NCD991278953_20090725_National Starch & Chemical Corp._FRBCERCLA LTRA_Request for Permission to Dispose Phase III Soils-OCR

~ARCADIS
MEMO
To:
Mr. Jon Bornholm
Remedial Project Manager
U.S. Environmental Protection Agency
Region IV
61 Forsyth Street, SW
Atlanta, Georgia 30303
From:
Elizabeth L. Rhine
Project Coordinator
Date:
July 25, 2009
Subject:
Copies:
Angela Dohl
David Mattison, NCDENR DWM
Debra Rubenstein, Esq.
Jerry McMurray
ARCADIS Project No.:
B0060013.0001
Request for Permission to Dispose Phase Ill Soils
National Starch and Chemical Company Site, Salisbury, North Carolina
Operating Unit 4 Remediation
Dear Jon:
ARCADIS
30 Patewood Drive
Suite 155
Greenville
South Carolina 29615
Tel 864.987,3900
Fax [phone]
ARCADIS is completing the soil removal portion of the third phase of the road replacement activity for the OU 4
remediation. We have accumulated approximately 2,000 cubic yards of soil which is currently being stockpiled on-
site.
ARCADIS sampled each of these piles to determine the optimum soil disposal methods. The stockpile was sampled
six times with samples placed into laboratory provided containers, and delivered under chain of custody to Pace
Analytical Laboratories in Huntersville, North Carolina for analyses. The samples were analyzed for the presence of
volatile and semi-volatile organic compounds and total RCRA metals. After the first analytical reports from the small
stockpile were received, ARCADIS selected two of the samples for analysis using TCLP extraction followed by
analysis for volatile and semi-volatile organic compounds. This TCLP test results indicated that none of the samples
from the stockpile indicated the soils could be classified as hazardous (see Attachment for laboratory report).
The analytical results indicate that none of the soils could be classified as hazardous waste, however samples
collected from the stockpile contain concentrations of 1,2-dichloroethane (DCA) above the site cleanup standard of
169 micrograms per kilogram. It is our understanding from discussions with you, the presence of DCA in excess of
the cleanup standard necessitates the off-site disposal of these soils.
Page:
1/2
ARCADIS
ARCADIS and AkzoNobel are planning on the continued use of the already approved Earthtec Environmental,
Incorporated soil composting and bioremediation facility located in Chatham County, North Carolina. This is the
facility which received and is treating the Phase II soils from the site.
Our target date for off-site disposal of the Phase Ill soils is mid-next week. Should you have any questions regarding
this request, do not hesitate to contact the Project Coordinator.
Sincerely,
ARCADIS
/,." ' • 1\,1' l V,,\ • I l./
Elizabeth L. Rhine
Project Coordinator
Attachment
Page:
2/2
www.paoolabs.com
Pace Analytical Services, tnc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville. NC 28078
[phone]
July 22, 2009
Mr. Thomas Marr
LFR
113 Charter Place
Mooresville, NC 28117
RE: Project: AKZONOBEL
Pace Project No.: 9246497
Dear Mr. Marr:
Enclosed are the analytical results for sample(s) received by the laboratory on June 12, 2009. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NE LAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
n~'J-1=
Brandon Helton for
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc ..
Page 1 of 65
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Project: AKZONOBEL
Pace Project No.: 9246497
Charlotte Certification IDs
West Virginia Certification #: 357
Virginia Certification#: 00213
Tennessee Certification#: 04010
South Carolina Drinking Water Cert. #: 990060003
South Carolina Certification#: 990060001
Pennsylvania Certification#: 68-00784
Connecticut Certification#: PH-0104
Asheville Certification IDs
West Virginia Certification#: 356
Virginia Certification#: 00072
Connecticut Certification#: PH-0106
Florida/NELAP Certification#: E87648
Tennessee Certification#: 2980
South Carolina Certification#: 99030001
South Carolina Bioassay Certification#: 99030002
Eden Certification IDs
North Carolina Wastewater Certification#: 633
Virginia Drinking Water Certification#: 00424
Pace Analytical Services, Inc.
2225 Riverside Dr.
CERTIFICATIONS
Asheville, NC 28804
[phone]
North Carolina Field Services Certification #: 5342
North Carolina Drinking Water Certification#: 37706
New Jersey Certification#: NC012
Louisiana/LELAP Certification #: 04034
Kentucky UST Certification#: 84
F!orida/NELAP Certification#: E87627
North Carolina Wastewater Certification#: 12
Pennsylvania Certification#: 68-03578
North Carolina Wastewater Certification#: 40
North Carolina Drinking Water Certification#: 37712
North Carolina Bioassay Certification#: 9
New Jersey Certification#: NC011
Massachusetts Certification#: M-NC030
Louisiana/LELAP Certification #: 03095
North Carolina Drinking Water Certification #: 37738
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 65
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
2225 Riverside Dr. 9800 Kincey Ave. Suite 100
www pace/abs.com Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
SAMPLE ANALYTE COUNT
Project: AKZONOBEL
Pace Project No.: 9246497
Analytes
Lab ID Sample lD Method Analysts Reported Laboratory
9246497001 STK 3.1 ASTM 02974-87 TNM PASI-C
EPA6010 EWS 7 PASI-A
EPA 7471 JMW PASI-A
EPA8260 OLK 71 PASI-C
EPA8270 BET 75 PASI-C
9246497002 STK 3.2 ASTM 02974-87 TNM PASI-C
EPA6010 EWS 7 PASI-A
EPA 7471 JMW PASI-A
EPA8260 OLK 71 PASI-C
EPA 8270 BET 75 PASI-C
9246497003 STK 3.3 ASTM 02974-87 TNM PASI-C
EPA6010 EWS 7 PASI-A
EPA 7471 JMW PASI-A
EPA8260 OLK 15 PASI-C
EPA8260 OLK 71 PASI-C
EPA 8270 BET 75 PASI-C
EPA8270 BET 18 PASI-C
9246497004 STK 3.4 ASTM 02974-87 TNM PASI-C
EPA6010 EWS 7 PASI-A
EPA 7471 SHB PASI-A
EPA8260 OLK 15 PASI-C
EPA8260 OLK 71 PASI-C
EPA 8270 BET 75 PASI-C
EPA 8270 BET 18 PASI-C
9246497005 STK 3.5 ASTM 02974-87 TNM PASI-C
EPA6010 EWS 7 PASI-A
EPA 7471 SHB PASI-A
EPA8260 OLK 71 PASI-C
EPA8270 BET 75 PASI-C
9246497006 STK 3.6 ASTM 0297 4-87 TNM PASI-C
EPA6010 EWS 7 PASI-A
EPA 7471 SHB PASI-A
EPA 8260 OLK 71 PASI-C
EPA 8270 BET 75 PASI-C
9246497007 CONC 3.1 EPA6010 SHB 7 PASI-A
EPA 7470 SAJ PASI-A
EPA 8260 OLK 15 PASI-C
REPORT OF LABORATORY ANALYSIS Page 3 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
./>~ r--'°;{_f?,• ~" ... 11nelac,
www.paoolabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Lab ID Sample ID
9246497008 CONC 3.2
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
{828)254-7176
SAMPLE ANALYTE COUNT
Method Analysts
EPA8270
EPA6010
EPA 7470
EPA 8260
EPA 8270
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc ..
BET
SHB
SAJ
OLK
BET
Pace Analytical Services, lnc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytes
Reported Laboratory
18 PASI-C
7 PASl·A
PASI-A
15 PASI-C
18 PASI-C
Page 4 of 65
wwwpaceJabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.1
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497001 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 0.33 0611510916:14 0611610918:47 7440-38-2
Barium 40.1 mg/kg 0.33 0611510916:14 06116109 18:47 7440-39-3
Cadmium 7.8 mg/kg 0.066 06115109 16:14 06116109 18:47 7440-43-9
Chromium 23.8 mg/kg 0.33 06115109 16:14 06116109 18:47 7440-47-3
Lead 4.4 mg/kg 0.33 06115109 16:14 06116109 18:47 7439-92-1
Selenium 1.8 mg/kg 0.66 0611510916:14 06116109 18:47 7782-49-2
Silver ND mg/kg 0.33 0611510916:14 06/16109 18:47 7440-22-4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.051 mg/kg 0.0041 06115109 10:20 06/15109 17:51 7439-97-6
8270 MSSV Microwave Analytical Method: EPA8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 330 06125/09 14:20 07/01/09 08:14 83-32-9
Acenaphthylene ND ug/kg 330 06125109 14:20 07101109 08:14 208-96-8
Aniline NO ug/kg 330 06125109 14:20 07101109 08:14 62-53-3
Anthracene NO ug/kg 330 06125109 14:20 07101109 08:14 120-12-7
Benzo(a)anthracene ND ug/kg 330 06125109 14:20 07101109 08:14 56-55-3
Benzo(a)pyrene ND ug/kg 330 06125109 14:20 07101109 08:14 50-32-8
Benzo(b)fluoranthene ND uglkg 330 06125109 14:20 07101109 08:14 205-99-2
Benzo{g ,h ,i)perylene NO uglkg 330 06/25/09 14:20 07101109 08:14 191-24-2
Benzo(k)fluoranthene ND uglkg 330 06125109 14:20 07101109 08:14 207-08-9
Benzoic Acid NO uglkg 1650 06/25/09 14:20 07101109 08:14 65-85-0
Benzyl alcohol ND ug/kg 660 06125109 14:20 07101/09 08:14 100-51-6
4-Bromopherlylphenyl ether ND ug/kg 330 06/25/09 14:20 07101109 08:14 101-55-3
Butyl benzyl phth ala le ND uglkg 330 06125109 14:20 07101109 08:14 85-68-7
4-Chloro-3-methylphenol ND ug/kg 660 06125109 14:20 07101109 08:14 59-50-7
4-Chloroaniline ND uglkg 1650 06125109 14:20 07101109 0814 106-47-8
bis(2-Chloroethoxy)methane ND uglkg 330 06125109 14:20 07101109 08:14 111-91-1
bis(2-Chloroethyl) ether ND uglkg 330 06125109 14:20 07101109 08:14 111-44-4
bis(2-Chloroisopropyl) ether ND ug/kg 330 06/25/09 14:20 07101109 08:14 108-60-1
2-Chloronaphthalene ND uglkg 330 06125109 14:20 07101109 08:14 91-58-7
2-Chlorophenol ND uglkg 330 06125109 14 20 07/01/09 08:14 95-57-8
4-Chlorophenylphenyl ether ND ug/kg 330 06125109 14 20 07101109 08:14 7005-72-3
Chrysene ND uglkg 330 06125109 14:20 07101109 08:14 218-01-9
D ibenz( a, h) a nth racene NO ug/kg 330 06125109 14 20 07101109 08:14 53-70-3
Dibenzofuran ND uglkg 330 06125109 14:20 07/01109 08:14 132-64-9
1,2-Dichlorobenzene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 95-50-1
1,3-Dich!orobenzene ND ug/kg 330 06125109 14:20 07101109 08:14 541-73-1
1,4-Dichlorobenzene ND ug/kg 330 06/25/09 14:20 07101109 0814 106-46-7
3,3'-Dichlorobenzidine ND ug/kg 1650 06125109 14 20 07/01/09 08:14 91-94-1
2.4-Dichlorophenol ND ug/kg 330 06125109 14 20 07/01109 08:14 120-83-2
Diethylphthalate ND ug/kg 330 06125109 14:20 07101109 08:14 84-66-2
2,4-Dimethylphenol ND ug/kg 330 06125109 14 20 07101109 08:14 105-67-9
Dimethylphthalate ND ug/kg 330 06125109 14:20 07101/09 08:14 131-11-3
Di-n-butylphthalate ND ug/kg 330 06125109 14:20 07101109 08:14 84-74-2
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 5 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
--·:''t "ift'--g1ne c,
wwwpece/abs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.1 Lab ID:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
9246497001 Collected: 06/12109 00:00 Received: 06/12/09 16:20
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "wet•weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
4,6-Dinitro-2-methylphenol ND ug/kg 660 06/25/09 14:20 07/01/09 08:14 534-52-1
2,4-Dinitrophenol ND ug/kg 1650 06/25/09 14:20 07/01/09 08:14 51-28-5
2,4-Dinitrololuene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 121-14-2
2,6-Dinitrotoluene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 606-20-2
Di-n-octylphthalate ND ug/kg 330 06/25/09 14 20 07/01/09 08:14 117-84-0
1,2-Diphenylhydrazine ND ug/kg 330 06/25/09 14 20 07/01/09 08:14 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 117-81-7
Fluoranthene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 206-44-0
Fluorene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 86-73-7
Hexachloro-1,3-butadiene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 87-68-3
Hexachlorobenzene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 118-74-1
Hexachlorocyclopentadiene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 77-47-4
Hexachloroethane ND ug/kg 330 06/25/09 14 20 07/01/09 08:14 67-72-1
lndeno(1,2,3-cd)pyrene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 193-39-5
lsophorone ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 78-59-1
1-Methylnaphthalene ND ug/kg 330 06/25/09 14 20 07/01/09 08:14 90-12-0
2-Methylnaphthalene ND ug/kg 330 06/25/09 14:20 07/01/09 08: 14 91-57-6
2-Methylphenol(o-Cresol) ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 95-48-7
3&4-Methylphenol(m&p Cresol) ND ug/kg 330 06/25/09 14:20 07/01/09 08:14
Naphthalene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 91-20-3
2-Nitroaniline ND ug/kg 1650 06/25/09 14:20 07/01/09 08:14 88-74-4
3-Nitroaniline ND ug/kg 1650 06/25/09 14:20 07/01/09 08:14 99-09-2
4-Nitroaniline ND ug/kg 660 06/25/09 14:20 07/01/09 08:14 100-01-6
Nitrobenzene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 98-95-3
2-Nitrophenol ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 88-75-5
4-Nitrophenol ND ug/kg 1650 06/25/09 14:20 07/01/09 08:14 100-02-7
N-Nitrosodimethylamine ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 62-75-9
N-Nitroso-di-n-propylamine ND ug/kg 330 06/25/09 14:20 07/01/09 0814 621-64-7
N-N itros od i p henylami ne ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 86-30-6
Pentachlorophenol ND ug/kg 1650 06/25/09 14:20 07/01/09 08:14 87-86-5
Phenanthrene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 85-01-8
Phenol ND ugikg 330 06/25/09 14:20 07/01/09 08:14 108-95-2
Pyrene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 129-00-0
1,2.4-Trichlorobenzene ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 120-82-1
2,4 ,5-Trichlorophenol ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 95-95-4
2,4 ,6-Trichlorophenol ND ug/kg 330 06/25/09 14:20 07/01/09 08:14 88-06-2
Nitrobenzene-dS {S) 51 % 30-150 06/25/09 14:20 07/01/09 08:14 4165-60-0
2-Fluorobiphenyl (S) 61 % 46-120 06/25/09 14:20 07/01/09 08:14 321-60-8
Terphenyl-d14 (S) 64 % 38-108 06/25/09 14:20 07/01/09 08:14 1718-51-0
Phenol-d6 (S) 49 % 35-120 06/25/09 14:20 07/01/09 08:14 13127-88-3
2-Fluorophenol (S) 48 % 24-120 06/25/09 14:20 07/01/09 08:14 367-12-4
2,4,6-Tribromophenol (S) 67 % 44-136 06/25/09 14:20 07/01/09 08:14 118-79-6
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 75.3 06/22/09 20: 11 67-64-1
Benzene ND ug/kg 3.8 06/22/09 20 11 71-43-2
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 6 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
.. ~,:f!..{-•C~~'.'._o_,(<',.-11nelac,,
www.pecelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.1
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 9246497001 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA8260
Bromobenzene ND ug/kg 3.8 06/22/09 20: 11 108-86-1
Bromochloromethane ND ug/kg 3.8 06/22/09 20: 11 74-97-5
Bromodichloromethane ND ug/kg 3.8 06/22/09 20: 11 75-27-4
Bromoform ND u9/k9 3.8 06/22/09 20: 11 75-25-2
Bromomethane ND u9/k9 7.5 06/22/09 20: 11 74-83-9
2-Butanone (MEK) ND u9/kg 75.3 06/22/09 20:11 78-93-3
n-Butylbenzene ND ug/kg 3.8 06/22/09 20:11 104-51-8
sec-Butyl benzene ND ug/kg 3.8 06/22/09 20:11 135-98-8
tert-Butylbenzene ND ug/kg 3.8 06/22/09 20:11 98-06-6
Carbon tetrachloride ND u9/kg 3.8 06/22/09 20:11 56-23-5
Chlorobenzene ND ug/k9 3.8 06/22/09 20: 11 108-90-7
Chloroethane ND u9/k9 7.5 06/22/09 20 11 75-00-3
Chloroform ND u9/k9 3.8 06/22/09 20: 11 67-66-3
Chloromethane ND u9/k9 7.5 06/22/09 20: 11 74-87-3
2-Chlorotoluene ND u9/k9 3.8 06/22/09 20: 11 95-49-8
4-Chloroto1uene ND u9/kg 3.8 06/22/09 20: 11 106-43-4
1,2-Dibromo-3-chloropropane ND ug/kg 3.8 06/22/09 20:11 96-12-8
Dibromochloromethane ND ug/kg 3.8 06/22/09 20:11 124-48-1
1,2-Dibromoethane (EDS) ND ug/kg 3.8 06/22/09 20:11 106-93-4
Dibromomethane ND ug/kg 3.8 06/22/09 20: 11 74-95-3
1,2-Dichlorobenzene ND u9/k9 3.8 06/22/09 20: 11 95-50-1
1,3-Dichlorobenzene ND ug/kg 3.8 06/22/09 20:11 541-73-1
1,4-Dichlorobenzene ND ug/kg 3.8 06/22/09 20:11 106-46-7
Dichlorodifluoromethane ND u9/kg 7.5 06/22/09 20:11 75-71-8
1, 1-Dichloroethane ND ug/kg 3.8 06/22/09 20:11 75-34-3
1,2-Dichloroethane 31.3 ug/kg 3.8 06/22/09 20:11 107-06-2
1, 1-Dichloroethene ND ug/kg 3.8 06/22/09 20:11 75-35-4
cis-1,2-Dichloroethene ND ug/kg 3.8 06/22/09 20:11 156-59-2
trans-1,2-Dichloroethene ND ug/kg 3.8 06/22/09 20:11 156-60-5
1,2-Dichloropropane ND ug/kg 3.8 06/22/09 20:11 78-87-5
1,3-Dichloropropane ND ug/kg 3.8 06/22/09 20: 11 142-28-9
2,2-Dichloropropane ND ug/kg 3.8 06/22/09 20:11 594-20-7
1, 1-Dichloropropene ND ug/k9 3.8 06/22/09 20:11 563-58-6
cis-1,3-Dichloropropene ND u9/k9 3.8 06/22/09 20:11 10061-01-5
trans-1,3-Dichloropropene ND ug/kg 3.8 06/22/09 20: 11 10061-02-6
Diisopropyl ether ND u9/kg 3.8 06/22/09 20: 11 108-20-3
Ethyl benzene ND ug/kg 3.8 06/22/09 20:11 100-41-4
Hexachloro-1,3-butadiene ND ug/kg 3.8 06/22/09 20: 11 87-68-3
2-Hexanone ND ug/kg 37.7 06/22/09 20 11 591-78-6
lsopropylbenzene (Cumene) ND ug/kg 3.8 06/22/09 20:11 98-82-8
p-lsopropyltoluene ND ug/kg 3.8 06/22/09 20:11 99-87-6
Methylene Chloride ND ug/kg 15.1 06/22/09 20:11 75-09-2
4-Methyl-2-pentanone {MIBK) ND u9/k9 37.7 06/22/09 20:11 108-10-1
Methyl-tert-butyl ether ND ug/kg 3.8 06/22/09 20:11 1634-04-4
Naphthalene ND ug/kg 3.8 06/22/09 20:11 91-20-3
n-Propylbenzene ND ug/kg 3.8 06/22/09 20:11 103-65-1
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 7 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
~"-?-r-·~?_..~"~ o,nelac, :.'l -\:
www.pacelabs.com
Project AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.1
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
Lab ID: 9246497001 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8260/5035A Volatile Organics
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1.2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichloronuoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Oibromonuoromethane (S)
Toluene-dB (S)
4-Bromonuorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA 8260
ND ug/kg 3.8
ND uglkg 3.8
ND uglkg 3.8
ND ug/kg 3.8
ND uglkg 3.8
ND ug/kg 3.8
NO ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND uglkg 3.8
ND uglkg 3.8
ND uglkg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND uglkg 37.7
ND uglkg 7.5
ND uglkg 7.5
ND ug/kg 7.5
ND uglkg 3.8
109 % 79-116
98 % 88-110
96 % 74-115
109 % 69-121
Analytical Method: ASTM D2974-87
21.3 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc
Analyzed CAS No. Oual
06122109 20:11 100-42-5
06122109 20: 11 630-20-6
06122109 20: 11 79-34-5
06122109 20:11 127-18-4
06122109 20:11 108-88-3
06122109 20:11 87-61-6
06122109 20:11 120-82-1
06122109 20: 11 71-55-6
06122109 20: 11 79-00-5
06122109 20: 11 79-01-6
06122109 20: 11 75-69-4
06122109 20:11 96-18-4
06122109 20:11 95-63-6
06122109 20:11 108-67-8
06122109 20:11 108-05-4
