NCD981927502_19990305_Geigy Chemical Corporation_FRBCERCLA RA_1999 Annual Operating Report Groundwater Remediation-OCR

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1999 Annual Operating Report
Groundwater Remediation Permit No. WQ0009949
Geigy Chemical Corporation {:ERCLA Site
Aberdeen, North Carolina
March 5, 1999
Prepared by:
Earth Tech
10 Patewood Drive
Bldg. VI, Suite 500
Greenville, South Carolina 29615
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Geigy Chemical Corporation Site
Aberdeen, North Carolina
Committee Correspondence
March 5, 1999
Ms. Giezelle Bennett
Remedial Project Manager
USEPA Region IV, North Superfund Remedial Branch
11th Floor
RECEIVED
MAR O 8 1999
SUPERFUND SECTION
61 Forsyth Street, SW
Atlanta, GA 30303-3104 VIA OVERNIGHT DELIVERY
RE: Annual Operating Report
Groundwater Remediation Permit No. WQ0009949
Geigy Chemical Corporation CERCLA Site
Aberdeen, North Carolina
Dear Giezelle:
On behalf of Olin Corporation, Novartis Crop Protection and Kaiser Aluminum· & Chemical
Corporation, please find enclosed one copy of the Annual Operating Report for the Geigy
Chemical Corporation CERCLA Site groundwater extraction, treatment and discharge system.
Information provided in this letter report includes:
• Monitoring requirements summary table (Attachment I);
• Site extraction and treatment system layout (Attachment 2)
o Monitoring events analytical results summary tables (Attachment 3);
• Beta-BHC concentration trend graphs for site indicator wells (Attachment 4); and
• Completed copies of NCDENR Division of Water Quality, Groundwater Section form GW-
59, with corresponding field groundwater sample collection records and analytical laboratory
data reports (Attachment 5).
Information provided in Attachment 5 of this submittal is intended to fulfill the annual reporting
requirements described in Section IV, paragraph 4 of the Site Groundwater Remediation Permit:
Accordingly, one copy of this report has been sent to NCDENR's Division of Water Quality,
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Groundwater Section. Additional copies have been sent to Randy McElveen of NCDENR and
Tim Eggert of CDM.
The system performed as designed during 1998 and experienced minimal down-time. Pumping
of the Upper Black Creek Aquifer extraction wells (PW-ID, 2D and 3D) continues to fulfill the
closed-loop requirement of the Site Groundwater Remediation Permit and prevent the release of
groundwater containing pesticides into the area downgradient of the facility property.
Concentration trend graphs are provided in Attachment 4. Graphs include baseline data from
December 1996 and monitoring data from I 997 and l 998 to facilitate review of the groundwater
quality monitoring data. Beta-BHC was selected as an indicator parameter for the graphs as· this
constituent typically exhibits the highest concentrations and detection frequency among the
pesticides included in the sample analyses. In reviewing the graphs, please note that wells MW-
l 6S, I 7S and l 8S are completed in the surficial aquifer and serve to monitor the infiltation
gallery. Wells MW-16D and 17D are completed in the Upper Black Creek aquifer and are
located hydraulically upgradient of the Site.
If you require additional copies of the enclosed materials, or have any questions about this
information, please contact me at [phone] .
Regards,
Garland Hilliard
Project Coordinator
/Enclosure
c: NCDENR Groundwater Division
R. McElveen (NCDENR)
T. Eggert (CDM)
R. McClure (Olin)
H. Moats (Novartis)
H. Grubbs, Esq. (WCS&R)
B. Vinzant (Kaiser)
M. Sheehan (Earth Tech)
D. Shoopman (Earth Tech)
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ATTACHMENT I
!!!!! !!!!!!I l!!llS == == -- -
GROUNDWATER EXTRACTION AND TREATMENT SYSTEM
ANALYTICAL MONITORING REQUIREMENTS
-----
Parameters of Analysis Sampling Requirement Frequency
Location TCL Pesticides TCE PSVP Groundwater FinalO&M Year I -quarterly Other
Remediation Permit Manual Year 2 -semiannually
Annually thereafter
MW-4S
MW-5S
MW-6S
MW-10S
MW-I ID
MW-16S
MW-16D
MW-l7S .
MW-17D .
MW-l8S
MW-18D
MW-30D .
After Lead Quarterly
Canisters
Effluent . Years I and 2 -
quarterly
Annually thereafter
Notes:
I. Monitoring wells MW-ID and MW-15D sampled for TCE during baseline event to address State request.
2. Treatment system influent sampled for TCE and pesticides during baseline event to address system startup requirements.
3. Sampling requirements during post-extraction hydraulic equilibrium monitoring and performance standards verification phases will be in accordance with the
Site Performance Standards Verification Plan.
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ATTACHMENT 2
I r-:::::-~-:-----:-_,__ __ L _ _J_---:----L--_:____.i.--__ ___,__~ _ ___,__ ______ -----,
NORTH
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MW-5~
PW-IS♦
WP-1¾,-
NOTts:
Wa:!ill
EXISTING MONITORING WELL
EXISTING EXTRACTION WEtl.
EXISTING WELL POINT PIEZOMETER
FENCE
EXTRACTION WELL FORCE MAIN
.'
1. TOPO MAPPING BY WOOLPERT CONSULTANTS BASED ON
AERIAL PHOTOGRAPHY Fl.OWN MARCH 26, 1989 WITH
GROUND CONTROL TIED TO THE STATE PLANE COORDINATE
SYSTEM.
2. PLANIMETRIC FEATURES WERE nELD IDENTIFIED
ON MAY 16, 1969 BY WOOLPERT CONSULTANTS.
3. FOR TYPICAL TRENCH CROSS SECTION SEE
DRAWING 86619-C-04.
4.. ~OCATIOH Of ACCESS ROAD SHOWN OH THIS DRAWING IS
APPROXIMATE. EXACT LOCATION WILL BE DETERMINED IN THE nELD
BY OWNER'S REPRESEHTATrvE. FOR CONSTRUCTION DETAIL SEE
TYPICAL GRAVEL ROAD CROSS SECTION ON DRAWING 86619-C-04.
.J AS BUILTS 12/H
2 f"DIA1. OCSIOH KU -12/0!/95
1 SUBWITTAL TO EPA KU JHM fJ/15/'15
0 ruo;r Rrn[W KU .... 5/t'i/"
Rt'IIS>ONS --CH< "'" HO.
L_
/~ ---------~ __ ..,,..
/
YAOC o« DAT£ NO.
·,,~OW-20
, ______ .... /-"'<,
w.o£ 0« OAlI
\ /
~ //
TREATED ~ROUHDWATER
DISCHARGE l.JNE
IHFlLTRATION GAL1.£RIES
+ MW-16S
DA11:
5/19/95
5/19/95
EXTRACTION AND
TREATMENT SYSTEM
SITE LAYOUT
'
G(JGY CHEMICAi.' CORPORATIOH SIT£
AIIERDErH, >!ORTH CAROIJHA
/
(
MW-1-10 + i f
MW-17D
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· .. --·-
/
IFH lll"V' ENVIRONNiENT & ll~U>II INFRASfRUCTURE
PRCU:CT NUMBfJI 377~.000 ·
a.on owe
"""""
OAT[ 01/9/97
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Influent
Effluent
Sample
Port V-54
Sample
Port V-49
Sample
Port V-52
Sample
Port V-48
Sample
Port V-51
EARTHOTECH
A tqca INTERNAnONAL LTD. COMPANY
Transfer
Pump P-6
Transfer
Pump P-7
Sample
Port V-47
Sample
Port V-50
Treatment System
Process Layout
Geigy Chemical Corporation Site
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ATTACHMENT 3
--- -- -
Sample Event Baseline
Sample ID MW-4S
Date Sampled 12/2/'J6
Performance Standard
Voliltile Oroanks (lJa11 )· _ -·.> -.• ---•
Trichloroethene NA
Pesticides (UP/I ) -·· . ·i· .,
Aldrin 0.05 < 2.5 <
alpha-BHC 0.05 < 2.5 <
beta-BHC 0.05 IS
dclta-BHC 0.05 10 <
gamma-BHC (Lindane) 0.05 < 2.5 <
alpha-Chlordane -< 2.5 <
gamma-Chlordane --< 2.5 <
Dieldrin 0.1 < 5.0
4,4'-DDD --< 5.0 <
4,4'-DDE -· < 5.0 <
4,4'-DDT --< 5.0 <
Endosulfan I --< 2.5 <
Endosulfan II -< 5.0 <
Endosulfan sulfate --< 5.0 <
Endrin -< 5.0 <
Endrin aldehyde -NA <
Endrin ketone 0.1 < 5.0 <
Heptachlor -< 2.5 <
Heptachlor epoxide -< 2.5 <
Methoxychlor -< 25 <
Toxaphene I < so <
Total Pesticides 25
Notes:
-
2Q98
MW-4S
4/21198
NA
2.5
2.5
16
2.5
2.5
2.5
2.5
2 J
5
s
5
2.5
s s
s
s s
2.5
2.5
25
so
18
--- -Table I
Surfkial Aquifer Moniloring Results
Annual Oprrating Report
Geigy Chtrnical Corporation Sile
Aberdeen, North Carolina
4Q98 Baseline 2Q98
MW-4S MW-5S MW-5S
-
10/29198 12/2196 4/21198
-
NA NA NA
'
< 0.55 < 2.5 < 0.5
< 0.55 < 2.5 < 0.5
4.2 17 2.5
2.8 S.6 0.59
< 0.55 < 2.5 0.05 J
< 0.55 < 2.5 < 0.5
< 0.55 < 2.5 < 0.5
0.27 J < 5.0 0.44 J
< I.I < 5.0 < I
< I.I < 5.0 < I
< I.I < 5.0 < I
< 0.55 < 2.5 < 0.5
< I.I < 5.0 < I
< I. I < 5.0 < I
< I.I < 5.0 < I
< I.I < NA < I
< I.I < 5.0 0.27 J
< 0.55 < 2.5 < 0.5
< 0.55 < 2.5 0.07 J
< S.5 < 25 < s
< II < so 15
7.3 23 18.9
Baseline sampling event on December 3, 1996. Extraction system start-up on January 15. 1997.
• r -Estimated value.
NA -Not Analyzed
Page I of3
-- ---.. -
4Q98 Baseline 2Q98 4Q98
MW-5S MW-6S MW-6S MW-6S
10/29198 12/2196 4/21198 10/29198
--------
NA NA NA NA
----.
< 0.59 < 0.50 < 0.5 < 0.56
0.31 J 2.1 2.9 1.8
8.6 5.8 6.6 7.1
2 2.5 6 4.6
0.25 J 1.5 2.4 I.I
0.08 J < 0.50 < 0.5 < 0.56
< 0.59 < 0.50 < 0.5 < 0.56
0.79 J < 1.0 0.58 J 0.25 J
< 1.2 < 1.0 < I < I. I
< 1.2 < 1.0 < I < I.I
< 1.2 < 1.0 < I < I.I
< 0.59 < 0.50 < 0.5 < 0.56
< 1.2 < 1.0 < I < I. I
< 1.2 < 1.0 < I < I. I
< 1.2 < 1.0 < I < I. I
< 1.2 NA < I < I. I
< 1.2 < 1.0 0.62 J < I.I
< 0.59 < 0.50 < 0.5 < 0.56
0.18 J < 0.50 < 0.5 0.12 J
< S.9 < 5.0 < s < 5.6
12 < 10 20 II
24.2 11.9 39.1 26
- ---- --
Sample Evtnt Bauline 2Q98
- -- -
Tablt I
Surficial Aquirrr Monitoring Resulls
Annual Optrating Rtport
Gtigy Chemical Corporation Site
Abudcen, North Carolina
4Q98 Baseline 2Q98
-
Sample ID MW-10S MW-IOS MW-10S MW-16S MW-16S
Date Sampled 12/2196 4/21198 10/29198
Perrormance Standard
Volatile Organics (uu11 ,. > . .
Trichloroethene < 5.0 < 5 < I
Pesticides (lig/L).
Aldrin 0.05 < 0.050 < 0.5 < 0.56
alpha-BHC 0.05 0.03 J 0.39 J 0.09 J
beta-BHC 0.05 0.58 7 4.5
delta-BHC 0.05 0.05 J 1.6 0.41 J
gamma-BHC (Lindane) 0.05 0.070 0.34 J 0.11 J
alpha-Chlordane .. < 0.50 < 0.5 < 0.56
gamma-Chlordane .. < 0.50 < 0.5 < 0.56
Dieldrin 0.1 < 0.10 0.9 J 0.27 J
4,4'-000 -< 0.10 < I < I.I
4,4'-OOE --< 0.10 < I < I.I
4.4'-OOT -< 0.10 < I < I.I
Endosulfan I -< 0.050 < 0.5 < 0.56
Endosulfan II -< O.IO < I < I.I
Endosulfan sulfate -< 0.10 < I < I.I
Endrin -< 0.10 < I < I.I
Endrin aldehyde -NA < I < I.I
Endrin ketone 0.1 < 0.10 1.8 < I.I
Heptachlor -< 0.050 < 0.5 < 0.56
Heptachlor epoxide -< 0.050 < 0.5 < 0.56
Methoxychlor -< 0.50 < 5 < 5.6
Toxaohene I < 1.0 8.4 J < II
Total Pesticides 0.72 20.4 5.4
Notes:
Baseline sampling event on December 3, 1996. Extraction system start-up on January 15, 1997.
•J" -Estimated value.
NA -Not Analyzed
12/2196 4/21198
< 5.0 < 5
.
< 0.050 < 0.05
< 0.050 < 0.05
< 0.050 < 0.05
< 0.050 < 0.05
< 0.050 < 0.05
< 0.50 < 0.05
< 0.50 < 0.05
< 0.10 < 0.1
< 0.10 < 0.1
< 0.10 < 0.1
< 0.10 < 0.1
< 0.050 < 0.05
< 0.10 < 0.1
< 0.10 < 0.1
< 0.10 < 0.1
NA < 0.1
< 0.10 < 0.1
< 0.050 < 0.05
< 0.050 < 0.05
< 0.50 < 0.5
< 1.0 < I
0 0
Page 2 of3
- ----..
4Q98 Baseline 2Q98 4Q98
MW-16S MW-17S MW-17S MW-17S
10/29198 12/2196 4/21198 10/29198
. . . . ..
< I < 5.0 < 5 < I .
< 0.05 < 0.050 < 0.05 < 0.05
< 0.05 < 0.050 < 0.05 < 0.05
< 0.05 < 0.050 < 0.05 < 0.05
< 0.05 < 0.050 < 0.05 < 0.05
< 0.05 < 0.050 < 0.05 < 0.05
< 0.05 < 0.050 < 0.05 < 0.05
< 0.05 < 0.050 < 0.05 < 0.05
< 0.1 < 0.10 < 0.1 < 0.1
< 0.1 < 0.10 < 0.1 < 0.1
< 0.1 < 0.10 < 0.1 < 0.1
< 0.1 < 0.10 < 0.1 < 0.1
< 0.05 < 0.050 < 0.05 < 0.05
< 0.1 < 0.10 < 0.1 < 0.1
< 0.1 < 0.10 < 0.1 < 0.1
< 0.1 < 0.10 < 0.1 < 0.1
< 0.1 NA < 0.1 < 0.1
< 0.1 < 0.10 < 0.1 < 0.1
< 0.05 < 0.050 < 0.05 < 0.05
< 0.05 < 0.050 < 0.05 < 0.05
< 0.52 < 0.50 < 0.5 < 0.52
< I < 1.0 < I < I
0 0 0 0
- - - ----
Sample [vent
Sample ID
Date Sampled
Performance Standard
Volatile Organics (ue11) . .
Trichloroethene <
Prsticides (UP/I ) .
Aldrin 0.05 <
alpha-BHC 0.05 <
beta-BHC 0.05 <
dclta-BHC 0.05 <
gamma-BHC (Lindane) 0.05 <
alpha-Chlordane --<
gamma-Chlordane -<
Dieldrin 0.1 <
4,4'-DDD -<
4,4'-DDE --<
4,4'-DDT --<
Endosul fan I -<
Endosulfan II -<
Endosulfan sulfate -<
Endrin -<
Endrin aldehyde -
Endrin ketone 0.1 <
Heptachlor --<
Heptachlor epoxide --<
Methoxychlor --<
Toxaphene I <
Total Pesticides
Notes:
-
Baseline
MW-18S
12/2196
.. ..
5.0
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.10
0.10
0.10
0.10
0.050
0.10
0.IO
0.10
NA
0.10
0.050
0.050
0.50
1.0
0
- --Table I
Surficial Aquifer Monitoring Results
Annual Operating Report
Geigy Chemkal Corporation Site
Aberdeen, North Carolina
2Q98 4Q98
MW-18S MW-18S
4/21198 10/29198
.
< 5 < I
< 0.05 < 0.06
< 0.05 < 0.06
< 0.05 < 0.06
< 0.05 < 0.06
< 0.05 < 0.06
< 0.05 < 0.06
< 0.05 < 0.06
< 0.1 < 0.12
< 0.1 < 0.12
< 0.1 < 0.12
< 0.1 < 0.12
< 0.05 < 0.06
< 0.1 < 0.12
< 0.1 < 0.12
< 0.1 < 0.12
< 0.1 < 0.12
< 0.1 < 0.12
< 0.05 < 0.06
< 0.05 < 0.06
< 0.5 < 0.59
< I < 1.2
0 0
-
Baseline sampling event on December 3, 1996. Extraction system start-up on January 15, 1997.
"J" • Estimated value.
NA -Not Analyzed
Page J of3
-- - -.. iiill -
- - -- --
Sample Event Bastline 2Q98
Sample ID MW-11D MW-IID
Datt Sampled 12/2196 4/21/98
Pe.-formann Standard
Volatile Organics (a2/L), .. ..
Trichlorocthene NA NA
Pestiddr, (ug/L)
Aldrin 0.05 < 0.50 < 0.05
alpha-BHC 0.05 3.7 0.14
beta-BHC 0.05 5.0 0.52
delta-BBC 0.05 1.5 0.14
gamma-BHC (Lindane) 0.05 1.6 0,05 J
alpha-Chlordane .. < 0.50 < 0.05
gamma-~hlordane .. < 0.50 < 0.05
Dieldrin 0.1 < 1.0 0.05 J
4.4'-DDD --< 1.0 < 0.1
4,4'-DDE .. < 1.0 < 0.1
4,4'-DDT .. < 1.0 < 0.1
Endosulfan I .. < 0.50 < 0.05
Endosulfan II --< 1.0 < 0.1
Endosulfan sulfate .. < 1.0 < 0.1
Endrin .. < 1.0 < 0,1
Endrin aldehyde .. NA < 0.1
Endrin ketone 0.1 < 1.0 0,06 J
Heptachlor .. < 0.50 < 0.05
J-leptachlor epoxide .. < 0.50 < 0,05
Methoxychlor .. < 5.0 < 0.5
Toxaohcne 1.0 < 10 < I
Total Pesticides 11.8
Notes:
-- - --
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
Table 2
Uppu Black Crttk Aquifer Monitor-ing Resull!i
Annual Operating Report
4Q98
MW-IID
10/29/98
NA
0.53
1.6
4.9
0.98
0.52
0.53
0.53
0.21
I.I
I.I
I.I
0.53
I.I
I.I
I.I
I. I
I. I
0.53
0.53
5.3
II
8.2
Geigy Chemical Corporation Silt
Abttdten, North Carolina
BHrlint 2Q98
MW-16D MW-16D
12/1/96 4/21/98
230 290
< 0.050 < 0.05
< 0.050 < 0.05
< 0.050 < 0.05
< 0.050 < 0.05
J < 0.050 < 0.05
< 0.050 < 0.05
< 0.050 < 0.05
J < 0.10 < 0.1
< 0.10 < 0.1
< 0.10 < 0.1
< 0.10 < 0,1
< 0.050 < 0.05
< 0.IO < 0.1
< 0.10 < 0.1
< 0.10 < 0.1
NA < 0.1
< 0.10 < 0.1
< 0.050 < 0.05
< 0.050 < 0.05
< 0.50 < 0.5
< 1.0 < I
0 0
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
Baseline sampling event on December 3, 1996. Extraction system start-up on January 15, 1997.
• J" • Estimated result.
Page I of2
-- - - - --
4Q98 Baseline 2Q98 4Q98
MW-16D MW-17D MW-17D MW-17D
10/29/98 12/1/96 4/21/98 10/29/98
'.
270 320 320 350
0.05 < 0.050 < 0.05 < 0.058
0.05 < 0.050 < 0.05 < 0.058
0.05 < 0.050 < 0.05 < 0.058
0.05 < 0.050 < 0.05 < 0.058
0.05 < 0.050 < 0.05 < 0.058
0.05 < 0.050 < 0.05 < 0.058
0.05 < 0.050 < 0.05 < 0.058
0.11 < 0.10 < 0.1 < 0.12
0.11 < 0.10 < 0,1 < 0.12
0.11 < 0.IO < 0,1 < 0.12
0.11 < 0.10 < 0.1 < 0.12
0.05 < 0.050 < 0.05 < 0.058
0,11 < 0.10 < 0,1 < 0.12
0.11 < 0.10 < 0.1 < 0.12
0.11 < 0.10 < 0.1 ·< 0.12
0.11 NA < 0.1 < 0.12
0.11 < 0.10 < 0,1 < 0.12
0.05 < 0.050 < 0.05 < 0.058
0.05 < 0.050 < 0.05 < 0.058
0.53 < 0.50 < 0.5 < 0.58
I.I < 1.0 < I < 1.2
0 0 0 0
- - - - -
Sample Evtnt
Sample ID
Date Sampled
Performante Standard
Volatile Organics (ug/L)
Trichlorocthene
PestitidH (ug/L) ,.
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4,4'-DDE
4,4'-DDT
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epox:ide
Methoxychlor
Toxaohcne
Total Pesticides
Notes:
---- --
Hanline
MW-18D
1212/96
< 5.0
< 0.50
4.6
5.9
1.0
2.8
< 5.0
< 5.0
< 1.0
< 1.0
< 1.0
< 1.0
< 0.50
< 1.0
< 1.0
< 1.0
NA
< 1.0
< 0.50
< 0.50
< 5.0
< JO
20.3
Table 2
Upper Black Crrek Aquif«-r Monitoring Result,
Annual Operating Report
<
<
<
<
<
<
<
<
<
<
<
<
<
<
Geigy Chemital Corporation Site
Aberdeen, North Carolina
2Q98 4Q98
MW-18D MW-18D
4/21/98 10/29/98
6.2 4.2
.
0.5 < I
1.7 1.6
6.5 8.2
1.6 1.9
I.I I
0.5 < I
0.5 < I
0.66 J 0.5 J
I < 2
I < 2
I < 2
0.5 < I
I < 2
I < 2
I < 2
I < 2
I.I < 2
0.5 < I
0.08 J < I
5 < JO
JO < 20
12.7 13.2
Bauline
MW-3-0D
12/2/96
NA
< 0.50
2.8
6.3
2.4
I.I
< 0.50
< 0.50
< 1.0
< 1.0
< 1.0
< 1.0
< 0.50
< 1.0
< 1.0
< 1.0
NA
< 1.0
< 0.50
< 0.50
< 5.0
< 10
12.6
Baseline sampling event on December 3, 1996. Extraction system start-up on January 15, I 997.
"r -Estimated result.
Page 2 of2
-- ---
2Q98 4Q98
MW-30D MW-30D
4/21/98 10/29/98
NA NA
< 0.5 < I
I.I 2.3
4.8 9.8
I 2
0.73 0.15 J
< 0.5 < I
< 0.5 < I
0.51 J 0.5 J
< I < 2
< I < 2
< I < 2
< 0.5 < I
< I < 2
< I < 2
< I < 2
< I < 2
0.81 J < 2
< 0.5 < I
< 0.5 < I
< 5 < 10
< JO < 20
9 15.4
- - - -
Sample Event
Sample ID
Date Sampled
Performance Standard
.Volatile 0'ltBDicS (UP/I )
Trichloroethene
Pesticides (uo/1 ) ·
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha..Chlordane
gamma.Chlordane
Dieldrin
4,4'-DDD
4.4'-DDE
4,4'-DDT
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Meptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Total Pesticides
Notes:
"J" -Estimated value.
NA -Not analyzed.
.
-·-
0.05
0.05
0.05
0.05
0.05
--
0.1 ----..
---
0.1 ---
1.0
---
2Q98 JQ98
V47 (Train A) V48 (Train A)
4121198 7122198
. ' ~,· ';;·· ,;,:.
4.2 J 0.56 J ..
< 0.05 < 0.05
0.2 < 0.05
0.61 < 0.05
0.25 < 0.05
0.11 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
0.077 J < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.05 < 0.05
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
<· 0.1 < 0.1
0.1 < 0.1
< 0.05 < 0.05
< 0.05 < 0.05
< 0.5 < 0.5
0.86 J < I
2.2 0
- ---- -
Table 3
Trutment Plant Monitoring Results
Annu~I Optrating Report
Geigy Chemical Corporation Site
Aberdeen. North Carolina
Effluent From Lead Carbon Canisters
4Q98 IQ99 2Q98
LudC.U.A V-49 (Train A) V-50 (Train 8)
J0/27198 1/14199 4121198
.
0.23 J 1.3 2.9 J . . .
< 0.05 < 0.05 < 0.05
< 0.05 0.031 J 0.094
< 0.05 0.11 0.3
< 0.05 0.034 J 0.1
< 0.05 0.013 J 0.041 J
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.1 < 0.1 0.031 J
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.05 < 0.05 < 0.05
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 < 0.1 < 0.1
< 0.1 NA 0.052 J
< 0.05 < 0.05 < 0.05
< 0.05 < 0.05 < 0.05
< 0.5 < 0.5 < 0.5
< I < 2 < I
0 0.2 0.6
Page I of2
JQ98
V5I (Train 8)
7122198
r_.;_ . ·-·
0.38 J
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.1
< 0.1
< 0.1
< 0.1
< 0.05
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.05
< 0.05
< 0.5
< I
0
.. -.. -
4Q98 IQ99
LndC.U.B V-52 (Train B)
J0/27198 1/14199
--. . .-, . . "' --
< I < I
--":
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.05 < 0.05
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.05 < 0.05
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 < 0.1
< 0.1 NA
< 0.05 < 0.05
< 0.05 < 0.05
< 0.5 < 0.5
< I < 2
0 0
- -- -- - - - - - -
Tablt J
Trratmrnt Planl Monitoring Results
Annual O~rating Report
Grigy Chemical Corporation Sitt
Abtrdttn, North Carolina
-
Final Effluent
Sample Event
Sample ID
Date Sampled
Performance Standard
Volatile _Onranits (uP/1 )
Trichloroethene
Pesticides ( 0111/L)
Aldrin
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Dieldrin
4,4'-DDD
4.4'-DDE
4,4'-DDT
Endosulfan I
Endosulfan'II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Total Pesticides
Notes:
•r -Estimated value.
NA -Not analyzed.
-
0.05
0.05
0.05
0.05
0.05
--
0.1
----
--------
0.1
---
1.0
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
<
2Q98 JQ98
V-54 V54
4/21/98 7/22/98
' ,.
5 < 5
0.05 < 0.05
0.05 < 0.05
0.05 < 0.05
0.05 < 0.05
0.05 < 0.05
0.05 < 0.05
0.05 < 0.05
0.1 < 0.1
0.1 < 0.1
0.1 < 0.1
0.1 < 0.1
0.05 < 0.05
0.1 < 0.1
0.1 < 0.1
0.1 < 0.1
0.1 < 0.1
0.1 < 0.1
0.05 < 0.05
0.05 < 0.05
0.5 < 0.5
I < I
0 0
Page 2 of2
-- - --..
4Q98
Effluent
10/27/98
,. . .,._,.
< I
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.1
< 0.1
< 0.1
< 0.1
< 0.05
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.05
< 0.05
< 0.5
< I
0
n
0 n,
n
n
,0
i 0
' I :o
I
'
D
0
Q
Q
l[j
0
0
[ '
[ .
[
0
ATTACHMENT4
-------------------
-..:I oil :,
~
C 0 -= .. .. -C .. ..
C 0 u
MW-4S Beta-BHC Concentration
20 ·.------------------------------------~
•
15 ♦
to
•
• •
5
•
O'-------------------------~-----------'
Date
♦ Sample result
-Linear Fit
-------------------
C 0 ·-~ ~ C
8
MW-5S Beta-BHC Concentration
18 .-------------------------------~
♦
16
14
12
10
8
6
4
2 ♦
0 -t---r---.-----,----.---r---r----,----r---r---.----,----'
Date
• . Sample result
-Linear Fit
-------------------
---~ = -= .s -.. .. -= .. " = 0 u
MW-6S Beta-BHC Concentration
8
7 ♦
♦ ♦
6 ♦
5.
4 ♦
♦
3
2.
1 .
01----....---....---....---....---....---....---....---....---....---....---....--'
~" ~ ~-t
Date
♦ Sample result
-Linear Fit
--- -.. - - -.. -- - - - - -.. .. ..
C .!: -f -C fl C
8
MW-10S Beta-BHC Concentration
8-.---------------------------------,
7 •
6
5 -
4
3 -
2 •
1 -
•
0
~ 5'1"°' (\ 5'1"°' (\ (\ (\ 5','l::, R, 5','l::, R, R, -'1,:,;, t:°' ~°' ..:°' r§f°' t:°' ~°' ..:""' ~q;; ~~ ~~ \'§I' ~-::; c:f ~ ~~ ~~ \~~ ~-::; c(.;
Date
♦ Sample result
-Linear Fit
._ -1!11!!!1 -~ -fliiiil -----------iilll
•
-~ :,
~
C .s -.. .. -C .. ... C 0 u
0.050
0.045
0.040
0.035
0.030
0.025
0.020
0.015
0.010
0.005
MW-16S Beta-BHC Concentration
-+-Sample result
-Linear Fit
Date
Note: All results were below the method detection limit. Results shown are 1/2 of the method detection limit.
