NCD980840409_19950407_Charles Macon Lagoon & Drum_FRBCERCLA RD_Monthly Progress Reports 1994 - 1995-OCR

I
1-iH,.v,-., lXlvr.
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APR 131995
Macon/Dockery Site SUPERFUND SECTION 1
Richmond County, North Carolina
April 7, 1995
Ms. Giezelle Bennett
Remedial Project Manager
us EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
Reply to: Technical Committee
c/o David L. Jones
Clark Equipment Company
P. o. Box 7008
South Bend, IN 46634
Phone: [phone]
Fax: [phone]
RE: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress Report -March 1995
Dear Ms. Bennett: ..
On behalf of the Macon/Dockery Site Group ("Group"), the Marqh 1995 Monthly Progress
Report is herewith submitted in accordance with Section XV " PROGRESS REPORTS of
the Unilateral Administrative Order (effective date~ June 30, 1992) for the Macon/Dockery
Site. This report describes those activities which occurred during the month of March as
part of the Remedial Design and Remedial Action phase of this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH MARCH 1995:
Results of Sampling and Testing and Other Data Received:
• None.
Plans, Reports. Deliverables and Procedures Completed:
• Conducted competitive bidding procedures for the peripheral containment
pump and treat systems and the SVE system.
• Opened competitive bids on March 23, 1995 and began bid evaluations.
• On March 29, 1995, the Group received a letter from the U.S. EPA granting
approval to discharge treated water from the Upper Macon Source Area air
stripper system directly to the onsite infiltration gallery without treating for
manganese. This approval is conditioned on the provision that the system
design must be "closed loop" meaning that the infiltration gallery must be
upgradient to the injection wells which must subsequently be able to
recapture the discharge to the infiltration gallery.
,
Ms. Giezelle Bennett
April 7, 1995
Page 2 of 2
•
TASKS PLANNED FOR APRIL 1995:
•
• Submit the 90% Design documents for the Upper Macon Source Area
groundwater treatment system to the U.S. EPA for review.
• Select a Construction Contractor and submit the names, qualifications, and
experience for the RA Construction Manager, Construction Contractor, and
IQAT to the U.S. EPA for approval.
• Receive U.S. EPA approval of the RA Construction Manager, Construction
Contractor, and IQA T.
• Conduct the Pre-Construction conference following, U.S. EPA approval of the
RA Construction Manager, Construction Contractor and IQAT.
• Proceed with RA mobilization for the construction of the peripheral
containment pump and treat systems and the SVE system.
PROBLEMS AND DELAYS:
• None.
If there are any questions, please do not hesitate to contact me at 803-537-9794.
Very truly yours,
t{)r~~
Kenny Gulledge fi7
Project Coordinator
MHS/jca
cc: Macon/Dockery Site Group Members
Wayne F. Barto, de maximis, inc.
Paul Furtick, RMT, Inc.
F:IPROJECTS\3068\MPRMAR.95
•
Macon/Dockery Site
RECEIVED
FEB 1 71995
SUPERFUND SECTION Richmond County, North Carolina
February 9, 1995
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
Reply to: Technical Committee
c/o David L. Jones
Clark Equipment Company
P. 0. Box 7008
South Bend, IN 46634
Phone: [phone]
Fax: [phone]
RE: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress Report -January 1995
Dear Ms. Bennett:
On behalf of the Macon/Dockery Site Group ("Group"), the January 1995 Monthly Progress
Report is herewith submitted in accordance with Section XV -PROGRESS REPORTS of the Unilateral Administrative Order (effective date -June 30, 1992) for the Macon/Dockery
Site. This report describes those activities which occurred during the monih of January
as part of the Remedial Design and Waste Removal Phase for this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH JANUARY 1995:
Results of Sampling and Testing and Other Data Received:
• Results of laboratory analytical data received during January 1995 for
groundwater samples collected from monitoring wells in the MW-09 vicinity
· are attached. This data was collected in support of the bioremediation
demonstration program at this location.
Plans. Reports, Deliverables and Procedures Completed:
• On January 6, 1995, the Group transmitted a facsimile to the U.S. EPA
containing a revised Table 1 showing results in micro-molar units for MW-09
area groundwater as apposed to ug/I units shown in the original
Bioremediation Pilot Study Interim Report. A revised Figure 11 from the
Report was also submitted with this facsimile.
• This facsimile was forwarded prior to a teleconference call held later that
same day. On the call, representatives from U.S. EPA, NCDEHNR, COM-
Federal Programs, USEPA"s Robert S. Kerr Environmental
Researchlaboratory in Ada. Oklahoma, as well as representatives from the
' •
Ms. Giezelle Bennett
February 9, 1995
Page 2 of 3
Group and their consultants discussed U.S. EPA comments on the
Bioremediation Pilot Study Report.
• On January 13, 1995, the Group submitted to U.S. EPA responses prepared
on behalf of the Group by their consultant, DuPont Environmental
Remediation Services (DERS) to the second set of U.S. EPA comments on
the report entitled, "Macon Dockery Site -Bioremediation Pilot Study Interim
Report".
• On January 23, 1995, the Group received U.S. EPA's approval and final
comments on the Group's responses to the agency comments on the Final
Remedial Design deliverables submitted on December 19, 1995.
• Also on January 23, 1995, the Group's Technical Committee met with their
consultants to discuss progress and analytical results for the Bioremediation
Demonstration Program.
• Following the January 23, 1995 meeting the Group elected to discontinue
the Bioremediation Pilot Study and follow the extraction and treatment option
for site source areas due to significant time constraints and unfavorable cost
evaluations.
• On January 30, 1995, the Group's consultant, RMT, Inc., transmitted the
document entitled "Completion Report for the Removal of Wastes from
Lagoon 10, Vessels, and Drums" to U.S. EPA for their review.
TASKS PLANNED FOR FEBRUARY 1995:
• On February 3, 1995, DERS discontinued the introduction of nutrients in the
MW-09 location of the Upper Macon area of the site for the Bioremediation
Demonstration Program.
• Submit the Final Design documents to U.S. EPA no later than
February 17, 1995.
• Complete the development of a Remedial Action Groundwater and SVE
Treatment System bid package and begin competitive bidding procedures
pending U.S. EPA's approval of the Final Design documents.
' •,, •
Ms. Giezelle Bennett
February 9, 1995
Page 3 of 3
•
• Begin preparation of the Prefinal Design elements for all site source area extraction
and treatment systems.
PROBLEMS AND DELAYS:
• None.
If there are any questions, please do not hesitate to contact me at 219-239-0195.
Very truly yours,
:~!~~
Project Coordinator
Macon/Dockery Technical Committee Chairman
WFB/jca
Attachments
cc: Macon/Dockery Site Group Members
Wayne F. Barto, de maximis, inc.
Paul Furtick, RMT, Inc.
Kevin White, DERS
F:'PROJECTS\3068\MPRJAN.95
TOC
Date PM-1 ·PM-1A PM-2
3/1/93 NA NA NA
9/21/94 NA NA NA
10/13/94 NA NA NA
12/19/94 10.10 28.28 12.60
12/28/94 11.00 2.30 14.00
1/3/95 17.00 15.00 15.00
1/6/95 12.00 8.40 13.00
1/10/95 12.00 3.40 14.00
COD
Date PM-1 PM-1A PM-2
3/1/93 NA NA NA
9/21/94 NA NA NA
10/13/94 NA NA NA,.
12/19/94 41.00 <15 40.00
12/28/94 59.00 <25 75.00
1/3/95 97.00 76.00 67.00
1/6/95 61.00 52.00 68.00
1/10/95 66.00 28.00 59.00
TCA
Date PM-1 PM-1A PM-2
3/1/93 NA NA NA
9/21/94 NA NA NA
10/13/94 22.00 11.00 22.00
12/19/94 NA NA NA
12/28/94 NA NA NA
1/3/95 NA NA NA
1/6/95 19.00 10.00 18.00
1/10/95
PM-3
NA
NA
NA
27.70
31.00
29.00
33.00
28.00
PM-3
NA
NA
NA
160.00
170.00
160.00
130.00
140.00
PM-3
NA
NA
<0.072
NA
NA
NA
<2
Macon Dockery
Analytical Results
uy'l
PM-4 PM-4A PM-5
NA NA NA
NA NA NA
NA NA NA
35.50 4.80 34.20
75.00 5.80 32.00
81.00 24.00 30.00
71.00 27.00 34.00
79.00 24.00 34.00
PM-4 PM-4A PM-5
NA NA NA
NA NA NA
NA NA NA
148.00 23.00 34.20
270.00 <25 150.00
290.00 81.00 170.00
280.00 170.00 160.00
330.00 100.00 170.00
PM-4 PM-4A PM-5
NA NA NA
NA NA NA
1.90 8.50 21.00
NA NA NA
NA NA NA
NA NA NA
<5 9.00 20.00
.
PM-6 PM-6A PM-7 PM-7A MW-09 PM-SA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
18.60 <1 21.00 2.04 46.00 2.22
22.00 1.40 19.00 1.80 64.00 7.30
27.00 36.00 20.00 2.00 66.00 16.00
25.00 11.00 22.00 2.30 80.00 16;00
25.00 4.60 20.00 3.20 120.00 5.20
PM-6 PM-6A PM-7 PM-7A MW-09 PM-SA
NA NA NA NA NA NA
NA NA NA NA NA NA
NA NA NA NA NA NA
18.60 <1 86.00 <15 186.00 15.00
110.00 <25 79.00 <25 250.00 33.00
150.00 170.00 97.00 <25 360.00 86.00
99.00 59.00 87.00 <25 350.00 99.00
96.00 26.00 78.00 <25 320.00 <25
PM-6 PM-6A PM-7 PM-7A MW-09 PM-SA
NA NA NA NA 11.00 NA
NA 7.00 NA NA NA NA
<1 3.60 NA 2.30 7 70 13.00
NA NA 16.00 NA <10 NA
NA NA NA NA NA NA
NA NA NA NA NA NA
<5 15.00 6.00 5.00 16.00
1, 1-DCE
Date PM-1 PM-1A
3/1/93 NA NA
9/21/94 NA NA
10/13/94 28.00 24.00
12/19/94 NA NA
12/28/94 NA NA
1/3/95 NA NA
1/6/95 24.00 22.00
1/10/95
PCE
Date PM-1 PM-1A
3/1/93 NA NA
9/21/94 NA NA
10/13/94 32.00 29.00
12/19/94 NA NA
12/28/94 NA NA
1/3/95 NA NA
1/6/95 25.00 19.00
1/10/95
TCE
Date PM-1 PM-1A
3/1/93 NA NA
9/21/94 NA NA
10/13/94 46.00 42.00
.12/19/94 NA NA
12/28/94 NA NA
1/3/95 NA NA
1/6/95 42.00 30.00
1/10/95
• •
PM-2 PM-3 PM-4
NA NA NA
NA NA NA
31.00 <1.2 <1.2
NA NA NA
NA NA NA
NA NA NA
24.00 <2 <5
PM-2 PM-3 PM-4
NA NA NA
NA NA NA
35.00 <2.1 8.10
NA NA NA
NA NA NA
NA NA NA
32.00 3.00 5.00
PM-2 PM-3 PM-4
NA NA NA
NA NA NA
38.00 1.80 8.10
NA NA NA
NA NA NA
NA NA NA
32.00 <2 5.00
Macon Dockery
Analytical Results
UCJt'l
PM-4A PM-5
NA NA
NA NA
15.00 9.10
NA NA
NA NA
NA NA
21.00 <20
PM-4A PM-5
NA NA
NA NA
18.00 23.00
NA NA
NA NA
NA NA
17.00 20.00
PM-4A PM-5
NA NA
NA NA
27.00 48.00
NA NA
NA NA
NA NA
28.00 50.00
Page 2
PM-6 PM-6A
NA NA
NA 16.00
4.20 13.00
NA NA
NA NA
NA NA
<5
PM-6 PM-6A
NA NA
NA 13.00
20.00 10.00
NA NA
NA NA
NA NA
18.00
PM-6 PM-6A
NA NA
NA 21.00
13.00 12.00
NA· NA
NA NA
NA NA
13.00
PM-7 PM-7A MW-09 PM-9A
NA NA 12.00 NA
NA NA NA NA
NA <1.3 5.40 28.00
69.00 NA <10 NA
NA NA NA NA
NA NA NA NA
14.00 11.00 <5 30.00
PM-7 PM-7A MW-09 PM-9A
NA NA 25.00 NA
NA NA NA NA
NA 6.70 23.00 24.00
34.00 NA 21.00 NA
NA NA NA NA
NA NA NA NA
27.00 7.00 13.00 21.00
PM-7 PM-7A MW-09 PM-9A
NA NA 28.00 NA
NA NA NA NA
NA 6.80 28.00 38.00
47.00 NA 14.00 NA
NA NA NA NA
NA NA NA NA
46.00 10.00 16.00 46.00
•
CIS 1,2 DCE
Date PM-1 PM-1A PM-2 PM-3
3/1/93 NA NA I NA NA
9/21/94 NA NA I NA NA
10/13/94 98.00 160.00 72.00 9.90
12/19/94 NA NA I NA NA
12/28/94 NA NA I NA NA
1/3/95 NA NA I NA NA
1/6/95 84.00 85.00 64.00 <2
1/10/95 I
TRANS 1,2 DCE
Date PM-1 PM-1A l?M-2 PM-3
3/1/93 NA NA I NA NA
9/21/94 NA NA I NA NA
10/13/94 <1.3 <1.3 :<1.3 <1.3
12/19/94 NA NA I NA NA
12128/94 NA NA I NA NA
1/3/95 NA NA I NA NA
1/6/95 <5 <5 I <5 . <2
1/10/95 I
1.2-DCE
•
Date PM-1 PM-1A RM-2 PM-3
3/1/93 NA NA I NA NA
9/21/94 NA NA I NA NA
10/13/94 98.00 160.00 72.00 9.90
12/19/94 NA NA I NA NA
12/28/94 NA NA I NA NA
1/3/95 NA NA I NA NA
1/6/95 NL NL I NL NL
1/10/95 I
1,2-DCA
Date PM-1 PM-1A RM-2 PM-3
3/1/93 NA NA INA NA
9/21/94 NA NA INA NA
10/13/94 NL NL I NL NL
12/19/94 NA NA INA NA
12/28/94 NA NA INA NA
1/3/95 NA NA INA NA
1/6/95 <5 <5 I <5 <2
1/10/95 I
Macon Dockery
Analytical Results
u_J/1
PM-4 PM-4A PM-5
NA NA NA
NA NA NA
23.00 47.00 890.00
NA NA NA
NA NA NA
NA NA NA
8.00 <2 800.00
PM-4 PM-4A PM-5
NA NA NA
NA NA NA
<1.3 <1.3 8.70
NA NA NA
NA NA NA
NA NA NA
<5 <2 <20
PM-4 PM-4A PM-5
NA NA NA
NA NA NA
23.00 47.00 900.00
NA NA NA
NA NA NA
NA NA NA
NL NL NL
PM-4 PM-4A PM-5
NA NA NA
NA NA NA
NL NL NL
NA NA NA
NA NA NA
NA NA NA
<5 <2 <20
· Page 3
•
PM-6 PM-6A
NA NA
NA <5
58.00 110.00
NA NA
NA NA
NA NA
43.00
PM-6 PM-6A
NA NA
NA <5
4.10 <1.3
NA NA
NA NA
NA NA
<5
PM-6 PM-6A
NA NA
NA NL
62.00 110.00
NA NA
NA NA
NA NA
NL NL
PM-6 PM-6A
NA NA
NA <5
NL NL
NA NA
NA NA
NA NA
<5
PM-7 PM-7A MW-09 PM-9A
NA NA NL NA
NA NA NA NA
NA 60.00 84.00 59.00
<1 NA <1 NA
NA NA NA NA
NA · NA NA NA
90.00 30.00 52.00 63.00
PM-7 PM-7A MW-09 PM-9A
NA NA NL NA
NA NA NA NA
NA <1.3 <1.3 <1.3
<10 NA <10 NA
NA NA NA NA
NA NA NA NA
<5 <10 <5 <2
PM-7 PM-7A MW-09 PM-9A
NA NA NL NA
NA NA NA NA
NA 50.00 84.0D 59.00.
92.00 NA NL NA
NA NA NA NA
NA NA NA NA
NL NL NL NL
PM-7 PM-7A MW-09 PM-9A
NA NA NL NA
NA NA NA NA
NL NL NL NL
NL NA <1 NA
NA NA NA NA
NA NA NA NA
<5 <20 <5 <2
• • Macon Dockery
Analytical Results
U_J/1
1,1-DCA
Date PM-1 PM-1A PM-2 PM-3 PM-4 PM-4A PM-5 PM-6 PM-6A PM-7 PM-7A MW-09 PM-9A
3/1/93 NA NA NA NA NA NA NA NA NA NA NA 160.00 NA
9/21/94 NA NA NA NA NA NA NA NA 42.00 NA NA NA NA
10/13/94 150.00 85.00 140.00 69.00 92.00 41.00 280.00 150.00 28.00 NA 16.00 140.00 53.00
12/19/94 NA NA NA NA NA NA NA NA NA <10 NA 130.00 NA
12/28/94 NA NA NA NA NA NA NA NA NA NA NA NA NA
1/3/95 NA NA NA NA NA NA NA NA NA NA NA NA NA
1/6/95 120.00 48.00 140.00 57.00 74.00 70.00 260.00 120.00 110.00 15.00 120.00 57.00
1/10/95
CA
Date PM-1 PM-1A PM-2 PM-3 PM-4 PM-4A PM-5 PM-6 PM-6A PM-7 PM-7A MW-09 PM-9A
3/1/93 NA NA NA NA NA NA NA. NA NA NA NA NL NA
9/21/94 NA NA NA NA NA NA NA NA <5 NA NA NA NA
10/13/94 68.00 23.00 58.00 260.00 210.00 25.00 390.00 260.00 3.80 NA <2.3 220.00 60.00
12/19/94 NA NA NA NA NA NA NA NA NA 93.00 NA 170.00 NA
12/28/94 NA NA NA NA NA NA NA NA NA NA NA NA NA
1/3/95 NA NA NA NA NA NA NA NA NA NA NA NA NA
1/6/95 42.00 10.00 30.00 150.00 170.00 51.00 230.00 160.00 90.00 <5 170.00 34.00
1/10/95
VG
Date PM-1 PM-1A PM-2 PM-3 PM-4 PM-4A PM-5 PM-6 PM-6A PM-7 PM-7A MW-09 PM-9A
3/1/93 NA NA NA NA NA NA NA NA NA NA NA 350.00 NA
9/21/94 NA NA NA NA NA NA NA NA 98.00 NA NA NA NA
10/13/94 220.00 170.00 170.00 <1 150.00 90.00 1000.00 350.00 66.00 NA <1 270.0(I 180.00
12/19/94 NA NA NA NA NA NA NA NA NA 190.00 NA 190.00 NA
12/28/94 NA NA NA NA NA NA NA NA NA NA NA NA NA
1/3/95 NA NA NA NA NA NA NA NA NA NA NA NA NA
1/6/95 120.00 61.00 79.00 5.00 94.00 20.00 560.00 160.00 10.00 130.00 81.00 82.00
1/10/95
Page 4
METHANE ,
Date PM-1 PM-1A PM-2 PM-3 PM-4
3/1/93 NA NA NA NA NA
9/21/94 NA NA NA NA NA
10/13/94 31.00 14.00 15.00 39.00 180.00
12/19/94 NA NA NA NA NA
12/28/94 NA NA NA NA NA
1/3/95 NA NA NA NA NA
1/6/95
1/10/95
ETHANE
Date PM-1 PM-1A PM-2 PM-3 PM-4
3/1/93 NA NA NA NA NA
9/21/94 NA NA NA NA NA
10/13/94 <1 <1 <1 <1 <1
12/19/94 NA NA NA NA NA
12/28/94 NA NA NA NA NA
1/3/95 NA NA NA NA NA
1/6/95
1/10/95
ETHENE
Date PM-1 PM-1A PM-2 PM-3 PM-4
3/1/93 NA NA NA NA NA
9/21/94 NA NA NA NA NA
10/13/94 3.80 <1 <1 46.00 110.00
12/19/94 NA NA NA NA NA
12/28/94 NA NA NA NA NA
1/3/95 NA NA NA NA NA
1/6/95
1/10/95
Macon Dockery
Analytical Results
uy1
PM-4A PM-5
NA NA
NA NA
15.00 68.00
NA NA
NA NA
NA NA
PM-4A PM-5
NA NA
NA NA
<1 <1
NA NA
NA NA
NA NA
PM-4A PM-5
NA NA
NA NA
<1 140.00
NA NA
NA NA
NA NA
Page 5
•
PM-6 PM-6A
NA NA
NA NA
76.00 8.40
NA NA
NA NA
NA NA
PM-6 PM-6A
NA NA
NA NA
<1 <1
NA NA
NA NA
NA NA
PM-6 PM-6A
NA NA
NA NA
76.00 <1
NA NA
NA NA
NA NA
PM-7 PM-7A MW-09 PM-9A
NA NA NA NA
NA NA NA NA
270.00 7.00 42.00 33.00
NA NA 71.00 NA
NA NA NA NA
NA NA NA NA
PM-7 PM-7A MW-09 PM-9A
NA NA NA NA
NA NA· NA NA
NA <2 <1 <1
<25 NA <25 NA
NA NA NA NA
NA NA NA NA
PM-7 PM-7A MW-09 PM-9A
NA NA NA NA
NA NA NA NA
NA <1 <2 <1
<25 NA <25 NA
NA NA NA NA
NA NA NA NA
MOLECULAR WEIGHT
TCA MW= 97.00
Date PM-1 PM-1A
9121/94
10/13194 0.23 0.11
12119194
12/28194
1/3195
1/6/95 0.20 0.10
1/10195
1,1-DCE MW= 97.00
Date PM-1 PM-1A
9/21/94
10/13194 0.29 0.25
12119/94
12/28194
1/3195
1/6195 0.25 0.23
1/10/95
PCE MW= 166.00
Date PM-1 PM-1A
9/21/94
10/13/94 0.19 0.17
12119/94
12128/94
113195
1/6/95 0.15 0.11
1/10195
TCE MW= 131.00
Date PM-1 PM-1A
9/21/94
10/13/94 0.35 0.32
12119/94
12128/94
1/3195
1/6/95 0.32 0.23
1/10/95
• •
PM-2 PM-3 PM-4
0.23 0.02
0.19
PM-2 PM-3 PM-4
0.32
0.25
PM-2 PM-3 PM-4
0.21 0.05
0.19 0.02 0.03
PM-2 PM-3 PM-4
0.29 0.01 0.06
0.24 0.04
Macon Dockery
Analytical Results
i:g,nole
PM-4A PM-5
0.09 0.22
0.09 0.21
PM-4A PM-5
0.15 0.09
0.22
PM-4A PM-5
0.11 0.1.4
0.10 0.12
PM-4A PM-5
0.21 0.37
0.21 0.38
PM-6 PM-6A
0.04
0.00
..
PM-6 PM-6A
0.04 0.13
0.00
PM-6 PM-6A
0.12. 0.06
0.11 0.00
PM-6 PM-6A
0.10 0.09
0.10 0.00
PM-7 PM-7A MW-09 PM-9A
0.02 0.08 0.13
\
0.15 0.06 0.05 0.16
PM-7 PM-7A MW-09 PM-9A
0.06 0.29
0.14 0.11 0.31
PM-7 PM-7A MW-09 PM-9A
0.04 0.14 0.14
0.16 0.04 0.08 0.13
..
PM-7 PM-7A MW-09 PM-9A
0.05 0.21 0.29
0.35 0.08 0.12 0.35
•
. CIS-1,20C MW= 97.00
Date PM-1 PM-1A PM-2 PM-3
9/21/94
10/13/94 1.01 1.65 0.74 0.10
12/19/94
12/28/94
1/3/95
1/6/95 0.87 0.88 0.66
1/10/95
T-1,2-0CE MW= 97.00
Date PM-1 PM-1A PM-2 PM-3
9/21/94
10/13/94
12/19/94
12/28/94
1/3/95
1/6/95
1/10/95
1,2 DCE MW= 97.00
Date PM-1 PM-1A PM-2 PM-3
9/21/94
10/13/94 1.01 1.65 0.74 0.10
12/19/94
12/28/94
1/3/95
1/6/95
1/10/95 .
1,1 DCA MW= 99.00
Date PM-1 PM-1A PM-2 PM-3
9/21/94
10/13/94 1.52 0.86 1.41 0.70
12/19/94
12/28/94
1/3/95
1/6/95 1.21 0.48 1.41 0.58
1/10/95
PM-4
0.24
0.08
PM-4
PM-4
0.24
PM-4
0.93
Macon Dockery
Analytical Results
UJ,1I01e
PM-4A PM-5
0.48 9.18
8.25
PM-4A PM-5
0.09
PM-4A PM-5
0.48 9.28
PM-4A PM-5
0.41 2.83
0.75 0.71 2.63
Page 7
•
PM-6 PM-6A
0.60 1.13
0.44 0.00
PM-6 PM-6A
0.04
0.00
PM-6 PM-6A
0.64 1.13
PM-6 PM-6A
1.52 0.28
1.21 0.00
PM-7 PM-7A MW-09 PM-9A
0.62 0.87 0.61
0.93 0.31 0.54 0.65
PM-7 PM-7A MW-09 PM-9A
PM-7 PM-7A MW-09 PM-SA
0.52 0.87 0.61
PM-7 PM-7A MW-09 PM-SA
0.16 1.41 0.54
1.11 0.15 1.21 0.58
• •
CA MW= 64.00
Date PM-1 PM-1A PM-2 PM-3 PM-4
9/21/94
10/13/94 1.06 0.36 0.91 4.06 3.28
12/19/94
12/28/94
1/3/95
1/6/95 0.66 0.16 0.47 2.34 2.66
1/10/95
vc t-,W,J= 63.00
Date PM-1 PM-1A PM-2 PM-3 PM-4
9/21/94
10/13/94 3.49 2.70 2.70 2.38
12/19/94
12/28/94
1/3/95
1/6/95 1.90 0.97 1.25 0.08 1.49
1/10/95
METHAN MW= 16.00
Date PM-1 PM-1A PM-2 PM-3 PM-4
9/?.1/94
10/13/94 1.94 0.88 0.94 2.44 11.25
12/19/94
12/28/94
1/3/95
1/6/95 0.00 0.00 0.00 0.00 0.00
1/10/95
ETH ENE MW= 28.00
Date PM-1 PM-1A PM-2 PM-3 PM-4
9/21/94
10/13/94 0.14 1.64 3.93
12/19/94
12/28/94
1/3/95
1/6/95 0.00 0.00 0.00 0.00 0.00
1/10/95
Macon Dockery
Analytical Results
UJ1I01e
PM-4A PM-5
0.39 6.09
0.80 3.59
PM-4A PM-5
1.43 15.87
0.32 8.89
PM-4A PM-5
0.94 4.25
0.00 0.00 ·
PM-4A PM-5
5.00
0.00 0.00
Page 8
•
PM-6 PM-6A
4.06 0.06
2.50 0.00
PM-6 PM-6A
.
5.56 1.05
2.54 0.16
PM-6 PM-6A
... 4.75. 0.53
0.00 0.00
PM-6 PM-6A
2.71
0.00 0.00
PM-7 PM-7A MW-09 PM-9A
3.44 0.94
1.41 · 2.66 0.53
PM-7 PM-7A MW-09 PM-9A
4.29 2.86
2.06 0.00 1.29 1.30
PM-7 PM-7A MW-09 PM-9A
16.88 0.44 2.63 2.06
0.00 0.00 0.00 0.00
PM-7 PM-7A MW-09 PM-9A
0.00 0.00 0.00 0.00
•
Macon/Dockery Site
• RECEIVED I
JAN 201995
Richmond County, North Carolina
SUPERFUND SECTION
January 9, 1995
Ms. Giezelle Bennett
Remedial Project Manager
U.S. EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
Re: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress Report -December 1994
Dear Ms. Bennett:
Reply to: Technical Committee
c/o David L. Jones
Clark Equipment Company
P. 0. Box 7008
South Bend, IN 46634
Phone: [phone]
Fax: [phone]
On behalf of the Macon/Dockery Site Group ("Group), the December 1994 Monthly Progress Report is herewith
submitted in accordance with Section XV -PROGRESS REPORTS of the Unilateral Administrative Order (effective
date -June 30, 1992) for the Macon/Dockery Site. This report describes those activities which occurred during the
month of December as part of the Remedial Design and Waste Removal Phase for this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH DECEMBER 1994:
Results of Sampling and Testing and Other Data Received:
No additional laboratory analytical data, sampling or testing results were received during December, 1994.
