NCD980799019_19961004_Cherokee Oil_FRBCERCLA C_Correspondence 1995 - 1996-OCR

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CHEROKEE OIL COMPANY
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Site Info I Aliases I Operable Units I Contacts
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Site Name: CHEROKEE OIL COMPANY
Street 1201 BERRY HILL ROAD
City/ State / ZIP: CHARLOTTE, NC 28208
NPL Status: Not on the NPL
Non-NPL Status: NFRAP
EPA ID: NCD980799019
EPA Region: 04
County: MECKLENBURG
Federal Facility Flag: Not a Federal Facility
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informational purposes use by employees of the U.S. Environmental Protection Agency for
management of the Superfund program. They are not intended for use in calculating Cost
Recovery Statutes of Limitations and cannot be relied upon to create any rights, substantive or
procedural, enforceable by any party in litigation with the United States. EPA reserves the right
to change these data at any time vvthout public notice.
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Contacts
Site Info I Aliases I Operable Units I Contacts
Actions I Contaminants I Site-Specific Documents
Title Name Phone Number
' Remedial Project Manager (RPM) GIEZELLE BENNETT [phone]
' Remedial Project Manager (RPM) JON BORNHOLM [phone]
Remedial Project Manager (RPM) Luis Flores [phone]
Remedial Project Manager (RPM) BEVERLY HUDSON [phone]
' Remedial Project Manager (RPM) KEN LUCAS (404) 56~-8953
Remedial Project Manager (RPM) KEN MALLARY [phone]
I
Remedial Project Manager (RPM) MICHAEL TOWNSEND [phone]
Remedial Project Manager (RPM) SAMANTHA URQUHART F [phone]
Remedial Project Manager (RPM) Phil Vorsatz [phone]
Site Assessment Manager (SAM) Jennifer Wendel [phone]
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DISCLAIMER: Be advised that the data contained in these profiles are intended solely for
informational purposes use by employees of the U.S. Environmental Protection Agency for
management of the Superfund program. They are not intended for use in calculating Cost
Recovery Statutes of Limitations and cannot be relied upon to create any rights, substantive or
procedural, enforceable by any party in litigation with the United States. EPA reserves the right
to change these data at any time without public notice.
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CHEROKEE OIL COMPANY
Actions
Site Info I Aliases I Operable Units I Contacts
Actions I Contaminants I Site-Specific Documents
OU Action Name Qualifier Lead Actual Start
00 DISCOVERY F
00 ADMINISTRATIVE V F 10/26/1994
RECORDS
00 INTEGRATED H F 11/02/1994
ASSESSMENT
00 Public Notice Published F
00 REMOVAL C F 11/02/1994
00 PRELIMINARY N s
ASSESSMENT
00 SITE INSPECTION N s
00 ADMIN ORDER ON FE
CONSENT
00 ADMIN ORDER ON FE
CONSENT
00 CONSENT DECREE FE 10/10/1997
00 ADMIN ORDER ON FE
CONSENT
Actual
Comeletion
02/011/1994
10/26/1994
11/02/1994
12/09/1994
12/22/1995
10/15/1996
10/15/1996
07/24/1997
10/15/1997
01/12/1998
05/26/1999
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DISCLAIMER: Be advised that the data contained in these profiles are intended solely for
informational purposes use by employees of the U.S. Environmental Protection Agency/or
management of the Superfund program. They are not intended for use in calculating Cost
Recovery Statutes of Limitations and cannot be relied upon to create any rights, substantive or
procedural, enforceable by any party in litigation with the United States. EPA reserves the right
to change these data at any time without public notice.
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9/21/2005 4:32 PM
MAR 05'98 17:11 No .009 P.02 NORTH SUPERFUND
\
10: •
REME~IA' SIT!; ASSESSMENT DECISION;.: ·tPA .l'IEGION IV-SlteNamo, Ch~r'ok(IB Oil Com PPOY EPA IDII, NCO 980 799 019 ··,as Site Nm,es: ----------
CJ1y, Charfotte County or Parls-h: Mepklenburg
Refer to Report bot&d: . Qctpber 4 1 1 58§
Repatt developed by: Dpug Moore. NCOEHNR
>O' OECISION:
' ,;'.~,:~--
Roport typo: Combined PAIS!
1. Further R~li>k°o1 Sltli Assessm611t under CERCLA ISuperfundl Is ruu' requlr!ld becau•a:
jx~J 1 a, Site does not qualify for further remedial site assessment under CERCLA / I 1 b, Sito may qualify for further J · I RCRA action, but is doforrod to: I / NRG (No Further Romedlal Action Pla1med • NFRAPJ
I 2 .. Furthor Assessment Needed Undor CEl!ClA,
2b. Activity
Type: I I SI
PA
I
I I Other:
I I ESI
HRS ev:1Juation
2o. (optjonol) Priority: / I Higtier I Lower
DISCUSSION/RATIONALE: Based on th\!. i;o_nclusions formed in the Integrated PA/SI. this •ite does not pose a
threat to human hoalth and the onslronmont. Duo to the Jow potential targets valuos a disposition of No Further Action wao
BSSilJIIOd.
Report R~vlewed
aod Approved by: Cynthia K. Gurley Signature:
10115/96 Sita DocJslon
Made by: P,nthia K, Gu~ey
101)6196
El"Af'orm69100·3
,-~~s-;; -
'· ,·,
I :';:,
.. ~{~'
• • NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WASTE MANAGEMENT
December 8, 1997
f IL£ COPY
Mr. Henry Sutton
Solid and Hazardous Waste Program Manager
Mecklenburg County Department of Environmental Protection
700 North Tryon Street
Charlotte, North Carolina 28202
RE: Removal Coordination
Cherokee Oil Company
NCD 980 799 019
Dear Mr. Sutton:
David Lilley of the NC Superfund Section spoke with Ms. Sarah Edwards of your office
today to notify you that the NC Superfund Section will conduct a site reconnaissance of the subject
site located in Mecklenburg County, North Carolina. The reconnaissance will be conducted on
December 18 and 19, 1997 by Doug Moore of the NC Superfund Section. The purpose of the
reconnaissance is to determine if the site poses a hazard to public health or the environment because
of releases of contaminants to soil, surface water, groundwater, or air. You may want to have your
representative meet the inspection team at the site. If so, please contact Doug Moore at (919) 733-
2801, ext. 315 and he will coordinate a meeting.
If the reconnaissance indicates the need for future study of the site, we will contact your
office to advise. if you have any questions, please don't hesitate to call David Lilley or me at (919)
733-2801. .
cc: Phil Prete
Doug Holyfield
Pat Williamson
Scott Ross
David Lilley
Donna Keith
Pat DeRosa, Head
Site Evaluation and Removal Branch
NC Superfund Section
401 OBERLIN ROAD, SUITE 150, RALEIGH, NC 27605
PHONE [phone] FAX 919·71 S-3605
AN EQUAL OPPORTUNITY/ AFFIRMATIVE ACTION EMPLOYER· 50% RECYCLED/I 0% POST-CONSUMER PAPER
Federal A
~p Notification & Authorizatio"'Pr
Prepared by: 1)_ Moolu= Today's Date: 1::zftfh1
I · Use D!ack Ink or Typewriter only-Staff 10 fill out first 2 blocks only.
Site Trip
Date of Trip: j/ecewibfr /'i" -/7 , /99 2 •
If trip date changed or cancelled note below:
Trip Date Changed To: Cancelled: --
NCO#: Ucti c/'150 7~'1 Qi~ Site Name: ct.erokc. o,"[ Co,...._!"", City: C/4q,-/o/k County: A,/r -ev lt2n tzv ry
Reason for Trip: {_~~ (!.oer-a:L,;,,.,J, ~
Name of Hotel (Overnight Trip): Hotel Telephone Number: ( )_-
Authorized by: ~ii
Project Team Leader: -::2',b~ &Do,(£
Assistants: ~ Rv,,,,Fo!G). • ,
Attach To Notification Form: I copy each: Preliminary Assessment Form (First page only) Submit to the Site Map
Industrial Hygienist PA Transmittal Letter
(!'leas: list appropriate County li~alth Department contact_ pmon to call to advise of trip) . · _ / / I/,',{ 1· i/c, ?. W:z5. Environmental Supervisor or Health Director to call: _((}·r. /kor"' Soc 'fiE>'\ Title: fr,,tJ,·a11,t1Jl,.:-:
_/ ,r t/ ' (Note if Dr., M.P., etc.)
Telephone Number: {lo-f)s:::;;:1 -,rs-oo
Notes: Health Department Official Contacted: f{\ s: faral /;clvc,l,
Back Up Letter Required: Yes ~ No
Note: Si~cd original to Data Manu~cr
&wr:-:rd rn>. &dwo.-.& &" /JJr, s:.,J-k ..... ,.....__
l~-~-17 (DB.0
• State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Waste Management
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
William L. Meyer, Director
Mr. Myron D. Lair, Chief
Emergency'Response and Removal Branch
US EPA, Region IV
61 Forsyth Street, 11th Floor
Atlanta, Georgia 30303
November 26, 1997
Subject: Immediate Removal Evaluation Request
Cherokee Oil Company Site
Dear Mr. Lair:
120 I Berryhill Road
Charlotte, Mecklenburg County, NC
US EPA ID: NCD 980 799 019
•
Last Wednesday, November 19, 1997, Steve Spurlin of the EPA Region IV Emergency Response and Removal
Branch notified the NC Superfund Section that he had received a report indicating demolition workers experienced ill
-effects while demolishing the remains of a burned building at the site. As he was busy with another site, he requested the
NC .Superfund Section investigate the reports to determine any additional need for EPA ERRB response action at the site.
At Mr. Spwiin's request, Doug Moore called Mike Jenkins, city of Charlotte, to interview him about the reported incident.
Mr. ;Jenkins said that workers were removing debris from a low area near the east side of the site along the boundary with
· ·suburban Propane when they experienced ill effects, including runny eyes and noses, dizziness and vomiting. The
demolition operation was ceased immediately and the workers are reportedly undergoing medical monitoring.
Between November 1994-December 1995, the EPA Region IV Emergency Response and Removal Branch
. conducted an emergency removal action at the site. The extensive removal action included removal of 2,856 drums, two
tanker trailers, three 20,000 gallon underground storage tanks, six 30,000 gallon above-ground storage tanks, six 10,000
. gallon above-ground storage tanks, several roll-off containers and over 70,000 gallons of free-standing oily waste and
: sludge from three ooncrete diked containment basins. At accessible areas, EPA also removed several feet of contaminated
. soil and backfilled these areas with clean fill. The area where the workers experienced the ill effects correlates to an area
. of soil contaminated with hazardous substances that was not removed due to it's inaccessibility. Subsequent soil samples
· taken by NC Superl'und Section personnel in March 1996 identified numerous hazardous substances in surficial soils in
this area (see CO-004-SL of Figure I and Table IA) above EPA human-health based soil exposure benchmarks.
On Monday, November 24, 1997, Doug Moore and Doug Rumford of the Site Evaluation and Removal Branch
travelled to the site to conduct an onsite reconnaissance. The scope of the investigation consisted of an onsite
reconnaissance to determine if any detectable volatile substances were present in the air at the site, to document the site
conditions, interview neighbors and to determine the need for additional EPA emergency response action at the site. The
onsite reconnaissance indicates that the site is unsecured with numerous large piles of charred wood, twisted metal and
concrete debris. There is no fence along the north side of the site, the gate at the northwest comer of the site is damaged
and the gate at the southwest comer of the site is not locked. No elevated HNu PID readings were detected offsite along
Berryhill Road or l1nift Road, and no elevated HNu PID readings were detected on the site downwind of the debris piles
P.O. Box 29603, Raleigh, North Carolina 27611-9603 Telephone [phone]
An Equal Opportunity Affirmative Action Employer 50% Recycled / 10% Post•Consumer Paper
Letter to Mr. Lair
Cherokee Oil Company Site
November 26, I 997
Page 2
• •
and in the vicinity of the low area near the east side of the site. An oily sheen was observed on top of a small pool of
. standing water at the low area Slight deflections of 1-2 meter units above the background ambient air were detected in
soil test boring holes surrounding the small pool at the low area along the east side of the site. There are stained soils
remaining at the low area and in the overland runoff pathway from the site.
Our staff toxicologist reviewed the available file information relating to the remaining soil contamination at the
site. She was unable to fmd data that indicates that short term exposure to high concentrations of polynuclear aromatic
hydrocarbons (P AH's) and phthalates such as those found in the soil could cause the adverse health effects experienced
by worl<ers conducting the cleanup. However, since there is concern, and the concentrations of P AH's and phthalates that
remain at the site are several orders of magnitude higher than acceptable residential exposure levels, she recommended
that the site be referred to EPA (see attachment).
Since soil samples exhibited hazardous substances above State of North Carolina Remediation Goals, workers
at the site have reportedly experienced adverse health effects consistent with chemical exposure, and the site is unsecured
from nearby residents and trespassers, posing a potential direct contact or inhalation threat, the NC Superfund Section
recommends that EPA re-evaluate the site for additional removal action. In addition, we request that the site information
be referred to ATSDR to evaluate potential for risk associated with occupational exposures. State funds for this removal
action are not available at this time. Please Jet us know if and when an evaluation of this site can be conducted, so that
we may coordinate your site visit with our staff. If you have any questions concerning 'Ibis site, please contact Doug
Moore (ext. 315) ormyself(ext. 290) at [phone]. ·
Attachments
cc w/o attachments:
cc w/attachments:
Jack Butler, DWM
Mike Kelly, DWM
Doug Holyfield, DWM
Phil Prete, DWM
Pat Williamson, DWM
Charlotte Jesneck, DWM
Phil Vorsatz, US EPA Region IV
Mike Norman, US EPA Region IV
Dennis Tyndall, Mecklenburg County DEP
Mike Jenkins, City of Charlotte
PatDeRosa
Site Evaluation and Removal Branch
NC Superfund Section
P.O. Box 29603, Raleigh, North Carolina 27611-9603 Telephone [phone]
An Equal Opportunity Affirmative Action Employer 509& Recycled / 1 0% Post-Consumer Paper
•
TO: Doug Moore
Environmental Chemist
Site Assessment Branch
FROM: Hanna Assefa J,/,1,<
Environm~ntal Toxicologist
Inactive Hazardous Sites Branch
RE: Cherokee Resources
Charlotte, Mecklenburg County
•
MEMORANDUM
November 25, 1997
I am unable to find data that indicates that short-term exposure to high concentrations of PAH's and phthalates
such as those detected in soil at the subject site could cause some of the adverse health effects experienced
by workers that were conducting cleanup of debris from the burned building. However, it is likely that in that
short period of time they inhaled and ingested a lot of particulates that were potentially contaminated with
these and other waste oil chemicals. Some residual contamination from whatever was stored in the building
prior to burning may also have existed in the debris. Since there is concern, and the concentrations of PaHs
and phthalates that remain at the site are several orders of magnitude higher than acceptable levels I
recommend notifying EPA of the circumstances.
lll~re 2. ·
JfayoutMap
:Ji_ejj>kee Oil Company
fBerryhill Road
)otte, Mecklenburg Co., N.C.
'PA ID: NCD 980 799 019
ot to Scale
~;prawn By: D. Moore (Aug. 1996)
fl~ Fence
D
l].. Overland Drainage P.athway
~: -Underground Product Distribution Line
it,,_,_ Abandoned Railroad Line
" Existing Concrete Wall ..,
t.. Former Concrete Wall r Underground Storm Sewer
•
i
I
. CO-00 I-SL (background surface soil) : 0 { "'·"'' .,. "'"""'""' • ,,.,., '~" D
•
~
• _si; (surface soil)--<,::::::=o\..O.\ \ \ .•. ,---~
C0-003-SB (@2.5-3.0fei°t)~ I CO-WS-28 (UST#8@ 10-12 feet)~-, I . 11 J CO-WS-31 (UST#7·@ 10-l2feet). . _ _\ L-,..---6 1 CO-WS-38 (UST#7@ 10-12 feet). i f t)+<,.::--=-' I
. -CO-002-SB (@ 2.s-3.0 ee '-----·
Figure 3.
Source Sample Location Map Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg Co., N.C. US EPA JD: NCD 980 799 019 Map Not to Scale
Map Drawn By: D. Moore (Aug. 1996)
Soil Samples
\ \
Contaminant Units CO-OJI-SL
Acetone < 20,0
Meth lene Chloride < 5,0
l, 1-Dichloroethane <5.0
2-Butanone < 20.0
Cls-1.2-Dichloroethene < 5,0
Chloroform < 5,0
l. l, 1-Trich!oroethane < 5.0
Benzene <5.0
1,2-Dichloroethane < 5,0
Trichloroethene < 5,0
Bromodichloromethane <5,0
Toluene <5,0
l, 1,2-Trichloroethane <5.0
2-Hexanone <10,0
etrachloroethene < 5,0
Chlorobenzene < 5,0
Eth I Benzene <5.0
X lene s <5,0
1,4-Dichlorobenzene <5.0
l,2-Dichlorob < 5,0
Meth 1-tert-bu < 5,0
CO-OJI-SB
5J,C
7J,C
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
Table !A
Cherokee Oil Company
Charlotte, Mecklenburg County, N.C,
US EPA ID: NCD 980 799 019
Analytlcal Data -March 1996 Source Samples
CO-OJ2-SB CO-0J5-SL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
10
CO-0J6.SL EPA Soil Stds m /k •
BDL
2J,C
BDL
BDL
BDL
BDL
BDL no
BDL 22
BDL 7,0
BDL 58
BDL 10
BDL 16,
BDL 11
BDL
BDL • BDL 1,
BDL 7,8
BDL 160,
BDL 27
BDL 7,
BDL
/ ,
/
/ -· /
, ,
/ / /
/,,
Contaminant Units CO-OJl-SL CO-OJl-SB
< 330.0 BDL
< 330.0 BDL
< 330.0 BDL
< 330.0 BDL
Phenanthrene < 330.0 BDL
Anthracene < 330.0 BDL
F!uoranthene < 330.0 BDL
< 330.0 BDL
Be thracene < 330.0 BDL
C < 330.0 BDL
< 1650.0 BDL
< 1650.0 BDL
< 1650.0 BDL
< 1650.0 BDL
< 1650.0 BDL
< 330.0 BDL
< 330.0 BDL
Di < 330.0 BDL
Bu < 330.0 BDL
Bis < 330.0 BDL
< 330.0. BDL
PCB 1254 <0.l < 0.1
Table lA.
Cherokee Oil Company
Chartotte, Mecklenburg County, N.C.
US EPA ID: NCD 980 799 019
Analytical Data -March 1996 Source Samples
CO-002-SB CO-OJS-SL
330 K
330 K
BDL
BDL
330 K
<0.l
11
CO-006-SL EPA Soil Stds m /k
330 K
330K
BDL
BDL
non
•
1Fcontaminant Units CO-OJl-SL CO-OJl-SB
Arsenic mQik0 2.8 4.4
TCLP-Arsenic moil <0.01 <0.01
Barium moiko 124 68
CLP-Barium ma/l 0.59 0.44
Cadmium maika < 10.0 < 10.0
CLP-Cadmium mail· <D.05 <D.05
Chromium maika 22 30
CLP-Chromium mail <0.05 <D.05
Co 1r er maika 34 52
CLP-Conner moil-<0.05 <0.05
Lead maika 36 20
TCLP-Lead mail <0.10 <0.10
Mercurv maika <0.l <0.l
CLP-Mercurv mQil <0.01 <0.01'
Selenlum moiko < 1.0 < 1.0
CLP-Selenium mc,il <0.005 <0.005
Sliver maika <10.0 < 10.0
CLP-Silver mail <0.05 <0.05
inc maiko 56 62
CLP-Zinc mail 0.07 · 0.12
Table lA.
Cherokee Oil Company
Charlotte, Mecklenburg County, N.C.
US EPA ID: NCD 980 799 019
Analytical Data -March 1996 Sour~e Samples
CO-OJ2-SB CO-OJ3-SB llli!"@!()()if-SL CO-OJS-SL
2.6 2 2.5 2.9
<0.0l <0.01 <0.01 <0.01
82 124 140 63
0.75 1.27 -0.67 0.43
<10.0 <10.0 < 9.8 <9.8
<0.05 <0.05 <0.05 <0.05
30 38 55 16
<0.05 <0.05 <0.05 . <0.05
62 46" 55 55
<0.05 <0.05 <D.05 <0.05
58 20 90
· <0.10 <0.10 I© <0.10
<0.l <0.1 <0.1
<0.01 <0.01 <0.01 <0.01
< 1.0 < LO < l.0 < l.0
<0.005 <0.005 <0.005 <0.005
<10.0 < 10.0 <9.8 < 9.8
<0.05 <0.05 <0.05 <0.05
92 44 N,f,
0.32 0.09 P•Ji
CO-006-SL
2.9
<D.Ol
57
0.49
<9.8
<0.05
41
<0.05
37
<D.05
DW
<0.10 .
<0.1
<0.01
< 1.0
<0.005
< 9.8
<0.05
Shading indicates >I= 3 x background, or > background. if bkgd. = ND BDL = Below Detection Limit
Bold Indicates a concentration in excess of applicable EPA soil exposure or TCLP regulatory standards.
CPF • refers to the August 19, 1996 EPA SCDM Cancer Risk Screening Concentration standard (Ref. 17).
RfD · refers to the August 19, 1996 EPA SCDM Reference Dose Screening Concentration standard (Ref. 17).
EPA -refers to the EPA soil lead guidance level (Ref. 42). ·
J = estimated concentration
C = possible lab contaminant
TCLP -refers to the Toxicity Charactenstic Leaching Procedure as outlined In NCAC Title 15A Chapter 13A Appendix II. Method 1311.
TCLP Limit -refers to the TCLP regulatory standard (NCAC. Ttile 15A Chapter 13A. Subpart C, section 261.24. table I). (see Ref. 41 ).
12
EPA Soil Stds.
0.43 m□ika (CPFl
5.0 mail CTCLP Limit) • 5,500 m□ika (RID)
100.0 mail (]CLP)
39 maika (RID)
1.0 mail (]CLP Limit)
390 maika (RID)
5.0 mail (!CLP Limit)
none Issued
none issued
400.0 mQika (EPA)
5.0 mail (]CLP Limit)
23 maika (RID)
0.2 mail CTCLP Limit)
390 maika <RIDl '
1.0 mnil (]CLP)
390 maiko (RID)
5.0 mail (TCLP)
23,000 maika (RID)
none Issued •
•. _ ~ederal _ .•
inp Not1ficat1on & Authonzat:J.on
Prepared by: 7). Mo-oil£
• Use Dlack Ink or Typewriter only-S1aff to fill out first :? blocks only.
Site Trip.
Date of Trip: Nove:ei~,,_ 2.lJ. l'l<f ""> I
If trip date changed or cancelled note below:
Trip Date Changed To: Cancelled: --
NCD#: qi 1'l'l 0 ''I-Site Name: C-u-e/tD~
,:) I~ Ct:1M.PA#'f
R,,c~DoJ!ieS .,.
City: On,,eu,zn=;: County: MeaL~IJtwy,.
Reason for Trip: O;J -S,Tt? · RFcoNw~, S-SkAJ t--e:.
Name of Hotel (Overnight Trip):
Project Team Leader: fevG,w,s. ~
Assistants: ~""'~ ,el'!!I.Fl:JM
Attach To Notification Form: 1 copy each:
Submit to the
Industrial Hygienist
Hotel Telephone Number: ( )_-
Authorized by: Q•jg/Jt I , --i'/4
~Industrial n£<n1st
, '
Preliminary Assessment Form (First page only)
Site Map
PA Transmittal Letter
(!'lease list appropriate County Health Department contact person to call lO adviSc of trip) S"c ;; d 1 1£ c: , t,.;,.-
Title: r:.,,.,,,,~. A:,-Environmental Supervisor or Health Director to call: /kn'7 ')er f.k.,.,
(Note ir Dr., M.l'., etc.)
Telephone Number: (?cy) s $~ -J :coo
Notes: Health Department Official Contacted:/rt,S",vc,L [,-fuN,-/f
Back Up Letter Required: Yes No /
/1/o±,CeJ /:ls~ C J,,Jevis "'-J/-:Jit-•/ 7 £,
Note: Sil!flcd original to Data Manai,:cr
EPA asks
city to pay
in waste
cleanup
By BETTIE FENNELL
SJ11ff Writer
Wilminglon's use of an oil rccy-
ding company 10 years ago ha.<;
cu11n; \J;u;k tu h;mul the cily.
Wilmington is one of about JOU
governments and businesses thal
arc being asked to pay Enviro11-
111c11tal l'rutcctiun Agc11<,;y L·x-
penscs to clean up two haz:irduus
waste oi!"sites ownt<d by Cherokee
Oil !{(:sources in Charlotte.
In 1986-87, Wihnin&tun had a
one-year contract with the com-
pany to recycle waste oil from the
.-.city garage, said City Atturn_cy
<:;,,... _ _Tom Pollard. Records ,shOYf the
·:,·, city sent 3,136 gallons of waste oil.
· · · to Cherokee Oil. ,
The El'A says the city's shai-c lo
properly di!!posc of the oil and re-
.. ~·· imbursc El'A for its administrative
-1,· costis$3,734. ,·
The EPA ~ays Cherokee Oil
mishandled waste oil and other
hazardous matcri,1\s al ils two
sites, •including one lhat was nut
permitted. After determining thal
the materials posed an immediate
threat to nearby residents and
businesses, tlie: EPA.had ·it .re•·
moved nn<l disposed of ii, a· perrnit-
ti::<l facility. .
The company's two top cxecu-
Liv'-'s W(.:nl lu prism1 in lalt: HJLM f,.r
flushing, toxic wastes down Char-
\ullc sewt:rs. '111c El'A dismantlt:d
steel storage tanks on the properly
and sold the co11taminalcd steel as
,;t:r.111 for $10,UUU. l.lut El'A rult:s
don't allow the mOney lo be used to
pay for the cleanup.
When :, ,company violates El'A
rules, the federal agcncy·secks tu
rt:L'OVCr its cost from the "poten-
tially responsible parties" or thhse
that sent waste products to the
cu111pany, Mr. Pollard said. Tht: ·
EPA 'estimated the cleanup wi!l
cost $6.5 million aud said -the
·money it is• trying tu collect ·from
. ,Cherokee Oil's customeis will pay
· only a small part of the total co~t.
· Tlie. state ·Tr~nsportatio11"·Ue-
·Jl:iflme11t is among lhosc that EPA
hopes to collccl from. !{econ.ls
: show the Transportation· Dcp,1rt-
. ment Owes.$5,715. · -··
Others' include several· nation-
wide Lruckini: c;ompanie:;, retailers
. such as K mart and St!ars, numer-
ous ·gasolin_e .. slations ind ·a Wil-
mington car dealership. '.-' ·_,:'"
The EPA is lryin~ to collect be-
tween $1,620 to $23,663 from each
company and gOvernment, c\t!pend·
ing on the ·amount ;md toXicity of
the waste each st!nt lo Cherokee to
be proccssed,'Mr .. Pollard said:
Those that arc bcin~ ;1skcd lo
pay fur the ckanu11 sc11t between
1,350 gallons _and 20,000 gallons of
w;,ste products. · · ·
Mr. l'ollarcl said El'A has been·
criticized for Lhe way it handk.·s
dc;u1u11s, especially. its IIC)licy of
"retroactive liability." When the
city contracled with the Cherokee
Oil, it believed the company would
~d-ispose o.f the Oil, he \\id.
• • State of. North Caro1ina
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
January 20, 1997
Attn: Mr. Gene Miller
Miller Sherrill Blake, CPA PA
2415 Tuckaseegee Road
P.O. Box 668307
Charlotte, North Carolina 28266
Subj.: Soil Sample Analytical Results
Cherokee Oil Company Site
120 I Berryhill Road
Charlotte, Mecklenburg County, NC
US EPA ID: NCD
Dear Mr. Miller:
As you are aware, the NC Superfund Section collected two soil samples (labeled CO-001-SL and
CO-001-SB) from a grass-covered lot directly south of the parking lot behind your office to represent
typical background conditions of regional soils, as part of an environmental assessment of the subject
site. One soil sample was taken from the top 6 inch profile (CO-001-SL) and the second was taken
from 2-3 feet below the surface (CO-001-SB). Both soil samples were analysed by the State Laboratory
of Public Health for the chemicals listed on the attached sheets.
Acetone and methylene chloride were detected at estimated concentrations in the subsurface soil
sample. The laboratory report indicates that these two compounds are artifacts generated during the
analyses of these sarnples and should not be considered actual contamination. No other organic
chemicals were found in the two soil samples. Arsenic, barium, chromium, copper, lead and zinc were
detected in both soil samples. However, these metals were all detected at levels below the State
Inactive Hazardous Sites branch health-based soil remediation goals. Therefore, they are not considered
to pose a threat to workers or residents at the site.
A copy of_ the analytical results are attached for your review. Thank you for your help during our
recent sampling trip. If you have any questions, please contact me at (919) 733,280 I, ext. 315.
cc: File
Pat DeRosa
Sincerely,
Douglas Moore
Environmental Chemist
NC Superfund Section
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ l 0% post-consumer paper
l m 77 17712 7 1FTNF3¥M f@R ISYW s:smr rn sn
1-.:.,C. r.::;p_:.:,r::r:1cn( of Emiron:i1cnt,
. ; i..:.::lth, & Natur;:il Resources.
·\.:;:i(l. \1/;,st.:. ~1.10:igcrncnt Division
Name of Site
C0-001-SL 03/06/96 · 1501 GRAB
Cherokee Oil Company, .NC BACKGROUND SURFA.CE SOIV .
ESD LAB VOA Soil
1
DOUG HOORE
iu.Y--uatc l...OHcctcd Time
Colkcted By _______ ~------------------------
Agency: Haz.1rdous Waste Solid Waste /superf1rnd
Sample Type
Concentrate Com111ents
___ Ground water (1) _ Solid (5)
__ Surface water (2) ___ Liquid (6) ____________ _
/ Soil (3) _ Sludge (7) _______ _ ·---
-· Other (4) Other (8)
Or-ganic Chemistry Inorganic Chemistry
Parameter Results(mg/l) Parameter Results(mg/1) (mg/kg) vi'&TGC/MS
{'<~.Acid B/N Ext.
,: -MTJ3E
·--------
·-------
--------
Arsenic
Barium --Cadmium --Chloride
Chromium --
--Copper
--
Fluoride
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium --
Silver --, Radiochemistry
1·---------------l Sulfates
' l';irametcr
____ Gross Alpha
Cl ro.ss Beta
Results (PCi/1)
Mic:rnbiology
Pararnc!cr Results (Col/1001111)
-----------
., ... \ ,,.
Zinc --_pH
__ Conductivity
TDS --TOC
-------
TCLP Compounds
IuorgJ.nic Compounds
Arsenic --Barium. --Cadmium --Chromium --Lead --Mercury ---
Scknium --Silver --
--
--
--
--
Organic Con1po;1nds
benzene --carbon tetrachloride
Rcsults(mg/1)
Rcsults(mg/1)
----------chlordane --ch!orObenzcnc --chloroform --o-,:rcsol --m-crcso! --
--p-Crc.sol
ere.so! --1,4-dichlorobenzene ----1,2:dichloroelhane •
1,1-diehloroeth ylcn c --2)4-dinitrololucnc. --
--hcrtachlor
hcxachlorobcnzcnc --h -;x,1 ch lorobu tad icnc --hex.a ch !oroe th anc ----methyl ethyl ketone
nitrobcnzcnc ----pentachlorophcnol
__ pyridine
__ tctrachloroethylcnc _______ _
__ trichlorocthylc11c
__ 2,4,5-trichlorophcnol
__ 2,4,6-trichlorophcnol
__ vinyl chloride
------1
N.C. Dcp..:1irr1cnt of En•1ironmcnt,
j ·; k.illh, & Natur:il Resources
WIPLE ANALY:.,IS REQUEST • .:~'..~_le i ... 1b0ralo1y of Public ! lc:d:h
P.O. Den 2&}17, 306 N. \Vilmington _S1rc~t
R.a"tcii;h, N0tlh Carnlina 27611 I _-Solid Waste Man::igc."n:icnt Division
•.. Site Number_ CO·OOl·SL 03/06/96 1501 GRAB
Cherokee Oil Company, NC
BACKGROUND SURFACE SOIL
DOUG HOORE Number r-1~'.~>.
, .. 'Name of Site ESO LAB EXT/PEST Soil
2 Collected By __________ _
Agency: Hazardous Waste Solid Waste ✓ Superfuod
Sample Type
Environmental Concentrate Comments
_ Solid (5) __ Ground water (1)
__ Surface water (2)
v'soil (3)
_ Liquid (6) __________ _
Sludge (7) __________ _
__ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
.
Pilrnmcter Results(mg/1) Parameter Results(mg/l)(mg/kg) ·
Radiochemistry
Parumdt.:r Results (PCi/1)
__ Gross Alpha~-------
Gross Beta
Arsenic
Barium --Cadmium --Chloride
Chromium --
--Copper
--
--
Fluoride
Iron
Lead
Silver
Sulfates
Zinc
__ pH
__ Conductivity ______ _
TDS --TOC ~--------------_J --
tvl i cro bi o Io gy
Par:1n1t.:lcr Results (Col/lO0ml)
-------
-----
-------~----'----'----
TCLP Compounds
Inorganic Compounds
Arsenic --
--
--
--
--
--
--
--
--
Barium
Ca<lmiu111
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon tetrachloride
Rcsults(mgilj
Rcsults(mg/1)
---------
--
--
chlordane
chlorobenzcnc
chloroform
o-cresol
ri:i-crcsol
--p-crcsol
crcsol
__ 1,4-d:chlorobcnzene ______ _
__ 1,2-dichloroe~hanc
__ 1,1-dichloroethylcne ______ _
__ 2,4-dinilrotoluenc
__ heplachlor
hexachlorobenzcne
hexachlorobul adiene --__ _:_ __ ~--
hcxachloroel hone --
--methyl ethyl ketone -----~-
nitrobcnzcnc ----pentachlorophenol
__ pyridine
__ telrachlorocthylenc
__ trichloroethylcne
__ 2;4,5-trichlorophenol -~----~
__ 2,4,6-trichlorophenol ______ _
__ ,inyl chloride
e:1drin --lindane
__ ,,,cthoxychlor
__ tOXJ[)ht:nc
--2,.: I)
__ 2,~,5-TP (S:l:cx)
---·-----
--------
'
~.:.C. [),~p;ir;:-:·,cnt c.i En,.ironr.1cn1,
' ! [c;,lth, & i','al11rJl Resources
Sc-lid \1/:is:c ;,,...i.:.11;:gc:nc:H Di .. i.~ion
SA.i\<IPLE A.t"iALYSIS RE(_; EST
Site Number_
,f>;.:·.,e of Site
• co-ooi-sL 03106/96 1so1 · GRAB ·
Cherokee Oil Company, NC
BACKGROUND SURFACE SOIL
ESD LAB METALS Soil
DOUG MOORE Number
St:itc !,..1t,0:JIO!"/ 0: :·uc11~ !1c~;:.---:
r.O. 110.~ 2S.0--:7, 3()6 t<. \1.,'i!r.,ini1on _St rec:
•· . R.alo:it,h, North Urolina 27611
------------------
Collected By_
3 ....... u<'-' vvu1.:.1...lCd Tln1c ----------------------
Agency: Hazardous Waste Solid Waste V Superfund TCLP Compounds
------
Sample Type Inorganic Compound.'> Results(mg/1)
Environ men ta 1 Concentr3te Comments V Arsenic <c_.-.\
vBarium Cl,,!i9
Ground water (1) _ Solid (5) ✓Cadmium .L.O,a:j
--V-Cbromium ""'-0-05
Surface water (2) _ Liquid (6) vLead -<'....~-, .. \a
--l/'"ivfercury -<c. c]
✓soil (3) _ Sludge (7) v Selenium -~t:}11,~c:1
v"'Silver .Zo,D.5
Other (4) Other (8) _g:: (..,,Ee-.L_ C , C ~·
:Z.,;.11; .... Q-O:J --
--
Oraanic Chemistry Inorgan.ic Chemistry
b --
Parnmeler Results(~1g/l) Parameter Results.-.) (mg/kg) Org,111ic Com pour.. ds Results(mg/1)
__ P&T:GC/MS v" Arsenic J.8 bt:i17.CIIC --
VBarium __ Acid:B/N fat. ) '.1 'i . carbon lttrachloride --
,-, •• Co"'. MTBE v Cadmium -<:.)Q chlordane
"<.(;:_. -----. -~-Chloride chlorobenzcnc
<..-:• ------
--V""Cbromium J.:), chloroform --
--V"'"Copper -⇒'::\ o-cresol --
Fluoride m-crcsol
------
--]ran __ p·cresol --
--vLead 'JC:-, crcsol ----
--__ Manganese --1, 4-dichl orobcnzene
--.,.,---Mere u ry < ()_, i --I, 2-dic h lo roe thane
--Nitrate 1, 1-dichloroethylenc
----
✓Selenium -<. \ 2, 4-di ni lrolo I u enc --
✓Silver 4iC __ hcplachlor
Radiochemistry Sulfates -heuchlorobenzcne
----... ✓Zinc .5G. hcxachlorobut a<licnc
----
P11rameter (PCi/1) hcxachloroclhane Results _pH
__ Gross Alpha __ . _ Conductivity = me:hyl ethyl ketone
--Gross Beta TDS nitrobcnzcnc
----
TOC penlaehlorophenol . ,
----__ pyridine
--l'v!icrohiology ----let r achloroc th ylcne
trichluroethylenc
Parameter Results (Col/l00rnl) -----2,4,S·trichlorophcnol
----
--2, 4 ,6-tricWorop heno I
----vinyl chloride
-----endrin
'·,
--
" lind:1.nc
Date Received
---
Reported by r:1cthoxych!or
------
D'1te Rcp,1rtccl_j_4:_~~
__ toxripbcnc
D:ilc Ex:.r:1ctct! 2,"-D --'1Ql/c-14 .,., I 2' 5-TP (S"" "•) u . .._,; ~•·t I• I,\ '-; __ , ,, .. 1 .. c ..
