NCD991278953_19951001_National Starch & Chemical Corp._FRBCERCLA LTRA_Quarterly Report - Third Quarter 1995 OU-1 and OU-2-OCR

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Quarterly Report
Third Quarter 1995
Operable Units No. 1 and 2
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDN
Environmental Data Management, Inc.
Chapel Hill, NC
October 1995
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Quarterly Report
Third Quarter 1995
Operable Units No. 1 and 2
(ri)f?llll
CT 2 7 19
~~u V
IPA -REGION IV
/,TLANTA, GA
National Starch and Chemical Company Site
Cedar Springs Road
Salisbury, North Carolina
Prepared By:
EDII
Environmental Data Management, Inc.
Chapel Hill, NC
October 1995
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Table of Contents
1.0 Groundwater Monitoring Activities for the Third Quarter 1995 ..
2.0 Planned Groundwater Monitoring Activities .
3. 0 References ........ .
Appendix -Certificates of Analysis
Appendix A -Report of Laboratory Analysis
Appendix B -Sample Delivery Group Narrative
Appendix C -Volatile Organics Analysis Data Sheets
Appendix D -Semivolatile Organics Analysis Data Sheets
Appendix E -Inorganics Analysis Data Sheets
Appendix F -Chain-of-Custody Records
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List offables
Table Title
List of Sample Analysis and Water Level Monitoring Performed
2 ROD (OU!) Contaminants and Selected Water Quality Parameters in
Groundwater, Third Quarter 1995,. Operable Unit No. I
3 ROD (OU2) Contaminants and Selected Water Quality Parameters in
Groundwater, Third Quarter 1995, Operable Unit No. 2
4 Groundwater Cleanup Criteria, Operable Unit No. 1
5 Water Level Measurements, Third Quarter 1995, Operable Unit No. I
6 Water Level Measurements, Third Quarter 1995, Operable Unit No. 2
List of Figures
Figure
1 Site Map
2
3
4
5
6
Quarterly Summary of Acetone
Quarterly Summary of 1,2-Dichloroethane
Quarterly Summary of 1,2-Dichloropropane
Quarterly Summary ofBis(2-chloroethyl)ether
Groundwater Contour Map for July 10, 1995
I Environmental Dota Management, Inc.
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1.0 Groundwater Monitoring Activities for Third Quarter 1995
This report for the third quarter of I 995 presents the findings from the groundwater
monitoring conducted at Operable Units No. I and 2 at the National Starch and Chemical
Company site on Cedar Springs Road, Salisbury, North Carolina. This report is prepared
in accordance with Record of Decisions (ROD) issued by the U.S. EPA on September 30,
1988 for Operable Unit No. I (OU!) and on September 30, 1990 for Operable Unit No. 2
(OU2). Operable Unit No. I consists of contaminated groundwater area located in the
east-southeast portion of the facility. Operable Unit No. 2 consists of contaminated soils
and surface water/sediments in tributaries surrounding a trench area east of the plant
operation area.
Operable Unit No. 1
Groundwater samples from the four downgradient groundwater monitoring wells (NS29,
NS30, NS31, and NS32) and four bedrock extraction wells (EX0I, EX02, EX03, and
EX04) were collected on July I 0-11, 1995. All samples were analyzed for Target
Compound List (TCL) volatile and semivolatile organic compounds (VOC and SVOC),
Target Analyte List (T AL) metals, and general chemistry. In addition, samples from the
monitoring wells and extraction wells were analyzed for selected water quality parameters
to monitor influent loadings for the Combined Pretreatment System (CPS). A sample
analysis summary is provided in Table I. The samples were collected in accordance with
U.S. EPA (Region IV) protocols. The TCL and TAL compounds were analyzed
supporting U.S. EPA Level IV Contract Laboratory Program (CPL) protocol.
All four plume periphery extraction wells were operational. The trench area extraction
wells were not operational because of the RCRA closure of Lagoon No.2.
Results from the chemical analysis for Operable Unit No. I and Operable Unit No. 2 are
presented in Tables 2 and 3, respectively. The list of compounds presented in these tables
represents the contaminants specified in Operable Unit No. I Record of Decision (ROD).
The list of designated compounds from the ROD (OU!) and associated cleanup levels are
provided in Table 4. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
The results ofthis quarters sampling indicatt:d that four organic compounds, acetone, 1,2-
dichloroethane ( 1,2-DCA), 1-2-dichloropropane ( 1,2-DCP), and bis(2-chloroethyl)ether
exhibited levels that exceeded cleanup levels (shaded bold faced values in Table 2). The
acetone levels decreased from the previous quarter in three of the four extraction wells
(EX0I, EX02, EX03) and increased in EX04
Also, acetone levels exceeded cleanup standard in monitoring wells NS29 and NS30. The
level of acetone in NS29 marks a significant increase over the previous quarter sampling.
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In addition, levels of 1,2-DCA and 1,2-DCP also increased in wells NS29 and NS30 over
the previous quarter sampling. The elevated VOC levels in wells NS29 and NS30 are
most likely attributed to the fact that extraction well EX02 was experiencing pump
problems during the startup phase of the groundwater recovery program. The pump in
well EX02 has been repaired and is currently pumping continuously. Previous quarterly
reports have shown that contaminant concentrations have generally decreased over time in
wells NS29, NS30, and NS3 l. Monitoring well NS32 continues to show that no
contaminants are present.
Extraction well EX0 1 did not exceed the cleanup standards for any of the VOC
compounds. However since the first quarter 1995 sampling event, EX0l did exceed the
cleanup standard for bis(2-chloroethyl)ether (see Table 2).
The general trends for the four organic compounds that have exceeded the cleanup criteria
over the past four quarterly sampling events are presented in graphical form on Figures 2
through 5. These four organic compounds are acetone, 1,2-dichloroethane, 1,2-
dichloropropane, and bis(2-chloroethyl)ether.
Water level measurements were taken on July 10-11, 1995, from seventeen selected
monitoring wells, four extraction wells, and two stream gauges located in Operable Units
No. 1 and 2. The static water level for NS32 was not measured, due to artesian
conditions. Well NS32 has been under artesian conditions during all previous sampling
events. The results of the water level measurements are presented in Table 5. Figure 6
presents a groundwater contour map of the subject area.
During the past quarter, all of the plume periphery extraction wells increased their
pumping capacity. The combined average quarterly pumping rate for the four extraction
wells (EX0 1, EX02, EX03 and EX04) increased from about 3 5 gpm for the first quarter
1995 to about 80 gpm during the second quarter 1995. The efficiency of the plume control
and hydraulic control will be evaluated in more detail after all trench area extraction wells
are fully operating.
Operable Unit No. 2
Groundwater samples were collected from monitoring wells NS09, NSl0, NS! 1, and
NS15 on July 10, 1995. All samples were analyzed for selected TCL VOCs and SVOCs,
T AL metals, total dissolved solids (TDS), and chloride. A sample analysis summary is
provided in Table 1. The samples were collected in accordance with U.S. EPA (Region
IV) protocol. The TCL and TAL· compounds were analyzed under U.S. EPA Level IV
CLP protocol.
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Results from the chemical analysis for Operable Unit No. 2 are presented in Table 3. The
list of compounds presented in Table 3 represents the contaminants specified in Operable
Unit No. I ROD. The list of compounds from the ROD and associated cleanup levels are
provided in Table 4. Figure I is a site map showing the well locations. The certificates of
analysis are provided in the Appendix.
All four monitoring wells (NS09, NSI0, NS! I, and NS15) in Operable Unit No. 2 had
compounds that exceeded the cleanup standards (See Table 3). The concentration of
acetone in well NS09 declined below the cleanup standard. Monitoring well NS 11 slightly
exceeded the standard for 1,2-DCA, but previously had no compounds to exceed the
standard. Vinyl chloride exceeded the cleanup standard in wells NS09 and NS 15.
Monitoring well NS09 continues to exhibit the most number of contaminants in a single
well to exceed the cleanup standard. They are 1,2-DCA, 1,1-DCE, vinyl chloride, barium
and manganese.
As with the first and second quarter 1995 sampling, manganese exceeded clean up levels
in three monitoring wells (NS09, NS I 0, and NS I 5). Monitoring well NS 11 continues to
have manganese concentrations below the cleanup standard.
Water level measurements were taken on July 10, 1995 from each of the four monitoring
wells. The results are provided in Table 6. A groundwater contour map of the subject
area is provided in Figure 6.
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2.0 Planned Groundwater Monitoring Activities
Operable Unit No. 1
Groundwater monitoring will continue. Due to the increased concentrations of acetone,
1,2-DCA, 1,2-DCP, and Bis(2-chloroethyl)ether in wells NS29 and NS3 l EX02, care will
be taken to closely monitor the daily pumping rates of the extraction well system.
Particular attention will made to assure that all plume periphery extraction wells continue
to pump at optimum efficiency and that downtime for pump maintenance is minimized.
The implementation of the extraction well system will continue as planned with the
continued operation of the plume periphery extraction wells EX0 1, EX02, EX03, and
EX04.
Because of the high concentrations of acetone, 1,2-DCA, and 1,2-DCP in the
groundwater samples obtained from some of the extraction and monitoring wells National
Starch and Chemical Company will continue to alert laboratory personnel of samples from
wells with known high VOC concentrations.
Operable Unit No. 2
Groundwater monitoring will continue. Like the groundwater samples from the wells in
Operable Unit One, the samples from monitoring well NS IO contains high concentrations
of 1,2-DCA. Therefore, the analytical procedure for VOC analysis will be modified when
analyzing the sample from well NS IO. The procedure modification will ensure greater
accuracy in the VOC analytical results.
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3. References
EDM, Inc., August 1995, "Quarterly Report -Second Quarter 1995 Operable Units
No. 1 & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, May 1995 , "Quarterly Report -First Quarter 1995 Operable Units
No. 1 & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, February 1995,"Quarterly Report -Fourth Quarter 1994 Operable Units
No. 1 & 2", National Starch and Chemical Company, Salisbury, NC.
IT Corporation, October 1994,"Quarterly Report -Third Quarter 1994 Operable Units
No. 1 & 2", National Starch and Chemical Company, Salisbury, NC.
North Carolina Environmental Management Commission, North Carolina Administrative
Code: 15A NCAC Subchapter 2L (August 1993).
U.S. EPA, September 30, 1990, Record of Decision (ROD) for Operable Unit No 2,
National Starch and Chemical Company, Salisbury, NC.
U.S. EPA, September 30, 1988, Record of Decision (ROD) for Operable Unit No 1,
National Starch and Chemical Company, Salisbury, NC.
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- - - ---------- -- - - -Table 1
List of Sample Analysis and Water Level Monitoring Performed
Third Quarter 1995
Operable Units No. 1 and 2
National Starch and Chemical Company
Well Number TCL
Well Tvoe• VOCs0
Ooerable Unit No. 2
NS09 X
Salisbury, North Carolina
TCL
SVOCs0
TAL
Metals0 TDSC
X
Chloride
• SM --~ X
X
X
X
X
X
X
X
·······-······-·· X
X
X
X
........................
NS10
NS11
NS15
. SM ,·
SM
BE
X
X
X
X
X
X
•sE = Bedrock extraction well, BM = Bedrock monitonng well, SM -Saprohte (shallow) momtonng well
bProject TCL consisting of 13 VOCs, 2 SVOCs, and 9 metals, and meets Operable Unit No. 1 cleanup criteria (Table 4).
cTDS -Total dissolved solids
dCOD -Chemical oxygen demand
eTKN -Total Kjeldahl nitrogen
1 Iron pins in southwest tributary for monitoring stream elevations.
gNA -Not Applicable
CODd
X
X
TKN•
Water
Level
X
X ....
