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HomeMy WebLinkAbout10010 Dixe Trucking MW Sampling Letter Report 20110117 Hart & Hickman, PC Appendix A Laboratory Analytical Results and Chain of Custody Record 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 December 29, 2010 Client: Attn: Work Order: Project Name: Project Nbr: Date Received: Hart & Hickman (NC) PTT-001 / Former Dixie Trucking NTL2985 12/22/10 Charlotte, NC 28203-5449 Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Steve Hart P/O Nbr: 5:43:19PM SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE AND TIME NTL2985-01HHMW-1 12/21/10 11:10 NTL2985-02Trip Blank 12/21/10 00:01 An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at 1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accreditation. This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you have received this material in error, please notify us immediately at 615-726-0177. North Carolina Certification Number: 387 These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory. Report Approved By: Ken A. Hayes Senior Project Manager The Chain(s) of Custody, 2 pages, are included and are an integral part of this report. Estimated uncertainty is available upon request. This report has been electronically signed. All solids results are reported in wet weight unless specifically stated. Page 1 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 ANALYTICAL REPORT Analyte FlagResult Units Dilution FactorMRL Method Batch Analysis Date/Time Sample ID: NTL2985-01 (HHMW-1 - Water) Sampled: 12/21/10 11:10 Volatile Organic Compounds by EPA Method 8260B 50.0ND 12/25/10 19:301 SW846 8260BAcetoneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BBenzeneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BBromobenzeneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BBromochloromethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BBromodichloromethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BBromoformug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BBromomethaneug/L 10L5947 50.0ND 12/25/10 19:301 SW846 8260B2-Butanone ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Bsec-Butylbenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Bn-Butylbenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Btert-Butylbenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BCarbon disulfide ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BCarbon Tetrachloride ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BChlorobenzeneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BChlorodibromomethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BChloroethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BChloroformug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BChloromethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B2-Chlorotoluene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B4-Chlorotoluene ug/L 10L5947 5.00ND 12/25/10 19:301 SW846 8260B1,2-Dibromo-3-chloropropane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2-Dibromoethane (EDB)ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BDibromomethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,4-Dichlorobenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,3-Dichlorobenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2-Dichlorobenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BDichlorodifluoromethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,1-Dichloroethane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2-Dichloroethane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Bcis-1,2-Dichloroethene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,1-Dichloroethene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Btrans-1,2-Dichloroethene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,3-Dichloropropane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2-Dichloropropane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B2,2-Dichloropropane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Bcis-1,3-Dichloropropene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Btrans-1,3-Dichloropropene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,1-Dichloropropene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BEthylbenzeneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BHexachlorobutadieneug/L 10L5947 50.0ND 12/25/10 19:301 SW846 8260B2-Hexanone ug/L 10L5947 L 1.00ND 12/25/10 19:301 SW846 8260BIsopropylbenzeneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Bp-Isopropyltoluene ug/L 10L5947 Page 2 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 ANALYTICAL REPORT Analyte FlagResult Units Dilution FactorMRL Method Batch Analysis Date/Time Sample ID: NTL2985-01 (HHMW-1 - Water) - cont. Sampled: 12/21/10 11:10 Volatile Organic Compounds by EPA Method 8260B - cont. 1.00ND 12/25/10 19:301 SW846 8260BMethyl tert-Butyl Ether ug/L 10L5947 5.00ND 12/25/10 19:301 SW846 8260BMethylene Chloride ug/L 10L5947 10.0ND 12/25/10 19:301 SW846 8260B4-Methyl-2-pentanone ug/L 10L5947 5.00ND 12/25/10 19:301 SW846 8260BNaphthaleneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260Bn-Propylbenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BStyreneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,1,1,2-Tetrachloroethane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,1,2,2-Tetrachloroethane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BTetrachloroetheneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BTolueneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2,3-Trichlorobenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2,4-Trichlorobenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,1,2-Trichloroethane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,1,1-Trichloroethane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BTrichloroetheneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BTrichlorofluoromethaneug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2,3-Trichloropropane ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,3,5-Trimethylbenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2,4-Trimethylbenzene ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BVinyl chloride ug/L 10L5947 3.00ND 12/25/10 19:301 SW846 8260BXylenes, total ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260BDiisopropyl Ether ug/L 10L5947 1.00ND 12/25/10 19:301 SW846 8260B1,2-Dichloroethene (total)ug/L 10L5947 102 %Surr: 1,2-Dichloroethane-d4 (63-140%)12/25/10 19:30 SW846 8260B 10L5947 100 %Surr: Dibromofluoromethane (73-131%)12/25/10 19:30 SW846 8260B 10L5947 105 %Surr: Toluene-d8 (80-120%)12/25/10 19:30 SW846 8260B 10L5947 96 %Surr: 4-Bromofluorobenzene (79-125%)12/25/10 19:30 SW846 8260B 10L5947 Sample ID: NTL2985-02 (Trip Blank - Water) Sampled: 12/21/10 00:01 Volatile Organic Compounds by EPA Method 8260B 50.0ND 12/24/10 03:041 SW846 8260BAcetoneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BBenzeneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BBromobenzeneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BBromochloromethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BBromodichloromethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BBromoformug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BBromomethaneug/L 10L5751 50.0ND 12/24/10 03:041 SW846 8260B2-Butanone ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Bsec-Butylbenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Bn-Butylbenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Btert-Butylbenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BCarbon disulfide ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BCarbon Tetrachloride ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BChlorobenzeneug/L 10L5751 Page 3 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 ANALYTICAL REPORT Analyte FlagResult Units Dilution FactorMRL Method Batch Analysis Date/Time Sample ID: NTL2985-02 (Trip Blank - Water) - cont. Sampled: 12/21/10 00:01 Volatile Organic Compounds by EPA Method 8260B - cont. 1.00ND 12/24/10 03:041 SW846 8260BChlorodibromomethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BChloroethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BChloroformug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BChloromethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B2-Chlorotoluene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B4-Chlorotoluene ug/L 10L5751 5.00ND 12/24/10 03:041 SW846 8260B1,2-Dibromo-3-chloropropane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2-Dibromoethane (EDB)ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BDibromomethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,4-Dichlorobenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,3-Dichlorobenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2-Dichlorobenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BDichlorodifluoromethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,1-Dichloroethane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2-Dichloroethane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Bcis-1,2-Dichloroethene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,1-Dichloroethene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Btrans-1,2-Dichloroethene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,3-Dichloropropane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2-Dichloropropane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B2,2-Dichloropropane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Bcis-1,3-Dichloropropene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Btrans-1,3-Dichloropropene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,1-Dichloropropene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BEthylbenzeneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BHexachlorobutadieneug/L 10L5751 50.0ND 12/24/10 03:041 SW846 8260B2-Hexanone ug/L 10L5751 L 1.00ND 12/24/10 03:041 SW846 8260BIsopropylbenzeneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Bp-Isopropyltoluene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BMethyl tert-Butyl Ether ug/L 10L5751 5.00ND 12/24/10 03:041 SW846 8260BMethylene Chloride ug/L 10L5751 10.0ND 12/24/10 03:041 SW846 8260B4-Methyl-2-pentanone ug/L 10L5751 5.00ND 12/24/10 03:041 SW846 8260BNaphthaleneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260Bn-Propylbenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BStyreneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,1,1,2-Tetrachloroethane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,1,2,2-Tetrachloroethane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BTetrachloroetheneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BTolueneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2,3-Trichlorobenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2,4-Trichlorobenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,1,2-Trichloroethane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,1,1-Trichloroethane ug/L 10L5751 Page 4 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 ANALYTICAL REPORT Analyte FlagResult Units Dilution FactorMRL Method Batch Analysis Date/Time Sample ID: NTL2985-02 (Trip Blank - Water) - cont. Sampled: 12/21/10 00:01 Volatile Organic Compounds by EPA Method 8260B - cont. 1.00ND 12/24/10 03:041 SW846 8260BTrichloroetheneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BTrichlorofluoromethaneug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2,3-Trichloropropane ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,3,5-Trimethylbenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2,4-Trimethylbenzene ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BVinyl chloride ug/L 10L5751 3.00ND 12/24/10 03:041 SW846 8260BXylenes, total ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260BDiisopropyl Ether ug/L 10L5751 1.00ND 12/24/10 03:041 SW846 8260B1,2-Dichloroethene (total)ug/L 10L5751 91 %Surr: 1,2-Dichloroethane-d4 (63-140%)12/24/10 03:04 SW846 8260B 10L5751 96 %Surr: Dibromofluoromethane (73-131%)12/24/10 03:04 SW846 8260B 10L5751 101 %Surr: Toluene-d8 (80-120%)12/24/10 03:04 SW846 8260B 10L5751 95 %Surr: 4-Bromofluorobenzene (79-125%)12/24/10 03:04 SW846 8260B 10L5751 Page 5 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA Blank Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5751-BLK1 ug/L 10L5751<25.0 10L5751-BLK1 12/24/10 02:09Acetone ug/L 10L5751<0.270 10L5751-BLK1 12/24/10 02:09Benzene ug/L 10L5751<0.220 10L5751-BLK1 12/24/10 02:09Bromobenzene ug/L 10L5751<0.440 10L5751-BLK1 12/24/10 02:09Bromochloromethane ug/L 10L5751<0.370 10L5751-BLK1 12/24/10 02:09Bromodichloromethane ug/L 10L5751<0.220 10L5751-BLK1 12/24/10 02:09Bromoform ug/L 10L5751<0.470 10L5751-BLK1 12/24/10 02:09Bromomethane ug/L 10L5751<1.70 10L5751-BLK1 12/24/10 02:092-Butanone ug/L 10L5751<0.200 10L5751-BLK1 12/24/10 02:09sec-Butylbenzene ug/L 10L5751<0.220 10L5751-BLK1 12/24/10 02:09n-Butylbenzene ug/L 10L5751<0.200 10L5751-BLK1 12/24/10 02:09tert-Butylbenzene ug/L 10L5751<0.290 10L5751-BLK1 12/24/10 02:09Carbon disulfide ug/L 10L5751<0.270 10L5751-BLK1 12/24/10 02:09Carbon Tetrachloride ug/L 10L5751<0.380 10L5751-BLK1 12/24/10 02:09Chlorobenzene ug/L 10L5751<0.300 10L5751-BLK1 12/24/10 02:09Chlorodibromomethane ug/L 10L5751<0.410 10L5751-BLK1 12/24/10 02:09Chloroethane ug/L 10L5751<0.470 10L5751-BLK1 12/24/10 02:09Chloroform ug/L 10L5751<0.180 10L5751-BLK1 12/24/10 02:09Chloromethane ug/L 10L5751<0.250 10L5751-BLK1 12/24/10 02:092-Chlorotoluene ug/L 10L5751<0.270 10L5751-BLK1 12/24/10 02:094-Chlorotoluene ug/L 10L5751<0.200 10L5751-BLK1 12/24/10 02:091,2-Dibromo-3-chloropropane ug/L 10L5751<0.340 10L5751-BLK1 12/24/10 02:091,2-Dibromoethane (EDB) ug/L 10L5751<0.430 10L5751-BLK1 12/24/10 02:09Dibromomethane ug/L 10L5751<0.250 10L5751-BLK1 12/24/10 02:091,4-Dichlorobenzene ug/L 10L5751<0.490 10L5751-BLK1 12/24/10 02:091,3-Dichlorobenzene ug/L 10L5751<0.200 10L5751-BLK1 12/24/10 02:091,2-Dichlorobenzene ug/L 10L5751<0.140 10L5751-BLK1 12/24/10 02:09Dichlorodifluoromethane ug/L 10L5751<0.320 10L5751-BLK1 12/24/10 02:091,1-Dichloroethane ug/L 10L5751<0.380 10L5751-BLK1 12/24/10 02:091,2-Dichloroethane ug/L 10L5751<0.380 10L5751-BLK1 12/24/10 02:09cis-1,2-Dichloroethene ug/L 10L5751<0.360 10L5751-BLK1 12/24/10 02:091,1-Dichloroethene ug/L 10L5751<0.360 10L5751-BLK1 12/24/10 02:09trans-1,2-Dichloroethene ug/L 10L5751<0.280 10L5751-BLK1 12/24/10 02:091,3-Dichloropropane ug/L 10L5751<0.330 10L5751-BLK1 12/24/10 02:091,2-Dichloropropane ug/L 10L5751<0.260 10L5751-BLK1 12/24/10 02:092,2-Dichloropropane ug/L 10L5751<0.190 10L5751-BLK1 12/24/10 02:09cis-1,3-Dichloropropene ug/L 10L5751<0.160 10L5751-BLK1 12/24/10 02:09trans-1,3-Dichloropropene ug/L 10L5751<0.300 10L5751-BLK1 12/24/10 02:091,1-Dichloropropene ug/L 10L5751<0.320 10L5751-BLK1 12/24/10 02:09Ethylbenzene ug/L 10L5751<0.310 10L5751-BLK1 12/24/10 02:09Hexachlorobutadiene ug/L 10L5751<2.20 10L5751-BLK1 12/24/10 02:092-Hexanone Page 6 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA Blank - Cont. Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5751-BLK1 ug/L 10L5751<0.240 10L5751-BLK1 12/24/10 02:09Isopropylbenzene ug/L 10L5751<0.210 10L5751-BLK1 12/24/10 02:09p-Isopropyltoluene ug/L 10L5751<0.320 10L5751-BLK1 12/24/10 02:09Methyl tert-Butyl Ether ug/L 10L5751<0.150 10L5751-BLK1 12/24/10 02:09Methylene Chloride ug/L 10L5751<1.60 10L5751-BLK1 12/24/10 02:094-Methyl-2-pentanone ug/L 10L5751<0.170 10L5751-BLK1 12/24/10 02:09Naphthalene ug/L 10L5751<0.220 10L5751-BLK1 12/24/10 02:09n-Propylbenzene ug/L 10L5751<0.220 10L5751-BLK1 12/24/10 02:09Styrene ug/L 10L5751<0.220 10L5751-BLK1 12/24/10 02:091,1,1,2-Tetrachloroethane ug/L 10L5751<0.250 10L5751-BLK1 12/24/10 02:091,1,2,2-Tetrachloroethane ug/L 10L5751<0.220 10L5751-BLK1 12/24/10 02:09Tetrachloroethene ug/L 10L5751<0.330 10L5751-BLK1 12/24/10 02:09Toluene ug/L 10L5751<0.140 10L5751-BLK1 12/24/10 02:091,2,3-Trichlorobenzene ug/L 10L5751<0.240 10L5751-BLK1 12/24/10 02:091,2,4-Trichlorobenzene ug/L 10L5751<0.380 10L5751-BLK1 12/24/10 02:091,1,2-Trichloroethane ug/L 10L5751<0.350 10L5751-BLK1 12/24/10 02:091,1,1-Trichloroethane ug/L 10L5751<0.370 10L5751-BLK1 12/24/10 02:09Trichloroethene ug/L 10L5751<0.300 10L5751-BLK1 12/24/10 02:09Trichlorofluoromethane ug/L 10L5751<0.460 10L5751-BLK1 12/24/10 02:091,2,3-Trichloropropane ug/L 10L5751<0.230 10L5751-BLK1 12/24/10 02:091,3,5-Trimethylbenzene ug/L 10L5751<0.200 10L5751-BLK1 12/24/10 02:091,2,4-Trimethylbenzene ug/L 10L5751<0.360 10L5751-BLK1 12/24/10 02:09Vinyl chloride ug/L 10L5751<0.870 10L5751-BLK1 12/24/10 02:09Xylenes, total ug/L 10L5751<0.370 10L5751-BLK1 12/24/10 02:09Diisopropyl Ether ug/L 10L5751<0.740 10L5751-BLK1 12/24/10 02:091,2-Dichloroethene (total) 10L5751 10L5751-BLK1 12/24/10 02:0990%Surrogate: 1,2-Dichloroethane-d4 10L5751 10L5751-BLK1 12/24/10 02:0995%Surrogate: Dibromofluoromethane 10L5751 10L5751-BLK1 12/24/10 02:09100%Surrogate: Toluene-d8 10L5751 10L5751-BLK1 12/24/10 02:0995%Surrogate: 4-Bromofluorobenzene 10L5947-BLK1 ug/L 10L5947<25.0 10L5947-BLK1 12/25/10 16:45Acetone ug/L 10L5947<0.270 10L5947-BLK1 12/25/10 16:45Benzene ug/L 10L5947<0.220 10L5947-BLK1 12/25/10 16:45Bromobenzene ug/L 10L5947<0.440 10L5947-BLK1 12/25/10 16:45Bromochloromethane ug/L 10L5947<0.370 10L5947-BLK1 12/25/10 16:45Bromodichloromethane ug/L 10L5947<0.220 10L5947-BLK1 12/25/10 16:45Bromoform ug/L 10L5947<0.470 10L5947-BLK1 12/25/10 16:45Bromomethane ug/L 10L5947<1.70 10L5947-BLK1 12/25/10 16:452-Butanone ug/L 10L5947<0.200 10L5947-BLK1 12/25/10 16:45sec-Butylbenzene ug/L 10L5947<0.220 10L5947-BLK1 12/25/10 16:45n-Butylbenzene Page 7 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA Blank - Cont. Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5947-BLK1 ug/L 10L5947<0.200 10L5947-BLK1 12/25/10 16:45tert-Butylbenzene ug/L 10L5947<0.290 10L5947-BLK1 12/25/10 16:45Carbon disulfide ug/L 10L5947<0.270 10L5947-BLK1 12/25/10 16:45Carbon Tetrachloride ug/L 10L5947<0.380 10L5947-BLK1 12/25/10 16:45Chlorobenzene ug/L 10L5947<0.300 10L5947-BLK1 12/25/10 16:45Chlorodibromomethane ug/L 10L5947<0.410 10L5947-BLK1 12/25/10 16:45Chloroethane ug/L 10L5947<0.470 10L5947-BLK1 12/25/10 16:45Chloroform ug/L 10L5947<0.180 10L5947-BLK1 12/25/10 16:45Chloromethane ug/L 10L5947<0.250 10L5947-BLK1 12/25/10 16:452-Chlorotoluene ug/L 10L5947<0.270 10L5947-BLK1 12/25/10 16:454-Chlorotoluene ug/L 10L5947<0.200 10L5947-BLK1 12/25/10 16:451,2-Dibromo-3-chloropropane ug/L 10L5947<0.340 10L5947-BLK1 12/25/10 16:451,2-Dibromoethane (EDB) ug/L 10L5947<0.430 10L5947-BLK1 12/25/10 16:45Dibromomethane ug/L 10L5947<0.250 10L5947-BLK1 12/25/10 16:451,4-Dichlorobenzene ug/L 10L5947<0.490 10L5947-BLK1 12/25/10 16:451,3-Dichlorobenzene ug/L 10L5947<0.200 10L5947-BLK1 12/25/10 16:451,2-Dichlorobenzene ug/L 10L5947<0.140 10L5947-BLK1 12/25/10 16:45Dichlorodifluoromethane ug/L 10L5947<0.320 10L5947-BLK1 12/25/10 16:451,1-Dichloroethane ug/L 10L5947<0.380 10L5947-BLK1 12/25/10 16:451,2-Dichloroethane ug/L 10L5947<0.380 10L5947-BLK1 12/25/10 16:45cis-1,2-Dichloroethene ug/L 10L5947<0.360 10L5947-BLK1 12/25/10 16:451,1-Dichloroethene ug/L 10L5947<0.360 10L5947-BLK1 12/25/10 16:45trans-1,2-Dichloroethene ug/L 10L5947<0.280 10L5947-BLK1 12/25/10 16:451,3-Dichloropropane ug/L 10L5947<0.330 10L5947-BLK1 12/25/10 16:451,2-Dichloropropane ug/L 10L5947<0.260 10L5947-BLK1 12/25/10 16:452,2-Dichloropropane ug/L 10L5947<0.190 10L5947-BLK1 12/25/10 16:45cis-1,3-Dichloropropene ug/L 10L5947<0.160 10L5947-BLK1 12/25/10 16:45trans-1,3-Dichloropropene ug/L 10L5947<0.300 10L5947-BLK1 12/25/10 16:451,1-Dichloropropene ug/L 10L5947<0.320 10L5947-BLK1 12/25/10 16:45Ethylbenzene ug/L 10L5947<0.310 10L5947-BLK1 12/25/10 16:45Hexachlorobutadiene ug/L 10L5947<2.20 10L5947-BLK1 12/25/10 16:452-Hexanone ug/L 10L5947<0.240 10L5947-BLK1 12/25/10 16:45Isopropylbenzene ug/L 10L5947<0.210 10L5947-BLK1 12/25/10 16:45p-Isopropyltoluene ug/L 10L5947<0.320 10L5947-BLK1 12/25/10 16:45Methyl tert-Butyl Ether ug/L 10L5947<0.150 10L5947-BLK1 12/25/10 16:45Methylene Chloride ug/L 10L5947<1.60 10L5947-BLK1 12/25/10 16:454-Methyl-2-pentanone ug/L 10L5947<0.170 10L5947-BLK1 12/25/10 16:45Naphthalene ug/L 10L5947<0.220 10L5947-BLK1 12/25/10 16:45n-Propylbenzene ug/L 10L5947<0.220 10L5947-BLK1 12/25/10 16:45Styrene ug/L 10L5947<0.220 10L5947-BLK1 12/25/10 16:451,1,1,2-Tetrachloroethane ug/L 10L5947<0.250 10L5947-BLK1 12/25/10 16:451,1,2,2-Tetrachloroethane Page 8 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA Blank - Cont. Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5947-BLK1 ug/L 10L5947<0.220 10L5947-BLK1 12/25/10 16:45Tetrachloroethene ug/L 10L5947<0.330 10L5947-BLK1 12/25/10 16:45Toluene ug/L 10L5947<0.140 10L5947-BLK1 12/25/10 16:451,2,3-Trichlorobenzene ug/L 10L5947<0.240 10L5947-BLK1 12/25/10 16:451,2,4-Trichlorobenzene ug/L 10L5947<0.380 10L5947-BLK1 12/25/10 16:451,1,2-Trichloroethane ug/L 10L5947<0.350 10L5947-BLK1 12/25/10 16:451,1,1-Trichloroethane ug/L 10L59470.430 10L5947-BLK1 12/25/10 16:45Trichloroethene ug/L 10L5947<0.300 10L5947-BLK1 12/25/10 16:45Trichlorofluoromethane ug/L 10L5947<0.460 10L5947-BLK1 12/25/10 16:451,2,3-Trichloropropane ug/L 10L5947<0.230 10L5947-BLK1 12/25/10 16:451,3,5-Trimethylbenzene ug/L 10L5947<0.200 10L5947-BLK1 12/25/10 16:451,2,4-Trimethylbenzene ug/L 10L5947<0.360 10L5947-BLK1 12/25/10 16:45Vinyl chloride ug/L 10L5947<0.870 10L5947-BLK1 12/25/10 16:45Xylenes, total ug/L 10L5947<0.370 10L5947-BLK1 12/25/10 16:45Diisopropyl Ether ug/L 10L5947<0.740 10L5947-BLK1 12/25/10 16:451,2-Dichloroethene (total) 10L5947 10L5947-BLK1 12/25/10 16:45100%Surrogate: 1,2-Dichloroethane-d4 10L5947 10L5947-BLK1 12/25/10 16:4597%Surrogate: Dibromofluoromethane 10L5947 10L5947-BLK1 12/25/10 16:45104%Surrogate: Toluene-d8 10L5947 10L5947-BLK1 12/25/10 16:4598%Surrogate: 4-Bromofluorobenzene Page 9 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA LCS Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ Target Range Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5751-BS1 56 - 150 10L575125021084% ug/L 12/24/10 00:20Acetone 80 - 121 10L575150.0 49.0 98% ug/L 12/24/10 00:20Benzene 72 - 130 10L575150.0 46.5 93% ug/L 12/24/10 00:20Bromobenzene 73 - 137 10L575150.0 49.7 99% ug/L 12/24/10 00:20Bromochloromethane 75 - 131 10L575150.0 51.8 104% ug/L 12/24/10 00:20Bromodichloromethane 65 - 140 10L575150.0 46.6 93% ug/L 12/24/10 00:20Bromoform 50 - 150 10L575150.0 47.2 94% ug/L 12/24/10 00:20Bromomethane 70 - 144 10L575125022791% ug/L 12/24/10 00:202-Butanone 72 - 140 10L575150.0 55.8 112% ug/L 12/24/10 00:20sec-Butylbenzene 68 - 140 10L575150.0 49.4 99% ug/L 12/24/10 00:20n-Butylbenzene 76 - 135 10L575150.0 54.5 109% ug/L 12/24/10 00:20tert-Butylbenzene 74 - 137 10L575150.0 44.3 89% ug/L 12/24/10 00:20Carbon disulfide 71 - 137 10L575150.0 51.9 104% ug/L 12/24/10 00:20Carbon Tetrachloride 80 - 121 10L575150.0 50.9 102% ug/L 12/24/10 00:20Chlorobenzene 68 - 137 10L575150.0 49.5 99% ug/L 12/24/10 00:20Chlorodibromomethane 50 - 146 10L575150.0 45.1 90% ug/L 12/24/10 00:20Chloroethane 73 - 131 10L575150.0 48.4 97% ug/L 12/24/10 00:20Chloroform 30 - 132 10L575150.0 48.5 97% ug/L 12/24/10 00:20Chloromethane 74 - 135 10L575150.0 50.0 100% ug/L 12/24/10 00:202-Chlorotoluene 74 - 132 10L575150.0 50.8 102% ug/L 12/24/10 00:204-Chlorotoluene 56 - 145 10L575150.0 43.4 87% ug/L 12/24/10 00:201,2-Dibromo-3-chloropropane 80 - 135 10L575150.0 53.6 107% ug/L 12/24/10 00:201,2-Dibromoethane (EDB) 78 - 133 10L575150.0 48.8 98% ug/L 12/24/10 00:20Dibromomethane 80 - 120 10L575150.0 50.4 101% ug/L 12/24/10 00:201,4-Dichlorobenzene 80 - 128 10L575150.0 51.6 103% ug/L 12/24/10 00:201,3-Dichlorobenzene 80 - 125 10L575150.0 51.6 103% ug/L 12/24/10 00:201,2-Dichlorobenzene 30 - 132 10L575150.0 43.2 86% ug/L 12/24/10 00:20Dichlorodifluoromethane 75 - 125 10L575150.0 45.1 90% ug/L 12/24/10 00:201,1-Dichloroethane 70 - 134 10L575150.0 42.8 86% ug/L 12/24/10 00:201,2-Dichloroethane 71 - 132 10L575150.0 46.8 94% ug/L 12/24/10 00:20cis-1,2-Dichloroethene 73 - 125 10L575150.0 52.8 106% ug/L 12/24/10 00:201,1-Dichloroethene 77 - 125 10L575150.0 44.8 90% ug/L 12/24/10 00:20trans-1,2-Dichloroethene 76 - 125 10L575150.0 50.3 101% ug/L 12/24/10 00:201,3-Dichloropropane 72 - 120 10L575150.0 45.7 91% ug/L 12/24/10 00:201,2-Dichloropropane 50 - 150 10L575150.0 39.7 79% ug/L 12/24/10 00:202,2-Dichloropropane 70 - 140 10L575150.0 55.2 110% ug/L 12/24/10 00:20cis-1,3-Dichloropropene 62 - 139 10L575150.0 51.2 102% ug/L 12/24/10 00:20trans-1,3-Dichloropropene 78 - 126 10L575150.0 47.7 95% ug/L 12/24/10 00:201,1-Dichloropropene 78 - 133 10L575150.0 53.4 107% ug/L 12/24/10 00:20Ethylbenzene 70 - 150 10L575150.0 51.1 102% ug/L 12/24/10 00:20Hexachlorobutadiene 60 - 150 10L5751250256103% ug/L 12/24/10 00:202-Hexanone Page 10 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA LCS - Cont. Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ Target Range Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5751-BS1 69 - 120 10L575150.0 61.0 122%L1 ug/L 12/24/10 00:20Isopropylbenzene 72 - 134 10L575150.0 53.9 108% ug/L 12/24/10 00:20p-Isopropyltoluene 76 - 120 10L575150.0 42.3 85% ug/L 12/24/10 00:20Methyl tert-Butyl Ether 80 - 133 10L575150.0 50.3 101% ug/L 12/24/10 00:20Methylene Chloride 62 - 146 10L5751250251100% ug/L 12/24/10 00:204-Methyl-2-pentanone 71 - 139 10L575150.0 52.5 105% ug/L 12/24/10 00:20Naphthalene 70 - 143 10L575150.0 53.0 106% ug/L 12/24/10 00:20n-Propylbenzene 80 - 136 10L575150.0 55.5 111% ug/L 12/24/10 00:20Styrene 80 - 130 10L575150.0 57.9 116% ug/L 12/24/10 00:201,1,1,2-Tetrachloroethane 73 - 131 10L575150.0 47.6 95% ug/L 12/24/10 00:201,1,2,2-Tetrachloroethane 77 - 131 10L575150.0 53.9 108% ug/L 12/24/10 00:20Tetrachloroethene 78 - 125 10L575150.0 51.3 103% ug/L 12/24/10 00:20Toluene 71 - 138 10L575150.0 52.3 105% ug/L 12/24/10 00:201,2,3-Trichlorobenzene 74 - 136 10L575150.0 53.1 106% ug/L 12/24/10 00:201,2,4-Trichlorobenzene 80 - 123 10L575150.0 50.3 101% ug/L 12/24/10 00:201,1,2-Trichloroethane 75 - 137 10L575150.0 45.8 92% ug/L 12/24/10 00:201,1,1-Trichloroethane 74 - 139 10L575150.0 51.4 103% ug/L 12/24/10 00:20Trichloroethene 60 - 133 10L575150.0 40.7 81% ug/L 12/24/10 00:20Trichlorofluoromethane 64 - 127 10L575150.0 46.2 92% ug/L 12/24/10 00:201,2,3-Trichloropropane 75 - 134 10L575150.0 53.9 108% ug/L 12/24/10 00:201,3,5-Trimethylbenzene 77 - 134 10L575150.0 52.8 106% ug/L 12/24/10 00:201,2,4-Trimethylbenzene 60 - 122 10L575150.0 42.3 85% ug/L 12/24/10 00:20Vinyl chloride 78 - 134 10L5751150159106% ug/L 12/24/10 00:20Xylenes, total 63 - 136 10L575150.0 46.1 92% ug/L 12/24/10 00:20Diisopropyl Ether 78 - 126 10L575110091.6 92% ug/L 12/24/10 00:201,2-Dichloroethene (total) 63 - 140 10L575125.0 21.1Surrogate: 1,2-Dichloroethane-d4 84% 12/24/10 00:20 73 - 131 10L575125.0 24.0Surrogate: Dibromofluoromethane 96% 12/24/10 00:20 80 - 120 10L575125.0 25.4Surrogate: Toluene-d8 101% 12/24/10 00:20 79 - 125 10L575125.0 23.3Surrogate: 4-Bromofluorobenzene 93% 12/24/10 00:20 10L5947-BS1 56 - 150 10L594725023694% ug/L 12/25/10 14:55Acetone 80 - 121 10L594750.0 48.2 96% ug/L 12/25/10 14:55Benzene 72 - 130 10L594750.0 47.4 95% ug/L 12/25/10 14:55Bromobenzene 73 - 137 10L594750.0 46.4 93% ug/L 12/25/10 14:55Bromochloromethane 75 - 131 10L594750.0 51.9 104% ug/L 12/25/10 14:55Bromodichloromethane 65 - 140 10L594750.0 48.1 96% ug/L 12/25/10 14:55Bromoform 50 - 150 10L594750.0 44.9 90% ug/L 12/25/10 14:55Bromomethane 70 - 144 10L594725023594% ug/L 12/25/10 14:552-Butanone 72 - 140 10L594750.0 55.6 111% ug/L 12/25/10 14:55sec-Butylbenzene 68 - 140 10L594750.0 50.8 102% ug/L 12/25/10 14:55n-Butylbenzene Page 11 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA LCS - Cont. Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ Target Range Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5947-BS1 76 - 135 10L594750.0 53.6 107% ug/L 12/25/10 14:55tert-Butylbenzene 74 - 137 10L594750.0 45.4 91% ug/L 12/25/10 14:55Carbon disulfide 71 - 137 10L594750.0 50.5 101% ug/L 12/25/10 14:55Carbon Tetrachloride 80 - 121 10L594750.0 50.7 101% ug/L 12/25/10 14:55Chlorobenzene 68 - 137 10L594750.0 49.8 100% ug/L 12/25/10 14:55Chlorodibromomethane 50 - 146 10L594750.0 47.0 94% ug/L 12/25/10 14:55Chloroethane 73 - 131 10L594750.0 48.2 96% ug/L 12/25/10 14:55Chloroform 30 - 132 10L594750.0 47.2 94% ug/L 12/25/10 14:55Chloromethane 74 - 135 10L594750.0 50.2 100% ug/L 12/25/10 14:552-Chlorotoluene 74 - 132 10L594750.0 51.8 104% ug/L 12/25/10 14:554-Chlorotoluene 56 - 145 10L594750.0 43.2 86% ug/L 12/25/10 14:551,2-Dibromo-3-chloropropane 80 - 135 10L594750.0 53.6 107% ug/L 12/25/10 14:551,2-Dibromoethane (EDB) 78 - 133 10L594750.0 48.4 97% ug/L 12/25/10 14:55Dibromomethane 80 - 120 10L594750.0 50.9 102% ug/L 12/25/10 14:551,4-Dichlorobenzene 80 - 128 10L594750.0 51.4 103% ug/L 12/25/10 14:551,3-Dichlorobenzene 80 - 125 10L594750.0 52.6 105% ug/L 12/25/10 14:551,2-Dichlorobenzene 30 - 132 10L594750.0 37.4 75% ug/L 12/25/10 14:55Dichlorodifluoromethane 75 - 125 10L594750.0 44.9 90% ug/L 12/25/10 14:551,1-Dichloroethane 70 - 134 10L594750.0 44.5 89% ug/L 12/25/10 14:551,2-Dichloroethane 71 - 132 10L594750.0 47.8 96% ug/L 12/25/10 14:55cis-1,2-Dichloroethene 73 - 125 10L594750.0 53.3 107% ug/L 12/25/10 14:551,1-Dichloroethene 77 - 125 10L594750.0 47.0 94% ug/L 12/25/10 14:55trans-1,2-Dichloroethene 76 - 125 10L594750.0 52.5 105% ug/L 12/25/10 14:551,3-Dichloropropane 72 - 120 10L594750.0 46.1 92% ug/L 12/25/10 14:551,2-Dichloropropane 50 - 150 10L594750.0 43.5 87% ug/L 12/25/10 14:552,2-Dichloropropane 70 - 140 10L594750.0 57.4 115% ug/L 12/25/10 14:55cis-1,3-Dichloropropene 62 - 139 10L594750.0 54.3 109% ug/L 12/25/10 14:55trans-1,3-Dichloropropene 78 - 126 10L594750.0 47.0 94% ug/L 12/25/10 14:551,1-Dichloropropene 78 - 133 10L594750.0 54.4 109% ug/L 12/25/10 14:55Ethylbenzene 70 - 150 10L594750.0 49.5 99% ug/L 12/25/10 14:55Hexachlorobutadiene 60 - 150 10L5947250278111% ug/L 12/25/10 14:552-Hexanone 69 - 120 10L594750.0 62.2 124%L1 ug/L 12/25/10 14:55Isopropylbenzene 72 - 134 10L594750.0 54.4 109% ug/L 12/25/10 14:55p-Isopropyltoluene 76 - 120 10L594750.0 44.8 90% ug/L 12/25/10 14:55Methyl tert-Butyl Ether 80 - 133 10L594750.0 51.4 103% ug/L 12/25/10 14:55Methylene Chloride 62 - 146 10L5947250267107% ug/L 12/25/10 14:554-Methyl-2-pentanone 71 - 139 10L594750.0 53.3 107% ug/L 12/25/10 14:55Naphthalene 70 - 143 10L594750.0 53.5 107% ug/L 12/25/10 14:55n-Propylbenzene 80 - 136 10L594750.0 57.2 114% ug/L 12/25/10 14:55Styrene 80 - 130 10L594750.0 58.1 116% ug/L 12/25/10 14:551,1,1,2-Tetrachloroethane 73 - 131 10L594750.0 49.7 99% ug/L 12/25/10 14:551,1,2,2-Tetrachloroethane Page 12 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 PROJECT QUALITY CONTROL DATA LCS - Cont. Analyte UnitsKnown Val.Analyzed Val % Rec. BatchQ Target Range Analyzed Date/Time Volatile Organic Compounds by EPA Method 8260B 10L5947-BS1 77 - 131 10L594750.0 52.4 105% ug/L 12/25/10 14:55Tetrachloroethene 78 - 125 10L594750.0 51.8 104% ug/L 12/25/10 14:55Toluene 71 - 138 10L594750.0 51.8 104% ug/L 12/25/10 14:551,2,3-Trichlorobenzene 74 - 136 10L594750.0 52.5 105% ug/L 12/25/10 14:551,2,4-Trichlorobenzene 80 - 123 10L594750.0 52.5 105% ug/L 12/25/10 14:551,1,2-Trichloroethane 75 - 137 10L594750.0 44.9 90% ug/L 12/25/10 14:551,1,1-Trichloroethane 74 - 139 10L594750.0 49.1 98% ug/L 12/25/10 14:55Trichloroethene 60 - 133 10L594750.0 44.1 88% ug/L 12/25/10 14:55Trichlorofluoromethane 64 - 127 10L594750.0 47.0 94% ug/L 12/25/10 14:551,2,3-Trichloropropane 75 - 134 10L594750.0 54.4 109% ug/L 12/25/10 14:551,3,5-Trimethylbenzene 77 - 134 10L594750.0 53.8 108% ug/L 12/25/10 14:551,2,4-Trimethylbenzene 60 - 122 10L594750.0 43.9 88% ug/L 12/25/10 14:55Vinyl chloride 78 - 134 10L5947150164110% ug/L 12/25/10 14:55Xylenes, total 63 - 136 10L594750.0 48.5 97% ug/L 12/25/10 14:55Diisopropyl Ether 78 - 126 10L594710094.7 95% ug/L 12/25/10 14:551,2-Dichloroethene (total) 63 - 140 10L594725.0 23.4Surrogate: 1,2-Dichloroethane-d4 94% 12/25/10 14:55 73 - 131 10L594725.0 24.2Surrogate: Dibromofluoromethane 97% 12/25/10 14:55 80 - 120 10L594725.0 26.3Surrogate: Toluene-d8 105% 12/25/10 14:55 79 - 125 10L594725.0 23.4Surrogate: 4-Bromofluorobenzene 94% 12/25/10 14:55 Page 13 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate LCS Dup PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5751-BSD1 205 3 31 10L5751 250 82%ug/L 56 - 150 12/24/10 00:47Acetone 48.6 0.7 12 10L5751 50.0 97%ug/L 80 - 121 12/24/10 00:47Benzene 46.5 0.02 23 10L5751 50.0 93%ug/L 72 - 130 12/24/10 00:47Bromobenzene 49.8 0.2 32 10L5751 50.0 100%ug/L 73 - 137 12/24/10 00:47Bromochloromethane 52.0 0.4 13 10L5751 50.0 104%ug/L 75 - 131 12/24/10 00:47Bromodichloromethane 47.5 2 18 10L5751 50.0 95%ug/L 65 - 140 12/24/10 00:47Bromoform 46.7 1 50 10L5751 50.0 93%ug/L 50 - 150 12/24/10 00:47Bromomethane 232 2 37 10L5751 250 93%ug/L 70 - 144 12/24/10 00:472-Butanone 55.0 1 21 10L5751 50.0 110%ug/L 72 - 140 12/24/10 00:47sec-Butylbenzene 48.7 1 11 10L5751 50.0 97%ug/L 68 - 140 12/24/10 00:47n-Butylbenzene 54.2 0.4 20 10L5751 50.0 108%ug/L 76 - 135 12/24/10 00:47tert-Butylbenzene 44.0 0.7 28 10L5751 50.0 88%ug/L 74 - 137 12/24/10 00:47Carbon disulfide 51.8 0.2 26 10L5751 50.0 104%ug/L 71 - 137 12/24/10 00:47Carbon Tetrachloride 50.2 2 11 10L5751 50.0 100%ug/L 80 - 121 12/24/10 00:47Chlorobenzene 49.5 0.1 16 10L5751 50.0 99%ug/L 68 - 137 12/24/10 00:47Chlorodibromomethane 44.3 2 35 10L5751 50.0 89%ug/L 50 - 146 12/24/10 00:47Chloroethane 48.5 0.4 32 10L5751 50.0 97%ug/L 73 - 131 12/24/10 00:47Chloroform 48.4 0.3 34 10L5751 50.0 97%ug/L 30 - 132 12/24/10 00:47Chloromethane 49.4 1 22 10L5751 50.0 99%ug/L 74 - 135 12/24/10 00:472-Chlorotoluene 50.6 0.4 22 10L5751 50.0 101%ug/L 74 - 132 12/24/10 00:474-Chlorotoluene 44.5 2 21 10L5751 50.0 89%ug/L 56 - 145 12/24/10 00:471,2-Dibromo-3-chloropropane 53.6 0.1 10 10L5751 50.0 107%ug/L 80 - 135 12/24/10 00:471,2-Dibromoethane (EDB) 48.8 0.1 11 10L5751 50.0 98%ug/L 78 - 133 12/24/10 00:47Dibromomethane 50.2 0.3 10 10L5751 50.0 100%ug/L 80 - 120 12/24/10 00:471,4-Dichlorobenzene 51.1 1 18 10L5751 50.0 102%ug/L 80 - 128 12/24/10 00:471,3-Dichlorobenzene 51.5 0.2 11 10L5751 50.0 103%ug/L 80 - 125 12/24/10 00:471,2-Dichlorobenzene 43.2 0.07 32 10L5751 50.0 86%ug/L 30 - 132 12/24/10 00:47Dichlorodifluoromethane 44.6 1 34 10L5751 50.0 89%ug/L 75 - 125 12/24/10 00:471,1-Dichloroethane 42.5 0.6 25 10L5751 50.0 85%ug/L 70 - 134 12/24/10 00:471,2-Dichloroethane 46.4 0.9 32 10L5751 50.0 93%ug/L 71 - 132 12/24/10 00:47cis-1,2-Dichloroethene 51.7 2 31 10L5751 50.0 103%ug/L 73 - 125 12/24/10 00:471,1-Dichloroethene 44.2 1 32 10L5751 50.0 88%ug/L 77 - 125 12/24/10 00:47trans-1,2-Dichloroethene 50.3 0.04 20 10L5751 50.0 101%ug/L 76 - 125 12/24/10 00:471,3-Dichloropropane 45.4 0.6 11 10L5751 50.0 91%ug/L 72 - 120 12/24/10 00:471,2-Dichloropropane 39.5 0.3 11 10L5751 50.0 79%ug/L 50 - 150 12/24/10 00:472,2-Dichloropropane 54.9 0.6 35 10L5751 50.0 110%ug/L 70 - 140 12/24/10 00:47cis-1,3-Dichloropropene 51.4 0.5 26 10L5751 50.0 103%ug/L 62 - 139 12/24/10 00:47trans-1,3-Dichloropropene 47.7 0.04 18 10L5751 50.0 95%ug/L 78 - 126 12/24/10 00:471,1-Dichloropropene 52.6 1 12 10L5751 50.0 105%ug/L 78 - 133 12/24/10 00:47Ethylbenzene 50.4 1 21 10L5751 50.0 101%ug/L 70 - 150 12/24/10 00:47Hexachlorobutadiene 260 1 20 10L5751 250 104%ug/L 60 - 150 12/24/10 00:472-Hexanone Page 14 