06122109 20:11 75-01-4
06122109 20: 11 1330-20-7
06122109 20:11 1330-20-7
06122/09 20: 11 95-47-6
06122109 20:11 1868-53-7
06122109 20:11 2037-26-5
06122109 20:11 460-00-4
06122109 20:11 17060-07-0
06118109 15:22
Page 8 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.2
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab/O: 9246497002 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual
6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 0.46 06/15/09 16:14 06/16/09 18:52 7440-38-2
Barium 29.0 mg/kg 0.46 06/15/09 16:14 06/16/09 18:52 7440-39-3
Cadmium 7.5 mg/kg 0.093 06/15/09 16:14 06/16/09 18:52 7440-43-9
Chromium 23.8 mg/kg 0.46 06/15/09 16:14 06/16/09 18:52 7440-47-3
Lead 3.3 mg/kg 0.46 06/15/09 16:14 06/16/09 18:52 7439-92-1
Selenium 2.4 mg/kg 0.93 06/15/0916:14 06/16/09 18:52 7782-49-2
Silver ND mg/kg 0.46 06/15/09 16:14 06/16/0918:52 7440-22-4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.016 mg/kg 0.0044 06/15/09 10:20 06/15/09 17:56 7439-97-6 R1
8270 MSSV Microwave Analytical Method: EPA8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 83-32-9
Acenaphthylene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 208-96-8
Aniline ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 62-53-3
Anthracene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 120-12-7
Benzo(a)anthracene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 56-55-3
Benzo(a)pyrene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 50-32-8
Benzo(b)fluoranthene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 205-99-2
Benz o (g ,h, i) pe ryle ne ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 191-24-2
Benzo(k)fluoranthene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 207-08-9
Benzoic Acid ND ug/kg 1650 06/25/09 14:20 07/01/09 08:39 65-85-0
Benzyl alcohol ND ug/kg 660 06/25/09 14:20 07/01/09 08:39 100-51-6
4-Bromophenylphenyl ether ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 101-55-3
Butylbenzylphthalate · ND ug/kg 330 06/25/09 14 20 07/01/09 08:39 85-68-7
4-Chloro-3-methylphenol ND ug/kg 660 06/25/09 14:20 07/01/09 08:39 59-50-7
4-Chloroaniline ND ug/kg 1650 06/25/09 14 20 07/01/09 08:39 106-47-8
bis(2-Chloroethoxy)methane ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 111-91-1
bis(2-Chloroethyl) ether ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 111-44-4
bis(2-Chloroisopropyl) ether ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 108-60-1
2-Chloronaphthalene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 91-58-7
2-Chlorophenol ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 95-57-8
4-Chlorophenylphenyl ether ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 7005-72-3
Chrysene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 218-01-9
Di be nz( a, h )a nth racene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 53-70-3
Dibenzofuran ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 132-64-9
1,2-Dichlorobenzene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 95-50-1
1,3-Dichlorobenzene ND ug/kg 330 06/25/09 1420 07/01/09 08:39 541-73-1
1,4-0ichlorobenzene ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 106-46-7
3,3'-Dichlorobenzidine ND ug/kg 1650 06/25/09 14:20 07/01/09 08:39 91-94-1
2,4-Dichlorophenol ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 120-83-2
Oielhylphthalate ND ug/kg 330 06/25/09 14 20 07/01/09 08:39 84-66-2
2,4-Dimethylphenol ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 105-67-9
Oimethylphthalate ND ug/kg 330 06/25/09 14:20 07/01/09 08 39 131-11-3
Di-n-butylphthalate ND ug/kg 330 06/25/09 14:20 07/01/09 08:39 84-74-2
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 9 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,,o_'.~_:~~D,,
i1nelac;,,
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.2
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
{828)254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497002 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8270 MSSV Microwave
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydrazine
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-N itrosod i phenyl amine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2 ,4-Trichlorobenzene
2,4,5-T richlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
826015035A Volatile Organics
Acetone
Benzene
Date: 07/22/2009 04:35 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND ug/kg 660 06/25/09 14:20
ND ug/kg 1650 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 1650 06/25/09 14:20
ND ug/kg 1650 06/25/09 14:20
ND ug/kg 660 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 1650 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 1650 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
ND ug/kg 330 06/25/09 14:20
40 % 30-150 06/25/09 14 20
48 % 46-120 06125109 14:20
49 % 38-108 06125109 14:20
32 % 35-120 06125109 14 20
39 % 24-120 06/25/09 14:20
55 % 44-136 06/25/09 14:20
Analytical Method: EPA8260
1170 ug/kg 76.9
ND ug/kg 3.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CAS No. Qua\
07/01/09 08:39 534-52-1
07/01/09 08:39 51-28-5
07/01/09 08:39 121-14-2
07/01/09 08:39 606-20-2
07/01/09 08:39 117-84-0
07/01/09 08:39 122-66-7
07/01/09 08:39 117-81-7
07/01/09 08:39 206-44-0
07/01/09 08:39 86-73-7
07/01/09 08:39 87-68-3
07/01/09 08:39 118-74-1
07/01/09 08:39 77-47-4
07/01/09 08:39 67-72-1
07/01/09 08:39 193-39-5
07/01/09 08:39 78-59-1
07/01/09 08:39 90-12-0
07/01/09 08:39 91-57-6
07/01/09 08:39 95-48-7
07/01/09 08:39
07/01/09 08:39 91-20-3
07/01/09 08:39 88-74-4
07/01/09 08:39 99-09-2
07/01/09 08:39 100-01-6
07/01/09 08:39 98-95-3
07/01/09 08:39 88-75-5
07/01/09 08:39 100-02-7
07/01/09 08:39 62-75-9
07/01/09 08:39 621-64-7
07/01/09 08:39 86-30-6
07/01/09 08:39 87-86-5
07/01/09 08:39 85-01-8
07/01/09 08:39 108-95-2
07/01/09 08:39 129-00-0
07/01/09 08:39 120-82-1
07/01/09 08:39 95-95-4
07/01/09 08:39 88-06-2
07/01/09 08:39 4165-60-0
07101/09 08:39 321-60-8
07101109 08:39 1718-51-0
07/01/09 08 39 13127-88-3 2g
07/01/09 08:39 367-12-4
07/01/09 08:39 118-79-6
06/22/09 20:29 67-64-1
06/22/09 20:29 71-43-2
E
Page10of65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.2
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497002 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene ND uglkg 3.8 06122109 20:29 108-86-1
Bromochloromethane ND uglkg 3.8 06122109 20:29 74-97-5
Bromodichloromethane ND ug/kg 3.8 06122109 20:29 75-27-4
Bromoform ND ug/kg 3.8 06122109 20:29 75-25-2
Bromomethane ND u9/k9 7.7 06122109 20:29 74-83-9
2-Butanone (MEK) ND u9/kg 76.9 06122109 20:29 78-93-3
n-Butylbenzene ND u9/kg 3.8 06122/09 20:29 104-51-8
sec-Butylbenzene ND ug/kg 3.8 06122109 20:29 135-98-8
tert-Butylbenzene ND ug/kg 3.8 06122109 20:29 98-06-6
Carbon tetrachloride ND uglkg 3.8 06122109 20:29 56-23-5
Chlorobenzene ND uglkg 3.8 06122109 20:29 108-90-7
Chloroethane ND ug/kg 7.7 06122109 20:29 75-00-3
Chloroform ND uglkg 3.8 06122/09 20:29 67-66-3
Chloromethane ND ug/kg 7.7 06122109 20:29 74-87-3
2-Chlorotoluene ND uglkg 3.8 06122/09 20:29 95-49-8
4-Chlorotoluene ND uglkg 3.8 06122109 20 29 106-43-4
1,2-Dibromo-3-chloropropane ND uglkg 3.8 06122109 20:29 96-12-8
Dibromochloromethane ND uglkg 3.8 06122109 20:29 124-48-1
1,2-Dibromoethane (EDB) ND ug/kg 3.8 06122109 20:29 106-93-4
Dibromomethane ND uglkg 3.8 06/22109 20:29 74-95-3
1,2-Dichlorobenzene ND ug/kg 3.8 06122109 20:29 95-50-1
1,3-Dichlorobenzene ND uglk9 3.8 06122109 20:29 541-73-1
1,4-Oich!orobenzene ND u9/kg 3.8 06122/09 20 29 106-46-7
Dichlorodifluoromethane ND ug/kg 7.7 06122109 20:29 75-71-8
1, 1-Dichloroethane ND ug/kg 3.8 06122109 20:29 75-34-3
1,2-Dichloroethane 88.3 ug/kg 3.8 06122109 20:29 107-06-2
1, 1-Dichloroethene ND ug/kg 3.8 06/22109 20:29 75-35-4
cis-1,2-Dichloroethene ND ug/kg 3.8 06122109 20:29 156-59-2
trans-1,2-Dichloroethene ND ug/kg 3.8 06122109 20:29 156-60-5
1,2-Dichloropropane ND u9/k9 3.8 06122109 20:29 78-87-5
1,3-Dichloropropane ND ug/kg 3.8 06122109 20:29 142-28-9
2 ,2-Dichloropropane ND ug/kg 3.8 06122109 20:29 594-20-7
1, 1-Dichloropropene ND u9/kg 3.8 06122109 20:29 563-58-6
cis-1,3-Dichloropropene ND u9/kg 3.8 06122109 20:29 10061-01-5
lrans-1,3-Oichloropropene ND ug/kg 3.8 06122/09 20:29 10061-02-6
Dlisopropyl ether ND ug/kg 3.8 06122109 20 29 108-20-3
Ethylbenzene 10.4 ug/kg 3.8 06122/09 20 29 100-41-4
Hexachloro-1,3-butadlene ND ug/kg 3.8 06122109 20:29 87-68-3
2-Hexanone ND ug/k9 38.5 06122109 20:29 591-78-6
lsopropylbenzene (Cumene) ND ug/kg 3.8 06122109 20:29 98-82-8
p-lsopropyltoluene 5.1 ug/kg 3.8 06/22109 20:29 99-87-6
Methylene Chloride ND u9lk9 15.4 06122109 20:29 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/kg 38.5 06/22109 20:29 108-10-1
Methyl-tert-butyl ether ND u9/k9 3.8 06122109 20:29 1634-04-4
Naphthalene 8.1 ug/kg 3.8 06122109 20:29 91-20-3
n-Propylbenzene ND ug/kg 3.8 06122109 20:29 103-65-1
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 11 of 65
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc ..
. -~~---~,..sr-~.".·, ,•/1 la,, i1□e C's
www.pocolabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.2
Pace Analytical Services, Inc.
2225 Riverside Or.
ANALYTICAL RESULTS
Asheville, NC 28804
{828)254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497002 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
826015035A Volatile Organics
Styrene
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
a-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene {$)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA8260
ND u9/k9 3.8
ND u9/kg 3.8
ND u9/kg 3.8
ND uglk9 3.8
17500 uglkg 1010 250
ND uglk9 3.8
ND u9/k9 3.8
ND u9/k9 3.8
ND u9/kg 3.8
ND u9/kg 3.8
ND u9/kg 3.8
ND ug/k9 3.8
ND uglk9 3.8
ND ug/kg 3.8
ND uglk9 38.5
ND ug/kg 7.7
40-4 u9/kg 7.7
33.1 u9/kg 7.7
7.3 u9/kg 3.8
110 % 79-116
98 % 88-110
95 % 74-115
106 % 69-121
Analytical Method: ASTM D2974-87
23.7 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Analyzed CAS No. Qual
06122109 20:29 100-42-5
06122109 20:29 630-20-6
06122109 20:29 79-34-5
06122/09 20:29 127-18-4
06123/09 10:33 108-88-3
06122109 20:29 87-61-6
06122109 20:29 120-82-1
06/22109 20:29 71-55-6
06122109 20:29 79-00-5
06122109 20:29 79-01-6
06122109 20:29 75-69-4
06122/09 20:29 96-18-4
06122109 20:29 95-63-6
06122109 20:29 108-67-8
06122109 20:29 108-05-4
06122/09 20:29 75-01-4
06122109 20:29 1330-20-7
06122109 20:29 1330-20-7
06122/09 20:29 95-47-6
06/22/09 20:29 1868-53-7
06/22/09 20:29 2037-26-5
06/22/09 20:29 460-00-4
06/22/09 20:29 17060-07-0
06/18/09 15:22
Page 12 of 65
www.pectJlabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.3
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497003 Collected: 06/12/09 00:00 Received: 06/12/0916:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 0.46 06/16/09 15:22 06/17/09 17:06 7440-38-2
Barium 24.9 mg/kg 0.46 06/16/09 15:22 06/17/09 17:06 7440-39-3
Cadmium 8.9 mg/kg 0.093 06/16/09 15:22 06/17/09 17 06 7440-43-9
Chromium 26.4 mg/kg 0.46 06/16/09 15:22 06/17/09 17 06 7440-47-3
Lead 2.8 mg/kg 0.46 06/16/09 15:22 06/17/09 17:06 7439-92-1
Selenium 2.1 mg/kg 0.93 06/16/09 15:22 06/17/09 17:06 7782-49-2
Silver ND mg/kg 0.46 06/16/09 15:22 06/17/09 17:06 7440-22-4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.044 mg/kg 0.0050 06/15/09 10:20 06/15/09 18:00 7439-97-6
8~70 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 83-32-9
Acenaphthylene ND ug/kg 330 06/18/09 09:00 06/26/09 09: 1 5 208-96-8
Aniline ND ug/kg 330 06/18/09 09:00 06/26/09 09 15 62-53-3
Anthracene ND ug/kg 330 06/18/09 09:00 06/26/09 091 5 120-12-7
Benzo(a)anthracene ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 56-55-3
Benzo(a)pyrene ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 50-32-8
Benzo(b )fluoranthene ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 205-99-2
Benzo(g ,h,i)perylene ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 191-24-2
Benzo(k)fluoranthene ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 207-08-9
Benzoic Acid ND ug/kg 1650 06/18/09 09:00 06/26/09 09:15 65-85-0
Benzyl alcohol NO ug/kg 660 06/18/09 09:00 06/26/09 09:15 100-51-6
4-Bromophenylphenyl ether ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 101-55-3
Butylbenzylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 85-68-7
4-Chloro-3-methylphenol ND ug/kg 660 06/18/09 09:00 06/26/09 09: 15 59-50-7
4-Chloroaniline ND ug/kg 1650 06/18/09 09:00 06/26/09 09: 15 106-47-8
bis(2-Chloroethoxy)methane ND ug/kg 330. 06/18/09 09:00 06/26/09 09 15 111-91-1
bis(2-Chloroethyl) ether ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 111-44-4
bis(2-Chloroisopropyl) ether ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 108-60-1
2-Chloronaphthalene ND ug/kg 330 06/18/09 09:00 06/26/09 09: 1 5 91-58-7
2-Chlorophenol ND ug/kg 330 06/18/09 09:00 06/26/09 09: 1 5 95-57-8
4-Chlorophenylphenyl ether ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 7005-72-3
Chrysene ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 218-01-9
Dibenz( a, h) a nthra cene ND ug/kg 330 06/18/09 09:00 06/26/09 09 15 53-70-3
Dibenzofuran ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 132-64-9
1,2-Oichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 09 15 95-50-1
1,3-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 541-73-1
1,4-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 09: 1 5 106-46-7
3,3'-Dichlorobenzidine ND ug/kg 1650 06/18/09 09:00 06/26/09 09:15 91-94-1
2,4-Dichlorophenol ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 120-83-2
Diethylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 09: 15 84-66-2
2,4-Dimethylphenol ND ug/kg 330 06/18/09 09 00 06/26/09 09:15 105-67-9
Dimethylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 131-11-3
Di-n-bulylphlhalate ND ug/kg 330 06/18/09 09:00 06/26/09 09:15 84-74-2
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 13 of65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
_,-;(.:\q'-!.o,.,~ ibelac;,,
www.pacolabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.3 Lab ID:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
ANALYTICAL RESULTS
9246497003 Collected: 06/12/09 00:00 Received: 06/12/09 16:20
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8270 MSSV Microwave
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitroto!uene
Di-n-octylphthalate
1,2-Diphenylhydrazine
bis{2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachtoro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno{1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2.4 ,5-T richlorophenol
2.4 ,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromopheno! (S)
Date: 07/22/2009 04:35 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND ug/kg 660 06/18/09 09:00
ND ug/kg 1650 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
1230 ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 1650 06/18/09 09:00
ND ug/kg 1650 06/18/09 09:00
ND ug/kg 660 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 1650 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 1650 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
39 % 30-150 06/18/09 09:00
61 % 46-120 06/18/09 09:00
66 % 38-108 06/18/09 09:00
49 % 35-120 06/18/09 09:00
43 % 24-120 06/18/09 09:00
79 % 44-136 06/18/09 09 00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Analyzed CAS No. Oual
06/26/09 09:15 534-52-1
06/26/09 09: 15 51-28-5
06/26/09 09: 15 121-14-2
06/26/09 09: 15 606-20-2
06/26/09 09: 15 117-84-0
06/26/09 09:15 122-66-7
06/26/09 09:15 117-81-7
06/26/09 09:15 206-44-0
06/26/09 09:15 86-73-7
06/26/09 09: 15 87-68-3
06/26/09 09: 1 5 118-74-1
06/26/09 09: 15 77-47-4
06/26/09 09: 15 67-72-1
06/26/09 09:15 193-39-5
06/26/09 09:15 78-59-1
06/26/09 09:15 90-12-0
06/26/09 09:15 91-57-6
06/26/09 09: 15 95-48-7
06/26/09 09 15
06/26/09 09: 15 91-20-3
06/26/09 09: 15 88-74-4
06/26/09 09:15 99-09-2
06/26/09 09:15 100-01-6
06/26/09 09:15 98-95-3
06/26/09 09: 15 88-75-5
06/26/09 09: 15 100-02-7
06/26/09 09: 15 62-75-9
06/26/09 09: 15 621-64-7
06/26/09 09: 15 86-30-6
06/26/09 09:15 87-86-5
06/26/09 09:15 85-01-8
06/26/09 09:15 108-95-2
06/26/09 09:15 129-00-0
06/26/09 09:15 120-82-1
06/26/09 09:15 95-95-4
06/26/09 09:15 88-06-2
06/26/09 09:15 4165-60-0
06/26/09 09:15 321-60-8
06/26/09 09:15 1718-51-0
06/26/09 09: 15 13127-88-3
06/26/09 09: 15 367-12-4
06/26/09 09: 15 118-79-6
Page 14 of 65
WWW(Jlloolabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.3
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville. NC 28804
{828)254-7176
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497003 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-buladiene
Hexach!orobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
N\trobenzene
Pentachlorophenol
Pyridine
2,4,5-T richlorophenol
2 ,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1, 1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
1,2-Oichloroethane-d4 (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
8260/5035A Volatile Organics
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA8270 Preparation Method: EPA3510
Leachate Method/Date: EPA 1311; 07/16/09 00:00
ND ug/L 50.0 07/17/09 14:DD
NO ug/L 50.D 07/17/09 14 DD
ND ug/L 50.D 07/17/09 14:DD
ND ug/L 50.D 07/17/09 14:00
NO ug/L 50.D 07/17/09 14:DD
ND ug/L 50.D 07/17/09 14:DD
ND ug/L 50.D 07/17/0914:DD
ND ug/L 50.D 07/17/09 14:DD
ND ug/L 50.D 07/17/09 14:DD
ND ug/L 50.D 07/17/09 14:00
ND ug/L 50.D 07/17/09 14:00
ND ug/L 50.D 07/17/09 14:00
81 % 30-150 07/17/09 14:00
74 % 30-150 07/17/09 14:DD
78 % 30-150 07/17/09 14:00
31 % 25-150 07/17/09 14:DD
37 % 25-150 07/17/09 14:DD
77 % 25-150 07/17/09 14:DD
Analytical Method: EPA8260
ND ug/L 100 20
507 ug/L 200 20
ND ug/L 100 20
NO ug/L 100 20
ND ug/L 100 20
ND ug/L 100 20
ND ug/L 100 20
NO ug/L 100 20
ND ug/L 100 20
NO ug/L 100 20
NO ug/L 100 20
88 % 79-120 20
96 % 70-120 20
100 % 87-109 20
97 % 85-115 20
Analytical Method: EPA8260
ND ug/kg 4030 50
ND ug/kg 201 50
ND ug/kg 201 50
ND ug/kg 201 50
ND ug/kg 201 50
ND ug/kg 201 50
NO ug/kg 403 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services. Inc.
