12022 Amity Garden Sewer Line Approval-Memo 20180309

State of North Carolina | Environmental Quality | Waste Management
1646 Mail Service Center | 217 West Jones Street | Raleigh, NC 27699-1646
919 707 8200 T

March 9, 2018

Sent Via Email [e-mail]
Todd Ware
Johnston, Allison, & Hord
1065 East Morehead St.
Charlotte, NC 36469 Subject: Approval of Storm Water Drainage Line Work revised
Amity Garden Brownfields Property
Charlotte, Mecklenburg County
Brownfields Project Number 12022-08-060 Dear Mr. Ware:

The North Carolina Department of Environmental Quality (DEQ) Brownfields Program
received a phone call and follow up email correspondence for a storm water drainage line replacement project that crosses a small portion of the above reference property. (see attached figure for location) I have reviewed the information you provided in the March 2 and March 5
emails, and reviewed historical DEQ brownfields files. The area that will be impacted does not
have any known soil or groundwater impacts.
If during the storm water drainage line removal activities, if impacted soils are discovered with staining or distinct unnatural color, strong odor, or materials of concern (chemical, tanks,
drums, etc.) are found, please notify DEQ Brownfields Program. In your correspondence, you
stated soils would not be imported or exported during this project. If this assumption changes,
please notify the DEQ Brownfields Program prior to exporting or importing soil to the brownfields property.

Be advised that this approval from the Brownfields Program does not waive any
applicable requirement to obtain any necessary permits, licenses or certifications for the above
listed activities nor does it waive any requirement to comply with applicable law for such activities. If you have questions about this correspondence or require additional information,
please contact me by phone at 704/661-0330, or by e-mail at [e-mail].

Sincerely,
Carolyn Minnich
Carolyn Minnich Brownfields Project Manager
Division of Waste Management

DECISION MEMORANDUM

FROM: Carolyn Minnich

TO: BF Post Recordation File
DATE: March 9, 2018

RE: former Amity Garden (Wal Mart RN)
Charlotte, Mecklenburg County Brownfields Project No. 12022-08-060

On Friday, March 2, NCDENR Brownfields Program was notified by Todd Ware
of Johnson Allison and Hord Attorneys via phone call and then e-mail about soil
disturbance activities for a storm drainage line removal and replacement on a portion of the above referenced brownfields site. The following is his message, a pdf is attached to
this memo.

Carolyn, Thanks for your time this afternoon and offer to assist on my client’s situation. Attached
is the WalMart Redevelopment Plan from 2010, which I have been told was approved by
DENR. The Site Location Map on page 13 is what I was looking at and referring to on
our call. Also attached is an easement exhibit document that shows the area of the easement rights being granted to my client, with the actual pipe being located as shown in the center of the 40’ PDE. As mentioned, the work on the brownfields property will be
limited to excavating a trench along the existing 84” pipe to a depth of 7- 18’, removing
the existing pipe and replacing it with approximately 67 lf of new pipe on the brownfields
property, with the original material to be backfilled, and cleaning out the ditch below the headwall. No exporting or importing of soil is planned. I have also attached plan sheets that show existing conditions and the new drainage pipe. I will update my client and be
back in touch. Ideally, we would simply formally notify DEQ of our plans, which would
not require any analytical assessment or other formal action/approval.
Cameron Todd Ware, Partner
Site History:
The area of impact on the brownfields property is minor. It is near southwest near the
creek, behind the former Amity Garden Plaza and away from Wal-Mart Store. There are
two soil samples GP-16 (7-8) and GP-16 (11-12), one shallow groundwater well
monitoring well MW-6, and one deep monitoring well DMW-11 near the work area.
Please refer to attached map for locations.

Potential Receptors:
Workers (construction/outdoor)

Contaminated Media: Groundwater: one shallow and one deep well are in the area. DMW-11 and MW-6.
Groundwater contaminants (in micrograms per liter, the equivalent of parts per billion),
the standards for which are in Title 15A of the North Carolina Administrative Code,
Subchapter 2L, Rule .0202:

Well Depth
(ft)
Date Benzene Toluene Barium
2L Standard 10/3/2008 1 600 700
MW-6 20 10/3/2008 5.4 5.4 124
MW-6 (DUP) 20 10/3/2008 2.8 3.8 122
Notes: units in ug/L
Samples from S&ME Progress Report #1 dated 10/22/2008
Deep Monitoring Well DMW-11 had not contaminates above 2L Standards.
Soil: No soil impacts are known in this area, nor was it an area of concern in past investigations.

Location Depth
(ft) Date Bis(2-
ethylhexyl
phthalate)
Methylene
Chloride Barium Cadmium Chromium
(Total)
VI/III
Lead Selenium Silver
PSRG Residential 39 58 3100 14 0.31/23000 400 78 78
PSRG Ind/Comm 160 650 47000 200 6.5/350000 1200 1200
PSRG POG 14 0.025 580 3 3.8/360000 250 2.1 3.4
GP-16 7-8 9/29/2008 ND 0.0711 130 7.6 206 6 3.9 0.67
GP-16 11-12 9/29/2008 0.601 ND 97.5 2.8 48.9 2.4 1.8 ND
Notes: Results are in parts per million, mg/kg
ND: Not Detected at or Above Method Detection Limits
Samples from S&ME Progress Report #1 dated 10/22/2008
Recommendation:
Prepare HASP or work plan addressing potential soil impacts if observed during soil
work. This is to include proper PPE, containerization, disposal, monitoring, and other
areas as needed. If soil is to be imported or exported from the Brownfields Property,
DEQ Brownfields needs to be notified.
No additional assessment is necessary. Summary report should be sent to BF Program when the project is complete.
From:Ware, Todd
To:Minnich, Carolyn
Subject:[External] RE: Project # 12022-08-60
Date:Monday, March 05, 2018 10:22:59 AM
Attachments:image002.png
May 2010 Revised Redevelopment Plan Walmart #1666-04.pdf
June 24 2010 WM#1666 NCBP Letter.pdf
Approval Letter From Joe.pdf
CAUTION: External email. Do not click links or open attachments unless verified. Send all suspicious email as an
attachment to Report Spam.
Carolyn,

Counsel for WalMart reached out this morning to inform that the Redevelopment Plan they shared
with me last week, and I shared with you, was not the final version. The final version of the
Redevelopment Plan, a supplemental letter and DEQ’s approval letter are attached. Upon review of
the situation and information I have provided, please let me know what formal steps will be required
in connection with the drainage pipe replacement.