-IIDl!!Y ;;ii .... _ --'-'liiil ---~-->---
C
0
0.045
0.040
0.035
0.030
·.::: 0.025 f ..
C ~ 0.020
C 0 U 0.015
0.010
0.005
MW-17S Beta-BHC Concentration
Date
♦ Sample result
-Linear Fit
Note: All results were below the method detection limit. Results shown as 1/2 of the method detection limit.
MW-18S Beta-BHC Conentration
0.050 --------------------------------
0.040
-~ 0.030 = -C Q • • Sample result -~ .. .. .. -Linear Fit .. .,
C 0.020 " C
Q u
0.010
0.000 --------------------------------'
\:)lo \:'I" ~~f ~~-
Date
-~ ::, ._,
= .5l -" .. -= .. .. = 0 u
MW-11D Beta-BHC Concentration
6.0 ..---------------------------------,
5.0 • • •
• 4.0
3.0
2.0
1.0
•
0.0 ---------------------------------'
~lo ~ ~~
Date
• Sample result
-Linear Fit
0.050
0.045
0.040
0.035
~ ~ 0.030 ::, -C " ., 0.025 E -C .. u 0.020 C
" u
0.015
0.010
0.005
MW-16D Beta-BHC Concentration
Date
1111;, _____ , ___
♦ Sample result
-Linear Fit
Notes: All results were below the method detection limit. Results shown are 1/2 of the method detection limit.
0.050
0.045
0.040
0.035 -~ 0.030 ::,
~ ·" ~ 0.025 .. .. -.. .. 0.020 .. .. 0 u 0.015
0.010
0.005
MW-17D
Beta-BHC Concentration
Date
♦ Sample result
-Linear Fit
Notes: All results were below the method detection limit. Results shown are 1/2 of the method detection limit.
MW-18D Beta-BHC Concentration
9
8 • • • • 7
• ,-. 6 ~ •
= -= 5 .5l • Sample result -.. .. 4 -Linear Fit -= .. .. = 0 3 u
2
1
0
~lo 'i'i'°' ~ ~" ~ ~ ~" 'i','b ~ ~'b ~'b ~
~ ~~ ~'i', ~ ~~°' ..:°' ~ ~~ ~'i', '3~~ ~ ..:"" ~'l, ~~ '3~ -~-C" ~'l, ~~ ~~ C"
Date
,--.
~ = -= .Sl -= .. -= ..
" = 0 u
MW-30D Beta-BHC Concentration
12 ..------------------------------,
10 ♦
8
♦
6
♦
4
2
0---------------------------------' ~" ~ ~"'
Date
♦ Sample result
-Linear Fit
n
n
! []
I a
C
. G
0
·o
0
·. c·
0
0
D
0
0
0
D
,8
·n
ATTACHMENT 5
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SURFICIAL AQUIFER MONITORING WELL
MW-4S
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonal formt
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ ...,Ge,ee,igy"-"C"'he,eme,k"'•ecl C,c:o,,_rp.,,o,,_rae,t,sio,,.n ________ _
Address ___________ ..,D<,oe,me,ln,,,o_eD"'ri"'ve,_ _________ _
----~A=be~r~dee~•=N~C~283=t~s~---County, ____ .aMu,oo,na:a:_.. __ _
DIVISION OF WATER QUALITY. GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828·0578
(919) 733·3221
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NPDES ___________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
Well Location, _________________________ _ (REQUIRED) Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-4S Well Dep1h •1 27 Fl.
Well Diameter 2 o Sample (Screened) Interval 22 87 Ft. To 39 87 Ft.
Depth to Water Level 2B 82 ft. below measuring point (before sampling)
Measuring point is 2 62 ft. above land surface
Gallons of water pumped/bailed before samplinn lt.S
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application of Sludge
_X_ather
Rotary Distributor
Field Analysis: pH s,31 Specific Conductance 85 uMhos Temp. 18 °c Odor ___ Appearance, __ _
Date Sample Collected 4/llt28 Date Lab Sample Analyze,u.. _______ _
LabOratory Name Quanterra, West Sacramento, CA Certification No. ___ 2..,J"'61i"---
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND AELD ACIDIFIED __ YES __ NO
COD ______________ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrite (N02) as N _______ mg/I
Nitrate (N03) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total mg/I
pH (when analyzed) units
TOG mg/I
Chloride mg/I
Arsenic mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Mg -Magnesium mg/I
Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke,c.._ __________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8196
Date
• See back for Instructions.
" Submit blue and yellow copies only lo address above.
------ ---· -------·--·-
E A R T H © T E C H Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/04/21 Casing Diameter 2.0 Inches
Field Personnel R. Morgan I B. Dillard Casing Material Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 473.47 11100ft
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.67 1/100 ft
Well ID# MW-4S Land Surface Elevation 470.80 1/100 ft
D Upgradient l!!I Downgradient D Sidegradient Screened Interval 29.87 -39.87 1/100 ft
Weather Conditions Clear, Mild Dedicated Pump or Bailer l!!I Yes □No D Type Well Wizard
Air Temperature 65 •F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Well Depth (TWO) = 41.97 1/100 ft Locking Cap l!!I Yes □No
Depth to Ground Water (DGW) = 28.89 1/100 ft Protective Post/Abubnent □Yes l!!I No
Length of Water Column (LWC) a TWO • DGW = 13.08 1/100 ft Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCV) = LWC x 0.17 a 2.22 gal Well Yield □Low l!!I Moderate □High
3 Casing Volumes = 6.67 gal = Standard Evacuation Volume CommentsfObservations
Method of Well Evacuation Well Wizard Purged 5 volumes to decrease turbidi~.
Method of Sample Collection Well Wizard
Total Volume of Water Removed 11.5 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 2.25 4.5 6.75 9.0 11.5
TIME (military) 9:42 9:54 10:10 10:22 10:37 10:48
pH (S.U.) 5.95 5.40 5.33 5.27 5.22 5.31
Drawdown (ft.) - - -- - -
Sp. Cond. (l'mhoslcm) 141 92 87 86 85 85
Water Temp. ("C) 18 18 18 18 18 18
TURBIDITY (NTU)• 317 169 56 36 25 15
• Nenhalomatr1,:: Turbj.titu •• _..._ Refill: B Discharge: A 1/2
.
fOMMENTS/OBSERVATIONS SAMPLED AT 1100
I
Field Data/or GW
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Q" Puanterra
Environmental TCL Organochlorine Pesticides/PCBs Services
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-4S
Lab ID: 098752-0003-SA Matrix:
Authorized:
AQUEOUS Sampled: 21 APR 98 Received: 22 APR 98 22 APR 98 Prepared: 23 APR 98 Analyzed: 22 MAY 98
Parameter Result Units Rerorting imi t
alpha-BHC ND ug/L beta-BHC 16 ug/L delta-BHC ND ug/L gamma-BHC (Lindane) ND ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin 2.0 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4, 4' -ODD ND ug/L Endosulfan sulfate ND ug/L 4,4' -DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone ND ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene ND % Decachlorobiphenyl ND %
Note o Reportin~ limit(s) raised due to high level of analyte present 1n sample.
Note J
Note H
Result is detected below the reporting limit or is an estimated concentration.
Spiked analyte not detected because of required sample dilution.
ND a Not detected
NA= Not applicable
2.5
2.5
2.5
2.5
2.5
2.5
2.5
2.5 2.5 2.5
5.0 5.0
5.0 5.0 5.0 5.0 5.0 5.0 5.0
25 50
Reported By: Lisa Stafford Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
0
J
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-------------------
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
COMPLIANCE REPORT FORM
For additional forms
phta3e write or call:
RALEIGH, NC 27628·0578
[phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name ________ ___oGc;e;,.gY,_C;chc;em"',"'.ca"'-l-"'C"'oryo=ra,,,t,,cio,,_n _______ _ Non-Discharge WQ 0009949
Address ___________ _,,D,,,om,,,i,,,no,,D"-'n,.,_·v,_e _________ _ NPDES.,.,.......,.,=,..,..,,=---::--:::-:-c-:::-:-:=-=:: TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) ___ _,A""h""erc,edee=.,,n""N"'C~28=31e.e5 ____ County ___ ~Mwoo&a:~---
Well Location ________________________ _
Well Identification Number MW-4S Well Depth 41 27 Ft.
Well Diameter 2 o Sample (Screened) Interval 29,87 Ft. To 32 87 Ft.
Depth to Water Level 35 •• ft. below measuring point (before sampling)
Measuring point Is 2 •z ft. above land surface
Gallons of water pumped/bailed before samplin,._~---~4 ____ _
Lagoon
Spray Field
__ Septic Tank/Drain Field
__ Subsurface Low-Pressure
Piping (LPP)
Land Application ol SludQe
_X_Other
Rotary Distributor
Field Analysis: pH s.1 Specific Conductance ss uMhos Temp. JB 0c Odor ___ Appearance __ _
Date Sample Collected rn12212s Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. __ _.2~um.._ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/I Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
· Nitrate (NO3 ) as N mg/l
Phosphorus: Total as P mg/I
(N-: U"" MPN method for highly turbid aamplea) Al -Aluminum mg/I
Dissolved Solids: Total mg/1 Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOC mg/l Cd -Cadmium mg/I
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu -Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe -Iron mg/l
Hg-Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I Mg -Magnesium mg/I
Specific Conductance uMhos Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke.__ _________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached ug/1 ~--~-~~-~-----
--------------ug/1
~------------ug/1 Other (Specify Compounds and
Concentration untts)
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agenr)
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
-- - ----- ---- ---- -- -
Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/10/29 Casing Diameter 2.0 Inches
Field Personnel R. Moraan / N. Hicks Casing Material Stainless Steel
' Site Name Geigy Chemical Corporation Measuring Point Elevation 473.47 1/100 fl
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.67 1/10011
Well ID# MW-4S Land Surface Elevation 470.80 1/100 fl
D Upgradient D Downgradient D Sidegradient Screened Interval 29.87 -39.87 1/10011
Weather Conditions Sunnv Dedicated Pump or Baller l!!I Yes □No □Type
Air Temperature 55 •F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Well Depth (TWO) = 41.97 1/100 fl Locking Cap l!!I Yes □No
Depth to Ground Water (DGW) = 35.68 1/10011 Protective PosUAbutment □Yes l!!I No
Length of Water Column (LWC) = TWO -DGW = 6.29 1/10011 Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (DCV) = LWC x 0.163 = 1.03 gal Well Yield □Low l!!I Moderate □High
3 Casing Volumes = 3.08 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard Pesticides
Method of Sample Collection Well Wizard
Total Volume of Water Removed 4 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 1 2 3 4
TIME (military) 8:17 8:28 8:38 8:48 8:58
pH (S.U.) 5.12 5.29 5.26 5.13 5.10
Drawdown (fl.) -- --
Sp. Cond. (µmhos/cm) 92 75 62 55 55
Water Temp. (°C) 19 18 18 18 18
TURBIDITY (NTU)' 143 116.1 26.7 13.3 8.57
•_Na"helomP.trlc: T••rhldftv Units · Refill: B Discharge: A
EOMMENTS/OBSERVATIONS Sameled at 0900. I
Field Data/or GW
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Client Name:
Client ID:
LAB ID: Matrix:
Authorized:
Rust Environmental
MW-4S
302434-0014-SA AQUEOUS
30 OCT 98
Dilution Factor: 10
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane}
alpha-Chlordane
gamma-Chlordane Heptachlor
Aldrin Heptachlor epoxide
Endosulfan I
Dieldrin 4,4'-DDE
Endrin
Endosulfan II
4,4'-DDD
Endosulfan sulfate 4,4'-DDT
Endrin aldehyde
Endrin ketone
Methoxychlor Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
lj}\ ,euanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
ND ug/L 4.2 ug/L
2.8 ug/L ND ug/L ND ug/L ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L
0.27 ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Recovery
ND%
ND%
Received: 30 OCT 98
Analyzed: 17 NOV 98
Reporting
Limit
0.55
0.55
0.55
0.55
0.55 0.55
0.55
0.55
0. 55 .
0.55 I. I I.I I.I I. I
1.1
I . 1
I. I I.I
LI
5.5
11
MDL
0.088
0.044
0.066
0.11
0.077
0.088 0.077
0.066 0.088
0. 11
0.22
0 .16
0.22 0.32
0.055 0.36
0.22
0.32
0. 26
0.44
11
Qualifier
oR
J
Acceptable Range
55 115 H
35 -137 H
Note
Note
Note
Note
ND=
H = Spiked analyte not
J = Result is detected
o = Reporting limit(sl R = Reporting limit(s
Not. Detected
detected because of required sample dilution.
Reported By: Lisa Stafford
below the reporting limit or is an estimated concentration.
raised due to high level of analyte present in sample.
raised due to sample volume limitations.
Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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SURFICIAL AQUIFER MONITORING WELL
MW-5S
-------------------
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ _,G,_,e,.igy'-"Ch""c""m""ic,::a,_;I C"'o::.rec:•c:;ra::.:l:,:io::.n ________ _
Address ___________ _.D,,,o,::m,eine,o_,,D,_,rie.,ve~----------
----~A=h•=•=dce=n=N=C~28=31=5 ____ County ____ ~Mwoowr~•----
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626·0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPOES.,.,..--,,-=,,..,,,,,,,.,..,----,-,,---==== ~F DISPQSAL OPERATION BEING MONITORED
(REQUIRED) Well Location __________________________ _ Lagoon __ Septic Tank/Drain Freid
Well Identification Number MW-5S Well Depth 47 44 Ft.
Well Diameter 2 o Sample (Screened) Interval 35.24 Ft. To 45 24 Ft.
Depth to Water Level 30 7J ft. below measuring point (before sampling)
Measuring point is , 14 ft. above land surface
Gallons of water pumped/bailed before samplin,"s,..---~9~-0 ____ _
Spray Field __ Subsurface Low-Pressure
Piping (LPPJ
Land Application ol Sludge
_X_Other
Rotary Distributor
Field Analysis: pH 4.52 Specific Conductance 38 uMhos Temp. JB 0 c Odor ___ Appearance __ _
Date Sample Collected 4121(28 Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. --~2uJ~66,_ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES NO
COD -----,--,=-::c---,--------mg/I
Coliform: MF Fecal /100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Coliform: MF Total /1 00ml Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samp~s) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG mg/I
Chloride mg/I
Arsenic mg/I
Cd • Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Grease and Oils mg/I Fe -Iron mg/I
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I Mg • Magnesium mg/I
Specific Conductance uMhos Mn • Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke.__ _________ mg/I
Pb · Lead mg/I
Zn • Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should.reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent')
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
------
EARTH©TECH
-- --------- -
Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yrlmo/day) __________ .;;.98"1-"04-'-/"'2:..1 ________ _ Casing 0iameter ___________ ...;2=:·..::0 ________ lnches
Field Personnel ________ R_._M_o_r~g~a_n_l_B_. _D_ill_a_rd ______ _ Casing Material __________ s_1a_in_Ie_s_s_s_1e_e_I ________ _
Site Name __________ G_e..,igy~C_h_em_ica_l_C_o~rp_o_ra_ti_on ______ _ Measuring Point Elevatlon ________ 4_7_1_.34 ________ 11100 ft
Earth Tech Job Number ________ _,3'-'1.,,_8_.19=----------Height of Riser (above land surface) 3.14 11100 ft
Well ID # ____________ -"M:..W.c.·..::5..::S _______ _ Land Surface Elevation 468.20 11100 ft
D Upgradient 11!1 Downgradient D Sidegradient Screened Interval 35.24 -45.24 11100 ft
Weather Condltlons, ________ .=C.:.:le:=a"'r,'-"S::.;u"n"'n"-y ________ _ Dedicated Pump or Baller 11!1 Yes □No □ Type Well Wizard
Air Temperature ___________ 7--'5'----------•F Steel Guard Pipe Around Casing 11!1 Yes □No D Flushmounted
Total Well Depth (TWO) = ________ 4-"7'-'.44.:....;. _______ 11100 ft Locking Cap 11!1 Yes □No
Depth to Ground Water(DGW) = 30.71 11100 ft Protective Post/Abubnent □Yes 11!1 No
Length of Water Column (LWC) = TWO • DGW = ____ 1_6_. 7_3 ____ 11100 ft Well Integrity Satisfactory 11!1 Yes □No
1 Casing Volume (OCV) = LWC x 0.17 = ______ 2_.84 ______ gal WellYleld □Low D Moderate 11!1 High
3 Casing Volumes = 8.53 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuatlon, _______ .....:cW.:cee,I:..I W:..:..::iz,,,a::.;rd"-------
Method of Sample Collectlon. _______ W=e~ll...:W=iz~a'-'rd~------
Total Volume of Water Removed 9.0 gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (fl)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY (NTU)•
0
14:25
4.37
-
53
17
24.4
3 6 9
14:50 15:10 15:30
4.55 4.56 4.52 .
- - -
37 38 38
17 18 18
3.86 0.98 1.10
Refill: A 1/2 Discharge: A 1/2
COMMENTS/OBSERVATIONS ..::SccA:.cM;;.P-=LE=D::...:..A'-'-T--'1.;;.53"-'5'---------------------------------------i
-
Field Data for GW
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Client Name: Client ID:
Lab ID:
TCL Organochlorine Pesticides/PCBs
Method 8080
Rust Environmental & Infrastructure MW-5S
098752-0015-SA
lj~\ ~uanterra
Environmental
Servjces
Matrix: AQUEOUS Sampled: 21 APR 98 Received: 22 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98 Analyzed: 14 MAY 98
Parameter Result
Reporting
Units
alpha-BHC ND ug/L beta-BHC 2.5 ug/L delta-BHC 0.59 ug/L gamma-BHC (Lindane) 0.050 ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L A 1 dri n ND ug/L Heptachlor epoxide 0.068 ug/L Endosulfan I ND ug/L Dieldrin 0.44 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endri n ketone 0.27 ug/L Methoxychlor ND ug/L Toxaphene 15 ug/L
Surrogate Recovery
Tetrachloro-m-xylene % Decachlorobiphenyl %
Note o Reportin~ limit(s) raised due to high level of analyte present 1n sample.
Note J Result is detected below the reporting limit or
is an estimated concentration.
Note H Spiked analyte not detected because of required sample dilution.
ND= Not detected NA= Not applicable
Limit
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50 0.50
0.50
1.0
1.0
1.0
1.0
1.0 1.0
1.0
1.0
1.0 5.0 10
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
0
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J
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J
H H
------------ - --- - - -
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For eddltlonal forms
please write or eall:
Type or Use a ball-point pen and press firmly.
Facility Name _________ __:cG:.:c•i,..gy,_C:c:ch:::•:::m:::k:al,__,Ce,oe.,rpo=ra,,,Hcc••"---------
Address ____________ _,D,.,,o,eme,in,,,o_,,Decrie.,vee.... _________ _
____ ,.A,,,hes,.rd_,ee"'n"'-'-'N"'C~28-=31..,.S._ ___ County, ____ ~Mwoowc.._, ___ _
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27628-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949
NPDES-,-....,,=,,..,-,=====-=== JYPE OF DISPQSAL OPERATION BEING MONITORED
(REQUIRED) Well Location _________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-SS Well Depth 47 44 Ft.
Well Diameter 2 o Sample (Screened) Interval 35.24 Ft. To 45 24 Ft.
Depth to Water Level 38 21 ft. below measuring point (before sampling)
Measuring point Is J 14 ft. above land surface
Gallons of water pumped/bailed before samplin~----~4=•s ____ _
Spray Field __ Subsurface low-Pressure
Piping (LPP)
Lend Application of Sludge
_X_Other
Ro1ary Distributor
Field Analysis: pH 4.24 Specific Conductance 61 uMhos Temp. 16 °c Odor ___ Appearance __ _
Date Sample Collected lQ/29198 Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ___ 2ul~66~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/1 Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal /1 00ml
Coliform: MF Total 1100ml
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use UPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/1 Ba -Barium mg/I
pH (when analyzed) units Ca • Calcium mg/I
TOG mg/I Cd • Cadmium mg/I
Chloride mg/1 Chromium: Total mg/I
Arsenic mg/I Cu • Copper mg/I
Grease and Oils mg/1 Fe • Iron mg/I
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/1 K • Potassium mg/I
Sulfate mg/I Mg · Magnesium mg/I
Specific Conductance uMhos Mn • Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke'-----------mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
-'T'-'C'-=L'-'P-"es'-'ti"'ci:.:cdes=-•-"res"'u'-'lo'-'s"-atc=taoa<h'"edc=... _____ ug/I
Other (Specify Compounds and
Concentration units)
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. -~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8196
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
---------- -- --- - --
EARTH©T EC H Field Data Information Log for Ground Water Sampling
Page_1_of 1
Date (yr/molday) ___________ 9_81_1_0_12_9 ________ _ Casing 0lameter ___________ ...;2~·.:.0 ________ Inches
Field Per..onnel _________ R_. _M_o~,g~a_n_/_N_._H_i_ck_s~------casing Material __________ s_ta_in_Ie_s_s_s_Ie_e_I ________ _
Slte Name __________ Ge......,ig~y_C_h_em_ica_l_C_o...;rpc...o_ra_t_io_n _____ _ Measuring Point ElevaUon ________ 4_7_1_.34 ________ 1/100 ft
Earth Tech Job Number ________ ..,,3c.,.1,,_8"'19e_ ________ _ Height of Riser (above land surface) 3.14 1/100 ft
Well ID # MW-5S Land Surface Elevation 468.20 1/100 ft -------------------------□ Upgradient D Downgradient D Sidegradient Screened Interval 35.24 -45.24 1/100 ft
Weather CondlUons ________ C_l_e_ar_i_S_u_n_n~y ________ _ Dedicated Pump or Bailer l!!I Yes □No □Type
Air Temperature ___________ 5'-'5~---------"F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Well Depth (lWD) = ________ 4_7_._44 ________ 1/100 ft Locking Cap l!!I Yes □No
Depth to Ground Water (DGW) = 38.21 1/100 ft Protective Post/Abutment □Yes l!!I No
Length of Water Column (LWC) = lWD-DGW = ____ 9_._2_3 ____ 1/100 ft Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCV) = LWC x 0.163 = 1.50 gal WellYleld □Low l!!I Moderate □High
3 Casing Volumes= 4.51 gal= Standard Evacuation Volume Comments/Observations
Method of Well Evacuatfon _______ ~W~e~ll-'W=iz~•~rd~------Pesticides
Method of Sample CollecUon..._ ______ W=e"'ll-'W.,_iz=a""r'-=d..._ _____ _
Total Volume of Water Removed 4.5 gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. ("C)
TURBIDITY (NTU)•
Units
0
9:58
4.33
-
69
17
89
1.5
10:13
4.25
-
62
16
4.14
Refill: B
3.0 4.5
10:28 10:43
4.21 4.24
- -
60 61
16 16
1.54 1.28
.
Discharge: A
'COMMENTS/OBSERVATIONS ..:S:.::a::.:m;.cpc.:le;.::dc..;a:.:.t_;.1.:.04.:.:5:.:.· ______ -=-----------------------------------1
-
Field Data for G W
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IJ\ ,,uanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-5S
LAB ID: 302434-0004-SA
Matrix: AQUEOUS
Authorized: 30 OCT 98
Dilution Factor: 10
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin Heptachlor
Endosulfan
epoxide
I
Dieldrin
4,4' -ODE
Endrin
Endosulfan I I
4, 4' -ODD
Endosulfan sulfate
4,4'-DDT
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
Note H
Note J
Note o
Note R
ND= Not
= Spiked analyte not
Result is detected
= Reporting limit(sl = Reporting limit(s
Detected
·Reported By: Lisa Stafford
Sampled: 29 OCT 98 Received: 30 OCT 98 Prepared:_ 02 NOV 98 Analyzed: 16 NOV 98
Reporting Result Units Limit MDL Qualifier
0.31 ug/L 0.59 0.094 JoR 8.6 ug/L 0.59 0.047
2.0 ug/L 0.59 0,071
0.25 ug/L 0.59 0:12 J 0.078 ug/L _ 0.59· 0.082 J ND ug/L 0.59 0.094 ND ug/L 0.59 0.082
ND ug/L 0.59 0.071 0 .18 ug/L 0.59 0.094 J ND ug/L 0.59 0.12 0.79 ug/L 1. 2 0.24. J ND ug/L 1. 2 0.18
ND ug/L 1. 2 0.24 ND ug/L 1.2 0.34
ND ug/L 1. 2 0.059 ND ug/L 1.2 0.39
ND ug/L 1. 2 0.24
ND ug/L 1. 2 0.34
ND ug/L 1. 2 0.28
ND ug/L 5.9 0.47
12 ug/L 12 12
Recovery Acceptable Range
ND% 55 -115 H ND% 35 -137 H
detected because of required sample dilution.
below the reporting limit or is an estimated concentration.
raised due to high level of analyte present in sample.
raised due to sample volume limitations.
Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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SURFICIAL AQUIFER MONITORING WELL
MW-6S
-------------------GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press lirmly.
-~_._f:=acility Name _________ ~G~•~igy~C~h•~m~ic=•~• C~•=re~•~'"~'=;"="---------
-·-Address ___________ ~D=•=m=;·~•~D~ri~v•~----------
____ .,A,ohe~r~dee=•=N~C~28=31~5'-----County ____ =M=oo-a:~---
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER (REQUIRED)
Non-Discharge WO 0009949
NPDES
IY!.'E OF rnspo::-SA-:cl:-O=P:cER=:-A:--:T::-:IO=N-::Bc::Ec:IN-:-:G:-:-:Mc::OccN:::IT::0:-:R=Eo
(REQUIRED) Well Location _________________________ _ Lagoon __ Septic Tank/Drain Field
Well ldentilication Number MW-6S Well Deplh 47 OJ Ft.
Well Diameter 2 Q Sample (Screened) Interval 34,SJ Ft. To 44,SJ Ft.
Depth to Water Level 33 03 ft. below measuring point (belore sampling)
Measuring point Is z •1 ft. above land surface
Gallons of water pumped/bailed before samplinn 7.25
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application ol Sludae
_X_ Other
Rotary Oistribu1or
Field Analysis: pH 3.57 Specific Conductance fi43 uMhOs Temp. 12 s 0c Odor ___ Appearance __ _
Date Sample Collected 4/2J/'18 Date Lab Sample Analyze.~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. --~'~l-6/i~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/l
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrite (N02) as N _______ mg/I
Nitrate (N03) as N mg/I
Phosphorus: Total as P mg/I
(Note: UN MPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total mg/l Ba • Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOC mg/I
~~~ mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Arsenic mg/I Cu -Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe • Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Mg -Magnesium mg/I
Mn • Manganese mg/I
Total Ammonia mg/I· Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke~---------mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date
• See back for Instructions.
.. Submit blue and yellow copies only to address above.
-- ------- - - -------EARTH©TECH Field Data Information Log for Ground Water Sampling
Date (yr/molday) ___________ 9_8/_04_/2_1 ________ _
Field Personnel ----------'-R-".-'-M'--o'-r..,.g"-an'--'-/ -"-B-'-. .::.D.c.ill-"a-'rd'--------
Slte Name __________ Ge--=ig"-y_C_h_em_ica_l_C_o--'rpo'-ra_t_io_n _____ _
Earth Tech Job Number --------~3-'-1~8~19~---------
Well ID# MW-6S -------------------------□ Upgradient D Downgradient l!!I Sidegradient
Weather Condltlons _________ C_l_ea_r-'-,_M_il_d ________ _
Air Temperature ___________ 6'-'5'-----------'F
Total Well Depth (TWO) = ________ 4_7_._0_1 _______ 1/100 ft
Depth to Ground Water (DGW) = 33.03 1/100 ft
Length of Water Column (LWC) = TWD • DGW = ____ 1_3_.9_8 ____ 1/100 ft
1 Casing Volume (OCV) = LWC x 0.17 = 2.38 gal
3 Casing Volumes = 7 .13 gal = Standard Evacuation Volume
Method of Well Evacuation _______ ~W~e~ll--'W=iz=a~rd~------
Method of Sample CollecUon,_ ______ W=e"'ll-'W.,_i=z=ar"'d'-------
Total Volume of Water Removed 7.25 gal
Page_1_of
Casing 0lameter ____________ 2=.·;.;;0 ________ 1nches
casing Material __________ s_ta_in_le_s_s_s_te_e_l ________ _
Measuring Point Elevation ________ 464 __ . 7_3 ________ 1/100 ft
Height of Riser (above land surface) 2.61 1/100 ft
Land Surface Elevation 462 .10 1/100 ft
Screened Interval _________ 34_._8_1 __ 44_._81 ______ 1/100 ft
Dedicated Pump or Baller
Steel Guard Pipe Around Casing
Lock Ing Cap
Protective Post/Abutment
Well Integrity Satisfactory
Well Yield
Comments/Observations
l!!I Yes □No 0 Type Well Wizard
=--=---="'------------l!!I Yes □No D Flushmounted
l!!I Yes □No
□Yes l!!I No
l!!I Yes □No
□Low D Moderate l!!I High
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. ('C)
TURBIDITY INTU)•
0
8:48
3.33
-
626
18
350
2.5
9:06
3.49
-
635
19
56
Refill: A 1/2
4.75 7.25
9:18 9:29
3.52 3.57
- -
640 643
19.5 19.5
21 8.5
Discharge: ~
COMMENTS/OBSERVATIONS .;;S;;_A;;.;M;;.P.=L;:;ED=--:..A:..:.T..:9;.;:;3.::.5 ______________ ~~~'-'--'----------------------t
-
Field Data for GW
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Client Name:
Client ID:
Lab ID:
TCL Organochlorine Pesticides/PCBs
Method BOBO
Rust Environmental & Infrastructure MW-6S 098752-0001-SA
I}!\ ,euanterra
Environmenral
Services
Matrix: AQUEOUS Sampled: 21 APR 98 Received: 22 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98 Analyzed: 22 MAY 98
Parameter Result Reporting Units
alpha-BHC 2.9 ug/L beta-BHC 6.6 ug/L delta-BHC 6.0 ug/L gamma-BHC (Lindane) 2.4 ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin 0.58 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone 0.62 ug/L Methoxychlor ND ug/L Toxaphene 20 ug/L
Surrogate Recovery
Tetrachloro-m-xylene ND % Decachlorobiphenyl ND %
Note o Reportin9 limit(s) raised due to high level of analyte present Jn sample.