Dale /,.n:1!y·.1.cJ ·-.. --···-·--·· ... ........ . ... -·. L;1h Nun1hl·r ··-···-·---···-·-· . ----·---·--·-----
". ',· -·--·----······-·--·-··-·-----· I
, t'\'.C. Dcpnrtment of Environment,
·1 ltnlth, i NJlur:i\ Resources
· ··SOiid WastC Man:igcn1,;ni. Division
s,wPLE ANALYSIS REQUEST
C0-001-SB 03/06/96 1515 GRAB
Cherokee Oil Company, NC DOUG MOORE
BACKGROUND SUBSURFACE SOIL • ·•
ESO LAB VOA Subsurface Soil
• ."•.:ilc Labor.i.tory o( Public lkJllh
P.O. \';.:ix 2S0-47, 306 N. Wilmington _St reel
·: ~Zalc[gh, Nq_rth _µrolir111 _2_761 J
co-7 Collected By __________ _ ,d ___________ Timc ______ _
Agency: Hazardous Waste · Solid Waste v" Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Rcsults(mg/1)
Environmental Concentrate Comments Arsenic --Barium --Ground waler (1) _ Solid (5) Cadmium ----Chromium --Surface waler (2) _ Liquid (6) Lead ----
--Mercury
✓soil (3) _-_ Sludge (7) Selenium --Silver --
_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Pam meter Results(mg/1) Parameter Results (mg/I) (mg/kg) Organic Compounds Results(rng/1)
V P&T:GC/MS Arsenic benzene ----
I /:~Acid B/N Ext. Barium carbon tetrachloride ----MTBE Cadmium chlordane ----Chloride chlorobenzcnc ------Chromium chloroform ------
--__ Copper o-crcsol --Fluoride m-crcsol ------
--Iron p-crcsol ----Lead crcsol ------
--__ Manganese 1, 4-dich lorobcnzene --
--__ Mercury 1,2-d ichloroethanc --
--Nitrate 1, 1-dich loroet h ylene ----Selenium 2,4-dinitrotolucnc _ ----Silver heptachlor ----Rad iochcmistry Sulfates hcxachlorobenzene ----
Zinc hexach lorobut adicne ----Paraffleter Results (PCi/1) --pI--1 hc.xachlo roet h ane --__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobcnzene ------TOC pentachlorophcno\ . , -----
----pyridine
l\>licrobiology ----tel ra ch loroeth ylcnc
-trichloroethylcne ----
P,1r:1111ctcr Results (Col/JO0ml) 2, 4,5-trichlorophcnol ----2,4,6-'trichlorophenol ------
-----,onyl chloride
-... endrin --
.3-7-</,b'/;lff;tbcportcd by
lindanc
Date Received --mc.thoxych!or --tox.:1rhcnc. --Date Extracted Date Reported 2,-'.-D --2 -~ 5-TP ((.'i 1··cx'1 196'.ti-"i.:48 --, '' .J ' ' ' .I
D;1lc ,1-\:1:1!v>.cd 3-!8-9~7J(._j)-L:ih Number
N.C. Ccp:irtment of Environment,
! lc::iiih, & Natural Rc..:ourccs
Solid Waste Man::igerr:ic·nt DivisiOn
swPLE ANALYSIS REQUEST
co-ooi-sB 03/06/96 1515 GRAB
Cherokee Oil Company, NC DOUG MOORE Nllmbcr
BACKGROUND SUBSURFACE SOIL · · · ·
(SD LAB EXT/PEST Subsurface Soil
co-8
LJdlC ·\.....VllCCtCd
• .Statr-. l ..ab0ra,,:,y uf !'ubii:: He::lth
i~.u. Bo:c 250--l7, J.:{; N. Wilmington _Street
Ralcit:h, North Carolina 2761i
------------------
Time Collected By __________ _ ---------------------
Agency: Hazardous Waste Solid Waste V Superfund TCLP Compounds ------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments Arsenic --Bar:um --Ground water (1) _ Solid (5) Cadmium ----
Chromium --Surface water (2) _ Liquid (6) Lead ----
✓soil (3)
__ Mercury
_ Sludge (7) Sc!e.nium ---·· Silver --_ Other (4) --Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Pam meter Resu Its (mg/I) Parameter Results(mg/1) (mg/kg)· Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
.~··:•? Acid:B/N h1. ----Barium· carbon tetrachloride . ;.,:; .. ::-----\':·.·,,· MTBE Cadmium chlordane ,. ·✓ 7t:.8 '., /Pft',TI c.1 DcS ----Chloride chlorobcnzcnc
'Pci?f <C:,,/()pr------Chromium chloroform ------_ Et1cl1?.tN' . -<:O, I Al,{,,,.,, __ Copper o·crcsol
7/N~NE < 0,-7,0~,rt --Fluoride rn-crcsol ----r,7;, . _-r; . <: I• ,.. :-,-,:., lron p·cresol ----~.,. -/. -· ~ <:: 1 • /l TA.,._~ Lead . ere.sol f)Af:rj flt€: <O, -_, . ----__ Manganese --1, 4-dichlorobcnzenc _:;}~f,j,:6~4--=:o, tt! o/J"' __ Mercury --112-dich loroeth anc
~"'-Efi?o;,uu<o:7t(, Nitrate 1, l •dichlorocthylcne --Selenium 2)4-dinitrotoluenc. ----Silver __ heptachlor --Radiochemistry Sulfates hcx3chlorobcnzcne ----
Zinc hexac h lnrobu tad icnc ----Panirncler Results (PCi/1) pH hcxachloroclhanc ----_·_ Gross Alpha __ Conductivity methyl ethyl ketone --Gross Beta TDS nitrobcnzcnc ------TOC pentachlorophenol .. . , ----
----pyridir1~ ·
lV!icrobiology --__ tctrachlorocthy!cr.c
----trichlorocthylenc
Parameter Results (Col/l()0ml) --. _. _2,4,5-trichlorophc110l
----__ 2,4,6•trichlorophcnol
--__ vinyl chloride
'• .-endrin --
3-7-C/6 tv/3 At,i.cportcd by
lindanc
Date Received --mcthoxyCh!or --fay'r:Mr 3··1~--'TG AB --toxJphenc
\);ilc i:xt raucd 8-11 _q(c Sb..M ___ Date Reported ___ 2,t,.\) --
t3/Jlr ~7 'Pt?O.f '961'.4 '49 ' 2,·1,5•Tf' (S,! .. ·cx)
I);,[.'. ' • ' 1-i-. , .~ _ .. _;;:1h·?.U.'. , _., -.:1h N ln\ 1 '. . :Jl
1'.C.·D,:p..irtr.1c:1t of Environment,
! icJllh, & NJtu:JI Rc::ourcc~
·Solid Wa~lc ManJscrrycnt Division
SAMPLE ANALYSIS REQUEST • • St:ilc l...abor..11ory o( Pu.:,:.: H::l1h
r.O Oox 280•.:?, JC.6 :'i. Wilm;:-,gton .S!r:;::
Raleigh, North Carolina 2'/0i.l
· Site Number_ I 1?!:C,,
C0-001-SB 03/06/96 1515 GRAB
Cherokee Oil Company, NC DOUG MOORE
BACKGROUND SUBSURFACE SOIL .
Number _________________ _
l\L:aii1e of Site_ ESD LAB HETALS Subsurface Soil
co-9 Collected By __________ _ ________ -~··~--c:.d ___________ Time ______ _
Agency: Hazardous Waste Solid Waste V Superfund
Sample Type
Environmental Concen trJ te Comments
__ Ground water (1)
__ Surface water (2)
v"soil (3)
_ Solid (5)
_ Liquid (6) ___________ _
_ Sludge (7) __________ _
_ Olhcr (4) _ Other (8)
Organic Chemistry
Parnmeter
_P&T:GC/MS
Acid B/N Ext.
,<i.x MTBE ¼ ,!•-•. -
Results(mg/1)
Radiochemistry
Inorganic Chemistry
Parameter
.,/ Arsenic
,._.,,,--B a r i u m
✓Cadmium
Res11lt4': g,"'l'!:, g/kg)
':\ .. :'1
--Chloride
v Chromium
vCoppcr
Fluoride
Iron --,,,.,---r.e a d
__ Manganese _
V' Mercury
Nitrate
L/'" Selenium.
vSilver --
Sulfates
3c
< D, i
1--------------_____j v-"Zinc
Parameter
__ Gross Alpha --------Gross Beta
Results (PCi/1) __ pH
__ Conductivity _______ _
TDS
TOC
/vlicrobiolog)'
Par;.inu.:ter Results (Col/lO0ml)
------------, .... · -___________ J_ ___________ _j
Date R~ccivcd _________ Reported by __________ _
i);itc btrJClC~---------Dale Rm•· :1'",ie~ _._6 .... □ 'I I"". "ii '--",c11.!, ,~, .,",.-+<R.-'Q.U/.s--. , \ ') ·"'.' '-I u : V
LJh Nu;nbcr
TCLP Compounds
Inorganic Compounds
✓Arsenic
vBarium
Results(mg/1)
v Cadmium L.o. o5
---1,L Chromium
,__,.,.-Le a d
V--Mcrcury
v Selenium
✓Silver
""-0· oS
_ __ ..c... c ~ cc.:5
L....a.., c. S
✓ f'.._f',e-<v ✓ :hn"
Organic Compounds Results(mg/i)
benzene --carbon tetrachlori<lc --
cidordane --chlorobenzcnc --
chloroform --
o-cresol --m-crcsol --
--p-crcsol
crcsol --1,4-dich lorobenzene --1,2-dichloroctbanc --
--1, 1-dichloroethylcnc
2,4-dinitrololuenc. --
--heptachlor
hexachlorobenzcne --h e.xach Io robu I ad icnc --hc.x;ichloroelhane --
--methyl e.thyl ketone
nitrobenzenc --
--pentachlorophenol . '
p)Tidinc --tel rachlorocl h ylenc --trichloroclhylcnc
--2,4,5-lrichlorophenol --2, 4 ,6-trichloropbenol --
--vinyl chloride
endrin --lindanc --
rncth0.\)1Ch!or --
tox:1ph:..:11:..: --2,t.-D -·-__ 2,.1.5.Tr (S,!·,cx)
·----. ----------·-------
. STA~RATORY OF PUBI.lC HEALTH.
PO BOX 28047 -306 N. ~GTON ST .• RALEIGH, 27611
ORGANIC CHEMICAL ANALYSIS
i
I
~
I ,;
• • •
-
l'URGEABLE COMPOUNDS
COMPOUJVD
Clil,O RO AaT1L-\. '<1:
' VllfTL c.m...oRIDE
BROMOMEI'fil\..~
CHLORO?:TH.A?il:
TRlCl!LOROF"UrOROA,U;'I"1IA!'ll
,c,:rorrr;
1.1.ou:m..aRor:rm:m:
IO 001£!:TRAlr?;
JC!::Tl'fT1Z="1': CHLORIDE
C....-..UO!'f D1SOU"ID!:
TRA!'f'B.-1~-DI CHLO RO l:TH?.."f'E
f--. Jj/~:~?fn"lUU
l.l•DICILOROnB..-\I'a-
:l--BUTA1ml'O.
CIS--1,.3-Dtcm.DRO!:TlrDf!:
CRLOR01'0Rl(
1.1. ~ • nucm..o ROrI"l!AJ'rE
.
CARBO?( 'TE'TRACBI.ORID!:
=
1,:1--DtCBI.ORO!:TRA.N'E
TRICRLORO~
l.2•Dlcm.DROPROP.Alfl;
BROMODICBLORO~
LAB NO
FIELD NO
TYYE
M~s:? (ppb
J.0
,o
d0
10
JO
,;2.0
5
' /
XD
5
.;1c)
5
\ /
ff&'/'/ /d-}f '\; . '-'• -~ 9UJJI 4Gi
I co-+
( 3 l (3 l
'pp.)? ppm "(-pb ppm
.
LL I
'
'
IO;;). :J
/ j
\ I
u,
VJ -:s
3~
ll--
9
u...-
+:r
+rarP.
31
/.,L
' I J/
C-.Pc¼,e--.;: 1-Al3 <:o"'Tl'\Mlr'flTIO'-.i OR BAC.J;.6-~c:ul'JD.
I] J -X•ti.:nat ■d vUu.-
1';. -ActuaJ. va.lu ■ ia ·lcn.o,tu to b• l••• than va.lue given.
9Iff'JJ116-'
co-7
(3 I
rppb pprn
(,
.., I
5 J;C.
/j
,v'
7J,C..
U--
' I
9lol /8{] q&, II 5;;;__
CO-/ 0 CO-/ 3
( 3) ( 31
/ppb}pm lppb)ppm
I) u._
' I \ I
i O lJ,, :r ;;;_ ;;}_ 7 .:r
j J I
,/ /
3 T,C.
u -
\ / \
CJ ;J J.
5-:s 10-:r
fra.<-e.. ITl'll"P
+ra.c.1:..., frac.e.,
~J -/-,(), p
I I LL
.;zJ Lo
LL +rnc.P
/J +race..,
l,L. LJ__
J/ -1-rnrp
.
~ --'ctual va1ue is lclown to b4 greater than value ~ivon.
\, _,.. -XAteriaJ. waa ana.ly:z:•d t:or hut not datect•d. 'l'b• nu:mh•r i• th• ld.in.i.mum O.t ■ction Limit •
. NA -Sot a.naly.c ■d.
•
1/ -Tac.tative identification.
2/ -C:O"'-l'ou.\'io .Rfi.lJ",ElL-'f·DET"ECi"l'\'6U:: OIJL'/ lrJ tt l(rt-1 C.oNC<:,lTRf!TlclJ5,
v'-SA,-\PLtc 1-\1&1-\L'/ QILu.TE D, f-\Dc'-:> Do t-k>T APPL.'{.
I DEHNR 3065-0 (10/93)
C/(,;J I I 6L/-
<.o -1 G
( -3 l I
-'ppb) (P;n
lL.. I
;
" 1/
• • ••
. STATE IABORATORY OF PUBLIC HEALTH.
PO BOX 26047 -306 N. WILMINGTON ST., RALEIGH. NC 27611
.ORGANIC CHEMICAL ANALYSIS
PVRGEABLE COMPOUNDS LAB NO "9.1-Yi'iJll · ... @m~ .. 9/.o/ ll/1.() <if{JI I.Wfi, q0115D 9/.JJI ISd
FIELD NO I Co-tf co-7 CO-JD Co-13
.
COMPOUND TYPE ( 3 ) ( ,3) ( ) (3 ) (3 )
[?,~f/ 'ocb)pprn Pll b, }Pf'rtl ppb]pprn rppb)pprn rfPb)ppm
D rBROMO ~ 5 LL-LL / L-i I I
4-HZ'THYL-2-nNTAN'OK!: tO
CIS-1.:S·DICHLOROPROP?:_;Y?:. 5 ,I ,>-'/
TOLUL'f!: I 3oc1 ;)7 //70
TRAl'l'S-l~DIClll.lJROPROP!:.Nl:
(1 u__ I,
I l. l.2.l-TttRAC&OROE'T!lA1fE
J_;
1.1.:1-TlUCXLORDrnlA.'fl: ' / +race.., ' 1/
2.-Hl:X.A.,..OMJ; /0 ,/ I , if 'J !/
Trr"RI.CHI,DROnBZ:u; 5 30(., +ra.ce,, 7
DIBROMOCHLOROJ.O;raA.'T?:
/J I, LL
]t~.~ DtmtOMID~
Ji ,/ /
I ~RO~
I I frcu_e_
1,1,l~n:t"RACHJ..OROE'TBA?a
LL L,_ ' /
~ mm. BmZ!:1'!:
~34-+-race.. ;}.'7
== I II lP qJ I J.5
I = '
(1 {,,(__ u__
BROMOF'OR.K /0
TllMB--1.4--DlCRLORO-l-BO'TI::?f!: io
" 1,l.:S-TlUCBLOROPROPM?: 6 ,I
I 1.4.-DJc:m..oROBE117X?B I ~o ' I \
l.l-Dicm.oROB!:?rll:X!: '1,t 51 +rcue-+rru.e..,
1,2-DUlROMQ-.3-Clll.OROPROP..\l'(g ;;_t) l<-u__ LL
'VINTI. AJ:r'tAU:. ;x>O
Ji ,I/
MdAv 1-f-bul-,, I c.J.J.,,,, 5· I / , I ,/ / s frarP
'
..
I (!) 8 H (+ 0 (+-) ( +-
J/v/!rotor hc,n::, £°
5~b::,1-,fufed benZ;ne'
-f P°""'01..c 1-f\6 CCNTRMl>.lf\110N OR Bf\~l<Crt<OllND.
· Zstim.at ■d V'lllu ■ ·
.::~(~~--.lctual v&lu ■ i ■ :Jcncn,n to be l••• than Ylllu ■ aiv ■n.
L -1..ctual V11l.u ■ i ■ k:no,im to b• ar■at■r th.an Talu ■ g-iv.n.
'
U -Jilea.terial was &nA1}"'%■d for but not d ■t■_ct ■d. Tb• nu=zi.b ■r i■ th■ Mi..n.ui:ru=. D<at ■ction Lim.it. •
D. -llk)t ana.ly::z:ed.
1/ -Tentative identification.
3.1 -COMPoLJ.t-1D. ftE1.1Ae1.y oe,1:Cf'.F\'6L-E c~L'I 1N /-lIG-H coNCcNTRAT1ot,1:;,
✓-SAMPL!: l-116-HLY l)IL.u.TEo, ,'-\DL'o Do ~ APPL'/.
II DEIDiR 3068-0 (10/93)
9&/ 1.5+
CO•ILD
( 31
'ppb)ppm
I I
\/
PUllGCOM.OR•
• • · STATE LABOAATORY elf· PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILHINGTON, ST., RALEIGH, N.C. 27611
.. ORGANIC CHEMICAL ANALYSIS
JASE/NEUTRAL AND ACID LAB NO ti q1.~11,t:/.,\·1 "I'!." I I LI-'I' I Wt;,"o//Y.ft./J C/t,,-11 -=i I C/1,,//5 Ci' C/(p/ JC,.,
EXTRACT ABLES FIELD# .-:J r'o -:s-{'()-';,' Co-/ I ('O-/'I ('0-17
COMPOUND TYPE ( ,] ( ? ) ( 3) ( 31 (.:::) ( CS' l
UNITS . ..,,..u' un/kq nnt'1f uq/kq -' rrad ua/ka · u~ ua/ka -rrnH 11n/kq ..-,r ua/ka)
nitrosodirnethvlamine Ir,/ ,;''5() IA -I.A -A-IA-I I
s (2-ch loroethvl) ether
chlornnhenol
enol
3-dichlorobenzene
4-dichlorobenzene
2-dichlorobenzene
s(Z-chloroi l)ether
,xach l oroethane
-n i troso-cH -n--0roovlami ne
:trobenzene
;N'lhorone
-nitrr.nhenol
4-dirrethvlohenol
.
is(Z-chloroethoxvlrrethane
4-dichlo=henol / I / ,
2,4--trichlorobenzene
' ' I '
,nhtha 1 ene tJ{p I L/QO '5' :Zn v :::Z, ,,, I:'
exachlorobutadiene (.,t..-0--l,L;. J J.
-ct.·-.,a-ci-,n:.Creso l
ex.· ,._.;:•Orocvcl~ntadlene µ: 6:tri ch loroohenol / / /
-chloronaohthalene
~ " "'
cenaohthvlene :::?.G,, j ~~1 IC 'J ~ OIL
irrethvl Dhthalate I 1,(..... (,A_.· v-
6-dinitrotoluene " V--V--
LCen;inhthene Cf :3 C, J,-' ~7QY :i~nt:::
i,4-dinitrnnhenol S0///oS0 Ill---vL I.A--
4-dinitrotoluene /1'11330 I I ,
i-n i trooheno 1 so/. '-<::o \ ' ,Y
--iuorene /0/ '130 ~-OF-. ~-ni::: -s -,o k:'..
-ch l oroohenvl ohenvlether I"--(.,,L., I A -
liethvl ohthalate J,
1.6-di nitro-o-cresol )1',.t;/1 "'OI
iohenvlamine /0/330
JZobenzene
l-braroohenv l ohenvl ether
1exachlorobenzene "j I I ./ I
L>ntachlor~henol SO//t:,:fO ' ' ' I ' . )henanthrene //1 r:n" I, t.. (p'/ 5 ~ I -: '.2. ~ 'J 'JC
,nthracene I CJ ~.-, J:::. if 1, I '! "'" 7 :..; -:,1 le'
libutvl ohthalate I l./33 / v<-J., LD(p 7 0--
!luoranthene \ 1 1-oO / ,'i', «;?JV /A.non +.n~ ·,s
m"DL , , , '
} :stimated value. H,.o/.sot '-
" · ... Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
~
-Material was analyzed for but not detected, The nuroer
-Not analyzed.
-Tentative identification.
is the 11ini1TU11 Detection Limit. mT;L ----
fl -On NROC List of Priority Pollutants.
'
J
I
I
I
]
I
I
BASE/NEUTRAL ANO ACIO
EXTRACT ABLES
ro'IPOJND
ovrene
benzidlne
butvl benzvl ohlhalate
benz(a)anthracene
chrvsene
3.3--dlchlorobenzidlrre
bis (2---<ethvl hexvl \ nhtha 1 ate
di-n-octvl ohthalate
benzo(b) fluoranthene
benzo(k)fluoranthene
benzo(a)nvrene
indeno(l.2 3--<:d)nvrene
dibenzo(a h)anthracene
benzo(a h i1,.,,,rvlene
aniline
benzolC acid
,',enzvl alcohol
)''<=h 1 oroan i 1 i ne ·
. ·dibenzofuran
2-<rethvlnanhthalene
2-<rethvloheool
4-methylnheool
2-nitroani 1 ine
3-nitroaniline
4-<1 i troan i 1 i ne
2.4 5-trichlorooheool
I-I '-I' t)P oC. A-P ,0, Q/J <..
J -Estimated value.
• • STATE LAOORAlORY Of PUBLIC HEALlH
P.O. BOX 28047 -306 N. 141LM[NGTON, SJ., RALElGH. N.C. 27611
ORGANIC CHEMICAL ANALYSlS
LAB HO -1(,'/,;'C/ /_µ_ fj IQ/~//1./7 9u•I /LL 4 ct(,, I I"", I
FIELD# _:J (>,-,_' ('n-9 ,:-,-,-; I
TYPE ( '-5 ) (. ~) k:3) . t.3,
UNITS -~ .. a/kq ,~·11a/ko · · .,.11u/k11 b ~ ',/un/kn"""
/0/"''511 I -..,--0 :/ -'{ IA . 7 /. ~~ ",
"'" 111.,;o , IA vt-
10/:no S? 000 v'--
I , 1/L. .::i. &IA7
. , ;? ,I~·; ,£-1'.?~
'tt.. oO sol , 1,,L-'J l-' .
llo/ '130 .:;>o -;: 2 ., q ,av
110/.i.:?o 7,' R~: , i-<...-
sof,.,,a .J',~1.7 ·..,77:,_ 7.
'VI-
J
• ,L_
~ I '17) ">&:> 'JOO
t.'70O ..,;. :? :;13
/ , I,,<.-/ ,:.IL ,'.2 ~
,/ / <-11"3:i. ,1 '"' x'6O
/
,
I <o lu,,:-r, vC--(/L-, I . LIL.
, / .. , ' / ' I
/() /::...1'1 =?:=soi:::.. ~3,0k'
;:;: x'-1 -5 1.2.&,
'' ✓IA-
~/
S'o I, 1..,;-0
I / . ,
\J/ ' ,, ', ' I
----_,,..-..._
+I-(-J f + ) { -) ( +)
m1)1..
H-l-O/SotL
to be less than value given.
I'-/{,, I/. <;" ?
r' o-/(/
( -:.: ' . ___.,, . /ka
-5/ 2--~ ,',
130 l.1-7 ; ,
II. nnO
'vL-
17/l;;, ::;: 2 :i.,
I: --
/,,o, ooo
'I,,(....
l,..L, '•&7
191 1,& I ,, ' ;i 3 ~
/J . .! "1,/,1'"7
LA-
/
\ I
-5 ;i ;u"' ~-1/) K.
I
,
' ~
( J.., )
K -Actual value is known
L -Actual value is known
U -t\aterial was analyzed
NA -Not analyzed.
to be greater than value given.
for but not detected. The nuTber is the MinilTUll Detection Limit.
1/ -TenWtive identification.·
fl -on NROC List of Priority Pollutants.
t:/lnf/ ,<
l"0-/7
(0\
. "'"/ka '\
,-000
,, i ~
l .(_.
I" 1':,"c) ,.~ ,-z. ~ ,
L,(_.
JC/ ."'>5::Z
I,<-,o 2,--{~ ,
t./4-
i,). /J ~ =s
,.f 1.1., .
-.,, ,
~ /,200 ,
tA..-
,
' /
( _L)
.'-27
•
Memorandum
Date: December 12, 1996
To: File
From: Douglas Moore ~
Environmental Chemist
NC Superfund Section
Subj.: Fire Report
Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
•
On Monday, December 9, 1996, I received a voice mail from Joe Parker, waste
management specialist with the Hazardous Waste Section in Mooresville [phone].
In his message, he informed me that the main warehouse at the subject site was
essentially destroyed in a fire that occured the previous Sunday, Dec. 8. He was calling to
inquire about the status of site samples that we previously collected in our earlier
investigation of the site.
I called Mr. Parker back that afternoon and provided him with details on our previous soil
sampling results. I explained that our results detected residual soil contamination in
surface and subsurface soil samples at the site. At the time of our visit to the site (March
1996), there were no drums, tanks, or other containers of any hazardous materials left at
the site. I also stated that our soil sampling at the site was completed and that the results
indicated that no further remedial action was necesaary under the federal CERCLA
program at this time.
Mr. Parker indicated that he was writing a brief report on the fire investigation. I
requested that he send us a copy of his report for our site file.
·--' ,. • •
DEPARTMENT OF ENVIRONMENT, HEALTH and NATURAL RE~CES
DIVISION OF SOLID WASTE MANAGEMENT Ht:.CEIVED
HAZARDOUS WASTE SECTION
REPORT DEC 111996
SUPERFUND SECTION Subject: Cherokee Resources/Oil -Site Visit
NCO 980799019
Location: Mecklenburg Co. Date: 9 Dec 1996
Date closed: 9 Dec 1996
Address: 1201 Berryhill Rd. Time spent: 3
City: Charlotte, N.C. state: NC Zip:
By Whom: Josephs. Parker -Waste Management Specialist,
DEHNR
Persons contacted: Bart Massey -,Charlotte/Mecklenburg
Hazardous Materials Division
Paul Wilkinson -Charlotte/Mecklenburg Lead Fire
Investigator
Joe Boykin -Federal ATF
Jim Roberts -Federal ATF
Reason for visit: Site Visit
Copies to: Keith Masters
REPORT:
On the above day, Joseph Parker, Waste Management
Specialist for the State Hazardous Waste Section,
responded to a fire that had destroyed the Cherokee
Resources/Oil building located at 1201 Berryhill Road in
Charlotte, N.C. On that morning, I talked with Mr. Bart
Massey, of the Charlotte/Mecklenburg Fire Dept.,
concerning the situation. He told me that the fire had
started the day before, Sunday Dec. 8, 1996, around 1:30
pm. The cause· of the fire was still unclear, but
preliminary indications were that homeless people had
started the fire. Mr. Massey said that he could meet me
at the site that morning to clear up any questions our
Section would have concerning the property.
I met Mr. Massey at the site around 9:45 am. He
invited me to participate in a preliminary meeting with
himself, other fire investigators and the Federal ATF.
Individuals present at the meeting were as follows: (1)
Bart Masse¥ -Char./Meck. Hazardous Materials Program
(2) Paul Wilkinson -Char./Meck. Fire Dept. (Lead Fire
• •
Investigator)
(3) Joe Boykin -Federal ATF
(4) Jim Roberts -Federal ATF
(5) Joseph Parker -N.C. Hazardous Waste Section
The meeting was held to review safety issues and to
recap the site history of the site. Mr. Massey had
contacted USEPA Region IV in Atlanta, G.A. and spoke with
Mr. Steve Spurlin~ of the Remediation and Response Section
earlier that morning. Mr. Spurling was the On-Scene
Coordinator for the cleanup that had taken place in
1994-95. The cleanup had concluded around December of
1995. Mr. Spurling told Mr. Massey that all containers
and tanks containing hazardous and non-hazardous wastes
had been removed in the cleanup. They had left a tank
onsite, but it had been emptied before they were through.
As far as any onsite contamination, Mr. Doug Moore of the
N.C. Superfund in Raleigh was planning some soil sampling
for the site. Mr. Spurling was not sure if the sampling
was ever completed. He did say that ~uring the original
cleanup, they excavated alot of the soil in and around the
building located onsite and that the contamination level
of the soil would be minimal, ma~be 100 ppm. With this
information, Mr. Wilkinson explained that their
decontamination procedures would not be as extensive.
In reference to who has jurisdiction at the site, Mr.
Spurling said that the site had been referred back to the
property owner, Mr. Gabe Hartzell. To clarify, anything
that happens at the site is the property owners
responsibility. Mr. Wilkinson added to Mr. Massey's
information by telling us that Mr. Hartsell's
representative would not sign a waiver for the Char./Meck
Fire Dept. to be onsite to monitor the fire. Mr.
Wilkinson responded by telling him that he really didn't
need his permission if their was an imminent threat or
situation, such as a fire.
After concluding this meeting, all participants signed
the site log before entering the perimeter of the
building. The building itself was virtually destroyed,
with only the struts trying to hold up the roof. Mr.
Massey asked if I wanted to go inside the building itself
to investigate the scene. I respectively declined,
explaining that although I have extensive hazardous waste
training, it doesn't allow me to go into these types of
areas. I asked Mr. Massey to escort me around the
perimeter of the building so I can take a few photographs
for our records. These ~hotographs will be developed and
placed in the Cherokee File, located in the Mooresville
Regional Office.
I concluded my duties at the site at 10:45 am. During
a post-site visit conversation with Mr. Massey, I told him
• •
that I would contact Mr. Doug Moore of the Superfund
Section in Raleigh concerning the fire. I also asked him
to please contact me in the event of unknown containers or
items are discovered that might be related hazardous
waste. He then thanked me for coming out on such short
notice.
That afternoon, I left a message for Mr. Doug Moore
concerning the Cherokee Resources site. I also contacted
my immediate supervisor, Mr. Keith Masters. In my
conversation with Mr. Masters, It was determined that no
further action will be taken by the N.C. Hazardous Waste
Section.
This report will be faxed to the Hazardous Waste
Section's compliance Branch Head, Mr. Doug Holyfield.
From Mr. Holyfield's office it will be faxed to the
attorney's working on this case in the AG's office.
cc: Doug Holyfield -Compliance Branch Head
Keith Masters -Western Area Compliance Supervisor
Diane Long -Senior Field Officer
Joseph Parker -Waste Management Specialist
Attorney General's Office
Doug Moore -N.C. Superfund Section
Cherokee Resources/Oil File
Activity Type: Check Most Appropriate
1..
2.
3.
4.
5.
6.
Investigation
Compliance Assistance
Presentation
Training
Meeting
Other
X
....
\
• State of North Carolina
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
Mr. Tom Broom
Suburban Propane District Office
1333 Berryhill Road
Charlotte, N.C. 28208
July 31, 1996
Subject: Soil Sample Analytical Results
Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
Dear Mr. Broom:
• .WA
DEHNR
As you are aware, the NC Superfund Section collected two soil samples (labeled
CO-005-SL and CO-006-SL) from two drainage features located on the Suburban
Propane property, southwest of the main office building on March 6, 1996. The
approximate soil sample locations are represented in the attached figure. These samples
were collected to determine if releases from the subject site had impacted soils along the
overland runoff path from the site. As most soils have some measurable quantities of
metals, a background soil was collected from a grass-covered residential lot northwest of
the site (CO-001-SL), within the same soil type as the soils found at the site, to represent
the typical background soil conditions.
The soil samples were then submitted to the State Laboratory of Public Health for
volatile organics, semi-volatile organics, metals an'd PCB's/Pesticide analyses. The soil
sample results are summarized in the table attached to this letter. The analytical results of
the two samples collected on Suburban Propanes' property were then compared to the
background soil analytical results to determine if the contaminants concentrations exceed
three times the levels found in background. The contaminants found at elevated
concentrations are highlighted by shading in the table. These contaminant concentrations
were then compared to their respective EPA published human health-based soil exposure
screening benchmarks. Contaminants that exhibit concentrations above this standard are
noted by bold lettering in the table.
P.O. Box 27687. Raleigh. North Carolina 27611-7687 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ l 0% post-consumer paper
Letter to Mr. Broom
Analytical Results
Page 2
• •
The results found numerous polynuclear aromatic hydrocarbons compounds,
typically associated with oily wastes, at levels significantly elevated above background.
In addition, the soil samples contained elevated concentrations of bis(2-
ethylhexyl)phthalate, PCB-1254, lead and zinc.
Of the contaminants found at elevated concentrations in the two soil samples
taken from the Suburban Propane property, PCB-1254 and benzo(a)pyrene were
identified at concentrations that could pose a health risk to people who are routinely
exposed to the contaminated soil. However, the two samples were collected in relatively
inaccessible areas not normally used by workers, and not accessible to the public.
Therefore, the ct1rrent risk posed to workers and the public by contaminated soil at
Suburban Propane is considered minimal. Nonetheless, you should advise your workers
to avoid disturbing this area and regularly maintain the fence surrounding this area to
prevent incidental contact by trespassers. Also, removal of the contaminated soil may be
necessary, if changes in the future use of this area result in human contact.
Thank you for your help during our recent sampling trip. If I can be of further
assistance, please contact me at [phone], ext. 315.
cc: File
Pat DeRosa
Sincerely,
Douglas Moore
Environmental Chemist
NC Superfund Section
, ,· Figurr! 2 0 : . . -
n-S,te Samplin Cherokee Oil C g Locations
EPA ID· NCD ompany ,..:....r-., 98_0 7~9 019
M
~ Overland R ap Not to S 1 -unoff •. ca c -~ _.,
•
' ~ ,0
. '
' • • 1 '
\j
,.--,
\ I \'1
•
• .
-
' \
----------·' . ----------
• Contaminant Units
Acetone ua/ka
Methylene Chloride ua/ka
1, 1-Dichloroethane ua/ka
2-Butanone uo/ka
Cis-1,2-Dichloroethene uo/ko
Chloroform uo/ka
1. 1, 1-Trichloroethane uo/ko
Benzene ua/ka
1, 2-Dichloroethane ug/ka
Trichloroethene ug/kg
Bromodichloromethane ug/kg
Toluene ug/kg
1, 1,2-Trichloroethane ua/ko • 2-Hexanone uo/ko
Tetrachloroethene uo/ko
Chlorobenzene uo/ko
Ethyl Benzene ua/ko
Xylene(s) ua/ka
1,4-Dichlorobenzene ug/kg
1, 2-Dlchlorobenzene uo/kg
Methvl-tert-butvl ether ug/kg
Table l.
Cherokee Oil Company
Charlotte, Mecklenburg County, N.C.
US EPA ID: NCD 980 799 019
Analytical Data -March 1996 Source Samples
CO-001-SL 1"'CO-005-SL'' •"CO-006-SL
<20.0 BDL BDL
< 5.0 BDL 2J.C
< 5.0 BDL BDL
< 20.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 10.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
< 5.0 BDL BDL
Pagel.
EPA Soil Stds (ma/ka).
58,000 (RfD)
78 (CPF)
58,000 (RfD)
350,000 (RfD)
5,800 (RfD)
96 (CPF)
none issued
20 CCPF)
6.4 (CPF)
53 (CPF)
9.4 (CPF)
120,000 (RfD)
10 (CPF)
none issued
11 (CPF)
12,000 (RfD)
58,000 (RfDl
1,200,000 (RfD)
24 (CPF)
52,000 (CPF)
none issued
Contaminant Units
• Naohthalene ua/ka
Acenaphthylene ug/kg
Acenaphthene ug/kg
Fluorene ug/kg
Phenanthrene ug/kg
Anthracene ug/kg
Fluoranthene ug/kg
Pvrene ug/kg
Benz( a)anthracene ug/kg
Chrvsene ua/ka
Benzo(b)fluoranthene ua/ka
Benzo( a1nvrene ua/ka
lndeno( 1,2, 3-cd)ovrene ug/ka
Dibenzo( a, h)anthracene ug/ka
Benzo( a,h, i)oervlene ug/kg • Dibenzoluran ug/kg
2-methvlnaohthalene ug/kg
Dibutvlohthalate ua/ka
Butvl Benzvl Phthalate ua/ka
Bis(2-ethylhexvl)ohthalate ua/ka
Di-n-octyl phthalate ua/ka
PCB 1254 mg/kg
Table 1.