Thanks

Cameron Todd Ware, Partner
1065 East Morehead St. | Charlotte, NC 28204
P.O. Box 36469 | Charlotte, NC 28236
Phone: [phone] | Fax: [phone]
[e-mail] | My Profile | vCard | www.jahlaw.com
Member: Meritas Law Firms Worldwide
GENERAL NOTICE: This email (or any attachment) may contain privileged and confidential information
or other information that is protected under applicable law, and is intended solely for addressee. If not the
intended recipient, any reading, distribution, copying, or other use is prohibited. If received in error, please
call sender and delete. U.S. tax advice contained in this communication (or any attachment) is not
intended, and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code
or (ii) promoting to another party any transaction or matter. Unless expressly indicated herein, this
communication is not intended to be, nor shall it be deemed, an agreement or electronic signature.

From: Ware, Todd Sent: Friday, March 02, 2018 3:10 PMTo: '[e-mail]'Subject: Project # 12022-08-60

Carolyn,

Thanks for your time this afternoon and offer to assist on my client’s situation. Attached is the
WalMart Redevelopment Plan from 2010, which I have been told was approved by DENR. The Site
Location Map on page 13 is what I was looking at and referring to on our call. Also attached is an
easement exhibit document that shows the area of the easement rights being granted to my client,
with the actual pipe being located as shown in the center of the 40’ PDE. As mentioned, the work on
the brownfields property will be limited to excavating a trench along the existing 84” pipe to a
depth of 7- 18’, removing the existing pipe and replacing it with approximately 67 lf of new pipe on
the brownfields property, with the original material to be backfilled, and cleaning out the ditch
below the headwall. No exporting or importing of soil is planned. I have also attached plan sheets
that show existing conditions and the new drainage pipe. I will update my client and be back in
touch. Ideally, we would simply formally notify DEQ of our plans, which would not require any
analytical assessment or other formal action/approval.

Cameron Todd Ware, Partner
1065 East Morehead St. | Charlotte, NC 28204
P.O. Box 36469 | Charlotte, NC 28236
Phone: [phone] | Fax: [phone]
[e-mail] | My Profile | vCard | www.jahlaw.com
Member: Meritas Law Firms Worldwide
GENERAL NOTICE: This email (or any attachment) may contain privileged and confidential information
or other information that is protected under applicable law, and is intended solely for addressee. If not the
intended recipient, any reading, distribution, copying, or other use is prohibited. If received in error, please
call sender and delete. U.S. tax advice contained in this communication (or any attachment) is not
intended, and cannot be used, for the purpose of (i) avoiding penalties under the Internal Revenue Code
or (ii) promoting to another party any transaction or matter. Unless expressly indicated herein, this
communication is not intended to be, nor shall it be deemed, an agreement or electronic signature.

