1%2%MAX717.28717.303.3%716.50716.50RIM 716.302%MAX716.50RIM 716.30TW 716.50712711710710TW 715.17TW 713.84TW 712.50SWALE706.38706.15706.38706.38RIM 704.98BC 705.25RIM 705.50TC 706.00BC 705.803.9%RAILROAD R/WPROPERTYBOUNDARYFUTURE LIGHT RAILSTATION STAIRTHE YARDSAT NODAPROPERTYBOUNDARYFUTURE RAILROADTRACK CENTERLINERIM 706.00717.48RIM 717.39717.25717.46RIM 717.392% MAX2% MAXLEGEND:717.26SPOT ELEVATIONHARDSCAPE DRAINGRATE ELEVATIONTOP OF WALLTWBOTTOM OF WALLBWBREAK POINTBPSLOPELANDSCAPE DRAINHARDSCAPE DRAINTOP OF STAIRTSBOTTOM OF STAIRBS1%RIM717.26PRELIMINARYNOT FOR CONSTRUCTIONCHARLOTTE, NC 28205
CRESCENT NoDa10/01/201510550-00CRESCENT COMMUNITIES
SHEET TITLE
SCALE (U.N.O.)
JOB NAME
LOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABC DEFGHJK123456789101112131415‹/RUG$HFN6DUJHQWLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck Sargent1. PRICING - 10.01.150'15'15'30'60'OVERALL GRADING PLANC5.01" = 30'
PRELIMINARYNOT FOR CONSTRUCTIONCHARLOTTE, NC 28205
CRESCENT NoDa10/01/201510550-00CRESCENT COMMUNITIES
SHEET TITLE
SCALE (U.N.O.)
JOB NAME
LOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABC DEFGHJK123456789101112131415‹/RUG$HFN6DUJHQWLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck Sargent1. PRICING - 10.01.15GRADING NOTES:1.) REFER TO LAYOUT PLAN FOR RELATED NOTES.2.) ALL CONTOURS AND SPOT ELEVATIONS REFLECT FINISHED GRADE.3.) ALL FILL TO BE COMPACTED TO 98% A.A.S.H.O. STANDARD COMPACTION UNLESS OTHERWISE NOTED.4.) THE PROPOSED CONTOURS SHOWN IN DRIVES, PARKING LOTS AND SIDEWALKS ARE FINISHED ELEVATIONSINCLUDING ASPHALT. REFER TO PAVEMENT CROSS-SECTION DATA TO ESTABLISH CORRECT SUB-BASE OR AGGREGATEBASE COURSE ELEVATIONS.5.) LIMITS OF CLEARING SHOWN ON EROSION CONTROL PLANS ARE BASED ON CUT AND FILL SLOPES OR OTHERGRADING REQUIREMENTS.6.) ANY GRADING BEYOND THE LIMITS OF CONSTRUCTION SHOWN ON THE EROSION CONTROL PLAN IS SUBJECT TO AFINE.7.) STABILIZATION IS THE BEST FORM OF EROSION CONTROL. TEMPORARY SEEDING IS NECESSARY TO ACHIEVEEROSION CONTROL ON DENUDED AREAS AND ESPECIALLY WHEN THE CONSTRUCTION SEQUENCE REQUIRES IT. ALLGRADED SLOPES ARE TO BE SEEDED OR LANDSCAPED: WITHIN 7 CALENDAR DAYS FROM THE LAST LAND-DISTRUBINGACTIVITY FOR ALL PERIMETER DIKES, SWALES, PERIMETER SLOPES, AND ALL SLOPES STEEPER THAN 3 HORIZONTAL TO 1VERTICAL (3:1); AND AS SOON AS PRACTICABLE BUT IN ANY EVENT WITHIN 14 CALENDAR DAYS FROM LASTLAND-DISTURBING ACTIVITY FOR ALL OTHER DISTURBED AREAS.8.) CONTRACTOR SHALL INSTALL EROSION CONTROL MEASURES AS INDICATED ON EROSION CONTROL PLANS. NOEROSION CONTROL DEVICE MEASURE MAY BE REMOVED UNTIL THE SITE IS STABILIZED.9.) ON-SITE BURIAL PITS REQUIRE AN ON-SITE DEMOLITION LANDFILL PERMIT FROM THE ZONING ADMINISTRATOR.10.) SLOPES SHALL BE GRADED NO STEEPER THAN 2:1. FILL SLOPES GREATER THAN 10' REQUIRE ADEQUATETERRACING (CLDSM #30.16).11.) THE CITY ENGINEERING DEPARTMENT SHALL BE NOTIFIED 24 HOURS IN ADVANCE OF THE COMMENCEMENT OFCONSTRUCTION ACTIVITY.12.) NON-STANDARD ITEMS (IE: PAVERS, IRRIGATION SYSTEMS, ETC.) IN THE RIGHT-OF-WAY REQUIRE A RIGHT-OF-WAYENCROACHMENT AGREEMENT WITH THE CHARLOTTE DEPARTMENT OF TRANSPORTATION/NORTH CAROLINADEPARTMENT OF TRANSPORTATION BEFORE INSTALLATION.13.) PRIOR TO PLAT RECORDATION, OFFSITE R/W AND/OR CONSTRUCTION EASEMENTS ARE REQUIRED TO BE OBTAINEDACCORDING TO THE GUIDELINES OF THE "OFFSITE R/W ACQUISITION PROCESS". THESE NEEDED R/W ANDCONSTRUCTION LIMITS ARE CLEARLY SHOWN ON THE ROADWAY IMPROVEMENT PLAN.14.) THE DEVELOPER SHALL CONTACT THE CHARLOTTE DEPARTMENT OF TRANSPORTATION TO IDENTIFY ANYCONFLICTS WITH TRAFFIC SIGNALIZATION EQUIPMENT. 60-90 DAYS WILL BE REQUIRED TO COORDINATE RELOCATION.DEVELOPER SHALL BE RESPONSIBLE FOR ALL RELATED RELOCATION COST AND/OR ANY REPAIR COST CAUSED BY THECONTRACTOR/DEVELOPER.15.) IN ORDER TO ENSURE PROPER DRAINAGE, MAINTAIN MINIMUM 0.5% SLOPE ON ALL CURB.16.) STORM DRAIN PIPE TO FOLLOW THE APPROVED CITY OF CHARLOTTE STANDARDS AND SPECIFICATIONS. RCPSTORM DRAINAGE PIPE INSTALLED WITHIN EXISTING OR PROPOSED PUBLIC RIGHT-OF-WAY MUST BE APPROVED BY THECITY'S INSPECTOR PRIOR TO ANY BACKFILL BEING PLACED. BACKFILL MATERIAL MUST BE APPROVED BY THE CITYINSPECTOR PRIOR TO PLACEMENT OF THE MATERIAL WITHIN THE PUBLIC RIGHT-OF-WAY. THE CITY INSPECTOR MUSTBE PRESENT DURING THE BACKFILLING OPERATION AS WELL.A) BACKFILL MATERIAL USED TO INSTALL RCP PIPE WITHIN THE STREET RIGHT-OF-WAY SHALL BE SELECT MATERIAL,CLASS II-IV, AS DEFINED BY SECTION 1016-3 OF THE NCDOT STANDARD SPECIFICATIONS FOR ROADS AND STRUCTURES.UPON SUBMITTAL OF WRITTEN CERTIFICATION OF MATERIAL SUITABILITY BY A LICENSED GEOTECHNICAL ENGINEER,NCDOT CLASS I SELECT MATERIAL MAY BE USED. ALL BACKFILL MATERIAL SHALL BE APPROVED BY THE CITYINSPECTOR PRIOR TO PLACEMENT OF THE MATERIAL WITHIN THE STREET RIGHT-OF-WAY.17.) GRADING CONTRACTORS SHALL NOTIFY AND COOPERATE WITH ALL UTILITY COMPANIES OR FIRMS HAVINGFACILITIES ON OR ADJACENT TO THE SITE BEFORE DISTURBING, ALTERING, REMOVING, RELOCATING, ADJUSTING ORCONNECTING TO SAID FACILITIES. CONTRACTORS SHALL PAY ALL COSTS IN CONNECTION WITH THE ALTERATION OF ORRELOCATION OF THE FACILITIES. CONTRACTORS SHALL RAISE OR LOWER TOPS OF EXISTING MANHOLES AS REQUIREDTO MATCH FINISHED GRADES.18.) GRADING CONTRACTOR SHALL COOPERATE AND WORK WITH ALL OTHER CONTRACTORS PERFORMING WORK ONTHIS PROJECT TO INSURE PROPER AND TIMELY COMPLETION OF THIS PROJECT.19.) THE GRADING CONTRACTOR SHALL USE WHATEVER MEASURES ARE REQUIRED TO PREVENT SILT ANDCONSTRUCTION DEBRIS FROM FLOWING ONTO ADJACENT PROPERTIES. CONTRACTOR SHALL COMPLY WITH ALL LOCAL,STATE, AND FEDERAL EROSION SEDIMENT AND SILTATION ORDINANCES. CONTRACTOR SHALL REMOVE ALLTEMPORARY EROSION CONTROL STRUCTURES UPON COMPLETION OF PERMANENT DRAINAGE FACILITIES AND NOTBEFORE ALL AREAS DRAINING INTO THESE STRUCTURES ARE SUFFICIENTLY STABILIZED.20.) FOR ANY WORK ON THE STATE OR CITY RIGHT-OF-WAY, THE GRADING CONTRACTOR SHALL: A) NOT STOREMATERIAL, EXCESS DIRT OR EQUIPMENT IN THE RIGHT-OF-WAY IN CASE OF MULTILANE HIGHWAYS. THE PAVEMENTSHALL BE KEPT FREE FROM ANY MUD OR EXCAVATION WASTE FROM TRUCKS OR OTHER EQUIPMENT. ON COMPLETIONOF THE WORK ALL EXCESS MATERIAL SHALL BE REMOVED FROM THE RIGHT-OF-WAY; B) PROVIDE ALL NECESSARY ANDADEQUATE SAFETY PRECAUTIONS SUCH AS SIGNS, FLAGS, LIGHT BARRICADES AND FLAGMEN AS REQUIRED BY THELOCAL AUTHORITIES AND IN ACCORDANCE WITH THE MANUAL ON UNIFORM TRAFFIC CONTROL DEVICES. THE GRADINGCONTRACTOR SHALL BE SOLELY RESPONSIBLE FOR AND HOLD HARMLESS THE CITY OF CHARLOTTE, THE STATE OFNORTH CAROLINA, THE ARCHITECT/ENGINEER, AND THE OWNER FROM ANY CLAIMS FOR DAMAGE DONE TO EXISTINGPRIVATE PROPERTY, PUBLIC UTILITIES, OR TO THE TRAVELING PUBLIC; C) COMPLETE WORK TO THE SATISFACTION OFTHE CHARLOTTE MECKLENBURG UTILITIES DEPARTMENT (CMUD) AND OBTAIN A LETTER FROM THE DEPARTMENTSTATING THAT THE WORK IS ACCEPTABLE.21.) GRADING CONTRACTOR SHALL TAKE ALL AVAILABLE PRECAUTIONS TO CONTROL DUST. CONTRACTOR SHALLCONTROL DUST BY SPRINKLING, OR BY OTHER METHODS AS DIRECTED BY ENGINEER AND/OR OWNER'SREPRESENTATIVE AT NO ADDITIONAL COST TO OWNER.22.) GRADING CONTRACTOR TO COMPLY WITH ALL STATE AND LOCAL SEDIMENT CONTROL AND AIR POLLUTIONORDINANCES OR RULES.23.) BEFORE ANY MACHINE WORK IS DONE, CONTRACTOR SHALL STAKE OUT AND MARK THE ITEMS ESTABLISHED BYTHE SITE PLAN. CONTROL POINTS SHALL BE PRESERVED AT ALL TIMES DURING THE COURSE OF THE PROJECT. LACKOF PROPER WORKING POINTS AND GRADE STAKES MAY REQUIRE CESSATION OF OPERATIONS UNTIL SUCH POINTS ANDGRADES HAVE BEEN PLACED TO THE OWNER'S SATISFACTION.24.) "AS-BUILT" DRAWINGS AND PLANS OF THE STORM DRAINAGE SYSTEM, MUST BE SUBMITTED PRIOR TO FINALINSPECTION TO THE CITY/COUNTY ENGINEERING DEPARTMENT IN ACCORDANCE WITH THE CITY/COUNTY SUBDIVISIONORDINANCE.25.) CONTRACTOR SHALL REPAIR OR REPLACE IN-KIND ANY DAMAGE THAT OCCURS AS RESULT OF HIS WORK.26.) APPROVAL OF THIS PLAN IS NOT AN AUTHORIZATION TO GRADE ADJACENT PROPERTIES. WHEN FIELD CONDITIONSWARRANT OFF-SITE GRADING, PERMISSION MUST BE OBTAINED FROM THE AFFECTED PROPERTY OWNERS.27.) THE PURPOSE OF THE STORM DRAINAGE EASEMENT (SDE) IS TO PROVIDE STORM WATER CONVEYANCE. BUILDINGSARE NOT PERMITTED IN THE EASEMENT AREA. ANY OTHER OBJECTS WHICH IMPEDE STORM WATER FLOW OR SYSTEMMAINTENANCE ARE ALSO PROHIBITED.28.) PE SEALED SHOP DRAWINGS FOR RETAINING WALL MUST BE SUBMITTED TO CITY ENGINEER PRIOR TOCONSTRUCTION.29.) PRIOR TO INSTALLATION, PE SEALED SHOP DRAWINGS FOR UNDERGROUND DETENTION SYSTEMS MUST BEFURNISHED TO CITY OF CHARLOTTE ENGINEERING FOR APPROVAL.30.) CERTIFICATION AND STREET CUT PERMITS ARE REQUIRED FOR UTILITY CUTS ON CITY STREETS. ALLOW 7 DAYSPROCESSING FOR PERMIT. FOR INFORMATION CONTACT CHARLOTTE DEPARTMENT OF TRANSPORTATION (704-336-4025)OR VISIT HTTP://WWW.CHARMECK.ORG/DEPARTMENTS/TRANSPORTATION/STREET+MAINTENANCE/HOME.HTMLSITE ACCESSIBILITY NOTES1. ALL BUILDINGS WITHIN THE BOUNDARY OF THlS SITE, UNLESS OTHERWISESTATED AS EXEMPT, SHALL HAVE "ACCESSIBLE ROUTES" AS REQUIRED THATCONFORM TO THE REQUIREMENTS OF "THE AMERICANS WITH DISABILITIESACT", FAIR HOUSING STANDARDS, ICC ANSI A 117.1-209 AND GOVERNING STATEHANDICAP CODE STANDARDS.- THESE STANDARDS FOR ACCESSIBILITY INCLUDE, BUT ARE NOT LIMITEDTO:MAXIMUM WALK SLOPE - 5%MAXIMUM RAMP SLOPE - 8.33% WITH RAILINGMAXIMUM CROSS SLOPE - 2%2. ALL WALKS TO BE BROOM FINISHED CONCRETE UNLESS OTHERWISESPECIFIED ON THESE DRAWINGSMAXIMUM ACCESSIBLE ROUTE LENGTH (NC) - 200'3. THE PAVEMENT SLOPE WITHIN ACCESSIBLE PARKING SPACES SHALL NOTEXCEED 2% IN ALL DIRECTIONS.4. CONTRACTOR TO CONTACT THE APPROPRIATE AUTHORITY FOR ANYVARYING SITE CONDITIONS OR DISCREPANCIES AFFECTING SITE ACCESSIBILITYREQUIREMENTS.ADDITIONAL ACCESSIBLE ROUTE NOTES FOR ACCESSIBILITY COMPLIANCE WITHICC/ANSI A117.1-2009, AND 2010 ADA STANDARDS.1. PROTRUDING OBJECTS ON CIRCULATION PATHS WITHIN COMMON USEAREAS TO COMPLY WITH ANSI 2009 SECTION 307, INCLUDING:A.) PROTRUSION LIMITS: OBJECTS WITH LEADING EDGES MORE THAN 27"AND NOT MORE THAN 80" ABOVE THE FLOOR MAY PROTRUDE 4"MAXIMUM HORIZONTALLY INTO THE CIRCULATION PATH. EXCEPTIONSINCLUDE HANDRAILS, DOOR CLOSER, AND DOOR STOPS.B.) POST MOUNTED OBJECTS: OBJECTS ON POSTS OR PYLONS SHALL BEPERMITTED TO OVERHANG 4" MAXIMUM WHERE MORE THAN 27" AND NOTMORE THAN 80" ABOVE THE FLOOR. OBJECTS ON MULTIPLE POSTS ORPYLONS WHERE THE CLEAR DISTANCE BETWEEN THE POSTS OR PYLONSIS GREATER THAN 42" SHALL HAVE THE LOWEST EDGE OF SUCH OBJECTEITHER 27" MAXIMUM OR 80" MINIMUM ABOVE THE FLOOR.C.) REDUCED VERTICAL CLEARANCE: GUARDRAILS OR OTHER BARRIERSSHALL BE PROVIDED WHERE OBJECT PROTRUSION IS BEYOND THELIMITS ALLOWED BY SECTIONS 307.2 AND 307.3, AND WHERE THEVERTICAL CLEARANCE IS LESS THAN 80" ABOVE THE FLOOR. THELEADING EDGE OF SUCH GUARDRAIL OR BARRIER SHALL BE 27"MAXIMUM ABOVE THE FLOOR.2. PROTRUDING OBJECTS ON CIRCULATIONS PATHS WITHIN PUBLIC USE AREASTO COMPLY WITHIN 2010 ADA CODE, SECTION 307, INCLUDING:A.) 2010 ADA SECTION 307.2: OBJECTS PROJECTING FROM WALLSB.) 2010 ADA SECTION 307.4: MINIMUM CLEAR HEADROOM3. FLOOR AND GROUND SURFACES IN COMMON USE AREAS SHALL BE STABLE,FIRM AND SLIP-RESISTANT AND SHALL COMPLY WITHIN ANSI 2009 SECTIONS3O2.4. FLOOR AND GROUND SURFACES ALONG ACCESSIBLE ROUTES AND INACCESSIBLE ROOMS AND SPACES WITHIN PUBLIC USE AREAS SHALL BE STABLE,FIRM, AND SLIP-RESISTANT AND SHALL COMPLY WITH 2010 ADA SECTION 302.5. CHANGES IN LEVEL IN COMMON USE AREAS SHALL COMPLY WITH ANSI 2009.6. CHANGES IN LEVEL ALONG ACCESSIBLE ROUTES AND IN ACCESSIBLE ROOMSAND SPACES WITH PUBLIC USE AREAS SHALL COMPLY WITHIN 2010 ADASECTION 303.7. IF TREES OR OTHER PLANTINGS OVERHANG ALONG THE CIRCULATIONROUTES AT THE SIDEWALK WITHOUT PROTECTION AT 27" A.F.F. OR LOWER,ASSURE THEY DO NOT EXTEND GREATER THAN 4" INTO THE CIRCULATIONROUTE AT A HEIGHT OF 80" ABOVE GRADE OR LOWER (1986 ANSI, SECTION4.4.1).8. THE CONTROLS AT ANY ADDITIONAL COMMON USE ELEMENTS SUCH AS GATEHARDWARE, FIRE PIT, POOL SHOWER, ETC. WHICH ARE INTENDED TO BE USEDBY THE RESIDENTS AND THEIR GUESTS ARE LOCATED ON AN ACCESSIBLEROUTE, WITHIN THE REQUIRED REACH RANGE OF 15"-48" A.F.F. AND AREOPERABLE WITHIN ONE HAND USING 5LB MAXIMUM PRESSURE WITHOUT TIGHTGRASPING, PINCHING, OR TWISTING OF THE WRIST (1986 ANSI, SECTION 4.25AND ANSI 2009, SECTION 308).ADA DOOR and/or GATE POINTS OF ACCESSPLANSCALE: 1/2" = 1'-0"5'-0"5'-0"2% MAX SLOPE2% MAX SLOPE ADJACENT PAVINGAREA, REFER TOPAVING PLANADJACENT PAVINGOR LANDSCAPEAREA, REFER TOPAVING PLANFACE OFBUILDINGOR FENCEDOOR OR GATE1'-6"REQUIRED CLEARANCEON PULL SIDEOR LATCH SIDE OF DOOR OR GATEGRADING NOTES
C5.1AS SHOWN
N26°51'10"W 403.33'T
T
TUP
UP
MECH
088
ELEC
082
MECH
087
ELEC
081
ELEC
080
MECH
086
STAIR 04
094
CORR.
073
CORR.
072
STAIR 02
092
G1
A261
C1
A261
C1
A261
G1
A262
G1
A262
STORAGE 1
001
STORAGE 2
002
STORAGE 3
003
STORAGE 4
004
STORAGE 5
005
FACILITIES/STORAGE
074
SEE PARKING DECK PLAN
SHEET AP100
STAIR 05
095
A121
B1
STAIR 03
093
A313
A12
A314
A11
A316
A12
A3
A4
A5
A6 A7
T2
066
T3
065
T3
064
B1
059
B1
057
B2
054
A1
056
B1
058
A1
060
A1
052
A2
055
A2
053
A2
051
B2
048 A5
046
A5
044
A3
049
A1
050
TRASH/REC
076
A341
A12
B2
036
S1
038
A1
040
B2
042
MECH
085
MECH
089
DOG WASH
007
WORKSHOP
006
A1
A262
A1
A262
A122
A9
19
A217
E9
A217
H3
A217
F3
ELEVATOR
LOBBY
098
A217
A6
AB
C D SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:53:46 PMCHARLOTTE, NC 28205BASEMENT LEVEL FLOOR PLANCRESCENT NoDa10/01/2015
10550-00
A100CRESCENT COMMUNITIESA. DO NOT SCALE DRAWINGS, DIMENSIONS GOVERN.
B. ALL PARTITIONS ARE DIMENSIONED TO FACE OF
CONCRETE OR CENTERLINE OF OPENING UNLESS
NOTED OTHERWISE. ALL DIMENSIONS SHOWN ON
THE DRAWINGS ARE TO BE CONSIDERED CRITICAL.
IT SHALL BE THE RESPONSIBILITY OF THE
CONTRACTOR TO INFORM THE ARCHITECT OF ANY
DEVIATION IN THE PLACEMENT OF WORK PRIOR TO
INSTALLATION.
C. BUILDING DIMENSIONS ARE TYPICAL FOR ALL
LEVELS UNLESS NOTED OTHERWISE.
D. DOUBLE STUD CONSTRUCTION TO BE USED AT ALL
DOOR OPENINGS.
E. ALL FLOOR AND WALL PENETRATIONS IN RATED
ASSEMBLIES SHALL BE SEALED WITH APPROVED,
CURRENT, FIRESTOP ASSEMBLIES APPROPRIATE
FOR THE RATED WALL ASSEMBLY.
F. FURNISH CLASS A, B, C FIRE EXTINGUISHERS ON
BRACKETS AS INDICATED ON THE DRAWINGS
G. SLOPE ALL CONCRETE PARKING AREAS TO DRAIN.
H. PROVIDE SPECIFIED CLEAR SEALER AT ALL
EXPOSED CONCRETE.
I. GROUT ALL CMU PARTITIONS TO THE TOP OF
STRUCTURE.
J. GROUT ALL HOLLOW METAL FRAMES IN CONCRETE
PARTITIONS.
K. DOORS IN PARKING STRUCTURES TO BE PT-0.
REFER TO FINISH SCHEDULE.
L. PROVIDE MAXIMUM ¾” THRESHOLDS AT EXTERIOR
DOORS. WARP SLABS AS REQUIRED, TYP.
M. PROVIDE 114” CLEARANCE AT VAN ACCESSIBLE
PARKING SPACES WITH CLEAR PATH OF TRAVEL TO
DECK ENTRANCE. PROVIDE 98” CLEARANCE AT
ACCESSIBLE PARKING SPACES. COORDINATE
LIGHTING AND FIRE PROTECTION SYSTEMS IN
PARKING STRUCTURE TO MAINTAIN REQUIRED
HEIGHT CLEARANCES.
N. ALL UNIT DEMISING WALLS SHALL BE TYPE P-20
UNLESS NOTED OTHERWISE.
O. ALL CORRIDOR WALLS SHALL BE TYPE P-10 WITH
FIRE RETARDANT TREATED WOOD UNLESS NOTED
OTHERWISE. USE TYPE P-19 WHERE LOAD BEARING
– SEE STRUCTURAL.
P. FURNISH FIRE EXTINGUISHERS IN FULLY RECESSED
CABINETS IN ALL COMMON AREAS AND
CORRIDORS.
Q. PROVIDE GYP. BOARD CONTROL JOINTS @ 30’-0” ON
CENTER MAXIMUM OR AS INDICATED ON INTERIOR
ELEVATIONS.
R. REFER TO LIFE SAFETY DRAWINGS FOR FIRE
RATED PARTITION LOCATIONS AND INFORMATION.
S. ALL WOOD FRAMING AND BLOCKING BELOW THE
PODIUM TO BE FIRE RETARDANT TREATED.
T. SEE A201-A203 FOR BUILDING ELEVATIONS AND
A211 & A212 FOR SECTIONS.2040FT01 50% PRICING 10.1.15
2 City Comments 10.9.15
3 PRICING ADD. 1 10.9.15
3
N26°51'10"W 403.33'S U
A A S HT O 2 0 0 1 (U S)
T
T
T
TUP
UP
UP
UP
D WR EF
A202
G1
A201
B1
11
12
13
14
15
16
17
S
R
Q
3
2
1
A.4 B.4
A B C D
P
4
E
6
7
8
9
10
A215
A8
A2
F8
A216 F9
F3
A9
A3
F3
RETAIL AREA 1
2481 S.F.
RETAIL AREA 2
1193 S.F.
RETAIL AREA 3
1019 S.F.
RETAIL AREA 4
1179 S.F.
A1
5
MECH
187
ELEC
181 MECH
189
STOR.
174
ELEC
180
MECH
186
MECH
185
CORR.
172
STAIR 01
191
STAIR 02
192
STAIR 04
194
ELEC
179
ELECTRICAL
112
BOOSTER PUMP
111
FIRE PUMP
110
G1
A261
C1
A261
C1
A261
G1
A262
G1
A262
GREASE
SHAFT
ABOVE
105.64°
FITNESS CENTER
104
SEE PARKING DECK PLAN
SHEET AP101
CENTRAL TRASH
175
RETAIL CORR.
103.1
NOTE 1
STAIR 03
193
A312
A12
A313
A9
A314
A8
A315
A8
A316
D9
A2
A3
A4
A5
A6 A7
A217
A9
A340
A10
T2 Mezzanine
066T3 Mezzanine
065
T3 Mezzanine
064
B1
159
B1
157
B2
154
A1
156
B1
158
A1
160
B2
136
A5c ADA
138
S1
124
B2
142
A5
144
A5
146
B2
148
A1
150
A2
155
A2
153
A2
151
A3
149
A1
147
B1
145
B1
143
A1
141
A3
139
B2c ADA
120
S1
137
A1
135 B1
133
B1
131
S1
118
S1
116
B1
114
B2
126
S1
128
S1
130
S1
132
S1
134
A1
152
MAIL & RAIL
101
LEASING
100
ELEC/DATA
177
LOADING
113
18
CLUB ROOM
102
MECH
184
STAIR 05
195
TRASH/REC
176
A317
A12
A341
F12
A1
140
A1
122
MECH
183
RETAIL AREA 5
1744 S.F.
A1
A262
A1
A262
POOL EQUIP.
109
18" MIN.18" MIN.1 8 " M IN .
WOMENS
108
MENS
106
MANAGER
100.5
WORK ROOM
100.2
R.R.
100.1
PACKAGES
100.3
BREAK
100.4
CORR.
171.1
JAN.
108.1
CORR.
171
19
A217
E9
A217
H3
A217
F3
ELEVATOR
LOBBY
199
ELEVATOR
LOBBY
198
A217
A6
A6313
A317
A6
A217 A1
GROUP FITNESS
104.1
A608H5
AB
C D SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:53:54 PMCHARLOTTE, NC 28205LEVEL 1 FLOOR PLANCRESCENT NoDa10/01/2015
10550-00
A101CRESCENT COMMUNITIES1. PROVIDE TWO (2) HOUR RATING AT UNDERSIDE OF
ENTRANCE DRIVE BRIDGE.
2. JANITOR CLOSET MOP SINK: FIAT MSB-2424
A SEE GENERAL NOTES A100 TYP.
B ALL STAIRS TO BE METAL PAN STAIRS.
C CONTRACTOR SHALL MAKE WRITTEN REQUEST TO
OWNER FOR ANY AND ALL CONSTRUCTION
EASEMENTS THAT THE CONSTRACTOR DEEMS
NECESSARY PRIOR TO BEGINNING WORK
D TWO HOUR SHAFT AROUND TRASH CHUTE
E ALL UNIT DEMISING WALLS SHALL BE 1WD56G UNLESS
NOTED OTHERWISE.
F ALL CORRIDOR WALLS SHALL BE 1WD456 UNLESS
NOTED OTHERWISE.
G SLOPE ALL BALCONIES AT 2% FROM BUILDING
H PROVIDE TRAFFIC COATING AT ALL RESIDENTIAL
BALCONIES
I SEE ENLARGED PLANS FOR ADDITIONAL WALL TYPES
2040FT01 50% PRICING 10.1.15
2 PRICING ADD. 1 10.9.15
2
2
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
FP07
67' - 0"
ROOF
(+798')
78' - 2"
321 4 6 7 8 9 10
5
G1
A261
G1
A261
C1
A261
C1
A261
LAPSIDING TYPE- 1
6" EXPOSURE
ALUMINUM STORE
FRONT
CORRUGATED MTL -
TYPE 2
CORRUGATED MTL -
TYPE 1
CONCRETE/ METAL
CANOPY
PANEL AND CHANNEL
ALUMINUM
STOREFRONT
CORRUGATED
MTL. TYPE 1
LAPSIDING
TYPE 2
8" REVEAL
SIGNAGE -
METAL PANEL
PBPC
LAPSIDING
TYPE 1
8" REVEAL
T.O.
PARAPET 2
83' - 6"
PANEL AND
CHANNEL
PANEL AND CHANNEL
A211
F3
A211
A6
PERFORATED RAILING PERFORATED RAILINGVERTICAL PICKET RAILING
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
FP07
67' - 0"
A B C D EA1
CORRUGATED MTL.
TYPE 1
LAPSIDING TYPE 1
6" REVEAL
PANEL AND CHANNEL
CORRUGATED MTL.
TYPE 2
ALUMINUM
STOREFRONT
PANEL AND
CHANNEL
BRICK
BRICK
PANEL AND CHANNEL ALUMINUM
STOREFRONT
LAPSIDING TYPE 1;
6" REVEAL
A2
SIGNAGE - METAL
PANEL
A1
A262
A1
A262
T.O.
PARAPET 2
83' - 6"
A212
E5
A212
A5
A213
A4
PERFORATED RAILING
VERTICAL PICKET RAILING
BR-1 - BRICK - COLOR 1 -
MODULAR
CR-1 - CORRUGATED
METAL - TYPE 1
FC-1 - FIBER CEMENT
LAP SIDING - COLOR 1
FC-2 - FIBER CEMENT LAP
SIDING - COLOR 2
FCP-1 - FIBER CEMENT PANELIZED
CLADDING SYSTEM (PANEL AND
CHANNEL)
CR-2 - CORRUGATED
METAL - TYPE 2 - COLOR 1
FC-3 - FIBER CEMENT LAP
SIDING - COLOR 3
CR-3 - CORRUGATED
METAL - TYPE 2 - COLOR 2 SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONSEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
MATERIAL KEYNOTES GENERAL NOTES SHEET SPECIFIC NOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:54:38 PMCHARLOTTE, NC 28205EXTERIOR ELEVATIONSCRESCENT NoDa10/01/2015
10550-00
A201CRESCENT COMMUNITIESSCALE: 1/16" = 1'-0"
EAST ELEVATIONF4
SCALE: 1/16" = 1'-0"
SOUTH ELEVATIONB1 1632FT01. A STANDALONE MOCK-UP ILLUSTRATING ALL OF THE MAJOR EXTERIOR BUILDING
COMPONENTS WILL BE REQUIRED. THIS INCLUDES, EXTERIOR FINISHES, WINDOW
AND FLASHING ETC. A MOCK-UP DRAWINGS WILL BE PROVIDED BY ARCHITECT. THE
MOCK-UP SHALL REMAIN IN PLACE DURING THE DURATION OF CONSTRUCTION, BUT IS
NOT PERMANENT. MOCK-UP APPROVAL IS AT THE DISCRETION OF THE ARCHITECT
AND OWNER.
2. ELEVATIONS DEPICT MATERIAL TYPE ONLY, FINAL COLOR SECTIONS AND
LOCATIONS WILL BE REFINED BY ARCHITECT FOR 100% CD.
1 50% PRICING 10.1.15
2 City Comments 10.9.15
3 PRICING ADD. 1 10.9.15
3
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
A.4B.4
G1
A262
G1
A262
CORRUGATED
METAL TYPE 1
ALUMINUM
STOREFRONT
BRIDGE FROM
PARKING DECK
ALUMINUM FINS
CHAIN LINK
FENCE LAPSIDING TYPE
1; 6" REVEAL
P2P3P4P5P6P7P8 A6A7
A1
A262
A1
A262
T.O.
PARAPET 1
60' - 6"
LAPSIDING TYPE
1; 6" REVEAL
PANEL AND
CHANNEL
A214
A7
A214
A1
VERTICAL PICKET RAILING
PERFORATED RAILING
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
G1
A261
G1
A261
C1
A261
C1
A261
PANEL AND
CHANNEL
LAPSIDING TYPE 1;
6" REVEAL
CORRUGATED MTL
TYPE 1
CORRUGATED
MTL. TYPE 2
ACM METAL
CANOPY
CANOPY
GROUND LEVEL
ENTRY/EXIT PARKING
DECK
PA PB PCA3A4A5
PANEL AND
CHANNEL
19
T.O.
PARAPET 1
60' - 6"
A214
F7
A214
F1
A213
E6
VERTICAL PICKET RAILING
BR-1 - BRICK - COLOR 1 -
MODULAR
CR-1 - CORRUGATED
METAL - TYPE 1
FC-1 - FIBER CEMENT
LAP SIDING - COLOR 1
FC-2 - FIBER CEMENT LAP
SIDING - COLOR 2
FCP-1 - FIBER CEMENT PANELIZED
CLADDING SYSTEM (PANEL AND
CHANNEL)
CR-2 - CORRUGATED
METAL - TYPE 2 - COLOR 1
FC-3 - FIBER CEMENT LAP
SIDING - COLOR 3
CR-3 - CORRUGATED
METAL - TYPE 2 - COLOR 2 SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONSEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
MATERIAL KEYNOTES GENERAL NOTES SHEET SPECIFIC NOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
As indicatedC:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:54:41 PMCHARLOTTE, NC 28205EXTERIOR ELEVATIONSCRESCENT NoDa10/01/2015
10550-00
A202CRESCENT COMMUNITIESSCALE: 1/16" = 1'-0"
NORTH ELEVATIONG1
SCALE: 1/16" = 1'-0"
WEST ELEVATIONB4 1632FT01. A STANDALONE MOCK-UP ILLUSTRATING ALL OF THE MAJOR
EXTERIOR BUILDING COMPONENTS WILL BE REQUIRED. THIS
INCLUDES, EXTERIOR FINISHES, WINDOW AND FLASHING ETC. A
MOCK-UP DRAWINGS WILL BE PROVIDED BY ARCHITECT. THE
MOCK-UP SHALL REMAIN IN PLACE DURING THE DURATION OF
CONSTRUCTION, BUT IS NOT PERMANENT. MOCK-UP APPROVAL IS
AT THE DISCRETION OF THE ARCHITECT AND OWNER.
2. ELEVATIONS DEPICT MATERIAL TYPE ONLY, FINAL COLOR
SECTIONS AND LOCATIONS WILL BE REFINED BY ARCHITECT FOR
100% CD.
1 50% PRICING 10.1.15
2 City Comments 10.9.15
3 PRICING ADD. 1 10.9.15
3
FP01
(+717.5)
0' - 0"
FP02
11' - 2"
Basement
(+706.4)
-11' - 2"
FP03
22' - 4"
FP04
33' - 6"
FP05
44' - 8"
FP06
55' - 10"
FP07
67' - 0"
ROOF
(+798')
78' - 2"
P1P2P3P4P5P6P7P8
4' - 1 1/2"2' - 3"43' - 9"36' - 0"36' - 0"36' - 0"36' - 0"36' - 0"43' - 9"
TYP.D7
AP001
3' - 3"5' - 3"6' - 2"5' - 0"5' - 11"5' - 3"5' - 11"5' - 3"5' - 11"5' - 3"5' - 11"SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
1/16" = 1'-0"C:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/1/2015 1:53:50 PMCHARLOTTE, NC 28205PARKING DECK ELEVATIONSCRESCENT NoDa10/01/2015
10550-00
AP201CRESCENT COMMUNITIESSCALE: 1/16" = 1'-0"
PARKING DECK ELEVATION - NORTHA1 1632FT0
STORAGE 1 STORAGE 2 STORAGE 3 STORAGE 4 STORAGE 5T2T3T3B1B1B2 A1 B1 A1A1A2A2A2B2A5 A5A3A1B2S1A1B2A3A4A5A6A7A819SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABCDEFGHJK123456789101112131415© 2013 Lord Aeck SargentLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck SargentS1-01
STORAGE 3 STORAGE 4 STORAGE 5B2 A1 B1 A1A5 A5B2S1A1B24321678910A.4B.4CDE11121314151617518SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABCDEFGHJK123456789101112131415© 2013 Lord Aeck SargentLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck SargentS1-02
SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONSEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTIONLord, Aeck & Sargent, Inc.
Architect
M2 Strucural, LLC
Structural Engineer
Charlotte Mechanical
Mechanical/ Plumbing
LandDesign
Civil Engineer/ Landscape Design
1175 Peachtree Street NE
Suite 2400
Atlanta, GA 30361
[phone]
[phone] - Fax
887 West Marietta St.
Suite T-103
Atlanta, GA 30318
404-829-2612
14301 S Lakes Drive
Suite E
Charlotte, NC 28273
704-847-1198
704-847-4377 - Fax
223 North Graham Street
Charlotte, NC 28202
704-333-0325
704-332-3246 - Fax
LAS Project No.
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
MATERIAL KEYNOTES GENERAL NOTES SHEET SPECIFIC NOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
Power Design, Inc
Electrical
11600 Ninth Street North
St. Petersburg, FL, 33716
727-568-7953
727-210-0508 - Fax
Vignette Interior Design
Interior Designer
1514 South Church Street
Suite 107
Charlotte, NC 28203
704-315-2929
C:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/1/2015 4:31:58 PMCHARLOTTE, NC 28205COVER SHEETCRESCENT NoDa10/01/2015
10550-00
G001CRESCENT COMMUNITIESCRESCENT COMMUNITIES
CRESCENT NoDa
10550-00
10/01/2015
50% PRICING
1 50% PRICING 10.1.15
1
SHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONKEY PLAN
PROJECT NORTH
SEAL ISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
SHEET SPECIFIC NOTES
GENERAL NOTES
MATERIAL KEYNOTES
© 2013 Lord Aeck Sargent
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
3" = 1'-0"C:\LAS_CADD\10550_CrescentNoD_scolvin.rvt10/9/2015 4:55:20 PMCHARLOTTE, NC 28205UNIT AND AREA MATRIXCRESCENT NoDa10/01/2015
10550-00
G031CRESCENT COMMUNITIES1 50% PRICING 10.1.15
2 PRICING ADD. 1 10.9.15
2
EXISTING
FENCE (TYP)
EX. GRAVEL
EX. PAVEMENT/
CONCRETE/GRAVEL (TYP)
EX. PAVEMENT/
CONCRETE/GRAVEL (TYP)
EXISTING FIRE
HYDRANT (TYP)
EXISTING OVERHEAD
UTILITY (TYP)
EXISTING STORM
DRAINAGE (TYP)
EXISTING FENCE (TYP)
ABANDONED RAILROAD
TRACKS (TYP)
EXISTING GAS (TYP)
EXISTING
RETAINING WALL
AND FENCE
EXISTING UTILITY
POLE/FIRE HYDRANT (TYP)
EXISTING SANITARYSEWER (TYP)
EXISTING RAILROAD
TRACKS (TYP)
EXISTING
UNDERGROUND
ELECTRIC (TYP)
PROPERTY
BOUNDARY (TYP)
PROPERTY
BOUNDARY (TYP)
FUTURE LIGHT RAIL
STATION PER BLE PLANS
(UNDER CONSTRUCTION)
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
FUTURE RAILROAD
TRACK CENTERLINE
PER BLE PLANS
FUTURE LIGHT
RAIL STATION PER
BLE PLANS
15'15'30'60'
EXISTING STORM
DRAINAGE (TYP)
NOTES
1.THE CONTRACTOR IS CAUTIONED THAT THE LOCATION AND/OR
ELEVATION OF EXISTING UTILITIES AS SHOWN ON THESE PLANS
ARE BASED ON RECORDS OF THE VARIOUS UTILITY COMPANIES,
PREVIOUS DESIGN DOCUMENTS, AND WHERE POSSIBLE,
MEASUREMENTS TAKEN IN THE FIELD. THE INFORMATION IS NOT
TO BE RELIED ON AS BEING EXACT OR COMPLETE. THE LOCATION
OF EXISTING UTILITIES MUST BE VERIFIED IN THE FIELD BY THE
CONTRACTOR PRIOR TO CONSTRUCTION.
2.SHOULD UNCHARTED, OR INCORRECTLY CHARTED PIPING OR
OTHER UTILITIES BE ENCOUNTERED DURING CONSTRUCTION,
CONSULT PROJECT ENGINEER AND UTILITY OWNER FOR
IMMEDIATE ACTION.
3.PRIOR TO THE COMMENCEMENT OF CONSTRUCTION, THE
CONTRACTOR SHALL COORDINATE HIS/HER ACTIVITIES WITH ALL
UTILITY COMPANIES SERVING THIS AREA. THE CONTRACTOR IS
TO COORDINATE FULLY WITH THE UTILITY COMPANIES ON THE
EXACT LOCATION OF ALL UNDERGROUND UTILITIES PRIOR TO
DEMOLITION, CONSTRUCTION, AND EXCAVATION.
4.CONTRACTOR SHALL VERIFY AND PROTECT ALL PUBLIC UTILITIES.
ANY WORK ASSOCIATED WITH SAID UTILITIES TO BE
COORDINATED WITH APPROPRIATE UTILITY COMPANY.
EXISITING CONDITIONS SURVEY
SURVEY PROVIDED BY LDSI. LIGHT RAIL BLUE LINE AND 36TH STREET GRADING AND
LAYOUT INFORMATION PROVIDED BY CATS AND HAS BEEN INCORPORATED INTO THE BASE
INFORMATION. THESE PLANS HAVE BEEN DESIGNED BASED ON THE ABOVE COMBINATION
OF SURVEY AND LIGHT RAIL BLUE LINE DESIGN DATA. CONTRACTOR SHALL VERIFY THAT
THE LOCATION OF ALL BLE STRUCTURES AND UTILITIES, AS WELL AS OTHER
SURROUNDING UTILITIES, ARE CONSISTENT WITH DESIGN DATA SHOWN. IF DISCREPANCIES
ARE DISCOVERED, THE CONTRACTOR SHALL IMMEDIATELY NOTIFY CIVIL ENGINEER OF
RECORD.
EX. CONCRETE
INV: 696.23
INV: 696.19
EXISTING CONCRETE
RETAINING WALL
EXISTING BROKEN
CONCRETE RETAINING WALL
EX. GRAVEL
EX. GRAVEL
EX. CONCRETE
INV: 699.24
15" RCP
INV: 699.24
INV: 706.32
STMH RIM: 706.02
INV IN: 700.62
INV OUT: 699.40
STMH RIM: 708.09
INV CL: 703.05
INV: 692.56
INV: 698.60
STMH RIM: 703.95INV IN: 700.85
INV OUT: 693.10
18" RCP
24"
R
C
P18" CMP
EX. CONCRETE
15" RCP 15" RCP
INV: 703.0136" RCPABANDONED RAILROAD
TRACKS (TYP)
EXISTING RAILROAD
TRACKS (TYP)
APPROXIMATE
LOCATION OF TCE
PER DB 28247 PG 545 APPROXIMATE
LOCATION OF TCEPER DB 28247 PG 545
APPROXIMATE
LOCATION OF TCE
PER DB 28247 PG 545
APPROXIMATE
LOCATION OF TCEPER DB 29562 PG 94
APPROXIMATE
LOCATION OF TCE
PER DB 29562 PG 9418" RCPEX. LIGHT
POLE (TYP)
EX. OVERHEAD
UTILITY (TYP)
PERMANENT
EASEMENT PER
DB 28247 PG545
CURB PER CATS BLE
DESIGN PLANS (TYP)
SANITARY SEWER PER CATS
BLE DESIGN PLANS (TYP)
SIDEWALK PER CATS
BLE DESIGN PLANS (TYP)
42" RCP
15" RCP15" RCP42" RCP42" RCP42" STEEL36" RCP15" RCP8" PVC8" PVC8" PVC
8" PVC 8" PVC
8" P
V
C
BLE SSMH
RIM: 707.20
INV IN: 701.29
INV OUT: 701.09
BLE SSMH
RIM: 703.20
INV IN: 698.24
INV OUT: 698.04
BLE SSMHRIM: 696.40
INV IN: 692.07
INV OUT: 691.87
BLE SSMHRIM: 697.40
INV IN: 692.60
INV OUT: 691.40
BLE SSMH
RIM: 708.90INV IN: UNKNOWN
INV OUT: 696.82
WATER LINE PER CATSBLE DESIGN PLANS (TYP)12" DIP
WATER12" DIP WATER5.THE CONTRACTOR SHALL IMMEDIATELY REPORT TO THE OWNER
AND ENGINEER ANY DISCREPANCIES FOUND BETWEEN ACTUAL
FIELD CONDITIONS AND CONSTRUCTION DOCUMENTS AND SHALL
WAIT FOR INSTRUCTIONS PRIOR TO PROCEEDING.
6.PRIOR TO BEGINNING CONSTRUCTION THE CONTRACTOR IS
RESPONSIBLE TO VERIFY THAT ALL REQUIRED PERMITS AND
APPROVALS HAVE BEEN OBTAINED FROM ALL REGULATORY
AUTHORITIES AND SHALL BE THOROUGHLY FAMILIAR WITH
CONDITIONS OF SAID PERMITS AND INSPECTION REQUIREMENTS.
7.THE CONTRACTOR SHALL CONTACT ALL OWNERS OF EASEMENTS,
UTILITIES AND RIGHT-OF-WAYS, PUBLIC OR PRIVATE, PRIOR TO
WORKING IN THESE AREAS.
8.THE CONTRACTOR SHALL BE RESPONSIBLE FOR DAMAGE TO ANY
EXISTING ITEM AND/OR MATERIAL INSIDE OR OUTSIDE THE
CONSTRUCTION LIMITS.
9.LANDDESIGN SHALL NOT BE IN CONTROL OR CHARGE OF, AND
SHALL NOT BE RESPONSIBLE FOR ACTUAL CONSTRUCTION
MEANS, METHODS, TECHNIQUES, PROCEDURES, OR SAFETY
PRECAUTIONS IN CONNECTION WITH THE WORK, OR FOR THE
ACTS OR OMISSIONS OF CONTRACTORS OR ANY OTHER PERSONS
NOT UNDER THE EMPLOYMENT OF LANDDESIGN.
PROJECT INFORMATION
- ZONING: TOD
- JURISDICTION: CHARLOTTE
- DISTRICT: CENTRAL CATAWBA
- WITHIN DISTRESSED BUSINESS DISTRICT: YES NO
- WITHIN TRANSIT ORIENTED DISTRICT: YES NO
CHARLOTTE, NC 28205CRESCENT NoDa10/01/2015
10550-00CRESCENT COMMUNITIESSHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
J
K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
‹/RUG$HFN6DUJHQW
LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
1. PRICING - 10.01.15
EX. WOODEN
RETAINING WALL EXISTING CONDITIONSC1.1 1" = 30'
EXISTING FENCE TO
BE REMOVED
EX. PAVEMENT/
CONCRETE/GRAVEL TO BE
REMOVED (TYP)
EX. PAVEMENT/ CONCRETE/GRAVEL
TO BE REMOVED (TYP)
EX. PAVEMENT/ CONCRETE/GRAVEL
TO BE REMOVED (TYP)
EXISTING FENCE TOBE REMOVED
EXISTING UTILITY
POLE/FIRE HYDRANT
TO BE REMOVED (TYP)
EXISTING OVERHEAD
UTILITY TO BE REMOVED
EXISTING STORM
DRAINAGE TO BE
REMOVED OR RELOCATED
EXISTING FENCE
TO BE REMOVED
EXISTING RAILROAD
TRACKS TO BE REMOVED
EXISTING GAS TO
BE REMOVED (TYP)
EXISTING FENCE
TO BE REMOVED
EXISTING UTILITY
POLE/FIRE HYDRANT
TO BE REMOVED (TYP)
EXISTING SANITARY SEWER
TO BE REMOVED (TYP)
EXISTING RAILROAD
TRACKS TO BE REMOVED
EXISTING UNDERGROUNDELECTRIC TO BE
REMOVED (TYP)
EXISTING STORM
DRAINAGE TO BE
REMOVED
PROPERTY
BOUNDARY (TYP)
PROPERTY
BOUNDARY (TYP)
FUTURE LIGHT
RAIL STATION
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
RAILROAD R/W (TYP)
FUTURE RAILROAD
TRACK CENTERLINE
FUTURE LIGHT
RAIL STATION
15'15'30'60'
EXISTING STORM
DRAINAGE TO BEREMOVED
EXISTING GAS MAIN
EXISTING SANITARY SEWER
EXISTING WATER MAIN
EXISTING STORM DRAINAGE
LEGEND
EXISTING ELECTRIC
EXISTING UNDERGROUND TELEPHONE
EXISTING FENCE
DEMOLITION NOTES
1.EXISTING UTILITIES (ELECTRIC, CABLE, TELEPHONE, GAS, ETC.) TO BE
REMOVED/RELOCATED SHALL BE DONE BY OTHERS AND PAID FOR BY
CONTRACTOR UNLESS PREVIOUS NEGOTIATIONS HAVE BEEN MADE
WITH OWNER. ALL OTHER UTILITIES (WATER, SEWER, STORM AND
IRRIGATION) SHALL BE REMOVED BY CONTRACTOR.
2.DEMOLITION WORK SHALL NOT COMMENCE UNTIL DEMOLITION PERMIT
HAS BEEN ISSUED.
3.CONTRACTOR SHALL SUBMIT DEMOLITION SCHEDULE TO OWNER PRIOR
TO PROCEEDING WITH DEMOLITION ACTIVITIES.
4.EXTENT OF SITE CLEARING IS SHOWN ON EROSION CONTROL PLANS.
5.CONDUCT SITE DEMOLITION OPERATIONS TO ENSURE MINIMUM
INTERFERENCE WITH ROADS, STREETS, WALKS, AND OTHER ADJACENT
OCCUPIED OR USED FACILITIES. DO NOT CLOSE OR OBSTRUCT
STREETS, WALKS OR OTHER OCCUPIED OR USED FACILITIES WITHOUT
PERMISSION FROM AUTHORITIES HAVING JURISDICTION.
6.ALL PROPERTY AFFECTED BY THIS WORK SHALL BE RESTORED TO A
CONDITION EQUAL TO OR BETTER THAN THE EXISTING UNLESS
OTHERWISE SPECIFICALLY EXEMPTED BY THESE PLANS.
7.REMOVE WASTE MATERIALS AND UNSUITABLE AND EXCESS TOPSOIL
FROM PROPERTY AND DISPOSE OF OFF-SITE IN A LEGAL MANNER.
(PERMIT REQUIRED FOR OFF-SITE DISPOSAL)
8.LOCATE EXISTING ABOVE GROUND AND UNDERGROUND UTILITIES IN
AREAS OF WORK. IF UTILITIES ARE TO REMAIN IN PLACE, PROVIDE
ADEQUATE MEANS OF SUPPORT AND PROTECTION DURING DEMOLITION
OPERATION.
9.SHOULD UNCHARTED, OR INCORRECTLY CHARTED PIPING OR OTHER
UTILITIES BE ENCOUNTERED DURING DEMOLITION, CONSULT PROJECT
ENGINEER AND UTILITY OWNER FOR IMMEDIATE ACTION.
10.DEMOLISH AND COMPLETELY REMOVE FROM SITE MATERIAL INDICATED
ON PLAN OR NOTED "TO BE REMOVED".
11.PROTECT STRUCTURES, UTILITIES, SIDEWALKS, PAVEMENTS, AND
OTHER FACILITIES FROM DAMAGE CAUSED BY SETTLEMENT, LATERAL
MOVEMENT, UNDERMINING, WASHOUT AND OTHER HAZARDS CREATED
BY THE DEMOLITION OPERATION.
12.CONTRACTOR SHALL MAINTAIN POSITIVE STORM DRAINAGE DURING
CONSTRUCTION TO INSURE NO DAMAGE TO ADJACENT PROPERTIES
OCCURS DURING STORM EVENTS.
13.THE CONTRACTOR IS CAUTIONED THAT THE LOCATION AND/OR
ELEVATION OF EXISTING UTILITIES AS SHOWN ON THESE PLANS ARE
BASED ON RECORDS OF THE VARIOUS UTILITY COMPANIES, PREVIOUS
DESIGN DOCUMENTS, AND WHERE POSSIBLE, MEASUREMENTS TAKEN
IN THE FIELD. THE INFORMATION IS NOT TO BE RELIED ON AS BEING
EXACT OR COMPLETE. THE LOCATION OF EXISTING UTILITIES MUST BE
VERIFIED IN THE FIELD BY THE CONTRACTOR PRIOR TO CONSTRUCTION.
14.ALL DEMOLITION AND CONSTRUCTION SHALL COMPLY WITH
APPLICABLE BUILDING CODES AND LOCAL RESTRICTIONS. THE
CONTRACTOR MUST COMPLY WITH ALL OF THE CONTRACTOR
REGISTRATION REQUIREMENTS OF ALL GOVERNING AUTHORITIES.
15.PRIOR TO THE COMMENCEMENT OF DEMOLITION, THE CONTRACTOR
WILL COORDINATE HIS ACTIVITIES WITH ALL UTILITY COMPANIES
SERVING THIS AREA. THE CONTRACTOR IS TO COORDINATE FULLY WITH
THE UTILITY COMPANIES ON THE EXACT LOCATION OF ALL
UNDERGROUND UTILITIES PRIOR TO DEMOLITION, CONSTRUCTION, AND
EXCAVATION.
16.ALL PAVING REMOVAL AND DEMOLITION SHALL BE PERFORMED AS
SHOWN ON THE PLANS OR AS DIRECTED BY THE ENGINEER OR OWNER.
17.RELOCATION OR REMOVAL OF OVERHEAD OR UNDERGROUND UTILITIES
SHALL BE COORDINATED WITH THE APPROPRIATE UTILITY COMPANY.
18.ALL PROPOSED PAVEMENT CUTS SHALL BE SAW CUT ONLY.
19.CONTRACTOR SHALL PROVIDE A MINIMUM OF 72 HOURS ADVANCE
NOTICE TO THE OWNER PRIOR TO STARTING DEMOLITION ACTIVITIES.
20.CONTRACTOR SHALL VERIFY AND PROTECT ALL PUBLIC UTILITIES. ANY
WORK ASSOCIATED WITH SAID UTILITIES TO BE COORDINATED WITH
APPROPRIATE UTILITY COMPANY.
21.THE CONTRACTOR SHALL IMMEDIATELY REPORT TO THE OWNER AND
ENGINEER ANY DISCREPANCIES FOUND BETWEEN ACTUAL FIELD
CONDITIONS AND CONSTRUCTION DOCUMENTS AND SHALL WAIT FOR
INSTRUCTIONS PRIOR TO PROCEEDING.
22.PRIOR TO BEGINNING CONSTRUCTION THE CONTRACTOR IS
RESPONSIBLE TO VERIFY THAT ALL REQUIRED PERMITS AND
APPROVALS HAVE BEEN OBTAINED FROM ALL REGULATORY
AUTHORITIES AND SHALL BE THOROUGHLY FAMILIAR WITH CONDITIONS
OF SAID PERMITS AND INSPECTION REQUIREMENTS.
23.THE GENERAL CONTRACTOR SHALL CONTACT ALL OWNERS OF
EASEMENTS, UTILITIES AND RIGHT-OF-WAYS, PUBLIC OR PRIVATE,
PRIOR TO WORKING IN THESE AREAS.
24.THE CONTRACTOR SHALL BE RESPONSIBLE FOR DAMAGE TO ANY
EXISTING ITEM AND/OR MATERIAL INSIDE OR OUTSIDE THE
CONSTRUCTION LIMITS.
25.CONTRACTOR SHALL MAINTAIN THE SITE IN A MANNER SO THAT
WORKMEN AND PUBLIC ARE PROTECTED FROM INJURY.
26.LANDDESIGN SHALL NOT BE IN CONTROL OR CHARGE OF, AND SHALL
NOT BE RESPONSIBLE FOR ACTUAL CONSTRUCTION MEANS, METHODS,
TECHNIQUES, PROCEDURES, OR SAFETY PRECAUTIONS IN CONNECTION
WITH THE WORK, OR FOR THE ACTS OR OMISSIONS OF CONTRACTORS
OR ANY OTHER PERSONS NOT UNDER THE EMPLOYMENT OF
LANDDESIGN.
EXISTING ASPHALT/CONCRETETO BE REMOVED
EXISTING UTILITY TO BE REMOVED
EXISTING BLDG TO BE REMOVED
CHARLOTTE, NC 28205CRESCENT NoDa10/01/2015
10550-00CRESCENT COMMUNITIESSHEET TITLESCALE (U.N.O.)JOB NAMELOCATIONISSUE DATE
JOB. NO.
DWG. NO.
REVISION:50% PRICING - NOT FOR CONSTRUCTION1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
A
B
C
D
E
F
G
H
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K
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
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LordAeckSargent.com
Unless otherwise agreed to
in writing,this document is
the sole property of Lord
Aeck Sargent and is to be
returned upon demand. The
information herein is
confidential and may not be
used nor divulged without
the written permission of
Lord Aeck Sargent
1. PRICING - 10.01.15
EXISTING CONCRETE/RETAINAING WALL TO
BE REMOVED DEMOLITION PLANC2.0 1" = 30'27. CONTRACTOR SHALL NOT ENTER RAIL
ROAD R/W AT ANY TIME WITHOUT A PERMIT
OR AUTHORIZATION FROM THE
RESPONSIBLE PARTIES.
R/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WAPAPBBLLLLLRTTRTRRTLWFTVMTVMTVMTVM
1130+00PHASE 1PHASE 2T
TTPHASE 1PHASE 2PHASE 1PHASE 2R/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WR/WAPAPBBLLLLLRTTRTRRTLWFTVMTVMTVMTVM
1130+0012.00'12.00'30.00'18.00'18.00'8.00'6.00'6.00'
7.50'
TYP.23.50' TYP.5.00'22.00'9.50'6.00'6.50'8.00'15.00'8.00'TYP.8.00'30.44'23.07'
10.26'16.00'7.00'12.00'7.00'11.50'
6.00'8.00
'
5.80'6.00'5.16'22.00'6.00'11.00'11.00'8.50'P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.COURTYARD A(SEE COURTYARDLAYOUT PLAN THIS SET)COURTYARD B(SEE COURTYARDLAYOUT PLAN THIS SET)35TH STREETLYNX BLUE LINE EXTENSION - 36TH STREET STATION(UNDER CONSTRUCTION)PARKING STRUCTUREEXISTING RAILROADEXISTING RAILROADNODA PLAZA(SEE PLAZA LAYOUTPLAN THIS SET)REMNANT PIECE OFRAILROAD TRACK16' SETBACK16' SETBACK16' SETBACK61.00'R25.00'5.50'5.50'6.00'40.00'30.00'30.00'65.00'21.63'34.76'33.49'47.19'24.00'11.50'19.00'R40.00'P.A.P.A.P.A.P.A.12.00'12.00'
R18.00'TRASHSERVICE/LOADING24.00'8.00
'
8.00'R14.50'R13.00'R18.50'R17.00'R25.00'R
2
5
.
0
0
'R61.00'R39.00'R50.00'R36.00'R14.00'R10.50'R13.50'72.00'7.00'72.00'2.00'20.00
'20.00'25.00'BUILDINGABOVEP.A.P.A.P.A.P.A.14.00'1.50
'2.00'2.00
'16.00'5.00'18.63'2.00'12.00'23.28'6.59'15.98'R12.00'4.98'7.00'9.00' TYP.18.00
' TYP.8.00'
TYP.R20.00'R18.00'R
1
.
0
0
'

T
Y
P
.2.00
'14.54'LCLC4.50'TYP.4.50'TYP.8.00'1'-0" SIDEWALK EASEMENTFUTURECOMMERCIALPAD36TH STREET(UNDER CONSTRUCTION)P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.P.A.0'15'15'30'60'PRELIMINARYNOT FOR CONSTRUCTIONCHARLOTTE, NC 28205
CRESCENT NoDa10/01/201510550-00CRESCENT COMMUNITIES
SHEET TITLE
SCALE (U.N.O.)
