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Home My WebLink About16041 Fleming Lab SSD Install Report 20171108 Via Email November 8, 2017 NC DEQ - Brownfields Program 1646 Mail Service Center Raleigh, NC 27699-1646 Attention: Ms. Carolyn Minnich Re: Sub-Slab Depressurization System Installation Fleming Laboratories Charlotte, North Carolina Brownfields Project #16041-12-060 H&H Project No. FMG-005 Dear Carolyn: 1.0 Introduction Hart & Hickman, PC (H&H) is providing this letter report documenting Sub-Slab Depressurization (SSD) System installation activities at the Fleming Laboratories site (Brownfields # 16041-12- 060) located at 2215 Thrift Road in Charlotte, North Carolina. A site location map is included as Figure 1. In July 2016, H&H conducted sub-slab vapor sampling activities at the site to further evaluate the potential for vapor intrusion from groundwater impacts identified during assessment activities conducted in April 2016. The results the sub-slab vapor sampling indicated concentrations of chloroform, 1,1-dichloroethane, 1,1-dichloroethylene, tetrachloroethylene (PCE), and trichloroethylene (TCE) above their respective North Carolina Division of Waste Management (DWM) Non-Residential Soil Gas Screening Levels (SGSLs). Indoor air samples were collected on September 13, 2016 in accordance with the approved August 31, 2016 Indoor Air Sampling Work Plan, Revision 1. Chlorinated volatile organic compounds exceeded industrial screening levels in air samples collected. During an October 4, 2016 North Ms. Carolyn Minnich November 8, 2017 Page 2 S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-005 SSD Installation\SSD Install Report\SSD Install Report.docx Carolina Department of Environmental Quality (DEQ) conference call to discuss these data, it was determined that although there are no women of child bearing age in the facility, a SSD system was warranted. On October 14, 2016, Shaw’s Home Maintenance and Radon Testing & Mitigation performed communication testing to assist in preparing a SSD system design. Tight soils immediately below the building slab resulted in poor results during the first communication test. As a result, a second more detailed SSD communication test was performed on January 10, 2017 by Clean Vapor, LLC (Clean Vapor). The second SSD communication test was conducted after they performed floor sealing activities on December 26 through 28, 2016. The purpose of the floor sealing was to reduce the presence of preferential pathways in the slab of the building which could act as a potential conduit for subsurface vapor. To seal the potential preferential pathways in the slab, Clean Vapor applied Vulkem 116 (a polyurethane sealant) to expansion joints, cracks, and gaps identified in the facility. Backer rod was used to bridge large gaps such as where the slab floor met the perimeter wall. With the floor sealing and results of the Clean Vapor communication test, it was determined that SSD could be used to mitigate vapor intrusion at this site. On April 26, 2017, H&H submitted the initial Sub-Slab Depressurization Design work plan to DEQ for approval. Following DEQ comments regarding the initial design, a Revised Sub-Slab Depressurization Design was resubmitted to DEQ on May 18, 2017 which was approved by DEQ the same day. As agreed to in a May 18, 2017 email, the proposed SSD system was designed to apply a minimum cold weather vacuum of 0.008 inches water column (“WC) or 2 Pascals under the building slab to prevent vapor intrusion into the facility. Vacuum confirmation would be performed by measuring differential pressure at four sub-slab Cox-Colvin Vapor Pins® (vapor pins) previously installed by H&H during July 2016 sub-slab vapor sampling activities (Figure 2). Ms. Carolyn Minnich November 8, 2017 Page 3 S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-005 SSD Installation\SSD Install Report\SSD Install Report.docx 2.0 SSD System Installation Clean Vapor performed SSD system installation activities between June 29, 2017 and August 17, 2017. Following utility locating by Ground Penetrating Radar Systems Inc., 24 sub-slab suction points were installed within the facility building and manifolded together into four separate suction “fields”. Each of the suction points with the exception of SP4-5 (located inside the office portion of the building) were constructed of 2-inch and 3-inch diameter steel piping for protection from potential forklift impacts. Suction point SP4-5 was constructed of 3-inch diameter schedule 40 PVC pipe due to its location inside the office portion of the facility. Each suction field was then connected to a separate SSD blower mounted on the roof of the facility (Figure 3, Appendix A). Based on results of the January 20, 2017 communication testing performed by Clean Vapor, two types of blowers were used on the SSD system. Communication test results indicated soils around the perimeter of the building were more permeable and capable of a relatively high airflow. The soils under the center sections of the building were tighter and required fans capable of a higher vacuum. For the building perimeter suction points (Fields 1 and 4), Cincinnati PB-14A fans capable of 550 CFM @ 12” water column (“WC) were used. Vapor Dynamics IC 4519 compact radial blowers capable of 50 CFM @ 37 “WC were used for the less permeable interior suction Fields 2 and 3. Air flow from the suction fields and individual points can be controlled by varying the speed of the blowers (using variable frequency drives for the Cincinnati fans, and motor settings on the Vapor Dynamics radial blowers), and slide valves installed on each of the individual suction points. Applied vacuum on each of the four fields is displayed on one of four Magnahelic gauges mounted on the SSD system control panel in the northwestern corner of the facility. Vacuum sensors are installed on each suction field and are set to 0.25 “WC. In the event that any of the suction field vacuums drop below the 0.25 “WC set point (as a result of a blower or power failure), two red Ms. Carolyn Minnich November 8, 2017 Page 4 S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-005 SSD Installation\SSD Install Report\SSD Install Report.docx alarm lights will illuminate. One alarm light is installed on the same panel as the Magnahelic gauges which are mounted on the on the SSD control panel. The other alarm light is located inside the warehouse next to the southern office door (Figure 3). In addition, a Sensaphone 400 auto dialer mounted on the system panel is programed to contact Clean Vapor, Fleming Labs and H&H personnel in the event a loss of vacuum is detected. In the event of a power failure, all four fans are wired to automatically restart once power is restored. A more detailed description of the piping, blowers, controllers, gauges, switches and other system components is contained in Clean Vapors Report of Vapor Intrusion Mitigation located in Appendix B. 3.0 SSD System Start-up and Balancing On the afternoon of August 16, 2017, the SSD system was initially started, with final system balancing completed on August 17, 2017. Initially, all four blowers were operated at 100% of their capacity. However, with vacuum readings at the four permanent vapor pins and ten temporary test ports ranging from 2.26 to 15.9 “WC, it was determined that blower speeds could be reduced to save energy costs. A reduction in blower speed increases the longevity of the blower motors and decreases the electrical load (and thereby the electrical costs) required to operate the SSD system. Following system balancing on August 17, 2017, blower vacuums ranged from 1.21 to 3.40 ”WC, and vacuum on the 24 suction points ranged from 0.93 to 4.89 ”WC (Appendix B). On August 23, 2017, H&H personnel returned to the site to record sub-slab vapor pin vacuum readings following one week of system operation. Vapor pin vacuums ranged from 0.88 ”WC (SS-3), to 3.50 ”WC (SS-2). H&H personnel again returned to the site on September 25, 2017 (approximately one month after system start-up) and recorded vacuum readings at the four vapor pins. Vapor pin vacuums ranged from 0.91 ”WC (SS-3) to 3.40 ”WC (SS-2). These readings exceed the required 0.008 “WC vacuum requirement by two orders of magnitude. H&H vapor pin vacuum readings are provided in Table 1. Ms. Carolyn Minnich November 8, 2017 Page 5 S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-005 SSD Installation\SSD Install Report\SSD Install Report.docx 4.0 Investigation-Derived Waste Approximately 1 cubic foot of gravel mixed with soil was removed from each of the 24 suction points to maximize sub-slab air flow and vacuum propagation. The excavated material was placed into three 55 gallon drums as it was being removed. Following suction point completion, approximately 2.5 drums of investigation-derived waste (IDW) were generated. On July 27, 2017, H&H personnel collected a composite sample for waste disposal purposes. The composite sample was placed in laboratory supplied containers, marked with identifying labels, and placed in an iced cooler for shipment under chain-of-custody to a certified laboratory for analysis. The composite sample was then analyzed for volatile organic compounds (VOCs) by Environmental Protection Agency (EPA) Method 8260B, semi-volatile organic compounds (SVOCs) by EPA Method 8270D, RCRA Metals (EPA Method 6010D/7471B), Toxicity Characteristic Leaching Procedure (TCLP) VOCs by EPA SW-846 Method 1311/8260B, and TCLP RCRA Metals (EPA Method 6010D/7470A). Laboratory results for the IDW composite sample are contained in Appendix C. The results were within RCRA characteristically hazardous waste thresholds. Therefore, H&H arranged for EVO Corporation to remove and dispose of the IDW as a non-hazardous waste. Drum removal and disposal at a permitted facility was performed on August 29, 2017. The Waste Profile, Non-Hazardous Waste Manifest and Certificate of Disposal for the IDW are contained in Appendix D. 5.0 Summary and Conclusions The SSD system is operating as designed and meeting the design criteria of 0.008 “WC vacuum at each of the four permanent sub-slab vapor pins. The sub-slab vacuum readings exceed the required vacuum by two orders of magnitude. Vapor pin vacuum readings will be repeated during Table 1 Summary of Vapor Pin Vacuum Readings Fleming Laboratories Charlotte, North Carolina H&H Job No. FMG-005 Vapor Pin Location 8/16/2017 8/23/2017 9/25/2017 SS-1 7.86 1.55 1.50 SS-2 15.9 3.50 3.40 SS-3 4.87 0.88 0.91 SS-4 8.38 1.80 1.80 Notes: 1. Vapor Pin target vacuum = 0.008 "WC or greater (per May 11, 2017 DEQ agreement). 2. August 16, 2017 vacuum readings taken prior to August 17, 2017 final system balancing. Vacuum in Inches of Water Column ("WC) S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-005 SSD Installation\SSD Install Report\Table 1 Table 1 (Page 1 of 1) Hart & Hickman, PC SITE 0 2000 4000 APPROXIMATE SCALE IN FEET N U.S.G.S. QUADRANGLE MAPS QUADRANGLE 7.5 MINUTE SERIES (TOPOGRAPHIC) TITLE PROJECT SITE LOCATION MAP FLEMING LABORATORIES CHARLOTTE, NORTH CAROLINA DATE: JOB NO: REVISION NO: FIGURE: 10-10-17 0 1FMG-005 Charlotte East, North Carolina, 1988 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) THR IF T RO AD JAY S T R E E T GRAVEL PARKING SS-4 SS-3 SS-2 SS-1 FLEMING (OPERATING) JOB NO. FMG-005 REVISION NO. 0DATE: 10-10-16 FIGURE NO. 2 LEGEND SUBJECT PROPERTY BOUNDARY SUB-SLAB VAPOR PIN LOCATION FLEMING LABORATORIES 2215 THRIFT ROAD CHARLOTTE, NORTH CAROLINA SUB-SLAB VAPOR SAMPLE LOCATION MAP 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) License # C-1269 / #C-245 Geology S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-005 SSD Installation\SSD Install Report\Figures\Figures.dwg, FIG 1, 11/8/2017 1:08:23 PM, 4" PVC4" PVC3" PVC 4" PVC 4" PVC6" PVC 4" PVC4" PVC3" EMT PIPE4" PVC3" PVC3" PVC4" PVC6" PVC4" PVC3" PVC4" PVC3" PVC 4" PVC 4" PVC 3" PVC 4" PVC 3" PVC3" PVC3" PVCTP-3 TP-4 TP-5 TP-6 TP-2 TP-1 TP-9 TP-10 TP-7 TP-8 SS-3 SS-2 SS-4 SS-1 6" PVC UP VTR SYSTEM 1 PB14A BLOWER INSTALLED ON ROOF ABOVE SYSTEM 3 IC45-19 BLOWER INSTALLED ON ROOF ABOVE SYSTEM 4 PB14A BLOWER INSTALLED ON ROOF ABOVE SYSTEM 2 IC45-19 BLOWER INSTALLED ON ROOF ABOVE 6" PVC UP VTR 4" PVC UP VTR (TYP. OF 2) LOW VACUUM ALARM LIGHT LOW VACUUM ALARM LIGHT SSD CONTROL PANEL SP1-6 SP1-1 SP1-2 SP1-3 SP1-4 SP1-5 SP4-1 SP4-2 SP4-3 SP4-4 SP4-5 SP3-6 SP3-5 SP4-6 SP3-2 SP4-7 SP3-1 SP3-3 SP3-4 SP2-5 SP2-4 SP2-3 SP2-2 SP2-1 REVISION NO. 0 JOB NO. FMG-005 DATE: 10-12-17 FIGURE NO. 3 FLEMING LABORATORIES 2215 THRIFT ROAD CHARLOTTE, NORTH CAROLINA SUB-SLAB DEPRESSURIZATION SYSTEM LAYOUT - AS BUILT LEGEND SUCTION POINT TEMPORARY TEST POINT SUB-SLAB VAPOR PIN MONITORING PANEL SENSAPHONE CINCINNATI PB14A BLOWER VAPOR DYNAMICS IC45-19 BLOWER ELECTRIC PANEL 2923 South Tryon Street-Suite 100 Charlotte, North Carolina 28203 704-586-0007(p) 704-586-0373(f) License # C-1269 / #C-245 Geology NOTE: TEMPORARY TEST POINTS ABANDONED ON 8/17/17 FOLLOWING SSD SYSTEM BALANCING.S:\AAA-Master Projects\Fleming Labs (FMG)\FMG-005 SSD Installation\Figures\Sub-Slab Depressurization System Layout.dwg, FIG 3, 10/12/2017 11:16:41 AM, zbarlow Appendix A System Installation Photos Photograph 1: Sealing floor cracks and expansion joints with polyurethane caulk prior to communication testing. Photograph 2: Sub-slab utility clearance prior to coring activities.FMG-005Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 3: Sub-slab airflow being measured during SSD system communication testing Photograph 4: Measuring applied vacuum at temporary vacuum observation point.FMG-005Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 5: Core drilling concrete prior to installing suction point. Photograph 6: Installation of steel suction point in warehouse. Self leveling urethane being used in lifts to replace concrete removed during installation of suction point around roof support footer.FMG-005Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 7: Steel suction point with label and vacuum/sample port. Photograph 8: Suction point slide valve used to balance airflow between suction points.FMG-005Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 9: Overhead PVC conveyance piping. Suction points divided up into four separate fields. Photograph 10: Roof mounted Cincinnati (high flow) fan for building perimeter suction Field 1.FMG-005Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 11: Roof mounted Cincinnati PB14A (high flow) fan for building perimeter suction Field 4 on left. Two Vapor Dynamics IC45-19 (high vacuum) fans on right of photo for suction Fields 2 and 3. Photograph 12: SSD system control panel showing Magnahelic vacuum gauges, low vacuum alarm light, auto dialer, variable speed drives for Cincinnati fans and power supply. Additional alarm light located near warehouse office door.FMG-005Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Photograph 13: Magnahelic gauges measuring vacuum at each blower. Low vacuum alarm light mounted in center of gauges. Photograph 14: Magnahelic gauge (0-1 “WC) being used to measure vacuum at sub-slab vapor pin SS-3.FMG-005Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina 2923 S. Tryon Street, Suite 100 Charlotte, NC 28203 704.586.0007(p) 704.586.0373(f) Appendix B Report of Vapor Intrusion Mitigation www.cleanvapor.com Page 1 of 29 REPORT OF VAPOR INTRUSION MITIGATION for: Fleming Laboratories 2215 Thrift Road Charlotte, North Carolina Prepared for: Mr. Matt Bramblett, PE Hart Hickman 2923 South Tyron Street, Suite 100 Charlotte, North Carolina 28203 Prepared by: Mr. Thomas E. Hatton CEO-Project Director NRPP ID 104705 Clean Vapor, LLC 148 Route 94 PO Box 688 Blairstown, NJ 07825 October 3, 2017 Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 2 of 29 Table of Contents 1. Introduction ............................................................................................................................. 