Cherokee Oil Company
Charlotte, Mecklenburg County, N.C.
US EPA ID: NCO 980 799 019
Analytical Data -March 1996 Source Samples
CO-001-SL ~CO-005-Sl', •CO-OJ6-SL'
< 330.0 330 K 330 K
< 330.0 330 K 330 K
< 330.0 BDL BDL
< 330.0 BDL BDL
< 330.0 330 K 330K
< 330.0 330 K 330 K
< 330.0
< 330.0
EPA Soil Stds (mg/ka).
none issued
none issued
35,000 (RID)
23,000 (RID)
none issued
170,000 (RID)
23,000 (RID)
17,000 (RID)
< 330.0 111-,00 BDL none issued
< 330.0 BDL none issued
< 1650.0 lal'lrnl,233Ril] Rillll!900IIIB none issued
< 1650.0 IIIBl2:033Rill !llllMl3i2f7ilBI 11, '_8~:'.l I : / ,,. 0.08 (CPF)
< 1650.0 111B1276'67liEI IIIB5l'.26711!111 none issued
< 1650.0 BDL BDL none issued
< 1650.0 BW2J~'.20(!)\BII !J!:IB!f2L433_. none issued
< 330.0 330 K BDL none issued
< 330.0 330K BDL none issued
< 330.0 BDL BDL 58,000 (RID)
< 330.0 BDL BDL 120,000 CRID)
< 330.0 -l,9/533IB:I 1'7IB5~l33'r1!1lll! 42 (CPF)
< 330.0 BDL BDL 12,000 (RID)
< 0.1 < 0.1 -llill!!lil■IB 0.076 mg/kg (CPF)
Page 2.
•
•
Contaminant Units
Arsenic mg/kg
TC LP-Arsenic mq/L
Barium mq/kq
TCLP-Barium mq/L
Cadmium mq/kq
TCLP-Cadmium mo/L
Chromium mq/kq
TCLP-Chromium mo/L
Cooner mo/ko
TCLP-Coooer mo/L
Lead mo/ko
TCLP-Lead mo/L
Mercurv mo/ko
TCLP-Mercury ma/L
Selenium mq/kq
TCLP-Selenium mq/L
Sliver mq/kq
TC LP-Silver mo/L
Zinc mo/ko
TCLP-Zinc ma/L
Table l.
Cherokee Oil Company
Charlotte, Mecklenburg County, N.C.
US EPA ID: NCO 980 799 019
Analytical Data -March 1996 Source Samples
CO-001-SL ,CO-005-SL' ,,co-006-SL
2.8 2.9 2.9
<0.01 < 0.01 <0.01
124 63 57
0.59 0.43 0.49
< 10.0 < 9.8 <9.8
<0.05 <0.05 <0.05
22 16 41
<0.05 <0.05 <0.05
34 55 37
<0.05 <0.05 <0.05
36 90 UW~I~lil~
<0.10 < 0.10 <0.10
< 0.1 < 0.1 < 0.1
<0.01 <0.01 <0.01
< 1.0 < 1.0 < 1.0
< 0.005 < 0.005 < 0.005
< 10.0 < 9.8 < 9.8
EPA Soil Stds.
0.33 mq/kq (CPF)
5.0 mq/L (TCLP Limit)
41,000 mo/kq (RfD)
l 00.0 mo/L CI CLP)
290.0 mo/kq (RfD)
1.0 mo/LC ICLP Limit)
2,900 mo/ko CRfD)
5.0 mo/L CI CLP Limit)
none issued
none issued
400.0 mo/ko (EPA)
5.0 mo/L CICLP Limit)
l 70.0 mo/ka (RfD)
0.2 mq/L (TCLP Limit)
2,900 mq/kq (RfD)
l .0 mq/L (TCLP)
2,900 mo/ko (RfD)
< 0.05 < 0.05 < 0.05 5.0 mo/L (ICLP) -290-170,000 ma/kg (RfD) 56
0.07 2liW-none issued
Shading indicates >I= 3 x background, or> background, if bkgd. = ND
Bold indicates a concentration in excess of applicable EPA soil exposure or TCLP regulatory standards.
CPF -refers to the EPA SCDM Cancer Risk Screening Concentration benchmark (Ref. l 0).
RfD -refers to the EPA SCDM Reference Dose Screening Concentration benchmark (Ref. l 0).
EPA -refers to the EPA soil lead guidance level (Ref. 11 ).
TCLP -refers to the Toxicity Characteristic Leaching Procedure as outlined in NCAC Title 15A Chapter 13A, Appendix IL Method 1311 .
TCLP Limit -refers to the TCLP regulatory standard (NCAC, Ttile 15A. Chapter 13A Subpart C, section 261.24, table I).
Page 3.
I
1-\.C r.:~fJ::nmcn! of En•,;ronmcnt,
' ; ic::lth, & ;,,_ialur;il Resources
.IPLE A:·,ALYSIS REQUEs;/ i:._: ( \, ' .. , . __ .. ''""' [.ab1•1-rn><y U[ p.,,1;, ifolth
!'.l.1. !:r:,x 2~i. 3(X, :--:. Wilmington Sircc1
) ::C ~: (\ X /99f H .. alcigh,· Nori~ Carolina· 2_7{.11
:;:;tid Wac<:tc Mana~cincnt Division
Sile Number
C0-001-SL 03/0b/9b 1501 GRAB
Cherokee Oil Company, HC DOUG MOORE
BACKGROUND SURFACE SOIL
Number ,, .. ,
Name of Site ESD LAB VOA Soil
1
1uJt uatc L.oucctcd Time
Collected By --------------------------
Agency: Hn;irdous Waste Solid Waste /superfuncl
------
Sample Type
Environmental Concentrate Comments
___ Groundwater (1) _ Solid (5)
Surface water (2) __ Liquid (6)
/ Soil (3) _ Sludge (7) ·-·---
_ Other (4) --0Lher (8)
Organic Chemistry Inorganic Chemistry
Pam meter Rcsults(mg/1) Prirametcr Results (mg/l)(mg/kg)
-~&T:GC/MS Arsenic --
--Acid B /N Ext. Barium --
"t'v!TBE Cadmium ----Chloride ----Chromium
--•----
--__ Copper
Fluoride ----
' Iron
·----Lead ·---
--__ Manganese
--__ Mercury
Nitrate ----Selenium --Silver --
Radiochemistry --Sulfates
.... ---Zinc --
l\1rametcr Results (PCi/1) _pH
___ Gross Alpha --Conduclivity
Gross Bela TDS
---··· --T0C -------
lvlicrobiology --
--
Parameter Results (Col/100ml) --
----
----
Date Received 3_ 'J--_(({,, 1M:J.1cporlef,,vJ , ~ ,-r.A.t ~
Dale Rc~cd ffjp// "I b Date Extr.:1<.:tcJ '~6l1:4fl\ ,, .. , ~ .\ ,, . ' l,,. ,,, ,1 Z-JJ _ q(p Wff' l .:1h Numhc.r ------
TCLP Compounds
Inorganl c Compounds
cn1c --
--
--
---
--
---
--
--
--
--
---
--
Ars
Bari urr,
Cad 1111 urn
Chr Otll\i.1/ll
Lea d
cury
Il\U!n
er
Mer
Sele
Silv
Or;anic Compounds
zcnc --
---
--
--
--
--
--
hen
ca,b
chlo
ch\o
chlo
on tetrachloride
rdane
robenz.cnc
reform
o-,:r csol
m·C re sol
__ p-cr csol
--
--
--
--
--
--
--
--
--
--
--
crcs o!
dichlorobcnzcne 1,4-
1,2-dichloroethane
1,1-dichloroethylcne
2 4-' dinitrotolucnc.
hcpt
hcxa
hcxa
hcxa
met
nitr
achlor
chlorobenzcne
c_hlorobu tadicnc
chlorocthane
hyl ethyl ketone
obc·nzcnc
achlorophenol __ pent
--pyn dine ·
tetra --trich --2,4,5-
chlorocthylene
loroethylcnc
trichlorophcnol --2,4,6-trichlorophenol
__ ,,nyl chloride
endr in
7 __ linda ne
1oxych !or
phcnc
met! -toxo --2,~-I )
Rcsults(mg/1)
Results(mg/li
-------
-------
-------
-------
-------
245
716/1 --------
-TP (Sil·:ex)
-~-q, ~ ...il0_L-
.•
.. ·~p.:atmcnl o( Environment,
fk;:,lth, &. NaturJI Resources
Solid Waslc Man::igc1~cnt Division
&1PLE ANALYSIS REQUEST • St.ilc i.,nbor,1101y of Public ! lc:!lth
P.O. \10x J.S0-17, 306 N. Wilmington .Strc.::t
Ralci~h, N0tlh Carolina 27611
Site Number CO·OOl·SL 03/06/96 1501 GRAB
Cherokee Oil Company, NC
Name of Site BACKGROUND SURFACE SOIL
-ESD LAB EXT /PEST Soil
DOUG HOORE Number --------------
Collected By
2 --,.., ......,v., ........ ,ed 'fi.mc --------------------------
Agency: Hazardous Waste Solid Waste Lsuperfund
Sample Type
Environmental Concentrate Comments
__ Ground water (1) _Solid (5)
Surface water (2) --.
Liquid (6)
/soil (3) _ Sludge (7)
__ Other (4) _ Other (8)
Organic Chemistry
Results(mg/1)
Rad iochcmistry
····----------------<
Parameter
__ Gross Alpha
Gross Beta
Rcsull.s (PCi/1)
Inorganic Chemistry
Parameter Resulls(mg/I)(mg/kg)
Arsenic
Barium --Cadmium --Chloride
__ Chromium
__ Copper
Fluoride
Iron --Lead
Manganese
__ Mercury
Nitrate
Selenium --
Silver --
Sulfates --Zinc --_pH
__ Conductivity _______ _
TDS --TOC --1--------------l
Microbiology
P<1ramc{cr Results (Col/lOOml)
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium --Chromium --Lead --Mercury --Se!e.nium --Silver --
--
--
--
--
Organic Compounds
benzene
-
carbon tetrachloride
Rcsults(mgil)
Results(m'g/1)
----------
--
--
chlordane
chlorobcnzcne
chloroform
o-cresol
m-crcsol
--p-cresol
crcsol ----. 1,4-dichlorobenzenc ______ _
__ 1,2-dichloroethanc
__ 1,1-dichloroethylcnc ______ _
__ 2,4-dinitroioluenc.
__ heptachlor
hexachlorobenzene
hexach I orobu I ad icnc ----------
hcxaehloroet hanc ----methyl ethyl ketone
nitrobcnzenc ----pentachlorophenol
__ pyridine ·-
--tetrachloroethylene
trichloroethylenc
--2,4,5-tric h lorop heno 1
--2,4,6-trichlorophenol -------= vinyl chloride
endrin --lindane ----methoxychlor
__ toxaphcnc
__ 2,4-D
__ 2,4,5-TP (Sil·:cx)
I
_,.--· ... ,...,-""'.P?'·:-:·,cnt oc J.:.n~1ronr:1cnt,
: ic:-lth," &. l','3turJI Resources
Sc-lid W:tstc M<rn;!gcincnl Oi,,isi•);i
w!PLE ANALYSIS RE(_jEST • S1:itc L,1b0:-a1nr1 u: !'ubli~ Hc::ilth
r.U. Go.1 2&0--l7, 306 N. Wilmint::ton .Street
Rak.ibh, North Carolina 2i61 l
Site Number co-001-SL 03/06/96 1501 GRAB
Cherokee Oil Company, NC
BACKGROUNO SURFACE SOIL
DOUG MOORE
Number _________________ _
Name of Site ESD LAB METALS Soil
Collected By_
3 ...., ............ u,1~ued Ti.me -----------------------
Agency: Hazardous Waste Solid Waste V Superfund TCLP Compounds
------
Sample Type Inorganic Compounds Results(mg/1)
Environmental Concen trJ te Comments v Arsenic -<c_ 91
✓Barium u.59 --
__ Ground ,vater (1) Solid (5) ✓Cadmium .L'.o ,a5 --✓Chromium .c:_g_o5
--Surface water (2) _ Liquid (6) vLead ~~., .. ·\a
v-iv(ercury -<c, c]
v'soil (3) Sludge (7) V Selenium .,,L._t}sc'?C5 --v"Silvcr .z.o. oS
_ Other (4) --Other (8) ~ Cczf'Cb< .L.....o .. c~·
7-J',i V Q-07 --
--
Organic Chemistry Inorgariic Chemistry --
Parameter Results(mg/1) Parameter Results..,.)(mg/kg) Organic Compounds Results(rng/1)
__ P&T:GC/MS V Arsenic J.8 benzene
VBarium
--
--Acid:B/N Ext. ) di'i carbon lt{rnch!oride ----
MTJ3E v Cadmium .( ' C! chlordane ------Chloride chlcrobenzenc ------
--V---Chromium ;J.:l, chloroform --
--V--Copper .31:\ o-cresol --
Fluoride m-crcsol ------Iron __ p-cresol
-,------
--V-Lcad -:s Co cr~sol ----
--__ Manganese --1, 4-dich lorobcnzene
.....--Mercury < ()_, l --1,2-dich loroethane --Nitrate 1, 1-dichloroethylcne ------✓Selenium .. q 2, 4-di n i lroto 1 u enc --✓Silver .£. i c:, __ hcptachlor --
Radiochemistry Sulfates -hcxachlorobenzcne ----
✓Zinc 5G. hexachlorobut adicne --
Panu1H.:tt.:r l<csults {l'Ci/1) _pH hexachloroelhane --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta TDS nitrobcnzcnc ------TOC __ penlachlorophenol : ;
--__ pyridine --l'v!icrohio logy tctrachloroelh ylene ----trichloroelhylenc --Parameter Results (Col/1001111) __ 2,4,5-trichlorophcnol --2, 4,6-trichloro phenol ----= vinyl chloride ----endrin --
lindanc
Dale Received
---mc.thoxy(h!or Reported by --toxarhcnc
Date Ex~r:iclcd Dale l<cp,1rtcci_J_J_~
--
--2,n-D
00]4-44 1!,!, ' } 2 '-5-TP (S:1., ... ) --,,, .,,,(.,;,\
Dale ,~.n:d:-,1.cd .,.,. -· -----L;1h Number -----. --···-__ .. -. --·--··--··-·---···--------·-·--------------·------". ".
I
l I ' I
I
I
I
I
I
!
I
..
.!PLE ANA::...,Ysrs REQUEST • Seate l...rtbor.uo1y o( Public Hcl!th
P.O. nox 280-..7, 30:'.i N. Wilmingmn _Str:ct
R.alcibh, North Carolina _27611
Site Number_
Name of Site
C0-005-SL 03/06/96 1430 GRAB
Cherokee Oil Company, NC
SURFACE SOIL IN DRAINAGE O!TCH
ESD LAB VOA Soil
Number
OOUG HOORE ------------------
Collected By co-16 ad Ttme ------------------------------
Agency: --Hazardous Waste ---Solid Waste ✓ Superfund TCLP Compounds
Sample Type Inorganic Compounds Rcsults(mg/ij
Environmental Concentrate Comments Arsenic --Barium --__ Groundwater (l) _ Solid (5) Cadmium . --Chromium --__ Surface water (2) _ Liquid (6) Lead --
VSoil (3) --Mercury
_ Sludge (7) Selenium ---Silver --_ Other (4) _ Other (8) --
--
--Oroanic " Chemistry Inorganic Chemistry --
Parnmet1.:r Rcsults(mg/1) Parameter Results (mg/l)(mg/kg) Organic Compounds Results(mg/1)
v""P&T:GC/MS Arsenic benzene
Acid:B/N Ext. ----carbon tetrachloride --, Barium
MTBE ----
--Cadmium chlordane ----
--Chloride chlorobenzene ------Chromium chloroform ------Copper o-cresol ------Fluoride m-crcsol ----_,_ Iron p-cresol ------Lead crcsol --------Manganese --1,4-dichlorobenzcnc
----Mercury --l,2-dichlorocthane
--Nitrate !, 1-dichloroeth ylene ----Selenium 2,4-dinitrotoluene. ----Silver heptachlor ----Radiochemistry Sulfates hcxachlorobenzene ----
Zinc hexach I orob u tad iene
Parameter Results (PCi/1) ----pH hcx.:ichloroethane ----__ Gross Alpha Conductivity --methyl ethyl ketone
Gross Beta --
--TDS nitrobcnzenc ----T0C pcntachlorophenol .. . ,
----
--pyridine
Microbiology --tctrachloroethylene ----trichloroethylcne
Parameter Results (Col/lOOinl) ----2,4;5-trichlo"rophenol_ ----2, 4,6-t richforophenol --,inyl chloride ------cndrin --
J-?-'/k, ~Reported by
lindane
Date Received --mcihoxychlor --
--toxaphcnc
o·alc Extr:iclcc.l Dale Reported 2,/4-D --
Date .'\n:ilv.'cC 3-18~9&, 77/JJ G°i'''.k"· --2,4,5-TP (Sil·.,cx)
l, '.oh N,,,,.,h,,.-~.
.!PLE ANALYSIS REQUEST • 51.;tc l_. .. abor.itory of l'ub!i,: Hcl\lh
P.O. Do.'( 2~7. 306 N. Wilmi!'.gton .Strcc\
Raleigh, North Carolina 2_761J
C0-005-SL 03/06/96 1430 GRAB
Si le Number_ Cherokee Oil Company, NC OOUG HOO RE
SURFACE SOIL IN DRAINAGE DITCH
Number -----------------
Name of Site ESD LAB EXT/PEST Soil
co-17
Collected By -------~---J.VTI" --•-------
Agency: Hazardous Waste Solid Waste ~Superfund TCLP Compounds
----
Sample Type Inorganic Comp011nds Results(mg/1)
Environmental Concentrate Comments Arsenic --Barium --
__ .Groundwater (1) _ Solid (5) Cadmium --Chromium --
. __ Surface water (2) _ Liquid (6) Lead --
--Mercury
V Soil (3) _ Sludge (7) Selenium --Silver --
_ Olher (4) _ Other (8) ----
--
Organic Chemistry Inorganic ·Chemistry --
Parameter Results(mg/1) Parameter Results(mg/1) (mg/kg) Organic Compounds Results(mg/1)
P&T:GC/MS Arsenic benzene
v Acid:B/N Ext. ----
Barium carbon tetrachloride
----
l\!TBE Cadmium chlordane
7 Mr,/Pe<nc/Des
----
Chloride chlorobenzcne ------
----Pc:B.i-<,:,. lo~~~ Chromium chloroform
EAldt;_/;,J <o./o,I.!,~'
--
Copper o-creso! = L,',.,!d,1N'E < o. ~tf!n~~· ----
Fluoride m-cresol ----
~<U•')"Mr-<:~ Iron __ p-cresol --
_?Yx-1vw6¥'e ~ () Lead crcsol ----
~lodM!E£ < o, · . __ Manganese --1, 4-dichlorobenzene
J rt9.dlr /<_ -< o, · --Mercury --1,2-dich loroethane
~., , I.A Nitrate 1, 1-dichloroethylene
/ I ----,, Selenium 2,4-dinitrotoluene.
----
Silver heptachlor ----
Radiochemistry Sulfates hexachlorobenzcne
----. Zinc hexach lorobut ad iene ----
Parameter Results (PCi/1) _pH hcxachloroethane --
__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nilrobcnzenc
----TOC __ pentachlorophenol ..
----__ pyridine
Microbiology ----tetrachloroethylene
trichlorocthylene
--
Parameter Results (Col/lOOml) --__ 2,4,5-trichlorophenol
----__ 2,4,6-tricWorophcnol
------vinyl chloride
endrin --
Date Received 3-7-fl,, ~ Reported by
lindanc --mcthoxychlor --
, f~B/f.w:. 3·ts-% id! __ toxapbenc
Date Extracted 3-11-91, 5/\,M_ Date Reported 2,1-0
6VI/ iPU!J 5¥,C,ss-r ; ··--•-s,·: . · · 2,4,5-TP (Sil·.•ex)
~ '96'1155
D;itc s\n:i!v1c -)l-1_//.. 3-.:l/-fi€rt'Lab Number · ---··
·: ,.-,C:0.;ir1mcn> of Environmcn!, ·
,dC;!th; & ;"\"aturJI Resources
/5oliU Waste Managcrrycn! Di~ision
.ANIPLE ANALYSIS REQl;:~s• Siatc L1horato1y of Pl!li!i.: He::
l'.0 Gox 2~7, J06 N. w;1n1ingto:1 _S1:i:
Raleigh, North Carolin11 27(
Site Number C0-005-SL 03/06/96 1430 GRAB
Cherokee Oil Company, NC
SURFACE SOIL IN DRAINAGE DITCH
DOUG MOORE Number ----------------
Name of Site_ ESO LAB HETALS Soil
co-18 Collected By _________ _ .vau.., '-'VII\..Lled Ti.me ----------------------
Agency: Hazardous Waste Solid Waste V Superfund TCLP Compounds ----
Sample Type Inorganic Compounds Results(mg/ Environmental Concentrate Comments V Arsenic -<.o.c I --v Barium 0, l/ s ----Ground water (1) Solid (5) ~ Cadmium < Q, Q ,)-
vChromium <:o,os-__ Surface water (2) _ Liquid (6) ✓Lead <o, to --
VSoil (3)
·✓Mercury 4t::>-O\ _ Sludge (7) LSelenium -<= .cc 5. v Silver < o. o,C _ Other (4) Other (8) ✓~,-to, ~1 ✓ µnc-,7 .
--Organic Chemistry Inorganic Chemistry --
Purnmeter Results(mg/1) Parameter Resul~(mg/kg) Organic Com pounds Results(mg/1 P&T:GC/MS ✓ Arsenic :2. benzene ----_ Acid:B/N Ext. ...---Barium G,_ '.J carbon tetrachloride --MTBE ✓Cadmium ""-9 .s chlordane ------Chloride ch!orobenzcnc --------✓Chromium 11..;, chloroform ----✓Copper 55 o-cresol --Fluoride rn-crcsol ------, __ Iron p-cresol 1a ·----....-Lead crcsol --------Manganese .. --1, 4-dich lorobcnzenc
--v Mercury <o, / --1,2-dichlo roet hanc
--Nitrate 1, 1-dich loroeth ylcnc --vSelenium ..-<.' 2)4-dinitroto!ucnc. --•••••✓-Silver --<'-9.8 __ heptachlor ---Radiochemistry Sulfates -hexachlorobenzcne ----.,..-,Zinc (,: 3<."' hexach lorobut adienc --Parameter Results (PCi/1) --pH --hexachloroethane __ Gross Alpha --Conductivity me:hyl ethyl ketone --Gross Beta TDS nitrobcnzene ------TOC pentachlorophenol . , ----
----pyridine
!v!icrobiology ----tetrachloroeth ylene
trichloroethylcnc --Pi.Ira meter Results (Col/lOOml) --2,4,5-trichlorophcnol ------2, 4 ,6-trichlorophenol ----,1nyl chloride ------cndrin --lindanc --Dale Rccci'-d methoxych!or Reported by --
--lox:1phcnc Date ExtrJct..:d Dale ~n)ried Yfi I fJ 2,,[.l) u ]4,~) !.11.1 8 9b --2,t.,5-TJ' (Si! ,•ex) Dill . Iv,,,,! I .,I. Ni!mh ,. ,
LrLE ANALYSIS REQUEST • Stale f..abonltory of Public Hc2!1h
P.O. Oox 28047, J.C(j N. Wilmington _Slrcct
!ulcibh, North Carolin/\ 27611
C0-006-SL 03/06/96 1415 GRAB
Site Number_ Cherokee Oil Company, NC DOUG MOORE
SURFACE SOIL NEAR NW CORNER OF SUB. PROP
Narne or Site ESO LAB VOA Soil
co-19
Collected By ---------,----_____ -·-_______ d ___________ Ti.me ______ _
Agency: Hazardous Waste Solid Waste ,_,/ Superfund TCLP Compounds
------
Sample Type Inorganic Compounds Rcsulls(mg/1)
Envircinmcntal Concentrate Comments Arsenic --Barium --
__ Groundwater (1) _ Solid (5) Cadinium --Chromium --
__ Surface waler (2) _ Liquid (6) Lead --
v"soil (3)
Mercury
Sludge (7) --Selenium
----Silver --
·_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry. --
Parnmell:r Resu Its (mg/I) Parameter Results(mg/1) (mg/~) Organic Compounds Rcsults(mg/1)
v".°P&T GC/MS Arsenic benzene ----
Acid: B /N Ext. Barium carbon tetrachloride
------
MTBE Cadmium chlordane
------
Chloride cblorobenzcnc
------
Chromium chloroform
------
--Copper o-cresol ----
Fluoride rn-crcsol ----
' Iron __ p-crcsol
----Lead crcsol ------
----Manganese 1, 4-dichlorobcnzene --
----Mercury 1,2-d ichloroct hane --
--Nitrate 1, 1-dichloroel h ylcne ----
Selenium 2,4-dinilrotolucne. ----
--Silv.er __ heptachlor
Radiochemistry Sulfates hcxachlorobcnzcne ----
Zinc hexach lorobu l adicne ----hcxachloroclhane P.irnmetcr Results (PCi/1) _pH --
__ Gross Alpha __ Conductivity methyl ethyl ketone --
Gross Beta TDS nitrobcnzene
----= penlachlorophenol TOC ' --
--__ pyridine
Microbiology ----tetrachloroelhylene
lrichl oroetbylcne --
Parameter Results (Col/lOOml) --2,4,5-tricblorophcnol ----2, 4 ,6-trichlorophenol
------
------vinyl chloride
endrin --
3-]-yb~eported by
lindanc
Date Received
--mcthoxych!or --l toxaphenc --
Dale Extracted Dale Reported 2,,l-0
~-/9, _qfll -ru,n ,h N,,mh,•c '!9_6·11:56·;: '
= 2,4,5-TF (Si!·1cx)
I"'\ .. ,~ ·\~-,1,r,,.,!
I I
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I
! :
' ' I
i
!
.!!'LE ANALYSIS REQUEST • $(:ilc 1_..,boratory o( Public Health
P.O. Om W).47, 306 N. Wilmington _Street
Raleigh, North Carolina 27lll
Site Number_
C0-006-SL 03/06/96 1415 GRAB
Cherokee Oil Company, NC DOUG MOORE
SURFACE SOIL NEAR NW CORNER OF SUB. PROP
.'lumber -----------------
Name of Sile ESD LAB EXT/PEST Soil
co-20
Collected By -----------
Agency: Hazardous Waste Solid Waste ✓ S uperfu nd TCLP Compounds
----
Sample Type Inorganic Compounds Rcsults(mg/1)
Environmental Concentrate Comments Arsenic --Barium --
Ground water (1) Solid (5) Cadmium
----Chromium --
__ Surface water (2) _ Liquid (6) Lead --
✓Soil (3)
--Mercury
Sludge (7) Selenium ----Silver --
_ Other (4) _ Other (8) --
--
--
Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Rcsults(mg/1) (mg/kg) Organic Compounds Rcsults(mg/1)
_ P&T:GC/\1S Arsenic benzene
· 7Acid:B/N Ext. ----
Barium carbon tetrachloride ----
MTBE Cadmium chlordane
✓ ~r.-/PES11ca,e. · ----
Chloride chlorobenzene ----
-<'.BS-fl-?-o/)_ /, 1/#M Chromium chloroform ----
--61d~,'t./ -<:O,IP 'cpm __ Copper o-cresol --
_ L,Nd.-1.VE <O,.:IO~ Fluoride rn-crcsol
----
'_)¼c/4•'9""!,-: ab~ Iron __ p-cresol --
_llXA/?l{GVE ' . Lead crcsol ------
.22~~~ ~.;,;.~
__ Manganese --1,4-dichlorobenzene
__ Mercury --1,2-d ich loroethane
7ltjol,1('4/d.i!fw,x,-✓/.,:<,:,,/o~ --Nitrate --1,1-dichloroethylene
,. Selenium 2, 4-dinitrotoluene. ----
Silver __ heptachlor --
Radiochemistry Sulfates hexachlorobcn?.ene ----
Zinc hexachlorobu t adiene ----
Parumeter Results (PCi/1) __ pH hexachloroethanc --
__ Gross Alpha __ Conductivity __ methyl ethyl ketone
Gross Beta --TDS nitrobenzcnc --TOC __ pentachlorophenol ' --
----pyridine
Microbiology ----t etr achloroethylcne
--__ trichloroethylene
Parameter Results (Col/100111!) --__ 2,4,5-trichlorophcnol
. 2, 4,6-trichlorophcnol
------
--vinyl chloride ----endrin --
Date Received 3-7-C/b l/4:/1/zeportc<l by
lindane --methoxych!or --
P~e/M 3-t<c-9e, ,J-G . --toxaphenc
Date Extractcc_j-1,9.q 1, S/l. Date Reported 2,4-D
n:1lr. An•,lvlf•rllitc;/,, 171!1:lh-,t;cr 96·11·5,7 __ 2,4,5-TP (Si!·.•cx)
=l-:!Y?-~ ~ ~ L:1h Numhcr ---
I I
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'
.!PLE ANALYSIS REQUEST • Stale [,;ibor.11ory o( Public 1-!c:!lth
r.C. Oox :2$0-:7, JC6 N. Wilmington _Street
R.a!cigh, North Carolinll 27611
Site Number
Name of Site
C0-006-SL 03/06/96 1415 GRAB
Cherokee Oil Company, NC DOUG MOORE
SURFACE SOIL NEAR NU CORNER OF SUB. PROP
ESD LAB METALS Soil
Number -----------------
Collecied By co-21 cd Time ----------------------------
Agency: Hawrdous Waste Solid Waste ✓ Superfund TCLP Compounds ----
Sample Type Inorganic Compounds Resulls(mg/1)
Environmental Concentr;.ite Comments VArscnic -<!.c.ol --✓Barium ()_, y_q
__ Ground waler (1) _ Solid (5) . v Cadmium < c, c/c::-
.,.,-·chromium <o,6~
__ Surface water (2) Liquid (6) ✓Lead < (), i I~ --
/Soil (3)
✓Mercury L... C .c, 1
_ Sludge (7) v/Selenium .-4. c .. cc..!.5 --<( Q, (! ----v SilYcr \
Other (4) Other (8) ,/'6w--,r < 0, Q <;"'" ~ ~',,,c-'-;;J ,7 8.
--
Organic Chemistry Inorganic Chemistry --
Pam meter Results(mg/1) Parameter Resui's, g~( .. 1g/kg) Organic Compounds Rcsulls(mg/l)
P&T:GC/MS ✓ Arsenic ;J,,9 bc;izcnc ----
vBarium Acid:B/N Ext. 57 ca,bon tetrachloride ----MTBE v"'Cadmium L. 9.8 chlordane ----Chloride chlorobcnzene ------✓ Chromium '--'t 1 chloroform ----✓Copper --37 o-cresol --Fluoride m-crcsol ------
--Iron p-cresol --I 6 --
--vLead (I crcsol ----
--Manganese 1, 4-dich lorobcnzene --< o, L --
--,.,......-1vf er cu ry 1,2-dichloroethane
I --Nitrate 1, 1-dich loroet hylene ------✓Selenium ..(' 2,4-dinitrotoluene. --V"'Silver -<:.9.8 heptachlor ----Radiochemistry Sulfates -hexachlorobcnzcne --✓Zinc ···-· ;i-=io hexachl orob ut ad ienc ----Parameler Results (PCi/1) pH hcx.1chloroc I h ane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobcnzenc ----
TOC __ pentachlorophenol . , --
----pyridine
rvl icro biology ----tetra ch lorocth ylene
--__ trichloroethylcne
Par..1mctcr Results (Col/1001111) __ 2,4,5-trichlorophenol --
----__ 2,4,6-trichloro phenol
--,onyl chloride ----endrin --lind,1nc --Date Received r.1cthoxyCh!or Reported by --
--11;:.(:iph..;nc
!);Jlc Extr:.ictcd Date Reported 2,-:.1)
O (Jl 45Q~tl11 R 8 96 --2,>,5-TP (St!· c:~,1 --D;dr A n-,lv,,·ri 1 ..,1, 1'i .... ,\, .• ,..
:-._' "_<-:.·-~:·1,:-·-·.•.;•;:~.-=:_.;·. '; :;fr~---· -
;:·-..• ,.. -
,, • STATE LABORATORY OF POBLIC HEAL,
PO BOX 28047 -306 N. WILMINGTON ST •• RALEIGJI. NC 27611
PCIRG.EA.BLE COMPOUNDS
COMPOUND
VUfTl: CHLO RID .C
BRO !d OHETHA. 'a:
cm.oROrI"RA!Oe
TRICHLOROTUl"ORO~
ACrl'O !OI:
1. l•D1CHLOROETH?;m:
10 00 J,,Q;1""lIA. >a:
i,anrytz:a; CHLORID.C
C.-\Jt.BOl'f DI.Sut.n:D~
TRArrS--1.2· D !Cfil.O RO ETI:[L'f!:
AC!m.Ol\7l'RIIZ
1, l • mcm,o RO JtTH/iJ'fl:
:J..BCT.Al'IO?f?;
CIS--l~DICHLORO~ ,
cm..oROFORW
1.1.1-TIUCRLORO~
CARBOl"l n:TR.Aem.orunr:;
1.:1-DlCBI..OROrI'HAlfE
I.ABNO
FIELD NO
TYPE
J.O
10
J.0
10
10
;}_Q
5
,/
5
;)..D
5
ORGANIC CHEMICAL ANALYSIS
9wl!L/-6 Cf{.pl/80
1 co-+ co-7 C0-/0
(3) (.3) ( 3 ) l 3 l ( 3)
Vpi,b)ppm
lL-I I, /j /J
.... I \ I
.t3J",l.. Io lo :r
I J I J / A
.J/
7J,C...
1
\ I
(p q
f.L..
9
LL-I 1 LL
UJ
frnrP LL
TRicm.oRO~ 31 /J +r-Cl.(.P
l~-DICHLOROPROP.An'E LL
BROU:0D ICHLOROu:::r:rHA.!a , I \ I
C -,po~, e~ '-"6 <0o>fi"l'l~1tlf\T\OIV OR BAC:J:.G-£cuN D,
J -E•timated va.l.u•
X. -Actu&.l va.l.u■ i• 1t:nown to b■ l••• than va.lu• g-iTen.
L -Actual va.l.ue i• l:nc,-wn to be; gr■a.t■r than T&lu■ g-iyen.
tJ" -Kat•ria.1 waa ana.ly:r:ed t.or but not detactad~ The numb■r i• th■ M:i.rwmtm Detacticn Limit.
J5lA -5ot analy:r;

■
d.
1/ -T■ntativ■ identit.ication.
3/ -C<li".1'0~1'llO .Rf.LI l'\ElL'(-06l"ECi'l'l61.£ oJJL'/ IN H 1(,-,l C:O/•CC NTRR11c~.
✓-SA>IPLio Hl&HL¥ Q1L1<TSO. >-1oc•~ Do NOT p,Pf'L'{.
DEHNR 3065-0 (10/93)
LL.
(_;.__
PURGCOM.ORG
I
!
I
• • STATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
.
PURGEABLE COMPOCJNDS LAB NO <;f'{jf[f(filj 91c114w qc.o1 I 'f0 q(D/ 150 (J(.o I 16;)
FIELD NO I co-+ CD-7 c.0-1 D Co-1.3
COMPOUND TYPE ( 3 ) ( 3) ( ) (3 ) (3 )
fr~ft /ocb)ppm ppb \,pn, ppb;pprt1 ~pb pprn ffpb)ppm
DIBROMOMrrHAl'll: 5 LL-lL. I 1 . I I '
4-ldETHTL-Z..n~ANOrrt: ,o .
CIS-1.~-DtCHLOROPROn;oa; 5 . I •'/ ,,/
TOUJL"f?: 3oc1 ;).7 //70
TRAlfS-1..3-DtCHLOROPROn!'!'?; I ' u_ I '
1.1.2.l-TI:!"R.ACHI.ORO~ J,,
1.1.!l-TRICHLOROETHA.."f?; ' / +rare.., ' I/
:i-HEL\lt'ON"?; JO I I I J.f :r !/
~Ror:nn;ra 5 30(.p f rcue..., 7
DtBROMOCHLOROlil'THA."1'1: I ' I 1 u_
ETlITLr.f?; DrnROlo£ID!: ~ /
CHI.ORO~ II fra.Le_.
l,l.1.;z...n;nv.,cm..oR.Or.RNf"l: l-L.. L,._ ' /
rnrrL BmZ!:.n-?: ;}3if -1-rnce... ;).,
:rru::r,;s IJ/{_p q:r I ;).5
= ' I /1 (,,<._ 1
BROKOJ"OR:M /0
TRA?m-1.-1--DICHI.ORO-l-DUT?:~ io
1.2,3--TlUCHLOROPROP .Am: ..5 ' /
1 • .C-DICBLOROB!:l'rZX?B I ,}.O ' 'I 'I/
1,:'l-DtCHLOROB!:11Z!:l'fE 'V 51 +rcu.e.... +race..-
1,Z•DrBROM:0-3--CHLOROPROP.Ala ;it> lL U-LL
VINYL AC!;TATI; ;00 , I/ -,, /
r./ ~+h u 1-+-b, .4.., I -:-: 5 :, I/ ,/ \ I/ ~ s frru.P. ..