JOB NAME
LOCATIONISSUE DATEJOB. NO.DWG. NO.REVISION:50% PRICING - NOT FOR CONSTRUCTION123456789101112131415ABC DEFGHJK123456789101112131415‹/RUG$HFN6DUJHQWLordAeckSargent.comUnless otherwise agreed toin writing,this document isthe sole property of LordAeck Sargent and is to bereturned upon demand. Theinformation herein isconfidential and may not beused nor divulged withoutthe written permission ofLord Aeck Sargent1. PRICING - 10.01.15DEVELOPMENT SUMMARY:1.TAX PARCEL ID NUMBER:- #083031032.SITE JURISDICTION:- CITY OF CHARLOTTE3.EXISTING ZONING & USES:- TRANSIT ORIENTED DEVELOPMENT DISTRICT: MIXED-USE ORIENTED OPTIONAL (TOD-MO)4.PROPOSED USES:- MULTI-FAMILY APARTMENTS- RETAIL5.TOTAL SITE SF (ACREAGE):“6)“$&6.DIMENSIONAL REQUIREMENTS:- 16' SETBACK - 36TH STREET - MEASURED FROM FUTURE BACK OF CURB- 15' STREET SIDE YARD SETBACK TO SOUTH - EXISTING NCRR R.O.W (RESERVED FOR FUTURE CROSS CHARLOTTE TRAIL)- 54' BUILDING SIDE YARD SETBACK TO SOUTH - EXISTING NCRR R.O.W.- SIDE YARD SETBACK TO NORTH - NONE REQUIRED- 10' REAR YARD SETBACK - ADJACENT TO THE YARDS AT NODA7.TOTAL RESIDENTIAL UNITS:- 345 UNITSPARKING REQUIREMENTS:1A.VEHICULAR PARKING REQUIRED:- RETAIL:MAXIMUM OF ONE SPACE PER 250 SQ. FT.- RESIDENTIAL: MIN. OF 1 SPACE/UNIT, MAX. OF 1.6 SPACES/UNIT1B.VEHICULAR PARKING PROVIDED:- RETAIL: 100 SPACES WITHIN DECK- RESIDENTIAL: 446 SPACES WITHIN DECK- ON STREET: 5 ON-STREET PARALLEL SPACES ON PRIVATE ST. - TOTAL SPACES = 551 SPACES2A.BICYCLE PARKING REQUIRED:- RETAIL:- LONG TERM:2 SPACES REQUIRED- SHORT TERM:5% OF AUTO PARKING (6 SPACE REQUIRED)- RESIDENTIAL:- LONG TERM: NONE REQUIRED- SHORT TERM:1 SPACE PER 20 UNITS (17 SPACES REQUIRED)2B.BICYCLE PARKING PROVIDED:- 10 SPACES- 24 SPACES WITHIN DECK (LONG TERM)- TOTAL SPACES = 34 SPACESGENERAL NOTES:1. SITE SURVEY INFORMATION PROVIDED BY:LDSI, INC.508 WEST 5TH ST.CHARLOTTE, NC 28202704.337.8329VICINITY MAPNTSSITENORTH DAV
IDSON
STE. 36TH STNORTH TRYON
STLYNX BLUE LINENCRRLAYOUT NOTES:1.AT TIME OF STAKING, CONTRACTOR TO CONTACT LANDSCAPE ARCHITECT FOR DIGITAL SITE PLAN FILE FOR COORDINATIONOF STAKING.2.SHOULD ANY DISCREPANCIES OR ERRORS BETWEEN COORDINATE POINTS AND DIMENSIONS OR OMISSIONS OF CRITICALSTAKING INFORMATION BE DISCOVERED, CONTACT THE LANDSCAPE ARCHITECT IMMEDIATELY FOR A COORDINATEDSOLUTION.3.ALL DIMENSIONS AND RADII ARE TO THE BACK OF CURB UNLESS OTHERWISE NOTED.4.ALL SIDEWALKS SHALL BE FIELD STAKED FOR APPROVAL BY THE LANDSCAPE ARCHITECT.5.LAND DEVELOPMENT ENGINEER TO BE GIVEN 24 HOURS NOTICE PRIOR TO START OF CONSTRUCTION.6.ALL CONSTRUCTION SHALL COMPLY WITH CHARLOTTE/MECKLENBURG LAND DEVELOPMENT STANDARDS ANDSPECIFICATIONS.7.ALL PATCH WORK WITHIN LIMIT OF CONSTRUCTION SHALL BE CONSISTENT WITH ASSOCIATED ASPHALT PAVEMENT DETAIL.8.ELECTRICAL, TELEPHONE, AND CABLE LINES AND POLES TO BE ELIMINATED OR RELOCATED, SHALL BE COORDINATED WITHDUKE POWER, AT&T, AND TIME WARNER.9.ALL TRAFFIC SIGNS AND MARKINGS TO BE INSTALLED AND COMPLY WITH CURRENT CLDSM AND MUTCD STANDARDS ANDSPECIFICATIONS.10.REFER TO CIVIL DRAWINGS FOR ADDITIONAL INFORMATION.11.RIGHT -OF-WAY ENCROACHMENT AGREEMENT IS REQUIRED FOR THE INSTALLATION OF ALL NON-STANDARD ITEMS(IRRIGATION SYSTEMS, DECORATIVE CONCRETE PAVEMENT, BRICK PAVERS, ETC.) WITHIN A PROPOSED/EXISTING CITYMAINTAINED STREET RIGHT OF WAY BY A PRIVATE INDIVIDUAL, GROUP, BUSINESS, OR HOMEOWNER'S/BUSINESSASSOCIATION.12.PER SECTION 18-175(e) OF THE CITY CODE AND SECTION 10.0 OF THE CITY'S POST CONSTRUCTION CONTROLS EASEMENTS(PCCEs) MUST BE RECORDED PRIOR TO THE ISSUANCE OF THE CERTIFICATE OF OCCUPANCY.13.REFER TO ELECTRICAL PLANS FOR FINAL SITE LIGHTING LOCATIONS.8.TOTAL STORIES:- 7 STORIES ON PODIUM/5 STORIES PLUS BASEMENT LEVEL9.BUILDING HEIGHT:- MID-RISE RESIDENTIAL = 55'-10"- MID-RISE RESIDENTIAL ON PODIUM = 78'-2" (MAX HEIGHT ALLOWED = 85'-0"10.PROPOSED GROSS FLOOR AREA:- 290,500 SF11.REQUIRED URBAN OPEN SPACE:- NONE REQUIRED13.PROPOSED URBAN OPEN SPACE:- PUBLIC URBAN OPEN SPACE PROVIDED = +/- 36,580 SF- PRIVATE OPEN SPACE PROVIDED:+ POOL COURTYARD = +/- 7,000 SF+ AMENITY COURTYARD = +/- 5,420 SF+ ROOF DECK AMENITY SPACE = +/- 4,210 SF14.OFF STREET SERVICE*:- RETAIL/RESIDENTIAL LOADING SPACES:0 SPACES (NONE REQUIRED)- RECYCLING STATION REQUIRED:1 STATIONS @ 144 SF PER 80- RECYCLING STATION PROVIDED: 5 STATIONS @ 144 SF = 720 SF TOTAL- SOLID WASTE REQUIRED:SPACE FOR 8 CU. YD. COMPACTOR PER 90 UNITS- SOLID WASTE PROVIDED:SPACE FOR AN EQUIVALENT TO (4) 8 CU. YD. COMPACTORS*ALL SOLID WASTE AND RECYCLING SERVICES TO BE PROVIDED BY A PRIVATE COMPANY.THE YARDSAT NODAOVERALL LAYOUT PLANC3.01" = 30'35 TH ST
Appendix B:
Figures, Tables, and Laboratory Analytical
Results
#=CL#
March 26, 2015
LIMS USE: FR - STEPHEN BROWN
LIMS OBJECT ID: 92241876
92241876
Project:
Pace Project No.:
RE:
Mr. Stephen Brown
Terracon
2020 E Starita Road
Charlotte, NC 28206
Crescent NODA Site 71157713-A
Dear Mr. Brown:
Enclosed are the analytical results for sample(s) received by the laboratory on March 19, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Benjamin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 54
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 54
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Lab ID Sample ID Matrix Date Collected Date Received
92241876001 B-1 Water 03/18/15 18:30 03/19/15 10:03
92241876002 B-2 6'-8'Solid 03/18/15 19:50 03/19/15 10:03
92241876003 B-3 22'-24'Solid 03/18/15 16:45 03/19/15 10:03
92241876004 B-4 18'-20'Solid 03/18/15 16:15 03/19/15 10:03
92241876005 B-8 Water 03/18/15 17:45 03/19/15 10:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 54
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92241876001 B-1 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
92241876002 B-2 6'-8'EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CSLJ
92241876003 B-3 22'-24'EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CSLJ
92241876004 B-4 18'-20'EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CSLJ
92241876005 B-8 EPA 8270 74 PASI-CBPJ
EPA 8260 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-1 Lab ID: 92241876001 Collected: 03/18/15 18:30 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/24/15 16:50 83-32-903/24/15 07:0010.0 1.1 1
Acenaphthylene ND ug/L 03/24/15 16:50 208-96-803/24/15 07:0010.0 0.99 1
Aniline ND ug/L 03/24/15 16:50 62-53-303/24/15 07:0010.0 0.80 1
Anthracene ND ug/L 03/24/15 16:50 120-12-703/24/15 07:0010.0 0.47 1
Benzo(a)anthracene ND ug/L 03/24/15 16:50 56-55-303/24/15 07:0010.0 0.47 1
Benzo(a)pyrene ND ug/L 03/24/15 16:50 50-32-803/24/15 07:0010.0 0.57 1
Benzo(b)fluoranthene ND ug/L 03/24/15 16:50 205-99-203/24/15 07:0010.0 0.44 1
Benzo(g,h,i)perylene ND ug/L 03/24/15 16:50 191-24-203/24/15 07:0010.0 0.45 1
Benzo(k)fluoranthene ND ug/L 03/24/15 16:50 207-08-903/24/15 07:0010.0 0.53 1
Benzoic Acid ND ug/L 03/24/15 16:50 65-85-003/24/15 07:0050.0 4.9 1
Benzyl alcohol ND ug/L 03/24/15 16:50 100-51-603/24/15 07:0020.0 2.1 1
4-Bromophenylphenyl ether ND ug/L 03/24/15 16:50 101-55-303/24/15 07:0010.0 1.0 1
Butylbenzylphthalate ND ug/L 03/24/15 16:50 85-68-703/24/15 07:0010.0 0.48 1
4-Chloro-3-methylphenol ND ug/L 03/24/15 16:50 59-50-703/24/15 07:0020.0 2.0 1
4-Chloroaniline ND ug/L 03/24/15 16:50 106-47-803/24/15 07:0020.0 1.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/24/15 16:50 111-91-103/24/15 07:0010.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 03/24/15 16:50 111-44-403/24/15 07:0010.0 0.89 1
bis(2-Chloroisopropyl) ether ND ug/L 03/24/15 16:50 108-60-103/24/15 07:0010.0 0.86 1
2-Chloronaphthalene ND ug/L 03/24/15 16:50 91-58-703/24/15 07:0010.0 1.0 1
2-Chlorophenol ND ug/L 03/24/15 16:50 95-57-803/24/15 07:0010.0 1.0 1
4-Chlorophenylphenyl ether ND ug/L 03/24/15 16:50 7005-72-303/24/15 07:0010.0 1.1 1
Chrysene ND ug/L 03/24/15 16:50 218-01-903/24/15 07:0010.0 0.49 1
Dibenz(a,h)anthracene ND ug/L 03/24/15 16:50 53-70-303/24/15 07:0010.0 0.49 1
Dibenzofuran ND ug/L 03/24/15 16:50 132-64-903/24/15 07:0010.0 1.0 1
1,2-Dichlorobenzene ND ug/L 03/24/15 16:50 95-50-103/24/15 07:0010.0 0.71 1
1,3-Dichlorobenzene ND ug/L 03/24/15 16:50 541-73-103/24/15 07:0010.0 0.78 1
1,4-Dichlorobenzene ND ug/L 03/24/15 16:50 106-46-703/24/15 07:0010.0 0.81 1
3,3'-Dichlorobenzidine ND ug/L 03/24/15 16:50 91-94-103/24/15 07:0020.0 0.69 1
2,4-Dichlorophenol ND ug/L 03/24/15 16:50 120-83-203/24/15 07:0010.0 0.85 1
Diethylphthalate ND ug/L 03/24/15 16:50 84-66-203/24/15 07:0010.0 0.91 1
2,4-Dimethylphenol ND ug/L 03/24/15 16:50 105-67-903/24/15 07:0010.0 0.96 1
Dimethylphthalate ND ug/L 03/24/15 16:50 131-11-303/24/15 07:0010.0 0.62 1
Di-n-butylphthalate ND ug/L 03/24/15 16:50 84-74-203/24/15 07:0010.0 0.37 1
4,6-Dinitro-2-methylphenol ND ug/L 03/24/15 16:50 534-52-103/24/15 07:0020.0 1.1 1
2,4-Dinitrophenol ND ug/L 03/24/15 16:50 51-28-503/24/15 07:0050.0 2.5 1
2,4-Dinitrotoluene ND ug/L 03/24/15 16:50 121-14-203/24/15 07:0010.0 0.92 1
2,6-Dinitrotoluene ND ug/L 03/24/15 16:50 606-20-203/24/15 07:0010.0 2.1 1
Di-n-octylphthalate ND ug/L 03/24/15 16:50 117-84-003/24/15 07:0010.0 0.12 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/24/15 16:50 117-81-703/24/15 07:006.0 0.49 1
Fluoranthene ND ug/L 03/24/15 16:50 206-44-003/24/15 07:0010.0 0.41 1
Fluorene ND ug/L 03/24/15 16:50 86-73-703/24/15 07:0010.0 1.0 1
Hexachloro-1,3-butadiene ND ug/L 03/24/15 16:50 87-68-303/24/15 07:0010.0 0.90 1
Hexachlorobenzene ND ug/L 03/24/15 16:50 118-74-103/24/15 07:0010.0 0.76 1
Hexachlorocyclopentadiene ND ug/L 03/24/15 16:50 77-47-403/24/15 07:0010.0 1.1 1
Hexachloroethane ND ug/L 03/24/15 16:50 67-72-103/24/15 07:0010.0 0.90 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/24/15 16:50 193-39-503/24/15 07:0010.0 0.53 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-1 Lab ID: 92241876001 Collected: 03/18/15 18:30 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Isophorone ND ug/L 03/24/15 16:50 78-59-103/24/15 07:0010.0 0.92 1
1-Methylnaphthalene ND ug/L 03/24/15 16:50 90-12-003/24/15 07:0010.0 0.92 1
2-Methylnaphthalene ND ug/L 03/24/15 16:50 91-57-603/24/15 07:0010.0 1.0 1
2-Methylphenol(o-Cresol)ND ug/L 03/24/15 16:50 95-48-703/24/15 07:0010.0 1.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/24/15 16:5003/24/15 07:0010.0 1.0 1
Naphthalene ND ug/L 03/24/15 16:50 91-20-303/24/15 07:0010.0 0.93 1
2-Nitroaniline ND ug/L 03/24/15 16:50 88-74-403/24/15 07:0050.0 1.5 1
3-Nitroaniline ND ug/L 03/24/15 16:50 99-09-203/24/15 07:0050.0 1.3 1
4-Nitroaniline ND ug/L 03/24/15 16:50 100-01-603/24/15 07:0020.0 1.6 1
Nitrobenzene ND ug/L 03/24/15 16:50 98-95-303/24/15 07:0010.0 1.0 1
2-Nitrophenol ND ug/L 03/24/15 16:50 88-75-503/24/15 07:0010.0 0.71 1
4-Nitrophenol ND ug/L 03/24/15 16:50 100-02-703/24/15 07:0050.0 3.9 1
N-Nitrosodimethylamine ND ug/L 03/24/15 16:50 62-75-903/24/15 07:0010.0 0.94 1
N-Nitroso-di-n-propylamine ND ug/L 03/24/15 16:50 621-64-703/24/15 07:0010.0 0.85 1
N-Nitrosodiphenylamine ND ug/L 03/24/15 16:50 86-30-603/24/15 07:0010.0 0.64 1
Pentachlorophenol ND ug/L 03/24/15 16:50 87-86-503/24/15 07:0025.0 1.2 1
Phenanthrene ND ug/L 03/24/15 16:50 85-01-803/24/15 07:0010.0 0.53 1
Phenol ND ug/L 03/24/15 16:50 108-95-203/24/15 07:0010.0 1.1 1
Pyrene ND ug/L 03/24/15 16:50 129-00-003/24/15 07:0010.0 0.49 1
1,2,4-Trichlorobenzene ND ug/L 03/24/15 16:50 120-82-103/24/15 07:0010.0 1.3 1
2,4,5-Trichlorophenol ND ug/L 03/24/15 16:50 95-95-403/24/15 07:0010.0 1.0 1
2,4,6-Trichlorophenol ND ug/L 03/24/15 16:50 88-06-203/24/15 07:0010.0 0.85 1
Surrogates
Nitrobenzene-d5 (S)73 %03/24/15 16:50 4165-60-003/24/15 07:0021-110 1
2-Fluorobiphenyl (S)80 %03/24/15 16:50 321-60-803/24/15 07:0027-110 1
Terphenyl-d14 (S)98 %03/24/15 16:50 1718-51-003/24/15 07:0031-107 1
Phenol-d6 (S)29 %03/24/15 16:50 13127-88-303/24/15 07:0010-110 1
2-Fluorophenol (S)40 %03/24/15 16:50 367-12-403/24/15 07:0012-110 1
2,4,6-Tribromophenol (S)100 %03/24/15 16:50 118-79-603/24/15 07:0027-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/26/15 04:48 67-64-125.0 10.0 1
Benzene ND ug/L 03/26/15 04:48 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/26/15 04:48 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/26/15 04:48 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/26/15 04:48 75-27-41.0 0.18 1
Bromoform ND ug/L 03/26/15 04:48 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/26/15 04:48 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/26/15 04:48 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/26/15 04:48 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/26/15 04:48 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/26/15 04:48 75-00-31.0 0.54 1
Chloroform ND ug/L 03/26/15 04:48 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/26/15 04:48 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/26/15 04:48 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/26/15 04:48 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-1 Lab ID: 92241876001 Collected: 03/18/15 18:30 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/26/15 04:48 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/26/15 04:48 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/26/15 04:48 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/26/15 04:48 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/26/15 04:48 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/26/15 04:48 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/26/15 04:48 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/26/15 04:48 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/26/15 04:48 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/26/15 04:48 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/26/15 04:48 75-35-41.0 0.56 1
cis-1,2-Dichloroethene 4.2 ug/L 03/26/15 04:48 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/26/15 04:48 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/26/15 04:48 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/26/15 04:48 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/26/15 04:48 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/26/15 04:48 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/26/15 04:48 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/26/15 04:48 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/26/15 04:48 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/26/15 04:48 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/26/15 04:48 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/26/15 04:48 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/26/15 04:48 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/26/15 04:48 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/26/15 04:48 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/26/15 04:48 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/26/15 04:48 91-20-31.0 0.24 1
Styrene ND ug/L 03/26/15 04:48 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/26/15 04:48 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/26/15 04:48 79-34-51.0 0.40 1
Tetrachloroethene 94.1 ug/L 03/26/15 04:48 127-18-41.0 0.46 1
Toluene 0.48J ug/L 03/26/15 04:48 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/26/15 04:48 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/26/15 04:48 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/26/15 04:48 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/26/15 04:48 79-00-51.0 0.29 1
Trichloroethene 1.0 ug/L 03/26/15 04:48 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/26/15 04:48 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/26/15 04:48 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/26/15 04:48 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/26/15 04:48 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/26/15 04:48 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/26/15 04:48 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/26/15 04:48 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-1 Lab ID: 92241876001 Collected: 03/18/15 18:30 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)111 %03/26/15 04:48 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/26/15 04:48 17060-07-070-130 1
Toluene-d8 (S)96 %03/26/15 04:48 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-2 6'-8'Lab ID: 92241876002 Collected: 03/18/15 19:50 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 03/25/15 16:30 83-32-903/23/15 10:304671081
Acenaphthylene ND ug/kg 03/25/15 16:30 208-96-803/23/15 10:304671101
Aniline ND ug/kg 03/25/15 16:30 62-53-303/23/15 10:304671261
Anthracene ND ug/kg 03/25/15 16:30 120-12-703/23/15 10:304671051
Benzo(a)anthracene ND ug/kg 03/25/15 16:30 56-55-303/23/15 10:3046786.3 1
Benzo(a)pyrene ND ug/kg 03/25/15 16:30 50-32-803/23/15 10:3046789.2 1
Benzo(b)fluoranthene ND ug/kg 03/25/15 16:30 205-99-203/23/15 10:3046780.7 1
Benzo(g,h,i)perylene ND ug/kg 03/25/15 16:30 191-24-203/23/15 10:304671191
Benzo(k)fluoranthene ND ug/kg 03/25/15 16:30 207-08-903/23/15 10:3046792.0 1
Benzoic Acid ND ug/kg 03/25/15 16:30 65-85-003/23/15 10:30233084.9 1
Benzyl alcohol ND ug/kg 03/25/15 16:30 100-51-603/23/15 10:3093493.4 1
4-Bromophenylphenyl ether ND ug/kg 03/25/15 16:30 101-55-303/23/15 10:3046784.9 1
Butylbenzylphthalate ND ug/kg 03/25/15 16:30 85-68-703/23/15 10:3046799.1 1
4-Chloro-3-methylphenol ND ug/kg 03/25/15 16:30 59-50-703/23/15 10:3093496.2 1
4-Chloroaniline ND ug/kg 03/25/15 16:30 106-47-803/23/15 10:3023301301
bis(2-Chloroethoxy)methane ND ug/kg 03/25/15 16:30 111-91-103/23/15 10:304671091
bis(2-Chloroethyl) ether ND ug/kg 03/25/15 16:30 111-44-403/23/15 10:304671191
bis(2-Chloroisopropyl) ether ND ug/kg 03/25/15 16:30 108-60-103/23/15 10:304671251
2-Chloronaphthalene ND ug/kg 03/25/15 16:30 91-58-703/23/15 10:3046792.0 1
2-Chlorophenol ND ug/kg 03/25/15 16:30 95-57-803/23/15 10:304671271
4-Chlorophenylphenyl ether ND ug/kg 03/25/15 16:30 7005-72-303/23/15 10:3046796.2 1
Chrysene ND ug/kg 03/25/15 16:30 218-01-903/23/15 10:3046762.3 1
Dibenz(a,h)anthracene ND ug/kg 03/25/15 16:30 53-70-303/23/15 10:3046799.1 1
Dibenzofuran ND ug/kg 03/25/15 16:30 132-64-903/23/15 10:3046776.4 1
1,2-Dichlorobenzene ND ug/kg 03/25/15 16:30 95-50-103/23/15 10:304671251
1,3-Dichlorobenzene ND ug/kg 03/25/15 16:30 541-73-103/23/15 10:304671061
1,4-Dichlorobenzene ND ug/kg 03/25/15 16:30 106-46-703/23/15 10:304671321
3,3'-Dichlorobenzidine ND ug/kg 03/25/15 16:30 91-94-103/23/15 10:3023301021
2,4-Dichlorophenol ND ug/kg 03/25/15 16:30 120-83-203/23/15 10:304671021
Diethylphthalate ND ug/kg 03/25/15 16:30 84-66-203/23/15 10:3046772.2 1
2,4-Dimethylphenol ND ug/kg 03/25/15 16:30 105-67-903/23/15 10:304671841
Dimethylphthalate ND ug/kg 03/25/15 16:30 131-11-303/23/15 10:3046794.8 1
Di-n-butylphthalate ND ug/kg 03/25/15 16:30 84-74-203/23/15 10:3046776.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/25/15 16:30 534-52-103/23/15 10:3093493.4 1
2,4-Dinitrophenol ND ug/kg 03/25/15 16:30 51-28-503/23/15 10:30233076.4 1
2,4-Dinitrotoluene ND ug/kg 03/25/15 16:30 121-14-203/23/15 10:3046787.7 1
2,6-Dinitrotoluene ND ug/kg 03/25/15 16:30 606-20-203/23/15 10:3046797.6 1
Di-n-octylphthalate ND ug/kg 03/25/15 16:30 117-84-003/23/15 10:3046797.6 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/25/15 16:30 117-81-703/23/15 10:304671271
Fluoranthene ND ug/kg 03/25/15 16:30 206-44-003/23/15 10:3046767.9 1
Fluorene ND ug/kg 03/25/15 16:30 86-73-703/23/15 10:3046796.2 1
Hexachloro-1,3-butadiene ND ug/kg 03/25/15 16:30 87-68-303/23/15 10:3046780.7 1
Hexachlorobenzene ND ug/kg 03/25/15 16:30 118-74-103/23/15 10:3046759.4 1
Hexachlorocyclopentadiene ND ug/kg 03/25/15 16:30 77-47-403/23/15 10:3046786.3 1
Hexachloroethane ND ug/kg 03/25/15 16:30 67-72-103/23/15 10:304671231
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-2 6'-8'Lab ID: 92241876002 Collected: 03/18/15 19:50 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 03/25/15 16:30 193-39-503/23/15 10:3046796.2 1
Isophorone ND ug/kg 03/25/15 16:30 78-59-103/23/15 10:304671051
1-Methylnaphthalene ND ug/kg 03/25/15 16:30 90-12-003/23/15 10:304671221
2-Methylnaphthalene ND ug/kg 03/25/15 16:30 91-57-603/23/15 10:304671001
2-Methylphenol(o-Cresol)ND ug/kg 03/25/15 16:30 95-48-703/23/15 10:304671421
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/25/15 16:3003/23/15 10:304671841
Naphthalene ND ug/kg 03/25/15 16:30 91-20-303/23/15 10:304671151
2-Nitroaniline ND ug/kg 03/25/15 16:30 88-74-403/23/15 10:3023301441
3-Nitroaniline ND ug/kg 03/25/15 16:30 99-09-203/23/15 10:3023301271
4-Nitroaniline ND ug/kg 03/25/15 16:30 100-01-603/23/15 10:309341321
Nitrobenzene ND ug/kg 03/25/15 16:30 98-95-303/23/15 10:304671271
2-Nitrophenol ND ug/kg 03/25/15 16:30 88-75-503/23/15 10:304671131
4-Nitrophenol ND ug/kg 03/25/15 16:30 100-02-703/23/15 10:30233083.5 1
N-Nitrosodimethylamine ND ug/kg 03/25/15 16:30 62-75-903/23/15 10:304671511
N-Nitroso-di-n-propylamine ND ug/kg 03/25/15 16:30 621-64-703/23/15 10:3046789.2 1
N-Nitrosodiphenylamine ND ug/kg 03/25/15 16:30 86-30-603/23/15 10:304671391
Pentachlorophenol ND ug/kg 03/25/15 16:30 87-86-503/23/15 10:30233084.9 1
Phenanthrene ND ug/kg 03/25/15 16:30 85-01-803/23/15 10:3046777.8 1
Phenol ND ug/kg 03/25/15 16:30 108-95-203/23/15 10:304671401
Pyrene ND ug/kg 03/25/15 16:30 129-00-003/23/15 10:3046779.2 1
1,2,4-Trichlorobenzene ND ug/kg 03/25/15 16:30 120-82-103/23/15 10:3046790.6 1
2,4,5-Trichlorophenol ND ug/kg 03/25/15 16:30 95-95-403/23/15 10:304671441
2,4,6-Trichlorophenol ND ug/kg 03/25/15 16:30 88-06-203/23/15 10:304671031
Surrogates
Nitrobenzene-d5 (S)68 %03/25/15 16:30 4165-60-003/23/15 10:3023-110 1
2-Fluorobiphenyl (S)68 %03/25/15 16:30 321-60-803/23/15 10:3030-110 1
Terphenyl-d14 (S)72 %03/25/15 16:30 1718-51-003/23/15 10:3028-110 1
Phenol-d6 (S)25 %03/25/15 16:30 13127-88-303/23/15 10:3022-110 1
2-Fluorophenol (S)18 %03/25/15 16:30 367-12-403/23/15 10:3013-110 1
2,4,6-Tribromophenol (S)29 %03/25/15 16:30 118-79-603/23/15 10:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/22/15 19:44 67-64-114214.2 1
Benzene ND ug/kg 03/22/15 19:44 71-43-27.1 2.3 1
Bromobenzene ND ug/kg 03/22/15 19:44 108-86-17.1 2.8 1
Bromochloromethane ND ug/kg 03/22/15 19:44 74-97-57.1 2.4 1
Bromodichloromethane ND ug/kg 03/22/15 19:44 75-27-47.1 2.7 1
Bromoform ND ug/kg 03/22/15 19:44 75-25-27.1 3.3 1
Bromomethane ND ug/kg 03/22/15 19:44 74-83-914.2 3.5 1
2-Butanone (MEK)ND ug/kg 03/22/15 19:44 78-93-31424.1 1
n-Butylbenzene ND ug/kg 03/22/15 19:44 104-51-87.1 2.5 1
sec-Butylbenzene ND ug/kg 03/22/15 19:44 135-98-87.1 2.3 1
tert-Butylbenzene ND ug/kg 03/22/15 19:44 98-06-67.1 2.8 1
Carbon tetrachloride ND ug/kg 03/22/15 19:44 56-23-57.1 3.7 1
Chlorobenzene ND ug/kg 03/22/15 19:44 108-90-77.1 2.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-2 6'-8'Lab ID: 92241876002 Collected: 03/18/15 19:50 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 03/22/15 19:44 75-00-314.2 3.4 1
Chloroform ND ug/kg 03/22/15 19:44 67-66-37.1 2.3 1
Chloromethane ND ug/kg 03/22/15 19:44 74-87-314.2 3.4 1
2-Chlorotoluene ND ug/kg 03/22/15 19:44 95-49-87.1 2.4 1
4-Chlorotoluene ND ug/kg 03/22/15 19:44 106-43-47.1 2.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/15 19:44 96-12-87.1 5.1 1
Dibromochloromethane ND ug/kg 03/22/15 19:44 124-48-17.1 2.5 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/15 19:44 106-93-47.1 2.5 1
Dibromomethane ND ug/kg 03/22/15 19:44 74-95-37.1 3.5 1
1,2-Dichlorobenzene ND ug/kg 03/22/15 19:44 95-50-17.1 2.7 1
1,3-Dichlorobenzene ND ug/kg 03/22/15 19:44 541-73-17.1 2.8 1
1,4-Dichlorobenzene ND ug/kg 03/22/15 19:44 106-46-77.1 2.4 1
Dichlorodifluoromethane ND ug/kg 03/22/15 19:44 75-71-814.2 5.1 1
1,1-Dichloroethane ND ug/kg 03/22/15 19:44 75-34-37.1 2.1 1
1,2-Dichloroethane ND ug/kg 03/22/15 19:44 107-06-27.1 3.1 1
1,1-Dichloroethene ND ug/kg 03/22/15 19:44 75-35-47.1 2.5 1
cis-1,2-Dichloroethene ND ug/kg 03/22/15 19:44 156-59-27.1 2.0 1
trans-1,2-Dichloroethene ND ug/kg 03/22/15 19:44 156-60-57.1 2.7 1
1,2-Dichloropropane ND ug/kg 03/22/15 19:44 78-87-57.1 2.4 1
1,3-Dichloropropane ND ug/kg 03/22/15 19:44 142-28-97.1 2.7 1
2,2-Dichloropropane ND ug/kg 03/22/15 19:44 594-20-77.1 2.4 1
1,1-Dichloropropene ND ug/kg 03/22/15 19:44 563-58-67.1 2.1 1
cis-1,3-Dichloropropene ND ug/kg 03/22/15 19:44 10061-01-57.1 2.5 1
trans-1,3-Dichloropropene ND ug/kg 03/22/15 19:44 10061-02-67.1 2.1 1
Diisopropyl ether ND ug/kg 03/22/15 19:44 108-20-37.1 2.4 1
Ethylbenzene ND ug/kg 03/22/15 19:44 100-41-47.1 2.5 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/15 19:44 87-68-37.1 2.8 1
2-Hexanone ND ug/kg 03/22/15 19:44 591-78-670.8 5.5 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/15 19:44 98-82-87.1 2.7 1
p-Isopropyltoluene ND ug/kg 03/22/15 19:44 99-87-67.1 2.4 1
Methylene Chloride ND ug/kg 03/22/15 19:44 75-09-228.3 4.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/15 19:44 108-10-170.8 5.2 1
Methyl-tert-butyl ether ND ug/kg 03/22/15 19:44 1634-04-47.1 2.1 1
Naphthalene ND ug/kg 03/22/15 19:44 91-20-37.1 1.7 1
n-Propylbenzene ND ug/kg 03/22/15 19:44 103-65-17.1 2.4 1
Styrene ND ug/kg 03/22/15 19:44 100-42-57.1 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/15 19:44 630-20-67.1 3.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/15 19:44 79-34-57.1 2.7 1
Tetrachloroethene ND ug/kg 03/22/15 19:44 127-18-47.1 2.4 1
Toluene ND ug/kg 03/22/15 19:44 108-88-37.1 2.5 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/15 19:44 87-61-67.1 3.1 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/15 19:44 120-82-17.1 2.3 1
1,1,1-Trichloroethane ND ug/kg 03/22/15 19:44 71-55-67.1 2.5 1
1,1,2-Trichloroethane ND ug/kg 03/22/15 19:44 79-00-57.1 3.0 1
Trichloroethene ND ug/kg 03/22/15 19:44 79-01-67.1 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-2 6'-8'Lab ID: 92241876002 Collected: 03/18/15 19:50 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 03/22/15 19:44 75-69-47.1 3.1 1
1,2,3-Trichloropropane ND ug/kg 03/22/15 19:44 96-18-47.1 2.3 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/15 19:44 95-63-67.1 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/15 19:44 108-67-87.1 2.5 1
Vinyl acetate ND ug/kg 03/22/15 19:44 108-05-4 M170.8 12.5 1
Vinyl chloride ND ug/kg 03/22/15 19:44 75-01-414.2 2.5 1
Xylene (Total)ND ug/kg 03/22/15 19:44 1330-20-714.2 5.1 1
m&p-Xylene ND ug/kg 03/22/15 19:44 179601-23-114.2 5.1 1
o-Xylene ND ug/kg 03/22/15 19:44 95-47-67.1 2.7 1
Surrogates
Toluene-d8 (S)103 %03/22/15 19:44 2037-26-570-130 1
4-Bromofluorobenzene (S)97 %03/22/15 19:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %03/22/15 19:44 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 29.3 %03/23/15 10:260.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-3 22'-24'Lab ID: 92241876003 Collected: 03/18/15 16:45 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 03/25/15 17:02 83-32-903/23/15 10:3037586.4 1
Acenaphthylene ND ug/kg 03/25/15 17:02 208-96-803/23/15 10:3037588.6 1
Aniline ND ug/kg 03/25/15 17:02 62-53-303/23/15 10:303751011
Anthracene ND ug/kg 03/25/15 17:02 120-12-703/23/15 10:3037584.1 1
Benzo(a)anthracene ND ug/kg 03/25/15 17:02 56-55-303/23/15 10:3037569.3 1
Benzo(a)pyrene ND ug/kg 03/25/15 17:02 50-32-803/23/15 10:3037571.6 1
Benzo(b)fluoranthene ND ug/kg 03/25/15 17:02 205-99-2 R103/23/15 10:3037564.8 1
Benzo(g,h,i)perylene ND ug/kg 03/25/15 17:02 191-24-2 R103/23/15 10:3037595.4 1
Benzo(k)fluoranthene ND ug/kg 03/25/15 17:02 207-08-903/23/15 10:3037573.9 1
Benzoic Acid ND ug/kg 03/25/15 17:02 65-85-003/23/15 10:30187068.2 1
Benzyl alcohol ND ug/kg 03/25/15 17:02 100-51-603/23/15 10:3075075.0 1
4-Bromophenylphenyl ether ND ug/kg 03/25/15 17:02 101-55-303/23/15 10:3037568.2 1
Butylbenzylphthalate ND ug/kg 03/25/15 17:02 85-68-703/23/15 10:3037579.5 1
4-Chloro-3-methylphenol ND ug/kg 03/25/15 17:02 59-50-703/23/15 10:3075077.3 1
4-Chloroaniline ND ug/kg 03/25/15 17:02 106-47-803/23/15 10:3018701051
bis(2-Chloroethoxy)methane ND ug/kg 03/25/15 17:02 111-91-103/23/15 10:3037587.5 1
bis(2-Chloroethyl) ether ND ug/kg 03/25/15 17:02 111-44-403/23/15 10:3037595.4 1
bis(2-Chloroisopropyl) ether ND ug/kg 03/25/15 17:02 108-60-103/23/15 10:303751001
2-Chloronaphthalene ND ug/kg 03/25/15 17:02 91-58-7 R103/23/15 10:3037573.9 1
2-Chlorophenol ND ug/kg 03/25/15 17:02 95-57-803/23/15 10:303751021
4-Chlorophenylphenyl ether ND ug/kg 03/25/15 17:02 7005-72-303/23/15 10:3037577.3 1
Chrysene ND ug/kg 03/25/15 17:02 218-01-903/23/15 10:3037550.0 1
Dibenz(a,h)anthracene ND ug/kg 03/25/15 17:02 53-70-3 R103/23/15 10:3037579.5 1
Dibenzofuran ND ug/kg 03/25/15 17:02 132-64-903/23/15 10:3037561.4 1
1,2-Dichlorobenzene ND ug/kg 03/25/15 17:02 95-50-103/23/15 10:303751001
1,3-Dichlorobenzene ND ug/kg 03/25/15 17:02 541-73-103/23/15 10:3037585.2 1
1,4-Dichlorobenzene ND ug/kg 03/25/15 17:02 106-46-703/23/15 10:303751061
3,3'-Dichlorobenzidine ND ug/kg 03/25/15 17:02 91-94-103/23/15 10:30187081.8 1
2,4-Dichlorophenol ND ug/kg 03/25/15 17:02 120-83-203/23/15 10:3037581.8 1
Diethylphthalate ND ug/kg 03/25/15 17:02 84-66-203/23/15 10:3037557.9 1
2,4-Dimethylphenol ND ug/kg 03/25/15 17:02 105-67-903/23/15 10:303751481
Dimethylphthalate ND ug/kg 03/25/15 17:02 131-11-303/23/15 10:3037576.1 1
Di-n-butylphthalate ND ug/kg 03/25/15 17:02 84-74-203/23/15 10:3037561.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/25/15 17:02 534-52-103/23/15 10:3075075.0 1
2,4-Dinitrophenol ND ug/kg 03/25/15 17:02 51-28-503/23/15 10:30187061.4 1
2,4-Dinitrotoluene ND ug/kg 03/25/15 17:02 121-14-203/23/15 10:3037570.4 1
2,6-Dinitrotoluene ND ug/kg 03/25/15 17:02 606-20-203/23/15 10:3037578.4 1
Di-n-octylphthalate ND ug/kg 03/25/15 17:02 117-84-003/23/15 10:3037578.4 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/25/15 17:02 117-81-703/23/15 10:303751021
Fluoranthene ND ug/kg 03/25/15 17:02 206-44-003/23/15 10:3037554.5 1
Fluorene ND ug/kg 03/25/15 17:02 86-73-703/23/15 10:3037577.3 1
Hexachloro-1,3-butadiene ND ug/kg 03/25/15 17:02 87-68-303/23/15 10:3037564.8 1
Hexachlorobenzene ND ug/kg 03/25/15 17:02 118-74-103/23/15 10:3037547.7 1
Hexachlorocyclopentadiene ND ug/kg 03/25/15 17:02 77-47-4 R103/23/15 10:3037569.3 1
Hexachloroethane ND ug/kg 03/25/15 17:02 67-72-103/23/15 10:3037598.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-3 22'-24'Lab ID: 92241876003 Collected: 03/18/15 16:45 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 03/25/15 17:02 193-39-5 R103/23/15 10:3037577.3 1
Isophorone ND ug/kg 03/25/15 17:02 78-59-103/23/15 10:3037584.1 1
1-Methylnaphthalene ND ug/kg 03/25/15 17:02 90-12-0 R103/23/15 10:3037597.7 1
2-Methylnaphthalene ND ug/kg 03/25/15 17:02 91-57-6 R103/23/15 10:3037580.7 1
2-Methylphenol(o-Cresol)ND ug/kg 03/25/15 17:02 95-48-703/23/15 10:303751141
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/25/15 17:0203/23/15 10:303751481
Naphthalene ND ug/kg 03/25/15 17:02 91-20-303/23/15 10:3037592.0 1
2-Nitroaniline ND ug/kg 03/25/15 17:02 88-74-403/23/15 10:3018701161
3-Nitroaniline ND ug/kg 03/25/15 17:02 99-09-203/23/15 10:3018701021
4-Nitroaniline ND ug/kg 03/25/15 17:02 100-01-603/23/15 10:307501061
Nitrobenzene ND ug/kg 03/25/15 17:02 98-95-303/23/15 10:303751021
2-Nitrophenol ND ug/kg 03/25/15 17:02 88-75-503/23/15 10:3037590.9 1
4-Nitrophenol ND ug/kg 03/25/15 17:02 100-02-703/23/15 10:30187067.0 1
N-Nitrosodimethylamine ND ug/kg 03/25/15 17:02 62-75-903/23/15 10:303751221
N-Nitroso-di-n-propylamine ND ug/kg 03/25/15 17:02 621-64-703/23/15 10:3037571.6 1
N-Nitrosodiphenylamine ND ug/kg 03/25/15 17:02 86-30-603/23/15 10:303751111
Pentachlorophenol ND ug/kg 03/25/15 17:02 87-86-503/23/15 10:30187068.2 1
Phenanthrene ND ug/kg 03/25/15 17:02 85-01-803/23/15 10:3037562.5 1
Phenol ND ug/kg 03/25/15 17:02 108-95-203/23/15 10:303751121
Pyrene ND ug/kg 03/25/15 17:02 129-00-003/23/15 10:3037563.6 1
1,2,4-Trichlorobenzene ND ug/kg 03/25/15 17:02 120-82-103/23/15 10:3037572.7 1
2,4,5-Trichlorophenol ND ug/kg 03/25/15 17:02 95-95-4 R103/23/15 10:303751161
2,4,6-Trichlorophenol ND ug/kg 03/25/15 17:02 88-06-2 R103/23/15 10:3037582.9 1
Surrogates
Nitrobenzene-d5 (S)68 %03/25/15 17:02 4165-60-003/23/15 10:3023-110 1
2-Fluorobiphenyl (S)64 %03/25/15 17:02 321-60-803/23/15 10:3030-110 1
Terphenyl-d14 (S)82 %03/25/15 17:02 1718-51-003/23/15 10:3028-110 1
Phenol-d6 (S)65 %03/25/15 17:02 13127-88-303/23/15 10:3022-110 1
2-Fluorophenol (S)55 %03/25/15 17:02 367-12-403/23/15 10:3013-110 1
2,4,6-Tribromophenol (S)61 %03/25/15 17:02 118-79-603/23/15 10:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/22/15 20:04 67-64-179.2 7.9 1
Benzene ND ug/kg 03/22/15 20:04 71-43-24.0 1.3 1
Bromobenzene ND ug/kg 03/22/15 20:04 108-86-14.0 1.6 1
Bromochloromethane ND ug/kg 03/22/15 20:04 74-97-54.0 1.3 1
Bromodichloromethane ND ug/kg 03/22/15 20:04 75-27-44.0 1.5 1
Bromoform ND ug/kg 03/22/15 20:04 75-25-24.0 1.8 1
Bromomethane ND ug/kg 03/22/15 20:04 74-83-97.9 2.0 1
2-Butanone (MEK)ND ug/kg 03/22/15 20:04 78-93-379.2 2.3 1
n-Butylbenzene ND ug/kg 03/22/15 20:04 104-51-84.0 1.4 1
sec-Butylbenzene ND ug/kg 03/22/15 20:04 135-98-84.0 1.3 1
tert-Butylbenzene ND ug/kg 03/22/15 20:04 98-06-64.0 1.6 1
Carbon tetrachloride ND ug/kg 03/22/15 20:04 56-23-54.0 2.1 1
Chlorobenzene ND ug/kg 03/22/15 20:04 108-90-74.0 1.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-3 22'-24'Lab ID: 92241876003 Collected: 03/18/15 16:45 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 03/22/15 20:04 75-00-37.9 1.9 1
Chloroform ND ug/kg 03/22/15 20:04 67-66-34.0 1.3 1
Chloromethane ND ug/kg 03/22/15 20:04 74-87-37.9 1.9 1
2-Chlorotoluene ND ug/kg 03/22/15 20:04 95-49-84.0 1.3 1
4-Chlorotoluene ND ug/kg 03/22/15 20:04 106-43-44.0 1.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/15 20:04 96-12-84.0 2.9 1
Dibromochloromethane ND ug/kg 03/22/15 20:04 124-48-14.0 1.4 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/15 20:04 106-93-44.0 1.4 1
Dibromomethane ND ug/kg 03/22/15 20:04 74-95-34.0 2.0 1
1,2-Dichlorobenzene ND ug/kg 03/22/15 20:04 95-50-14.0 1.5 1
1,3-Dichlorobenzene ND ug/kg 03/22/15 20:04 541-73-14.0 1.6 1
1,4-Dichlorobenzene ND ug/kg 03/22/15 20:04 106-46-74.0 1.3 1
Dichlorodifluoromethane ND ug/kg 03/22/15 20:04 75-71-87.9 2.9 1
1,1-Dichloroethane ND ug/kg 03/22/15 20:04 75-34-34.0 1.2 1
1,2-Dichloroethane ND ug/kg 03/22/15 20:04 107-06-24.0 1.7 1
1,1-Dichloroethene ND ug/kg 03/22/15 20:04 75-35-44.0 1.4 1
cis-1,2-Dichloroethene ND ug/kg 03/22/15 20:04 156-59-24.0 1.1 1
trans-1,2-Dichloroethene ND ug/kg 03/22/15 20:04 156-60-54.0 1.5 1
1,2-Dichloropropane ND ug/kg 03/22/15 20:04 78-87-54.0 1.3 1
1,3-Dichloropropane ND ug/kg 03/22/15 20:04 142-28-94.0 1.5 1
2,2-Dichloropropane ND ug/kg 03/22/15 20:04 594-20-74.0 1.3 1
1,1-Dichloropropene ND ug/kg 03/22/15 20:04 563-58-64.0 1.2 1
cis-1,3-Dichloropropene ND ug/kg 03/22/15 20:04 10061-01-54.0 1.4 1
trans-1,3-Dichloropropene ND ug/kg 03/22/15 20:04 10061-02-64.0 1.2 1
Diisopropyl ether ND ug/kg 03/22/15 20:04 108-20-34.0 1.3 1
Ethylbenzene ND ug/kg 03/22/15 20:04 100-41-44.0 1.4 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/15 20:04 87-68-34.0 1.6 1
2-Hexanone ND ug/kg 03/22/15 20:04 591-78-639.6 3.1 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/15 20:04 98-82-84.0 1.5 1
p-Isopropyltoluene ND ug/kg 03/22/15 20:04 99-87-64.0 1.3 1
Methylene Chloride ND ug/kg 03/22/15 20:04 75-09-215.8 2.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/15 20:04 108-10-139.6 2.9 1
Methyl-tert-butyl ether ND ug/kg 03/22/15 20:04 1634-04-44.0 1.2 1
Naphthalene ND ug/kg 03/22/15 20:04 91-20-34.0 0.95 1
n-Propylbenzene ND ug/kg 03/22/15 20:04 103-65-14.0 1.3 1
Styrene ND ug/kg 03/22/15 20:04 100-42-54.0 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/15 20:04 630-20-64.0 1.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/15 20:04 79-34-54.0 1.5 1
Tetrachloroethene ND ug/kg 03/22/15 20:04 127-18-44.0 1.3 1
Toluene ND ug/kg 03/22/15 20:04 108-88-34.0 1.4 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/15 20:04 87-61-64.0 1.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/15 20:04 120-82-14.0 1.3 1
1,1,1-Trichloroethane ND ug/kg 03/22/15 20:04 71-55-64.0 1.4 1
1,1,2-Trichloroethane ND ug/kg 03/22/15 20:04 79-00-54.0 1.7 1
Trichloroethene ND ug/kg 03/22/15 20:04 79-01-64.0 1.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-3 22'-24'Lab ID: 92241876003 Collected: 03/18/15 16:45 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 03/22/15 20:04 75-69-44.0 1.7 1
1,2,3-Trichloropropane ND ug/kg 03/22/15 20:04 96-18-44.0 1.3 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/15 20:04 95-63-64.0 1.6 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/15 20:04 108-67-84.0 1.4 1
Vinyl acetate ND ug/kg 03/22/15 20:04 108-05-439.6 7.0 1
Vinyl chloride ND ug/kg 03/22/15 20:04 75-01-47.9 1.4 1
Xylene (Total)ND ug/kg 03/22/15 20:04 1330-20-77.9 2.9 1
m&p-Xylene ND ug/kg 03/22/15 20:04 179601-23-17.9 2.9 1
o-Xylene ND ug/kg 03/22/15 20:04 95-47-64.0 1.5 1
Surrogates
Toluene-d8 (S)104 %03/22/15 20:04 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %03/22/15 20:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %03/22/15 20:04 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.0 %03/23/15 10:260.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-4 18'-20'Lab ID: 92241876004 Collected: 03/18/15 16:15 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND ug/kg 03/25/15 18:38 83-32-903/23/15 10:304761101
Acenaphthylene ND ug/kg 03/25/15 18:38 208-96-803/23/15 10:304761131
Aniline ND ug/kg 03/25/15 18:38 62-53-303/23/15 10:304761281
Anthracene ND ug/kg 03/25/15 18:38 120-12-703/23/15 10:304761071
Benzo(a)anthracene ND ug/kg 03/25/15 18:38 56-55-303/23/15 10:3047688.0 1
Benzo(a)pyrene ND ug/kg 03/25/15 18:38 50-32-803/23/15 10:3047690.9 1
Benzo(b)fluoranthene ND ug/kg 03/25/15 18:38 205-99-203/23/15 10:3047682.2 1
Benzo(g,h,i)perylene ND ug/kg 03/25/15 18:38 191-24-203/23/15 10:304761211
Benzo(k)fluoranthene ND ug/kg 03/25/15 18:38 207-08-903/23/15 10:3047693.8 1
Benzoic Acid ND ug/kg 03/25/15 18:38 65-85-003/23/15 10:30238086.5 1
Benzyl alcohol ND ug/kg 03/25/15 18:38 100-51-603/23/15 10:3095295.2 1
4-Bromophenylphenyl ether ND ug/kg 03/25/15 18:38 101-55-303/23/15 10:3047686.5 1
Butylbenzylphthalate ND ug/kg 03/25/15 18:38 85-68-703/23/15 10:304761011
4-Chloro-3-methylphenol ND ug/kg 03/25/15 18:38 59-50-703/23/15 10:3095298.1 1
4-Chloroaniline ND ug/kg 03/25/15 18:38 106-47-803/23/15 10:3023801331
bis(2-Chloroethoxy)methane ND ug/kg 03/25/15 18:38 111-91-103/23/15 10:304761111
bis(2-Chloroethyl) ether ND ug/kg 03/25/15 18:38 111-44-403/23/15 10:304761211
bis(2-Chloroisopropyl) ether ND ug/kg 03/25/15 18:38 108-60-103/23/15 10:304761271
2-Chloronaphthalene ND ug/kg 03/25/15 18:38 91-58-703/23/15 10:3047693.8 1
2-Chlorophenol ND ug/kg 03/25/15 18:38 95-57-803/23/15 10:304761301
4-Chlorophenylphenyl ether ND ug/kg 03/25/15 18:38 7005-72-303/23/15 10:3047698.1 1
Chrysene ND ug/kg 03/25/15 18:38 218-01-903/23/15 10:3047663.5 1
Dibenz(a,h)anthracene ND ug/kg 03/25/15 18:38 53-70-303/23/15 10:304761011
Dibenzofuran ND ug/kg 03/25/15 18:38 132-64-903/23/15 10:3047677.9 1
1,2-Dichlorobenzene ND ug/kg 03/25/15 18:38 95-50-103/23/15 10:304761271
1,3-Dichlorobenzene ND ug/kg 03/25/15 18:38 541-73-103/23/15 10:304761081
1,4-Dichlorobenzene ND ug/kg 03/25/15 18:38 106-46-703/23/15 10:304761341
3,3'-Dichlorobenzidine ND ug/kg 03/25/15 18:38 91-94-103/23/15 10:3023801041
2,4-Dichlorophenol ND ug/kg 03/25/15 18:38 120-83-203/23/15 10:304761041
Diethylphthalate ND ug/kg 03/25/15 18:38 84-66-203/23/15 10:3047673.6 1
2,4-Dimethylphenol ND ug/kg 03/25/15 18:38 105-67-903/23/15 10:304761881
Dimethylphthalate ND ug/kg 03/25/15 18:38 131-11-303/23/15 10:3047696.6 1
Di-n-butylphthalate ND ug/kg 03/25/15 18:38 84-74-203/23/15 10:3047677.9 1
4,6-Dinitro-2-methylphenol ND ug/kg 03/25/15 18:38 534-52-103/23/15 10:3095295.2 1
2,4-Dinitrophenol ND ug/kg 03/25/15 18:38 51-28-503/23/15 10:30238077.9 1
2,4-Dinitrotoluene ND ug/kg 03/25/15 18:38 121-14-203/23/15 10:3047689.4 1
2,6-Dinitrotoluene ND ug/kg 03/25/15 18:38 606-20-203/23/15 10:3047699.5 1
Di-n-octylphthalate ND ug/kg 03/25/15 18:38 117-84-003/23/15 10:3047699.5 1
bis(2-Ethylhexyl)phthalate ND ug/kg 03/25/15 18:38 117-81-703/23/15 10:304761301
Fluoranthene ND ug/kg 03/25/15 18:38 206-44-003/23/15 10:3047669.2 1
Fluorene ND ug/kg 03/25/15 18:38 86-73-703/23/15 10:3047698.1 1
Hexachloro-1,3-butadiene ND ug/kg 03/25/15 18:38 87-68-303/23/15 10:3047682.2 1
Hexachlorobenzene ND ug/kg 03/25/15 18:38 118-74-103/23/15 10:3047660.6 1
Hexachlorocyclopentadiene ND ug/kg 03/25/15 18:38 77-47-403/23/15 10:3047688.0 1
Hexachloroethane ND ug/kg 03/25/15 18:38 67-72-103/23/15 10:304761251
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-4 18'-20'Lab ID: 92241876004 Collected: 03/18/15 16:15 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 03/25/15 18:38 193-39-503/23/15 10:3047698.1 1
Isophorone ND ug/kg 03/25/15 18:38 78-59-103/23/15 10:304761071
1-Methylnaphthalene ND ug/kg 03/25/15 18:38 90-12-003/23/15 10:304761241
2-Methylnaphthalene ND ug/kg 03/25/15 18:38 91-57-603/23/15 10:304761021
2-Methylphenol(o-Cresol)ND ug/kg 03/25/15 18:38 95-48-703/23/15 10:304761441
3&4-Methylphenol(m&p Cresol)ND ug/kg 03/25/15 18:3803/23/15 10:304761881
Naphthalene ND ug/kg 03/25/15 18:38 91-20-303/23/15 10:304761171
2-Nitroaniline ND ug/kg 03/25/15 18:38 88-74-403/23/15 10:3023801471
3-Nitroaniline ND ug/kg 03/25/15 18:38 99-09-203/23/15 10:3023801301
4-Nitroaniline ND ug/kg 03/25/15 18:38 100-01-603/23/15 10:309521341
Nitrobenzene ND ug/kg 03/25/15 18:38 98-95-303/23/15 10:304761301
2-Nitrophenol ND ug/kg 03/25/15 18:38 88-75-503/23/15 10:304761151
4-Nitrophenol ND ug/kg 03/25/15 18:38 100-02-703/23/15 10:30238085.1 1
N-Nitrosodimethylamine ND ug/kg 03/25/15 18:38 62-75-903/23/15 10:304761541
N-Nitroso-di-n-propylamine ND ug/kg 03/25/15 18:38 621-64-703/23/15 10:3047690.9 1
N-Nitrosodiphenylamine ND ug/kg 03/25/15 18:38 86-30-603/23/15 10:304761411
Pentachlorophenol ND ug/kg 03/25/15 18:38 87-86-503/23/15 10:30238086.5 1
Phenanthrene ND ug/kg 03/25/15 18:38 85-01-803/23/15 10:3047679.3 1
Phenol ND ug/kg 03/25/15 18:38 108-95-203/23/15 10:304761431
Pyrene ND ug/kg 03/25/15 18:38 129-00-003/23/15 10:3047680.8 1
1,2,4-Trichlorobenzene ND ug/kg 03/25/15 18:38 120-82-103/23/15 10:3047692.3 1
2,4,5-Trichlorophenol ND ug/kg 03/25/15 18:38 95-95-403/23/15 10:304761471
2,4,6-Trichlorophenol ND ug/kg 03/25/15 18:38 88-06-203/23/15 10:304761051
Surrogates
Nitrobenzene-d5 (S)69 %03/25/15 18:38 4165-60-003/23/15 10:3023-110 1
2-Fluorobiphenyl (S)81 %03/25/15 18:38 321-60-803/23/15 10:3030-110 1
Terphenyl-d14 (S)50 %03/25/15 18:38 1718-51-003/23/15 10:3028-110 1
Phenol-d6 (S)45 %03/25/15 18:38 13127-88-303/23/15 10:3022-110 1
2-Fluorophenol (S)43 %03/25/15 18:38 367-12-403/23/15 10:3013-110 1
2,4,6-Tribromophenol (S)54 %03/25/15 18:38 118-79-603/23/15 10:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND ug/kg 03/22/15 20:24 67-64-112512.5 1
Benzene ND ug/kg 03/22/15 20:24 71-43-26.2 2.0 1
Bromobenzene ND ug/kg 03/22/15 20:24 108-86-16.2 2.5 1
Bromochloromethane ND ug/kg 03/22/15 20:24 74-97-56.2 2.1 1
Bromodichloromethane ND ug/kg 03/22/15 20:24 75-27-46.2 2.4 1
Bromoform ND ug/kg 03/22/15 20:24 75-25-26.2 2.9 1
Bromomethane ND ug/kg 03/22/15 20:24 74-83-912.5 3.1 1
2-Butanone (MEK)ND ug/kg 03/22/15 20:24 78-93-31253.6 1
n-Butylbenzene ND ug/kg 03/22/15 20:24 104-51-86.2 2.2 1
sec-Butylbenzene ND ug/kg 03/22/15 20:24 135-98-86.2 2.0 1
tert-Butylbenzene ND ug/kg 03/22/15 20:24 98-06-66.2 2.5 1
Carbon tetrachloride ND ug/kg 03/22/15 20:24 56-23-56.2 3.2 1
Chlorobenzene ND ug/kg 03/22/15 20:24 108-90-76.2 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-4 18'-20'Lab ID: 92241876004 Collected: 03/18/15 16:15 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Chloroethane ND ug/kg 03/22/15 20:24 75-00-312.5 3.0 1
Chloroform ND ug/kg 03/22/15 20:24 67-66-36.2 2.0 1
Chloromethane ND ug/kg 03/22/15 20:24 74-87-312.5 3.0 1
2-Chlorotoluene ND ug/kg 03/22/15 20:24 95-49-86.2 2.1 1
4-Chlorotoluene ND ug/kg 03/22/15 20:24 106-43-46.2 2.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 03/22/15 20:24 96-12-86.2 4.5 1
Dibromochloromethane ND ug/kg 03/22/15 20:24 124-48-16.2 2.2 1
1,2-Dibromoethane (EDB)ND ug/kg 03/22/15 20:24 106-93-46.2 2.2 1
Dibromomethane ND ug/kg 03/22/15 20:24 74-95-36.2 3.1 1
1,2-Dichlorobenzene ND ug/kg 03/22/15 20:24 95-50-16.2 2.4 1
1,3-Dichlorobenzene ND ug/kg 03/22/15 20:24 541-73-16.2 2.5 1
1,4-Dichlorobenzene ND ug/kg 03/22/15 20:24 106-46-76.2 2.1 1
Dichlorodifluoromethane ND ug/kg 03/22/15 20:24 75-71-812.5 4.5 1
1,1-Dichloroethane ND ug/kg 03/22/15 20:24 75-34-36.2 1.9 1
1,2-Dichloroethane ND ug/kg 03/22/15 20:24 107-06-26.2 2.7 1
1,1-Dichloroethene ND ug/kg 03/22/15 20:24 75-35-46.2 2.2 1
cis-1,2-Dichloroethene ND ug/kg 03/22/15 20:24 156-59-26.2 1.7 1
trans-1,2-Dichloroethene ND ug/kg 03/22/15 20:24 156-60-56.2 2.4 1
1,2-Dichloropropane ND ug/kg 03/22/15 20:24 78-87-56.2 2.1 1
1,3-Dichloropropane ND ug/kg 03/22/15 20:24 142-28-96.2 2.4 1
2,2-Dichloropropane ND ug/kg 03/22/15 20:24 594-20-76.2 2.1 1
1,1-Dichloropropene ND ug/kg 03/22/15 20:24 563-58-66.2 1.9 1
cis-1,3-Dichloropropene ND ug/kg 03/22/15 20:24 10061-01-56.2 2.2 1
trans-1,3-Dichloropropene ND ug/kg 03/22/15 20:24 10061-02-66.2 1.9 1
Diisopropyl ether ND ug/kg 03/22/15 20:24 108-20-36.2 2.1 1
Ethylbenzene ND ug/kg 03/22/15 20:24 100-41-46.2 2.2 1
Hexachloro-1,3-butadiene ND ug/kg 03/22/15 20:24 87-68-36.2 2.5 1
2-Hexanone ND ug/kg 03/22/15 20:24 591-78-662.5 4.9 1
Isopropylbenzene (Cumene)ND ug/kg 03/22/15 20:24 98-82-86.2 2.4 1
p-Isopropyltoluene ND ug/kg 03/22/15 20:24 99-87-66.2 2.1 1
Methylene Chloride ND ug/kg 03/22/15 20:24 75-09-225.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 03/22/15 20:24 108-10-162.5 4.6 1
Methyl-tert-butyl ether ND ug/kg 03/22/15 20:24 1634-04-46.2 1.9 1
Naphthalene ND ug/kg 03/22/15 20:24 91-20-36.2 1.5 1
n-Propylbenzene ND ug/kg 03/22/15 20:24 103-65-16.2 2.1 1
Styrene ND ug/kg 03/22/15 20:24 100-42-56.2 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 03/22/15 20:24 630-20-66.2 2.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 03/22/15 20:24 79-34-56.2 2.4 1
Tetrachloroethene 6.8 ug/kg 03/22/15 20:24 127-18-46.2 2.1 1
Toluene ND ug/kg 03/22/15 20:24 108-88-36.2 2.2 1
1,2,3-Trichlorobenzene ND ug/kg 03/22/15 20:24 87-61-66.2 2.7 1
1,2,4-Trichlorobenzene ND ug/kg 03/22/15 20:24 120-82-16.2 2.0 1
1,1,1-Trichloroethane ND ug/kg 03/22/15 20:24 71-55-66.2 2.2 1
1,1,2-Trichloroethane ND ug/kg 03/22/15 20:24 79-00-56.2 2.6 1
Trichloroethene ND ug/kg 03/22/15 20:24 79-01-66.2 2.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-4 18'-20'Lab ID: 92241876004 Collected: 03/18/15 16:15 Received: 03/19/15 10:03 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260/5035A Volatile Organics
Trichlorofluoromethane ND ug/kg 03/22/15 20:24 75-69-46.2 2.7 1
1,2,3-Trichloropropane ND ug/kg 03/22/15 20:24 96-18-46.2 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 03/22/15 20:24 95-63-66.2 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 03/22/15 20:24 108-67-86.2 2.2 1
Vinyl acetate ND ug/kg 03/22/15 20:24 108-05-462.5 11.0 1
Vinyl chloride ND ug/kg 03/22/15 20:24 75-01-412.5 2.2 1
Xylene (Total)ND ug/kg 03/22/15 20:24 1330-20-712.5 4.5 1
m&p-Xylene ND ug/kg 03/22/15 20:24 179601-23-112.5 4.5 1
o-Xylene ND ug/kg 03/22/15 20:24 95-47-66.2 2.4 1
Surrogates
Toluene-d8 (S)102 %03/22/15 20:24 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %03/22/15 20:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %03/22/15 20:24 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 30.7 %03/23/15 10:260.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-8 Lab ID: 92241876005 Collected: 03/18/15 17:45 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Acenaphthene ND ug/L 03/24/15 17:18 83-32-903/24/15 07:0010.0 1.1 1
Acenaphthylene ND ug/L 03/24/15 17:18 208-96-803/24/15 07:0010.0 0.99 1
Aniline ND ug/L 03/24/15 17:18 62-53-303/24/15 07:0010.0 0.80 1
Anthracene 0.54J ug/L 03/24/15 17:18 120-12-703/24/15 07:0010.0 0.47 1
Benzo(a)anthracene ND ug/L 03/24/15 17:18 56-55-303/24/15 07:0010.0 0.47 1
Benzo(a)pyrene ND ug/L 03/24/15 17:18 50-32-803/24/15 07:0010.0 0.57 1
Benzo(b)fluoranthene 1.0J ug/L 03/24/15 17:18 205-99-2 B03/24/15 07:0010.0 0.44 1
Benzo(g,h,i)perylene ND ug/L 03/24/15 17:18 191-24-203/24/15 07:0010.0 0.45 1
Benzo(k)fluoranthene ND ug/L 03/24/15 17:18 207-08-903/24/15 07:0010.0 0.53 1
Benzoic Acid ND ug/L 03/24/15 17:18 65-85-003/24/15 07:0050.0 4.9 1
Benzyl alcohol ND ug/L 03/24/15 17:18 100-51-603/24/15 07:0020.0 2.1 1
4-Bromophenylphenyl ether ND ug/L 03/24/15 17:18 101-55-303/24/15 07:0010.0 1.0 1
Butylbenzylphthalate ND ug/L 03/24/15 17:18 85-68-703/24/15 07:0010.0 0.48 1
4-Chloro-3-methylphenol ND ug/L 03/24/15 17:18 59-50-703/24/15 07:0020.0 2.0 1
4-Chloroaniline ND ug/L 03/24/15 17:18 106-47-803/24/15 07:0020.0 1.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/24/15 17:18 111-91-103/24/15 07:0010.0 1.3 1
bis(2-Chloroethyl) ether ND ug/L 03/24/15 17:18 111-44-403/24/15 07:0010.0 0.89 1
bis(2-Chloroisopropyl) ether ND ug/L 03/24/15 17:18 108-60-103/24/15 07:0010.0 0.86 1
2-Chloronaphthalene ND ug/L 03/24/15 17:18 91-58-703/24/15 07:0010.0 1.0 1
2-Chlorophenol ND ug/L 03/24/15 17:18 95-57-803/24/15 07:0010.0 1.0 1
4-Chlorophenylphenyl ether ND ug/L 03/24/15 17:18 7005-72-303/24/15 07:0010.0 1.1 1
Chrysene ND ug/L 03/24/15 17:18 218-01-903/24/15 07:0010.0 0.49 1
Dibenz(a,h)anthracene ND ug/L 03/24/15 17:18 53-70-303/24/15 07:0010.0 0.49 1
Dibenzofuran ND ug/L 03/24/15 17:18 132-64-903/24/15 07:0010.0 1.0 1
1,2-Dichlorobenzene ND ug/L 03/24/15 17:18 95-50-103/24/15 07:0010.0 0.71 1
1,3-Dichlorobenzene ND ug/L 03/24/15 17:18 541-73-103/24/15 07:0010.0 0.78 1
1,4-Dichlorobenzene ND ug/L 03/24/15 17:18 106-46-703/24/15 07:0010.0 0.81 1
3,3'-Dichlorobenzidine ND ug/L 03/24/15 17:18 91-94-103/24/15 07:0020.0 0.69 1
2,4-Dichlorophenol ND ug/L 03/24/15 17:18 120-83-203/24/15 07:0010.0 0.85 1
Diethylphthalate ND ug/L 03/24/15 17:18 84-66-203/24/15 07:0010.0 0.91 1
2,4-Dimethylphenol ND ug/L 03/24/15 17:18 105-67-903/24/15 07:0010.0 0.96 1
Dimethylphthalate ND ug/L 03/24/15 17:18 131-11-303/24/15 07:0010.0 0.62 1
Di-n-butylphthalate ND ug/L 03/24/15 17:18 84-74-203/24/15 07:0010.0 0.37 1
4,6-Dinitro-2-methylphenol ND ug/L 03/24/15 17:18 534-52-103/24/15 07:0020.0 1.1 1
2,4-Dinitrophenol ND ug/L 03/24/15 17:18 51-28-503/24/15 07:0050.0 2.5 1
2,4-Dinitrotoluene ND ug/L 03/24/15 17:18 121-14-203/24/15 07:0010.0 0.92 1
2,6-Dinitrotoluene ND ug/L 03/24/15 17:18 606-20-203/24/15 07:0010.0 2.1 1
Di-n-octylphthalate ND ug/L 03/24/15 17:18 117-84-003/24/15 07:0010.0 0.12 1
bis(2-Ethylhexyl)phthalate 1.0J ug/L 03/24/15 17:18 117-81-7 B03/24/15 07:006.0 0.49 1
Fluoranthene 1.5J ug/L 03/24/15 17:18 206-44-003/24/15 07:0010.0 0.41 1
Fluorene ND ug/L 03/24/15 17:18 86-73-703/24/15 07:0010.0 1.0 1
Hexachloro-1,3-butadiene ND ug/L 03/24/15 17:18 87-68-303/24/15 07:0010.0 0.90 1
Hexachlorobenzene ND ug/L 03/24/15 17:18 118-74-103/24/15 07:0010.0 0.76 1
Hexachlorocyclopentadiene ND ug/L 03/24/15 17:18 77-47-403/24/15 07:0010.0 1.1 1
Hexachloroethane ND ug/L 03/24/15 17:18 67-72-103/24/15 07:0010.0 0.90 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/24/15 17:18 193-39-503/24/15 07:0010.0 0.53 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-8 Lab ID: 92241876005 Collected: 03/18/15 17:45 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic
Isophorone ND ug/L 03/24/15 17:18 78-59-103/24/15 07:0010.0 0.92 1
1-Methylnaphthalene ND ug/L 03/24/15 17:18 90-12-003/24/15 07:0010.0 0.92 1
2-Methylnaphthalene ND ug/L 03/24/15 17:18 91-57-603/24/15 07:0010.0 1.0 1
2-Methylphenol(o-Cresol)ND ug/L 03/24/15 17:18 95-48-703/24/15 07:0010.0 1.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/24/15 17:1803/24/15 07:0010.0 1.0 1
Naphthalene ND ug/L 03/24/15 17:18 91-20-303/24/15 07:0010.0 0.93 1
2-Nitroaniline ND ug/L 03/24/15 17:18 88-74-403/24/15 07:0050.0 1.5 1
3-Nitroaniline ND ug/L 03/24/15 17:18 99-09-203/24/15 07:0050.0 1.3 1
4-Nitroaniline ND ug/L 03/24/15 17:18 100-01-603/24/15 07:0020.0 1.6 1
Nitrobenzene ND ug/L 03/24/15 17:18 98-95-303/24/15 07:0010.0 1.0 1
2-Nitrophenol ND ug/L 03/24/15 17:18 88-75-503/24/15 07:0010.0 0.71 1
4-Nitrophenol ND ug/L 03/24/15 17:18 100-02-703/24/15 07:0050.0 3.9 1
N-Nitrosodimethylamine ND ug/L 03/24/15 17:18 62-75-903/24/15 07:0010.0 0.94 1
N-Nitroso-di-n-propylamine ND ug/L 03/24/15 17:18 621-64-703/24/15 07:0010.0 0.85 1
N-Nitrosodiphenylamine ND ug/L 03/24/15 17:18 86-30-603/24/15 07:0010.0 0.64 1
Pentachlorophenol ND ug/L 03/24/15 17:18 87-86-503/24/15 07:0025.0 1.2 1
Phenanthrene 2.9J ug/L 03/24/15 17:18 85-01-803/24/15 07:0010.0 0.53 1
Phenol ND ug/L 03/24/15 17:18 108-95-203/24/15 07:0010.0 1.1 1
Pyrene 0.96J ug/L 03/24/15 17:18 129-00-003/24/15 07:0010.0 0.49 1
1,2,4-Trichlorobenzene ND ug/L 03/24/15 17:18 120-82-103/24/15 07:0010.0 1.3 1
2,4,5-Trichlorophenol ND ug/L 03/24/15 17:18 95-95-403/24/15 07:0010.0 1.0 1
2,4,6-Trichlorophenol ND ug/L 03/24/15 17:18 88-06-203/24/15 07:0010.0 0.85 1
Surrogates
Nitrobenzene-d5 (S)33 %03/24/15 17:18 4165-60-003/24/15 07:0021-110 1
2-Fluorobiphenyl (S)34 %03/24/15 17:18 321-60-803/24/15 07:0027-110 1
Terphenyl-d14 (S)51 %03/24/15 17:18 1718-51-003/24/15 07:0031-107 1
Phenol-d6 (S)15 %03/24/15 17:18 13127-88-303/24/15 07:0010-110 1
2-Fluorophenol (S)21 %03/24/15 17:18 367-12-403/24/15 07:0012-110 1
2,4,6-Tribromophenol (S)65 %03/24/15 17:18 118-79-603/24/15 07:0027-110 1