Plans, Reports. Deliverables and Procedures Completed:
• On December 7, 1994, the Group received U.S. EPAcomments on the PreFinal Design Report prepared
by RMT, Inc.
The Group submitted a letter dated December 9, 1994 which summarized a telephone conversation between
· Giezelle Bennett and several Group representatives which was held to clarify several issues in U.S. EPA' s
December 7, 1994 transmittal on the PreFinal Design Report.
• On December 12, 1994, the Group received U.S. EPA comments on the responses prepared by DERS to the
first set of U.S. EPA comments on the report entitled, "Macon Dockery Site -Bioremediation Pilot Study
Interim Report".
On December 19, 1994, the Group submitted responses to U.S. EPA comments on the PreFinal Design
Report prepared by RMT, Inc.
On December 19, 1994, DERS began implementation of the bioremediation field demonstration program in
the MW-09 area located in the Upper Macon portion of the site.
• •
Ms. Giezelle Bennett.
January 9, 1995
Page 2
TASKS PLANNED FOR .JANUARY 1995:
• The Group anticipates receiving U.S. EPA approval of the Group's responses to the agency comments on
the Prefinal Remedial Design deliverables submitted on December 19, 1994.
The Group's consultant, RMT, Inc., will submit the Final Design documents following receipt of U.S. EPA
approval.
The Group will submit responses to the second set of U.S. EPA comments for the report entitled "Macon
Dockery Site -Bioremediation Pilot Study Interim Report" on January 13, 1995.
DERS will continue the Task 3 laboratory evaluation activities for assessing the viability of groundwater
bioremediation at all other source areas as outlined in DERS proposal attached to the September, 1994
monthly progress report.
DERS will continue the introduction of nutrients in the MW-09 location of the Upper Macon area of the site
for enhancing bioremediation of the constituents of concern. Sampling for Total Organic Carbon (TOC) and
Chemical Oxygen Demand (COD) to determine that adequate substrate amendment levels are maintained will
be performed along with the sampling for VOC constituents to determine the degree of enhancement of
biodegradation that may be occurring.
PROBLEMS AND DELAYS:
None.
If there are any questions, please do not hesitate to contact me at 219-239-0195.
Very truly yours,
d CM~_;J/,yzt7Z~
David L. Jones
Project Coordinator
Macon/Dockery Technical Committee Chairman
DU:ns
cc: Macon Dockery Site Group Members
Wayne F. Barto, de maximis, inc.
Paul Furtick, RMT, Inc.
Kevin White, DERS
• • Macon/Dockery Site
Richmond County, North Carolina
RECEIVF.D
DEC 1 4.1994
December 9, 1994
Ms. Giezelle Bennett
Remedial Project Manager
U.S. EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
Reply to: Tec.~~§~F~~~m3.~t:Te'e~1
c/o David L. Jones
Clark Equipment Company
P. 0. Box 7008
South Bend, IN 46634
Phone: [phone]
Fax:.[phone]
RE: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress Report -November 1994
Dear Ms. Bennett:
On behalf of the Macon/Dockery Site Group ("Group") the November 1994 Monthly Progress
Report is herewith submitted in accordance with Section XV -PROGRESS REPORTS of the
Unilateral Administrative Order (effective date -June 30, 1992) for the Macon/Dockery Site.
This report describes those activities which occurred during the month of November as part
of the Remedial Design and Waste Removal for this project.
PROIECT TASKS INITIATED OR COMPLETED THROUGH NOVEMBER 1994:
Results of Sampling and Testing and Other Data Received:
• Results of laboratory analytical data received during November 1994 for groundwater
samples collected from monitoring wells in the MW-09 vicinity have been previously
transmitted to the U.S. EPA with the DERS response to comments dated November 30,
1994.
Plans. Reports. Deliverables and Procedures Completed
• Nu-Way Environmental, Inc. (remedial contractor) completed the final off-site shipment
and disposal of soils associated with the vats and tanks. The final fieldwork activities
were completed on November 16, 1994.
• Approximately 22.7 tons of nonhazardous debris from drum consolidation activities
were shipped to the BFI Subtitle D Landfill in Charlotte, N.C. Approximately 1,414
tons of petroleum contaminated soil and debris (nonhazardous) from vessel removal
activities were also shipped to Laidlaw's landfill in Pinewood, S.C. The work areas
were graded and seeded to restore vegetation.
• •
Ms. Giezelle Bennett Page 2 December 9, 1994
• On November 16, 1994, the Group received U. 5. EPA comments on the report prepared by DERS entitled, "Macon Dockery Site -Bioremediation Pilot Study Interim
Report."
• On November 30, 1994 the Group responses to U. 5. EPA comments on the aforementioned report were submitted to U. 5. EPA.
• DERS continued to prepare for implementation of the bioremediation field
demonstration program in the MW-09 area located in the Upper Macon portion of the site.
TASKS PLANNED FOR DECEMBER 1994:
• The Group anticipates receiving U. 5. EPA comments on the Prefinal Remedial Design deliverables submitted on November 1, 1994.
• The Group's consultant, RMT, Inc., will develop responses to address U. 5. EPA's comments on the Prefinal Design documents.
• The Group also anticipates receiving U. 5. EPA comments on the submittal made to U. 5. EPA by DERS on November 30, 1994. As indicated previously in this Monthly Progress Report, this submittal contains responses to the initial U. 5. EPA comments on the report entitled, "Macon Dockery Site -Bioremediation Pilot Study Interim Report."
• The Group will respond to the second set of U. 5. EPA comments for the aforementioned bioremediation report prepared by DERS, or depending on the nature and extent of the comments, it may be advantageous to conduct a meeting between
U. S. EPA and their technical reviewers and the members of the Group Technical
Committee and their consultants.
• DERS will continue the Task 3 laboratory evaluation activities for assessing the viability of groundwater bioremediation at all other source areas as outlined in DERS proposal attached to the September 1994 monthly progress report.
• DERS will continue preparation for installation of the nutrient amendment wells and the introduction of nutrients in the MW-09 location of the Upper Macon area of the site. This will allow commencement of the field demonstration testing and nutrient
amendment addition for enhancing bioremediation of the constituents of concern in th is area.
• •
Ms. Giezelle Bennett Page 3 December 9, 1994
PROBLEMS AND DELAYS:
• None.
If there are any questions, please do not hesitate to contact me at [phone].
Very truly yours,
David L. Jones
Project Coordinator
Macon/Dockery Technical Committee Chairman
lb
cc: Macon/Dockery Site Group Members
Wayne F. Barto, de maximis, inc.
Paul Furtick -RMT, Inc.
Kevin White, DERS
•
Macon/Dockery Site
Richmond County, North Carolina
September 9, 1994
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
Reply to: Technical Committee
c/o David L. Jones
Clark Equipment Company
P. 0. Box 700_8
South Bend, IN 46634
Phone: [phone]
Fax: [phone]
RE: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress Report -August 1994
Dear Ms. Bennett:
On behalf of the Macon/Dockery Site Group ("Group"), the August 1994 Monthly
Progress Report is herewith submitted in accordance with Section XV -PROGRESS
REPORTS of the Unilateral Administrative Order (effective date -June 30, 1992) for the
Macon/Dockery Site. This report describes those activities which occurred during the
month of August as part of the Remedial Design and Waste Removal Phase of this
project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH AUGUST 1994:
Results of Sampling and Testing and Other Data Received:
• RMT provided final cPAH analytical results for the confirmation samples for
Lagoon 1 O to U.S. EPA under separate cover dated August 31, · 1994. A
request for U.S. EPA approval to backfill Lagoon 1 o with clean fill was
included in this correspondence.
• A summary of results for Tracer Test #3 performed by DERS as part of the
Bioremediation Pilot Study is provided herewith as Attachment 1 .
Plans, Reports, Deliverables and Procedures Completed
• Nu-Way Environmental, Inc. (remedial contractor) continued with waste
consolidation and removal activities at the site, including:
Shipping approximately 1,261 tons of hazardous waste from Lagoon
10 offsite to Laidlaw's Pinewood, South Carolina, Subtitle C lan.dfffC
Shipping approximately 993 tons of non-hazardous waste offsite to
BFl's Harrisburg, North Carolina, Subtitle D landfill.
' ..
Ms. Giezelle Bennett
September 9, 1994
Page 2 of 3
ce
Consolidation and characterization of waste oil from tanks.
Completion of tank decommissioning activities.
Completion of consolidation activities for RI-generated wastes.
Treatment of 22,000 gallons of contaminated water from results and
drums via carbon adsorption, and discharge of treated water to the
city of Rockingham POTW.
• Dupont Environmental Remediation Services remobilized to the site on
August 2, 1994 to implement the Tracer Test #3 work as approved by
U.S. EPA. A summary of the results is included as Attachment 1 to this
report. A proposed additional scope of work is included as Attachment 2.
TASKS PLANNED FOR SEPTEMBER 1994:
• Continue waste removal activities in accordance with the U.S. EPA-
approved Workplan.
• Excavate, characterize, and dispose of oil-stained soils under vessels, as
described in the approved Work Plan.
• Implement the additional work proposed by DERS. Ders is scheduled to
mobilize to the site to implement the work on September 20, 1994.
• Continue developing the Prefinal Design for the groundwater remedy.
• Continue developing the Operations and Maintenance Plan and Manual for
the SVE and groundwater remedy.
PROBLEMS AND DELAYS:
• The results of DERS tracer test #3 indicated that the hydrogeology of the
site in the Upper Macon area is significantly more complex than previously
indicated. The additional field work proposed by DERS will provide
sufficient information to allow a determination if similar conditions exist .
elsewhere on the site. Additional time will therefore be required to
complete the entire bioremediation pilot study in accordance with the
schedule included in Attachment 2.
..
Ms. Giezelle Bennett
September 9, 1994
Page 3 of 3
If there are any questions, please do not hesitate to contact me at 219-239-0195.
Very truly yours,
£) c;w,.c/ ~-~ ov --?!~
David L. Jones
Project Coordinator
Macon/Dockery Technical Committee Chairman
WFB/jca
Attachments
cc: Macon/Dockery Technical Committee Members
Wayne F. Barto, de maximis, inc.
Paul Furtick, RMT, Inc.
tprojects\3068\mpraug.94
..
Date:
Well Installation:
Groundwater Levels:
Summary of Results
Tracer Test #3
Upper Macon Area, near MW-09
August 31, 1994
de maximis, inc.
SEP O 7 1994
RECEIVED
One shallow and five deep piezometers were installed in the
study area during the week of August 1, 1994. Well construction
details are summarized below:
Well # Total Depth Screened Interval (feet
(feet below grade) below grade)
PM-7 50 40-50
PM-7A 66 56 -66
PM-lA 71 56 -71
PM-4A 60 55 -60
PM-6A 80 60 -80
PM-9A 70 55 -70
The shallow well, PM-7, was installed to a depth of 50 feet to
corresponded with the depths of the other shallow wells in the
monitoring array. The deep wells were installed to the top of
bedrock and screened in the partially weathered rock zone. The
subsurface was composed of an upper sedimentary unit, 15 to 20
feet thick, composed of clayey sand and quartz gravel
(Middendorf Formation) which was superimposed on five to ten
feet of red-brown saprolite derived from chemical weathering of
. the underlying bedrock. The saprolite graded downward into
very hard partially weathered rock (PWR) which exhibited relict
granitic texture, as well as, residual fracture zones in both
vertical and sub-horizontal orientations. Competent bedrock,
consisting of gray and black crystalline igneous rock, was
encountered at depths ranging from 60 (PM-4A) to 80 (PM-6A)
feet below grade. Soil boring logs are included as Appendix A.
The locations of the piezometers are. shown in Figure 1.
The location and elevation of each piezometer was surveyed·
following completion of each well. The well elevations are
recorded on the well construction logs included as Appendix B.
Depth to groundwater measurements were recorded in the
monitoring array and area monitoring wells prior to installation
of the new wells. Water level measurements were also recorded
PM-1A p
36.00
PM-1
34.00 ◊
32.00
30.00
p -3 PM-4
28.00 ◊
26.00
24.00
22.00·
PM-5 PM-6
20.00 ◊ ◊
8.00 10.00 12.00 14.00 16.00
PM-4A
◊
MW-9A
◊
MW-9
◊
PM-6A
18.00 20.00 22.00 24.00 26.00 28.00
p ~7
PM-7A
◊
30.00 32.00
Figure 1
Piezometer Location Map
Upper Macon Site
Scale: l" = 4 feet
•
:e
•
Summary of Results
Tracer Test #3
Upper Macon Area, near MW-09
Page 2
Slug Tests:
Tracer Test:
following the tracer test. The calculated groundwater elevations
are summarized in Table 2 and a groundwater elevation contour
map is included as Figure 2.
Slug tests (falling head) were performed in PM-6A and PM-9A
on August 8, 1994. Analysis of slug test data for PM-9A
indicated a hydraulic conductivity of 3. 3 x 10-4 ft/min. The
water level in PM-6A recovered too quickly for accurate data
evaluation.
The tracer test was conducted August 8 through 10, 1994
following collection of background samples from each of the
study area wells. Each of the samples was analyzed for the
presence of Rhodamine WT (rhodarnine), and all samples
exhibited less than one part per million (ppm) of this compound.
A tracer mixture consisting of 2,000 ppm rhodamine in 55
gallons of water was introduced into MW-09 at 3 pm on August
8, 1994. The tracer drained completely into the well in 1.25
hours. The water level in the well returned to static level less
than 2 hours after injecting the tracer.
Water samples were collected from PM-1, PM-lA, PM-4, PM-
4A, PM-6, PM-6A, PM-7 and PM-7A five to ten minutes after
completing tracer injection. Groundwater collected from PM-9A
and PM-4 exhibited strong pos1uves (pink color).
Spectrofluorometric analysis of the remaining samples indicated
positive results for PM-4 (1990 ppm), PM-9A (552 ppm) and
PM-6A (22.5 ppm). Analytical results for this and subsequent
sampling events are summarized in Table 3.
Three additional sampling events involving the above-listed wells
and MW-09 were conducted over the next 48 hours. Positive
results were recorded in MW-09, PM-4 and PM-9A through
August 9, 1994. Positive results above background levels were
not recorded in PM-6A after the initial sampling event. The
concentrations of rhodamine decreased to below background
levels in MW-9A by August 10, 1994.
All of the wens· in the array, including PM-2, PM-3, and PM-5
were sampled on the fourth sampling event. As noted in Table. 3,
no positive results were recorded for these wells. Samples from
AUGWL.XLS
TABLE 2
MACON-DOCKERY TRACER TEST
WATER LEVEL DATA SUMMARY
Elev. 8/8/94 8/8/94 8/1 0/94 8/1 0/94
Well No. TOC DTW GW Elev. DTW GW Elev.
PM·l 252.95
PM-lA 253.88
PM-2 251.93
PM-3 251.78
PM-4 252.99
PM-4A 253.38
PM-5 251.92
PM-6 252.84
PM-6A 252.11
PM-7 251.22
PM-7A 251.48
MW-09 254.08
PM-9A 254.43
MW-3 220.67
MW-19 236.89
MW-5 234.51
MW-8 234.54
MW-SA 234.44
MW-2 231.39 3 a. 15 %M!ltli!Zl.fi4
MW-2A 230.83
MW-10 265.1
Page 1
Table 3
Tracer Test, Results
Macon-Dockery Site
Well Background
8/8/1994 13:0
Blank # 3.31
PM-1 0.9
PM-1A 0.713
PM-4 0.658
PM-4A 0.659
PM-6 0.792
PM-6A 0.698
PM-7 0.532
PM-7A 0.613
MW-9 0.769
PM-9A 0.609
Notes: # =
NS=
+ =
• =
CHEM.XLS
Sample event Sample event Sample Event Sample event
8/8/94 1 6 :00 8/9/94 04:00 8/9/94 15:00 8/10/1994 +
3.60 0.67 1.29 1.76
NS 0.72 1.37 1.75
3.6 1.37 8.7 1.52
1990 1280 5530 4780
0.91 0.794 3.77 1.43
NS 4.9 5.51 3.61
22.5 2.08 3.33 5.33
0.744 0,755 1.62 2.51
0.658 0.846 1.15 1 .35
200000 125000 157000 58400
552 48.7 21.1 2.05
Blanks consisting of distilled water were prepared for comparison
for each sampling event. Blank concentration vary according to the
calibration setting (high, med. low) of the instrument
No sample collected
8/10/94 sampling event also included PM-2, PM-3 and PM-5
no positive results ( > 1 ppm) were recorded for these samples
Sample event
8/12/1994 •
1.50
NS
NS
450
NS
NS
NS
NS
NS
5230
NS
8/12/94 sampling event also included MW-3, MW-18, MW-7 and
MW-BA, no positive results. ( > 1 ppm) were recorded for these samples
Page 1
' -• •-••-••• ......... , .... •-••••M~~----••-•-•-•••••••• .... •••·••••uC,-··' ½-•• . ,,._,,,_.,, •• •-4--•• •·• • ..., •.• hd•,•~• ,._, ........... • Summary of Results
Tracer Test #3
Upper Macon Area, near MW--09
Page 3
MW-09 and PM-4 continued to show elevated, but decreasing
concentrations of rhodamine.
The injection well (MW-09) and PM-4 were sampled again on
August 19, 1994 along with downgradient monitoring wells MW-
19, MW-3, MW-5 and MW-SA to determine if the tracer had .
migrated to these locations. Positive, but significantly
decreased, readings were noted in samples from MW-09 and PM-
4. There were no positive readings ( > 1 ppm) for any of the
downgradient wells.
Summary and Conclusions: Soil borings indicate the presence of residual fractures m the
partial! y weathered rock zone.
Depth to competent bedrock is variable in the vicinity of the test
wells.
Water level measurements in the well pairs indicate the presence
of downward vertical gradients which tend to exceed the
horizontal hydraulic gradient in the vicinity of MW-09.
Rapid detection of the tracer injected at MW-09 in samples
obtained from PM-9A indicate that a portion of the groundwater
travels quickly along a vertical path.
Rapid detection of the tracer injected at MW-09 in samples from
PM-4 indicate a portion of the groundwater travels along a
horizontal path probably in a diffuse manner.
The tracer dissipated quickly in samples collected at PM-9A and
PM-6A and much more slowly in samples from PM-4. It appears
that groundwater moves faster in the lower PWR zone than in
the saprolite/upper PWR zone.
•
Appendix A
Soil Boring Logs
• Soil Boring Log
Project Project Number: Boring Number: Page __ of __
Name/Location: 31040 04 PM-7
Macon-Dockery
Cordova, NC
Land Owner: Macon Driller/Contractor Start: 8/2194 Finish: 8/2194
Mark Geel. Expl.
Geologist: Instrument: Pl D Time: 11 am Time: 14:15
M. Gauthier
Sample Sample Description of materials and conditions Instrument
No. Depth reading/observations (parts
(feet\ per million)
1 S -1 Red-brown clayey sand, dry 0.1
2 IO -12 Red-brown clayey sand, dry crumbly 0.1
3 IS -17 Red-brown clayey sand with rounded quartz 0.1
cobbles
4 20-22 Red-brown, mottled white clayey silt (saprolite), 0.4
dry and dense)·
s 25 -27 As above 0.1
6 30-32 As above 0.1
7 35 -37 Yellow brown/yellow/black mottled saprolite with 1.0
horizontal mineralized fracture zone
8 40-42 Green-blue and purple clay, wet and soft 0.7
9 45 .47 As above to 44.5 ft, then yellow brown PWR, 0.7
crumbles easily, moist to wet
10 SO-S2 Yellow clayey sand (PWR) with black mineralized 0.3
45 degree fractures.
Total depth = 52 feet, set PM-7 base at 50 feet
Groundwater encountered about 41 feet
--------------------------------·-······--·---··--------• (. Soil Boring Log
Project Project Number: Boring Number: Page __ of __
Name/Location: 31040 04 PM-7A
Macon-Dockery
Cordova, NC
Land Owner: Macon Driller/Contractor Start: 8/2/94 Finish: 8/2/94
Mark Geol. Expl.
Geologist: Instrument: PID Time: 13:50 am Time: 16:05
M. Gauthier
Sample Sample Description of materials and conditions Instrument No. Depth reading/observations
No sample to 45 feet 0.7
I 45 -46.5 Yellow-brown/white saprolite/PWR (clayey silt), 0.5
wet
2 46.5 • 48 No recovery (very hard layers) 0.3
3 48 • 49.5 Yellow-brown/white PWR w/ vertical black stained 0.3
residual fracture zones, wet
4 49.5 • 51 As above, wet 0.3
5 51 • 52.5 As above, wet 0.3
6 52.5 • 54 Mottled yellow-brown with dark black PWR with 0.3
horizontal fracture zone (0.2 ft thick), wet
7 54 • 55.5 As above, wet 0.3
8 55.5 -57 As above with sub vertical black stained fracture 0.3
zone 0.1 ft wide, wet
9 57 • 58.5 As above, with higher percentage of quartz, wet 0.2
10 58.5 • 60 Yellow-brown and black PWR (sand size residual 0.2
crystal shapes), crumbles easily, wet
II 60 • 61.5 As above with 0.1 ft wide 20 degree sub horizontal 0.3
fracture zone, wet
12 61.5 -63 As above with 0.05 ft wide fracture zone, wet 0.2
13 63. 64.5 As above with clayey residual fracture zone about 0.2
0.3 ft thick at 40 degree angle, wet
14 64.5 -66 As above (PWR) 0.2
15 66 Hard drilling, no penetration, black crystalline rock
chips recovered from base of split spoon.
Auger refusal at 66 feet
Total depth = 66 feet, set PM-7 A in boring
• Soil Boring Log
Project Project Number: Boring Number: Page __ of __
Name/Location: 31040 04 PM-1A
Macon-Dockery
Cordova, NC
Land Owner: Macon Driller/Contractor Start: 8/4/94 Finish: 8/4/94
Mark Geel. Expl.
Geologist: Instrument: PID Time: 8 am Time: 10:25
M. Gauthier
Sample Sample Description of materials and conditions Instrument
No. Depth reading/observations
No samples to 50 feet, hard drilling 25 to 50 feet
I 50 • 51.5 Yellow/brown/blk mottled PWR (clayey sand), wet 0.2
2 55 • 56.5 As above with 0.05 ft horizontal and 20 degree sub 0.2
horizontal fractures
3 60 • 61.5 As above with 0.1 ft ·dark gray crumbly rock 0.2
4 65 • 66.5 As above 0.2
5 70 • 71.5 As above to 71 feet, dark black and gray crystalline 0.2
rock at base
Auger refusal at 71 feet
TD = 71 feet, PM-lA set at base of boring
• Soil Boring Log
Project Project Number: Boring Number: Page __ of __
Name/Location: 31040 04 PM-4A
Macon-Dockery
Cordova, NC
Land Owner: Macon Driller/Contractor Start: 8/3/94 Finish: 8/3/94
Mark Geel. Expl.
Geologist: Instrument: PIO Time: 14:15 am Time: 16:15
M. Gauthier
Sample Sample Description of materials and conditions Instrument
No. Depth r reading/observations
No samples to 50 feet
1 50 -51.5 Mottled yellow-brown and tan w/ black saprolite, 0.2
horizontal fracture zone (0.05 ft thick), wet
2 55 -56.5 Mottled yellow-brown and tan PWR (sand), 0.2
crumbles easily, vertical iron stained fractures, wet
3 60 -61.5 Rock, dark black with white crystals 0.2
Auger refusal at 60 feet
TD = 60 feet, PM-4A set at base of boring
• Soil Boring Log
Project Project Number: Boring Number: Page __ of __
Name/Location: 31040 04 PM-9A
Macon-Dockery
Cordova, NC
Land Owner: Macon Driller/Contractor Start: 8/4/94 Finish: 8/4/94
Mark Geol. Expl.
Geologist: Instrument: PID Time: 14:15 am Time: 17:05
M. Gauthier
Sample Sample Description of materials and conditions Instrument
No. Depth readlng/observatlons
No sample to 50 feet
I so -51.5 Yellow-brown/white saprolite/PWR (clayey silt), 0.2
wet
2 55 -56.S As above 0.2
3 60 -61.5 (0.3 ft recovery) black and white mottled PWR 0.2
with wide (0.2 ft) black stained fracture zone, wet
4 65 -66.S Yellow-brown and black mottled PWR (clayey 0.5
sand) with black stringers, wet
s 70 -71.5 As above, with more sand sized crystals and large 0.2
rock fragments, wet
Auger refusal at 70 feet
Total depth of boring= 70 feet, set PM-9A in
boring
• Soil Boring Log
Project Project Number: Boring Number: Page __ of __
Name/Location: 31040 04 PM-6A
Macon-Dockery
Cordova, NC
Land Owner: Macon Driller/Contractor Start: 8/5/94 Finish: 8/5/94
Mark Geol. Expl.
Geologist: Instrument: PIO Time: 13:00 Time: 16:45
M. Gauthier
Sample Sample Description of materials and conditions Instrument
No. Depth reading/observations
No samples to 50 feet, hard drilling 25 to 50 feet
I so -51.S Yellow/brown/blk mottled PWR (clayey sand), wet 0.3
2 SS -56.S As above 0.2
3 60 -61.S As above, becoming more sandy and crumbly 0.3
4 65 -66.S Very little recovery (0 .1 ft), as above with dark 0.2
grey rock fragments
s 70 -71.5 As above with 0.05 ft wide 75 degree residual 0.2
fracture zone in PWR
6 75 -76.S Black and yellow mottled PWR (clayey sand) 0.2
7 80 -81.S No recovery
Auger refusal at 80 feet
TD = 80 feet, PM-6A set at base of boring
•
Appendix B
Monitoring Well Construction Details
•
l.'ELL NC.
TOP OF R!SC:R ELEV.;Tr□N, :JS i. °;?52,
••
•
• • • •• . . . • '
-----1----1/ATER-T!Gi-lT CA? • -~.4---FLUSH GR.;DE YELL CONSTRUCTION •
0
•
'
DIAMETER !. M:. TE:RIAL
TOTAL LENGTi-1
LENGTH BELO\/ GROUND
~_.:,._§,:~---,--THICKNESS!. TYPE OF SEAL
.,._, _____ DIAMETER, MATERIAL I. JOINT TY?E
OF RISER PIPE
TYPE OF BACKFILL AROUND RISER
'-----THICKNESS!. TYPE OF SEAL
DISTANCE OF FILTER SAND :.3CVE TOP OF SCREE:N
TYPE OF FILTER AROUND SCREC:N
1----'-----YELL SCREEN HA TERIAL
SCREEN GAUGE OR SIZE: OF C?EN,NG
<SLOT SIZ:J
1--..-:.-----DIAHETER !. LENGTH OF SCREEN
J-___ _;_-1-_ V----'-----DEPTH TO THE BOTTOM OF
YELL
DEPTH TD B □TTOH OF FILTER SAND
THICKNESS!. TYPE OF SEAL
DIAMETER OF B□REn□LE
RECGVERY '•E:LL II A TE.~ LEVEL
I 'Z ,, s-k..... /
IZ I/
'"R,.,.,c""'°" . .k.. pxl l., ;!.
;J_ {j..
:':?"---:\ d
Wr~J
no r,,o,,
Cz 25" I/
HEASURE!-iE:~TS I L1 =------FT
L2 = FT DATE I T!.~£ I l.'ATER L£V::L JI I
L 3 = IQ FT
L4 -_ __,G"-'0"'----FT
I I I
I I I
I I
'
.. -----------------------------·-· • i.
PROJECT• ~{\l\~~4-< ~9~"'-~J)~.,o.,r..,"'6=,_,,,,'------
JOB NO. _3d-'-') Q_L..~{~Q"'-'j..__ __ J ___ _
\,/ELL NC. J M_ -]
TOP OF RISER ELEVA TIQN, ")._ 5 (. d-'-f
-
• • •• . . .
• -1-... • ,---~-+----\I ATER-TIGHT CA? • -!i;;-:r't----FLUSH GRADE \/ELL CONSTRUCTION •
0
• •
DIAMETE:R &. MA Ei<IAL
TOTAL LENGTi-;
LENGTH BEL□V Gi<OUND
~--,-~~---THICKNESS&. TYPE OF SEAL
~-+-----DIAMETER, MATE:RIAL &. JOINT TY?E
OF RISEi< PIPE
TYPE OF BACKFILL AROUND RISE:i<
:;>-o-----THICKNESS !. TYPE OF SEAL
---DISTANCE OF FILTER SAND A3CVE: TOP
CF SCREE:N
TYPE OF FILTE:R AROUND SCREEN
-------\/ELL SCREEN MATE:RIAL
---+-----SCREEN GAUGE OR SIZE OF C?EN!NG
<SLOT SIZE>
,---;.--,-----DIAMETER &. LENGTH OF SCREEN
-'-----4--v---,-----DEPTH TO THE BOTTOM OF
\/ELL
DEPTH TO BOTTOM OF FILTE:i< SAND
THICKNESS &. TYPE OF SEAL --·-
----,------+-----DIAMETEi< OF BOREHOLE
RECGVERY 'J:'.LL VA T"R LEVEL
,,
2 '' ~.,{" '"' less ·
:<,k{' [..,s l-. -1-\-,,~
0 '-9:--i c.., .,.,._,_,,,_-{..