X
X
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Table 2
ROD (OU1 l Contaminants and Selected
Water Quality Parameters in Groundwater
Third Quarter 1995
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Extraction Wells Monitorino Wells
Well Number: EX01 EX02 I EX0J EX04
1110195 I 1111195 I 1110195
NS29 NSJO I NS31 I NS32
Sample Date: 7110195 1110195 1110195 I 7/10/95 I 7/10/95
Volatile Or!lanics (u!l/1)
32, 6500E; 10 U Acetone 70 j 32000 E , 1400 E 2200 E ' 35000 E;
Benzene SU! 250U' 17Ui 17U! 250Ui ···-----·· -------
Bromocti.~~~?~0-~-~~~-~~-·_:::~~:~.:~·~:Q.°~_'~:-_·_-·2~·-:~·; :·.:·. 17 u \·-17 u ; 2so·U [
Chloroform 5 Ui 250 Ui i·iui··· 17 Ui 250 U
5U• 32 U 5U · su' 32 U 5U
SU! 32 U 5U
....... 1.:3:IJ.i.C.hl~roethane 3 J · 570' 10 J j 17 U
I>---.. -... -.. -.-.... -. 1, 1 :IJichlo'.°."t~~ene 7 U 350 U 23 U ! 23 Uj 350 U
....... 1,2•Dichloropropane _. ___ 6_LJ_ ......... 890 ·. · ..... :)~ ........ 2.6.' ··· 1000
Ethylbenzene 10 U 500 U i 33 U 33 U , 500 U
690 5U! ·120 5U
7 U' 45 Ul 7U
5u; 260 6U
1ou' 65 U 10 U
Methylene Chloride 5 U 250 U ' 17 U 17U! 250 Uj 5Ui 32 U 5U
Toluene 10 U 280 J' 32 J 31 J! 200 J 10U 45 Ji 10 U
5Ui 250U! ······-·· · ···TriChioroethe·ne -·--·--··s··ur·· 2so·ur··
·············-······-········ 1, 1,2-Trichloroethane 17 U 1iu'· 250 U
17 U 17 U[ 250 U
5 U! 32 U 5U
5U! 32 U 5U
Vinyl Chloride 2 U I 100 U i 7U 7Uf 100 U 2Ui 13 U 2U
Xylene 10 U ! 500 U ! 33 u: 33 u: soouj 10 U' 65 U! 10 U
Semivolatile Oraanic fua/ll
Bis (2:~~lo'.<>et~.~>. ~ther . 14 I 120! 64' ,iiiu( i"4iill'
450! ·soo·ui .. • 12
27U!
130i 6 U •·· 4-Nitrophenol ·········25·-c1[ 130U! 28U
lnoraanics (uall)
Arsenic
Barium
Beryllium
Cadmium
1.9 u,
61.4Bi.
0.32 Bi
1.2 U ...... ., .......... .
Chromium 3.1 U
2.8 s:
,1820'
0.30 u:
1.9 u:
265
0.30 U
1.9U• .. 2.2BJ.
52.68! 190Bj
0.30 U! 0.30 Uj
1.9 Ui
19.7 B!
0.30U•
1.2 U! 1.2 U 1.2 Ui .. 1:.?IJ[ 1.2 u: s:(EiT 3.4 a ii u"i 3 1 u; . iiU ........ ·....•. . .· ......
Manganese 117 -18300 ! 3970 3210; 611 1800!
Nickel 7.2U! 7.2U[ 7.2 U 7.2 U' 7.2 U 7.2 U!
1.9 U! ····I··
207!
0.30U'
1.2 Ui
3.1 U
35.7
7.2 U --------1----+----s----· ······-·······-·· .............. ·-······-~--
Selenium 1.7 U i 1.8 8' 1.7 U 1.7 U;
Zinc 43.6! 2.6Ui 2.6U! 4.08!
3.08 2.08' .. 2.s-c;1 ·· ···-rs"t.1·i ·· 2.7 8
2.6 U
Water Quality (m!l/1)
2.3 8
89.7
0.30 U
1.2 U
3.1 U
107
7.2 U
2.0 8
2.6 U
··············C_<:l.□ ND 1100, 100! 100! NIA! NIA! ... Nl~L NIA Chloride 50 ... ··1·100[ ·--···200!"·-·-·130 -·-.... 400(-74! 1601 8.9
11---------'-----'-f--_;_+---.,-;---'---+--'='-----'·····'--..;_;_~-=:......--=:.::11
11 ________ N_rtr_og.,,__en_(T'-=K~N-'-)I --~N~□+-=4~.2,.;! __ ~1~.4.;j __ .:.0 . .:.9.:.! __ N.:..IA""-! _ _;_N.:../A-"-i _ _;_N.:../A.:.!!------'NIA
TDS 380i 3300! 1100j 740! 16001 480' 880! 230
Note Data Qualifier Definitions:
B !Organica) = Compound was detected in the associated blank.
B (lnorganics) = Compound concentration is below the contract-required detection limit.
J = Compound concentration is an estimate. Either the compound was positively
identified at a trace value, or it is a nontarget for which no calibration wes performed.
U = Compound was analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
mass spectrometry instrument.
ND= Not detected at or above the detection timit of anatyaia method.
NA= Not analyzed.
Also Note: Shaded bold face data indicates a detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9·30-88).
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Table 3
ROD (OU 1) Contaminants and Selected
Water Quality Parameters in Groundwater
Third Quarter 1995
Operable Unit No. 2
National Starch and Chemical Company
Salisbury, North Carolina
Monitorino Wells
Well Number: NS09 l NS10 I NS11 I
Sample Date: 1110195 I 1110195 I 111019s I
Volatile Oraanics lua/ll
Acetone 250 El
Benzene 5 Ui
Bromodichloromethane 5 U : ----················-· -·-····----··· ···-····-Chloroform 5 U !
1,2-Dichloroethane · ·11:"
170U)
83 u:
83 u:
83 u:
7800 E'
1, 1-Dichloroethylene ···········-·1 ·,'2~0iChiOropropaOe ······· -Etti~iienzen•
9! 120 u: ······· ·su: .... ·1oou:
Methylene Chloride
Toluene
1, 1,2-Trichloroethane
130
.. ., .. ; .. -
170U\
83 u:
170U'
83U\ -------------------················-··-· ··-··-·····--·-··-·-·····-···········-·-·-····· Trichloroethene 5 u j 83 u \
Vinyl Chloride 1 .... · ·. 81 I 33 U [ 11---------==:.:x.::.yt::e:.:n::e~:.....-~ 15~, ----'11"0-u'-'-j --
Semivolatile Oraanic lua/11
........ Bi~.\2:C:hl?roel~yl).E'lher ................. 28 .. U.!
4-Nitrophenol 140 U !
lnoraanics lua/ll
310 U'
1500U!
10 U.
5U
su·
su:
6
7U,
6U:
98 [
5U:
15'
5U:
5U.
2U'
661
6U;
28 u,
NS15
7110195
120
5U
5U
5U
250 E
7U
6U
10 U
5U
5J
5U
5U
4
10U
5U
27 U
2.2 B' 2.4 B 1.9 U
176 Bi 237' 387
Beryllium 0.30 U : 0.30 U' 0.55 B, 0.30 U
Cadmium 1.8 e: 1.2 u: 1.2 u 1.2 u ···········chrom;um 42:' s.10: s.20· 3.1 u
11 ________ _;M..;.•=n~g~a..;.nese=+·---'3"3::6~00~'~---~93:.:2~D-' ___ ·_·~2~,ie::'_'·_···_· __ 1~3400
9.4 Bl 20.6 Bl 12.0 B' 7.2 U Nickel
Selenium 2.0 B' 1.7 U: 3.6 B: ···--····· .. ··--··z1nc· ····················4e:f:t ········ ....... 1.,ie .. sr· ········· ··· ··41 .:if
Water Qualitv lmc/ll
COD NIA 250' rno: ...••••••... ··>··· ·• Chloride 1600: 590i 4.5
1.7 U
2.6 U
NIA
1100
NIA' NIA; _______ N_e_,og_,c_e_n.,.(T_K_N-'") ___ _;Ne.IA .. ' ____ _
TDS 3600[
..::.:cc._ __ _:_:NIA
1400! 320, 2400
Note Data Qualifier Definitions:
B (Organics) = Compound was detected in the auociated blank.
B Onorganics) = Compound concentration is below the contract-required detection limit.
J = Compound concentration is an estimate. Either the compound wes positively
identified at a trace value, or it is a nontarget for which no calibration was performed.
U = Compound was analyzed for but not detected at the listed concentration.
E = Compound concentration exceeds calibration range of the gas chromatography/
man spectrometry instrument.
ND = Not detected at or above the detection limit of analysis method.
NA= Not analyzed.
Also Note: Shaded bold face data indicates II detected concentration that exceeds
the Operable Unit One groundwater cleanup standard (US EPA 9-30-88).
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Table 4
Groundwater Cleanup Criteria
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Compound Cleanup Concentration (ug/1)
Volatile Organics
Acetone! 3500
Benzene! 5
Bromodichloromethane, 5 ····--···•··················•·······\····· Chlorotorn:ii 5
1,2-Dichloroethane(DCA)'-! --------'5'-----------II
1,1-Dichloroethylene! 7 ____ _
1,2-()ic:lllore>pre>panl:lj 6
. ........... .......... ........... E:thyl~eriz:ElnEl[ 3500
u _______ ...:M::ce::ct::..:hYlene Chlorider 5
Toluene, 2000
....... 1,1 .. 2~Tric:lllore>ethc1n.e (TGA) .. . 5
........ Trichloroethene (TCE) 5
_______ _::Vc:_:inxl Chloride 2
X~lene: 350
.. _·
...... E3is .. (2~CllloroElthyl).E:t11ElrL ....
4-Nitrochenol!
Arsenic!
Barium,
E3ElryllilJni ...
Cadmium ·············-········· ·-·-····· .......... ·········-Chromium
5
350
10
100~0------11
17.5
10
50
11 ___________ cc.M.c:ac:.cng,-=ac..nc=e-=s~e,_ _____ --'7'-'-700"--------1i
Nickel! 350 .... ,, .................... --·--··-·····;·"·•
Selenium I 10 ·················-·········•·f• Zinc, 7350
Reference: U.S. EPA, September 30, 1988, Record of Oec1s1on (ROD), Operable Unit No. 1,
National Starch end Chemical Company, Salisbury, North Carolina.
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Well Name
EX01
Table 5
Water Level Measurements
Third Quarter 1995
Operable Unit No. 1
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Date Reference (Ft. MSL) (Ft.)
7/10/95 ' TOC ! 731.85 ' 84.76 '
Water Level
Elevation
(Ft. MSL)
647.09
EX02 7/10/95 TOC . 718.24 60 . ....... ! ........ 658.24 ... ., .... """"""····--... -------EX03 7/11/95 ' TOC 740.46 75 ! 665.46 .. ·-······ ····-................... , ...... ......... . ........•..... .............. ... . ....
EX04 7/10/95 TOC 754.12 i . 84.23 669.89 ........... ·······--·· ··--·· .. . ............ ,
NS05 7/10/95 TOC 767.96 19.5 748.46
NS06 ' 7/10/95 TOC ' 738.87 7.2 731.67 ·•·-................. . ............
NS21 7/10/95 TOC 739.13 5.7 733.43 ....................... ,,,. •.•• y ... ............... ........ . ................ ·•·S•., . ., ············-•····· .. .. ······· ·-.. .. ······· ······· ...... ....
NS22 7/10/95 TOC ' 715.94 17 698.94 . . . ........ .. . . . ........ . ... ....... ..... .............................•....
NS23 ' 7/10/95 TOC 752.36 21.1 731.26
NS26 7/10/95 TOC 720.77 8.4 712.37 ....................
NS27 7/10/95 TOC 749.47 18.4 731.07 ... _,., .. ········•····· ·······-··-····•····· ......... ····-··-····· .. ., ... ........ ........ .......... ..
NS28 7/10/95 TOC 767.82 27.8 740.02 . , __ ... , ...... .. . ......... . .... . ...........
NS29 7/10/95 TOC 715.5 50.66 664.84
NS30 l 7/10/95 TOC 718.54 41.65 676.89 .......................
NS31 7/10/95 TOC 711.15 ' 40 . 671.15 ................... , ..... ··•·•·••·········•··· ·····························-·.·-·•·-...........................
NA•
.... N1>t . ........
NS32 7/10/95 TOC 699.48 ' --·-------.................... .......... _ ... ........ ........... .. ...... ...... .. .......... ...... .. ..... NA' .. .... NA" P01 7/10/95 TOC 708.09 i j
SG1 7/10/95 TOC 712.26 0 712.26 ....•. ....... ··········-SG2 7/10/95 TOC 693.9 0.17 693.73 • NA -Not Apphcable, well is artesian.
NAb -Not Applicable, well is dry, or stream level not measured.
I
I
g
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Environmental Data Management, Inc.
Table 6
Water Level Measurements
Third Quarter 1995
Operable Unit No. 2
National Starch and Chemical Company
Salisbury, North Carolina
Reference
Point Depth to
Measurement Point of Elevation Water
Well Name Date Reference (Ft. MSL) (Ft.)
NS09 i 7/10/95 ' TOC 778.45 28.7 '
NS10 7/10/95 TOC 786.72 32.5
NS11 i 7/10/95 TOC 775.65 18.1 ··--........................ .......... -······· . .............. ···-······· .......... ·••· .............
NS15 7/10/95 i TOC 792.6 44.4 . NA -Not Applicable, well 1s artesian.
NAb • Not Applicable, well is dry, or stream level not measured.
Water Level
Elevation
(Ft. MSL)
749.75
754.22 ............
757.55 ---. 748.2
----

-
..
-+
GROUNDW.1.l[R MONnoRmG .f.R[,1, (sec ncuRE l'i)
for OPCR-.SLC UNnS 1 & 2
[]8CJ
-
Environmental Data Management, Inc.