Analytical Method: EPA 82608260 MSV Low Level
Acetone ND ug/L 03/26/15 05:05 67-64-125.0 10.0 1
Benzene ND ug/L 03/26/15 05:05 71-43-21.0 0.25 1
Bromobenzene ND ug/L 03/26/15 05:05 108-86-11.0 0.30 1
Bromochloromethane ND ug/L 03/26/15 05:05 74-97-51.0 0.17 1
Bromodichloromethane ND ug/L 03/26/15 05:05 75-27-41.0 0.18 1
Bromoform ND ug/L 03/26/15 05:05 75-25-21.0 0.26 1
Bromomethane ND ug/L 03/26/15 05:05 74-83-92.0 0.29 1
2-Butanone (MEK)ND ug/L 03/26/15 05:05 78-93-35.0 0.96 1
Carbon tetrachloride ND ug/L 03/26/15 05:05 56-23-51.0 0.25 1
Chlorobenzene ND ug/L 03/26/15 05:05 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/26/15 05:05 75-00-31.0 0.54 1
Chloroform 1.4 ug/L 03/26/15 05:05 67-66-31.0 0.14 1
Chloromethane ND ug/L 03/26/15 05:05 74-87-31.0 0.11 1
2-Chlorotoluene ND ug/L 03/26/15 05:05 95-49-81.0 0.35 1
4-Chlorotoluene ND ug/L 03/26/15 05:05 106-43-41.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-8 Lab ID: 92241876005 Collected: 03/18/15 17:45 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
1,2-Dibromo-3-chloropropane ND ug/L 03/26/15 05:05 96-12-82.0 2.0 1
Dibromochloromethane ND ug/L 03/26/15 05:05 124-48-11.0 0.21 1
1,2-Dibromoethane (EDB)ND ug/L 03/26/15 05:05 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/26/15 05:05 74-95-31.0 0.21 1
1,2-Dichlorobenzene ND ug/L 03/26/15 05:05 95-50-11.0 0.30 1
1,3-Dichlorobenzene ND ug/L 03/26/15 05:05 541-73-11.0 0.24 1
1,4-Dichlorobenzene ND ug/L 03/26/15 05:05 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/26/15 05:05 75-71-81.0 0.21 1
1,1-Dichloroethane ND ug/L 03/26/15 05:05 75-34-31.0 0.32 1
1,2-Dichloroethane ND ug/L 03/26/15 05:05 107-06-21.0 0.12 1
1,1-Dichloroethene ND ug/L 03/26/15 05:05 75-35-41.0 0.56 1
cis-1,2-Dichloroethene ND ug/L 03/26/15 05:05 156-59-21.0 0.19 1
trans-1,2-Dichloroethene ND ug/L 03/26/15 05:05 156-60-51.0 0.49 1
1,2-Dichloropropane ND ug/L 03/26/15 05:05 78-87-51.0 0.27 1
1,3-Dichloropropane ND ug/L 03/26/15 05:05 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/26/15 05:05 594-20-71.0 0.13 1
1,1-Dichloropropene ND ug/L 03/26/15 05:05 563-58-61.0 0.49 1
cis-1,3-Dichloropropene ND ug/L 03/26/15 05:05 10061-01-51.0 0.13 1
trans-1,3-Dichloropropene ND ug/L 03/26/15 05:05 10061-02-61.0 0.26 1
Diisopropyl ether ND ug/L 03/26/15 05:05 108-20-31.0 0.12 1
Ethylbenzene ND ug/L 03/26/15 05:05 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/26/15 05:05 87-68-31.0 0.71 1
2-Hexanone ND ug/L 03/26/15 05:05 591-78-65.0 0.46 1
p-Isopropyltoluene ND ug/L 03/26/15 05:05 99-87-61.0 0.31 1
Methylene Chloride ND ug/L 03/26/15 05:05 75-09-22.0 0.97 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/26/15 05:05 108-10-15.0 0.33 1
Methyl-tert-butyl ether ND ug/L 03/26/15 05:05 1634-04-41.0 0.21 1
Naphthalene ND ug/L 03/26/15 05:05 91-20-31.0 0.24 1
Styrene ND ug/L 03/26/15 05:05 100-42-51.0 0.26 1
1,1,1,2-Tetrachloroethane ND ug/L 03/26/15 05:05 630-20-61.0 0.33 1
1,1,2,2-Tetrachloroethane ND ug/L 03/26/15 05:05 79-34-51.0 0.40 1
Tetrachloroethene ND ug/L 03/26/15 05:05 127-18-41.0 0.46 1
Toluene 0.61J ug/L 03/26/15 05:05 108-88-31.0 0.26 1
1,2,3-Trichlorobenzene ND ug/L 03/26/15 05:05 87-61-61.0 0.33 1
1,2,4-Trichlorobenzene ND ug/L 03/26/15 05:05 120-82-11.0 0.35 1
1,1,1-Trichloroethane ND ug/L 03/26/15 05:05 71-55-61.0 0.48 1
1,1,2-Trichloroethane ND ug/L 03/26/15 05:05 79-00-51.0 0.29 1
Trichloroethene ND ug/L 03/26/15 05:05 79-01-61.0 0.47 1
Trichlorofluoromethane ND ug/L 03/26/15 05:05 75-69-41.0 0.20 1
1,2,3-Trichloropropane ND ug/L 03/26/15 05:05 96-18-41.0 0.41 1
Vinyl acetate ND ug/L 03/26/15 05:05 108-05-42.0 0.35 1
Vinyl chloride ND ug/L 03/26/15 05:05 75-01-41.0 0.62 1
Xylene (Total)ND ug/L 03/26/15 05:05 1330-20-72.0 0.66 1
m&p-Xylene ND ug/L 03/26/15 05:05 179601-23-12.0 0.66 1
o-Xylene ND ug/L 03/26/15 05:05 95-47-61.0 0.23 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 54
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Sample: B-8 Lab ID: 92241876005 Collected: 03/18/15 17:45 Received: 03/19/15 10:03 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 82608260 MSV Low Level
Surrogates
4-Bromofluorobenzene (S)113 %03/26/15 05:05 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %03/26/15 05:05 17060-07-070-130 1
Toluene-d8 (S)98 %03/26/15 05:05 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30901
EPA 8260
EPA 8260
8260 MSV Low Level
Associated Lab Samples: 92241876001, 92241876005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1419174
Associated Lab Samples:92241876001, 92241876005
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/25/15 21:12
1,1,1-Trichloroethane ug/L ND 1.0 03/25/15 21:12
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/25/15 21:12
1,1,2-Trichloroethane ug/L ND 1.0 03/25/15 21:12
1,1-Dichloroethane ug/L ND 1.0 03/25/15 21:12
1,1-Dichloroethene ug/L ND 1.0 03/25/15 21:12
1,1-Dichloropropene ug/L ND 1.0 03/25/15 21:12
1,2,3-Trichlorobenzene ug/L ND 1.0 03/25/15 21:12
1,2,3-Trichloropropane ug/L ND 1.0 03/25/15 21:12
1,2,4-Trichlorobenzene ug/L ND 1.0 03/25/15 21:12
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/25/15 21:12
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/25/15 21:12
1,2-Dichlorobenzene ug/L ND 1.0 03/25/15 21:12
1,2-Dichloroethane ug/L ND 1.0 03/25/15 21:12
1,2-Dichloropropane ug/L ND 1.0 03/25/15 21:12
1,3-Dichlorobenzene ug/L ND 1.0 03/25/15 21:12
1,3-Dichloropropane ug/L ND 1.0 03/25/15 21:12
1,4-Dichlorobenzene ug/L ND 1.0 03/25/15 21:12
2,2-Dichloropropane ug/L ND 1.0 03/25/15 21:12
2-Butanone (MEK)ug/L ND 5.0 03/25/15 21:12
2-Chlorotoluene ug/L ND 1.0 03/25/15 21:12
2-Hexanone ug/L ND 5.0 03/25/15 21:12
4-Chlorotoluene ug/L ND 1.0 03/25/15 21:12
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/25/15 21:12
Acetone ug/L ND 25.0 03/25/15 21:12
Benzene ug/L ND 1.0 03/25/15 21:12
Bromobenzene ug/L ND 1.0 03/25/15 21:12
Bromochloromethane ug/L ND 1.0 03/25/15 21:12
Bromodichloromethane ug/L ND 1.0 03/25/15 21:12
Bromoform ug/L ND 1.0 03/25/15 21:12
Bromomethane ug/L ND 2.0 03/25/15 21:12
Carbon tetrachloride ug/L ND 1.0 03/25/15 21:12
Chlorobenzene ug/L ND 1.0 03/25/15 21:12
Chloroethane ug/L ND 1.0 03/25/15 21:12
Chloroform ug/L ND 1.0 03/25/15 21:12
Chloromethane ug/L ND 1.0 03/25/15 21:12
cis-1,2-Dichloroethene ug/L ND 1.0 03/25/15 21:12
cis-1,3-Dichloropropene ug/L ND 1.0 03/25/15 21:12
Dibromochloromethane ug/L ND 1.0 03/25/15 21:12
Dibromomethane ug/L ND 1.0 03/25/15 21:12
Dichlorodifluoromethane ug/L ND 1.0 03/25/15 21:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1419174
Associated Lab Samples:92241876001, 92241876005
Matrix: Water
Analyzed
Diisopropyl ether ug/L ND 1.0 03/25/15 21:12
Ethylbenzene ug/L ND 1.0 03/25/15 21:12
Hexachloro-1,3-butadiene ug/L ND 1.0 03/25/15 21:12
m&p-Xylene ug/L ND 2.0 03/25/15 21:12
Methyl-tert-butyl ether ug/L ND 1.0 03/25/15 21:12
Methylene Chloride ug/L ND 2.0 03/25/15 21:12
Naphthalene ug/L ND 1.0 03/25/15 21:12
o-Xylene ug/L ND 1.0 03/25/15 21:12
p-Isopropyltoluene ug/L ND 1.0 03/25/15 21:12
Styrene ug/L ND 1.0 03/25/15 21:12
Tetrachloroethene ug/L ND 1.0 03/25/15 21:12
Toluene ug/L ND 1.0 03/25/15 21:12
trans-1,2-Dichloroethene ug/L ND 1.0 03/25/15 21:12
trans-1,3-Dichloropropene ug/L ND 1.0 03/25/15 21:12
Trichloroethene ug/L ND 1.0 03/25/15 21:12
Trichlorofluoromethane ug/L ND 1.0 03/25/15 21:12
Vinyl acetate ug/L ND 2.0 03/25/15 21:12
Vinyl chloride ug/L ND 1.0 03/25/15 21:12
Xylene (Total)ug/L ND 2.0 03/25/15 21:12
1,2-Dichloroethane-d4 (S)%102 70-130 03/25/15 21:12
4-Bromofluorobenzene (S)%103 70-130 03/25/15 21:12
Toluene-d8 (S)%95 70-130 03/25/15 21:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1419175LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.650 113 70-130
1,1,1-Trichloroethane ug/L 59.150 118 70-130
1,1,2,2-Tetrachloroethane ug/L 45.550 91 70-130
1,1,2-Trichloroethane ug/L 48.850 98 70-130
1,1-Dichloroethane ug/L 49.850 100 70-130
1,1-Dichloroethene ug/L 52.250 104 70-132
1,1-Dichloropropene ug/L 51.650 103 70-130
1,2,3-Trichlorobenzene ug/L 48.550 97 70-135
1,2,3-Trichloropropane ug/L 47.950 96 70-130
1,2,4-Trichlorobenzene ug/L 44.950 90 70-134
1,2-Dibromo-3-chloropropane ug/L 49.450 99 70-130
1,2-Dibromoethane (EDB)ug/L 52.950 106 70-130
1,2-Dichlorobenzene ug/L 52.450 105 70-130
1,2-Dichloroethane ug/L 47.650 95 70-130
1,2-Dichloropropane ug/L 48.950 98 70-130
1,3-Dichlorobenzene ug/L 51.650 103 70-130
1,3-Dichloropropane ug/L 51.050 102 70-130
1,4-Dichlorobenzene ug/L 49.650 99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1419175LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 51.550 103 58-145
2-Butanone (MEK)ug/L 78.4100 78 70-145
2-Chlorotoluene ug/L 49.250 98 70-130
2-Hexanone ug/L 88.0100 88 70-144
4-Chlorotoluene ug/L 52.050 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 81.5100 81 70-140
Acetone ug/L 77.6100 78 50-175
Benzene ug/L 53.150 106 70-130
Bromobenzene ug/L 50.550 101 70-130
Bromochloromethane ug/L 52.250 104 70-130
Bromodichloromethane ug/L 47.850 96 70-130
Bromoform ug/L 51.550 103 70-130
Bromomethane ug/L 47.050 94 54-130
Carbon tetrachloride ug/L 56.650 113 70-132
Chlorobenzene ug/L 51.950 104 70-130
Chloroethane ug/L 45.150 90 64-134
Chloroform ug/L 46.550 93 70-130
Chloromethane ug/L 41.150 82 64-130
cis-1,2-Dichloroethene ug/L 50.750 101 70-131
cis-1,3-Dichloropropene ug/L 48.750 97 70-130
Dibromochloromethane ug/L 50.050 100 70-130
Dibromomethane ug/L 53.150 106 70-131
Dichlorodifluoromethane ug/L 49.450 99 56-130
Diisopropyl ether ug/L 45.550 91 70-130
Ethylbenzene ug/L 55.650 111 70-130
Hexachloro-1,3-butadiene ug/L 49.350 99 70-130
m&p-Xylene ug/L 111100 111 70-130
Methyl-tert-butyl ether ug/L 49.450 99 70-130
Methylene Chloride ug/L 49.650 99 63-130
Naphthalene ug/L 40.750 81 70-138
o-Xylene ug/L 49.250 98 70-130
p-Isopropyltoluene ug/L 46.950 94 70-130
Styrene ug/L 51.150 102 70-130
Tetrachloroethene ug/L 63.050 126 70-130
Toluene ug/L 53.650 107 70-130
trans-1,2-Dichloroethene ug/L 51.550 103 70-130
trans-1,3-Dichloropropene ug/L 49.950 100 70-132
Trichloroethene ug/L 56.150 112 70-130
Trichlorofluoromethane ug/L 48.550 97 62-133
Vinyl acetate ug/L 97.4100 97 66-157
Vinyl chloride ug/L 48.350 97 50-150
Xylene (Total)ug/L 160150 107 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1419190MATRIX SPIKE SAMPLE:
MSSpike
Result
92242186004
1,1,1,2-Tetrachloroethane ug/L 24.720 123 70-130ND
1,1,1-Trichloroethane ug/L 26.5 M12013370-130ND
1,1,2,2-Tetrachloroethane ug/L 18.720 93 70-130ND
1,1,2-Trichloroethane ug/L 20.220 101 70-130ND
1,1-Dichloroethane ug/L 21.220 106 70-130ND
1,1-Dichloroethene ug/L 22.320 112 70-166ND
1,1-Dichloropropene ug/L 22.120 111 70-130ND
1,2,3-Trichlorobenzene ug/L 15.820 79 70-130ND
1,2,3-Trichloropropane ug/L 20.320 102 70-130ND
1,2,4-Trichlorobenzene ug/L 15.220 76 70-130ND
1,2-Dibromo-3-chloropropane ug/L 16.720 84 70-130ND
1,2-Dibromoethane (EDB)ug/L 20.720 104 70-130ND
1,2-Dichlorobenzene ug/L 20.320 102 70-130ND
1,2-Dichloroethane ug/L 20.320 102 70-130ND
1,2-Dichloropropane ug/L 19.420 97 70-130ND
1,3-Dichlorobenzene ug/L 20.820 104 70-130ND
1,3-Dichloropropane ug/L 19.820 99 70-130ND
1,4-Dichlorobenzene ug/L 20.720 103 70-130ND
2,2-Dichloropropane ug/L 19.420 97 70-130ND
2-Butanone (MEK)ug/L 29.040 72 70-130ND
2-Chlorotoluene ug/L 21.220 106 70-130ND
2-Hexanone ug/L 31.540 79 70-130ND
4-Chlorotoluene ug/L 21.020 105 70-130ND
4-Methyl-2-pentanone (MIBK)ug/L 30.3 M1406170-1306.0
Acetone ug/L 32.540 72 70-130ND
Benzene ug/L 22.020 110 70-148ND
Bromobenzene ug/L 20.120 101 70-130ND
Bromochloromethane ug/L 22.720 114 70-130ND
Bromodichloromethane ug/L 20.620 103 70-130ND
Bromoform ug/L 20.620 103 70-130ND
Bromomethane ug/L 18.120 90 70-130ND
Carbon tetrachloride ug/L 28.4 M12014270-130ND
Chlorobenzene ug/L 22.120 110 70-146ND
Chloroethane ug/L 21.420 107 70-130ND
Chloroform ug/L 18.920 94 70-130ND
Chloromethane ug/L 17.820 89 70-130ND
cis-1,2-Dichloroethene ug/L 19.920 100 70-130ND
cis-1,3-Dichloropropene ug/L 16.320 82 70-130ND
Dibromochloromethane ug/L 20.320 101 70-130ND
Dibromomethane ug/L 22.020 110 70-130ND
Dichlorodifluoromethane ug/L 23.720 118 70-130ND
Diisopropyl ether ug/L 15.320 77 70-130ND
Ethylbenzene ug/L 23.520 118 70-130ND
Hexachloro-1,3-butadiene ug/L 24.220 121 70-130ND
m&p-Xylene ug/L 46.940 117 70-130ND
Methyl-tert-butyl ether ug/L 17.820 89 70-130ND
Methylene Chloride ug/L 17.820 89 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1419190MATRIX SPIKE SAMPLE:
MSSpike
Result
92242186004
Naphthalene ug/L 12.6 M1206370-130ND
o-Xylene ug/L 18.620 93 70-130ND
p-Isopropyltoluene ug/L 18.520 93 70-130ND
Styrene ug/L 19.820 99 70-130ND
Tetrachloroethene ug/L 25.420 127 70-130ND
Toluene ug/L 22.120 111 70-155ND
trans-1,2-Dichloroethene ug/L 20.220 101 70-130ND
trans-1,3-Dichloropropene ug/L 19.820 99 70-130ND
Trichloroethene ug/L 24.220 121 69-151ND
Trichlorofluoromethane ug/L 23.820 119 70-130ND
Vinyl acetate ug/L 29.040 72 70-130ND
Vinyl chloride ug/L 20.120 100 70-130ND
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%96 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92242186002
1419189SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L 9.4 D6753020.7
Acetone ug/L ND 30ND
Benzene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92242186002
1419189SAMPLE DUPLICATE:
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%106 3109
4-Bromofluorobenzene (S)%105 1106
Toluene-d8 (S)%96 198
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/30860
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92241876002, 92241876003, 92241876004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1416733
Associated Lab Samples:92241876002, 92241876003, 92241876004
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 4.8 03/22/15 13:08
1,1,1-Trichloroethane ug/kg ND 4.8 03/22/15 13:08
1,1,2,2-Tetrachloroethane ug/kg ND 4.8 03/22/15 13:08
1,1,2-Trichloroethane ug/kg ND 4.8 03/22/15 13:08
1,1-Dichloroethane ug/kg ND 4.8 03/22/15 13:08
1,1-Dichloroethene ug/kg ND 4.8 03/22/15 13:08
1,1-Dichloropropene ug/kg ND 4.8 03/22/15 13:08
1,2,3-Trichlorobenzene ug/kg ND 4.8 03/22/15 13:08
1,2,3-Trichloropropane ug/kg ND 4.8 03/22/15 13:08
1,2,4-Trichlorobenzene ug/kg ND 4.8 03/22/15 13:08
1,2,4-Trimethylbenzene ug/kg ND 4.8 03/22/15 13:08
1,2-Dibromo-3-chloropropane ug/kg ND 4.8 03/22/15 13:08
1,2-Dibromoethane (EDB)ug/kg ND 4.8 03/22/15 13:08
1,2-Dichlorobenzene ug/kg ND 4.8 03/22/15 13:08
1,2-Dichloroethane ug/kg ND 4.8 03/22/15 13:08
1,2-Dichloropropane ug/kg ND 4.8 03/22/15 13:08
1,3,5-Trimethylbenzene ug/kg ND 4.8 03/22/15 13:08
1,3-Dichlorobenzene ug/kg ND 4.8 03/22/15 13:08
1,3-Dichloropropane ug/kg ND 4.8 03/22/15 13:08
1,4-Dichlorobenzene ug/kg ND 4.8 03/22/15 13:08
2,2-Dichloropropane ug/kg ND 4.8 03/22/15 13:08
2-Butanone (MEK)ug/kg ND 96.9 03/22/15 13:08
2-Chlorotoluene ug/kg ND 4.8 03/22/15 13:08
2-Hexanone ug/kg ND 48.4 03/22/15 13:08
4-Chlorotoluene ug/kg ND 4.8 03/22/15 13:08
4-Methyl-2-pentanone (MIBK)ug/kg ND 48.4 03/22/15 13:08
Acetone ug/kg ND 96.9 03/22/15 13:08
Benzene ug/kg ND 4.8 03/22/15 13:08
Bromobenzene ug/kg ND 4.8 03/22/15 13:08
Bromochloromethane ug/kg ND 4.8 03/22/15 13:08
Bromodichloromethane ug/kg ND 4.8 03/22/15 13:08
Bromoform ug/kg ND 4.8 03/22/15 13:08
Bromomethane ug/kg ND 9.7 03/22/15 13:08
Carbon tetrachloride ug/kg ND 4.8 03/22/15 13:08
Chlorobenzene ug/kg ND 4.8 03/22/15 13:08
Chloroethane ug/kg ND 9.7 03/22/15 13:08
Chloroform ug/kg ND 4.8 03/22/15 13:08
Chloromethane ug/kg ND 9.7 03/22/15 13:08
cis-1,2-Dichloroethene ug/kg ND 4.8 03/22/15 13:08
cis-1,3-Dichloropropene ug/kg ND 4.8 03/22/15 13:08
Dibromochloromethane ug/kg ND 4.8 03/22/15 13:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1416733
Associated Lab Samples:92241876002, 92241876003, 92241876004
Matrix: Solid
Analyzed
Dibromomethane ug/kg ND 4.8 03/22/15 13:08
Dichlorodifluoromethane ug/kg ND 9.7 03/22/15 13:08
Diisopropyl ether ug/kg ND 4.8 03/22/15 13:08
Ethylbenzene ug/kg ND 4.8 03/22/15 13:08
Hexachloro-1,3-butadiene ug/kg ND 4.8 03/22/15 13:08
Isopropylbenzene (Cumene)ug/kg ND 4.8 03/22/15 13:08
m&p-Xylene ug/kg ND 9.7 03/22/15 13:08
Methyl-tert-butyl ether ug/kg ND 4.8 03/22/15 13:08
Methylene Chloride ug/kg ND 19.4 03/22/15 13:08
n-Butylbenzene ug/kg ND 4.8 03/22/15 13:08
n-Propylbenzene ug/kg ND 4.8 03/22/15 13:08
Naphthalene ug/kg ND 4.8 03/22/15 13:08
o-Xylene ug/kg ND 4.8 03/22/15 13:08
p-Isopropyltoluene ug/kg ND 4.8 03/22/15 13:08
sec-Butylbenzene ug/kg ND 4.8 03/22/15 13:08
Styrene ug/kg ND 4.8 03/22/15 13:08
tert-Butylbenzene ug/kg ND 4.8 03/22/15 13:08
Tetrachloroethene ug/kg ND 4.8 03/22/15 13:08
Toluene ug/kg ND 4.8 03/22/15 13:08
trans-1,2-Dichloroethene ug/kg ND 4.8 03/22/15 13:08
trans-1,3-Dichloropropene ug/kg ND 4.8 03/22/15 13:08
Trichloroethene ug/kg ND 4.8 03/22/15 13:08
Trichlorofluoromethane ug/kg ND 4.8 03/22/15 13:08
Vinyl acetate ug/kg ND 48.4 03/22/15 13:08
Vinyl chloride ug/kg ND 9.7 03/22/15 13:08
Xylene (Total)ug/kg ND 9.7 03/22/15 13:08
1,2-Dichloroethane-d4 (S)%98 70-132 03/22/15 13:08
4-Bromofluorobenzene (S)%98 70-130 03/22/15 13:08
Toluene-d8 (S)%101 70-130 03/22/15 13:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1416734LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 53.251.5 103 74-137
1,1,1-Trichloroethane ug/kg 50.451.5 98 67-140
1,1,2,2-Tetrachloroethane ug/kg 44.551.5 86 72-141
1,1,2-Trichloroethane ug/kg 50.651.5 98 78-138
1,1-Dichloroethane ug/kg 51.751.5 100 69-134
1,1-Dichloroethene ug/kg 49.951.5 97 67-138
1,1-Dichloropropene ug/kg 51.151.5 99 69-139
1,2,3-Trichlorobenzene ug/kg 55.751.5 108 70-146
1,2,3-Trichloropropane ug/kg 49.651.5 96 69-144
1,2,4-Trichlorobenzene ug/kg 54.851.5 106 68-148
1,2,4-Trimethylbenzene ug/kg 56.351.5 109 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1416734LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 48.851.5 95 65-140
1,2-Dibromoethane (EDB)ug/kg 53.251.5 103 77-135
1,2-Dichlorobenzene ug/kg 54.151.5 105 77-141
1,2-Dichloroethane ug/kg 52.351.5 101 65-137
1,2-Dichloropropane ug/kg 51.951.5 101 72-136
1,3,5-Trimethylbenzene ug/kg 54.751.5 106 76-133
1,3-Dichlorobenzene ug/kg 53.551.5 104 74-138
1,3-Dichloropropane ug/kg 50.451.5 98 71-139
1,4-Dichlorobenzene ug/kg 53.651.5 104 76-138
2,2-Dichloropropane ug/kg 49.751.5 96 68-137
2-Butanone (MEK)ug/kg 91.9J103 89 58-147
2-Chlorotoluene ug/kg 61.051.5 118 73-139
2-Hexanone ug/kg 93.1103 90 62-145
4-Chlorotoluene ug/kg 54.851.5 106 76-141
4-Methyl-2-pentanone (MIBK)ug/kg 106103 103 64-149
Acetone ug/kg 88.6J103 86 53-153
Benzene ug/kg 54.151.5 105 73-135
Bromobenzene ug/kg 60.651.5 118 75-133
Bromochloromethane ug/kg 47.751.5 93 73-134
Bromodichloromethane ug/kg 49.651.5 96 71-135
Bromoform ug/kg 49.151.5 95 66-141
Bromomethane ug/kg 56.451.5 109 53-160
Carbon tetrachloride ug/kg 54.851.5 106 60-145
Chlorobenzene ug/kg 52.451.5 102 78-130
Chloroethane ug/kg 54.351.5 105 64-149
Chloroform ug/kg 47.551.5 92 70-134
Chloromethane ug/kg 47.951.5 93 52-150
cis-1,2-Dichloroethene ug/kg 53.651.5 104 70-133
cis-1,3-Dichloropropene ug/kg 55.151.5 107 68-134
Dibromochloromethane ug/kg 48.051.5 93 71-138
Dibromomethane ug/kg 52.551.5 102 74-130
Dichlorodifluoromethane ug/kg 43.351.5 84 40-160
Diisopropyl ether ug/kg 50.651.5 98 69-141
Ethylbenzene ug/kg 54.151.5 105 75-133
Hexachloro-1,3-butadiene ug/kg 52.251.5 101 68-143
Isopropylbenzene (Cumene)ug/kg 53.651.5 104 76-143
m&p-Xylene ug/kg 109103 105 75-136
Methyl-tert-butyl ether ug/kg 46.051.5 89 68-144
Methylene Chloride ug/kg 50.151.5 97 45-154
n-Butylbenzene ug/kg 53.951.5 105 72-137
n-Propylbenzene ug/kg 53.451.5 104 76-136
Naphthalene ug/kg 51.751.5 100 68-151
o-Xylene ug/kg 54.051.5 105 76-141
p-Isopropyltoluene ug/kg 52.851.5 102 76-140
sec-Butylbenzene ug/kg 52.951.5 103 79-139
Styrene ug/kg 55.451.5 107 79-137
tert-Butylbenzene ug/kg 52.651.5 102 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1416734LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 52.651.5 102 71-138
Toluene ug/kg 54.351.5 105 74-131
trans-1,2-Dichloroethene ug/kg 51.051.5 99 67-135
trans-1,3-Dichloropropene ug/kg 55.851.5 108 65-146
Trichloroethene ug/kg 54.351.5 105 67-135
Trichlorofluoromethane ug/kg 47.751.5 93 59-144
Vinyl acetate ug/kg 68.1 F31036640-160
Vinyl chloride ug/kg 45.851.5 89 56-141
Xylene (Total)ug/kg 163155 105 76-137
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1416996MATRIX SPIKE SAMPLE:
MSSpike
Result
92241876002
1,1,1,2-Tetrachloroethane ug/kg 23.528 84 70-130ND
1,1,1-Trichloroethane ug/kg 24.528 87 70-130ND
1,1,2,2-Tetrachloroethane ug/kg 23.728 85 70-130ND
1,1,2-Trichloroethane ug/kg 23.828 85 70-130ND
1,1-Dichloroethane ug/kg 24.728 88 70-130ND
1,1-Dichloroethene ug/kg 22.928 82 49-180ND
1,1-Dichloropropene ug/kg 25.428 91 70-130ND
1,2,3-Trichlorobenzene ug/kg 22.628 81 70-130ND
1,2,3-Trichloropropane ug/kg 24.428 87 70-130ND
1,2,4-Trichlorobenzene ug/kg 21.728 78 70-130ND
1,2,4-Trimethylbenzene ug/kg 24.728 88 70-130ND
1,2-Dibromo-3-chloropropane ug/kg 21.228 76 70-130ND
1,2-Dibromoethane (EDB)ug/kg 23.928 85 70-130ND
1,2-Dichlorobenzene ug/kg 23.828 85 70-130ND
1,2-Dichloroethane ug/kg 24.528 88 70-130ND
1,2-Dichloropropane ug/kg 23.728 85 70-130ND
1,3,5-Trimethylbenzene ug/kg 24.528 87 70-130ND
1,3-Dichlorobenzene ug/kg 22.528 80 70-130ND
1,3-Dichloropropane ug/kg 24.128 86 70-130ND
1,4-Dichlorobenzene ug/kg 23.928 85 70-130ND
2,2-Dichloropropane ug/kg 22.528 80 70-130ND
2-Butanone (MEK)ug/kg 45.1J56 80 70-130ND
2-Chlorotoluene ug/kg 26.628 95 70-130ND
2-Hexanone ug/kg 43.8J56 78 70-130ND
4-Chlorotoluene ug/kg 24.628 88 70-130ND
4-Methyl-2-pentanone (MIBK)ug/kg 46.7J56 83 70-130ND
Acetone ug/kg 42.6J56 76 70-130ND
Benzene ug/kg 25.628 91 50-166ND
Bromobenzene ug/kg 27.128 97 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
1416996MATRIX SPIKE SAMPLE:
MSSpike
Result
92241876002
Bromochloromethane ug/kg 27.328 98 70-130ND
Bromodichloromethane ug/kg 22.728 81 70-130ND
Bromoform ug/kg 22.028 78 70-130ND
Bromomethane ug/kg 27.328 97 70-130ND
Carbon tetrachloride ug/kg 24.228 87 70-130ND
Chlorobenzene ug/kg 24.128 86 43-169ND
Chloroethane ug/kg 24.828 89 70-130ND
Chloroform ug/kg 23.528 84 70-130ND
Chloromethane ug/kg 24.128 86 70-130ND
cis-1,2-Dichloroethene ug/kg 26.428 94 70-130ND
cis-1,3-Dichloropropene ug/kg 23.628 84 70-130ND
Dibromochloromethane ug/kg 21.428 76 70-130ND
Dibromomethane ug/kg 23.828 85 70-130ND
Dichlorodifluoromethane ug/kg 24.528 87 70-130ND
Diisopropyl ether ug/kg 24.228 86 70-130ND
Ethylbenzene ug/kg 25.128 90 70-130ND
Hexachloro-1,3-butadiene ug/kg 21.528 77 70-130ND
Isopropylbenzene (Cumene)ug/kg 24.828 88 70-130ND
m&p-Xylene ug/kg 50.556 90 70-130ND
Methyl-tert-butyl ether ug/kg 22.228 79 70-130ND
Methylene Chloride ug/kg 26.5J28 95 70-130ND
n-Butylbenzene ug/kg 23.128 83 70-130ND
n-Propylbenzene ug/kg 24.328 87 70-130ND
Naphthalene ug/kg 23.028 82 70-130ND
o-Xylene ug/kg 23.828 85 70-130ND
p-Isopropyltoluene ug/kg 23.328 83 70-130ND
sec-Butylbenzene ug/kg 23.828 85 70-130ND
Styrene ug/kg 24.328 87 70-130ND
tert-Butylbenzene ug/kg 23.828 85 70-130ND
Tetrachloroethene ug/kg 23.628 84 70-130ND
Toluene ug/kg 26.028 92 52-163ND
trans-1,2-Dichloroethene ug/kg 24.428 87 70-130ND
trans-1,3-Dichloropropene ug/kg 23.728 84 70-130ND
Trichloroethene ug/kg 23.928 85 49-167ND
Trichlorofluoromethane ug/kg 24.828 89 70-130ND
Vinyl acetate ug/kg 36.3J M1566570-130ND
Vinyl chloride ug/kg 24.828 88 70-130ND
1,2-Dichloroethane-d4 (S)%107 70-132
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%102 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92242126002
1416995SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92242126002
1416995SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 3012.8J
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg 64.3J 3077.1J
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
m&p-Xylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92242126002
1416995SAMPLE DUPLICATE:
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg 2.1J 302.9J
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%97 11117
4-Bromofluorobenzene (S)%86 985
Toluene-d8 (S)%100 8100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/33747
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples: 92241876002, 92241876003, 92241876004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1416902
Associated Lab Samples:92241876002, 92241876003, 92241876004
Matrix: Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 330 03/25/15 14:18
1,2-Dichlorobenzene ug/kg ND 330 03/25/15 14:18
1,3-Dichlorobenzene ug/kg ND 330 03/25/15 14:18
1,4-Dichlorobenzene ug/kg ND 330 03/25/15 14:18
1-Methylnaphthalene ug/kg ND 330 03/25/15 14:18
2,4,5-Trichlorophenol ug/kg ND 330 03/25/15 14:18
2,4,6-Trichlorophenol ug/kg ND 330 03/25/15 14:18
2,4-Dichlorophenol ug/kg ND 330 03/25/15 14:18
2,4-Dimethylphenol ug/kg ND 330 03/25/15 14:18
2,4-Dinitrophenol ug/kg ND 1650 03/25/15 14:18
2,4-Dinitrotoluene ug/kg ND 330 03/25/15 14:18
2,6-Dinitrotoluene ug/kg ND 330 03/25/15 14:18
2-Chloronaphthalene ug/kg ND 330 03/25/15 14:18
2-Chlorophenol ug/kg ND 330 03/25/15 14:18
2-Methylnaphthalene ug/kg ND 330 03/25/15 14:18
2-Methylphenol(o-Cresol)ug/kg ND 330 03/25/15 14:18
2-Nitroaniline ug/kg ND 1650 03/25/15 14:18
2-Nitrophenol ug/kg ND 330 03/25/15 14:18
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 03/25/15 14:18
3,3'-Dichlorobenzidine ug/kg ND 1650 03/25/15 14:18
3-Nitroaniline ug/kg ND 1650 03/25/15 14:18
4,6-Dinitro-2-methylphenol ug/kg ND 660 03/25/15 14:18
4-Bromophenylphenyl ether ug/kg ND 330 03/25/15 14:18
4-Chloro-3-methylphenol ug/kg ND 660 03/25/15 14:18
4-Chloroaniline ug/kg ND 1650 03/25/15 14:18
4-Chlorophenylphenyl ether ug/kg ND 330 03/25/15 14:18
4-Nitroaniline ug/kg ND 660 03/25/15 14:18
4-Nitrophenol ug/kg ND 1650 03/25/15 14:18
Acenaphthene ug/kg ND 330 03/25/15 14:18
Acenaphthylene ug/kg ND 330 03/25/15 14:18
Aniline ug/kg ND 330 03/25/15 14:18
Anthracene ug/kg ND 330 03/25/15 14:18
Benzo(a)anthracene ug/kg ND 330 03/25/15 14:18
Benzo(a)pyrene ug/kg ND 330 03/25/15 14:18
Benzo(b)fluoranthene ug/kg ND 330 03/25/15 14:18
Benzo(g,h,i)perylene ug/kg ND 330 03/25/15 14:18
Benzo(k)fluoranthene ug/kg ND 330 03/25/15 14:18
Benzoic Acid ug/kg ND 1650 03/25/15 14:18
Benzyl alcohol ug/kg ND 660 03/25/15 14:18
bis(2-Chloroethoxy)methane ug/kg ND 330 03/25/15 14:18
bis(2-Chloroethyl) ether ug/kg ND 330 03/25/15 14:18
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1416902
Associated Lab Samples:92241876002, 92241876003, 92241876004
Matrix: Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 330 03/25/15 14:18
bis(2-Ethylhexyl)phthalate ug/kg ND 330 03/25/15 14:18
Butylbenzylphthalate ug/kg ND 330 03/25/15 14:18
Chrysene ug/kg ND 330 03/25/15 14:18
Di-n-butylphthalate ug/kg ND 330 03/25/15 14:18
Di-n-octylphthalate ug/kg ND 330 03/25/15 14:18
Dibenz(a,h)anthracene ug/kg ND 330 03/25/15 14:18
Dibenzofuran ug/kg ND 330 03/25/15 14:18
Diethylphthalate ug/kg ND 330 03/25/15 14:18
Dimethylphthalate ug/kg ND 330 03/25/15 14:18
Fluoranthene ug/kg ND 330 03/25/15 14:18
Fluorene ug/kg ND 330 03/25/15 14:18
Hexachloro-1,3-butadiene ug/kg ND 330 03/25/15 14:18
Hexachlorobenzene ug/kg ND 330 03/25/15 14:18
Hexachlorocyclopentadiene ug/kg ND 330 03/25/15 14:18
Hexachloroethane ug/kg ND 330 03/25/15 14:18
Indeno(1,2,3-cd)pyrene ug/kg ND 330 03/25/15 14:18
Isophorone ug/kg ND 330 03/25/15 14:18
N-Nitroso-di-n-propylamine ug/kg ND 330 03/25/15 14:18
N-Nitrosodimethylamine ug/kg ND 330 03/25/15 14:18
N-Nitrosodiphenylamine ug/kg ND 330 03/25/15 14:18
Naphthalene ug/kg ND 330 03/25/15 14:18
Nitrobenzene ug/kg ND 330 03/25/15 14:18
Pentachlorophenol ug/kg ND 1650 03/25/15 14:18
Phenanthrene ug/kg ND 330 03/25/15 14:18
Phenol ug/kg ND 330 03/25/15 14:18
Pyrene ug/kg ND 330 03/25/15 14:18
2,4,6-Tribromophenol (S)%77 27-110 03/25/15 14:18
2-Fluorobiphenyl (S)%69 30-110 03/25/15 14:18
2-Fluorophenol (S)%69 13-110 03/25/15 14:18
Nitrobenzene-d5 (S)%74 23-110 03/25/15 14:18
Phenol-d6 (S)%74 22-110 03/25/15 14:18
Terphenyl-d14 (S)%82 28-110 03/25/15 14:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1416903LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 13201670 79 36-120
1,2-Dichlorobenzene ug/kg 12801670 77 41-120
1,3-Dichlorobenzene ug/kg 12101670 73 66-120
1,4-Dichlorobenzene ug/kg 12301670 74 42-120
1-Methylnaphthalene ug/kg 11901670 71 40-120
2,4,5-Trichlorophenol ug/kg 14801670 89 37-120
2,4,6-Trichlorophenol ug/kg 15501670 93 40-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1416903LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/kg 14201670 85 33-120
2,4-Dimethylphenol ug/kg 12201670 73 36-120
2,4-Dinitrophenol ug/kg 75808330 91 22-121
2,4-Dinitrotoluene ug/kg 18001670 108 60-120
2,6-Dinitrotoluene ug/kg 15501670 93 54-120
2-Chloronaphthalene ug/kg 12901670 78 41-120
2-Chlorophenol ug/kg 13801670 83 39-120
2-Methylnaphthalene ug/kg 10601670 64 26-120
2-Methylphenol(o-Cresol)ug/kg 13501670 81 41-120
2-Nitroaniline ug/kg 29503330 88 45-120
2-Nitrophenol ug/kg 12801670 77 35-120
3&4-Methylphenol(m&p Cresol)ug/kg 13301670 80 35-120
3,3'-Dichlorobenzidine ug/kg 27503330 82 16-125
3-Nitroaniline ug/kg 29603330 89 45-120
4,6-Dinitro-2-methylphenol ug/kg 31703330 95 46-120
4-Bromophenylphenyl ether ug/kg 15201670 91 36-120
4-Chloro-3-methylphenol ug/kg 27803330 83 37-120
4-Chloroaniline ug/kg 26603330 80 35-120
4-Chlorophenylphenyl ether ug/kg 15401670 92 30-120
4-Nitroaniline ug/kg 35203330 105 48-120
4-Nitrophenol ug/kg 92208330 111 43-120
Acenaphthene ug/kg 13901670 83 46-120
Acenaphthylene ug/kg 13401670 81 46-120
Aniline ug/kg 11901670 71 33-120
Anthracene ug/kg 13901670 83 63-120
Benzo(a)anthracene ug/kg 14201670 85 61-120
Benzo(a)pyrene ug/kg 14501670 87 59-120
Benzo(b)fluoranthene ug/kg 13401670 80 55-120
Benzo(g,h,i)perylene ug/kg 13501670 81 57-120
Benzo(k)fluoranthene ug/kg 13301670 80 56-120
Benzoic Acid ug/kg 47508330 57 13-120
Benzyl alcohol ug/kg 28303330 85 34-120
bis(2-Chloroethoxy)methane ug/kg 11701670 70 21-120
bis(2-Chloroethyl) ether ug/kg 12201670 73 25-120
bis(2-Chloroisopropyl) ether ug/kg 10901670 65 13-120
bis(2-Ethylhexyl)phthalate ug/kg 17901670 108 56-123
Butylbenzylphthalate ug/kg 17801670 107 57-120
Chrysene ug/kg 14001670 84 64-120
Di-n-butylphthalate ug/kg 17301670 104 58-120
Di-n-octylphthalate ug/kg 18301670 110 47-121
Dibenz(a,h)anthracene ug/kg 13601670 82 56-120
Dibenzofuran ug/kg 15901670 95 43-120
Diethylphthalate ug/kg 18901670 113 55-120
Dimethylphthalate ug/kg 15601670 94 54-120
Fluoranthene ug/kg 16101670 96 61-120
Fluorene ug/kg 16001670 96 51-120
Hexachloro-1,3-butadiene ug/kg 13201670 79 22-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1416903LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/kg 13901670 83 53-120
Hexachlorocyclopentadiene ug/kg 13101670 78 18-150
Hexachloroethane ug/kg 12801670 77 39-120
Indeno(1,2,3-cd)pyrene ug/kg 13801670 83 58-120
Isophorone ug/kg 12101670 72 38-120
N-Nitroso-di-n-propylamine ug/kg 13501670 81 30-120
N-Nitrosodimethylamine ug/kg 14601670 88 32-120
N-Nitrosodiphenylamine ug/kg 15401670 92 50-120
Naphthalene ug/kg 13301670 80 38-120
Nitrobenzene ug/kg 11801670 71 37-120
Pentachlorophenol ug/kg 31203330 93 10-120
Phenanthrene ug/kg 13501670 81 62-120
Phenol ug/kg 15201670 91 37-120
Pyrene ug/kg 15401670 92 63-120
2,4,6-Tribromophenol (S)%95 27-110
2-Fluorobiphenyl (S)%74 30-110
2-Fluorophenol (S)%82 13-110
Nitrobenzene-d5 (S)%67 23-110
Phenol-d6 (S)%83 22-110
Terphenyl-d14 (S)%93 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1416904MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241876003
1416905
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1900 74 18-11959 23 301900ND14001120
1,2-Dichlorobenzene ug/kg 1900 59 50-11059 0 301900ND11201120
1,3-Dichlorobenzene ug/kg 1900 70 27-11056 22 301900ND13301070
1,4-Dichlorobenzene ug/kg 1900 68 28-11056 18 301900ND12801070
1-Methylnaphthalene ug/kg R119009224-11661 41 301900ND17501150
2,4,5-Trichlorophenol ug/kg R119008528-11056 40 301900ND16001060
2,4,6-Trichlorophenol ug/kg R119008117-11754 41 301900ND15401020
2,4-Dichlorophenol ug/kg 1900 77 21-12862 22 301900ND14601170
2,4-Dimethylphenol ug/kg 1900 49 10-12039 22 301900ND924744
2,4-Dinitrophenol ug/kg 9460 68 10-10763 8 309460ND64205950
2,4-Dinitrotoluene ug/kg 1900 71 36-10967 6 301900ND13401270
2,6-Dinitrotoluene ug/kg 1900 86 32-11070 21 301900ND16201320
2-Chloronaphthalene ug/kg R119007430-10750 39 301900ND1400938
2-Chlorophenol ug/kg 1900 73 14-10660 19 301900ND13801140
2-Methylnaphthalene ug/kg R119008310-13555 41 301900ND15801040
2-Methylphenol(o-Cresol)ug/kg 1900 50 10-12447 8 301900ND955885
2-Nitroaniline ug/kg 3780 85 26-11666 25 303780ND32002480
2-Nitrophenol ug/kg 1900 81 28-10367 19 301900ND15401270
3&4-Methylphenol(m&pCresol)ug/kg 1900 50 10-10941 21 301900ND947770
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1416904MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241876003
1416905
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3,3'-Dichlorobenzidine ug/kg 3780 53 10-15043 303780ND19901620J
3-Nitroaniline ug/kg 3780 76 22-11063 19 303780ND28802380
4,6-Dinitro-2-methylphenol ug/kg 3780 64 13-12182 25 303780ND24103090
4-Bromophenylphenyl ether ug/kg 1900 64 31-10972 12 301900ND12101370
4-Chloro-3-methylphenol ug/kg 3780 80 13-12866 18 303780ND30102510
4-Chloroaniline ug/kg 3780 68 18-10257 18 303780ND25802160
4-Chlorophenylphenyl ether ug/kg 1900 65 29-11257 12 301900ND12201090
4-Nitroaniline ug/kg 3780 69 16-11171 4 303780ND26002690
4-Nitrophenol ug/kg 9460 77 14-13572 6 309460ND72506860
Acenaphthene ug/kg 1900 73 26-11462 16 301900ND13701180
Acenaphthylene ug/kg 1900 75 32-10863 16 301900ND14101200
Aniline ug/kg 1900 39 10-10732 20 301900ND737600
Anthracene ug/kg 1900 70 32-11162 13 301900ND13301170
Benzo(a)anthracene ug/kg 1900 74 25-11764 15 301900ND14001210
Benzo(a)pyrene ug/kg 1900 75 25-10667 12 301900ND14201260
Benzo(b)fluoranthene ug/kg R119007024-11051 32 301900ND1320957
Benzo(g,h,i)perylene ug/kg R119007919-11250 45 301900ND1490946
Benzo(k)fluoranthene ug/kg 1900 70 24-11452 29 301900ND1320988
Benzoic Acid ug/kg 9460 40 10-11034 16 309460ND37603200
Benzyl alcohol ug/kg 3780 69 24-10660 14 303780ND26302290
bis(2-Chloroethoxy)methane ug/kg 1900 73 13-11960 21 301900ND13901130
bis(2-Chloroethyl) ether ug/kg 1900 70 10-13457 21 301900ND13301070
bis(2-Chloroisopropyl) ether ug/kg 1900 50 10-11352 4 301900ND948985
bis(2-Ethylhexyl)phthalate ug/kg 1900 91 10-12577 17 301900ND17301460
Butylbenzylphthalate ug/kg 1900 79 18-11081 3 301900ND15001540
Chrysene ug/kg 1900 72 30-11059 19 301900ND13601120
Di-n-butylphthalate ug/kg 1900 87 19-11279 10 301900ND16601490
Di-n-octylphthalate ug/kg 1900 70 17-10565 8 301900ND13301240
Dibenz(a,h)anthracene ug/kg R119008623-11151 50 301900ND1630975
Dibenzofuran ug/kg 1900 66 35-10363 5 301900ND12501190
Diethylphthalate ug/kg 1900 75 27-11370 7 301900ND14301330
Dimethylphthalate ug/kg 1900 85 26-11169 22 301900ND16101300
Fluoranthene ug/kg 1900 65 33-10976 17 301900ND12201450
Fluorene ug/kg 1900 68 32-11359 14 301900ND12901120
Hexachloro-1,3-butadiene ug/kg 1900 79 16-11663 22 301900ND15001200
Hexachlorobenzene ug/kg 1900 63 27-12067 6 301900ND12001270
Hexachlorocyclopentadiene ug/kg R119007510-10848 43 301900ND1420915
Hexachloroethane ug/kg 1900 61 10-11749 22 301900ND1150923
Indeno(1,2,3-cd)pyrene ug/kg R119008610-12252 50 301900ND1640977
Isophorone ug/kg 1900 75 28-11463 18 301900ND14201190
N-Nitroso-di-n-propylamine ug/kg 1900 60 27-11350 18 301900ND1140951
N-Nitrosodimethylamine ug/kg 1900 63 10-10948 28 301900ND1200907
N-Nitrosodiphenylamine ug/kg 1900 58 10-12871 20 301900ND11001340
Naphthalene ug/kg 1900 73 25-11061 18 301900ND13901160
Nitrobenzene ug/kg 1900 74 18-11462 18 301900ND13901170
Pentachlorophenol ug/kg 3780 67 10-12259 13 303780ND25202220
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1416904MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241876003
1416905
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenanthrene ug/kg 1900 72 30-11461 17 301900ND13601150
Phenol ug/kg 1900 71 11-10264 10 301900ND13401220
Pyrene ug/kg 1900 64 25-11671 10 301900ND12201340
2,4,6-Tribromophenol (S)%63 27-11068
2-Fluorobiphenyl (S)%71 30-11048
2-Fluorophenol (S)%58 13-11046
Nitrobenzene-d5 (S)%70 23-11058
Phenol-d6 (S)%65 22-11061
Terphenyl-d14 (S)%74 28-11073
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/33761
EPA 3510
EPA 8270
8270 Water MSSV
Associated Lab Samples: 92241876001, 92241876005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1417495
Associated Lab Samples:92241876001, 92241876005
Matrix: Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 03/24/15 16:22
1,2-Dichlorobenzene ug/L ND 10.0 03/24/15 16:22
1,3-Dichlorobenzene ug/L ND 10.0 03/24/15 16:22
1,4-Dichlorobenzene ug/L ND 10.0 03/24/15 16:22
1-Methylnaphthalene ug/L ND 10.0 03/24/15 16:22
2,4,5-Trichlorophenol ug/L ND 10.0 03/24/15 16:22
2,4,6-Trichlorophenol ug/L ND 10.0 03/24/15 16:22
2,4-Dichlorophenol ug/L ND 10.0 03/24/15 16:22
2,4-Dimethylphenol ug/L ND 10.0 03/24/15 16:22
2,4-Dinitrophenol ug/L ND 50.0 03/24/15 16:22
2,4-Dinitrotoluene ug/L ND 10.0 03/24/15 16:22
2,6-Dinitrotoluene ug/L ND 10.0 03/24/15 16:22
2-Chloronaphthalene ug/L ND 10.0 03/24/15 16:22
2-Chlorophenol ug/L ND 10.0 03/24/15 16:22
2-Methylnaphthalene ug/L ND 10.0 03/24/15 16:22
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/24/15 16:22
2-Nitroaniline ug/L ND 50.0 03/24/15 16:22
2-Nitrophenol ug/L ND 10.0 03/24/15 16:22
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/24/15 16:22
3,3'-Dichlorobenzidine ug/L 1.4J 20.0 03/24/15 16:22
3-Nitroaniline ug/L ND 50.0 03/24/15 16:22
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/24/15 16:22
4-Bromophenylphenyl ether ug/L ND 10.0 03/24/15 16:22
4-Chloro-3-methylphenol ug/L ND 20.0 03/24/15 16:22
4-Chloroaniline ug/L ND 20.0 03/24/15 16:22
4-Chlorophenylphenyl ether ug/L ND 10.0 03/24/15 16:22
4-Nitroaniline ug/L ND 20.0 03/24/15 16:22
4-Nitrophenol ug/L ND 50.0 03/24/15 16:22
Acenaphthene ug/L ND 10.0 03/24/15 16:22
Acenaphthylene ug/L ND 10.0 03/24/15 16:22
Aniline ug/L ND 10.0 03/24/15 16:22
Anthracene ug/L ND 10.0 03/24/15 16:22
Benzo(a)anthracene ug/L 1.3J 10.0 03/24/15 16:22
Benzo(a)pyrene ug/L 1.3J 10.0 03/24/15 16:22
Benzo(b)fluoranthene ug/L 1.3J 10.0 03/24/15 16:22
Benzo(g,h,i)perylene ug/L 1.2J 10.0 03/24/15 16:22
Benzo(k)fluoranthene ug/L 1.4J 10.0 03/24/15 16:22
Benzoic Acid ug/L ND 50.0 03/24/15 16:22
Benzyl alcohol ug/L ND 20.0 03/24/15 16:22
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/24/15 16:22
bis(2-Chloroethyl) ether ug/L ND 10.0 03/24/15 16:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1417495
Associated Lab Samples:92241876001, 92241876005
Matrix: Water
Analyzed
bis(2-Chloroisopropyl) ether ug/L ND 10.0 03/24/15 16:22
bis(2-Ethylhexyl)phthalate ug/L 1.8J 6.0 03/24/15 16:22
Butylbenzylphthalate ug/L ND 10.0 03/24/15 16:22
Chrysene ug/L 1.4J 10.0 03/24/15 16:22
Di-n-butylphthalate ug/L ND 10.0 03/24/15 16:22
Di-n-octylphthalate ug/L 1.1J 10.0 03/24/15 16:22
Dibenz(a,h)anthracene ug/L 1.1J 10.0 03/24/15 16:22
Dibenzofuran ug/L ND 10.0 03/24/15 16:22
Diethylphthalate ug/L ND 10.0 03/24/15 16:22
Dimethylphthalate ug/L ND 10.0 03/24/15 16:22
Fluoranthene ug/L ND 10.0 03/24/15 16:22
Fluorene ug/L ND 10.0 03/24/15 16:22
Hexachloro-1,3-butadiene ug/L ND 10.0 03/24/15 16:22
Hexachlorobenzene ug/L ND 10.0 03/24/15 16:22
Hexachlorocyclopentadiene ug/L ND 10.0 03/24/15 16:22
Hexachloroethane ug/L ND 10.0 03/24/15 16:22
Indeno(1,2,3-cd)pyrene ug/L 1.0J 10.0 03/24/15 16:22
Isophorone ug/L ND 10.0 03/24/15 16:22
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/24/15 16:22
N-Nitrosodimethylamine ug/L ND 10.0 03/24/15 16:22
N-Nitrosodiphenylamine ug/L ND 10.0 03/24/15 16:22
Naphthalene ug/L ND 10.0 03/24/15 16:22
Nitrobenzene ug/L ND 10.0 03/24/15 16:22
Pentachlorophenol ug/L ND 25.0 03/24/15 16:22
Phenanthrene ug/L ND 10.0 03/24/15 16:22
Phenol ug/L ND 10.0 03/24/15 16:22
Pyrene ug/L ND 10.0 03/24/15 16:22
2,4,6-Tribromophenol (S)%84 27-110 03/24/15 16:22
2-Fluorobiphenyl (S)%71 27-110 03/24/15 16:22
2-Fluorophenol (S)%33 12-110 03/24/15 16:22
Nitrobenzene-d5 (S)%68 21-110 03/24/15 16:22
Phenol-d6 (S)%24 10-110 03/24/15 16:22
Terphenyl-d14 (S)%95 31-107 03/24/15 16:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1417496LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 33.550 67 31-120
1,2-Dichlorobenzene ug/L 30.650 61 38-120
1,3-Dichlorobenzene ug/L 28.250 56 30-122
1,4-Dichlorobenzene ug/L 30.450 61 37-120
1-Methylnaphthalene ug/L 36.950 74 34-113
2,4,5-Trichlorophenol ug/L 40.350 81 43-113
2,4,6-Trichlorophenol ug/L 40.350 81 42-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1417496LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dichlorophenol ug/L 38.050 76 30-120
2,4-Dimethylphenol ug/L 37.650 75 29-111
2,4-Dinitrophenol ug/L 201250 80 19-132
2,4-Dinitrotoluene ug/L 43.650 87 58-128
2,6-Dinitrotoluene ug/L 45.850 92 54-129
2-Chloronaphthalene ug/L 38.950 78 43-117
2-Chlorophenol ug/L 32.450 65 37-120
2-Methylnaphthalene ug/L 34.350 69 33-120
2-Methylphenol(o-Cresol)ug/L 26.650 53 31-120
2-Nitroaniline ug/L 83.2100 83 48-121
2-Nitrophenol ug/L 41.250 82 25-116
3&4-Methylphenol(m&p Cresol)ug/L 23.650 47 23-120
3,3'-Dichlorobenzidine ug/L 85.5100 86 10-154
3-Nitroaniline ug/L 78.7100 79 43-115
4,6-Dinitro-2-methylphenol ug/L 96.3100 96 44-124
4-Bromophenylphenyl ether ug/L 44.650 89 34-113
4-Chloro-3-methylphenol ug/L 71.8100 72 31-110
4-Chloroaniline ug/L 77.5100 77 20-120
4-Chlorophenylphenyl ether ug/L 42.550 85 34-116
4-Nitroaniline ug/L 77.9100 78 46-128
4-Nitrophenol ug/L 67.7250 27 11-120
Acenaphthene ug/L 39.150 78 48-114
Acenaphthylene ug/L 39.450 79 48-112
Aniline ug/L 25.450 51 26-120
Anthracene ug/L 41.750 83 57-118
Benzo(a)anthracene ug/L 44.650 89 56-121
Benzo(a)pyrene ug/L 43.550 87 55-127
Benzo(b)fluoranthene ug/L 43.950 88 53-128
Benzo(g,h,i)perylene ug/L 41.450 83 54-125
Benzo(k)fluoranthene ug/L 43.350 87 51-123
Benzoic Acid ug/L 64.0250 26 10-120
Benzyl alcohol ug/L 61.2100 61 27-120
bis(2-Chloroethoxy)methane ug/L 40.150 80 32-120
bis(2-Chloroethyl) ether ug/L 41.450 83 33-111
bis(2-Chloroisopropyl) ether ug/L 35.950 72 15-120
bis(2-Ethylhexyl)phthalate ug/L 44.650 89 50-145
Butylbenzylphthalate ug/L 44.950 90 54-138
Chrysene ug/L 45.950 92 58-127
Di-n-butylphthalate ug/L 43.950 88 56-125
Di-n-octylphthalate ug/L 43.150 86 50-134
Dibenz(a,h)anthracene ug/L 43.150 86 53-129
Dibenzofuran ug/L 41.350 83 45-120
Diethylphthalate ug/L 42.850 86 53-120
Dimethylphthalate ug/L 42.450 85 55-116
Fluoranthene ug/L 39.650 79 57-125
Fluorene ug/L 42.450 85 53-118
Hexachloro-1,3-butadiene ug/L 32.250 64 23-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1417496LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 43.350 87 49-116
Hexachlorocyclopentadiene ug/L 33.350 67 26-158
Hexachloroethane ug/L 27.650 55 30-114
Indeno(1,2,3-cd)pyrene ug/L 43.450 87 55-128
Isophorone ug/L 39.750 79 31-118
N-Nitroso-di-n-propylamine ug/L 36.350 73 32-119
N-Nitrosodimethylamine ug/L 19.750 39 13-120
N-Nitrosodiphenylamine ug/L 42.950 86 43-120
Naphthalene ug/L 36.250 72 32-120
Nitrobenzene ug/L 39.050 78 33-110
Pentachlorophenol ug/L 70.7100 71 10-137
Phenanthrene ug/L 41.650 83 57-117
Phenol ug/L 15.350 31 10-120
Pyrene ug/L 44.350 89 55-122
2,4,6-Tribromophenol (S)%93 27-110
2-Fluorobiphenyl (S)%80 27-110
2-Fluorophenol (S)%37 12-110
Nitrobenzene-d5 (S)%73 21-110
Phenol-d6 (S)%25 10-110
Terphenyl-d14 (S)%98 31-107
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1417497MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241917005
1417498
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 42 10-11044 5 30100ND42.1 44.3
1,2-Dichlorobenzene ug/L 100 40 10-11038 6 30100ND40.4 37.9
1,3-Dichlorobenzene ug/L 100 37 10-11035 8 30100ND37.5 34.7
1,4-Dichlorobenzene ug/L 100 38 10-11037 4 30100ND38.3 36.7
1-Methylnaphthalene ug/L 100 45 14-11050 10 30100ND45.0 49.7
2,4,5-Trichlorophenol ug/L 100 50 19-10554 7 30100ND50.5 54.0
2,4,6-Trichlorophenol ug/L 100 51 13-10860 16 30100ND50.9 59.8
2,4-Dichlorophenol ug/L 100 38 29-11141 8 30100ND37.7 41.0
2,4-Dimethylphenol ug/L 100 36 21-10342 15 30100ND35.6 41.6
2,4-Dinitrophenol ug/L 500 56 10-10948 15 30500ND278238
2,4-Dinitrotoluene ug/L 100 61 27-10453 15 30100ND61.1 52.7
2,6-Dinitrotoluene ug/L 100 59 28-10152 13 30100ND59.3 52.0
2-Chloronaphthalene ug/L 100 43 14-10242 2 30100ND42.6 41.8
2-Chlorophenol ug/L 100 42 16-11041 0 30100ND41.6 41.5
2-Methylnaphthalene ug/L 100 39 13-11043 10 30100ND39.1 43.0
2-Methylphenol(o-Cresol)ug/L 100 37 19-11036 4 30100ND37.1 35.7
2-Nitroaniline ug/L 200 57 26-10351 12 30200ND114102
2-Nitrophenol ug/L 100 40 20-11045 13 30100ND39.7 45.3
3&4-Methylphenol(m&pCresol)ug/L 100 37 20-11033 11 30100ND37.2 33.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1417497MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241917005
1417498
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
3,3'-Dichlorobenzidine ug/L 200 53 25-11247 12 30200ND10694.0
3-Nitroaniline ug/L 200 55 29-11050 10 30200ND111100
4,6-Dinitro-2-methylphenol ug/L 200 56 10-11749 13 30200ND11298.4
4-Bromophenylphenyl ether ug/L 100 55 20-10550 9 30100ND55.1 50.5
4-Chloro-3-methylphenol ug/L 200 51 22-11053 4 30200ND103107
4-Chloroaniline ug/L 200 43 20-10042 4 30200ND86.7 83.3
4-Chlorophenylphenyl ether ug/L 100 52 19-10247 12 30100ND52.3 46.5
4-Nitroaniline ug/L 200 61 29-11054 11 30200ND121109
4-Nitrophenol ug/L 500 38 10-11036 6 30500ND190179
Acenaphthene ug/L 100 46 17-10043 7 30100ND45.8 42.7
Acenaphthylene ug/L 100 46 21-10044 5 30100ND46.0 43.8
Aniline ug/L 100 35 10-11039 11 30100ND34.8 39.0
Anthracene ug/L 100 57 24-10952 10 30100ND56.9 51.6
Benzo(a)anthracene ug/L 100 57 22-11751 11 30100ND56.7 50.7
Benzo(a)pyrene ug/L 100 59 23-10451 14 30100ND58.8 50.9
Benzo(b)fluoranthene ug/L 100 56 23-10359 4 30100ND56.5 58.6
Benzo(g,h,i)perylene ug/L 100 54 18-11148 11 30100ND54.1 48.3
Benzo(k)fluoranthene ug/L 100 58 22-11357 1 30100ND58.2 57.4
Benzoic Acid ug/L 500 18 10-11017 30500ND89.5J 86.5J
Benzyl alcohol ug/L 200 39 19-10140 2 30200ND78.7 80.2
bis(2-Chloroethoxy)methane ug/L 100 34 22-11040 17 30100ND33.5 39.9
bis(2-Chloroethyl) ether ug/L 100 41 16-11041 0 30100ND40.9 40.9
bis(2-Chloroisopropyl) ether ug/L 100 36 14-11034 5 30100ND35.7 33.8
bis(2-Ethylhexyl)phthalate ug/L 100 64 23-10254 17 30100ND63.8 53.8
Butylbenzylphthalate ug/L 100 76 25-11064 17 30100ND75.6 64.0
Chrysene ug/L 100 56 23-11550 11 30100ND56.3 50.4
Di-n-butylphthalate ug/L 100 63 26-11071 13 30100ND62.5 71.2
Di-n-octylphthalate ug/L 100 58 22-11049 17 30100ND58.4 49.4
Dibenz(a,h)anthracene ug/L 100 54 21-11254 0 30100ND53.9 54.0
Dibenzofuran ug/L 100 52 19-10248 8 30100ND51.7 47.5
Diethylphthalate ug/L 100 63 29-11055 13 30100ND63.1 55.3
Dimethylphthalate ug/L 100 60 27-11054 12 30100ND60.2 53.5
Fluoranthene ug/L 100 57 23-11253 7 30100ND57.1 53.0
Fluorene ug/L 100 54 22-10450 8 30100ND54.2 50.1
Hexachloro-1,3-butadiene ug/L 100 41 10-11040 4 30100ND41.1 39.7
Hexachlorobenzene ug/L 100 52 21-11651 3 30100ND52.4 50.7
Hexachlorocyclopentadiene ug/L 100 39 10-11045 16 30100ND38.6 45.5
Hexachloroethane ug/L 100 42 10-11037 13 30100ND42.5 37.1
Indeno(1,2,3-cd)pyrene ug/L 100 56 20-11356 0 30100ND55.8 55.9
Isophorone ug/L M11003650-15042 16 30100ND35.8 41.8
N-Nitroso-di-n-propylamine ug/L 100 42 21-10542 1 30100ND42.1 41.6
N-Nitrosodimethylamine ug/L 100 43 10-11045 6 30100ND42.9 45.3
N-Nitrosodiphenylamine ug/L 100 54 23-10749 10 30100ND54.4 49.4
Naphthalene ug/L 100 43 10-11041 4 30100ND42.6 41.0
Nitrobenzene ug/L 100 36 20-11043 18 30100ND36.4 43.4
Pentachlorophenol ug/L 200 54 10-11845 19 30200ND10889.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1417497MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92241917005
1417498
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenanthrene ug/L 100 56 24-10650 11 30100ND56.2 50.3
Phenol ug/L 100 25 12-11029 14 30100ND25.0 28.8
Pyrene ug/L R11006824-11450 31 30100ND68.1 49.8
2,4,6-Tribromophenol (S)%52 27-11051
2-Fluorobiphenyl (S)%40 27-11048
2-Fluorophenol (S)%30 12-11031
Nitrobenzene-d5 (S)%35 21-11041
Phenol-d6 (S)%23 10-11027
Terphenyl-d14 (S)%67 31-10752
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 54
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/7640
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92241876002, 92241876003, 92241876004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92241877001
1415970SAMPLE DUPLICATE:
Percent Moisture %24.3 R1332517.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92241942003
1415971SAMPLE DUPLICATE:
Percent Moisture %23.4 0 2523.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 54
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.F3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 54
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92241876
Crescent NODA Site 71157713-A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92241876002 OEXT/33747 MSSV/10455B-2 6'-8'EPA 3546 EPA 8270
92241876003 OEXT/33747 MSSV/10455B-3 22'-24'EPA 3546 EPA 8270
92241876004 OEXT/33747 MSSV/10455B-4 18'-20'EPA 3546 EPA 8270
92241876001 OEXT/33761 MSSV/10454B-1 EPA 3510 EPA 8270
92241876005 OEXT/33761 MSSV/10454B-8 EPA 3510 EPA 8270
92241876001 MSV/30901B-1 EPA 8260
92241876005 MSV/30901B-8 EPA 8260
92241876002 MSV/30860B-2 6'-8'EPA 8260
92241876003 MSV/30860B-3 22'-24'EPA 8260
92241876004 MSV/30860B-4 18'-20'EPA 8260
92241876002 PMST/7640B-2 6'-8'ASTM D2974-87
92241876003 PMST/7640B-3 22'-24'ASTM D2974-87
92241876004 PMST/7640B-4 18'-20'ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 03/26/2015 04:56 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 54
Page53of54
Page54of54
Sample ID SB-1 SB-3 SB-4 SB-5 SB-6 SB-9 SB-10 SB-12
Date 3/14/2007 3/14/2007 3/14/2007 3/14/2007 3/14/2007 3/15/2007 3/15/2007 3/15/2007
Depth 1.5-2.5 ft 1.5-2.5 ft 14-15 ft 1.5-2.5 ft 1.5-2.5 ft 1.5-2.5 ft 1.5-2.5 ft 1.5-2.5 ft 7-10 ft 1.5-2.5 ft 14-15 ft 1.5-2.5 ft 1.5-2.5 ft 1.5-2.5 ft 10-11 ft 1.5-2.5 ft 1.5-2.5 ft 16-17 ft
Units mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
VOCs (8260B)
Acetone 0.16 0.1 NA <0.058 <0.067 <0.061 <0.068 0.16 NA 0.24 NA 0.16 <0.054 0.072 NA <0.062 <0.062 NA 2,800 14,000 54,000 ----
2-Butanone (MEK)0.018 <0.012 NA <0.012 <0.013 <0.012 <0.014 0.016 NA 0.026 NA <0.012 <0.011 <0.014 NA <0.012 <0.012 NA 4,400 22,000 110,000 ----
Naphthalene <0.0064 <0.0060 NA <0.0058 <0.0067 <0.0061 <0.0068 <0.0063 NA 0.046 NA <0.0061 <0.0054 <0.0068 NA <0.0062 <0.0062 NA 11.2 56 190 ----
SVOCs (8270C)
Acenaphthylene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 0.89 0.44 NS NS NS ----
Anthracene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 1.7 0.8 4,400 22,000 100,000 ----
Benzo(a)anthracene <0.43 0.4 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 2.5 1.8 0.62 0.62 2.1 ----
Benzo(b)fluoranthene <0.43 0.58 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 2.4 1.6 0.62 0.62 2.1 ----
Benzo(k)fluoranthene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 0.97 0.51 6.2 6.2 210 ----
Benzo(g,h,i)perylene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 0.89 0.5 NS NS NS ----
Benzo(a)pyrene <0.43 0.43 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 1.9 1.1 0.062 0.06 0.21 ----
Chrysene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 2.2 1.2 62 62 210 ----
Fluoranthene <0.43 0.58 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA 0.52 NA <0.40 <0.36 <0.42 NA <0.40 8.1 <7.8 460 2,300 22,000 ----
Fluorene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 0.44 <0.39 540 2,700 26,000 ----
Indeno(1,2,3-cd)pyrene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 0.85 0.5 0.62 0.62 2.1 ----
Naphthalene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 0.43 0.42 11.2 56 190 ----
Phenanthrene <0.43 <0.40 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA 0.52 NA <0.40 <0.36 <0.42 NA <0.40 9 <7.8 NS NS NS ----
Benzylbutyl phthalate <0.43 <0.40 <0.37 <0.38 1.3 0.56 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 <0.41 <0.39 2,400 12,000 100,000 ----
Bis(2-ethylhexyl)phthalate <0.43 0.41 <0.37 <0.38 0.85 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 1.1 <0.39 35 35 120 ----
Di-n-butyl phthalate <0.43 <0.40 <0.37 <0.38 0.55 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 <0.41 <0.39 1,220 6,100 62,000 ----
Pyrene <0.43 0.89 <0.37 <0.38 <0.44 <0.40 <0.45 <0.41 NA <0.42 NA <0.40 <0.36 <0.42 NA <0.40 6.5 <7.8 460 2,300 29,000 ----
Metals (6010B)
Arsenic <6.4 <1.2 NA <1.2 <1.3 <6.1 <6.8 <6.3 NA <6.4 NA 3 1.1 <6.4 NA <6.2 <6.2 NA 4.4 0.39 1.6 1.6-180
Barium 110 120 NA 230 66 230 45 57 NA 40 NA 120 81 51 NA 72 170 NA NS 5,400 67,000 4.1-420
Cadmium 1.7 1.3 NA 0.96 0.84 1.5 1.8 <1.6 NA 2.8 NA 3 1.6 8.5 NA67.7 NA 7.4 37 450 0.54-5.8
Chromium 120 49 NA 14 49 15 32 150 53 200 38 54 2 240 500 38 92 NA 44 30 64 2-150
Lead 43 100 NA 17 16 21 32 23 NA 39 NA 21 6.6 29 NA 22 27 NA 400 400 800 7.2-52
Selenium 9 2.4 NA 2 <34 11 <6.8 <6.3 NA <6.4 NA 2.2 <1.1 <6.4 NA <6.2 <6.2 NA 78 390 5100 NS
Metals (3060A/7196A)
Chromium IV NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2.4 NA NA NA 44 30 64 NS
Chromium III NA NA NA NA NA NA NA NA NA NA NA NA NA NA 390 NA NA NA 24,000 100,000 100,000 NS
Metals (7471)
Mercury 0.033 0.033 NA <0.023 0.039 <0.024 0.052 <0.025 NA 0.097 NA <0.024 <0.022 0.067 NA <0.025 <0.025 NA 4.6 23 310 0.02-0.16
Notes:
Bold values exceed screening levels.