Jl .. -1-oc,-.~l.o~, :, (!)Jr.;) H {+ 8 (+) (+
5ub:,t-,'fufed brnvn-e:
C -p~"'10LE Lf\6 CcNl"RMllo.\ATlO!s) OR BA~l::(rl<Oll'-1!).
J -Zatim.at•d valu• .
X. -J.ctual 'Value i• known tc b• l••• than 'VlLlue given.
L -J..ctual Talue i• Jcn.owu to be g-r•at ■r than <nLlu• giv.n.
U -Katerial wa• &na.lp■d tor but not detected. The number i• ~•-M~ D,et ■aion Lim.it. •
lD,. -Rot ana.ly::z:■d.
l,I -Tentative identification. .
~1 -c::oMPollt-lD-RE1..1i;a1..y oeT'i:CT'.f\BLE c1'lLY 1N t-11&-H col'lC£NTRAT1otJ.:;,
.,/-SAMPLE Hl6-HLY 1)11..uTED. f,,IDL'o Do >.:a, APPL'/.
DEIDiR 3068-0 (10/93)
~r-75l/-JpJ/ ...
COr/UJ
( 31
~pbJppm
I '
\ /
PURGCOM.ORG
' i
I i ' I
i
• • { STATE UBORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611
ORGANIC CBEMICALANALYSIS
PURGEABU: COMPOUJ\'DS LAB NO df[fi':ftr{ff'! 9C..O 116B q&11~D Clloilw;;l. CJ (Li I I I.P'-t CJ~IICD(o
FIELD NO CO-JC/ Co-Jd co-,;>. 5 co-,;29 co-31 Ca-3f
COMPOUND TYPE ( 3 ) ( 'I ) ( .;l_) ( + ) I ( .;t. ) I ( if ) I
M~S)s (l>Pb 'ppb pprn ~b.pprr: .lppb)pprn /ppbpprr: 1-'ppb)ppm j(ppb (Pi11
CHLORO!ll:TH.Ara JO I I I
VINYL CHLORIDE: 10
BRO MOMETRAI'a: ;;;_O
cm..oRO?:l"HA.Nl: JO
TRICRLOROTLUORO~ JO
AC'CTO!flO ;;J.0
1.1-DICBI.ORO~:O: 5
I r
1000 liOITHAl'f?: ' \
J.a:r'HTU:!'f?; cru...oRID& ~ J,C.. 3:Y,L
CARBOl'l' DI.SULl"ID& I , I 1
'TRMS-1.l·DICBLOROt:na."fl: '/
ACim.oNYTRJU ;;lD ,v
1,1-Dlcm...oRO~ 5 +race....
~ BUTAl'f O 1B .;20 I ,
CS--1.Z.DICELORO~ 5
CRLOROFOR.ll
1.1, l •TIUcm.o RO~
CAJlBOl'I Trl'ltACHI.ORIDZ:
"-"=""
l,:l-DICHLOROnBAn ' I
TRlcm..oRO~ +rnrP
1.!l-Dicm..oRO PROP Am: I ,
BROMOOICHLORO~ ' I \ / J;
c-.Po:»,ec,; I.AB <ec><Tf\1<11!'1PIT1oi'J oR BRC.J:.6-Rcu"1D,
J -X ■tila.a.tad va1ue
~ -Actu&l. value i• lcc.awn to b ■ le•• than valu■ given.
L -Actual value i■ kno,,ro to be gx-■atar than value given.
I ' LL
'\ I
4 'J,C.. \ I
I I +race...
LL
~ :s,c..
LL
\ /
I :r
I 1
I)'
}r11rP,
LL
1:r
LL-
·, / ,I/
U -Ka.taria.l waa ana.ly:z:ad for but not ~•t•ctad. Th• number i• the Mi.nilmm& Detacticn Li.:11.it.
!ilA -Not analy:.d.
1:_I -T•ntativa identification.
?J -cai,.1.1'0..,1110 .Ra.I l'\BL."f -06TEC,flt;3L£ Q/JL'/ IN HI (rt-I (.O/'JCf: NT/<ffTlcN5,
V-SAMPLt'. \-ll&!-11..'{ OIL"-TED. f.lDL'-:> Do NOT APf'L.'/.
DEHNR 3065-0 (10/93)
u_.. I,{ I
' /
/ 3",L
1
\ I
+race...
(j
' I ' I
Pt!RGCOIILORG
.j
y
• • STATE I.ABORATORY OF PUBLIC HEALTH
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH, NC 27611
ORGANIC CHEMICAL ANALYSIS
P'URG.EABLE COMPOUNDS LIB NO (J_fi,'f(5Gi 9u,1(59 9(.Q I U.DO C/G,/ [Ct,;;)_ 9Co/ il.t,'f
FIELD NO co-19 Co-;;I.;). Co -.).5 co-;)S co -31
COMPOUND TYPE l 3 l ( if ) ( ,;L ) ( 4 ) ( .2 )
n~~5 "ppbJppm jph fPrr1 '[ppb) l'F-"1 (PPO) ppm 'ffb'tJpm
D rn ROMO~ 5 I I LL_ I ' I L,L
4-1i4'ETHTL-2--P?:NTAN'ON"E ,o
CIS-1.-'·DICBl,OROPROP?:Nl: 5
TOLU?:!'{l;
TR.Al'fS-l...3--0 I CHLO RO PRO P'E:'f?:
1,1.l,l• Tl:TR.ACBU>R0rrnAI'f1;
1, l.l-TRicm.oROETHA...'fE ' I/ .
JO ' 7 / '7 ' /
l-lI!:XA."l'ON'?:
\
TlITRACRLOROE;"'I'lJ%!a 5 1:r 1:r I :r +r,,.,,..,,
DIBR.OMOCID.ORO~ LL I J . LA,_ I l
rnITl..r.fE DmROWID?;
ClII..ORO~
1.1,1~ n:TRACHLOR.0£TR...\lf!:
===
==
= -I -.
BROW:O_TOR.W 10
TRAml-1. 4--D lCHl.ORO-l-Bunn <J'O
l,!l,3-TIUC3J..OROPROP ~ ..5
1,4-DICRLOROB!;l'fZX:'B
.I/
1, :l, D1Cl!LOROBZ:1'"LE:a ' I +-rnre..L.t
l.:2-DIBROM0-3..-CHLOROPROPAN'E ,9.tJ . I .
VINYL AJ:XT An ;;i.c;o
~e+h, ,/-t-bu-J.c,) efhf'1 5 I / ·, i/ . I/ ' I '11
Hyclrol<a'loon:5 I!. ®/8 .Ef)-.,!n~.1_t R 0 (-) e , ,;,o
oub5·h'tuted benz.;, L,5
C • """,,•01..E Lf\0 CcNU'\Ml>-IAT\ON <>R BFl~l-&t<OU1'lD.
J -lstimAt ■d Vlllu■ ·
,;: -A.ctual va.lua i• lcnown to be l••• than value 11ivan.
L -Actual value i• known to be greater th.an value giV91n.
U -hterial wa.s ana.ly:z:ed t:or but not d•t•cted. 'l'h• number 1• th• Mi.nimu:m JJ,ate~ion Lim.it •.
n -J;ot analy:ed.
1/ -Tentative idontitication-
lt -COMPolli-!O, flELtr:.1:11.-y Oel'EcrAeLE t1'JL'{ IN t-lJG-t-1 coNCtNTRAnotJ.:;,
✓ -SAl'lPLf: H1G-H LY DI LltTED. f,,\DL'o Do >Joi' APPL'/.
DEHl'iR 3068--0 (10/93)
q(D I IUJ&
co~3'f
( if J
!ppb)ppm
(.;L,
\ I
+r11rP
/ J
' /
(-
PURGCOM.ORG
• • STATE LABORATORY Of PUBLIC HEALTH
P.O. BOX 28047 -306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
BASE/NEUTRAL AND ACID LA8 NO • l<-f f11"l·l,<::/:.v· l/& //4 '/
EXTRACTABLES FIELD# ,.:::} ('o -:S-
COMPOUND TYPE c ,_:n ( ,-; )
UNITS . .....-,,:,r " n / k a -andua/ka>
-~-ni trosodimethvl amine tr.I.:?~,-,
bis(Z-chloroethvl)ether
2-chlor""henol
ohenol
1 3-<iichlorobenzene
1. 4-di ch lorobenzene
1 2-<iichlorobenzene
bis ( 2-ch 1 oroi """r""v 1 ) ether
hexachloroethane
N-n i troso-di -n-..nroovl amine
nitrobenzene
lsoohorone
2-n i trooheno 1
2.4-<iimethvlohenol
bis(2-chloroethoxvlrrethane
2.4-<iichloroohenol
1 2 4-trichlorobenzene
nanhthalene
hexachlorobutadiene
4-ch 1 oro-<n-creso 1
hexach lorocvc l """n tad i ene
2.4.6-trichlor=henol
2-ch loronaohtha lene
acenanhthvlene
dimethyl ohthalate
2.6-<iinitrotoluene
acenaiihthene
2 4-<iinitroohenol
2.4-<iinitrotoluene
4-nitroohenol
fl uorene
4-ch loroohenvl ohenv 1 ether
diethvl ohthalate
4 6-<iinitro-o-cresol
diohenvlamine
azobenzene
4-b=henvlohenvlether
hexachlorobenzene
oentachloroohenol
ohenanthrene
anthracene
dibutvl Phthalate
fl uoranthene
J -Estimated value.
SO//~So
I t'J /. "?10
S"Oht-<:o
10/330
.,
"i"O' ~;_,,.,,
/01330
~
S0/16.5"0
'~/~~n
' ..
m1)L
H,..o/.sou ..
i -IA -
I
' 1./-(;. I
1,,-L-
I ..,
:;j' -Ole
IA-
I
'
➔-0/<.
1 ,<
I
'
/,t. /,'/
I '? 2~ v
. I J,/3 :~
-f 1-oO -
K -Actual value is known to be les·s than value given.
L -Actual value is known to be greater than value given.
.
Cf/,.,! I i..J.<-t <f/,-,IJ"f/
r'o-9 r-o-/ I
( ..::j) ( 3,
n-"""'1: uq/ka ,m--z::lf ua/ka
IA~ IA -
I
'
L/oo
I,(_..
I
' . ;;; (,, 7
IA
l.,L-
~ '.< ok'
~
I
'~
-?c ';) I:"
[.,,L,
,
' 5. ~--;
l) ,. -,
I v<-
I ;,r, ,{J7i ,
<l!,-//5 -<
(1 0-JV
(. =<1
.,..n,<-F ua/ka
(
/
~::,nv
IA.......
/ ..,
CJ;,,,, le'
I.A-
l.,C-
-? ?01': v--,
' -3· ~01<':
1 ,I. -
/
' J • , .7.-::S
11.1,-,
In I oC., I
/n. nnn ,
U -llaterial was analyzed for but not detected. The numer
NA -Not analyzed.
is the Minirrun Detection Limit. m"JJL ----1/ -Tentative identification. ff -On NROC List of Priority Pollutants.
CJ
'7'/p"I/E.c-;:;·
f'0-17
( Os')
...,_;.1/ »n/kn~
I -
.
,
' I
;:? () I::'...
J ,.
I
' I
''3 ; QI<'.
LA--
I ...
~:; "Jr ~-/) I<'.
0---
4,o3..,
I
• • STAIE L-TOOY Of PUBLlC HEALTH
P.O. SOX 28047 -306 N. ~ILMINGTON, ST., RALEIGH, N.C. 27611
OOGANIC QjEMICAL ANALYSIS
. --.
BASE/NEUTRAL AND ACID LAB NO llJ/,;tll_LJ "> IC//,//t./'l Zl7nl/t.L'-I '-ft;/151 Cj(,..11" -<
EXTRACTABLES FIELD# 7 f'lr,-, /'n-)I ,,,.,_; I r' o-l<I
O)MPCIJND TYPE ( ~) ( -?l (-3) (31 ~\
UN!TS --4ua/ka · .. n/ko .....LU,,n/ka .. r /ko '\ ~,/ c-;ka
ovrene /O/:J'?n I -..,q ::r-.:{ I -"' /, ~ --< .,, ;;.;/:;:,~2
benzidine ,:-~/,1,,,;o ' , , vL--,',
butvl benzvl ohthalate 10/_?30 x' ooo vt--,3 a.u,
bend a lanthracene '/;t..., .), /,{,, 7 \ ,
chrysene . ;;1 ,ln7 ,t ~:?:;;; Jt _ nQO
3 3-<lichlorobenzidine sottt.._,o , L,L-' ,,, / t/l-
bis(2-ethvlhexvllnhthalate lo/330 .:;,o "? ::z -< q ,av lf7/)~ =1-:.~
di-n-octvl ohthalate ilO/.i~o 7,' x'~ ' vL-' t .
benzo(blfluoranthene so/·~ ~• ,0/.7 --s77~·-=! /,,o, oe>O
benzo(klfluoranthene 1 I A ... A.~ 't;<.....
benzo(alnvrene .::;' J \7l ..,4, qoo I 2)./,,,&,7
indeno( 1 2 3-<:dlnvrene ,_·-;oo "',,.{ -z :;;/ ~ !'10 I.I. 7
dibenzo(a h)anthracene / ' t,<.-I .;JJ )~~ .JI , -< 3-:.:
benzo(Q.h. llnPrvlene \ / I '-112..,l, ~ I 1.;.1 x-oO /:J-i ·, 1,,,
/ ,
ani 1 ine <a/11.,.-n 1/1 -(.A_.. I , -VL LA-
benzoic acid
benzvl a 1 coho 1 ' / ,
4-ch 1 a roan i 1 i ne ' ~ ' I ' '
dibenzofuran I() /. z.:? /l ::i ~ 0 I:' ~301:'.'... J, -zf, V
2-rrethvl iunhtha lene .., 9~ ~ 1 Z&7 ➔ -::v, ~
2-rrethvl oheno 1 I' ✓~ o A
4-methvloheool ,,,
2-nitroa.niline S-of,t,,<::o
3~i troani line
4-il i troan i line I / ' ' I
2 4 5-trichlornnheool .·. ~I' I , ' / ' / \ I ' ----.,..--<',..
/--IV nP oC ,4f r, oD <. -I--I-{-} r --'-1 (-) ( --t-) ( -+--) -
m:n1-
J -Estimated value. H "2.01 Sci'-
K -Actual value is known to be less than value given.
L -Actual value is known to be greater than value given.
U -llaterial was analyzed for but not detected. The nurber is the Minil!UTI Detection Limit,
NA -Not analyzed.
l/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
"w::o/ r,., :::;.,,-.
l"0-/7
<--3,
~ ··"/ka \
,::-000
I ,
I .l.
In 7',---0
!. '" ~ 'v.-
I '-1 , -, J --/
LA--
!'--1.2."5.,,,
LA--
I.). n~ -s
,--:{ J. I~ 7
; ',
, /,2LJO
' .
I.I\_....
/: ' /
( I )
---..;_..,-
'
,
• • • STATE LABORATORY Of PUBLIC HEALTH
P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC QjEHICAL ANALYSIS
BASE/NEUTRAL AND ACID LAB NO
EXTRACT ABLES FIELD #
COt1POOND TYPE
UNITS
1-ni trosodirrethvlami ne 1r,l_:t3o
, is (2-<:h loroethvl l ether
'.-chloroohenol
lheno 1
i , 3--d; ch 1 orobenzene
I. 4-di ch lorobenzene
1, 2-cH ch lorobenzene
>is (2-eh loroi =roovl l ether
,exachloroethane
'l-n 1 troso-di -n-nrrv,vlami ne
1itrobenzene
i s.oohorone
~-ni trnnhenol
2. 4--d irrethvl oheno I
bis(Z-ehloroethoxvlrrethane
2. 4--di ch lormheno I
I 2 4-trichlorobenzene
nanhtha 1 ene
hexachlorobutadiene
4-<:h 1 oro-m---<:reso I
hexach lorocvc l=ntadi ene
2 4 6-trichloroohenol
2-eh loron,nhtha 1 ene
acenanhthvlene
dirrethvl ohthalate
2.6--dinitrotoluene
acen,nhthene
2 4--dinitr~henol sol/r,,so
2.4--dinitrotoluene /nl3'.iO
4-nit~henol . 'rOhl. ,;o
fluorene 10/:i=10
4-<:hloroohenvlohenvlether
diethvl ohthalate •V
4 6--dinitro-o--cresol so
diohenvlamine /01330
azobenzene
4-braroohenvlohenvlether
hexachlorobenzene ' =ntachlor~henol S0/1(,,:fO
ohenanthrene '""'~,:,""
anthracene
dibutvl ohthalate
fl uoranthene ' ,
J ... Estimated value.
m"])L
1--l,._O/.SOIL-
!-1/~/Z'itfi -J/ Cl/,, Ir, '7°
f'o-7.I') /"'r) -z, ..,
( ·s'l ( l/ l
~M¥ uo/kq ,-~ ,u1/ko-
, A I,.,;___
J ,v
'-{, c)K..
V(._...,
I
' ~ o~· ,..___.
.
I
"'?30JC
....: -501::.
V-I
7 r,r, '
K -Actua 1 va 1 ue .is known to be 1 ess than va 1 ue given.
Cl/.// t,, I Cf/, J / I"' ~
('o--2..1.,:, l?.o-ZQ
(.;i._) ( 'f-)
"n/1 ~ .. 'T'mi,!( uo/kq
(A-IA
/ I
' '
':ltc/fl~<c,
/1 n-'?,;J..
r ;;i_ l
., uQ/1' ..
t..,<_
/
\
L -Actual value is known to be greater than value given.
U ... Material was analyzed for but not detected. The nurber
NA -Not analyzed.
is the Hininun Detection Limit. m'JJL ----1/ -Tentative identification. fl -On NROC List of Priority Pollutants.
9/,,/ //,.-, /
/'Q-'-?"',
( (J..'
n,,,<.V "n/kn )
u._..
I
'
./!..
BASE/NEUTRAL AND ACID
EXTRACT ABLES
COMPOJND
nvrene
benzidine
butvl benzvl nhthalate
benz(a)anlhracene
chrvsene
3 3-<lichlorobenzidine
bis(2-<ethvlhexvllnhthalate
ai-n-octvl ohthalate
benzo(b)fluoranthene
benzo(k)f)uoranthene
benzo(a)ovrene
i ndeno (I. 2. 3-ed) nvrene
dibenzo(a.h)anthracene
benzo(o h, i)n,,rvlene
aniline
benzok acid
benzvl a I coho I
4-eh l oroan i ~ i rte
dibenzofuran
2-methvl runhtha lene
2...rethvlohenol
4-<rethvloheool
2---nitro.aniline
3---nitrooniline
4-nitroaniline
2.4 5-trichloroohenol
1-1-•rJ'J l::'.or, .,'J,' '1 /\ • i <;
J -Estimated value.
• •
STATE LABORATORY OF PUBLlC HEALTH
P.O. BOX 28047 -306 N. ~lLHlNGTON, Sl., RALElGH, N.C. 27611
ORGANIC CHEHlCAL ANALYSlS
LAB HO ; fl/,,:'17~? IQ(p//V-i q/;l/(o/ 7/✓-.:?
FIELD # -17 o-? " co-,;z.-;;: r'o-:?.h 10-JlJ
TYPE ( =!, ( '-/. I ( -<'.) ( Y.1
UNITS ,,,,..,.,r,,_/kn .-.<J/.',o/ka) un/1~ ,..,.,,,.✓., n /kn,
/0/7=if'l I lf'Y1 L,<..-LA--U-
,.-,, -1;,:,20 , ' ,
/Ol.'?30
_ I, I
S"07iz:,?,, '
10 1"3o .., 13..;
II0/3.~o 71,,<--
SO /Jt,,,;"n J, qoo , u<--
3. 2.J -,
,:;' ?I~ 7 ,
L,L. / / 7
' , J--J ,,~., ' 7
<'o 1,,,,;-r I , IA-J A . LA--
.... ~
101=,,
,J,
S"O ·, t,,,;o
/ I / /
,1/ \ \ \ '\
--~ --
-rl r _L) { ) r-J (-)
~
m:DL
HzOI Scli..
to be less .than value given.
V/4//b:5 f"o-:::>,
/~)
.. n;J 'l.~c-
L,L.,
I
\
/or
I.,<-
f
\
l.1---
/
'
~
7-,I
K -Actual value is known
L -Actual value is known
U -Platerial was analyzed
NA -Not analyzed. ·
to be greater than value given.
for but not detected. The nurber is the Mininun Detection Limit. ~
1/ -Tentative identification. fl -On NROC List of Priority Pollutants.
(t)
C//-//h7 ccr~,
( i.L,
~,r -/ko)
L,<...-
I
'\ I
CA-
'\ I
"' -C }.
Memo
Date: July 1, 1996
To:
From:
File
Douglas Moore
Environmental Chemist
NC Superfund Section
Re: Telephone Conversation with Jim Kuszaj.
Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg Co. NC
US EPA ID: NCO 980 799 019
Cherokee Oil Site
925 South Summit Ave.
Charlotte, Mecklenburg Co. NC
US EPA ID: NCO 986 190 239
On Monday, July I, 1996, I spoke with Mr. Jim Kuszaj of Ogletree Law Firm
[phone] about the status of both above-named sites. Mr. Kuszaj indicated that he
is coordinating actions for the PRP group, specifically at the Berryhill Road site. He
stated that last Thursday, June 27, 1996, EPA convened a meeting with the top 80 PRP's
related to the Berryhill Road site to outline EPA's position. At this time, he was told by
EPA that I was the State contact for these sites.
I told Mr. Kuszaj that the purpose of my sampling trips at each of these sites was
to make a determination whether either of these sites required further long term remedial
action under EPA's CERCLA authority. At the Summit Avenue site, I explained that we
did not find a sufficient enough threat to warrant further Federal action and that the site
was given a "No Further Remedial Action Planned" status under CERCLA. At the
Berryhill Road site, I explained that EPA completed its removal action and that we
subsequently collected environmental samples on and off-site to assess the threat posed to
a nearby fishery. I told him that we had recently received the sample results, but that I
had not had an opportunity to review the results for accuracy and write the report. I
indicated that I could not speculate at this time on the disposition of the Berryhill Road
site and stated that I would like to have the site report completed by Late August.
In response to Mr. Kuszaj's inquiry regarding future State actions at the site, I
referred him to Charlotte Jesneck for information on the future plans of the Inactive
Hazardous Sites branch at each of these sites.
cc: Rob Gelblum
Charlotte Jesneck
Pat DeRosa
State of North Cari:ila
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
Gene W. Hartsell 10688-058
Caller Box 8004 Sandhills B
June 20, 1996
FPC -Seymour Johnson AFB
Goldsboro, North Carolina 27533-8004
Subject: Soil Sample Analytical Results
Cherokee Oil Company Site
120 I Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
Dear Mr. Hartsell:
In the March 18, 1996 letter to you, I indicated the NC Superfund Section
collected three soil samples ( one surficial soil sample, labeled CO-004-SL, and two
subsurface soil boring samples, labeled CO-002-SB and CO-003-SB) as part of an Site
Inspection (SI) at the subject site. As most mineralized soils contain naturally occuring
levels of metals, two background soil samples were collected near the site in a residential
area ( one surficial soil background, labeled CO-00 I-SL, and one subsurface soil
background, labeled CO-00 I-SB) for comparison. The soil samples were submitted to
the State Laboratory of Public Health for volatile organics, semi-volatile organics
including PCB's/pesticides and inorganics analyses. The final analytical results were
received on May 22, 1996.
Following receipt, the analytical results were reviewed and a table was generated
detailing constituents that we detected at elevated levels. "Elevated" means that the
constituents were found in the release sample at a concentration that was at least 3 times
their respective background soil concentration, if it was detected in the background soil
sample; or above the detection limit for the analytical method, if the constituent was not
detected in the background sample. In the table, an elevated constituent is noted by a
shaded cell. Elevated contaminants were compared to EPA human health-based soil
exposure standards. Those contaminants found to be greater than their respective soil
exposure standards are highlighted in bold lettering.
P.O. Box 27687,
Roleigh, North Carolina 27611-7687
Voice 919-733-4996 f#MA•I-J£Srn
FAX [phone]
An Equal Opportunity Affirmative Action Employer
50% recycled/10% post-consumer paper
Letter to Mr. Hartsell
Analytical Results
Page 2.
• •
A copy of the analytical results for your property is forwarded to you with this
package of information. Likewise, the sample points are represented on the figure
included in this package. If you have any questions, please submit them in writing to
myself.
cc: CEi!e:::n
Rob Gelblum
Pat DeRosa
Respectfully,
Douglas Moore
Environmental Chemist
NC Superfund Section
-:::1 • l CO-001-SL (Background: surface soil)
CO-001:.S.B !'.Background: 0-2 feet)
Figure 1.
Soil Sample Locations
Cherokee Oil Company Site
1201 Berryhill Road
Charlotte, Mecklenburg Co .. N.C.
US EPA ID: NCD 980 799 019
Map Not to Scale
Map Drawn by: D. Moore
(June 1996)
--- -Former Concrete Berm
Drainage Pathway
•
Cherokee Oil Company
CO-004-SL (surface soil)
Suburban Propane
• Contaminant Units CO-001-SL
Acetone ua/ka < 20.0
Methylene Chloride UQ/kQ < 5.0
l. l-Dlchloroethane ua/ka < 5.0
2-Butanone uo/ko < 20.0
Cis-l. 2-Dichloroethene UQ/kQ < 5.0
Chloroform ua/ka < 5.0
l, l. l-Trichloroethane ug/ka < 5.0
Benzene uo/ko < 5.0
l .2-Dlchloroethane ua/ka < 5.0
Trlchloroethene uo/ko < 5.0
Bromodichloromethane ua/ka < 5.0
Toluene uo/ko < 5.0
l. l ,2-Trichlaraethane ug/ka < 5.0 • 2-Hexanone uo/ko <10.0
Tetrachloroethene ua/ka < 5.0
Chlorobenzene uo/ko < 5.0
Ethyl Benzene ug/ka < 5.0
Xvlene(s) uo/ko < 5.0
l .4-Dlchlorobenzene ua/ka < 5.0
l ,2-Dlchlorobenzene. uo/ko < 5.0
Methyl-tert-butyl ether ug/kg < 5.0
Table 1.
Cherokee Oil Company
Charlotte. Mecklenburg County. N.C.
US EPA ID: NCD 980 799 019
Analytical Data -March 1996 Source Samples
CO-001-SB CO-002-SB CO-003-SB CO-004-SL EPA Soil Stds (ma/kn\
5J,C Blal DZl!®--,~-m-22111.la 58,000 (RfD)
7J,C BDL 3J.C BDL 78 (CPF)
BDL -◊--9---2J 58,000 (RfD)
BDL 6J 5J l8J 350,000 (RfD)
BDL -32-trace trace 5,800 (RfD)
BDL BDL trace trace 96 (CPF)
BDL ~ 2J trace none issued
BDL 4J 2J -◊-l2 20 (CPF)
BDL trace BDL trace 6.4 (CPF)
BDL mmsa-lJ trace 53 (CPF)
BDL BDL BDL trace 9.4 CCPF)
BDL -..:s09.-l!BB27-.lal~k7;01lilii 120.000 (RfD)
BDL BDL trace BDL lO CCPF)
BDL BDL BDL 4J none issued
BDL · -386-trace ~ll(CPF)
BDL trace BDL 12.000 (RfD)
BDL trace -27Ma 58,000 rRfD)
BDL 4J -l25Bll 1,200,000 (RfD)
BDL BDL BDL 24 (CPF)
BDL ll-rwal5J-trace trace 52.000 (CPF)
BDL BDL .,-,i15-trace none issued
Contaminant Units C0-001-SL • Naohthalene ua/ka < 330.0
Acenaohthylene uo/ko < 330.0
Acenaohthene ua/ka < 330.0
Fluorene uo/ko < 330.0
Phenanthrene ua/ka < 330.0
Anthracene uo/ko < 330.0
Fluoranthene ua/ka < 330.0
Pvrene uo/ko < 330.0
Benz(alanthracene ua/ka < 330.0
Chrvsene uo/ko < 330.0
Benzo(bllluoranthene ua/ka < 1650.0
Benzo(aJpyrene uo/ko < 1650.0
lndeno(l ,2,3-cdlovrene ua/ka < 1650.0
Dibenzo(a.h)anthracene uo/ko < 1650.0
Benzorn,h,11nervlene ua/ka < 1650.0 • Dibenzoluran uo/ko < 330.0
2-methylnaphthalene uo/ko < 330.0
Dibutylphthalate uo/ko < 330.0
Butvl Benzvl Phthalate ua/ka < 330.0
Bls(2-ethylhexyllohthalatE uo/ko < 330.0
Dl-n-octvl ohthalate ua/ka < 330.0
PCB 1254 ma/ka < 0.1
Table l.
Cherokee Oil Company
Charlotte. Mecklenburg County, N.C.
US EPA ID: NCD 980 799 019
Analytical Data -March 1996 Source Samples
C0-001-SB C0-002-SB C0-003-SB C0-004-SL
BDL -461-• !l!li!lf400!i8i 330 K
BDL BDL ~l!l3o71!!wi 330 K
BDL 330 K 330 K 330 K
BDL 330 K 330 K 330 K
BDL -ll-'.467.IIBIJ i!iB583!iBI -1~333§!!0
BDL 330 K @!!hi!0467§!~ Rl!l"667B'n:
BDL -3;600-Hl8T500!hl! Nl0;000R
BDL E&A:105/933-f!)l'.Jl211'333!i8 E3:W333!i8
BDL BDL !llm2;667§!1!! BDL
BDL -.2120'11t,_ !111'!1!333l/.WI! Er6J000!1B
BDL l-2;0o71!m41 i!h!h37t7:33'/w1l \IJ!160J000!i8
BDL -3~,s~-. !l!IS6:9.00~11.l Rl21f667a
BDL --1~7.00Rl!I !l!.fi50J333'llfll RT1.90lo'67iil!
BDL BDL il!h!h2<11533!i8 E2l2l3338
BDL -4ri133r!h!hllll w1,~60L800~'ffl Bl28;667,ll!
BDL 330 K 330 K 330 K
BDL 15:BM-1!111!267l!m 330 K
BDL l!h!h!h!hB'" -, BDL EA:6T667l/.WI!
BDL BDL Bl30!6671!!!
BDL !il!lii,915001!!! E703;333!h!h
BDL !l;-;Z4833-~ BDL BDL
< 0.1 < 0.1 < 0.1 < 0.1
EPA Soil Stds (ma/kn\
none issued
none Issued
35,000 (RID)
23,000 (RID)
none issued
170,000 (RID)
23,000 (RID)
17,000 (RID)
none issued
none issued
none issued
0.08 (CPF)
none issued
none issued
none issued
none Issued
none Issued
58,000 (RID) i
120.000 (RID)
42 (CPF)
12.000 (RID)
0.076 mo/ko (CPF)
•
•
Contaminant Units C0-001-SL
Arsenic ma/ka 2,8
TC LP-Arsenic mq/L <0.0l
Barium ma/ka 124
TC LP-Barium ma/L 0,59
Cadmium mq/kq < 10.0
TCLP-Cadmium ma/L <0,05
Chromium mg/kq 22
TC LP-Chromium ma/L <0,05
Conner ma/ka 34
TC LP-Conner mo/L <0,05
Lead ma/ka 36
TC LP-Lead mo/L <0.10
Mercury ma/ka < 0.1
TCLP-Mercurv mo/L <0.01
Selenium ma/ka < l.O
TCLP-Selenium mo/L < 0.005
Sliver ma/ka. <10.0
TC LP-Silver mo/L <0,05
Zinc mg/kq 56
TCLP-Zinc mo/L 0.07
Table l.
Cherokee Oil Company
Charlotte, Mecklenburg County, N.C.
US EPA ID: NCD 980 799 019
Analytical Data -March 1996 Source Samples
C0-001-SB C0-002-SB C0-003-SB C0-004-SL
4.4 2.6 2 2.5
<0,01 < 0.01 <0,0l <0.0l
68 82 124 140
0,44 0.75 l.27 0.67
< 10.0 < 10.0 < 10.0 < 9,8
<0,05 <0.05 <0.05 <0.05
30 30 38 55
<0,05 <0.05 <0.05 <0.05
52 62 46 55
<0.05 < 0,05 <0.05 <0.05
20 58 20 2"'1·
<0,10 < 0.10 < 0.10 OI .
< O. l <0.l < 0.1 0~121t..ma-:i1
<0.01 <0,0l <0.0l <0,01
< l.O < l .O < 1.0 < l.O
< 0,005 < 0.005 < 0.005 < 0,005
<10.0 < 10,0 < 10.0 < 9,8
< 0.05 <0.05 < 0,05 < 0.05
62 92 44 o001lil'IIR!,l
0.12 0.32 0.09 ~1'Z71'~
Shading Indicates >/; 3 x background, or> background, 11 bkgd. ; ND
EPA Soil Stds.
0.33 ma/ka (CPFl
5,0 mn/L-11CLP Limit)
41,000 ma/ka /RfD)
100.0 ma/L CTCLPl
290.0 mo/ko /RID)
l ,O ma/L CT CLP Limit)
2,900 mo/ko /RfDl
5,0 ma/L CT CLP Limit\
none issued
none issued
400.0 ma/ka (EPA)
5,0 mn/L0CLP Limit)
170,0 ma/ka IRfDl
0.2 mn/L nCLP Umin
2,900 ma/ka IRfDl
l .O mn/L ncLP)
2,900 ma/ka rRfDl
5.0 mn/L nCLP1
170,000 ma/ka /RfDl
none issued
Bold Indicates a concentration In excess of applicable EPA SCDM soil exposure or TCLP regulatory standards,
CPF -refers to the EPA Superfund Chemical Data Matrix (SCDM) Cancer Risk Screening Concentration standard,
RfD -refers to the EPA SCDM Reference Dose Screening Concentration standard.
EPA -refers to the EPA soil lead guidance level.
TCLP -refers to the Toxicity Characteristic Leaching Procedure as outlined In NCAC Title 15A, Chapter 13A Appendix II, Method 131 l,
TCLP Limit -refers to the TCLP regulatory standard (NCAC, Ttile l 5A Chapter l 3A Subpart C, section 261.24, table I).
• • t-.:.C. Lcp;;nmcnt of En,iroomcnf,
lic~lth, ,; ~atur~I Resources
S::;iid Waste Mao~gcmcnt Division
SAMPLE A. ·ALYS IS REQUES~:: i::.C ;::: r:c; S1::1c. [,.1b0r.l101)• o( l'ul.Jii~ .Hcallh
Sile Number
Name of Site
C0-001-SL 03/06/96 1501 GRAB
Cherokee Oil Company, NC DOUG HOORE
BACKGROUND SURFACE SOIL
ESO LAB VOA Soil
1
['.(1. !!ox 2&}:/, .}()'., i-;, \\'ih1ir;iton Street '/996 llalcigh, Nort:J. Ulmlin11. 276! l
Collected By_~--------11.J ,;-ua(c LOJJcctcd Time ---------------------
Agency: Ha7..ardous Waste Solid Waste ✓superfuud TCLP Compounds -----
Sample Type lu?rg:-i.nic Compounds Results(mg/1)
Envirnnrnc11tsl Concentrate Commcn!s Arsenic --Bari uni --Ground water (1) _ Solid (5) Cadmium ----Chromium --Surface water (2) Liquid (6) Lca<l ----
--Mercury
/ Soil (3) _ Sludge (7) Sclrnium ---·· Silver --_ Other (4) _ Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Pam meter Results(mg/1) Pt1ramcter Resul Ls (mg/I) (mg/kg) Orbanic ComjlOUnd.s Rcsults(mg/1)
,.....-1> &T:GC/MS Arsenic bcn1.cnc ----Aeid:R/N Ext. Barium ca:-bon tetrad1loridc ------MTBE Cadmium chlordane ------Chloride chlorobcnzcnc ------Chromium chloroform ------
--__ Copper o-,:rcso! --Fluoride m-crcsol ------
·-'-Iron p-crcsol ----Lead crcso! ·-----
----Manganese l 14---dichlorobcnzcne ----__ Mercury 1,2-dichloroct bane --
--Nitrate 1, 1 •dichloroethylcnc ----Selenium 2,4•dinitrotoluenc. ----Silver hcptachlor ----Rad iochcmistry Sulfates hcx.Jchlorobcnzcne ----Zinc hex;ich lorobut ,1diene ----Results (l'Ci/1) P:1rnmcter pH hcxach loroet hane ----____ Gross·Alph;1 __ Condl!cti\~ty methyl ethyl ketone --Gross Beta TDS nitrobenzcnc --··· ----TOC pcntachlorophcnol . , ----pyridine ----!Vlicrobiology --tetra ch lo roe thy! enc --
--trichlorocthylcnc
Parameter Results (Col/l 00ml) --2,4,5-trich lorophcnol ----2, 4 ,6-tri chi o ro phenol ------
------Yiny! chloride
endrin --
O:itc Received 3-7-q(; /6!;:J_fcportc~' ) L ,<.Mt:L(_ 1/--lindanc
rnctboxych)or
Dale RcU'cJ 01P / / ?' r:; --toxt1phcnc
Dal,: l:.xtractcJ 2,o-D
·' --2,o,5-TP (S,!·_,cx) 1i96'1!rl!!1 A 0;!\:; An:1ly1-cd 3-1:J.-q{Q_ W..U-L:ih Numbt;r ._:;,t,;:--'7~_(/ t/ v-'7'_~ I /_(,_t._-··--·-------·--~L!...:..'::...~.Li.i;'.,:.:,.~l ·-------·----" '•
" .............. _. __ ••-•N -· .,__,,..