3 2. System Commissioning Measurements ................................................................................... 3 2.1. System Blower Measurements ......................................................................................... 4 2.2. Riser Pipe Performance Measurements............................................................................ 4 2.3. Sub Slab Vacuum Measurements ..................................................................................... 5 3. Suction Point Installation......................................................................................................... 5 4. Vapor Conveyance Pipe Installation ....................................................................................... 7 5. Gate Valves .............................................................................................................................. 9 6. Expansion Joint and Crack Sealing ....................................................................................... 10 7. Blower Installation ................................................................................................................ 11 8. Blower Wiring, Panels, and Breakers .................................................................................... 12 9. Frequency Inverter Control ................................................................................................... 13 10. Magnehelics & ASD System Alarm .................................................................................. 14 11. Auto Dialer Remote Notification ....................................................................................... 15 12. System Labeling................................................................................................................. 15 13. Vapor Pin Sub Slab Ports ................................................................................................... 17 14. Operations and Maintenance.............................................................................................. 18 14.1. General O&M Procedures .......................................................................................... 18 14.2. O&M Tables ............................................................................................................... 20 15. As-Built Drawings ............................................................................................................. 22 16. Permits ............................................................................................................................... 28 17. Cut Sheets .......................................................................................................................... 29 Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 3 of 29 1. Introduction This report summarizes the vapor intrusion mitigation activities performed at 2215 Thrift Road located in Charlotte, North Carolina. The Sub Slab Depressurization System (SSDS) has been designed and installed to mitigate vapor intrusion in the portions of the building identified as having elevated concentrations of sub slab vapors. This report and its appendices summarize the installation activities. The vapor mitigation system was installed in accordance with the approved VAPOR INTRUSION MITIGATION PLAN DESIGN for 2215 Thrift Road, Charlotte, North Carolina. Mitigation activities began with mobilization on Thursday, June 29, 2017. The soil depressurization blowers were started and the system commissioned on Thursday, August 17, 2017, completing the onsite mitigation activities. Four roof mounted blowers and twenty-four suction points were installed to mitigate the building areas of concern. The system is meeting all of the defined requirements for a successful Sub Slab Depressurization System as described in Section 2. Electrical and Mechanical permits were obtained through Mecklenburg County. The systems were inspected and final approval for Electric was issued on August 25, 2017, and final Mechanical approval was issued on August 31, 2017. Copies of the approval certificates are in the Appendix. 2. System Commissioning Measurements The design objective of the Vapor Intrusion Mitigation System was to create a negative pressure field with a minimum performance of -0.008 inches of water column ("w.c.) in areas of elevated soil gas concentrations. Post mitigation commissioning exhaust airflow, vacuum, and sub slab vacuum distribution measurements occurred on August 17, 2017. Sub slab vacuum measurements were taken using a digital micro-manometer capable of reading down to 0.0001 inches water column and airflow measured using a hot wire anemometer. Both measurements were taken on the roof at the access port mounted in the main riser pipes below the fans. All targeted areas of the sub slab are being depressurized to a vacuum level of -0.008 inches of water column or greater. The tables below show the system performance metrics as measured during commissioning. There is a difference in the airflow measured at the riser pipes as compared to the inlet of the blower. This is most likely due to high velocity turbulence. This Space Intentionally Left Blank Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 4 of 29 2.1. System Blower Measurements Blower # Blower Type Airflow (cfm) Vacuum ("wc) Current (amps) Blower Speed 1 Cincinnati Fan PB-14A 105 -1.21 0.45 20 Hz 2 Vapor Dynamics IC 4519 122 -3.00 0.20 N/A Brushless Motor 3 Vapor Dynamics IC 4519 112 -5.00 0.30 N/A Brushless Motor 4 Cincinnati Fan PB-14A 131 -1.40 0.59 20Hz 2.2. Riser Pipe Performance Measurements Blower System Riser # Vacuum ("wc) Airflow (cfm) 1 1-1 -0.93 44 1 1-2 -1.04 17 1 1-3 -1.06 37 1 1-4 -1.02 11 1 1-5 -1.03 10 1 1-6 -1.15 5 2 2-1 -4.70 28 2 2-2 -4.79 14 2 2-3 -4.90 6 2 2-4 -4.88 4 2 2-5 -4.89 11 3 3-1 -2.64 24 3 3-2 -2.71 0.8 3 3-3 -2.71 11 3 3-4 -2.69 8 3 3-5 -2.72 2 3 3-6 -2.63 22 4 4-1 -1.15 23 4 4-2 -1.16 22 4 4-3 -1.19 17 4 4-4 -1.11 34 4 4-5 -1.13 3 4 4-6 -1.14 20 4 4-7 -1.04 40 Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 5 of 29 2.3. Sub Slab Vacuum Measurements The locations of the temporary sub slab test ports are noted on the As-Built drawings (Section 15). The Temporary Test Ports (TP) were installed and sealed by Clean Vapor. For future sub slab readings, permanent vapor pin test ports were installed by Hart Hickman, PC. 8/17/2017 Readings Temporary Test Ports Vacuum ("w.c.) TP-1 -2.109 TP-2 -0.8020 TP-3 -0.2478 TP-4 -0.2071 TP-5 -0.6320 TP-6 -1.6550 TP-7 -1.5924 TP-8 -1.5834 TP-9 -1.3956 TP-10 -0.2964 9/25/2017 Readings Vapor Pin Test Ports Vacuum ("w.c.) SS-1 -1.50 SS-2 -3.40 SS-3 -0.91 SS-4 -1.80 3. Suction Point Installation A total of twenty-four (24) suction points were installed as shown in the As-Built drawing. All suction point riser pipes for blower systems one and four are three-inch Schedule 40 steel with the exception of SP# 4-5 which is three-inch schedule 40 PVC. All riser pipes for blower systems two and three are two-inch Schedule 40 steel. All the suction points were created using a five-inch diameter concrete coring bit and were sealed following clean out and riser pipe installation. Where necessary, multiple holes were cored in an overlapping pattern in order to create a trench off of column pads or footings. Gun-grade urethane caulking and backer rod was used below the surface of the concrete as a preliminary seal followed by self-leveling urethane to seal the suction points flush with the concrete floor. The riser pipes were secured above each suction point with pipe clamps attached to columns or walls. Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 6 of 29 Picture 3.1 Trench Suction Point Filled and Sealed Picture 3.2 Single Hole Suction Point Sealed with Self Leveling Urethane Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 7 of 29 Picture 3.3 Steel Riser and Sampling Port 4. Vapor Conveyance Pipe Installation All horizontal pipe runs between the roof mounted fan and the suction points were installed with a 1-inch slope back to a suction point for every ten feet of horizontal pipe run. All vertical pipe runs were installed plumb. Piping was installed so that there are no possible water traps between the blowers and the suction points. All overhead piping and fittings installed, with the exception of the horizontal three inch EMT pipe run connecting SP# 1-1 and 1-2 riser pipes, are Schedule 40 PVC and clamped and supported according to the current national plumbing code. Pipe is not supported by other building piping or ducts. Examples of piping, clamps, and supports are shown in the following pictures. This Space Intentionally Left Blank Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 8 of 29 Picture 4.1 Horizontal Overhead Conveyance Piping Picture 4.2 Steel Riser Pipes Transitioning into Overhead PVC Pipe Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 9 of 29 Picture 4.3 Overhead Conveyance Pipe above Office Space 5. Gate Valves Inline slide valves were installed for all suction points. All valves are currently in the 100% open position. Optimum sub slab vacuum extension is being achieved in targeted mitigation areas. Picture 5.1 Gate Valve (100% open) Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 10 of 29 6. Expansion Joint and Crack Sealing Visible expansion joints and slab cracks that had an approximate 1/16 inch or greater opening were sealed. Cracks and expansion joints were hand cleaned of debris using a cotter pin puller and the dust removed with a vacuum. Once cleaned the cracks were sealed with a gun-grade urethane caulk sealant. Expansion joints that are greater than ¼ inch in width or greater than 3/8 inch below the floor surface required a two-part process where the gun-grade urethane caulk was installed as a base layer and self-leveling urethane installed above the gun-grade urethane caulk flush to the level of the concrete floor. Most sealing of expansion joints and cracks occurred in December of 2016 before the initial diagnostic test in order to obtain more accurate readings when diagnosing the building. In addition, minor sealing occurred on Wednesday, August 16, 2017, after the blowers started when technicians examined the floor and listened for negative pressure leaks. See Section 15 Sheet 2 for floor openings sealed. Picture 6.1 Picture 6.2 Sealed Expansion Joints Sealed Floor Crack Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 11 of 29 7. Blower Installation Two roof mounted Cincinnati Fan PB-14A and two roof mounted Vapor Dynamics IC 4519 blowers were installed. The blowers are mounted on Unistrut stands and installed on Dura Block rubber mounts to minimize vibrations. The blower exhausts are shielded with factory supplied wire varmint guards. The exhaust discharge extends a minimum of 2 feet above the roofline and terminates at least 20 feet from intakes or other openings. The blower was specified based on previous diagnostic vacuum and air flow measurements. The location of the blower is noted on the As-Built Drawing Sheet. The following pictures show the roof mounted blowers. Picture 7.1 Roof Mounted Cincinnati Fan PB-14A Radial Blower Picture 7.2 Roof Mounted Vapor Dynamics IC 4519 Blowers Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 12 of 29 8. Blower Wiring, Panels, and Breakers Three (3) dedicated 480v circuit breakers were used to power the four blower systems. One dedicated circuit breaker is allocated for both 240v single phase Vapor Dynamics IC 4519 blowers and one dedicated circuit breaker for each of the 480v 3 phase Cincinnati Fan PB-14A radial blowers. All breakers have yellow labels with the text “ASD Blower Circuit, Do Not Power Off”. A picture of the labeled circuit breakers is shown below. Picture 14.1 Electrical Control System Indicator Panel Picture 8.1 Labeled Circuit Breakers Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 13 of 29 9. Frequency Inverter Control Each of the two radial blowers are powered through a Mitsubishi F800 Frequency inverter, more commonly known as a Variable Frequency Drive (VFD). The Frequency Inverter has the ability to adjust the motor speed from 60 Hertz (Hz) to 6 Hz. At no time shall the motor operate below 18 Hz. The frequency inverter’s performance is based on the ability to reduce the cycles per second, Hz at which Alternating Current (AC) power “bumps’ the motor. The installation of a VFD allows us to tune the radial blower’s performance to apply the most effective and efficient vacuum to the suction points in the system. The system was designed to create a minimum pressure differential of -0.008″ w.c. at the outer extent of the negative pressure field under cold weather conditions. Since the system was commissioned on a warm day in August where there was little temperature difference between the indoor and outdoor air, it is difficult to predict how the building will react to temperature differentials that may exist in January or February. For this reason, the VFD was adjusted to the lower end of the control at 20 Hz. At that VFD setting, the lowest measurement at a Vapor Pin location VP-3 measured -0.91" w.c., much higher than the minimum required pressure differential. This summer time set point should be more than sufficient and continuously exceed the cold weather goal of -0.008″w.c. If for some reason these winter time goals are not achieved, the VFD can be adjusted so the blower operates at greater capacity which will result in greater pressure differential values. The VFD also allows for an incremental and even distribution of voltage during start up or in the event of a power outage. The VFD at this site is not integrated into dynamic controls or a remote management system. Picture 9.1 Frequency Inverter Control Units Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 14 of 29 10. Magnehelics & ASD System Alarm Four (4) Magnehelics were installed to indicate the static vacuum generated by the blower system. The Magnehelic panel is mounted alongside the Frequency Inverters (VFD) and Sensaphone 400 auto dialer. Two red light alarm indicators were installed and are set to actuate whenever a blower vacuum is below approximately 0.25"w.c. An alarm light indicator was installed on the Magnehelic panel as shown below, and a second light indicator is located on the wall adjacent the warehouse to office entrance door. The locations are shown on the As-Built Drawing Sheet 3 and a photo of the Magnehelic panel is shown below. Picture 10.1 Magnehelic Panel with ASD System Alarm This Space Intentionally Left Blank Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 15 of 29 11. Auto Dialer Remote Notification A Sensaphone 400 Auto Dialer was installed to monitor the vacuum that is created by the blower system. If the blower fails to generate vacuum, the diaphragm switch circuit is completed and a call is made to the person responsible for managing the system indicating that a malfunction or low applied vacuum condition exists. In addition to a call, the ASD System Alarm will also sound. The auto dialer and phone line are powered by the building’s electrical system. Picture 11.1 Sensaphone 400 12. System Labeling At least every 20 feet of exposed contaminant vent pipe length has a label that reads “Active Soil Depressurization System, Do Not Alter” attached to the pipe. All labels are readable from three feet away. Each blower was labeled with an engraved weatherproof label that reads ASD Blower # 1-4 as indicated on the As-Built Drawings. See picture below for an example of an installed system label. Picture 12.1 Sample Port and System Labeling Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 16 of 29 Picture 12.2 Labeling on Overhead Conveyance Piping Picture 12.2 Installed Blower Label Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 17 of 29 13. Vapor Pin Sub Slab Ports Permanent vapor pin sub slab test ports were installed for verifying sub slab vacuum at Operations and Maintenance visits. The locations of these ports are shown in the As-Built Drawing. The photo below shows an example of a vapor pin sub slab test port. The vapor pin can be easily accessed by removing the plastic cover that sits flush with the warehouse floor. Picture 13.1 Vapor Pin Sub Slab Test Port Picture 13.2 Vapor Pin Sub Slab Test Port Cover Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 18 of 29 14. Operations and Maintenance There shall be an Active Operations Maintenance and Mentoring (OM&M) Program in effect as long as the mitigation system operates. 