1. NC DENR Data Table, Background Metals in NC Soils, August 31, 2006.
Table 1
Summary of Soil Analytical Detections
Former Newco Fibre Company
Charlotte, North Carolina
H&H Job No. MFP-005
SB-2 SB-7 SB-8 SB-11 SB-13 NC IHSB
Health-Based
SRGs
(mg/kg)
EPA Region IX
Residential
PRGs
(mg/kg)
NC DENR
Background NC
Soils Range1
(mg/kg)
EPA Region IX
Industrial PRGs
(mg/kg)
3/15/2007
All concentrations shown in milligrams per kilogram (mg/kg); only those analytes detected are shown in this table; EPA method follows the analysis in parenthesis.
VOCs=volatile organic compounds; SVOCs=semi-volatile organic compounds; NA=not analyzed; NS=not specified; PRGs=preliminary remediation goals.
3/14/2007 3/14/2007 3/14/2007 3/15/2007
Sample ID SB-9 SB-10 TW-1 TW-2 TW-3
Date 3/15/2007 3/15/2007 5/18/2007 5/18/2007 5/18/2007
Units µg/L µg/L µg/L µg/L µg/L µg/L
Metals(6010B)
Barium 2,000 98 550 58 59 54
Chromium 50 <10 20 <10 <10 <10
Lead 15 5.6 35 <5 <5 <5
Selenium NS <20 <20 26 <20 <20
VOCs (8260B)
Xylenes, Total 530 <3 3.4 <3 <3 <3
SVOCs (8270C)varies BDL BDL BDL BDL BDL
Notes:
H&H Job No. MFP-005
NC 2L
Standards
All concentrations shown in micrograms per liter (µg/L); only those analytes detected are shown in table;
EPA method number follows analysis in parenthesis; BDL=below detection limits;
Bold values exceed NC 2L Standards.
Table 2
Summary of Groundwater Analytical Detections
Former Newco Fibre Company
Charlotte, North Carolina
Figure
DIAGRAM IS FOR GENERAL LOCATION ONLY,AND IS NOT INTENDED FOR CONSTRUCTION
PURPOSES 2020-E Starita Road
Charlotte, NC
BORING LOCATION PLANProject Manager:
Drawn by:
Checked by:
Approved by:
CLC Project No.
File Name:
Date:
Scale:
71157713A
ALF
August 2015CLC
CLC
1” ~ 125’
430 E. 36th St
Crescent Noda Site
430 East 36th Street
Charlotte, North Carolina
denotes approximate site
boundary
denotes approximate railroad
right-of-way
denotes approximate location
of August 2015 soil borings
Parking
ULTIMATE
GYM
CHOP
SHOP
FUTURE LIGHT
RAIL STATION
FLOW
FABRICATION
Dust Collection
Building
(Former Refinery
Property)
B-3
B-2
B-4
B-1
B-5
B-6
B-7
B-8
denotes approximate location
of March 2015 soil borings
B-10
B-9
B-11
B-13
B-12
2
Table 1
Summary of Soil Sampling
Soil Analytical Results
Cresent Noda
Charlotte, North Carolina
Terracon Project: 71157713A
Sample
I.D.
Sample Depth
(feet)Date Collected
AcetoneMethyleneChlorideTetrachloroethene1,2,4-TrimethylbenzeneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluorantheneChryseneDibenz(a,h)anthraceneFluorantheneIndeno(1,2,3-cd)pyrenePhenanthrenePyreneB-2 22-24 3/18/2015
B-3 6-8 3/18/2015
B-4 18-20 3/18/2015 ND ND 0.0068 ND
B-9 14-15.5 8/5/2015 ND 0.0109J ND 0.0022J
B-10 19-20 8/5/2015 ND 0.0115J ND ND 0.181J 0.542 0.586 0.705 0.445 0.279J 0.563 0.126J 1.160 0.359J 0.707 0.895
B-11 19-20 8/5/2015 0.0187J 0.0064J ND ND
B-12 13-14 8/5/2015 ND 0.0532 0.0016J ND
B-13 15-16 8/5/2015 ND 0.106J 0.141J 0.180J ND ND 0.121J ND 0.231J ND 0.110J 0.213J
24 0.023 0.005 6.7 660 0.18 0.059 0.6 7,800 5.9 18 0.19 330 3.5 68 220
12000 57 16 12 3400 0.15 0.015 0.15 NA 1.5 15 0.015 460 0.15 NA 340
100000 640 78 48 46000 2.9 0.290 2.9 NA 29 290 0.290 6000 2.9 NA 4600
• Laboratory results reported in milligrams per kilogram (mg/kg).
• ND = Not Detected at concentrations above the method detection limit.
NA = Not Applicable
Exceedance of Protection of Groundwater standard depicted in bold font
Exceedance of Residential PSRG depicted by gray shading
Exceedance of Industrial PSRG depicted by yellow shading
Not Detected
EPA 8270
Semi-Volatiles
Not Detected
Not Detected
Not Detected
Not Detected
Preliminary Industrial Soil Remediation Goal (mg/kg)
Analytical Method
Contaminant of Concern
Preliminary Residential Soil Remediation Goal (mg/kg)
EPA 8260
Volatiles
Not Detected
Protection of Groundwater Preliminary Soil Remediation
Goal (mg/kg)
Not Detected
Not Detected
Not Detected
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
SC Certification No. 99012
NC Drinking Water Cert No. 37735
Case Narrative
01/21/2016
Geoscience Group
Tom Hassett
500-K Clanton Rd.
Charlotte, NC 28217
Project: 1201 Central Ave
Lab Submittal Date: 01/14/2016
Prism Work Order: 6010230
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 229
Data Qualifiers Key Reference:
A Due to an instrument problem, there is no Low-Level CCV at the end of this batch as required by SW-846 Method
6010C.
Aa MB greater than one half of the RL. Recovery of initial Low-level CCV (195%) is greater than the upper control limit
(130%). Result might have a slight high bias.
Ab Recovery of initial Low-level CCV (149%) is greater than the upper control limit (130%). Result might have a slight
high bias.
BH MB greater than one half of the RL, but the sample concentrations are greater than 10x the MB.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
M Matrix spike outside of the control limits.
MI Matrix spike outside of the control limits. Matrix interference suspected.
SR Surrogate recovery outside the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 229
Sample Receipt Summary
01/21/2016
Prism Work Order: 6010230
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6010230-01 01/13/16HA-1-2 01/14/16Solid
6010230-02 01/13/16HA-1-5 01/14/16Solid
6010230-03 01/13/16HA-1-9 01/14/16Solid
6010230-04 01/13/16HA-2-2 01/14/16Solid
6010230-05 01/13/16HA-2-5 01/14/16Solid
6010230-06 01/13/16HA-2-9 01/14/16Solid
6010230-07 01/13/16HA-3-2 01/14/16Solid
6010230-08 01/13/16HA-3-5 01/14/16Solid
6010230-09 01/13/16HA-3-9 01/14/16Solid
6010230-10 01/13/16HA-4-2 01/14/16Solid
6010230-11 01/13/16HA-4-5 01/14/16Solid
6010230-12 01/13/16HA-4-9 01/14/16Solid
6010230-13 01/13/16HA-5-2 01/14/16Solid
6010230-14 01/13/16HA-5-5 01/14/16Solid
6010230-15 01/13/16HA-5-9 01/14/16Solid
6010230-16 01/13/16HA-6-2 01/14/16Solid
6010230-17 01/13/16HA-6-5 01/14/16Solid
6010230-18 01/13/16HA-6-9 01/14/16Solid
6010230-19 01/13/16HA-7-2 01/14/16Solid
6010230-20 01/13/16HA-7-5 01/14/16Solid
6010230-21 01/13/16HA-7-9 01/14/16Solid
6010230-22 01/13/16HA-8-2 01/14/16Solid
6010230-23 01/13/16HA-8-5 01/14/16Solid
6010230-24 01/13/16HA-8-9 01/14/16Solid
6010230-25 01/13/16HA-9-2 01/14/16Solid
6010230-26 01/13/16HA-9-5 01/14/16Solid
6010230-27 01/13/16HA-9-9 01/14/16Solid
6010230-28 01/13/16HA-10-2 01/14/16Solid
6010230-29 01/13/16HA-10-5 01/14/16Solid
6010230-30 01/13/16HA-10-9 01/14/16Solid
6010230-31 01/13/16HA-11-2 01/14/16Solid
6010230-32 01/13/16HA-11-5 01/14/16Solid
6010230-33 01/13/16HA-11-9 01/14/16Solid
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 229
Samples were received in good condition at 3.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 229
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6010230
01/21/2016
Summary of Detections
3.0 Ab mg/kg dry6010230-01 HA-1-2 Arsenic *6010C
49 mg/kg dry6010230-01 HA-1-2 Barium *6010C
2.1 Aa mg/kg dry6010230-01 HA-1-2 Chromium *6010C
4.7 mg/kg dry6010230-01 HA-1-2 Lead *6010C
2.3 Ab mg/kg dry6010230-02 HA-1-5 Arsenic *6010C
110 mg/kg dry6010230-02 HA-1-5 Barium *6010C
3.3 Aa mg/kg dry6010230-02 HA-1-5 Chromium *6010C
4.3 mg/kg dry6010230-02 HA-1-5 Lead *6010C
2.2 Ab mg/kg dry6010230-03 HA-1-9 Arsenic *6010C
94 mg/kg dry6010230-03 HA-1-9 Barium *6010C
1.9 Aa mg/kg dry6010230-03 HA-1-9 Chromium *6010C
3.9 mg/kg dry6010230-03 HA-1-9 Lead *6010C
0.028 mg/kg dry6010230-04 HA-2-2 Mercury *7471B
3.0 Ab mg/kg dry6010230-04 HA-2-2 Arsenic *6010C
54 mg/kg dry6010230-04 HA-2-2 Barium *6010C
24 Aa, BH mg/kg dry6010230-04 HA-2-2 Chromium *6010C
5.1 mg/kg dry6010230-04 HA-2-2 Lead *6010C
3.6 Ab mg/kg dry6010230-05 HA-2-5 Arsenic *6010C
82 mg/kg dry6010230-05 HA-2-5 Barium *6010C
3.8 Aa, BH mg/kg dry6010230-05 HA-2-5 Chromium *6010C
13 mg/kg dry6010230-05 HA-2-5 Lead *6010C
1.6 Ab mg/kg dry6010230-06 HA-2-9 Arsenic *6010C
80 mg/kg dry6010230-06 HA-2-9 Barium *6010C
5.0 Aa, BH mg/kg dry6010230-06 HA-2-9 Chromium *6010C
7.1 mg/kg dry6010230-06 HA-2-9 Lead *6010C
3.5 Ab mg/kg dry6010230-07 HA-3-2 Arsenic *6010C
150 mg/kg dry6010230-07 HA-3-2 Barium *6010C
11 Aa, BH mg/kg dry6010230-07 HA-3-2 Chromium *6010C
11 mg/kg dry6010230-07 HA-3-2 Lead *6010C
2.4 Ab mg/kg dry6010230-08 HA-3-5 Arsenic *6010C
44 mg/kg dry6010230-08 HA-3-5 Barium *6010C
1.7 Aa mg/kg dry6010230-08 HA-3-5 Chromium *6010C
3.8 mg/kg dry6010230-08 HA-3-5 Lead *6010C
2.2 Ab mg/kg dry6010230-09 HA-3-9 Arsenic *6010C
50 mg/kg dry6010230-09 HA-3-9 Barium *6010C
2.6 Aa mg/kg dry6010230-09 HA-3-9 Chromium *6010C
5.3 mg/kg dry6010230-09 HA-3-9 Lead *6010C
1.2 Ab mg/kg dry6010230-10 HA-4-2 Arsenic *6010C
35 mg/kg dry6010230-10 HA-4-2 Barium *6010C
0.29 Aa mg/kg dry6010230-10 HA-4-2 Chromium *6010C
1.6 mg/kg dry6010230-10 HA-4-2 Lead *6010C
1.7 Ab mg/kg dry6010230-11 HA-4-5 Arsenic *6010C
28 mg/kg dry6010230-11 HA-4-5 Barium *6010C
0.41 Aa mg/kg dry6010230-11 HA-4-5 Chromium *6010C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 229
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6010230
01/21/2016
Summary of Detections
4.0 mg/kg dry6010230-11 HA-4-5 Lead *6010C
1.5 Ab mg/kg dry6010230-12 HA-4-9 Arsenic *6010C
31 mg/kg dry6010230-12 HA-4-9 Barium *6010C
0.28 Aa mg/kg dry6010230-12 HA-4-9 Chromium *6010C
2.1 mg/kg dry6010230-12 HA-4-9 Lead *6010C
0.052 mg/kg dry6010230-13 HA-5-2 Mercury *7471B
2.1 Ab mg/kg dry6010230-13 HA-5-2 Arsenic *6010C
25 mg/kg dry6010230-13 HA-5-2 Barium *6010C
12 Aa, BH mg/kg dry6010230-13 HA-5-2 Chromium *6010C
18 mg/kg dry6010230-13 HA-5-2 Lead *6010C
0.033 mg/kg dry6010230-14 HA-5-5 Mercury *7471B
1.9 Ab mg/kg dry6010230-14 HA-5-5 Arsenic *6010C
22 mg/kg dry6010230-14 HA-5-5 Barium *6010C
3.7 Aa mg/kg dry6010230-14 HA-5-5 Chromium *6010C
5.3 mg/kg dry6010230-14 HA-5-5 Lead *6010C
1.6 Ab mg/kg dry6010230-15 HA-5-9 Arsenic *6010C
22 mg/kg dry6010230-15 HA-5-9 Barium *6010C
7.2 BH mg/kg dry6010230-15 HA-5-9 Chromium *6010C
3.0 mg/kg dry6010230-15 HA-5-9 Lead *6010C
0.056 mg/kg dry6010230-16 HA-6-2 Mercury *7471B
3.8 Ab mg/kg dry6010230-16 HA-6-2 Arsenic *6010C
13 mg/kg dry6010230-16 HA-6-2 Barium *6010C
35 Aa, BH mg/kg dry6010230-16 HA-6-2 Chromium *6010C
5.1 mg/kg dry6010230-16 HA-6-2 Lead *6010C
2.2 Ab mg/kg dry6010230-17 HA-6-5 Arsenic *6010C
18 mg/kg dry6010230-17 HA-6-5 Barium *6010C
7.1 Aa, BH mg/kg dry6010230-17 HA-6-5 Chromium *6010C
5.9 mg/kg dry6010230-17 HA-6-5 Lead *6010C
2.2 Ab mg/kg dry6010230-18 HA-6-9 Arsenic *6010C
41 mg/kg dry6010230-18 HA-6-9 Barium *6010C
8.1 Aa, BH mg/kg dry6010230-18 HA-6-9 Chromium *6010C
6.9 mg/kg dry6010230-18 HA-6-9 Lead *6010C
0.035 mg/kg dry6010230-19 HA-7-2 Mercury *7471B
2.3 A mg/kg dry6010230-19 HA-7-2 Arsenic *6010C
11 A mg/kg dry6010230-19 HA-7-2 Barium *6010C
9.2 A mg/kg dry6010230-19 HA-7-2 Chromium *6010C
5.2 A mg/kg dry6010230-19 HA-7-2 Lead *6010C
0.99 A mg/kg dry6010230-19 HA-7-2 Silver *6010C
0.054 mg/kg dry6010230-20 HA-7-5 Mercury *7471B
1.7 A mg/kg dry6010230-20 HA-7-5 Arsenic *6010C
23 A mg/kg dry6010230-20 HA-7-5 Barium *6010C
6.2 A mg/kg dry6010230-20 HA-7-5 Chromium *6010C
6.1 A mg/kg dry6010230-20 HA-7-5 Lead *6010C
0.90 A mg/kg dry6010230-20 HA-7-5 Silver *6010C
1.9 A mg/kg dry6010230-21 HA-7-9 Arsenic *6010C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 229
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6010230
01/21/2016
Summary of Detections
52 A mg/kg dry6010230-21 HA-7-9 Barium *6010C
2.8 A mg/kg dry6010230-21 HA-7-9 Chromium *6010C
7.0 A mg/kg dry6010230-21 HA-7-9 Lead *6010C
0.71 A mg/kg dry6010230-21 HA-7-9 Silver *6010C
2.6 Ab mg/kg dry6010230-22 HA-8-2 Arsenic *6010C
85 mg/kg dry6010230-22 HA-8-2 Barium *6010C
3.9 Aa, BH mg/kg dry6010230-22 HA-8-2 Chromium *6010C
6.2 mg/kg dry6010230-22 HA-8-2 Lead *6010C
2.5 Ab mg/kg dry6010230-23 HA-8-5 Arsenic *6010C
190 mg/kg dry6010230-23 HA-8-5 Barium *6010C
1.4 Aa mg/kg dry6010230-23 HA-8-5 Chromium *6010C
3.9 mg/kg dry6010230-23 HA-8-5 Lead *6010C
0.013 J mg/kg dry6010230-23 HA-8-5 Acetone 8260B
2.8 A mg/kg dry6010230-24 HA-8-9 Arsenic *6010C
120 A mg/kg dry6010230-24 HA-8-9 Barium *6010C
2.4 A mg/kg dry6010230-24 HA-8-9 Chromium *6010C
5.1 A mg/kg dry6010230-24 HA-8-9 Lead *6010C
0.82 A mg/kg dry6010230-24 HA-8-9 Silver *6010C
2.2 A mg/kg dry6010230-25 HA-9-2 Arsenic *6010C
82 A mg/kg dry6010230-25 HA-9-2 Barium *6010C
2.4 A mg/kg dry6010230-25 HA-9-2 Chromium *6010C
1.0 A mg/kg dry6010230-25 HA-9-2 Lead *6010C
0.32 A mg/kg dry6010230-25 HA-9-2 Silver *6010C
0.044 J mg/kg dry6010230-25 HA-9-2 Acetone 8260B
3.9 A mg/kg dry6010230-26 HA-9-5 Arsenic *6010C
90 A mg/kg dry6010230-26 HA-9-5 Barium *6010C
3.6 A mg/kg dry6010230-26 HA-9-5 Chromium *6010C
2.2 A mg/kg dry6010230-26 HA-9-5 Lead *6010C
3.0 A mg/kg dry6010230-27 HA-9-9 Arsenic *6010C
52 A mg/kg dry6010230-27 HA-9-9 Barium *6010C
4.3 A mg/kg dry6010230-27 HA-9-9 Chromium *6010C
3.4 A mg/kg dry6010230-27 HA-9-9 Lead *6010C
0.66 A mg/kg dry6010230-27 HA-9-9 Silver *6010C
0.0065 J mg/kg dry6010230-27 HA-9-9 Acetone 8260B
2.2 mg/kg dry6010230-28 HA-10-2 Arsenic *6010C
42 mg/kg dry6010230-28 HA-10-2 Barium *6010C
7.4 mg/kg dry6010230-28 HA-10-2 Chromium *6010C
8.5 mg/kg dry6010230-28 HA-10-2 Lead *6010C
1.4 mg/kg dry6010230-28 HA-10-2 Silver *6010C
2.6 mg/kg dry6010230-29 HA-10-5 Arsenic *6010C
87 mg/kg dry6010230-29 HA-10-5 Barium *6010C
4.6 mg/kg dry6010230-29 HA-10-5 Chromium *6010C
5.9 mg/kg dry6010230-29 HA-10-5 Lead *6010C
1.2 mg/kg dry6010230-29 HA-10-5 Silver *6010C
2.6 mg/kg dry6010230-30 HA-10-9 Arsenic *6010C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 229
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6010230
01/21/2016
Summary of Detections
140 mg/kg dry6010230-30 HA-10-9 Barium *6010C
3.2 mg/kg dry6010230-30 HA-10-9 Chromium *6010C
5.3 mg/kg dry6010230-30 HA-10-9 Lead *6010C
0.82 mg/kg dry6010230-30 HA-10-9 Silver *6010C
0.0058 J mg/kg dry6010230-30 HA-10-9 Acetone 8260B
0.026 mg/kg dry6010230-31 HA-11-2 Mercury *7471B
3.9 mg/kg dry6010230-31 HA-11-2 Arsenic *6010C
26 mg/kg dry6010230-31 HA-11-2 Barium *6010C
23 mg/kg dry6010230-31 HA-11-2 Chromium *6010C
7.0 mg/kg dry6010230-31 HA-11-2 Lead *6010C
1.3 mg/kg dry6010230-31 HA-11-2 Silver *6010C
2.5 mg/kg dry6010230-32 HA-11-5 Arsenic *6010C
26 mg/kg dry6010230-32 HA-11-5 Barium *6010C
11 mg/kg dry6010230-32 HA-11-5 Chromium *6010C
4.1 mg/kg dry6010230-32 HA-11-5 Lead *6010C
1.4 mg/kg dry6010230-32 HA-11-5 Silver *6010C
2.2 mg/kg dry6010230-33 HA-11-9 Arsenic *6010C
32 mg/kg dry6010230-33 HA-11-9 Barium *6010C
13 mg/kg dry6010230-33 HA-11-9 Chromium *6010C
3.6 mg/kg dry6010230-33 HA-11-9 Lead *6010C
1.2 mg/kg dry6010230-33 HA-11-9 Silver *6010C
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-2
Prism Sample ID: 6010230-01
Prism Work Order: 6010230
Time Collected: 01/13/16 09:26
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
71.9 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0721,2,4-Trichlorobenzene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0701,2-Dichlorobenzene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0651,3-Dichlorobenzene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0671,4-Dichlorobenzene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0891-Methylnaphthalene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0862,4,6-Trichlorophenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0892,4-Dichlorophenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0702,4-Dimethylphenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0642,4-Dinitrophenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0562,4-Dinitrotoluene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0612,6-Dinitrotoluene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0672-Chloronaphthalene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0652-Chlorophenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0732-Methylnaphthalene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0592-Methylphenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0842-Nitrophenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0913,3’-Dichlorobenzidine
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0573/4-Methylphenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0694,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0794-Bromophenyl phenyl ether
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0644-Chloro-3-methylphenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0554-Chloroaniline
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0604-Chlorophenyl phenyl ether
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.0714-Nitrophenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.062Acenaphthene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.067Acenaphthylene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.074Anthracene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.061Azobenzene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.060Benzo(a)anthracene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.050Benzo(a)pyrene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.053Benzo(b)fluoranthene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.050Benzo(g,h,i)perylene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.060Benzo(k)fluoranthene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.039Benzoic Acid
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.061Benzyl alcohol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.080bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.065Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.078Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.068Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-2
Prism Sample ID: 6010230-01
Prism Work Order: 6010230
Time Collected: 01/13/16 09:26
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.065Butyl benzyl phthalate
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.058Chrysene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.056Dibenzo(a,h)anthracene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.070Dibenzofuran
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.063Diethyl phthalate
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.061Dimethyl phthalate
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.065Di-n-butyl phthalate
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.056Di-n-octyl phthalate
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.059Fluoranthene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.066Fluorene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.073Hexachlorobenzene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.083Hexachlorobutadiene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.082Hexachlorocyclopentadiene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.077Hexachloroethane
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.053Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.062Isophorone
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.074Naphthalene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.065Nitrobenzene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.072N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.070N-Nitrosodiphenylamine
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.054Pentachlorophenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.060Phenanthrene
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.068Phenol
BRL 8270D P6A019810.46 1/14/16 17:49 JMVmg/kg dry 0.061Pyrene
Surrogate Recovery Control Limits
39-13278 %2,4,6-Tribromophenol
44-11571 %2-Fluorobiphenyl
35-11568 %2-Fluorophenol
37-12275 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12780 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.027 1/15/16 11:55 JABmg/kg dry 0.0017Mercury
3.0 *6010C P6A021110.34 1/15/16 21:05 bgmAbmg/kg dry 0.076Arsenic
49 *6010C P6A021110.69 1/15/16 21:05 bgmmg/kg dry 0.37Barium
BRL *6010C P6A021110.34 1/15/16 21:05 bgmmg/kg dry 0.0073Cadmium
2.1 *6010C P6A021110.34 1/15/16 21:05 bgmAamg/kg dry 0.047Chromium
4.7 *6010C P6A021110.34 1/15/16 21:05 bgmmg/kg dry 0.036Lead
BRL *6010C P6A021110.69 1/15/16 21:05 bgmmg/kg dry 0.050Selenium
BRL *6010C P6A021110.34 1/15/16 21:05 bgmmg/kg dry 0.0056Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000501,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-2
Prism Sample ID: 6010230-01
Prism Work Order: 6010230
Time Collected: 01/13/16 09:26
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000411,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000541,1,2-Trichloroethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000331,1-Dichloropropylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000781,2,3-Trichloropropane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000451,2,4-Trichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000471,2,4-Trimethylbenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000361,2-Dichloroethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000461,3,5-Trimethylbenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000401,3-Dichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000312-Chlorotoluene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000364-Chlorotoluene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.000294-Isopropyltoluene
BRL 8260B P6A020010.061 1/14/16 13:22 MWWmg/kg dry 0.0015Acetone
BRL 8260B P6A020010.0037 1/14/16 13:22 MWWmg/kg dry 0.00035Benzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00051Bromobenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00034Bromochloromethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00069Bromoform
BRL 8260B P6A020010.012 1/14/16 13:22 MWWmg/kg dry 0.00075Bromomethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00032Chlorobenzene
BRL 8260B P6A020010.012 1/14/16 13:22 MWWmg/kg dry 0.00051Chloroethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00044Chloroform
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00041Chloromethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00023Ethylbenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00036Isopropylbenzene (Cumene)
BRL 8260B P6A020010.012 1/14/16 13:22 MWWmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P6A020010.061 1/14/16 13:22 MWWmg/kg dry 0.00055Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-2
Prism Sample ID: 6010230-01
Prism Work Order: 6010230
Time Collected: 01/13/16 09:26
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.12 1/14/16 13:22 MWWmg/kg dry 0.00055Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.061 1/14/16 13:22 MWWmg/kg dry 0.00052Methyl Isobutyl Ketone
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00034Methylene Chloride
BRL 8260B P6A020010.012 1/14/16 13:22 MWWmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P6A020010.012 1/14/16 13:22 MWWmg/kg dry 0.00019Naphthalene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00031n-Butylbenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00036n-Propylbenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00025o-Xylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00037Styrene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00035Toluene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00036trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00039Trichloroethylene
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00039Trichlorofluoromethane
BRL 8260B P6A020010.030 1/14/16 13:22 MWWmg/kg dry 0.00083Vinyl acetate
BRL 8260B P6A020010.0061 1/14/16 13:22 MWWmg/kg dry 0.00029Vinyl chloride
BRL 8260B P6A020010.018 1/14/16 13:22 MWWmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12998 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-5
Prism Sample ID: 6010230-02
Prism Work Order: 6010230
Time Collected: 01/13/16 09:40
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
78.3 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0591,3-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0811-Methylnaphthalene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0792,4,6-Trichlorophenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0822,4-Dichlorophenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0652,4-Dimethylphenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0602-Chlorophenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0672-Methylnaphthalene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0542-Methylphenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0772-Nitrophenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0833,3’-Dichlorobenzidine
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0634,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0724-Bromophenyl phenyl ether
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0514-Chloroaniline
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.0654-Nitrophenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.057Acenaphthene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.061Acenaphthylene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.068Anthracene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.056Azobenzene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.046Benzo(a)pyrene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.055Benzo(k)fluoranthene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.056Benzyl alcohol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-5
Prism Sample ID: 6010230-02
Prism Work Order: 6010230
Time Collected: 01/13/16 09:40
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.053Chrysene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.064Dibenzofuran
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.058Diethyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.054Fluoranthene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.061Fluorene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.067Hexachlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.075Hexachlorocyclopentadiene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.071Hexachloroethane
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.057Isophorone
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.068Naphthalene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.060Nitrobenzene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.066N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.050Pentachlorophenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.055Phenanthrene
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.062Phenol
BRL 8270D P6A019810.42 1/14/16 18:11 JMVmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13268 %2,4,6-Tribromophenol
44-11566 %2-Fluorobiphenyl
35-11561 %2-Fluorophenol
37-12269 %Nitrobenzene-d5
34-12161 %Phenol-d5
54-12771 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.026 1/15/16 12:08 JABmg/kg dry 0.0017Mercury
2.3 *6010C P6A021110.32 1/15/16 21:32 bgmAbmg/kg dry 0.072Arsenic
110 *6010C P6A021110.65 1/15/16 21:32 bgmmg/kg dry 0.35Barium
BRL *6010C P6A021110.32 1/15/16 21:32 bgmmg/kg dry 0.0069Cadmium
3.3 *6010C P6A021110.32 1/15/16 21:32 bgmAamg/kg dry 0.044Chromium
4.3 *6010C P6A021110.32 1/15/16 21:32 bgmmg/kg dry 0.034Lead
BRL *6010C P6A021110.65 1/15/16 21:32 bgmmg/kg dry 0.047Selenium
BRL *6010C P6A021110.32 1/15/16 21:32 bgmmg/kg dry 0.0053Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000561,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-5
Prism Sample ID: 6010230-02
Prism Work Order: 6010230
Time Collected: 01/13/16 09:40
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000331,1,1-Trichloroethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000461,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000611,1,2-Trichloroethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000881,2,3-Trichloropropane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000521,2,4-Trimethylbenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000451,3-Dichlorobenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P6A020010.069 1/14/16 13:49 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020010.0041 1/14/16 13:49 MWWmg/kg dry 0.00040Benzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00057Bromobenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00038Bromodichloromethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00078Bromoform
BRL 8260B P6A020010.014 1/14/16 13:49 MWWmg/kg dry 0.00085Bromomethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00036Chlorobenzene
BRL 8260B P6A020010.014 1/14/16 13:49 MWWmg/kg dry 0.00057Chloroethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00050Chloroform
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00046Chloromethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6A020010.014 1/14/16 13:49 MWWmg/kg dry 0.00063m,p-Xylenes
BRL 8260B P6A020010.069 1/14/16 13:49 MWWmg/kg dry 0.00062Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-5
Prism Sample ID: 6010230-02
Prism Work Order: 6010230
Time Collected: 01/13/16 09:40
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.14 1/14/16 13:49 MWWmg/kg dry 0.00062Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.069 1/14/16 13:49 MWWmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6A020010.014 1/14/16 13:49 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020010.014 1/14/16 13:49 MWWmg/kg dry 0.00022Naphthalene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00041Styrene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00039Toluene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00045Trichloroethylene
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00044Trichlorofluoromethane
BRL 8260B P6A020010.034 1/14/16 13:49 MWWmg/kg dry 0.00094Vinyl acetate
BRL 8260B P6A020010.0069 1/14/16 13:49 MWWmg/kg dry 0.00033Vinyl chloride
BRL 8260B P6A020010.021 1/14/16 13:49 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-9
Prism Sample ID: 6010230-03
Prism Work Order: 6010230
Time Collected: 01/13/16 10:03
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
77.8 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0601,3-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0821-Methylnaphthalene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0802,4,6-Trichlorophenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0822,4-Dichlorophenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0652,4-Dimethylphenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0602-Chlorophenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0682-Methylnaphthalene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0542-Methylphenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0772-Nitrophenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0843,3’-Dichlorobenzidine
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0644,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0734-Bromophenyl phenyl ether
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0514-Chloroaniline
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.0654-Nitrophenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.058Acenaphthene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.061Acenaphthylene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.068Anthracene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.056Azobenzene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.046Benzo(a)pyrene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.056Benzo(k)fluoranthene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.056Benzyl alcohol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.074bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-9
Prism Sample ID: 6010230-03
Prism Work Order: 6010230
Time Collected: 01/13/16 10:03
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.053Chrysene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.064Dibenzofuran
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.058Diethyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.054Fluoranthene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.061Fluorene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.067Hexachlorobenzene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.076Hexachlorocyclopentadiene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.071Hexachloroethane
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.057Isophorone
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.068Naphthalene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.060Nitrobenzene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.067N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.050Pentachlorophenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.055Phenanthrene
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.063Phenol
BRL 8270D P6A019810.42 1/14/16 18:33 JMVmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13272 %2,4,6-Tribromophenol
44-11570 %2-Fluorobiphenyl
35-11565 %2-Fluorophenol
37-12271 %Nitrobenzene-d5
34-12165 %Phenol-d5
54-12772 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.026 1/15/16 12:13 JABmg/kg dry 0.0017Mercury
2.2 *6010C P6A021110.32 1/15/16 21:40 bgmAbmg/kg dry 0.070Arsenic
94 *6010C P6A021110.63 1/15/16 21:40 bgmmg/kg dry 0.34Barium
BRL *6010C P6A021110.32 1/15/16 21:40 bgmmg/kg dry 0.0067Cadmium
1.9 *6010C P6A021110.32 1/15/16 21:40 bgmAamg/kg dry 0.043Chromium
3.9 *6010C P6A021110.32 1/15/16 21:40 bgmmg/kg dry 0.033Lead
BRL *6010C P6A021110.63 1/15/16 21:40 bgmmg/kg dry 0.046Selenium
BRL *6010C P6A021110.32 1/15/16 21:40 bgmmg/kg dry 0.0052Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000541,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-9
Prism Sample ID: 6010230-03
Prism Work Order: 6010230
Time Collected: 01/13/16 10:03
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000321,1,1-Trichloroethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000441,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000581,1,2-Trichloroethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000361,1-Dichloropropylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000371,2,3-Trichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000841,2,3-Trichloropropane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000491,2,4-Trichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000501,2,4-Trimethylbenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000261,2-Dibromoethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000311,2-Dichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000391,2-Dichloroethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000411,2-Dichloropropane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000501,3,5-Trimethylbenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000331,3-Dichloropropane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000312,2-Dichloropropane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000342-Chlorotoluene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000394-Chlorotoluene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.000324-Isopropyltoluene
BRL 8260B P6A020010.066 1/14/16 14:17 MWWmg/kg dry 0.0016Acetone
BRL 8260B P6A020010.0039 1/14/16 14:17 MWWmg/kg dry 0.00038Benzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00055Bromobenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00036Bromochloromethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00075Bromoform
BRL 8260B P6A020010.013 1/14/16 14:17 MWWmg/kg dry 0.00081Bromomethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00035Chlorobenzene
BRL 8260B P6A020010.013 1/14/16 14:17 MWWmg/kg dry 0.00055Chloroethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00048Chloroform
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00044Chloromethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00027Dibromochloromethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00030Dichlorodifluoromethane
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00025Ethylbenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00039Isopropylbenzene (Cumene)
BRL 8260B P6A020010.013 1/14/16 14:17 MWWmg/kg dry 0.00061m,p-Xylenes
BRL 8260B P6A020010.066 1/14/16 14:17 MWWmg/kg dry 0.00059Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-1-9
Prism Sample ID: 6010230-03
Prism Work Order: 6010230
Time Collected: 01/13/16 10:03
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.13 1/14/16 14:17 MWWmg/kg dry 0.00059Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.066 1/14/16 14:17 MWWmg/kg dry 0.00056Methyl Isobutyl Ketone
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00037Methylene Chloride
BRL 8260B P6A020010.013 1/14/16 14:17 MWWmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P6A020010.013 1/14/16 14:17 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00039n-Propylbenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00027o-Xylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00040Styrene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00022tert-Butylbenzene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00031Tetrachloroethylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00038Toluene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00039trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00043Trichloroethylene
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P6A020010.033 1/14/16 14:17 MWWmg/kg dry 0.00090Vinyl acetate
BRL 8260B P6A020010.0066 1/14/16 14:17 MWWmg/kg dry 0.00032Vinyl chloride
BRL 8260B P6A020010.020 1/14/16 14:17 MWWmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12998 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-2
Prism Sample ID: 6010230-04
Prism Work Order: 6010230
Time Collected: 01/13/16 09:34
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
82.0 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0591,4-Dichlorobenzene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0771-Methylnaphthalene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0752,4,6-Trichlorophenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0782,4-Dichlorophenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0562,4-Dinitrophenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0582-Chloronaphthalene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0572-Chlorophenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0642-Methylnaphthalene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0732-Nitrophenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0793,3’-Dichlorobenzidine
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0694-Bromophenyl phenyl ether
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0564-Chloro-3-methylphenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.0624-Nitrophenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.058Acenaphthylene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.065Anthracene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-2
Prism Sample ID: 6010230-04
Prism Work Order: 6010230
Time Collected: 01/13/16 09:34
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.057Butyl benzyl phthalate
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.051Chrysene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.061Dibenzofuran
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.057Di-n-butyl phthalate
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.051Fluoranthene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.058Fluorene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.064Hexachlorobenzene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.072Hexachlorobutadiene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.072Hexachlorocyclopentadiene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.067Hexachloroethane
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.054Isophorone
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.065Naphthalene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.057Nitrobenzene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.061N-Nitrosodiphenylamine
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.052Phenanthrene
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.059Phenol
BRL 8270D P6A019810.40 1/14/16 18:55 JMVmg/kg dry 0.053Pyrene
Surrogate Recovery Control Limits
39-13258 %2,4,6-Tribromophenol
44-11555 %2-Fluorobiphenyl
35-11554 %2-Fluorophenol
37-12257 %Nitrobenzene-d5
34-12153 %Phenol-d5
54-12758 %Terphenyl-d14
Total Metals
0.028 *7471B P6A021210.023 1/15/16 12:17 JABmg/kg dry 0.0015Mercury
3.0 *6010C P6A021110.31 1/15/16 21:49 bgmAbmg/kg dry 0.069Arsenic
54 *6010C P6A021110.63 1/15/16 21:49 bgmmg/kg dry 0.33Barium
BRL *6010C P6A021110.31 1/15/16 21:49 bgmmg/kg dry 0.0066Cadmium
24 *6010C P6A021110.31 1/15/16 21:49 bgmAa, BH mg/kg dry 0.043Chromium
5.1 *6010C P6A021110.31 1/15/16 21:49 bgmmg/kg dry 0.033Lead
BRL *6010C P6A021110.63 1/15/16 21:49 bgmmg/kg dry 0.045Selenium
BRL *6010C P6A021110.31 1/15/16 21:49 bgmmg/kg dry 0.0051Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000551,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-2
Prism Sample ID: 6010230-04
Prism Work Order: 6010230
Time Collected: 01/13/16 09:34
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000331,1,1-Trichloroethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000451,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000601,1,2-Trichloroethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000381,2,3-Trichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000861,2,3-Trichloropropane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000501,2,4-Trichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000511,2,4-Trimethylbenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000401,2-Dichloroethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000421,2-Dichloropropane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000511,3,5-Trimethylbenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000404-Chlorotoluene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.000324-Isopropyltoluene
BRL 8260B P6A020010.067 1/14/16 14:45 MWWmg/kg dry 0.0016Acetone
BRL 8260B P6A020010.0040 1/14/16 14:45 MWWmg/kg dry 0.00039Benzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00056Bromobenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00076Bromoform
BRL 8260B P6A020010.013 1/14/16 14:45 MWWmg/kg dry 0.00083Bromomethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00036Chlorobenzene
BRL 8260B P6A020010.013 1/14/16 14:45 MWWmg/kg dry 0.00056Chloroethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00049Chloroform
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00045Chloromethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P6A020010.013 1/14/16 14:45 MWWmg/kg dry 0.00062m,p-Xylenes
BRL 8260B P6A020010.067 1/14/16 14:45 MWWmg/kg dry 0.00061Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-2
Prism Sample ID: 6010230-04
Prism Work Order: 6010230
Time Collected: 01/13/16 09:34
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.13 1/14/16 14:45 MWWmg/kg dry 0.00061Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.067 1/14/16 14:45 MWWmg/kg dry 0.00057Methyl Isobutyl Ketone
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00038Methylene Chloride
BRL 8260B P6A020010.013 1/14/16 14:45 MWWmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P6A020010.013 1/14/16 14:45 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00040Styrene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00039Toluene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00040trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00044Trichloroethylene
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P6A020010.034 1/14/16 14:45 MWWmg/kg dry 0.00092Vinyl acetate
BRL 8260B P6A020010.0067 1/14/16 14:45 MWWmg/kg dry 0.00033Vinyl chloride
BRL 8260B P6A020010.020 1/14/16 14:45 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-5
Prism Sample ID: 6010230-05
Prism Work Order: 6010230
Time Collected: 01/13/16 09:45
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
78.0 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0601,3-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0811-Methylnaphthalene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0792,4,6-Trichlorophenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0822,4-Dichlorophenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0652,4-Dimethylphenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0602-Chlorophenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0682-Methylnaphthalene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0542-Methylphenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0772-Nitrophenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0843,3’-Dichlorobenzidine
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0644,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0734-Bromophenyl phenyl ether
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0514-Chloroaniline
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.0654-Nitrophenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.058Acenaphthene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.061Acenaphthylene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.068Anthracene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.056Azobenzene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.046Benzo(a)pyrene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.055Benzo(k)fluoranthene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.056Benzyl alcohol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-5
Prism Sample ID: 6010230-05
Prism Work Order: 6010230
Time Collected: 01/13/16 09:45
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.053Chrysene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.064Dibenzofuran
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.058Diethyl phthalate
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.054Fluoranthene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.061Fluorene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.067Hexachlorobenzene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.075Hexachlorocyclopentadiene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.071Hexachloroethane
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.057Isophorone
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.068Naphthalene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.060Nitrobenzene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.067N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.050Pentachlorophenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.055Phenanthrene
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.062Phenol
BRL 8270D P6A019810.42 1/14/16 19:17 JMVmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13260 %2,4,6-Tribromophenol
44-11559 %2-Fluorobiphenyl
35-11557 %2-Fluorophenol
37-12261 %Nitrobenzene-d5
34-12155 %Phenol-d5
54-12761 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.025 1/15/16 12:22 JABmg/kg dry 0.0016Mercury
3.6 *6010C P6A021110.32 1/15/16 21:58 bgmAbmg/kg dry 0.072Arsenic
82 *6010C P6A021110.65 1/15/16 21:58 bgmmg/kg dry 0.35Barium
BRL *6010C P6A021110.32 1/15/16 21:58 bgmmg/kg dry 0.0069Cadmium
3.8 *6010C P6A021110.32 1/15/16 21:58 bgmAa, BH mg/kg dry 0.044Chromium
13 *6010C P6A021110.32 1/15/16 21:58 bgmmg/kg dry 0.034Lead
BRL *6010C P6A021110.65 1/15/16 21:58 bgmmg/kg dry 0.047Selenium
BRL *6010C P6A021110.32 1/15/16 21:58 bgmmg/kg dry 0.0053Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000601,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-5
Prism Sample ID: 6010230-05
Prism Work Order: 6010230
Time Collected: 01/13/16 09:45
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000351,1,1-Trichloroethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000491,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000641,1,2-Trichloroethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000201,1-Dichloroethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000321,1-Dichloroethylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000401,1-Dichloropropylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000411,2,3-Trichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000931,2,3-Trichloropropane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000541,2,4-Trichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000561,2,4-Trimethylbenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000291,2-Dibromoethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000341,2-Dichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000431,2-Dichloroethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000451,2-Dichloropropane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000551,3,5-Trimethylbenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000481,3-Dichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000361,3-Dichloropropane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000291,4-Dichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000352,2-Dichloropropane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000372-Chlorotoluene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000434-Chlorotoluene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.000354-Isopropyltoluene
BRL 8260B P6A020010.073 1/14/16 15:14 MWWmg/kg dry 0.0018Acetone
BRL 8260B P6A020010.0044 1/14/16 15:14 MWWmg/kg dry 0.00042Benzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00061Bromobenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00040Bromochloromethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00041Bromodichloromethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00083Bromoform
BRL 8260B P6A020010.015 1/14/16 15:14 MWWmg/kg dry 0.00090Bromomethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00036Carbon Tetrachloride
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00039Chlorobenzene
BRL 8260B P6A020010.015 1/14/16 15:14 MWWmg/kg dry 0.00061Chloroethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00052Chloroform
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00049Chloromethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00031cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00024cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00030Dibromochloromethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00033Dichlorodifluoromethane
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00028Ethylbenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00030Isopropyl Ether
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00043Isopropylbenzene (Cumene)
BRL 8260B P6A020010.015 1/14/16 15:14 MWWmg/kg dry 0.00067m,p-Xylenes
BRL 8260B P6A020010.073 1/14/16 15:14 MWWmg/kg dry 0.00066Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-5
Prism Sample ID: 6010230-05
Prism Work Order: 6010230
Time Collected: 01/13/16 09:45
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.15 1/14/16 15:14 MWWmg/kg dry 0.00066Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.073 1/14/16 15:14 MWWmg/kg dry 0.00062Methyl Isobutyl Ketone
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00041Methylene Chloride
BRL 8260B P6A020010.015 1/14/16 15:14 MWWmg/kg dry 0.00023Methyl-tert-Butyl Ether
BRL 8260B P6A020010.015 1/14/16 15:14 MWWmg/kg dry 0.00023Naphthalene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00037n-Butylbenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00043n-Propylbenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00030o-Xylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00035sec-Butylbenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00044Styrene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00025tert-Butylbenzene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00035Tetrachloroethylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00042Toluene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00043trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00038trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00047Trichloroethylene
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00047Trichlorofluoromethane
BRL 8260B P6A020010.036 1/14/16 15:14 MWWmg/kg dry 0.0010Vinyl acetate
BRL 8260B P6A020010.0073 1/14/16 15:14 MWWmg/kg dry 0.00035Vinyl chloride
BRL 8260B P6A020010.022 1/14/16 15:14 MWWmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-9
Prism Sample ID: 6010230-06
Prism Work Order: 6010230
Time Collected: 01/13/16 09:57
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
84.4 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0611,2,4-Trichlorobenzene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0591,2-Dichlorobenzene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0551,3-Dichlorobenzene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0571,4-Dichlorobenzene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0751-Methylnaphthalene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0732,4,6-Trichlorophenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0762,4-Dichlorophenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0602,4-Dimethylphenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0552,4-Dinitrophenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0482,4-Dinitrotoluene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0522,6-Dinitrotoluene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0572-Chloronaphthalene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0552-Chlorophenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0632-Methylnaphthalene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0502-Methylphenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0712-Nitrophenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0773,3’-Dichlorobenzidine
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0483/4-Methylphenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0594,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0674-Bromophenyl phenyl ether
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0554-Chloro-3-methylphenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0474-Chloroaniline
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0514-Chlorophenyl phenyl ether
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.0604-Nitrophenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.053Acenaphthene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.057Acenaphthylene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.063Anthracene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.052Azobenzene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.051Benzo(a)anthracene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.042Benzo(a)pyrene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.045Benzo(b)fluoranthene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.043Benzo(g,h,i)perylene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.051Benzo(k)fluoranthene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.033Benzoic Acid
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.052Benzyl alcohol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.068bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.055Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.067Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.058Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-9
Prism Sample ID: 6010230-06
Prism Work Order: 6010230
Time Collected: 01/13/16 09:57
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.056Butyl benzyl phthalate
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.049Chrysene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.048Dibenzo(a,h)anthracene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.059Dibenzofuran
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.054Diethyl phthalate
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.052Dimethyl phthalate
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.056Di-n-butyl phthalate
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.048Di-n-octyl phthalate
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.050Fluoranthene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.056Fluorene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.062Hexachlorobenzene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.070Hexachlorobutadiene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.070Hexachlorocyclopentadiene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.066Hexachloroethane
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.045Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.053Isophorone
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.063Naphthalene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.056Nitrobenzene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.062N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.059N-Nitrosodiphenylamine
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.046Pentachlorophenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.051Phenanthrene
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.058Phenol
BRL 8270D P6A019810.39 1/14/16 19:40 JMVmg/kg dry 0.052Pyrene
Surrogate Recovery Control Limits
39-13262 %2,4,6-Tribromophenol
44-11560 %2-Fluorobiphenyl
35-11558 %2-Fluorophenol
37-12260 %Nitrobenzene-d5
34-12158 %Phenol-d5
54-12763 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.023 1/15/16 12:27 JABmg/kg dry 0.0015Mercury
1.6 *6010C P6A021110.29 1/15/16 22:06 bgmAbmg/kg dry 0.064Arsenic
80 *6010C P6A021110.58 1/15/16 22:06 bgmmg/kg dry 0.31Barium
BRL *6010C P6A021110.29 1/15/16 22:06 bgmmg/kg dry 0.0061Cadmium
5.0 *6010C P6A021110.29 1/15/16 22:06 bgmAa, BH mg/kg dry 0.039Chromium
7.1 *6010C P6A021110.29 1/15/16 22:06 bgmmg/kg dry 0.030Lead
BRL *6010C P6A021110.58 1/15/16 22:06 bgmmg/kg dry 0.042Selenium
BRL *6010C P6A021110.29 1/15/16 22:06 bgmmg/kg dry 0.0047Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000551,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-9
Prism Sample ID: 6010230-06
Prism Work Order: 6010230
Time Collected: 01/13/16 09:57
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000321,1,1-Trichloroethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000451,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000591,1,2-Trichloroethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000361,1-Dichloropropylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000381,2,3-Trichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000851,2,3-Trichloropropane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000491,2,4-Trichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000511,2,4-Trimethylbenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000311,2-Dichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000401,2-Dichloroethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000411,2-Dichloropropane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000501,3,5-Trimethylbenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000331,3-Dichloropropane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000342-Chlorotoluene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000404-Chlorotoluene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.000324-Isopropyltoluene
BRL 8260B P6A020010.066 1/14/16 15:41 MWWmg/kg dry 0.0016Acetone
BRL 8260B P6A020010.0040 1/14/16 15:41 MWWmg/kg dry 0.00039Benzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00055Bromobenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00075Bromoform
BRL 8260B P6A020010.013 1/14/16 15:41 MWWmg/kg dry 0.00082Bromomethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00035Chlorobenzene
BRL 8260B P6A020010.013 1/14/16 15:41 MWWmg/kg dry 0.00055Chloroethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00048Chloroform
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00045Chloromethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00027Dibromochloromethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00030Dichlorodifluoromethane
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00039Isopropylbenzene (Cumene)
BRL 8260B P6A020010.013 1/14/16 15:41 MWWmg/kg dry 0.00061m,p-Xylenes
BRL 8260B P6A020010.066 1/14/16 15:41 MWWmg/kg dry 0.00060Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-2-9
Prism Sample ID: 6010230-06
Prism Work Order: 6010230
Time Collected: 01/13/16 09:57
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.13 1/14/16 15:41 MWWmg/kg dry 0.00060Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.066 1/14/16 15:41 MWWmg/kg dry 0.00057Methyl Isobutyl Ketone
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00037Methylene Chloride
BRL 8260B P6A020010.013 1/14/16 15:41 MWWmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P6A020010.013 1/14/16 15:41 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00039n-Propylbenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00027o-Xylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00040Styrene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00022tert-Butylbenzene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00038Toluene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00040trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00043Trichloroethylene
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P6A020010.033 1/14/16 15:41 MWWmg/kg dry 0.00091Vinyl acetate
BRL 8260B P6A020010.0066 1/14/16 15:41 MWWmg/kg dry 0.00032Vinyl chloride
BRL 8260B P6A020010.020 1/14/16 15:41 MWWmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-2
Prism Sample ID: 6010230-07
Prism Work Order: 6010230
Time Collected: 01/13/16 14:52
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
66.1 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0781,2,4-Trichlorobenzene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0761,2-Dichlorobenzene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0701,3-Dichlorobenzene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0731,4-Dichlorobenzene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0961-Methylnaphthalene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0942,4,6-Trichlorophenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0972,4-Dichlorophenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0772,4-Dimethylphenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0702,4-Dinitrophenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0612,4-Dinitrotoluene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0662,6-Dinitrotoluene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0722-Chloronaphthalene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0712-Chlorophenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0802-Methylnaphthalene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0642-Methylphenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0912-Nitrophenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0993,3’-Dichlorobenzidine
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0623/4-Methylphenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0754,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0864-Bromophenyl phenyl ether
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0704-Chloro-3-methylphenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0604-Chloroaniline
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0654-Chlorophenyl phenyl ether
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.0774-Nitrophenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.068Acenaphthene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.072Acenaphthylene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.081Anthracene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.066Azobenzene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.065Benzo(a)anthracene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.054Benzo(a)pyrene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.058Benzo(b)fluoranthene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.055Benzo(g,h,i)perylene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.066Benzo(k)fluoranthene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.042Benzoic Acid
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.066Benzyl alcohol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.087bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.071Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.085Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.074Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-2
Prism Sample ID: 6010230-07
Prism Work Order: 6010230
Time Collected: 01/13/16 14:52
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.071Butyl benzyl phthalate
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.063Chrysene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.061Dibenzo(a,h)anthracene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.076Dibenzofuran
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.069Diethyl phthalate
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.066Dimethyl phthalate
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.071Di-n-butyl phthalate
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.061Di-n-octyl phthalate
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.064Fluoranthene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.072Fluorene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.079Hexachlorobenzene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.090Hexachlorobutadiene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.089Hexachlorocyclopentadiene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.084Hexachloroethane
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.057Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.068Isophorone
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.080Naphthalene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.071Nitrobenzene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.079N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.076N-Nitrosodiphenylamine
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.059Pentachlorophenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.065Phenanthrene
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.074Phenol
BRL 8270D P6A019810.50 1/14/16 20:02 JMVmg/kg dry 0.066Pyrene
Surrogate Recovery Control Limits
39-13276 %2,4,6-Tribromophenol
44-11573 %2-Fluorobiphenyl
35-11569 %2-Fluorophenol
37-12276 %Nitrobenzene-d5
34-12169 %Phenol-d5
54-12778 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.029 1/15/16 12:31 JABmg/kg dry 0.0019Mercury
3.5 *6010C P6A021110.39 1/15/16 22:16 bgmAbmg/kg dry 0.086Arsenic
150 *6010C P6A021110.77 1/15/16 22:16 bgmmg/kg dry 0.41Barium
BRL *6010C P6A021110.39 1/15/16 22:16 bgmmg/kg dry 0.0082Cadmium
11 *6010C P6A021110.39 1/15/16 22:16 bgmAa, BH mg/kg dry 0.053Chromium
11 *6010C P6A021110.39 1/15/16 22:16 bgmmg/kg dry 0.041Lead
BRL *6010C P6A021110.77 1/15/16 22:16 bgmmg/kg dry 0.056Selenium
BRL *6010C P6A021110.39 1/15/16 22:16 bgmmg/kg dry 0.0063Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000601,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-2
Prism Sample ID: 6010230-07
Prism Work Order: 6010230
Time Collected: 01/13/16 14:52
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000351,1,1-Trichloroethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000491,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000641,1,2-Trichloroethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000201,1-Dichloroethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000321,1-Dichloroethylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000401,1-Dichloropropylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000411,2,3-Trichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000931,2,3-Trichloropropane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000541,2,4-Trichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000551,2,4-Trimethylbenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000291,2-Dibromoethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000341,2-Dichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000431,2-Dichloroethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000451,2-Dichloropropane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000551,3,5-Trimethylbenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000481,3-Dichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000361,3-Dichloropropane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000291,4-Dichlorobenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000352,2-Dichloropropane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000372-Chlorotoluene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000434-Chlorotoluene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.000354-Isopropyltoluene
BRL 8260B P6A020010.073 1/14/16 16:37 MWWmg/kg dry 0.0018Acetone
BRL 8260B P6A020010.0044 1/14/16 16:37 MWWmg/kg dry 0.00042Benzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00061Bromobenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00040Bromochloromethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00041Bromodichloromethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00083Bromoform
BRL 8260B P6A020010.015 1/14/16 16:37 MWWmg/kg dry 0.00090Bromomethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00036Carbon Tetrachloride
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00038Chlorobenzene
BRL 8260B P6A020010.015 1/14/16 16:37 MWWmg/kg dry 0.00061Chloroethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00052Chloroform
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00049Chloromethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00031cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00024cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00030Dibromochloromethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00033Dichlorodifluoromethane
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00028Ethylbenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00030Isopropyl Ether
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00043Isopropylbenzene (Cumene)
BRL 8260B P6A020010.015 1/14/16 16:37 MWWmg/kg dry 0.00067m,p-Xylenes
BRL 8260B P6A020010.073 1/14/16 16:37 MWWmg/kg dry 0.00066Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-2
Prism Sample ID: 6010230-07
Prism Work Order: 6010230
Time Collected: 01/13/16 14:52
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.15 1/14/16 16:37 MWWmg/kg dry 0.00066Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.073 1/14/16 16:37 MWWmg/kg dry 0.00062Methyl Isobutyl Ketone
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00041Methylene Chloride
BRL 8260B P6A020010.015 1/14/16 16:37 MWWmg/kg dry 0.00023Methyl-tert-Butyl Ether
BRL 8260B P6A020010.015 1/14/16 16:37 MWWmg/kg dry 0.00023Naphthalene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00037n-Butylbenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00043n-Propylbenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00030o-Xylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00035sec-Butylbenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00044Styrene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00025tert-Butylbenzene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00035Tetrachloroethylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00042Toluene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00043trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00038trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00047Trichloroethylene
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00047Trichlorofluoromethane
BRL 8260B P6A020010.036 1/14/16 16:37 MWWmg/kg dry 0.00099Vinyl acetate
BRL 8260B P6A020010.0073 1/14/16 16:37 MWWmg/kg dry 0.00035Vinyl chloride
BRL 8260B P6A020010.022 1/14/16 16:37 MWWmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-5
Prism Sample ID: 6010230-08
Prism Work Order: 6010230
Time Collected: 01/13/16 15:04
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