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Existing and ProposedMonitoring Well LocationsProposed Wal-Mart Store # 1666-04Charlotte, North Carolina31354-06-263HAS SHOWNCJF10.01.08JLBFIGURE NO.SCALE:PROJECT NO:DATE:DRAWN BY:CHECKED BY:WWW.SMEINC.COM!(Geoprobe, Shallow Well Locations (GP)
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Location of Former Pad-Mounted Tranformers
Streets
Buildings
Approximate Location of the Subject Property
REFERENCE: 2005 AERIAL PHOTOGRAPHS
THE GEOPROBE, SHALLOW WELL LOCATIONS, LOCATION OF TRANSFORMERS AND INTERMEDIATE DEPTH WELL LOCATIONS WERE FIELD LOCATED USING GPS UNITS CAPABLE OF SUB-
METER ACCURACY. THE PROPOSED WAL-MART LOCATION LAYER WAS DERIVED FROM A CAD DRAWING PROVIDED BY WAL-MART,INC. AERIAL PHOTOGRAPHS AND THE STREETS
COVERAGES WERE OBTAINED FROM THE MECKLENBURG COUNTY GIS DEPARTMENT. PLEASE NOTE THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. IT IS NOT MEANT FOR DESIGN,
LEGAL, OR ANY OTHER USES. THERE ARE NO GUARANTEES ABOUT ITS ACCURACY. S&ME, INC. ASSUMES NO RESPONSIBILITY FOR ANY DECISION MADE OR ANY ACTIONS TAKEN BY THE
USER BASED UPON THIS INFORMATION.
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Offices
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Building 2:
Haverty's Furniture
Haunted House
Highland Mills
Outlet Area
Former JAMCO
Famous Mart
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Former Burger King
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GP - 16
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Intermediate Depth Well (DMW)Status
!(Active/Proposed
!(Abandoned, Dry
!(Proposed Location of Bedrock Wells (BMW)
!U Approximate Monitoring Well/Existing Shallow Well Location (MW)
Proposed Wal-Mart Location
Location of Former Pad-Mounted Tranformers
Streets
Buildings
Approximate Location of the Subject Property
REFERENCE: 2005 AERIAL PHOTOGRAPHS
THE GEOPROBE, SHALLOW WELL LOCATIONS, LOCATION OF TRANSFORMERS AND INTERMEDIATE DEPTH WELL LOCATIONS WERE FIELD LOCATED USING GPS UNITS CAPABLE OF SUB-
METER ACCURACY. THE PROPOSED WAL-MART LOCATION LAYER WAS DERIVED FROM A CAD DRAWING PROVIDED BY WAL-MART,INC. AERIAL PHOTOGRAPHS AND THE STREETS
COVERAGES WERE OBTAINED FROM THE MECKLENBURG COUNTY GIS DEPARTMENT. PLEASE NOTE THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. IT IS NOT MEANT FOR DESIGN,
LEGAL, OR ANY OTHER USES. THERE ARE NO GUARANTEES ABOUT ITS ACCURACY. S&ME, INC. ASSUMES NO RESPONSIBILITY FOR ANY DECISION MADE OR ANY ACTIONS TAKEN BY THE
USER BASED UPON THIS INFORMATION.
0 100 200 300
Feet
±
Highland Mills
Warehouse Area
Building 5:
Antiques Consignments
Offices
Former Craftsman Quality Cleaners
1960-1985
See Figure 2A for Details
Building 2:
Haverty's Furniture
Haunted House
Highland Mills
Outlet Area
Former JAMCO
Famous Mart
Building 6:
KioskBuilding 3:
Former Burger King
Building 4: Bank
Harbor Freight
Check Into Cash
Beauty Salon
Amity Gardens Shopping CenterIndependence Boulevard and Pierson DriveCharlotte, North CarolinaSoil Sample IDSample DateSample Depth (ft bls)PCE TCE c-1,2 DCE t-1,2-DCE2-ButanoneEthyl-benzenep-isopropyl tolueneToluenebis(2-ethylhexyl) phthalateMethylene ChlorideArsenic Barium CadmiumChromium (Total)Lead Selenium Silver MercuryGP-159/29/2008 6 - 7 10.7 ND 7.8 ND ND ND ND ND ND ND 1000 12600 1200 13100 4200 3300 ND 9.8GP-159/29/2008 15 - 16 ND ND ND ND ND ND 48.9 ND ND ND 1000 50100 4500 31600 8300 2000 ND 24GP-169/29/2008 7 - 8 ND ND ND ND ND ND ND ND ND 71.1 ND 130000 7600 206000 6000 3900 670 NDGP-169/29/2008 11 - 12 ND ND ND ND ND ND ND ND 601 ND ND 97500 2800 48900 2400 1800 ND NDGP-179/30/2008 5 - 6 ND ND ND ND ND ND ND ND 565 27.8 ND 85000 5300 82300 3500 1600 ND 30GP-179/30/2008 22 - 23 ND ND ND ND ND ND ND ND ND ND ND 99900 2400 16600 3600 790 ND NDGP-189/30/2008 11 - 12 ND ND ND ND ND ND ND ND 488 ND 1800 6900 4400 17300 2200 4600 ND 11GP-189/30/2008 19 - 20 ND ND ND ND ND ND ND ND ND ND ND 69500 1300 14600 1600 2800 ND 6.8GP-1910/1/2008 11 - 12 ND ND ND ND ND ND ND ND ND ND ND 90400 7000 19100 3300 7300 ND NDGP-1910/1/2008 15 -16 ND ND ND ND ND ND ND ND ND ND ND 80100 5800 21900 2200 5600 ND NDGP-2010/1/2008 5.5 - 6.5 ND ND ND ND ND ND ND ND ND ND ND 75000 6400 42200 7400 7200 ND 15.0GP-2010/1/2008 15 - 16 ND ND ND ND ND ND ND ND ND ND ND 341000 5800 17500 3300 5000 ND NDGP-2110/1/2008 9.5 - 10.5 ND ND ND ND ND ND ND ND ND ND 560 56500 580 48300 540 1700 ND 69.0GP-2110/1/2008 31 - 32 ND ND ND ND ND ND ND ND ND ND ND 64200 1900 30600 980 ND ND NDGP-DUP (GP-19)10/1/2008 11 - 12 ND ND ND ND ND ND ND ND ND ND ND 78100 3100 11600 3600 6400 ND NDTrip Blank9/30/2008 NA ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA570 2800 160000 220000 5600000 5700 NS 930000 35000 11000 4400 3000000 14000 24000000 400000 78000 78000 1300GP Rinseate10/1/2008 NA ND ND ND ND 12.8 ND ND 1.3 ND ND NA NA NA NA NA NA NA NANotes: ●Results are reported in parts per billion. The soil data is in micrograms per kilogram and the rinsate data is in micrograms per liter.●ND : Not Detected at or Above Method Detection Limit●NA: No Analysis for this analyte●J = Estimated value between the Reporting Limit and Method Detection Limit.●PCE : Tetrachloroethene●TCE: Trichloroethene●c-1,2-DCE: cis-1,2-Dichloroethene●t-1,2-DCE: trans-1,2-Dichloroethene●1,1,-DCE: 1,1-Dichloroethene●NS : No Standard●IHSB: Inactive Hazardous Sites Branch●Samples were analyzed via EPA Method 8260B, 8270C, 6010D, and 7471.IHSB Health-Based Soil Remediation GoalsTable 1 (Continued)Summary of Geoprobe Soil Sample Analyses - Phase 4 ESAS&ME Project 1354-06-263H