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate LCS Dup - Cont. PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5751-BSD1 60.1 1 15 10L5751 50.0 120%ug/L 69 - 120 12/24/10 00:47Isopropylbenzene 53.8 0.2 18 10L5751 50.0 108%ug/L 72 - 134 12/24/10 00:47p-Isopropyltoluene 42.5 0.4 32 10L5751 50.0 85%ug/L 76 - 120 12/24/10 00:47Methyl tert-Butyl Ether 49.7 1 36 10L5751 50.0 99%ug/L 80 - 133 12/24/10 00:47Methylene Chloride 255 2 35 10L5751 250 102%ug/L 62 - 146 12/24/10 00:474-Methyl-2-pentanone 53.7 2 30 10L5751 50.0 107%ug/L 71 - 139 12/24/10 00:47Naphthalene 52.5 0.9 23 10L5751 50.0 105%ug/L 70 - 143 12/24/10 00:47n-Propylbenzene 54.9 1 29 10L5751 50.0 110%ug/L 80 - 136 12/24/10 00:47Styrene 57.8 0.2 11 10L5751 50.0 116%ug/L 80 - 130 12/24/10 00:471,1,1,2-Tetrachloroethane 48.5 2 28 10L5751 50.0 97%ug/L 73 - 131 12/24/10 00:471,1,2,2-Tetrachloroethane 53.4 0.9 16 10L5751 50.0 107%ug/L 77 - 131 12/24/10 00:47Tetrachloroethene 50.4 2 35 10L5751 50.0 101%ug/L 78 - 125 12/24/10 00:47Toluene 53.0 1 28 10L5751 50.0 106%ug/L 71 - 138 12/24/10 00:471,2,3-Trichlorobenzene 53.6 0.9 23 10L5751 50.0 107%ug/L 74 - 136 12/24/10 00:471,2,4-Trichlorobenzene 50.0 0.7 21 10L5751 50.0 100%ug/L 80 - 123 12/24/10 00:471,1,2-Trichloroethane 45.2 1 29 10L5751 50.0 90%ug/L 75 - 137 12/24/10 00:471,1,1-Trichloroethane 50.8 1 11 10L5751 50.0 102%ug/L 74 - 139 12/24/10 00:47Trichloroethene 40.4 0.6 33 10L5751 50.0 81%ug/L 60 - 133 12/24/10 00:47Trichlorofluoromethane 47.0 2 25 10L5751 50.0 94%ug/L 64 - 127 12/24/10 00:471,2,3-Trichloropropane 53.5 0.8 21 10L5751 50.0 107%ug/L 75 - 134 12/24/10 00:471,3,5-Trimethylbenzene 52.5 0.6 20 10L5751 50.0 105%ug/L 77 - 134 12/24/10 00:471,2,4-Trimethylbenzene 42.0 0.8 32 10L5751 50.0 84%ug/L 60 - 122 12/24/10 00:47Vinyl chloride 158 1 18 10L5751 150 105%ug/L 78 - 134 12/24/10 00:47Xylenes, total 45.7 0.8 32 10L5751 50.0 91%ug/L 63 - 136 12/24/10 00:47Diisopropyl Ether 90.6 1 33 10L5751 100 91%ug/L 78 - 126 12/24/10 00:471,2-Dichloroethene (total) 21.2 10L5751 25.0 85%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/24/10 00:47 24.1 10L5751 25.0 96%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/24/10 00:47 25.2 10L5751 25.0 101%Surrogate: Toluene-d8 ug/L 80 - 120 12/24/10 00:47 23.5 10L5751 25.0 94%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/24/10 00:47 10L5947-BSD1 260 10 31 10L5947 250 104%ug/L 56 - 150 12/25/10 15:22Acetone 45.8 5 12 10L5947 50.0 92%ug/L 80 - 121 12/25/10 15:22Benzene 46.3 2 23 10L5947 50.0 93%ug/L 72 - 130 12/25/10 15:22Bromobenzene 44.6 4 32 10L5947 50.0 89%ug/L 73 - 137 12/25/10 15:22Bromochloromethane 49.7 4 13 10L5947 50.0 99%ug/L 75 - 131 12/25/10 15:22Bromodichloromethane 47.0 2 18 10L5947 50.0 94%ug/L 65 - 140 12/25/10 15:22Bromoform 41.6 8 50 10L5947 50.0 83%ug/L 50 - 150 12/25/10 15:22Bromomethane 240 2 37 10L5947 250 96%ug/L 70 - 144 12/25/10 15:222-Butanone 52.5 6 21 10L5947 50.0 105%ug/L 72 - 140 12/25/10 15:22sec-Butylbenzene 47.9 6 11 10L5947 50.0 96%ug/L 68 - 140 12/25/10 15:22n-Butylbenzene Page 15 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate LCS Dup - Cont. PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5947-BSD1 51.3 4 20 10L5947 50.0 103%ug/L 76 - 135 12/25/10 15:22tert-Butylbenzene 41.7 9 28 10L5947 50.0 83%ug/L 74 - 137 12/25/10 15:22Carbon disulfide 47.8 6 26 10L5947 50.0 96%ug/L 71 - 137 12/25/10 15:22Carbon Tetrachloride 48.6 4 11 10L5947 50.0 97%ug/L 80 - 121 12/25/10 15:22Chlorobenzene 48.6 2 16 10L5947 50.0 97%ug/L 68 - 137 12/25/10 15:22Chlorodibromomethane 42.9 9 35 10L5947 50.0 86%ug/L 50 - 146 12/25/10 15:22Chloroethane 46.3 4 32 10L5947 50.0 93%ug/L 73 - 131 12/25/10 15:22Chloroform 44.6 6 34 10L5947 50.0 89%ug/L 30 - 132 12/25/10 15:22Chloromethane 48.1 4 22 10L5947 50.0 96%ug/L 74 - 135 12/25/10 15:222-Chlorotoluene 49.8 4 22 10L5947 50.0 100%ug/L 74 - 132 12/25/10 15:224-Chlorotoluene 43.6 0.8 21 10L5947 50.0 87%ug/L 56 - 145 12/25/10 15:221,2-Dibromo-3-chloropropane 52.4 2 10 10L5947 50.0 105%ug/L 80 - 135 12/25/10 15:221,2-Dibromoethane (EDB) 46.8 3 11 10L5947 50.0 94%ug/L 78 - 133 12/25/10 15:22Dibromomethane 48.7 4 10 10L5947 50.0 97%ug/L 80 - 120 12/25/10 15:221,4-Dichlorobenzene 49.4 4 18 10L5947 50.0 99%ug/L 80 - 128 12/25/10 15:221,3-Dichlorobenzene 50.8 4 11 10L5947 50.0 102%ug/L 80 - 125 12/25/10 15:221,2-Dichlorobenzene 35.5 5 32 10L5947 50.0 71%ug/L 30 - 132 12/25/10 15:22Dichlorodifluoromethane 43.3 4 34 10L5947 50.0 87%ug/L 75 - 125 12/25/10 15:221,1-Dichloroethane 42.7 4 25 10L5947 50.0 85%ug/L 70 - 134 12/25/10 15:221,2-Dichloroethane 45.8 4 32 10L5947 50.0 92%ug/L 71 - 132 12/25/10 15:22cis-1,2-Dichloroethene 49.2 8 31 10L5947 50.0 98%ug/L 73 - 125 12/25/10 15:221,1-Dichloroethene 43.1 9 32 10L5947 50.0 86%ug/L 77 - 125 12/25/10 15:22trans-1,2-Dichloroethene 51.1 3 20 10L5947 50.0 102%ug/L 76 - 125 12/25/10 15:221,3-Dichloropropane 43.9 5 11 10L5947 50.0 88%ug/L 72 - 120 12/25/10 15:221,2-Dichloropropane 41.3 5 11 10L5947 50.0 83%ug/L 50 - 150 12/25/10 15:222,2-Dichloropropane 55.4 3 35 10L5947 50.0 111%ug/L 70 - 140 12/25/10 15:22cis-1,3-Dichloropropene 52.8 3 26 10L5947 50.0 106%ug/L 62 - 139 12/25/10 15:22trans-1,3-Dichloropropene 44.6 5 18 10L5947 50.0 89%ug/L 78 - 126 12/25/10 15:221,1-Dichloropropene 51.6 5 12 10L5947 50.0 103%ug/L 78 - 133 12/25/10 15:22Ethylbenzene 47.6 4 21 10L5947 50.0 95%ug/L 70 - 150 12/25/10 15:22Hexachlorobutadiene 282 1 20 10L5947 250 113%ug/L 60 - 150 12/25/10 15:222-Hexanone 58.4 6 15 10L5947 50.0 117%ug/L 69 - 120 12/25/10 15:22Isopropylbenzene 51.9 5 18 10L5947 50.0 104%ug/L 72 - 134 12/25/10 15:22p-Isopropyltoluene 42.6 5 32 10L5947 50.0 85%ug/L 76 - 120 12/25/10 15:22Methyl tert-Butyl Ether 47.7 7 36 10L5947 50.0 95%ug/L 80 - 133 12/25/10 15:22Methylene Chloride 263 1 35 10L5947 250 105%ug/L 62 - 146 12/25/10 15:224-Methyl-2-pentanone 53.1 0.3 30 10L5947 50.0 106%ug/L 71 - 139 12/25/10 15:22Naphthalene 51.2 4 23 10L5947 50.0 102%ug/L 70 - 143 12/25/10 15:22n-Propylbenzene 54.1 6 29 10L5947 50.0 108%ug/L 80 - 136 12/25/10 15:22Styrene 55.9 4 11 10L5947 50.0 112%ug/L 80 - 130 12/25/10 15:221,1,1,2-Tetrachloroethane 49.0 1 28 10L5947 50.0 98%ug/L 73 - 131 12/25/10 15:221,1,2,2-Tetrachloroethane Page 16 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate LCS Dup - Cont. PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5947-BSD1 49.9 5 16 10L5947 50.0 100%ug/L 77 - 131 12/25/10 15:22Tetrachloroethene 49.6 4 35 10L5947 50.0 99%ug/L 78 - 125 12/25/10 15:22Toluene 51.2 1 28 10L5947 50.0 102%ug/L 71 - 138 12/25/10 15:221,2,3-Trichlorobenzene 51.0 3 23 10L5947 50.0 102%ug/L 74 - 136 12/25/10 15:221,2,4-Trichlorobenzene 50.4 4 21 10L5947 50.0 101%ug/L 80 - 123 12/25/10 15:221,1,2-Trichloroethane 42.6 5 29 10L5947 50.0 85%ug/L 75 - 137 12/25/10 15:221,1,1-Trichloroethane 46.7 5 11 10L5947 50.0 93%ug/L 74 - 139 12/25/10 15:22Trichloroethene 41.0 7 33 10L5947 50.0 82%ug/L 60 - 133 12/25/10 15:22Trichlorofluoromethane 46.3 1 25 10L5947 50.0 93%ug/L 64 - 127 12/25/10 15:221,2,3-Trichloropropane 52.2 4 21 10L5947 50.0 104%ug/L 75 - 134 12/25/10 15:221,3,5-Trimethylbenzene 51.4 5 20 10L5947 50.0 103%ug/L 77 - 134 12/25/10 15:221,2,4-Trimethylbenzene 41.2 6 32 10L5947 50.0 82%ug/L 60 - 122 12/25/10 15:22Vinyl chloride 156 5 18 10L5947 150 104%ug/L 78 - 134 12/25/10 15:22Xylenes, total 46.8 4 32 10L5947 50.0 94%ug/L 63 - 136 12/25/10 15:22Diisopropyl Ether 88.9 6 33 10L5947 100 89%ug/L 78 - 126 12/25/10 15:221,2-Dichloroethene (total) 23.4 10L5947 25.0 94%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/25/10 15:22 24.3 10L5947 25.0 97%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/25/10 15:22 26.4 10L5947 25.0 105%Surrogate: Toluene-d8 ug/L 80 - 120 12/25/10 15:22 23.7 10L5947 25.0 95%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/25/10 15:22 Page 17 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Analyte Units PROJECT QUALITY CONTROL DATA Orig. Val.MS Val Spike Conc % Rec. Target Range Matrix Spike Q Analyzed Date/Time Sample SpikedBatch Volatile Organic Compounds by EPA Method 8260B 10L5751-MS1 209 250 NTL2991-05 84%ND 10L575156 - 150ug/L 12/28/10 11:11Acetone 50.6 50.0 NTL2991-05 101%ND 10L575165 - 151ug/L 12/28/10 11:11Benzene 48.9 50.0 NTL2991-05 98%ND 10L575169 - 142ug/L 12/28/10 11:11Bromobenzene 48.4 50.0 NTL2991-05 97%ND 10L575164 - 154ug/L 12/28/10 11:11Bromochloromethane 54.0 50.0 NTL2991-05 108%ND 10L575175 - 138ug/L 12/28/10 11:11Bromodichloromethane 49.6 50.0 NTL2991-05 99%ND 10L575155 - 153ug/L 12/28/10 11:11Bromoform 45.8 50.0 NTL2991-05 92%ND 10L575113 - 176ug/L 12/28/10 11:11Bromomethane 231 250 NTL2991-05 93%ND 10L575145 - 164ug/L 12/28/10 11:112-Butanone 59.7 50.0 NTL2991-05 119%ND 10L575168 - 159ug/L 12/28/10 11:11sec-Butylbenzene 54.0 50.0 NTL2991-05 108%ND 10L575167 - 151ug/L 12/28/10 11:11n-Butylbenzene 57.4 50.0 NTL2991-05 115%ND 10L575173 - 153ug/L 12/28/10 11:11tert-Butylbenzene 