~rou ~
-:&, "'-+o V\. I .j._ ~ ( (,,-l .
3 ~)-
;J,'' 10 ~ J
so£~
5nC.
MEASURE!-1E:STS I L1 =------FT
L2 = FT DATE: I T!.~E I \IATEi< LEVEL " I
L3 = / 0 FT
L • = --•-2'~0~---FT
I I I
I I I
I I
I I '
I I --··-· ;
•
PROJECT• _,_d...J.!!.."CO"'-~•...:.:Ll::....:o:.::c.::.:..:L-=_-::/-f----lo/ELL NC.
J□B No. _3...,_,_,1 o"--4..J-...l·o..'.,,_/,.J_1 ______ _ TOP OF RrSER ELEV A TICN• '.J5'-f-53
2
•• . 0 • • •
• • • ••
•
' \/ELL CONSTR!JCTlON ' . ,
DIAMETER !. MATERIAL
0
TOTAL LENGTH .. LENGTH BELOV • GROUND
THICKNESS !. TYPE OF SEAL
I--+-----DIAMETER, MATERIAL !. JOINT TYPE
OF RISER PIPE
TYPE OF BACKFILL AROUND RISE.R
~------THICKNESS !. TYPE OF SEAL
DISTANCE OF FILTER SAND A3.::VE
OF SCREEN
TYPE OF FILTER AROUND SCREEN
~------\/ELL SCREEN MATERIAL
.. _......, _____ SCREEN GAUGE OR SIZE OF CPENING
(SLOT SIZE)
i---:.-----DIAMETER !. LENGTH OF SC.~EEN
.._ ____ _,___ V---..:....-----DEPTH TO THE BOTTOM OF , I VELL
•-------!-~.•----DEPTH TO BOTTOM OF FILTER SAND _ ~-THICKNESS!. TYPE OF SEAL
DIAMETER OF BOREHOLE
;j;t i;'' oLl
..Jr; l-'t'+
;;J f+-Co~c,,:.,k
1 '. . ":>±½ ;,,_ C.. s s
~( f(":, I... "+-\,,r~c J
/1,p;t ~+ 6,o, 1-
W r LH. J £.:f.,,4ss
~(
0 010
70.C+
nol'.':,L,-
r s'' Q, z_
L 1 -------FT RE:CGVERY 'JS.LL v,; 7E:R LEVE!.. MEASURE!-1E~TS I
L2 -FT
L3 -/5: FT
L. = _7.i;Cl,L) __ _ Fi
DATE I T!"'~ I \/ATER LEVE!.. " I
I I I
I I I
I I
I I '
IN~T ,!,LLA T~~) ?GHF!...::T:::J1
DA TE• "'Of'(f'i'{
I I ,,, ·-··-· ;
TI)-!E, _______ _
\JELL NC.
TOP OF RISER El.EVA T!ON• ')_ 5 °2>. f2J_
••
•• • •
• •• ••
• •
I
I
I
I
I
I
I
~--l:lt--1----VATER-TIGHT CA?
-~.+---FLUSH GRADE VELL CONSTRUCTION •
0
• •
DIAMETER !. MATERIAL
TOTAL LENGTH
LENGTH BELDV GROUND
~_:,..&~---THICKNESS !. TYPE OF SEAL
i--1------DIAMETER, MATERIAL !. JOINT TYPE
OF RISER PIPE
TY?E OF BACKFILL AROUND RISER
THICKNESS!. TY?E OF SEAL
DISTANCE OF FILTER SAND A3i:VE TOP
OF SCREEN
TYPE OF FILTER AROUND SCREEN
-~-----VELL SCREEN MATE.~IAL
SCREEN GAUGE DR SIZE OF C?ENlNG
<SLOT SITE)
1--......:..-----DIAMETE.~ !. LENGTH OF SCREEN
-'----~-'--V-------------DE?TH TO rnE BOTTOM OF . I VELL
.L
------I-· .• ____ DE?TH TD BOTTOM OF FILTER SAND ~-THICKNESS!. TYPE OF SEAL
DIAMETER OF BDR:::-i□LE
Z II
I f;JtO,, .:,_ (_, :sS
5kg !J +l.u::,h, <\.irrrec-
~+ ~.J-
<Ou -i-
.{2,""--s: l,c. <,.....
Sc..."'-J
~tw4~1v-.b
0.0(0
}
71 ft-
71 t-1-
C 7 -,, ._.5
L 1 = FT
Lz-------FT
L3 = /5" FT
Li:vEL HEASURE~ENTS
DATE I TI.~E I VATER LEVEL "
L4 = _]...µ./ ____ FT
•
\JELL NC.
TQP OF R!SC:R ELEVA Tl□N• ;:;2. 5 J. (./·($
. 0 • • •
•
0 • 0.
~--~-!----\/ATER-TIGHT CA?
-~.4---FLUSH GRADE \/ELL CONSTRUCTION
0
0
• •
DIAMETE:R &. MA TC:.RIAL
TOTAL LENGTH
LENGTH BELO\/ GROUND
..__;:;,,_--' •_j----THICKNESS !. TYPE OF SEAL
'--+-----DIAMETER, MATE:RIAL &. JD!NT TYPE
OF RISER PIPE
TYPE OF BACKFILL AROUND RISC:R
,?-.,.....----THICKNESS!. TYPE OF SEAL
DISTANCE OF FIL TE:R SAND A::!CVE: TOP
OF SCREEN
TYPE OF FILTE:R AROUND SCREC:N
~------\/ELL SCREEN MAT~RIAL
=--+------SCRESN GAUGC: DR srz::: □F OPENING
(SLOT SIZ::)
1--..-....-----D!AMETER I. LENGTH OF SC.~EEN
.._ ____ ..__ \.,:-_ _,_ ____ DEPTH TD THE BOTTOM OF
\/ELL
DEPTH TO BOTTOM OF FILTE:R SAND
THICKNESS!. TYPE OF SEAL -:'--·_
_____ ,__ ___ .....J _____ DIAMETER OF BORS:-i□LE
7h,,cyo,vk.. pd\..+
J. t-+
l,J~ $fr,._, "-(,_"?
0.010
(,_DI/
L1 =------FT RECCVS.RY 'JELL \/ATER LEVEL MEASURE!<ENTS I
Lz -FT
L3 = l FT
L • = -J.Jl&c1..flt__ __ FT
DATE: I T!l,,IC-I \/ATi:R LEVEL " I
I I I
I I I
I I '
'
•
'JELL NC. PR□JECT• -'""'Nk--"-'-'==. -'-'--=o:.._.,,_c..=k·=~...,1 __ _
JOB NO. ______________ _ TC!P OF R!SE:R El.EVA TIGN• 7-5'?.' I s::
Lz
••
0 •
•• : ..
r---!'<',--1----\IATER-TIGHT CA?
-:!t;,"t----FLUSH GRADE \IELL CONSTRUCTION •
0
• •
DIAMETER !. MA T:'.RIAL
TOTAL LENGTH
LENGTH BELO\I GROUND
~-,-~~---THICKNESS!. TYPE OF SEAL
,._-+-----DIAMETER, MATERIAL !. JDINT TY?E
OF RISER PIPE
TYPE OF BACKFILL AROUND RISER
-----THICKNESS!. TYPE OF SEAL
---DISTANCE OF FILTER SAND A3CVE TOP
OF SCREEN
TYPE OF FILTER AROUND SCREEN
f---:------\IELL SCREEN MATERIAL
.., _ _.,_ _____ SCREEN GAUGE: DR SIZE: OF C?E.'JiNG
<SLOT STI:'.)
,----;,--,-----DIAMETE.'< !. LENGTH OF SCREE::-1
~-----+-v-----t-----DE?TH TO THE: BOTTOM OF . . I \IELL
~-----,..·---
---------'------DIAMETER OF BOREHOLE
DEPTH TO BOTTOM OF FILTER SAND
THICKNESS g, TYPE OF SEAL
FT ~ECGVE.~Y 'J:'.LL VA7::~ LEVEL
:fr:d~Yt-
~ ~
l,1~QD.L sh,"'<a~
O.D/6
:2" aor~ )
79/ ..
D. ZS 11
H:'.ASURE:!<£ms L1 =
Lz = FT DATE: I T!'-'"" I \IATER L:'.V:'.!.. "
L3 -Zn FT
L• -~D FT
I I
I I
I I
I I
IN:_~MLLA mf ~!c~7E!l• D A I :.I ~!./5.. f..:1:::t_
I I ... .. --·-·
TI~E1 _______ _
North Carolina • Department of Envi.ent, Health, and Natural Resources
' Division of Environmental Management -Groundwater Sectio·n
P.O. Box 29535 · Raleigh, N.C. 27626-0535
Phone [phone]
WELL CONSTRUCTION RECORD
DRILLING CONTRACTOR: Geologic Exploration, Inc.
DRILLER REGISTRATION NUMBER: 1175
STATE WELL CONSTRUCTION
PERMIT NUMBER:
1. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Cordova County: ___ R_i_c_h_mo_n_d _______ _
State Road 1103
(Road, Community, or Subdivision and Lot No.)
2_ OWNER Macon Dockery
ADDRESS 5 Cheraw Road
Rockingham
{Street or Roule No.)
N.C. 28739
City or Town Stale Zip Code
3. DATE DRILLED· 8-5-94 USE OF WELL Monitor
4. TOTAL DEPTH 79.0 feet
5. CUTTINGS COLLECTED YES(!] NO □
6. DOES WELL REPLACE EXISTING WELL? YES O NOQ9
7. STATIC WATER LEVEL Below-Top of Casing: ___ FT.
8. TOP OF CASING IS 3. 5
(Use"+" if Above Top of Casing)
FT. Above Land Surface•
DEPTH
From To
0.0' 10.0'
10.0' 15.0'
15.0' 40.0'
40.0' 50.0'
50.0' 79.0'
• Casing Terminated at/or below land surface Is Illegal unless a variance Is Issued----------
In accordance with 15A NCAC 2C .0118
9. YIELD (gpm): N/A METHOD OF TEST _.,N,._/A"'-----________ _
10. WATER ZONES (depth):-~N~A~---------________ _
DRILLING LOG
Formation Description
Red Brown CLAY
White Quartz Cobbles
Red CLAY
Red CLAY with rock
fragments
Tan Gray Sandy CLAY
11. CHLORINATION: Type ~N=/~A~ ___ Amount N/A If additional space is needed use back of form
12. CASING:
LOCATION SKETCH
Depth Diameter
To 59.O Ft. 2 inch
Wall Thickness
or WeighVFt.
Sch.1O
Material (Show direction and distance from at least two State
stainless Roads, or other map reference points) From O.O
From----To---Ft.----
From To Fl.----
steel
13. GROUT:
Depth Material Method
From 0.0 To 55.O Ft. Portland/Bentonite slurry
From ___ To ___ Ft. __________ _
14. SCREEN:
Depth Diameter Slot Size Material
From 59.O To 79.0 Ft _2 __ in .• 010 in. Stainless steel
From __ To __ Ft. __ in. __ in. ____ _
From __ To ___ Ft. __ in. __ in. ____ _
15. SAND/GRAVEL PACK:
Depth Size Material
From 57 .0 To 79.O Ft. 20-60 Fine silica sand
From __ _ To ___ Ft. ___________ _
NC-tlv0
vs-1
16. REMARKS:_-=-P-"M'--6""A'-'--'B=e"-n,.,t=o-"n=-i t=-e'°-'pe==l=l-=e-=ts=--cf=r=orn~=-55=--•c.coc.....=t=o-=-57'-.'"'O'-"f=e=e-=t-'--. _____________ _
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL _
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIOED TO THE WELL OWNER.
8-24-94
DATE GW-1 REV. 9,91 Submil original to Division of Environmental Management and copy to well owner.
North Carolina • Department of Envi.ent, Health, and Natural Resources
' Division of Environmental Management • Groundwater Section
P.O. Box 29535 · Raleigh, N.C. 27626-0535
Phone [phone]
WELL CONSTRUCTION RECORD
DRILLING CONTRACTOR: Geologic Exploration,
DRILLER REGISTRATION NUMBER: 1175
1. WELL LOCATION: (Show sketch of the location below)
Inc.
STATE WELL CONSTRUCTION
PERMIT NUMBER:
NearestTown: Cordova, N,C,
State Road 1103
County: __ .....,R""i.,.c,..hino'"",..n.,,.,d~------
(Road, Convnunity, or Subdivision and Lot No.)
2. OWNER Macon Dockecy
ADDRESS 5 Cheraw Road
Rockingham
(Street or Route No.)
N.C. 28739
City or Town State Zip Code
3. DATE DRILLED 8-3-94 USE OF WELL Monitor
4. TOTAL DEPTH 60.0 feet
5. CUTTINGS COLLECTED YES O NO[!]
6. DOES WELL REPLACE EXISTING WELL? YES O NO[!]
· 7. STATIC WATER LEVEL Below-Top of Casing: ___ FT.
8. TOP OF CASING IS 2 • 5
{Use•+ .. if Above Top of Casing)
FT. Above Land Surface•
• C8slng Terminated aUor below land surface la Illegal union a variance la Issued
In accordance with 15A NCAC 2C ,0118
DEPTH
From
0.0'
7.0'
38.0'
To
7.0'
38.0'
60.0'
9. YIELD (gpm): NIA METHOD OF TEST _ __,N.,,/_.A,.._ ___________ _
10. WATER ZONES (depth): __ N=..,A"-----------________ _
DRILLING LOG
Formation Description
Red CLAY
Red Clayey SAND
Tan CLAY
11. CHLORINATION: Type --"N~/=A-~_ Amount -~N,,,/'--'A~ If additional space is needed use back of form
12. CASING: ==================
LOCATION SKETCH
Depth
From 0.0 To 55 .o Diameter
2 inch FI.----
Wall Thickness
or Weig!,l/Ft. Sch.10 Material (Show direction and distance from at least two State
stai~less Roads, or other map reference points)
From,----To---
From T0---
13. GROUT:
Ft.---
Fl..---
stee
Depth Material Method
From 0.0 To5l.O Ft.Portland Bentonite slurry
From ___ To ___ Ft. __________ _
14. SCREEN:
Depth Diameter Slot Size Ma1erial
From 55.0 To 60.0 Ft __ 2_ in. .010 in. stainless steel
From ___ To ___ Ft. __ in. __ in. ____ _
From ___ To ___ Ft. __ in. __ in. ____ _
15. SAND/GRAVEL PACK:
Depth Size Material
From 53.Q To 60 0 Ft. 2°=:60 Fine si 1 j ca sand
From ___ To ___ Ft. ___ _
lJS I
16. REMARKS:, __c.P!!M=-4~Ac:!...!B~e:!.n~t"'o!!n:.i t=:e:.....tape=l~l-=et=:s:......!f:::r_,,om~S~l,:.:.~0'.....!:te:o~5~3:'.:.~0~f-=e-=e.:.t_,_. ______________ _
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL-
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
8-24-94
GW-1 REV.9'91 DATE
Submit original to Division of Environmental Managemenl and copy to well Owner.
North Carolina -Department of Envir.nt, Health, and Natural Resources
' ' Division of Environmental Management -Groundwater Section
P.O. Box 29535 -Raleigh, N.C. 27626-0535
Phone [phone]
WELL CONSTRUCTION RECORD
DRILLING CONTRACTOR: Geologic Exploration,
DRILLER REGISTRATION NUMBER: 1175
Inc.
STATE WELL CONSTRUCTION
PERMIT NUMBER:
1. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Cordova County: ___ Rcci:...c:...hlno:....c:...n_d _______ _
state Raad 1103
(Road, Community, or Subdivision and Lot No.)
2. OWNER Macon Dockery
ADDRESS 5 Cheraw Road
(Street or Route No.)
Rockingham N.C. 28739
City or Town State Zip Code
3. DATE DRILLED· 8-3-94 USE OF WELLMonitor
4. TOTAL DEPTH 66.0 feet
5. CUTTINGS COLLECTED YES CT] NO □
6. DOES WELL REPLACE EXISTING WELL? YES O NO(!]
7. STATIC W_ATER LEVEL 8elow·Top of Casing: ___ FT.
8. TOP OF CASING IS 0.0
(Use~+~ if Above Top of Casing}
FT. Above Land Surface•
• Casing Terminated auor below land aurface la Illegal unless a varlanca Is Issued
DEPTH
From To
0.0' 12.0'
12.0' 15.0'
15.0' 41.0'
41.0' 66.0'
In accordance with 15A NCAC 2C .0118 ----------
9. YIELD (gpm): NIA METHOD OF TEST _...i:Nul..t1A~---________ _
10. WATERZONES(deplh): _ _.N!U:!A~---------________ _
DRILLING LOG
Formafon Description
Brown Red Clayey SAND
Red Clayey SAND with
white quartz cobbles
Red and Grey Clayey
SAND
Brown Black Clayey
SAND
11. CHLORINATION: Type _..,_N,_,/A"-~--Amount ~N.,,(c..,:A,___ U additional space ls needed use back of form
12. CASING: ==================
LOCATION SKETCH
Depth Diameter
From 0.0 To 56.0 Ft. 2 inch
Wall Thickness
orWeighVFI. Material (Show direction and distance from at least two State
stainless Roads, or other map reference points)
From----To---Ft.----
From To Fl.----
13. GROUT:
Sch.1O
steel
Depth Material Method
From 0.0 To 52.O Ft. Portland/Bentonite slur!-"Y
From ___ To ___ Ft. __________ _
14. SCREEN:
Depth Diameter Slot Size Material f'IC, \IU'3
From 56.O To66.O Ft _2 __ in .• 010 in. stainless steel
From __ To __ Ft. __ in. __ in. ____ _
From ___ To ___ Ft. __ in. ___ in. ____ _
15. SANO/GRAVEL PACK:
Depth Size Material
From 54.0 To 66.0 Ft. 2(r6O Fi.n.ee,,__,S"'1"'· l"'i,,_,c""a'-"S"'a""n"'d~
From ___ To ___ Ft. ___ _
16. REMARKS: PM-7A Bentonite pellets from 52.O to 54.O feet.
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL ...
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
Ml«,, :Ji;_,, 8-24-94
VSI
StGNAr6RE OF CONTRACQRORAGENT DATE
GW-1 REV. 9,9\ Submit original lo Division of Environmental Management and copy to well owner.
North Carolina• Department of Envir.nt, Health, ·and Natural Resources
Division of Environmental Management • Groundwater Section
P.O. Box 29535 . Raleigh, N.C. 27626-0535
Phone [phone]
WELL CONSTRUCTION RECORD
DRILLING CONTRACTOR: Geologic Explor-ation,
DRILLER REGISTRATION NUMBER: 1175
1. WELL LOCATION: (Show sketch of the location below)
Inc. fl-{e
STATE WELL CONSTRUCTION
PERMIT NUMBER:
NearestTown: Cordova, N.C. County; __ R""'-ic"'hrno'-""S<n,.d,,_ _______ _
State Road 1103
(Road, Community, or Subdivision and Lot No.)
2. OWNER Macon Dockery
ADDRESS 5 Cher-aw Road
(Street or Route No.)
Rockingham N.C. 28739
City or Town State Zip Code
3. DATE DRILLED · 8-4-94 USE OF WELL Monitor-
4. TOTAL DEPTH 71.0 feet
5. CUTTINGS COLLECTED YES [xJ NO□
6. DOES WELL REPLACE EXISTING WELL? YES O NO[RJ
7. STATIC WATER LEVEL Below-Top of Casing: ___ Ff.
8. TOP OF CASING IS 2.5
(Use·+· if Above Top of Casing)
Ff. Above Land Surface•
DEPTH
From To
0.0' 12.0'
12.0' 15.0'
15.0' 37.0'
37.0' 71.0'
• Casing Terminated at/or below land surface ls Illegal unless a variance Is Issued----------
In accordance with 15A NCAC 2C .0118
9. YIELD (gpm): N/A METHOD OF TEST _..,N,,_/..c,A,__ ___________ _
10. WATER ZONES (depth):---"N"-/-'-'A'----------________ _
DRILLING LOG
Formation Description
Red CLAY
Red CLAY with
white quar-tz cobbles
Red CLAY
Tan and Gr-ay CLAY
11. CHLORINATION: Type _.N.,L"A~~--Amount _N,.,.,,,-,(n.___ If additional space is needed use back of form
12. CASING: ==================
LOCATION SKETCH
Depth Diameter
From_o_. __ o __ To 56.O Ft. _2_i_n_ch_
Wall Thickness
or Weigt,l[Ft. Schau Material (Show direction and distance from at least two State stainless .
From,----TO---Ft.----
From To Ft.----
13. GROUT:
--,--...1-Roads, or other map reference points) stee
From 0.0
From
Depth Material Method 1 To 52.O Ft. Por-tland/Bentonite slur-ry
___ To ___ Ft. _____ _
14. SCREEN:
Depth Diameter Slot Size Material
From 56.0 To 71.0 Ft _2_ in. .010 in. stainless steel
From __ To __ Ft. ___ in. __ in. ____ _
From __ To __ Ft. __ in. __ in. ____ _
15. SAND/GRAVEL PACK:
Depth Size Material
From 54.0 To 71.0 Ft 20-60 Fine Silica Sand
From __ _ To ___ Ft. ___________ _
16. REMARKS:. _.::.P:.:M_-.::.lA:.:....:B:.:e:.:n:..:t:.:o:.:;n:.:i:.::t:.::e-"'pe::.l.::.l:.:e:.:t:.:s::.....:f:.:r-:.::om::::....:::5.::2.::.. O=-t:c:o::.....:5:...4:.:-:.::O:.....::f:.::e:.::e:.::t.:... ______________ _
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER.
8-24-94
GW·1 REV.9"31 DATE
Submit original to Division of Environmental Management and copy to well owner.
09/09/94 14:48
~
REGIONAL OPERATIONS• CHARLOTTE
OU PollT ENVIRONMENTAL REMEDIATION SERVICES
6324 Falr.iaw Road·
Charlotta, North Caronna 28210
(704) 362~630
[phone] Fax
September 8, 1994
Mr. Wayne Barto
de maxlmls, inc. -Suite 401
9041 Executive Park Drive
Knoxville, Tennessee 37923 ·
Dear Wayne:
DU PONT ENVIRONII (.
DuPont Environmental Remediation Services (DERS) is pleased to submit this
Scope of Work for the additional field activities associated with the evaluation of
· bloremedlation applicability to the Macon-Dockery site. We have prepared this
Scope of Work and budget based upon the technical committee conference call
conducted last Tuesday (23 August, 1994) and supplemented by the conversation
between Marilyn Gauthier and yourself Thursday (25 August, 1994). Based upon
these discussions DERS understands that the next work phase includes four tasks;
evaluation of flow from a selected group of existing site wells, gathering soil and
groundwater samples from areas of Upper and Lower Dockery and Lower Macon
that exhibit elevated concentrations of chlorinated aliphatic constituents of
concern, completion of bioremediation precursor studies upon the samples, and
completion of a field pilot bioremedlation test program based upon the success of
the preceding tasks.
The scope of each task is discussed below in greater detail. A schedule for
completion is attached.
TASK 1 Well Flow Ev.aluatlon
DERS will review the existing well installation data and select twelve site wells for
well flow characterization. As the purpose of this task is the identification of
additional bioremediation sites, only those wells previously exhibiting elevated
concentrations of chlorinated compounds will be considered for testing. The
characterization study will consist of applying a static water head (up to 40 feet)
by introducing 1 • 5 gpm of water into the selected wells. The cumulative h,eight
of any resulting water column in the well will be measured and the decay of the
water column will be monitored to evaluate the discharge flow capacity of the well
and the surrounding geology.
~001
. '
09/09/94 14:50 DU PONT ENVIROr.
Mr. Barto Page 2 September 8, 1994
The data gathered by these activities will be utilized to calculate the expected flow
rates through each study area. This information will be essential to the placement
and design of an efficient and effective · nutrient delivery system for any
bioremedial treatment applied at this site,
Should a suitable nutrient addition point be identified, DERS personnel will gather
samples from surrounding piezometers and wells. DERS is proposing that 14
surrounding piezometers or wells will be sampled. These samples will be analyzed
at a DuPont qualified laboratory to determine current (i.e., baseline) concentrations
of 1, 1, 1-and 1, 1, 2-TCA, 1, 1-and 1,2-DCA, PCE, TCE, cis and trans 1,2-DCE,
1, 1 -DCE, chloroethane, and vinyl chloride.
The deliverable from this task will consist of a written summary documenting the
activities conducted in the • field, presenting well flow and constituent
concentration data in tabular • format, and discussing the interpretation and
implications of well characterization data .
Based on 1993 analytical data, DERS has Identified the following piezometers and
wells for flow evaluation;
•
•
•
•
TASK 2
Upper Macon Wells; MW-05, MW-06, MW-08, MW-18, UMPZ-01,
UMPZ-02, PM-7, Pl\4-6, and PM-1,
Lower Macon Well, :MW-13,
Upper Dockery Well, MW-15, and
Lower Dockery Well, MW-16 .
Subsurface Sampling
DERS personnel will mobilize to: the field to gather soil and groundwater samples
from areas. of Upper and Lower Dockery and Lower Macon that have been
documented as exhibiting elevated concentrations of chlorinated aliphatic
constituents, namely, MW-13, MW-15, and MW-16, One groundwater sample will
be gathered from these existing monitor wells (total three samples). Soil samples
will be gathered from below the water table using hollow stem augers and split
spoon samplers at locations immediately adjacent (i.e., less than ten feet) to the
sampled monitor wells. All. soil and groundwater sampling activities will be
conducted in accordance with the procedures detailed in 31 May, 1994 Scope of
Work for the initial laboratory bioremediation pilot study. The samples will be
transported to the DuPont bioremediation laboratory located in Glasgow,
Delaware.
~002
. ' . 09/09/94 14:52 DU PONT ENV!RO.
Mr. Barto Page 3 September 8, 1994
TASK 3 Bioremediation Laboratory Pilot Testing
Personnel located at the DuPont bioremedlation laboratory will receive the soil and
groundwater samples gathered in Task 2, will prepare the samples for biological activity characterization testing, ·and will conduct the test program. All laboratory
activities for this task will be· conducted in accordance with the procedures
presented In the 31 May, 1994 Scope of Work discussing the initial laboratory
bioremediatlon pilot test; however, an additional focus of this laboratory study will
be the identification of alternative, lower cost nutrient mixtures. DuPont
laboratory personnel have Indicated that this study can be completed within ten weeks of soil and groundwater sample receipt.
The deliverable from this task will be a written summary of laboratory test findings including recommendations including the optimum microbe nutrient mixture(s) for use at the site.
TASK 4 Field Pilot Test of Anaerobic Dechlorination
At this time, there is insufficient definition of the governing variables to permit the
development of a responsible scope of work and estimate of reasonable accuracy.
The scope of this task will include the selection of a site for addition of the nutrients, determination of the. proper nutrient addition rates, definition of the
frequency of site visitations by DEAS personnel for system maintenance and site
sampling, determination of utilities available at the site, and definition of system
shelter, protection, and security requirements for the site.
Resolution of these variables will require analysis of data not yet available (from Tasks 1 -3) and site inspection by system design personnel. The deliverable for a
conceptual design will include nutrient system delivery Process Flow Diagrams
(PFDs), definition of ingredient storage requirements, approximate utility supply
requirements, and operating manpower estimates.
The final design effort would involve specifying individual equipment pieces and
installation details, utility connections, site lay-out drawings, and equipment
arrangement drawings. The outcome of this effort will be the Installation of a specified nutrient preparation station, ingredient storage, and nutrient addition
system at the selected site. Operating procedures for this system will also be
prepared as part of the final design effort and will define the frequency of sampling and analysis, required sample analyses, operational requirements, and routine
maintenance activities.
i4J OOJ
• 09/09/94 14:54 DU PONT ENV!RO~
Mr. Barto Page 4 ! September 8, 1994
In summary, the data currently available to DERS Is insufficient to enable accurate definition of the subsurface variables. The unexpected patterns and high rates of groundwater flow from the wells utilized in the recent tracer study test program are not consistent with site hydraulic · data generated during previous investigations. Since the tracer test data is not consistent with the previous data, DERS can no longer support previous scopes and/or estimates for system design, construction, and operation. DEAS expects that the additional field activities described above (Tasks 1 through 3) will confirm that the site subsurface geology is heterogeneous, This situation may well enable the placement of nutrient addition system(s) at location(s) permitting significantly reduced design, installation, and operating expenditures. Pending the successful completion of Tasks 1 through 3, DEAS will develop a scope of work to address Task 4 -Field Pilot Test and will submit it' for group review and subsequent U.S.E.P.A. concurrence.