Note J Result is detected below the reporting limit or
is an estimated concentration.
Note H Spiked analyte not detected because of required sample dilution.
ND c Not detected NA= Not applicable
Limit
0.50 0.50 0.50 0.50 0.50
0.50 0.50
0.50 0.50
0.50 1.0 1.0
1.0 1.0
1.0 1.0
1.0
1.0
1.0
5.0 10
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For adcfltlonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name ________ ~G~•i=gy~C=h=•m=l=ca=l~Co=rpo=ra=t=ion~--------
Address ___________ ~Do=m=i•=o~D="=·ve~----------
___ _,_A~be~r=dee=•-~N=C~28=3=1=5 ____ County ___ __.,Mwooo,,ru.•----
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27U2U·0578
(919) 733-32,21
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949
NPDES _______ ~~--
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-6S Well Depth •z 01 Ft.
Well Diameter 2 o ·sample (Screened) Interval 34,8! Ft. To 44 Bl Ft.
Depth to Water Level •o 2Q It. below measuring point (before sampling)
Measuring point Is 261 It. above land surface
Gallons of water pumped/bailed before samplinn,._ ___ s=.o'------
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application ol SludQe
_X_ Qther
Rotary Distributor
Field Analysis: pH 3.42 Specific Conductance •7J uMhos Temp. 18 °c Odor ___ Appearance __ _
Date Sample Collected !Ql29/28 Date Lab Sample Analyze,~--------
Laboratory Name Quanterm, West Sacramento, CA Certification No. ___ 2_J6(i __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND RELD ACIDIFIED __ YES __ NO
COD ____________ mg/I Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Uae MPN method for hlgtlly turbid samp~s) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Fe -Iron mg/I
Hardness: Total mg/I
Phenol mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Sulfate mg/I Mg -Magnesium mg/I
Specific Conductance uMhos Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke __________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached Ug/1 ...c...c.~=~~~=~----
Other (Specify Compounds and
Concentration units)
u g/ I
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent')
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
- - - - - -- - -- --- ----E A R T H C H Field Data Information Log for Ground Water Sampling
Page_1_of 1
Dale (yr/mo/day) 98/10/29 Casing Diameter -2.0 Inches
Field Personnel R. Mor9an IN. Hicks Casing Material Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 464.73 11100ft
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.61 11100ft
Well ID# MW-6S Land Surface Elevation 462.10 11100ft
D Upgradient D Downgradient D Sidegradient Screened Interval 34.81 -44.81 1/100 ft
Weather Conditions Clear I Sunnl Dedicated Pump or Baller l!!I Yes □No □Type
Air Temperature 55 •F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Well Depth (TWO) = 47.01 1/100 ft Locking Cap l!!I Yes □No
Depth to Ground Water (DGW) = 40.20 1/100 ft Protective Post/Abutment □Yes l!!I No
Length of Water Column (LWC) = TWD -DGW = 6.81 1/100 ft Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCV) = LWC x 0.163 = 1.11 gal Well Yield □Low l!!I Moderate □High
3 Casing Volumes = 3.33 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard Pesticides
Method of Sample Collection Well Wizard
Total Volume of Water Removed 5.0 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 1.25 2.5 3.75 5.0 -TIME (military) 10:55 11 :10 11:25 11:45 12:00
pH (S.U.) 3.35 3.42 3.43 3.42 3.42
Drawdown (fl) --- -
Sp. Cond. (µmhos/cm) 817 742 670 640 623
Water Temp. ('C) 19 18 18 18 18 -
TURBIDITY (NTU)• 86 20 5.43 2.62 2.24
• .,""helom•"'• Tumid!"' Un"" Refill: B Discharge: A
COMMENTS/OBSERVATIONS Sampled at 1205. -I
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Field Data for GW
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Client Name:
Client ID:
LAB ID:
Matrix:
Authorized:
Rust Environmental
MW-6S
302434-0005-SA
AQUEOUS
30 OCT 98
Dilution Factor: 10
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin
Heptachlor epoxide
Endosul fan I
Dieldrin
4,4' -DOE Endrin
Endosulfan I I
4,4' -DOD
Endosul fan sulfate
4,4'-DDT
Endrin aldehyde
Endri n ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
feuanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
1.8 ug/L 7.1 ug/L
4.6 ug/L
I. I ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
0. 12 ug/L
ND ug/L
0.25 ug/L
ND ug/L ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
II ug/L
Recovery
ND%
ND%
Received: 30 OCT 98
Analyzed: 17 NOV 98
Reporting
Limit MDL Qualifier
0.56 0.089 oR 0.56 0.045
0.56 0.067
0.56 0. I I
0.56 0.078
0.56 0.089
0.56 0.078
0.56 0.067
0.56 0.089 J
0.56 0. I I
I.I 0.22 J
I.I 0. I 7 ·
I. I 0.22 I. I 0.32
I.I 0.056
I.I 0.37
I.I 0.22
I.I 0.32
I. I 0.27
5.6 0.45
II II
'
Acceptable Range
55 -115 H
35 -137 H
Note H
Note J Note o
Note R
ND= Not
= Spiked analyte not
= Result is detected
= Reporting limit(s)
= Reporting limit(s)
detected because of required sample dilution.
Detected
Reported By: Lisa Stafford
below the reporting limit or is an estimated con~entration.
raised due to high level of analyte present in sample.
raised due to sample volume limitations.
Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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SURFICIAL AQUIFER MONITORING WELL
MW-10S
------------ - - - - - --·
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM .
For addltlonel forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name, __________ G:cc•::,lgY"'-'Ch=•m"'l"'ca"-1 -"Co"'rpo=ra"'t"'lo"'n ________ _
Address, ___________ _,D,,,o,,,m,,,lne,Oc,D""n""·v,_e -----------
____ .,cA~he,er,,d,,,eee,n..,N.,,C"-"'283"""'15._ ___ Countyf ____ _oM11001<ta:a:__ __ _
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NPDES ___________ _
TYPE OF DISPQSAL OPERATION BEING MONITORED
(REQUIRED) Well Location _______________________ c_ __ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-JOS Well Depth 41 36 Ft.
Well Diameter 2 o Sample (Screened) Interval 29.16 Ft. To 38,86 Ft.
Depth to Water Level 20 40 ft. below measuring point (before sampling)
Measuring point is 2 36 ft. above land surface
Gallons of water pumped/bailed before samplinn 17.75
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Lend Appfication of SludQe
_X_other
Rotary Distribu1or
Field Analysis: pH 4 98 Specific Conductance 29 uMhos Temp. 1• 0 c Odor ___ Appearance __ _
Date Sample Collected 4121(28 Date Lab Sample Analyze•~--------
LabOratory Name Quanterra, West Sacramento, CA Certification No. ___ ..1,.21LD66"---
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total /100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3 ) as N mg/I
Phosphorus: Total as P mg/I
(Note: Uae MPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I Mg -Magnesium mg/I
Specific Conductance uMhos Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium · mg/I
TKN as N mg/I
Ni -Nicke,L._ _________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent')
GW-59 REV. 8196
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
- - -- - - - - ------- -
E A R T H C H Field Data Information Log for Ground Water Sampling
Date (yr/mo/day), __________ ..:9.;.8/..:04--=/2'-1 ________ _
Field Personnel _______ _;R..:.·:.cM=or:.gc:a:::n..:./..:Bcc·..:Dccil;_:lac.rd=-------
Site Name _________ ...:G:..:e.:eigy"---'CC.hc:.em=ica;;:;l;..C:..:o"'rp"o"-ra:ct;.:io"n------
Earth Tech Job Number ---------"3'-'1"'8""19"----------
Well ID •-------::---------:=-::----'M=W'---'-10'-S:::-::-:--,------0 Upgradient D Downgradient 181 Sidegradient
Weather Conditions. ________ ...::;C;_:le;.::a;;.,r,..:.Mcciccld'---------
Alr Temperature ___________ 7:..:0=----------•f
Total Well Depth (TWD) • ________ 4-'-1" . ..:3.;.6 ______ _ 1/10011
Depth to Ground Water (DGW} = _______ 2_0_.4_0 ______ _ 1/10011
Length of Water Column (LWC) = TWD -DGW = ____ 2_0_.9_6 ___ _ 1/10011
1 Casing Volume (OCV) = LWC x 0.17 •------'3'-.56'-'------gal
3 Casing Volumes= 10.69 gal = Standard Evacuation Volume
Method of Well Evacuatlon. _______ .......aW=el~I W=iz"'a~r~d ______ _
Method of Sample Collection._ ______ .;.W'-'e"-'11'-'W'-=iza,:aaard'-------
Total Volume of Water Removed 17.75 gal
Page_1_of
Casing Oiameter ____________ 2_.0 ________ Inches
casing Material ________ s_c_h _40_Pv_c_,_s_ta_in_te_s_s_s_te_e_t ______ _
Measuring Point Elevatlon ________ 4_6_1_.5_0 ________ 1/100 ft
Height of Riser (above land surface) 2.36 1/100 ft
Land Surface Elevation 459.12 1/100 ft
Screened Interval _________ 2_9._1_6 __ 3_8_.8_6 _____ 1/100 ft
Dedicated Pump or Baller 181 Yes 0 No O Type Well Wizard
Steel Guard Pipe Around Casing 181 Yes 0 No O Flushmounted
Locking Cap 181 Yes □No
Protective PosUAbutment □Yes 181 No
Well Integrity Satisfactory 181 Yes □No
Well Yield □Low D Moderate 181 High
Comments/Observations
BEGIN PURGING SLOWLY TO AVOID TURBIDITY.
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY fNTUl"
0
13:20
5.04
-
33
19
25
4 8 11
13:27 13:39 13:56
4.90 4.59 5.12
---
31 30 29
19 19 19
143 94 77
Refill: B 1/2 Discharge: ~
14.5 17.75
14:37 14:54
5.40 4.98
--
29 29
19 19
34 30
-
· fOMMENTS/OBSERVATIONS SAMPLED AT 1500 . -i
Field Data for GW
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(!l:\ r/Uanterra
TCL Organochlorine Pesticides/PCBs Environmental
Services
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-lOS Lab ID: 098752-0005-SA Matrix: AQUEOUS Sampled: 21 APR 98 Received: 22 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98 Analyzed: 22 MAY 98
Parameter Result Units Reporting
alpha-BHC 0.39 ug/L beta-BHC 7.0 ug/L delta-BHC 1.6 ug/L gamma-BHC (Lindane) 0.34 ug/L a 1 pha-Chl ordane. ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin 0.90 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endri n ketone 1.8 ug/L Methoxychlor ND ug/L Toxaphene 8.4 ug/L
Surrogate Recovery
Tetrachloro-m-xylene ND % Decachlorobiphenyl ND %
Note J Result is detected below the reporting limit or is an estimated concentration.
Note H Spiked analyte not detected because of required sample dilution.
ND a Not detected NA= Not applicable
Limit
0.50 0.50
0.50 0.50
0.50
0.50 0.50
0.50 0.50 0.50
1.0
1.0
1.0 1.0
1.0 1.0
1.0
1.0
1.0 5.0
10
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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Volatile Organics
Method 8260
Client Name:
Client ID: LAB ID:
Rust Environmental & Infrastructure
MW-lOS 098752-0005-SA Matrix: Authorized: AQUEOUS Sampled: 21 APR 98
22 APR 98 Prepared: NA
Dilution Factor: 5.0
Parameter Result Units
Trichloroethene ND ug/L
Surrogate Recovery
Toluene-dB 95 % 4-Bromofluorobenzene 96 % l,2-Dichloroethane-d4 113 %
NA= Not Applicable ND= Not Detected
~uanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 29 APR 98
Rerorting imit . Qualifier
5.0
Acceptable Range
85 -111 81 -117 75 -121
Reported By: Matt Culver Approved By: Karin Yee
The cover letter is an integral part of this report. Rev 230787
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For eddltlon1I forms
plea:,e write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ ...:G"'ec:,igY"-"'C::;h•,:;m::,ic,::ae..l C:,;o,:.rpo=:.ra:::l:::io,:.n ________ _
Address ___________ _,D,,,o::;m,,,in,,.o.eD:.erie.eve,.._ _________ _
____ ,,A.,be.,_n1,.ee,,..n._cN,,.C~28=J.._,1s'-----County, ____ _aMu,oo.,,rec,;_ __ _
-DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828·0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NPDES ___________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location, _________________________ _ Lagoon __ Septic Tank/Drain Field
Well ldentilication Number MW-JOS Well Dep1h 41 36 Ft.
Well Diameter 2 o Sample (Screened) Interval 29.16 Ft. To 38,86 Ft.
Deplh to Water Level 211 77 It. below measuring point (before sampling)
Measuring point Is 2 36 ft. above land surface
Spray Field __ Subsurface Low-Pressure
Piping (LPP}
Land Application of Sludae
• _!{_ Other
Rotary Distributor Gallons of water pumped/bailed before samplinn 6.25
Field Analysis: pH 4.79 Specific Conductance 32 uMhos Temp. 18 °c Odor ___ Appearance, __ _
Date Sample Collected maw• Date Lab Sample Analyze"'---------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ___ .,2Ju,66o_ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FJELD ACIDIFIED __ YES __ NO
COD ____________ mg/I Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Uae UPN method for highly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total mg/I
pH (when analyzed) units
TOG mg/I
Chloride mg/I
Arsenic mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Mg -Magnesium mg/I
Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke,,_ _________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
.. E .. , -,_ ... --; -_, - -~ -., ----1!1!11
A R T H @ T E C H Field Data Information Log for Ground Water Sampling
·':
Date (yrlmolday) _________ ..;9::;8::,1,:,:10::,12::;9:_ _______ _
Field Personnel ________ R""-'. M=o'-'rg"'a"'n-"/-"N-".-"H-'ick=s ______ _
Site Name ----------'Ge'-'igy"--'C'--h-'e_m..;ica-'---1 C_o_rp:,..o_ra_t_io_n _____ _
Earth Tech Job Number ________ _,3:,,1,,.8,,c19:c... ________ _
Well lD# _____________ MM=:,.-.:.10::,;S:_ ______ _
D Upgradient D Downgradient D Sidegradient
Weather Conditions. _________ ..;,S..;,u_n-'n._ ________ _
AlrTemperature ___________ 6_5 __________ °F
Total Well Depth (TWO) = _______ 4_1_._36 _______ 11100 ft
Depth to Ground Water (DGW) = 28. 77 11100 ft
Length of Water Column (LWC) =TWO· DGW = 12.59 11100 ft
1 Casing Volume (OCV) = LWC x 0.163 = 2.05 gal
3 Casing Volumes= 6.16 gal = Standard Evacuation Volume
Method of Well Evacuatlon, _______ ...,!W,,,:ee,1:,..1 W=ize,a,erd,,._ _____ _
Method of Sample Collection. _______ W.:.,.:e..,11'-'W=iz"'a"'rd,_ _____ _
Total Volume of Water Removed 6.25 gal
Page_1_of
Casing Oiameter ___________ ..;2cc·..c0 ________ lnches
Sch 40 PVC/Stainless Steel Casing Material ______________________ _
Measuring Point Elevatlon ________ 46_1_.5_0 ________ 11100 ft
Height of Riser (above land surface) 2.36 11100 ft
Land Surface Elevation 459.12 11100 ft
Screened Interval 29.16 -38.86 11100 ft
Dedicated Pump or Baller l!!I Yes D No D Type
Steel Guard Pipe Around Casing l!!I Yes D No D Flushmounted
Locking Cap
Protective Post/Abutment
Well Integrity Satisfactory
Well Yield
Comments/Observations
Pesticides TCE
l!!I Yes D No
l!!I Yes D No
l!!I Yes D No
D Low l!!I Moderate D High
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S,U,)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp, (°C)
TURBIDITY fNTU)•
0
9:11
4.81
-
33
19
28.5
2 4 6.25
9:16 9:25 9:39
4.66 4.74 4.79
-- -
32 32 32
18 18 18
62.8 2.29 0.81
Refill: Discharge: __ _
·roMMENTSIOBSERVATIONS .::S:::a:!m!l:p::::le~d~a::,1~0,:::94:::0::;.. _______________________________________ ---t
Field Dara for CW
I ~\ r/Uanterra
TCL Organochlorine Pesticides/PCBs
Method 8080 I Client Name: Rust Environmental & Infrastructure
Client ID: MW-lOS
I LAB ID: 302434-0009-SA
Matrix: AQUEOUS
Authorized: 30 OCT 98 ,,. Dilution Factor: 10
Parameter
I alpha-BHC
beta-BHC
I delta-BHC
gamma-BHC (Lindane) alpha-Chlordane
gamma-Chlordane
I Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
I Oieldrin
4,4' -ODE
Endrin
Endosulfan I I
I 4, 4' -ODD
Endosulfan sulfate 4,4'-DDT
I Endrin aldehyde Endri n ketone
Methoxychlor
Toxaphene ,.
Surrogate
I Tetrachloro-m-xylene Decachlorobiphenyl
I
I Note H Spiked analyte not = Result is detected
= Reporting limit(s) = Reporting limit(s)
Note J '· Note o I Note R
ND= Not Detected
Reported By: Lisa Stafford
Sampled: 29 OCT 98 Received: 30 OCT 98
Prepared: 02 NOV 98 Analyzed: 17 NOV 98
Result Units
Reporting
Limit MDL Qualifier
0.085 ug/L 0.56 0.089 JoR 4.5 ug/L 0.56 0.045 0.41 ug/L 0.56 0.067 J 0.11 ug/L 0.56 0 .11 J ND ug/L 0.56 0.078
ND ug/L 0.56 0.089
ND ug/L 0.56 0.078
ND ug/L 0.56 0.067 ND ug/L 0.56 0.089 ND ug/L 0.56 0.11 0.27 ug/L 1.1 0.22 J ND ug/L 1.1 0 .17·
ND ug/L 1.1 0.22 ND ug/L 1.1 0.32 ND ug/L 1.1 0.056
ND ug/L 1.1 0.37
ND ug/L 1.1 0.22
ND ug/L 1.1 0.32
ND ug/L 1.1 0.27
ND ug/L 5.6 0.45
ND ug/L 11 11
Recovery Acceptable Range
ND% 55 -115 H
ND% 35 -137 H
detected because of required sample dilution. below the reporting limit or is an estimated concentration.
raised due to high level of analyte present in sample.
raised due to sample volume limitations.
Approved By: Mike Orbanosky I The cover letter is an integral part of this report.
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(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental MW-!OS
302434-0009-SA
AQUEOUS
30 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-0ichloroethane-d4
Toluene-dB 4-Bromofluorobenzene
ND= Not detected
NA= Not applicable
Reported By: RRAMIREZ
& Infrastructure
Sampled: 29 OCT 98
Prepared: JO NOV 98
Result
ND
Recovery
Units
ug/L
96 %
101 %
98 %
Received: 30 OCT 98
Analyzed: JO NOV 98
Reporting
Limit
1.0
Approved By: FKENT
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Rev 230787
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SURFICIAL AQUIFER MONITORING WELL
MW-16S
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name ________ __cG~••~·gy,._C=h~•m=ica~l~C=orpo=ra=t~io~n ________ _
Address ___________ ~D=om~l~no~D~n~·v~• _________ _
___ __.A""he~rc,,dee=n"-N,_,C~28=31~5 ____ County ___ __,Mwoo&a:a:'-----
Well Location ________________________ _
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NPDES __________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-J6S Well Depth 68 Q4 Ft.
Well Diameter 2 o Sample (Screened) Interval 54,ll Ft. To 64 s Ft. Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Depth to Water Level 43 20 ft. below measuring point (before sampling)
Measuring point is 2 63 ft. above land surface
. Land Application ol Sludae __ X_ Other
Rotary Distributor Gallons of water pumped/bailed before samplinn 12.1s
Field Analysis: pH s.4 Specific Conductance 22 uMhos Temp. 12 °c Odor ___ Appearance __ _
Date Sample Collected 4/21/98 Date Lab Sample Analyzeu_ _______ _
Laboratory Name Quanterra, West Sacramento, CA Certification No. __ __.2..,J6(i.._ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
coo _______________ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3 ) as N mg/I
Phosphorus: Total as P mg/I
(Note: UN MPN method for hlghty turbld samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mgn Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOC I mg/I Cd -Cadmium mgn
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu -Copper mg/I
Grease and Oils mgn Fe -Iron mgn
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mgn Mg -Magnesium mg/I
Specific Conductance uMhos Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni· Nicke~---------mg/I
Pb • Lead mg/I
Zn-Zinc mgn
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/1
ug/I
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. -~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
- - - -.. -· -_,_ - -- ---E A. R T H © T E C H Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/04/21 Casing Diameter 2.0 Inches
Field Personnel R. Moraan / B. Dillard Casing Material Sch 40 PVC/Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 484.56 11100ft
Earth Tech Job Number 31819 Height of Riser {above land surface) 2.63 11100ft
Well ID# MW-16S Land Surface Elevation 481.93 11100ft
D Upgradient 181 Downgradient D Sidegradient Screened Interval 54.80 -64.80 11100ft
Weather Conditions Part!}'. Clou~. Mild Dedicated Pump or Baller 181 Yes □No D Type Well Wizard
Air Temperature 64 "F Steel Guard Pipe Around Casing 181 Yes □No D Flushmounted
Total Well Depth (TWD) = 68.04 1/100 ft Locking Cap 181 Yes □No
Depth to Ground Water (DGW) = 43.20 11100ft Protective Post/Abutment □Yes 181 No
Length of Water Column (LWC) = TWD • DGW c 24.84 1/100 ft Well Integrity Satisfactory 181 Yes □No
1 Casing Volume (OCV) = LWC x 0.17 = 4.22 gal Well Yield □Low D Moderate 181 High
3 Casing Volumes = 12.67 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard
Method of Sample Collection Well Wizard
Total Volume of Water Removed 12.75 gal
I
FIELD ANALYSES
VOLUME PURGED (gallons) 0 4.5 9.0 12.75
TIME (military) 11:54 12:02 12:16 12:25
pH (S.U.) 6.59 5.45 5.43 5.40
Drawdown (ft.) ----
Sp. Cond. (µmhos/cm) 52 35 29 29
Water Temp. ("C) 19 19 19 19
TURBIDITY (NTUI• 15 1.5 1.5 1.2
• N--h,,.lometrir Turb1.1:... Unitct Refill: B Discharge: B 1/2 --
OMMENTS/OBSERVATIONS SAMPLED AT 1230
Field Dal a for G W
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TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name': Rust Environmental & Infrastructure Client ID: MW-16S Lab ID: 098752-0004-SA Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC ND ug/L beta-BHC ND ug/L delta-BHC ND ug/L gamma-BHC (Lindane) ND ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Die 1 dri n ND ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone ND ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene 75 % Decachlorobiphenyl 68 %
ND c Not detected NA c Not applicable
~}\ ,euanterra
Environmental
Services
Received: 22 APR 98 Analyzed: 14 MAY 98
Rerorting imit
0.050
0.050
0.050 0.050 0.050
0.050 0.050
0.050 0.050
0.050
0.10
0.10
0 .10
0.10
0.10
0.10
0.10
0 .10 0.10
0.50 1.0
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
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Volatile Organics Method 8260
Client Name: Client ID:
LAB ID:
Rust Environmental & Infrastructure
MW-16S
098752-0004-SA Matrix:
Authorized: AQUEOUS Sampled: 21 APR 98 22 APR 98 Prepared: NA
Dilution Factor: 5.0
Parameter Result Units
Trichloroethene ND ug/L
Surrogate Recovery
Toluene-dB 95 % 4-Bromofluorobenzene 98 % l,2-Dichloroethane-d4 114 %
NA a Not Applicable I ND a Not Detected --.....__
{ffeuanterra
Environmental
Services
Received: 22 APR 98 Analyzed: 29.APR 98
Rerorting imit Qualifier
5.0
Acceptable Range
85 -111
81 -117 75 -121
Reported By: Matt Culver Approved By: Karin Yee
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The cover letter is an integral part of this report ..
Rev 230787
---·-- - - ---·-- - - ---.. ---
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press lirmly.
Facility Name _________ _.:cG:,:cel,..gy'--"'Ch::,:ec:,m:,:icac:,l:..:Ce,o:,,rye,o:,,ra:,:li::,cone.__ _______ _
Address ____________ .:,D:,com=in,,_o""D,.,_riv,_,e~------,------
____ A~b=•=rd=ee=•=•-~N=C__,283=1=5 ____ County ____ M"""'oo"'re"------
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non•Oischarge WO 0009949
NPDES.,.,......,..,,.,,,,.,.,,,,.,,,.,.,,======
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location _________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-16.5 Well Depth 63 04 Ft
Well Diameter 20 Sample (Screened) Interval 54.i! Ft. To 64.8 Ft.
Depth to Water Level 45 SI ft below measuring point (before sampling)
Measuring point is 263 ft, above land surface
Gallons of water pumped/bailed before samplinn.,_ ___ __,1"-1 ____ _
Field Analysis: pH S,f9 Specific Conductance J• · uMhos Temp, J7 °c
Spray Field __ Subsurface Low.Pressure
Piping (LPP)
Land Application ot SludQe
_X_ather
Rotary Distribu1or
Odor ___ Appearance __ _
Date Sample Collected maw• Date Lab Sample Analyze"'---------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ___ 2.,fwe66._ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD-------,--------mg/I Coliform: MF Fecal /1 00ml
Coliform: MF Total /100ml
Nitr~e (N02) as N _______ mg/I
Nitrate (N03) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method lor highly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG I mg/I Cd -Cadmium mg/I
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu • Copper mg/I
Grease and Oils mg/I Fe • Iron mg/I
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I Mg -Magnesium mg/I
Specific Conductance uMhos Mn • Manganese mg/I
Total Ammonia mg/I Na • Sodium mg/I
TKN as N mg/I
Ni• Nicke.__ _________ mg/I
Pb • lead mg/I
Zn • Zinc mg/I
Pesticides/Herbicides
{Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent')
GW-59 A EV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
- -- ---- --_, ----
C H Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) __________ 9=-8:::l.:.1;:;0l..:2c;9 ________ _ Casing Diameter ____________ 2_._0 ________ Inches
Field Personnel ________ R_. M_or~g~a_n_l_N_._H_ick~s ______ _ casing Material ________ s_ch_40_Pv_c_,_s_1a_in_Ie_s_s_s_1e_e_I ______ _
Site Name __________ G_e~ig~y_C_h_e_m_ica_I_c_o-'rp'-o_ra_t_io_n _____ _ Measuring Point Elevation ________ 48_4_.56 ________ 1/100 ft
Earth Tech Job Number ________ _,,3c,.1"8-"19e.... ________ _ Height of Riser (above land surface) 2.63 1/100 ft
Well ID # _____________ MW=::..-.:.16::.;S=---------Land Surface Elevation 481.93 1/100 ft
D Upgradient D Downgradient D Sidegradient Screened Interval 54.80 -64.80 1/100 ft
Weather Condltions ________ C_l_e_a_r I_S_u_n_n~y ________ _ Dedicated Pump or Bailer □Yes □No □Type
Air Temperature ___________ 6""5'----------°F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Well Depth (TWO) = ________ 6_8_.04 ________ 1/100 ft Locking Cap □Yes □No
Depth to Ground Water (DGW) = 45.51 1/100 ft Protective Post/Abutment □Yes □No
Length of Water Column (LWC) = TWO -DGW = ____ 2_2_.5_3 ____ 1/100 ft Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x 0.163 = 3.67 gal Well Yield □Low D Moderate 181 High
3 Casing Volumes = 11.02 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation, _______ _,_W,_,e,,llc;W=iz"'a"'rd"-------Pesticides TCE
Method of Sample Collectlon'-______ W=e~ll~W=iz=ar~d,__ _____ _
Total Volume of Water Removed 11 gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (mllltary)
pH (S.U.)
Drawdown (fl)
Sp. Cond. (µmhos/cm)
Water Temp. ('C)
TURBIDITY (NTIJ)•
0
10:00
5.03
-
33
19
2.81
4
10:10
4.99
-
47
18
24.3
Refill:
8 11
10:25 10:32
5.23 5.19
--
40 36
18 17
5.88 3.24
Discharge:
-
FOMMENTSIOBSERVATIONS·..:S;.:a;;.:m.:cec.:1e:..:dc.:a:.:.t.:.1-=-03::.;5:.:.: _______________________________________ ----I
Field Data/or GW
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Client Name:
Client ID: LAB ID:
Matrix:
Authorized:
Rust Environmental
MW-16S 302434-0010-SA
AQUEOUS
30 OCT 98
Dilution Factor: 1.0
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4' -ODE
Endrin
Endosulfan II
4,4' -ODD
Endosulfan sulfate
4, 4' -DDT
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
#})\ ~uanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Recovery
96 %
81 %
Received: 30 OCT 98
Analyzed: 17 NOV 98
Reporting
Limit MDL Qualifier
0.052 0.0083 R 0.052 0.0041
0.052 0.0062
0.052 0.010
0.052 0.0073
0.052 0.0083
0.052 0.0073
0.052 0.0062
0.052 0.0083
0.052 0.010
0 .10 0.021 0 .10 0.016'
0.10 0.021 0 .10 0.030 0.10 0.0052
0 .10 0.034
0 .10 0.021
0 .10 0.030
0 .10 0.025
0.52 0.041
1.0 1.0
Acceptable Range
55 -115
35 -137
Note R = Reporting limit(s) raised due to sample volume limitations. ND= Not Detected
Reported By: Lisa Stafford __ Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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~)\ ... ~uanaerra
(8240 list} -Volatile Organics Target Compound List (TCL}
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental
MW-l6S
302434-0010-SA
AQUEOUS
30 OCT 98
Parameter
Trichloroethene
Surrogate
J,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
ND= Not detected
NA= Not applicable
Reported By: RRAMIREZ
& Infrastructure
Sampled: 29 OCT 98 Prepared: JO NOV 98
Result Units
ND ug/L
Recovery
94 %
IOI %
98 %
Received: 30 OCT 98
Analyzed: JO NOV 98
Reporting
Limit
1.0
Approved By: · FKENT
The cover letter is an integral part of this report.