--, --

-
-
National Starch & Chemical Company
Cedar Springs Road
Saltsbury, Morth Carolina
-----
: I I
+ Monitoring Well
-Roads, Buildings. etc.
Fence Line
t++++++ Railroad
-Property Line
Tributary Stream
-
-Tn -Topographic Contour Ltnc
(Ft., M5L) Contour lntervol • 5ft.
0 400 800 1200
1--;.1 l l
Scale in Feet
Scale 1 Inch = 800 Feet
Site Map
3rd Quarter Report 1995
For
Operable Units I & 2
-
- - -- ----------Figure 2
Quarterly Summary of Acetone Concentration
-----
40,000 ~--------------------------------------
35,000 -!---------
30,000
:::: 25,000 01 ::,
,5
C
0 ., 20,000 I!! .. C .. " C 0 15,000 (,)
10,000 +-------
5,000 +-------
EX01
EDN
Environmental Data Management, Inc.
October 1995
EX02
3,500 ug/1 Groundwater Cteanup Cone.
EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Unit No, 1
National Starch and Chemical Company
Salisbury, North Carolina
NS30
m Qtr4-'94
llD Qtr1-'95
1111 Qtr2-'95
■Qtr3-'95
NS31
Quarterly Report For
Operable Units No. 1 & 2
3rd Quarter 1995
- - - -- - ---- - - -Figure 3
Quarterly Summary of 1,2 Dichloroethane
100
::::
"' :,
C
C 0 .,
~ -C .. u C 0
0
10
EX01 EX02 EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
Note: Concentrations depicted at or below 5 ug/1 represent detection limit of laboratory
EDN
Environmenlal Data Management. Inc.
October 1995
National Starch and Chemical Company
Salisbury, North Carolina
--
NS30
-
NS31
- -
mQtr4-'94
IIIl Qtr1-'95
1111 Qtr2-'95
■Qtr3-'95
5 ug/1 -Cleanup
Concentration
Quarterly Report For
Operable Units No. 1 & 2
3rd Quarter 1995
-
--
~ ::,
C:
C:
0 ~ -C: .,
'-' C: 0 u
- -- -
EX01 EX02
--- - - --Figure 4
Quarterly Summary of 1,2 Dichloropropane
EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
Note: Concentrations depicted at or below 6 ug/1 represent detection limit of laboratory
EDN
Environmental Data Management, Inc.
Oclober 1995
National Starch and Chemical Company
Salisbury, North Carolina
--
NS30
-
NS31
--
I!! Qtr4-'94
11D Qtr1-'95
II Qtr2-'95
■Qtr3-'95
Quarterly Report For
Operable Units No. 1 & 2
3rd Quarter 1995
-
- - ---------------Figure 5 - -
1,000
100
e:: c:11 ::,
C
C 0 .,
I! -C .,
u
C 0 u
10
1
EX01
EDN
Environmental Data Management, Inc.
October 1995
EX02
Quarterly Summary of Bis(2-chloroethyl)ether
EX03 EX04 NS29
Monitoring and Extraction Wells -Operable Units No. 1
National Starch and Chemical Company
Salisbury, North Carolina
NS30
l!!l Qtr4-'94
IIll Qtr1-'95
1111 Qtr2-'95
■Qtr3-'95
5ug/l
-Cleanup Concentration
NS31
Quarterly Report For
Operable Units No. 1 & 2
3rd Quarter 1995
__ _,_.., __ _
(
+
0 200 400 800 ~-! !
Scale in Feet
Scale 1 Inch = 400 Feel
Legend
Roads, Buildings, etc.
Fence Line
-· · -Property Line
-Tributary Stream
-725-Groundwater Contour Line !Ft. MSLl + Monitoring Well
v Stream Gauge
'v
Stream I
( Gauge #1 I
\ I
National Starch & Chemical Company
Cedar Springs !Road
Salisbury, North Carolina
Environmental Data Management, Inc.
NS09
NS!5 +
PLANT AREA
Q[ l]
Figure 6
/ I
Groundwater Contour Map
for July 10, 1995
3rd Quarter Report 1995
For
Operable Units I & 2
I
I
I ,,
II)
I
I
I
I
I
I
'I
11
I
11
I
I
I
I
Appendix A
Report of Laboratory Analysis
I
I
I
I
·1
I
I
I
II
,I'
,I
I.
I .,
ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
August 01, 1995
Mr. Ken Kluttz
National Starch & Chemical Company
P.O. Box 399
Salisbury, NC 28144
RE: PACE Project No. 650711.507
Client Reference: Quarterly Monitoring -CLP
Dear Mr. Kluttz:
Enclosed is the report of laboratory analyses for samples received
July 11, 1995.
Footnotes are given at the end of the report.
If you have any questions concerning this report, please feel free
to contact us.
Sincerely,
Kris H. Kommalan
Project Manager
Enclosures
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: 704-ll75-9092
FAX: [phone]
An Equal Opportunity Employer
(wlij
ENVIRONMENTAL LABORATORIES
National Starch & Chemical Company
P.O. Box 399
Salisbury, NC 2B144
Attn: Mr. Ken Kluttz
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
I
Client Reference: Quarterly Monitoring -CLP
"
" I
I
I
PACE Sample Number:
Date Co 11 ected:
Ti me Co 11 ected:
Date Received:
Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
. Target Analyte List -Inorganics Ii
I
i
'I
' I,
' I
I
I
i ,,
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List
Target Compounds List
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
-Semivolatiles
-Volatiles
Units
mg/L
mg/L
MDL
1.0
1
92 0431898
07/10/95
11 :50
07/11/95
NS-32 ____ METHOD DATE ANALYZED
8.9
230
071395
071795
071995
407B
160.l
CLP, EPA
CLP, EPA
CLP, EPA
07/13/95
07/14/95
07/13/95
07/17/95
07/19/95
An Equal Opportunity Employer .
:I
I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
.,· Mr. Ken Kluttz
Page 2 i Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
I. Time Collected:
Date Received:
Client Sample ID: I Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved -:I Target Analyte List -Inorganics
•' ,, ,,
I
·1,
Ji
I
t
I
I
I ,,·
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -
Target Compounds List -
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Semivolatiles
Volatiles
Units
mg/L
mg/L
MDL
1.0
1
August 01, 1995
PACE Project Number: 650711507
92 0431901
07/10/95
14:00
07 /11/95
NS-15
----
1100
2400
071395
071795
071995
METHOD DATE ANALYZED
4078
160.l
CLP, EPA
CLP, EPA
CLP, EPA
07/13/95
07/14/95
07 /13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I
I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
,, Mr. Ken Kluttz
Page 3 1. Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
,I. Time Collected: Date Received:
Client Sample ID: .I• Parameter
INORGANIC ANALYSIS
' ,.
l
t
·1 ,,
I
.i
I
1:
i ,,
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
MDL
1.0
1
August 01, 1995
PACE Project Number: 650711507
92 0431910
07/10/95
14:15
07 /11/95
NS-09
----
1600
3600
071395
071795
071995
METHOD DATE ANALYZED
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
07/13/95
07/14/95
07 /13/95
07/17/95
07/19/95
An Equal Opportunity Employer
ENVIRONMENTAL LABORATORIES
,1 Mr. Ken Kluttz
Page 4
j, Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
,, Time Collected:
Date Received:
Client Sample ID:
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
92 0431928
07/10/95
14:45
07/11/95
NS-10 I Parameter Units MDL METHOD DATE ANALYZED
INORGANIC ANALYSIS ·Ii INDIVIDUAL PARAMETERS Chemical Oxygen Demand
Chloride i Solids, Total Dissolved 'I Target Analyte List -Inorganics
:Ii
t·
.'. ... I
I
I·
I
II
j ,,
I
I
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
mg/L
mg/L
mg/L
10
1.0
1
----
250
590
1400
071395
071795
071995
8000
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
07/19/95
07/13/95
07 /14/95
07/13/95
07/17/95
07 /19/95
An Equal Opportunity Employer
I
l ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
•.I Mr. Ken Kluttz Page 5
,, Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
,, Time Collected:
Date Received:
Client Sample ID: Ii Parameter
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Solids, Total Dissolved
l
:I. Target Analyte List -Inorganics
I' ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -
,, Target Compounds Li st -
I
1: ,,
II
I,
' 11
I
I
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: 704•875•9091
Semivolatiles
Volatiles
Units
mg/L
mg/L
mg/L
MDL
10
1.0
1
August 01, 1995
PACE Project Number: 650711507
92 0431936
07 /10/95
15:00
07 /11/95
NS-11
____ METHOD DATE ANALYZED
180
4.5
320
071395
071795
071995
8000
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
07/28/95
07/13/95
07 /14/95
07 /13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I
1· ENVIRONMENTAL LABORATORIES
I. Mr. Ken Kluttz
Page 6
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
t
l
:g,
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Time Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
·1· INDIVIDUAL PARAMETERS
., Chloride
Solids, Total Dissolved I Target Analyte List -Inorganics
ORGANIC ANALYSIS
I,
I
i
-,,
I
I
.I·
I, ,,
I
I
INDIVIDUAL PARAMETERS
Target Compounds List -
Target Compounds List -
l-,
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Semivolatiles
Volatiles
Units
mg/L
mg/L
MDL
1.0
1
92 0431944
07/10/95
I5:30
07 /11/95
NS-31
----
160
880
071395
071795
071995
METHOD DATE ANALYZED
4078
160.I
CLP, EPA
CLP, EPA
CLP, EPA
07/13/95
07/14/95
07 /13/95
07 /17 /95
07/19/95
An Equal Opportunity Employer
I
I,
1
ENVIRONMENTAL LABORATORIES
Mr. Ken Kluttz
Page 7 I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
,,-Date Received:
Client Sample ID:
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
92 0431952
07 /10/95
07 /11/95
NS-29
Parameter Units MDL METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved
Target Analyte List -Inorganics
ORGANIC ANALYSIS
-INDIVIDUAL PARAMETERS I Target Compounds List -Semivolatiles
Target Compounds List -Volatiles ,,
,,
I
I
'I
I,
I
,1 ,,
I
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL1 7=75-9092
FAX: [phone]
mg/L
mg/L
1.0
l
----
400
1600
071395
071795
071995
407B
160.l
CLP, EPA
CLP, EPA
CLP, EPA
07/13/95
07/14/95
07/13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I Bl I ENVIRONMENTAL LABORATORIES
'I· Mr. Ken Kluttz Page 8
REPORT OF LABORATORY ANALYSIS
August OJ, 1995
PACE Project Number: 650711507
I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
.,··. Ti me Co 11 ected:
Date Received:
Client Sample ID: 'I, Parameter
INORGANIC ANALYSIS ,, INDIVIDUAL PARAMETERS
Chloride
Solids, Total Dissolved I
I
I
Target Analyte List -Inorganics
I
I,
I,
·1
I
I
I
I:
I
ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -
Target Compounds List -
9800 Kincey Avenue, Sui le 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Semivolatiles
Volatiles
Units
mg/L
mg/L
MDL
1.0
I
92 0431960
07/10/95
18:30
07/11/95
NS-30
----
74
480
071395
071795
071995
METHOD DATE ANALYZED
407B
160.1
CLP, EPA
CLP, EPA
CLP, EPA
07/13/95
07 /14/95
07/13/95
07 /17 /95
07/19/95
An Equal Opportunity Employer
I
I ENVIRONMENTAL LABORATORIES
·1; Mr. Ken Kluttz
Page 9 :I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected: I Time Collected:
Date Received:
Client Sample ID:
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
92 0431979
07/10/95
19:00
07 /11/95
EX-01 I Parameter Units MDL METHOD DATE ANALYZED
INORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
I Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
I ORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
I
·1
I
I
I
I
i
I
9800 Kincey Avenue, Suite 100
I Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
mg/L
mg/L
mg/L
mg/L
10
1.0
0.5
l
----
ND
50
ND
380
071395
071795
071995
8000
407B
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
07/28/95
07/13/95
07/27/95
07/14/95
07 /13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I
I ENVIRONMENTAL LABORATORIES
I Mr. Ken Kluttz
Page 10
I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected: I Time Collected:
Date Received:
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
92 0431987
07/10/95
19:15
07/11/95
EX-02 Client Sample ID:
,,, Parameter Units MDL ____ METHOD DATE ANALYZED
I
I
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Chemical Oxygen Demand
Chloride
Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics I ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
·•-Target Compounds List -Semivolatiles Target Compounds List -Volatiles
I
I
I
I
I
I
I
' I
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
mg/L
mg/L
mg/L
mg/L
10
1.0
0.5
1
1100
1100
4.2
3300
071395
071795
071995
8000
407B
351.3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
07/28/95
07 /13/95
07/27/95
07/14/95
07/13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I
I ENVIRONMENTAL LABORATORIES
1. Mr. Ken Kluttz
Page 11
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
I
I
I
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
Time Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
, Chemical Oxygen Demand
Chloride
I., Nitrogen, Kjeldahl
Solids, Total Dissolved
Target Analyte List -Inorganics
I ORGANIC ANALYSIS
I
I
I
I
I! ,,
I
I
I
I
INDIVIDUAL PARAMETERS
Target Compounds List -Semivolatiles
Target Compounds List -Volatiles
9800 Kincey Avenue, Suite 100
Huntersvil!e, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
MDL
10
1.0
0.5
I
92 0431995
07/10/95
19:30
07/11/95
EX-04
----
100
130
0.9
740
071395
071795
071995
METHOD DATE ANALYZED
8000
4078
351.3
160. l
CLP, EPA
CLP, EPA
CLP, EPA
07/28/95
07/13/95
07/27/95
07/14/95
07/13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I
I ENVIRONMENTAL LABORATORIES
·1· Mr. Ken Kluttz Page 12
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
I
I
Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected:
Time Co 11 ected:
Date Received:
Client Sample ID: I Parameter
INORGANIC ANALYSIS
I INDIVIDUAL PARAMETERS
· Chemical Oxygen Demand
Chloride
I Nitrogen, Kjeldahl
. Solids, Total Dissolved
Target Analyte List -Inorganics
I ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
I. Target Compounds List -Semivolatiles
! Target Compounds List -Volatiles
I
I
I
I
I
I
I
I
I
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Units
mg/L
mg/L
mg/L
mg/L
MDL
10
1.0
0.5
I
92 0432002
07/11/95
10:00
07 /11/95
EX-03
____ METHOD DATE ANALYZED
100
200
]. 4
1100
071395
071795
071995
8000
407B
351. 3
160.1
CLP, EPA
CLP, EPA
CLP, EPA
07/28/95
07 /13/95
07/27/95
07/14/95
07/13/95
07/17/95
07/19/95
An Equal Opportunity Employer .