14.1. General O&M Procedures It is recommended that Vapor Intrusion Mitigation Systems (VIMS) be inspected annually. All maintenance on a VIMS should be performed by qualified maintenance personnel. Inspections should consist of a visual inspection of major system components, recording of major system metrics and measurement of sub slab vacuum levels at the permanent test ports. The table in Section 14.2 can be used to assist in the O&M inspections. The first column of the Table has been filled out with the commission values. • Visual Inspection: All mechanical components, pipe, and sealing should be visually inspected to ensure no damage has occurred. • Vapor Pin Test Ports: The sub slab vacuum at each vapor pin test port should be measured and recorded to ensure that the sub slab vacuum has not dropped below -0.008" w.c. • Risers: The static vacuum, airflow yield, and gate valve position should be recorded. • Blower: The blower should be checked for any visual signs of damage. The static vacuum and airflow of the blower should be measured and recorded. • VFD: The two Mitsubishi F800 frequency inverters shall be read at the time of the system inspection. The Hertz and amperage shall be noted in the inspection log. At no time shall the operational frequency be changed without measuring and recalibrating all of the system performance metrics. Any changes from the current 20 Hz set point shall be noted along with the rationale for changing the set points. Mitsubishi F800 Manual Link http://www.allied-automation.com/wp- content/uploads/2015/05/MITSUBISHI_manual_vfd_f800_installation.pdf • Sensaphone: A Sensaphone 400 Auto dialer is located under the Magnehelic panel enclosure. During the inspection, the auto dialer shall be tested. This is performed by de- energizing the blower and must be conducted in coordination with the individual who manages the mitigation system or the person who is programmed to receive the phone call. The Sensaphone will produce an audible that says “zone 2 alarm condition.” Sensaphone 400 Manual Link http://www.sensaphone.com/pdf/LIT-0129_400_Manual_v1.5.1_WEB.pdf Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 19 of 29 This Page Intentionally Left Blank www.cleanvapor.com Page 20 of 29 14.2. O&M Tables System Component Date Condition Date Condition/Reading Date Condition/Reading Sealing 8/17/2017 New Good Pipe 8/17/2017 New Good Blower#1 Dasdasddd 8/17/2017 New Good Blower#2 8/17/2017 New Good Blower#3 8/17/2017 New Good Blower#4 8/17/2017 New Good FR 800 VFD #1 8/17/2017 New 20 Hz FR 800 VFD #4 8/17/2017 New 20 Hz Sensaphone 400 8/17/2017 New Operational Blower Number Date Vacuum ("w.c.) Airflow (cfm) Date Vacuum ("w.c.) Airflow (cfm) Date Vacuum ("w.c.) Airflow (cfm) B1 8/17/2017 -1.21 105 B2 8/17/2017 -3.00 122 B3 8/17/2017 -5.00 112 B4 8/17/2017 -1.40 131 Vapor Pin Date Measurement ("w.c.) Date Measurement ("w.c.) Date Measurement ("w.c.) SS-1 9/25/2017 -1.50 SS-2 9/25/2017 -3.40 SS-3 9/25/2017 -0.91 SS-4 9/25/2017 -1.80 Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 21 of 29 Blower System # Riser# Date Vacuum ("w.c.) Airflow (cfm) Gate Valve Position Date Vacuum ("w.c.) Airflow (cfm) Gate Valve Position Date Vacuum ("w.c.) Airflow (cfm) Gate Valve Position 1 1 8/17/2017 -0.93 44 100% 1 2 8/17/2017 -1.04 17 100% 1 3 8/17/2017 -1.06 37 100% 1 4 8/17/2017 -1.02 11 100% 1 5 8/17/2017 -1.03 10 100% 1 6 8/17/2017 -1.15 5 100% 2 1 8/17/2017 -4.70 28 100% 2 2 8/17/2017 -4.79 14 100% 2 3 8/17/2017 -4.90 6 100% 2 4 8/17/2017 -4.88 4 100% 2 5 8/17/2017 -4.89 11 100% 3 1 8/17/2017 -2.64 24 100% 3 2 8/17/2017 -2.71 0.8 100% 3 3 8/17/2017 -2.71 11 100% 3 4 8/17/2017 -2.69 8 100% 3 5 8/17/2017 -2.72 2 100% 3 6 8/17/2017 -2.63 22 100% 4 1 8/17/2017 -1.15 23 100% 4 2 8/17/2017 -1.16 22 100% 4 3 8/17/2017 -1.19 17 100% 4 4 8/17/2017 -1.11 34 100% 4 5 8/17/2017 -1.13 3 100% 4 6 8/17/2017 -1.14 20 100% 4 7 8/17/2017 -1.04 40 100% www.cleanvapor.com Page 22 of 29 15. As-Built Drawings DRAWING LISTCCover1 Diagnostic Test Holes2 Sealing Plan3 Suction Points & Blowers4Mechanical DetailsACTIVE SOIL DEPRESSURIZATION SYSTEM FLEMING LABORATORIES2215 THRIFT ROADCHARLOTTE, NORTH CAROLINA 28208FEBRUARY 7, 2016AS-BUILTS 9-29-17 ACTIVE SOIL DEPRESSURIZATION FLEMING LABORATORIES 2215 THRIFT ROAD CLEAN VAPOR LLC P.O. BOX 688, BLAIRSTOWN, NJ 07825 Ph. 908 362- 5616 Fax. 908 362-5433THOMAS E. HATTONNEHAI.D. 104705NJDEP MIS 102451 ACTIVE SOIL DEPRESSURIZATION FLEMING LABORATORIES 2215 THRIFT ROAD CLEAN VAPOR LLC P.O. BOX 688, BLAIRSTOWN, NJ 07825 Ph. 908 362- 5616 Fax. 908 362-5433THOMAS E. HATTONNEHAI.D. 104705NJDEP MIS 102452 ACTIVE SOIL DEPRESSURIZATION FLEMING LABORATORIES 2215 THRIFT ROAD CLEAN VAPOR LLC P.O. BOX 688, BLAIRSTOWN, NJ 07825 Ph. 908 362- 5616 Fax. 908 362-5433THOMAS E. HATTONNEHAI.D. 104705NJDEP MIS 102453 ACTIVE SOIL DEPRESSURIZATION FLEMING LABORATORIES 2215 THRIFT ROAD CLEAN VAPOR LLC P.O. BOX 688, BLAIRSTOWN, NJ 07825 Ph. 908 362-5616 Fax. 9708 362-5433THOMAS E. HATTONNEHAI.D. 104705NJDEP MIS 102454 Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 28 of 29 16. Permits Mechanical Permit Final Electrical Permit Final Vapor Intrusion Mitigation Report Fleming Laboratories 2215 Thrift Road, Charlotte North Carolina www.cleanvapor.com Page 29 of 29 17. Cut Sheets Vapor Dynamics IC 4519 Compact Radial Blower Backed by 32 Years of Mitigation Experience Performance Vapor Dynamics IC 4519 45" WC @ 7% of 190 CFM max flow capacity Dynamic or manual speed control to achieve specified performance ranges 12 month warranty Design Compact design 18" x 16" x 10" weighing under 25 lbs 3" Schedule 40 inlet and exhaust UL listed components and enclosure for outside use Internal condensate bypass Motor designed to convey combustion gases Dynamic or manual speed control Quick connect couplers to facilitate ease of changing motors Accepts 120-240 voltage without alteration www.vapordynamics.com  (973) 862-0070 Performance Chart Static Vacuum 0" 10" 20" 30" 37" Wattage Airflow 220V 197 162 130 89 50 800-1100 COMPLETE UNIT $ 1,390.00 3 YEAR WARRANTY $ 425.00 Cost Page 1 of 2 Vapor Dynamics IC 4519 Compact Radial Blower Specifications Continued Enclosure Specifications Blower Specifications www.vapordynamics.com  (973) 862-0070 Page 2 of 2 DURA-BLOK is made from 100% recycled rubber and qualifies for LEED credits. Reflective strips on both sides allow for easy product visibility. Channels are through bolted on all sizes for added strength and a 1” (25.4mm)gap between blocks allows water to flow freely around longer assemblies. Product composition is not sharp or abrasive, helping to extend the roof life and no penetration through the roof is required. The DURA-BLOK dampens vibration, needs no supplemental rubber pad, and will not float or blow away. DURA-BLOK can be used to support piping, HVAC/Ducts, roof walkways, conduit and cable tray.DURA-BLOKRooftop SupportsAll dimensions in charts and on drawings are in inches. Dimensions shown in parentheses are in millimeters unless otherwise specified. DURA-BLOK™Rooftop Supports Pipe Hangers & Supports273 DURA-BLOKRooftop SupportsBase Only Dimensions - 4” (101mm)High x 6” (152mm)Wide x Base Length Material - 100% recycled rubber, UV resistant Ultimate Load Capacity - (uniform load) * DBP = 500 lbs. (2.22kN) DBM = 200 lbs. (0.89kN) DURA-BLOK channel support is designed as an economical support for piping systems, cable tray, HVAC equipment and many other applications. The DURA-BLOK is UV resistant and is suitable for any type of roofing material or other flat surfaces. Material effectively accepts screw fasteners for securing accessories. Base Only Part No.Weight Each DBP 4.48 (2.03kg) DBM 2.35 (1.07kg) Part No.Height Width Length DBP 4” (101mm)6” (152mm)9.6” (244mm) DBM 4” (101mm)6” (152mm)4.8” (122mm) DBP DBM * For Roof Loading, Consult Roofing Manufacturer or Engineer. As with most commercial roofs, the weakest point may be the insulation board beneath the rubber membrane. All dimensions in charts and on drawings are in inches. Dimensions shown in parentheses are in millimeters unless otherwise specified. DURA-BLOK™Rooftop Supports 274Pipe Hangers & Supports Base with 14 ga. (1.9mm)Galv. Channel - 1” (25.4mm)high Dimensions - 5” (127mm)High x 6” (152mm)Wide x Length (overall length) Material - 100% recycled rubber, UV resistant Ultimate Load Capacity -(uniform load) * DB5 = 500 lbs. (2.22kN) DB10 = 500 lbs. (2.22kN) DB20 = 1,000 lbs. (4.45kN) DB30 = 1,500 lbs. (6,67kN) DB40 = 2,000 lbs. (8.89kN) DB48 = 2,500 lbs. (11.12kN) DURA-BLOK DB-Series channel support is designed for superior support of piping systems, cable tray, HVAC equipment, walkway systems and many other applications. The DURA-BLOK is UV resistant and suitable for installation on any type of roofing material or other flat surfaces. For sloped roofs see adjustable hinge fitting (B634). DB - Series For pipe straps/clamps, rollers and roller supports that can be used with these DURA-BLOK supports, see page 284. Part No.Weight Each DB5 2.75 (1.25kg) DB10 5.28 (2.39kg) DB20 10.63 (4.82kg) DB30 15.99 (7.25kg) DB40 21.34 (9.68kg) DB48 26.70 (12.4kg) Part No.Height Width Overall Length DB5 5” (127mm)6” (152mm)4.8” (122mm) DB10 5” (127mm)6” (152mm)9.6” (244mm) DB20 5” (127mm)6” (152mm)20.2” (513mm) DB30 5” (127mm)6” (152mm)30.8” (782mm) DB40 5” (127mm)6” (152mm)41.4” (1052mm) DB48 5” (127mm)6” (152mm)52.0” (1321mm) DB10 DB20 DB5 * For Roof Loading, Consult Roofing Manufacturer or Engineer. As with most commercial roofs, the weakest point may be the insulation board beneath the rubber membrane. DB30DURA-BLOKRooftop SupportsAll dimensions in charts and on drawings are in inches. Dimensions shown in parentheses are in millimeters unless otherwise specified. DURA-BLOK™Rooftop Supports Pipe Hangers & Supports275 DURA-BLOKRooftop SupportsDB6 - Series Part No.Height Width Overall Length DB610 67/16” (167mm)6” (152mm)9.6” (244mm) DB620 67/16” (167mm)6” (152mm)20.2” (513mm) DB630 67/16” (167mm)6” (152mm)30.8” (782mm) DB640 67/16” (167mm)6” (152mm)41.4” (1052mm) DB648 67/16” (167mm)6” (152mm)52.0” (1321mm) Part No.Weight Each DB610 6.36 (2.88kg) DB620 12.90 (5.85kg) DB630 19.45 (8.82kg) DB640 26.00 (11.79kg) DB648 32.55 (14.76kg) DB610 DB630 Base with 12 ga. (2.6mm)Galv. Channel - 27/16” (62mm)high Dimensions - 67/16” (163mm)High x 6” (152mm)Wide x Length (overall length) Material - 100% recycled rubber, UV resistant Ultimate Load Capacity -(uniform load) * DB610 = 500 lbs. (2.22kN) DB620 = 1,000 lbs. (4.45kN) DB630 = 1,500 lbs. (6.67kN) DB640 = 2,000 lbs. (8.89kN) DB648 = 2,500 lbs. (11.12kN) DURA-BLOK DB6-Series channel support is designed for superior support of piping systems, cable tray, HVAC equipment, walkway systems and many other applications. The DURA-BLOK is UV resistant and suitable for installation on any type of roofing material or other flat surfaces. For sloped roofs see adjustable hinge fitting (B634). * For Roof Loading, Consult Roofing Manufacturer or Engineer. As with most commercial roofs, the weakest point may be the insulation board beneath the rubber membrane. For pipe straps/clamps, rollers and roller supports that can be used with these DURA-BLOK supports, see page 284. DB620 All dimensions in charts and on drawings are in inches. Dimensions shown in parentheses are in millimeters unless otherwise specified. DURA-BLOK™Rooftop Supports 276Pipe Hangers & Supports Differential Pressure GagesPRESSUREDWYER INSTRUMENTS, INC.| www.dwyer-inst.com4 Series2000 Magnehelic®Differential Pressure Gages Indicate Positive, Negative or Differential, Accurate within 2%RoHS Select the Dwyer®Magnehelic®gage for high accuracy — guaranteed within 2% of full-scale — and for the wide choice of 81 models available to suit your needs precisely. Using Dwyer's simple, frictionless Magnehelic®gage movement, it quicklyindicates low air or non- corrosive gas pressures — either positive, negative (vacuum) or differential. The design resists shock, vibration and over-pressures. No manometer fluid to evaporate, freeze or cause toxic or leveling problems. It's inexpensive, too. The Magnehelic®gage is the industry standard to measure fan and blower pressures, filter resistance, air velocity, furnace draft, pressure drop across orifice plates, liquid levels with bubbler systems and pressures in fluid amplifier or fluidic systems. It also checks gas-air ratio controls and automatic valves, and monitors blood and respiratory pressures in medical care equipment. Mounting A single case size is used for most models of Magnehelic®gages. They can be flush or surface mounted with standard hardware supplied. Although calibrated for vertical position, many ranges above 1˝ may be used at any angle by simply re-zeroing. However, for maximum accuracy, they must be calibrated in the same position in which they are used. These characteristics make Magnehelic®gages ideal for both stationary and portable applications. A 4-9/16˝ hole is required for flush panel mounting. Complete mounting and connection fittings, plus instructions, are furnished with each instrument. See page 7 for more information on mounting accessories. SPECIFICATIONS Service: Air and non-combustible, compatible gases (natural gas option available). Note:May be used with hydrogen. Order a Buna-N diaphragm. Pressures must be less than 35 psi. Wetted Materials:Consult factory. Housing: Die cast aluminum case and bezel, with acrylic cover. Exterior finish is coated gray to withstand 168 hour salt spray corrosion test. Accuracy: ±2% of FS (±3% on - 0, -100 Pa, -125 Pa, 10MM and ±4% on - 00, -60 Pa, -6MM ranges), throughout range at 70°F (21.1°C). Pressure Limits: -20 in Hg to 15 psig† (-0.677 to 1.034 bar); MP option: 35 psig (2.41 bar); HP option: 80 psig (5.52 bar). Overpressure: Relief plug opens at approximately 25 psig (1.72 bar), standard gages only. See Overpressure Protection Note on next page. Temperature Limits: 20 to 140°F* (-6.67 to 60°C). -20°F (-28°C) with low temperature option. Size: 4˝ (101.6 mm) diameter dial face. Mounting Orientation: Diaphragm in vertical position. Consult factory for other position orientations. Process Connections: 1/8˝ female NPT duplicate high and low pressure taps - one pair side and one pair back. Weight: 1 lb 2 oz (510 g), MP & HP 2 lb 2 oz (963 g). Standard Accessories: Two 1/8˝ NPT plugs for duplicate pressure taps, two 1/8˝ pipe thread to rubber tubing adapter, and three flush mounting adapters with screws. (Mounting and snap ring retainer substituted for three adapters in MP & HP gage accessories.) Agency Approval:RoHS. Note: -SP models not RoHS approved. 