Rev 230787
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SURFICIAL AQUIFER MONITORING WELL
MW-17S
.---- - - - - - - - - - - - - -I!!!!!!! l!!l!l
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name, ________ ___:G"'•c:i:iJQ'"--"Ch:::•c:,m:.:,k,ealc,C"'oryo=ra"'-t:::io,,,n ________ _
Address, __________ __,,D,,.om,,,1,,,no"-"D"'n"'·vc,.e _________ _
----'A"'be""-'rd""ee"'n'-'.N"-'C'--"'283"""15,__ ___ County, ___ _,M"-""oowre'-----
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NPDES __________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-17S Well Depth S2 42 Ft.
Well Diameter 2 o Sample (Screened) Interval 46.s Ft. To 56.s Ft.
Depth to Water Level 43 31 ft. below measuring point (before sampling)
Measuring point is 2 S4 ft. above land surface
Spray Field __ Subsur1ace Low-Pressure
Piping (LPP}
__ Land Application of Sludge
_x_other
Rotary Distribu1or Gallons of water pumped/bailed before samplinn 8.25
Field Analysis: pH s,06 Specific Conductance s• uMhos Temp. 12 °c Odor ___ Appearance __ _
Date Sample Collected 4121(98 Date Lab Sample Analyze•~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ---'2u.J6fioo_ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghfy turbid samples) Al • Aluminum mg/I
Dissolved Solids: Total · mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Mg • Magnesium mg/I
Mn • Manganese mg/I
Na • Sodium mg/I
TKN as N mg/I
Ni -Nicke,. __________ mg/I
Pb · Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached
Other (Specify Compounds and
Concentration units)
TCE • resulls attached
ug/1
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date
• See back for Instructions.
.. Submit blue and yellow copies only to address above.
---- ------- - --
C H Field Data Information Log for Ground Water Sampling
Page_1_ of __
Date (yr/mo/day) 98/04/21 Casing Diameter 2.0 Inches
Field Personnel R. Morgan/ B. Dillard Casing Material Sch 40 PVC/Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 480.20 1/100 fl
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.54 1/100 fl
Well ID# MW-17S Land Surface Elevation 477.66 1/100 fl
D Upgradient D Downgradient D Sidegradient Screened Interval 46.50 -56.50 1/100 fl
Weather Conditions Clear Dedicated Pump or Baller 181 Yes □No 0 Type Well Wizard
Air Temperature 80 •F Steel Guard Pipe Around Casing 181 Yes □No D Flushmounted
Total Well Depth (TWO) = 59.42 1/100 fl Locking Cap 181 Yes □No
Depth to" Ground Water (DGW) = 43.31 1/10011 Protective Post/Abubnent □Yes 181 No
Length of Water Column (LWC) = TWO -DGW = 16.11 1/10011 Well Integrity Satisfactory 181 Yes □No
1 Casing Volume (OCV) = LWC x 0.17 = 2.74 gal Well Yield 181 Low D Moderate □High
3 Casing Volumes = 8.22 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard
Method of Sample Collection Well Wizard
Total Volume of Water Removed 8.25 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 2.75 5.5 8.25
TIME (military) 12:37 12:44 12:57 13:07
pH (S.U.) 7.16 5.63 5.20 5.06
Orawdown (ft.) -' - --
Sp. Cond. (µmhos/cm) 34 61 63 58
Water Temp. ("C) 19 19 19 19
TURBIDITY (NTU)" 60 35 35 3
• Neohelnm~tri• T",...IA"" llnits Refill: B Discharge: A 1/2
COMMENTS/OBSERVATIONS SAMPLED AT 1315 I
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Field Data/or CW
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TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-17S Lab ID: 098752-0008-SA Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC ND ug/L beta-BHC ND ug/L delta-BHC ND ug/L gamma-BHC (Lindane) ND ug/L alpha-Chlordane ND ug/L Aamma-Chlordane ND ug/L eptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin ND ug/L 4,4' -ODE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L
4,4' -DOD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone ND ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene 82 % Decachlorobiphenyl 57 %
ND c Not detected NA c Not applicable
IJ)\ ,euanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 14 MAY 98
Reforting imit
0.050 0.050
0.050 0.050 0.050
0.050 0.050
0.050 0.050 0.050 o. 10
0 .10
0.10
0.10
0 .10
0.10
0.10
0 .10
0 .10
0. 50
1.0
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
I Volatile Organics
I Client Name:
Method 8260
Rust Environmental & Infrastructure MW-17S Client ID: LAB ID: I Matrix:
Authorized:
098752-0008-SA
AQUEOUS Sampled: 21 APR 98 22 APR 98 Prepared: NA
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Dilution Factor: 1.0
Parameter
Trichloroethene
Surrogate
Toluene-dB 4-Bromofluorobenzene
l,2-Dichloroethane-d4
Result Units
ND ug/L
Recovery
93 % 98 % 114 %
~}!\ I ~uanterra
' Environmental
Services
Received: 22 APR 98
Analyzed: 29 APR 98
Relorting imit Qualifier
5.0
Acceptable Range
85 -111 81 -117 75 -121
NA c Not Applicable I ND c Not. Detected
Reported By: Matt Culver Approved By: Karin Yee
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The cover letter is an integral part of this report.
Rev 230787
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GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addlllonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ ..,G:.=e,.igy"-"'-C"'he"'m"'ic"'a'-'I C"'o""rp"'o"'ra:.:.ti::c••::..... _______ _
Address ___________ .,,Dc,co,,,m,,,ineco-"D_,__,ri.,__,ve~----------
----"'Ah,,,e"'rd.,eeec,ne,., • .,__,N,eC_,28"""'31"'5 ____ County ____ wMwoo~a:_._ __ _
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949
NPDES_-c-c-c-c-------,--,,,..,.,= ~F DISPQSAL OPERATION BEING MONITORED
(REQUIRED) Well Location __________________________ _ lagoon __ Septic Tank/Drain Field
Well ldenlification Number MW-17S Well Depth 52 42 Ft.
Well Diameter 2 o Sample (Screened) Interval 4§ 5 Ft. To 56,5 Fl.
Depth to Water Level 46 45 ft. below measuring point (before sampling)
Measuring point is 254 ft. above land surface
Gallons of water pumped/bailed before samplin'.' I3.5
Spray Field __ Subsurface Low-Pressure
Piping (LPP}
Land Application of Sludge
_X_ Other
Rotary Distribu1o,
Field Analysis: pH 5,01 Specific Conductance 44 uMhos Temp. fO 0 c Odor ___ Appearance __ _
Date Sample Collected IQl29/'/8 Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ---~2tw66~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/I Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Uae UPN method lor hlghty turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
Ba -Barium mg/I
Ca -Calcium mg/I
TOC mg/I Cd -Cadmium mg/I
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu • Copper mg/I
Grease and Oils mg/I Fe -Iron mg/I
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Mg -Magnesium mg/I
Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke..._ _________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/I
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent')
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
--- - -
liii --- ----
C H Field Data Information Log for Ground Water Sampling
Date (yr/mo/day) __________ .:;9:::81:...:1..::0::12:::9'---------
Fleld Personnel ________ ccR.;... -"M"o"rg"a"-n-'/-'N-'._H-'i"-ck-"s'--------
Slte Name __________ G_e..,ig"-y-'C_h-'-em--'ica.;..I_C_o--'rp'-o-ra_l_io_n _____ _
Earth Tech Job Number ________ _,3'-'1.,,8c.s19"----------
Well ID # _____________ MW_'--_17_S _______ _
D Upgradient D Downgradient D Sidegradient
Weather Conditlons. ________ C=le-"a"-r '-/ "-S"-un_n~y ________ _
Air Temperature __________ _;5:.;0:_ _________ °F
Total Well Depth (TWO) = ________ 5_9_._42 ________ 1/100 ft
Depth to Ground Water (DGW) = 46.45 1/100 ft
Length of Water Column (LWC) = TWO -DGW = ____ 1_2_._97 ____ 1/100 ft
1 Casing Volume (OCV) = LWC x 0.163 = 2.11 gal
3 Casing Volumes = 6.34 gal = Standard Evacuation Volume
Method of Well EvacuaUon. _______ __,W-'-e""l"-1 W=iz~a~,d~------
Method of Sample CollecUon, _______ .a.W:.:e"'ll'-'W=iz"'a,_,rd,_ _____ _
Total Volume of Water Removed 13.5 gal
Page_1_of
Casing Olameter ____________ 2=.·;.;;0 ________ inches
casing Material ________ s_ch_40_Pv_c_,_s_1a_in_1e_s_s_s_1e_e_1 ______ _
Measuring Point Elevation ________ 4_8_0_._20 ________ 1/100 ft
Height of Riser (above land surface) 2.54 1/100 ft
Land Surface Elevation 477.66 1/100 ft
Screened Interval 46.50 -56.50 1/100 ft
Dedicated Pump or Baller
Steel Guard Pipe Around Casing
Locking Cap
Protective Post/Abutment
Well Integrity Satisfactory
Well Yield
Comments/Observations
Pesticides TCE
11!1 Yes □No □Type
=---'=---=------------11!1 Yes □No D Flushmounted
11!1 Yes □No
□Yes 11!1 No
11!1 Yes □No
□Low 11!1 Moderate □High
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY fNTIJl"
0
8:31
6.62
-
55
18
126
2.25 4.5
8:41 8:51
5.17 5.15
- -
37 29
16 16
35.4 41.1
Refill: B Discharge: A
6.75 9.0 11.25 13.5
9:01 9:11 9:22 9:33
5.18 5.04 5.03 5.01
- ---
25 38 42 44
16 16 16 10
50 79 65 58
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f OMMENTS/OBSERVATIONS .::S:::a::.:m.:tp::.:le:::d:...:a:.:.1..::0..::92:::5:.:.· _______________________________________ -i
Field Data for GW
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Client Name:
Client ID:
LAB ID:
Matrix:
Authorized:
Rust Environmental
MW-I 7S
302434-0003-SA
AQUEOUS
30 OCT 98
Dilution Factor: 1.0
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin
Heptachlor epoxide
Endosul fan I Dieldrin
4,4' -ODE
Endrin
Endosulfan II
4, 4' -ODD
Endosulfan sulfate
4, 4' -DDT
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
~~\ ,:euanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
Recovery
99 %
74 %
Received: 30 OCT 98
Analyzed: 16 NOV 98
Reporting
Limit MDL Qualifier
0.052 0.0084 R 0.052 0.0042
0.052 0.0063
0.052 0.010 ·
0.052 0.0073
0.052 0.0084
0.052 0.0073
0.052 0.0063
0.052 0.0084
0.052 0.010
0. JO 0.021 0. JO 0.016
0 .10 0.021
0 .10 0.030
0. JO 0.0052
0 .10 0.035
0. JO 0.021
0. JO 0.030
0. JO 0.025
0.52 0.042
1.0 1.0
Acceptable Range
55 -115
35 -137
I . Note R = Reporting limit(s) raised due to sample volume limitations.
ND= Not Detected
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Reported By: Lisa Stafford Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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ll)\ ,:euanferra
(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix: Authorized:
Rust Environmental MW-17S
302434-0003-SA
AQUEOUS 30 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
ND= Not detected
NA= Not applicable
Reported By: RRAMIREZ
& Infrastructure
Sampled: 29 OCT 98
Prepared: 10 NOV 98
Result
ND
Recovery
Units
ug/L
95 %
102 %
98 %
Received: 30 OCT 98
Analyzed: 10 NOV 98
Reporting
Limit
1.0
Approved By: FKENT
The cover letter is an integral part of this report.
Rev 230787
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SURFICIAL AQUIFER MONITORING WELL
MW-18S
------------ - - - -iiiil --
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ ~G~•~lgy~Ch:!!•~m!!!ic:a=I C~•!!.rpl!!o!!.ra!!!t!!!io"-n ________ _
Address ____________ ..!o,, • ..,m!!!iD!!!O_!!D~ri'!!vee_ _________ _
____ ,,A,,,bes,.r,edee....,n _,:N,,aC~28=3,_IS'----County, ____ .ll!MlllQO<llll:"'----Well Location _________________________ _
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (AEQUIAEDI
Non-Discharge WQ 0009949 NPDES ___________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-JRS Well Depth 42 75 Ft.
Well Diameter 2 o Sample (Screenedl Interval 38,9 Ft. To 48,9 Ft.
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Depth to Water Level 47 46 ft. below measuring point (before sampling)
Measuring point Is 2 7Q ft. above land surface
Land Application of Slu1e __ Other
Rotary Distributor Gallons of water pumped/bailed before samplin-y_ ___ _.2,,,.0 ____ _
Field Analysis: pH 4.31 Specific Conductance 22 uMhos Temp. 18 °c Odor ___ Appearance __ _
Date Sample Collected 4i2!{9H Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ___ ..J2Ju,66o_ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES NO
COD--=--:--_______ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total _______ mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
Al -Aluminum mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Mg -Magnesium mg/I
Mn -Manganese mg/I
Na -Sodium mg/I
TKN as N mg/I
Ni -Nickel_ _________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration unHs)
TCE -results attached
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. · ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent•)
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
- -
!!!!I -iiilii --- -- -------Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/04/21 Casing Diameter 2.0 Inches
Field Personnel R. Mor9an I B. Dillard Casing Material Sch 40 PVC
Site Name Geigy Chemical Corporation Measuring Point Elevation 467.83 1/100 fl
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.70 1/100 fl
Well ID# MW-18S Land Surface Elevation 465.11 1/100 fl
D Upgradient D Downgradient D Sidegradient Screened Interval 38.90 -48.90 1/10011
Weather Conditions Clear, Mild Dedicated Pump or Baller l!!I Yes □No D Type Well Wizard
Air Temperature 55 'F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Well Depth (lWD) = 49.75 1/100 fl Locking Cap l!!I Yes □No
Depth to Ground Water (DGWJ = 47.46 1/100 fl Protective Post/Abutment □Yes l!!I No
Length of Water Column (LWC) = TWD • DGW = 2.29 1/10011 Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCV) = LWC x 0.17 = 0.39 gal WellYleld l!!I Low D Moderate □High
3 Casing Volumes= 1.17 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard
Method of Sample Collection Well Wizard
Total Volume of Water Removed 2.0 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 0.5 1.0 1.25 1.75 2.0
TIME (mllltary) 7:36 7:42 7:47 7:51 7:57 8:02
pH (S.U.) 5.74 4.69 4.66 4.51 4.45 4.31
Drawdown (ft.) - ----- -
Sp. Cond. (µmhos/cm) 30 118 85 74 89 97
Water Temp. ('C) 16 17 17 18 18 18
TURBIDITY (NTUI" 8.8 1.21 1.10 1.05 0.78 0.68
• N--helometrtr 'T'--rbldftu ••-,jttt Refill: B Discharge: B
FOMMENTS/OBSERVATIONS SAMPLED AT 0810 I
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Field Data for GW
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TCL Organochlorine Pesticides/PCBs Environmenral
Services
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-18S Lab ID: 098752-0002-SA Matrix: AQUEOUS Sampled: 21 APR 98 Received: 22 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98 Analyzed: 14 MAY 98
Parameter Result Units Reporting
Limit
alpha-BHC ND ug/L 0.050 beta-BHC ND ug/l 0.050 delta-BHC ND ug/L 0.050 gamma-BHC (Lindane) ND ug/L 0.050 alpha-Chlordane ND ug/L 0.050 gamma-Chlordane ND ug/L 0.050 Heptachlor ND ug/L 0.050 Aldrin ND ug/l 0.050 Heptachlor epoxide ND ug/L 0.050 Endosul fan I ND ug/L 0.050 Dieldrin ND ug/L 0.10 4,4'-DDE ND ug/L 0.10 Endrin ND ug/l 0.10 Endosulfan II ND ug/L 0.10 4,4'-DDD ND ug/L 0.10 Endosulfan sulfate ND ug/L 0. 10 4,4'-DDT ND ug/L 0. 10 Endrin aldehyde ND ug/L o. 10 Endrin ketone ND ug/L 0 .10 Methoxychlor ND ug/L 0.50 Toxaphene ND ug/L 1.0
Surrogate Recovery
Tetrachloro-m-xylene 80 % Decachlorobiphenyl 77 %
ND= Not detected NA= Not applicable
Reported By: Jon Edmondson Approved By: Mike 0rbanosky
The cover letter is an integral part of this report.
Rev 230787
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Client Name: Rust Environmental Client ID: MW-18S LAB ID: 098752-0002-SA Matrix: AQUEOUS Authorized: 22 APR 98
Dilution Factor: 1.0
Parameter
Trichloroethene
Surrogate
Toluene-dB
4-Bromofluorobenzene
l,2-Dichloroethane-d4
NA= Not Applicable
ND= Not Detected
Volatile Organics Method 8260
& Infrastructure
Sampled: 21 APR 98 Prepared: NA
Result Units
ND ug/L
Recovery
94 %
97 %
110 %
{!puanterra
Em'ironmental
Services
Received: 22 APR 98 Analyzed: 29 APR 98
Rerorting imit Qualifier
5.0
Acceptable Range
85 -111 81 -117
75 -121
Reported By: Matt Culver Approved By: Karin Yee
The cover letter is an integral part of this report.
Rev 230787
-------------------
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For llddltlonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name_~--------'G"-'e"'igy<-=Chec•cccmecica=l.:cCccorpo=ra"'t"'io"'n ________ _
Address ___________ __,,D""om,,,ie,no"'D"-'n"-'·v-"e _________ _
___ _,A_,,he,,_nl,.,,,,eee,n._;N,.,C'-"'28"'31,.5c...... ___ County, ___ _JMnoooo.are,.._ __ _
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER (REQUIREDI
Non-Discharge WQ 0009949 NPOES __________ _
TYPE OF DISPQSAL OPERATION BEING MONITORED
. (REQUIRED) Well Location, ________________________ _ Lagoon __ Septic Tank/Drain Fiekl
Well Identification Number MW-Jil'i Well Depth 49 75 Ft.
Well Diameter 2 Q Sample (Screened) Interval 38 9 Ft. To 48 9 Ft.
Depth to Water Level 49 31 ft. below measuring point (before sampling)
Measuring point is 2 zo ft. above land surface
Spray Field __ Subsurface low-Pressure
Piping (LPP)
Land Application ol SludQe
_X_Other
Rotary Distributor
Gallons of water pumped/bailed before samplin-1.0
Field Analysis: pH 4,IZ Specific Conductance 14fi uMhos Temp. 1• 0 c Odor ___ Appearance, __ _
Date Sample Collected JQ/2'/L'/8 Date Lab Sample Analyze,., ________ _
Laboratory Name . Quanterra, West Sacramento, CA Certification No. __ _,2'-l!J6,o6c...... __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES NO
COD ____________ mg/1
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrite {NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use IIPN method for hlgllly turbid samples) Al -Aluminum mg/1
Dissolved Solids: Total ______ mg/1
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I·
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/1
Chromium: Total mg/I
Cu • Copper mg/I
Grease and Oils mg/1
Hardness: Total mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Mg -Magnesium mg/1
Mn • Manganese mg/1
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke,L._ _________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results alt.ached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on. back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
- ----- - -----C H Field Data Information Log for Ground Water Sampling
Date (yr/mo/day) __________ .;_98""/-'-1"-0/-"2""9 ________ _
Field Personnel ________ R;_;,;_. M=o:...,g<.:a.:..:n..:./..:.N.:..:·..:.H.:..:ic°'k'"'s'--------
Site Name __________ G:..;e...,i9""y-'C'-h..:.e_m...;ica.;_I_C:...o:...rpc..oc...ra:...t...:io_n _____ _
Earth Tech Job Number --------~3..:.1~8~19~---------
Well ID # ______________ MW __ -1_8:...S ________ _
D Upgradient D Downgradient D Sidegradient
Weather Conditions. ________ C"-1'-'e-"a'--r /_S""u"'n-'--n'-'y ________ _
Air Temperature ___________ 6_5 __________ °F
Total Well Depth (TWO) = ________ 4..:.9..:.. 7_5'-_______ 1/100 ft
Depth to Ground Water (DGW) = 49.37 1/100 ft
Length of Water Column (LWC) =. TWO -DGW = _____ 0._3_8 ____ 1/100 ft
1 Casing Volume (OCV) = LWC x 0.163 = 0.06 gal
3 Casing Volumes = 0.19 gal = Standard Evacuation Volume
Method of Well Evacuatlon, _______ ~W~e~ll:...Wi=iz=•~rd~------
Method of Sample Collectlon. _______ W=e"'ll-'W"'1=·z,,_ar"d,_ _____ _
Total Volume of Water Removed 1.0 gal
Page_1_of
Casing Diameter ____________ 2_._0 ________ inches
Casing Material __________ S:..ch:..:...4_0:._:...P_V...:C ________ _
Measuring Point Elevation ________ 4_6_7_.8_3 ________ 1/100 ft
Height of Riser (above land surface) 2.70 1/100 ft
Land Surface Elevation 465.11 1/100 ft
Screened Interval 38.90 -48.90 1/100 ft
Dedicated Pump or Baller l!!I Yes □No □Type
Steel Guard Pipe Around Casing =---=----'=------------l!!I Yes □No D Flushmounted
Locking Cap
Protective Post/Abutment
Well Integrity Satisfactory
WellYleld
Comments/Observations
Pesticides TCE
Du licate
l!!I Yes □No
□Yes l!!I No
l!!I Yes □No
l!!I Low D Moderate □High
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (llmhos/cm)
Water Temp. {°C)
TURBIDITY (NTU)"
0
12:30
4.42
-
192
18
9.93
0.25
12:36
4.18
-
153
17
3.54
Refill: 8
0.50 0.75
12:42 12:48
4.20 4.17
- -
141 146
17 16
1.22 0.90
Discharge: A
-
f OMMENTS/OBSERVATIONS ~S::::a::.:m.:te:::le:::,d~•~l..:1:;.25:,::0::.;. __________ ~~__;-_.;__ ________________________ ---i
Field DaJajor GW
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Client Name: Rust Environmental Client ID: MW-18S
LAB ID: 302434-0006-SA
Matrix: AQUEOUS
Authorized: 30 OCT 98
Dilution Factor: 1.0
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane) alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan I I
4, 4' -DDD
Endosulfan sulfate 4,4'-DDT
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
II}\ ,euanterra
TCL Organochlorine Pesticides/PCBs
Method B080
& Infrastructure
Sampled: 29 OCT 98 Received: 30 OCT 98
Prepared: 02 NOV 98 Analyzed: 17 NOV 98
Reporting
Result Units Limit MDL Qualifier
ND ug/L 0.059 0.0094 R ND ug/L 0.059 0.0047 ND ug/L 0.059 0. 0071 ND ug/L 0.059 0.012 ND ug/L 0.059 0.0082
ND ug/L 0.059 0.0094 ND ug/L 0.059 0.0082
ND ug/L 0.059 0. 0071 ND ug/L 0.059 0.0094
ND ug/L 0.059 0.012
ND ug/L 0.12 0.024 ND ug/L 0. 12 0.018
ND ug/L 0 .12 0.024 ND ug/L 0 .12 0.034
ND ug/L 0 .12 0.0059 ND ug/L 0 .12 0.039 ND ug/L 0.12 0.024
ND ug/L 0.12 0.034
ND ug/L 0. 12 0.028
ND ug/L 0.59 0.047 ND ug/L I. 2 I. 2
Recovery Acceptable Range
99 % 55 -115
103 % 35 -137
I Note R = Reporting limit(s) raised due to sample volume limitations.
ND= Not Detected I Reported By:
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Lisa Stafford Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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~)\ ~uanterra
(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental
MW-JBS
302434-0006-SA
AQUEOUS
30 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-0ichloroethane-d4
Toluene-dB 4-Bromofluorobenzene
NO= Not detected
NA= Not applicable
Reported By: RRAMIREZ
& Infrastructure
Sampled: 29 OCT 98 Received: 30 OCT 98
Prepared: 10 NOV 98 Analyzed: IO NOV 98
Reporting
Result Units Limit
NO ug/L 1.0
Recovery
95 %
99 % 97 %
Approved By: FKENT
The cover letter is an integral part of this report.
Rev 230787
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UPPER BLACK CREEK AQUIFER MONITORING WELL
MW-11D
iiiiil liilll liiil liMl ~ iiii]
WATER RESOURCES SEMINAR
Monday, June 27, 2000
"Algal Bacteria, and BOD Responses to Nutrient Gradients in
' " Coastal Plain Watersheds
Research Associate Professor Michael A. Mallin
Center for Marine Science Research
University of North Carolina at Wilmington
Room 1132, Jordan Hall
North Carolina State University Campus
3:00 p.m. 0
For additional information, please contact Robert Holman,
Associate Director at [phone]
WATER RESOURCES RESEARCH INSTITUTE
OF THE UNIVERSITY OF NORTH CAROLINA
iiiil liiil \iiiil
- -~ --l --· - ---
GROUNDWATER QUALITY MONITORING: For additional forms
please write or call: COMPLIANCE REPORT FORM
Type or Use a ball-point pen and press firmly.
Facility N~me ________ ~G~•l~gy~C~h~•=m~ica=l~C~ory=o~ra~•~io~•---------
Address __________ ~D=om=i=•o~D=n~·v~• ----------
___ __,A~be~•~d=ee=•~N~C~28=31~S ____ County ___ __,Mwoo""'a:'-----
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NPOES __________ _
IYf.s.QF P)SpoSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Fteld
Well Identification Number MW-IJD Well Depth 75 32 Ft.
. Well Diameter 2 n Sample (Screened) Interval 59,4 Ft. To 69 6 Ft.
Depth to Water Level 52 85 ft below measuring point (before sampling)
Measuring point is 2 32 ft. above land surface
Spray Field __ Subsurface Low-Pressure
Piping (LPP}
Land Application ol Sludae
_X_ Qther
Rotary Distribu1or Gallons of water pumped/bailed before samplin" 17.75
Field Analysis: pH 4 73 Specific Conductance 21 uMhos Temp. 16 °c Odor ___ Appearance __ _
Date Sample Collected 4Qll28 Date Lab Sample Analyzeu_ _______ _
Laboratory Name Quanterra, West Sacramento, CA Certification No. __ _,,2,.,)6.,6 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/I Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total /100ml
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghty turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba • Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOC mg/I Cd -Cadmium mg/I
Chloride mg/I
Arsenic mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Grease and Oils mg/I Fe -Iron mg/I
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I Mg · Magnesium mg/I
Specific Conductance uMhos Mn -Manganese mg/I
Total Ammonia mg/I Na • Sodium mg/I
TKN as N mg/I
Ni· Nicke,_ _________ mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached
Other (Specify Compounds and
Concentration units)
ug/I
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
-------.. Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/04/21 Casing Diameter 2.0 inches
Field Personnel R. Morgan / B. Dillard Casing Material Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 463.43 1/10011
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.39 1/100 fl
Well ID# MW-110 Land Surface Elevation 461.02 1/100 fl
O Upgradient O Downgradient l!!I Sidegradient Screened Interval 59.40 -69.60 1/10011
Weather Conditions Clear, Sunnl Dedicated Pump or Bailer l!!I Yes □No 0 Type Well Wizard
Air Temperature 60 'F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Well Depth (TWD) = 75.39 1/100 fl Locking Cap l!!I Yes □No
Depth to Ground Water (DGW) = 59.85 1/10011 Protective Post/Abutment □Yes l!!I No
Length of Water Column (LWC) = TWD -DGW = 15.54 1/10011 Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCV) = LWC x 0.17 = 2.64 gal WellYleld □Low D Moderate l!!I High
3 Casing Volumes = 7.93 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard
Method of Sample Collection Well Wizard
Total Volume of Water Removed 17.75 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 2.75 5.5 8.25
TIME (military) 10:33 10:43 10:53 11:03
pH (S.U.) 4.49 4.69 4.71 4.73
Drawdown (fl.) - -- -
Sp. Cond. (µmhos/cm) 43 20 20 21
Water Temp. ("C) 16 16 16 16
TURBIDITY (NTUJ• 222 28.5 4.81 1.90
• Nenhelometrle Tufbfdilv llnih< Refill: B Discharge: B
COMMENTS/OBSERVATIONS SAMPLED AT 1105 . I
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Field Data/or GW
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••
TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-llD
Lab ID: 098752-0016-SA
Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC 0 .14 ug/L beta-BHC 0.52 ug/L delta-BHC 0. 14 ug/L gamma-BHC (Lindane) 0.045 ug/L alpha-Chlordane ND ug/L
Ramma-Ch l ordane ND ug/L eptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin 0.053 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endri n ketone 0.056 ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene 85 % Decachlorobiphenyl 75 %
Note J : Result is detected below the reporting limit or is an estimated concentration.
ND= Not detected
NA= Not applicable
IJ!' ~uanterra
Environment.al
Services
Received: 22 APR .98
Analyzed: 14 MAY ·98
Reporting
Limit
0.050 0.050
0.050 0.050 J 0.050
0.050 0.050 0.050 0.050 0.050
0.10 J 0.10
0.10 0.10
0.10 0.10
0.10
0.10
0.10 J
0.50
1.0
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For eddltlonel forms
pl&ase write or call:
Type or Use a ball-point pen and press lirmly.