DERS is available to discuss the various specifics aspects of this proposal with you at your convenience. Please contact Kevin White at [phone] should you wish to discuss this subject further or in greater detail.
Sincerely,
Kevin P. White
Sr. Project Manager aO
~;,~"a-
Attachment
CC: M. A. Gauthier
File 3104.504
~004
Macon Dockery Scl1edule
8129/94
September I
ID Task Name DuraUon 8128 I 9/4 I 9/11 I 9118 I 9/25 I
1 Planning 7d . .
2 Waler tank order/dollver 6d
3 Bailitr ordetldelivery 6d
4 Sample supplles order!d 5d
6 Waler level order/deUver 5d
6 Orllling Contract 1d
7 Slug lestolsampllng 27d
y
8 Slug tes1• 2d • 9 Sample 13 wells 1d
. ·-····-. . -· . ··-··. ·-·--··--10 Sample Analysis 21d
11 Oat.I E\laluatlon 5d
12 Drllllng/Samplo Colloctlon 4d ;: ;
13 Site Prep 1d '\. 14 Drill[ng/Soll Semple Coll 2d
15 Water Sampling 1d Ii. 16 Samples lo Glasgow Od 9123
17 Bio Bench Te&t 36d
"' 18 Rscelve &amples 1d Ii 19 Conduct Test, 30d
20 Data Evaluatlcm 5d
21 · Prepare report Od
Task Summery • Project Progreu Roned Up Task Date: Fri 919/94
; Mlle.st.one ♦ RoDed Up Milestone ◊
Page 1
October I
1012 I 1019 I 10/16 I 10123 I 10130
T
. . ... . . -·. .... ···-.
.
• Rolled Up Progress
November
I 1116 I 11113
. ······-· . . ..
T
:. ♦ 11/14
• • l
•
0 ., ....
0 ., .... ., ...
... ...
"' ..
Ci • ..
"' .. .. ... ..
i!9
0
0
"'
\
Macon/ooaery Site • Richmond County, North Carolina
August 9, 1994
Reply to: Technical Committee
c/o David L. Jones
Clark Equipment Company
P. 0. Box 7008
South Bend, IN 46634
Phone: [phone]
Fax: [phone]
Ms. Giezelle Bennett
Remedial Project Manager
U. 5. EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
RE: Macon/Dockery Site• Cordova, North Carolina
Monthly Progress Report• July 1994
Dear Ms. Bennett:
AUG 2 2 1994
SUPERfllND SECTION
On behalf of the Macon/Dockery Site Group ("Group") the July 1994 Monthly Progress Report
is being submitted in accordance with Section XV -PROGRESS REPORTS of the Unilateral
Administrative Order (effective date -June 30, 1992) for the Macon/Dockery Site. This report
describes those activities which occurred during the month of July as part of the Remedial
Design and Waste Removal Phase Phase of this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH JULY 1994:
Results of Sampling and Testing and Other Data Received
• Copies of waste characterization and confirmational sampling analytical data from
Lagoon 10 activities are attached. Confirmational samples collected from the sidewall
of the Lagoon 10 excavation and also at five of the six lagoon bottom sampling
locations have achieved the 2 ppm cPAH performance standard. The remaining sector
of the Lagoon 10 bottom will undergo additional excavation and confirmational
sampling to achieve the performance standard.
Plans. Reports. Deliverables and Procedures Completed
• Nu-Way Environmental, Inc. (remedial contractor) continued with waste consolidation
and removal activities at the site, including:
An additional 200 cubic yards of affected soil were removed from the bottom
of the Lagoon 10 excavation, which is now at a total depth of 14 feet below
grade. Confirmation samples were collected as described in the workplan. All
samples achieved the 2 ppm total carcinogenic PAH performance standard
except one (VS-14, Southwest Quadrant of the Lagoon Floor, 4.36 ppm total
cPAHs). Additional soil from the Southwest Quadrant will be excavated to
• •
Ms. Giezelle Bennett Page 2 August 9, 1994
15 feet below grade as soon as waste hauling operations commence. A second
confirmation sample will then be collected and analyzed.
• Nu-Way removed rainwater from the eight vats and consolidated the water in
a frac tank for treatment via carbon absorption canisters.
• Nu-Way removed the solids from each vat and cleaned the metal using a high-
pressure steam cleaner.
• Nu-Way continued the consolidation of drummed materials for characterization
and disposal.
• Nationwide Tank, a subcontractor to Nu-Way, began dismantling vats for
shipment to a metal recycler. Seven of eight vats were completely dismantled
in July.
• RMT provided a letter to U.S. EPA dated July 21, 1994 outlining the proposed facilities
and schedule for disposal of waste generated during the Waste Removal Project.
• Correspondence dated July 28, 1994 was received which provided U.S. EPA's written
approval of the Workplan for the Removal of Wastes from Lagoon 10, Vessels, and
Drums and the Final Remedial Design Report for Soil Vapor Extraction.
• DuPo~t Environmental Remediation Services remobilized to the site on August 2, 1994
to implement the Tracer Test #3 work as approved by U. S. EPA.
TASKS PLANNED FOR AUGUST 1994:
• Continue waste removal activities in accordance with the U. S. EPA-approved
Workplan.
• Continue the performance of Tracer Test #3.
• Continue developing the Prefinal Design for the groundwater remedy.
PROBLEMS AND DELAYS
• No additional problems or schedule delays are foreseen.
' • • Ms. Giezelle Bennett Page 3 August 9, 1994
If there are any questions, please do not hesitate to contact me at [phone].
Very truly yours,
g~:7~
David L. Jones
Project Coordinator
Macon/Dockery Technical Committee Chairman
lb
alt.
cc: Macon/Dockery Technical Committee Members Wayne F. Barto, de maximis, inc.
Paul Furtick -RMT, Inc.
lllHIAY SAIIPLE ID
llP-A-11 AIID llP-8-fl
IIP-8-12
•
llP-C-tl, WP-C-12, IIPC-13 & IIP-D-tl
IIP-D-12, IIP-D-13, IIP-D-14 & VS-fl
IIP-E-tl
VS-12
WP-E-12
VS-13
WP-E-13
VS-12 vs-t4, vs-ts, vs-t6, vs-11, vs-ts VS-19, VS-lf, VS-11 & EQ-8LK-tl
•
MACOII-DOCKERY REPORTS EIICLOSED
LAB ID
84-16-372
84-16-411 (S-8446)
84-16-469
84-16-486
84-16-573
84-16-579
84-16-572
B4-17-121
B4-17-121
B4-17-119 (S-8779)
B4-17-121 (S-8771-81)
AIIALYSIS PERFORMED
HAZARDOUS WASTE CHARACTERISTICS
HAZARDOUS WASTE CHARACTERISTICS
HAZARDOUS WASTE CHARACTERISTICS
HAZARDOUS WASTE CIIARCATERISTICS
AIID CPAH
HAZARDOUS IIASTE CBACTERISTICS .
CPAH
HAZARDOUS WASTE CHARACTERISTICS
CPAH
HAZARDOUS IIASTE CHARACTERISITCS
CPAH
CPAH
c1unom1cs Laoora1ory, inc.
South Caronna Division
• 200 Rich Lex Drive Phone: -) 796-8989
Lexington, South Carolina 29072 Fax: [phone]
NU-WAY
1741 CALKS FERRY RD
LEXINGTON, SC 29073
Attn: J, ROBLEY
Invoice Number:
NC CERT #327
Sample Sample
South Carolina Certification Number: 96012
South Carolina Lab ID Number: 32117
Order#: B4-06-372
Date: 06/29/94 10:49
Work ID: PROJ #94045
Dace Received: 06/21/94
Date Completed: 06/29/94
Client Code: NU_WAY_JR
SAMPLE IDENTIFICATION
Sample Sample
Number ---=D~e~s~c~r~i~p~c~i~o~n~---Number ---~D:e:szcr..,..ip=ci~·o~n..._ __ _ 01 WP-A-01 02 WP-B-01
Certified By
TERESA KUBBARD, LAB. MGR.
Client Nome:
Addroao:
. CUSTODY TRANSFERS:-..'.._C
1: 'if;";,~ :JI~ Received by:
2. --~-----,-
3. --------
.•. l_ . loborotory R~mork~: ;.:::. --~
. .. ·w "';t~ Blonom1cs Laboratory, Inc. Soulh Carolina olvlslon
200 Rich Lex Drive Lexlnglon, $oulh Carolina 29072 [phone] Fax [phone] · ~ SC l.,A,B ID #32117 ,: SC CERT.9601t/ ~ CHAIN OF CUSTODY RECORD -. :· • _ -st
,.;_
I
Oat■: Tim•:
~--~
.6:."'. uoi.
I
I
Pllrameter
Analvsii; ·
/~
w;oj1 _ ;,\';:7E~7}"(J/~;y'f;J!J};{\\3'.!,
•
, Order# B4·06·372
06/29/94 l0:49
Sample: 0lD WP·A·0l
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
Sample: 02D WP·B·0l
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
TEST RESULTS BY SAMPL.
Collected: 06/20/94
Result ~ Units
> 70 Degrees Cent.
.PASS PASS/FAIL
5.43 pH UNITS
Collected: 06/20/94
Result ~ Units
> 70 Degrees Cent.
PASS PASS/FAIL
7.33 pH UNITS
.Page 2
,1la!lali::zed §l::
06/29/94 SB
06/23/94 TY
06/23/94 KM
Anali::zed §l::
06/29/94 SB
06/23/94 DTY
06/23/94 KM
• order I B4-06-372
06/29/94 lO :49 • TEST RESULTS BY SAMPL •
S.mple De•cripti0l1: JIP-A-Ol
Test Description: REACT!VITY
Collected: 06/20/94 15:15
PARAHETER
H2S
CN
RESULT
BDL
BDL
Lab No: OlD
Hee.hod: $11-846 8.J
LIMIT ANALYST
..Bf.
..Bf.
Notes .nd Detilliti011s tor this Report:
DATE RUN
UNITS
Sample Description: WP-A-01
Test Description: TCLP HBTALS SCAN
Collected: 06/20/94 15:15
PAP.J\HETER
Arsenic
Barium
Cadmi.wn
Chromium
Lead
Hercury
Selenium
Sil var
6{23-28/94
mqJ'ka
RESULT
< 0.100
0.75
< 0.010
< a. 010
< 0.050
< 0.002
< o.)oo
< o.q10
Lab No: OlD
Heehod: 6010/7410
SPIICE_RECOV
!5 t
92 t
14 t
19 t
11 t
!' t
•! • 65 I
Notes &e1d Delin.itJ.Ol16 tor t.111• Repcrc,
DATE RUN
UNITS
S.mple Descriptioa: IIP-A-01
06/23/94
mg(L
Test De11cripti011: TCLP SBMI'-'VOLATILBS ONLr
Coll•cted: 06/20/94 15:15
z..b No: OlD
Hecbod: UA 125
0-Cresol
11-Cre•ol
P•Cre•ol
lU!StlLT LIMIT SPX_ UC0V Q
-~•,.,,D=L _LJ
-~B,.,,D.,L _LJ
_ _,s,.o.,L ~
---~'~'~' ll __ __.1.,0~• ll __ __.,,.g~• !l
Te.sc Code: R&\CTI
Test Code: TCLP_H
Test Code: TC_625
Page 3
, order I B◄-06~312
OGi29/9< l0,49 ___ .'{~ RESULTS BY SAHP(,E:
Sample Descripc.ioa: h'P-A-01
Test Description: TCLP SQU-VOL,\TILSS ONLY
Collected: 06/20/94 15:15
L&b No: OlD
Hee.hod: EPA 625
2, 4,5 Tricb.lorophenol BDL ____,Q,.d, 125 2. 4, 6 Trichloropbe.r,.ol BDL ---2..:.1. 117 Pentac.bloropbe.aol BDL _..!LJ. f9.6 Pyridine BDL ----1L:.l. 2,2,. 2, Nitrobenzene BDL _LJ po Hexachloroee.hane BDL --2..:.l ~5.4 Hex•chlorobutadiene BDL -.2..:.l 1~-4 Hexachlorobezene SDL ---9..:.l. J~O 2,< Di.D..itrocoluene SDL ---9..:.l. 86.4 l,4-Dichlorobenzene BDL __!l._;_l ,~I·
Notes and Definitions tor this Report:
E:XTRACTE:D
lJATE RUN
06(23/94
06/26/94
ANALYST ~
INSTR'1MEll'1' _l.W,
FILE ID
CONC FACTOR
13689
UNITS mq/L
Sample Descriptioa: COMPOSITE A-1--A-5
Test Description: TCLP VOLATILBS ONLY
Collected: 06/20/94 lS:15
PARAMBTER RBSfJLT
Vinyl Chloride B!2L l,l-Dic.bloroee.hene BD&l
Hee.hyl Ethyl Ketone BD~ Chlorotozm BDL C•rbaa Teeracbloride BDL
Benzene O-H~ l,2-Dichloroet.hcne SDL
Trichloroet.bene BDL Tetraclzloroet.hene BDfl Chlorobeaze.ae BDL l,4-Qicb:lorobenzene so,
u.b No:
Hee.hod:
LIHIT
---9..:.l.
-9.,,,ll
-LI
_L,ll
-9..,.R§.
-9..,.R§.
-9.,,,ll
-Lil
-9.,,,ll
-9.,,,ll
.....9.,.il
OlB
EPA ...
SPK_RECCV
ai-i
ti&
9:iiil
tOG
102
.101
i~,2
~02
§9.2
l24
!~d
Not•• &Dd Defin.1ti.oa• Lor t.b.t• R-i,ort:
==
DATB RaN
ANAl,r5T ~
INSTRUHBNT ...Jlli
06/23/94
06/2Glj4
Test Code: TC'_625
!!
!!
!!
!!
!!
!!
!!
JI.
!!
!!
Test Code: TC"_624
Q
!!
!!
!!
JI.
!!
!l
!!
!!
!!
JI.
r Order I B4-0G-372
06/29/94 l0:4J ---~lsr RESULTS BY SAHPL£
Suiple D••cripcion: C'CWPOSITB A-1 --A-5
Tesc Descr:i.pci.on: 7'CLP VOLATILES
Collected: 06/20/94 15 '15
FILE IlJ
CONC FACTOR
UNITS
Sample Descr:i.ptiOll: JtiP-B-01
Te.st Description: REACTIVI'TY
Collected: 06/20/94 11:00
PAJW<ETER
H2S
CN
ONLY
~7807
l
mq/L
RESULT
3.0
Lab No: OlB
Hee.bod: BPA 624
Lab No: 02D
Heehod: SJI-B46 8.3
LIMIT ANALYST
..JS!:! ___ ... , ..JS!:!
Notes •nd Def:i.ni tioz:ur for chis Report:
.DAn" RUN
UNITS
Sample De.scr.i.ptiOZI: JtiP-8-0l
Te.st Description: TCLP HJrrALS SCAN
Coll•cced: 06/20/94 18:00
PAJW<ETER
Arsenic
B•rium
C•dmium
Chromium
Le,ad
Hereuzy
Selenium
Silver
6/23-28/94
RESDLT
< 0.100
J. 02
< 0 010
< a. 010
c0.0~!2
< 0 002
< O.JOO
< o. 010
Lab NO: 02D
Met.bod: 6010/7470
SPIXE_RECOV
21 •
88 •
14 !
18 •
12 •
84 •
100 !
f4 •
Note• .ad De.tiD.i tioa• tor tlti• Report:
tlA2"Jr RtlN
UNITS mg/L
Test Code: 'Tc:_624
Te.s C Code: R.BACTI
Test Code: TCLJI_H
.Order II· B4-06-372
06/29/94 l0:49 • _____ TE._..S"'-T"-'RE=S=<-UL=T""S"'--'B"'-Y"-'S"'mF=..,•=----
Sample Descripcicn: JtlP-B-01
Test De:icripti.oa: TC'LP S!Ml'•VOLATILES ONLr
Collected: 06/20/94 18:00
PARAHE'rER RESULT
0-Cresol BDL
H-Cresol BDL
P-cresol BDL
2,4,S Tricbloropbenol BDL
2, 4, 6 Tr:J.cblorapbenol BDL
Pe.aC•chlorophenol BDL
Pyridine BDL
Ni erobenzene BDL
Hex•chloroe Chane BDL
He:uchlorcbutadiene BQL
Hexachlorobenzene BDL
2,4 Oinitrocoluene BDL
J,4-Dichlorobenzene BDL
Lab No: 02D
He thocf: EPA 625
LIMIT SPIC_RECOV
_LJ AlJ
____Q,J J04
_.JL1. ~04
~ t2S
-.lU 111
-.lU Bf.6
_Ll 29-9
--2...:..:!. 120
~ 55.4
_.£.:..! 42.4
_2..:.1. 150
~ 86. 4
---2..:..4. 15.l
Notes .nd Definitions .tor this Report:
EXTRACTED
DATE RCJN
ANALYST ,J:Y.
06/23/94
96 {26 /94
INSTRUMENT 5910
FILE ID 13691
CONC FACTOR l
UNITS mo/L
Sample De•cr:J.pcioa: COHPOSI'T.B' B-1·-B-5
Te.st Description: TCL.P VOLA7'IL&S ONLY
Collected: 06/20/94 18:00
PAJWJl!TEll RESULT
Vinyl Chlori.de s12.,
1, 1-Di. c:.b.loroe Chene B12,L
HeCb.yl B'tbyl Ket:cae SDI.,,
CbJoroform BD' c.rbc:m Tet:racb.lor1de !.D!I. Be.aseae 0114£
l, 2-Dj c::bloroetba.ae BQL
Trieh.loroe.t:b.aae §.DIJ.
Tet:racbloroetbaae BDL
Cb.lorobeDzene BD!i,
l,4-Dicbloroben:zaae BDIJ.
.L.b No: 02B
lteebod: BPA 624
LIMIT SPX_RECOV
-.lU f2.J
----9..:.H u.2
-.lU 2_2.3
__9.,.M. H'
---LM 402
J& io7
__9.,.M. ilQ.!
-1Wa J02
___/}_& at,. 2,
~ 104
~ 85,-1
Test: Code: TC_G25
0
!l
!l
!l
!l
!l
!l
!l
!l
!l
!l
!l
!l
!l
Te•t: Code: 7'C'_624
0
!l
!l
!l
!l
!l
!l
!l
Sl
!l
!l
Page 6
' O~er I 84-06'-372
06/2!J/!J4 J0:49
' Sample Descripei. 0n:
Te•t Description:
Collect~:
----T"EST RESC]I,TS BY SAMPLE
CCHPOSITE B-l--B-5 Wb No:
TCL2 VOLATILES ONLY Mee.bod:
OG/20/94 18: 00
Notes and Definitions for Chis
EXTAACTED 06/2J/94
DATE RUN
ANALYST 2£
INSTRUMENT ____!ll!
FILE ID 27808
06(26/94
CONC FACTOR 1
UNITS mg(L
•. ,
02E
UA 624 Test Code: TC'_6'24
Report:
,Order'#'B4-06-372
06/29/!14 10:49 •
IGNITABILITY-PENSKY MARTEN
Method:
Samp Sample Description
OlD WP-A-Ol
02D WP-B-Ol
PAINT FILTER
Method: 9095
~ Sample Description
OlD WP-A-Ol
02D WP-B-Ol
pH
Method: EPA 150.l
Samo Sample Description
OlD WP-A-Ol
02D WP-B-01
REGUr.AR TEST RESULTS BY •---
Page 8
Minimum:
Result
> 70
> 70
Minimum:
Result
PASS
PASS
Minimum:
Result
5.43
7.33
Units
Degrees Cent.
Degrees Cent.
Limit Prepared Analyzed .rue
06/29/94 SB
06/29/94 SB
Maximum:
Units
PASS/FAIL
PASS/FAIL
Limit Prepared Analyzed .rue
06/23/94 TY
06/23/94 DTY
Maximum:
Il1fil.§..
pH UNITS
pH UNITS
biJJ1LJ;. Prepared Analyzed~
06/23/94 KM
06/23/94 KM
tuonom1cs Lat>oratory, Inc.
South Carolina Division• ·
• 200 Rich Lex Drive Phone:~) 796-8989 Lexington,.South Carolina 29072 Fax: [phone]
South Carolina Certification Number. 96012
South Carolina Lab ID Number: 32117
NU-WAY
l74l CALKS FERRY RD
LEXINGTON, SC 29073
ACCn: J, ROBLEY
Invoice NUmber:
NC CERT#327
Sample Sample
Nµmber Description
Ol B-6--B-lO COMPOSITE S-8446
Order#: B4-06-400
Dace: 06/29/94 10:48
Work ID: PROJ #94045 S-8446
Dace Received: 06/22/94
Dace Completed: 06/29/94
Clienc Code: NU_WAY_JR
SAMPLE IDENTIFICATION
Sample Sample
Number --~D~e=s=c=r~i~p~c~i~on~---
02 WP-B-02 S-8446
Certified By
TERESA HUBBARD, LAB. MGR.
c1u11u1111<;s Laooratory, Inc. South Carolina Division
200 Rich Lex Drive Lexington, South Carolina 29072 [phone] Fax [phone] & SC LAB ID U32117 SC CERT. 96012 . ,# CHAIN OF CUSTODY RECORD "
~ f-
CUent Name: M / .. \ ,-_ ""7""1;.. .A u-, _vr,,, ,7~/11Dr>l-e/1-t,,,_/ ,, , /JC,
Roo/Prol.Monooor: -:-r: 'l<__ ,...,6 /r,,
Prolocl ID: Q-464<; --.I P.O.I:
Colloclod bv: lu~-'r'\1 /, -
Somolo ID Cate Time Samole location ."If-/,.,
A-'7
l<.8-9 I
, o.ra l l,6 I.S
' .
., I l -' •
D•••: Tim•:
1,t,11-lit 7,0.30
2. -------~
3. --------
/) .:1,_ ,II,
laboratory Remarks:
,\
'
Order·# B4-06-400
06/29/94 10:48 • Sample: 02A WP-B-02 S-8446
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
TEST RESULTS BY SAMPL •'---
Collected: 06/21/94
Result
> 70
PASS
5.95
Units
Degrees Cent.
PASS/FAIL
pH UNITS
Page 2
Analyzed Jay
06/29/94 SE
06/23/94 TY
06/23/94 SE
Order# B4·06·400
06/29/94 10:48 • TEST RESULTS BY SAMPLE ,,._ __
Sample Descripcion: B-6--B-lO C'OHPOSITE S-8446 Lab No: OlA
Test De:rcriptioa.: TC.LP VOLA.TIL&S ONLY
Collected: 06/2J/94
PARAHETER RESULT
V1nyl Chlor.i.de BD~
l,l-Dichloroechene BDIJ
Heebyl Ethyl Ketone BDL
Chloroform Bf2.f1.
C.a.rbo.a Tetrachloride BDf,.
Benzene 0.0~~
l,2-Dichloroethane sbr,
Trichloroethene BDf,.
Tecrachloroeebene BDL
Cblorobenzene 812,f,.
1,4-Dichlorobenzene BDL
Method: BPA 624
LIHIT SPJC_R.ECOV
_,Ll 93,2
~ PZ.
_,Ll 92.3
~ 106
~ 102
_Q.J!l ~!27
~ ~02
~ 102
~ 89,2
~ 104
_Q_..£1 85.4
Notes and Defini ci0.lls for this Report:
EXTRACttD
DATE RUN
ANALYST ~
INSTRUMENT --llZ1.
FILE ID
CONC FACTOR
21804
UNITS ma/L
06/23/94
06 (26 (94
Sample Description: tfP-B-02 S-8446
Test Desc:iption: REACTIVITY
Collected: 06/21/94 10:55
L.sb No: 02A
Hecbod: SW-846 8.J
112S
CN
RESULT LIMIT ANALYST
--~•~D~L ---~ ..J!!i --~3.., .... l l ..!!:!:!,
Note• .acd DefUlit.i.012• for tb.i.s Report:
DAtt RUN
UNITS
Test Code: TC_624
0
!l
Sl
!l
!l
!l
!l
!l
!l
!l
!l
Test Code: .R.DCTI
Page 3
'
·Order'# B4•06·400
06/29/94 10:48 • TEST RESULTS BYSAMPL. __ _
S.uiple Descripcioa: JfP-B-02 S-8446
Tesc Descripcion: TC'L.P MlrrALS SCAN
Collected: 06/21/94 10:55
Lab No: 02A
Method: 6010/1410
PAJIAHETER RESULT SPIXE_RECOV
Arsenic < 0.100 t• t
Barium 1.02 B1 t
Cadmium < 0. 010 77 t
Chromium < 0.010 79 t
Lead 0.065 ·~ t
Herc-uzy < 0.002 95 t
Selenium < 0~ 100 ~01 t
Silver < 0.010 67 t
Notes and Detini tions tor this Report:
DATE Rt!N
UNITS
06/23/94
mg/L
Sample Descripti01J: WP-B-02 S-8446 wb No: 02A
Test Descripr::ion: TCLP SEMI-VOLATILES ONI.Y
Collected: 06/21/94 10:55
He tbod: EPA 625
PARAl<ETER RESULT LIJ(IT SPK_RECOV
0-Cresol BD!J, ____!L_l llJ
H-Cre.sol SDL ____!L_l 104
P-Cresol BD/J ____!L_l 104
2,4,5 Triehlorcphenol BD~ ____!L_l ps
2,4,6 Tricbloropbenol §.Dlt. ~ !17
Pent•ehloropheaol BDf:t. ____!L_l 89.6
Pyridine BD"h ~ U-9
Ni trobeazene BDI4 ____!L_l po
Bexach.loroedUlne BD!J, ____!L_l S5.4
Hexac:h.lorobucadiene SD~ ......L.t p.,
Hexaeb.lorobenzeae BDf,, ____!L_l l~O
2,4 Diaitrocolueae BDf:t. ____!L_l B6. 4
1.4-Dic:hlorobeaze.ae BO£,. ----A! ?~.~
Note• &ad Det!lli.c.1.0D.,9 tor tlu• Report:
==
.D.\rB RC1N
ANALYST ,lld;.
INST1tc1HENT .......1.2:z.g_
FILB ID
OG/23/21
06/26/91
0
!l
!!.
!l
!l
!l
!l
!l
!l
!l
!l
!l
!l
Jl
Test Code: TCLP_H
Test Code: n::_625
Page 4
• ~rder I 84-06-400
06/29/94 10148 ___ .... T RESULTS BY SAMPLE
Sample De•cripeiot2: JtP-s-02 S-8446
Te•t Descripei.011: TCr.P SEXI-VOLATILES cm,y
Collected: 06/21/94 10:55
CONC FACTOR l
rJNITS mq/L
L.tb No: 02A
Method: KPA 625 Teat Code: TC:_625
Order# B4-06-400
06/29/94 10:48 •
IGNITABILITY-.PENSKY MARTEN
Method:
Samp Sample Description
02A WP-B-02 S-8446
PAINT FILTER
Method: 9095
~ Sample Description
02A WP-B-02 S-8446
pH
Method: EPA 150.l
Samp Sample Description
02A WP-B-02 S-8446
REGULAR TEST RESULTS BY •---
.Page 6
M1nimum:
Result
> 70
M1nimum:
Result
PASS
M1nimum:
Result
5.95
Ha.ximum:
fl!llli
Degrees Cent.
Limit Prepared Analyzed~
06/29/94 SB
Maxi.mum:
Units
PASS/FAIL
Limit Prepared Analyzed~
06/23/94 TY
Ma.ximum:
!!ll.llJ1
pH UNITS
Limit Prepared Analyzed~
06/23/94 SB
' ' Bionomics Laboratory, Inc.
• South Carolina Division.
200 Rich Lex Drive Phone: [phone]
Lexington, South Carolina 29072 Fax: [phone]
NU-WAY
l 741 CALKS FERRY RD
LEXINGTON, SC 29073
Attn: J. ROBLEY
Invoice Number:
Sample Sample
South Carolina Certification Number: 96012
South Carolina Lab ID Number: 32117
Order#: B4-06-469
Date: 07/08/94 14:55
Work ID: PROJ #94045
Date Received: 06/24/94
Date Completed: 07/08/94
Client Code: NU WAY JR
SAMPLE IDENTIFICATION
Sample Sample
Number ---~D~e~s~c~r~i~p~t:i~o~n __ _ Number ---~D~e~s~c~r:i~o~t~1·~on,._ __ _
Ol C-Al--C-A5 COMPOSITE 05 C-B6,B7,C2,C4,C6 COMP.