1/8 FEMALE NPTHIGH PRESSURECONNECTION 1-3/4(44.45) 1/2(12.70) 1/8 FEMALENPT LOWPRESSURE CONNECTION 11/16(17.46) 17/32(13.49)ø4-3/4 (120.65) PANEL CUTOUT ø5(127) ø4-47/64(120.27) 3/16 (4.76)2-17/32(64.29) 15/32(11.91) ø4-1/2(114.3) 1-1/4(31.75) ø5-1/2(139.70) MOUNTING RING RUBBER PRESSURE RELIEF PLUG WILL UNSEAT ITSELFWHEN GAGE ISOVERPRESSURIZED (3) 6-32 X 3/16 (4.76) DEEP HOLESEQUALLY SPACED ON A Ø4-1/8 (104.78) BOLT CIRCLE FORPANEL MOUNTING 1/8 FEMALE NPTHIGH PRESSURE CONNECTION 1-3/4(44.45) 1/2(12.70) 1/8 FEMALE NPTLOW PRESSURECONNECTION 11/16(17.46) 15/32(11.91) 1-11/16 (42.86) Ø4-1/2(114.3) 1-1/4(31.75) 17/32(13.49) .025 (.64) SPACE CREATED BY 3SPACER PADS WHEN SURFACE MOUNTED. DO NOT OBSTRUCT. PROVIDES PATH FOR RELIEF OF OVERPRESSURE. 1/8 FEMALENPT HIGH PRESSURECONNECTION 1/8 FEMALENPT LOW PRESSURECONNECTION 7/16(11.11) Ø4-3/4 (120.65) Flush, Surface or Pipe Mounted Enclosure Mounted ACCESSORIES †For applications with high cycle rate within gage total pressure rating, next higher rating is recommended. See Medium and High pressure options at lower left. A-605B Air Filter Gage Accessory Kit, Air filter kit with two plastic open/close valves, two 4˝ steel static tips, plastic tubing and mounting flange A-605C Air Filter Gage Accessory Kit, Air filter kit with two plastic open/close valves, two plastic static tips, plastic tubing and mounting flange Model A-432 Portable Kit Combine carrying case with any Magnehelic®gage of standard range, except high pressure connection. Includes 9 ft (2.7 m) of 3/16˝ ID rubber tubing, standhang bracket and terminal tube with holder. Model A-605 Air Filter Gage Accessory Kit Adapts any standard Magnehelic®gage for use as an air filter gage. Includes aluminum surface mounting bracket with screws, two 5 ft (1.5 m) lengths of 1/4˝ aluminum tubing two static pressure tips and two molded plastic vent valves, integral compression fittings on both tips and valves. 004_Layout 2 7/12/13 11:17 AM Page 4 Differential Pressure GagesPRESSURE5 Series 2000 Magnehelic®Gage Models & Ranges Dual Scale Air Velocity Units For use with pitot tube Zero Center Ranges 2300-6MM†••2300-10MM†•2300-20MM†• Model 2000-00AV†•• 2000-0AV†• 2001AV 2002AV 2005AV 2010AV Model 2000-60NPA†••2000-60PA†•• 2000-100PA†•2000-125PA†• 2000-250PA2000-300PA 2000-500PA2000-750PA 2000-1000PA Model 2000-6MM†••2000-10MM†•2000-15MM2000-25MM2000-30MM2000-50MM2000-80MM2000-100MM2000-125MM2000-150MM2000-200MM2000-250MM2000-300MM Model2000-0.5KPA2000-1KPA2000-1.5KPA2000-2KPA2000-2.5KPA2000-3KPA2000-4KPA2000-5KPA2000-8KPA2000-10KPA2000-15KPA2000-20KPA2000-25KPA2000-30KPA 2300-1KPA2300-2KPA2300-2.5KPA2300-3KPA Model2300-60PA†••2300-100PA†•2300-120PA2300-200PA2300-250PA2300-300PA2300-500PA2300-1000PA Dual Scale English/Metric Models Model 2000-00D†••2000-0D†•2001D2002D2003D2004D2005D2006D2008D2010D2015D2020D2025D2050D2060D Range,in w.c.0-.250-0.50-1.00-2.00-3.00-4.00-5.00-6.00-8.00-100-150-200-250-500-60 Zero Center Ranges Zero Center Ranges 2300-00†••2300-0†• 23012302 23042310 23202330 Model 220122022203220422052210*2215*2220*2230** Model2000-15CM2000-20CM2000-25CM2000-50CM2000-80CM2000-100CM2000-150CM2000-200CM 2000-250CM2000-300CM 2300-4CM 2300-10CM2300-30CM Model 2000-00N†••2000-00†••2000-0†•2001200220032004200520062008201020122015202020252030204020502060208021002120215021602180* 2250* †These ranges calibrated for vertical scale position. • Accuracy +/-3% • • Accuracy +/-4%*MP option standard **HP option standard Zero Center Ranges Zero Center Ranges O-ring seal for cover assures pressure integrity of case. OVERPRESSURE PROTECTIONBlowout plug is comprised of a rubber plug on the rear whichfunctions as a relief valve by unseating and venting the gageinterior when over pressure reaches approximately 25 psig (1.7bar). To provide a free path for pressure relief, there are fourspacer pads which maintain 0.023˝ clearance when gage issurface mounted. Do not obstruct the gap created by these pads.The blowout plug is not used on models above 180˝ of waterpressure, medium or high pressure models, or on gages whichrequire an elastomer other than silicone for the diaphragm.The blowout plug should not be used as a system overpressurecontrol. High supply pressures may still cause the gage to fail dueto over pressurization, resulting in property damage or seriousinjury. Good engineering practices should be utilized to preventyour system from exceeding the ratings or any component. Die cast aluminum case is precision made and iridite-dipped towithstand 168 hour salt spray corrosion test. Exterior finished inbaked dark gray hammerloid. One case size is used for allstandard pressure options, and for both surface and flushmounting. Silicone rubber diaphragm with integrally molded O-ring issupported by front and rear plates. It is locked and sealed inposition with a sealing plate and retaining ring. Diaphragm motionis restricted to prevent damage due to overpressures. Samarium Cobalt magnet mounted at one end of range springrotates helix without mechanical linkages. Bezel provides flange for flush mounting in panel. Clear plastic face is highly resistant to breakage. Providesundistorted viewing of pointer and scale. Precision litho-printed scale is accurate and easy to read. Red tipped pointerof heat treated aluminum tubing is easyto see. It is rigidly mounted on the helix shaft. Pointer stops of molded rubber prevent pointer over-travelwithout damage. “Wishbone” assembly provides mounting for helix, helixbearings and pointer shaft. Jeweled bearings are shock-resistant mounted;providevirtually friction-free motion for helix. Motion damped with high viscosity silicone fluid. Zero adjustment screw is conveniently located in the plastic cover, and is accessible without removing cover. O-ring seal provides pressure tightness. Helix is precision made from an alloy of high magnetic permeability. Mounted in jeweled bearings, it turns freely, following the magnetic field to move the pointer across the scale. Calibrated range spring is flat spring steel. Small amplitude of motion assures consistency and long life. It reacts to pressure on diaphragm. Live length adjustable for calibration. VELOCITY AND VOLUMETRIC FLOW UNITS Scales are available on the Magnehelic®that read in velocity units (FPM, m/s) or volumetric flow units (SCFM, m3/s, m3/h). Stocked velocity units with dual range scales in inches w.c. and feet per minute are shown above. For other ranges contact the factory. When ordering volumetric flow scales please specify the maximum flow rate and its corresponding pressure. Example: 0.5 in w.c. = 16,000 CFM. CONTACT US | U.S. 219/879-8000 | U.K. (+44) (0)1494-461707 | A.U. (+61) (0) 2 4272 2055 | China +852-23181007 Range in W.C./Velocity F.P.M.0-.25/300-2000 0-.50/500-2800 0-1.0/500-4000 0-2.0/1000-5600 0-5.0/2000-8800 0-10/2000-12500 .5-0-.51-0-11.25-0-1.251.5-0-1.5 Range,kPa0-0.5 0-10-1.50-20-2.50-30-40-50-80-100-150-200-250-30 Range,Pa or kPa0-62 Pa0-125 Pa0-250 Pa0-500 Pa0-750 Pa0-1.0 kPa0-1.25 kPa0-1.5 kPa0-2.0 kPa0-2.5 kPa0-3.7 kPa0-5 kPa0-6.2 kPa0-12.4 kPa0-15 kPa 3-0-35-0-510-0-10 Range, Pa10-0-500-600-1000-125 0-250 0-3000-500 0-7500-1000 Range MMof Water0-6 0-100-150-250-30 0-500-80 0-1000-1250-1500-2000-2500-300 Range, Pa30-0-3050-0-5060-0-60100-0-100125-0-125150-0-150250-0-250500-0-500 0.125-0-0.125.25-0-.25.5-0-.51-0-12-0-25-0-510-0-1015-0-15 2-0-25-0-5 15-0-15 Range Inches of Water .05-0-.20-.25 0-.500-1.0 0-2.0 0-3.0 0-4.0 0-5.0 0-6.0 0-8.0 0-100-12 0-15 0-20 0-25 0-30 0-400-50 0-600-80 0-1000-120 0-1500-160 0-1800-250 RangePSI 0-10-2 0-30-4 0-50-10 0-150-20 0-30 Range, CM ofWater 0-150-20 0-25 0-50 0-80 0-100 0-150 0-200 0-2500-300 A-310A 3-Way Vent Valves In applications where pressure is continuous and the Magnehelic®gage is connected by metal or plastic tubing which cannot be easily removed, we suggest using Dwyer A-310A vent valves to connect gage. Pressure can then be removed to check or re-zero the gage. ACCESSORIES A-321, Safety Relief Valve A-448, 3-piece magnet kit for mounting Magnehelic®gage directly to magnetic surface A-135, Rubber gasket for panel mounting A-401, Plastic Carry Case 005_Layout 2 7/12/13 11:19 AM Page 5 Appendix C Drum Composite Laboratory Results ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-133655-1 Client Project/Site: FMG-005 For: Hart & Hickman, PC 2923 S Tryon Street Suite 100 Charlotte, North Carolina 28203 Attn: Matt Bramblett Authorized for release by: 8/10/2017 5:10:56 PM Ken Hayes, Project Manager II (615)301-5035 ken.hayes@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 9 10 11 12 13 Table of Contents Client: Hart & Hickman, PC Project/Site: FMG-005 TestAmerica Job ID: 490-133655-1 Page 2 of 38 TestAmerica Nashville8/10/2017 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12 QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29 Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .33 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .34 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .35 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .36 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .38 1 2 3 4 5 6 7 8 9 10 11 12 13 Sample Summary TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Lab Sample ID Client Sample ID ReceivedCollectedMatrix 490-133655-1 Drum Composite Solid 07/27/17 12:15 07/28/17 09:10 TestAmerica Nashville Page 3 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Case Narrative Client: Hart & Hickman, PC TestAmerica Job ID: 490-133655-1 Project/Site: FMG-005 Job ID: 490-133655-1 Laboratory: TestAmerica Nashville Narrative Job Narrative 490-133655-1 Comments No additional comments. Receipt The sample was received on 7/28/2017 9:10 AM; the sample arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 0.3º C. GC/MS VOA Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 490-449039. Method 8260B: The TCLP leachate blank for batch 490-449520 contained a target analyte above the reporting limit (RL). None of the samples associated with this leachate blank contained this target analyte; therefore, re-extraction of the samples was not performed. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC/MS Semi VOA Method 8270D: The continuing calibration verification (CCVIS) associated with batch 490-449182 recovered above the upper control limit for 2,4-Dinitrophenol and 2-Nitrophenol. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following sample was impacted: (CCVIS 490-449182/3). Method 8270D: The continuing calibration verification (CCV) for analytical batch 490-449182 was outside the method criteria for hexachlorocyclopentadiene . A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable; therefore, the data is reported. (CCVIS 490-449182/3) Method 8270D: The laboratory control sample and/or the laboratory control sample duplicate (LCS/LCSD) for preparation batch 490-449026 and analytical batch 490-449182 recovered outside control limits for the following analyte: Hexachlorocyclopentadiene. This target has been identified as a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed. These results have been reported and qualified. Method 8270D: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 490-449026 and analytical batch 490-449182. Method 8270D: The continuing calibration verification (CCVIS) analyzed in batch 490-449182 was outside the method criteria for bis (2-chloroisopropyl) ether. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is considered estimated. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Metals Method 6010D: The low level continuing calibration verification (CCVL) associated with batch 490-449842 recovered above the upper control limit for Selenium. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. Method 6010D: The low level continuing calibration verification (CCVL) associated with batch 490-448979 recovered above the upper control limit for Arsenic. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Organic Prep TestAmerica NashvillePage 4 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Case Narrative Client: Hart & Hickman, PC TestAmerica Job ID: 490-133655-1 Project/Site: FMG-005 Job ID: 490-133655-1 (Continued) Laboratory: TestAmerica Nashville (Continued) No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica NashvillePage 5 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Definitions/Glossary TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Qualifiers GC/MS VOA Qualifier Description F1 MS and/or MSD Recovery is outside acceptance limits. Qualifier B Compound was found in the blank and sample. GC/MS Semi VOA Qualifier Description *LCS or LCSD is outside acceptance limits. Qualifier Metals Qualifier Description ^ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits. Qualifier F1 MS and/or MSD Recovery is outside acceptance limits. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 6 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Lab Sample ID: 490-133655-1Client Sample ID: Drum Composite Matrix: SolidDate Collected: 07/27/17 12:15 Date Received: 07/28/17 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) RL MDL Acetone ND 0.0499 mg/Kg ☼07/27/17 11:15 07/31/17 15:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Benzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Bromobenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Bromochloromethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Bromodichloromethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Bromoform ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Bromomethane ND 0.0499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼2-Butanone (MEK)ND 0.00499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Carbon disulfide ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Carbon tetrachloride ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Chlorobenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Chlorodibromomethane ND 0.00499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Chloroethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Chloroform ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Chloromethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼2-Chlorotoluene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼4-Chlorotoluene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼cis-1,2-Dichloroethene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼cis-1,3-Dichloropropene ND 0.00499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2-Dibromo-3-Chloropropane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2-Dibromoethane (EDB)ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Dibromomethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2-Dichlorobenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,3-Dichlorobenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,4-Dichlorobenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Dichlorodifluoromethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,1-Dichloroethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2-Dichloroethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,1-Dichloroethene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2-Dichloroethene, Total ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2-Dichloropropane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,3-Dichloropropane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼2,2-Dichloropropane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,1-Dichloropropene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Diisopropyl ether ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Ethylbenzene ND 0.00499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Hexachlorobutadiene ND 0.0499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼2-Hexanone ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Isopropylbenzene ND 0.00997 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Methylene Chloride ND 0.0499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼4-Methyl-2-pentanone (MIBK)ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Methyl tert-butyl ether ND 0.00499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Naphthalene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼n-Butylbenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼N-Propylbenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼p-Isopropyltoluene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼sec-Butylbenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Styrene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼tert-Butylbenzene ND TestAmerica Nashville Page 7 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Lab Sample ID: 490-133655-1Client Sample ID: Drum Composite Matrix: SolidDate Collected: 07/27/17 12:15 Date Received: 07/28/17 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 1,1,1,2-Tetrachloroethane ND 0.00199 mg/Kg ☼07/27/17 11:15 07/31/17 15:04 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,1,2,2-Tetrachloroethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Tetrachloroethene 0.00290 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Toluene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼trans-1,2-Dichloroethene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼trans-1,3-Dichloropropene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2,3-Trichlorobenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2,4-Trichlorobenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,1,1-Trichloroethane ND 0.00499 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,1,2-Trichloroethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Trichloroethene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Trichlorofluoromethane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2,3-Trichloropropane ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,2,4-Trimethylbenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼1,3,5-Trimethylbenzene ND 0.00199 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Vinyl chloride ND 0.00598 mg/Kg 07/27/17 11:15 07/31/17 15:04 1☼Xylenes, Total ND 4-Bromofluorobenzene (Surr)90 70-130 07/27/17 11:15 07/31/17 15:04 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)100 07/27/17 11:15 07/31/17 15:04 170-130 1,2-Dichloroethane-d4 (Surr)97 07/27/17 11:15 07/31/17 15:04 170-130 Toluene-d8 (Surr)98 07/27/17 11:15 07/31/17 15:04 170-130 Method: 8260B - Volatile Organic Compounds (GC/MS) - TCLP RL MDL 1,1-Dichloroethene ND 0.0100 mg/L 08/02/17 18:34 10 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0100 mg/L 08/02/17 18:34 101,2-Dichloroethane ND 0.500 mg/L 08/02/17 18:34 102-Butanone (MEK)ND 0.0100 mg/L 08/02/17 18:34 10BenzeneND 0.0100 mg/L 08/02/17 18:34 10Carbon tetrachloride ND 0.0100 mg/L 08/02/17 18:34 10ChlorobenzeneND 0.0100 mg/L 08/02/17 18:34 10TetrachloroetheneND 0.0100 mg/L 08/02/17 18:34 10TrichloroetheneND 0.0100 mg/L 08/02/17 18:34 10Vinyl chloride ND 0.0100 mg/L 08/02/17 18:34 10ChloroformND 1,2-Dichloroethane-d4 (Surr)81 70-130 08/02/17 18:34 10 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)99 08/02/17 18:34 1070-130 Dibromofluoromethane (Surr)91 08/02/17 18:34 1070-130 Toluene-d8 (Surr)97 08/02/17 18:34 1070-130 Method: 8270D - Semivolatile Organic Compounds (GC/MS) RL MDL Acenaphthene ND 0.0812 mg/Kg ☼07/31/17 09:32 07/31/17 19:02 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Acenaphthylene ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Anthracene ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Benzo[a]anthracene ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Benzo[a]pyrene ND TestAmerica Nashville Page 8 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Lab Sample ID: 490-133655-1Client Sample ID: Drum Composite Matrix: SolidDate Collected: 07/27/17 12:15 Date Received: 07/28/17 09:10 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL Benzo[b]fluoranthene ND 0.0812 mg/Kg ☼07/31/17 09:32 07/31/17 19:02 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Benzo[g,h,i]perylene ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Benzo[k]fluoranthene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Bis(2-chloroethoxy)methane ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Bis(2-chloroethyl)ether ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼bis (2-chloroisopropyl) ether ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Bis(2-ethylhexyl) phthalate ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼4-Bromophenyl phenyl ether ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Butyl benzyl phthalate ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Carbazole ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼4-Chloroaniline ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼4-Chloro-3-methylphenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2-Chloronaphthalene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2-Chlorophenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼4-Chlorophenyl phenyl ether ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Chrysene ND 0.807 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Cresols ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Dibenz(a,h)anthracene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Dibenzofuran ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼1,2-Dichlorobenzene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼1,3-Dichlorobenzene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼1,4-Dichlorobenzene ND 0.812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼3,3'-Dichlorobenzidine ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2,4-Dichlorophenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Diethyl phthalate ND 0.812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2,4-Dimethylphenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Dimethyl phthalate ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Di-n-butyl phthalate ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼4,6-Dinitro-2-methylphenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2,4-Dinitrophenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2,4-Dinitrotoluene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2,6-Dinitrotoluene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Di-n-octyl phthalate ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Fluoranthene ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Fluorene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Hexachlorobenzene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Hexachlorobutadiene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Hexachlorocyclopentadiene ND * 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Hexachloroethane ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Indeno[1,2,3-cd]pyrene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Isophorone ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼1-Methylnaphthalene ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2-Methylnaphthalene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2-Methylphenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼3 & 4 Methylphenol ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Naphthalene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2-Nitroaniline ND 0.812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼3-Nitroaniline ND 0.812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼4-Nitroaniline ND TestAmerica Nashville Page 9 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Lab Sample ID: 490-133655-1Client Sample ID: Drum Composite Matrix: SolidDate Collected: 07/27/17 12:15 Date Received: 07/28/17 09:10 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) RL MDL Nitrobenzene ND 0.404 mg/Kg ☼07/31/17 09:32 07/31/17 19:02 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2-Nitrophenol ND 0.812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼4-Nitrophenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼N-Nitrosodi-n-propylamine ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼n-Nitrosodiphenylamine(as diphenylamine) ND 0.812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Pentachlorophenol ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Phenanthrene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Phenol ND 0.0812 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼Pyrene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼1,2,4-Trichlorobenzene ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2,4,5-Trichlorophenol ND 0.404 mg/Kg 07/31/17 09:32 07/31/17 19:02 1☼2,4,6-Trichlorophenol ND 2-Fluorobiphenyl (Surr)59 29-120 07/31/17 09:32 07/31/17 19:02 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 2-Fluorophenol (Surr)53 07/31/17 09:32 07/31/17 19:02 110-120 Nitrobenzene-d5 (Surr)55 07/31/17 09:32 07/31/17 19:02 127-120 Phenol-d5 (Surr)57 07/31/17 09:32 07/31/17 19:02 110-120 Terphenyl-d14 (Surr)63 07/31/17 09:32 07/31/17 19:02 113-120 2,4,6-Tribromophenol (Surr)66 07/31/17 09:32 07/31/17 19:02 110-120 Method: 6010D - Metals (ICP) RL MDL Arsenic 6.30 2.41 mg/Kg ☼08/02/17 09:49 08/02/17 22:01 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 2.33 mg/Kg 08/08/17 12:01 08/08/17 18:56 1☼Barium 53.3 1.20 mg/Kg 08/02/17 09:49 08/02/17 22:01 1☼Cadmium ND 1.20 mg/Kg 08/02/17 09:49 08/02/17 22:01 1☼Chromium 20.9 1.20 mg/Kg 08/02/17 09:49 08/02/17 22:01 1☼Lead 16.7 2.41 mg/Kg 08/02/17 09:49 08/02/17 22:01 1☼Selenium ND ^ 1.16 mg/Kg 08/08/17 12:01 08/08/17 18:56 1☼Silver ND Method: 6010D - Metals (ICP) - TCLP RL MDL Silver ND 0.500 mg/L 07/30/17 13:07 07/31/17 12:02 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier 0.500 mg/L 07/30/17 13:07 07/31/17 02:02 1ArsenicND^ 10.0 mg/L 07/30/17 13:07 07/31/17 02:02 1BariumND 0.100 mg/L 07/30/17 13:07 07/31/17 02:02 1CadmiumND 0.500 mg/L 07/30/17 13:07 07/31/17 02:02 1ChromiumND 0.500 mg/L 07/30/17 13:07 07/31/17 02:02 1LeadND 0.100 mg/L 07/30/17 13:07 07/31/17 02:02 1SeleniumND Method: 7470A - Mercury (CVAA) - TCLP RL MDL Mercury ND 0.00200 mg/L 08/01/17 10:58 08/01/17 17:41 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Method: 7471B - Mercury (CVAA) RL MDL Mercury ND 0.123 mg/Kg ☼07/31/17 14:52 07/31/17 20:41 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 10 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Client Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Lab Sample ID: 490-133655-1Client Sample ID: Drum Composite Matrix: SolidDate Collected: 07/27/17 12:15 Date Received: 07/28/17 09:10 General Chemistry RL RL Percent Solids 81.8 0.1 %07/30/17 11:16 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier TestAmerica Nashville Page 11 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-449039/9 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449039 RL MDL Acetone ND 0.0500 mg/Kg 07/31/17 14:04 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00200 mg/Kg 07/31/17 14:04 1Bromobenzene ND 0.00200 mg/Kg 07/31/17 14:04 1Benzene ND 0.00200 mg/Kg 07/31/17 14:04 1Bromochloromethane ND 0.00200 mg/Kg 07/31/17 14:04 1Bromodichloromethane ND 0.00200 mg/Kg 07/31/17 14:04 1Bromoform ND 0.00200 mg/Kg 07/31/17 14:04 1Bromomethane ND 0.0500 mg/Kg 07/31/17 14:04 12-Butanone (MEK) ND 0.00500 mg/Kg 07/31/17 14:04 1Carbon disulfide ND 0.00200 mg/Kg 07/31/17 14:04 1Carbon tetrachloride ND 0.00200 mg/Kg 07/31/17 14:04 1Chlorobenzene ND 0.00200 mg/Kg 07/31/17 14:04 1Chlorodibromomethane ND 0.00500 mg/Kg 07/31/17 14:04 1Chloroethane ND 0.00200 mg/Kg 07/31/17 14:04 1Chloroform ND 0.00200 mg/Kg 07/31/17 14:04 1Chloromethane ND 0.00200 mg/Kg 07/31/17 14:04 12-Chlorotoluene ND 0.00200 mg/Kg 07/31/17 14:04 14-Chlorotoluene ND 0.00200 mg/Kg 07/31/17 14:04 1cis-1,2-Dichloroethene ND 0.00200 mg/Kg 07/31/17 14:04 1cis-1,3-Dichloropropene ND 0.00500 mg/Kg 07/31/17 14:04 11,2-Dibromo-3-Chloropropane ND 0.00200 mg/Kg 07/31/17 14:04 11,2-Dibromoethane (EDB) ND 0.00200 mg/Kg 07/31/17 14:04 1Dibromomethane ND 0.00200 mg/Kg 07/31/17 14:04 11,2-Dichlorobenzene ND 0.00200 mg/Kg 07/31/17 14:04 11,3-Dichlorobenzene ND 0.00200 mg/Kg 07/31/17 14:04 11,4-Dichlorobenzene ND 0.00200 mg/Kg 07/31/17 14:04 1Dichlorodifluoromethane ND 0.00200 mg/Kg 07/31/17 14:04 11,1-Dichloroethane ND 0.00200 mg/Kg 07/31/17 14:04 11,2-Dichloroethane ND 0.00200 mg/Kg 07/31/17 14:04 11,1-Dichloroethene ND 0.00200 mg/Kg 07/31/17 14:04 11,2-Dichloroethene, Total ND 0.00200 mg/Kg 07/31/17 14:04 11,2-Dichloropropane ND 0.00200 mg/Kg 07/31/17 14:04 11,3-Dichloropropane ND 0.00200 mg/Kg 07/31/17 14:04 12,2-Dichloropropane ND 0.00200 mg/Kg 07/31/17 14:04 11,1-Dichloropropene ND 0.00200 mg/Kg 07/31/17 14:04 1Diisopropyl ether ND 0.00200 mg/Kg 07/31/17 14:04 1Ethylbenzene ND 0.00500 mg/Kg 07/31/17 14:04 1Hexachlorobutadiene ND 0.0500 mg/Kg 07/31/17 14:04 12-Hexanone ND 0.00200 mg/Kg 07/31/17 14:04 1Isopropylbenzene ND 0.0100 mg/Kg 07/31/17 14:04 1Methylene Chloride ND 0.0500 mg/Kg 07/31/17 14:04 14-Methyl-2-pentanone (MIBK) ND 0.00200 mg/Kg 07/31/17 14:04 1Methyl tert-butyl ether ND 0.00500 mg/Kg 07/31/17 14:04 1Naphthalene ND 0.00200 mg/Kg 07/31/17 14:04 1n-Butylbenzene ND 0.00200 mg/Kg 07/31/17 14:04 1N-Propylbenzene ND 0.00200 mg/Kg 07/31/17 14:04 1p-Isopropyltoluene ND 0.00200 mg/Kg 07/31/17 14:04 1sec-Butylbenzene ND 0.00200 mg/Kg 07/31/17 14:04 1Styrene TestAmerica Nashville Page 12 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-449039/9 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449039 RL MDL tert-Butylbenzene ND 0.00200 mg/Kg 07/31/17 14:04 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00200 mg/Kg 07/31/17 14:04 11,1,1,2-Tetrachloroethane ND 0.00200 mg/Kg 07/31/17 14:04 11,1,2,2-Tetrachloroethane ND 0.00200 mg/Kg 07/31/17 14:04 1Tetrachloroethene ND 0.00200 mg/Kg 07/31/17 14:04 1Toluene ND 0.00200 mg/Kg 07/31/17 14:04 1trans-1,2-Dichloroethene ND 0.00200 mg/Kg 07/31/17 14:04 1trans-1,3-Dichloropropene ND 0.00200 mg/Kg 07/31/17 14:04 11,2,3-Trichlorobenzene ND 0.00200 mg/Kg 07/31/17 14:04 11,2,4-Trichlorobenzene ND 0.00200 mg/Kg 07/31/17 14:04 11,1,1-Trichloroethane ND 0.00500 mg/Kg 07/31/17 14:04 11,1,2-Trichloroethane ND 0.00200 mg/Kg 07/31/17 14:04 1Trichloroethene ND 0.00200 mg/Kg 07/31/17 14:04 1Trichlorofluoromethane ND 0.00200 mg/Kg 07/31/17 14:04 11,2,3-Trichloropropane ND 0.00200 mg/Kg 07/31/17 14:04 11,2,4-Trimethylbenzene ND 0.00200 mg/Kg 07/31/17 14:04 11,3,5-Trimethylbenzene ND 0.00200 mg/Kg 07/31/17 14:04 1Vinyl chloride ND 0.00600 mg/Kg 07/31/17 14:04 1Xylenes, Total 4-Bromofluorobenzene (Surr)89 70-130 07/31/17 14:04 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 101 07/31/17 14:04 1Dibromofluoromethane (Surr)70-130 98 07/31/17 14:04 11,2-Dichloroethane-d4 (Surr)70-130 98 07/31/17 14:04 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449039/3 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449039 