Analyzed CAS No. Qual
07/21/09 15:40 106-46-7
07/21/09 15:40 121-14-2
07/21/09 15:40 87-68-3
07/21/09 15:40 118-74-1
07/21/09 15:40 67-72-1
07/21/09 15:40 95-48-7
07/21/09 15:40
07/21/09 15:40 98-95-3
07/21/09 15:40 87-86-5
07/21/09 15:40 110-86-1
07/21/09 15:40 95-95-4
07/21/09 15:40 88-06-2
07/21/09 15:40 4165-60-D
07/21/0915:40 321-60-8
07/21/09 15:40 1718-51-0
07/21/09 15:40 13127-88-3
07/21/0915:40 367-12-4
07/21/0915:40 118-79-6
07/22/09 09: 19 71-43-2
07/22/09 09:19 78-93-3
07/22/09 09: 19 56-23-5
07/22/09 09:19 108-90-7
07/22/09 09:19 67-66-3
07/22/09 09:19 106-46-7
07/22/09 09:19 107-06-2
07/22/09 09:19 75-35-4
07/22/09 09:19 127-18-4
07/22/09 09:19 79-01-6
07/22/09 09:19 75-01-4
07/22/09 09:19 17060-07-0
07/22/09 09: 19 2037-26-5
07 /22/09 09: 19 460-00-4
07 /22/09 09: 19 1868-53-7
06/23/09 10:15 67-64-1
06/23/0910:15 71-43-2
06/23/09 10:15 108-86-1
06/23/09 10:15 74-97-5
06/23/09 1 D: 15 75-27-4
06/23/09 1 D: 15 75-25-2
06/23/09 1 D: 15 74-83-9
Page 15 of 65
WW'W'paoolabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.3
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
LablD: 9246497003 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA8260
2-Butanone (MEK) ND ug/kg 4030 • 50 06/23/09 10:15 78-93-3
n-Butylbenzene ND ug/kg 201 50 06/23/09 10:15 104-51-8
sec-Butylbenzene NO ug/kg 201 50 06/23/09 10:15 135-98-8
tert-Butylbenzene NO ug/kg 201 50 06/23/09 10:15 98-06-6
Carbon tetrachloride ND ug/kg 201 50 06/23/09 10: 15 56-23-5
Chlorobenzene ND ug/kg 201 50 06/23/09 1 O: 15 108-90-7
Chloroethane ND ug/kg 403 50 06/23/09 10:15 75-00-3
Chloroform NO ug/kg 201 50 06/23/0910:15 67-66-3
Ch!oromethane NO ug/kg 403 50 06/23/09 10:15 74-87-3
2-Chlorotoluene NO ug/kg 201 50 06/23/09 1 0: 15 95-49-8
4-Chlorototuene ND ug/kg 201 50 06/23/09 10: 15 106-43-4
1,2-0ibromo-3-chloropropane NO u9/k9 201 50 06/23/09 10:15 96-12-8
Dibromochloromethane NO u9/k9 201 50 06/23/0910:15 124-48-1
1,2-Dibromoethane (EDS) ND u9/k9 201 50 06/23/09 10:15 106-93-4
Dibromomethane ND ug/kg 201 50 06/23/09 10:15 74-95-3
1,2-Dichlorobenzene ND u9/k9 201 50 06/23/09 10:15 95-50-1
1,3-Dichlorobenzene NO ug/kg 201 50 06/23/09 10:15 541-73-1
1,4-Dichlorobenzene ND ug/kg 201 50 06/23/09 10: 15 106-46-7
Dichlorodifluoromethane NO u9/k9 403 50 06/23/09 10:15 75-71-8
1.1-Dichloroethane NO u9/k9 201 50 06/23/09 10:15 75-34-3
1,2-Dichloroethane 342 ug/kg 201 50 06/23/09 10:15 107-06-2
1, 1-Dichloroethene ND u9/k9 201 50 06/23/09 10:15 75-35-4
cis-1,2-Dichloroethene ND u9/k9 201 50 06/23/0910:15 156-59-2
trans-1,2-Dichloroethene ND ug/kg 201 50 06/23/09 10:15 156-60-5
1,2-Dichtoropropane NO u9/k9 201 50 06/23/09 10: 15 78-87-5
1,3-Dich!oropropane ND ug/kg 201 50 06/23/09 10:15 142-28-9
2,2-Dichloropropane ND ug/kg 201 50 06/23/09 10:15 594-20-7
1, 1-Dichloropropene ND u9/k9 201 50 06/23/09 10:15 563-58-6
cis-1,3-Dichloropropene NO u9/k9 201 50 06/23/09 10:15 10061-01-5
trans-1,3-0ichloropropene ND u9/k9 201 50 06/23/09 10:15 10061-02-6
Diisopropyl ether NO u9/k9 201 50 06/23/09 10:15 108-20-3
Ethylbenzene ND ug/kg 201 50 06/23/09 10:15 100-41-4
Hexachloro-1,3-buladiene 92000 ug/kg 10100 2500 06/23/09 23:36 87-68-3
2-Hexanone ND u9/k9 2010 50 06/23/09 10:15 591-78-6
lsopropylbenzene {Cumene) ND u9/k9 201 50 06/23/09 10: 15 98-82-8
p-lsopropy!toluene ND u9/k9 201 50 06/23/09 10: 15 99-87-6
Methylene Chloride ND u9/k9 805 50 06/23/09 10: 15 75-09-2
4-Methyl-2-pentanone (MIBK) ND u9/k9 2010 50 06/23/09 10 15 108-10-1
Methyl-tert-butyl ether ND ug/kg . 201 50 06/23/09 10:15 1634-04-4
Naphthalene ND u9/k9 201 50 06/23/09 10:15 91-20-3
n-Propylbenzene NO u9/k9 201 50 06/23/09 10:15 103-65-1
Styrene ND u9/k9 201 50 06/23/09 10:15 100-42-5
1,1, 1,2-Tetrachloroethane NO u9/k9 201 50 06/23/0910:15 630-20-6
1, 1,2,2-Tetrachtoroethane ND u9/k9 201 50 06/23/09 10: 15 79-34-5
Tetrachloroethene ND ug/kg 201 50 06/23/09 10: 15 127-18-4
Toluene 261 ug/kg 201 50 06/23/09 10: 15 108-88-3
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 16 of65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
-."-)'!:\·~--~?~>~ 1:nelac1;
www.pecelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.3
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, 1nc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497003 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
826015035A Volatile Organics
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
T richlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
a-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 0712212009 04:35 PM
Results Unlts Report Limit OF Prepared
Analytical Method: EPA 8260
ND uglkg 201 50
ND uglkg 201 50
ND uglkg 201 50
ND ug/kg 201 50
ND uglkg 201 50
ND uglkg 201 50
ND uglkg 201 50
ND ug/kg 201 50
ND uglkg 201 50
ND uglkg 2010 50
ND uglkg 403 50
ND uglkg 403 50
ND uglkg 403 50
ND uglkg 201 50
110 % 79-116 50
102 % 88-110 50
93 % 74-115 50
110 % 69-121 50
Analytical Method: ASTM 02974-87
28.4 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc.
Analyzed GAS No. Qual
06123109 10:15 87-61-6
06/2310910:15 120-82-1
06123109 10:15 71-55-6
06123109 10: 15 79-00-5
06123109 10: 15 79-01-6
06123109 1 0: 15 75-69-4
06123109 1 0: 15 96-18-4
06123109 1 0: 15 95-63-6
06/2310910:15 108-67-8
06123109 10:15 108-05-4
06123109 10:15 75-01-4
06123109 10:15 1330-20-7
06123109 1 0: 15 1330-20-7
06123109 1 0: 15 95-47-6
0612310910:15 1868-53-7
0612310910:15 2037-26-5
0612310910:15 460-00-4
06123109 10: 15 17060-07-0
06118/09 15:23
Page 17 of 65
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.4
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497004 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit · DF Prepared Analyzed CAS No. Oual
6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 0.44 06/16/09 15:22 06/17/0917:10 7440-38-2
Barium 26.0 mg/kg 0.44 06/16/09 15:22 06/17/09 17: 10 7440-39-3
Cadmium 6.3 mg/kg 0.088 06/16/09 15:22 06/17/09 17: 10 7440-43-9
Chromium 21.2 mg/kg 0.44 06/16/09 15:22 06/17/0917:10 7440-47-3
Lead 3.7 mg/kg 0.44 06/16/09 15:22 06/17/0917:10 7439-92-1
Selenium 1.9 mg/kg 0.88 06/16/0915:22 06/17/0917:10 7782-49-2
Silver ND mg/kg 0.44 06/16/09 15:22 06/17/09 17:10 7440-22-4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.050 mg/kg 0.0044 06/16/09 19:30 06/17/09 14:07 7439-97-6 R1
8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 83-32-9
Acenaphthylene ND ug/k9 330 06/18/09 09:00 06/26/09 09:40 208-96-8
Aniline ND ug/k9 330 06/18/09 09:00 06/26/09 09:40 62-53-3
Anthracene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 120-12-7
Benzo(a)anthracene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 56-55-3
Benzo(a)pyrene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 50-32-8
Benzo(b)fiuoranthene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 205-99-2
Benzo(g ,h,i)perylene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 191-24-2
Benzo(k)fiuoranthene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 207-08-9
Benzoic Acid ND ug/kg 1650 06/18/09 09:00 06/26/09 09:40 65-85-0
Benzyl alcohol ND ug/kg 660 06/18/09 09:00 06/26/09 09:40 100-51-6
4-Bromophenylphenyl ether ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 101-55-3
Butyl be nzylphthal ate ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 85-68-7
4-Chloro-3-methylphenol ND ug/kg 660 06/18/09 09:00 06/26/09 09:40 59-50-7
4-Chloroaniline ND ug/kg 1650 06/18/09 09:00 06/26/09 09:40 106-47-8
bis(2-Chloroethoxy)methane ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 111-91-1
bis(2-Chloroethyl) ether ND ug/k9 330 06/18/09 09:00 06/26/09 09:40 111-44-4
bis(2-Chloroisopropyl) ether ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 108-60-1
2-Chloronaphthalene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 91-58-7
2-Chlorophenol ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 95-57-8
4-Chlorophenylphenyl ether ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 7005-72-3
Chrysene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 218-01-9
Dibenz(a ,h)anthracene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 53-70-3
Dibenzofuran ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 132-64-9
1,2-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 95-50-1
1,3-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 541-73-1
1,4-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 106-46-7
3,3'-Dichlorobenzidine ND ug/kg 1650 06/18/09 09:00 06/26/09 09:40 91-94-1
2,4-Dichlorophenol ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 120-83-2
Diethylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 84-66-2
2,4-Dimethylphenol ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 105-67-9
Dimethylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 131-11-3
Di-n-butylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 09:40 84-74-2
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 18 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Seivices, !nc ..
.. ~-:':-\."-~~t-",'s'..-~ ;,nelae:,
www.paceJabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.4 Lab ID:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
9246497004 Collected: 06/12/09 00:00 Received: 06/12/09 16:20
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8270 MSSV Microwave
4,6-Dinitro-2-methylphenol
2.4-Dinitrophenol
2.4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydrazine
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachtorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Creso!)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzeile
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2.4 ,5-Trich!orophenol
2.4 ,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-dB (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND ug/kg 660 06/18/09 09:00
ND u9/k9 1650 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
1420 u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 1650 06/18/09 09:00
ND u9/k9 1650 06/18/09 09:00
ND u9/k9 660 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND ug/kg 1650 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND ug/kg 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 1650 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
ND u9/k9 330 06/18/09 09:00
53 % 30-150 06/18/09 09:00
63 % 46-120 06/18/09 09:00
65 % 38-108 06/18/09 09:00
52 % 35-120 06/18/09 09:00
42 % 24-120 06/18/09 09:00
83 % 44-136 06/18/09 09:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed GAS No. Qual
06/26/09 09:40 534-52-1
06/26/09 09:40 51-28-5
06/26/09 09:40 121-14-2
06/26/09 09:40 606-20-2
06/26/09 09:40 117-84-0
06/26/09 09:40 122-66-7
06/26/09 09:40 117-81-7
06/26/09 09:40 206-44-0
06/26/09 09:40 86-73-7
06/26/09 09:40 87-68-3
06/26/09 09:40 118-74-1
06/26/09 09:40 77-47-4
06/26/09 09:40 67-72-1
06/26/09 09:40 193-39-5
06/26/09 09:40 78-59-1
06/26/09 09:40 90-12-0
06/26/09 09:40 91-57-6
06/26/09 09:40 95-48-7
06/26/09 09:40
06/26/09 09:40 91-20-3
06/26/09 09:40 88-74-4
06/26/09 09:40 99-09-2
06/26/09 09:40 100-01-6
06/26/09 09:40 98-95-3
06/26/09 09:40 88-75-5
06/26/09 09:40 100-02-7
06/26/09 09:40 62-75-9
06/26/09 09:40 621-64-7
06/26/09 09:40 86-30-6
06/26/09 09:40 87-86-5
06/26/09 09:40 85-01-8
06/26/09 09:40 108-95-2
06/26/09 09:40 129-00-0
06/26/09 09:40 120-82-1
06/26/09 09:40 95-95-4
06/26/09 09:40 88-06-2
06/26/09 09:40 4165-60-0
06/26/09 09:40 321-60-8
06/26/09 09:40 1718-51-0
06/26/09 09:40 13127-88-3
06/26/09 09:40 367-12-4
06/26/09 09:40 118-79-6
Page 19 of 65
wwwpacelabs.oom
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.4
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497004 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4 ,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1 , 1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
8260/S0JSA Volatile Organics
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA8270 Preparation Method: EPA3510
Leachate Method/Date: EPA 1311; 07/16/09 00:00
ND ug/L 50.0 07117109 14:00
ND u9/L 50.0 07117109 14:00
ND u9/L 50.0 0711710914:00
ND u9/L 50.0 0711710914:00
ND u9/L 50.0 07117109 14:00
ND u9/L 50.0 07117109 14:00
ND ug/L 50.0 07117109 14:00
ND u9/L 50.0 07117109 14:00
ND u9/L 50.0 07117/0914:00
ND u9/L 50.0 0711710914:00
ND u9/L 50.0 07/17109 14:00
ND u9/L 50.0 07/17/09 14:00
40 % 30-150 07117109 14:00
45 % 30-150 07117/09 14:00
39 % 30-150 07/17/09 14:00
25 % 25-150 07/17/09 14:00
34 % 25-150 07/17/09 14:00
36 % 25-150 07/17/09 14:00
Analytical Method: EPA8260
ND ug/L 5.0
57.7 ug/L 10.0
ND u9/L 5.0
ND ug/L 5.0
ND ug/L 5.0
ND ug/L 5.0
296 ug/L 5.0
ND ug/L 5.0
ND u9/L 5.0.
ND u9/L 5.0
7.7 u9/L 5.0
112 % 79-120
98 % 70-120
gg % 87-109
111 % 85-115
Analytical Method: EPA 8260
684 ug/kg 76.3
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND u9/k9 3.8
ND ug/kg 3.8
ND ug/kg 7.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Seivices, Inc ..
Analyzed CAS No. Qual
07121109 16:30 106-46-7
07121109 16:30 121-14-2
07121109 16:30 87-68-3
07121/0916:30 118-74-1
0712110916:30 67-72-1
07121109 16:30 95-48-7
07121109 16:30
07121109 16:30 98-95-3
07121109 16:30 87-86-5
07121109 16:30 110-86-1
07/21/09 16:30 95-95-4
07/21/09 16:30 88-06-2
07121/09 16:30 4165-60-0
07121/09 16:30 321-60-8
07/21/09 16:30 1718-51-0
07/21/09 16:30 13127-88-3
07/21109 16:30 367-12-4
07/21/0916:30 118-79-6
06122/09 21:06 71-43-2
06/22/09 21 :06 78-93-3
06/22/09 21:06 56-23-5
06/22/09 21:06 108-90-7
06/22/09 21:06 67-66-3
06/22109 21 :06 106-46-7
06/22/09 21 :06 107-06-2 E
06/22/09 21:06 75-35-4
06122/09 21 :06 127-18-4
06122/09 21 :06 79-01-6
06/22/09 21 :06 75-01-4
06/22/09 21:06 17060-07-0
06/22/09 21:06 2037-26-5
06/22109 21 :06 460-00-4
06/22/09 21 :06 1868-53-7
06/22/09 21 :06 67-64-1 E
06/22/09 21 :06 71-43-2
06/22/09 21 :06 108-86-1
06/22/09 21 :06 74-97-5
06/22/09 21 :06 75-27-4
06122109 21 :06 75-25-2
06/22/09 21 :06 74-83-9
Page 20 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.4
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497004 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
826015035A Volatile Organics
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1, 1-Dichloroethane
1,2-Dichloroethane
1, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1, 1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether
Ethyl benzene
Hexachloro-1,3-butadiene
2-Hexanone
lsopropylbenzene {Cumene)
p-lsopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachtoroethane
Tetrachloroethene
Toluene
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA 8260
ND ug/kg 76.3
ND ugikg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 7.6
ND ug/kg 3.8
ND ug/kg 7.6
ND ug/kg 3.8
ND ugikg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 7.6
ND ug/kg 3.8
226 ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ugikg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 38.2
ND ugikg 3.8
ND ugikg 3.8
ND ug/kg 15.3
ND ug/kg 38.2
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ugikg 3.8
ND ug/kg 3.8
160 ug/kg 3.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analy2ed CAS No. Qual
06/22/09 21 :06 78-93-3
06/22/09 21 :06 104-51-8
06/22/09 21:06 135-98-8
06/22/09 21:06 98-06-6
06/22/09 21 :06 56-23-5
06/22/09 21 :06 108-90-7
06/22/09 21 :06 75-00-3
06/22/09 21 :06 67-66-3
06/22/09 21:06 74-87-3
06/22/09 21:06 95-49-8
06/22/09 21:06 106-43-4
06/22/09 21:06 96-12-8
06/22/09 21:06 124-48-1
06/22/09 21 :06 106-93-4
06/22/09 21 :06 74-95-3
06/22/09 21 :06 95-50-1
06/22/09 21:06 541-73-1
06/22/09 21:06 106-46-7
06/22/09 21 :06 75-71-8
06/22/09 21 :06 75-34-3
06/22/09 21 :06 107-06-2 E
06/22/09 21:06 75-35-4
06/22/09 21:06 156-59-2
06/22/09 21:06 156-60-5
06/22/09 21:06 78-87-5
06/22/09 21:06 142-28-9
06/22/09 21:06 594-20-7
06/22/09 21 :06 563-58-6
06/22/09 21 :06 10061-01-5
06/22/09 21 :06 10061-02-6
06/22/09 21 :06 108-20-3
06/22/09 21 :06 100-41-4
06/22/09 21 :06 87-68-3
06/22/09 21:06 591-78-6
06/22/09 21:06 98-82-8
06/22/09 21 :06 99-87-6
06/22/09 21 :06 75-09-2
06/22/09 21 :06 108-10-1
06/22/09 21 :06 1634-04-4
06/22/09 21 :06 91-20-3
06/22/09 21 :06 103-65-1
06/22/09 21 :06 100-42-5
06/22/09 21 :06 630-20-6
06/22/09 21 :06 79-34-5
06/22/09 21 :06 127-18-4
06/22/09 21 :06 108-88-3 E
Page 21 of 65
www.paClllabs_com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.4
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
{704)875-9092
LablD: 9246497004 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8260/S0JSA Volatile Organics
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethyfbenzene
1,3,5-T rimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
a-Xylene
Dibromofluoromethane (S}
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 07/22/2009 04:35 PM •
Results Units Report Limit OF Prepared
Analytical Method: EPA8260
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND u9/kg 3.8
ND ug/kg 3.8
ND ug/kg 3.8
ND ug/k9 3.8
ND ug/kg 3.8
ND ug/kg 38.2
ND ug/kg 7.6
ND ug/kg 7.6
ND ug/kg 7.6
ND uglkg 3.8
111 % 79-116
98 % 88-110
99 % 74-115
112 % 69-121
Analytical Method: ASTM D2974-87
29.7 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed GAS No. Qual
06/22/09 21 :06 87-61-6
06/22/09 21 :06 120-82-1
06/22/09 21 :06 71-55-6
06/22/09 21 :06 79-00-5
06/22/09 21:06 79-01-6
06/22/09 21:06 75-69-4
06/22/09 21 :06 96-18-4
06/22/09 21 :06 95-63-6
06/22/09 21 :06 108-67-8
06/22/09 21 :06 108-05-4
06/22/09 21:06 75-01-4
06/22/09 21:06 1330-20-7
06/22/09 21 :06 1330-20-7
06/22109 21 :06 95-47-6
06/22109 21 :06 1868-53-7
06122/09 21 :06 2037-26-5
06122/09 21 :06 460-00-4
06122/09 21:06 17060-07-0
06/18109 15:23
Page 22 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.5
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497005 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua1
6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 0.40 06116109 15:22 06117109 17:15 7440-38-2
Barium 49.0 mg/kg 0.40 06116109 15:22 06117109 17: 15 7440-39-3
Cadmium 6.2 mg/kg 0.081 06/16109 15:22 06/17/0917:15 7440-43-9
Chromium 31.6 mg/kg 0.40 06116109 15:22 06117109 17:15 7440-47-3
Lead 4.3 mg/kg 0.40 06116109 15:22 06117109 17:15 7439-92-1
Selenium 1.8 mg/kg 0.81 06116109 15:22 06117109 17:15 7782-49-2
Silver ND mg/kg 0.40 06116109 15:22 06117109 17:15 7440-22-4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.075 mg/kg 0.0035 06116109 19:30 06117109 14:17 7439-97-6
8270 MSSV Microwave Analytical Method: EPA8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 330 06118109 09:00 06/26109 10:06 83-32-9
Acenaphthylene ND ug/kg 330 06118109 09:00 06126109 10:06 208-96-8
Aniline ND ug/kg 330 06118109 09:00 06126109 10:06 62-53-3
Anthracene ND uglkg 330 06118109 09:00 06126109 10:06 120-12-7
Benzo(a)anthracene ND ug/kg 330 06118109 09:00 06126109 10:06 56-55-3
Benzo(a)pyrene ND uglkg 330 06118109 09:00 06126109 10:06 50-32-8
Benzo(b)fluoranthene ND uglkg 330 06118109 09:00 06126109 10:06 205-99-2
Benz o (g, h, i) pe ryle ne ND uglkg 330 06118109 09:00 06126109 10:06 191-24-2
Benzo(k)fluoranthene ND ug/kg 330 06118109 09:00 06126109 10:06 207-08-9
Benzoic Acid ND uglkg 1650 06118109 09:00 06126109 10:06 65-85-0
Benzyl alcohol ND ug/kg 660 06118109 09:00 06126109 10:06 100-51-6
4-Bromophenylphenyl ether ND uglkg 330 06118109 09:00 06126109 10:06 101-55-3
Butylbenzylphthalate ND uglkg 330 06118109 09:00 06126109 10:06 85-68-7
4-Chloro-3-methylphenol ND uglkg 660 06118109 09:00 06126109 10:06 59-50-7
4-Chloroaniline ND ug/kg 1650 06118109 09:00 06/26109 10:06 106-47-8
bis(2-Chloroethoxy)methane ND uglkg 330 06/18/09 09:00 06126109 10:06 111-91-1
bis(2-Chloroethyl) ether ND ug/kg 330 06118109 09:00 06126109 10:06 111-44-4
bis(2-Chloroisopropyl) ether ND ug/kg 330 06118109 09:00 06126109 10:06 108-60-1
2-Chloronaphthalene ND uglkg 330 06118109 09:00 06126109 10:06 91-58-7
2-Chlorophenol ND ug/kg 330 06118109 09:00 06126/09 10:06 95-57-8
4-Chlorophenylphenyl ethe_r ND uglkg 330 06118109 09:00 06126109 10:06 7005-72-3
Chrysene ND uglkg 330 06118109 09:00 06126109 10:06 218-01-9
Oibe nz( a, h )a nlhracene ND ug/kg 330 06118109 09:00 06126109 10:06 53-70-3
Dibenzofuran ND uglkg 330 06118/09 09:00 06126/09 10:06 132-64-9
1,2-Dichlorobenzene ND uglkg 330 06118/09 09:00 06126109 10:06 95-50-1
1,3-Oich!orobenzene ND ug/kg 330 06118109 09:00 06126/09 10:06 541-73-1
1.4-Dichlorobenzene ND uglkg 330 06118109 09:00 06126109 10:06 106-46-7
3,3'-Dichlorobenzidine ND ug/kg 1650 06118/09 09:00 06126109 10:06 91-94-1
2.4-Dichlorophenol ND uglkg 330 06118109 09:00 06126109 10:06 120-83-2
Oiethylphthalate NO ug/kg 330 06118109 09:00 06126109 10:06 84-66-2
2,4-Oimethylphenol ND ug/kg 330 06/18109 09 00 06126109 10:06 105-67-9
Dimethylphthalate ND ug/kg 330 06118109 09:00 06126109 10:06 131-11-3
Di-n-bulylphthalate ND ug/kg 330 06/18/09 09:00 06/26109 1006 84-74-2
Date: 0712212009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 23 of 65
This report shall not be reproduced. except in full,
without the written consent of Pace Analytical Services, Inc ..