Well IDSample Interval (ft)PCE TCE c-1,2 DCE t-1,2-DCE 1,1-DCEVinyl ChlorideBenzene Toluenep-isopropyl tolueneMethylene ChlorideChloroform BariumGP-15/MW514.9-24.9 ND ND 1.00 ND ND ND ND 2.5 2.2 ND ND 94.2GP-16/MW-610.0-20.0 ND ND ND ND ND ND5.45.4 ND ND ND 124GP-17/MW-719.4-29.4 ND ND ND ND ND ND ND 82.40 ND ND ND 45.5GP-18/MW-815.0-25.0 ND ND ND ND ND ND ND 30.00 ND ND ND 15.3Dup (GP-16/MW-6)NA ND ND ND ND ND ND2.803.80 ND ND ND 122GP-1910.4-20.4 ND ND ND ND ND ND ND 3.10 ND ND ND 13.3GP-2010.5-20.5 ND ND ND ND ND ND ND 4.70 ND ND 2.70 20Trip BlankNA ND ND ND ND ND ND ND ND ND ND ND NA0.7 2.8 70.0 100.0 7.0 0.015 1.0 1000.0 NS 4.6 70.02000.0Notes: ●All results are reported in micrograms per liter (ug/L). ●ND : Not Detected at or Above Method Detection Limit●NA : No Analysis for this Analyte●NS : No Standard for this Analyte●J = Estimated value between the Reporting Limit and Method Detection Limit.●PCE : Tetrachloroethene●TCE: Trichloroethene●c-1,2-DCE: cis-1,2-Dichloroethene●t-1,2-DCE: trans-1,2-Dichloroethene●Samples were analyzed via EPA Method 8260B, 8270C, 6010D, and 7471.15A NCAC 2L.0202 StandardsTable 2Summary of Shallow Well Groundwater Analysis Data - Phase 4 ESASample Collection Date: October 3, 2008Amity Gardens Shopping CenterIndependence Boulevard and Pierson DriveCharlotte, North CarolinaS&ME Project 1354-06-263H
ANALYTICAL RESULTS
Pace Project No.:
Project:
9228971
AMITY GARDENS/IND W-M
Sample:GP-16 (7-8)Lab ID:9228971003 Collected:09/29/08 16:20 Received:09/30/08 18:20 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 0.48 1 10/02/08 17:32 7440-38-210/02/08 10:550.31
Barium 130 mg/kg 0.48 1 10/02/08 17:32 7440-39-310/02/08 10:550.019
Cadmium 7.6 mg/kg 0.096 1 10/02/08 17:32 7440-43-910/02/08 10:550.058
Chromium 206 mg/kg 0.48 1 10/02/08 17:32 7440-47-310/02/08 10:550.029
Lead 6.0 mg/kg 0.48 1 10/02/08 17:32 7439-92-110/02/08 10:550.46
Selenium 3.9 mg/kg 0.96 1 10/02/08 17:32 7782-49-210/02/08 10:550.37
Silver 0.67 mg/kg 0.48 1 10/02/08 17:32 7440-22-410/02/08 10:550.029
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury ND mg/kg 0.0048 1 10/06/08 16:06 7439-97-610/03/08 10:150.000097
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 458 1 10/03/08 16:11 83-32-910/02/08 00:00106
Acenaphthylene ND ug/kg 458 1 10/03/08 16:11 208-96-810/02/08 00:00108
Aniline ND ug/kg 458 1 10/03/08 16:11 62-53-310/02/08 00:00124
Anthracene ND ug/kg 458 1 10/03/08 16:11 120-12-710/02/08 00:00103
Benzo(a)anthracene ND ug/kg 458 1 10/03/08 16:11 56-55-310/02/08 00:0084.7
Benzo(a)pyrene ND ug/kg 458 1 10/03/08 16:11 50-32-810/02/08 00:0087.5
Benzo(b)fluoranthene ND ug/kg 458 1 10/03/08 16:11 205-99-210/02/08 00:0079.2
Benzo(g,h,i)perylene ND ug/kg 458 1 10/03/08 16:11 191-24-210/02/08 00:00117
Benzo(k)fluoranthene ND ug/kg 458 1 10/03/08 16:11 207-08-910/02/08 00:0090.3
Benzoic acid ND ug/kg 2290 1 10/03/08 16:11 65-85-010/02/08 00:0083.3
Benzyl alcohol ND ug/kg 917 1 10/03/08 16:11 100-51-610/02/08 00:0091.7
4-Bromophenylphenyl ether ND ug/kg 458 1 10/03/08 16:11 101-55-310/02/08 00:0083.3
Butylbenzylphthalate ND ug/kg 458 1 10/03/08 16:11 85-68-710/02/08 00:0097.2
4-Chloro-3-methylphenol ND ug/kg 917 1 10/03/08 16:11 59-50-710/02/08 00:0094.4
4-Chloroaniline ND ug/kg 2290 1 10/03/08 16:11 106-47-810/02/08 00:00128
bis(2-Chloroethoxy)methane ND ug/kg 458 1 10/03/08 16:11 111-91-110/02/08 00:00107
bis(2-Chloroethyl) ether ND ug/kg 458 1 10/03/08 16:11 111-44-410/02/08 00:00117
bis(2-Chloroisopropyl) ether ND ug/kg 458 1 10/03/08 16:11 108-60-110/02/08 00:00122
2-Chloronaphthalene ND ug/kg 458 1 10/03/08 16:11 91-58-710/02/08 00:0090.3
2-Chlorophenol ND ug/kg 458 1 10/03/08 16:11 95-57-810/02/08 00:00125
4-Chlorophenylphenyl ether ND ug/kg 458 1 10/03/08 16:11 7005-72-310/02/08 00:0094.4
Chrysene ND ug/kg 458 1 10/03/08 16:11 218-01-910/02/08 00:0061.1
Dibenz(a,h)anthracene ND ug/kg 458 1 10/03/08 16:11 53-70-310/02/08 00:0097.2
Dibenzofuran ND ug/kg 458 1 10/03/08 16:11 132-64-910/02/08 00:0075.0
1,2-Dichlorobenzene ND ug/kg 458 1 10/03/08 16:11 95-50-110/02/08 00:00122
1,3-Dichlorobenzene ND ug/kg 458 1 10/03/08 16:11 541-73-110/02/08 00:00104
1,4-Dichlorobenzene ND ug/kg 458 1 10/03/08 16:11 106-46-710/02/08 00:00129
3,3'-Dichlorobenzidine ND ug/kg 2290 1 10/03/08 16:11 91-94-110/02/08 00:00100
2,4-Dichlorophenol ND ug/kg 458 1 10/03/08 16:11 120-83-210/02/08 00:00100
Diethylphthalate ND ug/kg 458 1 10/03/08 16:11 84-66-210/02/08 00:0070.8
2,4-Dimethylphenol ND ug/kg 458 1 10/03/08 16:11 105-67-910/02/08 00:00181