02 WP-C-Ol 06 WP-C-03
03 C-Bl--C-B5 COMPOSITE 07 D-El--D-E5 COMPOSITE
04 WP-C-02 08 WP-D-Ol
Certified By
TERESA HUBBARD, LAB MGR
Order# B4-06-469
07/08/94 14:55
Sample: 02A WP-C-Ol
•
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
Sample: 04A WP-C-02
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
Sample: 06A WP-C-03
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
Sample: OBA WP-D-01
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
TEST RESULTS BY SAMPLE •
Collected: 06/22/94
Result
>70
PASS
9.18
Limit Units
Degrees Cent.
PASS/FAIL
pH UNITS
Collected: ,06/22/94
Result
>70
PASS
9.59
Units
Degrees Cent.
PASS/FAIL
pH UNITS
Collected: 06/23/94
Result
>70
PASS
10.70
Units
Degrees Cent.
PASS/FAIL
pH UNITS
Collected: 06/23/94
Result
>70
PASS
ll. Ol
~
Degrees Cent.
PASS/FAIL
pH UNITS
Page 2
Analyzed fuc
07/07/94 SR
07/01/94 TY
06/24/94 KM
Analyzed fuc
07/07/94 SR
07/01/94 TY
06/24/94 KM
Analyzed fuc
07/07/94 SR
07/01/94 TY
06/24/94 KM
Analyzed fuc
07/07/94 SR
07/01/94 TY
06/24/94 KM
'
Order# B4-06-469
07/08/94 14:55 • TEST RESULTS BY SAMPLE. __ _
Sample Description: C-Al--C-AS CCMPOSITB
Test Description: TCLP VOLATILES ONLY
Collected: 06/22/.94 00:00
Lab No: 01A
Hethod: BPA 624
PARAHETER RESULT LIMIT SPK_RECOV
Vinyl Chloride BDL ~ 65.5
1,1-Dichloroethene BDL ~ 88.l
Methyl Ethyl Ketone l!QL ____£__J_ 119
Chloroform BDL ~ 82_.4
Carbon Tetrachloride BDL --1l.:..M. 77.5
Benzene 7,17 ~ 86.1
1,2-Dichloroethane BDL ~ 144
Trichloroethene BDL ~ 105
. Tetrachloroethene BDL ~ 84.l
Chlorobenzl!!lle BDL ~ 10~
1,4-Dichlorobenzene BDL ~ .91.a
Notes and Definitions for this Report:
EXTRAcn'D
DATE RUN
ANALYST .2§.
INSTRUMENT _.illi
FILE ID
CONC FACTOR
UNITS
Su,ple Description: WP-C-01
21893
mg/L
06/30/94
07/06(94
Lab No: 02A
t
t
t
t
t
t
t
t
t
t
t
Teat Code: TC_624
Q
fl
fl
fl
fl
fl
!!
fl
!Z
!Z
!Z
fl
Tesc Description: REACTIVITY
Collected: 06/22/94 14:23
Method: Stf-846 B.J Te.st Code: R&\CTI
PARAMETER
H2S
CN
RESULT LIMIT ANALYST
4.5 ---''~-~o ...J!Z!
26. 7 ---''~-~o ...J!Z!
Notes .nd Definitions tor th.i.• Report:
DATE RUN
UNITS
07/06/94
mg/Xg
Page 3
Order# B4-06-469
07/08/94 14:55 • TEST RESULTS BY SAMPLE •
Sample Description: WP-C-01
Test Description: TCLP HETALS SCAN
Collected: 06/22/94 H:23
Lab No: 02A
Method: 6010/7470
PARAMETER
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
RESULT SPIKE_RECOV
<D.100
0,468
<0.010
0.011
0.053
<0.002
< 0. 100
< 0. 010
Notes and Definitions tor Chis
DATE Rrm
UNITS
07/07/94
mg:(L
88 •
80 •
77 •
78 •
76 •
105 •
96 •
15 •
Report::
Sample Description: NP-C-01
Test: Descript:ion: TCLP SENI-VOLA.TILES ONLY
Collected: 06/22/94 14:23
Lab Na: 02A
Method: EPA 625
PARAMETER RESULT LIMIT SPK_RECOV
0-Cresol ~ ____QJ, 56 t
M-Cresol _m ....:...Q...l 58
P-Cresol ______fill!, ____QJ, 58 t
2, 4,5 Trichlorophenol _.§QI, ____QJ, 5~
2,4,6 Trichlorophenol _.§QI, ____QJ, " Pent:achlorophenol __..§l2f ____QJ, 85 I
Pyridine _.§QI, ~ •l I
Nitrobenzene ______fill!, ___iLl 57
Hexachloroethane _.§QI, ___iLl " Hexachlorobucadiene ~ ---2.:...! ll •
Hexachlorobenzene _.§QI, ___iLl 70
2, 4 Dinit:rot:oluene _.§QI, _fL1. •1 I
1,4-Dichlorobenzene __..Mb ____QJ, ..
Notes and DeLi.tlit1ona for Chis Report:
E:XTRACTED
DATE RUN
ANALYST ...!!Q
INSTRUMENT ~
FILE ID 1.31.38
06(29/94
01/01/91
Q
g
r;
r;
r;
ll
ll
ll
ll
r;
ll
ll
ll
ll
Test Code: TCLP_H
rest Code: TC'_625
Page 4
Order# IU-06-469
01/08/94 lf:55 • RESULTS BY SAMPLE
Sample Description: JIP-C-01
Test Description: TCLP SEMI-VOLATILBS ONLY
Collected: 06/22/94 14:23
Lab No: 02A
Method: EPA 625
CONC FACTOR
UNITS mg(L
Sample Description: C-B1--C-B5 CCWPOSITB
Test Descript:ion: TCLP VOLATILES ONLY
Collected: 06/22/94
Lab No: OJA
Method: EPA 624
PARAMETER RESULT LIMIT SPK_RECOV
Vinyl Chloride BDL _Q.:.l 65. 5
1,1-Dichloroethene BDL ~ 88.l
Methyl Ethyl Ketone BDL _LJ 119
Chloroform BDL ~ 8[!_.4
Carbon Tetrachloride BDL ~ 11.5
Benzene 5.25 ~ 86.1
1,2-Dichloroethane BDL ~ 144
Trichloroethene BDL ~ 105
Tecrach.1 oroethene BDL ~ 84.;t;
Chl orobenzene BDL ~ 105
l, 4-Dich.lorobenzene BDL ~ f!.3.5
Notes and Definitions for this Report:
EXTRACTED
DATE RUN
ANALYST ~
INSTROMENT ~
FILE ID 27895
06/30/94
01/06/94
CONC FACTOR l
UNITS mg/L
Sample Description: WP-C-02 Lab No: 04A
• • • • • • • • • • •
Test Description: R&\CTIVITY
Collected: 06/22/94 15:40
Method: SW-846 B.3
H2S
CN
RESULT LIHIT ANALYST
------''""6 l.Q .JS!:!
---=•,.,oc.,.,_J 1. o JI!1
Notes and Defin.itions for this Report:
Page 5 •
Test: Code: TC'_625
Test Code: TC'_624
Q
I!.
I!.
I!.
I!.
I!.
!!
I!.
I!.
I!.
I!.
I!.
Test Code: R&\CTI
Order I 84-06-469
07/08/94 14:55 ____ • RESULTS BY SAMPLE
Sample Description: JIP-C-02
Test Description: R&\C"TIVI'TY
Collected: 06/22/94 15:40
DATE RUN
UNITS
Sample Description: JIP-C-02
Test Description: TCLP HBTALS SCAN
Collected: 06/22/94 15:40
PARAMETER
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Lab No: 04A
Method: SW-846 B.3
07 /06/94
mq(Kq
RESULT
<0.100
0.591
<0.010
0. Oll
0. Q6l
<0.0CJ2
<0.100
<0. 010
Lab No: 04A
Method: 6010/7470
SPIKE_RECOV
97 t
82 t
82 t
82 t
81 t
109 t
103 t
2l: t
Notes and Detini tions for this Report:
DATE RUN
UNITS
07/07(94
mq(L
Sample Description: JIP-C-02
Test Description: TCLP saa-voL,U'ILES ONLY
Collected: 06/22/94 15:40
PARAMETER RESULT
0-Cresol _§!I!,
H-Cresol _§!I!,
P-Cresol _§!I!,
2,4,S Tric.hlorophenol _§!I!,
2,4,6 Trichlorophenol _§!I!,
Pentachlorophenol _§!I!,
Pyridine _§!I!,
Ni troben.zene _§!I!,
Hexachloroethane ___!!II,
Hexachlorobutadiene ___!!II,
Hexaehlorobenzene ---1!2f
Lab No: 04A
Method: EPA 625
LIMIT SPK_RECOV
--2.d 56 t
---.Q.d 58 t
_.Qd 58 t
--2d l:8 t
_.Qd 54 t
___Q_,_l, 85 t
--..R.d 43 t
_.Qd 57 t
_.£.al ,. t
_.Qd 31 t
_____Qd 70 t
0
!Z
!Z
!Z
!Z
!Z
!I
!Z
!Z
!Z
!Z
!Z
Page.
Te.!it Code: R&\CTI
Test Code: TCLP_H
Test Code: TC_625
Order I 84-06-469
07/08/94 H:55 • RESULTS BY SAMPLE
Sample Description: WP-C-02
Test Description: TC'LP SDCI-VOLATILBS ONLY
Collected: 06/22/94 15:40
Lab No: 04A
He thod: EPA 625
2,4 Dinitrotoluene
1,4-Dichlorobenzene
_____fil2b ~
_Mf~
53 t fl
46 t Jl
Notes and Definitions tor this Report:
EXTRACTED
DATE RUN
ANALYST ..5
INSTRUMENT ~
FILE ID 13739
CONC FACTOR
UNITS !!!9:{._L
Sample Description: C-B6,87,C2,C4,C6 CCIIP.
Test Description: TCLP VOLATILBS ONLY
Collected: 06/23/94
06{._29{._94
07 {._07 /94
1
Lab No: 05A
Method: EPA 624
PARAMETER RESULT LIMIT SPK_RECOV
Vinyl Chloride BDL ~ 84.0 • 1,1-Dichloroethene BDL ~ 111 • Methyl Ethyl Ketone BDL ~ 102 • Chloroform BDL ~ 97.l •
Carbon Tetrachloride BDL ---2..:..M 98.2 • Benzene 7.73 ~ 104 •
1,2-Dichloroethane BDL ~ 113 • Trichloroethene BDL -11..:..M. 100 ' Tetrachloroethene BDL ---9..:.2.2. 92. 7 ' C.hlorobenzene BDL ~ 100 ' 1,4-Dichlorobenzene BDL ~ BJ. 9 •
Note• and Delini tions for t:hi.s Report:
EXTRACTED 07{._06{._94
DATE RUN 07{._07{._94
ANALYST ..'1§.
INSTR'OHEN'1' ~
FILE ID 21916
CONC FACTOR 1
UNITS E!!!t..&
Q
!!
!!
!!
!!
!!
!2
!!
!Z
!Z
!Z
!Z
Page 7 •
Test Code: TC_62S
Test Code: TC_624
'
Order# B4·06·469
07/08/94 14:55 • TEST RESULTS BY SAMPLE •
Sample Description: JiP-C-OJ
Test Description: REACTIVITY
Collected: 06/23/94 10:20
H2S
CN
Lab No: 06A
Hee.hod: Sti-846 8.3
RESULT LIMIT ANALYST
--~9"-~2 1.0 -1SJt
--~5'-'6'-'._,4 1. D ..JQ:!
Notes and De!ini tions for Chis Report:
DATE RUN
UNITS
Sample Description: JiP-C-OJ
Test Description: TCLP KETALS SCAN
Collected: 06/23/94 10:20
PARAMETER
Arsenic
Barium
Cadmium
Chromium
Lead
Merr:ury
Selenium
Silver
01/06/94
mg/Kq
RESULT
< 0 .100
0.582
< 0. 010
<0. 010
< 0. 050
<0. 002
<0.100
< 0. 010
Lab No: 06A
Method: 6010/1470
SPIKE_RECOV
96 t
78 t
75 t
78 t
80 t
!09 t
95 t
J4 t
Notes and Definitions tor this Report:
DATE RUN
UNITS
Sample Description: lliP•C-03
01/07/94
mq(L
Test Description: '1'CLP S.EXl-VOLATILlCS ClNLY
Collected: 06/23/94 10:20
Lab No: 06A
Heehod: BPA 625
PARAMETER
0-Cresol
N-Cresol
P-Cresol
RESULT LIMIT SPJC_RECOV Q
-----1M2l! ____QJ
-----1M2l! ____Q_;,1,
~ _..!:.1,
56 t Jl
SB t .Q'
58 t .Q'
Test Code: REACTI
Test Code: 'I'CLP_H
Test Code: TC'_625
Page 8
Order# B4-06-469
07 /08/9'4 H: 55 ____ • RESULTS BY SAMPLE
Sample Description: WP-C-OJ
Test Description: TCLP SEMI-VOLATILBS ONLY
Collected: 06/23/9'4 10:20
Lab No: 06A
Method: EPA 625
2, 4,5 Trichlorophenol --1!!!!, _____Q2 58
2, 4, 6 Trichlorophenol --1!!!!, ____QJ 54
Pentachlorophenol -----1!Qf _____Q2 85
Pyridine --1!!!!, ---1Ld. 43
Ni trobenzene ~ __Q,J, 57
Hexachloroethane --1!!!!, __Q,J, " Hexachlorobutadiene ~ ----L!. Jl
Hexachlorobenzene ___,!fil:: __.u 70
2,4 Dinitrotoluene ___,!fil:: _.LI 63
l,4-Dichlorabenzene --1!!!!, ---...Q..:.1 45
Notes and Definitions tor this Report:
EXTRACTS])
DATE RUN
ANALYST ...J:19..
INSTRUMENT ---2.21.Q
FILE ID
CONC FACTOR
lJ?-40
UNITS mq/L
06/29/94
07/08(94
• • • • • • • • • •
Sample Description: D-El--D-ES CCBPOSITE
Test Description: TCLP VOLATILES ONLY
Collected: 06/23/94
Lab No: 07A
Method: EPA 624
PAJIAMETER RESULT l.IMIT SPK_RECOV
Vinyl Chloride w. __Q,J, 55. l
l,l-Dichloroethene BDL ~ 88.
Meehyl £Chyl Keeone BDL __Q,J, l l l
Chloroform BDL ~ 89. 1
Carbon Teerachloride BDL ~ 77. ~
Benzene 4.46 ~ 86.7 I
l,2-Dichloroeebane BDL ~ ,.,
Trichloroetherze BDI< ___Q_,_M_ 10:i:
Teerachloroet:hene BDL ___Q_,_M_ 84. l
Chlorobenzene BDL ~ lO:i;
l,'4-Dichlorobenzane BDL --L.il 93.~
Notes .and DeL1niciona Lor Chi• Reporc:
EXTRACTS])
DATE RUN
ANALYST ~
INSTRUMENT ---2..21.l
06/J0/94
01/06/94
Page.
Tese Code: TC_625
!l
!l
!l
!l
!l
!l
!l
!l
!l
!l
resc Code: TC_62'4
0
ii
!l
!l
ll
!J
ll
ll
ll
ll
ll
!l
•
Order# B4-06-469
01 /08/94 l4: 55 • RESULTS BY SAMPLE
Sample Description; D-El--D-BS CCHPOSITB
Test Description: TCLP VOLATILES ONLY
Collected: 06/23/94
Lab No: 01A
Method: EPA 624
FILE ID
CONC FACTOR
2?896
UNITS mq/L
Sample Description: WP-D-Ol
Test Description: R£ACTIVITY
Collected; 06/23/94 12:10
PARAMETER
H2S
CN
Lab No: OBA
Method: Sfi-846 8.3
RESULT LIMIT ANALYST
--~1~'~-~o l. o _JS!:!
----""=· 5 l. 0 _JS!:!
Notes and Definitions for this Report:
DATE RUN
UNITS
Sample Description: WP-D-01
Test Description: TCLP l!ETALS SCAN
Collected: 06/23/94 12:10
PARAMETER
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
07/06/94
mq/Xg
RESULT
<0.100
o.524
<0.010
<0. Ql0
0.054
<0.002
<0.100
<0. 0lQ
Lab No: OBA
Method: 6010/7470
SPIKE_RECOV
94 •
'2 • ,. •
77 •
73 •
106 •
106 •
23 •
Notes and Detini tions tor this Report:
DATE RUN
UNITS
01/01/94
mq(L
Pago •
Test Code: TC'_62f
Test Code: REACT'I
Test Code: TCLP_H
Order# B4-06-469
07/08/94 14:55 • ____ T,..E,..S._T,___,R,.,E,.,S._,UL=T,.,S"--'B'-'Y'-'S"-"'M=P-=L"'E'--.-"""---
Sample Description: NP-D-Ol
Test Description: TCLP saa-VOLATILES ONLY
Collected: 06/23/94 12:10
PARAMETER RESULT
0-Cresol ___§J2f
H-Cresol ___§J2f
P-Cresol ~
2,4,S Trichlorophenol _..w.
2,4,6 Trichlorophenol _..w.
Pencachlorophenol __JJ2f
Pyridine ___§J2f
Ni crobenzene _..w.
Hexachloroethane ___§J2f
Hexachlorobucadiene __JJ2f
Hexachlorobenzene _.§!!I,
2,4 Dinitrotoluene __JJ2f
l,4-Dichlorobenzene _.§!!I,
Lab No: OBA
Method: BPA 625
LIMIT SPK_RECOV
~ 56 t
__u 58 t
___£_l, 58 t
__LJ 58 t
__LJ Sf t
__LJ 85 t
~ 43 t
__LJ 57 •
__LJ 34 •
__LJ 31 •
__LJ 70 •
_!L1, 63 •
~ 45 •
Notes and Defi.ni cion:11 for th.is Report:
EXTRACTED
DATE RW
ANALYST J!Q
INSTRUMENI' 5970
FILE ID
CONC FACTOR
13141
UNITS mq/L
06/29(94
07/07/'}4
Test Code: Tr:_625
Q
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
Page ll
I •
' r Blonomlcs Laboratory, !,a(:.
• South Carolina Division•
200 Rich Lex Drive Phone: [phone]
Lexington, South Carolina 29072 Fax: [phone]
South Carolina Certification Number. 96012
South Carolina Lab ID Number: 32117
NU-WAY
1741 CALK'S FEmlY ROAD
LEXING!m, SC 29073
AT'm: J. RABLEY
NC CERT# 327
Order#: B4-06-486
Date: 07/12/94
Work ID: PROJ # 94047
Date Received: 06/27 /94
Date Carpleted: 07/12/94
Client Code: NU_W11Y_JR
Sl\MPLE IDENTIFICATIC!f
Sarrple Sant>le
Nunber Description
01 a:MPOSITE D-E6,E7,F5--F7
02 WP-D-02
03 CCMPOSITE D-Fl--F4,G7
04 WP-D-03
Sarrp le Sant>l e
Nurber Description
05 a:MPOSITE D-Gl---05
06 WP-D-04
07 VS-01
~~(J__J
Certified By
TERESA HUBIWID
Laboratory Manager
Client Neme:
Address:
(vu lc..l T Urr-JM..ow---d
r~ -5dGL:j
-;--u. rrr::v,>v .---.c.('
Bionomics Laboratory, Inc.
South Carolina Division
200 Rich Lex Drive Lexington, South Carolina 29072
[phone] Fax [phone]
SC LAB ID #32117 SC CERT. 96012
CHAIN OF CUSTODY RECORD
Pnrameler
Anoly6iS
11h ••. Only: _. . . . .
w.0.11_· _'..:c;/J:....,0c..><bC-'-'0c_.,_4.l,Ll?G=--· _
age_._ of_. ·O•le Due: __ _
CUSTODY TRANSFERS: ~ ( R•li~,..•hod by, /O ."""°"'•db> •
1. f)O.,V1::C.... H<>-dl.O ~-4:'.:t
Delive;ed D~ectl/ i6 Leh i:i'. Sh~ked~ ..
' Melhoi~,_~hi;m~~;; i~ptfj';utrlJ ·•··••·b,11.r:.,.;··.·_ .... .,.. .. ~~'------
Rec~!yed:· in· co~!~r yesJJ no O ··\+:~~~--~~ :.:-< :/7': · :.:.. pH cho~ked In lob: yee O no
2. -------~
3. --------
LebReciJl~ni: .. ··. ··• .. • ~I,~:dhh Time:. C/0U
Laboratory Remarka:
Bionomics Laboratory, Inc. ,:j'
Soulh Carolina Division -13
~ 200 Rich Lex Drive Lexington, Soulh Carolina 2907:1 !t.<£
[phone] Fax [phone] ~
SC LAB ID #32117 SC CERT. 9601~
CHAIN OF CUSTODY RECORD 0Q_':-
Client Nome: N u..-Wo.y E11 vlrcn ,-;e.~+a_O
Address: / 7LJ / f",d /,, <: . "D::>.rn., 12cft,
Ren/Prol.Menener: ,I. P nhlev: -..__/ Phone f: 0,",/'\-(\ \ 'l. ~
Proiect ID: 0 4f\ LL... . P.D.f:
' Semnle ID Dale Time Semnle Location
I ,.__,
,:....--"
L
o8ge . __ :of_._·· :o,t9 Due: ---
•
I
IJ-G.?.. ,-ft Jlf.S6 r_--m_k:, .e:::. · --' wD-c,~ '.,~ ,· -~ I
) -r:... ·7 _ u-, ~; J u,-.;; G,7> .h Sub --' . -J)-c... 7 c. ~0~'.}\ 1
fl'\ ~ n,-.,A-lv--i, A-f
,--'1-i.t-? ~ ~i?-l_:,
CUSTODY TRANSFERS:
~•linqul1hed by:
1. L'tJ-V ,.._ / 'or::1LU
2. --------
3. --------
Leboralory Remarks:
_...,--
v
Delivered· D~e·c11~·itJ. l.eb.(J :·. Sh~~;d· [) ·· ·.·.··::'··::_:··,
· Method~f ,;,;i~e~tl FedEx•~· UPS O 6the;: • _/ ••·.·•
Recel~-~d-: {~-: CO(?!~;·:~-~& 'o_'-~~--[J :T·~~~-~~---:':.·: ·· ..... :··. --:--·.';.-;,_~~H-. ~-fl--~-~--ke'-d-ln ... _-leb-_: ~~~-D no [
Order# B4-06-486
07 /12/94 17: 07
Sample: 02A WP-D-02
•
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
Sample: 04A WP-D-03
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
Sample: 06A WP-D-04
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
• TEST RESULTS BY SAMPLE
Collected: 06/23/94
Result ~ Units
> 70 Degrees Cent.
PASS PASS/FAIL
8.23 pH UNITS
Collected: 06/24/94
Result Limit Units
> 70 Degrees Cent.
PASS PASS/FAIL
l0.38 pH UNITS
Collected: 06/24/94
Result Limit Units
> 70 Degrees Cent.
PASS PASS/FAIL
9. 44 pH UNITS
Page 2
Anal;:zed ID:'
07/08/94 SR
07/01/94 TY
06/29/94 KM
Anal;:zed ID:'
07/08/94 SR
07/01/94 TY
05/29/94 KM
Anal;:zed ID:'
07/08/94 SR
07/0l/94 TY
05/29/94 KM
• Order# B4-06-486
07/12/94 17:07 • TEST RESULTS BY SAMPLE
Sample DescripCion: <X«POSITB D-B6,B7,F5--E7
Test Description: TCLP VOLATILES ONLY
Collect~: 06/23/94 00:00
PARAMETER RESULT
Vinyl Chloride BDL
l,l-Dichloroethene BDL
Methyl Ethyl Ketone BDL
Chloroform BDL
Carbon Tetrachloride BDL
Benzene 2. 1l
l,2-Dichloroethane BDL
Trichloroethene BD~
Tetrachloroethene BDL
ChlOrobMZene BDL
l,4-Dichlorobenzene BDL
Lab No: OlA
Method: BPA 624
LIMIT SPK_RECOV
__Q.:J, 65.5
~ 88. l
_-BJ 119
~ 82,.4
--9..:.M. 71.5
--9...:..Q.§. ~6.7
~ 144
...J..:..Qj 105
~ B·Ll
~ 105
_g_:..9j 93.5
Notes and Delin.i. tion• tor Ch.i.s Report:
==
DATE RUN
ANALYST ~
INSTRUMENT ......§l.Zl
FILE ID
CONC FACTOR
27897
UNITS mq/L
Sample Description: rtP-D-02
07(06(94
Lab No: 02A
Test Code: TC_624
Q
JI
!!
!!
!!
!!
!!
!!
JI
!!
!!
JI
Test Description: REACTIVITY
Collected: 06/23/94 16:25
Method: Stf-846 8.J Test Code: REA.CT.l
PARAMETER
H2S
CH
RESVLT
1.9
ll 6
LIMIT ANALYST
___ _.l ...Ef.
___ .. , ...E!.
Notes and Deli.ni tions tor Chi.s Report:
DATE RUN
UNITS
1/6 -6/29/94
mq/Xq
Page 3
• • Order# B4·06·486
07/12/94 17:07 TEST RESULTS BY SAMPLE
Sample Description: JiP-D-02
Test Description: TCLP HE'I'ALS SCAN
Collected: 06/2J/!J4 16:25
Lab No: 02A
Method: 6010/7470
RESULT SPIKE_RECOV
Arsenic
Barium
Cadmium
Chromium
Lead
Nercu:y
Selenium
Silver
< O. l 00
0.880
<0,010
<0. 010
0. 48!J
<0.002
<D.100
<0.010
86 •
16 •
16 •
18 •
86 •
l05 t
9l t
l1 t
Notes and Definitions for this Report:
DATE Rr:JN
tmITS
07/07(94
mq/L
Sample Description: JiP-D-02
Test Descripcion: TCLP SEMI-VOLATILES ONLY
Collected: 06/23/94 16:25
Lab No: 02A
Method: EPA 625
PARAMETER RESULT LIMIT SPK_RECOV
0-Cresol ~ _..f!..:.l 84
H-Cresol ........!2!, ----'Ll 85
P-Cresol ........!2!, ----'Ll 8~
2, 4,5 Trichlorophenol ........!2!, _..f!..:.l 16
2,4,6 Trichlorophenol ........!2!, ----'Ll 16
Pentac:hlorophenol ........!2!, _..f!..:.l llO
Pyridine ........!2!, __Ll 65
Nitrobenzene ........!2!, _..f!..:.l 82
Hexachloroethane ........!2!, _..f!..:.l '5
He.xachlorobutadiene ........!2!, _..f!..:.l J8
Hexachlorobenzene ........!2!, _..f!..:.l 9J
2,4 Dinitrotoluene ........!2!, _..f!..:.l 15
1,4-Dichlorobenzene ........!2!, _..f!..:.l 65
Notes and Del1.niti0116 tor this Report:
EXTR,\CTEI)
DATE RUN
ANALYST _l!Q
INSTRUMENT --211,Q
FILE ID l374f
06(28/94
07/08(94
a
Q
Q
!!
Q
!!
Q
Q
Q
!!
Q
Q
Q
Q
Test Code: TCLP_N
Test Code: TC'_625
Page 4
• Order I B4-06-486
07/12/94 17:07 TEST RESULTS BY SAMPLE
Sample Description: tfP-D-02
Test Descripr:.ion: TCLP SDII-YOLATILES ONLY
Collecr:.ed: 06/23/94 16:25
CONC FACTOR
UNITS mg(L
Sample Descripr:.ion: cr:MPOSITB D-Fl--F4,G7
Test Description: TCLP VOLATILES ONLY
Collected: 06/24/94 00:00
PARAMETER RESULT
Vinyl Chloride BDL
1,1-Dichloroeehene BDL
Methyl Ethyl Ke Cone BDL
Chloroform BDL
Carbon Ter:.rachloride BDL
Benzene 6.60
l,2-Dichloroet:hane BDL
Trichloroethe.ne BDL
Tecrachloroeehene BDL
Chlorobenzene BDL
l,4-Dichlorobenzene BDL
Lab No: 02A
MeChod: BPA 625
Lab No: OJA
Method: BPA 624
LIMIT SPK_RECOV
_£..:.1 65.S
~ 88.l
_£..:.1 119
-2..:.M 89.4
~ 77 .5
--1l..J}.§. 86.7
--1l..J}.§. 144
~ 105
~ 84.l
~ 105
~ 93.5
Notes and Definitions for this Report:
EXTRACTED
DATE RUN
ANALYST ~
INSTRUMENT ___il1l
FILE ID
CONC FACTOR
UNITS
Suiple Description: WP-D-03
Test Descripr:.ion: R&\CTIVrTY
Collected: 06/24/94 09:05
27898
mq(L
RESULT
07/06/91
J.?