,,;;.{.!~?-°;-,,. ibelac;,
wwwpece/abs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.5
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497005 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8270 MSSV Microwave
4,6-Dinitro-2-methytphenol
2,4-Dinitrophenol
2 ,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydrazine
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
1-Methylnaphthatene
2-Methylnaphthatene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nilrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2 ,4,6-Trichlorophenol
Nitrobenzene-dS (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-dB (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260/5035A Volatile Organics
Acetone
Benzene
Date: 07/22/2009 04:35 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA8270 Preparation Method: EPA3546
ND u9/k9 660 06118109 09:00
ND u9/k9 1650 06118109 09:00
ND.u9/k9 330 06118109 09:00
ND ug/kg 330 06/18/09 09:00
ND u9/k9 330 06118109 09:00
ND uglkg 330 06118/09 09:00
ND ug/kg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND ug/kg 330 06118109 09:00
ND ug/kg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglk9 330 06118109 09:00
ND ug/kg 330 06118109 09:00
ND u9/kg 330 06118109 09:00
ND ug/kg 1650 06118109 09:00
ND uglkg 1650 06118109 09:00
ND uglkg 660 06118109 09:00
ND uglk9 330 06118109 09:00
ND uglkg 330 06118109 09:00
ND uglkg 1650 06118109 09:00
ND ug/kg 330 06118109 09:00
ND ug/kg 330 06118109 09:00
ND ug/kg 330 06118109 09:00
ND uglkg 1650 06118109 09:00
ND ug/kg 330 06118109 09:00
ND ug/kg 330 06118109 09:00
ND ug/kg 330 06118109 09 00
ND u9lkg 330 06118109 09:00
ND ug/kg 330 06118109 09:00
ND uglkg 330 06118109 09 00
54 % 30-150 06118109 09 00
71 % 46-120 06118109 09:00
75 % 38-108 06118109 09:00
64 % 35-120 06118109 09:00
60 % 24-120 06118109 09:00
90 % 44-136 06118109 09:00
Analytical Method: EPA8260
ND uglkg 7370 100
ND ug/kg 369 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed GAS No. Oual
06126109 1 0 06 534-52-1
06126109 10:06 51-28-5
06126109 10:06 121-14-2
06126109 10:06 606-20-2
06126109 10:06 117-84-0
06126109 10:06 122-66-7
06126109 10:06 117-81-7
06126109 10:06 206-44-0
06126109 10:06 86-73-7
06126/09 10:06 87-68-3
06126109 10:06 118-74-1
06126109 10:06 77-47-4
06126109 10:06 67-72-1
06126109 10:06 193-39-5
06126109 10:06 78-59-1
06126109 10:06 90-12-0
06126109 10:06 91-57-6
06126109 10:06 95-48-7
06126109 10:06
06126109 10:06 91-20-3
06126109 10:06 88-74-4
06126109 10:06 99-09-2
06126109 10:06 100-01-6
06/26109 10:06 98-95-3
06126109 10:06 88-75-5
06126109 10:06 100-02-7
06126109 1 0:06 62-75-9
06126109 10:06 621-64-7
06126109 10:06 86-30-6
06126109 10:06 87-86-5
06126109 10:06 85-01-8
06126109 10:06 108-95-2
06126109 10:06 129-00-0
06126/09 10:06 120-82-1
06126109 10:06 95-95-4
06126109 10:06 88-06-2
06126109 10:06 4165-60-0
06126109 10:06 321-60-8
06126109 1 0:06 1718-51-0
06126109 1 0:06 13127-88-3
06126109 10:06 367-12-4
06126109 10:06 118-79-6
06122109 21:42 67-64-1
06122109 21 :42 71-43-2
Page 24 of 65
www.paCDlabs.com
Project: AKZO NOBEL
Pace Project No.: 9246497
Sample: STK 3.5
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497005 Collected: 06/12/09 00:00 Received: 06/12/0916:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed GAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromobenzene ND ug/kg 369 100 06/22/09 21:42 108-86-1
Bromochloromethane ND ug/kg 369 100 06/22/09 21:42 74-97-5
Bromodichloromethane ND ug/kg 369 100 06/22/09 21:42 75-27-4
Bromoform ND ug/kg 369 100 06/22/09 21 :42 75-25-2
Bromomethane ND ug/kg 737 100 06/22/09 21 :42 74-83-9
2-Butanone {MEK) ND ug/kg 7370 100 06/22/09 21 :42 78-93-3
n-Butylbenzene ND ug/kg 369 100 06/22/09 21 :42 104-51-8
sec-Butyl benzene ND ug/kg 369 100 06/22/09 21:42 135-98-8
tert-Butylbenzene ND ug/kg 369 100 06/22/09 21:42 98-06-6
Carbon tetrachloride ND ug/kg 369 100 06/22/09 21:42 56-23-5
Chlorobenzene ND ug/kg 369 100 06/22/09 21:42 108-90-7
Ch\oroethane ND ug/kg 737 100 06/22/09 21 :42 75-00-3
Chloroform ND ug/kg 369 100 06/22/09 21 :42 67-66-3
Chloromethane ND ug/kg 737 100 06/22/09 21:42 74-87-3
2-Chlorotoluene ND ug/kg 369 100 06/22/09 21:42 95-49-8
4-Chlorotoluene ND ug/kg 369 100 06/22/09 21:42 106-43-4
1,2-DibrorTio-3-chloropropane. ND ug/kg 369 100 06/22/09 21:42 96-12-8
Dibromochloromethane ND ug/kg 369 100 06/22/09 21 :42 124-48-1
1,2-Dibromoethane {EDB) ND ug/kg 369 100 06/22/09 21 :42 106-93-4
Dibromomethane ND ug/kg 369 100 06/22/09 21 :42 74-95-3
1,2-Dichlorobenzene ND ug/kg 369 100 06/22/09 21 :42 95-50-1
1,3-Dichlorobenzene ND ug/kg 369 100 06/22/09 21 :42 541-73-1
1,4-Dichlorobenzene ND ug/kg 369 100 06/22/09 21 :42 106-46-7
Dichlorodifluoromethane ND ug/kg 737 100 06/22/09 21 :42 75-71-8
1 , 1-Oichloroethane ND ug/kg 369 100 06/22/09 21:42 75-34-3
1,2-Dichloroethane 1260 ug/kg 369 100 06/22/09 21:42 107-06-2
1, 1-Dichloroethene ND ug/kg 369 100 06/22/09 21:42 75-35-4
cis-1,2-Dichloroethene ND ug/kg 369 100 06/22/09 21:42 156-59-2
trans-1,2-Dichloroethene ND ug/kg 369 100 06/22/09 21 :42 156-60-5
1,2-Dichloropropane ND ug/kg 369 100 06/22/09 21 :42 78-87-5
1,3-Dichloropropane ND ug/kg 369 100 06/22/09 21:42 142-28-9
2,2-Dichloropropane ND ug/kg 369 100 06/22/09 21:42 594-20-7
1, 1-Dichloropropene ND ug/kg 369 100 06/22/09 21:42 563-58-6
cis-1,3-Dichloropropene ND ug/kg 369 100 06/22/09 21:42 10061-01-5
trans-1.3-Dichloropropene ND ug/kg 369 100 06/22/09 21:42 10061-02-6
Oiisopropyl ether ND ug/kg 369 100 06/22/09 21:42 108-20-3
Ethylbenzene 424 ug/kg 369 100 06/22/09 21:42 100-41-4
Hexachloro-1,3-butadiene 1020 ug/kg 369 100 06/22/09 21 :42 87-68-3
2-Hexanone ND ug/kg 3690 100 06/22/09 21 :42 591-78-6
lsopropylbenzene {Cumene} ND ug/kg 369 100 06/22/09 21:42 98-82-8
p-lsopropyltoluene 770 ug/kg 369 100 06/22/09 21:42 99-87-6
Methylene Chloride ND ug/kg 1470 100 06/22/09 2142 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/kg 3690 100 06/22/09 2142 108-10-1
Methyl-tert-butyl ether ND ug/kg 369 100 06/22/09 2142 1634-04-4
Naphthalene 755 ug/kg 369 100 06/22/09 21 :42 91-20-3
n-Propylbenzene ND ug/kg 369 100 06/22/09 21 :42 103-65-1
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 25 of 65
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc ..
--·:"{'"ll~t--i,ne ct,
www.ptJcelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.5 Lab ID:
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
9246497005 Collected: 06/12/09 00:00 Received: 06/12/09 16:20
Pace Analytical Services. Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
826015035A Volatile Organics
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1, 1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2.4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
a-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA8260
ND ug/k9 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
148000 ug/kg 18400 5000
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 369 100
ND ug/kg 3690 100
ND ug/kg 737 100
1950 ug/kg 737 100
1630 ug/kg 737 100
ND ug/kg 369 100
107 % 79-116 100
100 % 88-110 100
101 % 74-115 100
112 % 69-121 100
Analytical Method: ASTM D2974-87
22.9 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except 1n full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CAS No. Qual
06/22/09 21 :42 100-42-5
06/22/09 21 :42 630-20-6
06/22/09 21:42 79-34-5
06/22/09 21 :42 127-18-4
06/23/09 10:52 108-88-3
06/22/09 21:42 87-61-6
06/22/09 21 :42 120-82-1
06/22/09 21 :42 71-55-6
06/22/09 21 :42 79-00-5
06/22/09 21:42 79-01-6
06/22/09 21 :42 75-69-4
06/22/09 21:42 96-18-4
06/22/09 21:42 95-63-6
06/22/09 21 :42 108-67-8
06/22/09 21 :42 108-05-4
06/22/09 21 :42 75-01-4
06/22/09 21:42 1330-20-7
06/22/09 21 :42 1330-20-7
06/22/09 21:42 95-47-6
06/22/09 21:42 1868-53-7
06/22/09 21:42 2037-26-5
06/22/09 21:42 460-00-4
06/22/09 21 :42 17060-07-0
06/18/09 15:23
Page 26 of 65
www pace/abs.com
Project AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.6
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497006 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Oual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic ND mg/kg 0.32 06/16/09 15:22 06/17/0917:19 7440-38-2
Barium 38.4 mg/kg 0.32 06/16/09 15:22 06/17/09 17:19 7440-39-3
Cadmium 7.8 mg/kg 0.063 06/16/09 15:22 06/17/09 17:19 7440-43-9
Chromium 26.1 mg/kg 0.32 06/16/09 15:22 06/17/09 17:19 7440-47-3
Lead 3.5 mg/kg 0.32 06/16/09 15:22 06/17/09 17:19 7439-92-1
Selenium 2.1 mg/kg 0.63 06/16/09 15:22 06/17/0917:19 7782-49-2
Silver ND mg/kg 0.32 06/16/09 15:22 06/17/09 17:19 7440-22-4
7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury 0.042 mg/kg 0.0050 06/16/09 19:30 06/17/09 14:19 7439-97-6
8270 MSSV Microwave Analytical Method: EPA8270 Preparation Method: EPA 3546
Acenaphthene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 83-32-9
Acenaphthylene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 208-9_6-8
Aniline ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 62-53-3
Anthracene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 120-12-7
Benzo(a)anthracene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 56-55-3
Benzo(a)pyrene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 50-32-8
Benzo(b)fiuoranthene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 205-99-2
Benzo(g ,h, i)pery!ene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 191-24-2
Benzo(k)fiuoranthene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 207-08-9
Benzoic Acid ND ug/kg 1650 06/18/09 09:00 06/26/09 10:31 65-85-0
Benzyl alcohol ND ugikg 660 06/18/09 09:00 06/26/09 10:31 100-51-6
4-Bromopheny!phenyl ether ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 101-55-3
Butyl benzyl p htha late ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 85-68-7
4-Chloro-3-methy!phenol ND ug/kg 660 06/18/09 09:00 06/26/09 10:31 59-50-7
4-Chloroaniline ND u9/k9 1650 06/18/09 09:00 06/26/09 10:31 106-47-8
bis{2-Chloroethoxy)methane ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 111-91-1
bis{2-Chloroethyl) ether. ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 111-44-4
bis{2-Chloroisopropyl} ether ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 108-60-1
2-Chloronaphthalene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 91-58-7
2-Chlorophenol ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 95-57-8
4-Chlorophenylphenyl ether ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 7005-72-3
Chrysene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 218-01-9
D ibenz (a, h) a nthra cene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 53-70-3
Dibenzofuran ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 132-64-9
1,2-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 95-50-1
1,3-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 541-73-1
1,4-Dichlorobenzene ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 106-46-7
3,3'-Dichlorobenzidine ND ug/kg 1650 06/18/09 09:00 06/26/09 10:31 91-94-1
2,4-Dichlorophenol ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 120-83-2
Diethylphthatate ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 84-66-2
2,4-Dimethylphenol ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 105-67-9
Dimethylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 131-11-3
Di-n-butylphthalate ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 84-74-2
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 27 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,. ><Co• ~-;\--~:::p~~ .. ~ 1:nelac;
www.pscelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.6
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID: 9246497006 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8270 MSSV Microwave
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2 ,4-Dinitrotoluene
2 ,6-Dinitrotoluene
Di-n-octylphthalate
1,2-Diphenylhydrazine
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexach1oroethane
lndeno( 1,2,3-cd)pyrene
lsophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethy1amine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2 ,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-FluorobiPhenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Ftuorophenol (S)
2,4,6-Tribromophenol (S)
8260/5035A Volatile Organics
Acetone
Benzene
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND u9/k9 660 06/18/09 09:00 06/26/09 10:31 534-52-1
ND u9/k9 1650 06/18/09 09:00 06/26/09 10:31 51-28-5
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 121-14-2
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 606-20-2
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 117-84-0
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 122-66-7
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 117-81-7
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 206-44-0
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 86-73-7
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 87-68-3
ND u9/k9 330 06/18/09 09:00 06/26/09 1 0: 31 118-74-1
ND ug/kg 330 06/18/09 09:00 06/26/0910:31 77-47-4
ND u9/k9 330 06/18/09 09:00 06/26/0910:31 67-72-1
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 193-39-5
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 78-59-1
·ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 90-12-0
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 91-57-6
ND u9/k9 330 06/18/09 09:00 06/26/09 1 O: 31 95-48-7
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31
ND ug/kg 330 06/18/09 09:00 06/26/0910:31 91-20-3
ND ug/kg 1650 06/18/09 09:00 06/26/09 10:31 88-74-4
ND ug/kg 1650 06/18/09'09:00 06/26/09 10:31 99-09-2
ND u9/k9 660 06/18/09 09:00 06/26/09 10: 31 100-01-6
ND ug/kg 330 06/18/09 09:00 06/26/0910:31 98-95-3
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 88-75-5
ND u9/k9 1650 06/18/09 09:00 06/26/09 10:31 100-02-7
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 62-75-9
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 621-64-7
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 86-30-6
ND u9/k9 1650 06/18/09 09:00 06/26/09 10:31 87-86-5
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 85-01-8
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 108-95-2
ND ug/kg 330 06/18/09 09:00 06/26/09 10:31 129-00-0
ND ug/kg 330 06/18/09 09:00 06/26/09 1 O: 31 120-82-1
ND u9/k9 330 06/18/09 09:00 06/26/09 10:31 95-95-4
ND u9/k9 330 06/18/09 09:00 06/26/0910:31 88-06-2
37 % 30-150 06/18/09 09:00 06/26/09 10:31 4165-60-0
54 % 46-120 06/18/09 09:00 06/26/0910:31 321-60-8
48 % 38-108 06/18/09 09:00 06/26/09 10:31 1718-51-0
62 % 35-120 06/18/09 09:00 06/26/09 10:31 13127-88-3
60 % 24-120 06/18/09 09:00 06/26/09 10:31 367-12-4
65 % 44-136 06/18/09 09:00 06/26/09 10:31 118-79-6
Analytical Method: EPA 8260
368 ug/kg 89.3 06/22/09 21:24 67-64-1 E
ND ug/kg 4.5 06/22/09 21:24 71-43-2
REPORT OF LABORATORY ANALYSIS Page 28 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
www.pacelabs.com
Project: AKZO NOBEL
Pace Project No.: 9246497
Sample: STK 3.6
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
LablD: 9246497006 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units Report Limit OF Prepared Analyzed GAS No. Qual
826015035A Volatile Organics Analytical Method: EPA8260
Bromobenzene ND ug/kg 4.5 06/22/09 21 :24 108-86-1
Bromochloromethane ND u9/k9 4.5 06/22/09 21 :24 74-97-5
Bromodichloromethane ND ug/kg 4.5 06/22/09 21 :24 75-27-4
Bromoform ND ug/kg 4.5 06/22/09 21:24 75-25-2
Bromomethane ND ug/kg 8.9 06/22/09 21:24 74-83-9
2-Butanone (MEK) ND ug/kg 89.3 06/22/09 21:24 78-93-3
n-Butylbe~zene ND ug/kg 4.5 06/22/09 21:24 104-51-8
sec-Butyl benzene ND ug/kg 4.5 06/22/09 21 :24 135-98-8
tert-Butylbenzene ND ug/kg 4.5 06/22/09 21 :24 98-06-6
Carbon tetrachloride ND ug/kg 4.5 06/22/09 21 :24 56-23-5
Chlorobenzene ND ug/kg 4.5 06/22/09 21 :24 108-90-7
Chloroethane ND ug/kg 8.9 06/22/09 21:24 75-00-3
Chloroform ND ug/kg 4.5 06/22/09 21:24 67-66-3
Chloromethane ND ug/kg 8.9 06/22/09 21:24 74-87-3
2-Chlorotoluene ND ug/kg 4.5 06/22/09 21:24 95-49-8
4-Chlorotoluene ND ug/kg 4.5 06/22/09 21:24 106-43-4
1,2-Dibromo-3-chloropropane ND ug/kg 4.5 06/22/09 21 :24 96-12-8
Dibromochloromethane ND ug/kg 4.5 06/22/09 21 :24 124-48-1
1,2-Dibromoethane (EDB) ND ug/kg 4.5 06/22/09 21 :24 106-93-4
Dibromomethane ND ug/kg 4.5 06/22/09 21:24 74-95-3
1,2-Dichlorobenzene ND ug/kg 4.5 06/22/09 21:24 95-50-1
1,3-Dichlorobenzene ND ug/kg 4.5 06/22/09 21:24 541-73-1
1,4-Dichlorobenzene ND ug/kg 4.5 06/22/09 21 :24 106-46-7
Dichlorodifluoromethane ND ug/kg 8.9 06/22/09 21:24 75-71-8
1,1-Dichloroethane ND ug/kg 4.5 06/22/09 21 :24 75-34-3
1,2-Dichloroethane 502 ug/kg 4.5 06/22/09 21 :24 107-06-2 E
1, 1-Dichloroethene ND ug/kg 4.5 06/22/09 21 :24 75-35-4
cis-1,2-Dichloroethene ND ug/kg 4.5 06/22/09 21:24 156-59-2
trans-1,2-Dichloroethene ND ug/kg 4.5 06/22/09 21 :24 156-60-5