Dimethylphthalate ND ug/kg 458 1 10/03/08 16:11 131-11-310/02/08 00:0093.1
Di-n-butylphthalate ND ug/kg 458 1 10/03/08 16:11 84-74-210/02/08 00:0075.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/08/2008 03:13 PM Page 13 of 52
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9228971
AMITY GARDENS/IND W-M
Sample:GP-16 (7-8)Lab ID:9228971003 Collected:09/29/08 16:20 Received:09/30/08 18:20 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
4,6-Dinitro-2-methylphenol ND ug/kg 917 1 10/03/08 16:11 534-52-110/02/08 00:0091.7
2,4-Dinitrophenol ND ug/kg 2290 1 10/03/08 16:11 51-28-510/02/08 00:0075.0
2,4-Dinitrotoluene ND ug/kg 458 1 10/03/08 16:11 121-14-210/02/08 00:0086.1
2,6-Dinitrotoluene ND ug/kg 458 1 10/03/08 16:11 606-20-210/02/08 00:0095.8
Di-n-octylphthalate ND ug/kg 458 1 10/03/08 16:11 117-84-010/02/08 00:0095.8
1,2-Diphenylhydrazine ND ug/kg 458 1 10/03/08 16:11 122-66-710/02/08 00:0079.2
bis(2-Ethylhexyl)phthalate ND ug/kg 458 1 10/03/08 16:11 117-81-710/02/08 00:00125
Fluoranthene ND ug/kg 458 1 10/03/08 16:11 206-44-010/02/08 00:0066.7
Fluorene ND ug/kg 458 1 10/03/08 16:11 86-73-710/02/08 00:0094.4
Hexachloro-1,3-butadiene ND ug/kg 458 1 10/03/08 16:11 87-68-310/02/08 00:0079.2
Hexachlorobenzene ND ug/kg 458 1 10/03/08 16:11 118-74-110/02/08 00:0058.3
Hexachlorocyclopentadiene ND ug/kg 458 1 10/03/08 16:11 77-47-410/02/08 00:0084.7
Hexachloroethane ND ug/kg 458 1 10/03/08 16:11 67-72-110/02/08 00:00121
Indeno(1,2,3-cd)pyrene ND ug/kg 458 1 10/03/08 16:11 193-39-510/02/08 00:0094.4
Isophorone ND ug/kg 458 1 10/03/08 16:11 78-59-110/02/08 00:00103
1-Methylnaphthalene ND ug/kg 458 1 10/03/08 16:11 90-12-010/02/08 00:00119
2-Methylnaphthalene ND ug/kg 458 1 10/03/08 16:11 91-57-610/02/08 00:0098.6
2-Methylphenol(o-Cresol)ND ug/kg 458 1 10/03/08 16:11 95-48-710/02/08 00:00139
3&4-Methylphenol(m&p Cresol)ND ug/kg 458 1 10/03/08 16:1110/02/08 00:00181
Naphthalene ND ug/kg 458 1 10/03/08 16:11 91-20-310/02/08 00:00112
2-Nitroaniline ND ug/kg 2290 1 10/03/08 16:11 88-74-410/02/08 00:00142
3-Nitroaniline ND ug/kg 2290 1 10/03/08 16:11 99-09-210/02/08 00:00125
4-Nitroaniline ND ug/kg 917 1 10/03/08 16:11 100-01-610/02/08 00:00129
Nitrobenzene ND ug/kg 458 1 10/03/08 16:11 98-95-310/02/08 00:00125
2-Nitrophenol ND ug/kg 458 1 10/03/08 16:11 88-75-510/02/08 00:00111
4-Nitrophenol ND ug/kg 2290 1 10/03/08 16:11 100-02-710/02/08 00:0081.9
N-Nitrosodimethylamine ND ug/kg 458 1 10/03/08 16:11 62-75-910/02/08 00:00149
N-Nitroso-di-n-propylamine ND ug/kg 458 1 10/03/08 16:11 621-64-710/02/08 00:0087.5
N-Nitrosodiphenylamine ND ug/kg 458 1 10/03/08 16:11 86-30-610/02/08 00:00136
Pentachlorophenol ND ug/kg 2290 1 10/03/08 16:11 87-86-510/02/08 00:0083.3
Phenanthrene ND ug/kg 458 1 10/03/08 16:11 85-01-810/02/08 00:0076.4
Phenol ND ug/kg 458 1 10/03/08 16:11 108-95-210/02/08 00:00137
Pyrene ND ug/kg 458 1 10/03/08 16:11 129-00-010/02/08 00:0077.8
1,2,4-Trichlorobenzene ND ug/kg 458 1 10/03/08 16:11 120-82-110/02/08 00:0088.9
2,4,5-Trichlorophenol ND ug/kg 458 1 10/03/08 16:11 95-95-410/02/08 00:00142
2,4,6-Trichlorophenol ND ug/kg 458 1 10/03/08 16:11 88-06-210/02/08 00:00101
Nitrobenzene-d5 (S)46 %30-150 1 10/03/08 16:11 4165-60-010/02/08 00:00
2-Fluorobiphenyl (S)56 %46-120 1 10/03/08 16:11 321-60-810/02/08 00:00
Terphenyl-d14 (S)44 %38-108 1 10/03/08 16:11 1718-51-010/02/08 00:00
Phenol-d6 (S)50 %35-120 1 10/03/08 16:11 13127-88-310/02/08 00:00
2-Fluorophenol (S)48 %24-120 1 10/03/08 16:11 367-12-410/02/08 00:00
2,4,6-Tribromophenol (S)54 %44-136 1 10/03/08 16:11 118-79-610/02/08 00:00
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 105 1 10/03/08 19:10 67-64-110.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/08/2008 03:13 PM Page 14 of 52
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9228971
AMITY GARDENS/IND W-M
Sample:GP-16 (7-8)Lab ID:9228971003 Collected:09/29/08 16:20 Received:09/30/08 18:20 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Benzene ND ug/kg 5.3 1 10/03/08 19:10 71-43-21.7
Bromobenzene ND ug/kg 5.3 1 10/03/08 19:10 108-86-12.1
Bromochloromethane ND ug/kg 5.3 1 10/03/08 19:10 74-97-51.8
Bromodichloromethane ND ug/kg 5.3 1 10/03/08 19:10 75-27-42.0
Bromoform ND ug/kg 5.3 1 10/03/08 19:10 75-25-22.4
Bromomethane ND ug/kg 10.5 1 10/03/08 19:10 74-83-92.6
2-Butanone (MEK)ND ug/kg 105 1 10/03/08 19:10 78-93-33.1
n-Butylbenzene ND ug/kg 5.3 1 10/03/08 19:10 104-51-81.9
sec-Butylbenzene ND ug/kg 5.3 1 10/03/08 19:10 135-98-81.7
tert-Butylbenzene ND ug/kg 5.3 1 10/03/08 19:10 98-06-62.1
Carbon tetrachloride ND ug/kg 5.3 1 10/03/08 19:10 56-23-52.7
Chlorobenzene ND ug/kg 5.3 1 10/03/08 19:10 108-90-72.0
Chloroethane ND ug/kg 10.5 1 10/03/08 19:10 75-00-32.5
Chloroform ND ug/kg 5.3 1 10/03/08 19:10 67-66-31.7
Chloromethane ND ug/kg 10.5 1 10/03/08 19:10 74-87-32.5
2-Chlorotoluene ND ug/kg 5.3 1 10/03/08 19:10 95-49-81.8
4-Chlorotoluene ND ug/kg 5.3 1 10/03/08 19:10 106-43-41.9
1,2-Dibromo-3-chloropropane ND ug/kg 5.3 1 10/03/08 19:10 96-12-83.8
Dibromochloromethane ND ug/kg 5.3 1 10/03/08 19:10 124-48-11.9