I
I ENVIRONMENTAL LABORATORIES
I-Mr. Ken Kluttz
Page 13
I Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Collected:
I Time Collected:
Date Received:
Client Sample ID:
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
92 0432010
07/11/95
10:05
07 /11/95
EX-03 I Parameter Units MDL MS METHOD DATE ANALYZED
INORGANIC ANALYSIS
INDIVIDUAL PARAMETERS I Target Analyte List -lnorganics
I ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
I Target Compounds List -
Target Compounds List -
Ii
I
I
I
I
I
I
I
I
I
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Semivolatiles
Volatiles
----
071395
071795
071995
CLP, EPA
CLP, EPA
CLP, EPA -
. 07/13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I
I ENVIRONMENTAL LABORATORIES
I·. Mr. Ken Kluttz Page 14
REPORT OF LABORATORY ANALYSIS
August 01, 1995
PACE Project Number: 650711507
I Client Reference: Quarterly Monitoring -CLP
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PACE Sample Number:
Date Collected:
Time Collected:
Date Received:
Client Sample ID:
Parameter
INORGANIC ANALYSIS
I·. INDIVIDUAL PARAMETERS Target Analyte List -Inorganics
I ORGANIC ANALYSIS
INDIVIDUAL PARAMETERS
Target Compounds List -I Target Compounds Li st -,.
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9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
Semivolatiles
Volatiles
Units MDL
92 0432029
07/11/95
10:10
07 /11/95
EX-03
MSD METHOD DATE ANALYZED
071395
071795
071995
CLP, EPA
CLP, EPA
CLP, EPA
07 /13/95
07/17/95
07/19/95
An Equal Opportunity Employer
I
I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
I Mr. Ken Kluttz
· Page 15
1 Client Reference: Quarterly Monitoring -CLP
PACE Sample Number:
Date Co 11 ected: I Time Collected:
Date Received:
Client Sample ID: I Parameter
ORGANIC ANALYSIS
Units
I INDIVIDUAL PARAMETERS
Target Compounds List -Volatiles
MDL
I These data have been reviewed and are approved for release.
~~
•· Charles M. Cabaniss
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Manager, Inorganic Chemistry
---ry, ., -+ ,}, i \ J I ' ~ ·''<1,,t(,,,_.uf y:'.:J ,---:; ['i . -I Margare~ S. ·H;rdi~g ,,. '-"•" ,.,.y,'\
Manager, Organic Chemistry
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9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: 704-ll75-9092
FAX: [phone]
August 01, 1995
PACE Project Number: 650711507
92 0432037
07 /11/95
10:10
07 /11/95
Trip Blank
----
071995
METHOD DATE ANALYZED
CLP, EPA 07/19/95
An Equal Opportunity Employer .
I
I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
I Mr. Ken Kluttz
Page . 16
FOOTNOTES
for pages 1 through 15
1 Client Reference: Quarterly Monitoring -CLP
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MDL
ND
Method Detection Limit
Not detected at or above the MDL.
9800 Kincey Avenue, Sui!e 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
August 01, 1995
PACE Project Number: 650711507
An Equal Opportunity Employer
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ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
Mr. Ken Kluttz
Page 17
QUALITY CONTROL DATA August 01, 1995
Client Reference: Quarterly Monitoring
Chemical Oxygen Demand
Batch: 92 38136
Samples: 92 0431928
METHOD BLANK ANO SAMPLE DUPLICATE:
Parameter
Chemical Oxygen Demand
LABORATORY CONTROL SAMPLE:
Parameter
Chemical Oxygen Demand
9800 Kincey Avenue, Suite 100
Huntersvi!le, NC 28078
TEL: [phone]
FAX: [phone]
-CLP
Units MDL
mg]L Io
Units MDL
mg/L To
PACE Project Number: 650711507
Duplicate
Method of
Blank 920427858 92 0427858 RPO
ND 420 420 0%
Reference
Value Recv
750 100%
An Equal Opportunity Employer
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I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA August 01, 1995 I Mr. Ken Kluttz
Page 18 PACE Project Number: 650711507
I Client Reference: Quarterly Monitoring -CLP
Chloride
Batch: I Samples:
92 37926
92 0431898,
92 0431944,
92 0431995,
92 0431901,
92 0431952,
92 0432002
92 0431910, 92 0431928, 92 0431936
92 0431960, 92 0431979, 92 0431987
I METHOD BLANK AND SAMPLE DUPLICATE:
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Parameter
Chloride
SPIKE:
Parameter
Chloride
LABORATORY CONTROL SAMPLE:
Parameter
Chloride
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: 704·875-9091
Units
mg/L
Units
iiig7L
Units
mg/L
MDL
1.0
MDL
1.0
MDL
1.0
Method
Blank
ND
Duplicate
920431898 of
NS-32 92 0431898 ~c'--"---8. 9 8. 9
920432002 Spike
Recv
100%
EX-03 Spike
200 10
Reference
Va 1 ue Recv
100 100%
An Equal Opportunity Employer
RPO
0%
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I ENVIRONMENTAL LABORATORIES
I Mr. Ken Kluttz
Page 19
REPORT OF LABORATORY ANALYSIS
QUALITY CONTROL DATA August 01, 1995
PACE Project Number: 650711507
I Client Reference: Quarterly Monitoring -CLP
Solids, Total Dissolved
Batch: 92 38088
I Samples: 92 0431898,
92 0431944,
92 0431995,
I METHOD BLANK:
92 0431901,
92 0431952,
92 0432002
I Parameter
Solids, Total Dissolved
I LABORATORY CONTROL SAMPLE:
I Parameter
Solids, Total Dissolved
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9800 Kincey Avenue, Suite 100
I Huntersville, NC 28078
TEL: 704-87&-9092
FAX: [phone]
92 0431910, 92 0431928, 92 0431936
92 0431960, 92 0431979, 92 0431987
Units
mg/L
Units
mg7L
MDL -1-
MDL -1-
Method
Blank
ND
Reference
Value Recv
100 Tio%
An Equal Opportunity Employer
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I ENVIRONMENTAL LABORATORIES REPORT OF LABORATORY ANALYSIS
I Mr. Ken Kluttz
. Page 20
FOOTNOTES
for pages 17 through 19
I Client Reference: Quarterly Monitoring -CLP
MDL
I ND
RPD
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Method Detection Limit
Not detected at or above the MDL.
Relative Percent Difference
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
TEL: [phone]
FAX: [phone]
August 01, 1995
PACE Project Number: 650711507
An Equal Opportunity Employer
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I Appendix B
I Sample Delivery Group Narrative
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THE ASSURANCE Of QUALITY
July 28, 1995
Mr. Ken Kluttz
National Starch & Chemical Company
485 Cedar Spring Road
Salisbury, NC 28144
SAMPLE DELIVERY GROUP NARRATIVE
Case: PCHAR
SDG: NAS08
Laboratory: PACE New England -New Hampshire Laboratory, Hampton, NH
Lab Numbers: 44609
Analytical Protocol: OLM01.8/ILM03.0 with modified target lists. Format A disk--
Form I sample data.
Samele Receiot: Samples for this SDG were received at PACE's Charlotte Laboratory
on July 11, 1995. They were forwarded by Federal Express carrier to PACE New
Hampshire for analysis. PACE New Hampshire laboratory sample numbers were assigned
as listed on the Sample Table which follows this narrative. Field sample identifiers
were modified to six-characters to accommodate CLP software requirements. The sample
table cross references the modified ID's with the field ID's. Although temperature
blanks were not included with the shipments, samples were received cool. Bottles and
labels matched the Chains-of-Custody (COC) provided. Details of sample delivery are
noted as follows:
The samples received at PACE New Hampshire on 7/12/95 were assigned PACE lab# 44609.
Samples were accompanied by coc documents. One VOA vial of sample "EX02" was
received empty. Both caps were cracked during shipment of the BNA aliquots of the
sample designated "NS-10 7-10-95". One of the bottles appeared to have lost about
SOmls of sample. No other problems were encountered with the shipment of these
samples. The sample designated on the COC for QC for this SDG was "EX03."
Volatiles Analvsis: Samples were analyzed within holding time under the CLP OLMOl.8
water method. In accordance with project requirements, the protocol was modified to
a target list of fourteen compounds with special detection limits. Nontarget
searches were not required. In addition, the client requested that samples needing
dilution be run a second time at lesser dilution to achieve lower detection limits.
Eight samples therefore have two sets of data reported. All samples except NSllXX
were determined to have pH< 2 at time of analysis.
Samples were run within compliant twelve-hour tune
calibration criteria for the compounds of interest.
target compound contamination.
windows. Standards met CLP
Method blanks were free of
Matrix spike analyses were conducted on sample EX03XX, which exhibited acceptable
accuracy and precision. Values reported on the Form III spike recovery sheet should
be considered accurate to two significant figures.
Internal standard areas were compliant for all analyses. Surrogate recoveries were
also compliant with the exception of high DCE recoveries in samples NSlOXX and
NS15XX. These samples had high 1,2-dichloroethane content which caused an
interference with the surrogate. Surrogate recoveries were ~~ceptable in the diluted
analyses of these two samples.
Samples EX02XX, EX03XX, EX04XX, NS09XX, NS29XX, and NS31XX required dilutions due to
P.O. Box 2130
One Lafayette Road
Hampton, NH 03842
TEL: 603-926-nn
B-1
An Equal Opportunity Employer
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THE ASSURANCE OF QUALITY
SDG Narrative
Case: PCHAR, SDG: NASOB
high acetone levels, Samples NSlOXX and NS15XX required dilutions due to high 1,2-
dichloroethane levels. Concentrations for these analytes exceeded the calibration
range ( "E" qualifier) in the lesser dilutions; results should be taken from the
secondary dilutions as necessary.
The reporting software caused the Form I sample data sheets to contain an extra
trailing zero in the mass/volume field. Volumes should be considered accurate to the
tenth of a milliliter.
Semivolatiles Analysis: Samples were extracted and analyzed within holding time
under the CLP OLMOl.B water method. In accordance with project requirements, the
protocol was modified to a target list of bis(2-chloroethyl)ether and 4-nitrophenol
with special detection limits. Nontarget searches were ~ct required.
Samples were analyzed within compliant DFTPP tuning
calibration criteria for the compounds of interest.
target compound contamination.
windows. Standards met CLP
The method blank was free of
Matrix spike analyses were conducted on sample EX04XX, which showed high recoveries
for 4-nitrophenol (105, 104% > 80%). This may have resulted from the use of
continuous liquid/liquid extractors which have higher statistical recovery windows
than those set for separatory funnels. In addition, the spikes were run at a four-
fold dilution due to high nontarget compound concentrations. No corrective action
was required for the high recoveries. Values reported on the Form III spike recovery
sheet should be considered accurate to two significant figures.