Lab No: 04A
Method: Sfl-846 8.3
LIHIT ANALYST
H2S
r:N 32.5
...1!!!
...1!!!
Notes and Detinitiona tor th.is Report:
Par,e 5 •
Test Code: 1'C_625
Test Code: TC'_624
Q
!!.
!!.
!!.
!!.
!!.
Q
!!.
!!
!!
!!.
!!.
Test Code: R&\CTI
• • Order I B4-06-486
07 /l2/9f 17: 07 TEST RE SUL TS BY SAMPLE
Sample Description: WP-D-03
Test Description: TCLP SE21I-VOLATILBS ONLY
Collected: 06/24/9◄ 09:05
Lab No: 04A
Method: EPA 625
2,4 Dinitrotoluene
l,4-Dichlorobenzene
---~1_.S /l
__ __,, ... s !!.
Notes and Definitions for this Report:
EXTRACTED
DATE RUN
ANALYST _.!§.
INSTRUMENT -l11Jl
FILE ID
CONC FACTOR
13745
UNITS mq(L
06/28(9◄
07/08/94
Sample Description: COHPOSITB D-G1--G5
Test: Description: TCLP VOLATILES ONLY
Collected: 06/24/94 00:00
Lab No: OSA
Method: EPA 624
PARAMETER RESULT LIMIT SPK_RECOV
Vinyl Chloride BDL --...2.:.l 65.S
l,l-Dichloroethene BDL ~ 88.1
Methyl Ethyl Ketone BDL ~ ll9
Chloroform BDL ~ 89.4
Carbon Tetrachloride BDL ~ 77 ·2
Benzene 7.96 ~ 86.0
1,2-Dichloroethane BDL --fL.Qa '" Trichloroethene /;P.L ~ l!Zi
Tetrachloroethene BDL ~ 84iJr,
Chl orabenzene BD!. ~ lQi
l,◄-Dichlorobenzene BDL _Q.:.M 93.5
Note• and Definition• for this Report:
EXTRACTED
DATE RUN
ANALYST ~
INSTROMBNT 5971
FILB ID
CONC FACTOR
27899
UNITS ma/L
07/06(94
0
!l
!l
!l
!!.
!l
!l
!l
!l
!l
!l
!l
Page, •
Test Code: TC'_625
Test Code: TC'.'_624
• • • Order# B4-06-486
07/12/94 17:07 TEST RESULTS BY SAMPLE
Sample Description: IIP-D-04
Test Description: RBA.CTIV!TY
Collected: 06/24/94 15:00
PAR.AMETF:R
H2S
CN
RESULT
J.8
Sl.5
Lab No: 06A
Method: Sfi-846 8.J
LIMIT ANALYST
---~l .JS!!. ---~l .JS!!.
Notes and Definitions tor this Report:
DATE RUN
fJNITS
Sample Description: IIP-D-04
Test Description: TCLP METALS SCAN
Collected: 06/24/94 15:00
PARAMETER
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
7(11 • 1/8/94
mq(Kq
RESULT
<0.100
o. 646
<0.0!0
< 0. 010
<0,050
Lab No: 06A
Method: 6010/1470
SPIKE_RECOV
96 •
92 •
BJ •
87 t
85 t
<0, 002' 109 t
<0.,I00 100 t
< O, 01 O 75 •
Notes and Detinitiona tor this Report:
DATE RUN
UNITS
07/07/gf
m9/L
S11111ple Description: JIP-D-04
Test Description: TCLP SBIII-VOLATILBS QtiLY
Collected: 06/24/94 15:00
PAR.AMETF:R RESULT
Lab No: 06A
Method: BPA 62S
LIMIT SPX_R.ECOV 0
0-Cresol _.J!Q!, ___Q_d, 8f !! H-Cresol _.J!Q!, _Ll 85 l/
P-Cresol _.J!Q!, ~ 85 !!
Test Code: R&\CTI
Test Code: TCLP_lf
Page 8
.. Order# B4-06-486
01 /12/94 11: 07 • TEST RESULTS BY SAMPLE
Sample Description: JIP-D-04
Test Description: TCLP SEXI-VOLATILES ONLY
Collected: 06/24/94 15:00
Lab No: 06A
Method: EPA 625
2, 4,5 Trichlorophenol ____fil2b ----fl..:1. 76
2, 4, 6 Tric-hlorophenol ~ ------2.:..! 76
Pentachlorophtrnol ~ ----fl..:1. 110
Pyridine __J!Q& ---1L.1 65
Nit:robenzene ~ ----fl..:1. 82
Hexachloroethane ~ ----fl..:1. 45
Hexachlorobutadiene ~ --LI ,.
Hexachlorobenzene ~ _LJ 93
2,4 Dinitrot:oluene ~ __Q.:.l 75
1,4-Dichlorobenzene ~ _..Q....l 65
Notes and Definitions for chis Report:
EXTRACTED 06{.28{.94
DATE RUN 07{.DB{.94
ANALYST _!!fi
INSTRUMENT _a.21.Q
FILE ID 13146
CONC FACTOR l
UNITS /JIQ'(L
Sample Description: VS-01 Lab No: 01A
Page •
Test: Code: TC_625
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
Test Description: POLYNUC. ARCWATIC-GC
Collected: 06/24/94 ll:20
Method: EPA 8100/610 Test: Code: PAH_GC
PAJUIHETE:R RESULT LIMIT 0
Acenapht.hene BDL 165 .JJ.
83-32-92
Acenaphthylene BDlt 665. .JJ.
208-96-8
Anth.racene BDL 165 .JJ.
120-12-7
Benzo (a) anthracene BDL 165 .JJ.
56-55-JB
Benzo {a) pyrene BDL 330 .JJ.
50-J2-8
Benzo lb) fl uoran c:hene BDL J.1.0 .JJ.
205-99-2
Benzo (ghi) perylene BDL J,30 .JJ.
191-24-2
Benzo (kl Eluoranc.hene BDL 330 .JJ.
207-08-9
Chzysene BDft J:30 .JJ.
218-01-9
order I B4-06-486
01/12/94 11:01 -RESULTS BY SAMPLE
Sample Descr.iption: vs-01
Test Descript.ion: POLYNUC. ARCMA.TIC-GC
Collected: 06/24/94 11:20
Dibenzo (a,h) anthacene
53-70-3
Fluoranthene
206-44-0
Fluorene
86-7J-7
Indeno (l,2,3-cd) pyrene
193-39-5
Naphthalene
91-20-3
Phenan ehrene
85-01-8-4
Pyrene
Lab No:
Method:
BDL 330
BDL 165
BDL 165
BDL 3JO
BDL 165
BDL 165
BDL 165
Page.
O?A
8PA 8100/610 Test Code: PAH_GC
..!!
..!!
..!!
..!!
..!!
..!!
..!!
Notes and Delini tions for this Report:
EXTRACTED
DATE RWI
ANALYST ....Ir
INSTRUMENT _..1.ill
06(28/']4
06/30/94
PAH06JO
33
FILE ID
CONC FACTOR
UNITS ua/Kq
COLUMN DB-SMD
Bionomics Laboratory, ~-
• South Carolina Division.
200 Rich Lex Drive Phone: [phone]
Lexington. South Carolina 29072 Fax: [phone]
South Carolina Certification Number. 96012
South Carolina Lab ID Number: 32117
NU-WAY
1741 CALKS FERRY RD
LEXINGTON, SC 29073
Attn: J. ROBLEY
Invoice Number:
Sample Sample
Number ---~D~e~s~cArAi~p~tAio~n,._, __ _
01 COMPOSITE E-Ol--E-05
Order#: B4-06-573
Date: 07/13/94 09:01
Work ID: PROJ# 94047
Date Received: 06/30/94
Date Completed: 07/13/94
Client Code: NU_WAY_JR
SAMPLE IDENTIFICATION
Sample Sample
Number ---~D~e~s~cArAi~p~tAi:on,._, __ _
02 WP-E-01
Certified By
MARK KROMIS, CHEMIST
'
CUSTODY TRANSFERS: ...
J!,6~ Bionomics l.'.iil>qrato~, Inc. South Carolina Division \ ' 200 Rich Lex Drive Lexinglon, Soulh Carolina 29072 [phone] Fax [phone] SC LAB ID #32117 SC CERT. 96012 CHAIN OF CUSTODY RECORD
• ---
•
-I
V
Order# B4-06-573
07 /13/94 09: 01
S1111Jple: 02A WP-E-01
•
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
• TEST RESULTS BY SAMPLE
Collected: 06/28/94
Result
> 70
PASS
ll. 71
Limit Uni ts
Degrees Cent.
PASS/FAIL
pH UNITS
Page 2
Analyzed ~
07 /07 /94 SMR
07/01/94 TY
07/01/94 KM
• • Order# B4-06-573
07/13/94 09:01 TEST RESULTS BY SAMPLE
Sample Description: COMPOSITE B-01--B-05
Test Description: TCLP VOLATILBS ONLY
Collected: 06/28/94
Lab No: OlA
Method: EPA 624
PARAMETER RESULT LIMIT SPK_RECOV
Vinyl Chloride BDL --9..:.1. ., l,l-Dichloroethene BDL ~ lli; Methyl Ethyl Ketone BDL --9...:.1. 102 Chloroform BDL ____Q_,M 97. l Carbon Tetrachloride BDL ~ 98.2 Benzene 1.8 ~ l 04 1,2-Dichloroethane BDL ~ llJ Trichloroethene BDL ~ 100 Tetrachloroeehene BDL ~ 92.7
Chlorobenzene BDL ......L..Q1 100 1,4-Dichlorobenzene BDL ~ 83.9
Notes and Definitions tor this Report:
EXTRACTED
DATE RUN
ANALYST ~
INSTRUHENT __J,_2J.l
FILE ID 27918
07/06/94
07/07/94
CONC FACTOR 1
UNITS mq/L
Sample Description: IIP-B-01 Lab No: 02A
t
t
t
t
t
t
t
t
t
t
t
Test Description: REACTIVITY
Collected: 06/28/94 15:58
Method: SW-846 8.J
PARAM>:TER
H2S
CN
RESULT LIMIT ANALYST
___ _.2~ . .._7 l ....21
---~/~O l ....21
Notes and Definition• tor this Report:
DATB Rrnl
UNITS
1/7-ll/94
mq/Xq
Test Code: TC_624
0
!l
!l
!l
!l
!l
!l
!l
!l
!l
!l
Test Code: REA.CTI
Page 3
• • Order# B4-06-573
07/13/94 09:01 TEST RESULTS BY SAMPLE
Sample Description: WP-B-01
Test Description: TCLP MBTALS SCAN
Collected: 06/28/94 15:58
Lab No: 02A
Method: 6010/1410
PARAMETER
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
RESULT SPIKE_RECOV
<0 .100 21 t
0.414 81 t
<0.010 90 t
<0.010 87 t
<0.050 78 t
<0. 002 109 t
< O. l 00 101 t
<0.010 2 t
Notes and Definitions for this Report:
DATE RUN
UNITS
01/07/94
mq(L
Sample Description: WP-B-01
Test Description: TCLP SElfI-VOLATILBS ONLY
Collected: 06/28/94 15:58
Lab No: 02A
Method: EPA 625
PARAMETER RESULT LIMIT SPK_RECOV
0-Cresol BDL ----2..:.l 76 t
M-Cresol BDL _..Q..:.l 75 t
P-Cresol BDL _£.:.1. 75 t
2,4,S Trichlorophenol BDL ______Q_d 60 t
2,4,6 Trichlorophenol BDL --2..J. 60 t
Pentachlorophenol BDL _..Q..:.l 87 t
Pyridine BDL _Jl.d. 74 t
Ni trobenzene BDL ____QJ 85 t
Hexachloroethane BDL _..Q..:.l 48 t
Hexachlorobutadiene BDL __Q,;_l 39 t
Hexachlorobenzene BDL ~ 94 t
2,4 Dinitrotoluene BDL ~ 83 t
l,4-Dichlorobenzene BDL ~ 68 t
Notes and Definitions for this Report:
EXTRACTED
DATE RUN
ANALYST ..1!!i.
INSTRUMENT __zfil
FILE ID 13752
07 /01/94
07/09(94
Q
l!
l!
l!
l!
l!
l!
)l
)l
)l
l!
)l
!!.
l!
Test Code: TCLP_H
Test Code: TC_625
Page 4
• • Ord,r # B4-06-573
07/13/94 09:01 TEST RESULTS BY SAMPLE
Sample Description: WP-B-01
Test Description: TCLP SEMI-VOLATILES ONLY
Collected: 06/28/94 15:58
CONC FACTOR 1
UNITS mg/L
Lab No: 02A
Method: BPA 625 Test Code: TC_625
Order# B4-06-573
07 /13/94 09: 01 •
IGNITABILITY-PENSICY MARTEN
Method:
Samp Sample Description
02A WP-E-01
PAINT PILTBR
Method: 9095
Sa.mp Sample Description
02A WP-E-01
pH
Method: BPA 150.l
Samp Sample Description
02A WP-E-01
• REGULAR TEST RESULTS BY TEST
Minimwn: Maximwn:
Result JlUill Limit
> 70 Degrees Cent.
Minimwn: Maximwn:
Result Units Limit
PASS PASS/FAIL
Min.imwn: Maximwn:
Result Units Limit
ll. 71 pH UNITS
Page 6
Prel2_ared Anali::zed ID:
07/07/94 SMR
PreQared Anali::zed ID:
07/01/94 TY
Prepared Anali::zed ID:
07/01/94 KM
Bionomics Laboratory, Inc.
• South Carolina Division.
200 Rich Lex Drive Phone: [phone]
Lexington, South Carolina 29072 Fax: [phone]
South Carolina Certification Number: 96012
NU-WAY
1741 CALKS FERRY RD
LEXINGTON, SC 29073
Attn: J, ROBLEY
Invoice Number:
Sample Sample
Number Description
01 VS-02
South Carolina Lab ID Number: 32117
Order#: B4-06-579
Date: 07/05/94 13:35
Work ID: PROJ# 94047
Date Received: 06/30/94
Date Completed: 07/05/94
Client Code: NU_WAY_JR
SAMPLE IDENTIFICATION
Sample Sample
Number __ __;D~e~s~c~r~i~p~t~i~o~n __ _
Certified By
TERESA HUBBARD, LAB MGR
\IC...-{)?
l'~ Bionomi<;s L.:~bqratory, Inc. Soulh Carolina Division \ ·• 200 Rich lex Drive Lexinglon, Soulh Carolina 29072 [phone] Fax [phone] · SC LAB ID #32117 SC CERT. 96012 CHAIN OF CUSTODY RECORD
•
-'
V
Order# B4·06·579
07/05/94 13:35
Sa.mple Description: VS-02
• • TEST RESULTS BY SAMPLE
Lab No: OlA
Test ~scripci.on: POLYNUC. ARQQTIC-GC
Collected: 06/28/94 13:00
Method: BPA 8100/610 Te.st Code: PAH_GC
Acenaphthene
Acenaphchylene
208-96-8
Anthracene
120-12-7
Benzo (a.J onthracl!lle
Benzo (a) pyrene
50-32-8
Benzo (b) tluoranchene
205-99-2
Benzo (1hiJ pezylene
191-24-2
Benzo (k) fluoranthene
207-08-9
Cluysene
218-01-9
Dibenzo (11.,h) anthacMe
53-70-3
Fl uoranchene
206-44-0
Fluorene
86-73-7
Indeno (1,2,3-cd) pyrene
193-39-5
Naphthalene
91-20-3
Phenanch.rene
85-01-8-4
Pyrene
129-00-0
RESULT
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
741
453
LIMIT 0
__ ... 1c,6s,5 .JZ
--~le,6s,5 .JZ
--~'"""5 .JZ
--~'"""5 .JZ
--~'"'"'o .JZ
--~'"''"'o .JZ
--~'"'"'a .JZ
--~'"''"'a .JZ
--~''-''"'o .JZ
--~'"''"'o .JZ
---'''"'""5 .JZ
---''""~5 .JZ
--~'"''"o .JZ
--~'"""5 .JZ
165
165
Notes and Det,ini t:.1ona tor thia Report:
EXTRACTED
.DATE RUN
ANALYST !2II
INSTRrR!EN'l' ---1.tQ.Q
FILE ID
07/01/94
07/01(94
CONC FACTOR 3]
UNITS uq(Kq
COLUMN DBSffS
Page 2
Bionomics JJ~ry., Inc. South Carolina Division X
200 Rich Lex Drive Lexington, South Carolina 29072 [phone] Fax [phone] SC LAB ID #32117 SC CERT. 96012 CHAIN OF CUSTODY RECORD
Clienl Nem•Jvu-u_,b.__1,: F;jV/nY)J{e/J""lv.--1 J 17->c-, \_
Address: / 741 ( ~ lkf--l-ern-1 1?,0 J..c>ict'r,,,--(G, :s .c. Reri/Prol.Maneoer: '7J: P,,.,b /,,::,,1 ..._} Phona f: '1,S '7-9) '1...J Proiecl ID: <?L/M? _J P.O.f:
'
CUSTODY TRANSFERS:
0•1•: Tin-.:
•
'
V
•
Bionomics Laboratory, 1'1.c.
South Carolina Division.
200 Rich Lex Drive Phone: [phone]
Lexington, South Carolina 29072 Fax: [phone]
NU-WAY
1741 CALKS FERRY RD
LEXINGTON, SC 29073
Attn: J. ROBLEY
Invoice Number:
Sample Sample
Number Description
South Carolina Certification Number. 96012
South Carolina Lab ID Number: 32117
Order#: B4-05-572
Date: 07/13/94 08:58
Work ID: PROJ# 94047
Date Received: 05/30/94
Date Completed: 07/13/94
Client Code: NU_WAY_JR
SAMPLE IDENTIFICATION
Sample Sample
Number Description
01 COMPOSITE E-05--E-10 "j;;,,.': ILbtruJ
Certified By
MARK KR.OMIS, CHEMIST
i_
'i!'S., 1· . . ' -1 · '
. I • ; . ) ;
Bionomics L:.abor~tory, Inc.
· South_ Carolin~ ~!v'lslon ·
200 Rich Lex Qrive Lexingto/( South Carolina 29072
(803) 796--8989 ·Fax'(803) 796--1602
SC LAB ID #32117 i SC CERT. 96012
CHAIN OF CUSTODY RECORD
:t '.
Client Nome: Nu-l<.Ja.u Envt'nrH-er,-f-o..{J 1Ln~, -
Address: )'JLJ/ <'al'r--1 ~errv !2cfl. LEv,',,-,,;--fcn ~-C'.
Ren/Prol.Manaoer: '-/_ '1,--.t-/.,:,,.'-' Phone I: '-'9,<;F')-9/ ?. '\'
Prolect ID: CJ/J /16 '7 , J P.O.#:
Collected bv: ~ ft TI • A
Samnle ID Date Time c ........ Samole Location
I ./'
I; ./'
t==:--r,o.
,. --
E-10
·CUSTODY TRANSFERS:
I.· R~fu,ho~ 0Cfd1µ
_,
R~v•d. by: Time:
2. -----~-~
3. --------"
-laboratory Remarks:
.t> .. 1.! .. :0ntv;.,·: w.o:;,-· >i5t:l/2~/@51:t;;;.-•·•0·-·•··•-···
~•g\~r'~ !~:r:. •'7 ---__ . ___ --.. _-.. _--_
.jv i> -~
of' F -()/ o ._J A,; • --1-
~ 5-Vorl'>.
,, 9-h,. ..,,,,, J'l'I/(_ ,C,
Order# B4•06·572
07/13/94 08:58
Sample: 02A WP·B-02
•
Test Description
IGNITABILITY•PENSKY MARTEN
PAINT FILTER
pH
• TEST RESULTS BY SAMPLE
Collected: 06/29/94
Result
> 70
PASS
5.30
~ Units
Degrees Cent.
PASS/FAIL
pH UNITS
Page 2
Analyzed fl:,::
07/12/94 SMR
07/01/94 TY
07/01/94 KM
, .
I • • Order# B4-06-572
07/13/94 08:58 TEST RESULTS BY SAMPLE
Sample Description: COMPOSITE E-06--B-10
Test Description: TCLP VOLATILES ONLY
Collected: 06/29/94
Lab No: 01A
Method: BPA 624
PARAMETER RESULT LIMIT SPK_RECOV
Vinyl Chloride BDL -Ll 84
1,1-Dichloroethene BDL ~ lll
Hethyl Ethyl Ketone BDL -Ll 102
Chloroform BDL ---12..:..Q2 97.1
Carbon Tetrachloride BDL ~ 98.2
Benzene BDL ~ 104
1,2-Dichloroethane BDL ---1L.M. ll3
Trichloroethene BDL ~ 100
Tetrachloroethene BDL ~ 92,7
Chlorobenzene BDL ~ l 00
1,4-Dichlorobenzene BDL ~ 83.9
Notes and Definitions tor this Report:
EXTRACTED
DATE RUN
ANALYST ~
INSTRUMENT _l.fil
FILE ID 21917
07 /06/94
07 /01 /94
CONC FACTOR l
UNITS mq/L
Sample Description: WP-E-02 Lab No: 02A
• • • • • • • • • • •
Test Description: REACTIVITY
Collected: 06/29/94 11:10
Method: SW-846 8.3
PARAMETER
H2S
CN
RESULT LIMIT ANALYST
--~B=D"'L l. 0 _JS!:!
--~·=D"'L l _JS!:!
Notes and Definitions for this Report:
DATE RUN
UNITS
7(7-ll/94
mq/Xq
Test Code: TC_624
Q
!!
!!
!!.
!!
!!.
!!.
!!
!!.
!!
!!
!!
Test Code: REA.CTI
Page 3
i .. • Order# B4-06-572
07/13/94 08:58 TEST RESULTS BY SAMPLE
Sample Description: JIP-B-02
Tesc Description: TCLP SESI-VOLATILES ONLY
Collected: 06/29/94 11:10
CONC FACTOR 2
UNITS mg/L
Lab No: 02A
Method: EPA 625 Test Code: TC_625
.ionomics Laboratory,,.
South Carolina Division
200 Rich Lex Drive Phone: [phone]
Lexington, South Carolina 29072 Fax: [phone]
NU-WAY
l 741 CALKS FERRY RD
LEXINGTON, SC 29073
Attn: J. ROBLEY
Invoice Number:
Sample Sample
Number Description
South Carolina Certification Number. 96012
South Carolina Lab ID Number: 32117
Order#: B4-07-020
Date: 07/05/94 13:39
Work ID: PROJ #94047
Date Received: 07/01/94
Date Completed: 07/05/94
Client Code: NU WAY JR
SAMPLE IDENTIFICATION
Sample Sample
Number --~D~e~s~c~r~i~p~t~i~o~n~--01 VS-03 NW LAGOON FLOOR
Certified By
TERESA HUBBARD, LAB MGR
Bionomics Laboratory, Inc.
South Carolina Division -et' fl~ tusk ('72-hi?_.
'1"UfNA(c)U--d _j ()', y 0 -(8 200 Rich Lex Drive Lexington, South Carolina 29072
[phone] Fax [phone]
SC LAB ID U32117 SC CERT. 96012
CHAIN OF CUSTODY RECORD
Clionl Nnmo: A / /, 1 r:_ • ; 11 ·-r-, / I/ t.....l -U--,JO..<../ r/} VI n.1-it((!.,.-,TCLJ/ , ,L.J;(',
Reo/Proi.Manaoor: 'J". l!able11 J Phone #:-9.J?-9 /'7..._')
Proiecl ID: q/jr) <{'J / P.O.#:
Collocled bv: /.(, fk:O.Z~
Semnle ID 08te Time Semol8 locelion
... ,, ...
' \\',:)-. ~. . /
.v . '
I
•
----
I ◄t, ,,,, '',_'):; · ,,,,• :i-'1 •'., IP""..-cHi L. ieat/1.( f~
VS-0'2,
lt---t--t--+--t-------t-
1
-l--+--+---lf-----t-l---+--l--f--l--------l• i
CUSTODY TRANSFERS:
1. "7{'R~ V -
A•ceiv•d by: Date: Time:
2. -------~
3. --------
.
Lebor8tory Remarks:
f.o-(lott5.
• • •Order# B4-07-020
07/05/94 13:39
Sample Description: VS-03 NW LAGOON FLOOR
Test Description: POLYNUC. AROMATIC-Ge
Collected: 05/29/94 15:07
TEST RESULTS BY SAMPLE
Lab No: OlA
Method: EPA 8100/610 Test Code: PAH_GC
PARAMETER RESULT LIMIT Q
Acenaphthene BDL 1650 ...!!.
83-32-92
Acenaphthylene BDL 1650 ...!!.
208-96-8
Anthracene BDL 1650 ...!!.
120-12-7
Benzo (al anthracene BDL 1650 ...!!.
56-55-38
Benzo (al pyrene BDL 3300 ...!!.
50-32-8
Benza (bl fluorant:hene BDL 3300 ...!!.
205-99-2
Benzo (ghi) perylene BDL 3300 ...!!.
191-24-2
Benzo (kl fluoranthene BDL 3300 ...!!.
207-08-9
Chrysene BDL 3300 ...!!.
218-01-9
Dibenzo (a,h) anthacene BDL 3300 ...!!.
53-70-3
Fluoranthene BDL 1650 ...!!.
206-4-11-0
Fluorene BDL 1650 ...!!.
86-7 3-7
Indeno (1,2,3-cd) pyrene BDL 3300 ...!!.
193-39-5
Naphthalene BDL 1650 ...!!.
91-20-3
Phenan ehrene BDL 1550 ...!!.
85-01-8-4
Pyrene BDL 1650 ...!!.
129-00-0
Notes and Definitions for this Report:
EXTRACTE:D 07 (..01/..94
DATE RUN 01 t..01 /..94
ANALYST Q!r
INSTRUMENT ---1.!QQ
FILE ID
CONC FACTOR JJO
UNITS ug,!'.Kg
COLUMN DBSMS
Page 2
.Bionomics Laboratory, A.
South Carolina Division
200 Rich Lex Drive Phone: [phone]
Lexington, South Carolina29072 Fax: [phone]
South Carolina Certification Number: 96012
NU-WAY
1741 CALKS FERRY RD
LEXINGTON, SC 29073
Attn: J. ROBLEY
Invoice Number:
Sample Sample
Number Description
01 COMPOSITE E-1l--E15
South Carolina Lab ID Number: 32117
Order#: B4-07-021
Date: 07/14/94 10:28
Work ID: PROJ #94047
Date Received: 07/01/94
Date Completed: 07/14/94
Client Code: NU_WAY_JR
SAMPLE IDENTIFICATION
Sample Sample
Number --~D~e~s~c~r~i~·p~t~i~o~n~--
02 WP-E-03
~ C dJ~ .. /2.fu / JJ
Certified By
TERESA HUBBARD, LAB MGR
-it' f 1~ eus 1-.. l,., 2--ht!_.
-+ut-NPrrou-d J CY1 y:5-~
Bionomics Laboratory, Inc.
South Carollna Division
200 Rich Lex Drive Lexington, South Carolina 29072
[phone] Fax [phone]
SC LAB ID U32117 SC CERT. 96012
CHAIN OF CUSTODY RECORD
Client Nome: A / /. ~ r-_ • I. 11 ·-r-_ /1/ 1....l -1.....1....JC'-<-/ r /Jvtni-,tte,,-,ra.Y , -1... n<!,
Aeo/Proi.Manoner: 'J' . .Pa bleu J Phone /JC07 -91 ·7..)
Proiecl ID: q/;(1 <('7 f P.O.#:
Collected bv: J{ HC::or2-'!..-
Semnle 10 Date Time c__.c-.,.~ S11mpl8 location
I .----
I -I l.c---
I L---
J "/
2.. ~ ........ \\';>-,!', -/
.... ,
IP•o• _._. of ~ Oa1e Due: C-
. . .. ·· . ;I::-,.
.. , OJ ._v
I
•
.
lf------+---+---+---t-----1--• +---f--1---,1---+--+-t-+---+-t--~---
CUSTODY TRANSFERS:
1. ""[A~ V -
Time:
2. --------
3. --------
.
Leboretory Remarks:
• • Order# B4-07-021
07/14/!,4 10:28
Sample: 02A WP-E-03
Test Description
IGNITABILITY-PENSKY MARTEN
PAINT FILTER
pH
TEST RESULTS BY SAMPLE
Collected: 06/30/!,4
Result
> 70
PASS
5.16
Limit Units
Degrees Cent.