75.4 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0681,2,4-Trichlorobenzene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0661,2-Dichlorobenzene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0621,3-Dichlorobenzene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0641,4-Dichlorobenzene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0841-Methylnaphthalene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0822,4,6-Trichlorophenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0852,4-Dichlorophenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0672,4-Dimethylphenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0612,4-Dinitrophenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0532,4-Dinitrotoluene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0582,6-Dinitrotoluene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0632-Chloronaphthalene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0622-Chlorophenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0702-Methylnaphthalene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0562-Methylphenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0802-Nitrophenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0863,3’-Dichlorobenzidine
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0543/4-Methylphenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0664,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0754-Bromophenyl phenyl ether
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0614-Chloro-3-methylphenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0534-Chloroaniline
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0574-Chlorophenyl phenyl ether
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.0674-Nitrophenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.060Acenaphthene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.063Acenaphthylene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.071Anthracene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.058Azobenzene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.057Benzo(a)anthracene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.051Benzo(b)fluoranthene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.048Benzo(g,h,i)perylene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.037Benzoic Acid
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.058Benzyl alcohol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.076bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.062Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.075Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.065Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-5
Prism Sample ID: 6010230-08
Prism Work Order: 6010230
Time Collected: 01/13/16 15:04
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.062Butyl benzyl phthalate
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.055Chrysene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.053Dibenzo(a,h)anthracene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.067Dibenzofuran
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.060Diethyl phthalate
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.058Dimethyl phthalate
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.062Di-n-butyl phthalate
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.054Di-n-octyl phthalate
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.056Fluoranthene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.063Fluorene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.069Hexachlorobenzene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.079Hexachlorobutadiene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.078Hexachlorocyclopentadiene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.073Hexachloroethane
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.050Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.059Isophorone
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.070Naphthalene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.062Nitrobenzene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.069N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.067N-Nitrosodiphenylamine
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.052Pentachlorophenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.057Phenanthrene
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.065Phenol
BRL 8270D P6A019810.44 1/14/16 20:24 JMVmg/kg dry 0.058Pyrene
Surrogate Recovery Control Limits
39-13271 %2,4,6-Tribromophenol
44-11565 %2-Fluorobiphenyl
35-11563 %2-Fluorophenol
37-12268 %Nitrobenzene-d5
34-12163 %Phenol-d5
54-12771 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.025 1/15/16 12:36 JABmg/kg dry 0.0016Mercury
2.4 *6010C P6A021110.33 1/15/16 22:24 bgmAbmg/kg dry 0.073Arsenic
44 *6010C P6A021110.66 1/15/16 22:24 bgmmg/kg dry 0.35Barium
BRL *6010C P6A021110.33 1/15/16 22:24 bgmmg/kg dry 0.0070Cadmium
1.7 *6010C P6A021110.33 1/15/16 22:24 bgmAamg/kg dry 0.045Chromium
3.8 *6010C P6A021110.33 1/15/16 22:24 bgmmg/kg dry 0.035Lead
BRL *6010C P6A021110.66 1/15/16 22:24 bgmmg/kg dry 0.048Selenium
BRL *6010C P6A021110.33 1/15/16 22:24 bgmmg/kg dry 0.0054Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000561,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-5
Prism Sample ID: 6010230-08
Prism Work Order: 6010230
Time Collected: 01/13/16 15:04
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000331,1,1-Trichloroethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000461,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000601,1,2-Trichloroethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000871,2,3-Trichloropropane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000521,2,4-Trimethylbenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000421,2-Dichloropropane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000511,3,5-Trimethylbenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000451,3-Dichlorobenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P6A020010.068 1/14/16 17:05 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020010.0041 1/14/16 17:05 MWWmg/kg dry 0.00040Benzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00057Bromobenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00038Bromodichloromethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00077Bromoform
BRL 8260B P6A020010.014 1/14/16 17:05 MWWmg/kg dry 0.00084Bromomethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00036Chlorobenzene
BRL 8260B P6A020010.014 1/14/16 17:05 MWWmg/kg dry 0.00057Chloroethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00049Chloroform
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00046Chloromethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P6A020010.014 1/14/16 17:05 MWWmg/kg dry 0.00063m,p-Xylenes
BRL 8260B P6A020010.068 1/14/16 17:05 MWWmg/kg dry 0.00061Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-5
Prism Sample ID: 6010230-08
Prism Work Order: 6010230
Time Collected: 01/13/16 15:04
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.14 1/14/16 17:05 MWWmg/kg dry 0.00061Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.068 1/14/16 17:05 MWWmg/kg dry 0.00058Methyl Isobutyl Ketone
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00038Methylene Chloride
BRL 8260B P6A020010.014 1/14/16 17:05 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020010.014 1/14/16 17:05 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00041Styrene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00039Toluene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00044Trichloroethylene
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00044Trichlorofluoromethane
BRL 8260B P6A020010.034 1/14/16 17:05 MWWmg/kg dry 0.00093Vinyl acetate
BRL 8260B P6A020010.0068 1/14/16 17:05 MWWmg/kg dry 0.00033Vinyl chloride
BRL 8260B P6A020010.020 1/14/16 17:05 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-9
Prism Sample ID: 6010230-09
Prism Work Order: 6010230
Time Collected: 01/13/16 15:20
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
76.6 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0612-Chlorophenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0782-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0853,3’-Dichlorobenzidine
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.0664-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.059Acenaphthene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.069Anthracene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-9
Prism Sample ID: 6010230-09
Prism Work Order: 6010230
Time Collected: 01/13/16 15:20
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.054Chrysene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.066Dibenzofuran
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.062Fluorene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.058Isophorone
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.069Naphthalene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.064Phenol
BRL 8270D P6A019810.43 1/14/16 20:46 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13279 %2,4,6-Tribromophenol
44-11574 %2-Fluorobiphenyl
35-11568 %2-Fluorophenol
37-12276 %Nitrobenzene-d5
34-12170 %Phenol-d5
54-12778 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.024 1/15/16 12:40 JABmg/kg dry 0.0016Mercury
2.2 *6010C P6A021110.32 1/15/16 22:32 bgmAbmg/kg dry 0.071Arsenic
50 *6010C P6A021110.64 1/15/16 22:32 bgmmg/kg dry 0.34Barium
BRL *6010C P6A021110.32 1/15/16 22:32 bgmmg/kg dry 0.0068Cadmium
2.6 *6010C P6A021110.32 1/15/16 22:32 bgmAamg/kg dry 0.043Chromium
5.3 *6010C P6A021110.32 1/15/16 22:32 bgmmg/kg dry 0.034Lead
BRL *6010C P6A021110.64 1/15/16 22:32 bgmmg/kg dry 0.046Selenium
BRL *6010C P6A021110.32 1/15/16 22:32 bgmmg/kg dry 0.0052Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000601,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-9
Prism Sample ID: 6010230-09
Prism Work Order: 6010230
Time Collected: 01/13/16 15:20
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000351,1,1-Trichloroethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000491,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000641,1,2-Trichloroethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000201,1-Dichloroethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000321,1-Dichloroethylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000401,1-Dichloropropylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000411,2,3-Trichlorobenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000931,2,3-Trichloropropane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000541,2,4-Trichlorobenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000551,2,4-Trimethylbenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000291,2-Dibromoethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000341,2-Dichlorobenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000431,2-Dichloroethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000451,2-Dichloropropane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000551,3,5-Trimethylbenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000481,3-Dichlorobenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000361,3-Dichloropropane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000291,4-Dichlorobenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000352,2-Dichloropropane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000372-Chlorotoluene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000434-Chlorotoluene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.000354-Isopropyltoluene
BRL 8260B P6A020010.072 1/14/16 17:33 MWWmg/kg dry 0.0018Acetone
BRL 8260B P6A020010.0043 1/14/16 17:33 MWWmg/kg dry 0.00042Benzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00060Bromobenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00040Bromochloromethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00040Bromodichloromethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00082Bromoform
BRL 8260B P6A020010.014 1/14/16 17:33 MWWmg/kg dry 0.00089Bromomethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00036Carbon Tetrachloride
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00038Chlorobenzene
BRL 8260B P6A020010.014 1/14/16 17:33 MWWmg/kg dry 0.00060Chloroethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00052Chloroform
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00049Chloromethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00031cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00024cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00030Dibromochloromethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00033Dichlorodifluoromethane
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00028Ethylbenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00030Isopropyl Ether
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00043Isopropylbenzene (Cumene)
BRL 8260B P6A020010.014 1/14/16 17:33 MWWmg/kg dry 0.00067m,p-Xylenes
BRL 8260B P6A020010.072 1/14/16 17:33 MWWmg/kg dry 0.00066Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-3-9
Prism Sample ID: 6010230-09
Prism Work Order: 6010230
Time Collected: 01/13/16 15:20
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.14 1/14/16 17:33 MWWmg/kg dry 0.00066Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.072 1/14/16 17:33 MWWmg/kg dry 0.00062Methyl Isobutyl Ketone
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00041Methylene Chloride
BRL 8260B P6A020010.014 1/14/16 17:33 MWWmg/kg dry 0.00023Methyl-tert-Butyl Ether
BRL 8260B P6A020010.014 1/14/16 17:33 MWWmg/kg dry 0.00023Naphthalene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00037n-Butylbenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00043n-Propylbenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00030o-Xylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00035sec-Butylbenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00044Styrene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00025tert-Butylbenzene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00035Tetrachloroethylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00042Toluene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00043trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00038trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00047Trichloroethylene
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00047Trichlorofluoromethane
BRL 8260B P6A020010.036 1/14/16 17:33 MWWmg/kg dry 0.00099Vinyl acetate
BRL 8260B P6A020010.0072 1/14/16 17:33 MWWmg/kg dry 0.00035Vinyl chloride
BRL 8260B P6A020010.022 1/14/16 17:33 MWWmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-2
Prism Sample ID: 6010230-10
Prism Work Order: 6010230
Time Collected: 01/13/16 10:29
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
90.2 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0571,2,4-Trichlorobenzene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0561,2-Dichlorobenzene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0521,3-Dichlorobenzene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0541,4-Dichlorobenzene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0701-Methylnaphthalene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0692,4,6-Trichlorophenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0712,4-Dichlorophenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0562,4-Dimethylphenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0512,4-Dinitrophenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0442,4-Dinitrotoluene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0492,6-Dinitrotoluene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0532-Chloronaphthalene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0522-Chlorophenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0592-Methylnaphthalene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0472-Methylphenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0672-Nitrophenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0723,3’-Dichlorobenzidine
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0453/4-Methylphenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0554,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0634-Bromophenyl phenyl ether
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0514-Chloro-3-methylphenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0444-Chloroaniline
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0484-Chlorophenyl phenyl ether
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.0564-Nitrophenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.050Acenaphthene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.053Acenaphthylene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.059Anthracene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.048Azobenzene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.048Benzo(a)anthracene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.040Benzo(a)pyrene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.042Benzo(b)fluoranthene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.040Benzo(g,h,i)perylene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.048Benzo(k)fluoranthene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.031Benzoic Acid
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.048Benzyl alcohol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.063bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.052Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.062Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.054Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-2
Prism Sample ID: 6010230-10
Prism Work Order: 6010230
Time Collected: 01/13/16 10:29
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.052Butyl benzyl phthalate
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.046Chrysene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.045Dibenzo(a,h)anthracene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.056Dibenzofuran
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.050Diethyl phthalate
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.048Dimethyl phthalate
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.052Di-n-butyl phthalate
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.045Di-n-octyl phthalate
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.047Fluoranthene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.053Fluorene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.058Hexachlorobenzene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.066Hexachlorobutadiene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.065Hexachlorocyclopentadiene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.061Hexachloroethane
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.042Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.050Isophorone
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.059Naphthalene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.052Nitrobenzene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.058N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.056N-Nitrosodiphenylamine
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.043Pentachlorophenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.048Phenanthrene
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.054Phenol
BRL 8270D P6A019810.37 1/14/16 21:08 JMVmg/kg dry 0.048Pyrene
Surrogate Recovery Control Limits
39-13270 %2,4,6-Tribromophenol
44-11564 %2-Fluorobiphenyl
35-11560 %2-Fluorophenol
37-12264 %Nitrobenzene-d5
34-12159 %Phenol-d5
54-12766 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.022 1/15/16 12:45 JABmg/kg dry 0.0014Mercury
1.2 *6010C P6A021110.28 1/15/16 22:40 bgmAbmg/kg dry 0.062Arsenic
35 *6010C P6A021110.56 1/15/16 22:40 bgmmg/kg dry 0.30Barium
BRL *6010C P6A021110.28 1/15/16 22:40 bgmmg/kg dry 0.0060Cadmium
0.29 *6010C P6A021110.28 1/15/16 22:40 bgmAamg/kg dry 0.038Chromium
1.6 *6010C P6A021110.28 1/15/16 22:40 bgmmg/kg dry 0.030Lead
BRL *6010C P6A021110.56 1/15/16 22:40 bgmmg/kg dry 0.041Selenium
BRL *6010C P6A021110.28 1/15/16 22:40 bgmmg/kg dry 0.0046Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000551,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-2
Prism Sample ID: 6010230-10
Prism Work Order: 6010230
Time Collected: 01/13/16 10:29
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000321,1,1-Trichloroethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000451,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000591,1,2-Trichloroethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000381,2,3-Trichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000851,2,3-Trichloropropane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000501,2,4-Trichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000511,2,4-Trimethylbenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000311,2-Dichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000401,2-Dichloroethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000411,2-Dichloropropane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000501,3,5-Trimethylbenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000331,3-Dichloropropane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000342-Chlorotoluene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000404-Chlorotoluene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.000324-Isopropyltoluene
BRL 8260B P6A020010.067 1/14/16 18:00 MWWmg/kg dry 0.0016Acetone
BRL 8260B P6A020010.0040 1/14/16 18:00 MWWmg/kg dry 0.00039Benzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00056Bromobenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00076Bromoform
BRL 8260B P6A020010.013 1/14/16 18:00 MWWmg/kg dry 0.00082Bromomethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00035Chlorobenzene
BRL 8260B P6A020010.013 1/14/16 18:00 MWWmg/kg dry 0.00056Chloroethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00048Chloroform
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00045Chloromethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00027Dibromochloromethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00030Dichlorodifluoromethane
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00039Isopropylbenzene (Cumene)
BRL 8260B P6A020010.013 1/14/16 18:00 MWWmg/kg dry 0.00061m,p-Xylenes
BRL 8260B P6A020010.067 1/14/16 18:00 MWWmg/kg dry 0.00060Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-2
Prism Sample ID: 6010230-10
Prism Work Order: 6010230
Time Collected: 01/13/16 10:29
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.13 1/14/16 18:00 MWWmg/kg dry 0.00060Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.067 1/14/16 18:00 MWWmg/kg dry 0.00057Methyl Isobutyl Ketone
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00037Methylene Chloride
BRL 8260B P6A020010.013 1/14/16 18:00 MWWmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P6A020010.013 1/14/16 18:00 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00027o-Xylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00040Styrene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00038Toluene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00040trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00043Trichloroethylene
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P6A020010.033 1/14/16 18:00 MWWmg/kg dry 0.00091Vinyl acetate
BRL 8260B P6A020010.0067 1/14/16 18:00 MWWmg/kg dry 0.00032Vinyl chloride
BRL 8260B P6A020010.020 1/14/16 18:00 MWWmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123107 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-5
Prism Sample ID: 6010230-11
Prism Work Order: 6010230
Time Collected: 01/13/16 10:42
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
94.1 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0551,2,4-Trichlorobenzene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0531,2-Dichlorobenzene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0491,3-Dichlorobenzene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0511,4-Dichlorobenzene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0671-Methylnaphthalene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0662,4,6-Trichlorophenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0682,4-Dichlorophenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0542,4-Dimethylphenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0492,4-Dinitrophenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0432,4-Dinitrotoluene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0472,6-Dinitrotoluene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0512-Chloronaphthalene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0502-Chlorophenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0562-Methylnaphthalene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0452-Methylphenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0642-Nitrophenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0693,3’-Dichlorobenzidine
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0433/4-Methylphenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0534,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0604-Bromophenyl phenyl ether
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0494-Chloro-3-methylphenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0424-Chloroaniline
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0464-Chlorophenyl phenyl ether
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.0544-Nitrophenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.048Acenaphthene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.051Acenaphthylene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.056Anthracene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.046Azobenzene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.046Benzo(a)anthracene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.038Benzo(a)pyrene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.041Benzo(b)fluoranthene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.038Benzo(g,h,i)perylene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.046Benzo(k)fluoranthene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.030Benzoic Acid
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.046Benzyl alcohol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.061bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.049Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.060Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.052Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-5
Prism Sample ID: 6010230-11
Prism Work Order: 6010230
Time Collected: 01/13/16 10:42
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.050Butyl benzyl phthalate
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.044Chrysene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.043Dibenzo(a,h)anthracene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.053Dibenzofuran
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.048Diethyl phthalate
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.046Dimethyl phthalate
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.050Di-n-butyl phthalate
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.043Di-n-octyl phthalate
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.045Fluoranthene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.050Fluorene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.056Hexachlorobenzene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.063Hexachlorobutadiene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.063Hexachlorocyclopentadiene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.059Hexachloroethane
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.040Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.047Isophorone
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.056Naphthalene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.050Nitrobenzene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.055N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.053N-Nitrosodiphenylamine
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.041Pentachlorophenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.046Phenanthrene
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.052Phenol
BRL 8270D P6A019810.35 1/14/16 21:31 JMVmg/kg dry 0.046Pyrene
Surrogate Recovery Control Limits
39-13268 %2,4,6-Tribromophenol
44-11560 %2-Fluorobiphenyl
35-11558 %2-Fluorophenol
37-12262 %Nitrobenzene-d5
34-12157 %Phenol-d5
54-12765 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.021 1/15/16 12:58 JABmg/kg dry 0.0014Mercury
1.7 *6010C P6A021110.27 1/15/16 23:00 bgmAbmg/kg dry 0.060Arsenic
28 *6010C P6A021110.54 1/15/16 23:00 bgmmg/kg dry 0.29Barium
BRL *6010C P6A021110.27 1/15/16 23:00 bgmmg/kg dry 0.0058Cadmium
0.41 *6010C P6A021110.27 1/15/16 23:00 bgmAamg/kg dry 0.037Chromium
4.0 *6010C P6A021110.27 1/15/16 23:00 bgmmg/kg dry 0.029Lead
BRL *6010C P6A021110.54 1/15/16 23:00 bgmmg/kg dry 0.040Selenium
BRL *6010C P6A021110.27 1/15/16 23:00 bgmmg/kg dry 0.0045Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000521,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-5
Prism Sample ID: 6010230-11
Prism Work Order: 6010230
Time Collected: 01/13/16 10:42
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000311,1,1-Trichloroethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000431,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000561,1,2-Trichloroethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000281,1-Dichloroethylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000351,1-Dichloropropylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000361,2,3-Trichlorobenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000811,2,3-Trichloropropane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000471,2,4-Trichlorobenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000481,2,4-Trimethylbenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000301,2-Dichlorobenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000381,2-Dichloroethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000391,2-Dichloropropane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000481,3,5-Trimethylbenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000421,3-Dichlorobenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000321,3-Dichloropropane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000332-Chlorotoluene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000384-Chlorotoluene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.000304-Isopropyltoluene
BRL 8260B P6A020010.063 1/14/16 18:28 MWWmg/kg dry 0.0015Acetone
BRL 8260B P6A020010.0038 1/14/16 18:28 MWWmg/kg dry 0.00037Benzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00053Bromobenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00035Bromochloromethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00072Bromoform
BRL 8260B P6A020010.013 1/14/16 18:28 MWWmg/kg dry 0.00078Bromomethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00034Chlorobenzene
BRL 8260B P6A020010.013 1/14/16 18:28 MWWmg/kg dry 0.00053Chloroethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00046Chloroform
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00043Chloromethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00027cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00029Dichlorodifluoromethane
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00024Ethylbenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00037Isopropylbenzene (Cumene)
BRL 8260B P6A020010.013 1/14/16 18:28 MWWmg/kg dry 0.00058m,p-Xylenes
BRL 8260B P6A020010.063 1/14/16 18:28 MWWmg/kg dry 0.00057Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-5
Prism Sample ID: 6010230-11
Prism Work Order: 6010230
Time Collected: 01/13/16 10:42
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.13 1/14/16 18:28 MWWmg/kg dry 0.00057Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.063 1/14/16 18:28 MWWmg/kg dry 0.00054Methyl Isobutyl Ketone
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00036Methylene Chloride
BRL 8260B P6A020010.013 1/14/16 18:28 MWWmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6A020010.013 1/14/16 18:28 MWWmg/kg dry 0.00020Naphthalene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00038n-Propylbenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00026o-Xylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00031sec-Butylbenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00038Styrene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00036Toluene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00038trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00041Trichloroethylene
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00041Trichlorofluoromethane
BRL 8260B P6A020010.032 1/14/16 18:28 MWWmg/kg dry 0.00087Vinyl acetate
BRL 8260B P6A020010.0063 1/14/16 18:28 MWWmg/kg dry 0.00031Vinyl chloride
BRL 8260B P6A020010.019 1/14/16 18:28 MWWmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-9
Prism Sample ID: 6010230-12
Prism Work Order: 6010230
Time Collected: 01/13/16 10:59
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
91.9 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0561,2,4-Trichlorobenzene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0551,2-Dichlorobenzene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0511,3-Dichlorobenzene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0531,4-Dichlorobenzene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0691-Methylnaphthalene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0672,4,6-Trichlorophenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0692,4-Dichlorophenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0552,4-Dimethylphenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0502,4-Dinitrophenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0442,4-Dinitrotoluene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0482,6-Dinitrotoluene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0522-Chloronaphthalene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0512-Chlorophenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0572-Methylnaphthalene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0462-Methylphenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0652-Nitrophenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0713,3’-Dichlorobenzidine
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0443/4-Methylphenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0544,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0624-Bromophenyl phenyl ether
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0504-Chloro-3-methylphenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0434-Chloroaniline
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0474-Chlorophenyl phenyl ether
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.0554-Nitrophenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.049Acenaphthene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.052Acenaphthylene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.058Anthracene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.047Azobenzene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.047Benzo(a)anthracene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.039Benzo(a)pyrene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.042Benzo(b)fluoranthene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.039Benzo(g,h,i)perylene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.047Benzo(k)fluoranthene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.030Benzoic Acid
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.047Benzyl alcohol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.062bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.051Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.061Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.053Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-9
Prism Sample ID: 6010230-12
Prism Work Order: 6010230
Time Collected: 01/13/16 10:59
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.051Butyl benzyl phthalate
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.045Chrysene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.044Dibenzo(a,h)anthracene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.055Dibenzofuran
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.050Diethyl phthalate
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.047Dimethyl phthalate
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.051Di-n-butyl phthalate
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.044Di-n-octyl phthalate
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.046Fluoranthene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.052Fluorene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.057Hexachlorobenzene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.065Hexachlorobutadiene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.064Hexachlorocyclopentadiene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.060Hexachloroethane
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.041Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.049Isophorone
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.058Naphthalene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.051Nitrobenzene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.057N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.055N-Nitrosodiphenylamine
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.042Pentachlorophenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.047Phenanthrene
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.053Phenol
BRL 8270D P6A019810.36 1/14/16 21:53 JMVmg/kg dry 0.048Pyrene
Surrogate Recovery Control Limits
39-13271 %2,4,6-Tribromophenol
44-11567 %2-Fluorobiphenyl
35-11564 %2-Fluorophenol
37-12267 %Nitrobenzene-d5
34-12164 %Phenol-d5
54-12772 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.023 1/15/16 13:03 JABmg/kg dry 0.0015Mercury
1.5 *6010C P6A021110.27 1/15/16 23:08 bgmAbmg/kg dry 0.059Arsenic
31 *6010C P6A021110.54 1/15/16 23:08 bgmmg/kg dry 0.29Barium
BRL *6010C P6A021110.27 1/15/16 23:08 bgmmg/kg dry 0.0057Cadmium
0.28 *6010C P6A021110.27 1/15/16 23:08 bgmAamg/kg dry 0.036Chromium
2.1 *6010C P6A021110.27 1/15/16 23:08 bgmmg/kg dry 0.028Lead
BRL *6010C P6A021110.54 1/15/16 23:08 bgmmg/kg dry 0.039Selenium
BRL *6010C P6A021110.27 1/15/16 23:08 bgmmg/kg dry 0.0044Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000571,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-9
Prism Sample ID: 6010230-12
Prism Work Order: 6010230
Time Collected: 01/13/16 10:59
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000341,1,1-Trichloroethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000621,1,2-Trichloroethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000401,2,3-Trichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000891,2,3-Trichloropropane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000521,2,4-Trichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000331,2-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000421,2-Dichloroethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000531,3,5-Trimethylbenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000424-Chlorotoluene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.000344-Isopropyltoluene
BRL 8260B P6A020010.070 1/14/16 18:56 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020010.0042 1/14/16 18:56 MWWmg/kg dry 0.00041Benzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00058Bromobenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00079Bromoform
BRL 8260B P6A020010.014 1/14/16 18:56 MWWmg/kg dry 0.00086Bromomethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00035Carbon Tetrachloride
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00037Chlorobenzene
BRL 8260B P6A020010.014 1/14/16 18:56 MWWmg/kg dry 0.00058Chloroethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00050Chloroform
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00047Chloromethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00030cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00032Dichlorodifluoromethane
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00027Ethylbenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6A020010.014 1/14/16 18:56 MWWmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P6A020010.070 1/14/16 18:56 MWWmg/kg dry 0.00063Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-4-9
Prism Sample ID: 6010230-12
Prism Work Order: 6010230
Time Collected: 01/13/16 10:59
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.14 1/14/16 18:56 MWWmg/kg dry 0.00063Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.070 1/14/16 18:56 MWWmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6A020010.014 1/14/16 18:56 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020010.014 1/14/16 18:56 MWWmg/kg dry 0.00022Naphthalene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00036n-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00029o-Xylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00034sec-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00042Styrene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00024tert-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00040Toluene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00042trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00037trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00045Trichloroethylene
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P6A020010.035 1/14/16 18:56 MWWmg/kg dry 0.00096Vinyl acetate
BRL 8260B P6A020010.0070 1/14/16 18:56 MWWmg/kg dry 0.00034Vinyl chloride
BRL 8260B P6A020010.021 1/14/16 18:56 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-2
Prism Sample ID: 6010230-13
Prism Work Order: 6010230
Time Collected: 01/13/16 11:43
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
77.5 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0601,3-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0821-Methylnaphthalene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0802,4,6-Trichlorophenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0822,4-Dichlorophenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0652,4-Dimethylphenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0602-Chlorophenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0682-Methylnaphthalene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0782-Nitrophenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0843,3’-Dichlorobenzidine
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0644,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0734-Bromophenyl phenyl ether
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0514-Chloroaniline
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.0664-Nitrophenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.058Acenaphthene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.069Anthracene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.056Azobenzene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.046Benzo(a)pyrene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.056Benzo(k)fluoranthene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.056Benzyl alcohol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.074bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.073Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 57 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-2
Prism Sample ID: 6010230-13
Prism Work Order: 6010230
Time Collected: 01/13/16 11:43
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.054Chrysene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.065Dibenzofuran
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.054Fluoranthene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.061Fluorene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.076Hexachlorocyclopentadiene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.071Hexachloroethane
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.058Isophorone
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.068Naphthalene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.060Nitrobenzene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.067N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.065N-Nitrosodiphenylamine
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.050Pentachlorophenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.055Phenanthrene
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.063Phenol
BRL 8270D P6A021510.43 1/15/16 15:21 JMVmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13261 %2,4,6-Tribromophenol
44-11557 %2-Fluorobiphenyl
35-11556 %2-Fluorophenol
37-12257 %Nitrobenzene-d5
34-12154 %Phenol-d5
54-12761 %Terphenyl-d14
Total Metals
0.052 *7471B P6A021210.025 1/15/16 13:39 JABmg/kg dry 0.0016Mercury
2.1 *6010C P6A021110.32 1/16/16 0:16 bgmAbmg/kg dry 0.070Arsenic
25 *6010C P6A021110.63 1/16/16 0:16 bgmmg/kg dry 0.34Barium
BRL *6010C P6A021110.32 1/16/16 0:16 bgmmg/kg dry 0.0067Cadmium
12 *6010C P6A021110.32 1/16/16 0:16 bgmAa, BH mg/kg dry 0.043Chromium
18 *6010C P6A021110.32 1/16/16 0:16 bgmmg/kg dry 0.033Lead
BRL *6010C P6A021110.63 1/16/16 0:16 bgmmg/kg dry 0.046Selenium
BRL *6010C P6A021110.32 1/16/16 0:16 bgmmg/kg dry 0.0052Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000571,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 58 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-2
Prism Sample ID: 6010230-13
Prism Work Order: 6010230
Time Collected: 01/13/16 11:43
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000341,1,1-Trichloroethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000621,1,2-Trichloroethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000401,2,3-Trichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000891,2,3-Trichloropropane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000521,2,4-Trichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000331,2-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000421,2-Dichloroethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000531,3,5-Trimethylbenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000424-Chlorotoluene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.000344-Isopropyltoluene
BRL 8260B P6A020010.070 1/14/16 19:24 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020010.0042 1/14/16 19:24 MWWmg/kg dry 0.00041Benzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00058Bromobenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00079Bromoform
BRL 8260B P6A020010.014 1/14/16 19:24 MWWmg/kg dry 0.00086Bromomethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00035Carbon Tetrachloride
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00037Chlorobenzene
BRL 8260B P6A020010.014 1/14/16 19:24 MWWmg/kg dry 0.00058Chloroethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00050Chloroform
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00047Chloromethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00030cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00032Dichlorodifluoromethane
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00027Ethylbenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6A020010.014 1/14/16 19:24 MWWmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P6A020010.070 1/14/16 19:24 MWWmg/kg dry 0.00063Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 59 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-2
Prism Sample ID: 6010230-13
Prism Work Order: 6010230
Time Collected: 01/13/16 11:43
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.14 1/14/16 19:24 MWWmg/kg dry 0.00063Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.070 1/14/16 19:24 MWWmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6A020010.014 1/14/16 19:24 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020010.014 1/14/16 19:24 MWWmg/kg dry 0.00022Naphthalene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00036n-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00029o-Xylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00034sec-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00042Styrene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00024tert-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00040Toluene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00042trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00037trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00045Trichloroethylene
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P6A020010.035 1/14/16 19:24 MWWmg/kg dry 0.00096Vinyl acetate
BRL 8260B P6A020010.0070 1/14/16 19:24 MWWmg/kg dry 0.00034Vinyl chloride
BRL 8260B P6A020010.021 1/14/16 19:24 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 60 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-5
Prism Sample ID: 6010230-14
Prism Work Order: 6010230
Time Collected: 01/13/16 11:55
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
80.7 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0791-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0792,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0652-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0742-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0813,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.066Anthracene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 61 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-5
Prism Sample ID: 6010230-14
Prism Work Order: 6010230
Time Collected: 01/13/16 11:55
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.052Chrysene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.059Fluorene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.073Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.055Isophorone
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.064N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.060Phenol
BRL 8270D P6A021510.41 1/15/16 15:43 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13250 %2,4,6-Tribromophenol
44-11547 %2-Fluorobiphenyl
35-11548 %2-Fluorophenol
37-12249 %Nitrobenzene-d5
34-12147 %Phenol-d5
54-12753 %Terphenyl-d14 SR
Total Metals
0.033 *7471B P6A021210.024 1/15/16 13:16 JABmg/kg dry 0.0016Mercury
1.9 *6010C P6A021110.31 1/15/16 23:35 bgmAbmg/kg dry 0.068Arsenic
22 *6010C P6A021110.61 1/15/16 23:35 bgmmg/kg dry 0.33Barium
BRL *6010C P6A021110.31 1/15/16 23:35 bgmmg/kg dry 0.0065Cadmium
3.7 *6010C P6A021110.31 1/15/16 23:35 bgmAamg/kg dry 0.042Chromium
5.3 *6010C P6A021110.31 1/15/16 23:35 bgmmg/kg dry 0.032Lead
BRL *6010C P6A021110.61 1/15/16 23:35 bgmmg/kg dry 0.045Selenium
BRL *6010C P6A021110.31 1/15/16 23:35 bgmmg/kg dry 0.0050Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000611,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 62 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-5
Prism Sample ID: 6010230-14
Prism Work Order: 6010230
Time Collected: 01/13/16 11:55
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000361,1,1-Trichloroethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000501,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000651,1,2-Trichloroethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000211,1-Dichloroethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000331,1-Dichloroethylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000411,1-Dichloropropylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000421,2,3-Trichlorobenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000941,2,3-Trichloropropane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000551,2,4-Trichlorobenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000561,2,4-Trimethylbenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000301,2-Dibromoethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000351,2-Dichlorobenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000441,2-Dichloroethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000461,2-Dichloropropane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000561,3,5-Trimethylbenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000491,3-Dichlorobenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000371,3-Dichloropropane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000291,4-Dichlorobenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000352,2-Dichloropropane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000382-Chlorotoluene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000444-Chlorotoluene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.000364-Isopropyltoluene
BRL 8260B P6A020010.074 1/14/16 19:52 MWWmg/kg dry 0.0018Acetone
BRL 8260B P6A020010.0044 1/14/16 19:52 MWWmg/kg dry 0.00043Benzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00062Bromobenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00041Bromochloromethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00041Bromodichloromethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00084Bromoform
BRL 8260B P6A020010.015 1/14/16 19:52 MWWmg/kg dry 0.00091Bromomethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00037Carbon Tetrachloride
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00039Chlorobenzene
BRL 8260B P6A020010.015 1/14/16 19:52 MWWmg/kg dry 0.00062Chloroethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00053Chloroform
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00050Chloromethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00031cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00025cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00030Dibromochloromethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00034Dichlorodifluoromethane
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00028Ethylbenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00030Isopropyl Ether
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00044Isopropylbenzene (Cumene)
BRL 8260B P6A020010.015 1/14/16 19:52 MWWmg/kg dry 0.00068m,p-Xylenes
BRL 8260B P6A020010.074 1/14/16 19:52 MWWmg/kg dry 0.00067Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 63 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-5
Prism Sample ID: 6010230-14
Prism Work Order: 6010230
Time Collected: 01/13/16 11:55
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.15 1/14/16 19:52 MWWmg/kg dry 0.00067Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.074 1/14/16 19:52 MWWmg/kg dry 0.00063Methyl Isobutyl Ketone
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00042Methylene Chloride
BRL 8260B P6A020010.015 1/14/16 19:52 MWWmg/kg dry 0.00024Methyl-tert-Butyl Ether
BRL 8260B P6A020010.015 1/14/16 19:52 MWWmg/kg dry 0.00023Naphthalene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00038n-Butylbenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00044n-Propylbenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00030o-Xylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00036sec-Butylbenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00044Styrene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00025tert-Butylbenzene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00035Tetrachloroethylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00042Toluene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00044trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00039trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00048Trichloroethylene
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00048Trichlorofluoromethane
BRL 8260B P6A020010.037 1/14/16 19:52 MWWmg/kg dry 0.0010Vinyl acetate
BRL 8260B P6A020010.0074 1/14/16 19:52 MWWmg/kg dry 0.00036Vinyl chloride
BRL 8260B P6A020010.022 1/14/16 19:52 MWWmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 64 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-9
Prism Sample ID: 6010230-15
Prism Work Order: 6010230
Time Collected: 01/13/16 12:09
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
81.1 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0781-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0762,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0792,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0652-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0742-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0803,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.066Anthracene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 65 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-9
Prism Sample ID: 6010230-15
Prism Work Order: 6010230
Time Collected: 01/13/16 12:09
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.051Chrysene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.058Fluorene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.073Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.068Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.055Isophorone
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.065Naphthalene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.064N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.060Phenol
BRL 8270D P6A021510.41 1/15/16 16:06 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13270 %2,4,6-Tribromophenol
44-11566 %2-Fluorobiphenyl
35-11562 %2-Fluorophenol
37-12266 %Nitrobenzene-d5
34-12162 %Phenol-d5
54-12770 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.023 1/15/16 13:21 JABmg/kg dry 0.0015Mercury
1.6 *6010C P6A021110.30 1/15/16 23:43 bgmAbmg/kg dry 0.067Arsenic
22 *6010C P6A021110.60 1/15/16 23:43 bgmmg/kg dry 0.32Barium
BRL *6010C P6A021110.30 1/15/16 23:43 bgmmg/kg dry 0.0064Cadmium
7.2 *6010C P6A021110.30 1/15/16 23:43 bgmBHmg/kg dry 0.041Chromium
3.0 *6010C P6A021110.30 1/15/16 23:43 bgmmg/kg dry 0.032Lead
BRL *6010C P6A021110.60 1/15/16 23:43 bgmmg/kg dry 0.044Selenium
BRL *6010C P6A021110.30 1/15/16 23:43 bgmmg/kg dry 0.0049Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000631,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 66 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-9
Prism Sample ID: 6010230-15
Prism Work Order: 6010230
Time Collected: 01/13/16 12:09
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000371,1,1-Trichloroethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000521,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000681,1,2-Trichloroethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000211,1-Dichloroethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000341,1-Dichloroethylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000421,1-Dichloropropylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000431,2,3-Trichlorobenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000981,2,3-Trichloropropane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000571,2,4-Trichlorobenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000581,2,4-Trimethylbenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000311,2-Dibromoethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000361,2-Dichlorobenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000461,2-Dichloroethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000471,2-Dichloropropane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000581,3,5-Trimethylbenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000511,3-Dichlorobenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000381,3-Dichloropropane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000301,4-Dichlorobenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000362,2-Dichloropropane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000392-Chlorotoluene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000464-Chlorotoluene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.000374-Isopropyltoluene
BRL 8260B P6A020010.077 1/14/16 20:20 MWWmg/kg dry 0.0019Acetone
BRL 8260B P6A020010.0046 1/14/16 20:20 MWWmg/kg dry 0.00045Benzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00064Bromobenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00042Bromochloromethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00043Bromodichloromethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00087Bromoform
BRL 8260B P6A020010.015 1/14/16 20:20 MWWmg/kg dry 0.00094Bromomethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00038Carbon Tetrachloride
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00041Chlorobenzene
BRL 8260B P6A020010.015 1/14/16 20:20 MWWmg/kg dry 0.00064Chloroethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00055Chloroform
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00051Chloromethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00033cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00026cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00032Dibromochloromethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00035Dichlorodifluoromethane
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00029Ethylbenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00031Isopropyl Ether
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00045Isopropylbenzene (Cumene)
BRL 8260B P6A020010.015 1/14/16 20:20 MWWmg/kg dry 0.00071m,p-Xylenes
BRL 8260B P6A020010.077 1/14/16 20:20 MWWmg/kg dry 0.00069Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 67 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-5-9
Prism Sample ID: 6010230-15
Prism Work Order: 6010230
Time Collected: 01/13/16 12:09
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.15 1/14/16 20:20 MWWmg/kg dry 0.00069Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.077 1/14/16 20:20 MWWmg/kg dry 0.00065Methyl Isobutyl Ketone
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00043Methylene Chloride
BRL 8260B P6A020010.015 1/14/16 20:20 MWWmg/kg dry 0.00024Methyl-tert-Butyl Ether
BRL 8260B P6A020010.015 1/14/16 20:20 MWWmg/kg dry 0.00024Naphthalene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00039n-Butylbenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00045n-Propylbenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00031o-Xylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00037sec-Butylbenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00046Styrene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00026tert-Butylbenzene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00036Tetrachloroethylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00044Toluene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00046trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00040trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00050Trichloroethylene
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00049Trichlorofluoromethane
BRL 8260B P6A020010.038 1/14/16 20:20 MWWmg/kg dry 0.0010Vinyl acetate
BRL 8260B P6A020010.0077 1/14/16 20:20 MWWmg/kg dry 0.00037Vinyl chloride
BRL 8260B P6A020010.023 1/14/16 20:20 MWWmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123107 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 68 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-2
Prism Sample ID: 6010230-16
Prism Work Order: 6010230
Time Collected: 01/13/16 13:23
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
78.1 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0601,3-Dichlorobenzene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0811-Methylnaphthalene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0792,4,6-Trichlorophenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0822,4-Dichlorophenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0652,4-Dimethylphenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0602-Chlorophenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0682-Methylnaphthalene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0542-Methylphenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0772-Nitrophenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0833,3’-Dichlorobenzidine
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0634,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0734-Bromophenyl phenyl ether
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0514-Chloroaniline
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.0654-Nitrophenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.057Acenaphthene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.061Acenaphthylene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.068Anthracene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.056Azobenzene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.046Benzo(a)pyrene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.055Benzo(k)fluoranthene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.056Benzyl alcohol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 69 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-2
Prism Sample ID: 6010230-16
Prism Work Order: 6010230
Time Collected: 01/13/16 13:23
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.053Chrysene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.064Dibenzofuran
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.058Diethyl phthalate
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.054Fluoranthene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.061Fluorene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.067Hexachlorobenzene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.075Hexachlorocyclopentadiene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.071Hexachloroethane
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.057Isophorone
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.068Naphthalene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.060Nitrobenzene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.067N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.050Pentachlorophenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.055Phenanthrene
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.062Phenol
BRL 8270D P6A021510.42 1/15/16 16:28 JMVmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13275 %2,4,6-Tribromophenol
44-11568 %2-Fluorobiphenyl
35-11568 %2-Fluorophenol
37-12270 %Nitrobenzene-d5
34-12168 %Phenol-d5
54-12773 %Terphenyl-d14
Total Metals
0.056 *7471B P6A021210.024 1/15/16 13:26 JABmg/kg dry 0.0016Mercury
3.8 *6010C P6A021110.32 1/15/16 23:51 bgmAbmg/kg dry 0.071Arsenic
13 *6010C P6A021110.64 1/15/16 23:51 bgmmg/kg dry 0.34Barium
BRL *6010C P6A021110.32 1/15/16 23:51 bgmmg/kg dry 0.0067Cadmium
35 *6010C P6A021110.32 1/15/16 23:51 bgmAa, BH mg/kg dry 0.043Chromium
5.1 *6010C P6A021110.32 1/15/16 23:51 bgmmg/kg dry 0.033Lead
BRL *6010C P6A021110.64 1/15/16 23:51 bgmmg/kg dry 0.046Selenium
BRL *6010C P6A021110.32 1/15/16 23:51 bgmmg/kg dry 0.0052Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000501,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 70 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-2
Prism Sample ID: 6010230-16
Prism Work Order: 6010230
Time Collected: 01/13/16 13:23
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000411,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000541,1,2-Trichloroethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000331,1-Dichloropropylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000341,2,3-Trichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000771,2,3-Trichloropropane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000451,2,4-Trichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000461,2,4-Trimethylbenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000361,2-Dichloroethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000461,3,5-Trimethylbenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000401,3-Dichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000312-Chlorotoluene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000364-Chlorotoluene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.000294-Isopropyltoluene
BRL 8260B P6A020010.061 1/14/16 20:48 MWWmg/kg dry 0.0015Acetone
BRL 8260B P6A020010.0036 1/14/16 20:48 MWWmg/kg dry 0.00035Benzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00051Bromobenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00033Bromochloromethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00034Bromodichloromethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00069Bromoform
BRL 8260B P6A020010.012 1/14/16 20:48 MWWmg/kg dry 0.00075Bromomethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00030Carbon Tetrachloride
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00032Chlorobenzene
BRL 8260B P6A020010.012 1/14/16 20:48 MWWmg/kg dry 0.00051Chloroethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00044Chloroform
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00041Chloromethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00023Ethylbenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00036Isopropylbenzene (Cumene)
BRL 8260B P6A020010.012 1/14/16 20:48 MWWmg/kg dry 0.00056m,p-Xylenes
BRL 8260B P6A020010.061 1/14/16 20:48 MWWmg/kg dry 0.00055Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 71 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-2
Prism Sample ID: 6010230-16
Prism Work Order: 6010230
Time Collected: 01/13/16 13:23
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.12 1/14/16 20:48 MWWmg/kg dry 0.00055Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.061 1/14/16 20:48 MWWmg/kg dry 0.00052Methyl Isobutyl Ketone
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00034Methylene Chloride
BRL 8260B P6A020010.012 1/14/16 20:48 MWWmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P6A020010.012 1/14/16 20:48 MWWmg/kg dry 0.00019Naphthalene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00031n-Butylbenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00036n-Propylbenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00025o-Xylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00037Styrene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00035Toluene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00036trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00032trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00039Trichloroethylene
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00039Trichlorofluoromethane
BRL 8260B P6A020010.030 1/14/16 20:48 MWWmg/kg dry 0.00083Vinyl acetate
BRL 8260B P6A020010.0061 1/14/16 20:48 MWWmg/kg dry 0.00029Vinyl chloride
BRL 8260B P6A020010.018 1/14/16 20:48 MWWmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 72 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-5
Prism Sample ID: 6010230-17
Prism Work Order: 6010230
Time Collected: 01/13/16 13:38
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
82.4 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0621,2,4-Trichlorobenzene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0561,3-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0591,4-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0771-Methylnaphthalene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0752,4,6-Trichlorophenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0772,4-Dichlorophenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0612,4-Dimethylphenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0562,4-Dinitrophenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0582-Chloronaphthalene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0572-Chlorophenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0642-Methylnaphthalene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0512-Methylphenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0732-Nitrophenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0793,3’-Dichlorobenzidine
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0694-Bromophenyl phenyl ether