Some samples required dilutions due to high non target compound concentrations. These
dilutions were required in order to maintain instrument performance. Internal
standard areas and surrogate recoveries were compliant for all analyses. Surrogates
were diluted out of range for samples EX02XX, NSlOXX, and NS29XX,
The reporting software caused the Form I sample data sheets to contain an extra
trailing zero in the mass/volume field. Volumes should be considered accurate to the
milliliter.
Metals Analysis: The analytical protocol for metals analytes established for this
project was compliant with the EPA CLP SOW (Document Number ILM03.0) except as noted
below. Samples were analyzed within holding time for the client-designated target
list of nine metals (As, Ba, Be, Cd, Cr, Mn, Ni, Se, Zn). Matrix QC was performed
on sample EX03XX. Field ID' s were modified in order to satisfy a six-character
software requirement. The original ID's have been included as comments on the Form
I data sheets.
ICP Analysis: Samples were prepared in one water batch on 07/13/95. Analyses were
conducted in one sequence (07/13/95) on the TJAOl instrument for seven metals, and
in one sequence (07 /14/95) on the TJA02 instrument for arsenic and selenium.
standards and blanks met all compliance criteria. The spike recovery and duplicate
precision for sample EX03XX were acceptable. The laboratory control sample also
demonstrated acceptable accuracy. No difficulties were encountered during metals
analysis.
P.O. Box2130
One Lafayette Road
Hampton, NH 03842
TEL: [phone]
11-2
An Equal Opportunity Employer
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TIH ASSURANCE Of QUALITY
SDG Narrative
Case: PCHAR, SDG: NASOS
Statement of Compliancy and Data Authorization
I certify that this data package is in compliance with the terms and conditions of
the contract, both technically and for completeness, for other than the conditions
detailed above. Release of the data contained in this hardcopy data package and in
the computer-readable data submitted on floppy diskette has been authorized by the
Laboratory Manager or his designee, as verified by the following signature.
Richard Wellman, Operations Manager
PACE Incorporated, New England-New Hampshire
P.O. Box 2130
One Lafayette Road
Hampton, NH 03842
TU: 603-926-7777
c•v. i::n'l 0'11': -,i,-,(1
S-3
July 28, 1995
An Equal Opportunity Employer
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SAMPLE TABLE
CLIENT ID.
REPORTED AS MATRIX
------
NS-32
NS32XX WATER
NS-15
NS15XX WATER
NS15XXDL (VOA)
NS-09
NS09XX WATER
NS09XXDL (VOA)
NS-10
NSl0XX WATER
NSl0XXDL (VOA)
NS-11
NSllXX WATER
NS-31
NS31XX WATER
NS31XXDL (VOA)
NS-29
NS29XX WATER
NS29XXDL (VOA)
PACE#
----------
44609-001
44609-015
44609-028
44609-002
44609-016
44609-029
44609-003
44609-017
44609-030
44609-004
44609-018
44609-031
44609-005
44609-019
44609-032
PARAMETERS
----------
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, ~.n, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
44609-006 Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
44609-020 ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
44609-033 GC/MS VOA
44609-007 · Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
44609-021 ACID EXTRACTABLES
BASE/NEUTRP.L EXTRACTABLES
44609-034 GC/MS VOA
~,Q~t.
Ht u1u, .. ,1 Df auu11,
C-1
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SAMPLE TABLE
(CONTINUED)
CLIENT ID.
NS-30
EX-01
EX-02
EX-04
EX-03
TRIP
REPORTED AS MATRIX PACE#
NS30XX WATER
EX0lXX WATER
EX02XX WATER
EX02XXDL (VOA)
EX04XX WATER
EX04XXDL (VOA)
EX03XX (SQC) WATER
EX03XXDL (VOA)
BLANK
TBLK0l WATER
44609-008
44609-022
44609-035
44609-009
44609-023
44609-036
44609-010
44609-024
44609-037
44609-011
44609-025
44609-038
44609-012
44609-026
44609-039
44609-040
C -l..
PARAMETERS
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
Ba, Be, Cd, Cr, Mn, Ni, Zn,
As, Se
ACID EXTRACTABLES
BASE/NEUTRAL EXTRACTABLES
GC/MS VOA
GC/MS VOA
e,Q.~,.
1'1 UIUIUtl ~I U0111'
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Appendix C
Volatile Organics Analysis Data Sheets
I 1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
lb Name: PACE NEW ENGLA Contract:
EX01XX
Lab Code: Case No. PC HAR SAS No. SDG No. NAS08
ltrix: (soil/water) WATER Lab Sample ID: 44609-36
lmple wt/vol: 5.00 (g/mL) ML Lab File ID: C9429
Level: (low/med) LOW Date Received: 07/11/95
Date Analyzed: 07/19/95 ,~oisture: not dee.
GC Column: SP1DOO lil Extract Volume:
ID: 2.00 (mm) Oil.ution Factor: 1. 0
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( u L) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone ---------------75 -35 -4 - - - - - - - - -1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ____________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane ------78-87-5---------1 ,2-0ichloropropane ______ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1,2-Trichloroethane ____ _
71-43-2---------Benzene ---------------108 -88 - 3 - - - - - - - -Toluene ______________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
FORM I VOA
2
5
70
7
5
3
5
6
5
5
5
10
1 0
10
( u L)
Q
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u
u
u
u
u
3/90
I 1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
L. Name: PACE NEW ENGLA
EX02XX
Contract:
Lab Code: Case No.: PCHAR SAS No. : SDG No.: NAS08
irix: (soil./water) WATER
srpl.e wt/vol.: 5.00 (g/mL) ML
Level.: (l.ow/med) LOW
Lab Sampl.e ID:
Lab Fil.e ID:
Date Received:
Date Anal.yzed:
44609-37
C9430
07/11/95
07/19/95 +oisture: not dee.
GC Col.umn: SP1000
sl1 Extract Volume:
ID: 2.00 (mm) Dil.ution Factor: 50.0
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(uL) Soil. Al.iquot Vol.ume: (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L 6r ug/Kg) UG/L
75-01-4---------Vinyl. Chl.oride _________ _
75-09-2---------Methyl.ene Chl.oride ______ _
100
250
67-64-1---------Acetone 32000 --------------75 -35 - 4 - - - - - - - - -1 1 1-Dichloroethene ______ _ 350
67-66-3---------Chl.oroform ___________ _ 250
107-06-2--------1 ,2-Dichl.oroethane ______ _ 570
75-27-4---------Bromodichloromethane 250 ------78-87-5---------1 ,2-Dichl.oropropane _____ _ 890
79-01-6---------Trichloroethene ________ _ 250
79-00-5---------1,1,2-Trichloroethane ____ _ 250
71-43-2---------Benzene _____________ _ 250
108-88-3--------Tol.uene _____________ _ 280
100-41-4--------Ethyl.benzene __________ _ 500
1330-20-7-------Xyl.ene (total.) ________ _ 500
FORM I VOA
Q
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3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
tb Name: PACE NEW ENGLA
EX02XXDL
Contract:
Lab Code: Case No. PC HAR SAS No. : SDG No.: NAS08
Jtrix: (soil./water) WATER Lab Sampl.e ID: 44609-37DL
Lab Fil.e ID: C9412 lmpl.e wt/vol.:
Level.: (l.ow/med)
5.00 (g/mL) ML
LOW Date Received: 07/11/95
tMoisture: not dee.
GC Col.umn: SP1000
Date Anal.yzed: 07/18/95
ID: 2.00 (mm) Dilution Factor: 250.0
Extract Vol.ume: (uL) Soil. Al.iquot Vol.ume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl. Chl.oride ________ _ 500
75-09-2---------Methyl.ene Chl.oride ______ _ 1200
67-64-1---------Acetone _____________ _ 29000
75-35-4---------1 ,1-Dichloroethene ______ _ 1800
67-66-3---------Chl.oroform ___________ _ 1 200
107-06-2--------1,2-Dichl.oroethane ______ _ 1200
75-27-4---------Bromodichl.oromethane _____ _ 1200
78-87-5---------1 ,2-Dichloropropane _____ _ 1500
79-01-6---------Trichloroethene 1200 ---------79 -00 -5 - - - - - - - - -1, 1, 2 -Tri ch lo roe thane ____ _ 1200
71-43-2---------Benzene _____________ _ 1200
108-88-3--------Tol.uene _____________ _ 2500
100-41-4--------Ethyl.benzene __________ _ 2500
1330-20-7-------Xyl.ene (total.) _________ _ 2500
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FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
LI Name: PACE NEW ENGLA Contract:
EX03XX
Lab Code: Case No.: PCHAR SAS No. SDG No.: NAS08
Mir ix: (soil/water) WATER
srple wt/vol: 5.00 (g/mL) ML
Level: (low/med) LOW
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
44609-39
C9433
07/11/95
07/19/95 % •. oisture: not dee.
GC Column: SP1000
sl1 Extract Volume:
ID: 2.00 (mm) Dilution Factor: 3.3
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(uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
7
17
67-64-1---------Acetone _____________ _ 1400
75-35-4---------1 ,1-Dichloroethene ______ _ 23
67-66-3---------Chloroform ___________ _ 1 7
107-06-2--------1 ,2-Dichloroethane ______ _ 10
75-27-4---------Bromodichloromethane _____ _ 17
78-87-5---------1 ,2-Dichloropropane _____ _ 24
79-01-6---------Trichloroethene ________ _ 17
79-00-5---------1 ,1 ,2-Trichloroethane ____ _ 17
71-43-2---------Benzene _____________ _ 1 7
108-88-3--------Toluene _____________ _ 32
100-41-4--------Ethylbenzene __________ _ 33
1330-20-7-------Xylene (total) ________ _ 33
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FORM I VOA 3/90
I 1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
lb Name: PACE NEW ENGLA Contract:
EX03XXDL
Lab Code: Case No.: PCHAR SAS No. SDG No. : NAS08
ltr.ix: (soil/water) WATER
lmple wt/vol: 5.00 (g/mL) ML
Level: (low/med) LOW
Lab Sample ID:
Lab File ID:
Date Received:
Date Anal.yzed:
44609-39DL
C9432
07/11/95
07/19/95 IMoisture: not dee.
GC Column: SP1000
·~l Extract Volume:
ID: 2.00 (mm) Dil.ution Factor: 16.7
I
I
I
I
I
I
I
I
I
I
I
I
(uL) Soil Aliquot Volume: (UL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
33
83
67-64-1---------Acetone _____________ _ 2500
75-35-4---------1 1 1-Dichl.oroethene ______ _ 120
67-66-3---------Chloroform ___________ _ 83
107-06-2--------1 ,2-Dichloroethane ______ _ 83
75-27-4---------Bromodichloromethane _____ _ 83
78-87-5---------1 ,2-Dichl.oropropane _____ _ 100
79-01-6---------Trichloroethene ________ _ 83
79-00-5---------1 ,1 ,2-Trichloroethane ____ _ 83
71-43-2---------Benzene _____________ _ 83
108-88-3--------Toluene _____________ _ 45
100-41-4--------Ethylbenzene __________ _ 170
1330-20-7-------Xylene (total) ________ _ 170
FORM I VOA
Q
I
IU
1u
ID
IU
1u
1u
IU
1u
IU
IU
1u
IDJ
IU
1u
I
3/90
I 1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
lb Name: PACE NEW ENGLA Contract:
EX04XXDL
Lab Code: Case No.: PCHAR SAS No. : SDG No.: NAS08
Jtrix: (soil./water) WATER
lmpl.e wt/vol.: S.00 (g/mL) ML
Level.: (l.ow/med) LOW
Lab Sampl.e ID:
Lab Fil.e ID:
Date Received:
Date Anal.yzed:
44609-38DL
C9413
07/11/95
07/18/95 IMoisture: not dee.
GC Col.umn: SP1000
Iii Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor: 20.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil. Al.iquot Vol.ume: (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl. Chl.oride ________ _
75-09-2---------Methyl.ene Chl.oride ______ _
40
100
67-64-1---------Acetone _____________ _ 2000
75-35-4---------1,1-Dichloroethene ______ _ 140
67-66-3---------Chl.oroform ___________ _ 100
107-06-2--------1 ,2-Dichl.oroethane ______ _ 100
75-27-4---------Bromodichloromethane _____ _ 100
78-87-5---------1 ,2-Dichloropropane _____ _ 120
79-01-6---------Trichloroethene ________ _ 100
79-00-5---------1,1,2-Trichloroethane ____ _ 100
71-43-2---------Benzene _____________ _ 100
108-88-3--------Tol.uene _____________ _ 200
100-41-4--------Ethyl.benzene __________ _ 290
1330-20-7-------Xyl.ene (total.) _________ _ 200
FORM I VOA
a
u
u
D
u
u
u
u
u
u
u
u
u
u
u
3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
L. Name: PACE NEW ENGLA
EX04XX
Contract:
Lab Code: Case No. PCHAR SAS No. : SDG No.: NAS08
Mlrix: (soil/water) WATER Lab Sample ID: 44609-38
Stple wt/vol:
Level: (low/med)
5.00 (g/mL) ML
LOW
Lab File ID:
Date Received:
C9431
Date Analyzed: +oisture: not dee.