_ -p~rtmcnr o( Environnicnt,
l lcalth, & Natur:il Resources
Solid Waste Manl[;crrycnt Divi~ion
• SA.tv!PLI~ ANALY',IS REQUEST • .St::itc i .. abor.1\01y of l'ublic l!c~l:h
P.O. fkn. :!S0-17, J06 N. \1.iilmlngton ~In:~\
R.alcit:h, Nl•1\h Cuulina 27611
· b C0-001-SL 03/06/96 1501 GRAB Site Num er_
Cherokee Oil Coapany, HC DOUG MOORE
Number ________________ _
Name of Site BACKGROUND SURFACE SOIL
-ESD LAB EXT/PEST Soil
Collected By 2
-----------
Agency: Hazardous Waste Solid Waste Lsuperfund
Sample Type
Environmcn(:11 Concentrate Comments
__ Groundwater (1)
__ Surface water (2)
✓ Soil (3)
_ Solid (5)
_ Liquid (6) __________ _
_ Sludge (7) __________ _
_ Other (4) _ Other (8)
Organic Chemistry
Parameter
P&T:GC/MS
✓ Acid:B/K Ext.
MTBE
✓ Pc/31
' /ffin<-tDE3-
Resutts(mg/1)
Inorganic Chemistry
Parameter Resulls(mg/l)(mg/kg)
Arsenic
Barium --Cadmium --Chloride --~~--
_ 'f{!B'S -<o,/0~: Chromium _ E"Nc/R./1/ -c::::o,~ == Copper
_ JjNcbw'E -<,:;,.2.IJJ _ Fluoride
~A_ -< /, .. t:, ..... ... Iron
....,. t1Wc < .:::7 -..-~ Lead
r \/J,,:u/AA/t: -<O, Manganese
t!cl-' Ehf:~'12?'/'!_C.~':,,fl."' £~,:,,<!H:.,-c:::s~o2'-cJ(J2 ·Jli;lOL~I __ Mercury
7i¥AM!t~pt-,/t=<O, · __ Nitrate
Radiochemistry
Parameter
__ Gross Alpha
Gross Bela
Results (PCi/1)
Selenium --Silver --Sulfates
Zinc --__ pH
__ Conductivity
TDS --TOC --~--------------!
Microbiology
l\iramctcr Results (Col/lO0ml)
.
Time ______ _
TCLP Compounds
Inorganic Com1rnunds
Arsenic --Barium --Cadmium
Cluomium --Lead
Results(mg/1)
__ Mercury
Selenium
Silver -··--------
Organic Compounds
benzene
carbon tetrachloride
Results(mg/1)
---------
chlordane
chlorobcnzcnc --chloroform
o-cresol --m-crcsol
__ p-crcs~l
crcsol
__ 1,4-dichlorobcnzcnt ______ _
__ 1,2-dich!orocthanc
__ 1,1-dichloroethylcne
__ 2,4-dinitrotolucnc.
__ hcptachlor
hexachlorobcnzcnc --
--hex.1chlorobu1adicnc ______ _
hcx.::ichloroclhanc --
--methyl ethyl ketone
nitrobcnzenc ----pentachlorophcnol
__ pyridine
__ tctrach!orocthylenc
__ trichlorocthy!e □c
__ 2,4,5-trichlorophcnol
__ 2,4,6-trich..lorophenol
__ v'iny! chloride
endrin --lindanc
__ rnctboxyCh!or
__ tox2phcnc
__ 2,'i-D
__ 2,4,5-TP (Si!·.·ex)
----------
; ;,
,1r\~1cnt o( En-,i"-l,1mcn1,
r~I"& Natural Resources ~-,. '
· Solid Waste Managcn1cnt Division
SAMPLE ANALYSIS REQUEST :-.. 11c [,;i!;,or-JtOf)' o( Public Hcal1h
l'.0 l';.:.,x 280-i7, Yli N. \l.'ilmington _Stn:ct
llalci&h, Nor1h Carolina 2761 J
Sile Number C0-001-SB 03/06/96 1515 GRAB
Cherokee Oil Company, NC DOUG HOORE
BACKGROUND SUBSURFACE SOIL
fombcr ________________ _
Name of Site ESD LAB VOA Subsurface Soil
co-7 Collected By __________ _ .d Time -----------------
Agency: Hazardous Waste Solid Waste v" Superf"und
Sample Type
Environmental Concentrate Comments
__ Ground water (1) Solid (5)
__ Surface water (2) Liquid (6) ____________ _
✓ Soil (3) _ Sludge (7) __________ _
_ Other (4) Other (8)
Organic Chemistry Inorganic Chemistry
Parameter Results(mg/1) Parameter Results(mg/l)(mg/kg)
V P&T:GC/MS
Acid:B/N Ext.
MTBE
_, --------------
Rad iochemistt)'
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
Parameter Results (PCi/1) pH
__ Gross Alpha ______ _
Gross Beta
Microbiology
Results (Col/lO0rnl)
__ Conductivity
TDS
TOC
Dale Rccc;vcd .3--]-9'/,~eported by ________ _
Dulc Exlractcd _________ Dale Reported ________ _
D,ite Ana!y1.cd 3-18-9~ 7]'-',; Loh Number <-~\1.4:"48J)
:·11 : :-; .1 ! '' I ( :-:---;,,_.,1 .'111; -,
TCLI' Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Cb.romium
Lead
Mercury
Selenium
Si!ver
Organic Compounds
benzene
Results(mg/1)
Rcsulls(rng/1)
carbon tetrachloride ______ _
chlordane
chlorobenzene
chloroform
o-cresol
m-crcsol
p-c:-esol
crcso!
1, 4-d ich I a robcnie n c -------l,2-dichloroell1anc
1,1-dichloroethylenc ______ _
2,4-dinitrotoluenc.
hcptach!or
hcxJchlorobenzcne
hex;i,chlorobutaJienc ______ _
hcxachloroclhanc
methyl ethyl ketone ______ _
nitrobcnzenc
pcntach!orophcnol
pyridine
tetra chloroe th ylcnc
trichloroethylenc
--2,4,5-trich!orophcno! ______ _
--2.,4,6-trichlorophcnol ______ _
--\~ny! chloride
e.ndrin
lindane
mcthoxyC:h!or
tox.:ipht.:ne
2,•1-D
2,4,5-TP (Si!·:cx)
.1!11~n1 of Env,ronmenc,
.inf/ J.,. NaturJ! Resources
s~-li~ W~s(c Mann~cmcnt Division
SAMPLE ANALYSIS REQUEST S1:1:r. f ~"'b0r.i.,,. ,-; uf l'ubii: llc:ith
t.O. Box 251}:7, 3C<; N. Wilmington _Strc,1
Raleigh, North Carolina 27611
Site Number_ C0-001-SB 03/06/96 1515 GRAB
Cherokee Oil Company, NC DOUG MOORE
BACKGROUND SUBSURFACE SOIL
Nlimbcr
Name of Site ESO LAB EXl/PEST Subsurface Soil
co-8 Collected By __________ _ LJ-tlc ...__uucctcd ----
Agency: Hazardous Waste Solid Waste V Superfund
Sample Type
Envirnnmcnta! Concentrate Comments
__ Ground waler (1) __ Solid (5)
Surface waler (2) Liquid (6) -------'--------
✓soil (3) _ Sludge (7) -~---------
-Other (4) Other (8) ___________ _
Organic Chemistry Inorganic Chemistry
P:irnmctcr Resulls(mg/1) Parameter Results (mg/I) (mg/kg)
P&T:GC/MS Arsenic
7 Acid:B/N Ext. Barium
MTBE Cadmium
. ? ~te:D,cE'c,S'-------Chloride __ Pcm-__:<:,,__!O~,L'.~clr201 Chromium
Eil/d.Rt'# -<:Q, _ Copper
Al' NE Fluoride
Radiochemistry
P;1rametcr Results (PCi/1)
__ Gross Alpha ______ _
Gross Beta
1vlicrobiology
P.in.1rnctcr Results (Col/l00ml)
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
Conductivity ______ _
TDS
TOC
----------------
_________ Time ______ _
TCLI' Compounds
Inorganic Compounds
Arsenic
Barium
Cadmiuru
Chwmium
Lead
Mercury
Selenium
Silver
Oq~anic Compour..ds
bcn7.cnc
carbon tetrachloride
ch!or~anc
ch!orobcnzcnc
chloroform
o-crcsol
m-c,csol
p-crcsol
ere.sol
1, 4-d ich lorobcnzen J,
1,2-dichlorocthanc
Rcsulis(mg/1)
Rcsults(mg/1)
------
------
l,l•dichloroethylene ______ _
2,4-di nitrololucnc
heptachlor
hcx3chlorobcnzcne
hcxachlorobu( ad icne
hcXJ.chlorocthanc ------
methyl ethyl ketone ______ _
nitrobcnzcnc
pcnlachlorophcnol
pyridin~ ·
tctrachloroct hylcnc
trichlorocthylc□ c
--2,4,5-trichlorophcnot ______ _
--2,4,6-trichlorophenol ______ _
vinyl chloride
endrin
lindanc
mcthoxych!or
toxaphcnc
2,4-D = 2,4,5-TP (Si!,•c:x)
.. ,.. .. rtmcn! c,i E.rwire:imcnl,
.,calth, & r<J1ur:il Rcsour~cs
.so:id Waste \~anJgc.n:cnt Division
• SA1'v!PLJ<: ANAJ..,YSIS REQUE';T • S1a1,:. l,;1bor.itor)' or !'ubli,; i!c~lth
r.O. !Jot :!SIJ.17, ~ N. Wi!min~lo:1 _St~ct
Ra!r.i&h, N0rth Carclina 27611
Site Number C0-002-SB 03/06/96 1150 GRAB
Cherokee Oil Company, HC OOUG MOORE
. N11rnbc.r _________________ _
Name of Site SUBSURFACE SOIL AREA II .
-ESD LAB VOA Subsurface Soil
co-Collected Br 4
,._,.,,,._, '-VIII., -..:tcd Time
Agency: Hazardous Waste Solid Waste . v"' Superfund TCLP Compounds ·-----
Sample Type Inorganic Compounds Rcsults(mg/1)
Environmental Concentrate Comments Arsenic --Barium --Cadmium Ground water (1) __ Solid (5) ----Chromium --Liquid (6) Surface water (2) Lead ------
--Mercury ✓ Soil (3) _ Sludge (7) Selenium --Silver --_ Other (4) --Other (8) --
--
--Organic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Rcsul ls (mg/l)(mg/kg) Organic Compounds Results(mg/1) ✓P&T:GC/MS Arsenic benzene ----
--Aeid:B/N fat. Barium carbon lctrachkiride ----MTBE Cadmium chlo.rdanc ------Chloride --chloroben1.cr1c ---~
Chromium --chloroform ------__ Copper o-crcsol --
--Fluoride m-crcsol ----, Iron p-crcsol ------Lead crcsol ----
--__ Manganese --1,4-dich!orobcnzenc
--__ Mercury 1,2-d i ch !orocthanc --
--Nitrate I, 1-dichloroethylcne ----Se!cniurn . 2,4-dinitrotoluenc. --Silver heptachlor ----Radiochemistry Sulfates hexachlorobcnzcne ----Zinc hex;i.chlorobutad icnc
Paramcti.:r (PCi/1) ----Results pH hcx.::ichlorocthanc ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
--Gross Beta TDS nitrobcnzene ----TOC pentachlorophenol . , ----
----pyridine
Microbiology ----tetra chloroet hy!cnc
--trichloroethylcnc
Parameter Results (Col/!OOml) = 2, 4,5-trichlorophcnol --
----2, 4 ,6-t ricWoro phcn al
----Yinyl chloride
endrin --lindane
Date Received 3..,.7--_q(, -~.!@ Reported by --r;ictho;,,.1Ch!or --
--toxnphcnc
Datl'. Extr:iclcd D;ite Reported 2,t.-D --2,4,5-TP (Si!·.n) 3-IJ.-9&.7'/u.r ,961.~1"46 ,,,,,,, --Date i-\n:dylcC L1h Nurnhcr ,~-• -<"I~•,
! \! :\ .. l,! '.JJ ( !·'.-•• ' ? /'i .. --· -------
. .. . ·····----· --·
• ,,.. .. rfmcnl of Environ men!,
, 1t;11h, t:. /"atural Resources
Solid Waste Man~gcr?cnt Division
SA1v!PLE ANALYSIS REQUEST
Sile Number C0-002-SB 03/06/96 1150 GRAB
Cherokee Oil Company, NC DOUG MOORE
Number
Name of Sile SUBSURFACE SOIL AREA 11
-ESO LAB EXT/PEST Subsurface Soil co-
Colleeled By_
5
Agency: Hazardous Waste Solid Waste / Supcrfund -----
Sample Type
Envirnnmcntal Concentrate Comments
~-Ground waler (1) _Solid (5)
-· Surface water (2) _ Liquid (6)
✓ Soil (3) _ Sludge (7)
_ Other (4) _ Other (8)
O,·ganic Chemistry Inorganic Chemistry
Parameter Rcsults(mg/1) Parameter Resu lt.s(mg/l)(mg/kg)
__ P&T:GC/,1S Arsenic --✓-Acid:B/N Ex1. Barium --MTBE Cadmit.:r-..1
v P,;1;'•/,,ff-r/CIDE.5
--Chloride --_ pc:p. s-< 0 • I II .,..,. Chromium --EJ/f,jlff ·-~,10• ·-~ __ Copper --Li~ ~.-VE _ __... _ _.. ~-Fluoride
, 7ll«Afo/cAktR-< /. ~ .:.. -· --Iron --~me: ="' .,,. ~-Lead --__ Manganese ~ = t ~;,•·L"Hl~ __ Mercury
~~~. /CJ --Nitrate --. , Selenium --Silver --Rad iochernistry Sulfates --···-Zinc --
Parameter Results (PCi/1) --pH
__ Gross Alpha --Conductivity
Gross Beta TDS ----TOC --
--
Microbiology --
--Parameter Results (Coi/lOOrnl) --
----
----
Date Received 3-]....:.C/_f_~j;f,Rcported by
tcB/tad 3-1 o-9(, JP,/
Dale loxlraclcu 3-/1-q/2 $~ Dale Reported
96'1::4'4 7 ~~,t' 61-11 pees_~
~1~~;c<~~~;:{,~:~:~-~{;~\I_ 3-1/-?'yp,ab Number ~-· \ ;a,_,;,.,,,
.,: •' '-~-~ ,o..: •• ·, __ , .. ~. ·• u, ----·-· ·--·----.• -.
• State l_.1bor~1ory o( Public I !c~i:h
P.O. Oox 2S0.17, JO:$ N. Wilrningtor. S1:-:::~1
Raleigh, North Ca.ro!ir.B ?76! l
----------------
TCLP Compounds
Inorganic Compounds Results(mg/1)
Arsenic --Barium --Cadmium --Chromium --Lead --Mercury
--Sele~ium --Silver --
--
--
--
--
Organic Compounds Rcsults(mg/1)
benzene --carbon tetrachloride --chlordane --chlorobenzcnr, --chloroform --o-cresol --m-crcsol --__ p-crcsol
crcsol --
--1, 4-d ichlprobcnzenc
--1,2-diclilo roe l han c
1, 1-dichloroethylene --
--2,4-dinitrololucnc.
__ heptachlor
hcxachlorobcnzcne --hexilch!orobutad icne --hcxachloroct hane --
--methyl ethyl ketone
nitrobcnzcnc --pentachloropheno I . ,
__ pyridine
t et rachlo roe th ylenc --__ trichlorocthylcoc
__ 2, 4 ,5-trich !orophc no!
__ 2,4,6-trichlorophcnol
__ vinyl chloride
rndrin --lindane --
--mcthoxychlor
--toxaphcnc
·2,0.1) --
--2,,,5-TP (Si!·,cx)
--
·~•nic-,;1 of Eriviionmcnt.
.. n1(s.: r<.;.tur~I Rc~ourLcS
•S~rl W;istc M.in;igc.mcnt Division
SA.iv!PLE ANALYSIS REQUEST Selle L.1horJIOl)' o( l'ub!ic Hc:i.!th
f'.(l !~ui 2W7, 306 N. Wilmington _St rec:
R.Jlcii;h, North Carolina 2i611
Sile Number C0-003-SB 03/06196 (140 GRAB
Cherokee Oil Co•pany, NC DOUG MOORE
SUBSURFACE SOIL AREA 11
Number ________________ _
Name of Site EID LAB VOA Subsurface Soil
co-10 Collected By _________ _ ·d T~c -----·· ---··· --:==========..:..=,::=:====-,
Agency: Hazardous Waste Solid Waste v" Superfund
Sample Type
Environmental Conccnlratc Com men Ls
Ground water (1) __ Solid (5)
Surface water (2) __ Liquid (6) ____________ _
✓ Soil (3) _ Sludge (7) __________ _
Other ( 4) _Other(8) ------~----
Organic Chemistry Inorganic Chemistry
Pam meter Results(mg/1) Pnrameter Results(mg/1) (mg/kg)
_l'.'.'.'.'P&T GC/MS
Acid:B/N h1.
MTBE
I
Radiochemistry
Parameter Results (I'Ci/1)
Gross Alpha -------Gross Beta
i'v!icrobio logy
Parameter Results (Col/l00ml)
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride ·
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
Conductivity
TDS
TOC
Date Received S--7--f,6 fifrtl:J:eportc<l by _______ _
Dale Extr:.ictcd _________ Dale Rcrorted ________ _
D»lc An,dy-1cd 3-f'cr'?&., 71W-Lib Number 9k_1;,li5Q_<;.:•
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Le,d
Mercury
Selenium
Silver
Organic Compounds
benzene
Rcsulls(mg/1)
Rcsults(mg/1)
carbon lctrachloridc ______ _
chlordane
ch!oiobcnzcnc
chloroform
o-crcsol
m·crcsol
p•crcsol
--ere.sol
1,4-dichlorobcnzenc ----'---
1,2-d ich lo roe th anc
1,1-dichloroethylenc ______ _
2,4-dinitrotolucnc.
__ hcptach!or
hc.uchlorobcnzcne
hexachlorobu!adicnc ______ _
hcxachloroct h anc
methyl elhyl ketone
nitrobcnzcnc
__ pen!achlorophenol
__ pyridine
let r ach lo roe th ylenc
trichloroct hy!cnc
--2,4,5-tric!1lorophcnol ______ _
--2,4,6-trichlorophcnol ______ _ = viny! chloride
cndrin
lind;rnc
rncthoxyi:hlor
toxaphcnc .
2,4-D
2,4,5-TP (Sil·.•cx)
-------------
. // .
.. ..-r1C~i:-~f En~ironmcni,
ith'& ,,•3tur:il Resources
SAMPLE k'\'ALYSIS REQUEST
_.,. .. u , Solid wa.nc Mll11~1:cr1:cnl Division
s;te Number C0-003-SB 03/06/96 1240 GRAB
Cherokee Oil Company, NC DOUG MOORE Number
SUBSURFACE SOIL AREA 12
Name or Site_ ESO LAB EXT/PEST Subsurface Soil
co-11 Collected By -----------
Agency: Hazardous Waste Solid Waste V"' Superfund -----
Sample Type
Erlvironmcntal Concentrate Comments
__ Ground water (1) _ Solid (5)
--Surface water (2) Liquid (6)
v"soil (3) _ Sludge (7)
_ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
.
Parnmctcr Resu I ts (mg/I) Parameter Resulls(mg/1) (mg/kg)
P&TGC/MS Arsenic
✓Acid:B/N Ext. --Barium --MTBE Cadmium --
~, .. /'?LBS /pCs77c1CJG..5 Chloride --_ -PC.85--<:: 0,/ Orprr, Chromium --_ ~ -<::o, /Op/'°' __ Copper
_ ' ~ -s:o,-<bR,PtX Fluoride --1JiE·~ ~-'RR<. /10 ., .. ./-... fron
_T~i<~o',~-, --Lead --
i?. Wi <o, ~h ~~ M,rnganese
--l/__t:'.,.,rA " --c::-o,ld ,,.._ --Mercury
-Ve; d / /,:r,e~'j=<o, ,'.:'.-Nitrate
I I, Selenium --Silver --R~diochemistry --Sulfates
Zinc --Parameter Results (l'Ci/1) --pH
__ Gross Alpha --Conductivity
Gross Beta TDS ----TOC --
--Microbiology --
--Parameter Results (Col/l00ml) --
--------
Date Receive~ ~-7--Jh ~Reported by
tC/J/f.iJt 3 ·· 1-,-%, ,t1J
Date btrsclcdj!;/1-91~,ig~~alc ·Repcn"d _
Dale Analy1edJ_:}~ 3-.2/-'1'6_1-fo"ah Numhcr _~9,~';i;-1-51)};,c;; ____
I l! '.'' ~:·:: /1.',··.: ··: ."'"
St~lc f_.1horJtory o( l'ub!ic Ile.11th
r.n O:ix: 2ron, 305 N. Wilmington _Stn:ct
R..1lcij;h, North Carolin,. 27611
----------------
TCLP Compounds
lnorgnnic Compounds Rcsults(mg/1)
Arsenic --Barium --Cadmium --Chromium --Lead --Mercury --Selenium --Silver --
--
--
--
--
Organic Compounds Results(mg/1)
benzene --carbon tetrachloride --chlordane --chlorobenzene --chloroform --o-cresol --m-cresol --__ p-cresol
crcso! --1, 4--d i ch lo robe nzc nc --1,2-dichloroethanc --1, 1-dichloroethylene --2,4-dinitrotolucnc. --__ heptachlor
hcxachlorobenzcne --hex,1ch I orobu tad i enc --heXJchloroel hanc --__ methyl ethyl ketone
nitrobcnzcne --__ pentachlorophcno\ . ,
__ pyridine
__ tetrachloroethylene
trichloroethylcnc --__ 2,4,5-trich!orophcnol
__ 2,4,6-trich..lorophcnol
__ V1ny! chloride
endrin --lindanc --mclhoxychlor --toxnphcnc ---2,'1-D
__ 2,4,5-TP (Si!·,cx)
·-------
---·--·-
SAlv!PLE ANALYSIS REQUEST
Site Number_ C0-004-Sl 03/06/96 1205 GRAB
Cherokee Oil Company, NC
STAINED SURFACE SOIL AREA 13 Name of Site -ESD LAB VOA Soil
Number
DOUG H00RE
Stale l...aborJlory o( l'ublic Hc~ith
P.O. r1ox 2Sl}J7, 305 N. Wilmini::ton _S!r'Ccl
Rakigh, Norih Carol_ina 27611
----------------
co-13 Collceted By __________ _ cd Ti.me -----------------
Agency: Hazardous Waste Solid Waste ✓ Superfund
Sample Type
Envirnnmcntal Concentrate Comments
Ground water (1)
__ Surface water (2)
Vsoil (3)
___ Solid (5)
_ Liquid (6) ___________ _
Sludge (7) __________ _
_ Other (4) _ Other (8)
Organic Chemistry Inorganic Chemistry
Parnrnctcr
__ VP&TGC/MS
Acid:B/N Ext.
MTBE
Rcsults(mg/1) Parameter Results(mg/l)(mg/kg)
Radiochemistry
Arsenic
Barium
Cadmium
Chloride
Chromium
__ Copper
Fluoride
Iron
Lead
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Paramell!r
Zinc
Results (PCi/1) __ pH
__ G russ Alpha --------Gross Beta
__ Conductivity _______ _
TDS
TOC
!vlicrobiology
Paran1e[cr Results (Col/100111!)
Date Received 3~ 7---'t{, /f!;tt'5Reportcd by _________ _
Date Extrat.:tcd Dale Reported ________ _
TCLP Compounds
Inorganic Compo11nrl.s
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
carbon lctrach!oridc
chlordane
ch!orobenzcne
chloroform
o-cresol
m-crcso!
p-crcsol
cresol
Rcsults(mg/1)
Rcsults(mg/1)
------
l,4-dic11lorobcnzcnc ______ _
1,2-dichloroctkme
1,1-dichlorocthylcnc ______ _
2,4-dinitrotolucnc.
heptachlor
hc.xJch lorobcnzcnc
hcx,1chlorobutad ic nc
heXJch!oroc.thanc
methyl ethyl ketone
niirobcnzene
penlachloropheno!
pyridine
let r achlorocthylcnc
trichloroethylenc
--2,4,5-trichlorophcnol
--2,4,6-trichlorophcnol
------
------
--vinyl chloride -------
cndrin
!indanc
mcthoxych!or
tox:Jphcnc
2,4-D
2,4,5-TP (Si!';cx)
/ .
~·"',;,-:; of Environment,
~,,,;,--& r<;itur~I Resources
_,oJid Waste ManJgc.n_1cnt Division
• .:;A.t\1PLE ANALYSIS REQUEST Scale LaborJtory of Public Hc!::h
1'.0. noi !S(}.:7, 3C<i N. Wilmington _Slr~~l
f/..aki~h, Norih Carolina 276ll
Sile Number_ C0-004-SL 03/06/96 1205 GRAB
Cherokee Oil Coopany, NC
STAINED SURFACE SOIL AREA 13
✓umber ________________ _
DOUG MOORE
Name of Site ESD LAB EXT/PEST Soil
co-14 Collected By _________ _ d T~e : ----;:======---=--=-=-=-=-=-=-=-=-=-.
Agency: Hazardous Waste Solid Waste &..--'""" Supcrfund
Sample Type
Environmental Concentrate Comments
-.-Ground water (1) Solid (5)
. __ Surface water (2) __ Liquid (6) ____________ _
V Soil (3) Sludge (7) __________ _
_ Other (4) Other (8) ___________ _
Organic Chemistry Inorganic Chernistr)'
Pam meter Results (mg/I)
Radiochemistry
P,1ramcter Results (PCi/1)
__ Grnss Alpha ______ _
Gross Bet3.
Microbiology
Results (Col/l00ml)
Pam meter
Arsenic
B:1rium
Cadmium
Chloride
Chromium
Copper
Fluoride
Iron
Lead
Results(mg/1) (mg/kg)
__ Manganese
__ Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
pH
Conductivity ______ _
TDS
TOC
TCLP Compounds
Inorganic Compounds
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Organic Compounds
benzene
Rcsults(mg/1)
Rcsults(mg/1)
carbon tetn1chlori<lc ______ _
chlordane
chlor:obcnzcnc
chloroform
o-cresol
m-crcsol
__ p-crcsol
crcsol
1,4-dichlorobcnzcnc ______ _
1,2-dichloroethanc
1,1-dichloroethylcnc ______ _
__ 214-dinitrotolucnc.
__ heptachlor
hex:ichlorobcnzcne
hexachlorobutadicnc ______ _
hcx.::i.ch)orocl ha nc
methyl ethyl ketone ______ _
nitrobcnzcnc
pentachlorophcnol
__ pyridine
tel r a ch lo roe th ylcn c
trichlorocthylenc
--2,4,5-trichlorophcno! ______ _ = 2,4,6-trichlorophenol
__ vinyl chloride
end fin
lindanc
mcthoxychior
toxaphcnc
2,4-D
2,4,5-TP (Sd·:cx)
5rATE LABORATORY OF PUBLIC HEALTH
PO BOX 28047-306 N. WILMINGTON sr., RALEIGH.. NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGE.ABLE COMPOUNDS LAB NO 9lP.Y':P<f • }. C. %"'ll'Il'iJ 'filffiJ:4-6 '{l_(JF/50 'l!.'l&>"';:, 5 .;:i_
FIELD NO I co-+ c,o-7 CO -I 0 I CO-/ 3
COMPOUND TYPE ( 3 l (3 l (3 I ( 31 ( 31
M~S)5 /ppg ppm
'
Cppb ~b ppm ,;,pb)ppm /ppb'},pm 'ppb pp;n
,• ii !/ CHLOROMZTHA."f!: JO f.L I ,, I 1 I 1
I
I
VINTI. CHLO RID!; 10
BROMOMJITBA.'C!: d.0
cm.a RO rTHAlf?: 10
TRlCHLOROJ"LUORO~ /0 ' ' I 'I I /
ACITOlfl: .;20 /0~ J !J J',L }O(J) J ;;t;;i.7 :r
l.l·DICHLOROETBZ!'f!: 5 I 1 I) I 1 I
tODOM'.l:I'llA.!'I' J/ J,
lilTHTU:O: CHLORID!: 7 ;,,c.. .3 :,,c..
CAR.BOl'f DISUU"IDE {.,L-I
TRA1rS--1.2•DICHLORO l!:THLU: /
== ;;!.D ' I \/ ' I
l,l•DICHLOROrrHAIU; 5 (p CJ ;; :r
:l-BOTAl'l'.Ol'B ;;)_[> /..o -:s 5-s /9i :r
C::,..l_:l..DICHLORO~ 5 .3,;;i_ +ra.c.e__ -1-Yn,~
cm..oaoroR.M lL-+race_, frme..-
1.l,l•Tll.lCHLOROETHA1JJ; 9 ;i. ::r +--,-n, P
CARBO!'( n:TRACHLORIDE U--I I LL
= If J ,;1_ J u,
1.;l-OICHLORO~ +,n,P. L-L +rn,,o
TRicm..0RO~ 31 /J +ro..c.e..,
l..l·DICHLOROYR.OPM'l: LL u..... LL
l!ROMODJClil.OROJa;TIL,\/(l; ' /
' I J, 'I J/ f-rn rP
-C .Po~,a~ W\6 C.Cl'fTl'\M1t-lf\T\o~ OR 8AcJ::.CtR.cuND,
J -J:atim.atad value .
~ -Actu&.l val.u• i• lc:c.owc. to b• l••• than Tlllu• givon.
L -J.c:tual Ya.lu• i

■

knawu to b. gr•ater than valu• given.
U' -Xa.teria..l waa a.na.lyz•d !or but not d•t•cted. Th• number i• th• Mini=:u:a. Detection Lim.it.
ID. -5ot a.1:1.11,ly:i:ed.
'J:/ -Tentative id•nti!ic:ation.
~I -C"r,l,!'01.<l'IO ,RE.Ul'\BL'f·D£TECT'fl0Lc 0/JL'/ IN Hl!rH coNCOlTRATlc>,15.
V-SAMPL~ 1-IH,HL'{ 01L..4TED. MOL1j Do NOT APPLY,
DEHNR 3065-0 (10/93)
(j)
q~/15'-/
co -1 G
I 31
1-Prb) 01;n
le.-I
'\ I/
P'URGCOM.ORG
I
I
STATE LABORATORY OF PUBLIC HEALTII
PO BOX 28047 -306 N. WILMINGTON ST., RALEIGH. NC 27611
ORGANIC CHEMICAL ANALYSIS
PURGEA.BLE COMPOUNDS UBNO 1i1.!J11~•(,Ili-• Wil"J/ilii~ C[[plJi{W_,· q<EiJ5cY· qJ§)lf/'S;;)_,
FIELD NO I co-+ CD-7 co-,o L0-13
COMPOUND TYPE (3) I 3) ( ) (3 ) (3 )
i n,~F; /ooti)pom ppb)pp111 ppbJpf""' (ppb')pprn 'ff'b ppm
DIBROMOw.rraA:a: 5 { I [..(_ IL-, I,
4--)a;l"HTL-Z.PEN'l'Al'fO~ ,o
CIS-1;3-DICBLOROPROP?:N"J; 5 , I •'/ J.,-
TOLUE..'{?; i 3oC/ ;;J.7 //10
TRA.l'fS,..l..3-0tCHLOROP"R.OP?::'f!: I, u___ I '
i l, l ,:l,:J. T'?:TRACBLORO t:THAlQ: . J,,, I
I 1.1.l-Tltlcm..oRO ETilA."11: ' / +rare_. ..J,,.-
l-~"0M?; /0 •I I , i-f-'JV
T?':TilACHI.OROl!:TH!::U: 5 30(.(l -/-rru e.., 7
DmROMOCHLOROw:rrRA,."11!: I ' I , LL.
ETHTt.r.n: DmROWID!'! ]; ,/ ,
CHLOROer.ar:::rn: I I -lr=-e..
1.1.1,.;l--T?:TRACBL0RO ~ l.-L.. LL-. /
mm. ,u;:m;,a: ,;) 3'-/-./-rnce., ;;). '7
nu:=s I II '-2 'f :I ld-5
= ' I I, {_)_ I
BR.OKOF'Oall /0
"'nlA1m-1. 4--DICHLORO-l--BUTZ::rt; 'lo
l • .:Z,3-TIUCHI.ORDP'ROPIIJ'("£ ,5 I/
1.4-DlcmAROB!'!~ ,:}..O ' I
\ ,,
1,2-DICHLOROB!'!~ . , 51 -1-r()..LP +ra.c.a
l.l-Dt:BR0140-:S-CHI..OROP'ROP Amt ;it> {)____ LL LL
VINTI. A.a'TATE ;MO . I, ,I;
/l-lc+A--1-+-b,,.J. .. I e.JJ..--5 'I; ' I ·, / ~ s fra.cf'
I ,1 .J-ot -lo" A',, (!JIG (-1 (-F) 8 ( +-( +)
5~b::,t-,h.ded 6enz,n1''
c -P~~eLE. Lf\8 CcN11=H.l1tJATloN oR BA.c~C;rRouNo.
J -Xatimated TlU.u• •
JC -J..ctual va.lu• i• known, to b• l••• than v..lu• given.
L -J..ctual va.lu• i• lt:ncwc. to be gr•at ■r than Vlllu■ giV"■n.
O' -)laterial wa• an.a.lyud tor but not d•t•ct ■d. Th• number i• th• Minimum. Det ■ction Lbrlt. ·
n -Rot an.a.lped.
1/ -Tentative id•ntitication.
'it -COMPoi.Lt"D-l<ELIP.BLY oi;11:Cf'.F\'aLE tl.JLY IN Hlu-H CONCENTRAnoN.:;.
,/-SAl'lPL!o H16-HLf DILuTEo. ,'-\DL'o Do Jv;JT" APPL'/.
DEHNR 3068-0 (10/93)
9lPJ 15'-/-
C0-1/.J;
I .3l
'ppbjppm
I I
./
PURGCOM.ORG
"",,.
STATE LABORATORY Of PUBLIC HEALTH
P.O. BOX 28047 -306 N. _WILMINGTON, ST., RALEIGH, N.C. 27611
BASE/NEUTRAL ANO ACID LAB NO
EXTRACT ABLES FJELD#
COMPOONO TYPE
UNITS
/ nltrosodimethvlamine I'!/;;>~-
1 is (2--ch loroethv I) ether
!-ch l orNiheno l
lhenol
I 3--dichlorobenzene
I 4--dichlorobenzene
l 2--dichlorobenzene
Jis(2--chloroi l )ether
1exach loroethane
~ ni troso--di-n...nrrvwlamine
1i trobenzene
jc,v,,horone
~-nitNY'lhenol
2 4--dirrethvlphenol
)is(2-chloroethoxv)rrethane
2 4--d i ch 1 o......v1heno l
1 2.4-trichlorobenzene
1.lnhtha 1 ene
1exachlorobutadiene
~-ch l oro-m--creso 1
1exachlorocvclooentadiene
2 4 6-trichloNV\henol
2-ehloron~nhthalene
a.cenaohthvlene
dirrethvl ohtha late
2 6--dini trotoluene
a.cenaoKthene
2,4--dinitroohenol
2 4-dinitrotoluene
4-n it N'V"'lheno l
fluorene
4-chlo=henvlnhenvlether
diethvl ohthalate
4 6--dinitro-o-cresol
diohenvlcnine
dZobenzene
4--bl"'n'TYY'lhenvl ohenvl ether
hexachlorobenzene
r,.ontachlornnhenol
Dhenanthrene
anthracene
dibutvl ohthalate
fluoranthene
J -Estimated value.
SO.//t. <"o
I,.,/. -r.'10
s-o/ii.<:o
10/no
,
'l'Q "-'~ 10, .330
I
I
V
so/11,.:ro ,,, / ,,,,...
' m1>L
l{,.o/.sot J..
ORGANIC O<EMICAL ANALYSIS
Uf;'JII'-/.\ 1qtn/.fl-'7-' ICIJ~'Jf• (/.Cj
,;;) t'o -:s-lo-;,
(.51 r i1 ( :a \
.--.l.,Y ""/ka ·"' ~ m,-.. o/~
; -' . A -
I
LJ-1,. I
IA-
I
" ,-C, 1--'
II'-
I
\
;;/ -OK ,,
I
1, L r, ,
'I <A ,.
' I I. 1..3 ) /
-? 1-oO
K -Actual value is known to be less than value given.
I Cffi?ll,"-1 ··,;
Co-I I
( 3,
,m-ti ""/kn
IA -
I
L/oo
v<--
I
'
--< G, 7 ,,
L-<--
":(;;/QY
IA-
I ,
--JI
-?:,,,-,i,-
~
,
' ~ , :.;
I J ,. -1
L/4-
/9"1J7' ,
,,Y:l,"1/15,:;,
,10-1<1
( ;;/ \
~ .. q/kq
, -
I
~'.2./"\V
u__,
/
' -1 \oV
v<-
v<-
-'l '"v
V--,
' ::,, '.30~ . . .
/
\
I . -,.., ... ,,-_,.--,
, A , .c, 7
I -,:Z._ ,onr-, ,
L -Actual value is known to be greater than value given.