Acetone 0.250 0.2523 mg/Kg 101 45-145 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Bromobenzene 0.0500 0.04289 mg/Kg 86 67-130 Benzene 0.0500 0.04680 mg/Kg 94 70-130 Bromochloromethane 0.0500 0.04972 mg/Kg 99 70-133 Bromodichloromethane 0.0500 0.04336 mg/Kg 87 70-130 Bromoform 0.0500 0.04812 mg/Kg 96 59-137 Bromomethane 0.0500 0.05334 mg/Kg 107 32-150 2-Butanone (MEK)0.250 0.2105 mg/Kg 84 50-149 Carbon disulfide 0.0500 0.04937 mg/Kg 99 66-138 Carbon tetrachloride 0.0500 0.04472 mg/Kg 89 70-131 Chlorobenzene 0.0500 0.04643 mg/Kg 93 70-130 Chlorodibromomethane 0.0500 0.04632 mg/Kg 93 70-130 Chloroethane 0.0500 0.05105 mg/Kg 102 37-150 Chloroform 0.0500 0.04536 mg/Kg 91 70-130 Chloromethane 0.0500 0.05174 mg/Kg 103 53-150 2-Chlorotoluene 0.0500 0.04348 mg/Kg 87 70-132 4-Chlorotoluene 0.0500 0.04496 mg/Kg 90 67-135 cis-1,2-Dichloroethene 0.0500 0.04524 mg/Kg 90 70-132 TestAmerica Nashville Page 13 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449039/3 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449039 cis-1,3-Dichloropropene 0.0500 0.04109 mg/Kg 82 70-130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits 1,2-Dibromo-3-Chloropropane 0.0500 0.04280 mg/Kg 86 47-144 1,2-Dibromoethane (EDB)0.0500 0.04417 mg/Kg 88 69-130 Dibromomethane 0.0500 0.04483 mg/Kg 90 70-130 1,2-Dichlorobenzene 0.0500 0.04673 mg/Kg 93 70-134 1,3-Dichlorobenzene 0.0500 0.04675 mg/Kg 93 69-137 1,4-Dichlorobenzene 0.0500 0.04414 mg/Kg 88 66-134 Dichlorodifluoromethane 0.0500 0.03878 mg/Kg 78 32-150 1,1-Dichloroethane 0.0500 0.04525 mg/Kg 90 70-130 1,2-Dichloroethane 0.0500 0.04243 mg/Kg 85 65-134 1,1-Dichloroethene 0.0500 0.04516 mg/Kg 90 70-131 1,2-Dichloroethene, Total 0.100 0.08929 mg/Kg 89 70-130 1,2-Dichloropropane 0.0500 0.04387 mg/Kg 88 70-130 1,3-Dichloropropane 0.0500 0.04407 mg/Kg 88 70-130 2,2-Dichloropropane 0.0500 0.04156 mg/Kg 83 57-150 1,1-Dichloropropene 0.0500 0.04124 mg/Kg 82 70-130 Diisopropyl ether 0.0500 0.04129 mg/Kg 83 68-134 Ethylbenzene 0.0500 0.04348 mg/Kg 87 70-130 Hexachlorobutadiene 0.0500 0.04223 mg/Kg 84 64-137 2-Hexanone 0.250 0.2124 mg/Kg 85 47-148 Isopropylbenzene 0.0500 0.04188 mg/Kg 84 70-130 Methylene Chloride 0.0500 0.04995 mg/Kg 100 69-130 4-Methyl-2-pentanone (MIBK)0.250 0.2159 mg/Kg 86 48-150 Methyl tert-butyl ether 0.0500 0.04135 mg/Kg 83 54-145 Naphthalene 0.0500 0.04072 mg/Kg 81 55-149 n-Butylbenzene 0.0500 0.04170 mg/Kg 83 57-150 N-Propylbenzene 0.0500 0.04412 mg/Kg 88 62-150 p-Isopropyltoluene 0.0500 0.04400 mg/Kg 88 66-147 sec-Butylbenzene 0.0500 0.04382 mg/Kg 88 68-147 Styrene 0.0500 0.04420 mg/Kg 88 70-131 tert-Butylbenzene 0.0500 0.04293 mg/Kg 86 70-138 1,1,1,2-Tetrachloroethane 0.0500 0.04523 mg/Kg 90 70-130 1,1,2,2-Tetrachloroethane 0.0500 0.04684 mg/Kg 94 61-134 Tetrachloroethene 0.0500 0.04720 mg/Kg 94 70-130 Toluene 0.0500 0.04517 mg/Kg 90 70-130 trans-1,2-Dichloroethene 0.0500 0.04405 mg/Kg 88 70-130 trans-1,3-Dichloropropene 0.0500 0.04050 mg/Kg 81 67-130 1,2,3-Trichlorobenzene 0.0500 0.03879 mg/Kg 78 57-146 1,2,4-Trichlorobenzene 0.0500 0.03857 mg/Kg 77 47-150 1,1,1-Trichloroethane 0.0500 0.04456 mg/Kg 89 70-130 1,1,2-Trichloroethane 0.0500 0.04257 mg/Kg 85 70-130 Trichloroethene 0.0500 0.04448 mg/Kg 89 70-130 Trichlorofluoromethane 0.0500 0.04557 mg/Kg 91 53-150 1,2,3-Trichloropropane 0.0500 0.04331 mg/Kg 87 60-139 1,2,4-Trimethylbenzene 0.0500 0.04461 mg/Kg 89 70-140 1,3,5-Trimethylbenzene 0.0500 0.04103 mg/Kg 82 69-141 Vinyl chloride 0.0500 0.04730 mg/Kg 95 63-150 Xylenes, Total 0.100 0.08321 mg/Kg 83 70-130 TestAmerica Nashville Page 14 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449039/3 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449039 4-Bromofluorobenzene (Surr)70 -130 Surrogate 86 LCS LCS Qualifier Limits%Recovery 97Dibromofluoromethane (Surr)70 -130 941,2-Dichloroethane-d4 (Surr)70 -130 97Toluene-d8 (Surr)70 -130 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-449039/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449039 Acetone 0.250 0.2486 mg/Kg 99 45-145 1 38 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Bromobenzene 0.0500 0.04329 mg/Kg 87 67-130 1 40 Benzene 0.0500 0.04834 mg/Kg 97 70-130 3 37 Bromochloromethane 0.0500 0.05134 mg/Kg 103 70-133 3 15 Bromodichloromethane 0.0500 0.04448 mg/Kg 89 70-130 3 20 Bromoform 0.0500 0.04814 mg/Kg 96 59-137 0 17 Bromomethane 0.0500 0.05419 mg/Kg 108 32-150 2 45 2-Butanone (MEK)0.250 0.2149 mg/Kg 86 50-149 2 39 Carbon disulfide 0.0500 0.04965 mg/Kg 99 66-138 1 41 Carbon tetrachloride 0.0500 0.04566 mg/Kg 91 70-131 2 41 Chlorobenzene 0.0500 0.04697 mg/Kg 94 70-130 1 40 Chlorodibromomethane 0.0500 0.04616 mg/Kg 92 70-130 0 14 Chloroethane 0.0500 0.05118 mg/Kg 102 37-150 0 50 Chloroform 0.0500 0.04664 mg/Kg 93 70-130 3 15 Chloromethane 0.0500 0.05254 mg/Kg 105 53-150 2 47 2-Chlorotoluene 0.0500 0.04326 mg/Kg 87 70-132 1 41 4-Chlorotoluene 0.0500 0.04473 mg/Kg 89 67-135 1 41 cis-1,2-Dichloroethene 0.0500 0.04714 mg/Kg 94 70-132 4 18 cis-1,3-Dichloropropene 0.0500 0.04203 mg/Kg 84 70-130 2 42 1,2-Dibromo-3-Chloropropane 0.0500 0.03811 mg/Kg 76 47-144 12 38 1,2-Dibromoethane (EDB)0.0500 0.04465 mg/Kg 89 69-130 1 17 Dibromomethane 0.0500 0.04485 mg/Kg 90 70-130 0 19 1,2-Dichlorobenzene 0.0500 0.04703 mg/Kg 94 70-134 1 40 1,3-Dichlorobenzene 0.0500 0.04744 mg/Kg 95 69-137 1 41 1,4-Dichlorobenzene 0.0500 0.04534 mg/Kg 91 66-134 3 41 Dichlorodifluoromethane 0.0500 0.03823 mg/Kg 76 32-150 1 50 1,1-Dichloroethane 0.0500 0.04656 mg/Kg 93 70-130 3 42 1,2-Dichloroethane 0.0500 0.04297 mg/Kg 86 65-134 1 16 1,1-Dichloroethene 0.0500 0.04683 mg/Kg 94 70-131 4 43 1,2-Dichloroethene, Total 0.100 0.09242 mg/Kg 92 70-130 3 41 1,2-Dichloropropane 0.0500 0.04494 mg/Kg 90 70-130 2 15 1,3-Dichloropropane 0.0500 0.04482 mg/Kg 90 70-130 2 15 2,2-Dichloropropane 0.0500 0.04300 mg/Kg 86 57-150 3 42 1,1-Dichloropropene 0.0500 0.04310 mg/Kg 86 70-130 4 41 Diisopropyl ether 0.0500 0.04246 mg/Kg 85 68-134 3 36 Ethylbenzene 0.0500 0.04505 mg/Kg 90 70-130 4 38 Hexachlorobutadiene 0.0500 0.04254 mg/Kg 85 64-137 1 44 2-Hexanone 0.250 0.2093 mg/Kg 84 47-148 1 38 TestAmerica Nashville Page 15 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-449039/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449039 Isopropylbenzene 0.0500 0.04342 mg/Kg 87 70-130 4 39 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Methylene Chloride 0.0500 0.05276 mg/Kg 106 69-130 5 19 4-Methyl-2-pentanone (MIBK)0.250 0.2158 mg/Kg 86 48-150 0 41 Methyl tert-butyl ether 0.0500 0.04168 mg/Kg 83 54-145 1 36 Naphthalene 0.0500 0.03934 mg/Kg 79 55-149 3 37 n-Butylbenzene 0.0500 0.04313 mg/Kg 86 57-150 3 39 N-Propylbenzene 0.0500 0.04415 mg/Kg 88 62-150 0 38 p-Isopropyltoluene 0.0500 0.04444 mg/Kg 89 66-147 1 38 sec-Butylbenzene 0.0500 0.04386 mg/Kg 88 68-147 0 38 Styrene 0.0500 0.04511 mg/Kg 90 70-131 2 40 tert-Butylbenzene 0.0500 0.03993 mg/Kg 80 70-138 7 38 1,1,1,2-Tetrachloroethane 0.0500 0.04707 mg/Kg 94 70-130 4 41 1,1,2,2-Tetrachloroethane 0.0500 0.04700 mg/Kg 94 61-134 0 16 Tetrachloroethene 0.0500 0.04808 mg/Kg 96 70-130 2 41 Toluene 0.0500 0.04632 mg/Kg 93 70-130 3 40 trans-1,2-Dichloroethene 0.0500 0.04528 mg/Kg 91 70-130 3 41 trans-1,3-Dichloropropene 0.0500 0.04161 mg/Kg 83 67-130 3 41 1,2,3-Trichlorobenzene 0.0500 0.03969 mg/Kg 79 57-146 2 42 1,2,4-Trichlorobenzene 0.0500 0.03616 mg/Kg 72 47-150 6 43 1,1,1-Trichloroethane 0.0500 0.04611 mg/Kg 92 70-130 3 41 1,1,2-Trichloroethane 0.0500 0.04340 mg/Kg 87 70-130 2 17 Trichloroethene 0.0500 0.04547 mg/Kg 91 70-130 2 41 Trichlorofluoromethane 0.0500 0.04859 mg/Kg 97 53-150 6 49 1,2,3-Trichloropropane 0.0500 0.04322 mg/Kg 86 60-139 0 16 1,2,4-Trimethylbenzene 0.0500 0.04416 mg/Kg 88 70-140 1 38 1,3,5-Trimethylbenzene 0.0500 0.04067 mg/Kg 81 69-141 1 38 Vinyl chloride 0.0500 0.04894 mg/Kg 98 63-150 3 46 Xylenes, Total 0.100 0.08585 mg/Kg 86 70-130 3 38 4-Bromofluorobenzene (Surr)70 -130 Surrogate 86 LCSD LCSD Qualifier Limits%Recovery 97Dibromofluoromethane (Surr)70 -130 941,2-Dichloroethane-d4 (Surr)70 -130 97Toluene-d8 (Surr)70 -130 Client Sample ID: Method BlankLab Sample ID: MB 490-449643/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449643 RL MDL Benzene ND 0.00100 mg/L 08/02/17 12:40 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.0500 mg/L 08/02/17 12:40 12-Butanone (MEK) ND 0.00100 mg/L 08/02/17 12:40 1Carbon tetrachloride ND 0.00100 mg/L 08/02/17 12:40 1Chlorobenzene ND 0.00100 mg/L 08/02/17 12:40 1Chloroform ND 0.00100 mg/L 08/02/17 12:40 11,2-Dichloroethane ND 0.00100 mg/L 08/02/17 12:40 11,1-Dichloroethene ND 0.00100 mg/L 08/02/17 12:40 1Tetrachloroethene TestAmerica Nashville Page 16 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-449643/6 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449643 RL MDL Trichloroethene ND 0.00100 mg/L 08/02/17 12:40 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.00100 mg/L 08/02/17 12:40 1Vinyl chloride 4-Bromofluorobenzene (Surr)98 70-130 08/02/17 12:40 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 92 08/02/17 12:40 1Dibromofluoromethane (Surr)70-130 81 08/02/17 12:40 11,2-Dichloroethane-d4 (Surr)70-130 100 08/02/17 12:40 1Toluene-d8 (Surr)70-130 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449643/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 449643 Benzene 0.0200 0.01731 mg/L 87 70-130 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits 2-Butanone (MEK)0.100 0.08620 mg/L 86 55-143 Carbon tetrachloride 0.0200 0.01443 mg/L 72 70-147 Chlorobenzene 0.0200 0.01656 mg/L 83 70-130 Chloroform 0.0200 0.01593 B mg/L 80 70-130 1,2-Dichloroethane 0.0200 0.01447 mg/L 72 70-130 1,1-Dichloroethene 0.0200 0.01670 mg/L 83 70-132 Tetrachloroethene 0.0200 0.01568 mg/L 78 70-130 Trichloroethene 0.0200 0.01603 mg/L 80 70-130 Vinyl chloride 0.0200 0.01929 mg/L 96 57-137 4-Bromofluorobenzene (Surr)70 -130 Surrogate 101 LCS LCS Qualifier Limits%Recovery 93Dibromofluoromethane (Surr)70 -130 851,2-Dichloroethane-d4 (Surr)70 -130 98Toluene-d8 (Surr)70 -130 Client Sample ID: Method BlankLab Sample ID: LB 490-449520/1-A Matrix: Solid Prep Type: TCLP Analysis Batch: 449643 RL MDL Benzene ND 0.00100 mg/L 08/02/17 16:06 1 LB LB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.0500 mg/L 08/02/17 16:06 12-Butanone (MEK) ND 0.00100 mg/L 08/02/17 16:06 1Carbon tetrachloride ND 0.00100 mg/L 08/02/17 16:06 1Chlorobenzene 0.008134 B 0.00100 mg/L 08/02/17 16:06 1Chloroform 0.003795 0.00100 mg/L 08/02/17 16:06 11,2-Dichloroethane ND 0.00100 mg/L 08/02/17 16:06 11,1-Dichloroethene ND 0.00100 mg/L 08/02/17 16:06 1Tetrachloroethene ND 0.00100 mg/L 08/02/17 16:06 1Trichloroethene ND 0.00100 mg/L 08/02/17 16:06 1Vinyl chloride TestAmerica Nashville Page 17 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: LB 490-449520/1-A Matrix: Solid Prep Type: TCLP Analysis Batch: 449643 4-Bromofluorobenzene (Surr)99 70-130 08/02/17 16:06 1 LB LB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 95 08/02/17 16:06 1Dibromofluoromethane (Surr)70-130 85 08/02/17 16:06 11,2-Dichloroethane-d4 (Surr)70-130 97 08/02/17 16:06 1Toluene-d8 (Surr)70-130 Client Sample ID: Matrix SpikeLab Sample ID: 490-133738-A-1-E MS Matrix: Solid Prep Type: TCLP Analysis Batch: 449643 Benzene ND 0.500 0.5250 mg/L 105 55-147 Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits 2-Butanone (MEK)ND 2.50 2.902 mg/L 116 50-143 Carbon tetrachloride ND 0.500 0.4364 mg/L 87 56-150 Chlorobenzene ND 0.500 0.4962 mg/L 99 70-130 Chloroform ND 0.500 0.4928 mg/L 99 66-138 1,2-Dichloroethane 0.758 F1 0.500 0.4705 F1 mg/L -57 64-136 1,1-Dichloroethene ND 0.500 0.5161 mg/L 103 54-150 Tetrachloroethene ND 0.500 0.4657 mg/L 93 57-138 Trichloroethene ND 0.500 0.4868 mg/L 97 63-135 Vinyl chloride ND 0.500 0.6014 mg/L 120 57-150 4-Bromofluorobenzene (Surr)70 -130 Surrogate 99 MS MS Qualifier Limits%Recovery 99Dibromofluoromethane (Surr)70 -130 861,2-Dichloroethane-d4 (Surr)70 -130 95Toluene-d8 (Surr)70 -130 Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-133738-A-1-E MSD Matrix: Solid Prep Type: TCLP Analysis Batch: 449643 Benzene ND 0.500 0.5310 mg/L 106 55-147 1 50 Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD 2-Butanone (MEK)ND 2.50 2.924 mg/L 117 50-143 1 19 Carbon tetrachloride ND 0.500 0.4417 mg/L 88 56-150 1 19 Chlorobenzene ND 0.500 0.5036 mg/L 101 70-130 1 14 Chloroform ND 0.500 0.4968 mg/L 99 66-138 1 18 1,2-Dichloroethane 0.758 F1 0.500 0.4787 F1 mg/L -56 64-136 2 17 1,1-Dichloroethene ND 0.500 0.5344 mg/L 107 54-150 3 20 Tetrachloroethene ND 0.500 0.4743 mg/L 95 57-138 2 17 Trichloroethene ND 0.500 0.4928 mg/L 99 63-135 1 17 Vinyl chloride ND 0.500 0.6100 mg/L 122 57-150 1 17 4-Bromofluorobenzene (Surr)70 -130 Surrogate 99 MSD MSD Qualifier Limits%Recovery 98Dibromofluoromethane (Surr)70 -130 861,2-Dichloroethane-d4 (Surr)70 -130 TestAmerica Nashville Page 18 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-133738-A-1-E MSD Matrix: Solid Prep Type: TCLP Analysis Batch: 449643 Toluene-d8 (Surr)70 -130 Surrogate 96 MSD MSD Qualifier Limits%Recovery Method: 8270D - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 490-449026/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 RL MDL Acenaphthene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Acenaphthylene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Anthracene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Benzo[a]anthracene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Benzo[a]pyrene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Benzo[b]fluoranthene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Benzo[g,h,i]perylene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Benzo[k]fluoranthene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Bis(2-chloroethoxy)methane ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Bis(2-chloroethyl)ether ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1bis (2-chloroisopropyl) ether ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Bis(2-ethylhexyl) phthalate ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 14-Bromophenyl phenyl ether ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Butyl benzyl phthalate ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Carbazole ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 14-Chloroaniline ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 14-Chloro-3-methylphenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12-Chloronaphthalene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12-Chlorophenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 14-Chlorophenyl phenyl ether ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Chrysene ND 0.666 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Cresols ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Dibenz(a,h)anthracene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Dibenzofuran ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 11,2-Dichlorobenzene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 11,3-Dichlorobenzene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 11,4-Dichlorobenzene ND 0.670 mg/Kg 07/31/17 09:32 07/31/17 16:48 13,3'-Dichlorobenzidine ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12,4-Dichlorophenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Diethyl phthalate ND 0.670 mg/Kg 07/31/17 09:32 07/31/17 16:48 12,4-Dimethylphenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Dimethyl phthalate ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Di-n-butyl phthalate ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 