Facility Name ________ --"G"'ei""gy'-'Ch=•m=i~ca"-1-=-C•c.crpo=ra~ti~••"----------
Address----------~D"'om,,,i=••,..,D~n'--'·v~•----------
___ ....:A»h"'er.,,d,,ee.,,n..cN,.,,C~28=31,.S ____ County ___ ~M~oo-re ___ _
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949
NPOES _____ -'----~~
TYPE OF rnseosAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Field
Well ldenlification Number MW-JJD Well Depth 2512 Ft.
Well Diameler 2 o Sample (Screened) Interval 59,4 Ft. To 69,6 Ft.
Deplh lo Water Level 52 61 It. below measuring poinl (before sampling)
Measuring point is 212 It. above land surface
Spray Field . __ Subsurface Low-Pressure
Piping (LPP)
Land Application ol Sludge
_X_ather
Rotary Distributor Gallons of water pumped/bailed before samplinn 7.7s
Field Analysis: pH 4,66 Specific Conductance 20 uMhos Temp. 16 °c Odor ___ Appearance __ _
Date Sample Collected IQa'll'/8 Dale Lab Sample Analyzeu_ _______ _
Laboratory Name Oµanterra, West Sacramento, CA Certification No. __ __._21 .. 6 ... 6 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD _________ -'----mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
(Note: Use MPN method for hlghty turbid samples)
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I .
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3 ) as N mg/I
Phosphorus: Total as P mg/I
Al -Aluminum mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Mg -Magnesium mg/I
Mn -Manganese mg/I
Na -Sodium mg/I
Ni -Nicke,__ _________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
..cTc..cCc=Lc.c.P.=escctic=cid~es=-•..cres=ul'-"ts-=•-"'tta=-'c""hedc.=..._____ Ug/I
Other (Specify Compounds and
Concentration unijs)
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. lli!le; Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
-- ----·----·----·· ----- -
Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) __________ 9.;..8.;../_10_/_2-'9 ________ _ Casing 0lameter ____________ 2_._0 ________ Inches
Field Personnel __________ R.;... "M"'o"',g"'a'"n""/---N---·c:H..ci.:cckc:s=---------Casing Material __________ s_1a_in_le_s_s_s_1e_e_I ________ _
Slte Name ------------G-'e..,igy:,_;C ___ h---em------ica.;..I __ C:.;occrpo=ra--1...:io.;_n _____ _ Measuring Point Elevation ________ 4_6_3_.4_3 ________ 1/100 ft
Earth Tech Job Number ________ _,3~1~8~19,_ ________ _ Height of Riser (above land surface) 2.39 1/100 ft
Well ID # ______________ M---W __ -1_1 __ D=-----------Land Surface Elevation 461.02 1/100 ft
D Upgradient D Downgradient D Sidegradient Screened Interval 59.40 -69.60 1/100 ft
Weather Condltlons ________ Cc..l.ce.c.ar--/_Sc..uc..n"'n"'y ________ _ Dedicated Pump or Baller 11!1 Yes □No □Type
Air Temperature ___________ 7:_;3:_ _________ •F Steel Guard Pipe Around Casing □Yes 11!1 No D Flushmounted
Total Well Depth (TWD) = ________ 7_5_._39 ________ 1/100 ft Locking Cap 11!1 Yes □No
Depth to Ground Water (DGW) = 59.63 1/100 ft Protective Post/Abutment □Yes 11!1 No
Length of Water Column (LWC) = TWD -DGW = ____ 1_5_. 7_6 ____ 1/100 ft Well Integrity Satisfactory 11!1 Yes □No
1 Casing Volume (OCV) = LWC x 0.163 = 2.57 gal Well Yield □Low D Moderate 11!1 High
3 Casing Volumes = 7. 71 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation _______ __,_W,_,e,,llccW=iz"'a"rd,_ _____ _ Pesticides
Method of Sample Collectlon ________ W=e~ll~W"'i~z~ar_,d _______ _
Total Volume of Water Removed 7.75 gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (fl)
Sp. Cond. (µmhos/cm)
Water Temp. ("C)
TURBIDITY (NTUl"
0
13:20
4.73
-
19
17
9.83
2.5
13:30
4.70
-
20
16
13.19
Refill: B
5.50 7.75
13:40 13:50
4.71 4.66
- -
19 20
16 16
3.29 1.85
Discharge: B
EOMMENTS/OBSERVATIONS .::S:::•::.:mcce::cle:::d:_;a::;.1...:1:::;35:c,5::;., _______________________________________ --i
F;e/d Data/or GW
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Client Name:
Client ID:
LAB ID:
Matrix:
Authorized:
Rust Environmental
MW-llD
302434-0012-SA
AQUEOUS
30 OCT 98
Dilution Factor: 10
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan I I 4,4'-DDD
Endosulfan sulfate
4,4'-DDT
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
#J)\ ~uanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
1.6 ug/L
4.9 ug/L
0.98 ug/L
0.52 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L
0.21 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Recovery
ND%
ND%
Received: 30 OCT 98
Analyzed: 17 NOV 98
Reporting
Limit
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53
0.53 0.53
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5.3
11
MDL
0.084
0.042
0.063
0 .11
0.074
0.084
0.074 0.063
0.084 0.11
0.21
0 .16·
0.21
0.31
0.053
0.35
0.21
0.31
0.25
0.42
11
Acceptable Range
55 -ll5
35 -137
Qualifier
oR
H
H
J
J
Note H Note J
Note o
Note R
ND= Not
= Spiked analyte not
= Result is detected
= Reporting limit(sl = Reporting limit(s
detected because of required sample dilution.
Detected
Reported By: Lisa Stafford
below the reporting limit or is an estimated concentration.
raised due to high level of analyte present in sample.
raised due to sample volume limitations.
Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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UPPER BLACK CREEK AQUIFER MONITORING WELL
MW-16D
-------------------
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name, ________ __,Ge,eeoigy'--"'Che,ee,me,k,eal'-"C"'orpo,=rac,,le,lo!!!n ________ _
Address, ___________ -"De,ome,le,no"'D"'n"""vc,se _________ _
-----'A~h~•nl=ee'"'nuN.,_,C=28~3~15~---County, ___ __JMnooOOJJce'-----
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949 NPDES __________ _
n:e.EQF DISPOSAL OPERATION BEING MONITORED
• · Well Location, ________________________ _ (REQUIRED) Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-16D Well Depth 123 57 Ft.
Well Diameter 2 o Sample (Screened) Interval JlJ.54 Ft. To ms, Ft.
Depth to Water Level 32 73 ft. below measuring point (before sampling)
Measuring point is 3 39 ft. above land surface
Gallons of water pumped/bailed belore samptin°11-------=28,._ ___ _
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application of Sludoe
_Ji:_ Other
Rotary Distribu1or
Field Analysis: pH 4.81 Specific Conductance 28 uMhos Temp. 16 °c Odor ___ Appearance __ _
Date Sample Collected 4121/9ff Date Lab Sample Analyze,u._ _______ _
Laboratory Name Quanterra, w~t Sacramento, CA Certification No. --~''-"l6.,,6c_ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND RELD ACIDIRED __ YES __ NO
COD ____________ mg/1
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note; u.., UPN molhod for highly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/1
pH (when analyzed) units
TOC mg/I
Chloride mg/1
Arsenic mg/1
Grease and Oils mg/1
Hardness: Total mg/1
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Fe -Iron mg/1
Hg -Mercury mg/I
Phenol mg/1
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
K -Potassium mg/I
Mg -Magnesium mg/I
Mn • Manganese mg/I
Na -Sodium mg/1
TKN as N mg/I
Ni -Nicke,. __________ mg/1
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached
Other (Specify Compounds and
Concentration untts)
TCE • results attached
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. · ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back) -
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
---- -----C H Field Data Information Log for Ground Water Sampling
Date (yr/mo/day) ___________ 98_/_04_/_2_1 ________ _
Field Personnel ________ R_._M_o~r~g~a_n_i_B_. _D_il_la_rd ______ _
Site Name __________ Ge__,igy"--C_h_em_ica_l_C_o~rp_o_ra_l_io_n _____ _
Earth Tech Job Number ________ .,.3..:.18,.1.,.9,_ ________ _
Well ID •--------------"M'-'W"---1;.:6;.:D;_ _______ _
D Upgradient D Downgradient 11!1 Sidegradient
Weather Condltions ________ C=.l;.:e;::a:.ir,..:S;.:u:cnc.:n,._y ________ _
AirTemperature ___________ 5~5 __________ •F
Total Well Depth (TWD) = _______ ...;1;::2"'3;.:.5"-7 _______ 1/100 ft
Depth to Ground Water (DGW) = 82.73 1/100 ft
Length of Water Column (LWC) = TWD -DGW = ____ 4_0_.8_4 ____ 1/100 ft
1 Casing Volume (OCV) = LWC x 0.17 = 6.94 gal
3 Casing Volumes = 20.83 gal = Standard Evacuation Volume
Method of Well Evacuation ________ W~e~ll~W=iz=a~rd~------
Method of Sample Collectlon'--------W=e~ll..:.W~i=za~r=d'--------
Total Volume of Water Removed 28 gal
Page_1_of 1
Casing Oiameter ____________ 2_ ..... o ________ inches
Stainless Steel Casing Material ______________________ _
Measuring Point Elevation ________ 4_8_7_.5_5 ________ 1/100 ft
Height of Riser (above land surface) 3.39 1/100 ft
Land Surface Elevation 484.16 1/100 ft
Screened Interval 113.54 -123.57 1/100 ft
Dedic3ted Pump or Baller
Steel Guard Pipe Around Casing
Lock Ing Cap
Protective Post/Abutment
Well Integrity Satisfactory
Well Yield
Comments/Observations
11!1 Yes □No 0 Type Well Wizard
11!1 Yes □No D Flushmounted ------------------11!1 Yes □No
□Yes 11!1 No
11!1 Yes □No
□Low · D Moderate 11!1 High
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY (NTUJ"
0
7:36
4.48
-
87
16
0.61
7 14
7:56 8:18
4.32 4.72
- -
29 28
16 16
0.51 0.48
Refill: B 1/2 Discharge: B
21 28
8:37 8:57
4.80 4.81
- -
28 28
16 16
0.33 0.27
Field Data/or GW
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TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-16D Lab ID: 098752-0007-SA
Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC ND ug/L beta-BHC ND ug/L delta-BHC ND ug/L gamma-BHC (Lindane) ND ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin ND ug/L 4,4'-DDE ND ug/L Endri n ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4' -DDT ND ug/L Endrin aldehyde ND ug/L Endri n ketone ND ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene 75 % Decachlorobiphenyl 50 %
ND c Not detected NA c Not applicable
IJ~\ ~uanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 14 MAY 98
Reporting
Limit
0.050
0.050
0.050
0.050 0.050
0.050 0.050
0.050 0.050 0.050 0 .10
0.10
0.10
0.10
0.10
0.10
0.10
0 .10
0.10
0.50
1.0
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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Client Name:
Client ID:
LAB ID: Matrix: Authorized:
Rust Environmental
MW-16D 098752-0007-SA AQUEOUS 22 APR 98
Dilution Factor: 2.0
Parameter
Trichloroethene
Surrogate
Toluene-dB 4-Bromofluorobenzene l,2-Dichloroethane-d4
Volatile Organics Method 8260
& Infrastructure
Sampled: 21 APR 98 Prepared: NA
Result
290
Recovery
94 % 97 %
115 %
Units
ug/L
{lpuanterra
Environmental
Services
Received: 22 APR 98 Analyzed: 29 APR 98
Reporting
Limit Qualifier
10 o
Acceptable Range
85 -111 81 -117
75 -121
Note o c Reporting limit(s) raised due to high level of analyte present in sample. I NA c Not Applicable
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Reported By: Matt Culver Approved By: Karin Yee
The cover letter is an integral part of this report. Rev 230787
-------------------
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ _,Ge=lgy"-"Ch""e""m"'k,::B::..I C,c:•e:.ryo=ra::1:,:lo::.n ________ _
Address, ___________ ..,De<00,,,m,,,1n,,,oc,D,,_n'-'·v,_e __________ _
____ ..cA,.,,h,aer"'d"'ee"'n..,_N,,c._.,28,.,3,.tS,._ ___ County, ____ ...,M,..ooo,ru;e ___ _
DIVISION OF WATER QUALITY· GROUNDWATER SECTION,
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NPDES ___________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location, _________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-16D Well Depth m 57 Ft.
Well Diameter 2 o Sample (Screened) Interval JJ3 54 Fl. To J23.S7 Ft.
Depth to Water Level 81 35 It. below measuring point (before sampling)
Measuring point Is , 39 fl. above land surface
Gallons of water pumped/bailed before samplin,::Y----~2~1 ____ _
Spray Field __ Subsurface low-Pressure
Piping (LPP)
Land Application of Sludge
_X_Other
Rotary Distributor
Field Analysis: pH 4.92 Specific Conductance 3Q uMhos Temp. 12 °c Odor ___ Appearance __ _
Date Sample Collected JOG'!/'18 Date Lab Sample Analyze·.,_ _______ _
Laboratory Name Quanterra, West Sacramento, CA Certification No. ___ ,1,.2J1066"---
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES NO
COD ____________ mg/1
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use UPN method for hlghty turbid samples) Al • Aluminum mg/I
Dissolved Solids: Total ______ mg/1
pH (when analyzed) units
TOG mg/I
Chloride mg/I
Arsenic mg/I
Ba • Barium mg/I
Ca • Calcium mg/I
Cd • Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Grease and Oils mg/I Fe • Iron mg/I
Hardness: Total mg/I Hg • Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I Mg • Magnesium mg/I
Specific Conductance uMhos Mn • Manganese mg/I
Total Ammonia mg/I Na • Sodium mg/I
TKN as N mg/I
Ni -Nicke,L.__ _________ mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached
Other (Specify Compounds and
Concentration units)
TCE • results attached
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
---- -- --- -
lliiii)
Field Data Information Log for Ground Water Sampling
Pago_1_of
Dato (yr/mo/day) ___________ 98_/_1_0/_2_9 ________ _ Casing Diameter ___________ ...;2::.;·.;;.0 ________ Inches
Field Personnel ________ R-"-. M---'-o'-'rg""a'-'n_/-'-N'-'-.-'-H'-'-ic'"'k"s ______ _ casing Material __________ s_1a_in_1e_s_s_s_1e_e_1 ________ _
Site Name __________ G_e...,ig""y_C_h_e_m_ic_al_C_o-'rp'-o_ra_t_io_n _____ _ Measuring Point Elevation ________ 4_8_7_.5_5 ________ 1/100 ft
Earth Tech Job Number --------~3~1~8~19~---------Height of Riser {above land surface) 3.39 1/100 ft
Well ID# MW-160 Land Surface Elevation 484.16 1/100 ft -------------------------□ Upgradient D Downgradient D Sidegradient Screened Interval 113.54 -123.57 1/100 ft
Weather Conditions _________ S~u_n_n_·s_e _________ _ Dedicated Pump or Baller l!!I Yes □No □Type
Air Temperature ___________ 5::.;0;_ _________ 'F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Woll Depth (TWD) = ________ 1_2_3_.5_7 _______ 1/100 ft Locking Cap l!!I Yes □No
Depth to Ground Water (DGW) = 81.35 1/100 ft Protective Post/Abutment □Yes l!!I No
Length of Water Column (LWC) = TWD -DGW = 42.22 1/100 ft Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCV) = LWC x 0.163 = _____ .;;.6...;.8...;8 _____ gal Well Yield □Low D Moderate l!!I High
3 Casing Volumes = 20.65 gal = Standard Evacuation Volume Comments/Observations
Method of Woll Evacuation _______ ~W~e~ll-'W=iz=a~,d~--:----Pesticides/TCE
Mothod of Sample Colloctlon'--------W=e"-'11-'W-'-i"'z"'ar"d'--------
Total Volume of Water Removed 21 gal
FIELD ANALYSES
VOLUME PURGED (gallons}
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (llmhos/cm)
Water Temp. ('C)
TURBIDITY (NTU)'
0
7:00
4.75
-
46
18
1.50
7
7:18
4.85
-
33
17
1.04
Refill: B 1/2
14 21
7:36 7:53
4.93 4.92
- -
32 30
17 17
0.69 0.73
Discharge: C f OMMENTS/OBSERVATIONS .;:S;.::a:;.;m'"pc.:le;.::dc..ca:.:.t..::0.:_75::;5:.:.· _______________________________________ --f
-
Field Data/or GW
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Client Name:
Client ID:
LAB ID:
Matrix:
Authorized:
Rust Environmental
MW-16D
302434-0008-SA
AQUEOUS
30 OCT 98
Dilution Factor: 1.0
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin 4,4'-DDE
Endri n
Endosulfan II
I 4,4' -ODD
Endosulfan sulfate
4, 4' -DDT
I Endri n aldehyde
Endrin ketone
Methoxychlor
Toxaphene
I Surrogate
I Tetrachloro-m-xylene , Decachlorobiphenyl
lj~\ . ~uanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
Recovery
96 %
102 %
Received: 30 OCT 98
Analyzed: 17 NOV 98
Reporting
Limit MDL Qualifier
0.053 0.0084 R
0.053 0.0042
0.053 0.0063
0.053 0.011
0.053 0.0074
0.053 0.0084
0.053 0.0074 0.053 0.0063
0.053 0.0084 0.053 0.011
0.11 0.021
0 .11 0.016-
0.11 0.021
0.11 0.031
0.11 0.0053
0.11 0.035 0 .11 0.021
0.11 0. 031 0 .11 0.025
0.53 0.042
I. 1 1.1
Acceptable Range
55 -115
35 -137
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Note R = Reporting limit(s) raised due to sample volume limitations.
ND= Not Detected
Reported By: Lisa Stafford Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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~}\ ~uanterra
(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental
MW-16D
302434-0008-SA
AQUEOUS
30 OCT 98
Parameter
Trichloroethene
Surrogate
J,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
ND= Not detected
NA= Not applicable
Reported By: RRAMIREZ
& Infrastructure
Sampled: 29 OCT 98 Received: 30 OCT 98
Prepared: 10 NOV 98 Analyzed: 10 NOV 98
Reporting
Result Units Limit
270
Recovery
ug/L
97 %
102 %
97 %
. Approved By: FKENT
5.0
The cover letter is an integral part of this report.
Rev 230787
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UPPER BLACK CREEK AQUIFER MONITORING WELL
MW-17D
-------------------
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonel forms
please write or call:
Type or Use a ball-point pen and press lirmly.
Facility Name _________ ...,Ge.:•c:cigy"'-"C:::h•:::m"'k""a'-1 C"'o"-'P"='""''"'io"-n ________ _
Address, ___________ _,D,,,o,,,m,,,ine,Oc,Dc,.n"-'v,_e -----------
____ .oA,.,,he,ar"'°d"'ee"'n..,_N,,C"-"'28""3,.,IS._ ___ County/ ____ ..11M'1lQOHlCncc_ __ _
Well Location, _________________________ _
DIVISION OF WATER DUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626·0578
[phone]
.PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949 NP0ES ___________ _
IY!'£..QF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Lagoon __ Septic Tank/Drain FiekS
Well Identification Number MW•J7P Well Depth 123 J7 Ft.
Well Diameter 2 o Sample (Screened) lnlerval 112,21 Ft. To 123,17 Ft. Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Depth to Water Level 84 55 ft. below measuring point (before sampling)
Measuring point is 2 65 ft. above land surface
Gallons of water pumped/bailed before samplin,~.,_ ___ ~2~0 ____ _
Field Analysis: pH 4.73 Specific Conductance 2li uMhos Temp. 55 °c
Land Appficalion of Sluclae
_X_Other
Rotary Oistribu1or
Odor ___ Appearance•---
Date Sample Collected 4121(28 Dale Lab Sample Analyze,"---------
Laboratory Name Quanlerra, West Sacramento, CA Certification No. ___ ... 2, .. 66,,_ __
SAMPLES FOR METALS WERE COLLECTED UNFIL TEAED AND FIELD ACIDIFIED __ YES NO
COD ____________ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: U• UPN method for highly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Ba -Barium mg/)
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
K -Potassium mg/I
Mg -Magnesium mg/I
Mn • Manganese mg/I
Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke,c_ _________ mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached ug/1
ug/I _____________ ug/1
Other (Specify Compounds and
Concentration units)
TCE • results attached
I CERTIFY THAT THIS REPORT IS TRUE [>.ND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW·59 REV. 8196
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
- - - - ----- - ----liiiil liiil liiill --Field Data Information Log for Ground Water Sampling
Pago_1_of
Dato (yr/mo/day) 98/04/21 Casing Diameter 2.0 Inches
Field Personnel R. Mor9an / B. Dillard Casing Material Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 489.60 1/10011
Earth Tech Job Number 31819 Height of Riser (above la!1d surface) 2.65 1/100 fl
Well ID# MW-17D Land Surface Elevation 486.95 1/100 fl
D Upgradient D Downgradient D Sidegradient Screened Interval 112.91 -123.17 1/100 fl
Weather Conditions Clear I Sunni Dedicated Pump or Baller l!!I Yes □No D Type Well Wizard
Air Temperature 60 "F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Woll Depth (TWO) = 123.17 1/100 fl Locking Cap l!!I Yes □No
Depth to Ground Waler (DGW) = 84.55 1/100 fl Protective Post/Abutment □Yes l!!I No
Length of Water Column (LWC) = TWO -DGW = 38.62 1/100 fl Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCVJ = LWC x 0.17 = 6.57 gal Woll Yield □Low D Moderate l!!I High
3 Casing Volumes= 19.70 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard
Method of Sample Collection Well Wizard
Total Volume of Water Removed 20 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 6.75 13.50 20.0
TIME (military) 9:17 9:35 9:52 10:10
pH ($.U.) 4.45 4.64 4.75 4.73
Drawdown (fl.) - - - -
Sp. Cond. (µmhos/cm) 31 25 26 26
Water Temp. (°C) 231 0.88 0.71 0.55
TURBIDITY (NTUJ• 16 16 16 16
• Nenh•lomelrl• Turbidllv • •nits Refill: B 1/2 Discharge: B
OMMENTS/OBSERVATIONS SAMPLED AT 1012
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Field Data/or GW
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TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-17D Lab ID: 098752-0009-SA Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC ND ug/L beta-BHC ND ug/L delta-BHC ND ug/L gamma-BHC (Lindane) ND ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosul fan I ND ug/L Dieldrin ND ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4' -ODD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone ND ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene 77 % Decachlorobiphenyl 69 %
ND= Not detected NA= Not applicable
IJ}\ ,:euanterra
Environmental
Services
Received: 22 APR.98
Analyzed: 14 MAY 98
Reporting Limit
0.050 0.050
0.050 0.050 0.050 0.050
0.050
0.050
0.050
0.050
0.10
0.10
0.10
0.10
0.10
0.10
0.10 0 .10 0.10
0.50 1.0
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
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Volatile Organics
Method 8260
Client Name: Client ID: LAB ID:
Rust Environmental & Infrastructure MW-17D 098752-0009-SA Matrix:
Authorized:
AQUEOUS Sampled: 21 APR 98 22 APR 98 Prepared: NA
Dilution Factor: 2.0
Parameter Result Units
Trichloroethene 320 ug/L
Surrogate Recovery
Toluene-dB 92 % 4-Bromofluorobenzene 96 % l,2-Dichloroethane-d4 115 %
~)\ ,euanterra
Em?.ronmental
Services
Received: 22 APR 98 Analyzed: 29 APR 98
Rerorting imi t Qualifier
10 o.
Acceptable Range
85 -111 81 -117 75 -121
Note o • Reporting limit(s) raised due to high level of analyte present in sample. NA c Not Applicable
Reported By: Matt Culver Approved By: Karin Yee
The cover letter is an integral part of this report. Rev 230787
-------------------
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name ---------"G'°'el,.,gy'-'Ch=•m::,i:o:c•::.1-"Co"'rpo=ra:::l:e:ion::_ _______ _
Address ___________ _:,cDo::,m::.,iD::.,O:.,D,en,,_·ve,._ _________ _
---~A=he=r"'dee=•·~N=C~28=3=1=5 ____ County, ___ __.M,..oo......,re.__ __ _
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949
NPDES..,.,......,,.===---=-=-=== TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number · MW-17D Well Depth 123 17 Ft.
Well Diameter 2 o Sample (Screened) Interval 112,21 Ft. To 123.11 Fl.
Depth to Water Level 83 08 It. below measuring point (before sampling)
Measuring point is 2 •s It. above land surface
Gallons of water pumped/bailed before samplin" 20.0
Spray Field __ Subsurface low-Pressure
Piping (LPP)
Land ApplicaUon ol Sluclae
_X_Qther
Ro1ary Distributor
Field Analysis: pH 4.61 Specific Conductance 22 uMhos Temp. J• 0c Odor ___ Appearance __ _
Date Sample Collected 1oa•t28 Date Lab Sample Analyze~-------
Laboratory Name Quanterra, West Sacramento, CA Certification No. __ __.2._J6ft,,__ __
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD_...,..,.=-=--,-------mg/I Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Uae MPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total mg/1 Ba • Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG mg/I Cd -Cadmium mg/I
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu -Copper mg/I
Grease and Oils mg/I Fe -Iron mg/I
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/1 Mg -Magnesium mg/I
Specific Conductance uMhos Mn • Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke,__ _________ mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • results attached
Other (Specify Compounds and
Concentration units)
TCE • results attached
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8196
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
---- ----------.. --Field Data Information Log for Ground Water Sampling
Date (yr/mo/day) ___________ 98_1_1_01_2_9 ________ _
Field Personnel ________ R_. M--'-o~rg"-a __ n_l_N--._H--icl<=s ______ _
Site Name __________ Ge_,ig"-y_C_h_e_m_ica_l_C_o--rp--o_ra_t_io_n _____ _
Earth Tech Job Number --------~3~1~8~19~---------
Well ID # _____________ M_W_-_17_D _______ _
0 Upgradient O Downgradient O Sidegradient
Weather Condltlons ________ C""l"e"'ar--/_Sc..u::.;n--n"'y ________ _
Air Temperature ___________ 5::.;0:__ _________ °F
Total Well Depth (lWD) = ________ 1_2_3._1_7 _______ 1/100 ft
Depth to Ground Water (DGW) = 83.08 1/100 ft
Length of Water Column (LWC) = TWO -DGW = ____ 4_0_.0_9 ____ 1/100 ft
1 Casing Volume (OCVJ = LWC x 0.163 = 6.53 gal
3 Casing Volumes= 19.60 gal= Standard Evacuation Volume
Method of Well Evacuatlon _______ --'-W~e"-11--W=iz~a~rd~------
Method of Sample Collectlonc_ ______ W=eaall_.W=iz,.ar:.,d,__ _____ _
Total Volume of Water Removed 20.0 gal
Page_1_of
Casing 0iameter ____________ 2_._0 ________ Inches
casing Material __________ s_ta_in_1e_s_s_s_tee_1 ________ _
Measuring Point Elevatlon ________ 4_8_9_.6_0 ________ 11100 ft
Height of Riser (above land surface) 2.65 1/100 ft
Land Surface Elevation 486.95 1/100 ft
Screened Interval 112.91 -123.17 1110011
Dedicated Pump or Baller l!!I Yes O No O Type
Steel Guard Pipe Around Casing l!!I Yes O No O Flushmounted
Locking Cap
Protective Post/Abubnent
Well Integrity Satisfactory
Well Yield
Comments/Observations
Pesticides TCE
l!!I Yes O No
D Yes l!!I No
l!!I Yes O No
D Low D Moderate l!!I High
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (fl.)
Sp. Cond. (llmhoslcm)
Water Temp. (°C)
TURBIDITY (NTUl"
0
7:00
5.21
-
152
16
0.33
6.75
7:25
4.60
-
29
16
1.43
Refill: B
13.5 20.0
7:50 8:15
4.56 4.61
--
27 27
16 16
0.78 0.70
Discharge: C f OMMENTSIOBSERVATIONS .::S:.::a'-'m"'p:.::le.::.d.=a;..;I 0:.:8:.::2.::.0·'----------------~~-----------------------t
Field Data for GIY
I
I Client Name:
Client ID:
I LAB ID: Matrix:
Authorized:
Rust Environmental
MW-17D
302434-0001-SA AQUEOUS
30 OCT 98 I Dilution Factor: 1.0
I
Parameter
alpha•BHC
beta•BHC
delta·BHC I gamma·BHC (Lindane) alpha-Chlordane
gamma-Chlordane
I Heptach l or
Aldrin Heptachlor epoxide
Endosulfan I
I Dieldrin 4,4'·DDE
Endrin
Endosulfan II
I 4, 4' •□DD Endosulfan sulfate
4,4'-DDT
I Endrin aldehyde Endri n ketone
Methoxychlor Toxaphene
I Surrogate
I Tetrachloro•m•xylene
Decachlorobiphenyl
I
I
~)\ ,euanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
ND ug/L ND ug/l
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/l
ND ug/L ND ug/L
ND ug/L ND ug/l
ND ug/L
ND ug/L
ND ug/L
ND ug/l
ND ug/l
ND ug/L ND ug/l
Recovery
98 %
98 %
Received: 30 OCT 98
Analyzed: 16 NOV 98
Reporting
Limit MDL Qualifier
0.058 0.0092 R 0.058 0.0046
0.058 0.0069
0.058 0.012
0.058 0.0081
0.058 0.0092
0.058 0.0081
0.058 0.0069
0.058 0.0092
0.058 0.012
0 .12 0.023 0 .12 0.017
0. 12 0.023
0 .12 0.034
0.12 0.0058
0 .12 0.038
0.12 0.023
0 .12 0.034
0 .12 0.028
0.58 0.046
1.2 !. 2
Acceptable Range
55 · 115
35 · 137
I Note. R = Reporting limit(s) raised due to sample volume limitations.