U -l'\aterial was analyzed for but not detected. The nt.JTOer is the '1ininun Detection Limit. mIJL
NA -Not analyzed. ----
1/ -Tentative identification. ~/ -On NROC List of Priority Pollutants.
C)
'If,,/ /_ZC:..,
?10-17
( :()
.....,.,..,/" 1-1Q/l(n'i
'
. .
-::z-I) I,'
' '
I
"'3 C Qkc
V'--
J
' ., -. ,,
~ ;:1;, lc'
0--4, A:,, -',
'
STATE LABOOATOOY Of f'UBllC IIEAllH
P.O. BOX 28041 -306 N. WILMINGTON, ST., RALEIGH, N.C. 21611
ORGANIC rnEMICAL ANALYSIS
BASE/NEUTRAL ANO ACID LAB NO ! w, ;,~, /_I.J-.., ?,7/!:!J I:~~/ C,/,:.>//fi.t.L.'i; <-_If;/ j,,7-/ I
EXTRACT ABLES FIELD # 7 /1,-,_) r'n• ·J? ,,,.,_//
CX\'1f'OONO TYPE ( ., ) ( ..,-1 ( "3 ) (31
UN[TS 1...,,,,d uo/kQ i --,,e;/, , o / k o -~ .. n/ko •~uo/ka
nvrene /o/::ion ' ...,-,f;. -{ I :-J/,.,/1-',
benzidine '"'" ltbSO
, j A vL-
butvl benzvl ohthalate /01 '<30 v "'00 LA-
benz (a) anthracene 1,,1..., ,;:i, I,& I
chr'lseoe ... ;;l ilr. ·1 ,l ~ '.< ~
3 .3-dich lorot>enzi dine .so it.<'o -L,'-.-, ,,
bis {2~thvl hexv l )nhtha 1 ate 'Jo, ·:,30 -o {'< " q,uv
di n-octvl nhtha\ate 110/.130 ,I'-<~ '//4.-
benzo(b) fluoranthene sol,-.on J' ,o •"/ ·-s7.7~ '-'(
benzo fkl fluoran thene I I A--,,_ -
benzo(a)nvrene :::; I '17) -5"&,' 00
indeoo(l 2.3-<:d'nvrene I 700 < ,., 2 ~
dibenzo(a.h)anthracer,e / , !,(.., / ...,, ·::.:1
benzo(a h j\n.arvlene ', I '-I.I'>~ ' I 1., c!O ,
ani 1 ine <c,ln.Kro 1,,1 ~ (/(._., I A -LIL
benzoic acid
benzvl alcohol -,
4-chloroani 1 ine " ,, ' I '
dibenzofuran 10 /Z-?11 :::i::ioi::... '3,?()k'..
2-methv\runhtha ler,e -< x';; -s I 2.&'I
2.....,thvl oheno I ' • I
4-<nethvloheool ,,
2-n i troan i l i oe S'O ,,,_,o
3-<li troani 1 i ne
4-ni troan i 1 i ne / , ,
2 4 5-trichlo,..,.-y,heool ,:, I ' ' ' I
---~
1-1 v ,,PoC ,qr ,q ou, --1-/-{ ) r ..J-> { -) ( --t-' ) --
mni..
J -Estimated value. H2.0/ Soll.
K -Actual value is known to be less than value given.
l't/;;>, /. -,. <
I' 0-/<.,I
-s
~ /ko
...,, 2 1 -s
' ,
130 1.1.-1 ;,
II. nQO
, t,JL..
r/()", -'\'?SI
' : -
I ,O, 000
'I,,(_
IJJIA&, I
/'1/J 1./,1 /
JI ;; 3 ~
J:2-,< ":J,,IA/
v{__...
/
' -s ~ /JV
. -3 v,I"
I
I
' ~
( _J... I
L -Actual value is known to be greater than value given.
U -~terial was analyzed for but not detected. The nurber is the Mini1TUT1 Detection Limit. ~
NA -Not analyzed.
1/ -Tentative identification.
~I -On NROC List of Priority Pollutants.
11/6//. ~-.
lr'0-17 r-..3,
1.7nd 11n/kq \
<:;"ooo ,,
' L •
la TSU
I h ,z .,
V-
/'1."->'3-i
I,<-
J'-1 z-,;.,
,.'.,(
,,;;.. 0~ ~
,,.: /,.,(,.,-/
-, ,
..:i /,200
t,/\.. ~
,
' -
( .L)
'--c.-'
• _,.:!'.-;;:;',,-;;cnt ,:.I En~ironr.1cn!,
! [,:~Ith, ,I ;,.;;ilurJ\ Resources
S01id W:istc MJ11~gc:iicnt Di~i5i•:in
SA.iv!PLE ANALYSIS RE(',JEST
Site l'filmbcr
Name of Site
C0-001-SL 03/06/96 1501 GRAB
Cherokee Oil Coopany, HC
BACKGROUND SURFACE SOIL
EID LAB METALS Soil
DOUG MOORE Number
• S1J1c [,..1bo:-.11or1 u! Public HcJith
:'.U no.t 2$().17, JC<i N. Wilmington .Sin:~:
Raki~h, North Urolin! 27611
----------------
Collected By_ 3 C:d Time _ ___ ...,..,,., ..__u,1\,;\..l __________ _ _____ _
Age:icy: Hazardou.~ Waste Solid Waste V Superfund TCL!' Compounds ----
Sample Type Inorganic Compounds Results(mg/1)
Environmental ConcentrJte Comments V Arsenic < c_ ~ \
✓Barium u _59 --__ · Ground water (1) --Solid (5) V--Cadrnium ..ca ,95
VChrornium .-::'...hl-05
__ Surface water (2) _ Liquid (6) vLead -i...~-, .. \a
✓soil (3)
v-ivfcrcury .<:'..c,cj
_ Sludge (7) V Selenium _.L. t} II("' C 5:
V-Silvcr <o-DS
_ Other (4) --Other (8) ✓ l~ee~y .L... O .. c~ ~ "2-t...., c...-0-07 --
--Orgnnic Chemistry Inorganic Chemistry --
Parameter Results(mg/1) Parameter Results.,..) (mg/kg) Org,1,nic Compounds Results(mg/1)
P&T:GC/MS V Arsenic J,8 benzene --VBarium --Acid:B/N Ext. ) 1,'-i carbon tetrachloride ----MTBE V Cadmium ..c:. ,a chlordane ------Chloride chlorObenzcnc ------
--V-Cbrornium :i.:i chloroform --
--V-Copper .;,':\ o-cresol --Fluoride m-crcsol --------Iron __ p-crcsol ----V-Lead ·:r 0 crcso! ----__ Manganese ' 1,4-dichlorobcnzenc ----
--~Mercury < Q, / 1,2-dichlorocthane --
--Nitrate I, 1-dichloroethylcnc ----✓Selenium -< \ 2,4-dinitrotoluenc .
,,,,.-silver .l... i C: __ heptachlor --
Radiochemistry Sulfates -hcx.'.lchlorobcnzcne ----~Zinc 5lo hex:\ch!orobut ad icne ----Parameter Results (PCi/1) --pH --hcx.'.lchlorocl hane
__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobcnzcnc ------TOC pentachlorophcnol . , ----
----pyridine
!vlicrobiology ----let r Jch !o roe th ylc n e
trichloroethylenc --Parameter Results (Col/l00ml) __ 214,5-trichlorophcnol --2, 4 ,6. t ri chi oro phcn o I ------\'1nyl chloride ------endrin --lind:rnc
Date R::::c:ivcd --mctha:,,,)'Ch!cr Reported by --tox:iphcnc
Date RcportcdJ.1-~
--Date Extr:1Clcd 2,"-D --Q0]4,14 i!d, } --2,4,5-TP (S,!·.•cx)
D<![C ,"-,r,;1!~-/.Cci L1f~ Number ---------··--·-··-·-· -------"' ,,. ------------------------------
I
• ,..,:p;-;;tr.icnt of Environment,
·r i~Jllh, J.:. /'."JturJl Resource~
Solid WJs1c Managc.~cnt Division
SA.iv!PLF: ANALYSIS REQUEST
Site Number CO-OOl-SB 03106196 l5l5 GRAB
Cherokee Oil Coopany, HC DOUG HDORE
Number
BACKGROUNO SUBSURFACE SOIL
EID LAB HETALS Subsurface Soil Name of Site
• S1:itc l..:ib?r.11ory o( Pu_:,:: H::i1h
P.O. 801 :?.SOJ7, Jf.,6 :''· Wilm;~.gton _Sl!':.~:
R.a!cit:h, Nor.~ Carolina 27611
----------------
co-9 Collected By _________ _ ____ -----~,cd Ti.me ----------------------
Agency: Hazardous Waste Solid Waste V Superfund TCLI' Compounds -----
Sample Type . Inorganic Compounds Results(mg/1)
Environmental Concentrate Comments VArsenic .L.._,e_c/
,.-,/Barium Q -"l':l:
__ Groundwater (!) _ Solid (5) v· Cadmium L-o.s;:25
_LC Chromium -"'-o.oS
. __ Surface water (2) Liquid (6) ~Lead L-0-\C,
/soil (3)
i..-----Mcrcury -< C .. cl
Sludge (7) ~Selenium .L..c_cc5 -,._,,.-Silver .L...C.; a :S
_ Other (4) _ Other (8) v-'r~e,e.cv :--!--O_c,~
,/" "2-,i,c b • 1 d--.
--Organic Chemistry Inorganic Che~istry --
Parameter Results(mg/1) Parameter Result-. s,'l!'(mg/kg) Organic Compounds Results(mg/i)
--P&T:GC/MS V Arsenic ':\ ., ':l be;-i.zcnc
✓Barium --Acid:B/N Ext. t..8 carbon tetrachloride ----MTBE v·cadmium "'-,a ciilo,dane ------
Chloride chlo"robcnzcnc ------
--V Chromium .30 chloroform
V--coppcr --
--5.'.), o-crcsol --Fluoride m-crcsol ------
--Ira□ p-crcsol
?..n ----v-1.ead crcsol --
--__ Manganese. --1, 4-d ic h 1 a robcnze n e
--v' Mercury < 0, l --1,2-dich lo roe th anc
--Nitrate 1, 1-dichloroethylcnc --~Selenium ..,_ ' --2,4-dinitrotoluenc.
~Silver "'-10 -heptachlor ----Radiochemistry Sulfates -hexJchlorobenzcne ----~inc ~2. hexachlorobut adienc --P;irnmetcr Results (PCi/1) pH hcx.::i.chlorocthane ----__ Gross Alpha --Conductivity --methyl ethyl ketone
Gross Beta TDS nil robcni.ene ------TOC pentachlorophenol . , ----
----pyridine
Microbiology ----t ctr ach lo roe th ylene
--__ trichlorocthy!enc
Parumctcr Results (Col/lO0ml) 2, 4, 5-trich loroph en o I ----2, 4,6-trichJorophcnol --------= v-inyl chloride
endrin --lindanc --Date Received rncthoxych]or Reported by --tox.Jphcnc --1);1\c Extr:..ictd Date Rnrrtcd M,',R B 9b 2,<-0 ,01~;t6 --2,4,5-TP (Si!.•cx) --Dr1lc An:d:,,1cJ Lih Number --····--------------••1••: ,,::• --···--· ----------------·--···-· ----------
·r',ift111cnl o( Environ111~n1,
. 1cii·i";-h, l: r--.:atu~al Rc~ourcc~
Solid Waste ManJbcr.:icnt Division
• SA.1v!PLE ANALYSIS REQUEST • ScJtc l,;iboro.tory o( Public Hc~lth
!'.(l. 0Jx :?.SO-.?, Y.Xi N. Wibinvon .S!n:ct
R.alcit:h, North Grciina 276ll
Sile Numbc1 C0-002-SB 03/06/96 1150 GRAB
Cherokee Oil Company, NC DOUG MOORE
Number ________________ _
Name of Site SUBSURFACE SOlL AREA 11
ESO LAB METALS Subsurface Soil
Collected By_ co-6 d T~c -------' ------------------
Ageocy: Hazardous Waste Solid Waste V Superfund
Sample Type
Environmental Concentrate Comments
--Ground water (1) Solid (5)
__ Surface water (2) --Liquid (6)
V Soil (3) --Sludge (7)
_ Other (4) --Other (8)
Organic Chemistry Inorganic Chemistry
Parameter
__ P&T:GC/MS
__ Acid:B/N Ext.
Results (mg/I) Parameter
-~Arsenic
✓Barium
,/'Cadmium
Results~ (mg/kg) a <.;;
MTBE
1 Chloride ===-----------7Chromium
v"Copper
Fluoride
. ---------------
·------------Manganese
v--r;1ercury
Nitrate
VScle ni um
,------------------j v"Si!ver
Radiochemistry Sulfates
1----------------1 ✓Zinc
!'ammeter Results (PCi/1)
__ Gross Alpha ______ _
Gross Beta
Microbiology
Parameter Results (Col/1001111)
_pH
__ Conducti\11ty
TDS --TOC
-30
/. ?
Date Received _________ Reported by _________ _
TCLP Compounds
Inorganic ~ompound.s Results(mg/1)
VArscn1c 4,c.,,cl
~ Barium c,. 1 5
vCadmiuru --<-o ,u"'J
V Chromium ~ o ... c:,;5
~Lead ---'--~P~-~·~, o=----
V---Mcrcury L.. c _ Ci
,._,/Selenium _ -4...~. e:. c..3·
V Silver ...:=:'... o ... q5 7 &ff?C ..,; c.65
,/ HrlC c. 3;:J,
O~anic Compounds
benzene
carbor, lctrachloride
Rcsults(mg/1)
---------
--chl9rdane
chlorobenzcne --chloroform --o•creso! --m-crcsvl --
--p-crc.so!
crcso! --__ 1,4-dichlorobcnzcne
__ 1,2-dichloroethane
---------
-··--------
__ 1,1-dichloroethylcne ______ _
__ 2,4-dinitrotolucnc.
__ heptachlor
hcxJch lorobcnzcne
hexachlorobut adicnc ---------hcx.:ichlorocthane ----methyl ethyl ketone
nitrobcnzenc ----pentachlorophcnol
__ pyridine
__ tetrachloroethylenc
__ trichloroethrlenc
2, 4 ,5· tric h lo ro p hen o I = 2,4,6-trichlorophcnol
__ vinyl chloride
endrin --lind:i.nc
__ mcthoxych!or
__ tox:iphcnc
2,,-D = 2,~,5-TP (Si!·ct.;:<)
• ..:6";·rtr.icn1 of E:,·.'\:-:;,1men[, SA.!v!PLE ANALYSIS REQUEST .. -. 1·lcal1h, cl 1"'-'.a1url! Rcsoun:cs
Solid W.is1c [\!:rnl~cr:i.:r,! Division
Site Number C0-003-SB 03/06/96 1140 GRAB
DOUG MOORE Cherokee Oil Company, NC
Name of Site SUBSURFACE SOIL AREA 11
-ESD LAB METALS Subsurface Soil
Number
• Sillc l..:1bor.1rnry of Pubtk Hc~\th
r.l.l. flol ~7, JCS N. Wilmingtor. _Stri:~:
Raleigh, North Carolinn 27611
----------------
Collected By _____ c_o_-____ 12 .ed Time -----------------
Agency: Hazardous Wa.Ste Solid Waste /superfund TCLP Compounds -----
Sample Type Inorganic Compound!i Rcsu I ts (mg/I)
Environmental Concentrate Comments ✓ Arsenic -c:::..c.,c I --V Barium \_ 'J,J
__ Groundwater (1) Solid (5) ---1.L Cadmium -<-0-05 --~Chromium -"'-O.o5
__ Surface water (2) --Liquid (6) V-Lead --"--a-,o --v-"Mercury L..c .. cl
VSoil (3) --Sludge (7) V""' Selenium .t...c.,caS:
&..-""" Si!ver <o.o5
_ Other (4) --Other (8) -&ee-L.c .. o~ v-:::Z..#'1 C. b-o":;j --
--
Organic Chemistry Inorga·nic Chemistry --
P:.:irnmctcr Results(mg/1) Parameter Resul~ (mg/kg) Orbadc Compounds Rcsu I ts (mg/I)
__ P&T:GC/MS V Arsenic J, ben7.cn::: --Acid:B/N Ext. ✓ Barium \d:, 'i carbon tetrachloride ----MTBE V Cadmium -<..IQ chlordane ------Chloride chlorobenzcne ----✓Chromium ?i,8 chloroform --...,.. Copper "-\le o-crcso! ----Fluoride rn-cresJl ----Iron p-crcsol -,-----..,,-Lead 'J_,\ crcso! -------
--__ Manganese --1,4-dich lorobcnze.nc ----vMercury C: 0, i --1,2-dich loroethane
--Nitrate 1, 1-dichloroethylcnc ----VSdenium .. q --2,4-dinitrotolucnc.
,...-Silver -<.lC ... heptachlor ---Radiochemistry Sulfates -hexJch lorobenzene
✓zinc -'-1 ':l --hexachlorobut adiene --Parameter Results (PCi/1) pH hcxachloroethane ----__ Gross Alpha __ Conductivity --methyl ethyl ketone
Gross Beta TDS nitrobcn?.enc ------TOC pen! achlorophcnol ; ; ------
--pyridine
l'\'licro hiology --
----tetra ch l oroc th yl en e
Parameter Results (Col/l00ml)
__ trichlorocthylcnc
__ 2,4,5-trichlorophcnol
----2, 4,6-trichJo,ophenol
----\1nyl chloride
endrin --lindanc
OZttC Received --mclho:,...ych!or Reported by --toxJph:.:nc --Date Extr:tctcd Dille Rcrorlcd 2,4-D
00 J ~ ,fl1ii'Jf 6 ~ 6 --· 2,4,5-TP (Si!·.·cx) --O;itc "An;ily-Lcd L:ih Numbcr --"; "-: , : ·;. _.,, .. -··----·-·------· ·--.. ... ---·-. -~----··--·---
• vc·p;rtmc:n1 o{ Environr:1tn1,
I l,;:il!h. J.:. /',:Jtur:il R,~ourcts
s"o1id W:11tc Man~gc~cnt Oi~ision
SAi'v!PL:C~ Ai"iALYSIS REQUEST
Site Number_ C0-004-SL 03/06/96 1105 GRAB
Cherokee Oil co,pany, NC
S!AINED SURFACE SOIL AREA 13
Name of Site ESD LAB METALS Soil
Number
DOUG MOORE
• Si:.:::. !_;ib-~:--~io1y cf Public Hc~ith
r.u. nox :sc.:-:, }-'.1/.: \'. \!/ilmi;i~{Qn _Sl~cl
Rakit:n, North Caro'.ine 276ll
----------------
co-15 Collected By __________ _ .ed Time -----------------
Agency: Hazardous Waste Solid Waste V" Superfund TCLP Compounds -----
Sample Type Ino~anic Compounds Results(mg/1)
Environmental Concentrate Comments V Aiscnic "'-.c cl --' v Barium (.J, l· +-
Ground water (!) Solid (5) V Cadmium < [,,Q ,---VCbromium < 0, c,,
Surface water (2) _·_ Liquid (6) v-Lead (; J '2 0 ----Vrvfcrcury L.. a .o) ✓soil (3) _ Sludge (7) V-Selenium -· < ~-cc5
. V Silver ::;:: Q, t\ \
_ Other (4) --Other (8) ✓ Ce,pp-,.--:S:: O, C ,I
~z_.;,,,_ ':/..]:_~
--Organic Chemistry Inorganic Chemistry --
P;.irnmetcr Rcsults(mg/1) Parameter Resu1f'"C g,111 (mg/~) Organic Compounds Results(mg/1)
P&T:GC/MS V Arseillc d.5 benzene ------Acid:B/N Ext. VBarium ,'\o carbon lctrachloride ----MTBE ,,,,,,.,,,.-Cadmium L_ 9 -6 chlordane ------Chloride chlorobenzcnc ----55 --V""'"Chrornium chloroform --
--.,,-,--copper 55 o-cresol --Fluoride rn-crcsol ------
--Iron p-crcsol --
--✓Lead ',L S::o crcsol --
--__ Manganese. --1, 4-d ich Io r obcnzene
--,./Mercury 6, l 'J... --1,2-dichlorocthanc
--Nitrate 1, 1-dichloroeth ylcnc ----,..,...--Selenium -<. \ --2,4-dinitrotoluenc.
,..........-Silver L. 9 .8 heptachlor -----
Radiochemistry Sulfates -hexach lorobcnzcne ----v"Zinc G, cc hexach!orobut ad icne --Parumdcr Results (PCi/1) --pH hcx.:ich!oroel hanc --__ Gross Alpha --Conductivity --methyl cthy! ketone
Gross Beta TDS ni1robenz.enc ------TOC pentachlorophenol . , . ----
----pyridine
Microbiology ----let r a ch lo roe th y!e n e
trichlorocthylc□c --Parumetcr Results (Col/lOOnil) __ 2,4,5-trich!orophcnol --
------2,4,6-t richlorophcnol
------vinyl chloride
endrin --lindanc --O;:itc R(:ccivcd Reported by mc(ho>.)'chlor --tox:iphcn:; --D:1tc Extri.lcld Dute Reported 2,o-D --(]0}~1.':.\ fPt'J B 9 ii 2,4,5-TP (Si!·.•c:c) .1:,1\ --D,1lc .~.n;1!y1.r:.J L:ih Number -·-··--··-·-···--· ··--·-····-----------·-·----·-·--------------·-· :••· -
State of North Carla
Department of Environment, Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L Meyer, Director
March 18, 1996
Gene W. Hartsell 10688-058
Caller Box 8004 Sandhills B
FPC -Seymour Johnson AFB
Goldsboro, North Carolina 27533-8004
Subject: Administrative Search Warrant -
Cherokee Oil Company Site
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
Dear Mr. Hartsell:
Enclosed please find a copy of the adininistrative search warrant served by the NC
Superfund Section on Wednesday, March 6, 1996 as part of an environmental site
inspection of the subject site. At this time, one surficial and two subsurface soil samples
were collected at the site and submitted to the State Laboratory of Public Health for
volatile organics, semi-volatile organics including PCB/Pesticides and inorganics
analyses. A copy of the analytical results from the soil samples collected at the site will
be forwarded to you following receipt. If you have any questions, please submit them in
writing to myself.
cc: File
Rob Gelblum
Pat DeRosa
P.O. Box 27687,
Raleigh, North Carolina 27611-7687
Voice 919-733-4996
Respectfully,
Douglas Moore
NC Superfund Section
FAX [phone]
f#ffidi/,'J@.hD
An Equal Opportunity Affirmative Action Employer
50% recycled/ I 0% post-consumer paper
,. • ' ,..... _______ .....;._..;.....;. ______ ....,. ____ _._ ___________ _
STATE OF NORTH CAROLINA
In The General' Court Of Justice-·
__ Me_c_k_lenb_ur___;;g;__ ____ County
[See Attached Affidavit;}
AFFIDAVIT TO.OBTAIN' -· ·--. '
ADMINISTRATIVE INSPECTION' . -
WARRANT FOR PARTICULAR
CONDmON OR ACTIVITY -·
I,_....;. ______ ..;·'-··_------'-----------------' being , --, .. (-your-• position}
duly swom and examinined under oath, state under_ oath that there is pn)bable cause for belleving that there is
(dssat>e condlian, ob/fJt:I. at:/ivlty, or...,.,_ wit/ch thlJ-.r:h s lnlardsdlD-orl8ll88/.J
at the property owned or possessed by
and described as follows: --------------------------
(pn,cise/y dssaibe the~ ID beb-,,ecmd.J
The facts which establish probable cause to belleve this are: ________________ _
1Sf9,lalln Of App/leant
SWORN AND SUBSCRIBED TO BEFORE ME
Dais
Asr/stantCSC DeputyCSC
0 Mag/sbal& · su,,,,,tor Court
Cle1c Of Superior Col.Vt D -D1st1ct eoutt
IMPORTANT: Attach the Affidavit ID the WARRANT if not on reverse side.
AOC-CR-913M
Rev. 7185 (Ra!>rinlad 1/ll3) (Over)
STATE OF NORTH CAROLINA
In The General Court Of Justice
_ _!.,:Me::;:ck=l;:;;en:.::b::.::ur=g _____ County
•
ADMINISTRATIVE INSPECTION
WARRANT FOR PARTICULAR
CONDITION OR ACTIVITY
G.S. 15-27.2
TO ANY LAWFUL OFFICIAL EMPOWERED TO CONDUCT THE INSPECTION AUTHORIZED BY THIS WARRANT:
Toa applicant named on the accompanying affldavil,.being duly sworn, has stated.to me that.there is.a conditlon, object,
activity, or cira.imstance legally justifying an inspection of the property desaibed in that affidavit. I have-examined this·
applicant under oath or affirmation and have verilled the accuracy of.the matters in the affidavi establishing.the legal
grounds for this Warrant. YOU ARE HEREBY COMMANDED TO INSPECT THE PROPERTY DESCRIBED IN THE
ACCOMPANYING AFFIDAVIT.
This inspection is authorized to check or reveal the conditions, objects, activities, or cirrumstances indicated in the
accompanying affidavt
This Warrant must be served upon the owner or possessor of the property described in the accompanying affidavit. If
the owner or possessor is not present on the property.at the time of inspection and you have made reasonable but
unsuccessful efforts to locate the owner or possessor, you may instead serve it by affixing this Warrant or a copy to the
property.
THIS WARRANT MAY BE EXECUTED ONLY BETWEEN THE HOURS OF 8:00 A.M. AND 8:00 P.M. AND ONLY WITHIN
24 HOURS AFTER IT WAS ISSUED. IT MUST BE RETURNED WITHIN 48 HOURS AFTER IT WAS ISSUED.
HOWEVER, IF THIS WARRANT IS ISSUED PURSUANT TO A FIRE INVESTIGATION AUTHORIZED BY G.S. 69-1, IT
MAY BE EXECUTED AT ANY TIME WITHIN 48 HOURS AFTER IT IS ISSUED. IT MUST BE RETURNED WITHOUT
UNNECESSARY DELAY AFTER ITS EXECUTION OR AFTER 48 HOURS FROM THE TIME IT WAS ISSUED IF IT WAS.
NOT EXECUTED.
Oats ~ rune ~~ F -~ !::JAM □ PM
Deputy csc □ SUperior Court
SUperior Court Judge . District Ccutt Judge
I certify that this WARRANT was executed on the date and time shown below.
DatsOt/:Jtacution S/gnalU9 Of l""l)IICllng Of/lcia
1
Tims Of /:Jtacution
This WARRANT has been returned to this office on the date ancl time shown below.
Oats Of Return S/gnaa.11'11
Time Of Return
0 AM· Q PM O Assistant CSC Q Deputy CSC Q C/etlc Of SuptJltor Court
IMPORT ANT: Attach ths Affidavit to ths Wanant if not on reverse side.
AOC-CR-913M. Sida Two
Rev. 7185 (Roc>rtntad 1193)
•
STATE OF NORTH CAROLINA
in the General Court of Justice
Mecklenburg County
)
)
)
)
)
)
•
AFFIDAVIT TO OBTAIN
ADMINISTRATIVE
INSPECTION WARRANT
FOR PARTICULAR
CONDITION OR
ACTIVITY
1. The undersigned is an Environmental Chemist with the CERCLA Branch of
the Superfund Section, Division of Solid Waste Management, North Carolina
Department of Environment, Health and Natural Resources appearing this day to
request a administrative search warrant for the Cherokee Oil Company Site ("site"),
1201 Berryhill Road, Charlotte, Mecklenburg County, North Carolina.
2. The site is registered as parcel #16, block #51, tax map #71 of the Mecklenburg
County Tax Assessors office.
3. The site is owned by Gene Wesley Hartsell, as recorded in Deed Book #5828,
Page #0131 at the Mecklenburg County Register of Deeds.
4. The site was formerly operated by Cherokee Resources ("Cherokee"), a North
Carolina corporation incorporated under the laws of the State of North Carolina with
its principal place of business at 1201 Berryhill Road, Charlotte, North Carolina.
5. Keith Norland Eidson was President and chief operating officer of Cherokee
and had a fifty percent (50%) ownership interest in Cherokee. Gene Wesley Hartsell
was Vice President of Cherokee and had a fifty (50%) ownership interest in Cherokee.
6. Cherokee was in the business of, among other things, reclaiming waste oil for
energy recovery and treating and disposing of oil-contaminated wastewaters, as well as
treating other industrial wastewaters at the site. Cherokee Resources used the site as a
waste oil processing facility.
7. In July 1991, a criminal investigation was conducted by the EPA Hazardous
Waste Section, the EPA Criminal Investigation Division, the Office of the FBI, and
several other state and local authorities. A criminal search warrant was served to the
owner of the site and a criminal investigation was conducted at the Cherokee Oil's 1201
Berryhill Road facility and a Cherokee Oil facility at 925 South Summit Avenue
locations.
8. As a result of the criminal investigation, Keith Norland Eidson, Gene Wesley
Hartsell and Theodore Karl Glauser were indicted on charges of conspiracy to violate
federal Clean Water Act regulations by illegally disposing of and otherwise handling
wastewaters in violation of permit limitations.
•
Affidavit for 1201 Berryhill Road
Page2
•
9. In 1991, EPA determined the Summit Avenue location posed an imminent and
substantial endangerment to public health, or welfare, or the environment. Between
August 1991 and March 1993, the EPA Emergency Response and Removal Branch
("ERRB") conducted an extensive emergency removal action at the Cherokee Oil's 925
South Summit Avenue location. The Summit Avenue location was an unpermitted
temporary storage facility operated by Cherokee Resources from August 1990 to
August 1991.
10. EPA identified approximately 6,096 drums, 13 roll-off containers of
contaminated soil, several tankers containing liquid waste and trailers containing
drums stored at the Summit Avenue site. The wastes stored at the Summit Avenue
location included polychlorinated biphenyls (PCB's), highly flammable solvents,
cyanides, strong acids and bases, hazardous organic compounds and hazardous
inorganic substances.
11. On June 29, 1994, Keith Norland Eidson and Gene Wesley Hartsell were
convicted of conspiracy to violate federal Clean Water Act regulations. On October 17,
1994, Eidson and Hartsell were each sentenced to 51 months active imprisonment which
they are currently serving at Seymour Johnson Air Force Base in Goldsboro, North
Carolina.
12. Cherokee also used the Berryhill Road site as an unpermitted temporary
storage facility housing drums, above-ground tanks, underground tanks, vats, tanker
trailers and roll-offs containing hazardous substances, including polychlorinated
biphenyls, flammable solids and liquids, strong acids and bases, hazardous organic
compounds, hazardous inorganic compounds, waste oil and sludges.
13. Many of the 2,856 drums found at the site were stacked both inside and outside
the warehouse with incompatible waste types stored adjacent to each other. A number
of containers had corroded causing the contents to leak onto the floor of the warehouse
and to the surface of the soil surrounding the warehouse. A large volume of free-
standing oily liquid and sludge covered the surface soils within three diked basin areas
on the site. In September 1994, EPA determined the 1201 Berryhill Road site posed an
imminent and substantial endangerment to public health, or welfare, or the
environment.
14. Between November 1994 and December 1995, EPA-ERRB conducted a second
extensive emergency removal action at Cherokee Oil's 1201 Berryhill Road facility to
remove the imminent threat.
' •
Affidavit for 1201 Berryhill Road
Page3
•
15. In 1990, Mecklenburg County Department of Environmental Protection
videotaped a release of an oily material leaving the site onto a neighboring property at
Suburban Propane. The historic releases may have resulted in actual or potential
exposure of workers to hazardous substances.
16. The overland runoff release was intercepted by three storm sewer manholes
where it was directed south underground to an outlet on an unnamed tributary of
Stewarts Creek ("UT"). The UT directs the runoff east to Stewarts Creek. Stewarts
Creek is reportedly used for recreational fishing. The historic release may pose an
actual or potential exposure to hazardous substances by nearby animals or food chain
species and/or human beings.
17. Samples collected by EPA during the removal action demonstrate residual soil
contamination at the site. Substances identified in soil samples from the site which are
hazardous pursuant to the Comprehensive Environmental Response, Compensation
and Liability Act ("CERCLA"), 42 U.S.C.§ 9601 et seq., include acetone, benzene, 2-
butanone, 1,1-dichloroethane, ethylbenzene, 4-methyl-2-pentanone, tetrachloroethene,
toluene, xylenes and bis (2-ethylhexyl) phthalate. Sampling of materials found stored at
the site identified additional CERCLA hazardous substances including polychlorinated
biphenyls and waste oils containing metals. However, additional samples need to .be
collected to confirm their presence in soils at the site. Releases from the site pose a
potential threat to humans and/or food chain species.
18. On Tuesday, January 30, 1996, I contacted Gene Wesley Hartsell in an attempt
to gain access to the site for the purpose of collecting environmental samples. Mr.
Hartsell stated that before he allows anyone to enter his property, he wants to inspect
the property following EPA' s removal action. He stated that he would be willing to
allow us to collect soil samples after he gets out of prison. When I asked him for a
specific time, Mr. Hartsell responded that his conviction was under appeal and that he
could be released as soon as Friday, February 2, 1996 or as late as August 1998.
19. I asked Mr. Hartsell if he could have a representative meet us at the site to
observe the sampling event. Mr. Hartsell stated that he wants to have a representative
at the site when any soil samples are taken from his property. We both agreed that he
would attempt to locate a representative and that I would contact him on Tuesday,
February 6, 1996 in order to discuss the sampling event.
20. I in fact telephoned Mr. Hartsell on February 6th, but was told by a Seymour
Johnson official named Robin Woodard, who left the phone to tell Mr. Hartsell of my
call, that Mr. Hartsell said that he would not speak to me, that his attorney had told
him he does not have to assent to our going on the site, and that he will write me a
' •
Affidavit for 1201 Berryhill Road
Page4
•
letter. Based on a call to the Fourth Circuit Court of Appeals on February 5th, oral
argument on Mr. Hartsell's appeal was heard on February 2nd.
21. On February 9, 1996, I received a letter from Mr. Hartsell. In it, he requested
copies of the statutes/regulations under which we seek access and a written explanation
of my reasons for wanting access, argued there is no basis for entry, reiterated his
position that access to the site should await his release from prison, and stated that he
wants to be present should I request access from a judge.
22. On February 13, 1996, I complied with Mr. Hartsell's request for copies of
relevant legal authorities and a written justification for access, but told him that, given
the contamination cited in this affidavit, I would be going to Charlotte on March 6,
1996 to seek an administrative search warrant and sample the site.
23. Due to the hazardous nature of residual contamination remaining at the site,
the potential threat posed by historic releases and the inability to coordinate the sampling
event with Mr. Hartsell, the CERCLA Branch requests an administrative search warrant
to collect additional environmental samples from the site as part of an environmental
assessment of 1201 Berryhill Road. The samples will be used to determine the threat
posed to human health and the environment from current or historic releases. The
assessment will also be used to determine the need for additional investigation under
CERCLA and/or other legal authorities.
Sworn and subscribed to before me.
Date
V
Douglas B. Moore
~ SttpeFi~r Court Judge
,/75 r n"tc r
•
Memo
To: File
Date: March 15, 1996
From: Douglas Moore &'!f',-/.3il,/""'-<--
Environmental Chemist
NC Superfund Section
Topic: Site Inspection -Sampling Trip
Cherokee Oil Company
120 l Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCO 980 799 019
•
On Tuesday, March 5, 1996, Douglas Moore of the NC Supefund Section departed the
Raleigh Office for Charlotte, NC. Arrived Charlotte at 16: 15 and finalized arrangements
to collect surface water, sediment samples at E.F. Lombardi Co. Doug Moore also
received permission from Jeff Meyer (or Mercer), the manager at Southern Electric Co.
across from the site, to collect a background soil sample. Doug Moore then checked in at
the Adams Mark Hotel for the night.
On Wednesday, March 6, 1996, at 07:30 am, Doug Rumford, Jeanette Stanley and Harry
Zinn from the NC Superfund Section departed the Raleigh Office for Charlotte, NC.
At 08:30, Doug Moore met with Chief District Court Judge James Lanning to obtain an
administrative search and inspection warrant for the purpose of collecting environmental
samples at the subject site. Judge Lanning reviewed the affidavit and had Doug Moore
swear to the facts contained in the affidavit. Judge Lanning then signed the
administrative search warrant and provided a copy to be used at the site during the
sampling event and a copy for our file. Judge Lanning and Doug Moore agreed that
Doug Moore would return to his office at Suite 3304, Criminal Courts Building, 700 East
Fourth Street, Charlotte, NC and meet with his secretary Pat Cheek, who would then sign
the warrant, documenting that it was served at the site. A copy of the administraive
search warrant is attached (attachment I).
At 11 :00, Doug Moore drove to the site and met with the three staff members who arrived
from Raleigh. At 11 :05, Tony Roux, Mecklenburg County Department of Environmental
P!otection -Water Quality Section, arrived at the site to observed the off-site sampling.
A representative of AT&T arrived at the site at 11:20 a.m. After discussing the sampling
• •
event with the representative, he indicated that there were no AT&T lines at the site. The
AT&T representative departed the site. No additional utilities locators arrived at the site.
Doug Moore discussed the sampling event with Tony Roux, outlining the on and off-site
sample points to be collected. At 11 :30, Team #1, consisting of Doug Rumford ("DR"),
Jeanette Stanley ("JS") and Tony Roux ("TR"), departed the site to collect the off-site
surface water and sediment samples.