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0564-Chloro-3-methylphenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.0624-Nitrophenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.054Acenaphthene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.058Acenaphthylene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.065Anthracene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.052Benzo(a)anthracene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 73 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-5
Prism Sample ID: 6010230-17
Prism Work Order: 6010230
Time Collected: 01/13/16 13:38
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.057Butyl benzyl phthalate
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.050Chrysene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.061Dibenzofuran
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.057Di-n-butyl phthalate
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.051Fluoranthene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.058Fluorene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.064Hexachlorobenzene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.072Hexachlorobutadiene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.071Hexachlorocyclopentadiene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.067Hexachloroethane
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.054Isophorone
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.064Naphthalene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.057Nitrobenzene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.061N-Nitrosodiphenylamine
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.047Pentachlorophenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.052Phenanthrene
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.059Phenol
BRL 8270D P6A021510.40 1/15/16 16:50 JMVmg/kg dry 0.053Pyrene
Surrogate Recovery Control Limits
39-13250 %2,4,6-Tribromophenol
44-11547 %2-Fluorobiphenyl
35-11545 %2-Fluorophenol
37-12247 %Nitrobenzene-d5
34-12145 %Phenol-d5
54-12750 %Terphenyl-d14 SR
Total Metals
BRL *7471B P6A021210.025 1/15/16 13:30 JABmg/kg dry 0.0016Mercury
2.2 *6010C P6A021110.30 1/15/16 23:59 bgmAbmg/kg dry 0.067Arsenic
18 *6010C P6A021110.61 1/15/16 23:59 bgmmg/kg dry 0.32Barium
BRL *6010C P6A021110.30 1/15/16 23:59 bgmmg/kg dry 0.0064Cadmium
7.1 *6010C P6A021110.30 1/15/16 23:59 bgmAa, BH mg/kg dry 0.041Chromium
5.9 *6010C P6A021110.30 1/15/16 23:59 bgmmg/kg dry 0.032Lead
BRL *6010C P6A021110.61 1/15/16 23:59 bgmmg/kg dry 0.044Selenium
BRL *6010C P6A021110.30 1/15/16 23:59 bgmmg/kg dry 0.0050Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000571,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 74 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-5
Prism Sample ID: 6010230-17
Prism Work Order: 6010230
Time Collected: 01/13/16 13:38
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000341,1,1-Trichloroethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000621,1,2-Trichloroethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000401,2,3-Trichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000891,2,3-Trichloropropane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000521,2,4-Trichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000331,2-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000421,2-Dichloroethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000531,3,5-Trimethylbenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000424-Chlorotoluene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.000344-Isopropyltoluene
BRL 8260B P6A020010.070 1/14/16 21:15 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020010.0042 1/14/16 21:15 MWWmg/kg dry 0.00041Benzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00058Bromobenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00079Bromoform
BRL 8260B P6A020010.014 1/14/16 21:15 MWWmg/kg dry 0.00086Bromomethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00035Carbon Tetrachloride
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00037Chlorobenzene
BRL 8260B P6A020010.014 1/14/16 21:15 MWWmg/kg dry 0.00058Chloroethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00050Chloroform
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00047Chloromethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00030cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00032Dichlorodifluoromethane
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00027Ethylbenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6A020010.014 1/14/16 21:15 MWWmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P6A020010.070 1/14/16 21:15 MWWmg/kg dry 0.00063Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 75 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-5
Prism Sample ID: 6010230-17
Prism Work Order: 6010230
Time Collected: 01/13/16 13:38
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.14 1/14/16 21:15 MWWmg/kg dry 0.00063Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.070 1/14/16 21:15 MWWmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6A020010.014 1/14/16 21:15 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020010.014 1/14/16 21:15 MWWmg/kg dry 0.00022Naphthalene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00036n-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00029o-Xylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00034sec-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00042Styrene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00024tert-Butylbenzene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00040Toluene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00042trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00037trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00045Trichloroethylene
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P6A020010.035 1/14/16 21:15 MWWmg/kg dry 0.00096Vinyl acetate
BRL 8260B P6A020010.0070 1/14/16 21:15 MWWmg/kg dry 0.00034Vinyl chloride
BRL 8260B P6A020010.021 1/14/16 21:15 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 76 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-9
Prism Sample ID: 6010230-18
Prism Work Order: 6010230
Time Collected: 01/13/16 13:52
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
80.6 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0791-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0792,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0662-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0532-Methylphenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0752-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0813,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0513/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.066Anthracene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 77 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-9
Prism Sample ID: 6010230-18
Prism Work Order: 6010230
Time Collected: 01/13/16 13:52
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.052Chrysene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.059Fluorene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.074Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.055Isophorone
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.060Phenol
BRL 8270D P6A021510.41 1/15/16 17:12 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13260 %2,4,6-Tribromophenol
44-11557 %2-Fluorobiphenyl
35-11553 %2-Fluorophenol
37-12256 %Nitrobenzene-d5
34-12152 %Phenol-d5
54-12762 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.024 1/15/16 13:35 JABmg/kg dry 0.0016Mercury
2.2 *6010C P6A021110.31 1/16/16 0:07 bgmAbmg/kg dry 0.068Arsenic
41 *6010C P6A021110.61 1/16/16 0:07 bgmmg/kg dry 0.33Barium
BRL *6010C P6A021110.31 1/16/16 0:07 bgmmg/kg dry 0.0065Cadmium
8.1 *6010C P6A021110.31 1/16/16 0:07 bgmAa, BH mg/kg dry 0.042Chromium
6.9 *6010C P6A021110.31 1/16/16 0:07 bgmmg/kg dry 0.032Lead
BRL *6010C P6A021110.61 1/16/16 0:07 bgmmg/kg dry 0.044Selenium
BRL *6010C P6A021110.31 1/16/16 0:07 bgmmg/kg dry 0.0050Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000521,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 78 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-9
Prism Sample ID: 6010230-18
Prism Work Order: 6010230
Time Collected: 01/13/16 13:52
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000311,1,1-Trichloroethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000431,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000561,1,2-Trichloroethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000281,1-Dichloroethylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000351,1-Dichloropropylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000361,2,3-Trichlorobenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000811,2,3-Trichloropropane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000471,2,4-Trichlorobenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000491,2,4-Trimethylbenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000261,2-Dibromoethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000301,2-Dichlorobenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000381,2-Dichloroethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000391,2-Dichloropropane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000481,3,5-Trimethylbenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000421,3-Dichlorobenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000321,3-Dichloropropane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000332-Chlorotoluene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000384-Chlorotoluene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.000314-Isopropyltoluene
BRL 8260B P6A020010.064 1/14/16 21:43 MWWmg/kg dry 0.0016Acetone
BRL 8260B P6A020010.0038 1/14/16 21:43 MWWmg/kg dry 0.00037Benzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00053Bromobenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00035Bromochloromethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00072Bromoform
BRL 8260B P6A020010.013 1/14/16 21:43 MWWmg/kg dry 0.00078Bromomethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00032Carbon Tetrachloride
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00034Chlorobenzene
BRL 8260B P6A020010.013 1/14/16 21:43 MWWmg/kg dry 0.00053Chloroethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00046Chloroform
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00043Chloromethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00027cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00029Dichlorodifluoromethane
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00024Ethylbenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00038Isopropylbenzene (Cumene)
BRL 8260B P6A020010.013 1/14/16 21:43 MWWmg/kg dry 0.00059m,p-Xylenes
BRL 8260B P6A020010.064 1/14/16 21:43 MWWmg/kg dry 0.00057Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 79 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-6-9
Prism Sample ID: 6010230-18
Prism Work Order: 6010230
Time Collected: 01/13/16 13:52
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.13 1/14/16 21:43 MWWmg/kg dry 0.00057Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.064 1/14/16 21:43 MWWmg/kg dry 0.00054Methyl Isobutyl Ketone
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00036Methylene Chloride
BRL 8260B P6A020010.013 1/14/16 21:43 MWWmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6A020010.013 1/14/16 21:43 MWWmg/kg dry 0.00020Naphthalene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00038n-Propylbenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00026o-Xylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00031sec-Butylbenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00038Styrene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00037Toluene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00038trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00041Trichloroethylene
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00041Trichlorofluoromethane
BRL 8260B P6A020010.032 1/14/16 21:43 MWWmg/kg dry 0.00087Vinyl acetate
BRL 8260B P6A020010.0064 1/14/16 21:43 MWWmg/kg dry 0.00031Vinyl chloride
BRL 8260B P6A020010.019 1/14/16 21:43 MWWmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123106 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 80 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-2
Prism Sample ID: 6010230-19
Prism Work Order: 6010230
Time Collected: 01/13/16 13:19
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
81.3 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0591,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0781-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0762,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0782,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0652-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0742-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0803,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.065Anthracene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 81 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-2
Prism Sample ID: 6010230-19
Prism Work Order: 6010230
Time Collected: 01/13/16 13:19
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.051Chrysene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.058Fluorene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.064Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.073Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.072Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.068Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.055Isophorone
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.065Naphthalene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.064N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.060Phenol
BRL 8270D P6A021510.41 1/15/16 17:35 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13260 %2,4,6-Tribromophenol
44-11555 %2-Fluorobiphenyl
35-11554 %2-Fluorophenol
37-12257 %Nitrobenzene-d5
34-12154 %Phenol-d5
54-12761 %Terphenyl-d14
Total Metals
0.035 *7471B P6A023010.025 1/18/16 11:03 JABmg/kg dry 0.0016Mercury
2.3 *6010C P6A022910.31 1/18/16 20:12 bgmAmg/kg dry 0.069Arsenic
11 *6010C P6A022910.62 1/18/16 20:12 bgmAmg/kg dry 0.33Barium
BRL *6010C P6A022910.31 1/18/16 20:12 bgmAmg/kg dry 0.0066Cadmium
9.2 *6010C P6A022910.31 1/18/16 20:12 bgmAmg/kg dry 0.042Chromium
5.2 *6010C P6A022910.31 1/18/16 20:12 bgmAmg/kg dry 0.033Lead
BRL *6010C P6A022910.62 1/18/16 20:12 bgmAmg/kg dry 0.045Selenium
0.99 *6010C P6A022910.31 1/18/16 20:12 bgmAmg/kg dry 0.0051Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000641,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 82 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-2
Prism Sample ID: 6010230-19
Prism Work Order: 6010230
Time Collected: 01/13/16 13:19
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000381,1,1-Trichloroethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000531,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000691,1,2-Trichloroethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000221,1-Dichloroethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000341,1-Dichloroethylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000431,1-Dichloropropylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000441,2,3-Trichlorobenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000991,2,3-Trichloropropane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000581,2,4-Trichlorobenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000591,2,4-Trimethylbenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000311,2-Dibromoethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000371,2-Dichlorobenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000461,2-Dichloroethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000481,2-Dichloropropane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000591,3,5-Trimethylbenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000521,3-Dichlorobenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000391,3-Dichloropropane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000311,4-Dichlorobenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000372,2-Dichloropropane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000402-Chlorotoluene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000464-Chlorotoluene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.000384-Isopropyltoluene
BRL 8260B P6A020010.078 1/14/16 22:11 MWWmg/kg dry 0.0019Acetone
BRL 8260B P6A020010.0047 1/14/16 22:11 MWWmg/kg dry 0.00045Benzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00065Bromobenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00043Bromochloromethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00043Bromodichloromethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00088Bromoform
BRL 8260B P6A020010.016 1/14/16 22:11 MWWmg/kg dry 0.00096Bromomethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00039Carbon Tetrachloride
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00041Chlorobenzene
BRL 8260B P6A020010.016 1/14/16 22:11 MWWmg/kg dry 0.00065Chloroethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00056Chloroform
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00052Chloromethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00033cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00026cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00032Dibromochloromethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00035Dichlorodifluoromethane
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00030Ethylbenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00032Isopropyl Ether
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00046Isopropylbenzene (Cumene)
BRL 8260B P6A020010.016 1/14/16 22:11 MWWmg/kg dry 0.00072m,p-Xylenes
BRL 8260B P6A020010.078 1/14/16 22:11 MWWmg/kg dry 0.00070Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 83 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-2
Prism Sample ID: 6010230-19
Prism Work Order: 6010230
Time Collected: 01/13/16 13:19
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.16 1/14/16 22:11 MWWmg/kg dry 0.00070Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.078 1/14/16 22:11 MWWmg/kg dry 0.00066Methyl Isobutyl Ketone
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00044Methylene Chloride
BRL 8260B P6A020010.016 1/14/16 22:11 MWWmg/kg dry 0.00025Methyl-tert-Butyl Ether
BRL 8260B P6A020010.016 1/14/16 22:11 MWWmg/kg dry 0.00025Naphthalene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00040n-Butylbenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00046n-Propylbenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00032o-Xylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00038sec-Butylbenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00047Styrene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00026tert-Butylbenzene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00037Tetrachloroethylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00045Toluene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00047trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00041trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00050Trichloroethylene
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00050Trichlorofluoromethane
BRL 8260B P6A020010.039 1/14/16 22:11 MWWmg/kg dry 0.0011Vinyl acetate
BRL 8260B P6A020010.0078 1/14/16 22:11 MWWmg/kg dry 0.00038Vinyl chloride
BRL 8260B P6A020010.023 1/14/16 22:11 MWWmg/kg dry 0.0015Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123109 %Dibromofluoromethane
76-12996 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 84 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-5
Prism Sample ID: 6010230-20
Prism Work Order: 6010230
Time Collected: 01/13/16 13:35
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
81.6 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0631,2,4-Trichlorobenzene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0591,4-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0781-Methylnaphthalene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0762,4,6-Trichlorophenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0782,4-Dichlorophenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0572-Chlorophenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0652-Methylnaphthalene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0742-Nitrophenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0803,3’-Dichlorobenzidine
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.0624-Nitrophenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.065Anthracene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.053Benzo(k)fluoranthene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.070bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.057Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.069Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 85 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-5
Prism Sample ID: 6010230-20
Prism Work Order: 6010230
Time Collected: 01/13/16 13:35
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.051Chrysene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.058Fluorene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.064Hexachlorobenzene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.073Hexachlorobutadiene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.072Hexachlorocyclopentadiene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.068Hexachloroethane
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.055Isophorone
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.065Naphthalene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.064N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.060Phenol
BRL 8270D P6A021510.40 1/15/16 17:57 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13262 %2,4,6-Tribromophenol
44-11557 %2-Fluorobiphenyl
35-11556 %2-Fluorophenol
37-12258 %Nitrobenzene-d5
34-12155 %Phenol-d5
54-12762 %Terphenyl-d14
Total Metals
0.054 *7471B P6A023010.025 1/18/16 11:17 JABmg/kg dry 0.0016Mercury
1.7 *6010C P6A022910.31 1/18/16 20:38 bgmAmg/kg dry 0.069Arsenic
23 *6010C P6A022910.62 1/18/16 20:38 bgmAmg/kg dry 0.33Barium
BRL *6010C P6A022910.31 1/18/16 20:38 bgmAmg/kg dry 0.0066Cadmium
6.2 *6010C P6A022910.31 1/18/16 20:38 bgmAmg/kg dry 0.042Chromium
6.1 *6010C P6A022910.31 1/18/16 20:38 bgmAmg/kg dry 0.033Lead
BRL *6010C P6A022910.62 1/18/16 20:38 bgmAmg/kg dry 0.045Selenium
0.90 *6010C P6A022910.31 1/18/16 20:38 bgmAmg/kg dry 0.0051Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000681,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 86 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-5
Prism Sample ID: 6010230-20
Prism Work Order: 6010230
Time Collected: 01/13/16 13:35
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000401,1,1-Trichloroethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000561,1,2,2-Tetrachloroethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000731,1,2-Trichloroethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000231,1-Dichloroethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000361,1-Dichloroethylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000451,1-Dichloropropylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000471,2,3-Trichlorobenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00111,2,3-Trichloropropane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000611,2,4-Trichlorobenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000631,2,4-Trimethylbenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000331,2-Dibromoethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000391,2-Dichlorobenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000491,2-Dichloroethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000511,2-Dichloropropane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000621,3,5-Trimethylbenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000551,3-Dichlorobenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000411,3-Dichloropropane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000321,4-Dichlorobenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000392,2-Dichloropropane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000432-Chlorotoluene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000494-Chlorotoluene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.000404-Isopropyltoluene
BRL 8260B P6A020010.082 1/14/16 22:39 MWWmg/kg dry 0.0020Acetone
BRL 8260B P6A020010.0049 1/14/16 22:39 MWWmg/kg dry 0.00048Benzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00069Bromobenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00045Bromochloromethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00046Bromodichloromethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00094Bromoform
BRL 8260B P6A020010.016 1/14/16 22:39 MWWmg/kg dry 0.0010Bromomethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00041Carbon Tetrachloride
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00044Chlorobenzene
BRL 8260B P6A020010.016 1/14/16 22:39 MWWmg/kg dry 0.00069Chloroethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00059Chloroform
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00055Chloromethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00035cis-1,2-Dichloroethylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00028cis-1,3-Dichloropropylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00034Dibromochloromethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00037Dichlorodifluoromethane
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00032Ethylbenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00034Isopropyl Ether
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00049Isopropylbenzene (Cumene)
BRL 8260B P6A020010.016 1/14/16 22:39 MWWmg/kg dry 0.00076m,p-Xylenes
BRL 8260B P6A020010.082 1/14/16 22:39 MWWmg/kg dry 0.00074Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 87 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-5
Prism Sample ID: 6010230-20
Prism Work Order: 6010230
Time Collected: 01/13/16 13:35
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020010.16 1/14/16 22:39 MWWmg/kg dry 0.00074Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020010.082 1/14/16 22:39 MWWmg/kg dry 0.00070Methyl Isobutyl Ketone
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00046Methylene Chloride
BRL 8260B P6A020010.016 1/14/16 22:39 MWWmg/kg dry 0.00026Methyl-tert-Butyl Ether
BRL 8260B P6A020010.016 1/14/16 22:39 MWWmg/kg dry 0.00026Naphthalene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00042n-Butylbenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00049n-Propylbenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00034o-Xylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00040sec-Butylbenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00050Styrene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00028tert-Butylbenzene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00039Tetrachloroethylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00047Toluene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00049trans-1,2-Dichloroethylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00043trans-1,3-Dichloropropylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00053Trichloroethylene
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00053Trichlorofluoromethane
BRL 8260B P6A020010.041 1/14/16 22:39 MWWmg/kg dry 0.0011Vinyl acetate
BRL 8260B P6A020010.0082 1/14/16 22:39 MWWmg/kg dry 0.00040Vinyl chloride
BRL 8260B P6A020010.025 1/14/16 22:39 MWWmg/kg dry 0.0015Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12997 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 88 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-9
Prism Sample ID: 6010230-21
Prism Work Order: 6010230
Time Collected: 01/13/16 13:50
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
76.6 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0612-Chlorophenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0782-Nitrophenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0853,3’-Dichlorobenzidine
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.0664-Nitrophenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.059Acenaphthene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.069Anthracene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 89 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-9
Prism Sample ID: 6010230-21
Prism Work Order: 6010230
Time Collected: 01/13/16 13:50
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.054Chrysene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.066Dibenzofuran
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.062Fluorene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.058Isophorone
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.069Naphthalene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.064Phenol
BRL 8270D P6A021510.43 1/15/16 18:19 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13258 %2,4,6-Tribromophenol
44-11553 %2-Fluorobiphenyl
35-11553 %2-Fluorophenol
37-12253 %Nitrobenzene-d5
34-12151 %Phenol-d5
54-12757 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.024 1/18/16 11:21 JABmg/kg dry 0.0016Mercury
1.9 *6010C P6A022910.32 1/18/16 20:47 bgmAmg/kg dry 0.071Arsenic
52 *6010C P6A022910.64 1/18/16 20:47 bgmAmg/kg dry 0.34Barium
BRL *6010C P6A022910.32 1/18/16 20:47 bgmAmg/kg dry 0.0068Cadmium
2.8 *6010C P6A022910.32 1/18/16 20:47 bgmAmg/kg dry 0.044Chromium
7.0 *6010C P6A022910.32 1/18/16 20:47 bgmAmg/kg dry 0.034Lead
BRL *6010C P6A022910.64 1/18/16 20:47 bgmAmg/kg dry 0.047Selenium
0.71 *6010C P6A022910.32 1/18/16 20:47 bgmAmg/kg dry 0.0053Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000551,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 90 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-9
Prism Sample ID: 6010230-21
Prism Work Order: 6010230
Time Collected: 01/13/16 13:50
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000321,1,1-Trichloroethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000451,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000591,1,2-Trichloroethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000381,2,3-Trichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000861,2,3-Trichloropropane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000501,2,4-Trichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000511,2,4-Trimethylbenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000401,2-Dichloroethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000421,2-Dichloropropane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000511,3,5-Trimethylbenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000404-Chlorotoluene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.000324-Isopropyltoluene
BRL 8260B P6A020110.067 1/14/16 14:14 MWWmg/kg dry 0.0016Acetone
BRL 8260B P6A020110.0040 1/14/16 14:14 MWWmg/kg dry 0.00039Benzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00056Bromobenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00076Bromoform
BRL 8260B P6A020110.013 1/14/16 14:14 MWWmg/kg dry 0.00083Bromomethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00036Chlorobenzene
BRL 8260B P6A020110.013 1/14/16 14:14 MWWmg/kg dry 0.00056Chloroethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00048Chloroform
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00045Chloromethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00030Dichlorodifluoromethane
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P6A020110.013 1/14/16 14:14 MWWmg/kg dry 0.00062m,p-Xylenes
BRL 8260B P6A020110.067 1/14/16 14:14 MWWmg/kg dry 0.00061Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 91 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-7-9
Prism Sample ID: 6010230-21
Prism Work Order: 6010230
Time Collected: 01/13/16 13:50
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.13 1/14/16 14:14 MWWmg/kg dry 0.00061Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.067 1/14/16 14:14 MWWmg/kg dry 0.00057Methyl Isobutyl Ketone
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00038Methylene Chloride
BRL 8260B P6A020110.013 1/14/16 14:14 MWWmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P6A020110.013 1/14/16 14:14 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00040Styrene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00039Toluene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00040trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00044Trichloroethylene
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P6A020110.034 1/14/16 14:14 MWWmg/kg dry 0.00092Vinyl acetate
BRL 8260B P6A020110.0067 1/14/16 14:14 MWWmg/kg dry 0.00032Vinyl chloride
BRL 8260B P6A020110.020 1/14/16 14:14 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-13096 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12990 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 92 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-2
Prism Sample ID: 6010230-22
Prism Work Order: 6010230
Time Collected: 01/13/16 10:32
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
76.4 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0661,2-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0612-Chlorophenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0792-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0853,3’-Dichlorobenzidine
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0614-Chloro-3-methylphenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.0674-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.059Acenaphthene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.070Anthracene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 93 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-2
Prism Sample ID: 6010230-22
Prism Work Order: 6010230
Time Collected: 01/13/16 10:32
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.054Chrysene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.053Dibenzo(a,h)anthracene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.066Dibenzofuran
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.062Fluorene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.069Hexachlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.078Hexachlorobutadiene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.050Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.058Isophorone
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.069Naphthalene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.064Phenol
BRL 8270D P6A019810.43 1/14/16 22:15 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13266 %2,4,6-Tribromophenol
44-11564 %2-Fluorobiphenyl
35-11559 %2-Fluorophenol
37-12266 %Nitrobenzene-d5
34-12159 %Phenol-d5
54-12767 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.026 1/15/16 13:07 JABmg/kg dry 0.0017Mercury
2.6 *6010C P6A021110.32 1/15/16 23:17 bgmAbmg/kg dry 0.071Arsenic
85 *6010C P6A021110.64 1/15/16 23:17 bgmmg/kg dry 0.34Barium
BRL *6010C P6A021110.32 1/15/16 23:17 bgmmg/kg dry 0.0068Cadmium
3.9 *6010C P6A021110.32 1/15/16 23:17 bgmAa, BH mg/kg dry 0.044Chromium
6.2 *6010C P6A021110.32 1/15/16 23:17 bgmmg/kg dry 0.034Lead
BRL *6010C P6A021110.64 1/15/16 23:17 bgmmg/kg dry 0.047Selenium
BRL *6010C P6A021110.32 1/15/16 23:17 bgmmg/kg dry 0.0053Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000561,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 94 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-2
Prism Sample ID: 6010230-22
Prism Work Order: 6010230
Time Collected: 01/13/16 10:32
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000331,1,1-Trichloroethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000461,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000601,1,2-Trichloroethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000871,2,3-Trichloropropane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000521,2,4-Trimethylbenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000421,2-Dichloropropane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000511,3,5-Trimethylbenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000451,3-Dichlorobenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P6A020110.068 1/14/16 14:45 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020110.0041 1/14/16 14:45 MWWmg/kg dry 0.00040Benzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00057Bromobenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00038Bromodichloromethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00077Bromoform
BRL 8260B P6A020110.014 1/14/16 14:45 MWWmg/kg dry 0.00084Bromomethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00036Chlorobenzene
BRL 8260B P6A020110.014 1/14/16 14:45 MWWmg/kg dry 0.00057Chloroethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00049Chloroform
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00046Chloromethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P6A020110.014 1/14/16 14:45 MWWmg/kg dry 0.00063m,p-Xylenes
BRL 8260B P6A020110.068 1/14/16 14:45 MWWmg/kg dry 0.00061Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 95 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-2
Prism Sample ID: 6010230-22
Prism Work Order: 6010230
Time Collected: 01/13/16 10:32
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.14 1/14/16 14:45 MWWmg/kg dry 0.00061Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.068 1/14/16 14:45 MWWmg/kg dry 0.00058Methyl Isobutyl Ketone
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00038Methylene Chloride
BRL 8260B P6A020110.014 1/14/16 14:45 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020110.014 1/14/16 14:45 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00041Styrene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00039Toluene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00044Trichloroethylene
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00044Trichlorofluoromethane
BRL 8260B P6A020110.034 1/14/16 14:45 MWWmg/kg dry 0.00093Vinyl acetate
BRL 8260B P6A020110.0068 1/14/16 14:45 MWWmg/kg dry 0.00033Vinyl chloride
BRL 8260B P6A020110.020 1/14/16 14:45 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130106 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12988 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 96 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-5
Prism Sample ID: 6010230-23
Prism Work Order: 6010230
Time Collected: 01/13/16 10:53
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
76.1 *SM2540 G P6A021910.100 1/15/16 16:00 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0681,2,4-Trichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0661,2-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0842,4-Dichlorophenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0532,4-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0582,6-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0632-Chloronaphthalene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0612-Chlorophenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0792-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0863,3’-Dichlorobenzidine
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0614-Chloro-3-methylphenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.0674-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.059Acenaphthene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.063Acenaphthylene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.070Anthracene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.057Benzo(a)anthracene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 97 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-5
Prism Sample ID: 6010230-23
Prism Work Order: 6010230
Time Collected: 01/13/16 10:53
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.062Butyl benzyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.055Chrysene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.053Dibenzo(a,h)anthracene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.066Dibenzofuran
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.060Diethyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.062Di-n-butyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.062Fluorene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.069Hexachlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.078Hexachlorobutadiene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.073Hexachloroethane
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.050Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.059Isophorone
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.070Naphthalene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.062Nitrobenzene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.064Phenol
BRL 8270D P6A019810.43 1/14/16 22:37 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13270 %2,4,6-Tribromophenol
44-11567 %2-Fluorobiphenyl
35-11562 %2-Fluorophenol
37-12270 %Nitrobenzene-d5
34-12161 %Phenol-d5
54-12773 %Terphenyl-d14
Total Metals
BRL *7471B P6A021210.028 1/15/16 13:12 JABmg/kg dry 0.0018Mercury
2.5 *6010C P6A021110.33 1/15/16 23:25 bgmAbmg/kg dry 0.074Arsenic
190 *6010C P6A021110.67 1/15/16 23:25 bgmmg/kg dry 0.36Barium
BRL *6010C P6A021110.33 1/15/16 23:25 bgmmg/kg dry 0.0071Cadmium
1.4 *6010C P6A021110.33 1/15/16 23:25 bgmAamg/kg dry 0.045Chromium
3.9 *6010C P6A021110.33 1/15/16 23:25 bgmmg/kg dry 0.035Lead
BRL *6010C P6A021110.67 1/15/16 23:25 bgmmg/kg dry 0.048Selenium
BRL *6010C P6A021110.33 1/15/16 23:25 bgmmg/kg dry 0.0055Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000511,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 98 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-5
Prism Sample ID: 6010230-23
Prism Work Order: 6010230
Time Collected: 01/13/16 10:53
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000301,1,1-Trichloroethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000421,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000551,1,2-Trichloroethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000281,1-Dichloroethylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000361,2,3-Trichlorobenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000801,2,3-Trichloropropane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000471,2,4-Trichlorobenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000481,2,4-Trimethylbenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000371,2-Dichloroethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000391,2-Dichloropropane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000471,3,5-Trimethylbenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000411,3-Dichlorobenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000374-Chlorotoluene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.000304-Isopropyltoluene
0.013 8260B P6A020110.063 1/14/16 15:17 MWWJmg/kg dry 0.0015Acetone
BRL 8260B P6A020110.0038 1/14/16 15:17 MWWmg/kg dry 0.00036Benzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00052Bromobenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00034Bromochloromethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00071Bromoform
BRL 8260B P6A020110.013 1/14/16 15:17 MWWmg/kg dry 0.00077Bromomethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00033Chlorobenzene
BRL 8260B P6A020110.013 1/14/16 15:17 MWWmg/kg dry 0.00052Chloroethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00045Chloroform
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00042Chloromethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00027cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00024Ethylbenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00037Isopropylbenzene (Cumene)
BRL 8260B P6A020110.013 1/14/16 15:17 MWWmg/kg dry 0.00058m,p-Xylenes
BRL 8260B P6A020110.063 1/14/16 15:17 MWWmg/kg dry 0.00057Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 99 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-5
Prism Sample ID: 6010230-23
Prism Work Order: 6010230
Time Collected: 01/13/16 10:53
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.13 1/14/16 15:17 MWWmg/kg dry 0.00057Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.063 1/14/16 15:17 MWWmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00035Methylene Chloride
BRL 8260B P6A020110.013 1/14/16 15:17 MWWmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6A020110.013 1/14/16 15:17 MWWmg/kg dry 0.00020Naphthalene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00026o-Xylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00038Styrene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00036Toluene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00041Trichloroethylene
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00040Trichlorofluoromethane
BRL 8260B P6A020110.031 1/14/16 15:17 MWWmg/kg dry 0.00086Vinyl acetate
BRL 8260B P6A020110.0063 1/14/16 15:17 MWWmg/kg dry 0.00030Vinyl chloride
BRL 8260B P6A020110.019 1/14/16 15:17 MWWmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123111 %Dibromofluoromethane
76-12988 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 100 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-9
Prism Sample ID: 6010230-24
Prism Work Order: 6010230
Time Collected: 01/13/16 11:11
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
76.5 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0612-Chlorophenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0782-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0853,3’-Dichlorobenzidine
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.0664-Nitrophenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.059Acenaphthene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.069Anthracene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 101 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-9
Prism Sample ID: 6010230-24
Prism Work Order: 6010230
Time Collected: 01/13/16 11:11
Time Submitted: 01/14/16 08:20
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.054Chrysene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.066Dibenzofuran
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.062Fluorene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.058Isophorone
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.069Naphthalene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.064Phenol
BRL 8270D P6A019810.43 1/14/16 22:59 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13273 %2,4,6-Tribromophenol
44-11568 %2-Fluorobiphenyl
35-11561 %2-Fluorophenol
37-12270 %Nitrobenzene-d5
34-12161 %Phenol-d5
54-12776 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.029 1/18/16 11:26 JABmg/kg dry 0.0019Mercury
2.8 *6010C P6A022910.32 1/18/16 20:56 bgmAmg/kg dry 0.071Arsenic
120 *6010C P6A022910.64 1/18/16 20:56 bgmAmg/kg dry 0.34Barium
BRL *6010C P6A022910.32 1/18/16 20:56 bgmAmg/kg dry 0.0068Cadmium
2.4 *6010C P6A022910.32 1/18/16 20:56 bgmAmg/kg dry 0.044Chromium
5.1 *6010C P6A022910.32 1/18/16 20:56 bgmAmg/kg dry 0.034Lead
BRL *6010C P6A022910.64 1/18/16 20:56 bgmAmg/kg dry 0.047Selenium
0.82 *6010C P6A022910.32 1/18/16 20:56 bgmAmg/kg dry 0.0053Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000561,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 102 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-9
Prism Sample ID: 6010230-24
Prism Work Order: 6010230
Time Collected: 01/13/16 11:11
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000331,1,1-Trichloroethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000461,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000611,1,2-Trichloroethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000881,2,3-Trichloropropane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000521,2,4-Trimethylbenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000451,3-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P6A020110.069 1/14/16 15:48 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020110.0041 1/14/16 15:48 MWWmg/kg dry 0.00040Benzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00057Bromobenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00038Bromodichloromethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00078Bromoform
BRL 8260B P6A020110.014 1/14/16 15:48 MWWmg/kg dry 0.00085Bromomethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00036Chlorobenzene
BRL 8260B P6A020110.014 1/14/16 15:48 MWWmg/kg dry 0.00057Chloroethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00050Chloroform
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00046Chloromethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6A020110.014 1/14/16 15:48 MWWmg/kg dry 0.00063m,p-Xylenes
BRL 8260B P6A020110.069 1/14/16 15:48 MWWmg/kg dry 0.00062Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 103 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-8-9
Prism Sample ID: 6010230-24
Prism Work Order: 6010230
Time Collected: 01/13/16 11:11
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.14 1/14/16 15:48 MWWmg/kg dry 0.00062Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.069 1/14/16 15:48 MWWmg/kg dry 0.00058Methyl Isobutyl Ketone
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6A020110.014 1/14/16 15:48 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020110.014 1/14/16 15:48 MWWmg/kg dry 0.00022Naphthalene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00041Styrene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00039Toluene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00044Trichloroethylene
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00044Trichlorofluoromethane
BRL 8260B P6A020110.034 1/14/16 15:48 MWWmg/kg dry 0.00094Vinyl acetate
BRL 8260B P6A020110.0069 1/14/16 15:48 MWWmg/kg dry 0.00033Vinyl chloride
BRL 8260B P6A020110.021 1/14/16 15:48 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130105 %4-Bromofluorobenzene
84-123100 %Dibromofluoromethane
76-12984 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 104 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-2
Prism Sample ID: 6010230-25
Prism Work Order: 6010230
Time Collected: 01/13/16 11:36
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
82.7 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0621,2,4-Trichlorobenzene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0611,2-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0561,3-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0581,4-Dichlorobenzene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0771-Methylnaphthalene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0752,4,6-Trichlorophenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0772,4-Dichlorophenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0612,4-Dimethylphenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0562,4-Dinitrophenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0582-Chloronaphthalene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0572-Chlorophenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0642-Methylnaphthalene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0512-Methylphenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0732-Nitrophenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0793,3’-Dichlorobenzidine
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0694-Bromophenyl phenyl ether
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0564-Chloro-3-methylphenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.0624-Nitrophenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.054Acenaphthene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.058Acenaphthylene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.064Anthracene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.052Benzo(a)anthracene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.052Benzo(k)fluoranthene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.069bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 105 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-2
Prism Sample ID: 6010230-25
Prism Work Order: 6010230
Time Collected: 01/13/16 11:36
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.057Butyl benzyl phthalate
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.050Chrysene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.061Dibenzofuran
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.057Di-n-butyl phthalate
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.051Fluoranthene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.057Fluorene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.063Hexachlorobenzene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.072Hexachlorobutadiene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.071Hexachlorocyclopentadiene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.067Hexachloroethane
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.054Isophorone
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.064Naphthalene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.057Nitrobenzene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.061N-Nitrosodiphenylamine
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.047Pentachlorophenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.052Phenanthrene
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.059Phenol
BRL 8270D P6A021510.40 1/15/16 18:41 JMVmg/kg dry 0.053Pyrene
Surrogate Recovery Control Limits
39-13264 %2,4,6-Tribromophenol
44-11559 %2-Fluorobiphenyl
35-11558 %2-Fluorophenol
37-12260 %Nitrobenzene-d5
34-12157 %Phenol-d5
54-12763 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.025 1/18/16 11:31 JABmg/kg dry 0.0017Mercury
2.2 *6010C P6A022910.31 1/18/16 21:06 bgmAmg/kg dry 0.068Arsenic
82 *6010C P6A022910.61 1/18/16 21:06 bgmAmg/kg dry 0.33Barium
BRL *6010C P6A022910.31 1/18/16 21:06 bgmAmg/kg dry 0.0065Cadmium
2.4 *6010C P6A022910.31 1/18/16 21:06 bgmAmg/kg dry 0.042Chromium
1.0 *6010C P6A022910.31 1/18/16 21:06 bgmAmg/kg dry 0.032Lead
BRL *6010C P6A022910.61 1/18/16 21:06 bgmAmg/kg dry 0.045Selenium
0.32 *6010C P6A022910.31 1/18/16 21:06 bgmAmg/kg dry 0.0050Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000551,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 106 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-2
Prism Sample ID: 6010230-25
Prism Work Order: 6010230
Time Collected: 01/13/16 11:36
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000321,1,1-Trichloroethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000451,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000591,1,2-Trichloroethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000291,1-Dichloroethylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000361,1-Dichloropropylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000381,2,3-Trichlorobenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000851,2,3-Trichloropropane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000491,2,4-Trichlorobenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000511,2,4-Trimethylbenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000311,2-Dichlorobenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000401,2-Dichloroethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000411,2-Dichloropropane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000501,3,5-Trimethylbenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000331,3-Dichloropropane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000342-Chlorotoluene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000404-Chlorotoluene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.000324-Isopropyltoluene
0.044 8260B P6A020110.066 1/14/16 16:19 MWWJmg/kg dry 0.0016Acetone
BRL 8260B P6A020110.0040 1/14/16 16:19 MWWmg/kg dry 0.00039Benzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00055Bromobenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00076Bromoform
BRL 8260B P6A020110.013 1/14/16 16:19 MWWmg/kg dry 0.00082Bromomethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00035Chlorobenzene
BRL 8260B P6A020110.013 1/14/16 16:19 MWWmg/kg dry 0.00055Chloroethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00048Chloroform
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00045Chloromethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00028cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00022cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00027Dibromochloromethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00030Dichlorodifluoromethane
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00039Isopropylbenzene (Cumene)
BRL 8260B P6A020110.013 1/14/16 16:19 MWWmg/kg dry 0.00061m,p-Xylenes
BRL 8260B P6A020110.066 1/14/16 16:19 MWWmg/kg dry 0.00060Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 107 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-2
Prism Sample ID: 6010230-25
Prism Work Order: 6010230
Time Collected: 01/13/16 11:36
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.13 1/14/16 16:19 MWWmg/kg dry 0.00060Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.066 1/14/16 16:19 MWWmg/kg dry 0.00057Methyl Isobutyl Ketone
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00037Methylene Chloride
BRL 8260B P6A020110.013 1/14/16 16:19 MWWmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P6A020110.013 1/14/16 16:19 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00039n-Propylbenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00027o-Xylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00040Styrene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00022tert-Butylbenzene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00038Toluene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00040trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00043Trichloroethylene
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P6A020110.033 1/14/16 16:19 MWWmg/kg dry 0.00091Vinyl acetate
BRL 8260B P6A020110.0066 1/14/16 16:19 MWWmg/kg dry 0.00032Vinyl chloride
BRL 8260B P6A020110.020 1/14/16 16:19 MWWmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12994 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 108 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-5
Prism Sample ID: 6010230-26
Prism Work Order: 6010230
Time Collected: 01/13/16 12:01
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
73.6 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0701,2,4-Trichlorobenzene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0681,2-Dichlorobenzene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0631,3-Dichlorobenzene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0661,4-Dichlorobenzene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0861-Methylnaphthalene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0842,4,6-Trichlorophenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0872,4-Dichlorophenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0692,4-Dimethylphenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0632,4-Dinitrophenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0542,4-Dinitrotoluene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0602,6-Dinitrotoluene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0652-Chloronaphthalene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0642-Chlorophenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0722-Methylnaphthalene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0572-Methylphenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0822-Nitrophenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0893,3’-Dichlorobenzidine
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0553/4-Methylphenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0674,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0774-Bromophenyl phenyl ether
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0634-Chloro-3-methylphenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0544-Chloroaniline
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0584-Chlorophenyl phenyl ether
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.0694-Nitrophenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.061Acenaphthene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.065Acenaphthylene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.072Anthracene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.059Azobenzene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.059Benzo(a)anthracene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.048Benzo(a)pyrene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.052Benzo(b)fluoranthene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.049Benzo(g,h,i)perylene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.059Benzo(k)fluoranthene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.038Benzoic Acid
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.059Benzyl alcohol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.078bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.063Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.077Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.067Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 109 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-5
Prism Sample ID: 6010230-26
Prism Work Order: 6010230
Time Collected: 01/13/16 12:01
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.064Butyl benzyl phthalate
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.057Chrysene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.055Dibenzo(a,h)anthracene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.068Dibenzofuran
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.062Diethyl phthalate
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.059Dimethyl phthalate
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.064Di-n-butyl phthalate
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.055Di-n-octyl phthalate
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.057Fluoranthene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.064Fluorene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.071Hexachlorobenzene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.081Hexachlorobutadiene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.080Hexachlorocyclopentadiene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.075Hexachloroethane
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.051Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.061Isophorone
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.072Naphthalene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.064Nitrobenzene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.071N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.068N-Nitrosodiphenylamine
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.053Pentachlorophenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.058Phenanthrene
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.066Phenol
BRL 8270D P6A021510.45 1/15/16 19:04 JMVmg/kg dry 0.059Pyrene
Surrogate Recovery Control Limits
39-13253 %2,4,6-Tribromophenol
44-11555 %2-Fluorobiphenyl
35-11549 %2-Fluorophenol
37-12256 %Nitrobenzene-d5
34-12149 %Phenol-d5
54-12759 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.027 1/18/16 11:36 JABmg/kg dry 0.0018Mercury
3.9 *6010C P6A022910.33 1/18/16 21:15 bgmAmg/kg dry 0.074Arsenic
90 *6010C P6A022910.66 1/18/16 21:15 bgmAmg/kg dry 0.35Barium
BRL *6010C P6A022910.33 1/18/16 21:15 bgmAmg/kg dry 0.0070Cadmium
3.6 *6010C P6A022910.33 1/18/16 21:15 bgmAmg/kg dry 0.045Chromium
2.2 *6010C P6A022910.33 1/18/16 21:15 bgmAmg/kg dry 0.035Lead
BRL *6010C P6A022910.66 1/18/16 21:15 bgmAmg/kg dry 0.048Selenium
BRL *6010C P6A022910.33 1/18/16 21:15 bgmAmg/kg dry 0.0054Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000711,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 110 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-5
Prism Sample ID: 6010230-26
Prism Work Order: 6010230
Time Collected: 01/13/16 12:01
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000421,1,1-Trichloroethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000581,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000771,1,2-Trichloroethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000241,1-Dichloroethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000381,1-Dichloroethylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000471,1-Dichloropropylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000491,2,3-Trichlorobenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00111,2,3-Trichloropropane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000641,2,4-Trichlorobenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000661,2,4-Trimethylbenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000351,2-Dibromoethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000411,2-Dichlorobenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000521,2-Dichloroethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000541,2-Dichloropropane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000651,3,5-Trimethylbenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000571,3-Dichlorobenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000431,3-Dichloropropane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000341,4-Dichlorobenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000412,2-Dichloropropane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000452-Chlorotoluene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000524-Chlorotoluene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.000424-Isopropyltoluene
BRL 8260B P6A020110.086 1/14/16 16:51 MWWmg/kg dry 0.0021Acetone
BRL 8260B P6A020110.0052 1/14/16 16:51 MWWmg/kg dry 0.00050Benzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00072Bromobenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00048Bromochloromethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00048Bromodichloromethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00098Bromoform
BRL 8260B P6A020110.017 1/14/16 16:51 MWWmg/kg dry 0.0011Bromomethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00043Carbon Tetrachloride
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00046Chlorobenzene
BRL 8260B P6A020110.017 1/14/16 16:51 MWWmg/kg dry 0.00072Chloroethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00062Chloroform
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00058Chloromethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00037cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00029cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00036Dibromochloromethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00039Dichlorodifluoromethane
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00033Ethylbenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00035Isopropyl Ether
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00051Isopropylbenzene (Cumene)
BRL 8260B P6A020110.017 1/14/16 16:51 MWWmg/kg dry 0.00080m,p-Xylenes
BRL 8260B P6A020110.086 1/14/16 16:51 MWWmg/kg dry 0.00078Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 111 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-5
Prism Sample ID: 6010230-26
Prism Work Order: 6010230
Time Collected: 01/13/16 12:01
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.17 1/14/16 16:51 MWWmg/kg dry 0.00078Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.086 1/14/16 16:51 MWWmg/kg dry 0.00074Methyl Isobutyl Ketone
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00049Methylene Chloride
BRL 8260B P6A020110.017 1/14/16 16:51 MWWmg/kg dry 0.00028Methyl-tert-Butyl Ether
BRL 8260B P6A020110.017 1/14/16 16:51 MWWmg/kg dry 0.00027Naphthalene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00044n-Butylbenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00051n-Propylbenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00035o-Xylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00042sec-Butylbenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00052Styrene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00029tert-Butylbenzene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00041Tetrachloroethylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00050Toluene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00052trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00045trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00056Trichloroethylene
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00056Trichlorofluoromethane
BRL 8260B P6A020110.043 1/14/16 16:51 MWWmg/kg dry 0.0012Vinyl acetate
BRL 8260B P6A020110.0086 1/14/16 16:51 MWWmg/kg dry 0.00042Vinyl chloride
BRL 8260B P6A020110.026 1/14/16 16:51 MWWmg/kg dry 0.0016Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123107 %Dibromofluoromethane
76-12984 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 112 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-9
Prism Sample ID: 6010230-27
Prism Work Order: 6010230
Time Collected: 01/13/16 12:28
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
79.5 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0651,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0631,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0611,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0801-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0782,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0802,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0642,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0582,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0552,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0602-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0592-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0662-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0532-Methylphenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0762-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0823,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0513/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0714-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0584-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0504-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.0644-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.060Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.067Anthracene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.055Azobenzene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.045Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.055Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.072bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.059Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.071Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.062Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 113 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-9
Prism Sample ID: 6010230-27
Prism Work Order: 6010230
Time Collected: 01/13/16 12:28
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.059Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.052Chrysene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.063Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.057Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.055Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.059Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.051Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.053Fluoranthene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.060Fluorene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.066Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.075Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.074Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.070Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.056Isophorone