ND= Not Detected
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Reported By: Lisa Stafford Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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#j)\ ,euanferra
(8240 list) · Volatile Organics Target Compound List {TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental
MW-17D
302434-0001-SA
AQUEOUS
30 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
ND= Not detected NA= Not applicable
Reported By: RRAMIREZ
& Infrastructure
Sampled: 29 OCT 98
Prepared: 10 NOV 98
Result Units
350
Recovery
ug/L
103 %
lll %
ll4 %
Received: 30 OCT 98
Analyzed: 10 NOV 98
Reporting
Limit
5.0
Approved By: FKENT
The cover letter is an integral part of this report.
Rev 230787
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UPPER BLACK CREEK AQUIFER MONITORING WELL
MW-18D
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
--
For addltlonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ ..,Gc.ce,,igy,._C"'h"'e"'m"'ica=l'-'C"'o"'rp"'o"'ra""ti"'on"---------
Address ____________ ~D~•m=in"-o"'-D'--'riv,.,e~------~---
____ A.,_be=rd.,ee,,n,._,_,N~C_,28=31,.,.5 ____ County ____ M=oo~•~e ___ _
- --lliii1 -liill
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949 NPDES ___________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location _________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-ISP Well Depth 72 3li Ft.
Well Diameter 2 o Sample (Screened) Interval 62 Q9 Ft. To 72,41 Ft.
Depth to Water Level 46 6J ft. below measuring point (before sampling)
Measuring point Is 2 M ft. above land surface
Gallons of water pumped/bailed before samplinn 13.5
Spray Field · __ Subsurface Low-Pressure
Piping (LPP)
Land Application ol Sludae
_X_ether
Rotary Distributor
Field Analysis: pH 4.1 Specific Conductance M uMhos Temp. f6 °c Odor ___ Appearance __ _
Date Sample Collected 4a!t26 Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ___ 2~1~66~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/I Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghty turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOC mg/I Cd -Cadmium mg/I
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu • Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I Mg -Magnesium mg/I
Specific Conductance uMhos Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke.__ _________ mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides • resull<i attached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on beck)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
-·----_, -liill
Field Data Information Log for Ground Water Sampling
Page_1_of 1
Date (yr/mo/day) 98/04/21 Casing Diameter 2.0 Inches
Field Personnel R. Moraan / B. Dillard Casing Material Sch 40 PVC/Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 447.71 1/10011
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.66 1/10011
Well ID# MW-18D Land Surface Elevation 444.75 1/100 fl
D Upgradient D Downgradient D Sidegradient Screened Interval 62.09 -72.41 1/100 fl
Weather Conditions Part!}: Cloudy Dedicated Pump or Baller l!!I Yes □No D Type Well Wizard
Air Temperature 65 "F Steel Guard Pipe Around Casing l!!I Yes □No D Flushmounted
Total Well Depth (TWO)= 72.36 1/10011 Locking Cap l!!I Yes □No
Depth to Ground Water (DGW) = 46.61 1/100 fl Protective Post/Abutment □Yes l!!I No
Length of Water Column (LWC) = TWO • DGW = 25.75 1/10011 Well Integrity Satisfactory l!!I Yes □No
1 Casing Volume (OCV) = LWC x 0.17 = 4.38 gal Well Yield □Low D Moderate 1!!1 High
3 Casing Volumes = 13.13 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard
Method of Sample Collection Well Wizard
Total Volume of Water Removed 13.5 gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0 4.5 9.0 13.5
TIME (military) 12:12 12:22 12:32 12:42
pH (S,U,) 3.89 4.00 4.02 4.10
Drawdown (fl) --- -
Sp. Cond, (µmhos/cm) 66 64 65 64
Water Temp, (°C) 17 16 16 16
TURBIDITY (NTU)• 0,96 0.60 0.56 0.27
• Nenhelo--..,e TP..,lditv "•I'-Refill: B 1/2 Discharge: B
COMMENTS/OBSERVATIONS SAMPLED AT 1245 I
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Field Da1afor CW
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Client Name: Client ID:
Lab ID:
TCL Organochlorine Pesticides/PCBs
Method 8080
Rust Environmental & Infrastructure MW-18D
098752-0010-SA
lj)\ ~uanterra
Environmental
Services
Matrix: AQUEOUS Sampled: 21 APR 98 Received: 22 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98 Analyzed: 14 MAY 98
Parameter Result Units
Reporting
alpha-BHC 1. 7 ug/L beta-BHC 6.5 ug/L delta-BHC 1.6 ug/L gamma-BHC (Lindane) 1.1 ug/L alpha-Chlordane ND ug/L Ramma-Chlordane .ND ug/L eptachlor ND ug/L A 1 dri n ND ug/L Heptachlor epoxide 0.075 ug/L Endosulfan I ND ug/L Dieldrin 0.66 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone 1.1 ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene ND % Decachlorobiphenyl ND %
Note o Reportin$ limit(s) raised due to high level of analyte present 1n sample.
Note J
Note H
Result is detected below the reporting limit or is an estimated concentration.
Spiked analyte not detected because of required sample dilution.
ND= Not detected NA= Not applicable
Limit
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0. 50
1.0
1.0 1.0 1.0
1.0
1.0 1.0
1.0 1.0 5.0 10
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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Volatile Organics Method 8260
Client Name:
Client ID:
LAB ID:
Rust Environmental & Infrastructure MW-18D
098752-0010-SA Matrix: Authorized: AQUEOUS Sampled: 21 APR 98 22 APR 98 Prepared: NA
Dilution Factor: 1.0
Parameter Result Units
Trichloroethene 6.2 ug/L
Surrogate Recovery
Toluene-dB 93 % 4-Bromofluorobenzene 97 % l,2-Dichloroethane-d4 118 %
I~)' ~uanterra
Environmental
Services
Received: 22 APR 98 Analyzed: 30 APR 98
Reeorting imit Qualifier
5.0
Acceptable Range
85 -111 81 -117 75 -121
NA~ Not Applicable
Reported By: Matt Culver Approved By: Karin Yee
, The cover letter is an integral part of this report. Rev 230787
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonel forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ ..,G~•~igy~Ch~•~m~ica~l~C~•~rpo=ra~•i~••~--------
Address ___________ ~D=•m=l•=•~D~riv~•~----------
____ A~be=•d~ee~•=N~C_,28=31~5 ____ Counly ____ M=oo~a:~---
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626·0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949 NPOES ___________ _
IYEE.QF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________ ~---------Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-JRQ Well Depth 72 36 Ft.
Well Diameter 2 o Sample (Screened) Interval 62,09 Ft. To n 41 Ft.
Depth to Water Level 46 12 ft. below measuring point (before sampling)
Measuring point is 2 66 ft. above land surface
Gallons of water pumped/bailed before samplinn-___ ..,1-"J ____ _
Spray Field __ Subsurface low-Pressure
Piping (LPP)
Land Application of Sludae
_X_Other
Ro1ary Oistribu1or
Field Analysis: pH 4.07 Specific Conductance JOI uMhos Temp. 17 °c Odor ___ Appearance __ _
Date Sample Collected 1oaw• Dale Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramenlo, CA Certification No. ---'-1=66~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD -....,...,.c,-,c--,-------mg/I Coliform; MF Fecal /100ml
Coliform; MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (N03 ) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG mg/I
Chloride mg/I
Arsenic mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Grease and Oils mg/I
Hardness; Total mg/I
Phenol mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Mg -Magnesium mg/I
Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke~ _________ mg/1
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
TCE • results attached
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent')
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
--_,_ --------------EARTH©T EC H Field Data Information Log for Ground Water Sampling
Date (yr/mo/day) __________ .:.98"'/-'1-'-0/-=2cc9 ________ _
Field Personnel ________ R_. M_o~rg~a_n_/_N_._H_ic_k_s ______ _
Site Name __________ G_e~igy~C_h_em_ica_l_C_o~rp_o_ra_li_o_n _____ _
Earth Tech Job Number ________ .,,3_,_18,,_1.,_,9,_ ________ _
Well ID # _____________ -"M-"W-'---1'-'8"0'---------
□ Upgradient D Downgradient D Sidegradient
Weather Conditlons. _________ _:Sccu"'n"n._ ________ _
AlrTemperature ___________ 6_5 __________ °F
Total Well Depth (TWD} = ________ 7cc2cc·.:.36"--_______ 1/100 It
Depth to Ground Water (DGW) = 46. 72
Length of Water Column (LWC) = TWD -DGW = 25.64
1/10011
1/10011
1 Casing Volume (OCV) = LWC x 0.163 = ______ 4_.1_8 _____ gal
3 Casing Volum~ = 12.54 gal = Standard Evacuation Volume
Method of Well EvacuaUon ________ W.,_,_,e.,,ll"W=iz.,a.,rd,_ _____ _
Method of Sample CollecUon. _______ W=e~ll~W=iz~a'-'rd,_ _____ _
Total Volume of Water Removed 13 gal
Page_1_of
Casing Dlameter ____________ 2_._0 ________ 1nches
Sch 40 PVC/Stainless Steel Casing Material ______________________ _
Measuring Point Elevation ________ 44_7_. 7_1 ________ 1/100 It
Height of Riser (above land surface) 2.66 1/100 ft
Land Surface Elevation 444. 75 1/100 It
Screened Interval 62.09 -72.41 1/100 It
Dedicated Pump or Baller l!!I Yes □No □Type
Steel Guard Pipe Around Casing =--=--==------------l!!I Yes □No D Flushmounted
Locking Cap
Protective Post/Abutment
Well Integrity Satisfactory
Well Yield
Comments/Observations
Pesticides TCE
l!!I Yes
□Yes
l!!I Yes
□Low
□No
l!!I No
□No
D Moderate l!!I High
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (It.}
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY INTU)•
0
10:58
4.21
-
63
18
0.74
4 9 13
10:10 11:23 11:33
4.03 4.07 4.07
---
86 100 101
17 17 17
1.68 1.01 1.42
Refill: Discharge: f OMMENTS/OBSERVATIONS ..:S..:a""m""p"'le..:d...;:ac,;,t_;,1..;.13;,,;5;__ _______________________________________ -,
1
Field Da1afor GW
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~\ r/Uanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: MW-18D
LAB ID: 302434-0011-SA
Matrix: AQUEOUS
Authorized: 30 OCT 98
Dilution Factor: 20
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane) alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin 4,4'-DDE
Endrin
Endosulfan I I
4,4'-DDD
Endosulfan sulfate
4, 4' -DDT
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
Note
Note
Note
ND=
H = Spiked analyte not
J = Result is detected
o = Reporting limit(s)
Not Detected
Sampled: 29 OCT 98 Received: 30 OCT 98
Prepared: 02 NOV 98 Analyzed: 17 NOV 98
Result Units
Reporting
Limit MDL Qualifier
1. 6 ug/L 1.0 0 .16 0 8. 2 ug/L 1.0 0.081
1. 9 ug/L 1.0 0.12
1.0 ug/L 1.0 0.20
ND ug/L 1.0 0 .14
ND ug/L 1.0 0 .16
ND ug/L 1.0 0 .14
ND ug/L 1.0 0 .12 ND ug/L 1.0 0 .16 ND ug/L 1.0 0.20
0.50 ug/L 2.0 0.40 J ND ug/L 2.0 0.30
ND ug/L 2.0 0.40 ND ug/L 2.0 0.59
ND ug/L 2.0 0 .10 ND ug/L 2.0 0.67 ND ug/L 2 .0 0.40
ND ug/L 2.0 0.59 ND ug/L 2 .0 0.49
ND ug/L 10 0.81 ND ug/L 20 20
Recovery Acceptable Range
ND% 55 -115 H
ND% 35 -137 H
detected because of required sample dilution.
below the reporting limit or is an estimated concentration. raised due to high level of analyte present in sample.
I Reported By: Lisa Stafford Approved By: Mike Orbanosky
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Rev 230787
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~}\ ,euanterra
(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental MW-180
302434-0011-SA AQUEOUS
30 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-Dichloroethane-d4
Toluene-dB
4~Bromofluorobenzene
ND= Not detected NA= Not applicable
Reported By: RRAMIREZ
& Infrastructure
Sampled: 29 OCT 98 Received: 30 OCT 98
Prepared: 10 NOV 98 Analyzed: 10 NOV 98
Reporting
Result Units Limit
4.2 ug/L 1.0
Recovery
94 %
IOI %
97 %
Approved By: FKENT
The cover letter is an integral part of this report.
Rev 230787
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UPPER BLACK CREEK AQUIFER MONITORING WELL
MW-30D
-liil iiiii iiil iiiii ----== -= m!! l!!!I!!!! -------GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name __________ G_e_igy~C~h_e_m_k~al_C~•~·rp~•=ra~li=••~--------
Address ___________ ~D~om=in~•=D~ri•~•~----------
____ A,.be=rd,,.,ee,.,n,,_, • .,_,N,.C_.28=31.,5 ____ County ____ M=oo~a,._ __ _
DIVISION OF WATER QUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WO 0009949
NPOES __ =~-----~== ~F rnspoSAL OPERATION BEING MONITORED
(REQUIRED) Well Location _________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-30D Well Depth 25 38
Well Diameter 2 o Sample (Screened) Interval 62.49 Ft. To 73
Depth to Water Level •• 20 ft. below measuring point (before sampling)
Measuring point Is 2 20 ft. above land surface
Gallons of water pumped/bailed before samplinn 18.0
Ft.
Ft. Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Lend Application ol Sludie __ Other
Ro1ary Distributor
Field Analysis: pH 4,7 Specific Conductance 30 uMhos Temp. 16 °c Odor ___ Appearance __ _
Date Sample Collected 4{1J/28 Date Lab Sample Analyze~--------
Laboratory Name Quanlerra, West Sacramento, CA Certification No. ___ 2~1=66~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ____________ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for highly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
Ba • Barium mg/I
Ca -Calcium mg/I
TOG mg/I
Chloride mg/I
Arsenic mg/I
Cd • Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/)
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Fe -Iron mg/)
Hg -Mercury mg/I
K · Potassium mg/I
Mg · Magnesium mg/I
Mn • Manganese mg/I
Na · Sodium mg/I
Ni -Nicke __________ mg/I
Pb · Lead mg/I
. Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentralion units)
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back lor Instructions.
•• Submit blue and yellow copies only to address above.
- -
--iiii illii iiliii l!!!!!!!I -- -- --Field Data Information Log for Ground Water Sampling
Pege_1_ of _1_
Date (yr/mo/day) 98/04/21 Casing Diameter 2.0 Inches
Field Personnel R. Morllan / B. Dillard Casing Materlal Sch 40 PVC/Stainless Steel
Site Name Geigy Chemical Corporation Measuring Point Elevation 451.25 1/100 It
Earth Tech Job Number 31819 Height of Riser (above land surface) 2.20 1/100 It
Well ID# MW-30D Land Surface Elevation 449.03 1/100 It
D Upgradient D Downgradient D Sidegradient Screened Interval 62.49 -73.00 1/100 It
Weather Conditions Clear, Sunnl Dedicated Pump or Baller l!ll Yes □No D Type Well Wizard
Air Temperature 60 "F Steel Guard Pipe Around Casing l!ll Yes □No D Flushmounted
Total Well Depth (TWO) a 75.38 1/100 It Locking Cap l!ll Yes □No
Depth to Ground Water (DGW) = 49.20 1/100 It Protective Post/Abutment □Yes l!ll No
Length of Water Column (LWC) = TWO-DGW -26.18 1/100 It Well Integrity Satisfactory l!ll Yes □No
1 Casing Volume (OCV) = LWC x 0.17 C 4.45 gel Well Yield □Low D Moderate l!ll High
3 Casing Volumes= 13.35 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation Well Wizard
Method of Sample Collection Well Wizard
Total Volume of Water Removed 18.0 gel
FIELD ANALYSES
VOLUME PURGED (gallons) 0 4.5 9.0 13.5 18.0
TIME (mlll1ary) 11 :15 11:25 11:35 11:45 11:55
pH (S.U.) 4.39 4.44 4.69 4.74 4.70
Orawdown (It.) ----------
Sp. Cond. (l'mhos/cm) 48 31 31 31 30
Water Temp. ("C) 16 16 16 16 16
TURBIDITY (NTU)• 0.82 2.51 2.08 1.39 1.11
• Neohelometrlc Turbldltv Units Rellil: B 1/2 Discharge: B
fOMMENTS/OBSERVATIONS. SAMPLED AT 1158. I
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(/l)uanterra
Client Name: Client ID:
Lab ID:
TCL Organochlorine Pesticides/PCBs
Method 8080
Rust Environmental & Infrastructure MW-30D
098752-0017-SA
Emironmental
Services
Matrix: AQUEOUS Sampled: 21 APR 98 Received: 22 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98 Analyzed: 14 MAY 98
Parameter Result . Reporting Units
alpha-BHC 1.1 ug/L beta-BHC 4.8 ug/L delta-BHC 1.0 ug/L gamma-BHC (Lindane) 0.73 ug/L alpha-Chlordane ND ug/L ~amma-Chlordane ND ug/L eptachlor · ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin 0.51 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4, 4' -DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone 0.81 ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene ND % Decachlorobiphenyl ND %
Note o Reportin~ limit(s) raised due to high level of analyte present 1n sample.
Note J Result is detected below the reporting limit or
is an estimated concentration.
Note H Spiked analyte not detected because of required sample dilution.
ND= Not detected
NA= Not applicable
Limit
0.50
0.50 0.50
0.50 0.50 0.50 0.50 0.50 0.50 0.50
1.0 1.0
1.0 1.0
1.0
1.0
1.0
1.0 1.0
5.0
10
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
0
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- -I!!!! == -iiil - - - --- - -- - --·-
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addlUonal forms
please write or call:
• Type or Use a ball-point pen and press firmly.
Facility Name __________ G_e,-"·gc..y _C_he_m_k_a_l C_o_r"-po_r_a1_;o_n ________ _
Address ____________ o_o_m_;n_o_o_,;_••-----------
____ A=b•_rd_•_•n~,_N_C_2_8_Jt~5 ____ County _____ M~•·~'~·----
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27828-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPDES
TYPE OF rnspo""sA.,.,I-O=PE"'RA=r=-1o""N:-:-::B:::E:::IN-,:G::-:-:M:::Oc,N:::IT::O:-:R=Eo
(REQUIRED) Well Location __________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number MW-JOO Well Depth 75.38
Well Diameter 2.0 Sample (Screened) Interval 62.49 Ft. To 73
Depth to Water Level 49.08 ft. below measuring point (before sampling)
Measuring point is 2.20 ft. above land surface
Gallons of water pumped/bailed before samplin,n,,_ ____ t_J ____ _
Ft.
Ft. Spray Field __ Subsur1ace Low-Pressure
Piping (LPP)
Land Application ot Slu~e
_·_Other
Rotary Distributor
Field Analysis: pH 4.67 Specific Conductance JO uMhos Temp. 17 °c Odor ___ Appearance __ _
Date Sample Collected t0/29198 Date Lab Sample Analyze~--------
Laboratory Name Quanttrra, West Sacramento, CA Certification No. ---=21~6~6 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
coo ___________ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG mg/I Cd -Cadmium mg/I
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu -Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Fe -Iron mg/I
Hg -Mercury mg/1
K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
Mg -Magnesium mg/I
Mn -Manganese mg/I
Na -Sodium mg/I
~N~N m~
Ni -Nicke~---------mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
Other (Specify eo·mpounds and
Concentration units)
u~
u~
u~
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on beck)
Signature of Permittee (or Authorized Agent')
GW-59 REV. 8/96
Date • See back for Instructions.
•• Submit blue and yellow copies only to address above.
. . --. . --------
=-- -- - - -- ---- - -
iiil
EARTH©TECH Field Data Information Log for Ground Water Sampling
Page __ of
Date (yrlmo/day) ___________ 9_81_1_0_/2_9 ________ _ Casing Dlameter ___________ ....:a2·;.:0 ________ lnches
Field Personnel __________ R_. _M-'o~rg"a_n_i_N--._H_i-'-ci<-'-s'---------casing Material ________ s_ch_40_Pv_c_1_s_ta_in_Ie_s_s_s_te_e_I ______ _
Slte Name ---------'G"'e""ig.,y._C-'-h--e'-'m=ica"'-I C-'-o"rp-"-"o'-'ra"'ti-'-o--n _____ _ Measuring Point Elevation ________ 4_5_1_.2_5 ________ 11100 ft
Earth Tech Job Number _________ 3_1_81_9 _________ _ Height of Riser (above land surface) 2.20 11100 ft
Well ID# MW-30D Land Surface Elevation 449.03 11100 ft -------------------------□ Upgradient D Downgradient D Sidegradient Screened Interval 62.49 -73.00 11100 ft
Weather Conditlons. ________ C---'le __ a_r _I S----""-"~Y ________ _ Dedicated Pump or Baller 11!1 Yes □No □Type
Air Temperature -------------'7'-'5'------------°F Steel Guard Pipe Around Casing 11!1 Yes □No D Flushmounted
Total Well Depth (TWO) = ________ 7_5_._38 ________ 11100 ft Locking Cap 11!1 Yes □No
Depth to Ground Water (DGW) = 49.08 11100 ft Protective Post/Abutment □Yes 11!1 No
Length of Water Column (LWC) = TWO -DGW = ____ 2_6_.3_0 ____ 11100 ft Well Integrity Satisfactory 11!1 Yes □No
1 Casing Volume (OCVJ = LWC x 0.163 = 4.29 gal Well Yield □Low D Moderate 11!1 High
3 Casing Volumes = 12.86 gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation _______ ~W~e~I __ I W=iz~a~,d~------Pesticides
Method of Sample Collectlon. _______ W=e.,,11_,W=iz.,a:..,rd,._ _____ _
Total Volume of Water Removed 13 gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY (NTUI•
0 4.5 9.0
14:07 14:16 14:26
4.56 4.54 4.64
-- -
39 32 31
18 17 17
14.1 9.76 7.21
Refill: Discharge:
le collected at 1438.
13.0 .
14:30
4.67
-
30
17
8.84
-
Field Data/or GW
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Client Name:
Client ID:
LAB ID:
Matrix:
Authorized:
Rust Environmental
MW-30D 302434-0013-SA
AQUEOUS
30 OCT 98
Dilution Factor: 20
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane gamma-Chlordane
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin
Endosulfan II
I 4,4'-DDD
Endosulfan sulfate
4, 4' -DDT
Endrin aldehyde
I Endri n ketone
Methoxychlor
Toxaphene
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Surrogate
Tetrachloro-m-xylene Decachlorobiphenyl
#}~\ ,:euanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 29 OCT 98
Prepared: 02 NOV 98
Result Units
2.3 ug/L 9.8 ug/L 2.0 ug/L
0.75 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L 0.50 ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Recovery
ND%
ND%
Received: 30 OCT 98
Analyzed: 17 NOV 98
Reporting
Limit
1.0
1.0 1.0
1.0
1.0
1. 0
1. 0
1.0
1.0
1.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
IO
20
MDL
0 .16
0.081 0.12
0.20
0 .14
0 .16
0.14
0.12
0.16
0.20
0.41
0.31
0.41
0.59
0.10
0.67
0.41
0.59
0.49
0.81
20
Qualifier
0
J
J
Acceptable Range
55 -115 H
35 -137 H
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I Note H = Spiked analyte not
J = Result is detected
o = Reporting limit(s) Not Detected
detected because of required sample dilution.
I Note
Note
ND=
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Reported By: Lisa Stafford
below the reporting limit or is an estimated concentration.
raised due to high level of analyte present in sample.
Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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TREATMENT SYSTEM
EFFLUENT FROM LEAD CARBON CANISTER
TRAIN A
------------ - - - - ---GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonal forms
please write or call:
Type or Use a batl•polnt pen and press firmly.
Facility Name __________ G_ri-"gy,_C_h_r_m_ic_a1_c_o_rp,_o_ra_1_io_n _______ _
Address ____________ D_o_m_in..c.o_Dc.ri_ve'------------
____ ;..:A;:;;b•:.:.r;:;;d•:..:•""''-'-N-'C'-2"'8"'3:..:15'-----County, ____ =M=•=•r~•----
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPDES-:,-,-,--,-==-:c========-=· TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) · Well Location __________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number V-47 Well Depth ____ Ft.
Well Diameter ___ Sample (Screened) Interval Ft. To Ft.
Depth to Water Level ___ It. below measuring point (before sampling) .
Measuring point is ____ ft. above land surface
Gallons of water pumped/bailed before samplinn,,_ ________ _
Spray Field __ Subsurface Low•Pressure
Piping (LPP)
Land Application ol Slu~e _. __ Other
Rotary Distributor
Field Analysis: pH J.72 Specific Conductance 184 uMhos Temp. 17 °c Odor ___ Appearance __ _
Date Sample Collected 4/21198 Date Lab Sample Analyze,~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ---=21~66~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ___________ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3 ) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlgl'lty turt>kl samples) Al • Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG mg/I
Chloride mg/I
Arsenic mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe • Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K • Potassium mg/I
Sulfate mg/I Mg • Magnesium mg/I
Specific Conductance uMhos
Total Ammonia mg/1
Mn • Manganese mg/I
Na • Sodium mg/I
TKN as N mg/I
Ni -Nicke __________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Soecify Compounds) TcL Pesticidrs -results attachtd
Other (Specify Compounds and
Concentration units)
TCE -rrsults aUachtd
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. NQ!e;_ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8196
Date • See back for Instructions.
•• Submit blue and yellow copies only to address above.
------- ------Field Data Information Log for Ground Water Sampling
• Page_1_of
Date (yrlmo/day) ___________ 98_/_04_/_2_1 ________ _ Casing Oiameter _____________________ inches
Field Personnel ________ R_._M_o.:..r~g.:..a_n_/_B_. -'D_iii-'a_rd'--------Casing Material ______________________ _
Slte Name __________ G_e..,ig~y_C_h_e_m_ica_i C_o_rpa..o_ra_t_io_n _____ _ Measuring Point Elevation _________________ 1/100 ft
Earth Tech Job Number ________ _,3'-'1,,8..,_19e..._ ________ _ Height of Riser (above land surface) 1/100 ft
Well ID # ______________ V.:..-4...:..:.7 _________ _ Land Surface Elevation 1/100 ft
D Upgradient D Downgradient D Sidegradient Screened Interval ____________________ 1/100 ft
Weather Conditions. ____________________ _ Dedicated Pump or Bailer □Yes □No □Type
AlrTemperature _____________________ •F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Well Depth (lWD) = _________________ 1/100 ft Locking Cap □Yes □No
Depth to Ground Water (DGW) = 1/100 ft Protective Post/Abutment □Yes □No
Length of Water Column (LWC) = TWO-DGW = 1/100 ft Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x. ___ = ____________ gal Well Yield □Low D Moderate □High
3 Casing Volumes= gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation. __________________ _
Method of Sample Collection'-------------------
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (fl)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY (NTU!"
0
13:20
3.72
-
184
17
0.18
Refill: Discharge:
rOMMENTS/OBSERVATIONS -"S'-AM=P-=L::cED::...;_A:..:.T...:1.;::32::;5:..._ _ _.;. ___________________ -~--------------t
-
Field Data/or GW
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TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: V-47 Lab ID: 098752-0011-SA Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC 0.20 ug/L beta-BHC 0.61 ug/L delta-BHC · 0.25 ug/L gamma-BHC (Lindane) 0.11 ug/L a 1 pha-Ch 1 ordane. ND ug/L Ramma-Chlordane ND ug/L eptachlor ND ug/L A 1 dri n ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin 0.077 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone 0.10 ug/L Methoxychlor ND ug/L Toxaphene 0.86 ug/L
Surrogate Recovery
Tetrachloro-m-xylene 82 % Decachlorobiphenyl 75 %
Note J : Result is detected below the reporting limit or is an estimated concentration.
ND c Not detected NA c Not applicable
IJ~\ • . ,euanaerra
Environmental
Services
Received: 22 APR 98 Analyzed: 22 MAY 98
Relorting imit
0.050
0.050
0.050
0.050
0.050
0.050
0.050
0.050 0.050
0.050
0.10 J 0.10
0.10
0.10
0.10
0.10 0.10 0.10 0.10 0.50 1.0 J
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
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I Volatile Organics
Method 8260
Client Name: Rust Environmental & Infrastructure V-47 LAB ID: 098752-0011-SA I Client ID:
Matrix: Authorized: AQUEOUS Sampled: 21 APR 98 22 APR 98 Prepared: NA I Dilution Factor: 1.0
I Parameter
Trichloroethene
I Surrogate
Toluene-dB I 4-Bromofl uorobenzene
l,2-Dichloroethane-d4
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Result Units
4.2 ug/L
Recovery
98 %
9B % 120 %
(/}uanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 29 APR 98
Rerorting imit Qualifier
5.0 J
Acceptable Range
85 -111
81 -117 75 -121
I Note J • Result is detected below the reporting limit or is an estimated concentration. NA= Not Applicable
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Reported By: Matt Culver Approved By: Karin Yee
The cover letter is an integral part of this report.
Rev 230787
-------------------GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For addltlonal forms
please wrl1e or call:
Type or Use a ball-point pen end press firmly.
Facility Name _________ G_ei"'gyc...C_h_em_i_ca_l_C_or.,_po_r_at_io_n _______ _
AddreSS-----------"-Do'---m'---i"-'no'-'D'-'-r'---ivc..• _________ _
___ _;_A:.::bt.:.:•..:.d•:.:•c:,••.:..N:.::C--'2:.:8"-'31:.::5 ____ County ___ .,.-"~~loo~•~·----
DIVISION OF WATER OUALITY -GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPDES-,-....,.=====::-===-=-= TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic T ank/Orain Field
Well ldenlilication Number CUA2 (V48) Well Depth ____ Ft.
Well Diameler ___ Sample (Screened) Interval ____ Ft. To Ft.