1,2-Dichloropropane ND ug/kg 4.5 06/22/09 21 :24 78-87-5
1,3-Dichloropropane ND ug/kg 4.5 06/22/09 21:24 142-28-9
2 ,2-Dichloropropane ND ug/kg 4.5 06/22/09 21 :24 594-20-7
1 , 1-Dich1oropropene ND ug/kg 4.5 06/22/09 21:24 563-58-6
cis-1,3-Dichloropropene ND ug/kg 4.5 06/22/09 21:24 10061-01-5
trans-1,3-Dichloropropene ND ug/kg 4.5 06/22/09 21:24 10061-02-6
Oiisopropyl ether ND ug/kg 4.5 06/22/09 21:24 108-20-3
Ethylbenzene ND ug/kg 4.5 06/22/09 21:24 100-41-4
Hexachloro-1,3-butadiene ND ug/kg 4.5 06/22/09 21 :24 87-68-3
2-Hexanone ND ug/kg 44.6 06/22/09 21 :24 591-78-6
lsopropylbenzene (Cumene) NO ug/kg 4.5 06/22/09 21 :24 98-82-8
p-lsopropyltoluene ND ug/kg 4.5 06/22/09 21 :24 99-87-6
Methylene Chloride ND ug/kg 17.9 06/22/09 21 :24 75-09-2
4-Methyl-2-pentanone (MIBK) ND ug/kg 44.6 06/22/09 21 :24 108-10-1
Methy!-tert-butyl ether, ND ug/kg 4.5 06/22/09 21 :24 1634-04-4
Naphthalene ND ug/kg 4.5 06/22/09 21 :24 91-20-3
n-Propylbenzene ND ug/kg 4.5 06/22/09 21 :24 103-65-1
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 29 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
'~o ;.~-' ':..c¾'-~" '. • lnelac\
www.p11co/abs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: STK 3.6
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497006 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results repo'!ed on a "wet-weight" basis
Parameters
8260/SOJSA Volatile Organics
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1, 1, 1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
T richlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
a-Xylene
Dibromofluoromethane (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA8260
ND ug/kg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
18.7 uglkg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
ND uglkg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
ND ug/kg 4.5
ND ug/kg 44.6
ND uglkg 8.9
ND ug/kg 8.9
ND ug/kg 8.9
ND uglkg 4.5
112 % 79-116
96 % 88-110
97 % 74-115
111 % 69-121
Analytical Method: ASTM D2974-87
28.5 % 0.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed CAS No. Qual
06122109 21:24 100-42-5
06122109 21 24 630-20-6
06122109 21:24 79-34-5
06122109 21:24 127-18-4
06122109 21 24 108-88-3
06122109 21 :24 87-61-6
06122109 21 :24 120-82-1
06122109 21 :24 71-55-6
06122109 21:24 79-00-5
06122109 21 :24 79-01-6
06122109 21:24 75-69-4
06/22/09 21 :24 96-18-4
06122109 21 24 95-63-6
06122109 21 :24 108-67-8
06/22/09 21 :24 108-05-4
06122/09 21 :24 75-01-4
06122109 21 :24 1330-20-7
06122/09 21 :24 1330-20-7
06122109 21 :24 95-47-6
06122109 21:24 1868-53-7
06122109 21:24 2037-26-5
06122109 21:24 460-00-4
06122109 21:24 17060-07-0
06118109 15:23
Page 30 of 65
wwwpacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: CONC 3.1
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497007 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2 ,4,5-Trichlorophenol
2,4,6-T richlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1 , 1-Dichloroethene
Tetrachloroethene
Trichloroethene
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA 6010 Preparation Method: EPA3010
Leachate Method/Date: EPA 1311; 07/09/09 09:07
0.033 mg/L 0.025 07/09/09 10:00
0.15 m9/L 0.Q25 07/09/09 10:00
ND m9/L 0.0050 07/09/09 10:00
ND m9/L 0.025 07/09/09 10:00
ND m9/L 0.025 07/09/09 10:00
ND mg/L 0.050 07/09/09 10:00
ND m9/L 0.025 07/09/09 10:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311: 07/09/09 09:07
Analyzed CAS No. Oual
07/09/09 14:30 7440-38-2
07/09/09 14:30 7440-39-3 R1
07/09/09 14:30 7440-43-9
07/09/09 14:30 7440-47-3
07/09/09 14:30 7439-92-1
07/09/09 14:30 7782-49-2
07/09/09 14:30 7440-22-4
ND u9/L 0.20 07/09/09 09:56 07/09/0911:58 7439-97-6
Analytical Method: EPA8270 Preparation Method: EPA3510
Leachate Method/Date: EPA 1311; 06/16/09 00:00
ND ug/L 50.0 06/23/09 12:30
ND ug/L 50.0 06/23/09 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123/09 12:30
ND ug/L 50.0 06123109 12 30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06/23109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
34 % 30-150 06123109 12:30
35 % 30-150 06123109 12:30
39 % 30-150 06123109 12:30
26 % 25-150 06123109 12:30
27 % 25-150 06123109 12:30
40 % 25-150 06123109 12:30
Analytical Method: EPA8260
ND ug/L 125 25
ND ug/L 250 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc ..
06/29/09 18:37 106-46-7
06/29109 18:37 121-14-2
06129109 18:37 87-68-3
06129/09 18:37 118-74-1
06129109 18:37 67-72-1
06129109 18:37 95-48-7
06129/09 18:37
06129109 18:37 98-95-3
06129109 18 37 87-86-5
06129/09 18:37 110-86-1
06129109 18:37 95-95-4
06129109 18:37 88-06-2
06129109 18:37 4165-60-0
06129/09 18:37 321-60-8
06129109 18:37 1718-51-0
06129/09 18:37 13127-88-3
06129109 18:37 367-12-4
06129109 18:37 118-79-6
06121109 10:30 71-43-2
06121109 10:30 78-93-3
06121109 10 30 56-23-5
06121109 10:30 108-90-7
06121109 10:30 67-66-3
06121109 10:30 106-46-7
06121109 10:30 107-06-2
06121109 10:30 75-35-4
06121/09 10:30 127-18-4
06121109 10:30 79-01-6
Page 31 of 65
www.pscelabs.com
Project AKZONOBEL
Pace Project No.: 9246497
Sample: CONC 3.1
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Ashevi!le, NC 28804
[phone]
Pace Analytical Services, lnc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
LablD: 9246497007 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8260 MSV TCLP
Vinyl chloride
1,2-Dichloroethane-d4 (S)
Toluene-dB (S)
4-Bromonuorobenzene (S}
Dibromonuoromethane (S)
Date: 07/22/2009 04:35 PM
Results Units Report Limit DF Prepared
Analytical Method: EPA 8260
ND ug/L 125 25
102 % 79-120 25
99 % 70-120 25
100 % 87-109 25
104 % 85-115 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Analyzed GAS No. Qual
06/21/09 10:30 75-01-4
06/21/09 10:30 17060-07-0
06/21/09 10:30 2037-26-5
06/21/09 10:30 460-00-4
06/21/0910:30 1868-53-7
Page 32 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: CONC 3.2
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablD: 9246497008 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet•weight" basis
Parameters
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4-Dichlorobenzene
2.4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol(o-Cresol)
3&4-Melhylphenof(m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trich!orophenol
2,4,6-T rich!orophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-dB (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV TCLP
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1, 1-Dichloroethene
Tetrachloroethene
Trichloroethene
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA 6010 Preparation Method: EPA3010
Leachate Method/Date: EPA 1311; 07109109 09:07
0.025 mg/L 0.025 07109109 10:00
0.22 mg/L 0.025 07109/09 10:00
ND mg/L 0.0050 07/09109 10:00
ND mg/L 0.025 07109109 10:00
ND mg/L 0.025 07109109 10:00
ND mg/L 0.050 07109109 10:00
ND mg/L 0.025 07109109 10:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 07/09/09 09:07
Analyzed GAS No. Qual
07109109 14:38 7440-38-2
07/09109 14:38 7440-39-3
07109/09 14:38 7440-43-9
07109109 14:38 7440-47-3
07109109 14:38 7439-92-1
07109109 14:38 7782-49-2
07/09/09 14:38 7440-22-4
ND ug/L 0.20 07109109 09:56 07109109 12:03 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 06/16/09 00:00
ND ug/L 50.0 06123/09 12:30
ND ug/L 50.0 06/23109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123/09 12:30
ND ug/L 50.0 06/23109 12:30
ND ug/L 50.0 06/23109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123109 12:30
ND ug/L 50.0 06123/09 12:30
47 % 30-150 06123109 12:30
53 % 30-150 06123109 12:30
56 % 30-150 06123109 12:30
28 % 25-150 06123109 12:30
26 % 25-150 06123109 12:30
61 % 25-150 06123109 12:30
Analytical Method: EPA8260
ND ug/L 125 25
ND ug/L 250 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
ND ug/L 125 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
06129/09 19:03 106-46-7
06129109 19:03 121-14-2
06129109 19:03 87-68-3
06129/09 19:03 118-74-1
06129109 19:03 67-72-1
06129109 19:03 95-48-7
06129/09 19:03
06/29109 19:03 98-95-3
06129109 19:03 87-86-5
06129109 19:03 110-86-1
06129/09 19:03 95-95-4
06129109 19:03 88-06-2
06129109 19:03 4165-60-0
06129109 19:03 321-60-8
06129109 19:03 1718-51-0
06129109 19:03 13127-88-3
06129109 19:03 367-12-4
06129109 19:03 118-79-6
06121109 10:11 71-43-2
06121109 10:11 78-93-3
06121109 10:11 56-23-5
06121109 10:11 108-90-7
06121109 10:11 67-66-3
06/21/09 10:11 106-46-7
0612110910:11 107-06-2
06121109 10:11 75-35-4
06121109 10:11 127-18-4
06121109 10:11 79-01-6
Page 33 of 65
www.pscelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Sample: CONC 3.2
Pace Analytical Services, Inc.
2225 Riverside Dr.
ANALYTICAL RESULTS
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LablO: 9246497008 Collected: 06/12/09 00:00 Received: 06/12/09 16:20 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters
8260 MSV TCLP
Vinyl chloride
1,2-Dichloroethane-d4 (S)
Toluene-dB (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Date: 07/22/2009 04:35 PM
Results Units Report Limit OF Prepared
Analytical Method: EPA8260
ND ug/L 125 25
105 % 79-120 25
100 % 70-120 25
99 % 87-109 25
109 % 85-115 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Seivices, Inc ..
Analyzed CAS No. Qual
06121109 10:11 75-01-4
06121109 10:11 17060-07-0
06121109 10:11 2037-26-5
06121109 10:11 460-00-4
06121109 10:11 1868-53-7
Page 34 of 65
wwwpscelabscom
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: MERP/2211 Analysis Method:
QC Batch Method: EPA 7471 Analysis Description:
Associated Lab Samples: 9246497001, 9246497002, 9246497003
METHOD BLANK: 294567 Matrix: Solid
Associated Lab Samples: 9246497001, 9246497002, 9246497003
Blank Reporting
EPA 7471
7471 Mercury
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 294568
Parameter Units
Mercury mg/kg
MATRIX SPIKE SAMPLE: 294569
Parameter Units
Mercury mg/kg
SAMPLE DUPLICATE: 294570
Parameter Units
Mercury mg/kg
Date: 07/22/2009 04:35 PM
ND 0.0050 06/15/09 17:46
Spike
Cone.
.067
9246497001
Result
LCS
Result
0.067
Spike
Cone.
0.051 .085
9246497002 Dup
LCS
% Rec
100
MS
Result
0.14
% Rec
Limits
80-120
MS
% Rec
91
Result Result RPO Qualifiers
0.016 0.042
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent or Pace Analytical Services, Inc ..
67 R1
Qualifiers
% Rec
Limits
75-125
Qualifiers
Page 35 of 65
www.paooJabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: MSV/7705
QC Batch Method: EPA 8260
Associated Lab Samples: 9246497003
METHOD BLANK: 310804
Associated Lab Samples: 9246497003
Parameter Units
1, 1-Dichloroethene ug/L
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
2-Butanone (MEK) ug/L
Benzene ug/L
Carbon tetrachloride ug/L
Chlorobenzene ug/L
Chloroform ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
Vinyl chloride ug/L
1,2-Dichloroethane-d4 (S) %
4-Bromofluorobenzene (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
LABORATORY CONTROL SAMPLE: 310805
Parameter Units
1, 1-Dichloroethene u9/L
1,2-Dichloroethane ug/L
1 ,4-Dichlorobenzene ug/L
2-Butanone (MEK) ug/L
Benzene ug/L
Carbon tetrachloride ug/L
Chlorobenzene ug/L
Chloroform ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
Vinyl chloride ug/L
1,2-Dichloroethane-d4 (S) %
4-Bromofluorobenzene (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
Date: 07/22/2009 04:35 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8260
Analysis Description: 8260 MSV TCLP
Matrix: Water
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Result Limit Analyzed Qualifiers
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 10.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
ND 5.0 07/22/09 00:55
84 79-120 07/22/09 00:55
101 87-109 07/22/09 00:55
94 85-115 07/22/09 00:55
96 70-120 07/22/09 00:55
Spike LCS LCS %Rec
Cone. Result %Rec
.50 70.7 141
50 66.5 133
50 73.5 147
100 81.7 82
50 72.5 145
50 82.1 164
50 75.8 152
50 73.0 146
50 85.2 170
50 76.9 154
50 61.1 122
82
84
96
99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Limits
50-150
50-150
50-150
50-150
50-150
50-150 L3
50-150 L3
50-150
50-150 L3
50-150 L3
50-150
79-120
87-109 so
85-115
70-120
Qualifiers
Page 36 of 65
Project AKZONOBEL
Pace Project No.: 9246497
QC Batch: MSV/7405
QC Batch Method: EPA 8260
Associated Lab Samples: 9246497007, 9246497008
METHOD BLANK: 297895
Associated Lab Samples: 9246497007, 9246497008
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8260
Analysis Description: 8260 MSV TCLP
Matrix: Water
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
1, 1-Dichloroethene ug/L
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
2-Butanone (MEK) ug/L
Benzene ug/L
Carbon tetrachloride ug/L
Chlorobenzene ug/L
Chloroform ug/L
Tetrach1oroethene ug/L
Trichloroethene ug/L
Vinyl chloride ug/L
1,2-Dichloroethane-d4 (S) %
4-Bromofluorobenzene (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
LABORATORY CONTROL SAMPLE: 297896
Parameter Units
1, 1-Dichloroethene ug/L
1,2-Dichloroethane ug/L
1,4-Dichlorobenzene ug/L
2-Butanone (MEK) ug/L
Benzene ug/L
Carbon tetrachloride ug/L
Chlorobenzene ug/L
Chloroform ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
Vinyl chloride ug/L
1,2-Dich!oroethane-d4 (S) %
4-Bromofluorobenzene {S) %
Oibromofluoromethane (S) %
Toluene-dB (S) %
Date: 07/22/2009 04:35 PM
ND 5.0 06/21/09 01 :23
ND 5.0 06/21/09 01 :23
ND 5.0 06/21/09 01:23
ND 10.0 06/21/09 01:23
ND 5.0 06/21/09 01:23
ND 5.0 06/21/09 01:23
ND 5.0 06/21/09 01 :23
ND 5.0 06/21/09 01 :23
ND 5.0 06/21/09 01:23
ND 5.0 06/21/09 01:23
ND 5.0 06/21/09 01:23
105 79-120 06/21/09 01:23
99 87-109 06/21/09 01 :23
107 85-115 06/21/09 01 :23
100 70-120 06/21/09 01 :23
Spike LCS LCS % Rec
Cone. Result % Rec
50 59.9 120
50 56.8 114
50 52.1 104
100 103 103
50 55.9 112
50 67.6 135
50 52.0 104
50 60.7 121
50 54.4 109
50 54.8 110
50 56.7 113
103
99
107
99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Limits
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
79-120
87-109
85-115
70-120
Qualifiers
Page 37 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: OEXT/7137
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804,
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8270
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 9246497003, 9246497004, 9246497005, 9246497006
METHOD BLANK: 296323 Matrix: Solid
Associated Lab Samples: 9246497003,9246497004,9246497005,9246497006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene ug/kg ND 330 06125109 18:35
1,2-Dichlorobenzene ug/kg ND 330 06/25109 18:35
1,2-Diphenylhydrazine ug/kg ND 330 06125109 18:35
1,3-Dichlorobenzene ug/kg ND 330 06125/09 18:35
1,4-Dichlorobenzene uglkg ND 330 06125109 18:35
1-Methylnaphthalene uglkg ND 330 06125109 18:35
2,4,5-Trichlorophenol ug/kg ND 330 06/25109 18:35
2,4 ,6-Trichlorophenol uglkg ND 330 06/25109 18:35
2,4-Dichlorophenol ug/kg ND 330 06125/09 18:35
2 ,4-Oimethylphenol ug/kg ND 330 06125109 18:35
2,4-Dinitrophenol ug/kg ND 1650 06/25/09 18:35
2,4-Dinitrotoluene ug/kg ND 330 06/25/09 18:35
2,6-Dinitrotoluene ug/kg ND 330 06/25/09 18:35
2-Chloronaphthalene ug/kg ND 330 06/25/09 18:35
2-Chlorophenol ug/kg ND 330 06/25/09 18:35
2-Methylnaphthalene ug/kg ND 330 06/25/09 18:35
2-Methylphenol(o-Cresol) ug/kg ND 330 06/25/09 18 35
2-Nitroaniline ug/kg ND 1650 06/25/09 18:35
2-Nitrophen0I ug/kg ND 330 06/25/09 18:35
3&4-Methylphenol(m&p Cresol) ug/kg ND 330 06/25/09 18:35
3,3'-Dichlorobenzidine ug/kg ND 1650 06/25/09 18:35
3-Nitroaniline ug/kg ND 1650 06/25/09 18:35
4 ,6-D i ni tro-2-methyl phenol ug/kg ND 660 06/25/09 18:35
4-Bromophenylphenyl ether ug/kg ND 330 06/25/09 18:35
4-Chloro-3-methylphenot ug/kg ND 660 06/25/09 18:35
4-Chloroaniline ug/kg ND 1650 06/25/09 18:35
4-Chlorophenylphenyl ether ug/kg ND 330 06/25/09 18:35
4-Nitroaniline ug/kg ND 660 06/25/09 18:35
4-Nitrophenol ug/kg ND 1650 06/25/09 18:35
Acenaphthene ug/kg ND 330 06/25/09 18:35
Acenaphthylene ug/kg ND 330 06/25/09 18:35
Aniline ug/kg ND 330 06/25/09 18:35
Anthracene ug/kg ND 330 06/25/09 18:35
Benzo(a)anthracene ug/kg ND 330 06/25/09 18:35
Benzo{a)pyrene ug/kg ND 330 06125/09 18:35
Benzo(b)fluoranthene ug/kg ND 330 06/25/09 18:35
Benzo(g ,h ,i)perylene ug/kg ND 330 06125/09 18:35
Benzo(k)fluoranthene ug/kg ND 330 06/25/09 18:35
Benzoic Acid ug/kg ND 1650 06/25/09 18 35
Benzyl alcohol ug/kg ND 660 06/25/09 18:35
bis(2-Chloroethoxy)methane ug/kg ND 330 06/25/09 18:35
bis{2-Chloroethyl) ether ug/kg ND 330 06/25/09 18:35
bis(2-Chloroisopropyl) ether ug/kg ND 330 06/25/09 18:35
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
-~"-'-~~ii~"•• J/'1 la',-, ?1ne c1,
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 65
www.paoolabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Pace Analytical Services, Inc.
2225 Riverside Dr.
QUALITY CONTROL DATA
Asheville, NC 28804
[phone]
METHOD BLANK: 296323
Associated Lab Samples:
Matrix: Solid
9246497003,9246497004,9246497005,9246497006
Stank Reporting
Paco Analytical Services, Inc.