GC Column: SP1000
slil Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor:
07/11/95
07/19/95
3.3
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
7
17
67-64-1---------Acetone _____________ _ 2200
75-35-4---------1,1-Dichloroethene ______ _ 23
67-66-3---------Chloroform ___________ _ 17
107-06-2--------1 ,2-Dichloroethane ______ _ 17
75-27-4---------Bromodichloromethane _____ _ 17
78-87-5---------1 ,2-Dichloropropane _____ _ 26
79-01-6---------Trichloroethene ________ _ 1 7
79-00-5---------1 ,1 ,2-Trichloroethane ____ _ 17
71-43-2---------Benzene _____________ _ 17
108-88-3--------Toluene _____________ _ 31
100-41-4--------Ethylbenzene __________ _ 33
1330-20-7-------Xylene (total) ________ _ 33
I 1u
IU
IE
IU
IU
1u
1u
I
IU
1u
1u
IJ
1u
1u
I
Q
(uL)
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
~b Name: PACE NEW ENGLA Contract:
NS09XX
Lab Code: Case No. PCHAR SAS No.: SDG No. : NAS08
~rix: (soil/water) WATER Lab Sample ID: 44609-30
Tple wt/vol: 5.00 (g/mL) ML Lab File ID: C9442
Level: (low/med) LOW Date Received: 07/11/95
Date Anal.yzed: 07/20/95 +oisture: not dee.
GC Column: SP1000
slil. Extract Vol.ume:
ID: 2.00 (mm) Dilution Factor: 1 . 0
I
I
I
I
I
I
I
I
(uL) Soil Al.iquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1,1-Dichl.oroethene ______ _
67-66-3---------Chloroform ------------107 -06 -2 - - - - - - - -1, 2 -Di ch l. or o ethane ______ _
75-27-4---~-----Bromodichl.oromethane ------78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichl.oroethene ________ _
79-00-5---------1 ,1 ,2-Trichl.oroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) _________ _
81
5 u
250 E
9
5 u
1 1
5 u
6 u
5 u
5 u
5 u
130 I
5 IJ
15 I
I
Q
(uL)
I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
NS09XXDL
Contract:
Lab Code: Case No.: PCHAR SAS No. : SDG No. : NAS08
irix: (soil/water) WATER tple wt/vol: 5.00 (g/mL) ML
Level: (low/med) LOW
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
44609-30DL
C9423
07/11/95
07/19/95 f~oisture: not dee.
GC Column: SP1000 .il. Extract Volume:
ID: 2.00 (mm)
( u L )
Dil.ution Factor: 2.3
I
I
I.
I
I
I
I
I
I
Soil Al.iquot Vol.ume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane ------78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1 ,2-Trichl.oroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
I
73 ID
1 1 IU
450 ID
8 IDJ
1 1 1u
1 1 IDJ
1 1 IU
14 1u
1 1 IU
1 1 1u
1 1 IU
130 ID
23 1u
16 IDJ
I
Q
(UL)
I
I
I
FORM I VOA 3/90
I 1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
LI Name: PACE NEW ENGL A Contract:
NS10XX
Lab Code: Case No. PCHAR SAS No.: SDG No.: NAS08
Mlrix: (soil/water) WATER Lab Sample ID: 44609-31
Siple wt/vol: 5.DD (g/mL) ML Lab File ID: C9427
Level: (low/med) LOW Date Received: 07/11/95
Date Analyzed: 07/19/95 %toist'ure: not dee_
GC Column: SP1DDD
slil Extract Volume:
ID: 2.00 (mm) Dilution Factor: 16.7
I
I
I
I
I
I
I
I ,,
I
(UL) Soil Aliquot Volume: (UL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
33
83
170
120
83
107-06-2--------1,2-Dichloroethane ______ _ 7800
75-27-4---------Bromodichloromethane 83 ------78-87-5---------1 ,2-Dichloropropane _____ _ 100
79-01-6---------Trichloroethene ________ _ 83
79-00-5---------1 ,1 ,2-Trichloroethane ____ _ 83
71-43-2---------Benzene _____________ _ 83
108-88-3--------Toluene _____________ _ 170
100-41-4--------Ethylbenzene __________ _ 170
1330-20-7-------Xylene (total) ________ _ 170
Q
I
IU
1u
1u
IU
IU
IE
IU
1u
IU
1u
1u
IU
IU
IU
I
!1
I
FORM I VOA 3/90
I
I 1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
lib Name: PACE NEW ENGLA
NS10XXDL
Contract:
lib Code: Case No.: PC HAR SAS No. SDG No.: NAS08
rltrix: (soil/water)
'mple wt /vol:
Level: (low/med)
IMoistur~: not dee.
WATER
5.00 (g/mL) ML
LOW
Lab Sample ID:
Lab Fil.e ID:
Date Received:
Date Analyzed:
44609-31DL
C9386
07/11/95
07/17/95
ID: 2.00 (mm) Dilution Factor: 83.3
I
I
I
I
I.
I
I
I
I
I
I
I
I
(UL) Soil Aliquot Volume: (uL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
170
420
830
580
420
107-06-2--------1,2-Dichloroethane ______ _ 7600
75-27-4---------Bromodichloromethane _____ _ 420
78-87-5---------1 ,2-Dichloropropane _____ _ 500
79-01-6---------Trichloroethene ________ _ 420
79-00-5---------1 1 1 ,2-Trichloroethane ____ _ 420
71-43-2---------Benzene _____________ _ 420
108-88-3--------Toluene _____________ _ 830
100-41-4--------Ethylbenzene __________ _ 830
1330-20-7-------Xylene (total.) _________ _ 830
FORM I VOA
Q
I
1u
\U
\U
\U
\U
ID
1u
IU
1u
\U
IU
\U
\U
\U
I
3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
LI, Name: PACE NEW ENGLA
NS11XX
Contract:
l b Code: Case No.: PCHAR SAS No.: SDG No.: NAS08
trix: (soil/water) WATER Lab Sample ID: 44609-32
~ple wt/vol: 5.00 (g/mL) ML Lab File ID: C9424
Level: (low/med) LOW Date Received: 07/11/95
Date Analyzed: 07/19/95 +oisture: not dee.
GC Column: SP1000
Jil Extract Vol.ume:
ID: 2.00 (mm)
(uL)
Dilution Factor: 1 . 0
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-0ichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1,2-Trichl.oroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
2
5
10
7
5
6
5
6
5
5
5
15
98
66
Q
u
u
u
u
u
u
u
u
u
u
(UL)
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
NS15XX
Contract:
Lab Code: Case No.: PCHAR SAS No. : SDG No.: NAS08
Jtrix: (soil/water) WATER Lab Sample ID: 44609-29
1mple wt /vol: 5.00 (g/mL) ML Lab File ID: C9426
Level: (low/med) LOW Date Received: 07/11/95
Date Analyzed: 07/19/95 tMoisture: not dee.
GC Column: SP1000
l11 Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor·: 1 . 0
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1 ,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-0ichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1 ,1 ,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) _________ _
4
5
120
7
5
250
5
6
5
5
5
5
10
10
Q
u
u
u
E
u
u
u
u
u
J
u
u
(UL)
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
1A I VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No. PCHAR
Jtrix: (soil/water) WATER
1mple
Level:
wt/vol:
(low/med)
5.00 (g/mL) ML
LOW
Contract:
SAS No.
Lab
Lab
Date
Date
EPA SAMPLE NO.
NS15XXDL
SDG No. NAS08
Sample ID: 44609-29DL
File ID: C9384
Received: 07/11/95
Anal.yzed: 07/17/95 tMoisture: not dee.
GC Column: SP1DOO
.±1 Extract Volume:
ID: 2.00 (mm) Dil.ution Factor: 2.0
I
I
I
I
I
I
I
I
I
I
I
I
I
( u L) Soil Aliquot Volume:
GAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone ______________ _
75-35-4---------1,1-Dichloroethene ______ _
67-66-3---------Chloroform ____________ _
107-06-2--------1,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane ______ _
79-01-6---------Trichl.oroethene ---------79 -00 - 5 - - - - - - - - -1, 1 ,2-Trichloroethane ____ _
71-43-2---------Benzene ______________ _
108-88-3--------Toluene ______________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) _________ _
FORM I VOA
4
1 0
20
14
10
250
1 0
1 2
10
10
10
6
20
20
(uL)
Q
D
u
u
u
u
D
u
u
u
u
u
DJ
u
u
3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
~b Name: PACE NEW ENGLA
NS29XX
Contract: l: Code: Case No.: PCHAR SAS No. : SDG No.: NAS08
rix: (soil/water) WATER
Tple wt/vol: 5.00 (g/mL) ML
Level: (low/med) LOW
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
44609-34
C9428
07/11/95
07/19/95 +oisture: not dee.
GC Column: SP1000
.il Extract Volume:
ID: 2.00 (mm)
(UL)
Dilution Factor: 50.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil Aliquot Volume: (UL)
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _ 100
75-09-2---------Methylene Chloride ______ _ 250
67-64-1---------Acetone _____________ _ 35000
75-35-4---------1 ,1-Dichloroethene ______ _ 350
67-66-3---------Chloroform ___________ _ 250
107-06-2--------1 ,2-Dichloroethane ______ _ 690
75-27-4---------Bromodichloromethane _____ _ 250
78-87-5---------1 ,2-Dichloropropane _____ _ 1000
79-01-6---------Trichloroethene ________ _ 250
79-00-5-------~-1 ,1 ,2-Trichloroethane ____ _ 250
71-43-2---------Benzene _____________ _ 250
108-88-3--------Toluene _____________ _ 200
100-41-4--------Ethylbenzene __________ _ 500
1330-20-7-------Xylene (total) _________ _ 500
FORM I VOA
a
I
IU
1u
IE
1u
IU
I 1u
I
1u
IU
1u
IJ
IU
IU
I
3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA Contract:
NS29XXDL
Lab Code: Case No.: PCHAR SAS No.: SDG No.: NAS08
rltrix: (soiJ./water) WATER Lab SampJ.e ID: 44609-34DL
lmpJ.e wt/vol.: 5.00 (g/mL) ML
Level.: (J.ow/med) LOW
Lab FiJ.e ID:
Date Received:
Date Analyzed:
C9409
07/11/95
07/18/95 IMoisture: not dee.
GC CoJ.umn: SP1000
Iii Extract Volume:
ID: 2.00 (mm)
( u L)
DiJ.ution Factor: 250.0
I
I
I
I
I
I
I
I
I
I
I
I
I
Soil. AJ.iquot VoJ.ume: (uL)
GAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------VinyJ. ChJ.oride _________ _ 500
75-09-2---------MethyJ.ene ChJ.oride ______ _ 1200
67-64-1---------Acetone _____________ _ 42000
75-35-4---------1 ,1-Dichloroethene ______ _ 1800
67-66-3---------ChJ.oroform ___________ _ 1200
107-06-2--------1,2-Dichloroethane ______ _ 1200
75-27-4---------Bromodichloromethane _____ _ 1200
78-87-5---------1 ,2-Dichloropropane _____ _ 940
79-01-6---------Trichloroethene ________ _ 1200
79-00-5---------1 ,1,2-Trichloroethane ____ _ 1200
71-43-2---------Benzene _____________ _ 1200
108-88-3--------ToJ.uene _____________ _ 2500
100-41-4--------EthyJ.benzene __________ _ 2500
1330-20-7-------XyJ.ene (total.) ________ _ 2500
FORM I VOA
a
u
u
D
u
u
u
u
DJ
u
u
u
u
u
u
3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
• Name: PACE NEW ENGLA Contract:
NS30XX
Lab Code: Case No. PCHAR SAS No.: SDG No.: NAS08
irix: (soil/water) WATER
Tple wt /vol: 5.00 (g/mL) ML
Level: (low/med) LOW
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
44609-35
C9410
07/11/95
07/18/95 +oisture: not dee.
GC Column: SP1DOO
slil Extract Volume:
ID: 2.00 (mm) Dilution Factor: 1. 0
(UL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ___________ _
107-06-2--------1,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1,1 ,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
I
2 \U
5 \U
32 I
7 \U
5 \U
5 \U
5 \U
6 \U
5 \U
5 \U
5 \U
10 \U
1 0 \U
10 \U
I
a
(UL)
I
I
I
I
I
I
I
I
I
I
I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA Contract:
NS31XX
Lab Code: Case No.: PCHAR SAS No. : SDG No.: NAS08
Jtrix: (soil./water) WATER
1mpl.e wt/vol.:
Level.: (l.ow/med)
5.00 (g/mL) ML
LOW
Lab Sampl.e ID:
Lab Fil.e ID:
Date Received:
Date Analyzed:
44609-33
C9425
07/11/95
07/19/95 tMoisture: not dee.