1,2-Dibromoethane (EDB)ND ug/kg 5.3 1 10/03/08 19:10 106-93-41.9
Dibromomethane ND ug/kg 5.3 1 10/03/08 19:10 74-95-32.6
1,2-Dichlorobenzene ND ug/kg 5.3 1 10/03/08 19:10 95-50-12.0
1,3-Dichlorobenzene ND ug/kg 5.3 1 10/03/08 19:10 541-73-12.1
1,4-Dichlorobenzene ND ug/kg 5.3 1 10/03/08 19:10 106-46-71.8
Dichlorodifluoromethane ND ug/kg 10.5 1 10/03/08 19:10 75-71-83.8
1,1-Dichloroethane ND ug/kg 5.3 1 10/03/08 19:10 75-34-31.6
1,2-Dichloroethane ND ug/kg 5.3 1 10/03/08 19:10 107-06-22.3
1,1-Dichloroethene ND ug/kg 5.3 1 10/03/08 19:10 75-35-41.9
cis-1,2-Dichloroethene ND ug/kg 5.3 1 10/03/08 19:10 156-59-21.5
trans-1,2-Dichloroethene ND ug/kg 5.3 1 10/03/08 19:10 156-60-52.0
1,2-Dichloropropane ND ug/kg 5.3 1 10/03/08 19:10 78-87-51.8
1,3-Dichloropropane ND ug/kg 5.3 1 10/03/08 19:10 142-28-92.0
2,2-Dichloropropane ND ug/kg 5.3 1 10/03/08 19:10 594-20-71.8
1,1-Dichloropropene ND ug/kg 5.3 1 10/03/08 19:10 563-58-61.6
cis-1,3-Dichloropropene ND ug/kg 5.3 1 10/03/08 19:10 10061-01-51.9
trans-1,3-Dichloropropene ND ug/kg 5.3 1 10/03/08 19:10 10061-02-61.6
Diisopropyl ether ND ug/kg 5.3 1 10/03/08 19:10 108-20-31.8
Ethylbenzene ND ug/kg 5.3 1 10/03/08 19:10 100-41-41.9
Hexachloro-1,3-butadiene ND ug/kg 5.3 1 10/03/08 19:10 87-68-32.1
2-Hexanone ND ug/kg 52.7 1 10/03/08 19:10 591-78-64.1
Isopropylbenzene (Cumene)ND ug/kg 5.3 1 10/03/08 19:10 98-82-82.0
p-Isopropyltoluene ND ug/kg 5.3 1 10/03/08 19:10 99-87-61.8
Methylene Chloride 71.1 ug/kg 21.1 1 10/03/08 19:10 75-09-2 C93.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 52.7 1 10/03/08 19:10 108-10-13.9
Methyl-tert-butyl ether ND ug/kg 5.3 1 10/03/08 19:10 1634-04-41.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/08/2008 03:13 PM Page 15 of 52
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9228971
AMITY GARDENS/IND W-M
Sample:GP-16 (7-8)Lab ID:9228971003 Collected:09/29/08 16:20 Received:09/30/08 18:20 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260/5035A Volatile Organics Analytical Method: EPA 8260
Naphthalene ND ug/kg 5.3 1 10/03/08 19:10 91-20-31.3
n-Propylbenzene ND ug/kg 5.3 1 10/03/08 19:10 103-65-11.8
Styrene ND ug/kg 5.3 1 10/03/08 19:10 100-42-51.9
1,1,1,2-Tetrachloroethane ND ug/kg 5.3 1 10/03/08 19:10 630-20-62.2
1,1,2,2-Tetrachloroethane ND ug/kg 5.3 1 10/03/08 19:10 79-34-52.0
Tetrachloroethene ND ug/kg 5.3 1 10/03/08 19:10 127-18-41.8
Toluene ND ug/kg 5.3 1 10/03/08 19:10 108-88-31.9
1,2,3-Trichlorobenzene ND ug/kg 5.3 1 10/03/08 19:10 87-61-62.3
1,2,4-Trichlorobenzene ND ug/kg 5.3 1 10/03/08 19:10 120-82-11.7
1,1,1-Trichloroethane ND ug/kg 5.3 1 10/03/08 19:10 71-55-61.9
1,1,2-Trichloroethane ND ug/kg 5.3 1 10/03/08 19:10 79-00-52.2
Trichloroethene ND ug/kg 5.3 1 10/03/08 19:10 79-01-62.2
Trichlorofluoromethane ND ug/kg 5.3 1 10/03/08 19:10 75-69-42.3
1,2,3-Trichloropropane ND ug/kg 5.3 1 10/03/08 19:10 96-18-41.7
1,2,4-Trimethylbenzene ND ug/kg 5.3 1 10/03/08 19:10 95-63-62.1
1,3,5-Trimethylbenzene ND ug/kg 5.3 1 10/03/08 19:10 108-67-81.9
Vinyl acetate ND ug/kg 52.7 1 10/03/08 19:10 108-05-49.3
Vinyl chloride ND ug/kg 10.5 1 10/03/08 19:10 75-01-41.9
Xylene (Total)ND ug/kg 10.5 1 10/03/08 19:10 1330-20-73.8
m&p-Xylene ND ug/kg 10.5 1 10/03/08 19:10 1330-20-73.8
o-Xylene ND ug/kg 5.3 1 10/03/08 19:10 95-47-62.0
Dibromofluoromethane (S)106 %79-116 1 10/03/08 19:10 1868-53-7
Toluene-d8 (S)116 %88-110 1 10/03/08 19:10 2037-26-5 S6
4-Bromofluorobenzene (S)106 %74-115 1 10/03/08 19:10 460-00-4
1,2-Dichloroethane-d4 (S)111 %69-121 1 10/03/08 19:10 17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 28.0 %0.10 1 10/02/08 14:550.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/08/2008 03:13 PM Page 16 of 52
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9229300
AMITY GARDONS/ IND. WAY
Sample:GP-16 Lab ID:9229300002 Collected:10/03/08 14:25 Received:10/03/08 16:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6010 MET ICP, Lab Filtered Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic ND ug/L 5.0 1 10/06/08 21:43 7440-38-210/06/08 14:092.7
Barium 124 ug/L 5.0 1 10/06/08 21:43 7440-39-310/06/08 14:090.20
Cadmium ND ug/L 1.0 1 10/06/08 21:43 7440-43-910/06/08 14:090.50
Chromium ND ug/L 5.0 1 10/06/08 21:43 7440-47-310/06/08 14:090.40
Lead ND ug/L 5.0 1 10/06/08 21:43 7439-92-110/06/08 14:094.0
Selenium ND ug/L 10.0 1 10/06/08 21:43 7782-49-210/06/08 14:093.8
Silver ND ug/L 5.0 1 10/06/08 21:43 7440-22-410/06/08 14:090.10
7470 Mercury, Lab Filtered Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury ND ug/L 0.20 1 10/08/08 16:53 7439-97-610/08/08 11:000.090
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene ND ug/L 11.1 1 10/10/08 18:41 83-32-910/08/08 00:003.1
Acenaphthylene ND ug/L 11.1 1 10/10/08 18:41 208-96-810/08/08 00:003.1
Aniline ND ug/L 11.1 1 10/10/08 18:41 62-53-310/08/08 00:005.7
Anthracene ND ug/L 11.1 1 10/10/08 18:41 120-12-710/08/08 00:003.2
Benzo(a)anthracene ND ug/L 11.1 1 10/10/08 18:41 56-55-310/08/08 00:003.1
Benzo(a)pyrene ND ug/L 11.1 1 10/10/08 18:41 50-32-810/08/08 00:003.4