9800 Kincey Ave. Suite 1 oo
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
bis(2-Ethylhexyl)phthalate
Buty!benzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz (a, h )a nth racene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentad\ene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2.4.6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-F!uorophenol (S)
Nitrobenzene-d5 (S)
Phenol-dB (S)
Terphenyl-d14 (S)
LABORATORY CONTROL SAMPLE:
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4 .5-Trichlorophenol
2 .4.6-Trichlorophenol
2.4-Dichiorophenol
Date: 07/22/2009 04:35 PM
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ugikg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
u9/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
296324
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 1650 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
ND 330 06/25/09 18:35
92 44-136 06/25/09 18:35
75 46-120 06/25/09 18:35
67 24-120 06/25/09 18:35
74 30-150 06/25/09 18:35
73 35-120 06/25/09 18:35
77 38-108 06/25/09 18:35
Spike LCS LCS % Rec
Cone. Result % Rec
1670 1210 73
1670 1040 62
1670 1350 81
1670 1000 60
1670 1080 65
1670 1080 65
1670 1480 89
1670 1500 90
1670 1280 77
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc .. .., .. -/\~:-;Ir~~<;-
i1□eld.C\,
Limits
50-150
50-150
43-130
50-150
50-150
50-150
50-150
50-150
50-150
Qualifiers
Page 39 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
LABORATORY CONTROL SAMPLE: 296324
Parameter Units
2,4-Dimethylphenol ug/kg
2,4-Dinitrophenol ug/kg
2,4-Dinitrotoluene ug/kg
2,6-Dinitrotoluene ug/kg
2-Chloronaphthalene ug/kg
2-Chlorophenol ug/kg
2-Methylnaphthalene ug/kg
2-Methylphenol(o-Creso!) ug/kg
2-Nitroaniline ug/kg
2-Nitrophenol ug/kg
3&4-Methylphenol(m&p Cresol) ug/kg
3,3'-Dichlorobenzidine ug/kg
3-Nitroaniline ug/kg
4,6-Dinitro-2-methylphenol ug/kg
4-Bromophenylphenyl ether ug/kg
4-Chloro-3-methylphenol ug/kg
4-Chloroaniline ug/kg
4-Chlorophenylphenyl ether ug/kg
4-Nitroaniline ug/kg
4-Nitrophenol ug/kg
Acenaphthene ug/kg
Acenaphthylene ug/kg
Aniline ug/kg
Anthracene ug/kg
Benzo(a)anthracene ug/kg
Benzo(a)pyrene ug/kg
Benzo(b)fluoranthene ug/kg
Benzo(g ,h, i)perylene ug/kg
Benzo(k)fluoranthene ug/kg
Benzoic Acid ug/kg
Benzyl alcohol ug/kg
bis(2-Chloroethoxy)methane ug/kg
bis(2-Chloroethyl) ether ug/kg
bis(2-Chloroisopropyl) ether ug/kg
bis(2-Ethy\hexyl)phthalate ug/kg
Butylbenzylphthalate ug/kg
Chrysene ug/kg
Di-n-butylphthalate ug/kg
Di-n-octylphthalate ug/kg
Di benz( a, h )anth racene ug/kg
Oibenzofuran ug/kg
Diethylphthalate ug/kg
Dimethylphthalate ug/kg
Ftuoranthene ug/kg
Fluorene ug/kg
Hexachloro-1,3-butadiene ug/kg
Hexachlorobenzene ug/kg
Hexachlorocyclopentadiene ug/kg
Date: 07/22/2009 04:35 PM
Paco Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Cone. Result % Rec Limits
1670 1130 68 50-150
1670 1150J 69 20-111
1670 1280 77 50-150
1670 1220 73 50-150
1670 1200 72 50-150
1670 1040 63 50-150
1670 1550 93 50-150
1670 1090 65 50-150
1670 1360J 81 50-150
1670 1180 71 50-150
1670 1120 67 50-150
1670 1170J 70 50-150
1670 1530J 92 50-150
1670 1290 78 15-136
1670 1440 86 50-150
1670 1190 72 50-150
1670 1740 104 50-150
1670 1490 90 50-150
1670 1400 84 50-150
1670 1940 116 33-105 LO
1670 1400 84 50-150
1670 1380 83 50-150
1670 934 56 50-150
1670 1390 84 50-150
1670 1320 79 50-150
1670 1330 80 50-150
1670 1290 78 50-150
1670 1570 94 24-117
1670 1100 66 50-150
1670 975J 59 15-104
1670 1070 64 50-150
1670 1280 77 50-150
1670 1110 67 50-150
1670 1080 65 50-150
1670 1220 73 50-150
1670 1180 71 50-150
1670 1360 82 50-150
1670 1320 79 50-150
1670 1170 70 50-150
1670 1440 87 17-128
1670 1380 83 50-150
1670 1210 73 50-150
1670 1280 77 50-150
1670 1500 90 50-150
1670 1440 87 50-150
1670 1380 83 50-150
1670 1540 92 50-150
1670 1290 77 15-114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
. :;,'/~ (·'9_~P~• ~"~ ;111Jelac,
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 40 of 65
www.paceJabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
LABORATORY CONTROL SAMPLE: 296324
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville. NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS %Rec
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Cone. Result % Rec Limits Qualifiers
Hexachloroethane ug/kg 1670 989 59 50-150
lndeno(1,2,3-cd)pyrene ug/kg 1670 1470 88 19-128
lsophorone ug/kg 1670 1280 77 50-150
N-Nitroso-di-n-propylamine ug/kg 1670 1230 74 50-150
N-Nitrosodimethylamine ug/kg 1670 1120 67 50-150
N-Nitrosodiphenylamine ug/kg 1670 1500 90 50-150
Naphthalene u9/k9 1670 1250 75 50-150
Nitrobenzene u9/k9 1670 1150 69 50-150
Pentachlorophenol ug/kg 1670 1520J 91 15-130
Phenanthrene u9/kg 1670 1470 88 50-150
Phenol ug/kg 1670 1080 65 42-120
Pyrene ug/kg 1670 1260 75 50-150
2,4,6-Tribromophenol (S) % 83 44-136
2-Fluorobiphenyl (S) % 74 46-120
2-Fluorophenol (S) % 58 24-120
Nitrobenzene-dS (S) % 65 30-150
Phenol-d6 (S) % 65 35-120
Terphenyl-d14 (S) % 73 38-108
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 296325 296326
Parameter Units
1,2,4-Trichlorobenzene ug/kg
1,4-Dichlorobenzene ug/kg
2,4-Dinitrotoluene ug/kg
2-Chlorophenol ug/kg
4-Chloro-3-methylphenol ug/kg
4-Nitrophenol ug/kg
Acenaphthene ug/kg
N-Nitroso-di-n-propylamine ug/kg
Pentachlorophenol ug/kg
Phenol ug/kg
Pyrene ug/kg
2,4,6-Tribromophenol (S) %
2-Fluorobiphenyl (S) %
2-Fluorophenol (S) %
Nitrobenzene-dS (S) %
Phenol-d6 (S) %
Terphenyl-d14 (S) %
Date: 07/22/2009 04:35 PM
MS MSD
9246388012 Spike Spike MS MSD MS
Result Cone. Cone. Result Result % Rec
ND 1920 1920 1260 1250
ND 1920 1920 1130 1260
ND 1920 1920 1310 1480
ND 1920 1920 1100 960
ND 1920 1920 1240 1330
ND 1920 1920 2200 2270
ND 1920 1920 1390 1280
ND 1920 1920 1310 1420
ND 1920 1920 1480J 1300J
ND 1920 1920 1150 1010
ND 1920 1920 1310 1450
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
66
59
68
57
65
115
72
68
77
60
68
69
62
53
62
56
65
MSD
% Rec
65
66
77
50
69
118
67
74
68
53
76
46
53
33
61
29
51
%Rec
Limits RPO Qual
50-150 .3
50-150 11
50-150 13
50-150 13
50-150 7
50-150 3
50-150 8
50-150 8
50-150
50-150 13
50-150 11
44-136
46-120
24-120
30-150
35-120 1g
38-108
Page 41 of 65
www.pacelabs.com
Project AKZONOBEL
Pace Project No.: 9246497
QC Batch: MSV/7419
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 9246497001, 9246497002, 9246497003, 9246497004, 9246497005, 9246497006
METHOD BLANK: 298024 Matrix: Solid
Associated Lab Samples: 9246497001, 9246497002,9246497003,9246497004,9246497005,9246497006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1, 1, 1,2-Tetrachloroethane uglkg ND 5.0 06/22/09 11 :41
1, 1, 1-Trichloroethane uglkg ND 5.0 06122/09 11 :41
1, 1,2,2-Tetrachloroethane uglkg ND 5.0 06122109 11 :41
1, 1,2-Trichloroethane uglkg ND 5.0 06122109 11 :41
1 , 1-Dichtoroethane uglkg ND 5.0 06122/09 11 :41
1 , 1-Dichloroethene uglkg· ND 5.0 06/22/09 11 :41
1, 1-Dichloropropene ug/kg ND 5.0 06122109 11 :41
1,2,3-Trich1orobenzene uglkg ND 5.0 06122109 11:41
1,2,3-Trichloropropane uglkg ND 5.0 06122109 11 :41
1,2,4-Trichlorobenzene ug/kg ND 5.0 06122109 11 :41
1,2,4-Trimethylbenzene ug/kg ND 5.0 06122109 11 :41
1,2-Dibromo-3-chloropropane uglkg ND 5.0 06122109 11 :41
1,2-Dibromoethane (EDB) ug/kg ND 5.0 06122109 11 :41
1,2-Dichlorobenzene ug/kg ND 5.0 06122109 11 :41
1,2-Dichloroethane ug/kg ND 5.0 06122109 11 :41
1,2-Dichloropropane uglkg ND 5.0 06122109 11 :41
1,3,5-Trimethylbenzene uglkg ND 5.0 06122109 11 :41
1,3-Dichlorobenzene ug/kg ND 5.0 06/22/0911:41
1,3-Dichloropropane ug/kg ND 5.0 0612210911:41
1,4-Dichlorobenzene ug/kg ND 5.0 06/22/09 11 :41
2,2-Dichloropropane ug/kg ND 5.0 06122/09 11 :41
2-Butanone (MEK) uglkg ND 100 06122109 11 :41
2-Chlorotoluene ug/kg ND 5.0 06/22/09 11 :41
2-Hexanone uglkg ND 50.0 06122109 11 :41
4-Chlorotoluene ug/kg ND 5.0 06122109 11 :41
4-Methyl-2-pentanone (MIBK) uglkg ND 50.0 06/2210911:41
Acetone ug/kg ND 100 06122109 11 :41
Benzene uglkg ND 5.0 06122109 11:41
Bromobenzene uglkg ND 5.0 06/22/09 11:41
Bromochloromethane ug/kg ND 5.0 06122109 11 :41
Bromodichloromethane ug/kg ND 5.0 06/22/09 11:41
Bromoform ug/kg ND 5.0 06122109 11 :41
Bromomethane ug/kg ND 10.0 06122109 11 :4 1
Carbon tetrachloride ug/kg ND 5.0 06/22/0911:41
Chlorobenzene ug/kg ND 5.0 06/22/09 11 :4 1
Chloroethane ug/kg ND 10.0 06/2210911:41
Chloroform ug/kg ND 5.0 06122109 11 :41
Chloromethane ug/kg ND 10.0 06/22/09 11 :41
cis-1,2-Dichloroethene ug/kg ND 5.0 06/2210911:41
cis-1,3-Dichloropropene uglkg ND 5.0 06122109 11 :41
Dibromochloromethane ug/kg ND 5.0 06122109 11:41
Dibromomethane ug/kg ND 5.0 0612210911:41
Dichlorodifluoromethane ug/kg ND 10.0 06122/09 11 :4 1
Date: 0712212009 04:35 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc
,,<;,".;'-~:~f?-o_,,,~
?1helac;\
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 65
www.pBcelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
METHOD BLANK: 298024
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Matrix: Solid
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Associated Lab Samples: 9246497001,9246497002,9246497003,9246497004,9246497005,9246497006
Parameter
Diisopropyl ether
Ethyl benzene
Hexachloro-1,3-butadiene
lsopropylbenzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-1sopropylto1uene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichtoroethane-d4 {S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
To1uene-d8 (S)
LABORATORY CONTROL SAMPLE:
Parameter
1, 1, 1,2-Tetrachloroethane
1, 1, 1-Trichloroethane
1, 1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1, 1-Dichloroethane
1 .1-Dichloroethene
1, 1-Dichloropropene
1,2,3-T richlorobenzene
1,2,3-Trichloropropane
1,2.4-Trichlorobenzene
1,2.4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EDB)
Date: 07/22/2009 04:35 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
298025
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11:41
ND 5.0 06/22/09 11 :41
ND 10.0 06/22/09 11 :41
ND 5.0 06/22/09 11:41
ND 20.0 06/22/09 11 :41
ND 5.0 06/22/09 11:41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :4 1
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/0911:41
ND 5.0 06/22/09 11 :41
ND 5.0 06/22/09 11 :41
ND 50.0 06/22/09 11 :41
ND 10.0 06/22/09 11 :41
ND 10.0 06/22/09 11 :41
111 69-121 06/22/09 11 :41
96 74-115 06/22/09 11 :41
107 79-116 06/22/09 11 :41
103 88-110 06/22/09 11 :41
Spike LCS LCS % Rec
Cone. Result % Rec
50 53.8 108
50 58.5 117
50 55.6 111
50 53.1 106
50 58.6 117
50 57.5 115
50 55.1 110
50 56.0 112
50 52.9 106
50 55.5 111
50 58.8 118
50 57.4 115
50 54.4 109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
limits Qualifiers
75-137
70-140
74-133
79-129
72-139
69-154
74-138
71-150
74-135
68-150
70-130
65-146
77-136
Page 43 of 65
www.paCBlabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
LABORATORY CONTROL SAMPLE: 298025
Parameter Units
1,2-Dichlorobenzene u9/k9
1,2-Dichloroethane uglkg
1,2-Dichloropropane uglkg
1,3,5-Trimethylbenzene ug/kg
1,3-Dichlorobenzene uglkg
1,3-Dichloropropane ug/kg
1,4-Dichlorobenzene ug/kg
2,2-Dichloropropane ug/kg
2-Butanone {MEK) ug/kg
2-Chlorotoluene ug/kg
2-Hexanone ug/kg
4-Chlorotoluene ug/kg
4-Methyl-2-pentanone {MIBK) ug/kg
Acetone uglkg
Benzene uglkg
Bromobenzene ug/kg
Bromochloromethane uglkg
Bromodichloromethane uglkg
Bromoform uglkg
Bromomethane ug/kg
Carbon tetrachloride uglkg
Chlorobenzene ug/kg
Chloroethane ug/kg
Chloroform ug/kg
Chloromethane ug/kg
cis-1,2-Dichloroethene ug/kg
cis-1,3-Dichloropropene uglkg
Dibromochloromethane uglkg
Dibromomethane ug/kg
Dichlorodifluoromethane uglkg
Diisopropyl ether ug/kg
Ethyl benzene ug/kg
Hexachloro-1,3-butadiene uglkg
lsopropylbenzene (Cumene) ug/kg
m&p-Xylene uglkg
Methyl-tert-butyl ether ug/kg
Methylene Chloride ug/kg
n-Butylbenzene ug/kg
n-Propylbenzene ug/kg
Naphthalene uglkg
a-Xylene uglkg
p-!sopropyltoluene ug/kg
sec-Butylbenzene ug/kg
Styrene uglkg
tert-Butytbenzene ug/kg
Tetrachloroethene uglkg
Toluene uglkg
trans-1,2-Dichloroethene uglkg
Date: 07/22/2009 04:35 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Cone. Result % Rec Limits
50 53.1 106 75-141
50 56.1 112 74-134
50 50.9 102 77-138
50 57.8 116 65-128
50 50.7 101 76-133
50 52.7 105 79-132
50 55.0 110 75-137
50 65.1 130 73-137
100 112 112 61-138
50 48.6 97 73-138
100 113 113 58-159
50 51.6 103 75-136
100 105 105 74-139
100 120 120 58-150
50 49.9 100 71-140
50 49.9 100 72-144
50 60.0 120 78-133
50 52.8 106 78-133
50 56.7 113 74-132
50 58.4 117 63-184
50 60.8 122 73-143
50 49.6 99 77-137
50 54.7 109 68-146
50 59.2 118 75-137
50 52.6 105 54-143
50 58.9 118 71-143
50 52.6 105 76-133
50 53.2 106 77-131
50 53.7 107 63-184
50 52.5 105 36-173
50 49.9 100 68-144
50 51.9 104 69-141
50 57.1 114 70-152
50 52.5 105 77-143
100 103 103 72-138
50 54.8 110 2-138
50 52.0 104 69-136
50 57.0 114 65-128
50 51.5 103 72-139
50 66.6 133 61-138
50 54.1 108 74-137
50 59.5 119 66-128
50 52.7 105 72-140
50 55.2 110 76-137
50 53.5 107 68-141
50 52.7 105 72-136
50 47.5 95 69-139
50 53.6 107 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc.
,,>':-{-'c,¥~".;-:,., lhelac;,
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Qualifiers
Page 44 of 65
www.paCB/abs.com
Project: AKZONOBEL
Pace Project No.: 9246497
LABORATORY CONTROL SAMPLE:
Parameter
trans-1,3-Dichloropropene
Trichloroethene
Tri chi orofluo ro methane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-dB (S)
MATRIX SPIKE SAMPLE:
Parameter
1,1-Dichloroethene
Benzene
Chlorobenzene
Toluene
Trichloroethene
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-dB (S)
SAMPLE DUPLICATE: 298253
Parameter
1, 1, 1,2-Tetrachloroethane
1, 1, 1-Trichloroethane
1, 1,2,2-Tetrachloroethane
1, 1,2-Trichloroethane
1, 1-Dichloroethane
1 , 1-Dichloroethene
1, 1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trich!oropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane (EOB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
Date: 07/22/2009 04:35 PM
298025
ug/kg
u9/k9
u9/k9
u9/k9
u9/k9
u9/k9
%
%
%
%
Units
298254
u9/k9
u9/k9
u9/k9
u9/k9
ug/kg
%
%
%
%
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
u9/k9
u9/k9
u9/k9
ug/kg
ug/kg
ug/kg
ug/kg
u9/k9
ug/kg
ug/kg
Units
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS
Cone. Result % Rec
50 55.9 112
50 51.4 103
50 57.6 115
100 156 156
50 53.6 107
150 157 105
110
97
110
96
9246642006 Spike MS
Result Cone. Result
ND 47.5 53.3
ND 47.5 45.4
ND 47.5 38.4
ND 47.5 37.9
ND 47.5 41.0
9246497001 Dup
Result Result RPD
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
31.3 35.2
ND ND
ND ND
ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
% Rec
Limits
73-135
75-136
69-144
50-150 L3
61-145
73-138
69-121
74-115
79-116
88-110
MS
%Rec
112
85
81
80
86
107
95
112
99
Qualifiers
12
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
% Rec
Limits Qualifiers
33-158
46-143
29-159
38-145
70-130
69-121
74-115
79-116
88-110
Page 45 of 65
www.pecelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
SAMPLE DUPLICATE: 298253
Parameter
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichtoropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Ch!oroethane
Chloroform
Chloromethane
cis-1,2•Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dich1orodifluoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
lsopropy!benzene (Cumene)
m&p-Xylene
Methyl-tert-butyl ether
Methylene Chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
p-lsopropyltoluene
sec-Butyl benzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Date: 07/22/2009 04:35 PM
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9246497001 Dup
Result Result RPO Qualifiers
ND ND
ND ND
ND ND
ND 4.2J
ND ND
ND ND
ND ND
ND ND
ND 47.lJ
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
• ~o_',"-'':.._~-!.c,, ,,161e1ac;,
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875•9092
Page 46 of 65
wwwpt1colabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
SAMPLE DUPLICATE: 298253
Parameter Units
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Dibromofluoromethane {S)
Toluene-dB (S)
Date: 07/22/2009 04:35 PM
ug/kg
%
%
%
%
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
QUALITY CONTROL DATA
9246497001 Dup
Result Result RPD
ND ND
109 108
96 97
109 109
98 99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services. Inc
Qualifiers
10
8
10
8
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 65
www.pscelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: MPRP/4595 Analysis Method:
QC Batch Method: EPA 3050 Analysis Description:
Associated Lab Sa'mples: 9246497003, 9246497004, 9246497005, 9246497006
METHOD BLANK: 295123 Matrix: Solid
Associated Lab Samples: 9246497003, 9246497004, 9246497005, 9246497006
EPA6010
6010 MET
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Arsenic mg/kg ND 0.50 06/17/09 16:51
Barium mg/kg ND 0.50 06/17/0916:51
Cadmium mg/kg ND 0.10 06/17/0916:51
Chromium mg/kg ND 0.50 06/17/09 16:51
Lead mg/kg ND 0.50 06/17/09 16:51
Selenium mg/kg ND 1.0 06/17/09 16:51
Silver mg/kg ND 0.50 06/17/09 16:51
LABORATORY CONTROL SAMPLE: 295124
Spike LCS LCS % Rec
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Cone. Result % Rec Limits Qualifiers
Arsenic mg/kg 50 44.4 89
Barium mg/kg 50 46.1 92
Cadmium mg/kg 50 45.2 90
Chromium mg/kg 50 45.5 91
Lead mg/kg 50 45.2 90
Selenium mg/kg 50 43.9 88
Silver mg/kg 25 23.0 92
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 295125 295126
MS MSD
9246339002 Spike Spike MS MSD
Parameter Units
Arsenic mg/kg
Barium mg/kg
Cadmium mg/kg
Chromium mg/kg
Lead mg/kg
Selenium mg/kg
Silver mg/kg
Date: 07/22/2009 04:35 PM
Result Cone. Cone. Result Result
5.5 56.2 34.3 53.5 34.5
35.8 56.2 34.3 89.7 73.5
ND 56.2 34.3 47.8 28.3
5.6 56.2 34.3 54.8 35.1
60.6 56.2 34.3 107 84.1
ND 56.2 34.3 48.1 28.7
ND 28.1 17.1 24.9 14.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc ..