GC Col.umn: SP100D
Jil Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor: 6.5
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl. Chl.oride ________ _
75-09-2---------Methyl.ene Chl.oride ______ _
13
32
67-64-1---------Acetone _____________ _ 6500
75-35-4---------1 ,1-Dichl.oroethene ______ _ 45
67-66-3---------Chloroform ___________ _ 32
107-06-2--------1 ,2-Dichloroethane ______ _ 1 20
75-27-4---------Bromodichloromethane _____ _ 32
78-87-5---------1 ,2-Dichloropropane _____ _ 260
79-01-6---------Trichloroethene 32 ---------79 -00 - 5 - - - - - - - - -1, 1, 2 -Tri ch lo roe thane ____ _ 32
71-43-2---------Benzene _____________ _ 32
108-88-3--------Toluene _____________ _ 45
100-41-4--------Ethyl.benzene __________ _ 65
1330-20-7-------Xylene (total) _________ _ 65
Q
u
u
E
u
u
u
u
u
u
J
u
u
(uL)
I
I
I
I
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I
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
NS31XXDL
Contract:
Lab Code: Case No. PCHAR SAS No. SDG No. NAS08
Jtr~x: (soil/water) WATER Lab Sample ID: 44609-33DL
lmple wt/vol:
Level: (low/med)
5.00 (g/mL) ML
LOW
Lab File ID: C9408
Date Received: 07/11/95
Date Analyzed: 07/18/95 tMoisture: not dee.
GC Column: SP1000
lil Extract Volume:
ID: 2.00 (mm)
(uL)
Dilution Factor: 40.0
I
I
I
I
I
I
I
I
I
I
I
Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride _________ _
75-09-2---------Methylene Chloride ______ _
80
200
67-64-1---------Acetone ______________ _ 4800
75-35-4---------1,1-Dichloroethene ______ _ 280
67-66-3---------Chloroform ____________ _ 200
107-06-2--------1 ,2-Dichloroethane ______ _ 200
75-27-4---------Bromodichloromethane _____ _ 200
78-87-5---------1 1 2-Dichloropropane ______ _ 240
79-01-6---------Trichloroethene ________ _ 200
79-00-5---------1,1,2-Trichloroethane ____ _ 200
71-43-2---------Benzene ______________ _ 200
108-88-3--------Toluene ______________ _ 400
100-41-4--------Ethylbenzene __________ _ 400
1330-20-7-------Xylene (total) _________ _ 400
Q
u
u
D
u
u
u
u
u
u
u
u
u
u
u
( u L)
I
I
FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
tb Name: PACE NEW ENGLA
NS32XX
Contract:
Lab Code: Case No. PCHAR SAS No. SDG No.: NASOS
~rix: (soil/water) WATER Lab Sample ID: 44609-28
Imp le wt /vol: 5.00 (g/mL) ML
Level: (low/med) LOW
Lab File ID:
Date Received:
Date Analyzed:
C9383
07/11/95
07/17/95 .oisture: not dee.
GC Column: SP1000 ID: 2.00 (mm) Dilution Factor: 1 . 0
Extract Volume: (uL) Soil Aliquot Volume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methylene Chloride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chloroform ------------107 -06 - 2 - - - - - - - -1, 2 -Di ch lo roe thane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1 ,1,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Toluene _____________ _
100-41-4--------Ethylbenzene __________ _
1330-20-7-------Xylene (total) ________ _
2
5
10
7
5
5
5
6
5
5
5
10
10
10
Q
u
u
u
u
u
u
u
u
u
u
u
u
u
u
(uL)
I
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FORM I VOA 3/90
I 1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
TBLK01
Contract:
Lab Code: Case No.: PCHAR SAS No. : SDG No.: NASOS
~•trix: (soil./water) WATER
lmple wt/vol:
Level.: (l.ow/med)
5.00 (g/mL) ML
LOW
Lab
Lab
Date
Date
Sampl.e ID: 44609-40
Fil.e ID: C9415
Received: 07/11/95
Anal.yzed: 07/18/95 91Moist·ure: not dee.
GC Col.umn: SP1000
lil Extract Volume:
ID: 2.00 (mm) Dilution Factor: 1 . 0
(uL) Soil. Al.iquot Vol.ume:
CAS NO. COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
75-01-4---------Vinyl Chloride ________ _
75-09-2---------Methyl.ene Chl.oride ______ _
67-64-1---------Acetone _____________ _
75-35-4---------1 ,1-Dichloroethene ______ _
67-66-3---------Chl.oroform ___________ _
107-06-2--------1,2-Dichloroethane ______ _
75-27-4---------Bromodichloromethane _____ _
78-87-5---------1 ,2-Dichloropropane _____ _
79-01-6---------Trichloroethene ________ _
79-00-5---------1 ,1 ,2-Trichloroethane ____ _
71-43-2---------Benzene _____________ _
108-88-3--------Tol.uene _____________ _
100-41-4--------Ethyl.benzene __________ _
1330-20-7-------Xyl.ene (total.) ________ _
J
2 JU
5 JU
10 JU
7 JU
5 JU
5 JU
5 JU
6 JU
5 JU
5 JU
5 JU
10 IU
10 1u
10 1u
I
Q
(UL)
I
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I
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I
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I
I
FORM I VOA 3/90
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! I
!
I
Appendix D
Semivolatile Organics Analysis Data Sheets
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
ltrix: (soil/water) WATER
lmple wt/vol:
Level: (low/med)
IMoisture:
Concentrated Extract
ljection Vol.ume:
905.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1 ooo
2.0(UL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EX01XX
Contract:
SAS No. : SDG No.: NASOS
(UL)
Lab Sample ID:
Lab Fi1e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-23
H8597
07/11/95
07/12/95
07/17/95
1 . 0
a
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 14
28
I
IU 100-02-7--------4-Nitrophenol _________ _
_______ 1 __ _
FORM I SV-1 3/90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
l b Code:
trix: (soil./water)
f'pl.e wt/vol.:
Level: (l.ow/med) + ois't:ure:
Concentrated Extract
Jjection Vol.ume:
Case No.: PCHAR
WATER
935.0 (g/mL) ML
LOW
decanted: (Y/N)
Vol.ume: 1 000
2.0(uL)
Cleanup: (Y /N) N pH:
CAS NO. COMPOUND
EX02XX
Contract:
SAS No.: SDG No. : NASOS
(uL)
Lab Sampl.e ID:
Lab Fil.e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-24
H8592
07/11/95
07/12/95
07/17/95
25.0
Q
I
T
I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chl.oroethyl.)ether ___ _ 570
670
I
IU 100-02-7--------4-Nitrophenol. _________ _
________ 1 __ _
FORM I SV-2 3/90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
rltrix: (soil./water) WATER
lmpl.e wt/vol.:
Level.: (l.ow/med)
tMoisture:
Concentrated Extract
ljection Vol.ume:
875.0 (g/mL) ML
LOW
decanted: (Y/N)
Vol.ume: 1000
2.0(uL)
Cl.eanup: (Y/N) N pH:
CAS NO. COMPOUND
EX03XX
Contract:
SAS No. : SDG No.: NAS08
(UL)
Lab Sampl.e ID:
Lab Fil.e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-26
H8587
07/11/95
07/12/95
07/17/95
4.0
Q
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chl.oroethyl.)ether ___ _ 120
11 0
I
1u 100-02-7--------4-Nitrophenol. _________ _
_______ 1 __ _
FORM I SV-3 3/90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
ltrix: (soil/water) WATER
'mple wt/vol:
Level: (low/med)
'Moisture:
Concentrated Extract
ljection Volume:
900.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1000
2.0(uL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
EX04XX
Contract:
SAS No.: SDG No. : NAS08
(uL)
Lab Samp1e ID:
Lab Fi1e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Oil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-25
H8593
07/11/95
07/12/95
07/17/95
5.0
Q
I I
I
I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 64
140
I
1u 100-02-7--------4-Nitrophenol. _________ _
_______ 1 __ _
FORM I SV-4 3/90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
Jtrix: (soil/water) WATER
lmple wt/vol:
Level: (low/med)
tMoisture:
905.0 (g/mL) ML
LOW
decanted: (Y/N)
Concentrated Extract Volume: 1000
ljection Volume: 2.0(uL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS09XX
Contract:
SAS No. SDG No.: NASOS
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dil.ution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-17
H8588
07/11/95
07/12/95
07/17/95
5.0
Q
I
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I
I
I
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 28
140
I
1u
IU 100-02-7--------4-Nitrophenol _________ _
________ 1 __ _
FORM I SV-5 3/90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
ltrix: (soil/water) WATER
lmple wt/vol:
Level: (low/med)
I Moisture:
Concentrated Extract
ljection Volume:
795.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1 000
2.0(UL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS10XX
Contract:
SAS No. : SDG No.: NAS08
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-18
H8589
07/11/95
07/12/95
07/17/95
50.0
Q
I
I
I
I
I
I
I
I.
111-44-4--------bis(2-Chloroethyl)ether ___ _ 310
1600
I
1u
1u
I
I
I
100-02-7--------4-Nitrophenol _________ _
FORM I SV-6
_______ 1 __ _
3 /90
1 B EPA SAMPLE NO. I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
L. Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
Mlrix: (soil/water) WATER Srple wt/vol:
Level: (low/med)
%toisture:
Concentrated Extract
II ection Volume:
900.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1000
2.0(uL)
C1eanup: (Y/N) N pH:
CAS NO. COMPOUND
NS 11 XX
Contract:
SAS No. SDG No.: NAS08
(uL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-19
H8595
07/11/95
07/12/95
07/17/95
1 . 0
Q
I
I
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 6
28
I
IU
JU
,.
I
I .,
I
I
100-02-7--------4-Nitrophenol _________ _ ________ ! __ _
FORM I SV-7 3/90
1 B EPA SAMPLE NO. :I SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No. PCHAR
~rix: (soil./water) WATER fpl.e wt/vol.:
Level.: (J.ow/med)
+oisture:
C~ncentrated Extract
ljection Volume:
920.0 (g/mL) ML
LOW
decanted: (Y/N)
Vol.ume: 1000
2.0(UL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS15XX
Contract:
SAS No. : SDG No. : NASOS
(uL)
Lab Sampl.e IO:
Lab Fi l.e ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-16
H8594
07/11/95
07/12/95
07/17/95
1 . 0
Q
111-44-4--------bis(2-Chl.oroethyl.)ether ___ _ 5
27
I
IU
\U
I
i
I
I
I
.I
I
I
I
I
100-02-7--------4-Nitrophenol. _________ _
FORM I SV-8
_______ 1 __ _
3/90
1 B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
L_., Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
Mlrix: (soil/water) WATER
'· sr,ple wt /vol:
Level: (low/med)
+oisture:
Concentrated Extract
rljection Volume:
900.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1000
2.0(uL)
Cleanup: (Y/N) N pH:
CAS NO. COMPOUND
NS29XX
Contract:
SAS No. : SDG No.: NAS08
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-21
H8591
07/11/95
07/12/95
07/17/95
25.0
Q
I
1
I
I
I
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 450
690
I
1u
I
I
I
I
I
100-02-7--------4-Nitrophenol _________ _
FORM I SV-9
_______ 1 __ _
3/90
1 B EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENG LA
NS30XX
Contract:
~,b Code: Case No. PCHAR SAS No. : SDG No.: NAS08
rltrix: (soil/water)
r.
l,mple
Leve1:
wt/vol:
(low/med)
tMoisture:
WATER
910.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1000 (uL)
Lab Sample ID: 44609-22
Lab File ID: H8596
Date Received: 07/11/95
Date Extracted: 07/12/95
Date Analyzed: 07/17/95 Concentrated Extract
ljection Volume: 2.0(uL) Dilution Factor: 1. 0
·1
I
I
I
I
I
I
I
I
I
I
Cleanup: (Y/N) N pH:
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L
111-44-4--------bis(2-Chloroethyl)ether ___ _
100-02-7--------4-Nitrophenol _________ _
1 2
27
I
I
IU
Q
________ 1 __ _
FORM I SV-1 3/90
1 8 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA ~-b :ode:
"'1:rix: ( soil. /water)
1mpl.e
Level.:
wt /vol.:
(l.ow/med)
... Moisture:
Concentrated Extract
ljection Vol.ume:
Case No.: PC HAR
WATER
970.D (g/mL) ML
LOW
decanted: (Y/N)
Vol.ume: 1 ooo
2.0(uL)
Cl.eanup: (Y/N) N pH:
CAS NO. COMPOUND
NS31XX
Contract:
SAS No.: SDG No.: NASD8
(UL)
Lab Sampl.e ID:
Lab File ID:
Date Received:
Date Extracted:
Date Anal.yzed:
Di l.ut ion Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-20
H8590
07/11/95
07/12/95
07/17/95
5.0
Q
I ., 111-44-4--------bis(2-Chl.oroethyl.)ether ___ _ 130
130
I
IU
I
I
I
I
I
100-02-7--------4-Nitrophenol. _________ _
FORM I SV-2
_______ 1 __ _
3/90
1 8 EPA SAMPLE NO.