Depth to Water Level ___ 11. below measuring point (before sampling)
Measuring point is ____ ft. above land surface
Gallons _of water pumped/bailed before samplinn,,_ ________ _
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application of Slu,e
__ Other
Rotary Distributor
Field Analysis: pH ____ Specific Conductance ___ uMhOs Temp. ___ 0 c Odor ___ Appearance __ _
Date Sample Collected 7122198 Date Lab Sample Analyze,~--------
Laboratory Name Quanterra, We!iit Sacramento, CA Certification No. ___ 2_16_6 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIRED __ YES __ NO
coo ___________ mg/I Nitrite (NO2) as N _______ mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
Nitrate (NO3 ) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples) Al -Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba -Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG mg/I Cd -Cadmium mg/I
Chloride mg/I Chromium: Total mg/I
Arsenic mg/I Cu -Copper mg/I
Grease and Oils mg/I Fe -Iron mg/I
Hardness: Total mg/I Hg -Mercury mg/I
Phenol mg/I K -Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Mg -Magnesium mg/I
Mn -Manganese mg/I
Total Ammonia mg/I Na -Sodium mg/I
TKN as N mg/I
Ni -Nicke __________ mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Soecily Compounds)
tCL Ptsticidts -rrsults attachrd
Other (Specify Compounds and
Concentration units)
TCE -rt5ult5 attachtd
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above.
------- - - ---.. liiiil
EARTH©T EC H Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/07/22 Casing Diameter Inches
Field Personnel N. Hicks Casing Material
Site Name Geigy Chemical Corporation Measuring Point Elevation 11100 fl
Earth Tech Job Number 31819 Height of Riser (above land surface) 11100 fl
Well ID# CUA2 (V48) Land Surface Elevation 11100 fl
D Upgradient D Downgradient D Sidegradient Screened Interval 11100 fl
Weather Conditions Dedicated Pump or Bailer □Yes □No □Type
Air Temperature •F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Well Depth (TWO) = 1/100 fl Locking Cap □Yes □No
Depth to Ground Water (OGW) = 1/100 fl Protective Post/Abutment □Yes □No
Length of Water Column (LWC) = TWO • DGW = 1/100 fl Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x = gal Well Yield □Low D Moderate □High
3 Casing Volumes = gal = Staildard Evacuation Volume Comments/Observations
Method of Well Evacuation
Method of Sample Collection
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (fl)
Sp. Cond. (l'mhos/cm)
Water Temp. ("C)
TURBIDITY
Refill: Discharge:
j OMMENTS/OBSERVATIONS Sampled at 1420. I
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Client Name:
I Client ID:
LAB ID:
Rust Environmental
CUA2(V48) 300553-0001-SA
AQUEOUS Matrix:
1 Authorized: 23 JUL 98
Dilution Factor: 1.0
I Parameter
alpha-BHC
I beta-BHC
delta-BHC gamma-BHC (Lindane)
I
alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin
I Heptachlor epoxide
Endosulfan I Dieldrin
4,4' -ODE
I Endri n Endosulfan II 4,4'-DDD Endosulfan sulfate
I 4 ,4' -DDT
Endrin aldehyde Endrin ketone Methoxychlor I Toxaphene
1 Surrogate
Tetrachloro-m-xylene Decachlorobiphenyl
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Marcia Reed
(!l>uanterra
TCL Organochlorine Pesticides/PCBs
Method .BOBO
& Infrastructure
Sampled: 22 JUL 98
Prepared: 24 JUL 98
Result Units
ND
ND
ND ND ND
ND
ND
ND ND
ND
ND
ND ND
ND ND ND ND
ND ND ND ND
Recovery
90 %
68 %
ug/L
ug/L ug/L ug/L ug/L
ug/L ug/L ug/L ug/L ug/L
ug/L
ug/L
ug/L
ug/L ug/L
ug/L ug/L
ug/L
ug/L ug/L ug/L
Received: 23 JUL 98
Analyzed: 01 AUG 98
Reporting
Limit Qualifier
0.050
0.050
0.050 0.050 0.050
0.050
0.050
0.050
0.050
0.050
0.10
0.10
0.10
0.10 0.10 0.10 0.10
0.10 0.10 0.50 1.0
Acceptable Range
55 -115 35 -137
Approved By: Jon Edmondson I Reported By:
The cover letter is an integral part of this report.
Rev 230787
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Client Name:
Client ID: LAB ID:
Matrix:
Authorized:
Rust Environmental
CUA2(V48)
300553-0001-SA
AQUEOUS
23 JUL 98
Dilution Factor: 1.0
Volatile Organics
Method 8260
& Infrastructure
Sampled: 22 JUL 98 Prepared: NA
{e>uanterra
Received: 23 JUL 98
Analyzed: 31 JUL 98
I Parameter
Reporting
Result Units Limit Qualifier
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Trichloroethene
Surrogate
Toluene-dB
4-Bromofluorobenzene
1,2-Dichloroethane-d4
0.56 ug/L
Recovery
87 % 82 % 85 %
5.0 J
Acceptable Range
85 -111 81 -117 75 -121
Note J = Result is detected below the reporting ·1imit or is an estimated concentration. NA= Not Applicable
Reported By: Michael Lucchesi Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
-------------------
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name __________ G_ci""gyc.C_h_,_m_ic_al_C_o~•Pc.o_ra_ti_o_n ________ _
Address ____________ D_o_m_in_o_D_ri_vc __________ _
----'-"AC.Cbtc..•d~•c..••~•c.N.cC_2c.c8.c..3'-Cl5 ____ County ____ ~M~o~o•~·----
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPDES.,-....,,.===-----=--=--c== TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location __________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number Ltad Cu. A Well Depth ____ Ft.
Well Diameler ___ Sample (Screened) Interval,__ ___ Ft. To Ft.
Depth to Water Level ___ It. below measuring point (before sampling)
Measuring point is _____ lt. above land surface
Gallons of water pumped/bailed before samplin,n,,_ ________ _
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application ol Slu~e
_·_Other
Rotary Distributor
Field Analysis: pH ____ Specific Conductance · uMhos Temp. ___ 0 c Odor ___ Appearance __ _
Date Sample Collected 10127/98 Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. ___ 2_1_66 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD __ ~---------mg/I Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method fo; hlghly turbid samples)
Dissolved Solids: Total mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Al • Aluminum mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd • Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K • Potassium mg/I
Mg • Magnesium mg/I
Mn -Manganese mg/I
Na -Sodium mg/I
Ni -Nicke~---------mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Soecify Compounds)
tCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
TCE • results attached
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloldal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8196
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
- -- - -- -- - ---Field Data Information Log for Ground Water Sampling
Pago_1_of
Dato (yr/mo/day) 98/10127 Casing Diameter Inches
Field Personnel D. Shoopman Casing Material
Sito Name Geigy Chemical Corporation Measuring Point Elevation 11100 ft
Earth Tech Job Number 31819 Height of Riser (above land surface) 11100 ft
Woll ID# Lead Cu. A Land Surface Elevation 1/100 ft
D Upgradient D Downgradient D Sidegradient Screened Interval 1/100 ft
Weather Conditions Dedicated Pump or Baller □Yes □No □Type
Air Temperature "F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Woll Depth (TWO) = 1/100 ft Locking Cap □Yes □No
Depth to Ground Water (DGW) = 11100 ft Protective PosUAbutment □Yes □No
Length of Water Column (LWC) a TWO -DGW = 1/100 ft Woll Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x = gal Woll Yield □Low D Moderate □High
3 Casing Volumes = gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation
Method of Sample Collection
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. ("C)
TURBIDITY
Refill: Discharge:
OMMENTS/OBSERVATIONS Sampled al 1005. I
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Field Data for G W
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{!puanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name:
Client ID: Rust Environmental & Infrastructure lead Cu. A
LAB ID: 302382-0001-SA
Matrix:
Authorized:
AQUEOUS Sampled: 27 OCT 98
28 OCT 98 Prepared: 03 NOV 98
Dilution Factor: 1.0
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane) alpha-Chlordane
gamma-Chlordane
Heptachlor
Aldrin
Heptachlor epoxide
Endosulfan I
Dieldrin 4,4'-DDE
Endrin
Endosulfan II
4,4' -ODD
Endosulfan sulfate
4,4' -DDT
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
ND= Not Detected
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/l
ND ug/L
ND ug/L
ND ug/l ND ug/L ND ug/L ND ug/l
ND ug/l
ND ug/L
ND ug/L
ND ug/l
ND ug/l
ND ug/l
ND ug/l
ND ug/l
ND ug/L
ND ug/L
ND ug/l
Recovery
74 %
83 %
Received: 28 OCT 98
Analyzed: 13 NOV 98
Reporting
Limit MDL Qualifier
0.050 0.0080 0.050 0.0040
0.050 0.0060
0.050 0.010
0.050 0.0070
0.050 0.0080
0.050 0.0070
0.050 0.0060
0.050 0.0080 0.050 0.010
0.10 0.020 0. 10 0.015
0. 10 0.020
0. 10 0.020
0. 10 0.0050
0. 10 0.033
0. 10 0.020
0. 10 0.029
0. 10 0.024 a.so 0.040
1.0 1.0
Acceptable Range
55 -115
35 -137
Reported By: Lisa Stafford Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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IJ)\ ~uanterra
(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name: Client ID:
Lab ID: Matrix:
Authorized:
Rust Environmental
Lead Cu. A
302382-0001-SA AQUEOUS
28 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-0ichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
& Infrastructure
Sampled: 27 OCT 98
Prepared: 09 NOV 98
Result Units
0.23. ug/L
Recovery
98 %
100 % 97 %
Note J : Result is detected below the reporting limit or
is an estimated concentration.
ND= Not detected
NA= Not applicable
Received: 28 OCT 98
Analyzed: 09 NOV 98
Reporting
Limit
1.0 J
Reported By: SWILLMS Approved By: DBAREWALD
The cover letter is an integral part of this report.
Rev 230787
-----·----·--llllla-SUBMIT FORM ON YELLOW PAPER ONLY ---·---00
Mail Original
·· · · ' to· . -.
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: _____ G_e~ig~y-=C_h_em_i_ca_l_C_o~rp_o_ra ... tio'-n_C_E_R_C __ LA'--S __ it ... e _______ _ PERMIT#: EXPIRATION DATE: 30-Nov-99
WQ 0009949 UIC Permit Name (if different): --:G:c-e'-"ig",y_C'-,h;::-ec-m __ ic ... a ... 1 Cc..co ... rpc.;o ... ra:;..;tI;.:;· o ... n ..::.S ... ite'------------Non-Discharge
NPDES --------
Facility Address: ___ _:D,.co:.cm.;;;in:"o ... D:;..;r.:..civ..::.e:-:::-----:c:-:-:-c---=--------,-:----
Aberdeen NC 28315 County Moore
Contact Person: Garland Hilliard ------''-="'----'-'--"-----Telephone#: [phone]
We II Location/ Site Name:
TYPE OF~PE=-R_M_I __ TT=ED::-CO_P __ E-RA_T_I_O_N_B_E_ING MONITORED
__ Lagoon
Spray Field
X Remediation: Infiltration Gallery
Remediation: No. of Wells to be Sampled: 7 -----------Rotary Distributor ---.----,------___ Land Application of Sludge (from Permit)
Well Identification Number (from Permit): V-49 For Groundwater Treatment Systems
Well Depth: ______ ft. Well Diameter: ___ in. Check One•
Screened Interval:....,. ___ ft. to,----ft. □ Influent (98)
Depth to Water Level: ___ ft. below measuring point
Measuring Point is ___ ft. above land surface. D Effluent 99
,---Other: 1---
NOTE: Values should reflect dissolved and
colloidal concentrations.
Gallons of water pumped/bailed before sampling: ------Date sampled collected: 14-Jan-99 Date sample analyzed: ___ _
Field Analysis: pH ___ , Specific Conductance _____ ~Mhos Laboratory Name: Quanterra (W. Sacramento)
Temp. •c, . Odor Appearance Certification No. 2166 -------
PARAMETERS (Samples for metals were collected unfiltered __ YES __ NO and field acidified YES NO)
COD -----------mg/I Nitrite (NO2) as N _______ mg/I Ni -Nickel ________ ___,mg/I
Coliform: MF Fecal _____ /100ml Nitrate (NO3) as N mg/I Pb-Lead _________ mg/I
Coliform: MF Total ______ /100ml Phosphorous: Total as P mg/I Zn -Zinc __________ mg/1
(Note: UseMPNmethodforhighlyturbidsamples) Orthophosphate g/1 Ammonia Nitrogen _______ mg/I
Dissolved Solids: Total _____ mg/I Al -Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) _____ units Ba -Barium mg/I
TOC ___________ mg/I Ca -Calcium mg/I
Chloride __________ mg/I Cd -Cadmium mg/I
Arsenic ___________ mg/I Chromium: Total mg/I
Grease and Oils ________ mg/I Cu -Copper mg/I
Phenol ___________ mg/I Fe -Iron mg/I
Sulfate ___________ mg/I . Hg -Mercury mg/I
Specific Conductance _____ µMhos K -Potassium mg/I
Total Ammonia ________ mg/I Mg -Magnesium mg/I
TKN as N __________ mg/I Mn -Manganese g/I
ORGANICS: (GC,GC/MS,HPLC)
(Specify lest and method #. Attach lab report.)
Report Attached? Yes_X_(1) No_ (0)
TCL Pesticides : method#= 8081A
-----------'-'-'C.......C---..;.T ..::.C ECC-_____ : method# =.:.8:cc26:.::0.=.B __ _
: method#=
.I certify that to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced
· il~i!!9~a·pprov.ed.methc,d!r~!~·¥.1\is.by:a,North ... Carolln{DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information,
including the possibility of fines·and imprisonment for knowing violations.
Permittee (or Authorized Agent) Name and Title -Please print or type
GW-59 Rev. 4/98
Signature of Permittee (or Authorized Agent) (Date)
- -- ---- - -
Geigy Chemical Corporation
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Date (dd-mmm-yy) 14-Jan-99 I Casing Diameter (inches) I
Field Personnel #1 R. Morgan I #21 N. Hicks I #31 Casing Material I
Project Name Geigy Chemical Corporation CERCLA Site I Measuring Point Elevation (feet, NGVD)
Site Name Geigy Site
Job Number 32240
Well Number V-49
Gradient Type I
Weather Conditions
Air Temperature (°FJ
Total Well Depth (TWD) from Top of Well Casing (feet)
Depth to Groundwater (DGW) from Top of Well Casing (feet)
Length of Water Column (LWC) = TWD • DGW (feet)
1 Casing Volume (gal)= LWC x I 0.16
3 Casing Volumes (gal)= 1 Casing Volume x 3
Method of Well Evacuation I
Method of Sample Collection I
Total Volume of Water Removed (gal)
Conment/Observations sampled at 1615.
= below land surface
= gallons per minute
I
bis
gpm
NGVD = National Geodetic Vertical Dattrrn
NTU
TOC
I Height of Riser Above Land Surface (feet)
Land Surface Elevation (feet, NGVD)
Screened Interval Depth (feel, bis)
D Dedicated Pump or Baller: Type I
D Protective Casing
D Locking Cap
0 Protective Post/Abutment
D Well Integrity Satisfactory
=
Well Yield I =
= Co1TD11ents/Observatlons
I
= I I
= Nephelometric Turbidity Untt
= Top of well casing
--Page 1 of 1
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2/251!19 03:47 PM
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Client Name:
Client ID: LAB ID:
Matrix:
Authorized:
Earth Tech
V-49
303669-0007-SA
AQUEOUS
15 JAN 99
Dilution Factor: 1.0
Parameter
Trichloroethene
Surrogate
l,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
NA= Not Applicable
Reported By: Michael Lucchesi
Volatile Organics
Method 82608
Sampled: 14 JAN 99
Prepared: NA
Result Units
l. 3 ug/L
Recovery
92 %
102 %
100 %
(/puanterra
Received: 15 JAN 99
Analyzed: 28 JAN 99
Reporting
Limit Qualifier
1.0
Acceptable Range
75 -121
85 111
81 117
Approved By: .Karin Yee
The cover letter is a,1 integral part of this report.
Rev 230787
I
I Client Name: Earth Tech
Client ID: V-49
I LAB ID: 303669-0007-SA
Matrix: AQUEOUS
Authorized: 15 JAN 99
I Dilution Factor: 1.0
I
Parameter
Aldrin alpha-BHC
I beta-BHC
delta-BHC
gamma-BHC (Lindane)
alpha-Chlordane
I gamma-Chlordane
Dieldrin
4, 4' -DDD
I 4,4'-DDE
4,4'-DDT
Endrin
Endrin-aldehyde
I Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
I Heptachlor epoxide Methoxychlor
Toxaphene
I Surrogate
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Tetrachloro-m-xylene
Decachlorobiphenyl
0rganochlorine Pesticides Method 8081A
Sampled: 14 JAN 99 Prepared: 20 JAN 99
Result Units
ND ug/L 0.031 ug/L 0. 11 ug/L 0.034 ug/L 0.013 ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
Recovery
74 %
93 %
IJ)\ ,euanterra
Received: 15 JAN 99
Analyzed: 01 FEB 99
Reporting
Limit Qualifier
0.050 0.050 J
0.050 0.050 J
0.050 J 0.050 0.050
0 .10
0 .10
0.10
0.10
0. 10
0.10
0.050
0.10
0. 10
0.050
0.050
0.50
2.0
Acceptable Range
70 -130 70 -130
I Note J = Result is detected below the reporting limit or is an estimated concentration. ND= Not Detected
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Reported By: Marcia Reed Approved By: Emily Uebelhoer
The cover l~tter is an integral part of this report.
Rev 230787
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TREATMENT SYSTEM
EFFLUENT FROM LEAD CARBON CANISTER
TRAINB
-------------·------GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For llddlllonal forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ ...:Gc:.ti:e:gy'--C.::.h::.:•c.:m::.:i'="c,I C:.:•c..'Pc.:•c..'":.:"=··=-·---------
Address ____________ ...:D:.::•.:::m::.:i•:.::•..:D::._ri:.:.vc=-----------
_____ A~b•ccr_d•-•~••_N_C_2_8_3~1S ____ County, ____ .::_M:,,oo:,.:rc,_c ___ _
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949 NPOES ___________ _
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location _________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number V-S0 Well Depth ____ Ft.
Well Diameter ___ Sample (Screened) Interval, ____ Ft. To Ft.
Depth to Waler Level ___ ft. below measuring point (before sampling)
Measuring point is. _____ ft. above land surface
Gallons of water pumped/bailed before samplinn!l----------
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application of Slu'ie
__ Other
Rotary Distributor
Fleld Analysis: pH 3.8 Specific Conductance 180 uMhos Temp. 11 °c Odor ___ Appearance, __ _
Dale Sample Collected 4121198 Dale Lab Sample Analyze,u... _______ _
Laboratory Name Quanttrra, Wrst Sarramenlo, CA Certification No. ___ 2_1_66 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD---,-,-,-,,---------mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples)
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Al • Aluminum mg/I
Ba • Barium mg/I
Ca -Calcium mg/I
Cd • Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Mg • Magnesium mg/I
Mn • Manganese mg/I
Na • Sodium mg/I
Ni. Nicke-~---------mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
TCE -results attachtd
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. NQ!e_;_ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent")
GW-59 REV. 8/96
Date • See back for Instructions.
" Submit blue and yellow copies only to address above.
------- - ---- ------EARTH©T EC H Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) __________ ;:.98""/-"04-'-/-=2c.c1 ________ _ Casing Diameter _____________________ Inches
Field Personnel _______ __:R..:;·c.:M.:.:o::;r"'g"'a'-'n.:../-=B.:... -=Dc::ili:::a::.;rd:._ _____ _ Casing Material ______________________ _
Site Name _________ ..:Ge=ige;Y..:C:.:h:=e;.;.m:::icac::;..I C:.;o:.:rpcco:.:ra:::l:::io:::n _____ _ Measuring Point Elevation _________________ 1/100 ft
Earth Tech Job Number ________ ..,3'-'1-"8.,.19,,_ ________ _ Height of Riser (above land surface) 1/100 ft
Well ID # _________________ -'V-'-5;;..;0;......_ _______ _
D Upgradient D Downgradient D Sidegradient
Land Surface Elevation 1/100 ft
Screened Interval 1/100 ft
Weather Conditions. ____________________ _ Dedicated Pump or Bailer □Yes □No □Type
Air Temperature _____________________ °F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Well Depth (TWO)=-----------------1/100 ft Locking Cap □Yes □No
Depth to Ground Water (DGW) =· _______________ 1/100 ft Protective Post/Abutment □Yes □No
Length of Water Column (LWC) = TWO -DGW = _________ 1/100 ft Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCVJ = LWC x ___ = ____________ gal WellYleld □Low D Moderate □High
3 Casing Volumes = _________ gal c Standard Evacuation Volume Comments/Observations
Method of Well Evacuation, __________________ _
Method of Sample Collection, _________________ _
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (fl)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY (NTU)•
0
13:35
3.80
-
180
17
0.06
Refill: Discharge:
fOMMENTS/OBSERVATIONS ~S::::A:!!M::._P~L:::.ED:::..:.:A:..:.T...:1.::34~0::_ ____________________________________ -i
-
Field Dara/or GW
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TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infrastructure Client ID: V-50 Lab ID: 098752-0012-SA Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC 0.094 ug/L beta-BHC 0.30 ug/L delta-BHC 0.10 ug/L gamma-BHC (Lindane) 0.041 ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosulfan I ND ug/L Dieldrin 0.031 ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4' -DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone 0.052 ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene 84 % Decachlorobiphenyl Bl %
Note J : Result is detected below the reporting limit or is an estimated concentration.
ND= Not detected
NA= Not applicable
{!puanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 14 MAY 98
Reporting
Limit
0.050 0.050
0.050 0.050 J 0.050 0.050 0.050 0.050
0.050 0.050
0.10 J 0.10 0.10
0.10
0.10
0 .10 0.10
0.10
0.10 J 0.50
1.0
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral part of this report. Rev 230787
I
Volatile Organics
Method 8260 I Client Name:
Client ID: Rust Environmental & Infrastructure V-50 098752-0012-SA I LAB ID:
Matrix:
Authorized: AQUEOUS Sampled: 21 APR 98 22 APR 98 Prepared: NA I Dilution Factor: 1.0
1 Parameter
Trichloroethene
I Surrogate
Toluene-dB
I 4-Bromofluorobenzene
1,2-Dichloroethane-d4
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Result
2.9
Recovery
95 % 97 %
115 %
Units
ug/L
I})\ ,:euanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 29 APR 98
Reporting
Limit Qualifier
5.0 J
Acceptable Range
85 -111 81 -117
75 -121
Note J ~ Result is detected below the reporting limit or is an estimated concentration. I NA c Not Applicable
m
B
B
Reported By: Matt Culver Approved By: Karin Yee
The cover letter is an integral part of this report. Rev 230787
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name ________ __:G_<i_,,gy'-C"::hcc•=mccica_l:c-C-:-or.,_p.:...o•=•'='"="---------
Address ________ -,-__ _;:_D;;.:•m::.:i::.:••;.;D:..;r.:...iv.;.•-----,,-----
____ A_b_er_d_ee_n,_N_C_2_8_31_5 ____ Coun~------'~~lo~•~••~---
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPDES---,,,--,-------,---c-,=
TYPE OF Pl$P0$AL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Field
Well ldenlification Number CUB2 (V51) Well Depth ____ Ft.
Well Diameter ___ Sample (Screened) lnlerval ____ Ft. To Ft.
Depth to Water Level ___ ft. below measuring point (before sampling)
Measuring point ls ____ ft. above land surface
Gallons of water pumped/bailed before samplin,n,,_ ________ _
Spray Field __ SubSurface Low-Pressure
Piping (LPP)
Land Application of Slu~e __ Other
__ . Rotary Oistribu1or
Field Analysis: pH ____ Specific Conductance ___ uMhos Temp. ___ 0 c Odor--~ Appearance __ _
Date Sample Collected 7122/98 Date Lab Sample Analyze"-----------
Laboratory Name Quanltrra, West Sacramento, CA Certification No. ___ 2_16_6 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ___________ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3 ) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples)
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Al -Aluminum mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Mg -Magnesium mg/I
Mn -Manganese mg/I
Na -Sodium mg/I
Ni -Nicke.~---------mg/I
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Soecify Compounds)
TCL Prsticidrs • rrsults attachrd
Other (Specify Compounds and
Concenlration units)
TCE • rrsults attachrd
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
liiil liiil -- --- - - --- -- ---E A R r H @D r E c H Field Data Information Log for Ground Water Sampling
Page_1_of 1
Date (yr/mo/day) 98/07/22 Casing Diameter Inches
Field Personnel N. Hicks Casing Material
Site Name Geigy Chemical Corporation Measuring Point Elevation 1/100 ft
Earth Tech Job Number 31819 Height of Riser (above land surface) 1/100 ft
Well ID# CUB2 (V51) Land Surface Elevation 1/100 ft D Upgradient D Downgradient D Sidegradient Screened Interval 1/100 ft
Weather Conditions Dedicated Pump or Bailer □Yes □No □Type
Air Temperature "F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Well Depth (TWO) = 1/10011 Locking Cap □Yes □No
Depth to Ground Water (DGW) = 1/100 ft Protective Post/Abutment □Yes □No
Length of Water Column (LWC) =TWO. DGW = 1/10011 Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x = gal WellYleld □Low D Moderate □High
3 casing Volumes = gal = Standard Evacuation Volume CommentslObservations
Method of Well Evacuation
Method of Sample Collection
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY
Refill: Discharge:
FOMMENTS/OBSERVATIONS Sampled at 1430. I
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Client ID:
LAB ID:
Rust Environmental CUB2(V51)
300553-0002-SA
AQUEOUS Matrix:
1 Authorized: 23 JUL 98
Dilution Factor: 1.0
I Parameter
alpha-BHC
I beta-BHC
delta-BHC
gamma-BHC {Lindane)
I alpha-Chlordane gamma-Chlordane Heptachlor Aldrin
I Heptachlor epoxide Endosulfan I
Dieldrin 4,4'-DDE
I Endrin Endosulfan II 4,4'-DDD Endosulfan sulfate
I 4,4' -DDT
Endrin aldehyde Endrin ketone
I Methoxychlor Toxaphene
Surrogate I Tetrachloro-m-xylene
Decachlorobiphenyl
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Marcia Reed
(12>uanterra
TCL Organochlorine Pesticides/PCBs
Method BOBO
& Infrastructure
Sampled: 22 JUL 98
Prepared: 24 JUL 98
Result Units
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L ND ug/L
ND ug/L ND ug/L
Recovery
89 %
71 %
Received: 23 JUL 98
Analyzed: 01 AUG 98
Reporting
Limit Qualifier
0.050 0.050
0.050 0.050 0.050
0.050 0.050
0.050 0.050
0.050 0.10 0.10 0.10 0 .10
0 .10 0. 10
0.10
0.10
0. 10
0.50
1.0
Acceptable Range
55 -115 35 -137
Approved By: Jon Edmondson g Reported By:
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Client ID:
LAB ID: Matrix:
Authorized:
Rust Environmental
CUB2(V51) 300553-0002-SA AQUEOUS
23 JUL 98
Dilution Factor: 1.0
Parameter
Trichloroethene
Surrogate
Toluene-dB 4-Bromofluorobenzene
l,2-Dichloroethane-d4
Volatile Organics
Method 8260
& Infrastructure
Sampled: 22 JUL 98
Prepared: NA
Result Units
0.38 ug/L
Recovery
95 % 86 %
93 %
(/!>uanterra
Received: 23 JUL 98
Analyzed: 31 JUL 98
Reporting
Limit Qualifier
5.0 J
Acceptable Range
85 -111 81 117
75 -121
Note J = Result is detected below the reporting limit or is an estimated concentration. NA= Not Applicable
Reported By: Michael Lucchesi Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER OUALITY • GROUNDWATER SECTION
P.O. BOX 29578
COMPLIANCE REPORT FORM
For eddltlonal formt
please write ~r call:
RALEIGH, NC 27626-0578
[phone]
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949 Facility Name _________ G_,i.c;gy:..C_h_,_m_ka_l_C_o,.,_po_,_at_io_n ________ _
AddreSS----------'---·--Do_m_i_no_D_,_;,.c..•----------
-----'-A'-'-b-'--e,-'--d'-'-""""':..N..cC:..2cc8.c.31~5----County ___ --'-M~•~·~"----
NPDES.,....--,-----,-,,-----,---,,-,~
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _
Well ldentilication Number Lead Cu. B · Well Depth ____ ft.
Well Diameter ___ Sample (Screened) lnterva• Ft. To Ft.
Depth to Water Level ___ ft. below measuring point (before sampling)
Measuring point is ____ ft. above land surface
Gallons of water pumped/bailed before samplin,n!I----------
Lagoon __ Septic Tank/Drain Field
Spray Field __ Subsurface Low-Pressure
Piping (LPP)
Land Application ol Slu~e
__ Other
Rotary Distributor
Fleld Analysis: pH ____ Specilic Conductance ___ uMhos Temp. ___ 0 c Odor ___ Appearance __ _
Date Sample Collected 10127/98 Date Lab Sample Analyze~--------
Laboratory Name Quanterra, West Sacramento, CA Certification No. --~2~166~--
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD_...,..,.=--,--------mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for highly turbid samples) Al • Aluminum mg/I
Dissolved Solids: Total ______ mg/I Ba • Barium mg/I
pH (when analyzed) units Ca -Calcium mg/I
TOG mg/I
Chloride mg/I
Arsenic mg/I
Cd • Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
Phenol mg/I K • Potassium mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
Mg · Magnesium mg/I
Mn • Manganese mg/I
Na · Sodium mg/I
TKN as N mg/I
Ni• Nicke~---------mg/I
Pb · Lead mg/I
Zn • Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
'fCL Pestkides -results attached g/1 _____________ u
_____________ ug/1
_____________ ug/1
Other (Specify Compounds and
Concentration units)
TCE -result5 attached
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for lnstructfons.