80-120
80-120
80-120
80-120
80-120
80-120
80-120
MS MSD %Rec
% Rec %Rec Limits RPO Qual
85 85 75-125 43 R1
96 110 75-125 20
85 82 75-125 51 R1
87 86 75-125 44 R1
82 68 75-125 24 MO,R1
85 83 75-125 51 R1
88 86 75-125 50 R1
Page 48 of 65
WMV.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: MERP/2256
QC Batch Method: EPA 7470
Associated Lab Samples: 9246497007, 9246497008
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
METHOD BLANK: 305492 Matrix: Water
Associated Lab Samples: 9246497007, 9246497008
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L
LABORATORY CONTROL SAMPLE: 305493
Parameter Units
Mercury ug/L
MATRIX SPIKE SAMPLE: 305494
Parameter Units
Mercury ug/L
SAMPLE DUPLICATE: 305495
Parameter Units
Mercury ug/L
Date: 07/22/2009 04:35 PM
ND 0.20 07/09/09 11:53
Spike
Cone.
2.5
9246497007
Result
LCS
Result
2.6
Spike
Cone.
ND 2.5
9246497008 Dup
Result Result
ND ND
LCS
% Rec
106
MS
Result
RPD
2.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc
-""";'"l:r,, i1□eld.C,
%Rec
Limits
80-120
MS
% Rec
89
Qualifiers
Qualifiers
% Rec
Limits
75-125
Qualifiers
Page 49 of 65
www.plloolabs.com
Project: AKZO NOBEL
Pace Project No.: 9246497
QC Batch: MPRP/4710
QC Batch Method: EPA3010
Associated Lab Samples: 9246497007, 9246497008
METHOD BLANK: 305498
Associated Lab Samples: 9246497007, 9246497008
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
QUALITY CONTROL DATA
Analysis Method: EPA 6010
Analysis Description: 6010 MET TCLP
Matrix; Water
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
LABORATORY CONTROL SAMPLE:
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
MATRIX SPIKE SAMPLE:
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
SAMPLE DUPLICATE: 305501
Arsenic
Barium
Cadmium
Chromium
Lead
Parameter
Date: 07/22/2009 04:35 PM
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
305499
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
305500
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Units
ND 0.025 07/09/09 14:24
ND 0.025 07/09/09 14:24
ND 0.0050 07/09/09 14:24
ND 0.025 07/09/09 14:24
ND 0.025 07/09/09 14:24
ND 0.050 07/09/09 14:24
ND 0.025 07/09/09 14:24
Spike LCS LCS % Rec
Cone. Result % Rec Limits
2.5 2.6 105 80-120
2.5 2.3 91 80-120
2.5 2.4 94 80-120
2.5 2.4 95 80-120
2.5 2.2 88 80-120
2.5 2.7 109 80-120
1.2 1.3 102 80-120
9246497007 Spike MS MS
Result Cone. Result %Rec
0.033 2.5 2.7 108
0.15 2.5 2.4 90
ND 2.5 2.3 91
ND 2.5 2.4 93
ND 2.5 2.2 86
ND 2.5 2.8 112
ND 1.2 1.3 103
9246497007 Dup
Result Result RPD Qualifiers
0.033 0.037 13
0.15 0.22 35 R1
ND ND
ND .02J
ND ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Qualifiers
% Rec
Limits Qualifiers
75-125
75-125
75-125
75-125
75-125
75-125
75-125
Page 50 of 65
www.paceJabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
SAMPLE DUPLICATE: 305501
Selenium
Silver
Parameter
Date: 07/22/2009 04:35 PM
mg/L
mg/L
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
QUALITY CONTROL DATA
9246497007 Dup
Result
ND
ND
Result
ND
ND
RPO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
..,.,s-:.~-~:~!';:~~~
11ne1c1c;
Qualifiers
Pace Analytical Services, lnc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
{704)875-9092
Page 51 of 65
www.pacelabs.com
Project AKZONOBEL
Pace Project No.: 9246497
QC Batch: MSV/7692
QC Batch Method: EPA 8260
Associated Lab Samples: 9246497004
METHOD BLANK: 310494
Associated Lab Samples: 9246497004
Parameter Units
1, 1-Dichloroethene ug/L
1,2-Dichloroethane ug/L
1.4-Dichlorobenzene ug/L
2-Butanone {MEK) ug/L
Benzene ug/L
Carbon tetrachloride ug/L
Chlorobenzene ug/L
Chloroform ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
Vinyl chloride ug/L
1,2-Dichloroethane-d4 (S) %
4-Bromofluorobenzene (S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
LABORATORY CONTROL SAMPLE 310495
Parameter Units
1, 1-Dichloroethene ug/L
1,2-Dichloroethane ug/L
1 ,4-Dichlorobenzene ug/L
2-Butanone (MEK) ug/L
Benzene ug/L
Carbon tetrachloride ug/L
Chlorobenzene ug/L
Chloroform ug/L
Tetrachloroethene ug/L
Trichloroethene ug/L
Vinyl chloride ug/L
1,2-Dich!oroethane-d4 {S) %
4-Bromofluorobenzene {S) %
Dibromofluoromethane (S) %
Toluene-dB (S) %
Date: 07122/2009 04:35 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8260
Analysis Description: 8260 MSV TCLP
Matrix: Water
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Resu!t Limit Analyzed Qualifiers
ND 5.0 06122109 11 :22
ND 5.0 06122109 11 :22
ND 5.0 06122/09 11 :22
ND 10.0 06/22109 11 :22
ND 5.0 06122109 11 :22
ND 5.0 06122109 11 :22
ND 5.0 06122109 11 :22
ND 5.0 06122/09 11 :22
ND 5.0 06122/09 11 :22
ND 5.0 06/22109 11 :22
ND 5.0 06/22109 11 :22
105 79-120 06122/09 11 :22
97 87-109 06122109 11 :22
110 85-115 06122/09 11 :22
102 70-120 06122109 11 :22
Spike LCS LCS % Rec
Cone. Result % Rec
50 57.5 115
50 56.1 112
50 55.0 110
100 112 112
50 49.9 100
50 60.8 122
50 49.6 99
50 59.2 118
50 52.7 105
50 51.4 103
50 53.6 107
110
97
110
96
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc ..
Limits
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
50-150
79-120
87-109
85-115
70-120
Qualifiers
Page 52 of 65
www.pecolabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: OEXT/7178
QC Batch Method: EPA3510
Associated Lab Samples: 9246497007, 9246497008
METHOD BLANK: 298346
Associated Lab Samples: 9246497007, 9246497008
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA8270
Analysis Description: 8270 TCLP MSSV
Matrix: Water
Blank Reporting
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
1,4-Dichlorobenzene ug/L
2,4,5-T richlorophenol ug/L
2 ,4,6-T richlorophenol ug/L
2 ,4-Dinitrotoluene u9/L
2 -Methyl phenol( o-Creso I} u9/L
3&4-Methylpheno!(m&p Cresol} ug/L
Hexachloro-1,3-butadlene u9/L
Hexachlorobenzene u9/L
Hexachloroethane ug/L
Nitrobenzene ug/L
Pentachlorophenol ug/L
Pyridine ug/L
2.4,6-Tribromophenol (S) %
2-Fluorobiphenyl (S) %
2-Fluorophenol (S) %
Nitrobenzene-d5 (S) %
Phenol-d6 (S) %
Terphenyl-d14 (S) %
LABORATORY CONTROL SAMPLE: 298347
Parameter Units
1,4-Dichlorobenzene ug/L
2.4,5-Trichlorophenol ug/L
2,4,6-Trichloropheno! ug/L
2,4-Dinitrotoluene ug/L
2-Methylphenol(o-Cresol) ug/L
3&4-Methylphenol(m&p Cresol) ug/L
Hexachlor0-1,3-butadiene ug/L
Hexachlorobenzene ug/L
Hexachloroethane ug/L
Nitrobenzene ug/L
Pentachlorophenol ug/L
Pyridine ug/L
2.4,6-Tribromophenol (S) %
2-Fluorobiphenyl (S) %
2-Fluorophenol (S) %
Nitrobenzene-d5 (S) %
Pheno!-d6 (S) %
Terphenyl-d14 (S) %
Date: 07/22/2009 04:35 PM
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND · 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
ND 50.0 06/29/09 15:39
76 25-150 06/29/09 15:39
71 30-150 06/29/09 15:39
38 25-150 06/29/09 15:39
66 30-150 06/29/09 15:39
25 25-150 06/29/09 15:39
71 30-150 06/29/09 15:39
Spike LCS LCS % Rec
Cone. Result %Rec
500 268 54
500 403 81
500 413 83
500 341 68
500 255 51
500 239 48
500 345 69
500 426 85
500 246 49
500 383 77
500 335 67
500 167 33
82
67
33
61
25
70
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Limits
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
30-150
25-150
30-150
25-150
30-150
25-150
30-150
Qualifiers
Page 53 of 65
wwwpacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: PMST/2539
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
QC Batch Method: ASTM 02974-87 Analysis Description: Dry WeighUPercent Moisture
Associated Lab Samples: 9246497001, 9246497002, 9246497003, 9246497004, 9246497005, 9246497006
SAMPLE DUPLICATE: 296421
Parameter Units
Percent Moisture %
SAMPLE DUPLICATE: 296422
Parameter Units
Percent Moisture %
Date: 0712212009 04:35 PM
9246385007 Dup
Result Resu!t . RPD
14.2 13.6
9246748002 Dup
Result Result RPD
23.3 24.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
4
3
Qualifiers
Qualifiers
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 65
www.pace/abs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: OEXT/7221
QC Batch Method: EPA 3546
Associated Lab Samples: 9246497001, 9246497002
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA8270
Analysis Description: 8270 Solid MSSV Microwave
METHOD BLANK: 299697 Matrix: Solid
Associated Lab Samples: 9246497001, 9246497002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,2,4-Trichlorobenzene ug/kg ND 330 06/30/09 14:11
1,2-Dich!orobenzene ug/kg ND 330 06/30/09 14:11
1,2-Diphenylhydrazine ug/kg ND 330 06/30/09 14:11
1,3-Dichlorobenzene ug/kg ND 330 06/30/09 14:11
1,4-Dichlorobenzene ug/kg ND 330 06/30/09 14:11
1-Methylnaphthalene ug/kg ND 330 06/30/09 14:11
2.4,5-Trichlorophenol ug/kg ND 330 06/30/09 14:11
2,4 ,6-Trichlorophenol ug/kg ND 330 06/30/09 14:11
2,4-Oichlorophenol ug/kg ND 330 06/30/09 14:11
2,4-Dimethylphenol ug/kg ND 330 06/30/09 14:11
2,4-Dinitrophenol ug/kg ND 1650 06/30/09 14:11
2.4-Dinitrotoluene ug/kg ND 330 06/30/09 14:11
2,6-Dinltrotoluene ug/kg ND 330 06/30/09 14:11
2-Ch!oronaphthalene ug/kg ND 330 06/30/09 14:11
2-Chlorophenol ug/kg ND 330 06/30/09 14:11
2-Methylnaphthalene ug/kg ND 330 06/30/09 14:11
2-Methylphenol(o-Cresol) ug/kg· ND 330 06/30/09 14:11
2-Nitroaniline ug/kg ND 1650 06/30/09 14:11
2-Nltrophenol ug/kg ND 330 06/30/09 14:11
3&4-Methylphenol(m&p Cresol) ug/kg ND 330 06/30/09 14:11
3,3'-Dichlorobenzidine ug/kg ND 1650 06/30/09 14:11
3-Nitroaniline ug/kg ND 1650 06/30/09 14:11
4,6-Dinitro-2-methylphenol ug/kg ND 66o' 06/30/09 14:11
4-Bromophenylphenyl ether ug/kg ND 330 06/30/09 14:11
4-Chloro-3-methylphenol ug/kg ND 660 06/30/09 14:11
4-Chloroaniline ug/kg ND 1650 06/30/09 14:11
. 4-Chlorophenylphenyl ether ug/kg ND 330 06/30/09 14:11
4-Nitroaniline ug/kg ND 660 06/30/09 14:11
4-Nitrophenol ug/kg ND 1650 06/30/09 14:11
Acenaphthene ug/kg ND 330 06/30/09 14:11
Acenaphthylene ug/kg ND 330 06/30/09 14:11
Aniline ug/kg ND 330 06/30/09 14:11
Anthracene ug/kg ND 330 06/30/09 14:11
Benzo(a)anthracene ug/kg ND 330 06/30/09 14:11
Benzo(a)pyrene ug/kg ND 330 06/30/09 14:11
Benzo(b )fluoranthene ug/kg ND 330 06/30/09 14:11
Be nzo(g, h, i) pe ryle ne ug/kg ND 330 06/30/09 14:11
Benzo(k)fluoranthene ug/kg ND 330 06/30/09 14:11
Benzoic Acid ug/kg ND 1650 06/30/09 14:11
Benzyl alcohol ug/kg ND 660 06/30/09 14:11
bis(2-Chloroethoxy)methane ug/kg ND 330 06/30/09 14:11
bis(2-Chloroethyl) ether ug/kg ND 330 06/30/09 14:11
bis(2-Chloroisopropyl) ether ug/kg ND 330 06/30/09 14:11
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
.., .. -:;-':.(-"~:!'~~" .. •,nelao, ::i --~
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
METHOD BLANK: 299697
Pace Analytical Services, Inc.
2225 Riverside Or.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Matrix: Solid
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Associated Lab Samples: 9246497001,9246497002
Parameter
bis(2-Ethylhexyl)phtha\ate
Butyl be nzylphtha la le
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz (a, h )a nthracene
Dibenzofuran
Diethylphthalate
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
lndeno(1,2,3-cd)pyrene
lsophorone
N-Nitroso-di-n-propylamine
N-Nitrosodimethylamine
N-N ltrosod i p henyla mine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
LABORATORY CONTROL SAMPLE:
Parameter
1,2,4-Trich!orobenzene
1,2-Dichlorobenzene
1,2-Diphenylhydrazine
1,3-0ichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4 ,5-Trichlorophenol
2,4,6-Trichlorophenol
2 ,4-Dichlorophenol
Date: 07122/2009 04:35 PM
Units
ug/kg
ug/kg
uglkg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
ug/kg
uglkg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
299698
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
uglkg
uglkg
ug/kg
Units
Blank Reporting
Result Limit Analyzed Qualifiers
ND 330 06130109 14:11
ND 330 06130/09 14:11
ND 330 06/30109 14:11
ND 330 06/30/09 14:11
ND 330 06/30109 14:11
ND 330 06/30109 14:11
ND 330 06130/09 14:11
ND 330 06130109 14:11
ND 330 06/30109 14:11
ND 330 06/30109 14:11
ND 330 06130109 14:11
ND 330 06130109 14:11
ND 330 06130/0914:11
ND 330 06/30109 14:11
ND 330 06/30109 14:11
ND 330 06130/09 14:11
ND 330 06130/09 14:11
ND 330 06130/09 14:11
ND 330 06130109 14:11
ND 330 06/30109 14:11
ND 330 06/30109 14:11
ND 330 06/30/09 14:11
ND 1650 06130/09 14:11
ND 330 06130/09 14:11
ND 330 06130/09 14:11
ND 330 06/30109 14:11
71 44-136 06/30109 14:11
68 46-120 06/30109 14:11
56 24-120 06130/09 14:11
57 30-150 06130/09 14:11
58 35-120 06130109 14:11
68 38-108 06/30109 1411
Spike LCS LCS %Rec
Cone. Result % Rec
1670 1080 65
1670 987 59
1670 1270 76
1670 944 57
1670 1010 60
1670 1070 64
1670 1350 81
1670 1350 81
1670 1150 69
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, Inc ..
Limits Qualifiers
50-150
50-150
43-130
50-150
50-150
50-150
50-150
50-150
50-150
Page 56 of 65
www.pt1C8Jabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
LABORATORY CONTROL SAMPLE: 299698
Parameter Units
2 ,4-Dimethylphenol u9/k9
2,4-Dinitrophenol ug/kg
2.4-Dinitrotoluene uglkg
2,6-Dinitrotoluene . ug/k9
2-Chloronaphthalene u9/k9
2-Chlorophenol u9/k9
2-Methylnaphtha!ene u9/kg
2-Methylphenol(o-Cresol) ug/kg
2-Nitroaniline ug/kg
2-Nitrophenol u9/k9
3&4-Methylphenol(m&p Cresol) u9/k9
3,3'-Dichlorobenzidine u9/kg
3-Nitroaniline ug/kg
4,6-Dinitro-2-methylphenol ug/kg
4-Bromophenylphenyl ether ug/k9
4-Chloro-3-methylphenol ug/kg
4-Chloroaniline ug/kg
4-Chlorophenylphenyl ether uglkg
4-Nitroaniline ug/kg
4-Nitrophenol uglkg
Acenaphthene ug/kg
Acenaphthylene uglkg
Aniline uglkg
Anthracene ug/kg
Benzo(a)anthracene ug/kg
Benzo(a)pyrene ug/kg
Benzo(b)fluoranthene ug/kg
Benzo(g ,h,i)perylene uglkg
Benzo(k)fiuoranthene uglkg
Benzoic Acid ug/kg
Benzyl alcohol ug/kg
bis(2-Chloroethoxy)methane ug/kg
bis(2-Chloroethyl) ether ug/kg
bis(2-Chloroisopropyl) ether ug/kg
bis(2-Ethylhexyl)phlhalate uglkg
B utylbenzyl p htha I ate ug/kg
Chrysene ug/kg
Di-n-butylphtha!ate ug/kg
Di-n-octylphtha1ate ug/kg
Di be nz( a, h )a nth ra cene ug/kg
Dibenzofuran uglkg
Diethy1phthalate ug/kg
Dimethylphthalate ug/kg
Fluoranthene ug/kg
Fluorene ug/kg
Hexachloro-1,3-butadiene ug/kg
Hexachlorobenzene ug/kg
Hexachlorocyclopentadiene ug/kg
Date: 0712212009 04:35 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
{828)254-7176
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Cone. Result % Rec Limits
1670 1060 64 50-150
1670 982J 59 20-111
1670 1220 73 50-150
1670 1080 65 50-150
1670 1080 65 50-150
1670 950 57 50-150
1670 1430 86 50-150
1670 959 58 50-150
1670 1230J 74 50-150
1670 1070 64 50-150
1670 1000 60 50-150
1670 1190J 72 50-150
1670 1280J 77 50-150
1670 1300 78 15-136
1670 1330 80 50-150
1670 1150 69 50-150
1670 1400J 84 50-150
1670 1450 87 50-150
1670 1180 71 50-150
1670 1130J 68 33-105
1670 1280 77 50-150
1670 1290 77 50-150
1670 833 50 50-150
1670 1310 79 50-150
1670 1240 75 50-150
1670 1270 76 50-150
1670 1270 76 50-150
1670 1660 100 24-117
1670 903 54 50-150
1670 472J 28 15-104
1670 933 56 50-150
1670 1120 67 50-150
1670 1140 68 50-150
1670 943 57 50-150
1670 1130 68 50-150
1670 1100 66 50-150
1670 1300 78 50-150
1670 1250 75 50-150
1670 1080 65 50-150
1670 1450 87 17-128
1670 1290 77 50-150
1670 1100 66 50-150
1670 1160 70 50-150
1670 1460 88 50-150
1670 1340 80 50-150
1670 1240 74 50-150
1670 1470 88 50-150
1670 1220 73 15-114
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, \nc ..
iib;~2;,
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 57 of 65
www.pacelabs.com
Project: AKZONOBEL
Pace Project N?.: 9246497
LABORATORY CONTROL SAMPLE: 299698
Parameter Units
Hexachloroethane ug/kg
lndeno( 1,2,3-cd)pyrene ug/kg
lsophorone ug/kg
N-Nitroso-di-n-propylamine ug/kg
N-Nitrosodimethylamine ug/kg
N-Nitrosodiphenylamine ug/kg
Naphthalene ug/kg
Nitrobenzene ug/kg
Pentachlorophenol ug/kg
Phenanthrene ug/kg
Phenol ug/kg
Pyrene ug/kg
2,4,6-Tribromophenol (S) %
2-Fluorobiphenyl (~) %
2-Fluorophenol {S) %
Nitrobenzene-d5 (S) %
Phenol-dB (S) %
Terphenyl-d14 (S) %
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 299699
9246803006
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Spike LCS LCS %Rec
Cone. Result % Rec Limits
1670 932 56 50-150
1670 1480 89 19-128
1670 1110 66 50-150
1670 1050 63 50-150
1670 905 54 50-150
1670 1460 88 50-150
1670 1110 66 50-150
1670 1140 68 50-150
1670 1300J 78 15-130
1670 1340 80 50-150
1670 981 59 42-120
1670 1210 73 50-150
84 44-136
69 46-120
54 24-120
56 30-150
56 35-120
68 38-108
299700
MS MSD
Spike Spike MS MSD MS MSD
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
% Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPO Qual
1,2,4-Trichlorobenzene ug/kg
1,4-Dichlorobenzene ug/kg
2,4-Dinltrotoluene ug/kg
2-Chlorophenol ug/kg
4-Chloro-3-methylphenol ug/kg
4-Nitrophenol ug/kg
Acenaphthene ug/kg
N-Nitroso-di-n-propylamine ug/kg
Pentachlorophenol ug/kg
Phenol ug/kg
Pyrene ug/kg
2,4,6-Tribromophenol (S) %
2-Fluorobiphenyl (S) %
2-Fluorophenol (S) %
Nitrobenzene-d5 (S) %
Phenol-dB (S) %
Terphenyl-d14 (S) %
Date: 07/22/2009 04:35 PM
ND 3580 3580 2180 2280
ND 3580 3580 2080 2180
ND 3580 3580 2240 2440
ND 3580 3580 1950 2070
ND 3580 3580 2250 2330
ND 3580 3580 1880J 1900J
ND 3580 3580 2390 2560
ND 3580 3580 2130 2310
ND 3580 3580 2270J 2570J
ND 3580 3580 1910 2020
ND 3580 3580 2440 2560
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
61 64 50-150 5
58 61 50-150 5
63 68 50-150 8
55 58 50-150 6
63 65 50-150 4
53 53 50-150
67 72 50-150 7
60 65 50-150 8
64 72 50-150
54 57 50-150 6
68 72 50-150 5
74 80 44-136
62 68 46-120
52 55 24-120
57 59 30-150
53 56 35-120
60 62 38-108
Page 58 of 65
www.pacelabs.com
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: MERP/2219 Analysis Method:
QC Batch Method: EPA 7471 Analysis Description:
Associated Lab Samples: 9246497004, 9246497005, 9246497006
METHOD BLANK: 295137 Matrix: Solid
Associated Lab Samples: 9246497004, 9246497005, 9246497006
Blank Reporting
EPA 7471
7471 Mercury
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 295138
Parameter Units
Mercury mg/kg
MATRIX SPIKE SAMPLE: 295139
Parameter Units
Mercury mg/kg
SAMPLE DUPLICATE: 295140
Parameter Units
Mercury mg/kg
Date: 07/22/2009 04:35 PM
ND 0.0050 06/17/09 13:57
Spike
Cone.