46.9 50.0 NTL2991-05 94%ND 10L575133 - 187ug/L 12/28/10 11:11Carbon disulfide 55.0 50.0 NTL2991-05 110%ND 10L575164 - 157ug/L 12/28/10 11:11Carbon Tetrachloride 52.8 50.0 NTL2991-05 106%ND 10L575178 - 136ug/L 12/28/10 11:11Chlorobenzene 52.4 50.0 NTL2991-05 105%ND 10L575164 - 145ug/L 12/28/10 11:11Chlorodibromomethane 41.9 50.0 NTL2991-05 84%ND 10L575148 - 159ug/L 12/28/10 11:11Chloroethane 50.3 50.0 NTL2991-05 101%ND 10L575172 - 145ug/L 12/28/10 11:11Chloroform 38.7 50.0 NTL2991-05 77%ND 10L575110 - 194ug/L 12/28/10 11:11Chloromethane 52.2 50.0 NTL2991-05 104%ND 10L575166 - 155ug/L 12/28/10 11:112-Chlorotoluene 53.6 50.0 NTL2991-05 107%ND 10L575169 - 149ug/L 12/28/10 11:114-Chlorotoluene 44.8 50.0 NTL2991-05 90%ND 10L575149 - 162ug/L 12/28/10 11:111,2-Dibromo-3-chloropropane 55.7 50.0 NTL2991-05 111%ND 10L575170 - 152ug/L 12/28/10 11:111,2-Dibromoethane (EDB) 50.2 50.0 NTL2991-05 100%ND 10L575175 - 141ug/L 12/28/10 11:11Dibromomethane 52.2 50.0 NTL2991-05 104%ND 10L575175 - 135ug/L 12/28/10 11:111,4-Dichlorobenzene 53.4 50.0 NTL2991-05 107%ND 10L575172 - 146ug/L 12/28/10 11:111,3-Dichlorobenzene 54.0 50.0 NTL2991-05 108%ND 10L575180 - 136ug/L 12/28/10 11:111,2-Dichlorobenzene 34.9 50.0 NTL2991-05 70%ND 10L575123 - 159ug/L 12/28/10 11:11Dichlorodifluoromethane 47.2 50.0 NTL2991-05 94%ND 10L575164 - 154ug/L 12/28/10 11:111,1-Dichloroethane 45.8 50.0 NTL2991-05 92%ND 10L575172 - 137ug/L 12/28/10 11:111,2-Dichloroethane 50.5 50.0 NTL2991-05 100%0.520 10L575157 - 154ug/L 12/28/10 11:11cis-1,2-Dichloroethene 55.2 50.0 NTL2991-05 110%ND 10L575134 - 151ug/L 12/28/10 11:111,1-Dichloroethene 47.6 50.0 NTL2991-05 95%ND 10L575157 - 157ug/L 12/28/10 11:11trans-1,2-Dichloroethene 53.8 50.0 NTL2991-05 108%ND 10L575171 - 137ug/L 12/28/10 11:111,3-Dichloropropane 47.6 50.0 NTL2991-05 95%ND 10L575171 - 139ug/L 12/28/10 11:111,2-Dichloropropane 47.9 50.0 NTL2991-05 96%ND 10L575110 - 198ug/L 12/28/10 11:112,2-Dichloropropane 58.7 50.0 NTL2991-05 117%ND 10L575156 - 156ug/L 12/28/10 11:11cis-1,3-Dichloropropene 56.7 50.0 NTL2991-05 113%ND 10L575147 - 157ug/L 12/28/10 11:11trans-1,3-Dichloropropene Page 18 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Analyte Units PROJECT QUALITY CONTROL DATA Orig. Val.MS Val Spike Conc % Rec. Target Range Matrix Spike - Cont. Q Analyzed Date/Time Sample SpikedBatch Volatile Organic Compounds by EPA Method 8260B 10L5751-MS1 50.4 50.0 NTL2991-05 101%ND 10L575170 - 155ug/L 12/28/10 11:111,1-Dichloropropene 56.8 50.0 NTL2991-05 114%ND 10L575168 - 157ug/L 12/28/10 11:11Ethylbenzene 55.1 50.0 NTL2991-05 110%ND 10L575147 - 173ug/L 12/28/10 11:11Hexachlorobutadiene 279 250 NTL2991-05 112%ND 10L575157 - 154ug/L 12/28/10 11:112-Hexanone 65.4 50.0 NTL2991-05 131%ND 10L575169 - 139ug/L 12/28/10 11:11Isopropylbenzene 57.8 50.0 NTL2991-05 116%ND 10L575169 - 151ug/L 12/28/10 11:11p-Isopropyltoluene 44.5 50.0 NTL2991-05 89%ND 10L575156 - 152ug/L 12/28/10 11:11Methyl tert-Butyl Ether 50.9 50.0 NTL2991-05 102%ND 10L575171 - 136ug/L 12/28/10 11:11Methylene Chloride 270 250 NTL2991-05 108%ND 10L575162 - 159ug/L 12/28/10 11:114-Methyl-2-pentanone 55.1 50.0 NTL2991-05 110%ND 10L575156 - 161ug/L 12/28/10 11:11Naphthalene 56.2 50.0 NTL2991-05 112%ND 10L575161 - 167ug/L 12/28/10 11:11n-Propylbenzene 58.7 50.0 NTL2991-05 117%ND 10L575169 - 150ug/L 12/28/10 11:11Styrene 60.8 50.0 NTL2991-05 122%ND 10L575180 - 140ug/L 12/28/10 11:111,1,1,2-Tetrachloroethane 51.1 50.0 NTL2991-05 102%ND 10L575176 - 141ug/L 12/28/10 11:111,1,2,2-Tetrachloroethane 55.6 50.0 NTL2991-05 111%ND 10L575163 - 155ug/L 12/28/10 11:11Tetrachloroethene 53.9 50.0 NTL2991-05 108%ND 10L575161 - 153ug/L 12/28/10 11:11Toluene 53.8 50.0 NTL2991-05 108%ND 10L575157 - 155ug/L 12/28/10 11:111,2,3-Trichlorobenzene 54.3 50.0 NTL2991-05 109%ND 10L575164 - 147ug/L 12/28/10 11:111,2,4-Trichlorobenzene 53.1 50.0 NTL2991-05 106%ND 10L575174 - 138ug/L 12/28/10 11:111,1,2-Trichloroethane 47.8 50.0 NTL2991-05 96%ND 10L575178 - 153ug/L 12/28/10 11:111,1,1-Trichloroethane 50.8 50.0 NTL2991-05 95%3.11 10L575174 - 139ug/L 12/28/10 11:11Trichloroethene 42.7 50.0 NTL2991-05 85%ND 10L575153 - 149ug/L 12/28/10 11:11Trichlorofluoromethane 48.3 50.0 NTL2991-05 97%ND 10L575149 - 148ug/L 12/28/10 11:111,2,3-Trichloropropane 56.6 50.0 NTL2991-05 113%ND 10L575167 - 151ug/L 12/28/10 11:111,3,5-Trimethylbenzene 55.5 50.0 NTL2991-05 111%ND 10L575169 - 150ug/L 12/28/10 11:111,2,4-Trimethylbenzene 41.4 50.0 NTL2991-05 83%ND 10L575153 - 137ug/L 12/28/10 11:11Vinyl chloride 171 150 NTL2991-05 114%ND 10L575168 - 158ug/L 12/28/10 11:11Xylenes, total 49.1 50.0 NTL2991-05 98%ND 10L575159 - 145ug/L 12/28/10 11:11Diisopropyl Ether 98.0 100 NTL2991-05 98%ND 10L575160 - 152ug/L 12/28/10 11:111,2-Dichloroethene (total) 23.2 25.0 NTL2991-05 Surrogate: 1,2-Dichloroethane-d4 93%10L575163 - 140ug/L 12/28/10 11:11 24.2 25.0 NTL2991-05 Surrogate: Dibromofluoromethane 97%10L575173 - 131ug/L 12/28/10 11:11 26.0 25.0 NTL2991-05 Surrogate: Toluene-d8 104%10L575180 - 120ug/L 12/28/10 11:11 23.4 25.0 NTL2991-05 Surrogate: 4-Bromofluorobenzene 94%10L575179 - 125ug/L 12/28/10 11:11 10L5947-MS1 114000 125000 NTL2991-09RE 1 92%ND 10L594756 - 150ug/L 12/29/10 11:27Acetone 24500 25000 NTL2991-09RE 1 98%ND 10L594765 - 151ug/L 12/29/10 11:27Benzene Page 19 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Analyte Units PROJECT QUALITY CONTROL DATA Orig. Val.MS Val Spike Conc % Rec. Target Range Matrix Spike - Cont. Q Analyzed Date/Time Sample SpikedBatch Volatile Organic Compounds by EPA Method 8260B 10L5947-MS1 24300 25000 NTL2991-09RE 1 97%ND 10L594769 - 142ug/L 12/29/10 11:27Bromobenzene 24100 25000 NTL2991-09RE 1 96%ND 10L594764 - 154ug/L 12/29/10 11:27Bromochloromethane 27200 25000 NTL2991-09RE 1 109%ND 10L594775 - 138ug/L 12/29/10 11:27Bromodichloromethane 25800 25000 NTL2991-09RE 1 103%ND 10L594755 - 153ug/L 12/29/10 11:27Bromoform 22200 25000 NTL2991-09RE 1 89%ND 10L594713 - 176ug/L 12/29/10 11:27Bromomethane 125000 125000 NTL2991-09RE 1 100%ND 10L594745 - 164ug/L 12/29/10 11:272-Butanone 28500 25000 NTL2991-09RE 1 114%ND 10L594768 - 159ug/L 12/29/10 11:27sec-Butylbenzene 25800 25000 NTL2991-09RE 1 103%ND 10L594767 - 151ug/L 12/29/10 11:27n-Butylbenzene 27700 25000 NTL2991-09RE 1 111%ND 10L594773 - 153ug/L 12/29/10 11:27tert-Butylbenzene 20400 25000 NTL2991-09RE 1 81%ND 10L594733 - 187ug/L 12/29/10 11:27Carbon disulfide 26300 25000 NTL2991-09RE 1 105%ND 10L594764 - 157ug/L 12/29/10 11:27Carbon Tetrachloride 25800 25000 NTL2991-09RE 1 103%ND 10L594778 - 136ug/L 12/29/10 11:27Chlorobenzene 26600 25000 NTL2991-09RE 1 106%ND 10L594764 - 145ug/L 12/29/10 11:27Chlorodibromomethane 21100 25000 NTL2991-09RE 1 84%ND 10L594748 - 159ug/L 12/29/10 11:27Chloroethane 24800 25000 NTL2991-09RE 1 99%ND 10L594772 - 145ug/L 12/29/10 11:27Chloroform 20400 25000 NTL2991-09RE 1 81%ND 10L594710 - 194ug/L 12/29/10 11:27Chloromethane 25300 25000 NTL2991-09RE 1 101%ND 10L594766 - 155ug/L 12/29/10 11:272-Chlorotoluene 26100 25000 NTL2991-09RE 1 104%ND 10L594769 - 149ug/L 12/29/10 11:274-Chlorotoluene 23800 25000 NTL2991-09RE 1 95%ND 10L594749 - 162ug/L 12/29/10 11:271,2-Dibromo-3-chloropropane 28300 25000 NTL2991-09RE 1 113%ND 10L594770 - 152ug/L 12/29/10 11:271,2-Dibromoethane (EDB) 25500 25000 NTL2991-09RE 1 102%ND 10L594775 - 141ug/L 12/29/10 11:27Dibromomethane 25900 25000 NTL2991-09RE 1 104%ND 10L594775 - 135ug/L 12/29/10 11:271,4-Dichlorobenzene 26100 25000 NTL2991-09RE 1 104%ND 10L594772 - 146ug/L 12/29/10 11:271,3-Dichlorobenzene 27100 25000 NTL2991-09RE 1 108%ND 10L594780 - 136ug/L 12/29/10 11:271,2-Dichlorobenzene Page 20 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Analyte Units PROJECT QUALITY CONTROL DATA Orig. Val.MS Val Spike Conc % Rec. Target Range Matrix Spike - Cont. Q Analyzed Date/Time Sample SpikedBatch Volatile Organic Compounds by EPA Method 8260B 10L5947-MS1 19300 25000 NTL2991-09RE 1 77%ND 10L594723 - 159ug/L 12/29/10 11:27Dichlorodifluoromethane 22200 25000 NTL2991-09RE 1 89%ND 10L594764 - 154ug/L 12/29/10 11:271,1-Dichloroethane 23000 25000 NTL2991-09RE 1 92%ND 10L594772 - 137ug/L 12/29/10 11:271,2-Dichloroethane 28800 25000 NTL2991-09RE 1 98%4270 10L594757 - 154ug/L 12/29/10 11:27cis-1,2-Dichloroethene 26200 25000 NTL2991-09RE 1 105%ND 10L594734 - 151ug/L 12/29/10 11:271,1-Dichloroethene 22700 25000 NTL2991-09RE 1 91%ND 10L594757 - 157ug/L 12/29/10 11:27trans-1,2-Dichloroethene 27500 25000 NTL2991-09RE 1 110%ND 10L594771 - 137ug/L 12/29/10 11:271,3-Dichloropropane 23600 25000 NTL2991-09RE 1 94%ND 10L594771 - 139ug/L 12/29/10 11:271,2-Dichloropropane 23100 25000 NTL2991-09RE 1 92%ND 10L594710 - 198ug/L 12/29/10 11:272,2-Dichloropropane 29800 25000 NTL2991-09RE 1 119%ND 10L594756 - 156ug/L 12/29/10 11:27cis-1,3-Dichloropropene 28700 25000 NTL2991-09RE 1 115%ND 10L594747 - 157ug/L 12/29/10 11:27trans-1,3-Dichloropropene 23900 25000 NTL2991-09RE 1 96%ND 