Benzo(b)fluoranthene ND ug/L 11.1 1 10/10/08 18:41 205-99-210/08/08 00:004.0
Benzo(g,h,i)perylene ND ug/L 11.1 1 10/10/08 18:41 191-24-210/08/08 00:003.4
Benzo(k)fluoranthene ND ug/L 11.1 1 10/10/08 18:41 207-08-910/08/08 00:003.3
Benzoic acid ND ug/L 55.6 1 10/10/08 18:41 65-85-010/08/08 00:0055.6
Benzyl alcohol ND ug/L 22.2 1 10/10/08 18:41 100-51-610/08/08 00:004.0
4-Bromophenylphenyl ether ND ug/L 11.1 1 10/10/08 18:41 101-55-310/08/08 00:002.7
Butylbenzylphthalate ND ug/L 11.1 1 10/10/08 18:41 85-68-710/08/08 00:003.2
4-Chloro-3-methylphenol ND ug/L 22.2 1 10/10/08 18:41 59-50-710/08/08 00:003.1
4-Chloroaniline ND ug/L 55.6 1 10/10/08 18:41 106-47-810/08/08 00:005.9
bis(2-Chloroethoxy)methane ND ug/L 11.1 1 10/10/08 18:41 111-91-110/08/08 00:006.4
bis(2-Chloroethyl) ether ND ug/L 11.1 1 10/10/08 18:41 111-44-410/08/08 00:005.3
bis(2-Chloroisopropyl) ether ND ug/L 11.1 1 10/10/08 18:41 108-60-110/08/08 00:004.4
2-Chloronaphthalene ND ug/L 11.1 1 10/10/08 18:41 91-58-710/08/08 00:004.0
2-Chlorophenol ND ug/L 11.1 1 10/10/08 18:41 95-57-810/08/08 00:004.9
4-Chlorophenylphenyl ether ND ug/L 11.1 1 10/10/08 18:41 7005-72-310/08/08 00:003.0
Chrysene ND ug/L 11.1 1 10/10/08 18:41 218-01-910/08/08 00:003.0
Dibenz(a,h)anthracene ND ug/L 11.1 1 10/10/08 18:41 53-70-310/08/08 00:003.2
Dibenzofuran ND ug/L 11.1 1 10/10/08 18:41 132-64-910/08/08 00:002.9
1,2-Dichlorobenzene ND ug/L 11.1 1 10/10/08 18:41 95-50-110/08/08 00:003.8
1,3-Dichlorobenzene ND ug/L 11.1 1 10/10/08 18:41 541-73-110/08/08 00:003.7
1,4-Dichlorobenzene ND ug/L 11.1 1 10/10/08 18:41 106-46-710/08/08 00:004.0
3,3'-Dichlorobenzidine ND ug/L 55.6 1 10/10/08 18:41 91-94-110/08/08 00:003.8
2,4-Dichlorophenol ND ug/L 11.1 1 10/10/08 18:41 120-83-210/08/08 00:006.4
Diethylphthalate ND ug/L 11.1 1 10/10/08 18:41 84-66-210/08/08 00:002.7
2,4-Dimethylphenol ND ug/L 11.1 1 10/10/08 18:41 105-67-910/08/08 00:006.2
Dimethylphthalate ND ug/L 11.1 1 10/10/08 18:41 131-11-310/08/08 00:002.7
Di-n-butylphthalate ND ug/L 11.1 1 10/10/08 18:41 84-74-210/08/08 00:003.2
4,6-Dinitro-2-methylphenol ND ug/L 22.2 1 10/10/08 18:41 534-52-110/08/08 00:008.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/13/2008 02:26 PM Page 9 of 43
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9229300
AMITY GARDONS/ IND. WAY
Sample:GP-16 Lab ID:9229300002 Collected:10/03/08 14:25 Received:10/03/08 16:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
2,4-Dinitrophenol ND ug/L 55.6 1 10/10/08 18:41 51-28-510/08/08 00:0011.1
2,4-Dinitrotoluene ND ug/L 11.1 1 10/10/08 18:41 121-14-210/08/08 00:002.9
2,6-Dinitrotoluene ND ug/L 11.1 1 10/10/08 18:41 606-20-210/08/08 00:003.1
Di-n-octylphthalate ND ug/L 11.1 1 10/10/08 18:41 117-84-010/08/08 00:003.2
1,2-Diphenylhydrazine ND ug/L 11.1 1 10/10/08 18:41 122-66-710/08/08 00:002.4
bis(2-Ethylhexyl)phthalate ND ug/L 11.1 1 10/10/08 18:41 117-81-710/08/08 00:002.3
Fluoranthene ND ug/L 11.1 1 10/10/08 18:41 206-44-010/08/08 00:003.2
Fluorene ND ug/L 11.1 1 10/10/08 18:41 86-73-710/08/08 00:002.9
Hexachloro-1,3-butadiene ND ug/L 11.1 1 10/10/08 18:41 87-68-310/08/08 00:003.7
Hexachlorobenzene ND ug/L 11.1 1 10/10/08 18:41 118-74-110/08/08 00:002.9
Hexachlorocyclopentadiene ND ug/L 11.1 1 10/10/08 18:41 77-47-410/08/08 00:004.1
Hexachloroethane ND ug/L 11.1 1 10/10/08 18:41 67-72-110/08/08 00:003.7
Indeno(1,2,3-cd)pyrene ND ug/L 11.1 1 10/10/08 18:41 193-39-510/08/08 00:003.3
Isophorone ND ug/L 11.1 1 10/10/08 18:41 78-59-110/08/08 00:007.2
1-Methylnaphthalene ND ug/L 11.1 1 10/10/08 18:41 90-12-010/08/08 00:004.0
2-Methylnaphthalene ND ug/L 11.1 1 10/10/08 18:41 91-57-610/08/08 00:003.8
2-Methylphenol(o-Cresol)ND ug/L 11.1 1 10/10/08 18:41 95-48-710/08/08 00:004.1
3&4-Methylphenol(m&p Cresol)ND ug/L 11.1 1 10/10/08 18:4110/08/08 00:003.3
Naphthalene ND ug/L 11.1 1 10/10/08 18:41 91-20-310/08/08 00:004.2
2-Nitroaniline ND ug/L 55.6 1 10/10/08 18:41 88-74-410/08/08 00:003.0
3-Nitroaniline ND ug/L 55.6 1 10/10/08 18:41 99-09-210/08/08 00:003.3
4-Nitroaniline ND ug/L 55.6 1 10/10/08 18:41 100-01-610/08/08 00:004.4
Nitrobenzene ND ug/L 11.1 1 10/10/08 18:41 98-95-310/08/08 00:004.9
2-Nitrophenol ND ug/L 11.1 1 10/10/08 18:41 88-75-510/08/08 00:005.1
4-Nitrophenol ND ug/L 55.6 1 10/10/08 18:41 100-02-710/08/08 00:002.0
N-Nitrosodimethylamine ND ug/L 11.1 1 10/10/08 18:41 62-75-910/08/08 00:003.4
N-Nitroso-di-n-propylamine ND ug/L 11.1 1 10/10/08 18:41 621-64-710/08/08 00:004.1
N-Nitrosodiphenylamine ND ug/L 11.1 1 10/10/08 18:41 86-30-610/08/08 00:007.3
Pentachlorophenol ND ug/L 55.6 1 10/10/08 18:41 87-86-510/08/08 00:001.8
Phenanthrene ND ug/L 11.1 1 10/10/08 18:41 85-01-810/08/08 00:003.0
Phenol ND ug/L 11.1 1 10/10/08 18:41 108-95-210/08/08 00:002.0
Pyrene ND ug/L 11.1 1 10/10/08 18:41 129-00-010/08/08 00:003.2
1,2,4-Trichlorobenzene ND ug/L 11.1 1 10/10/08 18:41 120-82-110/08/08 00:003.8
2,4,5-Trichlorophenol ND ug/L 11.1 1 10/10/08 18:41 95-95-410/08/08 00:006.2
2,4,6-Trichlorophenol ND ug/L 11.1 1 10/10/08 18:41 88-06-210/08/08 00:006.8
Nitrobenzene-d5 (S)78 %30-150 1 10/10/08 18:41 4165-60-010/08/08 00:00