14,6-Dinitro-2-methylphenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12,4-Dinitrophenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12,4-Dinitrotoluene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12,6-Dinitrotoluene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Di-n-octyl phthalate ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Fluoranthene TestAmerica Nashville Page 19 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-449026/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 RL MDL Fluorene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Hexachlorobenzene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Hexachlorobutadiene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Hexachlorocyclopentadiene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Hexachloroethane ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Indeno[1,2,3-cd]pyrene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Isophorone ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 11-Methylnaphthalene ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 12-Methylnaphthalene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12-Methylphenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 13 & 4 Methylphenol ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Naphthalene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12-Nitroaniline ND 0.670 mg/Kg 07/31/17 09:32 07/31/17 16:48 13-Nitroaniline ND 0.670 mg/Kg 07/31/17 09:32 07/31/17 16:48 14-Nitroaniline ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Nitrobenzene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12-Nitrophenol ND 0.670 mg/Kg 07/31/17 09:32 07/31/17 16:48 14-Nitrophenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1N-Nitrosodi-n-propylamine ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1n-Nitrosodiphenylamine(as diphenylamine) ND 0.670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Pentachlorophenol ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Phenanthrene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Phenol ND 0.0670 mg/Kg 07/31/17 09:32 07/31/17 16:48 1Pyrene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 11,2,4-Trichlorobenzene ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12,4,5-Trichlorophenol ND 0.333 mg/Kg 07/31/17 09:32 07/31/17 16:48 12,4,6-Trichlorophenol 2-Fluorobiphenyl (Surr)66 29-120 07/31/17 16:48 1 MB MB Surrogate 07/31/17 09:32 Dil FacPreparedAnalyzedQualifierLimits%Recovery 60 07/31/17 09:32 07/31/17 16:48 12-Fluorophenol (Surr)10-120 62 07/31/17 09:32 07/31/17 16:48 1Nitrobenzene-d5 (Surr)27-120 62 07/31/17 09:32 07/31/17 16:48 1Phenol-d5 (Surr)10-120 70 07/31/17 09:32 07/31/17 16:48 1Terphenyl-d14 (Surr)13-120 58 07/31/17 09:32 07/31/17 16:48 12,4,6-Tribromophenol (Surr)10-120 Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449026/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 Acenaphthene 1.67 1.190 mg/Kg 71 36-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Acenaphthylene 1.67 1.162 mg/Kg 70 38-120 Anthracene 1.67 1.190 mg/Kg 71 46-124 Benzo[a]anthracene 1.67 1.219 mg/Kg 73 45-120 Benzo[a]pyrene 1.67 1.111 mg/Kg 67 45-120 Benzo[b]fluoranthene 1.67 1.083 mg/Kg 65 42-120 TestAmerica Nashville Page 20 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449026/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 Benzo[g,h,i]perylene 1.67 1.156 mg/Kg 69 38-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Benzo[k]fluoranthene 1.67 1.330 mg/Kg 80 42-120 Bis(2-chloroethoxy)methane 1.67 0.9935 mg/Kg 60 32-120 Bis(2-chloroethyl)ether 1.67 0.9520 mg/Kg 57 31-120 bis (2-chloroisopropyl) ether 1.67 0.7396 mg/Kg 44 32-120 Bis(2-ethylhexyl) phthalate 1.67 1.127 mg/Kg 68 43-120 4-Bromophenyl phenyl ether 1.67 1.151 mg/Kg 69 40-120 Butyl benzyl phthalate 1.67 1.080 mg/Kg 65 43-133 Carbazole 1.67 1.227 mg/Kg 74 44-120 4-Chloroaniline 1.67 0.7410 mg/Kg 44 35-120 4-Chloro-3-methylphenol 1.67 1.283 mg/Kg 77 38-120 2-Chloronaphthalene 1.67 1.120 mg/Kg 67 34-120 2-Chlorophenol 1.67 1.093 mg/Kg 66 32-120 4-Chlorophenyl phenyl ether 1.67 1.223 mg/Kg 73 42-120 Chrysene 1.67 1.234 mg/Kg 74 43-120 Cresols 3.33 2.195 mg/Kg 66 36-129 Dibenz(a,h)anthracene 1.67 1.181 mg/Kg 71 32-128 Dibenzofuran 1.67 1.183 mg/Kg 71 41-120 1,2-Dichlorobenzene 1.67 1.070 mg/Kg 64 33-120 1,3-Dichlorobenzene 1.67 1.023 mg/Kg 61 32-120 1,4-Dichlorobenzene 1.67 1.045 mg/Kg 63 32-120 3,3'-Dichlorobenzidine 1.67 1.171 mg/Kg 70 39-120 2,4-Dichlorophenol 1.67 1.155 mg/Kg 69 32-120 Diethyl phthalate 1.67 1.310 mg/Kg 79 41-122 2,4-Dimethylphenol 1.67 0.8047 mg/Kg 48 32-120 Dimethyl phthalate 1.67 1.277 mg/Kg 77 55-120 Di-n-butyl phthalate 1.67 1.314 mg/Kg 79 46-127 4,6-Dinitro-2-methylphenol 3.33 2.715 mg/Kg 81 27-134 2,4-Dinitrophenol 3.33 2.600 mg/Kg 78 10-142 2,4-Dinitrotoluene 1.67 1.316 mg/Kg 79 43-120 2,6-Dinitrotoluene 1.67 1.362 mg/Kg 82 43-120 Di-n-octyl phthalate 1.67 1.212 mg/Kg 73 40-130 Fluoranthene 1.67 1.322 mg/Kg 79 46-120 Fluorene 1.67 1.252 mg/Kg 75 42-120 Hexachlorobenzene 1.67 1.273 mg/Kg 76 44-120 Hexachlorobutadiene 1.67 1.190 mg/Kg 71 31-120 Hexachlorocyclopentadiene 1.67 ND *mg/Kg 3 24-120 Hexachloroethane 1.67 0.9730 mg/Kg 58 33-120 Indeno[1,2,3-cd]pyrene 1.67 1.169 mg/Kg 70 41-121 Isophorone 1.67 0.5972 mg/Kg 36 33-120 1-Methylnaphthalene 1.67 1.152 mg/Kg 69 32-120 2-Methylnaphthalene 1.67 1.136 mg/Kg 68 28-120 2-Methylphenol 1.67 1.077 mg/Kg 65 36-120 3 & 4 Methylphenol 1.67 1.118 mg/Kg 67 37-120 Naphthalene 1.67 1.088 mg/Kg 65 32-120 2-Nitroaniline 1.67 1.172 mg/Kg 70 40-120 3-Nitroaniline 1.67 1.102 mg/Kg 66 42-120 4-Nitroaniline 1.67 1.200 mg/Kg 72 43-120 TestAmerica Nashville Page 21 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449026/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 Nitrobenzene 1.67 0.9672 mg/Kg 58 26-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits 2-Nitrophenol 1.67 1.252 mg/Kg 75 29-120 4-Nitrophenol 3.33 2.485 mg/Kg 75 32-136 N-Nitrosodi-n-propylamine 1.67 1.025 mg/Kg 62 35-120 n-Nitrosodiphenylamine(as diphenylamine) 1.42 1.110 mg/Kg 78 52-140 Pentachlorophenol 3.33 2.519 mg/Kg 76 44-134 Phenanthrene 1.67 1.219 mg/Kg 73 45-120 Phenol 1.67 1.076 mg/Kg 65 30-120 Pyrene 1.67 1.131 mg/Kg 68 43-120 1,2,4-Trichlorobenzene 1.67 1.150 mg/Kg 69 29-120 2,4,5-Trichlorophenol 1.67 1.302 mg/Kg 78 39-120 2,4,6-Trichlorophenol 1.67 1.239 mg/Kg 74 39-120 2-Fluorobiphenyl (Surr)29 -120 Surrogate 63 LCS LCS Qualifier Limits%Recovery 582-Fluorophenol (Surr)10 -120 62Nitrobenzene-d5 (Surr)27 -120 63Phenol-d5 (Surr)10 -120 69Terphenyl-d14 (Surr)13 -120 752,4,6-Tribromophenol (Surr)10 -120 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-449026/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 Acenaphthene 1.67 1.132 mg/Kg 68 36-120 5 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Acenaphthylene 1.67 1.102 mg/Kg 66 38-120 5 50 Anthracene 1.67 1.138 mg/Kg 68 46-124 5 49 Benzo[a]anthracene 1.67 1.159 mg/Kg 70 45-120 5 50 Benzo[a]pyrene 1.67 1.065 mg/Kg 64 45-120 4 50 Benzo[b]fluoranthene 1.67 1.038 mg/Kg 62 42-120 4 50 Benzo[g,h,i]perylene 1.67 1.092 mg/Kg 66 38-120 6 50 Benzo[k]fluoranthene 1.67 1.298 mg/Kg 78 42-120 2 45 Bis(2-chloroethoxy)methane 1.67 0.9617 mg/Kg 58 32-120 3 50 Bis(2-chloroethyl)ether 1.67 0.9150 mg/Kg 55 31-120 4 50 bis (2-chloroisopropyl) ether 1.67 0.7118 mg/Kg 43 32-120 4 50 Bis(2-ethylhexyl) phthalate 1.67 1.080 mg/Kg 65 43-120 4 50 4-Bromophenyl phenyl ether 1.67 1.108 mg/Kg 66 40-120 4 37 Butyl benzyl phthalate 1.67 1.019 mg/Kg 61 43-133 6 50 Carbazole 1.67 1.164 mg/Kg 70 44-120 5 46 4-Chloroaniline 1.67 0.7229 mg/Kg 43 35-120 2 50 4-Chloro-3-methylphenol 1.67 1.215 mg/Kg 73 38-120 6 49 2-Chloronaphthalene 1.67 1.057 mg/Kg 63 34-120 6 50 2-Chlorophenol 1.67 1.011 mg/Kg 61 32-120 8 50 4-Chlorophenyl phenyl ether 1.67 1.159 mg/Kg 70 42-120 5 50 Chrysene 1.67 1.176 mg/Kg 71 43-120 5 49 TestAmerica Nashville Page 22 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-449026/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 Cresols 3.33 2.043 mg/Kg 61 36-129 7 50 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Dibenz(a,h)anthracene 1.67 1.123 mg/Kg 67 32-128 5 50 Dibenzofuran 1.67 1.131 mg/Kg 68 41-120 4 50 1,2-Dichlorobenzene 1.67 1.001 mg/Kg 60 33-120 7 50 1,3-Dichlorobenzene 1.67 0.9812 mg/Kg 59 32-120 4 50 1,4-Dichlorobenzene 1.67 1.002 mg/Kg 60 32-120 4 50 3,3'-Dichlorobenzidine 1.67 1.121 mg/Kg 67 39-120 4 50 2,4-Dichlorophenol 1.67 1.103 mg/Kg 66 32-120 5 50 Diethyl phthalate 1.67 1.246 mg/Kg 75 41-122 5 45 2,4-Dimethylphenol 1.67 0.7653 mg/Kg 46 32-120 5 50 Dimethyl phthalate 1.67 1.214 mg/Kg 73 55-120 5 46 Di-n-butyl phthalate 1.67 1.256 mg/Kg 75 46-127 5 49 4,6-Dinitro-2-methylphenol 3.33 2.631 mg/Kg 79 27-134 3 50 2,4-Dinitrophenol 3.33 2.506 mg/Kg 75 10-142 4 50 2,4-Dinitrotoluene 1.67 1.255 mg/Kg 75 43-120 5 50 2,6-Dinitrotoluene 1.67 1.306 mg/Kg 78 43-120 4 50 Di-n-octyl phthalate 1.67 1.175 mg/Kg 70 40-130 3 50 Fluoranthene 1.67 1.274 mg/Kg 76 46-120 4 50 Fluorene 1.67 1.174 mg/Kg 70 42-120 6 50 Hexachlorobenzene 1.67 1.224 mg/Kg 73 44-120 4 50 Hexachlorobutadiene 1.67 1.124 mg/Kg 67 31-120 6 50 Hexachlorocyclopentadiene 1.67 ND *mg/Kg 3 24-120 13 50 Hexachloroethane 1.67 0.9207 mg/Kg 55 33-120 6 50 Indeno[1,2,3-cd]pyrene 1.67 1.115 mg/Kg 67 41-121 5 50 Isophorone 1.67 0.5868 mg/Kg 35 33-120 2 50 1-Methylnaphthalene 1.67 1.101 mg/Kg 66 32-120 5 50 2-Methylnaphthalene 1.67 1.089 mg/Kg 65 28-120 4 50 2-Methylphenol 1.67 0.9913 mg/Kg 59 36-120 8 50 3 & 4 Methylphenol 1.67 1.052 mg/Kg 63 37-120 6 50 Naphthalene 1.67 1.044 mg/Kg 63 32-120 4 50 2-Nitroaniline 1.67 1.114 mg/Kg 67 40-120 5 50 3-Nitroaniline 1.67 1.055 mg/Kg 63 42-120 4 49 4-Nitroaniline 1.67 1.152 mg/Kg 69 43-120 4 49 Nitrobenzene 1.67 0.9248 mg/Kg 55 26-120 4 50 2-Nitrophenol 1.67 1.196 mg/Kg 72 29-120 5 50 4-Nitrophenol 3.33 2.381 mg/Kg 71 32-136 4 45 N-Nitrosodi-n-propylamine 1.67 1.012 mg/Kg 61 35-120 1 50 n-Nitrosodiphenylamine(as diphenylamine) 1.42 1.068 mg/Kg 75 52-140 4 50 Pentachlorophenol 3.33 2.429 mg/Kg 73 44-134 4 50 Phenanthrene 1.67 1.144 mg/Kg 69 45-120 6 50 Phenol 1.67 1.007 mg/Kg 60 30-120 7 50 Pyrene 1.67 1.069 mg/Kg 64 43-120 6 50 1,2,4-Trichlorobenzene 1.67 1.081 mg/Kg 65 29-120 6 50 2,4,5-Trichlorophenol 1.67 1.227 mg/Kg 74 39-120 6 50 2,4,6-Trichlorophenol 1.67 1.173 mg/Kg 70 39-120 5 50 TestAmerica Nashville Page 23 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-449026/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449182 Prep Batch: 449026 2-Fluorobiphenyl (Surr)29 -120 Surrogate 67 LCSD LCSD Qualifier Limits%Recovery 622-Fluorophenol (Surr)10 -120 68Nitrobenzene-d5 (Surr)27 -120 68Phenol-d5 (Surr)10 -120 73Terphenyl-d14 (Surr)13 -120 802,4,6-Tribromophenol (Surr)10 -120 Method: 6010D - Metals (ICP) Client Sample ID: Method BlankLab Sample ID: MB 490-448938/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 448979 Prep Batch: 448938 RL MDL Arsenic ND ^0.0500 mg/L 07/30/17 13:07 07/31/17 00:28 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 1.00 mg/L 07/30/17 13:07 07/31/17 00:28 1Barium ND 0.0100 mg/L 07/30/17 13:07 07/31/17 00:28 1Cadmium ND 0.0500 mg/L 07/30/17 13:07 07/31/17 00:28 1Chromium ND 0.0500 mg/L 07/30/17 13:07 07/31/17 00:28 1Lead ND 0.0100 mg/L 07/30/17 13:07 07/31/17 00:28 1Selenium ND 0.0500 mg/L 07/30/17 13:07 07/31/17 00:28 1Silver Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-448938/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 448979 Prep Batch: 448938 Arsenic 0.200 0.1829 ^mg/L 91 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Barium 2.00 1.800 mg/L 90 80-120 Cadmium 0.200 0.1807 mg/L 90 80-120 Chromium 1.00 0.9069 mg/L 91 80-120 Lead 1.00 0.9036 mg/L 90 80-120 Selenium 0.200 0.1699 mg/L 85 80-120 Silver 0.200 0.1754 mg/L 88 80-120 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-448938/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 448979 Prep Batch: 448938 Arsenic 0.200 0.1929 ^mg/L 96 80-120 5 20 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Barium 2.00 1.926 mg/L 96 80-120 7 20 Cadmium 0.200 0.1937 mg/L 97 80-120 7 20 Chromium 1.00 0.9714 mg/L 97 80-120 7 20 Lead 1.00 0.9653 mg/L 97 80-120 7 20 Selenium 0.200 0.1853 mg/L 93 80-120 9 20 Silver 0.200 0.1886 mg/L 94 80-120 7 20 TestAmerica Nashville Page 24 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 6010D - Metals (ICP) (Continued) Client Sample ID: Method BlankLab Sample ID: MB 490-449616/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449842 Prep Batch: 449616 RL MDL Arsenic ND 1.95 mg/Kg 08/02/17 09:49 08/02/17 21:00 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.973 mg/Kg 08/02/17 09:49 08/02/17 21:00 1Cadmium ND 0.973 mg/Kg 08/02/17 09:49 08/02/17 21:00 1Chromium ND 0.973 mg/Kg 08/02/17 09:49 08/02/17 21:00 1Lead ND ^1.95 mg/Kg 08/02/17 09:49 08/02/17 21:00 1Selenium Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449616/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449842 Prep Batch: 449616 Arsenic 19.0 17.60 mg/Kg 92 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Cadmium 19.0 18.38 mg/Kg 97 80-120 Chromium 19.0 18.25 mg/Kg 96 80-120 Lead 19.0 18.29 mg/Kg 96 80-120 Selenium 19.0 17.85 ^mg/Kg 94 80-120 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-449616/26-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449842 Prep Batch: 449616 Arsenic 19.7 19.47 mg/Kg 99 80-120 10 20 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Cadmium 19.7 20.08 mg/Kg 102 80-120 9 20 Chromium 19.7 19.86 mg/Kg 101 80-120 8 20 Lead 19.7 19.82 mg/Kg 100 80-120 8 20 Selenium 19.7 19.31 ^mg/Kg 98 80-120 8 20 Client Sample ID: Matrix SpikeLab Sample ID: 490-133390-F-27-C MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 449842 Prep Batch: 449616 Arsenic 5.80 22.1 26.97 mg/Kg 96 75-125☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Cadmium ND 22.1 19.77 mg/Kg 88 75-125☼ Chromium 13.1 22.1 34.14 mg/Kg 95 75-125☼ Lead 20.2 F1 22.1 38.32 mg/Kg 82 75-125☼ Selenium ND ^22.1 19.46 ^mg/Kg 88 75-125☼ Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-133390-F-27-D MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 449842 Prep Batch: 449616 Arsenic 5.80 21.9 24.13 mg/Kg 84 75-125 11 20☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Cadmium ND 21.9 19.99 mg/Kg 90 75-125 1 20☼ Chromium 13.1 21.9 30.56 mg/Kg 80 75-125 11 20☼ Lead 20.2 F1 21.9 36.22 F1 mg/Kg 73 75-125 6 20☼ Selenium ND ^21.9 17.75 ^mg/Kg 81 75-125 9 20☼ TestAmerica Nashville Page 25 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Client Sample ID: Method BlankLab Sample ID: MB 490-451021/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 451197 Prep Batch: 451021 RL MDL Barium ND 1.97 mg/Kg 08/08/17 12:01 08/08/17 18:30 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 0.984 mg/Kg 08/08/17 12:01 08/08/17 18:30 1Silver Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-451021/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 451197 Prep Batch: 451021 Barium 20.0 21.54 mg/Kg 108 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Silver 20.0 16.75 mg/Kg 84 80-120 Client Sample ID: Drum CompositeLab Sample ID: 490-133655-1 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 451197 Prep Batch: 451021 Barium 53.3 24.5 76.09 mg/Kg 93 75-125☼ Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Silver ND 24.5 23.91 mg/Kg 97 75-125☼ Client Sample ID: Drum CompositeLab Sample ID: 490-133655-1 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 451197 Prep Batch: 451021 Barium 53.3 23.3 72.04 mg/Kg 80 75-125 5 20☼ Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Silver ND 23.3 21.82 mg/Kg 94 75-125 9 20☼ Client Sample ID: Method BlankLab Sample ID: LB 490-448730/1-B Matrix: Solid Prep Type: TCLP