10L594770 - 155ug/L 12/29/10 11:271,1-Dichloropropene 27500 25000 NTL2991-09RE 1 110%ND 10L594768 - 157ug/L 12/29/10 11:27Ethylbenzene 26200 25000 NTL2991-09RE 1 105%ND 10L594747 - 173ug/L 12/29/10 11:27Hexachlorobutadiene 148000 125000 NTL2991-09RE 1 118%ND 10L594757 - 154ug/L 12/29/10 11:272-Hexanone 31500 25000 NTL2991-09RE 1 126%ND 10L594769 - 139ug/L 12/29/10 11:27Isopropylbenzene 27700 25000 NTL2991-09RE 1 111%ND 10L594769 - 151ug/L 12/29/10 11:27p-Isopropyltoluene 23200 25000 NTL2991-09RE 1 93%ND 10L594756 - 152ug/L 12/29/10 11:27Methyl tert-Butyl Ether 25300 25000 NTL2991-09RE 1 101%ND 10L594771 - 136ug/L 12/29/10 11:27Methylene Chloride 144000 125000 NTL2991-09RE 1 115%ND 10L594762 - 159ug/L 12/29/10 11:274-Methyl-2-pentanone 28600 25000 NTL2991-09RE 1 114%ND 10L594756 - 161ug/L 12/29/10 11:27Naphthalene 27100 25000 NTL2991-09RE 1 108%ND 10L594761 - 167ug/L 12/29/10 11:27n-Propylbenzene 28800 25000 NTL2991-09RE 1 115%ND 10L594769 - 150ug/L 12/29/10 11:27Styrene 30100 25000 NTL2991-09RE 1 120%ND 10L594780 - 140ug/L 12/29/10 11:271,1,1,2-Tetrachloroethane Page 21 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Analyte Units PROJECT QUALITY CONTROL DATA Orig. Val.MS Val Spike Conc % Rec. Target Range Matrix Spike - Cont. Q Analyzed Date/Time Sample SpikedBatch Volatile Organic Compounds by EPA Method 8260B 10L5947-MS1 27000 25000 NTL2991-09RE 1 108%ND 10L594776 - 141ug/L 12/29/10 11:271,1,2,2-Tetrachloroethane 26500 25000 NTL2991-09RE 1 106%ND 10L594763 - 155ug/L 12/29/10 11:27Tetrachloroethene 26100 25000 NTL2991-09RE 1 105%ND 10L594761 - 153ug/L 12/29/10 11:27Toluene 27200 25000 NTL2991-09RE 1 109%ND 10L594757 - 155ug/L 12/29/10 11:271,2,3-Trichlorobenzene 27100 25000 NTL2991-09RE 1 109%ND 10L594764 - 147ug/L 12/29/10 11:271,2,4-Trichlorobenzene 27300 25000 NTL2991-09RE 1 109%ND 10L594774 - 138ug/L 12/29/10 11:271,1,2-Trichloroethane 23100 25000 NTL2991-09RE 1 92%ND 10L594778 - 153ug/L 12/29/10 11:271,1,1-Trichloroethane 83700 25000 NTL2991-09RE 1 M8 67%67000 10L594774 - 139ug/L 12/29/10 11:27Trichloroethene 21500 25000 NTL2991-09RE 1 86%ND 10L594753 - 149ug/L 12/29/10 11:27Trichlorofluoromethane 25600 25000 NTL2991-09RE 1 102%ND 10L594749 - 148ug/L 12/29/10 11:271,2,3-Trichloropropane 27400 25000 NTL2991-09RE 1 110%ND 10L594767 - 151ug/L 12/29/10 11:271,3,5-Trimethylbenzene 26900 25000 NTL2991-09RE 1 108%ND 10L594769 - 150ug/L 12/29/10 11:271,2,4-Trimethylbenzene 21100 25000 NTL2991-09RE 1 85%ND 10L594753 - 137ug/L 12/29/10 11:27Vinyl chloride 82800 75000 NTL2991-09RE 1 110%ND 10L594768 - 158ug/L 12/29/10 11:27Xylenes, total 23800 25000 NTL2991-09RE 1 95%ND 10L594759 - 145ug/L 12/29/10 11:27Diisopropyl Ether 51500 50000 NTL2991-09RE 1 94%4350 10L594760 - 152ug/L 12/29/10 11:271,2-Dichloroethene (total) 23.7 25.0 NTL2991-09RE 1 Surrogate: 1,2-Dichloroethane-d4 95%10L594763 - 140ug/L 12/29/10 11:27 24.5 25.0 NTL2991-09RE 1 Surrogate: Dibromofluoromethane 98%10L594773 - 131ug/L 12/29/10 11:27 26.1 25.0 NTL2991-09RE 1 Surrogate: Toluene-d8 105%10L594780 - 120ug/L 12/29/10 11:27 23.4 25.0 NTL2991-09RE 1 Surrogate: 4-Bromofluorobenzene 94%10L594779 - 125ug/L 12/29/10 11:27 Page 22 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate Matrix Spike Dup PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5751-MSD1 ND 204 3 31 10L5751 NTL2991-05 250 82%ug/L 56 - 150 12/28/10 11:38Acetone ND 45.5 11 12 10L5751 NTL2991-05 50.0 91%ug/L 65 - 151 12/28/10 11:38Benzene ND 43.8 11 23 10L5751 NTL2991-05 50.0 88%ug/L 69 - 142 12/28/10 11:38Bromobenzene ND 44.9 7 32 10L5751 NTL2991-05 50.0 90%ug/L 64 - 154 12/28/10 11:38Bromochloromethane ND 49.4 9 13 10L5751 NTL2991-05 50.0 99%ug/L 75 - 138 12/28/10 11:38Bromodichloromethane ND 46.6 6 18 10L5751 NTL2991-05 50.0 93%ug/L 55 - 153 12/28/10 11:38Bromoform ND 40.4 12 50 10L5751 NTL2991-05 50.0 81%ug/L 13 - 176 12/28/10 11:38Bromomethane ND 224 3 37 10L5751 NTL2991-05 250 89%ug/L 45 - 164 12/28/10 11:382-Butanone ND 49.8 18 21 10L5751 NTL2991-05 50.0 100%ug/L 68 - 159 12/28/10 11:38sec-Butylbenzene ND 44.9 18 11 10L5751 NTL2991-05R2 50.0 90%ug/L 67 - 151 12/28/10 11:38n-Butylbenzene ND 48.8 16 20 10L5751 NTL2991-05 50.0 98%ug/L 73 - 153 12/28/10 11:38tert-Butylbenzene ND 40.2 15 28 10L5751 NTL2991-05 50.0 80%ug/L 33 - 187 12/28/10 11:38Carbon disulfide ND 48.1 13 26 10L5751 NTL2991-05 50.0 96%ug/L 64 - 157 12/28/10 11:38Carbon Tetrachloride ND 47.5 11 11 10L5751 NTL2991-05 50.0 95%ug/L 78 - 136 12/28/10 11:38Chlorobenzene ND 47.9 9 16 10L5751 NTL2991-05 50.0 96%ug/L 64 - 145 12/28/10 11:38Chlorodibromomethane ND 36.9 13 35 10L5751 NTL2991-05 50.0 74%ug/L 48 - 159 12/28/10 11:38Chloroethane ND 45.4 10 32 10L5751 NTL2991-05 50.0 91%ug/L 72 - 145 12/28/10 11:38Chloroform ND 33.2 15 34 10L5751 NTL2991-05 50.0 66%ug/L 10 - 194 12/28/10 11:38Chloromethane ND 45.4 14 22 10L5751 NTL2991-05 50.0 91%ug/L 66 - 155 12/28/10 11:382-Chlorotoluene ND 46.7 14 22 10L5751 NTL2991-05 50.0 93%ug/L 69 - 149 12/28/10 11:384-Chlorotoluene ND 42.2 6 21 10L5751 NTL2991-05 50.0 84%ug/L 49 - 162 12/28/10 11:381,2-Dibromo-3-chloropropane ND 51.9 7 10 10L5751 NTL2991-05 50.0 104%ug/L 70 - 152 12/28/10 11:381,2-Dibromoethane (EDB) ND 46.4 8 11 10L5751 NTL2991-05 50.0 93%ug/L 75 - 141 12/28/10 11:38Dibromomethane ND 45.8 13 10 10L5751 NTL2991-05R2 50.0 92%ug/L 75 - 135 12/28/10 11:381,4-Dichlorobenzene ND 46.3 14 18 10L5751 NTL2991-05 50.0 93%ug/L 72 - 146 12/28/10 11:381,3-Dichlorobenzene ND 47.3 13 11 10L5751 NTL2991-05R2 50.0 95%ug/L 80 - 136 12/28/10 11:381,2-Dichlorobenzene ND 30.5 13 32 10L5751 NTL2991-05 50.0 61%ug/L 23 - 159 12/28/10 11:38Dichlorodifluoromethane ND 42.6 10 34 10L5751 NTL2991-05 50.0 85%ug/L 64 - 154 12/28/10 11:381,1-Dichloroethane ND 42.1 8 25 10L5751 NTL2991-05 50.0 84%ug/L 72 - 137 12/28/10 11:381,2-Dichloroethane 0.520 45.6 10 32 10L5751 NTL2991-05 50.0 90%ug/L 57 - 154 12/28/10 11:38cis-1,2-Dichloroethene ND 48.4 13 31 10L5751 NTL2991-05 50.0 97%ug/L 34 - 151 12/28/10 11:381,1-Dichloroethene ND 42.3 12 32 10L5751 NTL2991-05 50.0 85%ug/L 57 - 157 12/28/10 11:38trans-1,2-Dichloroethene ND 50.0 7 20 10L5751 NTL2991-05 50.0 100%ug/L 71 - 137 12/28/10 11:381,3-Dichloropropane ND 43.4 9 11 10L5751 NTL2991-05 50.0 87%ug/L 71 - 139 12/28/10 11:381,2-Dichloropropane ND 42.4 12 11 10L5751 NTL2991-05R2 50.0 85%ug/L 10 - 198 12/28/10 11:382,2-Dichloropropane ND 54.0 8 35 10L5751 NTL2991-05 50.0 108%ug/L 56 - 156 12/28/10 11:38cis-1,3-Dichloropropene ND 52.2 8 26 10L5751 NTL2991-05 50.0 104%ug/L 47 - 157 12/28/10 11:38trans-1,3-Dichloropropene ND 44.5 12 18 10L5751 NTL2991-05 50.0 89%ug/L 70 - 155 12/28/10 11:381,1-Dichloropropene ND 49.9 13 12 10L5751 NTL2991-05R2 50.0 100%ug/L 68 - 157 12/28/10 11:38Ethylbenzene ND 46.8 16 21 10L5751 NTL2991-05 50.0 94%ug/L 47 - 173 12/28/10 11:38Hexachlorobutadiene ND 265 5 20 10L5751 NTL2991-05 250 106%ug/L 57 - 154 12/28/10 11:382-Hexanone Page 23 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate Matrix Spike Dup - Cont. PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5751-MSD1 ND 56.4 15 15 10L5751 NTL2991-05 50.0 113%ug/L 69 - 139 12/28/10 11:38Isopropylbenzene ND 48.7 17 18 10L5751 NTL2991-05 50.0 97%ug/L 69 - 151 12/28/10 11:38p-Isopropyltoluene ND 41.7 6 32 10L5751 NTL2991-05 50.0 83%ug/L 56 - 152 12/28/10 11:38Methyl tert-Butyl Ether ND 46.2 10 36 10L5751 NTL2991-05 50.0 92%ug/L 71 - 136 12/28/10 11:38Methylene Chloride ND 257 5 35 10L5751 NTL2991-05 250 103%ug/L 62 - 159 12/28/10 11:384-Methyl-2-pentanone ND 49.2 11 30 10L5751 NTL2991-05 50.0 98%ug/L 56 - 161 12/28/10 11:38Naphthalene ND 47.9 16 23 10L5751 NTL2991-05 50.0 96%ug/L 61 - 167 12/28/10 11:38n-Propylbenzene ND 52.2 12 29 10L5751 NTL2991-05 50.0 104%ug/L 69 - 150 12/28/10 11:38Styrene ND 54.7 11 11 10L5751 NTL2991-05 50.0 109%ug/L 80 - 140 12/28/10 11:381,1,1,2-Tetrachloroethane ND 47.8 7 28 10L5751 NTL2991-05 50.0 96%ug/L 76 - 141 12/28/10 11:381,1,2,2-Tetrachloroethane ND 48.7 13 16 10L5751 NTL2991-05 50.0 97%ug/L 63 - 155 12/28/10 11:38Tetrachloroethene ND 48.3 11 35 10L5751 NTL2991-05 50.0 97%ug/L 61 - 153 12/28/10 11:38Toluene ND 46.3 15 28 10L5751 NTL2991-05 50.0 93%ug/L 57 - 155 12/28/10 11:381,2,3-Trichlorobenzene ND 46.1 16 23 10L5751 NTL2991-05 50.0 92%ug/L 64 - 147 12/28/10 11:381,2,4-Trichlorobenzene ND 48.9 8 21 10L5751 NTL2991-05 50.0 98%ug/L 74 - 138 12/28/10 11:381,1,2-Trichloroethane ND 42.4 12 29 10L5751 NTL2991-05 50.0 85%ug/L 78 - 153 12/28/10 11:381,1,1-Trichloroethane 3.11 45.3 11 11 10L5751 NTL2991-05 50.0 84%ug/L 74 - 139 12/28/10 11:38Trichloroethene ND 36.9 14 33 10L5751 NTL2991-05 50.0 74%ug/L 53 - 149 12/28/10 11:38Trichlorofluoromethane ND 45.6 6 25 10L5751 NTL2991-05 50.0 91%ug/L 49 - 148 12/28/10 11:381,2,3-Trichloropropane ND 48.3 16 21 10L5751 NTL2991-05 50.0 97%ug/L 67 - 151 12/28/10 11:381,3,5-Trimethylbenzene ND 48.0 15 20 10L5751 NTL2991-05 50.0 96%ug/L 69 - 150 12/28/10 11:381,2,4-Trimethylbenzene