At 11:35, Team #2, consisting of Doug Moore ("DM") and Harry Zinn ("HZ") walked to
the front gate of the site at Berryhill Road and affixed a copy of the administrative search
warrant to the front gate. A copy of the padlock key, previously provided to DM by John
Custance of OHM Remediation Services.was used to open the gate.
At 11 :45, HZ of Team #2 began augering a soil boring at Area #3. Soil is a red to orange,
coarse grained clay with gravel intermixed. At 2 feet, HZ encountered a dark stained soil.
Stained soil is a ash-gray to black coarse-grained clay. At 11 :50, HZ collected a soil
sample from the stained soil at the 2-3 foot interval. HZ collected VOC from bottom of
auger (2.5 -3 foot depth). The sample was then composited and collected for SVOC,
inorganics and PCB/Pesticide analyses. No odors were detected in the soil sample. HNu
readings indicated a slight deflection of the needle (0.1 meter units) in the sample
borehole. No elevated readings were detected in the ambient air above the borehole. The
sample was labeled "CO-002-SB".
At 12:00, Team #I arrived back at the site to discuss the sampling plan. Due to the rainy
conditions, Stewarts Creek is swollen, fast-flowing and hazardous. Thus, the surface
water and sediment samples originally planned for Stewarts Creek will have to be
postponed. Doug Moore told Team #I to collect the surface water and sediment samples
from the Unnamed Tributary to Stewarts Creek ("UT"), and to document the stream
conditions at Stewarts Creek and the UT.
At 12:25, HZ of Team #2 augered soil boring at Area #2. The soil profile at this location
consists of 0-4 inches of red clay, 4 inches to 2 feet of gray gravel, 2 + feet of dark red
clay. The dark red clay has a iridescent sheen. HNu needle deflection of I meter unit in
sample borehole. No elevated HNu readings in the ambient air above the sample
borehole
At 12:40, HZ of Team #2 collected subsurface soil sample from 2.5 feet below land
surface. No elevated HNu readings noted in soil sample. HZ collected VOC from
bottom of auger. The remainder was then composited in a clean pyrex pan and samples
were collected for SVOC, Inorganics and PCB/Pesticide analyses. Sample was labeled
"CO-003-SB".
At 12:30, JS of Team #I collected sediment sample CO-003-SD from the storm sewer
drainage ditch, approximately 100 feet south of storm grate near the intersection of Thrift
Road and Freedom Road. The storm sewer flows from Freedom Road along Armin
Products warehouse, under railroad spur to the UT. The sediment sample was collected
2
• •
from the 0-12 inch interval in the bed of the drainage pathway. The soil sample was a
poorly sorted, silty sand and gravel. The bottom inch was composed of a dark gray
material. JS collected VOC sediment sample from a clean pyrex sample pan prior to
compositing. Then, the soil was sampled for SVOC, Inorganics and PCB/Pesticides
analyses.
At 13:05, HZ of Team #2 collected a surface soil sample from the rear of the warehouse
. at Area #1. The soil profile consists of 2 inch of black organic rich soil with sand to 6 +
inches. HZ collected VOC soil sample prior to compositing in a clean pyrex pan. Then,
soil samples were collected for SVOC, Inorganics and PCB/Pesticides analyses. The
surface soil sainple was labeled "CO-004-SL".
At 13:35, HZ of Team #2 prepared to collect a surface soil sample from a vacant grass-
covered lot in front of Southern Electronics, directly across Berryhill Road from the site.
Mr. Jeff Meyer (or Mercer?), manager of Southern Electronics, had previously granted us
permission to collect the sample. The soil sample was abandoned at the request of a
person identifying himself as the landowner.
At 13:40, JS of Team #I collected a sediment sample from the unnamed tributary to
Stewarts Creek ("UT"), at a point approximately 6 feet downstream of the storm sewer
outfall. Due to the high flow of the UT, the sample was collected from the 3-6 inch
profile of the stream bed using a hand auger. The sediment sample was a brownish-gray,
silty clay that exhibited a pungent odor. The sediment was sampled for VOC first, then
composited in a clean pyrex pan for SVOC, metals ·and PCB/Pesticide analyses. The
sediment sample was labeled "CO-002-SD".
At 13:50, JS of Team #I collected a surface water sample from the UT at the same
location as CO-002-SD. The surface water was sampled for VOC, SVOC and metals
analyses. The surface water sample was labeled "CO-002-SW". The VOC sample was
pre-acidified using 5 drops of I: I HCL. The metals sample was field acidified to pH 2.0
using 40 drops of 50 % HNO3•
At 14:00, Team #2 met with Suburban Propane office manager Tom Broom and yard
manager Ralph Stewart to get access to the Suburban Propane soil sample locations
downgradient of the site in the overland runoff path.
At 14: 15, HZ of Team #2 collected a surface soil sample from the 0-6 inch profile in the
overland runoff path near the west corner of the Suburban Propane building. According
to the 1990 video, runoff from Area #2 was funnelled through this corridor. The top 4
inches are a dark-brown stained soil that grades to a red-orange clay. No odors were
detected in the top 6 inchs of soil. HZ collected for VOC first, then composited the
sample in a clean pyrex pan pnor to collecting samples for SVOC, metals and
PCB/Pesticides analyses. The soil sample was labeled "CO-006-SL".
3
• •
At 14:20, JS of Team #I collected a sediment sample at a point approximately 30 feet
upstream of the storm sewer outfall on the UT. The sediment is a silty fine sand. The
sediment was collected from the 0-6 inch profile of the streambed using a hand auger.
The sediment was sampled for VOC first, then composited in a clean pyrex pan for
SVOC, metals and PCB/Pesticide analyses. The sediment sample was labeled "CO-00 !-
SD".
At 14:30, JS of Team #I collected a surface water sample at the same location as CO-
001-SD. The surface water was sampled for VOC, SVOC and metals analyses. The
surface water sample was labeled ''.CO-00 I-SW". The VOC sample was pre-acidified
using 5 drops of I: I HCL. The metals sample was field acidified to pH 2.0 using 40
drops of 50 % HNO3.
At 14:30, HZ of team #2 collected a surface soil sample from the intermittent drainage
ditch that connects the Cherokee site to the storm sewer. The soil is a dark brown, sandy
clay. The soil sample was collected from the top 4 inch soil profile. The soil was
sampled for VOC analyses first, then composited in a clean pyrex pan prior to collecting
soil samples for SVOC, metals and PCB/Pesticide analyses. The soil sample was labeled
"CO-005-SL".
At 14:45, JS of Team #I prepared a trip blank in the field using organic free water and 5
drops of I: I HCL. Because of the high water level and fast stream flow encountered in
Stewarts Creek, Team # I was unable to collect surface water and sediment samples in
Stewarts Creek. These samples were scheduled to be collecting the following week.
At 15:01, HZ of Team #2 collected a surficial soil sample at serve as a background for
the area. The soil sample was collected from a grass-covered yard directly behind a
residential house located at 2415 Tuckaseegee Road near the corner of Thrift,
Tuckaseegee and Berryhill Roads. The house is the Charlotte Office of Miller, Sherrill,
Blake, CPA. Permission to collect the sample was obtained from Mr. Gene Miller. The
soil sampleis a dark red, clayey sand. No odors were detected in the soil and no elevated
HNu readings were detected inb the sample hole. HZ collected a soil sample for VOC
analyses first, then composited the soil in a a clean pyrex pan prior to collecting soil
samples for SVOC, metals, and PCB/Pesticide analyses. The soil sample was labeled
"CO-001-SL".
At 15: 13, HZ of Team #2 collected a subsurface soil sample from the 2 foot depth to
serve as a background from the same location as CO-00 I-SL. The soil is a dark red
clayey sand. No odors were detected in the soil and no elevated HNu readings were
detected in the sample boring, borehole or ambient air above the sample borehole. At
15: 15, HZ collected a soil sample for VOC analyses first, then composited the soil in a
clean pyrex pan prior to collecting soil samples for SVOC, metals, and PCB/Pesticide
analyses. The soil sample was labeled "CO-00 I-SB".
4
• •
Team #I arrived back at the site at 15:30. We departed the site for downtown Charlotte.
At 16:03, Doug Moore met with Mrs. Pat Cheek of Judge Lannings office, who signed
for receipt of the administrative search warrant and provided a copy for our records.
On Wednesday, March 13, 1996, Doug Moore and Stuart Parker of the NC Superfund
Section conducted a follow-up sampling event in Stewarts Creek. The purpose of the trip
was to gather the surface water and sediment samples that were unobtainable during the
previous weeks rainstorm. We arrived at the Freedom Road bridge over Stewarts Creek
at 17:45 and reconnect the sample collection points.
At 18:00, Doug Moore ("DM") used a hand auger to collect a sediment sample from the
0-6 inch profile of the stream bed of Stewarts Creek at a point approximately 30 feet
downstream of the confluence of the unnamed tributary to Stewarts Creek ("UT") and
Stewarts Creek. The sediment was a light gray, silty sediment with a small amount of
coarse-grained sand intermixed. No odors were detected in the sediment. The material
was transferred to a clean pyrex pan and handed up the bank to Stuart Parker ("SFP").
SFP collected a sediment sample from the pan for VOC analyses first, then composited
the sediment sample and collected samples for SVOC, metals and PCB/Pesticides
analyses. The sediment sample was labeled "CO-005-SD".
At 18:05, DM collected a surface water sample from Stewarts Creek, at a point
approximately 15 feet downstream of the confluence of the UT and Stewarts Creek. DM
collected surface water samples for VOC, SVOC and metals analyses. The samples were
labeled "CO-005-SW". The VOC sample was pre-acidified using 5 drops of I: I HCL.
The metals sample was field acidified to pH 2.0 using 40 drops of 50 % HNO3.
At 18:07, DM noted fishing line and a sinker hanging on bank vegetation at the sampling
site in Stewarts Creek.
At 18: 15, DM used a hand auger to collect a sediment sample from the 0-6 inch profile of
the stream bed of Stewarts Creek at a point approximately 63 feet upstream of the
confluence of the unnamed tributary to Stewarts Creek ("UT") and Stewarts Creek. The
sediment was a light gray, fine silty sediment. No odors were detected in the sediment.
The material was transferred to a clean pyrex pan and handed up the bank to Stuart Parker
("SFP"). SFP collected a sediment sample from the pan for VOC analyses first, then
composited the sediment sample and collected samples for SVOC, metals and
PCB/Pesticides analyses. The sediment sample was labeled "CO-004-SD".
At I 8:23, DM collected a surface water sample from Stewarts Creek, at a point
approximately 70 feet upstream of the confluence of the UT and Stewarts Creek. DM
collected surface water samples for VOC, SVOC and metals analyses. The samples were
labeled "CO-004-SW". The VOC sample was pre-acidified using 5 drops of I: I HCL.
The metals sample was field acidified to pH 2.0 using 40 drops of 50 % HNO3.
5
• •
At 18:45, SFP prepared a trip blank in the field using organic free water and acidified
with 5 drops of 1:1 HCL. At 18:50, DM prepared a preservative blank using deionized
water and preserved to pH 2.0 with 40 drops of 50% HNO3. Departed the site for
Raleigh.
6
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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
MAR G 8 1996
Mr. Dwayne Alexander
Vice President
· REGION-4
3◄5 COURTLAND'STREET, N.E.
ATLANTA. GEORGIA 30365
Rhyne, Alexander, Mattox Realty Co.
1100 South Tryon Street
Suite 205
Charlotte, NC 28203-4239
MAR 131996
RE: I EPA information related to property at 2401 Tuckaseegee Road
owned by Mr. Gene Miller
Dear Mr. Alexander:
Thia letter is to provide additional information you requested
related to the environmental condition of the above referenced
property. As you are aware, the U. S. Environme.ntal Pr9tection
Agen!,'.:y"(EPA) • Em.~rg~n_cy:-.~esponse ~; Removal· Branch:,:JERRil\'~ti:~ffzed
the '.property, as .. a-temp9rary: staging.• area: 'for--drwns\during, the.,
§'1,p~rf,u,nd;\~mo,y,lil ia,c:ti_oi:i;,"fo.r .. the.,cherokee Oil::·sife_.-,a~:r::e>'°'s· ~_he'
S·tr'ee·t,.···. · ... , ·· ,,: .. ··· " ·· ·· • ~ • ' Ii,;."~'', t,'f ,· •' :1.·, :.:" ::,,·· .. ;·,~·::.:
,11.;fter. ERIIB disposed ..of:: the drums and their contents offsite, the
top 3 · t'c>": 4. 'inch~a of soil was removed from the drum staging area.
This soil was teated (see attached·analytical;samples CO-WS-20 &
CO-WS-20), and EPA determined that the soil was not hazardous.
The soil was utilized to backfill and grade areas of the Cherokee
site across the street.
After removing the top layer of soil, the property was divided
into four (4) areas or grids for the purpose of collecting
samples to confirm that no significant· contamination remained.
The location of grids 1, 2, 3, ·. arid 4, and their associated sample
identification,are shown in Figure 1. 'The grid areas cover all
areas of the property that EPA conducted waste handling
activities. The samples were collected per EPA protocol, and the
results are attached.
The results indicate that no significant contamination remains on
the property. To restore the site to its original condition, a
minimum of 3 to 4 inches of clean topsoil was spread across the
staging area and the area was seeded. Although not needed, this
soil.serves as. an additional barrier between:the· surface and the
f~,z:ni~r ·. ~t:~gin_g, lir_ea, af,t~r., scraping;
A~ :r .. have indicated to you, EPA does not provide any .k.i.nd of.
c.~;!:tif_ic:~}~<;>n_,i.9-:F., :"cl13a.n,,bi;J.l· o~ theB:,lth'\, · for, any 'pr,op~r;!:iyiwe;,~re
in.y.91 Y;~d;,,:~itl_i 119 ~att;er;'.what ,the':circtinietahces_; 'howejver;, '. I :can, .
sa:y: that based. on ~he EPA,,s'ample .results• and my,;knowledge ·o.t· the
• L • • • • • •• • •
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activities EPA conducted on this property, the property poses no environmental or health threats. Of course, in the very unlikely circumstance that another source of contamination was discovered on the property (i.e. buried drums), EPA would re-evaluate the potential threats. ·
EPA ERRB plans no additional activities on the property with the exception of reseeding in the spring if necessary. The North Carolina Department of Environment, Health and Natural Resources (NCDEHNR) plans to conduct an investigation of the site which may or may not include the drum staging area. The NCDEHNR has been provided with the sample data and full1y understands the circumstances associated with the drum staging area. I suggest you contact Mr. Doug Moore of NCDEHNR at 919/733-2801 X315 for information regarding their investigation.
I hope this information will be of assistance, and as I've stated previously, I would be glad to discuss the site with any party who has a concern. I you wish to discuss the information, please call at 404/347-3931 X6135.
Sincerely,
~~
Steve Spu/lin
On-Scene Coordinator
Attachment(s)
cc: Gene Miller w/o attachments
P.oug Moore, NCDEHNR w/o attachments
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From:
Organization:
To:
Date sent:
Subject:
Priority:
Doug--
"Rob Gelblum" <n l [e-mail]>
SOLID WASTE MGMT.
[e-mail]
Fri, 1 Mar 1996 15: 17:45 + 1100
Cherokee Resources Admin. Search Warrant
normal
This is the e-mail I told you I'd be sending you summarizing the
status of the situation pursuant to my conversations w / Mecklenburg
County Superior Court secretary Harriet Fisher, Chief District Court
Judge James Lanning (who I told you runs an "environmental court" in
Mecklenburg), and his secretary Pat Cheek.
As I mentioned. the judge had some questions concerning matters such
as how many copies of the warrant are needed, and where to file the
executed/returned warrant. I agreed to look into those matters for
him, possibly by talking to Prof. Robert Farb at the Institute of
Government in Chapel Hill, whose book re: search warrants Judge
Lanning said he'd seen. I talked to Farb. who said he couldn't
imagine why more than copies for you, the court and "the property"
should be needed; as for filing, he didn't see why the court couldn't
simply establish a file on the matter in which to retain the returned
warrant.
I communicated the foregoing to Pat Cheek. We also discussed the
candidates for signing of the warrant reflecting its return to the
courthouse. When I mentioned that a magistrate (there's always one
on duty) could sign in the event you return after the judge departs,
Pat said the judge would prefer that you return prior to his standard
going-home time of 5 p.m. As I began to say I hope that leaves you
enough time at the site, given that you won't be getting to Charlotte
until mid-to-late morning, she said that you'd indicated you're now
considering spending the previous night in Charlotte. enabling you
to get to the courthouse nice and early.
It sounds like all your ducks are pretty much in a row. Make sure
you take to Charlotte the form warrant I gave you and the original
of yor affidavit. I'd also take either your entire Cherokee file or
cogent materials from it to back up the allegations in the
affidavit, in case the judge asks questions (though he, as you know,
has supposedly read the affidavit and approves the idea of your
going on the site).
• State of North Ccttolina
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
Mr. Henry Sutton
February 26, 19%
Solid and Hazardous W asre Program Manager
Mecklenburg County Department of Environmental Protection
700 N. Tryon Street
Charlotte, NC 28202
RE: Site Inspection
Cherokee Oil Company
NCD980799019
Dear Mr. Sutton:
····-·
.NA
DEHNR
f llE COfW
David Lilley of the NC Superfund Section spoke with you today to notify you that the NC Superfund Section will
conduct a site inspection of the subject site located in Mecklenburg County, North Carolina The inspection will be
conducted on March 6, 1996 by Doug Moore of the NC Superfund Section.
The purpose of the inspection is to detennine if the site poses a hazard to public health or the environment because
of releases of contaminants to soil, surface water, groundwater, or air. The inspection team will take samples on and around
the site to determine if a hazardous condition exists. Additionally, they will locate all nearby water supplies (surface and
groundwater, community and private) and any close sensitive environments, schools, and day care centers.
This inspection is not an emergency situation but is a normal step in the evaluation of all uncontrolled and
unregulated potential hazardous waste sites in North Carolina. You may want to have your representative meet the
inspectior team at the site. If so, please contact Doug Moore at [phone], ext. 315 and he will coordinate a meeting.
If the inspection indicates the need for future study of the site, we will contact your office to advise. If you have
any questions, please don't hesitate·to call David Lilley or me at [phone].
Enclosures
cc: Phil Prete
Doug Holyfield
Pat Williamson
Scott Ross
David Lilley
Donna Keith
Pat DeRosa, Head
CERCLA Branch
Superfund Section
P.O. Box 27687. Raleigh. North Carolina 27611-7687 Telephone [phone] FAX [phone]
An Equal Opportunity ~ffirmative Action Employer 50% recycled/ l 0% post-consumer paper
r )
I • Federal
sip Notification & Authorizatio-
Prepared by: ]. {)Ar,0 @£ Today's Date: (-2-2 -<t,
·use I3\ad: Ink or Typewriter only-Staff to fill out first~ blocks only.
Site Trip.
Date of Trip: M.ir rd. " I i'I (,
l
If trip date changed or cancelled note below:
Trip Date Changed To: Cancelled: --
NCD#: 980 7'o/'f c, l] Site Name: CAer" /s.ec. 0, t &,"'1'~.
City: Gfui r: I • I-le County: Me.~r, .. '5 C..
Reason for Trip: Sife_ ~£n.c,aLJ.Qt0 ,.
Name of Hotel (Overnight Trip): Hotel Telephone Number: ( ) --
Authorized by: Q,;;ul
Project Team Leader: fav6 /l,ioo ,Z.C
Assistants: 'pz,,_,_,, Ru,..,,.e.o~
Attach To Notification Form: 1 copy each:
Submit to the
Industrial Hygienist
, Jc~e77F ~7'h\J!d:f<,I , 6'At?fy ~N,/ r
Preliminary Assessment Form (First page only)
Site Map
PA Transmittal Letter
(Please !isl appropriate County Health Department contact person to call to advise of trip) <y;J,J•Y /-!-o, C-Wa j,.,_
Environmental Supervisor or Health Director to call: /J'r'-l•ieor~ '>,.-b Title: P.:-v-ir,i,~ /r0 ,
. r' ) -✓• (Note I Dr., M.P., etc.)
Telephone Number: (7cy)3::10 -Sson
Notes: Health Department Official Contacted: .1nr-c;,i:Hc----
Back Up Letter Required: Yes / No
,.J/Jvbt,J /J/r <;u o:; <Zb J -:1£-'lf,
Note: Sii,,cd on'~nal to Data Manager
CDtil)
State of North Ca.no
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr,, Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
February 13, 1996
Gene W. Hartsell 10688-058
Caller Box 8004 Sandhills B
FPC -Seymour Johnson AFB
Goldsboro, North Carolina 27533-8004
Subject: Site Access Information
Cherokee Oil Company Site
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCO 980 799 019
Dear Mr. Hartsell:
In response to your request for information, enclosed please find a copy of the
relevant sections of the North Carolina General Statutes, Chapter 130A-310.21 and
3.10.22, authorizing the N.C. Department of Environment, Health and Natural Resources
to administer the Superfund program and enter into "cooperative agreements with the
United States and to engage in any activity otherwise authorized by law to identify,
investigate, evaluate, and clean up any site or facility covered by CERCLA/SARA,
including but not limited to performing preliminary assessments, site investigations, ... "
and N.C.G.S., Chapter 130A-17, granting right of entry "upon the premises of any place
where entry is necessary to carry out the provisions of this Chapter". I also include a copy
of the relevant section of the State's cooperative agreement providing background
information on the Superfund Section and the 1995-1996 workplan, approved by EPA,
for the Section. As you can see, the subject site, titled "Cherokee Oil Company", is
scheduled as part of the I 995-1996 workplan approved by EPA for the NC Superfund
Section, and the subject sampling is a legitimate activity as described under the above
cited statutes.
Please note that N.C.G.S, Chapter 130A-l 7 also provides that "if consent of entry
is not obtained, an administrative search and inspection warrant shall be obtained
pursuant to G.S. 15-27.2.". Since sampling data as recent as 1995 demonstrates the
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ 1 ~ post-consumer paper
•
Letter to G.W. Hartsell
re: Cherokee Oil Company
February 13, 1996
Page 2
•
subject site still contains hazardous substances as defined under CERCLA, and available
file information demonstrates that historic spills originating at the site have migrated off-
site, there is probable cause for believing that a condition exists at this site that justifies
sampling and inspection of your property. The purpose of our investigation is to
determine if current or historic releases from the site pose a sufficient threat to the public
health or environment to warrant further action under CERCLA/SARA or other
appropriate authority. In consideration of your statement in your February 7, 1996 letter,
indicating that the State has "no reasonable or legitimate reason to need access to this
property", it seems there is no other recourse than to seek an administrative search and
inspection warrant.
Therefore, by this letter, I am notifying you the Superfund Section plans to
seek an administrative search and inspection warrant on March 6, 1996, for the
purpose of collecting environmental samples on that day as part of a site inspection
of the Cherokee Oil Company site at 1201 Berryhill Road in Charlotte. If I can be of
assistance, please contact me at [phone], ext. 315.
/ cc: c._ file
Robert Gelblum
PatDeRosa
Respectfully,
Douglas Moore
NC Superfund Section
§130A-13
ilns and" preceding "den•
ds.
1e possession of the
be confidential and
.J. 11985, C. 470, s. 2;
dd~tcd "of Human Re-
_ng "Department".
ty for Depart-
rogram consti-
tate of right to·
,w, by applying for
payment program
..itient or responsi-
d to have made an
' benefits, contrac-
> the extent of the
f uf the recipi~nt
: pa I 1en t shall be
Ith the following
im any amount of
. the recipient by
orn a third party:
<xed by the judg-
:urney represent-
"" obtaining the
Oile-third of the
e right of subro-
i.~.t.u:ce received
. chums against
third party to
Hi~ the amount
Ltl lied or recov-:; ;) 1 i ~.s: and
·llaining to the
u shall be enti-
1. Their shares
· pr;,pnrtionate
onre with the
iich H:-;sistance
1?JUrces coIIec-
lll'd party re-
nplement this
ll30A-14 ART. 1. GENERAL PROVISIONS !ll30A-18
§ 130A-14. Department may assist private non-
profit foundations.
(al The Secretary may allow employees of the Department to
assist any private ·nonprofit foundation that works directly with
aervices or programs of the Department and whose sole purpose is
to support the services and programs of the Department, and may
provide other appropriate services to any such founda:ion. No em-
ployee of the Department may work with a foundation for more
than 20 hours in any one month. Chapter 15013 of the General
Statutes does not apply to any assistance of services provided to a
private nonprofit foundation pursuant to this section.
(b) The board of directors of any private nonprnfit foundation
that receives assistance or services pursuant to this section sha1l-
&ecure and pay for the sevices of the Department of State Auditor or
shall employ a certified public accountant to conduct an annual
audit of the financial accounts of the foundation. The board of direc-
tors of the foundation shall transmit a copy of the annual financial
audit report to the Secretary. (1991, c. 761, s. 37.3.)
Editor's Note. --Session Laws 1991,
._ .. c. 761, s. 52, made this section eflCctive
July 16, 1991.
':.·
§§ 130A-15, 130A-16: Reserved for future codification pur-
poses.
Part 2. Remedies .
§ 130A-18. Injunction.
If a person shall violate any provision of this Chapter or the rules
adopted by the Commission or rules adopted by a local board of
health, the Secretary or a local health director may institute an
action for injunctive relief. irrespective of all other remedies at law,
in the superior court of the county where the violation 0ccurrecl or
where a defendant resides. I UJ83, c. 89 I, s. ~-1
OPINIONS OF AlTOHNEY GENEl!AL
As to North Carulinu prohibition
of the dumping of waslP materials
1uch as bags of mcdic:al refuse, 1.:,:;po.:·
cially that which may ho.: huz:mlou,:; or
infoclious, into the A1la1111r t kean. the
19
authurily uf North C:.trtJlina wiLh re:;µell
tu dumping lil'yond thn.:l: mile.:; in the
on·;,rn which r<.:~uh:; in wa."ite,:; entcrinv
Stak walo.:r:; ur l,o.:in~ dcr,osil.:d un lht'
St:1k slwn.::; and tit.: 1.:xt...:nt Stull: l: .. rn
'5\\
f~ iJ,
ij /{
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II f_; i
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'.'!
= "' ...
.,, ___ • *130A-:no.21 * 130A-310.22
~ 130A-310.2l. Administration of the Superfund
program .
... \,Tb]~~flffT.ffil4~~l!Jftw!V.t~l~J~]:2fii~-r19.~IJ~~~ff.iEiS@tiff ,su_b:<,J!],t_!_..":1thm the sohd waste manageme·nt_umt,aµt_ho_nzed liy G.S.1 ;
130,\-291 \2~1!!fY,;O,U~~-hose ac'(i',;itics}j'n'.\,·h icli''the'Staie'is~iiuth~ ;
%h~~.1\.\',1rpg]g~U1'!,der,.,C,ERC'Li\ SARA~ 1)989, C. 286, s. 10.)
§ 130A-310.22. Contracts authorized.
t a-1-The~DCj[{r7i ~•cfl't ~f~ulli1TT-17.CdtO"ef{tCLlnio ., con t?acts-and co-
1!JP~t,tJ_L\"'e'i1fri_iimems."'ii°h".!li,;<;.Uiii feel: Stal es"andJ_\i:_eiigage' iii ahy ,Oct i \'it ,-.~ot hefii/i se-atilhOii zed_~)-~ 1 n ;,1,-:· toJ dent i fr7:i nYeStig·a te';e\131u-.... -. ,..~~· •~~•\""'~•.,,_--,"!...--~•~-•.'""'~,....«-~--""".-.' ---.r,•"-""<"f\'•l•Tr.--·1 • , ll!,e .,;n nil ,c •~a n-1.u p ,if n y,s, te)or Jae, _Ii tj• ,·co~·erea ;h y:,:CE R_C_LA!St\l\A .•
lD£U~JJlifif;~~~D.~-it)I ~:WUP-Jl}.O ·.P~fQ!fT1~.riJ(~~~·~ IJ~ i n~_i)~ 'l~s_s"ff~rfie~t!! j;. ~!1~E.u:.t~.~~ .. ~t1~~c.u1 ... ec!1q!__1~x-~~Hg:~~l!!~.9,~•r.:a ... 1l9 feas_~ljJ,\~~Y1JJ.2.0Jes; :·:-
IP!.£P.I,!f_~t_!Q_Q_~9f;',r~~~~!A:~-!{.~~Ht~9.!!;,~.o~d,!:!.~.lJng_.,~w~rg~P.J;Ytf..~~P9.1!--~,v1· ;·remea,altand remoral;act10ns; and engaging m enforcement actm-,. {tJffli'1;ii'cfdfdiWiC'e\\Vith·tt11Et~pf{lVi~iOns··1,r-cERCLA;,sARA'. '
1b1 The Department may make all assurances required by red.
era I law or regulation including hut not limited to assuring that th,
State will assume responsibility for the operation and maintenanct
of any remedial action for the anticipated duration of the remedial .
action; assuring that the Stale will pro,·ide its share of the cost of -,.;
any remedial action al a site or facility which was privately owned ,,
or operated; assuring that the State will provide its share of the cost\?
of any removal, remedia!J'lanning, and remedial_action ata_s_iteor :~.
facility owned or operate by the State or a poht,cal subd1V1s10n or ;;_
the State; assuring the availability of off-site treatment, storage.or'?
disposal capacity needed to effectuate a remedial action; assuring Z
that the Stale will take title to, acquire an interest in, or accept /
transfer of any interest. in real property needed to effectuate a re-/i
medial action; assuring that the Slate has adequate capacity w ·•;,:
meet the assurances required by CERCLAISARA (42 U.S.C. J, ~ 9604(cli9ll; assuring access to the facility and any adjacent prop,:]
erty including the sec.uring of any right-of-way or easement needed ',
to effectuate a remedial action; and assuring that the State will :
satisfy all federal, State, and local requirements for permits and:··
approvals necessary to effectuate a remedial action. '.-.'.
fcl Each contract entered into by the Department under this se<-1
tion shall stipulate that .all obligations of the State are subject u, ';,
the availability of funds. Neither this section nor any contract en• X
tercd into under authority of this section shall be construed to obli-:;/
gate the General Assembly to make any appropriation to imp!., :',
ment this Part or any contract entered into under this section. Th, \'
Department shall implement this Part and any contract entered .f
into Lnder this section from funds otherwise available or appropri, ·;;
ated to the Department for such purpose. (1989, c. 286, s. 10; 1989 f
(Reg. Sess., 19901, c. 1004, s. 11; c. 1024, s. 30(cl.) _,.,
222
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·\! ·. ~ ,, Cross Referencl•s. -Set.> l::ditor·s warrants, S1:'C ~~ 15A-241 through
note following the nnalysis to this Chap· 15A-259.
ter, For present provisions us to i.earch
ARTICLE 4A.
Administrative Search and Inspection Warrants.
§ 15-27.2. Warrants to conduct inspections autho-
rized by law.
(a) Notwithstanding the provisions of Article 11 of Chapter 15A,
any official or employee of the State or of a unit of county or local
government of North Carolina may. under the conditions specified
in this section, obtain a warrant authorizing him to conduct a search
or inspection of property if such a search or inspection is one that is
elsewhere authorized by law. either with or without the consent of
the person whose privacy would be thereb;· invaded, and is one for
which such a warrant is constitutionally required.
(b) The warrant may be issued by any magistrate of the general
court of justice, judge. clerk, or assistant or deputy clerk of any court
of record whose territorial jurisdiction encompasses the property to
be inspected.
(c) The issuing officer shall issue the warrant when he is satisfied
the following conditions are met:
(1) The one seeking the warrant must establish under oath or
affirmation that the property to be searched or inspected is
to be searched or inspected as part of a legally authorized
program of inspection which naturally includes that prop-
erty, or that there is probable cause for believing that there
is a condition, object. acti,·ity or circumstance which legally
justifies such a search or inspection of that property:
(2) An affidavit indicating the basis for the establishment of
one of the grounds described in (11 above must be signed
under oath or affirmation by the affiant;
(3) The issuing official must examine the affiant under oath or
'';· affirmation to verifv the accuracy of the matters indicated
·:;, by the statement in the affidavit;
·' (d) The warrant shall be validly issued only if it meets the
.:, following requirements:
';;. ,:·. (1) Except as provided in subsection lei. it must be signed by the
issuing official and must bear the date and hour of its issu-
ance above his signature with a notation that the warrant
is valid for only 24 hours following its issuance;
(2) It must describe. either directly or by reference to the affida-
vit, the property where the search or inspection is to occur
and be accurate enough in description so that the executor
of the warrant and the owner or the possessor of the prop-
erty can reasonably determine from it what person or prop-
erty the warrant authorizes an inspection of;
17
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§ 15-27.2 CH. 15. CRIMINAL PROCEDURE
;f'·
§ 15-27.i
~& (3) It must indicate the conditions. objects. activities or circum:t stances which the inspection is intended to check or reveal" (4) It must be attached to the affidavit required to be made·'
order to obtain the warrant. '.:t,,,-• ,.;
. (e) Any warrant issued under this section for a search or inspeJ~~j\' tion shall be valid for only 24 hours after its issuance, must be:,Wif( personally served upon the owner or possessor of the property be-.J~r:,, tween the hours of 8:00 A.M. and 8:00 P.M. and must be returned','!,:,;:,;.<., within 48 hours. If the warrant, however, was procured pursuant to,;J,l,[! an investigation authorized by G.S. 69·1, the warrant may be exe:,E,)f,;;,', cuted at any hour, is valid for 48 hours after its issuance. and must ti%/', be returned without unnecessary delay after its execut10n or after:,,tr::, the expiration of the 48 hour period ifit is not executed. If the ow_ner111i~r. or possessor of the property 1s not present on the property at the time ,,,,,c•.··:: of the search or inspection and reasonable efforts to locate the owner'J)l//;'i · or possessor have been made and have failed. the warrant or a copy',;'.il'/f; the_reof may be affixed to the property and shall have the same effect;,;~;:;:, as 1f served personally upon the owner or possessor. . ,, ,JiJ(i, 11) No facts discovered or evidence obtamed ma search or mspec-~tt; tion conducted under authority ofa warrant issued under this sec••,};;~: tion shall be competent as evidence in any civil, criminal orJlq;;, administrative action, nor considered in imposing any civil. crima'"-.~!)_ inal, or administrative sanction against any person. nor as a basis 'ki'·' for_ further seeking to obtain a_ny w_arrant, if th_e _warra!'t is in".a\id :·,l'!W:;' or 1fwhat 1s discovered or obtamed 1s not a cond1t10n. obJect, activity ;;/ ... i1~.;;., or circumstance which it was the legal purpose of the search or\~_/ inspection to discover; but this shall not prevent any such facts or. ~"'".;t.' evidence to be so used when the warrant issued is not ·'lf,;f constitutionally required in _those circumst_ances.. · ":i:\f,f · ( g) The warrants authorized under this sectwn shall not be ·~, regarded as search warrants for the purposes of application of ,}),!} · Article 11 of Chapter 15A of the General Statutes of North Carolina. :;m):': (1967, C. 1260; 1979, C. 729; 1983, C. 294, SS. 1, 2; C. 739, SS. 1, 2,) ':iii
·:~,;~•/,~·
Effect of Amendments. -The first
1983 amendment. effective 'May ll.
1983. substituted "Article 11 of Chapter
15A" for "Article 4 of this Chapter'' near
the beginning of subsection ta) and in
subsection !gl.
The second 1983 amendment, effective
July 13. 1983. added "Except as provided
in subsection (el" at the beginning of sub•
'~•,: ifri;~:~e'~; ,:~;:t:~';;~,:~r :::,:!1: ~r
Legal Periodicals. -For comment as 1it
to warrants required for administrative ff,:,(
health inspections, see 4 Wake Forest ~i
Intra. L. Rev. 117119681. ,.fil;-..
For survev of 1979 constitutional law, \~\ see 58 N.c.L. Rev. 1326 (19801. ·' .. t,_r,:
CASE NOTES
Constitutionality. Subdivision
(cl( ll of this section is not
unconstitutionall_v void for vagueness.
Brooks v. Taylor Tobacco Enter., Inc .. 39
N.C. App. 529,251 S.E.2d 6:36. rev·d on
other grounds, 298 N.C. i59, 260 S.E.2d
419 (19/9).
Alternative Criteria for Basis of
Wnrrnnt. ---Subdivision rci1 l> of !his
for determining whether to issue a
warrant. The first, the "program of
inspection test.'' is that the property is to
be inspected as part of a legally autho•
rized program of inspection which nat·
urally includes that property. The second
is a probable cause le!:it. If an inspection
meets either of these ksts a warrant is
prnp•~rly under :-tatute. , , ____ J -

•

. , •
for the
"11>reiiminar'y'Xssessmenfs and
·---~~1w._~pectionsfor;,"J2!'/
; GJ!.RCLIS Sites
•
(Comprehensive Environmental Response, Compensation,
and Liability Information System)
March 1995
1
• •
March 1995
A. C,Backgrouncffii'formation for the CERCLA PA/SI Cooperative Agreement
North Carolina currently has 910 sites in the Comprehensive Environmental Response
Compensation and Liability Information System (CERCLIS). CERCLIS data was drawn from the
Hazardous Waste Data Management System, Site Tracking System, CERCLA 103(c) notifications and
other state and EPA inventories and reports. New sites are added to CERCLIS as they are discovered.