Analysis Batch: 448979 Prep Batch: 448938 RL MDL Arsenic ND ^0.500 mg/L 07/30/17 13:07 07/31/17 00:54 1 LB LB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier ND 10.0 mg/L 07/30/17 13:07 07/31/17 00:54 1Barium ND 0.100 mg/L 07/30/17 13:07 07/31/17 00:54 1Cadmium ND 0.500 mg/L 07/30/17 13:07 07/31/17 00:54 1Chromium ND 0.500 mg/L 07/30/17 13:07 07/31/17 00:54 1Lead ND 0.100 mg/L 07/30/17 13:07 07/31/17 00:54 1Selenium ND 0.500 mg/L 07/30/17 13:07 07/31/17 00:54 1Silver Client Sample ID: Matrix SpikeLab Sample ID: 490-133424-G-1-F MS Matrix: Solid Prep Type: TCLP Analysis Batch: 448979 Prep Batch: 448938 Arsenic ND ^2.00 1.873 ^mg/L 94 75-125 Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Barium ND 20.0 18.48 mg/L 90 75-125 Cadmium ND 2.00 1.782 mg/L 89 75-125 Chromium ND 10.0 8.945 mg/L 89 75-125 Lead ND 10.0 8.854 mg/L 89 75-125 Selenium ND 2.00 1.854 mg/L 90 75-125 TestAmerica Nashville Page 26 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 6010D - Metals (ICP) (Continued) Client Sample ID: Matrix SpikeLab Sample ID: 490-133424-G-1-F MS Matrix: Solid Prep Type: TCLP Analysis Batch: 448979 Prep Batch: 448938 Silver ND 2.00 1.820 mg/L 91 75-125 Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-133424-G-1-G MSD Matrix: Solid Prep Type: TCLP Analysis Batch: 448979 Prep Batch: 448938 Arsenic ND ^2.00 1.882 ^mg/L 94 75-125 0 20 Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Barium ND 20.0 18.72 mg/L 91 75-125 1 20 Cadmium ND 2.00 1.783 mg/L 89 75-125 0 20 Chromium ND 10.0 9.073 mg/L 91 75-125 1 20 Lead ND 10.0 8.948 mg/L 89 75-125 1 20 Selenium ND 2.00 1.919 mg/L 93 75-125 3 20 Silver ND 2.00 1.815 mg/L 91 75-125 0 20 Method: 7470A - Mercury (CVAA) Client Sample ID: Method BlankLab Sample ID: MB 490-449420/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449514 Prep Batch: 449420 RL MDL Mercury ND 0.000200 mg/L 08/01/17 10:58 08/01/17 17:28 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449420/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449514 Prep Batch: 449420 Mercury 0.00200 0.001967 mg/L 98 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Method BlankLab Sample ID: LB 490-448730/1-G Matrix: Solid Prep Type: TCLP Analysis Batch: 449514 Prep Batch: 449420 RL MDL Mercury ND 0.00200 mg/L 08/01/17 10:58 08/01/17 17:32 1 LB LB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Matrix SpikeLab Sample ID: 500-130395-A-12-D MS Matrix: Solid Prep Type: TCLP Analysis Batch: 449514 Prep Batch: 449420 Mercury ND 0.0200 0.02010 mg/L 100 75-125 Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits TestAmerica Nashville Page 27 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Sample Results TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method: 7470A - Mercury (CVAA) (Continued) Client Sample ID: Matrix Spike DuplicateLab Sample ID: 500-130395-A-12-E MSD Matrix: Solid Prep Type: TCLP Analysis Batch: 449514 Prep Batch: 449420 Mercury ND 0.0200 0.01906 mg/L 95 75-125 5 20 Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Method: 7471B - Mercury (CVAA) Client Sample ID: Method BlankLab Sample ID: MB 490-449187/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449260 Prep Batch: 449187 RL MDL Mercury ND 0.0966 mg/Kg 07/31/17 14:52 07/31/17 20:03 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-449187/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449260 Prep Batch: 449187 Mercury 0.160 0.1574 mg/Kg 98 80-120 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec. Limits Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-449187/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 449260 Prep Batch: 449187 Mercury 0.163 0.1486 mg/Kg 91 80-120 6 20 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec. Limits LimitRPD RPD Client Sample ID: Matrix SpikeLab Sample ID: 490-132661-B-9-B MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 449260 Prep Batch: 449187 Mercury ND 0.162 0.1440 mg/Kg 89 80-120 Analyte MS MS DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-132661-B-9-C MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 449260 Prep Batch: 449187 Mercury ND 0.164 0.1545 mg/Kg 94 80-120 7 20 Analyte MSD MSD DUnitResultQualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits LimitRPD RPD Method: Moisture - Percent Moisture Client Sample ID: DuplicateLab Sample ID: 490-133716-A-2 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 448928 Percent Solids 98.3 98.5 %0.2 20 Analyte DU DU DUnitResultQualifier Sample Result Sample Qualifier LimitRPD RPD TestAmerica Nashville Page 28 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 GC/MS VOA Prep Batch: 448920 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 5035490-133655-1 Drum Composite Total/NA Analysis Batch: 449039 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B 448920490-133655-1 Drum Composite Total/NA Solid 8260BMB 490-449039/9 Method Blank Total/NA Solid 8260BLCS 490-449039/3 Lab Control Sample Total/NA Solid 8260BLCSD 490-449039/4 Lab Control Sample Dup Total/NA Leach Batch: 449399 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 1311490-133738-A-1-E MS Matrix Spike TCLP Solid 1311490-133738-A-1-E MSD Matrix Spike Duplicate TCLP Leach Batch: 449520 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 1311490-133655-1 Drum Composite TCLP Solid 1311LB 490-449520/1-A Method Blank TCLP Analysis Batch: 449643 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8260B 449520490-133655-1 Drum Composite TCLP Solid 8260B 449520LB 490-449520/1-A Method Blank TCLP Solid 8260BMB 490-449643/6 Method Blank Total/NA Solid 8260BLCS 490-449643/4 Lab Control Sample Total/NA Solid 8260B 449399490-133738-A-1-E MS Matrix Spike TCLP Solid 8260B 449399490-133738-A-1-E MSD Matrix Spike Duplicate TCLP GC/MS Semi VOA Prep Batch: 449026 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3550C490-133655-1 Drum Composite Total/NA Solid 3550CMB 490-449026/1-A Method Blank Total/NA Solid 3550CLCS 490-449026/2-A Lab Control Sample Total/NA Solid 3550CLCSD 490-449026/3-A Lab Control Sample Dup Total/NA Analysis Batch: 449182 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 8270D 449026490-133655-1 Drum Composite Total/NA Solid 8270D 449026MB 490-449026/1-A Method Blank Total/NA Solid 8270D 449026LCS 490-449026/2-A Lab Control Sample Total/NA Solid 8270D 449026LCSD 490-449026/3-A Lab Control Sample Dup Total/NA Metals Leach Batch: 448730 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 1311490-133655-1 Drum Composite TCLP Solid 1311LB 490-448730/1-B Method Blank TCLP TestAmerica Nashville Page 29 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Metals (Continued) Leach Batch: 448730 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 1311LB 490-448730/1-G Method Blank TCLP Solid 1311490-133424-G-1-F MS Matrix Spike TCLP Solid 1311490-133424-G-1-G MSD Matrix Spike Duplicate TCLP Solid 1311500-130395-A-12-D MS Matrix Spike TCLP Solid 1311500-130395-A-12-E MSD Matrix Spike Duplicate TCLP Prep Batch: 448938 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3010A 448730490-133655-1 Drum Composite TCLP Solid 3010A 448730LB 490-448730/1-B Method Blank TCLP Solid 3010AMB 490-448938/1-A Method Blank Total/NA Solid 3010ALCS 490-448938/2-A Lab Control Sample Total/NA Solid 3010ALCSD 490-448938/3-A Lab Control Sample Dup Total/NA Solid 3010A 448730490-133424-G-1-F MS Matrix Spike TCLP Solid 3010A 448730490-133424-G-1-G MSD Matrix Spike Duplicate TCLP Analysis Batch: 448979 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 448938490-133655-1 Drum Composite TCLP Solid 6010D 448938LB 490-448730/1-B Method Blank TCLP Solid 6010D 448938MB 490-448938/1-A Method Blank Total/NA Solid 6010D 448938LCS 490-448938/2-A Lab Control Sample Total/NA Solid 6010D 448938LCSD 490-448938/3-A Lab Control Sample Dup Total/NA Solid 6010D 448938490-133424-G-1-F MS Matrix Spike TCLP Solid 6010D 448938490-133424-G-1-G MSD Matrix Spike Duplicate TCLP Analysis Batch: 449171 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 448938490-133655-1 Drum Composite TCLP Prep Batch: 449187 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B490-133655-1 Drum Composite Total/NA Solid 7471BMB 490-449187/1-A Method Blank Total/NA Solid 7471BLCS 490-449187/2-A Lab Control Sample Total/NA Solid 7471BLCSD 490-449187/3-A Lab Control Sample Dup Total/NA Solid 7471B490-132661-B-9-B MS Matrix Spike Total/NA Solid 7471B490-132661-B-9-C MSD Matrix Spike Duplicate Total/NA Analysis Batch: 449260 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7471B 449187490-133655-1 Drum Composite Total/NA Solid 7471B 449187MB 490-449187/1-A Method Blank Total/NA Solid 7471B 449187LCS 490-449187/2-A Lab Control Sample Total/NA Solid 7471B 449187LCSD 490-449187/3-A Lab Control Sample Dup Total/NA Solid 7471B 449187490-132661-B-9-B MS Matrix Spike Total/NA Solid 7471B 449187490-132661-B-9-C MSD Matrix Spike Duplicate Total/NA Prep Batch: 449420 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7470A 448730490-133655-1 Drum Composite TCLP TestAmerica Nashville Page 30 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Metals (Continued) Prep Batch: 449420 (Continued) Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7470A 448730LB 490-448730/1-G Method Blank TCLP Solid 7470AMB 490-449420/1-A Method Blank Total/NA Solid 7470ALCS 490-449420/2-A Lab Control Sample Total/NA Solid 7470A 448730500-130395-A-12-D MS Matrix Spike TCLP Solid 7470A 448730500-130395-A-12-E MSD Matrix Spike Duplicate TCLP Analysis Batch: 449514 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 7470A 449420490-133655-1 Drum Composite TCLP Solid 7470A 449420LB 490-448730/1-G Method Blank TCLP Solid 7470A 449420MB 490-449420/1-A Method Blank Total/NA Solid 7470A 449420LCS 490-449420/2-A Lab Control Sample Total/NA Solid 7470A 449420500-130395-A-12-D MS Matrix Spike TCLP Solid 7470A 449420500-130395-A-12-E MSD Matrix Spike Duplicate TCLP Prep Batch: 449616 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3051A490-133655-1 Drum Composite Total/NA Solid 3051AMB 490-449616/1-A Method Blank Total/NA Solid 3051ALCS 490-449616/2-A Lab Control Sample Total/NA Solid 3051ALCSD 490-449616/26-A Lab Control Sample Dup Total/NA Solid 3051A490-133390-F-27-C MS Matrix Spike Total/NA Solid 3051A490-133390-F-27-D MSD Matrix Spike Duplicate Total/NA Analysis Batch: 449842 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 449616490-133655-1 Drum Composite Total/NA Solid 6010D 449616MB 490-449616/1-A Method Blank Total/NA Solid 6010D 449616LCS 490-449616/2-A Lab Control Sample Total/NA Solid 6010D 449616LCSD 490-449616/26-A Lab Control Sample Dup Total/NA Solid 6010D 449616490-133390-F-27-C MS Matrix Spike Total/NA Solid 6010D 449616490-133390-F-27-D MSD Matrix Spike Duplicate Total/NA Prep Batch: 451021 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 3051A490-133655-1 Drum Composite Total/NA Solid 3051AMB 490-451021/1-A Method Blank Total/NA Solid 3051ALCS 490-451021/2-A Lab Control Sample Total/NA Solid 3051A490-133655-1 MS Drum Composite Total/NA Solid 3051A490-133655-1 MSD Drum Composite Total/NA Analysis Batch: 451197 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid 6010D 451021490-133655-1 Drum Composite Total/NA Solid 6010D 451021MB 490-451021/1-A Method Blank Total/NA Solid 6010D 451021LCS 490-451021/2-A Lab Control Sample Total/NA Solid 6010D 451021490-133655-1 MS Drum Composite Total/NA Solid 6010D 451021490-133655-1 MSD Drum Composite Total/NA TestAmerica Nashville Page 31 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 QC Association Summary TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 General Chemistry Analysis Batch: 448928 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Solid Moisture490-133655-1 Drum Composite Total/NA Solid Moisture490-133555-A-1 MS Matrix Spike Total/NA Solid Moisture490-133555-A-1 MSD Matrix Spike Duplicate Total/NA Solid Moisture490-133716-A-2 DU Duplicate Total/NA TestAmerica Nashville Page 32 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Lab Chronicle Client: Hart & Hickman, PC TestAmerica Job ID: 490-133655-1 Project/Site: FMG-005 Client Sample ID: Drum Composite Lab Sample ID: 490-133655-1 Matrix: SolidDate Collected: 07/27/17 12:15 Date Received: 07/28/17 09:10 Leach 1311 SCR08/01/17 19:21 TAL NSH449520 Type Batch Method Batch Prep Type LabAnalystRun Prepared or Analyzed Initial Amount Amount Final Batch NumberFactor Dil TCLP 1.0 g 1.0 mL Analysis 8260B 10 449643 08/02/17 18:34 C1A TAL NSHTCLP10 mL 10 mL Prep 5035 448920 07/27/17 11:15 JLP TAL NSHTotal/NA 6.129 g 5.0 mL Analysis 8260B 1 449039 07/31/17 15:04 SW1 TAL NSHTotal/NA 5 g 5 mL Prep 3550C 449026 07/31/17 09:32 MNM TAL NSHTotal/NA 30.25 g 1.00 mL Analysis 8270D 1 449182 07/31/17 19:02 T1C TAL NSHTotal/NA Leach 1311 448730 07/28/17 21:10 SCR TAL NSHTCLP1.0 g 1.0 mL Prep 3010A 448938 07/30/17 13:07 AJK TAL NSHTCLP5 mL 50 mL Analysis 6010D 1 448979 07/31/17 02:02 LCS TAL NSHTCLP Leach 1311 448730 07/28/17 21:10 SCR TAL NSHTCLP1.0 g 1.0 mL Prep 3010A 448938 07/30/17 13:07 AJK TAL NSHTCLP5 mL 50 mL Analysis 6010D 1 449171 07/31/17 12:02 LCS TAL NSHTCLP Prep 3051A 451021 08/08/17 12:01 BVH TAL NSHTotal/NA 0.525 g 100 mL Analysis 6010D 1 451197 08/08/17 18:56 RDF TAL NSHTotal/NA Prep 3051A 449616 08/02/17 09:49 BVH TAL NSHTotal/NA 0.508 g 100 mL Analysis 6010D 1 449842 08/02/17 22:01 LCS TAL NSHTotal/NA Leach 1311 448730 07/28/17 21:10 SCR TAL NSHTCLP1.0 g 1.0 mL Prep 7470A 449420 08/01/17 10:58 RDF TAL NSHTCLP3 mL 30 mL Analysis 7470A 1 449514 08/01/17 17:41 RDF TAL NSHTCLP Prep 7471B 449187 07/31/17 14:52 RDF TAL NSHTotal/NA 0.598 g 100 mL Analysis 7471B 1 449260 07/31/17 20:41 RDF TAL NSHTotal/NA Analysis Moisture 1 448928 07/30/17 11:16 BAA TAL NSHTotal/NA Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 33 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Method Summary TestAmerica Job ID: 490-133655-1Client: Hart & Hickman, PC Project/Site: FMG-005 Method Method Description LaboratoryProtocol SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH SW8466010DMetals (ICP)TAL NSH SW8467470AMercury (CVAA)TAL NSH SW8467471BMercury (CVAA)TAL NSH EPAMoisturePercent Moisture TAL NSH Protocol References: EPA = US Environmental Protection Agency SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177 TestAmerica Nashville Page 34 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Accreditation/Certification Summary Client: Hart & Hickman, PC TestAmerica Job ID: 490-133655-1 Project/Site: FMG-005 Laboratory: TestAmerica Nashville Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program EPA Region Identification Number Expiration Date North Carolina (WW/SW)3874State Program 12-31-17 Analysis Method Prep Method Matrix Analyte The following analytes are included in this report, but accreditation/certification is not offered by the governing authority: Moisture Solid Percent Solids TestAmerica Nashville Page 35 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 36 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Page 37 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Login Sample Receipt Checklist Client: Hart & Hickman, PC Job Number: 490-133655-1 Login Number: 133655 Question Answer Comment Creator: Vest, Laura E List Source: TestAmerica Nashville List Number: 1 N/ARadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. N/ASample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. N/ASample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. N/AResidual Chlorine Checked. TestAmerica Nashville Page 38 of 38 8/10/2017 1 2 3 4 5 6 7 8 9 10 11 12 13 Appendix D Drum Disposal Documentation