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.067Naphthalene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.059Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.063N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.049Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.054Phenanthrene
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.061Phenol
BRL 8270D P6A021510.41 1/15/16 19:26 JMVmg/kg dry 0.055Pyrene
Surrogate Recovery Control Limits
39-13256 %2,4,6-Tribromophenol
44-11555 %2-Fluorobiphenyl
35-11553 %2-Fluorophenol
37-12256 %Nitrobenzene-d5
34-12152 %Phenol-d5
54-12761 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.027 1/18/16 11:40 JABmg/kg dry 0.0018Mercury
3.0 *6010C P6A022910.32 1/18/16 21:23 bgmAmg/kg dry 0.071Arsenic
52 *6010C P6A022910.64 1/18/16 21:23 bgmAmg/kg dry 0.34Barium
BRL *6010C P6A022910.32 1/18/16 21:23 bgmAmg/kg dry 0.0068Cadmium
4.3 *6010C P6A022910.32 1/18/16 21:23 bgmAmg/kg dry 0.043Chromium
3.4 *6010C P6A022910.32 1/18/16 21:23 bgmAmg/kg dry 0.034Lead
BRL *6010C P6A022910.64 1/18/16 21:23 bgmAmg/kg dry 0.046Selenium
0.66 *6010C P6A022910.32 1/18/16 21:23 bgmAmg/kg dry 0.0052Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000551,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 114 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-9
Prism Sample ID: 6010230-27
Prism Work Order: 6010230
Time Collected: 01/13/16 12:28
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000321,1,1-Trichloroethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000451,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000591,1,2-Trichloroethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000301,1-Dichloroethylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000371,1-Dichloropropylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000381,2,3-Trichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000861,2,3-Trichloropropane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000501,2,4-Trichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000511,2,4-Trimethylbenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000271,2-Dibromoethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000401,2-Dichloroethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000421,2-Dichloropropane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000511,3,5-Trimethylbenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000441,3-Dichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000341,3-Dichloropropane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000261,4-Dichlorobenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000322,2-Dichloropropane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000352-Chlorotoluene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000404-Chlorotoluene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.000324-Isopropyltoluene
0.0065 8260B P6A020110.067 1/14/16 17:22 MWWJmg/kg dry 0.0016Acetone
BRL 8260B P6A020110.0040 1/14/16 17:22 MWWmg/kg dry 0.00039Benzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00056Bromobenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00037Bromochloromethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00037Bromodichloromethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00076Bromoform
BRL 8260B P6A020110.013 1/14/16 17:22 MWWmg/kg dry 0.00083Bromomethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00033Carbon Tetrachloride
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00036Chlorobenzene
BRL 8260B P6A020110.013 1/14/16 17:22 MWWmg/kg dry 0.00056Chloroethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00048Chloroform
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00045Chloromethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00030Dichlorodifluoromethane
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00026Ethylbenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00027Isopropyl Ether
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00040Isopropylbenzene (Cumene)
BRL 8260B P6A020110.013 1/14/16 17:22 MWWmg/kg dry 0.00062m,p-Xylenes
BRL 8260B P6A020110.067 1/14/16 17:22 MWWmg/kg dry 0.00061Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 115 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-9-9
Prism Sample ID: 6010230-27
Prism Work Order: 6010230
Time Collected: 01/13/16 12:28
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.13 1/14/16 17:22 MWWmg/kg dry 0.00061Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.067 1/14/16 17:22 MWWmg/kg dry 0.00057Methyl Isobutyl Ketone
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00038Methylene Chloride
BRL 8260B P6A020110.013 1/14/16 17:22 MWWmg/kg dry 0.00021Methyl-tert-Butyl Ether
BRL 8260B P6A020110.013 1/14/16 17:22 MWWmg/kg dry 0.00021Naphthalene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00034n-Butylbenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00040n-Propylbenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00027o-Xylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00032sec-Butylbenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00040Styrene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00032Tetrachloroethylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00038Toluene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00040trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00035trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00043Trichloroethylene
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00043Trichlorofluoromethane
BRL 8260B P6A020110.034 1/14/16 17:22 MWWmg/kg dry 0.00092Vinyl acetate
BRL 8260B P6A020110.0067 1/14/16 17:22 MWWmg/kg dry 0.00032Vinyl chloride
BRL 8260B P6A020110.020 1/14/16 17:22 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12993 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 116 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-2
Prism Sample ID: 6010230-28
Prism Work Order: 6010230
Time Collected: 01/13/16 14:40
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
80.1 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0791-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0802,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0552,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0602-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0662-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0532-Methylphenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0752-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0813,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0513/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0714-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0584-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0504-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.060Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.066Anthracene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.045Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 117 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-2
Prism Sample ID: 6010230-28
Prism Work Order: 6010230
Time Collected: 01/13/16 14:40
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.059Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.052Chrysene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.063Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.057Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.051Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.053Fluoranthene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.059Fluorene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.074Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.056Isophorone
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.063N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.049Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.054Phenanthrene
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.061Phenol
BRL 8270D P6A021510.41 1/15/16 19:48 JMVmg/kg dry 0.055Pyrene
Surrogate Recovery Control Limits
39-13252 %2,4,6-Tribromophenol
44-11549 %2-Fluorobiphenyl
35-11547 %2-Fluorophenol
37-12250 %Nitrobenzene-d5
34-12146 %Phenol-d5
54-12751 %Terphenyl-d14 SR
Total Metals
BRL *7471B P6A023010.026 1/18/16 11:45 JABmg/kg dry 0.0017Mercury
2.2 *6010C P6A022910.32 1/19/16 17:23 bgmmg/kg dry 0.070Arsenic
42 *6010C P6A022910.63 1/19/16 17:23 bgmmg/kg dry 0.34Barium
BRL *6010C P6A022910.32 1/19/16 17:23 bgmmg/kg dry 0.0067Cadmium
7.4 *6010C P6A022910.32 1/19/16 17:23 bgmmg/kg dry 0.043Chromium
8.5 *6010C P6A022910.32 1/19/16 17:23 bgmmg/kg dry 0.033Lead
BRL *6010C P6A022910.63 1/19/16 17:23 bgmmg/kg dry 0.046Selenium
1.4 *6010C P6A022910.32 1/19/16 17:23 bgmmg/kg dry 0.0052Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000571,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 118 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-2
Prism Sample ID: 6010230-28
Prism Work Order: 6010230
Time Collected: 01/13/16 14:40
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000341,1,1-Trichloroethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000611,1,2-Trichloroethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000891,2,3-Trichloropropane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000521,2,4-Trichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000331,2-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P6A020110.069 1/14/16 17:53 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020110.0042 1/14/16 17:53 MWWmg/kg dry 0.00040Benzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00058Bromobenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00079Bromoform
BRL 8260B P6A020110.014 1/14/16 17:53 MWWmg/kg dry 0.00086Bromomethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00035Carbon Tetrachloride
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00037Chlorobenzene
BRL 8260B P6A020110.014 1/14/16 17:53 MWWmg/kg dry 0.00058Chloroethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00050Chloroform
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00047Chloromethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00030cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00032Dichlorodifluoromethane
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00027Ethylbenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6A020110.014 1/14/16 17:53 MWWmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P6A020110.069 1/14/16 17:53 MWWmg/kg dry 0.00063Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 119 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-2
Prism Sample ID: 6010230-28
Prism Work Order: 6010230
Time Collected: 01/13/16 14:40
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.14 1/14/16 17:53 MWWmg/kg dry 0.00063Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.069 1/14/16 17:53 MWWmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6A020110.014 1/14/16 17:53 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020110.014 1/14/16 17:53 MWWmg/kg dry 0.00022Naphthalene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00034sec-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00042Styrene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00040Toluene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00045Trichloroethylene
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P6A020110.035 1/14/16 17:53 MWWmg/kg dry 0.00095Vinyl acetate
BRL 8260B P6A020110.0069 1/14/16 17:53 MWWmg/kg dry 0.00034Vinyl chloride
BRL 8260B P6A020110.021 1/14/16 17:53 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-13095 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12989 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 120 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-5
Prism Sample ID: 6010230-29
Prism Work Order: 6010230
Time Collected: 01/13/16 14:57
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
78.9 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0651,2,4-Trichlorobenzene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0591,3-Dichlorobenzene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0611,4-Dichlorobenzene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0811-Methylnaphthalene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0782,4,6-Trichlorophenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0812,4-Dichlorophenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0642,4-Dimethylphenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0582,4-Dinitrophenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0592-Chlorophenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0672-Methylnaphthalene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0542-Methylphenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0762-Nitrophenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0833,3’-Dichlorobenzidine
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0634,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0724-Bromophenyl phenyl ether
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0504-Chloroaniline
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.0654-Nitrophenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.057Acenaphthene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.061Acenaphthylene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.067Anthracene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.055Azobenzene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.045Benzo(a)pyrene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.055Benzo(k)fluoranthene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.055Benzyl alcohol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.059Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.062Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 121 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-5
Prism Sample ID: 6010230-29
Prism Work Order: 6010230
Time Collected: 01/13/16 14:57
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.053Chrysene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.064Dibenzofuran
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.058Diethyl phthalate
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.055Dimethyl phthalate
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.059Di-n-butyl phthalate
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.051Di-n-octyl phthalate
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.053Fluoranthene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.060Fluorene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.066Hexachlorobenzene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.075Hexachlorobutadiene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.075Hexachlorocyclopentadiene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.070Hexachloroethane
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.057Isophorone
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.067Naphthalene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.059Nitrobenzene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.066N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.049Pentachlorophenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.054Phenanthrene
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.062Phenol
BRL 8270D P6A021510.42 1/15/16 20:10 JMVmg/kg dry 0.055Pyrene
Surrogate Recovery Control Limits
39-13261 %2,4,6-Tribromophenol
44-11555 %2-Fluorobiphenyl
35-11555 %2-Fluorophenol
37-12259 %Nitrobenzene-d5
34-12154 %Phenol-d5
54-12763 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.026 1/18/16 11:50 JABmg/kg dry 0.0017Mercury
2.6 *6010C P6A022910.31 1/19/16 17:31 bgmmg/kg dry 0.069Arsenic
87 *6010C P6A022910.62 1/19/16 17:31 bgmmg/kg dry 0.33Barium
BRL *6010C P6A022910.31 1/19/16 17:31 bgmmg/kg dry 0.0066Cadmium
4.6 *6010C P6A022910.31 1/19/16 17:31 bgmmg/kg dry 0.042Chromium
5.9 *6010C P6A022910.31 1/19/16 17:31 bgmmg/kg dry 0.033Lead
BRL *6010C P6A022910.62 1/19/16 17:31 bgmmg/kg dry 0.045Selenium
1.2 *6010C P6A022910.31 1/19/16 17:31 bgmmg/kg dry 0.0051Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000571,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 122 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-5
Prism Sample ID: 6010230-29
Prism Work Order: 6010230
Time Collected: 01/13/16 14:57
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000331,1,1-Trichloroethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000611,1,2-Trichloroethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000881,2,3-Trichloropropane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000331,2-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.000334-Isopropyltoluene
BRL 8260B P6A020110.069 1/14/16 18:24 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020110.0042 1/14/16 18:24 MWWmg/kg dry 0.00040Benzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00058Bromobenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00079Bromoform
BRL 8260B P6A020110.014 1/14/16 18:24 MWWmg/kg dry 0.00085Bromomethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00037Chlorobenzene
BRL 8260B P6A020110.014 1/14/16 18:24 MWWmg/kg dry 0.00058Chloroethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00050Chloroform
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00047Chloromethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00027Ethylbenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6A020110.014 1/14/16 18:24 MWWmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P6A020110.069 1/14/16 18:24 MWWmg/kg dry 0.00063Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 123 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-5
Prism Sample ID: 6010230-29
Prism Work Order: 6010230
Time Collected: 01/13/16 14:57
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.14 1/14/16 18:24 MWWmg/kg dry 0.00063Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.069 1/14/16 18:24 MWWmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6A020110.014 1/14/16 18:24 MWWmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6A020110.014 1/14/16 18:24 MWWmg/kg dry 0.00022Naphthalene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00028o-Xylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00042Styrene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00040Toluene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00045Trichloroethylene
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P6A020110.035 1/14/16 18:24 MWWmg/kg dry 0.00095Vinyl acetate
BRL 8260B P6A020110.0069 1/14/16 18:24 MWWmg/kg dry 0.00033Vinyl chloride
BRL 8260B P6A020110.021 1/14/16 18:24 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12990 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 124 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-9
Prism Sample ID: 6010230-30
Prism Work Order: 6010230
Time Collected: 01/13/16 15:12
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
80.5 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0791-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0792,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0552,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0662-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0532-Methylphenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0752-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0813,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0513/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.066Anthracene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 125 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-9
Prism Sample ID: 6010230-30
Prism Work Order: 6010230
Time Collected: 01/13/16 15:12
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.052Chrysene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.059Fluorene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.074Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.056Isophorone
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.060Phenol
BRL 8270D P6A021510.41 1/15/16 20:33 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13245 %2,4,6-Tribromophenol
44-11548 %2-Fluorobiphenyl
35-11546 %2-Fluorophenol
37-12249 %Nitrobenzene-d5
34-12144 %Phenol-d5
54-12752 %Terphenyl-d14 SR
Total Metals
BRL *7471B P6A023010.024 1/18/16 11:54 JABmg/kg dry 0.0016Mercury
2.6 *6010C P6A022910.30 1/19/16 17:39 bgmmg/kg dry 0.067Arsenic
140 *6010C P6A022910.61 1/19/16 17:39 bgmmg/kg dry 0.32Barium
BRL *6010C P6A022910.30 1/19/16 17:39 bgmmg/kg dry 0.0064Cadmium
3.2 *6010C P6A022910.30 1/19/16 17:39 bgmmg/kg dry 0.041Chromium
5.3 *6010C P6A022910.30 1/19/16 17:39 bgmmg/kg dry 0.032Lead
BRL *6010C P6A022910.61 1/19/16 17:39 bgmmg/kg dry 0.044Selenium
0.82 *6010C P6A022910.30 1/19/16 17:39 bgmmg/kg dry 0.0050Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000621,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 126 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-9
Prism Sample ID: 6010230-30
Prism Work Order: 6010230
Time Collected: 01/13/16 15:12
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000361,1,1-Trichloroethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000511,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000671,1,2-Trichloroethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000211,1-Dichloroethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000331,1-Dichloroethylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000411,1-Dichloropropylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000431,2,3-Trichlorobenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000961,2,3-Trichloropropane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000561,2,4-Trichlorobenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000571,2,4-Trimethylbenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000301,2-Dibromoethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000351,2-Dichlorobenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000451,2-Dichloroethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000471,2-Dichloropropane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000571,3,5-Trimethylbenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000501,3-Dichlorobenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000381,3-Dichloropropane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000301,4-Dichlorobenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000362,2-Dichloropropane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000392-Chlorotoluene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000454-Chlorotoluene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.000364-Isopropyltoluene
0.0058 8260B P6A020110.075 1/14/16 18:55 MWWJmg/kg dry 0.0018Acetone
BRL 8260B P6A020110.0045 1/14/16 18:55 MWWmg/kg dry 0.00044Benzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00063Bromobenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00041Bromochloromethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00042Bromodichloromethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00085Bromoform
BRL 8260B P6A020110.015 1/14/16 18:55 MWWmg/kg dry 0.00093Bromomethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00037Carbon Tetrachloride
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00040Chlorobenzene
BRL 8260B P6A020110.015 1/14/16 18:55 MWWmg/kg dry 0.00063Chloroethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00054Chloroform
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00051Chloromethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00032cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00025cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00031Dibromochloromethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00034Dichlorodifluoromethane
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00029Ethylbenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00031Isopropyl Ether
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00044Isopropylbenzene (Cumene)
BRL 8260B P6A020110.015 1/14/16 18:55 MWWmg/kg dry 0.00069m,p-Xylenes
BRL 8260B P6A020110.075 1/14/16 18:55 MWWmg/kg dry 0.00068Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 127 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-10-9
Prism Sample ID: 6010230-30
Prism Work Order: 6010230
Time Collected: 01/13/16 15:12
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.15 1/14/16 18:55 MWWmg/kg dry 0.00068Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.075 1/14/16 18:55 MWWmg/kg dry 0.00064Methyl Isobutyl Ketone
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00042Methylene Chloride
BRL 8260B P6A020110.015 1/14/16 18:55 MWWmg/kg dry 0.00024Methyl-tert-Butyl Ether
BRL 8260B P6A020110.015 1/14/16 18:55 MWWmg/kg dry 0.00024Naphthalene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00038n-Butylbenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00045n-Propylbenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00031o-Xylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00036sec-Butylbenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00045Styrene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00025tert-Butylbenzene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00036Tetrachloroethylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00043Toluene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00045trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00040trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00049Trichloroethylene
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00049Trichlorofluoromethane
BRL 8260B P6A020110.038 1/14/16 18:55 MWWmg/kg dry 0.0010Vinyl acetate
BRL 8260B P6A020110.0075 1/14/16 18:55 MWWmg/kg dry 0.00036Vinyl chloride
BRL 8260B P6A020110.023 1/14/16 18:55 MWWmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123103 %Dibromofluoromethane
76-12989 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 128 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-2
Prism Sample ID: 6010230-31
Prism Work Order: 6010230
Time Collected: 01/13/16 15:32
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
80.0 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0631,2-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0791-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0802,4-Dichlorophenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0582,4-Dinitrophenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0552,6-Dinitrotoluene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0602-Chloronaphthalene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0662-Methylnaphthalene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0532-Methylphenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0752-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0813,3’-Dichlorobenzidine
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0513/4-Methylphenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0714-Bromophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0584-Chloro-3-methylphenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0504-Chloroaniline
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.0644-Nitrophenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.060Acenaphthylene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.066Anthracene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.045Benzo(a)pyrene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.072bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 129 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-2
Prism Sample ID: 6010230-31
Prism Work Order: 6010230
Time Collected: 01/13/16 15:32
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.059Butyl benzyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.052Chrysene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.063Dibenzofuran
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.057Diethyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.059Di-n-butyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.051Di-n-octyl phthalate
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.053Fluoranthene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.059Fluorene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.074Hexachlorobutadiene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.074Hexachlorocyclopentadiene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.056Isophorone
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.059Nitrobenzene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.063N-Nitrosodiphenylamine
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.049Pentachlorophenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.054Phenanthrene
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.061Phenol
BRL 8270D P6A021510.41 1/15/16 20:55 JMVmg/kg dry 0.055Pyrene
Surrogate Recovery Control Limits
39-13249 %2,4,6-Tribromophenol
44-11559 %2-Fluorobiphenyl
35-11552 %2-Fluorophenol
37-12262 %Nitrobenzene-d5
34-12154 %Phenol-d5
54-12767 %Terphenyl-d14
Total Metals
0.026 *7471B P6A023010.025 1/18/16 12:08 JABmg/kg dry 0.0016Mercury
3.9 *6010C P6A022910.32 1/19/16 17:48 bgmmg/kg dry 0.070Arsenic
26 *6010C P6A022910.63 1/19/16 17:48 bgmmg/kg dry 0.34Barium
BRL *6010C P6A022910.32 1/19/16 17:48 bgmmg/kg dry 0.0067Cadmium
23 *6010C P6A022910.32 1/19/16 17:48 bgmmg/kg dry 0.043Chromium
7.0 *6010C P6A022910.32 1/19/16 17:48 bgmmg/kg dry 0.033Lead
BRL *6010C P6A022910.63 1/19/16 17:48 bgmmg/kg dry 0.046Selenium
1.3 *6010C P6A022910.32 1/19/16 17:48 bgmmg/kg dry 0.0052Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000481,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 130 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-2
Prism Sample ID: 6010230-31
Prism Work Order: 6010230
Time Collected: 01/13/16 15:32
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000291,1,1-Trichloroethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000401,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000521,1,2-Trichloroethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000261,1-Dichloroethylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000321,1-Dichloropropylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000331,2,3-Trichlorobenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000751,2,3-Trichloropropane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000441,2,4-Trichlorobenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000451,2,4-Trimethylbenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000241,2-Dibromoethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000281,2-Dichlorobenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000351,2-Dichloroethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000371,2-Dichloropropane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000451,3,5-Trimethylbenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000391,3-Dichlorobenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000301,3-Dichloropropane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000231,4-Dichlorobenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000282,2-Dichloropropane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000302-Chlorotoluene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000354-Chlorotoluene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.000284-Isopropyltoluene
BRL 8260B P6A020110.059 1/14/16 19:27 MWWmg/kg dry 0.0014Acetone
BRL 8260B P6A020110.0035 1/14/16 19:27 MWWmg/kg dry 0.00034Benzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00049Bromobenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00032Bromochloromethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00033Bromodichloromethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00067Bromoform
BRL 8260B P6A020110.012 1/14/16 19:27 MWWmg/kg dry 0.00073Bromomethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00029Carbon Tetrachloride
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00031Chlorobenzene
BRL 8260B P6A020110.012 1/14/16 19:27 MWWmg/kg dry 0.00049Chloroethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00043Chloroform
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00040Chloromethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00025cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00020cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00024Dibromochloromethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00027Dichlorodifluoromethane
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00023Ethylbenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00024Isopropyl Ether
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00035Isopropylbenzene (Cumene)
BRL 8260B P6A020110.012 1/14/16 19:27 MWWmg/kg dry 0.00054m,p-Xylenes
BRL 8260B P6A020110.059 1/14/16 19:27 MWWmg/kg dry 0.00053Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 131 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-2
Prism Sample ID: 6010230-31
Prism Work Order: 6010230
Time Collected: 01/13/16 15:32
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.12 1/14/16 19:27 MWWmg/kg dry 0.00053Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.059 1/14/16 19:27 MWWmg/kg dry 0.00050Methyl Isobutyl Ketone
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00033Methylene Chloride
BRL 8260B P6A020110.012 1/14/16 19:27 MWWmg/kg dry 0.00019Methyl-tert-Butyl Ether
BRL 8260B P6A020110.012 1/14/16 19:27 MWWmg/kg dry 0.00019Naphthalene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00030n-Butylbenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00035n-Propylbenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00024o-Xylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00029sec-Butylbenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00036Styrene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00020tert-Butylbenzene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00028Tetrachloroethylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00034Toluene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00035trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00031trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00038Trichloroethylene
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00038Trichlorofluoromethane
BRL 8260B P6A020110.029 1/14/16 19:27 MWWmg/kg dry 0.00081Vinyl acetate
BRL 8260B P6A020110.0059 1/14/16 19:27 MWWmg/kg dry 0.00029Vinyl chloride
BRL 8260B P6A020110.018 1/14/16 19:27 MWWmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12987 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 132 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-5
Prism Sample ID: 6010230-32
Prism Work Order: 6010230
Time Collected: 01/13/16 15:44
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
76.6 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0671,2,4-Trichlorobenzene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0651,2-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0611,3-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0631,4-Dichlorobenzene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0831-Methylnaphthalene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0812,4,6-Trichlorophenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0832,4-Dichlorophenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0662,4-Dimethylphenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0602,4-Dinitrophenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0522,4-Dinitrotoluene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0572,6-Dinitrotoluene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0622-Chloronaphthalene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0612-Chlorophenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0692-Methylnaphthalene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0552-Methylphenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0782-Nitrophenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0853,3’-Dichlorobenzidine
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0533/4-Methylphenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0654,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0744-Bromophenyl phenyl ether
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0604-Chloro-3-methylphenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0524-Chloroaniline
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0564-Chlorophenyl phenyl ether
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.0664-Nitrophenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.059Acenaphthene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.062Acenaphthylene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.069Anthracene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.057Azobenzene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.056Benzo(a)anthracene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.047Benzo(a)pyrene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.050Benzo(b)fluoranthene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.047Benzo(g,h,i)perylene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.057Benzo(k)fluoranthene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.057Benzyl alcohol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.075bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.061Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.074Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.064Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 133 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-5
Prism Sample ID: 6010230-32
Prism Work Order: 6010230
Time Collected: 01/13/16 15:44
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.061Butyl benzyl phthalate
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.054Chrysene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.066Dibenzofuran
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.059Diethyl phthalate
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.057Dimethyl phthalate
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.061Di-n-butyl phthalate
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.053Di-n-octyl phthalate
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.055Fluoranthene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.062Fluorene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.068Hexachlorobenzene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.077Hexachlorobutadiene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.077Hexachlorocyclopentadiene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.072Hexachloroethane
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.058Isophorone
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.069Naphthalene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.061Nitrobenzene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.068N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.066N-Nitrosodiphenylamine
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.051Pentachlorophenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.056Phenanthrene
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.064Phenol
BRL 8270D P6A021510.43 1/15/16 21:17 JMVmg/kg dry 0.057Pyrene
Surrogate Recovery Control Limits
39-13263 %2,4,6-Tribromophenol
44-11560 %2-Fluorobiphenyl
35-11560 %2-Fluorophenol
37-12262 %Nitrobenzene-d5
34-12159 %Phenol-d5
54-12764 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.026 1/18/16 12:13 JABmg/kg dry 0.0017Mercury
2.5 *6010C P6A022910.33 1/19/16 17:57 bgmmg/kg dry 0.074Arsenic
26 *6010C P6A022910.67 1/19/16 17:57 bgmmg/kg dry 0.36Barium
BRL *6010C P6A022910.33 1/19/16 17:57 bgmmg/kg dry 0.0071Cadmium
11 *6010C P6A022910.33 1/19/16 17:57 bgmmg/kg dry 0.045Chromium
4.1 *6010C P6A022910.33 1/19/16 17:57 bgmmg/kg dry 0.035Lead
BRL *6010C P6A022910.67 1/19/16 17:57 bgmmg/kg dry 0.048Selenium
1.4 *6010C P6A022910.33 1/19/16 17:57 bgmmg/kg dry 0.0055Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000591,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 134 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-5
Prism Sample ID: 6010230-32
Prism Work Order: 6010230
Time Collected: 01/13/16 15:44
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000351,1,1-Trichloroethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000481,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000631,1,2-Trichloroethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000201,1-Dichloroethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000321,1-Dichloroethylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000391,1-Dichloropropylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000411,2,3-Trichlorobenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000911,2,3-Trichloropropane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000531,2,4-Trichlorobenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000551,2,4-Trimethylbenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000291,2-Dibromoethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000341,2-Dichlorobenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000431,2-Dichloroethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000441,2-Dichloropropane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000541,3,5-Trimethylbenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000471,3-Dichlorobenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000361,3-Dichloropropane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000281,4-Dichlorobenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000342,2-Dichloropropane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000372-Chlorotoluene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000434-Chlorotoluene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.000344-Isopropyltoluene
BRL 8260B P6A020110.072 1/14/16 19:58 MWWmg/kg dry 0.0017Acetone
BRL 8260B P6A020110.0043 1/14/16 19:58 MWWmg/kg dry 0.00042Benzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00060Bromobenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00039Bromochloromethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00040Bromodichloromethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00081Bromoform
BRL 8260B P6A020110.014 1/14/16 19:58 MWWmg/kg dry 0.00088Bromomethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00036Carbon Tetrachloride
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00038Chlorobenzene
BRL 8260B P6A020110.014 1/14/16 19:58 MWWmg/kg dry 0.00060Chloroethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00052Chloroform
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00048Chloromethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00030cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00024cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00029Dibromochloromethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00032Dichlorodifluoromethane
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00027Ethylbenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00029Isopropyl Ether
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00042Isopropylbenzene (Cumene)
BRL 8260B P6A020110.014 1/14/16 19:58 MWWmg/kg dry 0.00066m,p-Xylenes
BRL 8260B P6A020110.072 1/14/16 19:58 MWWmg/kg dry 0.00065Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 135 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-5
Prism Sample ID: 6010230-32
Prism Work Order: 6010230
Time Collected: 01/13/16 15:44
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.14 1/14/16 19:58 MWWmg/kg dry 0.00065Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.072 1/14/16 19:58 MWWmg/kg dry 0.00061Methyl Isobutyl Ketone
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00040Methylene Chloride
BRL 8260B P6A020110.014 1/14/16 19:58 MWWmg/kg dry 0.00023Methyl-tert-Butyl Ether
BRL 8260B P6A020110.014 1/14/16 19:58 MWWmg/kg dry 0.00023Naphthalene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00036n-Butylbenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00043n-Propylbenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00029o-Xylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00035sec-Butylbenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00043Styrene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00024tert-Butylbenzene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00034Tetrachloroethylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00041Toluene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00043trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00038trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00046Trichloroethylene
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00046Trichlorofluoromethane
BRL 8260B P6A020110.036 1/14/16 19:58 MWWmg/kg dry 0.00098Vinyl acetate
BRL 8260B P6A020110.0072 1/14/16 19:58 MWWmg/kg dry 0.00035Vinyl chloride
BRL 8260B P6A020110.021 1/14/16 19:58 MWWmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123115 %Dibromofluoromethane
76-12984 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 136 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-9
Prism Sample ID: 6010230-33
Prism Work Order: 6010230
Time Collected: 01/13/16 16:03
Time Submitted: 01/14/16 08:20
General Chemistry Parameters
74.7 *SM2540 G P6A024810.100 1/18/16 16:40 EGC% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0691,2,4-Trichlorobenzene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0671,2-Dichlorobenzene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0621,3-Dichlorobenzene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0651,4-Dichlorobenzene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0851-Methylnaphthalene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0832,4,6-Trichlorophenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0852,4-Dichlorophenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0682,4-Dimethylphenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0622,4-Dinitrophenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0542,4-Dinitrotoluene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0592,6-Dinitrotoluene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0642-Chloronaphthalene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0632-Chlorophenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0712-Methylnaphthalene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0572-Methylphenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0802-Nitrophenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0873,3’-Dichlorobenzidine
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0543/4-Methylphenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0664,6-Dinitro-2-methylphenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0764-Bromophenyl phenyl ether
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0624-Chloro-3-methylphenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0534-Chloroaniline
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0574-Chlorophenyl phenyl ether
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.0684-Nitrophenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.060Acenaphthene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.064Acenaphthylene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.071Anthracene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.058Azobenzene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.058Benzo(a)anthracene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.048Benzo(a)pyrene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.051Benzo(b)fluoranthene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.048Benzo(g,h,i)perylene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.058Benzo(k)fluoranthene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.037Benzoic Acid
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.058Benzyl alcohol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.077bis(2-Chloroethoxy)methane
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.062Bis(2-Chloroethyl)ether
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.076Bis(2-chloroisopropyl)ether
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.066Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 137 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-9
Prism Sample ID: 6010230-33
Prism Work Order: 6010230
Time Collected: 01/13/16 16:03
Time Submitted: 01/14/16 08:20
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.063Butyl benzyl phthalate
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.056Chrysene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.054Dibenzo(a,h)anthracene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.067Dibenzofuran
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.061Diethyl phthalate
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.058Dimethyl phthalate
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.063Di-n-butyl phthalate
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.054Di-n-octyl phthalate
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.056Fluoranthene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.063Fluorene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.070Hexachlorobenzene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.079Hexachlorobutadiene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.079Hexachlorocyclopentadiene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.074Hexachloroethane
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.051Indeno(1,2,3-cd)pyrene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.060Isophorone
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.071Naphthalene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.063Nitrobenzene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.070N-Nitroso-di-n-propylamine
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.067N-Nitrosodiphenylamine
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.052Pentachlorophenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.057Phenanthrene
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.065Phenol
BRL 8270D P6A021510.44 1/15/16 21:40 JMVmg/kg dry 0.059Pyrene
Surrogate Recovery Control Limits
39-13264 %2,4,6-Tribromophenol
44-11561 %2-Fluorobiphenyl
35-11558 %2-Fluorophenol
37-12262 %Nitrobenzene-d5
34-12157 %Phenol-d5
54-12766 %Terphenyl-d14
Total Metals
BRL *7471B P6A023010.027 1/18/16 12:18 JABmg/kg dry 0.0017Mercury
2.2 *6010C P6A022910.33 1/19/16 18:05 bgmmg/kg dry 0.073Arsenic
32 *6010C P6A022910.66 1/19/16 18:05 bgmmg/kg dry 0.35Barium
BRL *6010C P6A022910.33 1/19/16 18:05 bgmmg/kg dry 0.0070Cadmium
13 *6010C P6A022910.33 1/19/16 18:05 bgmmg/kg dry 0.045Chromium
3.6 *6010C P6A022910.33 1/19/16 18:05 bgmmg/kg dry 0.035Lead
BRL *6010C P6A022910.66 1/19/16 18:05 bgmmg/kg dry 0.048Selenium
1.2 *6010C P6A022910.33 1/19/16 18:05 bgmmg/kg dry 0.0054Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000631,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 138 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-9
Prism Sample ID: 6010230-33
Prism Work Order: 6010230
Time Collected: 01/13/16 16:03
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000371,1,1-Trichloroethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000521,1,2,2-Tetrachloroethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000681,1,2-Trichloroethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000211,1-Dichloroethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000341,1-Dichloroethylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000421,1-Dichloropropylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000431,2,3-Trichlorobenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000981,2,3-Trichloropropane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000571,2,4-Trichlorobenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000591,2,4-Trimethylbenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000311,2-Dibromoethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000361,2-Dichlorobenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000461,2-Dichloroethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000471,2-Dichloropropane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000581,3,5-Trimethylbenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000511,3-Dichlorobenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000381,3-Dichloropropane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000301,4-Dichlorobenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000362,2-Dichloropropane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000402-Chlorotoluene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000464-Chlorotoluene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.000374-Isopropyltoluene
BRL 8260B P6A020110.077 1/14/16 20:29 MWWmg/kg dry 0.0019Acetone
BRL 8260B P6A020110.0046 1/14/16 20:29 MWWmg/kg dry 0.00045Benzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00064Bromobenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00042Bromochloromethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00043Bromodichloromethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00087Bromoform
BRL 8260B P6A020110.015 1/14/16 20:29 MWWmg/kg dry 0.00095Bromomethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00038Carbon Tetrachloride
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00041Chlorobenzene
BRL 8260B P6A020110.015 1/14/16 20:29 MWWmg/kg dry 0.00064Chloroethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00055Chloroform
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00051Chloromethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00033cis-1,2-Dichloroethylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00026cis-1,3-Dichloropropylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00032Dibromochloromethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00035Dichlorodifluoromethane
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00029Ethylbenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00031Isopropyl Ether
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00045Isopropylbenzene (Cumene)
BRL 8260B P6A020110.015 1/14/16 20:29 MWWmg/kg dry 0.00071m,p-Xylenes
BRL 8260B P6A020110.077 1/14/16 20:29 MWWmg/kg dry 0.00069Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 139 of 229
Laboratory Report
01/21/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Sample Matrix: Solid
Client Sample ID: HA-11-9
Prism Sample ID: 6010230-33
Prism Work Order: 6010230
Time Collected: 01/13/16 16:03
Time Submitted: 01/14/16 08:20
BRL 8260B P6A020110.15 1/14/16 20:29 MWWmg/kg dry 0.00069Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P6A020110.077 1/14/16 20:29 MWWmg/kg dry 0.00065Methyl Isobutyl Ketone
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00043Methylene Chloride
BRL 8260B P6A020110.015 1/14/16 20:29 MWWmg/kg dry 0.00025Methyl-tert-Butyl Ether
BRL 8260B P6A020110.015 1/14/16 20:29 MWWmg/kg dry 0.00024Naphthalene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00039n-Butylbenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00045n-Propylbenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00031o-Xylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00037sec-Butylbenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00046Styrene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00026tert-Butylbenzene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00036Tetrachloroethylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00044Toluene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00046trans-1,2-Dichloroethylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00040trans-1,3-Dichloropropylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00050Trichloroethylene
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00049Trichlorofluoromethane
BRL 8260B P6A020110.038 1/14/16 20:29 MWWmg/kg dry 0.0010Vinyl acetate
BRL 8260B P6A020110.0077 1/14/16 20:29 MWWmg/kg dry 0.00037Vinyl chloride
BRL 8260B P6A020110.023 1/14/16 20:29 MWWmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-13096 %4-Bromofluorobenzene
84-123102 %Dibromofluoromethane
76-12985 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 140 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
Blank (P6A0200-BLK1)Prepared & Analyzed: 01/14/16
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 141 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
Blank (P6A0200-BLK1)Prepared & Analyzed: 01/14/16
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10452.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9848.9
LCS (P6A0200-BS1)Prepared & Analyzed: 01/14/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0505 0.0050 0.05000 72-115101
1,1,1-Trichloroethane mg/kg wet0.0472 0.0050 0.05000 67-13194
1,1,2,2-Tetrachloroethane mg/kg wet0.0452 0.0050 0.05000 56-12690
1,1,2-Trichloroethane mg/kg wet0.0466 0.0050 0.05000 70-13393
1,1-Dichloroethane mg/kg wet0.0468 0.0050 0.05000 74-12794
1,1-Dichloroethylene mg/kg wet0.0486 0.0050 0.05000 67-14997
1,1-Dichloropropylene mg/kg wet0.0475 0.0050 0.05000 71-13095
1,2,3-Trichlorobenzene mg/kg wet0.0489 0.0050 0.05000 68-13098
1,2,3-Trichloropropane mg/kg wet0.0469 0.0050 0.05000 60-13794
1,2,4-Trichlorobenzene mg/kg wet0.0475 0.0050 0.05000 66-12595
1,2,4-Trimethylbenzene mg/kg wet0.0471 0.0050 0.05000 69-12994
1,2-Dibromoethane mg/kg wet0.0483 0.0050 0.05000 70-13297
1,2-Dichlorobenzene mg/kg wet0.0459 0.0050 0.05000 72-12392
1,2-Dichloroethane mg/kg wet0.0464 0.0050 0.05000 68-12893
1,2-Dichloropropane mg/kg wet0.0464 0.0050 0.05000 73-13093
1,3,5-Trimethylbenzene mg/kg wet0.0469 0.0050 0.05000 69-12894
1,3-Dichlorobenzene mg/kg wet0.0467 0.0050 0.05000 71-12093
1,3-Dichloropropane mg/kg wet0.0467 0.0050 0.05000 75-12493
1,4-Dichlorobenzene mg/kg wet0.0456 0.0050 0.05000 71-12391
2,2-Dichloropropane mg/kg wet0.0524 0.0050 0.05000 50-142105
2-Chlorotoluene mg/kg wet0.0449 0.0050 0.05000 67-12490
4-Chlorotoluene mg/kg wet0.0449 0.0050 0.05000 71-12690
4-Isopropyltoluene mg/kg wet0.0472 0.0050 0.05000 68-12994
Acetone mg/kg wet0.0965 0.050 0.1000 29-19897
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 142 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
LCS (P6A0200-BS1)Prepared & Analyzed: 01/14/16
Benzene mg/kg wet0.0470 0.0030 0.05000 74-12794
Bromobenzene mg/kg wet0.0443 0.0050 0.05000 73-12589
Bromochloromethane mg/kg wet0.0498 0.0050 0.05000 72-134100
Bromodichloromethane mg/kg wet0.0486 0.0050 0.05000 75-12297
Bromoform mg/kg wet0.0483 0.0050 0.05000 66-13597
Bromomethane mg/kg wet0.0463 0.010 0.05000 20-18093
Carbon Tetrachloride mg/kg wet0.0494 0.0050 0.05000 64-14399
Chlorobenzene mg/kg wet0.0449 0.0050 0.05000 74-11890
Chloroethane mg/kg wet0.0496 0.010 0.05000 33-14999
Chloroform mg/kg wet0.0454 0.0050 0.05000 73-12791
Chloromethane mg/kg wet0.0623 0.0050 0.05000 45-143125
cis-1,2-Dichloroethylene mg/kg wet0.0464 0.0050 0.05000 76-13493
cis-1,3-Dichloropropylene mg/kg wet0.0514 0.0050 0.05000 71-125103
Dibromochloromethane mg/kg wet0.0481 0.0050 0.05000 73-12296
Dichlorodifluoromethane mg/kg wet0.0707 0.0050 0.05000 26-146141
Ethylbenzene mg/kg wet0.0457 0.0050 0.05000 74-12891
Isopropyl Ether mg/kg wet0.0440 0.0050 0.05000 59-15988
Isopropylbenzene (Cumene)mg/kg wet0.0476 0.0050 0.05000 68-12695
m,p-Xylenes mg/kg wet0.0938 0.010 0.1000 75-12494
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0465 0.050 0.05000 J61-15793
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0442 0.10 0.05000 J63-14988
Methyl Isobutyl Ketone mg/kg wet0.0446 0.050 0.05000 J57-16289
Methylene Chloride mg/kg wet0.0485 0.0050 0.05000 74-12997
Methyl-tert-Butyl Ether mg/kg wet0.0487 0.010 0.05000 70-13097
Naphthalene mg/kg wet0.0499 0.010 0.05000 57-157100
n-Butylbenzene mg/kg wet0.0474 0.0050 0.05000 65-13595
n-Propylbenzene mg/kg wet0.0475 0.0050 0.05000 67-13095
o-Xylene mg/kg wet0.0476 0.0050 0.05000 74-12695
sec-Butylbenzene mg/kg wet0.0480 0.0050 0.05000 66-13196
Styrene mg/kg wet0.0481 0.0050 0.05000 77-12196
tert-Butylbenzene mg/kg wet0.0482 0.0050 0.05000 67-13296
Tetrachloroethylene mg/kg wet0.0451 0.0050 0.05000 68-13090
Toluene mg/kg wet0.0468 0.0050 0.05000 71-12994
trans-1,2-Dichloroethylene mg/kg wet0.0468 0.0050 0.05000 73-13294
trans-1,3-Dichloropropylene mg/kg wet0.0519 0.0050 0.05000 68-123104
Trichloroethylene mg/kg wet0.0486 0.0050 0.05000 75-13397
Trichlorofluoromethane mg/kg wet0.0516 0.0050 0.05000 44-146103
Vinyl acetate mg/kg wet0.0508 0.025 0.05000 85-161102
Vinyl chloride mg/kg wet0.0563 0.0050 0.05000 48-147113
Xylenes, total mg/kg wet0.141 0.015 0.1500 74-12694
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.3
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 143 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
LCS Dup (P6A0200-BSD1)Prepared & Analyzed: 01/14/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0492 0.0050 0.05000 2072-11598 2
1,1,1-Trichloroethane mg/kg wet0.0455 0.0050 0.05000 2067-13191 4
1,1,2,2-Tetrachloroethane mg/kg wet0.0451 0.0050 0.05000 2056-12690 0.2
1,1,2-Trichloroethane mg/kg wet0.0465 0.0050 0.05000 2070-13393 0.3
1,1-Dichloroethane mg/kg wet0.0443 0.0050 0.05000 2074-12789 5
1,1-Dichloroethylene mg/kg wet0.0464 0.0050 0.05000 2067-14993 5
1,1-Dichloropropylene mg/kg wet0.0449 0.0050 0.05000 2071-13090 5
1,2,3-Trichlorobenzene mg/kg wet0.0465 0.0050 0.05000 2068-13093 5
1,2,3-Trichloropropane mg/kg wet0.0465 0.0050 0.05000 2060-13793 0.8
1,2,4-Trichlorobenzene mg/kg wet0.0460 0.0050 0.05000 2066-12592 3
1,2,4-Trimethylbenzene mg/kg wet0.0454 0.0050 0.05000 2069-12991 4
1,2-Dibromoethane mg/kg wet0.0474 0.0050 0.05000 2070-13295 2
1,2-Dichlorobenzene mg/kg wet0.0451 0.0050 0.05000 2072-12390 2
1,2-Dichloroethane mg/kg wet0.0451 0.0050 0.05000 2068-12890 3
1,2-Dichloropropane mg/kg wet0.0455 0.0050 0.05000 2073-13091 2
1,3,5-Trimethylbenzene mg/kg wet0.0452 0.0050 0.05000 2069-12890 4
1,3-Dichlorobenzene mg/kg wet0.0452 0.0050 0.05000 2071-12090 3
1,3-Dichloropropane mg/kg wet0.0463 0.0050 0.05000 2075-12493 0.9
1,4-Dichlorobenzene mg/kg wet0.0446 0.0050 0.05000 2071-12389 2
2,2-Dichloropropane mg/kg wet0.0499 0.0050 0.05000 2050-142100 5
2-Chlorotoluene mg/kg wet0.0436 0.0050 0.05000 2067-12487 3
4-Chlorotoluene mg/kg wet0.0439 0.0050 0.05000 2071-12688 2
4-Isopropyltoluene mg/kg wet0.0452 0.0050 0.05000 2068-12990 4
Acetone mg/kg wet0.0836 0.050 0.1000 2029-19884 14
Benzene mg/kg wet0.0453 0.0030 0.05000 2074-12791 4
Bromobenzene mg/kg wet0.0430 0.0050 0.05000 2073-12586 3
Bromochloromethane mg/kg wet0.0482 0.0050 0.05000 2072-13496 3
Bromodichloromethane mg/kg wet0.0474 0.0050 0.05000 2075-12295 2
Bromoform mg/kg wet0.0483 0.0050 0.05000 2066-13597 0.02
Bromomethane mg/kg wet0.0400 0.010 0.05000 2020-18080 14
Carbon Tetrachloride mg/kg wet0.0474 0.0050 0.05000 2064-14395 4
Chlorobenzene mg/kg wet0.0440 0.0050 0.05000 2074-11888 2
Chloroethane mg/kg wet0.0464 0.010 0.05000 2033-14993 7
Chloroform mg/kg wet0.0440 0.0050 0.05000 2073-12788 3
Chloromethane mg/kg wet0.0522 0.0050 0.05000 2045-143104 18
cis-1,2-Dichloroethylene mg/kg wet0.0443 0.0050 0.05000 2076-13489 5
cis-1,3-Dichloropropylene mg/kg wet0.0501 0.0050 0.05000 2071-125100 3
Dibromochloromethane mg/kg wet0.0478 0.0050 0.05000 2073-12296 0.7
Dichlorodifluoromethane mg/kg wet0.0657 0.0050 0.05000 2026-146131 7
Ethylbenzene mg/kg wet0.0448 0.0050 0.05000 2074-12890 2
Isopropyl Ether mg/kg wet0.0433 0.0050 0.05000 2059-15987 2
Isopropylbenzene (Cumene)mg/kg wet0.0462 0.0050 0.05000 2068-12692 3
m,p-Xylenes mg/kg wet0.0916 0.010 0.1000 2075-12492 2
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0462 0.050 0.05000 20 J61-15792 0.6
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0399 0.10 0.05000 20 J63-14980 10
Methyl Isobutyl Ketone mg/kg wet0.0441 0.050 0.05000 20 J57-16288 1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 144 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
LCS Dup (P6A0200-BSD1)Prepared & Analyzed: 01/14/16
Methylene Chloride mg/kg wet0.0471 0.0050 0.05000 2074-12994 3
Methyl-tert-Butyl Ether mg/kg wet0.0470 0.010 0.05000 2070-13094 3
Naphthalene mg/kg wet0.0482 0.010 0.05000 2057-15796 4
n-Butylbenzene mg/kg wet0.0449 0.0050 0.05000 2065-13590 5
n-Propylbenzene mg/kg wet0.0458 0.0050 0.05000 2067-13092 4
o-Xylene mg/kg wet0.0468 0.0050 0.05000 2074-12694 2
sec-Butylbenzene mg/kg wet0.0462 0.0050 0.05000 2066-13192 4
Styrene mg/kg wet0.0478 0.0050 0.05000 2077-12196 0.7
tert-Butylbenzene mg/kg wet0.0463 0.0050 0.05000 2067-13293 4
Tetrachloroethylene mg/kg wet0.0437 0.0050 0.05000 2068-13087 3
Toluene mg/kg wet0.0452 0.0050 0.05000 2071-12990 3
trans-1,2-Dichloroethylene mg/kg wet0.0447 0.0050 0.05000 2073-13289 5
trans-1,3-Dichloropropylene mg/kg wet0.0510 0.0050 0.05000 2068-123102 2
Trichloroethylene mg/kg wet0.0466 0.0050 0.05000 2075-13393 4
Trichlorofluoromethane mg/kg wet0.0479 0.0050 0.05000 2044-14696 7
Vinyl acetate mg/kg wet0.0502 0.025 0.05000 2085-161100 1
Vinyl chloride mg/kg wet0.0528 0.0050 0.05000 2048-147106 6
Xylenes, total mg/kg wet0.138 0.015 0.1500 2074-12692 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.6
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.5
ug/L 50.00 76-129Surrogate: Toluene-d8 10049.8
Matrix Spike (P6A0200-MS1)Prepared & Analyzed: 01/14/16 Source: 6010230-13
1,1,1,2-Tetrachloroethane mg/kg dry0.0417 0.0063 0.06298 BRL 60-12066
1,1,1-Trichloroethane mg/kg dry0.0428 0.0063 0.06298 BRL 52-13968
1,1,2,2-Tetrachloroethane mg/kg dry0.0375 0.0063 0.06298 BRL 39-13560
1,1,2-Trichloroethane mg/kg dry0.0396 0.0063 0.06298 BRL 44-14063
1,1-Dichloroethane mg/kg dry0.0417 0.0063 0.06298 BRL 59-13766
1,1-Dichloroethylene mg/kg dry0.0440 0.0063 0.06298 BRL 54-16270
1,1-Dichloropropylene mg/kg dry0.0418 0.0063 0.06298 BRL 55-13766
1,2,3-Trichlorobenzene mg/kg dry0.0371 0.0063 0.06298 BRL 34-12059
1,2,3-Trichloropropane mg/kg dry0.0388 0.0063 0.06298 BRL 45-13962
1,2,4-Trichlorobenzene mg/kg dry0.0354 0.0063 0.06298 BRL 35-11656
1,2,4-Trimethylbenzene mg/kg dry0.0382 0.0063 0.06298 BRL 38-14261
1,2-Dibromoethane mg/kg dry0.0397 0.0063 0.06298 BRL 49-13263
1,2-Dichlorobenzene mg/kg dry0.0374 0.0063 0.06298 BRL 42-13059
1,2-Dichloroethane mg/kg dry0.0412 0.0063 0.06298 BRL 51-13165
1,2-Dichloropropane mg/kg dry0.0403 0.0063 0.06298 BRL 55-13864
1,3,5-Trimethylbenzene mg/kg dry0.0383 0.0063 0.06298 BRL 44-14061
1,3-Dichlorobenzene mg/kg dry0.0378 0.0063 0.06298 BRL 41-12960
1,3-Dichloropropane mg/kg dry0.0397 0.0063 0.06298 BRL 53-12963
1,4-Dichlorobenzene mg/kg dry0.0372 0.0063 0.06298 BRL 44-13459
2,2-Dichloropropane mg/kg dry0.0416 0.0063 0.06298 BRL 30-14766
2-Chlorotoluene mg/kg dry0.0372 0.0063 0.06298 BRL 46-13259
4-Chlorotoluene mg/kg dry0.0368 0.0063 0.06298 BRL 44-13558
4-Isopropyltoluene mg/kg dry0.0378 0.0063 0.06298 BRL 32-14460
Acetone mg/kg dry0.0775 0.063 0.1260 BRL 34-14362
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 145 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
Matrix Spike (P6A0200-MS1)Prepared & Analyzed: 01/14/16 Source: 6010230-13
Benzene mg/kg dry0.0421 0.0038 0.06298 BRL 60-13567
Bromobenzene mg/kg dry0.0366 0.0063 0.06298 BRL 45-13558
Bromochloromethane mg/kg dry0.0445 0.0063 0.06298 BRL 55-13671
Bromodichloromethane mg/kg dry0.0420 0.0063 0.06298 BRL 55-12767
Bromoform mg/kg dry0.0390 0.0063 0.06298 BRL 40-13662
Bromomethane mg/kg dry0.0420 0.013 0.06298 BRL 30-13767
Carbon Tetrachloride mg/kg dry0.0433 0.0063 0.06298 BRL 48-15369
Chlorobenzene mg/kg dry0.0392 0.0063 0.06298 BRL 57-12562
Chloroethane mg/kg dry0.0455 0.013 0.06298 BRL 16-17772
Chloroform mg/kg dry0.0405 0.0063 0.06298 BRL 56-13764
Chloromethane mg/kg dry0.0509 0.0063 0.06298 BRL 40-14581
cis-1,2-Dichloroethylene mg/kg dry0.0415 0.0063 0.06298 BRL 58-14066
cis-1,3-Dichloropropylene mg/kg dry0.0412 0.0063 0.06298 BRL 42-13565
Dibromochloromethane mg/kg dry0.0397 0.0063 0.06298 BRL 49-12763
Dichlorodifluoromethane mg/kg dry0.0532 0.0063 0.06298 BRL 25-15184
Ethylbenzene mg/kg dry0.0397 0.0063 0.06298 BRL 44-14463
Isopropyl Ether mg/kg dry0.0383 0.0063 0.06298 BRL 51-15561
Isopropylbenzene (Cumene)mg/kg dry0.0396 0.0063 0.06298 BRL 41-14063
m,p-Xylenes mg/kg dry0.0799 0.013 0.1260 BRL 36-14863
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0354 0.063 0.06298 BRL J30-14756
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0352 0.13 0.06298 BRL J24-16056
Methyl Isobutyl Ketone mg/kg dry0.0363 0.063 0.06298 BRL J25-16358
Methylene Chloride mg/kg dry0.0461 0.0063 0.06298 BRL 53-14473
Methyl-tert-Butyl Ether mg/kg dry0.0405 0.013 0.06298 BRL 49-13564
Naphthalene mg/kg dry0.0372 0.013 0.06298 BRL 32-12759
n-Butylbenzene mg/kg dry0.0372 0.0063 0.06298 BRL 23-14859
n-Propylbenzene mg/kg dry0.0397 0.0063 0.06298 BRL 35-14463
o-Xylene mg/kg dry0.0400 0.0063 0.06298 BRL 43-14363
sec-Butylbenzene mg/kg dry0.0395 0.0063 0.06298 BRL 34-14463
Styrene mg/kg dry0.0403 0.0063 0.06298 BRL 42-13264
tert-Butylbenzene mg/kg dry0.0397 0.0063 0.06298 BRL 36-15063
Tetrachloroethylene mg/kg dry0.0364 0.0063 0.06298 BRL 47-14258
Toluene mg/kg dry0.0412 0.0063 0.06298 BRL 57-13565
trans-1,2-Dichloroethylene mg/kg dry0.0420 0.0063 0.06298 BRL 58-14167
trans-1,3-Dichloropropylene mg/kg dry0.0420 0.0063 0.06298 BRL 41-12467
Trichloroethylene mg/kg dry0.0424 0.0063 0.06298 BRL 38-16467
Trichlorofluoromethane mg/kg dry0.0458 0.0063 0.06298 BRL 30-15773
Vinyl acetate mg/kg dry0.0168 0.031 0.06298 BRL M, J61-15427
Vinyl chloride mg/kg dry0.0421 0.0063 0.06298 BRL 40-15667
Xylenes, total mg/kg dry0.120 0.019 0.1889 BRL 36-14863
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9849.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10452.2
ug/L 50.00 76-129Surrogate: Toluene-d8 9748.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 146 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
Matrix Spike Dup (P6A0200-MSD1)Prepared: 01/14/16 Analyzed: 01/15/16 Source: 6010230-13
1,1,1,2-Tetrachloroethane mg/kg dry0.0431 0.0063 0.06261 BRL 1560-12069 3
1,1,1-Trichloroethane mg/kg dry0.0467 0.0063 0.06261 BRL 2152-13975 9
1,1,2,2-Tetrachloroethane mg/kg dry0.0365 0.0063 0.06261 BRL 2239-13558 3
1,1,2-Trichloroethane mg/kg dry0.0395 0.0063 0.06261 BRL 2144-14063 0.3
1,1-Dichloroethane mg/kg dry0.0451 0.0063 0.06261 BRL 2159-13772 8
1,1-Dichloroethylene mg/kg dry0.0486 0.0063 0.06261 BRL 2254-16278 10
1,1-Dichloropropylene mg/kg dry0.0459 0.0063 0.06261 BRL 1955-13773 9
1,2,3-Trichlorobenzene mg/kg dry0.0381 0.0063 0.06261 BRL 4134-12061 3
1,2,3-Trichloropropane mg/kg dry0.0376 0.0063 0.06261 BRL 2545-13960 3
1,2,4-Trichlorobenzene mg/kg dry0.0353 0.0063 0.06261 BRL 6235-11656 0.3
1,2,4-Trimethylbenzene mg/kg dry0.0388 0.0063 0.06261 BRL 2438-14262 2
1,2-Dibromoethane mg/kg dry0.0388 0.0063 0.06261 BRL 1549-13262 2
1,2-Dichlorobenzene mg/kg dry0.0376 0.0063 0.06261 BRL 2142-13060 0.5
1,2-Dichloroethane mg/kg dry0.0411 0.0063 0.06261 BRL 1351-13166 0.1
1,2-Dichloropropane mg/kg dry0.0413 0.0063 0.06261 BRL 1655-13866 3
1,3,5-Trimethylbenzene mg/kg dry0.0393 0.0063 0.06261 BRL 2944-14063 2
1,3-Dichlorobenzene mg/kg dry0.0379 0.0063 0.06261 BRL 2441-12960 0.1
1,3-Dichloropropane mg/kg dry0.0391 0.0063 0.06261 BRL 1553-12962 1
1,4-Dichlorobenzene mg/kg dry0.0373 0.0063 0.06261 BRL 2144-13460 0.2
2,2-Dichloropropane mg/kg dry0.0459 0.0063 0.06261 BRL 2030-14773 10
2-Chlorotoluene mg/kg dry0.0381 0.0063 0.06261 BRL 2946-13261 3
4-Chlorotoluene mg/kg dry0.0375 0.0063 0.06261 BRL 2344-13560 2
4-Isopropyltoluene mg/kg dry0.0393 0.0063 0.06261 BRL 2232-14463 4
Acetone mg/kg dry0.0741 0.063 0.1252 BRL 4934-14359 4
Benzene mg/kg dry0.0450 0.0038 0.06261 BRL 2060-13572 7
Bromobenzene mg/kg dry0.0370 0.0063 0.06261 BRL 2545-13559 1
Bromochloromethane mg/kg dry0.0421 0.0063 0.06261 BRL 1855-13667 6
Bromodichloromethane mg/kg dry0.0428 0.0063 0.06261 BRL 1755-12768 2