2-Fluorobiphenyl (S)90 %30-150 1 10/10/08 18:41 321-60-810/08/08 00:00
Terphenyl-d14 (S)96 %30-150 1 10/10/08 18:41 1718-51-010/08/08 00:00
Phenol-d6 (S)33 %25-150 1 10/10/08 18:41 13127-88-310/08/08 00:00
2-Fluorophenol (S)44 %25-150 1 10/10/08 18:41 367-12-410/08/08 00:00
2,4,6-Tribromophenol (S)89 %25-150 1 10/10/08 18:41 118-79-610/08/08 00:00
8260 MSV Low Level Analytical Method: EPA 8260
Acetone ND ug/L 25.0 1 10/04/08 15:23 67-64-12.2
Benzene 5.4 ug/L 1.0 1 10/04/08 15:23 71-43-20.25
Bromobenzene ND ug/L 1.0 1 10/04/08 15:23 108-86-10.30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/13/2008 02:26 PM Page 10 of 43
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9229300
AMITY GARDONS/ IND. WAY
Sample:GP-16 Lab ID:9229300002 Collected:10/03/08 14:25 Received:10/03/08 16:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Analytical Method: EPA 8260
Bromochloromethane ND ug/L 1.0 1 10/04/08 15:23 74-97-50.17
Bromodichloromethane ND ug/L 1.0 1 10/04/08 15:23 75-27-40.18
Bromoform ND ug/L 1.0 1 10/04/08 15:23 75-25-20.26
Bromomethane ND ug/L 5.0 1 10/04/08 15:23 74-83-90.29
2-Butanone (MEK)ND ug/L 5.0 1 10/04/08 15:23 78-93-30.96
Carbon tetrachloride ND ug/L 1.0 1 10/04/08 15:23 56-23-50.25
Chlorobenzene ND ug/L 1.0 1 10/04/08 15:23 108-90-70.23
Chloroethane ND ug/L 1.0 1 10/04/08 15:23 75-00-30.54
Chloroform ND ug/L 1.0 1 10/04/08 15:23 67-66-30.14
Chloromethane ND ug/L 1.0 1 10/04/08 15:23 74-87-30.11
2-Chlorotoluene ND ug/L 1.0 1 10/04/08 15:23 95-49-80.35
4-Chlorotoluene ND ug/L 1.0 1 10/04/08 15:23 106-43-40.31
1,2-Dibromo-3-chloropropane ND ug/L 3.0 1 10/04/08 15:23 96-12-82.5
Dibromochloromethane ND ug/L 1.0 1 10/04/08 15:23 124-48-10.21
1,2-Dibromoethane (EDB)ND ug/L 1.0 1 10/04/08 15:23 106-93-40.27
Dibromomethane ND ug/L 1.0 1 10/04/08 15:23 74-95-30.21
1,2-Dichlorobenzene ND ug/L 1.0 1 10/04/08 15:23 95-50-10.30
1,3-Dichlorobenzene ND ug/L 1.0 1 10/04/08 15:23 541-73-10.24
1,4-Dichlorobenzene ND ug/L 1.0 1 10/04/08 15:23 106-46-70.33
Dichlorodifluoromethane ND ug/L 1.0 1 10/04/08 15:23 75-71-80.21
1,1-Dichloroethane ND ug/L 1.0 1 10/04/08 15:23 75-34-30.32
1,2-Dichloroethane ND ug/L 1.0 1 10/04/08 15:23 107-06-20.12
1,1-Dichloroethene ND ug/L 1.0 1 10/04/08 15:23 75-35-40.56
cis-1,2-Dichloroethene ND ug/L 1.0 1 10/04/08 15:23 156-59-20.19
trans-1,2-Dichloroethene ND ug/L 1.0 1 10/04/08 15:23 156-60-50.49
1,2-Dichloropropane ND ug/L 1.0 1 10/04/08 15:23 78-87-50.27
1,3-Dichloropropane ND ug/L 1.0 1 10/04/08 15:23 142-28-90.28
2,2-Dichloropropane ND ug/L 1.0 1 10/04/08 15:23 594-20-70.13
1,1-Dichloropropene ND ug/L 1.0 1 10/04/08 15:23 563-58-60.49
cis-1,3-Dichloropropene ND ug/L 1.0 1 10/04/08 15:23 10061-01-50.13
trans-1,3-Dichloropropene ND ug/L 1.0 1 10/04/08 15:23 10061-02-60.26
Diisopropyl ether ND ug/L 1.0 1 10/04/08 15:23 108-20-30.12
Ethylbenzene ND ug/L 1.0 1 10/04/08 15:23 100-41-40.30
Hexachloro-1,3-butadiene ND ug/L 1.0 1 10/04/08 15:23 87-68-30.71
2-Hexanone ND ug/L 5.0 1 10/04/08 15:23 591-78-60.46
p-Isopropyltoluene ND ug/L 1.0 1 10/04/08 15:23 99-87-60.31
Methylene Chloride ND ug/L 2.0 1 10/04/08 15:23 75-09-20.97
4-Methyl-2-pentanone (MIBK)ND ug/L 5.0 1 10/04/08 15:23 108-10-10.33
Methyl-tert-butyl ether ND ug/L 1.0 1 10/04/08 15:23 1634-04-40.21
Naphthalene ND ug/L 1.0 1 10/04/08 15:23 91-20-30.24
Styrene ND ug/L 1.0 1 10/04/08 15:23 100-42-50.26
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 10/04/08 15:23 630-20-60.33
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 10/04/08 15:23 79-34-50.40
Tetrachloroethene ND ug/L 1.0 1 10/04/08 15:23 127-18-40.46
Toluene 5.4 ug/L 1.0 1 10/04/08 15:23 108-88-30.26
1,2,3-Trichlorobenzene ND ug/L 1.0 1 10/04/08 15:23 87-61-60.33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/13/2008 02:26 PM Page 11 of 43
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9229300
AMITY GARDONS/ IND. WAY
Sample:GP-16 Lab ID:9229300002 Collected:10/03/08 14:25 Received:10/03/08 16:48 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
8260 MSV Low Level Analytical Method: EPA 8260
1,2,4-Trichlorobenzene ND ug/L 1.0 1 10/04/08 15:23 120-82-10.35
1,1,1-Trichloroethane ND ug/L 1.0 1 10/04/08 15:23 71-55-60.48
1,1,2-Trichloroethane ND ug/L 1.0 1 10/04/08 15:23 79-00-50.29
Trichloroethene ND ug/L 1.0 1 10/04/08 15:23 79-01-60.47
Trichlorofluoromethane ND ug/L 1.0 1 10/04/08 15:23 75-69-40.20
1,2,3-Trichloropropane ND ug/L 1.0 1 10/04/08 15:23 96-18-40.41
Vinyl acetate ND ug/L 2.0 1 10/04/08 15:23 108-05-40.35
Vinyl chloride ND ug/L 1.0 1 10/04/08 15:23 75-01-40.62
m&p-Xylene ND ug/L 2.0 1 10/04/08 15:23 1330-20-70.66
o-Xylene ND ug/L 1.0 1 10/04/08 15:23 95-47-60.23
4-Bromofluorobenzene (S)103 %87-109 1 10/04/08 15:23 460-00-4
Dibromofluoromethane (S)99 %85-115 1 10/04/08 15:23 1868-53-7
1,2-Dichloroethane-d4 (S)99 %79-120 1 10/04/08 15:23 17060-07-0
Toluene-d8 (S)101 %70-120 1 10/04/08 15:23 2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/13/2008 02:26 PM Page 12 of 43
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]