ND 35.9 14 32 10L5751 NTL2991-05 50.0 72%ug/L 53 - 137 12/28/10 11:38Vinyl chloride ND 151 13 18 10L5751 NTL2991-05 150 101%ug/L 68 - 158 12/28/10 11:38Xylenes, total ND 45.4 8 32 10L5751 NTL2991-05 50.0 91%ug/L 59 - 145 12/28/10 11:38Diisopropyl Ether ND 87.9 11 33 10L5751 NTL2991-05 100 88%ug/L 60 - 152 12/28/10 11:381,2-Dichloroethene (total) 23.1 10L5751 NTL2991-05 25.0 92%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/28/10 11:38 24.1 10L5751 NTL2991-05 25.0 97%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/28/10 11:38 25.9 10L5751 NTL2991-05 25.0 103%Surrogate: Toluene-d8 ug/L 80 - 120 12/28/10 11:38 23.3 10L5751 NTL2991-05 25.0 93%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/28/10 11:38 10L5947-MSD1 ND 110000 4 31 10L5947 NTL2991-09RE 1 125000 88%ug/L 56 - 150 12/29/10 11:54Acetone ND 24700 1 12 10L5947 NTL2991-09RE 1 25000 99%ug/L 65 - 151 12/29/10 11:54Benzene ND 24200 0.4 23 10L5947 NTL2991-09RE 1 25000 97%ug/L 69 - 142 12/29/10 11:54Bromobenzene ND 24300 0.8 32 10L5947 NTL2991-09RE 1 25000 97%ug/L 64 - 154 12/29/10 11:54Bromochloromethane ND 27300 0.3 13 10L5947 NTL2991-09RE 1 25000 109%ug/L 75 - 138 12/29/10 11:54Bromodichloromethane ND 25500 1 18 10L5947 NTL2991-09RE 1 25000 102%ug/L 55 - 153 12/29/10 11:54Bromoform Page 24 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate Matrix Spike Dup - Cont. PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5947-MSD1 ND 22200 0.2 50 10L5947 NTL2991-09RE 1 25000 89%ug/L 13 - 176 12/29/10 11:54Bromomethane ND 122000 3 37 10L5947 NTL2991-09RE 1 125000 98%ug/L 45 - 164 12/29/10 11:542-Butanone ND 29900 5 21 10L5947 NTL2991-09RE 1 25000 120%ug/L 68 - 159 12/29/10 11:54sec-Butylbenzene ND 27400 6 11 10L5947 NTL2991-09RE 1 25000 110%ug/L 67 - 151 12/29/10 11:54n-Butylbenzene ND 28700 3 20 10L5947 NTL2991-09RE 1 25000 115%ug/L 73 - 153 12/29/10 11:54tert-Butylbenzene ND 20700 2 28 10L5947 NTL2991-09RE 1 25000 83%ug/L 33 - 187 12/29/10 11:54Carbon disulfide ND 26600 1 26 10L5947 NTL2991-09RE 1 25000 107%ug/L 64 - 157 12/29/10 11:54Carbon Tetrachloride ND 26300 2 11 10L5947 NTL2991-09RE 1 25000 105%ug/L 78 - 136 12/29/10 11:54Chlorobenzene ND 26400 0.8 16 10L5947 NTL2991-09RE 1 25000 105%ug/L 64 - 145 12/29/10 11:54Chlorodibromomethane ND 20900 0.8 35 10L5947 NTL2991-09RE 1 25000 84%ug/L 48 - 159 12/29/10 11:54Chloroethane ND 25000 1 32 10L5947 NTL2991-09RE 1 25000 100%ug/L 72 - 145 12/29/10 11:54Chloroform ND 19900 3 34 10L5947 NTL2991-09RE 1 25000 79%ug/L 10 - 194 12/29/10 11:54Chloromethane ND 25900 2 22 10L5947 NTL2991-09RE 1 25000 104%ug/L 66 - 155 12/29/10 11:542-Chlorotoluene ND 26600 2 22 10L5947 NTL2991-09RE 1 25000 106%ug/L 69 - 149 12/29/10 11:544-Chlorotoluene ND 23500 1 21 10L5947 NTL2991-09RE 1 25000 94%ug/L 49 - 162 12/29/10 11:541,2-Dibromo-3-chloropropane ND 28000 1 10 10L5947 NTL2991-09RE 1 25000 112%ug/L 70 - 152 12/29/10 11:541,2-Dibromoethane (EDB) ND 25300 0.5 11 10L5947 NTL2991-09RE 1 25000 101%ug/L 75 - 141 12/29/10 11:54Dibromomethane ND 26500 2 10 10L5947 NTL2991-09RE 1 25000 106%ug/L 75 - 135 12/29/10 11:541,4-Dichlorobenzene ND 27000 3 18 10L5947 NTL2991-09RE 1 25000 108%ug/L 72 - 146 12/29/10 11:541,3-Dichlorobenzene ND 27600 2 11 10L5947 NTL2991-09RE 1 25000 110%ug/L 80 - 136 12/29/10 11:541,2-Dichlorobenzene ND 19200 0.7 32 10L5947 NTL2991-09RE 1 25000 77%ug/L 23 - 159 12/29/10 11:54Dichlorodifluoromethane ND 22800 3 34 10L5947 NTL2991-09RE 1 25000 91%ug/L 64 - 154 12/29/10 11:541,1-Dichloroethane ND 22900 0.5 25 10L5947 NTL2991-09RE 1 25000 92%ug/L 72 - 137 12/29/10 11:541,2-Dichloroethane 4270 29200 1 32 10L5947 NTL2991-09RE 1 25000 100%ug/L 57 - 154 12/29/10 11:54cis-1,2-Dichloroethene ND 26400 0.6 31 10L5947 NTL2991-09RE 1 25000 105%ug/L 34 - 151 12/29/10 11:541,1-Dichloroethene ND 22900 1 32 10L5947 NTL2991-09RE 1 25000 92%ug/L 57 - 157 12/29/10 11:54trans-1,2-Dichloroethene Page 25 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate Matrix Spike Dup - Cont. PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5947-MSD1 ND 26900 2 20 10L5947 NTL2991-09RE 1 25000 108%ug/L 71 - 137 12/29/10 11:541,3-Dichloropropane ND 24000 1 11 10L5947 NTL2991-09RE 1 25000 96%ug/L 71 - 139 12/29/10 11:541,2-Dichloropropane ND 23200 0.2 11 10L5947 NTL2991-09RE 1 25000 93%ug/L 10 - 198 12/29/10 11:542,2-Dichloropropane ND 29800 0.07 35 10L5947 NTL2991-09RE 1 25000 119%ug/L 56 - 156 12/29/10 11:54cis-1,3-Dichloropropene ND 28400 1 26 10L5947 NTL2991-09RE 1 25000 114%ug/L 47 - 157 12/29/10 11:54trans-1,3-Dichloropropene ND 24500 2 18 10L5947 NTL2991-09RE 1 25000 98%ug/L 70 - 155 12/29/10 11:541,1-Dichloropropene ND 28000 2 12 10L5947 NTL2991-09RE 1 25000 112%ug/L 68 - 157 12/29/10 11:54Ethylbenzene ND 28000 7 21 10L5947 NTL2991-09RE 1 25000 112%ug/L 47 - 173 12/29/10 11:54Hexachlorobutadiene ND 141000 5 20 10L5947 NTL2991-09RE 1 125000 113%ug/L 57 - 154 12/29/10 11:542-Hexanone ND 32400 3 15 10L5947 NTL2991-09RE 1 25000 130%ug/L 69 - 139 12/29/10 11:54Isopropylbenzene ND 29100 5 18 10L5947 NTL2991-09RE 1 25000 116%ug/L 69 - 151 12/29/10 11:54p-Isopropyltoluene ND 22500 3 32 10L5947 NTL2991-09RE 1 25000 90%ug/L 56 - 152 12/29/10 11:54Methyl tert-Butyl Ether ND 25100 0.8 36 10L5947 NTL2991-09RE 1 25000 101%ug/L 71 - 136 12/29/10 11:54Methylene Chloride ND 138000 4 35 10L5947 NTL2991-09RE 1 125000 110%ug/L 62 - 159 12/29/10 11:544-Methyl-2-pentanone ND 28700 0.4 30 10L5947 NTL2991-09RE 1 25000 115%ug/L 56 - 161 12/29/10 11:54Naphthalene ND 27800 3 23 10L5947 NTL2991-09RE 1 25000 111%ug/L 61 - 167 12/29/10 11:54n-Propylbenzene ND 29100 1 29 10L5947 NTL2991-09RE 1 25000 116%ug/L 69 - 150 12/29/10 11:54Styrene ND 30100 0 11 10L5947 NTL2991-09RE 1 25000 120%ug/L 80 - 140 12/29/10 11:541,1,1,2-Tetrachloroethane ND 26000 4 28 10L5947 NTL2991-09RE 1 25000 104%ug/L 76 - 141 12/29/10 11:541,1,2,2-Tetrachloroethane ND 27000 2 16 10L5947 NTL2991-09RE 1 25000 108%ug/L 63 - 155 12/29/10 11:54Tetrachloroethene ND 26500 1 35 10L5947 NTL2991-09RE 1 25000 106%ug/L 61 - 153 12/29/10 11:54Toluene ND 28600 5 28 10L5947 NTL2991-09RE 1 25000 114%ug/L 57 - 155 12/29/10 11:541,2,3-Trichlorobenzene ND 28700 6 23 10L5947 NTL2991-09RE 1 25000 115%ug/L 64 - 147 12/29/10 11:541,2,4-Trichlorobenzene ND 26700 2 21 10L5947 NTL2991-09RE 1 25000 107%ug/L 74 - 138 12/29/10 11:541,1,2-Trichloroethane ND 23400 1 29 10L5947 NTL2991-09RE 1 25000 94%ug/L 78 - 153 12/29/10 11:541,1,1-Trichloroethane 67000 83800 0.1 11 10L5947 NTL2991-09RE 1 M8 25000 67%ug/L 74 - 139 12/29/10 11:54Trichloroethene Page 26 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 Orig. Val.UnitsAnalyte Sample DuplicatedBatchRPDDuplicate Matrix Spike Dup - Cont. PROJECT QUALITY CONTROL DATA Q Spike Conc % Rec. Target Range Analyzed Date/TimeLimit Volatile Organic Compounds by EPA Method 8260B 10L5947-MSD1 ND 21400 0.6 33 10L5947 NTL2991-09RE 1 25000 85%ug/L 53 - 149 12/29/10 11:54Trichlorofluoromethane ND 24600 4 25 10L5947 NTL2991-09RE 1 25000 98%ug/L 49 - 148 12/29/10 11:541,2,3-Trichloropropane ND 28100 3 21 10L5947 NTL2991-09RE 1 25000 113%ug/L 67 - 151 12/29/10 11:541,3,5-Trimethylbenzene ND 27900 3 20 10L5947 NTL2991-09RE 1 25000 111%ug/L 69 - 150 12/29/10 11:541,2,4-Trimethylbenzene ND 20900 1 32 10L5947 NTL2991-09RE 1 25000 84%ug/L 53 - 137 12/29/10 11:54Vinyl chloride ND 84200 2 18 10L5947 NTL2991-09RE 1 75000 112%ug/L 68 - 158 12/29/10 11:54Xylenes, total ND 24100 0.9 32 10L5947 NTL2991-09RE 1 25000 96%ug/L 59 - 145 12/29/10 11:54Diisopropyl Ether 4350 52100 1 33 10L5947 NTL2991-09RE 1 50000 96%ug/L 60 - 152 12/29/10 11:541,2-Dichloroethene (total) 23.4 10L5947 NTL2991-09RE 1 25.0 93%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/29/10 11:54 24.4 10L5947 NTL2991-09RE 1 25.0 98%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/29/10 11:54 26.0 10L5947 NTL2991-09RE 1 25.0 104%Surrogate: Toluene-d8 ug/L 80 - 120 12/29/10 11:54 23.1 10L5947 NTL2991-09RE 1 25.0 92%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/29/10 11:54 Page 27 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 CERTIFICATION SUMMARY Method Matrix TestAmerica Nashville AIHA Nelac North Carolina Water XN/A XSW846 8260B Page 28 of 29 2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404 Client Attn Hart & Hickman (2162) 2923 South Tryon Street, Suite 100 Charlotte, NC 28203-5449 Steve Hart Project Name: Work Order: Hart & Hickman (NC) Received: Project Number:PTT-001 / Former Dixie Trucking 12/22/10 09:35 NTL2985 DATA QUALIFIERS AND DEFINITIONS L Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the acceptance limits. Analyte not detected, data not impacted. L1 Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above acceptance limits. M8 The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS). R2 The RPD exceeded the acceptance limit. ND Not detected at the reporting limit (or method detection limit if shown) METHOD MODIFICATION NOTES Page 29 of 29