PASS/FAIL
pH UNITS
Page 2
Analyzed
07/12/94
07/05/94
07/01/94
ID:
SMR
DTY
KM
• • Order# B4-07-021
07/14/94 10:28 TEST RESULTS BY SAMPLE
Sample Description: COMPOSITE E-11--815
Test Description: TCLP VOLATILES ONLY
Collected: 06/30/94
PARAMETER RESULT
Vinyl Chloride BDL
l, 1-Dichloroethene BDL
Methyl Ethyl Ketone BDL
Chloroform BDL
Carbon Tetrachloride BDL
Benzene BDL
1,2-Dichloroethane, BDL
Trichloroethene BDL
Tetrachloroethene BDL
Chl orobenzene BDL
1,4-Dichlorobenzene BDL
Lab No: OlA
Method: EPA 624
LIMIT SPK_RECOV
-----1!..:.1. 84 •
~ 111 •
-----1!..:.1. 102 •
~ 91.1 •
~ 98.2 •
~ 104 •
~ 113 •
~ 100 •
~ 92.7 •
--1l..:...Q§_ 100 •
~ 83.9 •
Notes and Definitions tor this Report:
EXTRACTED 07 /06/94
DATE RUN 01/01/94
ANALYST JLS
INSTRUMENT --1.211.
FILE ID
CONC FACTOR
UNITS
Sample Description: WP-E-03
Test Description: REACTIVITY
Collected: 06/30/94 09:40
PARAMETER
H2S
CN
27919
mq/L
RESULT
BDL
BDL
Lab No: 02A
Method: SW-846 8.3
LIMIT ARALYST
---~1 ..JS!i
..JS!i
Notes and Definitions for this Report:
DATE RUN
UNITS
1(1-11/94
mgKq
Test Code: TC_624
0
!!
!!
!!
!!
!!
!l
!!
!l
!l
!l
!l
Tesc Code: REA.CTI
Page 3
• • Order# B4-07-02l
07/14/94 10:28 TEST RESULTS BY SAMPLE
Sample Description: WP-E-03
Test Description: TCLP METALS SCAN
Collected: 06/30/94 09:40
Lab No: 02A
Mechod: 6010/7470
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
RESULT SPIKE_RECOV
<0.100 98 •
l.88 107 •
<0. 010 77 •
<0. 010 82 •
< 0. 050 80 •
<0.002 100 •
<0.100 112 •
<0. 010 39 •
Notes and Definitions for this Report:
DATE RUN
UNITS
07(13/94
mg/L
Sample Description: WP-E-03
Test Description: TCLP SEMI-VOLATILES ONLY
Collected: 06/30/94 09:40
Lab No: 02A
Method: EPA 625
PARAMETER RESULT LIMIT SPK_RECOV
0-Cresol -----1ll2b ----12..:.l.. 92 • M-Cresol -----Ell: --12..2 92 • P-Cresol ~ --..£.:2 92 • 2,4,5 Trichlorophenol ____N2.b --Ll 87 • 2,4,6 Trichlorophenol ~ _____Q2 84 • Pentachlorophenol _..£Qf --12..2 114 • Pyridine ______fil2b, ~ 0 • Ni trobenzene ~ --12..2 81 • Hexachl oroe thane _l!Qf --12..2 53 • Hexachlorobutadiene ~ ----12..:.l.. 44 • Hexachlorobenzene _..fill.f --12..2 89 • 2,4 Dinitrotoluene ______fil!b, -.Q..d 68 t
l,4-Dichlorobenzene ----1lli, ~ 76 •
Notes and Definitions tor this Report:
EXTRACTED
DATE RUN
ANALYST MG
INSTRCJMENT 5970
FILE ID 13166
07/08/94
01/12/94
0
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
!!
Test Code: TCLP_H
Test Code: TC_625
Page 4
• Order# B4-07-021
07/14/94 l0:28 TEST RESULTS BY SAMPLE
Sample Description: WP-E-03
Test: Descript:.ion: TCLP SFHI-VOLATILBS ONLY
Collected: 06/30/94 09:40
CONC FACTOR 2
UNITS mq/L
Lab No: D2A
Method: BPA 625
• Page 5
Test Code: TC_625
• Bionomics Laboratory, •· South Carolina Division
200 Rich Lex Drive Phone: [phone] Lexington. South Carolina 29072 Fax: [phone]
NCT-WAY
1741 CALICS FERRY RD
LEXINGTON, SC 29073
Aten: J. ROBLEY
:Invoice .NI.Unber:
S;ur,ple Sample
South Carolina Certification Number: 96012 South Carolina Lab ID Number. 32117
Order#: B4-07-ll9
Date: 07/12/94 14:08
Work ID: PROJ #94047 S-8779
Date Received: 07/08/94
Date Complered: 07/12/94
Clienc Code: NU_PIAY_JR.
SAMPLE IDENTIFICATION
sample Sample Number ---~D~es~c~r~1~·p~t~i~o~n._ __ Number __ _,D~e~s~c~r~i~p~t~i~on,.__ __ _ 01 VS-12 S-8779
'v<=liJ
Cerci.fied By
TERESA Ht/BB.ARD, LAB MGR
Order# B4·07·ll9
07/l:1/94 l4:08
S,urple Desa1pcion: va..-12 s-s11,
• TEST RESULTS BY SAMPLE
L.b Ho, 01A
rest JJ~•cripeJ.aa: CAR~C' PAR by GC/IIS Hcthoc:I: u.a. B270
Collcc-tcdr 0?/0~/!H ltr50
PAJW!STU RSGW.T ROL Q
Jilenzo t•I .nchracene ,!S.9 330 ....
56-5.5-JB
Chzy,rcn~ ,., 330 ..:!.
21s-01-,
Bon,o /bl Eluor.tnC.ben. BDt .no ..J!
:10s-n-2
B"""o /kl Lluor.a.atb.an• BDL .110 ..J!
207-08-9
""""" l•I pyrene BDL JJO ..J!
50-34-8
Dibenso l•,hJ ant.haceAe BDt JJO .Jl
53-10•3
.tndmo fl,2, J-cd) J>Yr408 JIDL .?JO ...!!.
193 .. 39.5
St.JXRCCA%'S t == LD<ITS
l,2-Dichloll:lbc:nrene _.!! ---1.§. -1.l.2
Nicrobe.a~en• -d5 __ ,_, ......ll _il£
2-Fluorcbiphenyl --E: __zg . ....J.ll
'terphenyl •dl4 ----1ll _..ll _!1.Z
Noce• ,and Dcl.i.4J..t.1ons tor cJu.s ~ort:
zrIXACT&O
==
AJJN;rsr ...!!2
INSffOl'!Dfl'. 5910
FILS n, lJ76J
DIL. FACTOR __ 1
-~9 -lJ!lL5s.
COLCHN m-s
07/ll/94
07/!l/Jf
• E'age 2
--:~ ....... ._ ·,.._..-· ... ..,.., ....... --'-'-' ... ~ ............ , , .. .__. ._.--.......... ,'-<,, ..... ,. .... .., . ....,_._ .................... ,-. .., ...
• Bionomics Laboratory, 41c.
South Carolina Division
200 Rich Lex Drive Phone: [phone] Lexington, South Carolina29072 Fax: [phone] South Carolina Certification Number: 96012
NU-WAY
1741 CAI.KS .!inRY RD
LJi/XIl/GTON, SC 29073
At:t:l!: J. ROBLEY
Invoice Number:
Sample Sample
Numb~;:-Descri~tiell
01 VS-04 S-8771
02 vs-os 5-8772
03 VS-06 5-8773
04 VS-07 S-8774
05 VS-08 S-877S
South Carolina Lab 10 Number: 32117
Order#: 84-07-121
Date: 07/15/94 12:22
Work ID: PROJ #94047 s-8771-8,81
D.>.ee Received: 07/08/94
Date Completed: 07/1S/94
Cl.ient Code: NtT_WAY_JR
SAMPLE IDENTIFICATION
Sample Sample
Number nes,r;r.ipt:ion
06 VS-09 S-8776
07 VS-10 5-8777
OB VS-11 5•8778
09 EQ•BLX-01 S-8781
TERESA HUllB;uw, LAB MGR
Client Name:
Address:
oou
.eboratory Remerks:
Bionomics Lat •. }atory, Inc.
South Carolina Division
200 Rich Lex Drive Lexington, South Carolina 29072
[phone] Fax [phone]
SC LAB ID #32117 SC CERT. 96012 CHAIN OF CUSTODY RECORD
~ ll ·;; ;;
8
~ 0
'
Parameter
Analysis
~it~li r1ff tt1t1mt1ri li11tWI]Pt;iJ,t}; ·\r•
\"g~ ,: ;' 'or·.•·• .. ,. ;' b•ti bu,: --'-~ /V\/-,:::·_:: .. ··-·-
• • Order# B4-07·121
0'1/15/94 l.'l:22 TEST RESULTS BY SAMPLE
Sampl~ De.scripdOD.: VS-Of 8-8171 Lab No: a.a
%'ewe Descr1pc.J.ooi ~c P.ur t,y ,:C/llS lteCIJod: BPA 8270
CcJlccced; D7/05/94 JP,30
PARAMBTER RESULT >QL '1
Scnzo (A) aaelu-.a:cene
5d-~5-JI
Olzysc:e
218-01-9
Ben2C (bl £lvora.arbeD.e
205-99-2
Bonzo (Jc) Eluor.anehene
207-0B-9 -(•J pyrene
so-J2-s
Dibe=o (•,hJ .anth.iceae
iJ-70-3
llldeno ll,2,J•cdJ pyrene
&ORRoc::ATS
1.2-DichJorobenzetJe
Ni. trobe:lzene -dS
2-Flucrobiphcnyl
Tezplle:nyl-dl4
JSJ-39■5
tll'C'CVD.Y
____,£_
____u
__!Z
_.lll
BO& :;!~ ..!l.
m,I, vo .Jl
BDL 120 ..!l.
BDL 23.0 ...!l
BDL u.o ...!l
w. JJO .Jl
BOL '30 ..!!.
UJU:rs
-l! -...l.l.Q
----3]. -ill
_2£ --ill:
-l! ....J1Z
Noeeo 4Dd De£.ini;.icos tor this Repcrt.1
DrT1IACTHD
A\TE .RDN
AllAL'fST ..5
DISTRU!ISNT _...U.Z.2
FIL'R ID jJ116
D!L, FAC'TOR __J.
UN7TS 1,.q/Xg
rrz s
07/11/Jf
07/1]/-'4
L.ab NO: Q.2.\
r~.t: Dcsic.r.ipticn, CAB:~C' .PAB by GC/'IIS Nee.hod: BP.I. 11270
Ccllccced', 07/0s/,t 16:JS
P.lR.V<S'l'BR
B~zo (ll.} illlt:hracene
56-55-JB
Chrysene
.usm.:r Q
__ ,.,,.,o. ..!l.
BPL -~•,_,J_.o ..!!.
'l'cst code: CPNI_S
Page 2
---------,,_, . ----· ·--· .. '. -· . . -· ·-• Qrder I Bf-07-J.21
07/JS/,f 12,~ I¥1 R.ESCTLTS Bf SN1PLE
Saq>J.e DcacripCS.Oll1 VB-OS S-8772 Lab Nor 02A resc Description.: G\RCINO::tKIC PAN by GC/1!SS lfethod: U.& B210
Collected; 07/0S/'4 16135
2i,.01-,
~ ...... (b) Ll~thcne
205-99-2
Bcuo (!c) Cluor.mchane
201-0B·S
Benso (•J pyrtme
50-32-B
D.ilHmzo ta.taJ ;mcharmie
5J-10-J
Indeno (1,2.l-o:JJ pyrene
lSJ•J9-S
==
J,3-Dichloroben~c:ie
N.i. tZ'QDC!zeae -dS
2-Tluoro/Jipht:Dyl
l'ezphcnyJ -dlf
tABCOV&:r
___E.
~
.__,!2
--U!
llDL ~20 Jl .,,, 120 .J!
BllL ~i)O Jl
!!!2L J20 ..!Z
!!!2L uo ..!!
LDll'f'S
_./.!. ..J},J!
_n . -!Ze
_l£ ~
___a . -llZ
J,locea and Dt!l.ini. t.ioa• tor c.b.!• .Report,
== m.ra RUN
....,,,,,,rsr ..!!,
INS"Tl>OHE!IT ~
PILB I.D 23777
Dll., PACTOR -l = ....l!!JLg
COL0Kli rrr s
07/ll /9-f.
01(l3/94
&.urple Descrs.pe.ign r n-o& S-8773 i,.t, lio: OJA
Teat Dcacripc.i.oa: ORCIJ10CI/N1C I.All by GC/11$ Hctbod: EPA 8270
Collected: 07/06/14 OJ,20
"'"""""""' RBW.T PQL "
Benzo /al iiZI. t.hracerut Ill)~ jlO J!
56-55-JB
Chzy&ea• 1!!l!, ~~o _fl
2l.8-0l-J
BelaO tbl llworuchm::ie BD~ ~lO Jl
205-19•2
Bcnzo lk! :tluor44tbe.ae l!!1l, JJO ...!!
207-08-J ........ (a) ,,,,...,,. llDL ~~o Jl
50-J2-B
•
T~e Code: CPAH_s
Test C~: aAH_S
~----___ ..., • Order# 84-07-121
01/l.5/~4 12;22 'ttST rursm.rs BY SAMPLE
Saple ~r:ripcJctu VS-06 S•817J Lab No: DlA Ten Descr.tpt.ioat CAPCIM;'C~r PAR by c;c/kS 1tethcd: BPA 8270
Collectod'r 07/06/1◄ 09120
Diber.ul:o {a,hJ iinc.baeenc
51-70-J
ZndfUlD 11.2,J-cd) wren•
SUAAOG.mr
l,2-DichJ.crobenaena
lli~robeAsc:n• -dS
2-rluo.robipbenyl
Tezpheayl-dlf
UJ-JJ-5
tZ!CDVXRY
~
__.2i
____22.
. ..--JU
BOL ,po .J!.
lJP.L J~O .J!.
UK!TS
_.},§. -~
-U ....l1£.
~ -.lll
--li -_il!.
Notc.s llnd De:ti.ttlci,ana ~or t.hi..s Reporc,
z:x:rR.AC'lSD D7{l1(94
D.U'S 6JJR 07/13/94
..WU.YS't ..1t!i
1DIS'U.CNEN'1' ~
l'ILS;ID 1377(/
DXL, ru:ro,,. -1.
UNITS ~
COLCIMN ms
Sample Dr:aciipcion, 'VS-07 S-B774
Tue Descripr:Jon, CA«t..LM.,G.kSl"-" PAH by GC/JG
Coll~r:tcdl 07/06/94 lJrJO
wb Jlo: oa
/fethoth II.PA 8210
PARAJ<ET1lR RJ;$ULT l'Ql. Q
Bcnzo (a) anthr.1cene ~ ,UQ ..1/
56-SS•JB
CJ:iry3e:ae BDL u.o ..1! 21, .. 01 .. 9 -·Q (bl tlucz.aachane .!DL j30 ..1!
205-99-2
Benzo (lt/ :tluOZ"aD theme BDL 3~0 .Jl
201-011-11
aenzo taJ pyrr:ne BDL 3io ..1!
50-J2-i
Dib,o,ao t • • h J .n t:h.i.c'en.e BDL ~a!!i! .J!
5J-7Q .. J
Indong (1,4,J-r:d) pyn:no BDL ;pQ ..J!
193-J!J-5
SC/llROG.\m tllCOVBRY LIHITR
l,2-D!chJ.on;ibc:nsc• -----ll -1! -.....!J,2
• ,....,., .
:re.st Code: au_s
------___ -, • Order II B4-07-l2l
01n.sJ91 1.2:aa TEST RRSm,TS BT SAMPLR
S.mpJe Doscr:tpclon: V.•01 S-877' Lab NOJ OM
TeBC .oe,cripCiQIJ: CAJtCDDiBJaC .PAil by r;c/11$ · llccllod: DA. 1270
Collected: 07/06/94 11:JO
Nitrcbanzene -d5
2-Fluorcb.iphcnyl
l"ez;,hmiyl-dlf
Notes .and DefUJir:ioas for CA.f.s ll,:port:
EXTAACTED 07/lJ/2:t
DA'Z'.E' R.f1N PZGJ/9•
.uw.rsr ...E
ZNS7XCHKN'l" ~
TILB lD ll772
D:U,. FACTOR -.J.
t/NITS _.IISLI!l
COLUl<N nr §
,Samplcr Oe11c:ripr.ion: VS-OB S•B775 Lab No, OS.A
TesC Oescr:i.priOD.: CBR~C PAR by CC/1IS &chod: BPA 8210
Collected: 01/06/94 14:05
PAJV.HETJ!a RESr:11,T PQL
-·· /a) an thrac:ene ""• H•SS-38
0i.ry.PCll8 1ml,
218-01-!J
Bcn:zo /bi fluoranchane BDL
205-99·2
Bcn:o /ki t'luorancb.l!lle SD~
207-08-9
Bc,,zc l•i pyreno lID!,
50•32•8
Dibcnzo (ii.,b.) .ii.llr.hacene BD•
SJ-70-i
Zndeno 11,Z, J•cd) pyrene BD;
l9J-J9•5
s=n-
1.2-D.ich.Jorcbc:nzc::nc
Ni CTObenzan.• -d5
2-Pluo•obiphcnyl
l'e.rphcny l • c:U 4
tRBC~Y LIJIUS
____u __ll
_E. ___..ll
___ui_ ___l.!! -
--W. ____u_ -
07/11/94
0
~~o .JZ
i}~O .!Z
JJO .!Z
J~O .!Z
330 ..J/
330 .J!
no .!Z
_ill!
_..W
.....w.
.....uz
•
reac Code: CPAB_s
resc Code: CPAB_s
------___ ..... • Clniar M IU•01-l2l
07/151•• 1.2,22 TEST RE5'pr.7'S 1!Y SAMPLE
Sample De.sc:ripcion: V.S•OB !l-1775 ,t.A.b No: OSA
Te3C Desc:riJ'ttga, CAi.CD:O'JBNIC PAB by GC/HB llechod: BPA B270
Collected, 01/06/!Jf l.41DS
ll.!.1'E RI11l
»w.YS1 ...I§
INSTR<HENT _ill2
13780
DIL, TA.C'7'0R --l.
I/MTS __uL!!S
COWMN rrr5
07/13/94
S.mple De11crtpti0ll: VS-OJ B-1116 Lab No: D&A.
Te•t De1.cripr:!Oll1 C,\RC'n«:X:&Nl"C .PAB by CC/HS llecl!od: BPA 8270
C'ollec:Ced'J 01/06/Jf lt:15
PARAHrTER REIJrJI,T FOL
.8cnzo (•J 4l'l Chro:ccne /!QL
5&-SS•JB
Chzy:,~e BDL
218-01-!i
Zlenzo lb} fluoraotlleae S!lL,
205-99-2
Ben.ao /kJ [luoraz::ichene BDL
201-oa.,
Benzo r ... J S')yrans BDL
60•32-8
Dibenzo (a,hl an r.Jurcaoe · llDL
5J-70•J
Inde.co fl.2,J•c~J pyrone BDL
l.~J-19•5
Gt>!lROG.ltt
i,J•Dic:b.lorob&ae:a•
NJ. trobenzcnc -dS
2•Fluo.rcbipbell:yl
T~zphcnyl •dH
tUC'OVXRY L1JfITS
_..li ---ll
___J2 -21 -
_ill --2E. -
-----1.ll --l.!
g
230 ..Jl
JJO ....!!
~JO ....!!
i3o .Jl
iJo .JJ.
JJO ..!!
330 ...1!.
---lll
_w
.....u.;:
....ill:
Not:c• •nd DeLin.1.c1oza tor t.hi.d R.~,
Ul'!lACTQ)
llATS RClli
ANALYST ~
~Dlm1T ......!!Z2
FILS ID 13781
DIL. FACTCIR __J,
CZNITS _sLE/,
COWHN m s
07/Il/94
07/ll/94.
,· ..... ,.,;, •
Test Code, Cl'.All_S
'J'eac Coc:fe: CPNI_S
----------• Ol'de~ I B4-07-Ul
01/15/94 l2;22 m:r &;sgr.rs Br SAMfirE
S;uzple Dt:si::ripc1on: VS-09 S-6776 L.b No1 D&A. Test: De.scripciont CJIRCTNtr"..QlI'C PAil by CC/IIS Nctbod, .EPA ll:Z70 CoJliec-ted: 01/0~/94 lf:J.5
S&mple oescr.tpciaa; vs-J.O s-8777 wb ND: 07A Tesc Deacript1tXI, G\RCDIOGBNIC PAE by OC/l!IS llllchodr DA '470
C'oll~c-red: 07/D~/94 J.t:20
P-'RAH!l1l!R USULr ,OL
Ben1ro lo/ o111 chra cene JJ!JL
56-55-JB
Chzy.scne BDL
:Zl.B-Dl.-S
Ben:zo Cb/ fla.11:~ranencnc l!J!.L
aos-1,-2
BezJBO /lei f"luoca.cthene BD&
207-08-J
B&z:1zo (a) pynne BD!,
SD-12-8
Dibe=o l•,hJ a..cchac:ecc PD;!i:
53-10-J
!nd<liD.O Cl,2,J-cdl pyrenc BDL
J9J-J!l-5
SORR.C:IGUZ
l,2-Dicl:iloro.ben~en•
N.J.c~rene -ds
2-Plugrobipbe.r:,,yJ.
:reqmecyl-dJ4
tUC'OVERY L!11ITS
_.u -l! -
_..J.P. -2.}..
--2. -29. -
~ -!! -
~
JlO ..J!.
JlO ..II.
Jlo ..II.
2l0 ..J!.
iJo ..II.
z1io .JI
330 ..!!.
---11.£
~
......u
__JJ2
NQtc• Uld De.t1n.Hi.on11 lcr th.ia Report,
==
DATE RUN
ANALYST _!:!Q
INS'l'Rtl!SNT 5!170
NLB ID l11f2
OIL, J"ACTOR _..,!
UlfITS _"5L./!f$.
COL<JIOI' XTI S
01/11/91
0103/91
• Page 7
Te6t Code: GAB_S
• • Ord.er# B4·07•l:Zl
07/15/S-f l:Z:22 TEST RESULTS BY SAMPLE
.Ealpl~ Dcsu:ripcicm, VS-11 . S-B77B .r..ab No1 au.
Te.st Deacripcion: CARCZM:;lllDIIC PAH by GC/l!IS
colleeecd': 07/06/H 00:00
llec:.bod: SPA "470
PARAHlm3< = PQz; 0
Benzo (a) aD.tbr,. c:-cne
56-55-J!
Chrysene
216-0l-g -·· /bi t'luoran~C"ne
205-H-2
Benao (ki tluoranthet.1s
207-08-9
Benzo (a) PY""""
50-3.-B
Dibe:ao (a,.b) .an.Chace.ne
&3-?0-3
Iodono u~2,J-~, pyrane
193-39-S
SURROOATE
l,2-D1dl.lorobc.czcnc
Nitrobari&ene -dS
2-Fluorobip~yl
Tczphenyl-dlf
tREC'CVERf
---1l
---2}.
_ll,
_____,!£>
!El< i-1~ ..!I.
SD~ 32!2 .Jl
BDL JZ!2 .Jl
BDL zi 0 .Jl
Wt JJO ..!l
~D~ po ..!Z
BDL JJO ..!Z
LIMITS
_,ll -~
_.zi .....lli
~ -.....w
......l1. _..LU
Jlctes a..cd De£in:J.cj0Z1B for chis Ilepore,
1/XT //ACTED
DATE RtIH
ARAkYS1 .11Q
IJlST11.'DllE]{T --llZ.2
PlLK ID 1J78J
DIL. E".-\CTOR __ l
WITS ....ESil!I
COI.<R<N XTI 5
sample Descr1peion., EO-BU-Ol S·B1Bl
01(l1/91
01/13(94
WJ::i J/01 051.\
Te:ic De=er.i.pcion, CARClN()C&'IIIC PAH .by CC/IIS Mee.hod: Bl'A 11270
Collc-ctcd, 01/06/S4 JB:00
Ben.zo ta) 41:lehr•c:ene
S&·H•JB
Chzy>en•
I.E3L1LT-
BDL
SDL
__ .,, .. o ..!l
T¢St eoder CPAH_W
Page 8
------___ ..,. • Order I IU-0,-.121
07/15/,C U:22. rm RESOLTS sr ,wgu
Sample Desc:r,1Jleion:o BC-.az:.E-01 S-87B1 Lab Jlo1 ....
Ten Dcaerjpcion: C\RCI!ia:ElllC PAJJ by GC/J<G Hechod: BPA s2,o
Coll &C' Ced I 01/06/9• l8100
218-01-9
Benzo lbJ n uaraa the.i::io
205-!U-2
.... 0 /kl Lluor.u:i.dieae
201-08-!i
Benro l•J -· S0-J2-B
DibenZo (ii,hJ antb,rcc:ne
SJ-70-J
I.ad,=, Cl .2, J-cd/ p;=,,e
smu,aa.u'll
l,2-Diehlorabcnzana
lliCZ'Obec.zcnc -d5
2-PlUW'Cbiphenyl
Tez:pbenyl •dl f
l9J-Jl•5
tRZCDVl!JIY
_J.l.
--ll
__ll
~
BDL '2 ....!l
Bl)~ .o ....!l
!lll.!, 10 ..!!.
/ll!.L 10 ..!!.
l1l1L, H! ...1l
= -li .._ll2
~ ___._u
.....!,1. -lll
._ll _w_
NocH· ond D,eLiD.lriOIUI Lor this J(eparc:
Er1'AACIED
"ATS RON
ANALYST .J!i
IN$7'R.UHIJN'1 ~
f'II,,,£ UJ ll792
DIL. TAC'TOR __l.
UNITS __J!SD,
~ rrz s
07/12/94
01/14/94
.............. _. .... ...,,_...,.,;. ,-. ...,.., •
Tear: C'ode: OAB_tt
TOTAL P.09
• • Macon/Dockery Site
Richmond County, North Carolina
July11,1994
Reply to: Technical Committee
c/o David L. Jones
Clark Equipment Company
Ms. Giezelle Bennett
Remedial Project Manager
U. 5. EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
JUL 1 8 1994
SUPERFUND SECTION
RE: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress Report -June 1994
Dear Ms. Bennett:
P. 0. Box 7008
South Bend, IN 46634
Phone: [phone]
Fax: [phone]
On behalf of the Macon/Dockery Site Group ("Group") the June 1994 Monthly Progress Report
is being submitted in accordance with Section XV -PROGRESS REPORTS of the Unilateral
Administrative Order (effective date -June 30, 1992) for the Macon/Dockery Site. This report
describes those activities which occurred during the month of June as part of the Remedial
Design Phase of this project.
PRO!ECT TASKS INITIATED OR COMPLETED THROUGH IUNE 1994:
Results of Sampling and Testing and Other Data Received
• A summary of the findings and results of DuPont's anaerobic bioremediation tracer test
studies is attached to this report. Although laboratory tests have confirmed that
microorganisms present at the site can effectively degrade the chlorinated aliphatic
constituents of concern, the tracer tests have not been able to confirm that the site
hydrogeology is appropriate for the full application of the technology. A proposal to.
implement a more comprehensive tracer test (identified as Tracer Test #3) is attached
for your review. It is hoped that conducting this test, with the proposed piezometer
network, will allow the detection of tracer and therefore also allow the future
assessment of the performance of the anaerobic bioremediation technology.
Plans, Reports. Deliverables and Procedures Completed
• Provided a revised project schedule for porposed removal activities to U. 5. EPA on
June 7, 1994.
• Received U.S. EPA approval of the "Workplan for Removal of Waste from Lagoon 10,
Vessels and Drums".
• •
Ms. Ciezelle Bennett Page 2 July 11, 1994
• Selected Nu-Way Environmental, Inc. on June 6, 1994 to perform the waste removal
activities.
• Mobilized to the site for implementation of the "Workplan for Removal of Waste from
Lagoon 10, Vessels and Drums" on June 13, 1994.
• Conducted the Pre-Construction Conference for waste removal activities on June 15,
1994.
• Constructed a waste staging area and began excavation of Lagoon 10 material on
June 15, 1994.
• Collected waste characterization samples from stockpiled material excavated from
Lagoon 10 beginning on June 17, 1994. Results will be included with the next
monthly progress report, immunoassay confirmation sampling also commenced on
June 17, 1994.
• Commenced drum consolidation activities on June 30, 1994.
• Submitted responses on June 13, 1994 to U. S. EPA's comments for the Prefinal
Remedial Design Report for Soil Vapor Extraction.
TASKS PLANNED FOR JULY 1994:
• Continue waste removal activities in accordance with the U. S. EPA-approved
Workplan.
• Initiate the proposed additional tracer test following U. S. EPA approval.
• Continue developing the Prefinal Design for the groundwater remedy.
PROBLEMS AND DELAYS
• No additional problems or schedule delays are foreseen.