Bromoform mg/kg dry0.0391 0.0063 0.06261 BRL 3540-13662 0.3
Bromomethane mg/kg dry0.0466 0.013 0.06261 BRL 3030-13774 11
Carbon Tetrachloride mg/kg dry0.0469 0.0063 0.06261 BRL 2348-15375 8
Chlorobenzene mg/kg dry0.0408 0.0063 0.06261 BRL 1457-12565 4
Chloroethane mg/kg dry0.0550 0.013 0.06261 BRL 4716-17788 19
Chloroform mg/kg dry0.0429 0.0063 0.06261 BRL 1856-13768 6
Chloromethane mg/kg dry0.0599 0.0063 0.06261 BRL 2640-14596 16
cis-1,2-Dichloroethylene mg/kg dry0.0441 0.0063 0.06261 BRL 2858-14070 6
cis-1,3-Dichloropropylene mg/kg dry0.0418 0.0063 0.06261 BRL 3242-13567 1
Dibromochloromethane mg/kg dry0.0398 0.0063 0.06261 BRL 2449-12764 0.08
Dichlorodifluoromethane mg/kg dry0.0580 0.0063 0.06261 BRL 3725-15193 9
Ethylbenzene mg/kg dry0.0425 0.0063 0.06261 BRL 1944-14468 7
Isopropyl Ether mg/kg dry0.0401 0.0063 0.06261 BRL 1351-15564 5
Isopropylbenzene (Cumene)mg/kg dry0.0410 0.0063 0.06261 BRL 2741-14066 3
m,p-Xylenes mg/kg dry0.0858 0.013 0.1252 BRL 2036-14868 7
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0356 0.063 0.06261 BRL 42 J30-14757 0.5
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0330 0.13 0.06261 BRL 42 J24-16053 6
Methyl Isobutyl Ketone mg/kg dry0.0355 0.063 0.06261 BRL 44 J25-16357 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 147 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0200 - 5035
Matrix Spike Dup (P6A0200-MSD1)Prepared: 01/14/16 Analyzed: 01/15/16 Source: 6010230-13
Methylene Chloride mg/kg dry0.0477 0.0063 0.06261 BRL 1453-14476 3
Methyl-tert-Butyl Ether mg/kg dry0.0406 0.013 0.06261 BRL 2249-13565 0.3
Naphthalene mg/kg dry0.0381 0.013 0.06261 BRL 4432-12761 2
n-Butylbenzene mg/kg dry0.0382 0.0063 0.06261 BRL 3923-14861 2
n-Propylbenzene mg/kg dry0.0412 0.0063 0.06261 BRL 2735-14466 4
o-Xylene mg/kg dry0.0424 0.0063 0.06261 BRL 1743-14368 6
sec-Butylbenzene mg/kg dry0.0415 0.0063 0.06261 BRL 2834-14466 5
Styrene mg/kg dry0.0419 0.0063 0.06261 BRL 2842-13267 4
tert-Butylbenzene mg/kg dry0.0418 0.0063 0.06261 BRL 2936-15067 5
Tetrachloroethylene mg/kg dry0.0401 0.0063 0.06261 BRL 2647-14264 10
Toluene mg/kg dry0.0447 0.0063 0.06261 BRL 2257-13571 8
trans-1,2-Dichloroethylene mg/kg dry0.0468 0.0063 0.06261 BRL 1858-14175 11
trans-1,3-Dichloropropylene mg/kg dry0.0412 0.0063 0.06261 BRL 2041-12466 2
Trichloroethylene mg/kg dry0.0457 0.0063 0.06261 BRL 1838-16473 7
Trichlorofluoromethane mg/kg dry0.0508 0.0063 0.06261 BRL 2730-15781 10
Vinyl acetate mg/kg dry0.0182 0.031 0.06261 BRL 35 M, J61-15429 8
Vinyl chloride mg/kg dry0.0481 0.0063 0.06261 BRL 3540-15677 13
Xylenes, total mg/kg dry0.128 0.019 0.1878 BRL 2036-14868 7
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9648.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10251.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9748.7
Batch P6A0201 - 5035
Blank (P6A0201-BLK1)Prepared & Analyzed: 01/14/16
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 148 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0201 - 5035
Blank (P6A0201-BLK1)Prepared & Analyzed: 01/14/16
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9648.2
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9748.6
ug/L 50.00 76-129Surrogate: Toluene-d8 8843.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 149 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0201 - 5035
LCS (P6A0201-BS1)Prepared & Analyzed: 01/14/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0490 0.0050 0.05000 72-11598
1,1,1-Trichloroethane mg/kg wet0.0503 0.0050 0.05000 67-131101
1,1,2,2-Tetrachloroethane mg/kg wet0.0481 0.0050 0.05000 56-12696
1,1,2-Trichloroethane mg/kg wet0.0536 0.0050 0.05000 70-133107
1,1-Dichloroethane mg/kg wet0.0474 0.0050 0.05000 74-12795
1,1-Dichloroethylene mg/kg wet0.0522 0.0050 0.05000 67-149104
1,1-Dichloropropylene mg/kg wet0.0463 0.0050 0.05000 71-13093
1,2,3-Trichlorobenzene mg/kg wet0.0561 0.0050 0.05000 68-130112
1,2,3-Trichloropropane mg/kg wet0.0488 0.0050 0.05000 60-13798
1,2,4-Trichlorobenzene mg/kg wet0.0548 0.0050 0.05000 66-125110
1,2,4-Trimethylbenzene mg/kg wet0.0452 0.0050 0.05000 69-12990
1,2-Dibromoethane mg/kg wet0.0521 0.0050 0.05000 70-132104
1,2-Dichlorobenzene mg/kg wet0.0495 0.0050 0.05000 72-12399
1,2-Dichloroethane mg/kg wet0.0495 0.0050 0.05000 68-12899
1,2-Dichloropropane mg/kg wet0.0472 0.0050 0.05000 73-13094
1,3,5-Trimethylbenzene mg/kg wet0.0476 0.0050 0.05000 69-12895
1,3-Dichlorobenzene mg/kg wet0.0501 0.0050 0.05000 71-120100
1,3-Dichloropropane mg/kg wet0.0472 0.0050 0.05000 75-12494
1,4-Dichlorobenzene mg/kg wet0.0488 0.0050 0.05000 71-12398
2,2-Dichloropropane mg/kg wet0.0508 0.0050 0.05000 50-142102
2-Chlorotoluene mg/kg wet0.0531 0.0050 0.05000 67-124106
4-Chlorotoluene mg/kg wet0.0472 0.0050 0.05000 71-12694
4-Isopropyltoluene mg/kg wet0.0442 0.0050 0.05000 68-12988
Acetone mg/kg wet0.104 0.050 0.1000 29-198104
Benzene mg/kg wet0.0493 0.0030 0.05000 74-12799
Bromobenzene mg/kg wet0.0454 0.0050 0.05000 73-12591
Bromochloromethane mg/kg wet0.0495 0.0050 0.05000 72-13499
Bromodichloromethane mg/kg wet0.0513 0.0050 0.05000 75-122103
Bromoform mg/kg wet0.0502 0.0050 0.05000 66-135100
Bromomethane mg/kg wet0.0756 0.010 0.05000 20-180151
Carbon Tetrachloride mg/kg wet0.0489 0.0050 0.05000 64-14398
Chlorobenzene mg/kg wet0.0489 0.0050 0.05000 74-11898
Chloroethane mg/kg wet0.0554 0.010 0.05000 33-149111
Chloroform mg/kg wet0.0485 0.0050 0.05000 73-12797
Chloromethane mg/kg wet0.0563 0.0050 0.05000 45-143113
cis-1,2-Dichloroethylene mg/kg wet0.0484 0.0050 0.05000 76-13497
cis-1,3-Dichloropropylene mg/kg wet0.0515 0.0050 0.05000 71-125103
Dibromochloromethane mg/kg wet0.0537 0.0050 0.05000 73-122107
Dichlorodifluoromethane mg/kg wet0.0540 0.0050 0.05000 26-146108
Ethylbenzene mg/kg wet0.0486 0.0050 0.05000 74-12897
Isopropyl Ether mg/kg wet0.0473 0.0050 0.05000 59-15995
Isopropylbenzene (Cumene)mg/kg wet0.0439 0.0050 0.05000 68-12688
m,p-Xylenes mg/kg wet0.0989 0.010 0.1000 75-12499
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0499 0.050 0.05000 J61-157100
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0510 0.10 0.05000 J63-149102
Methyl Isobutyl Ketone mg/kg wet0.0518 0.050 0.05000 57-162104
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 150 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0201 - 5035
LCS (P6A0201-BS1)Prepared & Analyzed: 01/14/16
Methylene Chloride mg/kg wet0.0521 0.0050 0.05000 74-129104
Methyl-tert-Butyl Ether mg/kg wet0.0515 0.010 0.05000 70-130103
Naphthalene mg/kg wet0.0563 0.010 0.05000 57-157113
n-Butylbenzene mg/kg wet0.0475 0.0050 0.05000 65-13595
n-Propylbenzene mg/kg wet0.0478 0.0050 0.05000 67-13096
o-Xylene mg/kg wet0.0513 0.0050 0.05000 74-126103
sec-Butylbenzene mg/kg wet0.0468 0.0050 0.05000 66-13194
Styrene mg/kg wet0.0475 0.0050 0.05000 77-12195
tert-Butylbenzene mg/kg wet0.0478 0.0050 0.05000 67-13296
Tetrachloroethylene mg/kg wet0.0503 0.0050 0.05000 68-130101
Toluene mg/kg wet0.0496 0.0050 0.05000 71-12999
trans-1,2-Dichloroethylene mg/kg wet0.0506 0.0050 0.05000 73-132101
trans-1,3-Dichloropropylene mg/kg wet0.0539 0.0050 0.05000 68-123108
Trichloroethylene mg/kg wet0.0517 0.0050 0.05000 75-133103
Trichlorofluoromethane mg/kg wet0.0596 0.0050 0.05000 44-146119
Vinyl acetate mg/kg wet0.0505 0.025 0.05000 85-161101
Vinyl chloride mg/kg wet0.0551 0.0050 0.05000 48-147110
Xylenes, total mg/kg wet0.150 0.015 0.1500 74-126100
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9145.5
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9145.6
ug/L 50.00 76-129Surrogate: Toluene-d8 8944.4
LCS Dup (P6A0201-BSD1)Prepared & Analyzed: 01/14/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0507 0.0050 0.05000 2072-115101 3
1,1,1-Trichloroethane mg/kg wet0.0507 0.0050 0.05000 2067-131101 0.8
1,1,2,2-Tetrachloroethane mg/kg wet0.0451 0.0050 0.05000 2056-12690 6
1,1,2-Trichloroethane mg/kg wet0.0550 0.0050 0.05000 2070-133110 3
1,1-Dichloroethane mg/kg wet0.0459 0.0050 0.05000 2074-12792 3
1,1-Dichloroethylene mg/kg wet0.0534 0.0050 0.05000 2067-149107 2
1,1-Dichloropropylene mg/kg wet0.0498 0.0050 0.05000 2071-130100 7
1,2,3-Trichlorobenzene mg/kg wet0.0550 0.0050 0.05000 2068-130110 2
1,2,3-Trichloropropane mg/kg wet0.0476 0.0050 0.05000 2060-13795 2
1,2,4-Trichlorobenzene mg/kg wet0.0540 0.0050 0.05000 2066-125108 2
1,2,4-Trimethylbenzene mg/kg wet0.0428 0.0050 0.05000 2069-12986 5
1,2-Dibromoethane mg/kg wet0.0528 0.0050 0.05000 2070-132106 1
1,2-Dichlorobenzene mg/kg wet0.0473 0.0050 0.05000 2072-12395 5
1,2-Dichloroethane mg/kg wet0.0510 0.0050 0.05000 2068-128102 3
1,2-Dichloropropane mg/kg wet0.0474 0.0050 0.05000 2073-13095 0.2
1,3,5-Trimethylbenzene mg/kg wet0.0420 0.0050 0.05000 2069-12884 13
1,3-Dichlorobenzene mg/kg wet0.0475 0.0050 0.05000 2071-12095 5
1,3-Dichloropropane mg/kg wet0.0506 0.0050 0.05000 2075-124101 7
1,4-Dichlorobenzene mg/kg wet0.0475 0.0050 0.05000 2071-12395 3
2,2-Dichloropropane mg/kg wet0.0515 0.0050 0.05000 2050-142103 1
2-Chlorotoluene mg/kg wet0.0460 0.0050 0.05000 2067-12492 14
4-Chlorotoluene mg/kg wet0.0438 0.0050 0.05000 2071-12688 8
4-Isopropyltoluene mg/kg wet0.0462 0.0050 0.05000 2068-12992 4
Acetone mg/kg wet0.120 0.050 0.1000 2029-198120 15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 151 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0201 - 5035
LCS Dup (P6A0201-BSD1)Prepared & Analyzed: 01/14/16
Benzene mg/kg wet0.0485 0.0030 0.05000 2074-12797 2
Bromobenzene mg/kg wet0.0436 0.0050 0.05000 2073-12587 4
Bromochloromethane mg/kg wet0.0519 0.0050 0.05000 2072-134104 5
Bromodichloromethane mg/kg wet0.0526 0.0050 0.05000 2075-122105 3
Bromoform mg/kg wet0.0514 0.0050 0.05000 2066-135103 2
Bromomethane mg/kg wet0.0739 0.010 0.05000 2020-180148 2
Carbon Tetrachloride mg/kg wet0.0504 0.0050 0.05000 2064-143101 3
Chlorobenzene mg/kg wet0.0481 0.0050 0.05000 2074-11896 2
Chloroethane mg/kg wet0.0494 0.010 0.05000 2033-14999 11
Chloroform mg/kg wet0.0476 0.0050 0.05000 2073-12795 2
Chloromethane mg/kg wet0.0532 0.0050 0.05000 2045-143106 6
cis-1,2-Dichloroethylene mg/kg wet0.0489 0.0050 0.05000 2076-13498 1
cis-1,3-Dichloropropylene mg/kg wet0.0529 0.0050 0.05000 2071-125106 3
Dibromochloromethane mg/kg wet0.0501 0.0050 0.05000 2073-122100 7
Dichlorodifluoromethane mg/kg wet0.0531 0.0050 0.05000 2026-146106 2
Ethylbenzene mg/kg wet0.0493 0.0050 0.05000 2074-12899 1
Isopropyl Ether mg/kg wet0.0463 0.0050 0.05000 2059-15993 2
Isopropylbenzene (Cumene)mg/kg wet0.0414 0.0050 0.05000 2068-12683 6
m,p-Xylenes mg/kg wet0.102 0.010 0.1000 2075-124102 3
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0570 0.050 0.05000 2061-157114 13
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0588 0.10 0.05000 20 J63-149118 14
Methyl Isobutyl Ketone mg/kg wet0.0557 0.050 0.05000 2057-162111 7
Methylene Chloride mg/kg wet0.0534 0.0050 0.05000 2074-129107 2
Methyl-tert-Butyl Ether mg/kg wet0.0565 0.010 0.05000 2070-130113 9
Naphthalene mg/kg wet0.0549 0.010 0.05000 2057-157110 3
n-Butylbenzene mg/kg wet0.0449 0.0050 0.05000 2065-13590 6
n-Propylbenzene mg/kg wet0.0433 0.0050 0.05000 2067-13087 10
o-Xylene mg/kg wet0.0502 0.0050 0.05000 2074-126100 2
sec-Butylbenzene mg/kg wet0.0446 0.0050 0.05000 2066-13189 5
Styrene mg/kg wet0.0478 0.0050 0.05000 2077-12196 0.7
tert-Butylbenzene mg/kg wet0.0444 0.0050 0.05000 2067-13289 7
Tetrachloroethylene mg/kg wet0.0540 0.0050 0.05000 2068-130108 7
Toluene mg/kg wet0.0476 0.0050 0.05000 2071-12995 4
trans-1,2-Dichloroethylene mg/kg wet0.0507 0.0050 0.05000 2073-132101 0.08
trans-1,3-Dichloropropylene mg/kg wet0.0554 0.0050 0.05000 2068-123111 3
Trichloroethylene mg/kg wet0.0512 0.0050 0.05000 2075-133102 1
Trichlorofluoromethane mg/kg wet0.0623 0.0050 0.05000 2044-146125 4
Vinyl acetate mg/kg wet0.0518 0.025 0.05000 2085-161104 2
Vinyl chloride mg/kg wet0.0551 0.0050 0.05000 2048-147110 0.02
Xylenes, total mg/kg wet0.152 0.015 0.1500 2074-126101 1
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 8844.0
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9346.3
ug/L 50.00 76-129Surrogate: Toluene-d8 8743.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 152 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0201 - 5035
Matrix Spike (P6A0201-MS1)Prepared & Analyzed: 01/14/16 Source: 6010230-26
1,1,1,2-Tetrachloroethane mg/kg dry0.0450 0.0068 0.06779 BRL 60-12066
1,1,1-Trichloroethane mg/kg dry0.0336 0.0068 0.06779 BRL M52-13950
1,1,2,2-Tetrachloroethane mg/kg dry0.0523 0.0068 0.06779 BRL 39-13577
1,1,2-Trichloroethane mg/kg dry0.0513 0.0068 0.06779 BRL 44-14076
1,1-Dichloroethane mg/kg dry0.0378 0.0068 0.06779 BRL M59-13756
1,1-Dichloroethylene mg/kg dry0.0348 0.0068 0.06779 BRL M54-16251
1,1-Dichloropropylene mg/kg dry0.0361 0.0068 0.06779 BRL M55-13753
1,2,3-Trichlorobenzene mg/kg dry0.0480 0.0068 0.06779 BRL 34-12071
1,2,3-Trichloropropane mg/kg dry0.0490 0.0068 0.06779 BRL 45-13972
1,2,4-Trichlorobenzene mg/kg dry0.0435 0.0068 0.06779 BRL 35-11664
1,2,4-Trimethylbenzene mg/kg dry0.0371 0.0068 0.06779 BRL 38-14255
1,2-Dibromoethane mg/kg dry0.0541 0.0068 0.06779 BRL 49-13280
1,2-Dichlorobenzene mg/kg dry0.0452 0.0068 0.06779 BRL 42-13067
1,2-Dichloroethane mg/kg dry0.0400 0.0068 0.06779 BRL 51-13159
1,2-Dichloropropane mg/kg dry0.0431 0.0068 0.06779 BRL 55-13864
1,3,5-Trimethylbenzene mg/kg dry0.0382 0.0068 0.06779 BRL 44-14056
1,3-Dichlorobenzene mg/kg dry0.0422 0.0068 0.06779 BRL 41-12962
1,3-Dichloropropane mg/kg dry0.0486 0.0068 0.06779 BRL 53-12972
1,4-Dichlorobenzene mg/kg dry0.0422 0.0068 0.06779 BRL 44-13462
2,2-Dichloropropane mg/kg dry0.0345 0.0068 0.06779 BRL 30-14751
2-Chlorotoluene mg/kg dry0.0430 0.0068 0.06779 BRL 46-13263
4-Chlorotoluene mg/kg dry0.0418 0.0068 0.06779 BRL 44-13562
4-Isopropyltoluene mg/kg dry0.0362 0.0068 0.06779 BRL 32-14453
Acetone mg/kg dry0.105 0.068 0.1356 BRL 34-14377
Benzene mg/kg dry0.0418 0.0041 0.06779 BRL 60-13562
Bromobenzene mg/kg dry0.0418 0.0068 0.06779 BRL 45-13562
Bromochloromethane mg/kg dry0.0473 0.0068 0.06779 BRL 55-13670
Bromodichloromethane mg/kg dry0.0401 0.0068 0.06779 BRL 55-12759
Bromoform mg/kg dry0.0460 0.0068 0.06779 BRL 40-13668
Bromomethane mg/kg dry0.0460 0.014 0.06779 BRL 30-13768
Carbon Tetrachloride mg/kg dry0.0322 0.0068 0.06779 BRL M48-15348
Chlorobenzene mg/kg dry0.0420 0.0068 0.06779 BRL 57-12562
Chloroethane mg/kg dry0.0253 0.014 0.06779 BRL 16-17737
Chloroform mg/kg dry0.0384 0.0068 0.06779 BRL 56-13757
Chloromethane mg/kg dry0.0247 0.0068 0.06779 BRL M40-14536
cis-1,2-Dichloroethylene mg/kg dry0.0380 0.0068 0.06779 BRL M58-14056
cis-1,3-Dichloropropylene mg/kg dry0.0451 0.0068 0.06779 BRL 42-13567
Dibromochloromethane mg/kg dry0.0434 0.0068 0.06779 BRL 49-12764
Dichlorodifluoromethane mg/kg dry0.0249 0.0068 0.06779 BRL 25-15137
Ethylbenzene mg/kg dry0.0423 0.0068 0.06779 BRL 44-14462
Isopropyl Ether mg/kg dry0.0415 0.0068 0.06779 BRL 51-15561
Isopropylbenzene (Cumene)mg/kg dry0.0368 0.0068 0.06779 BRL 41-14054
m,p-Xylenes mg/kg dry0.0819 0.014 0.1356 BRL 36-14860
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0622 0.068 0.06779 BRL J30-14792
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0518 0.14 0.06779 BRL J24-16076
Methyl Isobutyl Ketone mg/kg dry0.0541 0.068 0.06779 BRL J25-16380
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 153 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0201 - 5035
Matrix Spike (P6A0201-MS1)Prepared & Analyzed: 01/14/16 Source: 6010230-26
Methylene Chloride mg/kg dry0.0430 0.0068 0.06779 BRL 53-14463
Methyl-tert-Butyl Ether mg/kg dry0.0491 0.014 0.06779 BRL 49-13572
Naphthalene mg/kg dry0.0564 0.014 0.06779 BRL 32-12783
n-Butylbenzene mg/kg dry0.0382 0.0068 0.06779 BRL 23-14856
n-Propylbenzene mg/kg dry0.0392 0.0068 0.06779 BRL 35-14458
o-Xylene mg/kg dry0.0442 0.0068 0.06779 BRL 43-14365
sec-Butylbenzene mg/kg dry0.0364 0.0068 0.06779 BRL 34-14454
Styrene mg/kg dry0.0464 0.0068 0.06779 BRL 42-13268
tert-Butylbenzene mg/kg dry0.0358 0.0068 0.06779 BRL 36-15053
Tetrachloroethylene mg/kg dry0.0378 0.0068 0.06779 BRL 47-14256
Toluene mg/kg dry0.0440 0.0068 0.06779 BRL 57-13565
trans-1,2-Dichloroethylene mg/kg dry0.0379 0.0068 0.06779 BRL M58-14156
trans-1,3-Dichloropropylene mg/kg dry0.0486 0.0068 0.06779 BRL 41-12472
Trichloroethylene mg/kg dry0.0417 0.0068 0.06779 BRL 38-16462
Trichlorofluoromethane mg/kg dry0.0281 0.0068 0.06779 BRL 30-15741
Vinyl acetate mg/kg dry0.0413 0.034 0.06779 BRL 61-15461
Vinyl chloride mg/kg dry0.0232 0.0068 0.06779 BRL M40-15634
Xylenes, total mg/kg dry0.126 0.020 0.2034 BRL 36-14862
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.3
ug/L 50.00 SR84-123Surrogate: Dibromofluoromethane 8341.4
ug/L 50.00 76-129Surrogate: Toluene-d8 9748.5
Matrix Spike Dup (P6A0201-MSD1)Prepared & Analyzed: 01/14/16 Source: 6010230-26
1,1,1,2-Tetrachloroethane mg/kg dry0.0405 0.0068 0.06752 BRL 1560-12060 11
1,1,1-Trichloroethane mg/kg dry0.0377 0.0068 0.06752 BRL 2152-13956 12
1,1,2,2-Tetrachloroethane mg/kg dry0.0478 0.0068 0.06752 BRL 2239-13571 9
1,1,2-Trichloroethane mg/kg dry0.0505 0.0068 0.06752 BRL 2144-14075 2
1,1-Dichloroethane mg/kg dry0.0417 0.0068 0.06752 BRL 2159-13762 10
1,1-Dichloroethylene mg/kg dry0.0406 0.0068 0.06752 BRL 2254-16260 15
1,1-Dichloropropylene mg/kg dry0.0411 0.0068 0.06752 BRL 1955-13761 13
1,2,3-Trichlorobenzene mg/kg dry0.0437 0.0068 0.06752 BRL 4134-12065 9
1,2,3-Trichloropropane mg/kg dry0.0457 0.0068 0.06752 BRL 2545-13968 7
1,2,4-Trichlorobenzene mg/kg dry0.0404 0.0068 0.06752 BRL 6235-11660 8
1,2,4-Trimethylbenzene mg/kg dry0.0396 0.0068 0.06752 BRL 2438-14259 7
1,2-Dibromoethane mg/kg dry0.0504 0.0068 0.06752 BRL 1549-13275 7
1,2-Dichlorobenzene mg/kg dry0.0421 0.0068 0.06752 BRL 2142-13062 7
1,2-Dichloroethane mg/kg dry0.0431 0.0068 0.06752 BRL 1351-13164 7
1,2-Dichloropropane mg/kg dry0.0458 0.0068 0.06752 BRL 1655-13868 6
1,3,5-Trimethylbenzene mg/kg dry0.0389 0.0068 0.06752 BRL 2944-14058 2
1,3-Dichlorobenzene mg/kg dry0.0422 0.0068 0.06752 BRL 2441-12962 0.02
1,3-Dichloropropane mg/kg dry0.0467 0.0068 0.06752 BRL 1553-12969 4
1,4-Dichlorobenzene mg/kg dry0.0404 0.0068 0.06752 BRL 2144-13460 4
2,2-Dichloropropane mg/kg dry0.0401 0.0068 0.06752 BRL 2030-14759 15
2-Chlorotoluene mg/kg dry0.0431 0.0068 0.06752 BRL 2946-13264 0.3
4-Chlorotoluene mg/kg dry0.0381 0.0068 0.06752 BRL 2344-13556 9
4-Isopropyltoluene mg/kg dry0.0388 0.0068 0.06752 BRL 2232-14458 7
Acetone mg/kg dry0.103 0.068 0.1350 BRL 4934-14376 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 154 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6A0201 - 5035
Matrix Spike Dup (P6A0201-MSD1)Prepared & Analyzed: 01/14/16 Source: 6010230-26
Benzene mg/kg dry0.0485 0.0041 0.06752 BRL 2060-13572 15
Bromobenzene mg/kg dry0.0395 0.0068 0.06752 BRL 2545-13559 6
Bromochloromethane mg/kg dry0.0470 0.0068 0.06752 BRL 1855-13670 0.6
Bromodichloromethane mg/kg dry0.0416 0.0068 0.06752 BRL 1755-12762 4
Bromoform mg/kg dry0.0451 0.0068 0.06752 BRL 3540-13667 2
Bromomethane mg/kg dry0.0600 0.014 0.06752 BRL 3030-13789 26
Carbon Tetrachloride mg/kg dry0.0371 0.0068 0.06752 BRL 2348-15355 14
Chlorobenzene mg/kg dry0.0423 0.0068 0.06752 BRL 1457-12563 0.9
Chloroethane mg/kg dry0.0343 0.014 0.06752 BRL 4716-17751 30
Chloroform mg/kg dry0.0412 0.0068 0.06752 BRL 1856-13761 7
Chloromethane mg/kg dry0.0336 0.0068 0.06752 BRL 26 D40-14550 31
cis-1,2-Dichloroethylene mg/kg dry0.0426 0.0068 0.06752 BRL 2858-14063 12
cis-1,3-Dichloropropylene mg/kg dry0.0493 0.0068 0.06752 BRL 3242-13573 9
Dibromochloromethane mg/kg dry0.0423 0.0068 0.06752 BRL 2449-12763 3
Dichlorodifluoromethane mg/kg dry0.0322 0.0068 0.06752 BRL 3725-15148 26
Ethylbenzene mg/kg dry0.0413 0.0068 0.06752 BRL 1944-14461 3
Isopropyl Ether mg/kg dry0.0439 0.0068 0.06752 BRL 1351-15565 5
Isopropylbenzene (Cumene)mg/kg dry0.0399 0.0068 0.06752 BRL 2741-14059 8
m,p-Xylenes mg/kg dry0.0805 0.014 0.1350 BRL 2036-14860 2
Methyl Butyl Ketone (2-Hexanone)mg/kg dry0.0558 0.068 0.06752 BRL 42 J30-14783 11
Methyl Ethyl Ketone (2-Butanone)mg/kg dry0.0600 0.14 0.06752 BRL 42 J24-16089 15
Methyl Isobutyl Ketone mg/kg dry0.0561 0.068 0.06752 BRL 44 J25-16383 4
Methylene Chloride mg/kg dry0.0465 0.0068 0.06752 BRL 1453-14469 8
Methyl-tert-Butyl Ether mg/kg dry0.0502 0.014 0.06752 BRL 2249-13574 2
Naphthalene mg/kg dry0.0522 0.014 0.06752 BRL 4432-12777 8
n-Butylbenzene mg/kg dry0.0390 0.0068 0.06752 BRL 3923-14858 2
n-Propylbenzene mg/kg dry0.0383 0.0068 0.06752 BRL 2735-14457 2
o-Xylene mg/kg dry0.0426 0.0068 0.06752 BRL 1743-14363 4
sec-Butylbenzene mg/kg dry0.0369 0.0068 0.06752 BRL 2834-14455 1
Styrene mg/kg dry0.0440 0.0068 0.06752 BRL 2842-13265 5
tert-Butylbenzene mg/kg dry0.0387 0.0068 0.06752 BRL 2936-15057 8
Tetrachloroethylene mg/kg dry0.0406 0.0068 0.06752 BRL 2647-14260 7
Toluene mg/kg dry0.0442 0.0068 0.06752 BRL 2257-13565 0.5
trans-1,2-Dichloroethylene mg/kg dry0.0440 0.0068 0.06752 BRL 1858-14165 15
trans-1,3-Dichloropropylene mg/kg dry0.0493 0.0068 0.06752 BRL 2041-12473 1
Trichloroethylene mg/kg dry0.0450 0.0068 0.06752 BRL 1838-16467 8
Trichlorofluoromethane mg/kg dry0.0358 0.0068 0.06752 BRL 2730-15753 24
Vinyl acetate mg/kg dry0.0475 0.034 0.06752 BRL 3561-15470 14
Vinyl chloride mg/kg dry0.0320 0.0068 0.06752 BRL 3540-15647 32
Xylenes, total mg/kg dry0.123 0.020 0.2026 BRL 2036-14861 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 8944.6
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 9045.2
ug/L 50.00 76-129Surrogate: Toluene-d8 9245.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 155 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
Blank (P6A0198-BLK1)Prepared & Analyzed: 01/14/16
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 156 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
Blank (P6A0198-BLK1)Prepared & Analyzed: 01/14/16
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 762.52
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 681.13
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 662.19
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 701.16
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 652.16
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 761.26
LCS (P6A0198-BS1)Prepared & Analyzed: 01/14/16
1,2,4-Trichlorobenzene mg/kg wet0.997 0.33 1.667 34-11860
1,2-Dichlorobenzene mg/kg wet0.882 0.33 1.667 33-11753
1,3-Dichlorobenzene mg/kg wet0.829 0.33 1.667 30-11550
1,4-Dichlorobenzene mg/kg wet0.867 0.33 1.667 31-11552
1-Methylnaphthalene mg/kg wet1.12 0.33 1.667 40-11967
2,4,6-Trichlorophenol mg/kg wet1.00 0.33 1.667 39-12660
2,4-Dichlorophenol mg/kg wet1.04 0.33 1.667 40-12262
2,4-Dimethylphenol mg/kg wet1.03 0.33 1.667 30-12762
2,4-Dinitrophenol mg/kg wet0.877 0.33 1.667 27-12953
2,4-Dinitrotoluene mg/kg wet1.09 0.33 1.667 48-12665
2,6-Dinitrotoluene mg/kg wet1.12 0.33 1.667 46-12467
2-Chloronaphthalene mg/kg wet1.15 0.33 1.667 41-11469
2-Chlorophenol mg/kg wet0.929 0.33 1.667 34-12156
2-Methylnaphthalene mg/kg wet1.07 0.33 1.667 38-12264
2-Methylphenol mg/kg wet0.971 0.33 1.667 32-12258
2-Nitrophenol mg/kg wet0.991 0.33 1.667 36-12359
3,3’-Dichlorobenzidine mg/kg wet0.899 0.33 1.667 22-12154
3/4-Methylphenol mg/kg wet0.974 0.33 1.667 34-11958
4,6-Dinitro-2-methylphenol mg/kg wet0.992 0.33 1.667 29-13260
4-Bromophenyl phenyl ether mg/kg wet1.09 0.33 1.667 46-12465
4-Chloro-3-methylphenol mg/kg wet1.10 0.33 1.667 45-12266
4-Chloroaniline mg/kg wet1.04 0.33 1.667 17-10662
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 157 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
LCS (P6A0198-BS1)Prepared & Analyzed: 01/14/16
4-Chlorophenyl phenyl ether mg/kg wet1.10 0.33 1.667 45-12166
4-Nitrophenol mg/kg wet1.06 0.33 1.667 30-13264
Acenaphthene mg/kg wet1.07 0.33 1.667 40-12364
Acenaphthylene mg/kg wet1.11 0.33 1.667 32-13266
Anthracene mg/kg wet1.20 0.33 1.667 47-12372
Azobenzene mg/kg wet1.07 0.33 1.667 39-12564
Benzo(a)anthracene mg/kg wet1.16 0.33 1.667 49-12670
Benzo(a)pyrene mg/kg wet1.19 0.33 1.667 45-12971
Benzo(b)fluoranthene mg/kg wet1.12 0.33 1.667 45-13267
Benzo(g,h,i)perylene mg/kg wet1.14 0.33 1.667 43-13468
Benzo(k)fluoranthene mg/kg wet1.21 0.33 1.667 47-13273
Benzoic Acid mg/kg wet0.586 0.33 1.667 10-8335
Benzyl alcohol mg/kg wet1.08 0.33 1.667 29-12265
bis(2-Chloroethoxy)methane mg/kg wet1.07 0.33 1.667 36-12164
Bis(2-Chloroethyl)ether mg/kg wet0.905 0.33 1.667 31-12054
Bis(2-chloroisopropyl)ether mg/kg wet0.913 0.33 1.667 33-13155
Bis(2-Ethylhexyl)phthalate mg/kg wet1.14 0.33 1.667 51-13368
Butyl benzyl phthalate mg/kg wet1.12 0.33 1.667 48-13267
Chrysene mg/kg wet1.18 0.33 1.667 50-12471
Dibenzo(a,h)anthracene mg/kg wet1.18 0.33 1.667 45-13471
Dibenzofuran mg/kg wet1.07 0.33 1.667 44-12064
Diethyl phthalate mg/kg wet1.16 0.33 1.667 50-12469
Dimethyl phthalate mg/kg wet1.14 0.33 1.667 48-12469
Di-n-butyl phthalate mg/kg wet1.20 0.33 1.667 51-12872
Di-n-octyl phthalate mg/kg wet1.15 0.33 1.667 45-14069
Fluoranthene mg/kg wet1.20 0.33 1.667 50-12772
Fluorene mg/kg wet1.12 0.33 1.667 43-12567
Hexachlorobenzene mg/kg wet1.04 0.33 1.667 45-12263
Hexachlorobutadiene mg/kg wet0.996 0.33 1.667 32-12360
Hexachlorocyclopentadiene mg/kg wet0.884 0.33 1.667 32-11753
Hexachloroethane mg/kg wet0.841 0.33 1.667 28-11750
Indeno(1,2,3-cd)pyrene mg/kg wet1.03 0.33 1.667 45-13362
Isophorone mg/kg wet1.12 0.33 1.667 30-12267
Naphthalene mg/kg wet1.09 0.33 1.667 35-12365
Nitrobenzene mg/kg wet1.07 0.33 1.667 34-12264
N-Nitroso-di-n-propylamine mg/kg wet0.917 0.33 1.667 36-12055
N-Nitrosodiphenylamine mg/kg wet1.07 0.33 1.667 38-12764
Pentachlorophenol mg/kg wet1.10 0.33 1.667 25-13366
Phenanthrene mg/kg wet1.12 0.33 1.667 50-12167
Phenol mg/kg wet0.927 0.33 1.667 34-12156
Pyrene mg/kg wet1.20 0.33 1.667 47-12772
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 772.55
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 671.11
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 642.15
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 701.16
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 642.13
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 158 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
LCS (P6A0198-BS1)Prepared & Analyzed: 01/14/16
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 711.18
LCS Dup (P6A0198-BSD1)Prepared & Analyzed: 01/14/16
1,2,4-Trichlorobenzene mg/kg wet0.920 0.33 1.667 2034-11855 8
1,2-Dichlorobenzene mg/kg wet0.787 0.33 1.667 2033-11747 11
1,3-Dichlorobenzene mg/kg wet0.770 0.33 1.667 2030-11546 7
1,4-Dichlorobenzene mg/kg wet0.795 0.33 1.667 2031-11548 9
1-Methylnaphthalene mg/kg wet1.04 0.33 1.667 2040-11962 8
2,4,6-Trichlorophenol mg/kg wet0.909 0.33 1.667 2039-12655 10
2,4-Dichlorophenol mg/kg wet0.954 0.33 1.667 2040-12257 9
2,4-Dimethylphenol mg/kg wet0.944 0.33 1.667 2030-12757 9
2,4-Dinitrophenol mg/kg wet0.635 0.33 1.667 20 D27-12938 32
2,4-Dinitrotoluene mg/kg wet1.02 0.33 1.667 2048-12661 6
2,6-Dinitrotoluene mg/kg wet1.02 0.33 1.667 2046-12461 9
2-Chloronaphthalene mg/kg wet1.06 0.33 1.667 2041-11463 9
2-Chlorophenol mg/kg wet0.825 0.33 1.667 2034-12149 12
2-Methylnaphthalene mg/kg wet0.988 0.33 1.667 2038-12259 8
2-Methylphenol mg/kg wet0.861 0.33 1.667 2032-12252 12
2-Nitrophenol mg/kg wet0.891 0.33 1.667 2036-12353 11
3,3’-Dichlorobenzidine mg/kg wet0.896 0.33 1.667 2022-12154 0.4
3/4-Methylphenol mg/kg wet0.892 0.33 1.667 2034-11954 9
4,6-Dinitro-2-methylphenol mg/kg wet0.775 0.33 1.667 20 D29-13247 25
4-Bromophenyl phenyl ether mg/kg wet1.00 0.33 1.667 2046-12460 8
4-Chloro-3-methylphenol mg/kg wet1.04 0.33 1.667 2045-12262 6
4-Chloroaniline mg/kg wet0.980 0.33 1.667 2017-10659 6
4-Chlorophenyl phenyl ether mg/kg wet0.993 0.33 1.667 2045-12160 10
4-Nitrophenol mg/kg wet0.943 0.33 1.667 2030-13257 12
Acenaphthene mg/kg wet0.971 0.33 1.667 2040-12358 10
Acenaphthylene mg/kg wet1.00 0.33 1.667 2032-13260 10
Anthracene mg/kg wet1.12 0.33 1.667 2047-12367 7
Azobenzene mg/kg wet0.985 0.33 1.667 2039-12559 8
Benzo(a)anthracene mg/kg wet1.09 0.33 1.667 2049-12666 6
Benzo(a)pyrene mg/kg wet1.11 0.33 1.667 2045-12967 7
Benzo(b)fluoranthene mg/kg wet1.06 0.33 1.667 2045-13264 6
Benzo(g,h,i)perylene mg/kg wet1.07 0.33 1.667 2043-13464 6
Benzo(k)fluoranthene mg/kg wet1.13 0.33 1.667 2047-13268 7
Benzoic Acid mg/kg wet0.411 0.33 1.667 20 D10-8325 35
Benzyl alcohol mg/kg wet0.981 0.33 1.667 2029-12259 10
bis(2-Chloroethoxy)methane mg/kg wet0.969 0.33 1.667 2036-12158 10
Bis(2-Chloroethyl)ether mg/kg wet0.968 0.33 1.667 2031-12058 7
Bis(2-chloroisopropyl)ether mg/kg wet0.838 0.33 1.667 2033-13150 9
Bis(2-Ethylhexyl)phthalate mg/kg wet1.08 0.33 1.667 2051-13365 6
Butyl benzyl phthalate mg/kg wet1.08 0.33 1.667 2048-13265 4
Chrysene mg/kg wet1.10 0.33 1.667 2050-12466 7
Dibenzo(a,h)anthracene mg/kg wet1.11 0.33 1.667 2045-13467 6
Dibenzofuran mg/kg wet0.990 0.33 1.667 2044-12059 8
Diethyl phthalate mg/kg wet1.06 0.33 1.667 2050-12464 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 159 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
LCS Dup (P6A0198-BSD1)Prepared & Analyzed: 01/14/16
Dimethyl phthalate mg/kg wet1.05 0.33 1.667 2048-12463 9
Di-n-butyl phthalate mg/kg wet1.12 0.33 1.667 2051-12867 7
Di-n-octyl phthalate mg/kg wet1.06 0.33 1.667 2045-14064 8
Fluoranthene mg/kg wet1.10 0.33 1.667 2050-12766 8
Fluorene mg/kg wet1.03 0.33 1.667 2043-12562 9
Hexachlorobenzene mg/kg wet0.992 0.33 1.667 2045-12259 5
Hexachlorobutadiene mg/kg wet0.917 0.33 1.667 2032-12355 8
Hexachlorocyclopentadiene mg/kg wet0.801 0.33 1.667 2032-11748 10
Hexachloroethane mg/kg wet0.784 0.33 1.667 2028-11747 7
Indeno(1,2,3-cd)pyrene mg/kg wet0.971 0.33 1.667 2045-13358 6
Isophorone mg/kg wet1.02 0.33 1.667 2030-12261 9
Naphthalene mg/kg wet1.01 0.33 1.667 2035-12361 7
Nitrobenzene mg/kg wet0.996 0.33 1.667 2034-12260 7
N-Nitroso-di-n-propylamine mg/kg wet0.854 0.33 1.667 2036-12051 7
N-Nitrosodiphenylamine mg/kg wet1.02 0.33 1.667 2038-12761 5
Pentachlorophenol mg/kg wet0.972 0.33 1.667 2025-13358 12
Phenanthrene mg/kg wet1.04 0.33 1.667 2050-12162 7
Phenol mg/kg wet0.849 0.33 1.667 2034-12151 9
Pyrene mg/kg wet1.13 0.33 1.667 2047-12768 6
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 662.20
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 580.973
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 561.86
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 580.959
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 561.87
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 641.07
Matrix Spike (P6A0198-MS1)Prepared & Analyzed: 01/14/16 Source: 6010230-11
1,2,4-Trichlorobenzene mg/kg dry0.913 0.35 1.771 BRL 34-11852
1,2-Dichlorobenzene mg/kg dry0.804 0.35 1.771 BRL 33-11745
1,3-Dichlorobenzene mg/kg dry0.774 0.35 1.771 BRL 30-11544
1,4-Dichlorobenzene mg/kg dry0.785 0.35 1.771 BRL 31-11544
1-Methylnaphthalene mg/kg dry1.03 0.35 1.771 BRL 40-11958
2,4,6-Trichlorophenol mg/kg dry0.930 0.35 1.771 BRL 39-12652
2,4-Dichlorophenol mg/kg dry0.952 0.35 1.771 BRL 40-12254
2,4-Dimethylphenol mg/kg dry0.924 0.35 1.771 BRL 30-12752
2,4-Dinitrophenol mg/kg dry0.898 0.35 1.771 BRL 27-12951
2,4-Dinitrotoluene mg/kg dry1.01 0.35 1.771 BRL 48-12657
2,6-Dinitrotoluene mg/kg dry1.09 0.35 1.771 BRL 46-12461
2-Chloronaphthalene mg/kg dry1.08 0.35 1.771 BRL 41-11461
2-Chlorophenol mg/kg dry0.841 0.35 1.771 BRL 34-12148
2-Methylnaphthalene mg/kg dry0.995 0.35 1.771 BRL 38-12256
2-Methylphenol mg/kg dry0.874 0.35 1.771 BRL 32-12249
2-Nitrophenol mg/kg dry0.888 0.35 1.771 BRL 36-12350
3,3’-Dichlorobenzidine mg/kg dry0.863 0.35 1.771 BRL 22-12149
3/4-Methylphenol mg/kg dry0.905 0.35 1.771 BRL 34-11951
4,6-Dinitro-2-methylphenol mg/kg dry0.889 0.35 1.771 BRL 29-13250
4-Bromophenyl phenyl ether mg/kg dry1.00 0.35 1.771 BRL 46-12456
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 160 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
Matrix Spike (P6A0198-MS1)Prepared & Analyzed: 01/14/16 Source: 6010230-11
4-Chloro-3-methylphenol mg/kg dry1.02 0.35 1.771 BRL 45-12258
4-Chloroaniline mg/kg dry0.985 0.35 1.771 BRL 17-10656
4-Chlorophenyl phenyl ether mg/kg dry1.02 0.35 1.771 BRL 45-12158
4-Nitrophenol mg/kg dry0.973 0.35 1.771 BRL 30-13255
Acenaphthene mg/kg dry1.01 0.35 1.771 BRL 40-12357
Acenaphthylene mg/kg dry1.04 0.35 1.771 BRL 32-13258
Anthracene mg/kg dry1.13 0.35 1.771 BRL 47-12364
Azobenzene mg/kg dry1.00 0.35 1.771 BRL 39-12557
Benzo(a)anthracene mg/kg dry1.09 0.35 1.771 BRL 49-12662
Benzo(a)pyrene mg/kg dry1.10 0.35 1.771 BRL 45-12962
Benzo(b)fluoranthene mg/kg dry1.05 0.35 1.771 BRL 45-13259
Benzo(g,h,i)perylene mg/kg dry1.06 0.35 1.771 BRL 43-13460
Benzo(k)fluoranthene mg/kg dry1.13 0.35 1.771 BRL 47-13264
Benzoic Acid mg/kg dry0.923 0.35 1.771 BRL 10-8352
Benzyl alcohol mg/kg dry0.977 0.35 1.771 BRL 29-12255
bis(2-Chloroethoxy)methane mg/kg dry0.970 0.35 1.771 BRL 36-12155
Bis(2-Chloroethyl)ether mg/kg dry0.975 0.35 1.771 BRL 31-12055
Bis(2-chloroisopropyl)ether mg/kg dry0.836 0.35 1.771 BRL 33-13147
Bis(2-Ethylhexyl)phthalate mg/kg dry1.07 0.35 1.771 BRL 51-13360
Butyl benzyl phthalate mg/kg dry1.07 0.35 1.771 BRL 48-13260
Chrysene mg/kg dry1.10 0.35 1.771 BRL 50-12462
Dibenzo(a,h)anthracene mg/kg dry1.08 0.35 1.771 BRL 45-13461
Dibenzofuran mg/kg dry1.01 0.35 1.771 BRL 44-12057
Diethyl phthalate mg/kg dry1.08 0.35 1.771 BRL 50-12461
Dimethyl phthalate mg/kg dry1.06 0.35 1.771 BRL 48-12460
Di-n-butyl phthalate mg/kg dry1.11 0.35 1.771 BRL 51-12863
Di-n-octyl phthalate mg/kg dry1.05 0.35 1.771 BRL 45-14059
Fluoranthene mg/kg dry1.11 0.35 1.771 BRL 50-12762
Fluorene mg/kg dry1.05 0.35 1.771 BRL 43-12559
Hexachlorobenzene mg/kg dry0.989 0.35 1.771 BRL 45-12256
Hexachlorobutadiene mg/kg dry0.890 0.35 1.771 BRL 32-12350
Hexachlorocyclopentadiene mg/kg dry0.813 0.35 1.771 BRL 32-11746
Hexachloroethane mg/kg dry0.773 0.35 1.771 BRL 28-11744
Indeno(1,2,3-cd)pyrene mg/kg dry0.941 0.35 1.771 BRL 45-13353
Isophorone mg/kg dry1.03 0.35 1.771 BRL 30-12258
Naphthalene mg/kg dry0.997 0.35 1.771 BRL 35-12356
Nitrobenzene mg/kg dry0.978 0.35 1.771 BRL 34-12255
N-Nitroso-di-n-propylamine mg/kg dry0.863 0.35 1.771 BRL 36-12049
N-Nitrosodiphenylamine mg/kg dry1.00 0.35 1.771 BRL 38-12756
Pentachlorophenol mg/kg dry1.01 0.35 1.771 BRL 25-13357
Phenanthrene mg/kg dry1.04 0.35 1.771 BRL 50-12159
Phenol mg/kg dry0.857 0.35 1.771 BRL 34-12148
Pyrene mg/kg dry1.11 0.35 1.771 BRL 47-12763
mg/kg dry 3.542 39-132Surrogate: 2,4,6-Tribromophenol 652.29
mg/kg dry 1.771 44-115Surrogate: 2-Fluorobiphenyl 560.992
mg/kg dry 3.542 35-115Surrogate: 2-Fluorophenol 531.88
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 161 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
Matrix Spike (P6A0198-MS1)Prepared & Analyzed: 01/14/16 Source: 6010230-11
mg/kg dry 1.771 37-122Surrogate: Nitrobenzene-d5 581.03
mg/kg dry 3.542 34-121Surrogate: Phenol-d5 531.88
mg/kg dry 1.771 54-127Surrogate: Terphenyl-d14 601.06
Matrix Spike Dup (P6A0198-MSD1)Prepared & Analyzed: 01/14/16 Source: 6010230-11
1,2,4-Trichlorobenzene mg/kg dry0.931 0.35 1.771 BRL 2034-11853 2
1,2-Dichlorobenzene mg/kg dry0.838 0.35 1.771 BRL 2033-11747 4
1,3-Dichlorobenzene mg/kg dry0.790 0.35 1.771 BRL 2030-11545 2
1,4-Dichlorobenzene mg/kg dry0.812 0.35 1.771 BRL 2031-11546 3
1-Methylnaphthalene mg/kg dry1.04 0.35 1.771 BRL 2040-11959 0.7
2,4,6-Trichlorophenol mg/kg dry0.934 0.35 1.771 BRL 2039-12653 0.5
2,4-Dichlorophenol mg/kg dry0.969 0.35 1.771 BRL 2040-12255 2
2,4-Dimethylphenol mg/kg dry0.937 0.35 1.771 BRL 2030-12753 1
2,4-Dinitrophenol mg/kg dry0.791 0.35 1.771 BRL 2027-12945 13
2,4-Dinitrotoluene mg/kg dry1.07 0.35 1.771 BRL 2048-12660 5
2,6-Dinitrotoluene mg/kg dry1.08 0.35 1.771 BRL 2046-12461 0.6
2-Chloronaphthalene mg/kg dry1.07 0.35 1.771 BRL 2041-11460 0.7
2-Chlorophenol mg/kg dry0.847 0.35 1.771 BRL 2034-12148 0.6
2-Methylnaphthalene mg/kg dry0.998 0.35 1.771 BRL 2038-12256 0.3
2-Methylphenol mg/kg dry0.897 0.35 1.771 BRL 2032-12251 3
2-Nitrophenol mg/kg dry0.917 0.35 1.771 BRL 2036-12352 3
3,3’-Dichlorobenzidine mg/kg dry0.915 0.35 1.771 BRL 2022-12152 6
3/4-Methylphenol mg/kg dry0.937 0.35 1.771 BRL 2034-11953 3
4,6-Dinitro-2-methylphenol mg/kg dry0.842 0.35 1.771 BRL 2029-13248 5
4-Bromophenyl phenyl ether mg/kg dry1.03 0.35 1.771 BRL 2046-12458 3
4-Chloro-3-methylphenol mg/kg dry1.05 0.35 1.771 BRL 2045-12259 2
4-Chloroaniline mg/kg dry1.01 0.35 1.771 BRL 2017-10657 3
4-Chlorophenyl phenyl ether mg/kg dry1.03 0.35 1.771 BRL 2045-12158 0.9
4-Nitrophenol mg/kg dry0.996 0.35 1.771 BRL 2030-13256 2
Acenaphthene mg/kg dry0.997 0.35 1.771 BRL 2040-12356 1
Acenaphthylene mg/kg dry1.03 0.35 1.771 BRL 2032-13258 0.3
Anthracene mg/kg dry1.14 0.35 1.771 BRL 2047-12364 0.6
Azobenzene mg/kg dry1.02 0.35 1.771 BRL 2039-12558 2
Benzo(a)anthracene mg/kg dry1.10 0.35 1.771 BRL 2049-12662 0.7
Benzo(a)pyrene mg/kg dry1.13 0.35 1.771 BRL 2045-12964 3
Benzo(b)fluoranthene mg/kg dry1.07 0.35 1.771 BRL 2045-13261 2
Benzo(g,h,i)perylene mg/kg dry1.08 0.35 1.771 BRL 2043-13461 2
Benzo(k)fluoranthene mg/kg dry1.13 0.35 1.771 BRL 2047-13264 0.3
Benzoic Acid mg/kg dry0.892 0.35 1.771 BRL 2010-8350 3
Benzyl alcohol mg/kg dry1.04 0.35 1.771 BRL 2029-12259 6
bis(2-Chloroethoxy)methane mg/kg dry0.995 0.35 1.771 BRL 2036-12156 3
Bis(2-Chloroethyl)ether mg/kg dry1.01 0.35 1.771 BRL 2031-12057 3
Bis(2-chloroisopropyl)ether mg/kg dry0.870 0.35 1.771 BRL 2033-13149 4
Bis(2-Ethylhexyl)phthalate mg/kg dry1.10 0.35 1.771 BRL 2051-13362 3
Butyl benzyl phthalate mg/kg dry1.06 0.35 1.771 BRL 2048-13260 0.2
Chrysene mg/kg dry1.11 0.35 1.771 BRL 2050-12462 0.6
Dibenzo(a,h)anthracene mg/kg dry1.05 0.35 1.771 BRL 2045-13459 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 162 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0198 - 3546
Matrix Spike Dup (P6A0198-MSD1)Prepared & Analyzed: 01/14/16 Source: 6010230-11
Dibenzofuran mg/kg dry1.01 0.35 1.771 BRL 2044-12057 0.3
Diethyl phthalate mg/kg dry1.08 0.35 1.771 BRL 2050-12461 0.8
Dimethyl phthalate mg/kg dry1.08 0.35 1.771 BRL 2048-12461 1
Di-n-butyl phthalate mg/kg dry1.16 0.35 1.771 BRL 2051-12865 4
Di-n-octyl phthalate mg/kg dry1.08 0.35 1.771 BRL 2045-14061 2
Fluoranthene mg/kg dry1.13 0.35 1.771 BRL 2050-12764 2
Fluorene mg/kg dry1.04 0.35 1.771 BRL 2043-12559 0.9
Hexachlorobenzene mg/kg dry0.975 0.35 1.771 BRL 2045-12255 1
Hexachlorobutadiene mg/kg dry0.897 0.35 1.771 BRL 2032-12351 0.8
Hexachlorocyclopentadiene mg/kg dry0.840 0.35 1.771 BRL 2032-11747 3
Hexachloroethane mg/kg dry0.808 0.35 1.771 BRL 2028-11746 4
Indeno(1,2,3-cd)pyrene mg/kg dry1.28 0.35 1.771 BRL 20 D45-13372 31
Isophorone mg/kg dry1.05 0.35 1.771 BRL 2030-12259 2
Naphthalene mg/kg dry1.01 0.35 1.771 BRL 2035-12357 2
Nitrobenzene mg/kg dry0.977 0.35 1.771 BRL 2034-12255 0.2
N-Nitroso-di-n-propylamine mg/kg dry0.878 0.35 1.771 BRL 2036-12050 2
N-Nitrosodiphenylamine mg/kg dry1.02 0.35 1.771 BRL 2038-12757 2
Pentachlorophenol mg/kg dry0.978 0.35 1.771 BRL 2025-13355 3
Phenanthrene mg/kg dry1.05 0.35 1.771 BRL 2050-12160 1
Phenol mg/kg dry0.886 0.35 1.771 BRL 2034-12150 3
Pyrene mg/kg dry1.11 0.35 1.771 BRL 2047-12763 0.2
mg/kg dry 3.542 39-132Surrogate: 2,4,6-Tribromophenol 682.40
mg/kg dry 1.771 44-115Surrogate: 2-Fluorobiphenyl 581.02
mg/kg dry 3.542 35-115Surrogate: 2-Fluorophenol 572.02
mg/kg dry 1.771 37-122Surrogate: Nitrobenzene-d5 571.01
mg/kg dry 3.542 34-121Surrogate: Phenol-d5 561.97
mg/kg dry 1.771 54-127Surrogate: Terphenyl-d14 631.11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 163 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
Blank (P6A0215-BLK1)Prepared & Analyzed: 01/15/16
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 164 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
Blank (P6A0215-BLK1)Prepared & Analyzed: 01/15/16
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.332 39-132Surrogate: 2,4,6-Tribromophenol 662.21
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 601.01
mg/kg wet 3.332 35-115Surrogate: 2-Fluorophenol 602.00
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 621.04
mg/kg wet 3.332 34-121Surrogate: Phenol-d5 602.01
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 661.10
LCS (P6A0215-BS1)Prepared & Analyzed: 01/15/16
1,2,4-Trichlorobenzene mg/kg wet1.01 0.33 1.666 34-11861
1,2-Dichlorobenzene mg/kg wet0.904 0.33 1.666 33-11754
1,3-Dichlorobenzene mg/kg wet0.867 0.33 1.666 30-11552
1,4-Dichlorobenzene mg/kg wet0.884 0.33 1.666 31-11553
1-Methylnaphthalene mg/kg wet1.15 0.33 1.666 40-11969
2,4,6-Trichlorophenol mg/kg wet0.988 0.33 1.666 39-12659
2,4-Dichlorophenol mg/kg wet1.07 0.33 1.666 40-12264
2,4-Dimethylphenol mg/kg wet1.03 0.33 1.666 30-12762
2,4-Dinitrophenol mg/kg wet0.772 0.33 1.666 27-12946
2,4-Dinitrotoluene mg/kg wet1.08 0.33 1.666 48-12665
2,6-Dinitrotoluene mg/kg wet1.11 0.33 1.666 46-12467
2-Chloronaphthalene mg/kg wet1.15 0.33 1.666 41-11469
2-Chlorophenol mg/kg wet0.954 0.33 1.666 34-12157
2-Methylnaphthalene mg/kg wet1.10 0.33 1.666 38-12266
2-Methylphenol mg/kg wet0.993 0.33 1.666 32-12260
2-Nitrophenol mg/kg wet1.02 0.33 1.666 36-12361
3,3’-Dichlorobenzidine mg/kg wet0.925 0.33 1.666 22-12156
3/4-Methylphenol mg/kg wet1.02 0.33 1.666 34-11961
4,6-Dinitro-2-methylphenol mg/kg wet0.858 0.33 1.666 29-13252
4-Bromophenyl phenyl ether mg/kg wet1.09 0.33 1.666 46-12465
4-Chloro-3-methylphenol mg/kg wet1.12 0.33 1.666 45-12267
4-Chloroaniline mg/kg wet1.09 0.33 1.666 17-10665
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 165 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
LCS (P6A0215-BS1)Prepared & Analyzed: 01/15/16
4-Chlorophenyl phenyl ether mg/kg wet1.08 0.33 1.666 45-12165
4-Nitrophenol mg/kg wet1.01 0.33 1.666 30-13261
Acenaphthene mg/kg wet1.08 0.33 1.666 40-12365
Acenaphthylene mg/kg wet1.10 0.33 1.666 32-13266
Anthracene mg/kg wet1.21 0.33 1.666 47-12373
Azobenzene mg/kg wet1.03 0.33 1.666 39-12562
Benzo(a)anthracene mg/kg wet1.17 0.33 1.666 49-12670
Benzo(a)pyrene mg/kg wet1.19 0.33 1.666 45-12971
Benzo(b)fluoranthene mg/kg wet1.11 0.33 1.666 45-13267
Benzo(g,h,i)perylene mg/kg wet1.04 0.33 1.666 43-13462
Benzo(k)fluoranthene mg/kg wet1.22 0.33 1.666 47-13273
Benzoic Acid mg/kg wet0.532 0.33 1.666 10-8332
Benzyl alcohol mg/kg wet1.13 0.33 1.666 29-12268
bis(2-Chloroethoxy)methane mg/kg wet1.09 0.33 1.666 36-12166
Bis(2-Chloroethyl)ether mg/kg wet0.955 0.33 1.666 31-12057
Bis(2-chloroisopropyl)ether mg/kg wet0.896 0.33 1.666 33-13154
Bis(2-Ethylhexyl)phthalate mg/kg wet1.03 0.33 1.666 51-13362
Butyl benzyl phthalate mg/kg wet1.08 0.33 1.666 48-13265
Chrysene mg/kg wet1.17 0.33 1.666 50-12470
Dibenzo(a,h)anthracene mg/kg wet1.19 0.33 1.666 45-13472
Dibenzofuran mg/kg wet1.08 0.33 1.666 44-12065
Diethyl phthalate mg/kg wet1.12 0.33 1.666 50-12467
Dimethyl phthalate mg/kg wet1.13 0.33 1.666 48-12468
Di-n-butyl phthalate mg/kg wet1.16 0.33 1.666 51-12869
Di-n-octyl phthalate mg/kg wet1.08 0.33 1.666 45-14065
Fluoranthene mg/kg wet1.18 0.33 1.666 50-12771
Fluorene mg/kg wet1.11 0.33 1.666 43-12566
Hexachlorobenzene mg/kg wet1.07 0.33 1.666 45-12264
Hexachlorobutadiene mg/kg wet0.993 0.33 1.666 32-12360
Hexachlorocyclopentadiene mg/kg wet0.786 0.33 1.666 32-11747
Hexachloroethane mg/kg wet0.847 0.33 1.666 28-11751
Indeno(1,2,3-cd)pyrene mg/kg wet0.978 0.33 1.666 45-13359
Isophorone mg/kg wet1.09 0.33 1.666 30-12265
Naphthalene mg/kg wet1.11 0.33 1.666 35-12367
Nitrobenzene mg/kg wet1.06 0.33 1.666 34-12264
N-Nitroso-di-n-propylamine mg/kg wet0.931 0.33 1.666 36-12056
N-Nitrosodiphenylamine mg/kg wet1.09 0.33 1.666 38-12765
Pentachlorophenol mg/kg wet1.04 0.33 1.666 25-13362
Phenanthrene mg/kg wet1.11 0.33 1.666 50-12166
Phenol mg/kg wet0.961 0.33 1.666 34-12158
Pyrene mg/kg wet1.23 0.33 1.666 47-12774
mg/kg wet 3.331 39-132Surrogate: 2,4,6-Tribromophenol 742.47
mg/kg wet 1.666 44-115Surrogate: 2-Fluorobiphenyl 641.06
mg/kg wet 3.331 35-115Surrogate: 2-Fluorophenol 642.12
mg/kg wet 1.666 37-122Surrogate: Nitrobenzene-d5 661.11
mg/kg wet 3.331 34-121Surrogate: Phenol-d5 632.11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 166 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
LCS (P6A0215-BS1)Prepared & Analyzed: 01/15/16
mg/kg wet 1.666 54-127Surrogate: Terphenyl-d14 711.18
LCS Dup (P6A0215-BSD1)Prepared & Analyzed: 01/15/16
1,2,4-Trichlorobenzene mg/kg wet1.02 0.33 1.667 2034-11861 0.9
1,2-Dichlorobenzene mg/kg wet0.892 0.33 1.667 2033-11754 1
1,3-Dichlorobenzene mg/kg wet0.886 0.33 1.667 2030-11553 2
1,4-Dichlorobenzene mg/kg wet0.892 0.33 1.667 2031-11554 0.9
1-Methylnaphthalene mg/kg wet1.14 0.33 1.667 2040-11968 1
2,4,6-Trichlorophenol mg/kg wet1.03 0.33 1.667 2039-12662 4
2,4-Dichlorophenol mg/kg wet1.04 0.33 1.667 2040-12262 3
2,4-Dimethylphenol mg/kg wet1.02 0.33 1.667 2030-12761 0.9
2,4-Dinitrophenol mg/kg wet0.720 0.33 1.667 2027-12943 7
2,4-Dinitrotoluene mg/kg wet1.12 0.33 1.667 2048-12667 4
2,6-Dinitrotoluene mg/kg wet1.15 0.33 1.667 2046-12469 4
2-Chloronaphthalene mg/kg wet1.19 0.33 1.667 2041-11471 3
2-Chlorophenol mg/kg wet0.944 0.33 1.667 2034-12157 1
2-Methylnaphthalene mg/kg wet1.09 0.33 1.667 2038-12265 1
2-Methylphenol mg/kg wet0.995 0.33 1.667 2032-12260 0.3
2-Nitrophenol mg/kg wet0.997 0.33 1.667 2036-12360 2
3,3’-Dichlorobenzidine mg/kg wet0.922 0.33 1.667 2022-12155 0.3
3/4-Methylphenol mg/kg wet0.995 0.33 1.667 2034-11960 2
4,6-Dinitro-2-methylphenol mg/kg wet0.843 0.33 1.667 2029-13251 2
4-Bromophenyl phenyl ether mg/kg wet1.09 0.33 1.667 2046-12465 0.04
4-Chloro-3-methylphenol mg/kg wet1.11 0.33 1.667 2045-12266 1
4-Chloroaniline mg/kg wet1.07 0.33 1.667 2017-10664 2
4-Chlorophenyl phenyl ether mg/kg wet1.13 0.33 1.667 2045-12168 4
4-Nitrophenol mg/kg wet1.04 0.33 1.667 2030-13262 3
Acenaphthene mg/kg wet1.09 0.33 1.667 2040-12366 1
Acenaphthylene mg/kg wet1.12 0.33 1.667 2032-13267 2
Anthracene mg/kg wet1.23 0.33 1.667 2047-12374 2
Azobenzene mg/kg wet1.06 0.33 1.667 2039-12563 2
Benzo(a)anthracene mg/kg wet1.15 0.33 1.667 2049-12669 1
Benzo(a)pyrene mg/kg wet1.20 0.33 1.667 2045-12972 0.9
Benzo(b)fluoranthene mg/kg wet1.13 0.33 1.667 2045-13268 2
Benzo(g,h,i)perylene mg/kg wet1.14 0.33 1.667 2043-13469 10
Benzo(k)fluoranthene mg/kg wet1.21 0.33 1.667 2047-13273 0.2
Benzoic Acid mg/kg wet0.375 0.33 1.667 20 D10-8322 35
Benzyl alcohol mg/kg wet1.11 0.33 1.667 2029-12267 1
bis(2-Chloroethoxy)methane mg/kg wet1.09 0.33 1.667 2036-12165 0.6
Bis(2-Chloroethyl)ether mg/kg wet0.932 0.33 1.667 2031-12056 2
Bis(2-chloroisopropyl)ether mg/kg wet0.909 0.33 1.667 2033-13155 2
Bis(2-Ethylhexyl)phthalate mg/kg wet1.13 0.33 1.667 2051-13368 10
Butyl benzyl phthalate mg/kg wet1.06 0.33 1.667 2048-13264 2
Chrysene mg/kg wet1.16 0.33 1.667 2050-12470 1
Dibenzo(a,h)anthracene mg/kg wet1.18 0.33 1.667 2045-13471 0.8
Dibenzofuran mg/kg wet1.10 0.33 1.667 2044-12066 2
Diethyl phthalate mg/kg wet1.15 0.33 1.667 2050-12469 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 167 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
LCS Dup (P6A0215-BSD1)Prepared & Analyzed: 01/15/16
Dimethyl phthalate mg/kg wet1.16 0.33 1.667 2048-12470 3
Di-n-butyl phthalate mg/kg wet1.17 0.33 1.667 2051-12870 1
Di-n-octyl phthalate mg/kg wet1.12 0.33 1.667 2045-14067 4
Fluoranthene mg/kg wet1.19 0.33 1.667 2050-12772 1
Fluorene mg/kg wet1.15 0.33 1.667 2043-12569 4
Hexachlorobenzene mg/kg wet1.07 0.33 1.667 2045-12264 0.3
Hexachlorobutadiene mg/kg wet1.00 0.33 1.667 2032-12360 1
Hexachlorocyclopentadiene mg/kg wet0.784 0.33 1.667 2032-11747 0.2
Hexachloroethane mg/kg wet0.862 0.33 1.667 2028-11752 2
Indeno(1,2,3-cd)pyrene mg/kg wet1.05 0.33 1.667 2045-13363 7
Isophorone mg/kg wet1.08 0.33 1.667 2030-12265 0.8
Naphthalene mg/kg wet1.09 0.33 1.667 2035-12366 1
Nitrobenzene mg/kg wet1.05 0.33 1.667 2034-12263 0.8
N-Nitroso-di-n-propylamine mg/kg wet0.937 0.33 1.667 2036-12056 0.6
N-Nitrosodiphenylamine mg/kg wet1.10 0.33 1.667 2038-12766 1
Pentachlorophenol mg/kg wet1.05 0.33 1.667 2025-13363 1
Phenanthrene mg/kg wet1.13 0.33 1.667 2050-12168 2
Phenol mg/kg wet0.944 0.33 1.667 2034-12157 2
Pyrene mg/kg wet1.20 0.33 1.667 2047-12772 2
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 772.58
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 671.11
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 642.13
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 681.13
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 632.11
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 721.20
Matrix Spike (P6A0215-MS1)Prepared & Analyzed: 01/15/16 Source: 6010230-21
1,2,4-Trichlorobenzene mg/kg dry1.39 0.43 2.176 BRL 34-11864
1,2-Dichlorobenzene mg/kg dry1.20 0.43 2.176 BRL 33-11755
1,3-Dichlorobenzene mg/kg dry1.14 0.43 2.176 BRL 30-11553
1,4-Dichlorobenzene mg/kg dry1.18 0.43 2.176 BRL 31-11554
1-Methylnaphthalene mg/kg dry1.54 0.43 2.176 BRL 40-11971
2,4,6-Trichlorophenol mg/kg dry1.36 0.43 2.176 BRL 39-12662
2,4-Dichlorophenol mg/kg dry1.41 0.43 2.176 BRL 40-12265
2,4-Dimethylphenol mg/kg dry1.24 0.43 2.176 BRL 30-12757
2,4-Dinitrophenol mg/kg dry1.35 0.43 2.176 BRL 27-12962
2,4-Dinitrotoluene mg/kg dry1.48 0.43 2.176 BRL 48-12668
2,6-Dinitrotoluene mg/kg dry1.53 0.43 2.176 BRL 46-12470
2-Chloronaphthalene mg/kg dry1.59 0.43 2.176 BRL 41-11473
2-Chlorophenol mg/kg dry1.27 0.43 2.176 BRL 34-12158
2-Methylnaphthalene mg/kg dry1.50 0.43 2.176 BRL 38-12269
2-Methylphenol mg/kg dry1.28 0.43 2.176 BRL 32-12259
2-Nitrophenol mg/kg dry1.36 0.43 2.176 BRL 36-12363
3,3’-Dichlorobenzidine mg/kg dry0.966 0.43 2.176 BRL 22-12144
3/4-Methylphenol mg/kg dry1.30 0.43 2.176 BRL 34-11960
4,6-Dinitro-2-methylphenol mg/kg dry1.30 0.43 2.176 BRL 29-13260
4-Bromophenyl phenyl ether mg/kg dry1.48 0.43 2.176 BRL 46-12468
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 168 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
Matrix Spike (P6A0215-MS1)Prepared & Analyzed: 01/15/16 Source: 6010230-21
4-Chloro-3-methylphenol mg/kg dry1.49 0.43 2.176 BRL 45-12269
4-Chloroaniline mg/kg dry1.38 0.43 2.176 BRL 17-10663
4-Chlorophenyl phenyl ether mg/kg dry1.49 0.43 2.176 BRL 45-12169
4-Nitrophenol mg/kg dry1.41 0.43 2.176 BRL 30-13265
Acenaphthene mg/kg dry1.50 0.43 2.176 BRL 40-12369
Acenaphthylene mg/kg dry1.51 0.43 2.176 BRL 32-13269
Anthracene mg/kg dry1.62 0.43 2.176 BRL 47-12374
Azobenzene mg/kg dry1.43 0.43 2.176 BRL 39-12566
Benzo(a)anthracene mg/kg dry1.53 0.43 2.176 BRL 49-12670
Benzo(a)pyrene mg/kg dry1.53 0.43 2.176 BRL 45-12970
Benzo(b)fluoranthene mg/kg dry1.45 0.43 2.176 BRL 45-13267
Benzo(g,h,i)perylene mg/kg dry1.49 0.43 2.176 BRL 43-13469
Benzo(k)fluoranthene mg/kg dry1.54 0.43 2.176 BRL 47-13271
Benzoic Acid mg/kg dry1.47 0.43 2.176 BRL 10-8368
Benzyl alcohol mg/kg dry1.48 0.43 2.176 BRL 29-12268
bis(2-Chloroethoxy)methane mg/kg dry1.43 0.43 2.176 BRL 36-12166
Bis(2-Chloroethyl)ether mg/kg dry1.43 0.43 2.176 BRL 31-12066
Bis(2-chloroisopropyl)ether mg/kg dry1.25 0.43 2.176 BRL 33-13158
Bis(2-Ethylhexyl)phthalate mg/kg dry1.51 0.43 2.176 BRL 51-13369
Butyl benzyl phthalate mg/kg dry1.46 0.43 2.176 BRL 48-13267
Chrysene mg/kg dry1.55 0.43 2.176 BRL 50-12471
Dibenzo(a,h)anthracene mg/kg dry1.52 0.43 2.176 BRL 45-13470
Dibenzofuran mg/kg dry1.48 0.43 2.176 BRL 44-12068
Diethyl phthalate mg/kg dry1.54 0.43 2.176 BRL 50-12471
Dimethyl phthalate mg/kg dry1.55 0.43 2.176 BRL 48-12471
Di-n-butyl phthalate mg/kg dry1.58 0.43 2.176 BRL 51-12872
Di-n-octyl phthalate mg/kg dry1.48 0.43 2.176 BRL 45-14068
Fluoranthene mg/kg dry1.58 0.43 2.176 BRL 50-12773
Fluorene mg/kg dry1.51 0.43 2.176 BRL 43-12569
Hexachlorobenzene mg/kg dry1.41 0.43 2.176 BRL 45-12265
Hexachlorobutadiene mg/kg dry1.35 0.43 2.176 BRL 32-12362
Hexachlorocyclopentadiene mg/kg dry1.17 0.43 2.176 BRL 32-11754
Hexachloroethane mg/kg dry1.15 0.43 2.176 BRL 28-11753
Indeno(1,2,3-cd)pyrene mg/kg dry1.73 0.43 2.176 BRL 45-13380
Isophorone mg/kg dry1.48 0.43 2.176 BRL 30-12268
Naphthalene mg/kg dry1.50 0.43 2.176 BRL 35-12369
Nitrobenzene mg/kg dry1.45 0.43 2.176 BRL 34-12267
N-Nitroso-di-n-propylamine mg/kg dry1.30 0.43 2.176 BRL 36-12060
N-Nitrosodiphenylamine mg/kg dry1.41 0.43 2.176 BRL 38-12765
Pentachlorophenol mg/kg dry1.48 0.43 2.176 BRL 25-13368
Phenanthrene mg/kg dry1.50 0.43 2.176 BRL 50-12169
Phenol mg/kg dry1.27 0.43 2.176 BRL 34-12158
Pyrene mg/kg dry1.61 0.43 2.176 BRL 47-12774
mg/kg dry 4.351 39-132Surrogate: 2,4,6-Tribromophenol 753.27
mg/kg dry 2.176 44-115Surrogate: 2-Fluorobiphenyl 681.48
mg/kg dry 4.351 35-115Surrogate: 2-Fluorophenol 662.85
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 169 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
Matrix Spike (P6A0215-MS1)Prepared & Analyzed: 01/15/16 Source: 6010230-21
mg/kg dry 2.176 37-122Surrogate: Nitrobenzene-d5 701.52
mg/kg dry 4.351 34-121Surrogate: Phenol-d5 652.85
mg/kg dry 2.176 54-127Surrogate: Terphenyl-d14 711.55
Matrix Spike Dup (P6A0215-MSD1)Prepared & Analyzed: 01/15/16 Source: 6010230-21
1,2,4-Trichlorobenzene mg/kg dry1.23 0.43 2.176 BRL 2034-11856 13
1,2-Dichlorobenzene mg/kg dry1.08 0.43 2.176 BRL 2033-11750 10
1,3-Dichlorobenzene mg/kg dry1.01 0.43 2.176 BRL 2030-11547 12
1,4-Dichlorobenzene mg/kg dry1.06 0.43 2.176 BRL 2031-11549 11
1-Methylnaphthalene mg/kg dry1.38 0.43 2.176 BRL 2040-11963 11
2,4,6-Trichlorophenol mg/kg dry1.19 0.43 2.176 BRL 2039-12655 13
2,4-Dichlorophenol mg/kg dry1.29 0.43 2.176 BRL 2040-12259 9
2,4-Dimethylphenol mg/kg dry1.13 0.43 2.176 BRL 2030-12752 9
2,4-Dinitrophenol mg/kg dry1.24 0.43 2.176 BRL 2027-12957 8
2,4-Dinitrotoluene mg/kg dry1.35 0.43 2.176 BRL 2048-12662 9
2,6-Dinitrotoluene mg/kg dry1.39 0.43 2.176 BRL 2046-12464 10
2-Chloronaphthalene mg/kg dry1.43 0.43 2.176 BRL 2041-11466 11
2-Chlorophenol mg/kg dry1.13 0.43 2.176 BRL 2034-12152 11
2-Methylnaphthalene mg/kg dry1.33 0.43 2.176 BRL 2038-12261 12
2-Methylphenol mg/kg dry1.15 0.43 2.176 BRL 2032-12253 11
2-Nitrophenol mg/kg dry1.23 0.43 2.176 BRL 2036-12356 11
3,3’-Dichlorobenzidine mg/kg dry0.878 0.43 2.176 BRL 2022-12140 10
3/4-Methylphenol mg/kg dry1.17 0.43 2.176 BRL 2034-11954 11
4,6-Dinitro-2-methylphenol mg/kg dry1.17 0.43 2.176 BRL 2029-13254 11
4-Bromophenyl phenyl ether mg/kg dry1.33 0.43 2.176 BRL 2046-12461 11
4-Chloro-3-methylphenol mg/kg dry1.36 0.43 2.176 BRL 2045-12262 10
4-Chloroaniline mg/kg dry1.26 0.43 2.176 BRL 2017-10658 9
4-Chlorophenyl phenyl ether mg/kg dry1.36 0.43 2.176 BRL 2045-12163 9
4-Nitrophenol mg/kg dry1.25 0.43 2.176 BRL 2030-13258 11
Acenaphthene mg/kg dry1.36 0.43 2.176 BRL 2040-12363 10
Acenaphthylene mg/kg dry1.36 0.43 2.176 BRL 2032-13263 10
Anthracene mg/kg dry1.49 0.43 2.176 BRL 2047-12368 9
Azobenzene mg/kg dry1.29 0.43 2.176 BRL 2039-12559 10
Benzo(a)anthracene mg/kg dry1.42 0.43 2.176 BRL 2049-12665 8
Benzo(a)pyrene mg/kg dry1.44 0.43 2.176 BRL 2045-12966 6
Benzo(b)fluoranthene mg/kg dry1.33 0.43 2.176 BRL 2045-13261 9
Benzo(g,h,i)perylene mg/kg dry1.35 0.43 2.176 BRL 2043-13462 10
Benzo(k)fluoranthene mg/kg dry1.43 0.43 2.176 BRL 2047-13266 8
Benzoic Acid mg/kg dry1.35 0.43 2.176 BRL 2010-8362 8
Benzyl alcohol mg/kg dry1.34 0.43 2.176 BRL 2029-12261 10
bis(2-Chloroethoxy)methane mg/kg dry1.31 0.43 2.176 BRL 2036-12160 9
Bis(2-Chloroethyl)ether mg/kg dry1.30 0.43 2.176 BRL 2031-12060 9
Bis(2-chloroisopropyl)ether mg/kg dry1.11 0.43 2.176 BRL 2033-13151 12
Bis(2-Ethylhexyl)phthalate mg/kg dry1.38 0.43 2.176 BRL 2051-13364 9
Butyl benzyl phthalate mg/kg dry1.34 0.43 2.176 BRL 2048-13262 9
Chrysene mg/kg dry1.43 0.43 2.176 BRL 2050-12466 8
Dibenzo(a,h)anthracene mg/kg dry1.32 0.43 2.176 BRL 2045-13461 15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 170 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6A0215 - 3546
Matrix Spike Dup (P6A0215-MSD1)Prepared & Analyzed: 01/15/16 Source: 6010230-21
Dibenzofuran mg/kg dry1.31 0.43 2.176 BRL 2044-12060 12
Diethyl phthalate mg/kg dry1.40 0.43 2.176 BRL 2050-12464 9
Dimethyl phthalate mg/kg dry1.39 0.43 2.176 BRL 2048-12464 11
Di-n-butyl phthalate mg/kg dry1.45 0.43 2.176 BRL 2051-12866 9
Di-n-octyl phthalate mg/kg dry1.34 0.43 2.176 BRL 2045-14061 10
Fluoranthene mg/kg dry1.44 0.43 2.176 BRL 2050-12766 9
Fluorene mg/kg dry1.39 0.43 2.176 BRL 2043-12564 8
Hexachlorobenzene mg/kg dry1.30 0.43 2.176 BRL 2045-12260 8
Hexachlorobutadiene mg/kg dry1.19 0.43 2.176 BRL 2032-12355 13
Hexachlorocyclopentadiene mg/kg dry0.997 0.43 2.176 BRL 2032-11746 16
Hexachloroethane mg/kg dry1.03 0.43 2.176 BRL 2028-11747 12
Indeno(1,2,3-cd)pyrene mg/kg dry1.27 0.43 2.176 BRL 20 D45-13358 31
Isophorone mg/kg dry1.32 0.43 2.176 BRL 2030-12260 12
Naphthalene mg/kg dry1.33 0.43 2.176 BRL 2035-12361 12
Nitrobenzene mg/kg dry1.27 0.43 2.176 BRL 2034-12258 13
N-Nitroso-di-n-propylamine mg/kg dry1.17 0.43 2.176 BRL 2036-12054 10
N-Nitrosodiphenylamine mg/kg dry1.27 0.43 2.176 BRL 2038-12758 10
Pentachlorophenol mg/kg dry1.35 0.43 2.176 BRL 2025-13362 9
Phenanthrene mg/kg dry1.38 0.43 2.176 BRL 2050-12163 8
Phenol mg/kg dry1.17 0.43 2.176 BRL 2034-12154 8
Pyrene mg/kg dry1.47 0.43 2.176 BRL 2047-12768 9
mg/kg dry 4.351 39-132Surrogate: 2,4,6-Tribromophenol 703.06
mg/kg dry 2.176 44-115Surrogate: 2-Fluorobiphenyl 621.35
mg/kg dry 4.351 35-115Surrogate: 2-Fluorophenol 592.56
mg/kg dry 2.176 37-122Surrogate: Nitrobenzene-d5 591.27
mg/kg dry 4.351 34-121Surrogate: Phenol-d5 592.58
mg/kg dry 2.176 54-127Surrogate: Terphenyl-d14 661.43
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 171 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6A0211 - 3050B
Blank (P6A0211-BLK1)Prepared & Analyzed: 01/15/16
Arsenic mg/kg wetBRL0.25
Barium mg/kg wetBRL0.50
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wet0.357 0.25 BH
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL0.50
Silver mg/kg wetBRL0.25
LCS (P6A0211-BS1)Prepared & Analyzed: 01/15/16
Arsenic mg/kg wet23.0 0.25 25.00 80-12092
Barium mg/kg wet24.2 0.50 25.00 80-12097
Cadmium mg/kg wet22.4 0.25 25.00 80-12090
Chromium mg/kg wet24.3 0.25 25.00 80-12097
Lead mg/kg wet22.4 0.25 25.00 80-12089
Selenium mg/kg wet21.8 0.50 25.00 80-12087
Silver mg/kg wet9.00 0.25 10.00 80-12090
Matrix Spike (P6A0211-MS1)Prepared & Analyzed: 01/15/16 Source: 6010230-01
Arsenic mg/kg dry24.3 0.34 34.45 3.02 MI75-12562
Barium mg/kg dry79.7 0.69 34.45 49.1 75-12589
Cadmium mg/kg dry23.2 0.34 34.45 BRL MI75-12567
Chromium mg/kg dry27.6 0.34 34.45 2.12 MI75-12574
Lead mg/kg dry26.9 0.34 34.45 4.68 MI75-12565
Selenium mg/kg dry18.9 0.69 34.45 BRL MI75-12555
Silver mg/kg dry11.0 0.34 13.78 BRL 75-12580
Matrix Spike Dup (P6A0211-MSD1)Prepared & Analyzed: 01/15/16 Source: 6010230-01
Arsenic mg/kg dry25.0 0.35 34.62 3.02 20 MI75-12563 3
Barium mg/kg dry77.5 0.69 34.62 49.1 2075-12582 3
Cadmium mg/kg dry23.4 0.35 34.62 BRL 20 MI75-12568 0.8
Chromium mg/kg dry28.7 0.35 34.62 2.12 2075-12577 4
Lead mg/kg dry27.6 0.35 34.62 4.68 20 MI75-12566 3
Selenium mg/kg dry18.7 0.69 34.62 BRL 20 MI75-12554 0.7
Silver mg/kg dry11.0 0.35 13.85 BRL 2075-12580 0.2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 172 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6A0211 - 3050B
Post Spike (P6A0211-PS1)Prepared: 01/15/16 Analyzed: 01/16/16 Source: 6010230-01
Arsenic mg/L0.832 1.000 0.0867 MI80-12075
Barium mg/L2.10 1.000 1.41 MI80-12069
Cadmium mg/L0.656 1.000 -0.0144 MI80-12066
Chromium mg/L0.800 1.000 0.0610 MI80-12074
Lead mg/L0.798 1.000 0.134 MI80-12066
Selenium mg/L0.670 1.000 -0.0197 MI80-12067
Silver mg/L0.304 0.4000 -0.00203 MI80-12076
Batch P6A0212 - 7471B
Blank (P6A0212-BLK1)Prepared & Analyzed: 01/15/16
Mercury mg/kg wetBRL0.020
LCS (P6A0212-BS1)Prepared & Analyzed: 01/15/16
Mercury mg/kg wet0.411 0.020 0.4167 80-12099
Matrix Spike (P6A0212-MS1)Prepared & Analyzed: 01/15/16 Source: 6010230-01
Mercury mg/kg dry0.484 0.027 0.5522 0.00189 80-12087
Matrix Spike Dup (P6A0212-MSD1)Prepared & Analyzed: 01/15/16 Source: 6010230-01
Mercury mg/kg dry0.488 0.027 0.5611 0.00189 2080-12087 0.7
Batch P6A0229 - 3050B
Blank (P6A0229-BLK1)Prepared & Analyzed: 01/18/16
Arsenic mg/kg wetBRL0.25
Barium mg/kg wetBRL0.50
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wetBRL0.25
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL0.50
Silver mg/kg wetBRL0.25
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 173 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6A0229 - 3050B
LCS (P6A0229-BS1)Prepared & Analyzed: 01/18/16
Arsenic mg/kg wet24.9 0.25 25.00 80-12099
Barium mg/kg wet25.3 0.50 25.00 80-120101
Cadmium mg/kg wet25.6 0.25 25.00 80-120103
Chromium mg/kg wet25.5 0.25 25.00 80-120102
Lead mg/kg wet25.4 0.25 25.00 80-120101
Selenium mg/kg wet25.5 0.50 25.00 80-120102
Silver mg/kg wet9.98 0.25 10.00 80-120100
Matrix Spike (P6A0229-MS1)Prepared & Analyzed: 01/18/16 Source: 6010230-19
Arsenic mg/kg dry25.7 0.31 31.37 2.26 75-12575
Barium mg/kg dry48.8 0.63 31.37 10.9 75-125121
Cadmium mg/kg dry26.0 0.31 31.37 0.0397 75-12583
Chromium mg/kg dry36.6 0.31 31.37 9.17 75-12588
Lead mg/kg dry29.4 0.31 31.37 5.24 75-12577
Selenium mg/kg dry22.5 0.63 31.37 BRL MI75-12572
Silver mg/kg dry12.2 0.31 12.55 0.989 75-12589
Matrix Spike Dup (P6A0229-MSD1)Prepared & Analyzed: 01/18/16 Source: 6010230-19
Arsenic mg/kg dry25.5 0.31 30.90 2.26 2075-12575 0.7
Barium mg/kg dry48.7 0.62 30.90 10.9 2075-125123 0.03
Cadmium mg/kg dry25.9 0.31 30.90 0.0397 2075-12584 0.6
Chromium mg/kg dry36.6 0.31 30.90 9.17 2075-12589 0.09
Lead mg/kg dry29.3 0.31 30.90 5.24 2075-12578 0.2
Selenium mg/kg dry21.8 0.62 30.90 BRL 20 MI75-12570 3
Silver mg/kg dry12.2 0.31 12.36 0.989 2075-12591 0.02
Post Spike (P6A0229-PS1)Prepared: 01/18/16 Analyzed: 01/19/16 Source: 6010230-19
Arsenic mg/L0.912 1.000 0.0736 80-12084
Barium mg/L1.17 1.000 0.353 80-12082
Cadmium mg/L0.791 1.000 0.00129 MI80-12079
Chromium mg/L1.12 1.000 0.298 80-12082
Lead mg/L0.929 1.000 0.170 MI80-12076
Selenium mg/L0.816 1.000 -0.0524 80-12082
Silver mg/L0.376 0.4000 0.0322 80-12086
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 174 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P6A0230 - 7471B
Blank (P6A0230-BLK1)Prepared & Analyzed: 01/18/16
Mercury mg/kg wetBRL0.020
LCS (P6A0230-BS1)Prepared & Analyzed: 01/18/16
Mercury mg/kg wet0.429 0.020 0.4167 80-120103
Matrix Spike (P6A0230-MS1)Prepared & Analyzed: 01/18/16 Source: 6010230-19
Mercury mg/kg dry0.478 0.025 0.5211 0.0349 80-12085
Matrix Spike Dup (P6A0230-MSD1)Prepared & Analyzed: 01/18/16 Source: 6010230-19
Mercury mg/kg dry0.526 0.026 0.5394 0.0349 2080-12091 10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 175 of 229
1/21/16
Level II QC Report
500-K Clanton Rd.
Project: 1201 Central AveGeoscience Group
Charlotte, NC 28217
Attn: Tom Hassett
Prism Work Order: 6010230
Time Submitted: 1/14/2016 8:20:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P6A0219 - Solids, Dry Weight
Blank (P6A0219-BLK1)Prepared & Analyzed: 01/15/16
% Solids % by Weight1000.100
Duplicate (P6A0219-DUP3)Prepared & Analyzed: 01/15/16 Source: 6010230-02
% Solids % by Weight78.3 0.100 78.3 200.1
Duplicate (P6A0219-DUP4)Prepared & Analyzed: 01/15/16 Source: 6010230-12
% Solids % by Weight92.0 0.100 91.9 200.07
Batch P6A0248 - Solids, Dry Weight
Blank (P6A0248-BLK1)Prepared & Analyzed: 01/18/16
% Solids % by Weight99.9 0.100
Duplicate (P6A0248-DUP1)Prepared & Analyzed: 01/18/16 Source: 6010230-15
% Solids % by Weight81.2 0.100 81.1 200.1
Duplicate (P6A0248-DUP2)Prepared & Analyzed: 01/18/16 Source: 6010230-25
% Solids % by Weight82.7 0.100 82.7 200.02
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 176 of 229
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P6A02196010230-01 01/15/16 16:0030 30g g
P6A02196010230-02 01/15/16 16:0030 30g g
P6A02196010230-03 01/15/16 16:0030 30g g
P6A02196010230-04 01/15/16 16:0030 30g g
P6A02196010230-05 01/15/16 16:0030 30g g
P6A02196010230-06 01/15/16 16:0030 30g g
P6A02196010230-07 01/15/16 16:0030 30g g
P6A02196010230-08 01/15/16 16:0030 30g g
P6A02196010230-09 01/15/16 16:0030 30g g
P6A02196010230-10 01/15/16 16:0030 30g g
P6A02196010230-11 01/15/16 16:0030 30g g
P6A02196010230-12 01/15/16 16:0030 30g g
P6A02486010230-13 01/18/16 16:4030 30g g
P6A02486010230-14 01/18/16 16:4030 30g g
P6A02486010230-15 01/18/16 16:4030 30g g
P6A02486010230-16 01/18/16 16:4030 30g g
P6A02486010230-17 01/18/16 16:4030 30g g
P6A02486010230-18 01/18/16 16:4030 30g g
P6A02486010230-19 01/18/16 16:4030 30g g
P6A02486010230-20 01/18/16 16:4030 30g g
P6A02486010230-21 01/18/16 16:4030 30g g
P6A02196010230-22 01/15/16 16:0030 30g g
P6A02196010230-23 01/15/16 16:0030 30g g
P6A02486010230-24 01/18/16 16:4030 30g g
P6A02486010230-25 01/18/16 16:4030 30g g
P6A02486010230-26 01/18/16 16:4030 30g g
P6A02486010230-27 01/18/16 16:4030 30g g
P6A02486010230-28 01/18/16 16:4030 30g g
P6A02486010230-29 01/18/16 16:4030 30g g
P6A02486010230-30 01/18/16 16:4030 30g g
P6A02486010230-31 01/18/16 16:4030 30g g
P6A02486010230-32 01/18/16 16:4030 30g g
P6A02486010230-33 01/18/16 16:4030 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P6A01986010230-01 01/14/16 11:0030 1g mL
P6A01986010230-02 01/14/16 11:0030 1g mL
P6A01986010230-03 01/14/16 11:0030 1g mL
P6A01986010230-04 01/14/16 11:0030.05 1g mL
P6A01986010230-05 01/14/16 11:0030.02 1g mL
P6A01986010230-06 01/14/16 11:0030 1g mL
P6A01986010230-07 01/14/16 11:0030 1g mL
P6A01986010230-08 01/14/16 11:0030.04 1g mL
P6A01986010230-09 01/14/16 11:0030 1g mL
P6A01986010230-10 01/14/16 11:0030.02 1g mL
P6A01986010230-11 01/14/16 11:0030.04 1g mL
P6A01986010230-12 01/14/16 11:0030 1g mL
P6A02156010230-13 01/15/16 10:1530 1g mL
P6A02156010230-14 01/15/16 10:1530 1g mL
P6A02156010230-15 01/15/16 10:1530 1g mL
P6A02156010230-16 01/15/16 10:1530 1g mL
P6A02156010230-17 01/15/16 10:1530.02 1g mL
P6A02156010230-18 01/15/16 10:1530 1g mL
P6A02156010230-19 01/15/16 10:1530.01 1g mL
P6A02156010230-20 01/15/16 10:1530 1g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 177 of 229
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P6A02156010230-21 01/15/16 10:1530 1g mL
P6A01986010230-22 01/14/16 11:0030.03 1g mL
P6A01986010230-23 01/14/16 11:0030.04 1g mL
P6A01986010230-24 01/14/16 11:0030.03 1g mL
P6A02156010230-25 01/15/16 10:1530 1g mL
P6A02156010230-26 01/15/16 10:1530 1g mL
P6A02156010230-27 01/15/16 10:1530.01 1g mL
P6A02156010230-28 01/15/16 10:1530.04 1g mL
P6A02156010230-29 01/15/16 10:1530 1g mL
P6A02156010230-30 01/15/16 10:1530 1g mL
P6A02156010230-31 01/15/16 10:1530.03 1g mL
P6A02156010230-32 01/15/16 10:1530 1g mL
P6A02156010230-33 01/15/16 10:1530 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P6A02116010230-01 01/15/16 8:302.03 50g mL
P6A02116010230-02 01/15/16 8:301.97 50g mL
P6A02116010230-03 01/15/16 8:302.03 50g mL
P6A02116010230-04 01/15/16 8:301.95 50g mL
P6A02116010230-05 01/15/16 8:301.98 50g mL
P6A02116010230-06 01/15/16 8:302.05 50g mL
P6A02116010230-07 01/15/16 8:301.96 50g mL
P6A02116010230-08 01/15/16 8:302.02 50g mL
P6A02116010230-09 01/15/16 8:302.04 50g mL
P6A02116010230-10 01/15/16 8:301.97 50g mL
P6A02116010230-11 01/15/16 8:301.95 50g mL
P6A02116010230-12 01/15/16 8:302.03 50g mL
P6A02116010230-13 01/15/16 8:302.04 50g mL
P6A02116010230-14 01/15/16 8:302.02 50g mL
P6A02116010230-15 01/15/16 8:302.05 50g mL
P6A02116010230-16 01/15/16 8:302.01 50g mL
P6A02116010230-17 01/15/16 8:302 50g mL
P6A02116010230-18 01/15/16 8:302.03 50g mL
P6A02296010230-19 01/18/16 7:301.99 50g mL
P6A02296010230-20 01/18/16 7:301.98 50g mL
P6A02296010230-21 01/18/16 7:302.03 50g mL
P6A02116010230-22 01/15/16 8:302.04 50g mL
P6A02116010230-23 01/15/16 8:301.97 50g mL
P6A02296010230-24 01/18/16 7:302.04 50g mL
P6A02296010230-25 01/18/16 7:301.97 50g mL
P6A02296010230-26 01/18/16 7:302.05 50g mL
P6A02296010230-27 01/18/16 7:301.97 50g mL
P6A02296010230-28 01/18/16 7:301.97 50g mL
P6A02296010230-29 01/18/16 7:302.05 50g mL
P6A02296010230-30 01/18/16 7:302.05 50g mL
P6A02296010230-31 01/18/16 7:301.98 50g mL
P6A02296010230-32 01/18/16 7:301.96 50g mL
P6A02296010230-33 01/18/16 7:302.04 50g mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P6A02126010230-01 01/15/16 9:150.63 50g mL
P6A02126010230-02 01/15/16 9:150.58 50g mL
P6A02126010230-03 01/15/16 9:150.59 50g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 178 of 229
Sample Extraction Data
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P6A02126010230-04 01/15/16 9:150.64 50g mL
P6A02126010230-05 01/15/16 9:150.61 50g mL
P6A02126010230-06 01/15/16 9:150.61 50g mL
P6A02126010230-07 01/15/16 9:150.62 50g mL
P6A02126010230-08 01/15/16 9:150.63 50g mL
P6A02126010230-09 01/15/16 9:150.65 50g mL
P6A02126010230-10 01/15/16 9:150.61 50g mL
P6A02126010230-11 01/15/16 9:150.61 50g mL
P6A02126010230-12 01/15/16 9:150.56 50g mL
P6A02126010230-13 01/15/16 9:150.61 50g mL
P6A02126010230-14 01/15/16 9:150.61 50g mL
P6A02126010230-15 01/15/16 9:150.64 50g mL
P6A02126010230-16 01/15/16 9:150.64 50g mL
P6A02126010230-17 01/15/16 9:150.59 50g mL
P6A02126010230-18 01/15/16 9:150.61 50g mL
P6A02306010230-19 01/18/16 8:150.59 50g mL
P6A02306010230-20 01/18/16 8:150.59 50g mL
P6A02306010230-21 01/18/16 8:150.64 50g mL
P6A02126010230-22 01/15/16 9:150.61 50g mL
P6A02126010230-23 01/15/16 9:150.57 50g mL
P6A02306010230-24 01/18/16 8:150.55 50g mL
P6A02306010230-25 01/18/16 8:150.57 50g mL
P6A02306010230-26 01/18/16 8:150.6 50g mL
P6A02306010230-27 01/18/16 8:150.56 50g mL
P6A02306010230-28 01/18/16 8:150.57 50g mL
P6A02306010230-29 01/18/16 8:150.59 50g mL
P6A02306010230-30 01/18/16 8:150.61 50g mL
P6A02306010230-31 01/18/16 8:150.6 50g mL
P6A02306010230-32 01/18/16 8:150.6 50g mL
P6A02306010230-33 01/18/16 8:150.6 50g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P6A02006010230-01 01/14/16 9:025.71 5g mL
P6A02006010230-02 01/14/16 9:024.65 5g mL
P6A02006010230-03 01/14/16 9:024.88 5g mL
P6A02006010230-04 01/14/16 9:024.54 5g mL
P6A02006010230-05 01/14/16 9:024.41 5g mL
P6A02006010230-06 01/14/16 9:024.46 5g mL
P6A02006010230-07 01/14/16 9:025.21 5g mL
P6A02006010230-08 01/14/16 9:024.88 5g mL
P6A02006010230-09 01/14/16 9:024.5 5g mL
P6A02006010230-10 01/14/16 9:024.16 5g mL
P6A02006010230-11 01/14/16 9:024.2 5g mL
P6A02006010230-12 01/14/16 9:023.9 5g mL
P6A02006010230-13 01/14/16 9:024.62 5g mL
P6A02006010230-14 01/14/16 9:024.19 5g mL
P6A02006010230-15 01/14/16 9:024.03 5g mL
P6A02006010230-16 01/14/16 9:025.27 5g mL
P6A02006010230-17 01/14/16 9:024.35 5g mL
P6A02006010230-18 01/14/16 9:024.88 5g mL
P6A02006010230-19 01/14/16 9:023.95 5g mL
P6A02006010230-20 01/14/16 9:023.72 5g mL
P6A02016010230-21 01/14/16 9:044.86 5g mL
P6A02016010230-22 01/14/16 9:044.81 5g mL
P6A02016010230-23 01/14/16 9:045.25 5g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 179 of 229
Sample Extraction Data
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P6A02016010230-24 01/14/16 9:044.76 5g mL
P6A02016010230-25 01/14/16 9:044.55 5g mL
P6A02016010230-26 01/14/16 9:043.93 5g mL
P6A02016010230-27 01/14/16 9:044.69 5g mL
P6A02016010230-28 01/14/16 9:044.5 5g mL
P6A02016010230-29 01/14/16 9:044.58 5g mL
P6A02016010230-30 01/14/16 9:044.13 5g mL
P6A02016010230-31 01/14/16 9:045.3 5g mL
P6A02016010230-32 01/14/16 9:044.56 5g mL
P6A02016010230-33 01/14/16 9:044.37 5g mL
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Analysis
6010230-01 Hexavalent Chromium (Sub)
6010230-02 Hexavalent Chromium (Sub)
6010230-03 Hexavalent Chromium (Sub)
6010230-04 Hexavalent Chromium (Sub)
6010230-05 Hexavalent Chromium (Sub)
6010230-06 Hexavalent Chromium (Sub)
6010230-07 Hexavalent Chromium (Sub)
6010230-08 Hexavalent Chromium (Sub)
6010230-09 Hexavalent Chromium (Sub)
6010230-10 Hexavalent Chromium (Sub)
6010230-11 Hexavalent Chromium (Sub)
6010230-12 Hexavalent Chromium (Sub)
6010230-13 Hexavalent Chromium (Sub)
6010230-14 Hexavalent Chromium (Sub)
6010230-15 Hexavalent Chromium (Sub)
6010230-16 Hexavalent Chromium (Sub)
6010230-17 Hexavalent Chromium (Sub)
6010230-18 Hexavalent Chromium (Sub)
6010230-19 Hexavalent Chromium (Sub)
6010230-20 Hexavalent Chromium (Sub)
6010230-21 Hexavalent Chromium (Sub)
6010230-22 Hexavalent Chromium (Sub)
6010230-23 Hexavalent Chromium (Sub)
6010230-24 Hexavalent Chromium (Sub)
6010230-25 Hexavalent Chromium (Sub)
6010230-26 Hexavalent Chromium (Sub)
6010230-27 Hexavalent Chromium (Sub)
6010230-28 Hexavalent Chromium (Sub)
6010230-29 Hexavalent Chromium (Sub)
6010230-30 Hexavalent Chromium (Sub)
6010230-31 Hexavalent Chromium (Sub)
6010230-32 Hexavalent Chromium (Sub)
6010230-33 Hexavalent Chromium (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 180 of 229
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