•• Submit blue and yellow copies only to address above.
liiii
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A R E -C H Field Data Information Log for Ground Water Sampling
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Date (yr/mo/day) 98/10/27 Casing Diameter Inches
Field Personnel 0. Shoopman Casing Material
Site Name Geigy Chemical Corporation Measuring Point Elevation 1/100 ft
Earth Tech Job Number 31819 Height of Riser (above land surface) 1/100 ft
WelllD# Lead Cu. B Land Surface Elevation 1/100 ft
D Upgradient D Downgradient D Sidegradient Screened Interval 1/100 ft
Weather Conditions Dedicated Pump or Bailer □Yes □No □Type
Air Temperature "F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Well Depth (TWO) = 1/10011 Locking Cap □Yes □No
Depth to Ground Water (DGW) = 1/100 ft Protective Post/Abutment □Yes □No
Length of Water Column (LWC) = TWD • DGW = 1/100 ft Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x = gal Well Yield □Low D Moderate □High
3 casing Volumes = gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation
Method of Sample Collection
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (fl.)
Sp. Cond. (µmhos/cm)
Water Temp. ("C)
TURBIDITY
Refill: Discharge:
FOMMENTS/OBSERVATIONS Sampled at 1010. I
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Field Data/or GW
Client Name:
Client ID: LAB ID: Matrix:
Authorized:
Rust Environmental
lead Cu. B
302382-0002-SA
AQUEOUS
28 OCT 98
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Parameter
alpha-BHC ,
beta-BHC
delta-BHC I gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
I Heptach l or
Aldrin
Heptachlor epoxide Endosulfan I
I Dieldrin
4,4'-DDE
Endrin
Endosulfan II
I 4,4' -DDD
Endosulfan sulfate 4,4'-DDT
I Endrin aldehyde Endrin ketone
Methoxychlor
Toxaphene
I Surrogate
I Tetrachloro-m-xylene
Decachlorobiphenyl
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Reported By: Lisa Stafford
~~\ ,euanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
& Infrastructure
Sampled: 27 OCT 98
Prepared: 03 NOV 98
Result Units
ND ug/l ND ug/L
ND ug/l ND ug/l ND ug/L ND ug/l ND ug/L ND ug/L ND ug/L
ND ug/L ND ug/l ND ug/L .
ND ug/L ND ug/l
ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L
ND ug/L ND ug/l
Recovery
76 %
83 %
Received: 28 OCT 98
Analyzed: 13 NOV 98
Reporting
limit MDL Qualifier
0.050 0.0080
0.050 0.0040
0.050 0.0060 0.050 0.010 0.050 0.0070 0.050 0.0080 0.050 0.0070 0.050 0.0060
0.050 0.0080
0.050 0.010
0. 10 0.020
0. 10 0.015
0. 10 0.020 0. 10 0.020
0. 10 0.0050 0. ID 0.033 0. 10 0.020 0. 10 0.029 0. 10 0.024 0.50 0.040 1.0 1.0
Acceptable Range
55 -llS
35 -137
Approved By: Mike Orbanosky I The cover letter is an integral part of this report.
Rev 230787 I
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(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental
Lead Cu. B
302382-0002-SA ·
AQUEOUS
28 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-Dichloroethane-d4
Toluene-dB 4-Bromofluorobenzene
ND= Not detected
NA= Not applicable
Reported By: SWILLMS
& Infrastructure
Sampled: 27 OCT 98 Received: 28 OCT 98
Prepared: 09 NOV 98 Analyzed: 09 NOV 98
Reporting
Result Units Limit
ND ug/L 1.0
Recovery
98 % 102 %
98 %
Approved By: DBAREWALD
The cover l~tter is an integral part of this report.
Rev 230787
FACILITY INFORMATION Please Print Clearly or Type
Mail Original . , .. .: to: - - -
Facility Name: ------"G'-"e"'igy,_C_he'-m'-i'-ca'--I-'C'-o'-"rp'-or""a-'--tio"-n'-C'-'E"'-R'-'Cc..cLA"-'-"S"'it-'-e _______ ~ PERMIT#: EXPIRATION DATE: 30-Nov-99
WO 0009949 UIC Perm it Name (if different): --:Gc--e°"igy~C"ch::'e'-m"'ic"'a'--I C::..:o""rp"'o"'ra::..:ti"'o"-n ..::cS:..;;ite:.._ _________ _ Non~Discharge
NPDES --------
Facility Address: ----,D.,..o_m_in_o_D_ri_ve-c:-::----:-:c:-=----------,------
Aberdeen NC 28315 County Moore
Contact Person: Garland Hilliard ___ __:c..c:..;;=.;.;_cc.c..c.=..c_---Telephone#: [phone]
Well Location/ Site Name:
-----------,----TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ---Spray Field
X Remediation: Infiltration Gallery
Remediation: No. of Wells to be Sampled: 7 ------------Rotary Distributor ---,----,-------___ Land Application of Sludge (from Permit) --
Well Identification Number (from Permit): V-52 For Groundwater Treatment Systems
Well Depth: ______ ft. Well Diameter: ___ In. Check One:
Screened Interval: ____ ft. to ___ ft. □ Influent (98)
Depth to Waler Level: ___ ft. below measuring polnl
Measuring Point Is ___ ft. above land surface. D Effluent 99
Other: --
NOTE: Values should reflect dissolved and
cqlloidal concentrations.
Gallons of water pumped/bailed before sampling: _____ _
Field Analysis: pH ___ , Specific Conductance _____ µMhos
Temp. •c, Odor Appearance
Date sampled collected: 14-Jan-99 Date sample analyzed: ___ _
Laboratory Name: Quanterra (W. Sacramento)
Certification No. 2166 -'-'------
PARAMETERS (Samples for metals were collected unfiltered __ YES __ NO and field acidified YES __ NO)
COD -----------mg/I Nitrite (N02) as N _______ mg/1 Ni -Nickel -----------'.mg/I
Coliform: MF Fecal _____ /1OOml Nitrate (N03) as N mg/I Pb-Lead _________ mg/I
Coliform: MF Total ______ /1OOml Phosphorous: Total as P mg/I Zn -Zinc...,..,.,--________ mg/I
(Note: use MPN method for highly turbid samptes) Orthophosphate mg/I Ammonia Nitrogen _______ mg/I
Dissolved Solids: Total _____ mg/I Al -Aluminum mg/I Other (Specify Compounds and Concentration Units)
pH (when analyzed) · ______ units Ba -Barium mg/I
TOG ___________ mg/I Ca -Calcium g/I
Chloride __________ mg/I Cd -Cadmium g/I
Arsenic ___________ mg/I Chromium: Total mg/I
Grease and Oils ________ mg/1 Cu -Copper mg/I
Phenol ___________ mg/I Fe -Iron mg/I
Sulfate ___________ mg/I Hg -Mercury mg/I
Specific Conductance _____ µMhos K-Potassium mg/I
Total Ammonia ________ mg/I Mg -Magnesium mg/I
TKN as N __________ mg/I Mn -Manganese g/I
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes_X_(1) No_ (0)
Permittee (or Authorized Agent) Name and Title -Please print or type
GW-59 Rev. 4/98
Signature of Permittee (or Authorized Agent) (Dale)
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Geigy Chemical Corporation
FIELD DATA INFORMATION LOG FOR GROUNDWATER SAMPLING
Dale (dd-mmrn-yyJ 14-Jan•99 I Casing Diameter (inches) I
Field Personnel #1 R. Morgan 1 #21 N. Hicks 1 #31 Casing Material (
Project Name Geigy Chemical Corporation CERCLA Site I Measuring Point Elevation (feel, NGVDJ
Site Name Geigy Site I Height of Riser Above Land Surface (feel)
Land Surface Elevation (feel, NGVDJ Job Number 32240
Well Number ( V-52 I
Screened Interval Depth (feel, bis)
Gradient Type D Dedicated Puinp or Baller: Type I Weather Conditions D Protective Casing
Air Temperature (°F) D Locking Cap
Total Well Depth (TWDJ from Top of Well Casing (feet) D Protective PosVAbulmenl
Depth lo Groundwater (DGW) from Top of Well Casing (feel) D Well Integrity Satisfactory
Length of Waler Column (LWCJ = TWO • DGW (feel) •
1 Casing Volume (gal)= LWC x I 0.16 I Well Yield I =
3 Casing Volumes (gal)= 1 Casing Volume x 3 = Conwnents/Observations
Method of Wen Evacuation I
Method of Sample Collection I
T olal Volume of Water Removed (gal) • I I
CommenUObservations Sampled at 1605.
bis
gpm
NGVD
= below land surface
= gallons per minute
a National Geodetic Vertical Datum
NTU
TOC
= Nephelometric Turbidity Unit
= Top of well casing
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Client ID:
I LAB ID:
Matrix:
Authorized:
Earth Tech V-52
303669-0005-SA AQUEOUS 15 JAN 99
I Dilution Factor: 1.0
I Parameter
Aldrin
alpha-BHC
I beta-BHC
delta-BHC
gamma-BHC (Lindane) alpha-Chlordane
I gamma-Chlordane Dieldrin
4,4'-DDD
4,4'-DDE
I 4,4' -DDT
Endrin
Endrin aldehyde
Endosulfan I I Endosulfan·rr
Endosulfan sulfate Heptachlor
I Heptachlor epoxide
Methoxychlor
Toxaphene
I Surrogate
Tetrachloro-m-xylene I Decachlorobiphenyl
m ND = Not Detected
Reported By: Marcia Reed
0rganochlorine Pesticides
Method 8081A
Sampled: 14 JAN 99
Prepared: 20 JAN 99
Result Units
ND ug/L ND ug/L
ND ug/L
ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L ND ug/L
ND ug/L ND ug/L ND ug/L
Recovery
80 %
88 %
~~\ ~uanterra
Received: 15 JAN 99
Analyzed: 01 FEB 99
Reporting
Limit Qualifier
0.050 0.050 0.050
0.050
0.050
0.050
0.050
0 .10
0.10
0.10
0. 10
0. 10
0.10
0.050 o. 10
0.10 0.050
0.050
0.50
2.0
Acceptable Range
70 -130
70 -130
Approved By: Emily Uebelhoer
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Client Name:
Client ID: LAB ID:
Matrix:
Authorized:
Earth Tech V-52
303669-0005-SA
AQUEOUS
15 JAN 99
Dilution Factor: 1.0
Parameter
Trichloroethene
Surrogate
l,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
Reported By:
NA= Not Applicable
1 ND= Not Detected
Michael Lucchesi
Volatile Organics
Method 8260B
Sampled: 14 JAN 99 Prepared: NA
Result Units
ND ug/L
Recovery
86 %
98 %
96 %
~uanterra
Received: 15 JAN 99 Analyzed: 28 JAN 99
Reporting
Limit Qualifier
1.0
Acceptable Range
75 121
85 111
81 -117
Approved By: Karin Yee
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TREATMENT SYSTEM FINAL EFFLUENT
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For eddltlon■t forms
please write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ G_•i"'gyc..C_h_•m_i_ca_l_C_or.,_po_r_al_io_n _______ _
AddreSS---------·---"-Do_m_i..c••c..D..c.rc..iv-'-•----------
-~--'-A'-=b.;;:cr.c.d•c..c•cc••.c..N..cCc..2c.c8"-'31"-5----County ___ ~M~oo~•~•----
DIVISION OF WATER QUALITY· GROUNOWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPDES.,..,......,..===--=--:-==c=. JYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Field
Well ldentilication Number V-54 Well Depth ____ Ft.
Well Diameter ___ Sample (Screened) Interval ____ Ft. To Ft.
Depth 10 Water Level ___ ft. below measuring point (before sampling)
Measuring point is ____ ft. above land surface
Gallons of water pumped/bailed before sampling, ________ _
Spray Field __ SubSurface low-Pressure
Piping (LPP)
Land Application of Sluc~e __ Other
Rotary Distributor
Field Analysis: pH J.47 Specific Conductance 214 uMhos Temp. 17 °c Odor ___ Appearance __ _
Date Sample Collected 4/21/98 Date Lab Sample Analyze,~--------
Laboratory Name Quantrrra. Wrsl Sacramtnto. CA Certification No. ___ 2_166 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIRED _. _YES __ NO
COD ___________ mg/1
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
(Note: Use MPN method ror hlghly turbid samples)
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
TOG mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
Al -Aluminum · mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/I
Cu -Copper mg/I
Fe -Iron mg/I
Hg -Mercury mg/I
K -Potassium mg/I
Mg -Magnesium mg/I
Mn • Manganese mg/I
Na -Sodium mg/I
Ni -Nicke __________ mg/1
Pb -Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Specify Compounds) l'CL Pesticides -results attached
Other (Specify Compounds and
Concenfration units)
TCE -results attached
ug/1
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for Instructions.
•• Submit blue and yellow copies only to address above.
r=:I liiiiil liiiiil iiiiil --- - ---.. - - --l!!!!!!I m=:i
EARTH(DTECH Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/04/21 Casing Diameter Inches
Field Personnel R. Mor9an I B. Dillard Casing Material
Site Name Geigy Chemical Corporation Measuring Point Elevation 1/100 It
Earth Tech Job Number 31819 Height of Riser (above land surface) 1/100 It
Well ID# V-54 land Surface Elevation 1/100 It
D Upgradient D Downgradient D Sidegradient Screened Interval 1/100 It
Weather Conditions Dedicated Pump or Baller □Yes □No □Type
Air Temperature •F Steel Guard Pipe Around Casing □Yes □No D Flushmounted
Total Well Depth (TWO)= 1/100 It Locking Cap □Yes □No
Depth to Ground Water (DGW) = 1/10011 Protective Post/Abutment □Yes □No
Length of Water Column (LWC) = TWO -DGW = 1/10011 Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x = gal Well Yield □Low D Moderate □High
3 Casing Volumes = . gal = Standard Evacuation Volume Comments/Observatlo'ns
Method of Well Evacuation
Method of Sample Collection
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons) 0
TIME (military) 13:10
pH (S.U.) 3.47
Drawdown (fl) -
Sp. Cond. (µmhos/cm) 214
Water Temp. (°C) 17
TURBIDITY (NTUI" 0.13
• N--hAlnmetril": Turbirlftv 1,n...., Refill: Discharge:
OMMENTS/OBSERVATIONS SAMPLED AT 1315
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Field Data/or GW
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TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name: Rust Environmental & Infr.astructure Client ID: V-54 Lab ID: 098752-0013-SA Matrix: AQUEOUS Sampled: 21 APR 98 Authorized: 22 APR 98 Prepared: 23 APR 98
Parameter Result Units
alpha-BHC ND ug/L beta-BHC ND ug/L delta-BHC ND ug/L gamma-BHC (Lindane) ND ug/L alpha-Chlordane ND ug/L gamma-Chlordane ND ug/L Heptachlor ND ug/L Aldrin ND ug/L Heptachlor epoxide ND ug/L Endosul fan I ND ug/L Dieldrin ND ug/L 4,4'-DDE ND ug/L Endrin ND ug/L Endosulfan II ND ug/L 4,4'-DDD ND ug/L Endosulfan sulfate ND ug/L 4,4'-DDT ND ug/L Endrin aldehyde ND ug/L Endrin ketone ND ug/L Methoxychlor ND ug/L Toxaphene ND ug/L
Surrogate Recovery
Tetrachloro-m-xylene 83 % Decachlorobiphenyl 80 %
ND= Not detected
NA= Not applicable
~J)\ ,euanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 14 MAY 98
Reporting
Limit
0.050
0.050 0.050
0.050 0.050
0.050
0.050
0.050
0.050 0.050 0 .10 0.10 0.10
0.10 0.10
0.10 0.10
0.10 0. 10 0.50
1.0
Reported By: Jon Edmondson Approved By: Mike Orbanosky
The cover letter is an integral ·part of this report. Rev 230787
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Client Name: Rust Environmental Client ID: V-54 LAB ID: 098752-0013-SA Matrix: AQUEOUS Authorized: 22 APR 98
Oil ut ion Factor: 1.0
Parameter
Trichloroethene
Surrogate
Toluene-dB
4-Bromofluorobenzene
1,2-Dichloroethane-d4
NA a Not Applicable
ND= Not Detected
Volatile Organics Method 8260
& Infrastructure
Sampled: 21.APR 98 Prepared: NA
Result Units
ND ug/L
Recovery
94 %
97 %
114 %
~~\ ,:euanterra
Environmental
Services
Received: 22 APR 98
Analyzed: 29 APR 98
Rerorting imi t Qualifier
5.0
Acceptable Range
85 -111 81 -117
75 -121
Reported By: Matt Culver Approved By: Karin Yee
The cover letter is an integral part of this report.
Rev 230787
l=s =:a ;;;;a iiiil iiiiil iiii -- - - - - - ----iii)-
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For eddltlonal form1
pleaH write or call:
Type or Use a ball-point pen and press lirmly.
Facility Name __________ G_,l.ocgy'--C_h_•_m_ic_a_l C_o_rpc.o_ra_t_io_n_. _______ _
Address _____________ D_om_inc..o_D_ri-'n'-------------
DIVISION DF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578 .
RALEIGH, NC 27626-0578
[phone]
PERMIT NUMBER: (REQUIRED)
Noo-Discharge WQ 0009949
NPDES_--c=.,,.,.-,,---------,-.,-,,:--,== TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location __________________________ _ Lagoon __ Septic Tank/Drain Field
Well Identification Number Effiu,nt (V54) Well Depth ____ Ft.
Well Diameler ___ Sample (Screened) Interval ____ Ft. To Ft.
Depth to Water Level ___ ft. below measuring point (before sampling)
Measuring point is _____ ft. above land surface
Gallons of water pumped/bailed before samplinn,,_ ________ _
Spray Field __ Subsurface low-Pressure
Piping (LPP)
Land Application of Slu~e
__ 01her
Ro1ary Distribu1or
Field Analysis: pH ____ Specific Conductance ___ uMhos Temp. ___ 0 c Odor ___ Appearance __ _
Date Sample Collected 7122198 Date Lab Sample Analyze~--------
LabOratory Name Quanterra, West Sacramento, CA Certification No. ___ 2_1_6_6 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD ___________ mg/I
Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples)
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
TOG mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Al • Aluminum mg/I
Ba• Barium mg/I
Ca • Calcium mg/I
Cd • Cadmium mg/I
Chromium: Total mg/I
Cu • Copper mg/I
Fe -Iron mg/I
Hg • Mercury mg/I
K • Potassium mg/I
Mg • Magnesium mg/I
Mn • Manganese mg/I
Na • Sodium mg/I
Ni -Nicke ___________ mg/I
Pb • Lead mg/I
Zn -Zinc mg/I
Pesticides/Herbicides
(Soecify Compounds)
TCL Peslicidrs -resulls attached
Other (Specify Compounds and
Concentration units)
TCE -result! attached
ug/1
ug/1
ug/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. NQte.; Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date • Sae back for Instructions.
•• Submit blue and yellow copies only to address above.
- - - --- ----liiii --- -
EARTH©TECH Field Data Information Log for Ground Water Sampling
Page_1_of 1
Date {yr/mo/day) ___________ 98_/_0_7/2_2 ________ _ Casing Dlameter _____________________ lnches
Field Personnel ___________ N_._H_ick_s _________ _ Casing Material ______________________ _
Site Name __________ G_e..,ige.y_C_h_em_ica_l_C_o_,rp_o_ra_li_o_n _____ _ Measuring Point Elevation _________________ 1/100 ft
Earth Tech Job Number --------~3~1~8_19~---------Height of Riser {above land surface) 1/100 ft
Well ID # _____________ Effl_ue_n_t-'-(V_54-'-) _______ _ Land Surface Elevation 1/100 ft
D Upgradient D Downgradient D Sidegradient Screened Interval 1/100 ft
Weather Conditions. ____________________ _ Dedicated Pump or Bailer □Yes □No □Type
Air Temperature ________________ ...;... ____ °F Steel Guard Pipe Around Casing □.Yes □No D Flushmounted
Total Well Depth {TWD) = _________________ 1/100 ft Locking Cap □Yes □No
Depth to Ground Water {DGW) = 1/100 ft Protective PosUAbutment □Yes □No
Length of Water Column {LWC) = TWD • DGW = 1/100 ft Well Integrity Satisfactory □Yes □No
1 Casing Volume {OCV) = LWC x ___ = ____________ gal WellYleld □Low D Moderate □High
3 Casing Volumes = gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation. __________________ _
Method of Sample Collection. _________________ _
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED {gallons)
TIME {military)
pH {S.U.)
Drawdown {fl)
Sp. Cond. {µmhos/cm)
Water Temp. {°C)
TURBIDITY
Refill: Discharge:
fOMMENTS/OBSERVATIONS .:S:::a;;;m,:;pled=::al..:.1..:.44.:.:□:;.-________________________________________ -;
Field Data for GW
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(/!>uanterra
TCL Organochlorine Pesticides/PCBs
Method 8080
Client Name:
Client ID:
Rust Environmental & Infrastructure
Effluent (V54)
300553-0003-SA LAB ID:
Matrix: AQUEOUS Sampled: 22 JUL 98
Authorized: 23 JUL 98 Prepared: 24 JUL 98
Dilution Factor: 1.0
Parameter
alpha-BHC
beta-BHC
delta-BHC
gamma-BHC (Lindane) alpha-Chlordane
gamma-Chlordane Heptachlor
A 1 dri n
Heptachlor epoxide
Endosulfan I
Dieldrin
4,4'-DDE
Endrin Endosulfan II 4,4'-DDD Endosulfan sulfate 4, 4' -DDT ·
Endrin aldehyde
Endrin ketone
Methoxychlor
Toxaphene
Surrogate
Tetrachloro-m-xylene
Decachlorobiphenyl
Result Units
ND ug/L
ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L ND ug/L
ND ug/L
ND ug/L
Recovery
90 % 93 %
Received: 23 JUL 98
Analyzed: 01 AUG 98
Reporting
Limit Qualifier
0.050
0.050
0.050 0.050
0.050
0.050
0.050
0.050 0.050
0.050 0. 10
0. 10 0.10
0.10
0 .10
0 .10
0.10
0 .10 0.10
0.50
1.0
Acceptable Range
55 -ll5
35 -137
I ND= Not Detected
0
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Reported By: Marcia Reed Approved By: Jon Edmondson
The cover letter is an integral part of this report. Rev 230787
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Client Name:
Client ID: LAB ID: Matrix: Authorized:
Volatile Organics
Method 8260
Rust Environmental & Infrastructure
Effluent ( V54) 300553-0003-SA AQUEOUS Sampled: 22 JUL 98 23 JUL 98 Prepared: NA
(!!>uanterra
Received: 23 JUL 98 Analyzed: 31 JUL 98 I Dilution Factor: 1.0
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Parameter
Trichloroethene
Surrogate
Toluene-dB 4-Bromofluorobenzene l,2-Dichloroethane-d4
NA= Not Applicable ND= Not Detected
Reported By: Michael Lucchesi
Result
ND
Recovery
98 %
89 % 94 %
Units
Reporting
Limit Qualifier
ug/L 5.0
Acceptable Range
85 -II 1
81 -117
75 -121
Approved By: Mike Or~anosky
The cover letter is an integral part of this report.
Rev 230787
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
For additional forms
pleHe write or call:
Type or Use a ball-point pen and press firmly.
Facility Name _________ G_ri'"gy'-C'::-h-'rm...,i,...ca...,1::-C-:-or.,_po_r_al_io_n _______ _
AddreSS------,-,--:=-=-_.;:;D.;;;om""i"'no'-D'-'r-"iv-'-e-----,-,-----
____ A_b_rr_d_rr_n,~N_C_28_J_l5 ____ County ___ ~M~•~••c.a•----
DIVISION OF WATER QUALITY· GROUNDWATER SECTION
P.O. BOX 29578
RALEIGH, NC 27628·0578
[phone]
PERMIT NUMBER: (REQUIRED)
Non-Discharge WQ 0009949
NPDES __ ==----------,,-=== TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) Well Location ________________________ _ Lagoon __ Septic Tank/Drain Field
Well ldentilication Number Emurnl Well Depth ____ Ft.
Well Diameler ___ Sample (Screened) lnlerval, ____ Ft. To Ft.
Depth lo Water Level ___ ft. below measuring poinl (before sampling)
Measuring point is, ____ ft. above land surface
Gallons of water pumped/bailed before samplinng._ ________ _
Spray Field __ Subsurface Low.Pressure
Piping (LPP)
Land Application ol Slud£e
_,_. Other
__ Rotary Distributor
Field Analysis: pH ____ Specific Conductance ___ uMhos Temp. ___ o C Odor ___ Appearance __ _
Date Sample Collected 10127198 Date Lab Sample Analyze,~--------
Laboratory Name Quanlerra. West Satramenlo, CA Certification No. --~2~16~6 __ _
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED __ YES __ NO
COD--:-:-=--:::---:---------mg/1 Coliform: MF Fecal 1100ml
Coliform: MF Total 1100ml
Nitrite (NO2) as N _______ mg/I
Nitrate (NO3 ) as N mg/I
Phosphorus: Total as P mg/I
(Note: Use MPN method for hlghly turbid samples)
Dissolved Solids: Total ______ mg/I
pH (when analyzed) units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg/I
Al -Aluminum mg/I
Ba -Barium mg/I
Ca -Calcium mg/I
Cd -Cadmium mg/I
Chromium: Total mg/1
Cu -Copper mg/I
Fe -Iron mg/I .
Hg -Mercury mg/I
K -Potassium mg/1
Mg -Magnesium mg/I
Mn -Manganese mg/I
Na -Sodium mg/1
Ni -Nicke. __________ mg/1
Pb -Lead mg/1
Zn -Zinc mg/I
Pesticides/Herbicides
(Soecify Compounds)
TCL Pesticides -results attached
Other (Specify Compounds and
Concentration units)
TCE -results attached
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. ~ Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Signature of Permittee (or Authorized Agent*)
GW-59 REV. 8/96
Date
• See back for Instructions.
" Submit blue and yellow copies only to address above. ·
liill liiil ---- - - - --.. l!!I!!!!! I!!!!! == == lilil
EARTH(DT E C H Field Data Information Log for Ground Water Sampling
Page_1_of
Date (yr/mo/day) 98/10/27 Casing Diameter Inches
Field Personnel 0. Shoopman Casing Material
Site Name Geigy Chemical Corporation Measuring Point Elevation 1/10011
Earth Tech Job Number 31819 Height of Riser (above land surface) 1/100 ft
Well ID# Effluent Land Surface Elevation 1/100 ft
O Upgradient O Downgradient O Sidegradient Screened Interval 1/100 ft
Weather Conditions Dedicated Pump or Baller □Yes □No □Type
Air Temperature •F Steel Guard Pipe Around Casing □Yes □No O Flushmounted
Total Well Depth (TWO) = 11100ft Locking Cap □Yes □No
Depth to Ground Water (DGW) = 1/100 ft Protective Post/Abutment □Yes □No
Length of Water Column (LWC) =TWO· DGW = 1/100 ft Well Integrity Satisfactory □Yes □No
1 Casing Volume (OCV) = LWC x = gal WellYleld □Low D Moderate □High
3 Casing Volumes = gal = Standard Evacuation Volume Comments/Observations
Method of Well Evacuation
Method of Sample Collection
Total Volume of Water Removed gal
FIELD ANALYSES
VOLUME PURGED (gallons)
TIME (military)
pH (S.U.)
Drawdown (ft.)
Sp. Cond. (µmhos/cm)
Water Temp. (°C)
TURBIDITY
Refill: Discharge:
OMMENTS/OBSERVATIONS Sampled al 1015.
Field Data for GW
#j)\ ,euanterra I TCL Organochlorine Pesticides/PCBs Method 8080
I Client Name:
Client JD:
Rust Environmental & Infrastructure
Effluent
LAB JD: 302382-0003-SA I Matrix: AQUEOUS Sampled: 27 OCT 98
Authorized: 28 OCT 98 Prepared: 03 NOV 98
I Dilution Factor: 1.0
Parameter
I alpha-BHC beta-BHC
delta-BHC
I gamma-BHC (Lindane)
alpha-Chlordane
gamma-Chlordane
I Heptachlor
Aldrin Heptachlor epoxide
Endosul fan I
I Dieldrin
4,4'-DDE
Endrin
Endosulfan I I
I 4,4'-DDD
Endosulfan sulfate
4, 4' -DDT
I
Endrin aldehyde
Endri n ketone
Methoxychlor Toxaphene
I Surrogate
I Tetrachloro-m-xylene
Decachlorobiphenyl
I
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I ND = Not Detected
Result Units
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
ND ug/L
Recovery
75 %
50 %
Received: 28 OCT 98
Analyzed: 13 NOV 98
Reporting
Limit MDL Qualifier
0.050 0.0080
0.050 0.0040
0.050 0.0060
0.050 0.010
0.050 0.0070
0.050 0.0080
0.050 0.0070
0.050 0.0060
0.050 0.0080 0.050 0.010
0 .10 0.020 0 .10 0.015
0 .10 0.020
0.10 0.020
0.10 0.0050
0.10 0.033
0 .10 0.020
0 .10 0.029
0 .10 0.024
0.50 0.040
1.0 1.0
Acceptable Range
55 -115
35 -137
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Reported By: Lisa Stafford Approved By: Mike Orbanosky
The cover letter is an integral part of this report.
Rev 230787
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(8240 list) -Volatile Organics Target Compound List (TCL)
Method SW8260A
Client Name:
Client ID:
Lab ID:
Matrix:
Authorized:
Rust Environmental
Effluent
302382-0003-SA
AQUEOUS 28 OCT 98
Parameter
Trichloroethene
Surrogate
l,2-Dichloroethane-d4
Toluene-dB
4-Bromofluorobenzene
ND= Not detected
NA= Not applicable
Reported By: SWJLLMS
& Infrastructure
Sampled: 27 OCT 98 Received: 28 OCT 98
Prepared: 09 NOV 98 Analyzed: 09 NOV 98
Reporting
Result Units Limit
ND
Recovery
ug/L
98 %
102 %
98 %
Approved By: DBAREWALD
1.0
The cover letter is an integral part of this report.
Rev 230787