• •
Ms. Giezelle Bennett Page 3 July 11, 1994
If there are any questions, please do not hesitate to contact me at [phone].
Very truly yours,
g~;;:7~
David L. Jones
Project Coordinator
Macon/Dockery Technical Committee Chairman
lb
att.
CC: Macon/Dockery Technical Committee Members
Wayne F. Barto, de maximis, inc.
Paul Furtick -RMT, Inc.
• DU PONT ENVIRO •
July 7, 1994
Summary of Hydrogeologic Testing at Bioremediation Pilot Study Area
As proposed in the Anaerobic Bioremcdiation Workplan, DERS installed 6 piezometers in the
Upper Macon area. The piczometers were arrayed in two rows of three wells situated
downgradient of MW-09. The first row was 7.5 feet downgradient from MW-09 and the
second was 15 feet downgradicnt from MW-09. All wells were completed, with 10 feet long
wrapped stainless steel screens, at approximately 50 feet below grade.
The c--ompleted depths of the piezometers were designed to correspond with MW-09 's screened
interval. The spacing and configuration of the piezometers were designed using existing
groundwater data, including flow direction, hydraulic gradient, and horizontal hydraulic
conductivities, det.ermined from Upper Macon monitoring wells. nus data was used to
calculate the average travel time for a tracer inserted at MW-09 to reach one of the
down.gradient piezorneters. A travel time of 14 to·21 days was predicted using existing data.
Following completion of the piezometcrs, slug tests were performed in three of the new
pie:zometers and groundwater elevations in each of the wells were mapped. The horizontal
hydraulic conductivities ranged from 10-4 tO 10-3 cm/sec and the horizontal gradient in the
immediate area of MW-09 was calculated at 0.15 ft/ft. A revised travel time of 23 day was
calculated for the rest area.
Tracer Test #1
The primary tracer test was designed to determine the rate of groundwater movement between
MW-09 and the piezometers under natural head conditions. Background conditions were
determined by sampli.ag the piezomet.ers for bromide on April 22, 1994. The tracer was
injected in MW-09 on April 29, 1994.
Depth to water measurement were collected in MW-09 and all piezometers prior to the test.
'Three gallons of groundwater were removed from MW-09 using a bailer. This water was
· mixed with 2 gallons of distilled water to make up a slug of 5 gallons. One half ounce of
sodium bromide was mixed with the five gallons of water to make an initial tracer
concentration of 1,000 ppm bromide. The tracer mixture was then added to MW-09 until the
previously measured water level was achieved. Over the next 6 hours, approximately 3 gallom of tracer were trickled into the well. Care was taken not to increase the elevation of
the warer/tracer above the static level in MW-09. After six hours, a sample of the water in
MW-09 was collected for bromide analysis.
A monitoring plan based on a 23 day travel time was set up. Water level measurements and
groundwater samples were collected on a weekly basis from May 6 lO May 27, 1994. The
monitoring schedule was increased to two times per week when bromide began lO exceed
background levels in PM-4.
• DU PONT ENVIRO •
July 7, 1994
Page 2
Receipt of the initial analytical results from groundwater samples collected at MW-09 on the
first day of the tracer test prompted DERS to re-evaluate sire conditions. Although 1,000 ppm
bromide were injected in the well, at the end of the day only 370 ppm bromide were detected
in thf: well and one week later only background levels of bromide were detected.
Over the course of the first tracer test pedod (4 weeks) bromide was detected above
background concentrations only in PM-4 located 7.5 ft immediately down gradient from MW-
09. The maximum concentration of bromide detected in this well, 18 days after tracer
injection, were only four to five times the 0.5 ppm background level. The level of bromide
began decreasing in PM-4 after 21 days.
Tracer Test #2
Based on the inconclusive nature of the static-level test, DERS proposed a more intensive
induced-head test designed to determine wbether a sustained head in MW-09 would cause
sufficient dispersion and energy lo drive the tracer to the piezometer& at an accelerated rate.
Tho original test protocol called for the injection of 30 gallons of tracer at 2,000 ppm bromide
into 1"1W-09. If the hydrogeologic co.wlitions presumed for the Upper Macon area were
correct, it was calculated that it would take approximately 3 days ro discharge 30 gallons into
the aquifer while maintaining a constant head at the top of MW-09. Watl!r levels and
groundwater samples would be collected from the piezometers for at least three days following
the onset of the test.
The 3-d.ay induced head rest became a 30 gallon slug test within the first hour of the test on
May 31, 1994. All 30 gallons of the tracer were accepted by MW--09 in less than one hour
and the water level in MW-09 relllrned to near-static levels in Jess than 5 hours. Water levels
in the downgradient piezometers were only slightly affected by the injection of 30 gallons of
water. The water level in PM-4 rose approximately 1 foot within 5 hours and fell to static
levels within 18 hours. No other piezometer recorded large amoun1s of change.
Grow1dwater samples were collected from all piezometers and MW-09 on five occasions over
three days (5/31/94 through 6/2/94). The changes in bromide concentration (ppm) are
suroroar.ized in the following table:
~~lli2No't'."• .... ~B.It9.4;ii;!'600f .,,._, •-•--~:;,.• ...... .:,.,~ ~,_N,.. ... ,.,,,:;,,'>,', •~•--•• ~•f,: {6J:-l.'.t14.lm•~ ·,.;,,,,, . ,'(,. ,,:;, • ..;:.,<_,::; • ~4'}.91/:~16.00'' ···'''······"'·'·"'··'· ,-:.@i ;W{&l$EM®--~··g '::-.:-'·= • , .• •1 ·' -6½27_M".f600-! ';:.',_ ',",,.'t,. • :,>;:i .,.._, ,._, __ ..... ,,,_._, ;_,_..,,,.,:,..
MW-09 1730 804 375 116 &I
PM-1 2.0 2'.l 1.5 2.0 2.0
PM-2 1.5 1.5 2.0 2.0 1.5
PM-3 1.0 1.1 1.2 1.2 1.2
PM-4 3.5 17.2 17.7 22.4 23.3
PM-5 1.2 1.2 1.2 1.2 1.2
PM-6 1.5 0.6 0.6 0.5 0.5
• Dll PONT ENVIRO •
July 7, 1994
Page 3
The analytical results indicated chat the tracer was mobilized from MW-09, but less than ooe percent reached the nearest downgradient piewmeter (PM-4). Based on the inconclusive results of the tracer tests, groundwater flow conditions in the vicinity of MW-09 appear to be more complex thiln anticipated. Additional piezometers and further testing · is required to identify the appropriate depth and location for monitoring the . effectiveness of the bioronediation pilot test
Purpose:
Field Activities:
• DU POITT' ENVIRO •
Tracer Test #3
Macon-Dockery
Cordova, North Carolina
July 7, 1994
The Scope of Worl:: proposed in this document is intended to augment current knowledge about the rate and direction of groundwater flow in the vicinity of Lagoon 9 in the Upper Macon Portion of the Macon-
Dockery site. This information is required so that the performance of an anaerobic bioremediation pilot stndy can be monitored and evaluated.
Water Levels: Depth to water measurements will be collected in
selected Upper Macon monitoring wells and piezometers to determine if fluctuations in the. test area piezometcrs are related to test activities or to site-wide water table fluctuations. Water levels will be measured
twice, prior to, and during the tracer test period. Additional
measurements may be collected if precipitation events occur during the test period.
Piezometer Installation: The proposed investigation will use existing piezometers, PM-1, PM-4, PM-6 and MW-09. A "deep" piezometer will be installed adjacent (within 3 ft) to each of these piezometers and MW-09. An additional piezometer pair, consisting of a shallow and a deep piezometer (PM-7 and PM-7A), will be installed in an "upgradient"
position. This well pair will be located 7 .5 feet cast of MW-09.
Hollow stem augers will be used to advance the borings for installation
of the piezometcrs. All pi=meters will be constructed according to
procedures and materials specified in the site sampling and analysis plan (SAP).
The shallow piezometer (PM-7) will be constructed similarly to the piezometers installed for the initial tracer test with the well screen intercepting the upper 10 feet of the saprolite aquifer.
Based on boring logs from MW-08A, a depth of 75 feet is estimated for
the deep piezometers. Actual depths will vary according to the conditions encountered in each borehole. The length of the screened
interval in each of the deep piezometers will be adjusted to correspond
with the thickness of the partially weathered rock zone in each boring.
If the partially weathered zone is greater than 20 fec:t thick, only the lower 20 feet of the piezomt:ter will be screened.
To facilitate identification of the partially weathered zone, split barrel samplc:s will be collected continuously from water table (approximately
• DU PONT ENVIRO •
July 7, 1994
Page2
45 feet below grade) to a depth where penetration by auger or sampler is
no longer possible (competent bedrock). The samples will be described
in the field by a DERS geologist.
Proposed piezometer locations are shown in the attached figure. All
piezometers will be developed and purged following completion.
Surveying: The locations and elevations of the piezomerers will be
surveyed following completion of installation activities.
Hydraulic Conductivity: Hydraulic conductivity tests will be
performed in each of the deep piezometers. The results of these test in
combination with the hydraulic gradient determined via water levels will
be used to estimate groundwater velocity.
Background Sampling: Groundwater samples will be collected from
each of the test piezometers. These samples will be analyzed for the
presence of the proposed tracer chemical, rhodamine, to establish
background concentration, if any, of this non-toxic dye.
Tracer Test: An induced-head tracer test will be performed using MW-
09 as the injection point and rhodamine as the tracer c,hemical
The tracer test will consist of i.t:\iecting 60 gallons of distilled warer
mixed with rhodamine dye co form a tracer concentration of 2,000 parts
per million into MW--09. A sample of the injectate will be collected
during injection to verify this concentration. Monitoring of the tracer
test will be conducted over a three-day period.
Water levels will be measured in the piezometers prior to injection of the
dye and prior to any sampling events. Six rounds of sampling will take
place over the three day test period. The schedule for sampling will be
determined based on the flow velocity determined from slug rests
conducted on the piezometers.
The samples will be analyzed using a scanning spectrofluorometer. If·
suitable arrangements can be made, DERS plans to conduct the analyses
in the field immediately following each sampling event. At least one
sample from each sampling event will be split for laboratory verification
of field results. Should the field analysis prove impractical, the samples
will be submitted to Conoco Environmental Laboratory for analysis
following completion of field activities. Accelerated turn-around (5
days) will be requested for any laboratory analyses.
2
Data Evaluation:
Schedule:
• llU PON1' ENV I RONII •
July 7, 1994
Page3
Analytical results and hydraulic data collected during field activities will be evaluated to determine the capability of the monitoring array to assess the effectiveDCSS of biological nutrients iajected into the contaminant plume at MW-09. The results of the tracer test and recommendations concerning the feasibility of conducting the bioremediatio.n pilot test will be reported to the Tecbnical Committee and thereby to the USEP A m subsequent monthly progress reports.
The timeli.ne for conducting the proposed field and data evaluation activities is attached.
3
Tracer Test #3
I July Augu,t I SepterrDer ()cf-t w-., I Deco ID Name !Juraton Sdledl!ledS!Jrl Sdledimd F'nlsh I 3 10117 24 31 I 7 .. 21 a 4 11 1B 25 2 9 16 23130 e ll 20 21 4 II t ~ ~ l/1W4 7/'li.$4 \ I ~
2 Wa!i,Le,,l, 0.2w 71l.1.'34 1/'l5/M I
3 DIIRv/lel J""3\,11o~ 1w 712&'94 !/11" • 4 siui T~n; SompJrQ 0.2" !17J94 112/94 I
! TlllCOl Test o.s.r l/ll94 !Ml • 6 Om Enlual!on 1.S.-S/'in4 811ml -· ' 7 Ropo,t I><, a/1&'34 i 8/1~ Ill I
OERS SERO Clllcal l'qlffl 8"nwoa,y a a 11',,TE:1/Tm Nooafu!I Mllesbll! ■ -Upc
f'o9I! 1
10 0 10 20 30
SCALE IN FEET
0 PM2An..
L__PPM1
·PM1A L::s._
0 6.0p1,1,4 .MW9A hM7A
PM3 PM4A @MW9 ~ PM,7
0 Shallnw Piezometer . · (not to be used for Tracer Test #3)
0 L:iSPM6
~ Shallow Piezometer
.6._ Deep Piezomet~r
. Ourool
[r\Vtroran•nlol
lh1n•1lld1fan
Suvlcos
Pt.15 PM6A
IIIV..:.
·· ··Proposed and Existing Piezomerer f.ocations
Upper Macon Bioretnediation Pilot Study
Macon-Dockery Site
Cordova, NC
.... OU., l"ffCU. C. I HU.:
Cle<U:
, ,cuut 110.: i:--:-u=1r::--f;;;11L™v.:-, --
l
•
•
Macon/Dockery Site
Richmond County, North Carolina
May 9, 1994
Ms. Giezelle Bennett
Remedial Project Manager
U.S. EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
RE: Macon/Dockery Site -Cordova, North Carolina
Monthly Progress Report -April 1994
Dear Ms. Bennett:
• RIECle~\!lE[))
MAY 131994
SUPERFUND SECTIOI\I
Reply to: Technical Committee
do David L. Jones
Clark Equipment Company
P. 0. Box 7008
South Bend, IN 46634.
Phone: [phone]
Fax: [phone]
On Behalf of the Macon/Dockery Site Group "(Group") the April 1994 Monthly Progress
Report is being submitted in accordance with Section XV -PROGRESS REPORTS of the
Unilateral Administrative Order (effective date -June 30, 1992) for the Macon/Dockery Site.
This report describes those activities which occurred during the month of April as part of the
Remedial Design Phase of this project.
PROIECT TASKS INITIATED OR COMPLETED THROUGH APRIL 1994:
Results of Sampling and Testing and Other Data Received
• Raw data from DuPont's anaerobic bioremediation lab optimization study is included
as Attachment 1.
Plans. Reports Deliverables and Procedures Completed
• Submitted the "Workplan for Removal of Waste from Lagoon 10, Vessels, and Drums"
on April 6, 1994 for U.S. EPA review.
• Submitted the Prefinal Design for the SVE component of the remedy on April 22, 1994
for U.S. EPA review.
• During the week of April 4, six monitoring wells were installed downgradient of
MW-09, in accordance with the approved Anaerobic Bioremediation Pilot Study Work
Plan, by DuPont Environmental Remediation Services. Soil and groundwater samples
were collected during well installation for treatability analysis.
• • Ms. Giezelle Bennett Page 2 May 9, 1994
• The laboratory optimization study on soil microcosms was initiated on April 14, 1994.
This work is an integral part of the Anaerobic Bioremediation Pilot Study.
Dechlorination activity was confirmed after 14 days activity in two of the substrate
media: yeast extract (methanogenic conditions) and cellobiose (methanogenic and
sulfate-reducing conditions). Attachment 1 contains additional details of this work.
• The tracer study for the Anaerobic Bioremediation Pilot Study was initiated on April 29,
1994.
TASKS PLANNED FOR MAY 1994:
• Obtain U.S. EPA approval of the "Workplan for Removal of Waste from Lagoon 10,
Vessels and Drums."
• Commence the competitive bidding process by the Group for selection of a contractor
to perform the Lagoon 10, vessels, and drums work.
• Continue the Anaerobic Bioremediation Pilot Study.
PROBLEMS AND DELAYS:
• No additional problems or schedule delays are foreseen.
If there are any other questions, please do not hesitate to contact me at [phone].
Very truly yours,
ff~~~
David L. Jones
Project Coordinator
Macon/Dockery Technical Committee Chairman
lb
encs.
cc: Macon/Dockery Site Group Members
Wayne F. Barto, de maximis, inc.
Paul Furtick -RMT, Inc.
• •
The laboratory optimization study has been ongoing since April 14. The objectives of this
study are to determine if soil samples from Macon/Dockery can reductively dechlorinate PCE
and 1, 1, 1-TCA; to evaluate different substrates (acetate, trimethylamine, cellobiose, and yeast
extract); and to evaluate whether methanogenic or sulfate-reducing conditions gives the best
activity.
Duplicate 160 ml microcosms have been prepared with 10% soil and 90% groundwater. The
treatments include the following: 1. mercuric chloride poisoned control; 2. unamended
control; 3. methanogenic treatment with trimethylamine and sulfide; 4. methanogenic
treatment with yeast extract and sulfide; 5. methanogenic treatment with acetate and sulfide;
6. methanogenic treatment with cellobiose and sulfide; 7. sulfate-reducing treatment with
yeast extract, sulfate, and sulfide; 8. sulfate-reducing treatment with acetate, sulfate, and
sulfide; 9. sulfate-reducing treatment with cellobiose, sulfate, and sulfide. Each bottle was
spiked with 5 mg/L of PCE and 1, 1, 1 TCA. The concentrations of contaminants are analyzed
by GC/MS. Final metabolic end products (sulfide, ethene, ethane, and methane) and pH are
also being followed.
Dechlorination activity has been CONFIRMED after 14 days in two substrate media: yeast
extract (methanogenic conditions) and cellobiose (methanogenic and sulfate-reducing
conditions). A summary of the laboratory optimization study data is attached.
L~
i/lr /'14~
....... A,,,e
. Cl !
DCM i
' 1.1.l·TCA 1
1,2-DCE ·' . TCE
. PCE
u,nc,..
C2
1)(),.1
1,1,l·TCA
1.2•DCE
TCE
PCE
1 1-1:>CA
'
Ul
DCM I
1,1,J.TCA
l.2-DCE
TCE
· PCE
l.1°DCA
U2
DCM
l;l,l•TCA
1.2-DCE
TCE
. PCE
1.1-DCA
MTMA-1
DCM
1,1.l-TCA
1,2-DCE
TCE:
PCE
1,1-DCA
_MTMA-2·
DCM
1.1.l•TCA
l .2-DCE
TCE
PCE
1.1-DCA
D,1Y
0
~00
5300
<75
<7S
4300
·45,1
0
180
6000
<75
<75
ssoo
60.1 .
o·
390
5800
<15
<75
4400
<75
0
200
5900
<75
<15
4000
54.1
0
lllO
5800
<15
<TS
4600
60.l
0
230
5500
<15
<15
4400
S3,I
• •
Macon/Dockery Site ·
Anaerobic Bloremediation Pllot-S~dy · .
•.
7 14 MYE.-1 0 7 14
,420..2 390.2 DCM 390 4.SO ◄50
4600 4..,... 1.1.l-TCA 5200 4900 4400
<ISO <150 1.2-oce <TS <ISO 390(
<lSO <150
3600 4300
<1$0 <J.50
TCE <75 .<150 <!SC
PCE 4200 3600 "s\.'1
1.J.DCA <75 "iiii .
110.l
vc <300 <300 43. l /
7 14
390 380
!
MYE-2 J 0 7 14 ;
5200 4500 DCM 420 450 . 360
<150 <lSO 1.1.1-TCA ~ROO 5300 4500
<ISO <150 1.2-DCE <75 <ISO 3300
4100 3900 TCE <75 130.l <ISO ..
<150 <l.SO PCE 4800 4000 9Q,\ I
J.l·DCA <75 100.1 150
7 14 vc <300 <300 2A
360 360
.5200 .5200
<I.50 <150
<150 <ISO
4500 4300
MACE•l 0 7 14
DCM 360 390 390 I
1,1,1-TCA 5700 4900 5400
1.2-DCE <1S <lSO <ISO
<150 <1S0 TCE <15 <150 <150
~ 3800 3700 :sooo
7 14 1.1-DCA <75 2R.l <150
420 390 ·--·
5800 5700 ~CE-2 0 7 14 ·
<ISO <ISO DCM 360 390 380
<I.SO · <lSO
4800 4700
<150 <ISO
7 14
1.1,l-TCA 6200 5400 S400.
l.2•DCE <75 <1S0 <ISO c
TCE <75 <I.SO <lSO\
?CE 5000 4800 4600 l
J,l-DCA <75 <150 29.1
450 420
4900 · .sooo
<ISO <lSO
cl.SO <1S0
MCEL-1 0 7 14 /
DCM 390 420 4SO:
1_._!_ .1-TCA 6100. SlOO 4500 !
4000 4200 .!.,2-0CE <7S <150 <I.SO
<ISO <150 TCE <75 <lSO <150
PCE 4500 3800 3700
7 14 l.l·DCA <75 <ISO <150
390 420
5200 4r.tv MCEL,2 0 7 14
<l,0 <150
<150 <150
3900 3700
<ISO <150
DCM 450 420 480
I.I 1-TCA 4900 4300 3800
1.2-DCE <75 <l'° 71.l
TCE <75 <150 <150
PCE . 6200 4000 3000
1.1-DCA <75 90.1 41.1
• • SYE-1 0 ') 1• t(:M 390 420 440 U.l•TCA 6400 5800 3900 l.l•Pa <75 <150 <1,U Tct! <'7S dSO. 41.l PCE SOOD 4000 3500 C Control, poi.'\OnW with Hg□ 1.1-DCA <15 90.t IS30 u C'.on1rol, unamended
S'IE-2 0 7 14 MlMA Methanogenic, trimethyamine DCM 420 .t'MI A.d.11 MYE Methanogenic, yeast extraet l,J.1-TCA 6200 .saoo .tMll1 1.2-0CE . <1$ <150 <~ fCE <7S <l.50 ~-1
MA03 · Methanogenic, aa:tate
MCE.. Methanogenic, ccllobrosc r>C:E 5200 4300 "l1lll: SY£ Sulfate reducing, yeast ~ct 1,:-DCA <75 . 90.l l 10.l SACE Sulfate reducing, acetate SA,CE.-1 0 7 14 SCEL Sulfate reducing, ccllobrose QS:M 420 420 480 1.1.1-TCA 5900 S,00 4!100 1.2-DCE <75 <1.50 <150 TCE <~ <150 <150 !'.fE SIOOI 4()00 4000 1,1-DCA I <75 21.1 <150 I
SACE-2 0 7 14 DCM 350 390 4<l 1,1.1-TCA 6500 5800 . 5100 Jd:-DC'E <75 <150 <150 TCE <75 <UO <150 PC!, 5600 44001 3800 1.1-DCA <'?SI $4.l 49.1 I
SCU.-l I 0 7 14 DCM ! 390 480 450 T,T.'i:°TCAf 5700 5400 UM 1.2-DCE <75 <lSO 1nrr TCE <7S <150~ 30,l r~OCA 4300 4000 i4ne:
<75 45.1 110 I
'gL-2 0 7 14 DCM 450 480 450 J..:.W. • TCA 7100 5600 5200 1.2-DCE ••!7:S <ISO .210 TCE ' <75 <1'0 82.1 PCE ssoo 4400 3400 l.l-OCA <1S 69.1 64.1
•
Macon/Dockery Site
·rfii::~=-RECelVED ;
Richmond County, North Carolina
FEB 141994 I
SUPERFUN
February 8, 1994
Ms. Giezelle Bennett
Remedial Project Manager
US EPA, Region IV
345 Courtland Street
Atlanta, GA 30365
RE: Macon/Dockery Site • RD/RA
Reply to: Technical Commichee
c/o(Davi]CL._Jon~§J
Clark Equipment Company
P. 0. Box 7008
South Bend, IN 46634
Phone: [phone]
Fax: [phone]
Monthly Progress Report -January 1994
· Dear Ms. Bennett:
On behalf of the Macon/Dockery Site Group ("Group") the January 1994 Monthly Progress Report is being submitted in accordance with Section XV -PROGRESS REPORTS of the Unilateral Administrative Order (effective date -June 30, 1992) for the Macon/Dockery Site. This report describes those activities which occurred during the month of January as part of the Remedial Design Phase of this project.
PROJECT TASKS INITIATED OR COMPLETED THROUGH JANUARY 1994:
Results of Sampling and Testing and Other Data Received
o Prior to initiating the well point abandonment procedure, AMT, Inc. collected a full round of groundwater elevations from all monitoring wells and wellpoints. These elevation readings have been tabulated and are attached herewith. There were no anomalous readings that would affect previous interpretations of regional groundwater flow patterns. The data will also be included in the Final Design Report.
Plans, Reports, Deliverables and Procedures Completed
o Received on January 4, 1994, US EPA's approval of the proposed revisions to the Anaerobic Bioremediation Pilot Study Work Plan.
• Prepared and submitted .the final Anaerobic Bioremediation Pilot Study -Workplan on January 19, 1994. The final document incorporated the revisions approved in US EPA's January 4, 1994 letter.
Ms. Giezelle Bennett
February 8, 1994
Page 2 of 3
• •
• Submitted on January 10, 1994 procedures for abandonment of well points
installed on adjoining offsite property. These procedures were approved
by US EPA on January 12, 1994, and the abandonment was completed on
January 24, 1994.
• Received on January 25, 1994 US EPA's and NCDEHNR's comments on
the draft Intermediate Remedial Design Report, Plans and Specifications,•
Construction Health and Safety Plan, Performance Standards Verification
Plan and Remedial Action Work Plan.
• Held telephone discussions with Mr. David Lown, NCDEHNR -Superfund
Section, in January regarding procedures for submitting draft NPDES
permit applications for Non-Discharge Permit Applications. Mr. Lown
indicated that he would follow-up with DEHNR's Division of Water Quality
personnel regarding review of draft permit applications and establishment
of discharge permit requirements, parameters and monitoring procedures.
TASKS PLANNED FOR FEBRUARY 1994:
• Initiate work on the Anaerobic Bioremediation Pilot Study Work Plan
following USEPA approval of the revised document. Work will commence
in accordance with the Work Plan project schedule that will be forwarded
to U.S. EPA following their approval. The schedule will contain a project
start date that coincides with U.S. EPA's approval date.
• Meet with U.S. EPA to discuss technical issues contained in their
comments received on January 25, 1994.
• Prepare responses to U.S. EPA comments regarding the Intermediate
Design deliverables.
PROBLEMS AND DELAY:
• Pending the outcome of discussions to be held with U.S. EPA in February
1994 regarding the technical comments on the Intermediate Design
deliverables, it may be necessary to consider an extension to the Remedial
Ms. Giezelle Bennett
February 8, 1994
Page 3 of 3 ·
• •
Design project schedule. An update will be provided in the next Monthly
Progress Report.
If there are any other questions, please do not hesitate to contact me at 219-239-0195.
Very truly yours,
Ocwu! L. (b,,, o--:;;-es
David L. Jones
Project Coordinator
Macon/Dockery Technical Committee Chairman
WFB/jca
Attachment
cc: Macon/Dockery Site Group Members
Wayne F. Barto, de maximis, inc.
Paul Furtick, RMT, Inc.
f:\projects\3068\mrpjan.94
i • •
RMT INTERMEDIATE REMEDIAL DESIGN REPORT
MACON/DOCKERY SITE
1:\WP\70\7001720.TBUcdf94
TABLE X
SUMMARY OF MACON/DOCKERY GROUND WATER
ELEVATION MEASUREMENTS
MW01 263.46 234.79
MW02 231.39 192.36
MW02A 230.83 191.75
MW03 220.67 191.86
MW05 234.51 195.26
MW06 237.13 196.01
MW07 228.41 191.01
MW08 234.54 192.62
MW08A 234.44 188.14
MW09 254.08 206.79
MW10 265.51 222.0
MW11 271.92 236.86
P11-A 270.28 235.79
MW19 236.89 197.1
MW21 155.52 139.19
UMRW01 234.77 193.38
UMPZ01 235.8 193.35
UMPZ02 236.48 193.52
UMWP10 180.05 153.13
UMWP11 217.95 194.76 DRY
UMWP12 189.56 166.61
UMWP13 177.45 155.77
UMWP14 160.51 152.48
UMWP15 172.39 165.72
a All measurements are referenced to the National
Geodetic Vertical Datum (NGVD) and are recorded in feet
above mean sea level (MSL). Measurement point is
north side, top of casing.
JANUARY 1994
• •
RMT INTERMEDIATE REMEDIAL DESIGN REPORT
MACON/DOCKERY SITE
l:IWP\70\7001720. TBL/cdf94
TABLE X {Continued)
SUMMARY OF MACON/DOCKERY GROUND WATER
ELEVATION MEASUREMENTS
MW04 184.21 142.21
MW12 171.98 145.14
MW13 188.67 138.72
MW14 177.34 142.14
MW14R 175.95 139.76
LMWP05 126.29 122.29
LMWP06 154.17 125.72
DRY
LMWP07 140.45 126.75
LMWP08 161.23 152.7
LMWP09 177.91 134.75
MW15 257.10 218.58
MW15A 257.29 220.33
MW18 242.54 210.77
MW20 265.15 236.74
UDWP03 223.85 199.92
DRY
UDWP04 241.51 209.34
a All measurements are referenced to the National
Geodetic Vertical Datum (NGVD) and are recorded in feel
above mean sea level (MSL). Measurement point is
north side, top of casing.
JANUARY 1994