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
lb Name: PACE NEW ENGLA
Lab Code: Case No.: PCHAR
J~rix: (soil/water) WATER
lmple wt/vol:
Level: (low/med)
tMoisture:
Concentrated Extract
l,j ection Volume:
900.0 (g/mL) ML
LOW
decanted: (Y/N)
Volume: 1 ooo
2.0(UL)
Cleanup: (Y/N) N pH:
CA$ NO. COMPOUND
NS32XX
Contract:
SAS No.: SDG No. : NAS08
(UL)
Lab Sample ID:
Lab File ID:
Date Received:
Date Extracted:
Date Analyzed:
Dilution Factor:
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/L
44609-15
H8586
07/11/95
07/12/95
07/17/95
1 . 0
Q
I
I
111-44-4--------bis(2-Chloroethyl)ether ___ _ 6
28
I
1u
IU
I
I
I
I
I
I
I
100-02-7--------4-Nitrophenol _________ _
FORM I SV-3
________ 1 __ _
3/90
I
I
I
I
I
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I
'I
I
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I
I
I
I
I
I
I
.I
I
Appendix E
Inorganics Analysis Data Sheets
I
I U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET I Lab Name: PACE INC. , NE-NH Contract:
EXOlXX
I Lab Code: Case No.: PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-009
Date Received: 07/11/95 I Level (low/med) : LOW
% Solids: 0.0
I ,. Concentration Units (ug/L or mg/kg dry weight): UG/L
:1
I
I
I
I
I,
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
l omments:
EX-01
.I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 1.9 u
Barium 61.4 B
Beryllium 0.32 B
Cadmium 1.2 u
Calcium
Chromium 3.1 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 117
Mercury
Nickel 7.2 u
Potassium
Selenium 1.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 43.6
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I U.S. EPA -CLP
EPA SAMPLE NO.
1
INORGANIC ANALYSIS DATA SHEET ,I Lab Name: PACE INC. , NE-NH Contract:
EX02XX
I Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-010
Date Received: 07/11/95 I Level (low/med) : LOW
% Solids: 0.0
I, Concentration Units (ug/L or mg/kg dry weight): UG/L
1:, ,, ,,
I
I
I
I
I
.I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
. 7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
, lolor
Before: COLORLESS
After: YELLOW
I. omments:
EX-02
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.8 B
Barium 1820
Beryllium 0.30 u
Cadmium 1.2 u
Calcium
Chromium 5.1 B
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 18300
Mercury
Nickel 7.2 u
Potassium
Selenium 1.8 B
Silver
Sodium
Thallium
Vanadium
Zinc 2.6 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Art.if acts:
3/90
I
I U.S. EPA -CLP
. 1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET I Lab Name: PACE INC., NE-NH Contract:
EX03XX
I Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-012
Date Received: 07/11/95 I Level (low/med): LOW
% Solids: 0.0
.I Concentration Units (ug/L or mg/kg dry weight): UG/L
11
11,
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
l omments:
EX-03
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 1.9 u
Barium 265
Beryllium 0. 30 u
Cadmium 1.2 u
Calcium
Chromium 3.4 B
Cobalt
Co1212er
Iron
Lead
Magnesium
Manganese 3970
Mercury
Nickel 7.2 u
Potassium
Selenium 1.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 2.6 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET I Lab Name: PACE INC., NE-NH Contract:
EPA SAMPLE NO.
EX04XX
1 Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-011
Date Received: 07/11/95 1: Level (low/med): LOW
% Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
f omments:
EX-04
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 1. 9 u
Barium 52.6 B
Beryllium 0.30 u
Cadmium 1. 2 u
Calcium
Chromium 3.1 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 3210
Mercury
Nickel 7.2 u
Potassium
Selenium 1.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 4.0 B
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I U.S. EPA -CLP
EPA SAMPLE NO.
1
INORGANIC ANALYSIS DATA SHEET ,1 Lab Name: PACE INC., NE-NH
'Lab ~ode:
· Matrix (soil/water):
I Level (low/med):
% Solids:
Case No.: PCHAR
WATER
LOW
0.0
Contract:
SAS No.:
NS09XX
SDG No. : MNAS08
Lab Sample ID: 44609-003
Date Received: 07/11/95
I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: LT.BLACK
After: YELLOW
l omments:
NS-09
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 3.2 B
Barium 1200
Beryllium 0.30 u
Cadmium 1.8 B
Calcium
Chromium 42.0
Cobalt
COEEer
Iron
Lead
Magnesium
Manganese 33600
Mercury
Nickel 9.4 B
Potassium
Selenium 2.0 B
Silver
Sodium
Thallium
Vanadium
Zinc 46.6
cyanide
-
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I. U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE INC., NE-NH Contract:
NSlOXX
1. Lab Code: Case No.: PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-004
Date Received: 07/11/95 I Level (low/med): LOW
% Solids: 0.0 I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
.,omments:
NS-10
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.2 B
Barium 176 B
Beryllium 0.30 u
Cadmium 1. 2 u
Calcium
Chromium 6.7 B
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 9320
Mercury
Nickel 20.6 B
Potassium
Selenium 1.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 16.6 B
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I, U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET I Lab Name: PACE INC. , NE-NH Contract:
NSllXX
I Lab Code: Case No.: PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-005
Date Received: 07/11/95 ,, Level (low/med) :
% Solids:
LOW
0.0
I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
liolor
lolor
Before: BROWN
After: YELLOW
l omments:
NS-11
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.4 B
Barium 237
Beryllium 0.55 B
Cadmium 1. 2 u
Calcium
Chromium 5.2 B
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 248
Mercury
Nickel 12.0 B
Potassium
Selenium 3.6 B
Silver
Sodium
Thallium
Vanadium
Zinc 41. 3
Cyanide
-
Clarity Before: CLOUDY
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET I Lab Name: PACE INC., NE-NH contract:
NS15XX
1 Lab Code: Case No. : PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-002
Date Received: 07/11/95 I Level (low/med): LOW
% Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
l omments:
NS-15
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 1. 9 u
Barium 387
Beryllium 0.30 u
Cadmium 1.2 u
Calcium
Chromium 3.1 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 13400
Mercury
Nickel 7.2 u
Potassium
Selenium 1.7 u
Silver
Sodium
Thallium
Vanadium
Zinc 2.6 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Art.if acts:
3/90
I
I
I Lab Name:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
PACE INC. , NE-NH Contract:
EPA SAMPLE NO.
NS29XX
1 Lab Code:
Matrix (soil/water): WATER
Case No.: PCHAR SAS No.: SDG No.: MNAS08
Lab Sample ID: 44609-007
Date Received: 07/11/95 I Level (low/med): LOW
% Solids: 0.0
I concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
.omments: I NS-29
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.2 B
Barium 190 B
Beryllium 0.30 u
Cadmium 1.2 u
Calcium
Chromium 3.1 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 611
Mercury
Nickel 7.2 u
Potassium
Selenium 3.0 B
Silver
Sodium
Thallium
Vanadium
Zinc 2.6 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I
I Lab Name:
U.S. EPA -CLP
1
INORGANIC ANALYSIS DATA SHEET
PACE INC. , NE-NH Contract:
EPA SAMPLE NO.
NS30XX
1, Lab Code: Case No.: PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-008
Date Received: 07/11/95 I Level (low/med): LOW
% Solids: 0.0
I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
, I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
l omments:
NS-30
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 1.9 u
Barium 19.7 B
Beryllium 0.30 u
Cadmium 1.2 u
Calcium
Chromium 3.1 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 1800
Mercury
Nickel 7.2 u
Potassium
Selenium 2.0 B
Silver
Sodium
Thallium
Vanad.i,um
Zinc 2.6 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
-NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
I Lab Name: PACE INC., NE-NH Contract:
NS31XX
I Lab Code: Case No.: PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-006
Date Received: 07/11/95 , , Level (low/med) :
% Solids:
LOW
0.0
I
I
I
I
I
I
I
I
I
I
Concentration Units (ug/L or mg/kg dry weight): UG/L
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
l omments:
NS-31
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 1. 9 u
Barium 207
Beryllium 0. 30 u
Cadmium 1.2 u
Calcium
Chromium 3.1 ,U
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 35.7
Mercury
Nickel 7.2 u
Potassium
Selenium 2.7 B
Silver
Sodium
Thallium
Vanadium
Zinc 2.6 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I U.S. EPA -CLP
1
EPA SAMPLE NO.
INORGANIC ANALYSIS DATA SHEET
I' Lab Name: PACE INC. , NE-NH Contract:
NS32XX
1 Lab Code: Case No.: PCHAR SAS No.: SDG No.: MNAS08
Matrix (soil/water): WATER Lab Sample ID: 44609-001
Date Received: 07/11/95 I Level (low/med): LOW
% Solids: 0.0 I Concentration Units (ug/L or mg/kg dry weight): UG/L
I
I
I
I
I
I
I
I
I
CAS No.
7429-90-5
7440-36-0
7440-38-2
7440-39-3
7440-41-7
7440-43-9
7440-70-2
7440-47-3
7440-48-4
7440-50-8
7439-89-6
7439-92-1
7439-95-4
7439-96-5
7439-97-6
7440-02-0
7440-09-7
7782-49-2
7440-22-4
7440-23-5
7440-28-0
7440-62-2
7440-66-6
Color
lolor
Before: COLORLESS
After: COLORLESS
l omments:
NS-32
I
I
Analyte Concentration C
-Aluminum
Antimony
Arsenic 2.3 B
Barium 89.7 B
Beryllium 0.30 u
Cadmium 1. 2 u
Calcium
Chromium 3.1 u
Cobalt
coeeer
Iron
Lead
Magnesium
Manganese 107
Mercury
Nickel 7.2 u
Potassium
Selenium 2.0 B
Silver
Sodium
Thallium
Vanadium
Zinc 2.6 u
cyanide
-
Clarity Before: CLEAR
Clarity After: CLEAR
FORM I -IN
Q M
NR
NR
p
p
p
p
NR
p
NR
NR
NR
NR
NR
p
NR
p
NR
p
NR
NR
NR
NR
p
NR
-
Texture:
Artifacts:
3/90
I
I
I
I
I
Appendix F
I Chain-of-Custody Records
I
I
••
I
I
I
I
I
I
I
I
I
I
[c,4li;J ---
ENVIRONMENTAL LABORATORIES
Sampled By (PRINT):
5
-- -
Report To: fuA/ kl. -1./z
BillToPO, fio X JCJq
-
P.O.# I Billing Reference CJ 7 -J J 71/ l./
Project Name I No.
PRESERVATIVES Cf) a: w >--------~----z ~ z 0 (.)
u. 0
ci z
0 w ii' w Cf) w a: CL z ::,
- --- -210561
CHAIN-OF-CUSTODY RECORD.
Analytical Request
Pace Client NJ[!-~/ ·:,i(p
Pace Project Manager
"Requested Due Date:
REMARKS
SEE REVERSE SIDE FOR INSTRUCTIONS
[wli;J ---
ENVIRONMENTAL LABORATORIES
Client Ii /,1 b ~ 11 , a / <;fn rch f CJi C dL I C ,,;_ / ( ~ ✓, '/z' -,,:_v
Address L/ g tJ-" CPc/.n /? c;-,.d:1;'71 S: ,f,-:c ,~/
)o /, <:/2,, rv 11/C. :2'j&~ .r l I
Phone 7&-C:,? ?-17-?I Fx 203
- --
Report To: f'1L-' /J / )(/ , -1---/2
,
P.O.#/ Billing Reference 9~ / -J 7 l/~
Project Name/ No.
ffi 1--.'P'-'R-'E;cS:.:E::;.RrV"-A"-TrlV.:E:.::S,--l
J +
Sampler Sign ture.,
: ~(~J..,·'-~ : ~,.'7.Z, .. -,.
z g
0 0
0 w > a: w U) w a: a. z ::,
0 U)
£
r5 <( z O I >
-- -
CHAIN-OF-CUSTODY RECORD ·
Analytical Request
Pace Client No.
Pace Project Manager
Pace Project No .
•Requested Due Date:
REMARKS
,·.'.•'-":fi•;S> .,_.C•'{l'•<-1,;::;J'~'·',':),;-<·::·";Cp!c::) •:;,,;. '''l"~<-'1'"'"''"'•''"·"'·-'•' i'"'' . -,, , .. , "i/L•~<>•,., "'Ot·l,a .. ,<; • y 3 c• 1• o'i'. i;;-,
,-'l'}i,;
2
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