.067
9246505010
Result
LCS
Result
0.065
Spike
Cone.
0.059 .068
9246497004 Dup
Result Result
0.050 0.036
LCS
% Rec
98
MS
Result
0.091
RPO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
%Rec
Limits
80-120
MS
%Rec
48
Qualifiers
65 R1
Qualifiers
% Rec
Limits Qualifiers
75-125 MO
Page 59 of 65
www.paOOlabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: OEXT/7419
QC Batch Method: EPA3510
Associated Lab Samples: 9246497003, 9246497004
METHOD BLANK: 309749
Associated Lab Samples: 9246497003, 9246497004
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA8270
Analysis Description: 8270 TCLP MSSV
Matrix: Water
Blank Reporting
Pace Analytical Services, lnc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
1,4-Dichlorobenzene ug/L ND 50.0 07121109 14:24
2,4,5-T richlorophenol ug/L ND 50.0 07121109 14:24
2,4,6-Trichloi--ophenol ug/L ND 50.0 07/21109 14:24
2,4-Dinitrotoluene ug/L ND 50.0 07/21109 14:24
2-Methylphenol{o-Cresol) ug/L ND 50.0 07121109 14:24
3&4-Methylphenol{m&p Cresol) ug/L ND 50.0 07121109 14:24
Hexachloro-1,3-butadiene ug/L ND 50.0 07121/09 14:24
Hexachlorobenzene ug/L ND 50.0 07121109 14:24
Hexachloroethane ug/L ND 50.0 07121109 14:24
Nitrobenzene ug/L ND 50.0 07121109 14:24
Pentachlorophenol ug/L ND 50.0 07121109 14:24
Pyridine ug/L ND 50.0 07121109 14:24
2,4,6-Tribromophenol {S) % 70 25-150 07121/0914:24
2-Fluorobiphenyl {S) % 70 30-150 07121109 14:24
2-Fluorophenol {S) % 40 25-150 07/21109 14:24
Nitrobenzene-d5 {S) % 73 30-150 07/21/0914:24
Phenot-d6 (S) % 30 25-150 07121109 14:24
Terphenyl-d14 (S) % 75 30-150 07121109 14:24
LABORATORY CONTROL SAMPLE: 309750
Spike LCS LCS % Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
1,4-Dichlorobenzene ug/L 500 325 65 30-150
2,4,S-Trichlorophenol ug/L 500 378 76 30-150
2,4,6-Trichlorophenol ug/L 500 408 82 30-150
2,4-Dinitrotoluene ug/L 500 424 85 30-150
2-Methylphenol(o-Cresol) ug/L 500 313 63 30-150
3&4-Methylphenol(m&p Cresol) ug/L 500 315 63 30-150
Hexachloro-1,3-butadiene ug/L 500 360 72 30-150
Hexachlorobenzene ug/L 500 393 79 30-150
Hexachloroethane ug/L 500 324 65 30-150
Nitrobenzene ug/L 500 492 98 30-150
Pentachlorophenol ug/L 500 327 65 30-150
Pyridine ug/L 500 189 38 30-150
2,4,6-Tribromophenol {S) % 74 25-150
2-F!uorobiphenyl {S) % 72 30-150
2-Fluorophenol {S) % 40 25-150
Nitrobenzene-d5 {S) % 78 30-150
Phenol-d6 (S) % 33 25-150
Terphenyl-d14 (S) % 76 30-150
Date: 07/22/2009 04:35 PM REPORT OF LABORATORY ANALYSIS Page 60 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
. {-;::.(·'°.,_~tc:\~~ i1nelac\
www.pee&labs.com
Project: AKZONOBEL
Pace Project No.: 9246497
QC Batch: MPRP/4572
QC Batch Method: EPA 3050
Associated Lab Samples: 9246497001, 9246497002
METHOD BLANK: 294449
Associated Lab Samples: 9246497001, 9246497002
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method:
Analysis Description:
Matrix: Solid
Blank Reporting
EPA6010
6010 MET
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Parameter Units Result Limit Analyzed Qualifiers
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
LABORATORY CONTROL SAMPLE:
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
MATRIX SPIKE SAMPLE:
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Parameter
SAMPLE DUPLICATE: 294452
Arsenic
Barium
Cadmium
Chromium
Lead
Parameter
Date: 07/22/2009 04:35 PM
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
294450
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units
294451
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
Units
Units
ND 0.50 06/16/09 16:26
ND · 0.50 06/16/09 16:26
ND 0.10 06/16/09 16:26
ND 0.50 06/16/09 16:26
ND 0.50 06/16/09 16:26
ND 1.0 06/16/09 16:26
ND 0.50 06/16/09 16:26
Spike LCS LCS % Rec
Cone. Result % Rec
50 46.2 92
50 48.3 97
50 46.2 92
50 47.8 96
50 46.6 93
50 45.2 90
25 24.3 97
9246467001 Spike MS
Result Cone. Result
1.8 125 98.5
466 125 180
12.9 125 136
1.9 125 118
6840 125 19000
ND 125 102
ND 62.5 62.5
9246505001 Dup
Result Result RPO
5.3 5.8 10
18.7 19.9 6
4.6 4.0 15
11.8 11.1 6
19.4 19.4 .07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Limits
80-120
80-120
80-120
80-120
80-120
80-120
80-120
MS
%Rec
77
-228
99
93
9770
81
99
Qualifiers
Qualifiers
% Rec
Limits Qualifiers
75-125
75-125 MO
75-125
75-125
75-125 MO
75-125
75-125
Page 61 of 65
www.pacetabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
SAMPLE DUPLICATE: 294452
Selenium
Silver
Parameter
Date: 07/22/2009 04:35 PM
mg/kg
mg/kg
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
9246505001 Dup
Result
1.7
ND
Result
1.8
.092J
RPD
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
without the written consent of Pace Analytical Services, Inc.
Qualifiers
5
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 65
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: AKZONOBEL
Pace Project No.: 9246497
DEFINITIONS
OF -Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND -Not Detected at or above adjusted reporting limit.
J -Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method.Detection Limit.
S -Surrogate
1,2-Diphenylhydrazine {8270 tisted analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPO values.
LCS(D) -Laboratory Control Sample {Duplicate)
MS(D) -Matrix Spike (Duplicate)
DUP -Sample Duplicate
RPO -Relative Percent Difference
NC -Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the curr~nt list of accredited analytes.
U -Indicates the compound was analyzed for, but not detected.
LABORATORIES
PASI-A
PASI-C
Pace Analytical Services -Asheville
Pace Analytical Services -Charlotte
ANALYTE QUALIFIERS
1g
2g
E
LO
L3
MO
R1
so
Acid surrogate recovery is outside of control limits. The data was accepted based on valid recovery of the two remaining
acid surrogates.
Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the 2 remaining acid
surrogates.
Analyte concentration exceeded the calibration range. The reported result is estimated.
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.
Matrix spike recovery was outside laboratory control limits.
RPO value was outside control limits.
Surrogate recovery outside laboratory control limits.
Date: 0712212009 04:35 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Page 63 of 65
www.paooJabs.com
Project: AKZONOBEL
Pace Project No.: 9246497
Lab ID Sample ID
9246497001 STK 3.1
9246497002 STK 3.2
9246497001 STK 3.1
9246497002 STK 3.2
9246497003 STK 3.3
9246497003 STK 3.3
9246497004 STK 3.4
9246497005 STK 3.5
9246497006 STK 3.6
9246497004 STK 3.4
9246497005 STK 3.5
9246497006 STK 3.6
9246497003 STK 3.3
9246497004 STK 3.4
9246497005 STK 3.5
9246497006 STK 3.6
9246497001 STK 3.1
9246497002 STK 3.2
9246497003 STK 3.3
9246497004 STK 3.4
9246497005 STK 3.5
9246497006 STK 3.6
9246497007 CONC 3.1
9246497008 CONC 3.2
9246497001 STK 3.1
9246497002 STK 3.2
9246497003 STK 3.3
9246497004 STK 3.4
9246497005 STK 3.5
9246497006 STK 3.6
9246497007 CONC 3.1
9246497008 CONC 3.2
9246497001 STK 3.1
9246497002 STK 3.2
9246497007 CONC 3.1
9246497008 CONC 3.2
9246497007 CONC 3.1
9246497008 CONC 3.2
9246497003 STK 3.3
9246497004 STK 3.4
9246497004 STK 3.4
9246497003 STK 3.3
Date: 07/22/2009 04:35 PM
Pace Analytical Services, Inc.
2225 Riverside Dr
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
QC Batch Method QC Batch Analytical Method Batch
EPA3050 MPRP/4572 EPA6010 ICP/4257
EPA3050 MPRP/4572 EPA6010 ICP/4257
EPA 7471 MERP/2211 EPA 7471 MERC/2204
EPA 7471 MERP/2211 EPA 7471 MERC/2204
EPA 7471 MERP/2211 EPA 7471 MERC/2204
EPA3050 MPRP/4595 EPA 6010 ICP/4273
EPA3050 MPRP/4595 EPA6010 ICP/4273
EPA3050 MPRP/4595 EPA6010 ICP/4273
EPA 3050 MPRP/4595 EPA6010 ICP/4273
EPA 7471 MERP/2219 EPA 7471 MERC/2212
EPA 7471 MERP/2219 EPA 7471 MERC/2212
EPA 7471 MERP/2219 EPA 7471 MERC/2212
EPA3546 OEXT/7137 EPA 8270 MSSV/2815
EPA 3546 OEXT/7137 EPA 8270 MSSV/2815
EPA3546 OEXT/7137 EPA8270 MSSV/2815
EPA 3546 OEXT/7137 EPA 8270 MSSV/2815
ASTM D2974-87 PMST/2539
ASTM D2974-87 PMST/2539
ASTM D2974-87 PMST/2539
ASTM D2974-87 PMST/2539
ASTM D2974-87 PMST/2539
ASTM D2974-87 PMST/2539
EPA8260 MSV/7405
EPA8260 MSV/7405
EPA8260 MSV/7419
EPA 8260 MSV/7419
EPA8260 MSV/7419
EPA8260 MSV/7419
EPA 8260 MSV/7419
EPA8260 MSV/7419
EPA3510 OEXT/7178 EPA 8270 MSSV/2831
EPA3510 OEXT/7178 EPA 8270 MSSV/2831
EPA 3546 OEXT/7221 EPA 8270 MSSV/2838
EPA 3546 OEXT/7221 EPA8270 MSSV/2838
EPA 7470 MERP/2256 EPA 7470 MERC/2244
EPA 7470 MERP/2256 EPA 7470 MERC/2244
EPA3010 MPRP/4710 EPA6010 ICP/4374
EPA 3010 MPRP/4710 EPA6010 !CP/4374
EPA3510 OEXT/7419 EPA 8270 MSSV/2906
EPA3510 OEXT/7419 EPA 8270 MSSV/2906
EPA 8260 MSV/7692
EPA8260 MSV/7705
REPORT OF LABORATORY ANALYSIS Page 64 of 65
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
,. •<co•
,1~1eGi~,, .,, -,,
Project: AKZONOBEL
Pace Project No.: 9246497
Lab ID Sample ID --------
Date: 0712212009 04:35 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch Method QC Batch Analytical Method
Analytical
Batch ----
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc ..
Page 65 of 65
aeAna/ytica/"
._.,-c,!Hs.cam
CHAIN-OF-CUSTODY/ Analytical Request Document
The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately .
Section A Section B Section C
R1qulrad Client Information: R■quln,d Project Information; Invoice Information:
CompanE,~ Attention:
Company Name:
Page: / of /
1174412
DRINKING WATER
OTHER
~~~~q-~~~~~!!~:A~~IY.Si_~;!;m~!~<t('([N)Jf~. t?:~:1r=-~i~\",f•··.; ;)~-:.~-:---::,":-0
•• • ~
" " w t:
Section D
Requir&dClien1 lnformalioo
SAMPLE ID
{A-Z, 0-9 / ,-)
Sample IDs MUST BE UNJQUE
Matrix Code.
lMIBQI. I QQQE
Drinking Water DW
Water WT
Waste Water WW
Prcxluct p
SoiVSorid SL
Oil OL
V.,pe WP
'"' AR
Tissue TS
Other OT
j .: " B 0 I 0 " 0
i ~ ~ i " Q_
w a w a ~
" ~ X w ii' ~ ~ ~ " < " "'
COLLECTED
COMPOSITE
START
DATE TIME
COMPOSITE
END/GRAB
DATE TIME
"" "' w z ~ z 8
~ 0
"
Preservatives ?~1t.#fit, .:.lt.
Pace Project No./ Lab I.D.
1, 57)<'. 3./
-<'r-,< 3. 2-
fi.. ~
I< } l-.:+'"'-L'--=--=---'-''-------------i"":+::;:+---+--l-,;.::,~/:..::,:ll/.+------l""'-4-/:=:.+.,,-+++--a--+---l--4---< ,,;ii I " r v . l ltJ ( i ~i-:---t-:-t:--t-+-+-,rt---t---t-t-+-ft.:.._t-_______ --"i~,<(;1<.-i
-,-L',,=-~'=-------------t'-.--1-<'+--l---t--,'H--++P:1,++-H++H---1!(:~l l-,_,.' i--2'
3 -< 1"k'. :J , 3
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6, .5,/<. 3. (.,
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1 I, bll-.... ~ --"-lr--""--=___,c_.:.e:: __________ --lH'-+-++---+--+-+---le----l,+-1-"(,'-+--l---l---l--+-+-+-+-J ~A I d '-,_,,
~t--~~~~~------------+-++-1---t---+---+-l-'-+---++t-(,~t-+-+-+--+-+---I-Hi L, i.,, lJ.r
I '-I ,_, I.., ...
7 Co.A../ e::, J./ \ t--t-~~~,---=--::-----:--------tt---t--tt----t-------t~"<:---t---l-\-t-:----t---t---t-t-H-+-+--i&1
l-'-,f-----==--:=------==---=---'-----------+++-"'1--+-~+----1-1--+--l+-1-,Lf-+-+-+--a--+-+-+-lf"'l--:H-+~'-q...'---++-+-HH-+l+---------C(';,'~M~
t-=,1f------='--'--'-:...:,_-"---'---'=-------+.:.....+-----,f--+---+--'--(+---+-+3Y-+-+-+--a--+-+-+-l~HH--+=+,_....,=+-_..-+-+-+-H'-+--+-+------~\u'l.\'-I
t-'-t---------------------Jf--+-+---+-----J---+----+-l----l-l-t-++-+--+---l--lt~,t--t--t-t-+--+---1-t--t--t-t--t--+---1t-------------j
8 u,-./c 3. '2-{
,
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10 ~ rt--------------+-+-+--t------t---f---+--t---+-+++-H-+---t---J,;,,t--HH--+-+-+-+++++-+-+--------------l
'---",--------------------;--+-t----+---+------if----t-t--+-+-+---lf-t-+-t-J--l"~~".._+---1~+-+-t-+---1f-+-+-t-+---1f-+--------------J I. *' j2 •
/
-~~:t[¥.~1~~!~1~i~~~~:~t~~~~~Wt¥~Wt~~r~~~~~~l¾:~~ii:~r~:?
ORIGINAL PRINT Name of SAMPLER: /J /l,<J GE ~ ✓L£./
SIGNATURE of SAMPLER: ~~. ~ ,-,j-G.--~,7
"Important Not11: By signing this !om, you are accepbng Pace's NET 30 day p,aymont to,ms and agreeing to late ctwy'" of 1.5% per month for any invoices not paid within 30 days.
DATE Signed
(MM/DDIYY}: ot,/a./o1
SAMPLE CONDITIONS
IA J.}
l
F-ALL-O-020rev.07, 15-May-2007
,,....._,-
.,.,-·i ,f:J/ .
/ _ _,,PaceAnafytical Client Name_L~f_/?.,_.__ _____ _
~~1JwlrJR®:tl~@tf1D
Project #_q~,;..~lj_v~l/q_::;-_
C~urier: 0 Fed Ex O UPS O USPS ~t □rmercial [J Pace Other
Cus·tody Seal on Cooler/Box Pres~nt: 0 yes ~ no Seals intact: ·□ yes~
Packing Material: 0 Bubble Wrap 08ubble Bags D None Oother ez:-Thermometer Used 0 Type of Ice· Blue None Samples on ice, cooling process has...beoun
Cooler Temperature· lZ f Biological ssue is Frozen: Yes No NIA Date and !n~iaJ_o~~ers~g
contents: ./1/
T 60
Temp should be above freezing to 6°C , Comments: • / _/
Chain of Custody Present: ~e.,i □No 0NtA 1.
Chain of Custody Filled Out: 6e;,-□No □NIA 2.
Chain of Custody Relinquished: ~es 0No 0NIA 3.
Sampler Name & Signature on COC: G?¼s □No □NIA 4.
Samples Arrived within Hold Time: ~es □No □NIA 5
Short Hold Time Analysis (<72hr): □Yes efNo □NIA 6.
Rush Turn Around Time Requested· □Ye; ~o □NIA 7.
Sufficient Volume: efv~s 0No □NIA B
Correct Containers Used: z □No ON/A 9
-Pace Containers Used: Yes 0No· □NIA
Containers Intact: ~es 0No □NIA 10.
Filtered volume received for Dissolved tests □Ye~ ONo ~/A 11.
Sample Labels match COC: eftes □No □NIA 12.
-Includes date/time/ID/Analysis Matrix: SL All containers needing preservation have been checked.
Yes 0No □NIA 13
All containers needinQ preservation are found to be in ~' □No □NIA compliance with EPA recommen·dation. -exceplions: VOA, coliform. TOG, O&G, WI-ORO (water) OYes 0No , Initial when completed
Samples checked for dechlorination:· □Yes □No ~IA 14.
Headspace in VOA Vials ( >6mm): OYes □No c;n{,1' 15.
Trip Blank Present: □Yes 0No z 16.
Trip Blank Custody Seals Present □Yes 0No NIA
Pace Trip Blank Lot# (if purchased): NIA
Client Notification/ Resolution: Field Data Required? Y / N / NIA Person Contacted; 0ateffime: ---------------Comments/ Resolution: --------------------------------------
Project Manager Review: llilF
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ( i.e out of hold. incorrect preservative, out of temp, incorrect containers)