From November 1983 through June 1985 (21 months), 359 Preliminary Assessments of CERCLIS
sites were completed and submitted to EPA. From November 1983 through June 1985, 40 RCRA 3012
Site Investigations were initiated and completed by North Carolina. (From 1980 until 1986, CERCLIS
was called ERRIS, Emergency Response and Remedial Inventory System.) ·
The original Cooperative Agreement (V004500-85) was initiated in July 1985 and was amended
and extended through September 30, 1992. From July 1985 through September 1992, the PA/SI program
completed 444 Preliminary Assessments, 130 Site Investigations, 37 Screening Site Investigation Starts,
34 Screening Site Investigation Completions, 49 Screening Site Investigations, 3 Phase I Expanded Site
Investigations, and 2 Expanded Site Investigation Peer Reviews. In addition, 55 Phase I Screening Site
Investigations, and 58 Phase Il Screening Site Investigations have been completed by a private engineering
company under contract with the State, using funds provided in the Cooperative Agreement.
The current PA/SI Cooperative Agreement (V994270-0l) between the State and the US EPA
began September 15, 1992 and has continued through December 31, 1994. During this period, the State
completed 39 Preliminary Assessments, 1 Screening Site Investigation Completion, 6 Screening Site
Investigations, 11 Contractor Screening Site Investigations, 11 Site Inspections, 26 Site Inspection
Prioritiz.ations and 2 Expanded Site Inspections. The most recent amendment (V994270-0l-6) has
extended the project period through March 31, 1995 pending approval of this application.
This application proposes to amend the current PA/SI Cooperative Agreement beginning April 1,
1995 and continuing through June 30, 1996. The State proposes to complete 17 Preliminary Assessments,
24 Site Inspections, 6 Expanded Site Inspections, and 2 Hazard Ranking System Documentation Package.
Funding for these activities to be completed between April 1, 1995 and June 30, 1996 is outlined in this
Cooperative Agreement amendment. Additional work products remaining from the previous amendment
will also be completed during this project period as shown in the attached work program schedules.
Funding remaining from the previous amendment will be used to complete these outstanding work
products.
30
• • SITE INSPECTION
1995-96 WORK PROGRAM SCHEDULE
(7 March 1995)
NAME EPA ID NUMBER REPORTING DA1
Archer Daniels Midland PCB Spill Site NCD 986 215 671 31 Dec 95
*Benfield Chemicals NCD 986 171445 30 Sept 95
Furnace Road Abandoned Drums NCD 981 929 367 30 Sept 95
*Greenville Coal Gas Plant NCD 986 188 886 30 Sept 95
*McLean Bros. Farm NCD 986 172 500 30 Sept 95
*Pilot Mtn. Tire Fire NCD 986 166 379 30 Sept 95
Riley Battery Site NCD 986 232 700 31 Dec 95
Ward Transformer NCD 003 202 603 30 Sept 95
Parker Industries NCD 986 215 499 31 Dec 95
Ram Leather NCD 982 096 653 31 Dec 95
C. P. Properties NCO 000 998 336 31 Mar 96
A. C. Lawrence Leather Company NCO 000 195 701 31 Mar 96
Caier'offt/offco~pariy ' :;,;'Jltct>"980-199 019 :31,Miii'96'
Custom Processing & Manufacturing NCD 982 117 590 31 Mar 96
Gresham's Lake Industrial Park NCD 986 232 379 31 Mar 96
Hickory Grove Road TCE Site NCD 000 998 344 31 Mar 96
Tartan Marine Property NCO 000 828 566 30 Jun 96
Tom Sadler Road Wells NCD 986 231 967 31 Mar 96
Woody Wilson Battery NCD 986 230 597 30 Jun 96
1 Site TBA 30 Jun 96
36
•
SITE HEALTH AND SAFETY PLAN
A. General Information
•
Site Name Cherokee Oil Company ID# NCD 980 799 019
Location 1201 Berryhill Road, Charlotte,
Mecklenburg County, NC
Proposed Date of Investigation January 31, 1996
Date of Briefing ~J~a~n~u~a=r~y~3~9~-~1~9~9~6~--------------
Date of Debriefing ~F~e~b~r~u,.,.a~r~y'--1....._.---'1~9~9=6 ____________ _
Nature of Visit (check one): On-Site Reconnaissance
Off-Site Reconnaissance
Sampling
Sampling Overview
Remediation Overview
X
Health Department Official Contacted Sarah Edwards for Henry Sutton
Date of Contact January 25, 1996
Site Investigation Team: All site personnel have read the Site Health and
Safety Plan and are familiar with its provisions.
Personnel Responsibilities Signature
Team 1 Doug Moore team leader sampling
Team 1 Doug Rumford sampling -----,-.t,:::....J..-.~;=;;!;f-,(l::.=-,r=:-:::::: r
Team 2 Jeanette Stanley sampling
Team 2 Harry Zinn sampling
Plan Preparation: n 'I
Prepared By, David Lilley. Industrial Hygiene Consultant IJ)_~/3',
Reviewed By: Jack Bµtler, Superfund Section Chief ~
• •
B. SITE/WASTE CHARACTERISTICS
Waste Type (s) __ X_Liquid ___ Solid __ X_Sludge ___ Gas ___ Vapor
Characteristics ___ Corrosive ___ Ignitable ___ Radioactive
___ Volatile __ X_Toxic ___ Reactive ___ Other
List Known or Suspected Hazards (physical, chemical biological or
radioactive) on Site and their toxicological effects.
chemical amounts
Also, if known, list
HAZARD
P Bs
Acetone
Ethyl benzene
bis(2 ethylhexyllphthalate
Toluene
Xylenes
Naphthalene
Perchloroethylene
PAHs
Pyrene (noncarcinoqenic}
Benzo[a]pyrene (carcinogenic)
WARNING PROPERTIES
Odor Threshold -no data
OT 100 ppm
OT 0.25 200 ppm
OT -no data
OT -0,17 -40 ppm
OT 0.05 -200 ppm
OT 0,003 0,3 ppm
OT -4.68 50 ppm
vary according to compound, many are
carcinogenic-indicators listed below
OT no data
OT -no data PEL=
UNDERGROUND UTILITIES CHECKLIST
EXPOSURE
LIMIT
0.5 mg/m3
750 ppm
100 ppm
5 mg/m3
SO ppm
100 ppm
10 ppm
25 ppm
varies
no data
O. 2mg/m3
Utility
Power
Telephone
Gas
Locator/Contact Person Phone# Date of Location
Water
Sewer
;:;all made by: Doug Moore called Miss Utilities (1-800-632-4949) on January
29, 1996. Ticket # 44338.
2
• •
ID# NCD 980 799 019
Buildings e Facility Description: Size ~l~a~c~r~e~---
Disposal Methods Being Investigated
hauling and recycling facility.
Possible spillage from a waste oil
Unusual Features on Site (dike integrity, power lines, terrain, etc.):
none known
History of the Site: Cherokee was permitted to haul and recycle used waste
oil, In 1994, the owners were convicted of criminal violations of federal
statutes and imprisoned, Op November 3, 1994, EPA conducted an emergency
removal action on the site. There were 55-gallon drums, above-ground tanks,
tanker trucks, and underground storage tanks on-site.
C. HAZARD EVALUATION
The site can be toured and sampled in level D protection, PVC gloves will
be worn while collecting water, soil, and sediment samples, PVC
gloves over nitrile gloves will be worn if discolored soil or sediment is
to be sampled. A tyyek suit will be carried to the sediment sampling
location and will be worn if samples cannot be obtained without getting
clothing muddy, Steel toed work boots will be worn while conducting tour
and sampling the site, An HNU will be used to monitor breathing zone air
while augering. If the HNU readings exceed background in the breathing
zone, the sampling crew will stand upwind of the hole until the HNU reads
background, If a background reading cannot be obtained within 15 minutes,
the hole will be filled in and that area of the site will be evacuated. A
tyyek suit (saranex in wet conditions), steel toed work boots, and nitrile
gloves will be worn by the person augering.
D. WORK PLAN INSTRUCTION
Map or Sketch Attached? ~y~e~s~---
Perimeter Identified? ~n=o~----
Command Post Identified? ~n=o~----
Zones of Contamination Identified? ~n"'------
Personal Protective Equipment/Level of Protection: ___ c -~x __ D
Modifications Wear goggles, face shield, and PVC gloves while preparing
acid preserved samples, goggles and PVC gloves while collecting acid
preserved samples, Avoid breathing acid vapors,
3
Surveillance Equipment:
X HNU
OVA
Explosimeter
•
Decontamination Procedures
•
ID# NCD 980 799 019
Detector Tubes and Pumps
02 Meter
Radiation Monitor
_____ Level C Respirator wash, respirator removal, suit wash {if needed),
suit removal, boot wash, boot removal and glove removal.
--~x,__Level D Boot wash and rinse and boot removal, suit removal, glove
and goggle removal.
Modifications Dispose of trash properly, on site if possible,
Work Schedule/Visit Objectives The purpose qf this visit is to determine
if the site poses a threat to the public health or environment because of
releases of contaminants to soil, surface water, groundwater, or air,
Sampling may consist of surface and subsurface soil sampling, and surface
water and sediment sampling.
EMERGENCY PRECAUTIONS
Route of Exposure
E es
Inhalation
Ingestion
4
First Aid
irrigate immediately
soap and water wash
fresh air and artificial respiration
get medical attention immediately
X
X
X
• •
ID# NCD 980 799 019
Location of Nearest Phone: unknown (nearby residences/businesses?)
Hospital (Address and Phone Number)
Mercy Hospital, 2001 Vail Avenue, Charlotte, NC (7041 379-5000
can handle chemically contaminated patients
Emergency Transportation Systems (Phone Numbers)
Fire _.z,~lL-___________________ _
Ambulance _ _z_.l~lL-________________ _
Rescue Squad 1
Emergency Route to Hospital Take the access road back to Freedom Rd, and
follow it to the John Belk Frwy Exit onto 4th Street and travel southeast
to N Colonial Ave apd turn left, the hospital will be on the right.
PREVAILING WEATHER CONDITIONS AND FORECAST ________________ _
EQUIPMENT CHECKLIST
Air purifying respirator
Cartridges for respirator
Eye Wash Unit
X
X
X
First Aid Kit
3 gal. Deionized H20
Rain suit
HNU
OVA
Explosimeter
Radiation Monitor
Decontamination
Materials
X
X
X
X
x
Gloves (PE/PVC/nitrile/cloth)
Boots/Boot Covers
Coveralls (tyyek/saranex)
Eye Protection (goggles/shield)
Hard Hat
Poison Control Center -State Coordinator
Duke University Medical Center
Telephone: [phone]
Box 3024
Durham, NC 27710
ASHEVILLE
704-255-4490
Western NC Poison HENDERSONVILLE
Control Center 704-693-6522
Margaret R. Pardee
Memorial Hospital
Fleming St., 28739
LOTTE
704-379-5827
DURHAM
1-800-672-1697
GREENSBORO
919-379-4105
safeform.294b
Memorial Mission Hosp. Ext. 555,556
50 · tmore Ave. 28801
Mercy Hospital
2001 Vail Ave, 2820
Duke Univ. Med. Center
Box 3007, 27710
Moses Cone Hospital
1200 N. Elm St. 27420
HICKORY
704-322-6649
JACKSONVILLE
919-577-2555
WILMINGTON
919-343-7046
5
Catawba Mem. Hosp.
Fairgrove Chur. Rd 28601
Onslow Mem. Hospital
Western Blvd. 28540
New Hanover Mem. Hospital
2131 S. 17th St. 28401
.'.\,'7;;,'' '_'?·-~":.":.., --vl\ ,,_
~.~-~~·--,i_ -~ 1,_-_/ ~
.-1 ~-.·o _ 16 >, "'" ;.-, ';"----· : ,@,, --· ~ ,. ----,~ I .• , '· <"J' ·• ~-~ -,,.
I,''~.·,
-~J ... --'~~--~--.~·;.,c'""'·"'
-a··\'•• • ~-Ii "',-\' __ / ~ '
,, ~·-· \ ".\ •' ' ,rt>;-· ·-~5,'-?r.
. ·"
.:~ ,,
l
)_."
!"• ,
-~
., '
~->\
;.1,., I.· .::::•,\•; •,ilaj .3/·~"' • ._,, I
, ... ..,,
',' let ~~,.l' ;:/<f/ .fy ~---~ ' ' ';?:;--□-... f'fn. BLVD W/LKI SON ;i
,;.. ,( •• ,:;.., ~ SOIHHERNRR 74 BLV ~ . --1~\ ··~;. ' :: ~ :;/4
iifti~,l., tr--~ !:11 -, __ _
'I :s i ~~ \~ ~ ~ ,1 r I ' , \ 1: : \(~1,~, \
_j!1
\
. ~
' .
)~ ' ""',, i il'•LO-~ l ~ ~ a...,o,. ;'F':", _,. •1,' i' \ J ~ '~-
1 ""''f:o/ ... ,-....::: • ' , .. ~-/ •,'fY) t~•1, .;,~Ff.~/ /~c..,., ·• ,r 1 .~\ ----~• . , -, i-: •, ,,3/ ~, "'"·· ·,./ . ,. r . ~ , ,,,,,. __ ,_ ..,. ·,.:; :,......_•
• •
TO BE COMPLETED BY PROJECT MANAGER
PROJECT MANAGER: ~D~o~u~g,.__,M~o=o~r~e~-----PROJECT: Cherokee Oil Company
INVESTIGATION DATE: January 31. 1996
RECONNAISSANCE SAMPLING VISIT __ X_ REMEDIATION/SAMPLING OVERVIEW
Materials Used (Please insert a number in the blank)
Air Purifying respirator cartridges
Eye Wash Units
Gloves (nitrile)
Gloves (cloth)
First Aid Kit
Gloves (polyethylene)
Gloves (PVC)
Respirator Worn By
Boot covers
Coveralls (tyvek)
Coveralls (saranex)
Approximate Time in Respirator
Air Monitoring Data (Include Calibration Reading)
HNU:
OVA:
Explosimter:
Radiation Meter:
Were there any injuries? If yes, explain: ______________ _
If the maximum personal protective equipment as outlined in the Hazard
Evaluation Section was not used, please justify:
Visitors Present Organization Represented
Signature
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: PCBs toolvchlorioated binhenvls) 42% & 54\ chlorine
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula Cl2H7Cl3 142%1 & Cl2H7Cl5 154%1 1-3
Natural Physical State at 25°C _.l~i~qu.,..iud._ ____ ~ 1-3
Vapor Pressure ~P~-~P~P.l __ ~rn mm Hg at 20°C 1-3
Melting Point -19-10 °F/°r:.. Boiling Point 325-390 °F/°r:..rn _1-_3~---
Flash Point (open or closed cup) 349-432
Solubility -H,O insoluble
other-------------------~
1-3
Physical Features: (odor, color, etc.) colorless to dark brown liquid
with a mild hydrocarbon odor,
II. TOXICOLOGICAL DATA
1 ma/m3 (42%) 1 mo/m3 (42%) potential human
Standards: 0.5 maim' 154%1 141 TLV o.s mg/m' 154%1 151 PEL carcinogin 161 IDLH
Routes of Exposure: Inhalation, skin and ingestion
Acute/chronic symptoms: Irritates the eves. nose, and skin, can cause
chloracne, Liver injury is possible, Mav cause jaundice and dark urine, (21
First Aid: Inhalation; artificial respiration: Inaestion: get medical
attention immediately: Eve contact; irrigate immediately; Skin contact;
soap and water wash immediately
• •
Chemical Name: Lp~c~e~•~e._ _________ _
III. HAZARDOUS CHARACTERISTICS Reference
A. combustibility /Instability w/yery high heat)
Toxic by-products HCl & CO gases may be realeased
B. Flammability LEL .,Nc;c/_..A._ __ ~ UEL ____ _
1.3
1.3
c. Reactivity Hazard contact with strong oxidizers may .L..J..._
cause fire or explosion,
D. Corrosivity Hazard yes/no
Neutralizing agent:
E. Radioactive Hazard
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
pH:
1, chemical safety Pata Guide. BNA -1985.
Exposure Rate
2, Pocket Guide to Chemical Hazards, NIOSH -1990,
3, PA Chemical Emeroencv Preparedness Program -Chemical
Profiles -1985
4, Threshold Limit Values and Biological Exposure Indices for
1994-1995, ACGIH
5. 29 CFR 1910,1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Acetone
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula CH3COCH3
Natural Physical state at 2s0 c liquid
Vapor Pressure 180 mm Hg at 20°c
Melting Point -140°F/°C Boiling Point 133°F/°C
Flash Point (open or closed cup) _JJ_°C/':..1:.
Solubility -H,O miscilbe Other _____________ _
1.2
1.2
2
Physical Features: (odor, color, etc.) colorless liquid with a
fragrant. mint-like odor. IP 9.69 ev (2) HNU Relative
Response -6.3 with the 10.2 ev probe. OVA Relative Response -
II. TOXICOLOGICAL DATA
Standards: 750 ppm (3) TLV
20.000 ppm (2) IDLH
750 ppm (4) PEL
Routes of Exposure:
dryness. Inhalation. contact with skin will cause
Acute/Chronic Symptoms: Irritation of eyes. nose and throat.
Headaches. dizziness. and dermatitis. (2)
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate immediately; Skin contact: soap and water wash immediately.
• •
Chemical Name: Acetone
III. HAZARDOUS CHARACTERISTICS Reference
A. combustibility Yes x_ No
Toxic by-products
B. Flammability LEL 2.5% UEL 13%
2
c. Reactivity Hazard
D. Corrosivity Hazard
Neutralizing agent:
oxidizing material and acids
yes/no pH: -
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles
Gamma radiation
IV. REFERENCES
yes/no
yes/no
1. chemical safety Data Guide. BNA -1985.
2. Pocket Guide to chemical Hazards. NIOSH -1990.
3. Threshold Limit Values and Biological Exposure
Indices for 1994-1995
4. 29 CFR 1910,1000
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Ethyl Benzene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula cs Hl0
Natural Physical State at 25oC liguid
Vapor Pressure 10 mm Hg at 79oF
Melting Point =-l.12.oE/oC Boiling Point 2IJ..OE/OC
Flash Point (open or closed cupl 59-64oC/oE
Solubility - H20 0,01%
other miscible with usual organic
solvents
1.2
1.2
2
1,2
Physical Features: (odor, color, etc.) colorless,
flammable liguid with an aromatic odor. IP -s.76 ev
Relative Response ovA -100%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (3) TLV
2000 ppm (2) IDLH
100 ppm (4) PEL
Routes of Exposure:
contact
Inhalation, Ingestion, Skin/Eye
Acute/Chronic Symptoms:Irritation of the eyes and mucus
membranes, headache, skin problems, sleepiness, coma (2)
First Aid: Inhalation; artificial respiration; Ingestion;
get medical attention immediately; Eye contact; irrigate
immediately; skin contact; soap and water wash immediately
•
Chemical Name: Ethyl Benzene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes x_ No
Toxic by-products none known
B. Flammability LEL .l.......Ql. UEL 6.7%
c. Reactivity Hazard strong oxidizers
•
D. Corrosivity Hazard yes/DSJ. pH: --
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/DSJ.
Alpha particles yes/DSJ.
Beta particles yes/DSJ.
Gamma radiation yes/DSJ.
IV. REFERENCES
Cl) The Merck Index. 11th Edition. 1989
12) Pocket Guide to Chemical Hazards. NIOSH 1990
2
2
2
CJ) Threshold Limit values and Biological Exposure
Indices for 1994-95. ACGIH.
14} 29 CFR 1910.1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: bis <2-ethylhexvll pbthalate (Pi-sec-ocvtl nthalate)
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula ~G~2~4~6~J~6~P~4._ _________ _
Natural Physical State at 25°C .l~i~qu.,...i~d._ ____ _
Vapor Pressure -i~-~JM2 ___ mm Hg at 2O°C
Melting Point ____ °F/°C Boiling Point _____ °F/°C
Flash Point (QJ;llill or closed .l:J.U!) ~4~2~5~ ____ °C/':I
solubility -!,I/Ai.yo> insoluble in water
Other muscible w/ mineral oil and hexane
.l..__
.l..__
2....__
.l..__
.l..__
Physical Features: (odor, color, etc.) A light colored, odorless
liquid very viscous, (4)
II. TOXICOLOGICAL DATA
standards: Smg/m3(21 TLV s mg/m3(31 PEL none found IDLH
Routes of Exposure: inhalation, ingestion, eve contact, skin contact
Acute/chronic symptoms: a substance of low toxicity by all routes of
exposure irritating to eve, mucous membranes, nausea & diarrhea,
Suspect carcinoaen,{4)
First Aid: Inhalation; artificial respiration; Ingestion: aet
medical attention immediately; Eve contact; irrigate immediately:
Skin contact; soap and water wash immediately
• •
Chemical Name: bis {2-ethvlhexyl)phthalate
III. HAZARDOUS CHARACTERISTICS Reference
A. Combustibility Yes x__ No
Toxic by-products ~o~o~o~e.__ _____ _
B. Flammability LEL none found UEL
c. Reactivity Hazard ~o~o~o~e'--'f~o~uun~d.__ _________ _
D. Corrosivity Hazard yes/IJQ pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/IJQ
Alpha particles yes/IJQ
Beta particles yes/IJQ
Gamma radiation yes/IJQ
IV. REFERENCES
<4> Documentation of the TLYs, 4th Edition ACGIH, 1980
(5) Chemical Hazard Resconse Information System, us Coast
Guard. 1985
.5....__
.5....__
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Toluene (Methyl benzene. toluoll
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula C7H8 -~~~------
Natural Physical State at 25°C liquid
Vapor Pressure ----2..Q. mm Hg at 20°c
Melting Point ~°F/°C Boiling Point
Flash Point (open or closed cup) 40 ll0,6°F/°C
OC/°F.
1,2,3,4
1,2,3,4
1.3.4
1,2,3,4
Solubility -H20 slightly soluble 1,3.4
Other miscible with alcohol. 1.3.4
chloroform. ether. acetone.
glacial acetic acid. carbon
disulfide
Physical Features: (odor. color. etc.) colorless
liquid with an aromatic odor. IP 0.02 ev. (3) derived
from coal tar oil or petroleum Relative response on
II. TOXICOLOGICAL DATA
Standards: 50 ppm (5) TLV
100 ppm (6) PEL 2000 ppm (4) IDLH
Routes of Exposure:
contact. eye contact
inhalation; ingestion. skin
Acute/Chronic Symptoms:
headache. lassitude. and
Narcotic in high concentrations.
nausea. Chronic; anemia and
dermatitis. ( 2 l
First Aid: Inhalation; artificial respiration;
get medical attention immediately; Eye contact:
immediately; skin contact: soap and water wash
immediately
Ingestion;
irrigate
•
Chemical Name: .T~o~l~u~e~n~e~--------
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes x_ No
Toxic by-products
B. Flammability LEL .L...0..1 UEL -~7~-~0-%_
C. Reactivity Hazard strong oxidizers
•
D. Corrosivity Hazard yes/D!J_ pH: __
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/fill
Alpha particles yes/fill
Beta particles yes/fill
Gamma radiation yes/fill
IV. REFERENCES
(1) The Merck Index. 11th Edition. 1989
(2) Documentation of the TLV. 4th Edition. 19ao
3
(3) NIOSH Pocket Guide for Chemical Hazards. 1990
(4) NEPA. Protection Guide on Hazardous Materials.
8th Edition. 1984
(5) Threshold Limit values and Biological Exposure
Indices for 1994-1995.
(6) 29 CFR 1910.1000
4
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Xylene, o, M. & P (Dimethyl benzene}
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula ~--1iio--------
Natural Physical State at 25°C liquid
Vapor Pressure 1..::.2._ mm Hg at 20°c
Melting Point 13-14°F/0
~ Boiling Point 137-140°F/0
~ _l__
Flash Point (open or closed cup) 90/84/81°C/0
~
Solubility -H2O insoluble
Other soluble in alcohol, ether
and most other organic solvents.
Physical Features: (odor, color, etc.) colorless liguid with
aromatic/ benzene odor. common solvent for paints and coatings. IP -s.5 ev. HNU relative response with 10.2 ev probe -11.3, OVA relative response -111 -116%
II. TOXICOLOGICAL DATA
Standards: 100 ppm (2) TLV
IDLH
100 ppm (3) PEL 1,000 ppm (4)
Routes of Exposure: Inhalation, Ingestion, skin and/or Eye
contact
Acute/Chronic Symptoms: headache, fatigue. dizziness, lassitude.
narcotic effects in high concentrations [5.6). chronic effects not well defined (1),
First Aid: Inhalation: artificial respiration; Ingestion: get
medical attention immediately; Eye contact; irrigate immediately;
skin contact; soap and water wash immediately.
•
Chemical Name: Xylene. o. M. & P
III. HAZARDOUS CHARACTERISTICS Reference
E.
A. Combustibility Yes _x No
Toxic by-products
B. Flammability LEL 1.4% UEL .§...ll
c. Reactivity Hazard strong oxidizers
o. Corrosivity Hazard
Neutralizing agent:
Radioactive Hazard
Background yes/IlQ
Alpha particles yes/IlQ
Beta particles yes/IlQ
Gamma radiation yes/IlQ
yes/no pH:
Exposure Rate
IV. REFERENCES
111 The Merck Index. 11th Edition. 1989.
•
1.2.3.4
121 Threshold Limit Values and Biological Exposure Indices for 1994-1995.
13} 29 CFR 1910,1000
14} NIOSH Pocket Guide to chemical Hazards. 1990,
5} NFPA. Fire Protection Guide on Hazardous
Materials. Bth Edition. 1984,
16} Documentation of the TLV. 4th Edition. 1980
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Naphthalene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula _,,.C~l~O'--"H~8'-----------~
Natural Physical State at 25oC ~s~o~l~i~d~----~
Vapor Pressure _,,.Oi,~0~8'---mm Hg at 20oc
Melting Point 176°F/0 c Boiling Point -~42~4~~~•~F/°C
2
2
Flash Point (open or closed cupl 2
Solubility -H2O 0.0003\
other Benzene, absolute alcohol, ether
Physical Features: (odor, color, etc.)
with an odor of mothballs IP -8,12 ev C2l
II. TOXICOLOGICAL DATA
Colorless to brown solid
Standards: 10 ppm 14) TLV 10 ppm IS) PEL 500 ppm (2) IDLH
Routes of Exposure: Inhalation. skin absorption, Ingestion, Skin
and/or eve contact <2>
Acute/Chronic Symptoms: Eye irritation, headache, confusion,
excitement, malaise, nausea, vomiting, abdominal pain, irritation of
bladder, profuse sweating, jaundice, blood in the urine, presence of
free hemoglobin in the urine, kidney failure, dermatitis (2\,
First Aid: Inhalation: artificial respiration; Ingestion; aet
medical attention immediately; Eve contact; irrigate immediately;
Skin contact; soap and water wash immediately,
• •
Chemical Name; Nacthalene
III. HAZARDOUS CHARACTERISTICS Reference
A. Combustibility Yes ___z.. No ---2
Toxic by-products
B. Flammability LEL _ _.,o...,,_.9'-'%'--UEL 5.9%
c. Reactivity Hazard incompatible with strong oxidizers 2
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
Cl) The Merck Index. 11th Edition, 1989,
t2l NIOSH Pocket Guide to Chemical Hazards, 1990
(3) The Condensed Chemical Dictionary, 11th Edition, 1987
(4) Threshold Limit Values and Biological Exposure
Indicies. ACGIH. 1994-95
IS) 29 CFR 1910.1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: Perchloroethylene
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula _,,.C~2.......,,Cu1~4.__ __________ _
Natural Physical State at 25oC -~l~i~q~u~i~d._ ___ _
Vapor Pressure _ _...1~4 __ mm Hg at 200c
2
2
Melting Point _::-~2 __ 0~/oC Boiling Point 250 o~/oC __..2 __
Flash Point (open or closed cup) N/A oC/oF
Solubility - H20 0,015%
2
2
other misc with alcohol. ether,
chloroform, benzene
Physical Features: (odor, color, etc.) colorless
liquid with an odor like ether or chloroform IP-9.32 ev
r21 OVA Relative Response 70%
II. TOXICOLOGICAL DATA
suspect human
standards: 25 ppm/3)TLV 25 ppm /4)PEL carcinogen /2)IDLH
Routes of Exposure: Inhalation. Ingestion, Skin and/or
Eye contact /2}
Acute/Chronic Symptoms: Irritation of eyes, nose, and
throat. nausea. flushed face and neck. vertigo. dizziness,
incoordination, headache. carcinogen /2)
First Aid: Inhalation; artificial respiration;
get medical attention immediately; Eye contact;
immediately; Skin contact; soap and water wash
immediately.
Ingestion;
irrigate
•
Chemical Name: Perchloroethylene
III. HAZARDOUS CHARACTERISTICS
Reference
A. Combustibility Yes
Toxic by-products
B. Flammability LEL none
No _x__
UEL
•
none
c. Reactivity Hazard Incompatible with
oxidizers. chemically active metals. such as
lithium. and beryllium & barium; caustic soda;
hydroxide. potash <21
D. Corrosivity Hazard yes/no pH:
Neutralizing agent:
E. Radioactive Hazard Exposure Rate
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
1. The Merck Index. 11th Edition. 1989
2
strong
barium.
sodium
2. NIOSH Pocket Guide to Chemical Hazards. 1990
J. Threshold Limit values and Biological Exposure
Indices for 1994-95. ACGIH.
4. CFR 1910.1000.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: _P.y_r~e~n~e~-----------
I. PHYSICAL/CHEMICAL PROPERTIES
Reference
Chemical Formula .Q1.__J!1u----
Natural Physical State at 25°C _s_o_l_i-d~---~~
Vapor Pressure----~ mm Hg at 20°c
Melting Point ~°F/°C Boiling Point .i.QA°F/'.'..C
Flash Point (open or closed cup) ----~°C/°F
1. 2
1. 2
1. 2
Solubility -H2O insoluble 1.2
other partially soluble in organic solvents 1.2
=
Physical Features: (odor, color, etc.) Colorless
solid (impurities give a yellow color) (1,2)
II. TOXICOLOGICAL DATA
standards: no data TLV
IDLH
no data PEL
Routes of Exposure: Inhalation. Ingestion. Skin
absrobtion. Eye contact
no data
Acute/Chronic Symptoms: Pyrene is carcinogenic. absorbed
through the skin. and a skin irritant (3)
First Aid: Inhalation; artificial respiration; Ingestion;
get medical attention immediately; Eye contact; irrigate immediately; Skin contact; soap and water wash
immediately.
• •
Chemical Name: LP~y.r~e~o~e'-----------
III. HAZARDOUS CHARACTERISTICS Reference
A. Combustibility Yee~ No~
Toxic by-products When heated to combustion. pyreoe
emits acrid smoke and fumes
B.
c.
D.
Flammability LEL --~ UEL ---~
Reactivity Hazard
Corrosivity Hazard
Neutralizing agent:
E. Radioactive Hazard
Background yea/no
Alpha particles yea/no
Beta particles yea/no
Gamma radiation yea/no
IV. REFERENCES
yea/no pH:
Exposure Rate
1. The Merck Index. 11th Edition. 1989.
2. The condensed Chemical Dictionary. Hawley. 11th.
Edition. 1987.
J. CAMEO computer data base developed by EPA and NOAA.
1986.
• •
HAZARDOUS SUBSTANCE INFORMATION FORM
Chemical Name: ~a~e~n~z~o~c~a~J~p~yµr~e~n~e;;_ ______________ _
I. PHYSICAL/CHEMICAL PROPERTIES
Chemical Formula ~c~2~0_..a.1~2 ____ _
Natural Physical State at 2s0 c solid
Reference
1.2
1.2 Vapor Pressure _______ mm Hg at 20°c
Melting Point 179 °F/':..S;_ Boiling Point 310-312
1.2.3 Flash Point (open or closed cup) nonflanunable°C/°F
solubility -H2O insoluble in water 1.2.3
Other Slightly soluble in alcohol and
methanol. slightly soluble in benzene.
Physical Features: (odor, color, etc.)
faint aromatic odor 11.2.3)
II. TOXICOLOGICAL DATA
1.2
toluene. xylene,
Yellowish crystals
standards: TLV suspected human carcinogen (5)
PEL worker exposure by all routes should be carefully
controlled (4)
no data IDLH
with a
Routes of Exposure: Ingestion. Inhalation. skin/Eye contact
Acute/Chronic Symptoms: Irritation of lungs and skin.
bronchitis. coughing. breathing difficulty. Long-term exposure
may affect lungs. kidneys. skin. urinary tract. reproductive
First Aid: Inhalation; artificial respiration; Ingestion: get
medical attention immediately; Eye contact: irrigate
immediately; Skin contact: soap and water wash immediately.
•
Chemical Name: Benzo(aJpyrene
III. HAZARDOUS
CHARACTERISTIC
s Reference
A. Combustibility Yes No _x__
Toxic by-products this is a product-
of incomplete combustion
•
B. Flammability LEL ___ UEL ___ _
c. Reactivity Hazard Incompatible with strong oxidizers
D. Corrosivity Hazard
Neutralizing agent:
E. Radioactive Hazard
Background yes/no
Alpha particles yes/no
Beta particles yes/no
Gamma radiation yes/no
IV. REFERENCES
yes/no pH:
1. The Merck Index. 11th Edition. 1989.
Exposure Rate
2. The condensed chemical Dictionary. Hawley. 11th.
Edition. 1987.
3. chemical safety Data Guide. The Bureau of National
Affairs. 1985.
4. Threshold Limit Values and Biological Exposure Indices
for 1994-1995. ACGIH
5. 29 CFR 1910.1000
Frank G. Johns
Clerk
Terry T. Leitner
Chiol Deputy Clerk
•· •
UNITED STATES DISTRICT COURT
OFFtce OF THE CLERl< WF.STERN 01smlCT "~ NORTH CAROLINA ROOM 20•, CHARLES R. JONAS FEOEnAl. BUiLCINO •01 wesr mAoe STru!ET CHARLOTT!!, ~ORlll CIIROUNA 20202
FAX TRANSMISSION COVER SHEET
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DOCUMENT DESCRIPTlON: ___ J)YJ: ,>hte~/ . -~ (JS-I! {Is-(J;<1.rakc'c>
'
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coMMENTS:
(excluding transmittal page)
\
IP THERE ARE ANY PROBLtMS Wini THIS TRANSMISSION, PLEASE CALL(l<U)344-6200.
rn0 3110l~~H) -1~noJ l)l~lSICT sn
I 704)344•6203
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FAX(704)34~-6703 )
(
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Proceedings include ~vents between 6/20/94 and ?./12/96.
3,93crl86-ALL USA v. :Cherokee, et al MAG APPEAL
CLOSED
MAG APPEAL
CLOSEO . U.S. District Court
Western District of North Carolina (Charlotte)
CRIMINAL]DOCKET FOR CASE#: 93-CR-186-ALL
USA v. Cherokee, et ~l Filed: 0B/05/93 Dkt# in other court: iNone
6/20/94
6/21/94
6/21/94
6/22/.94
6/?.3/94
6/24/94
6/?.7/94
6/28/94
u'ury trial as to Resources Inc. Cherokee, Keith Norland
Ei.dF)on, Gene Wesley (Gabe) Hartsell held/continues w/
Govt: 1 s evidence. (srg) [Entry date 07 /11/94]
Jury trial as to Resources Inc. Cherokee, Keith Norland
Eid.ion, Gene Wesley (Gabe) Hartsell held/continues w/Govt's
evic)ence. (erg) [Entry date 07 /ll/94]
Jury trial as to Resources Inc. Cherokee, Keith Norland
Eidson, Gene Wesley (Gabe) Hartsell held/continues w/Govt's
evidence. (erg) (Entry date 07 /11/94] !
Jury trial as to Resources Inc. Cherokee, Keith Norland
Eidson, Gene Wesley (Gabe) Hartsell held/continues w/Govt's
evidence. At the conclitsion of Govt' s evidence, Def ts made
the !following MOTIONS; 1) to DISMISS, 2) to STRIKE
testiimony of Mr. Cornelius, 3) to DISMISS and 4) for
JUDGMENT OF ACQ. MOTIONS DENIED. DENIED. (srg) (Entry date 07/11/94) i
,Jur:\i' trial as to Resources Inc. Cherokee, Keith Norland
F.itl.sjon, Gene Wesley (Gabe) Hartsell held/continues. Defte
proceed to offer evitl.ence. (sr.g) [Entry date 07 /ll/94]
Jury trial as to Resources Inc. Cherokee, Keith Norland
Eid~on, Gene Wesley (Gabe) Hartsell held/continues w/Defts'
evidence. (srg) [Entry date 07 /11/94]
,Jur~ tri.al as to Resources Inc. Cherokee, Keith Norland
Eidson, Gene Wesley (Gabe) Hartsell held/continues w/Defts'
evidence. (See Defts' proffered evidence, Exhibit #88,
vid~o tapes.) (srg) [Entry date 07 /11/94)
Jury trial as to Resources 1.nc. Cherokee, Keith Norland
Eidson, Gene Wesley (Gabe) Hartsell held/continues w/Defts'
evidence. (See Oefts' offer of proof as recorded in the
recdrd.) Defts rest. GOVT'S REBUTTAL EVIDENCE -The Govt
proqeeds to offer rebuttal testimony. At the conclusion of
rebuttal evidence, the Govt rest. Defts renew Rule 29
Motion, Motion to Dismiss. MOTIONS OENIED. Final
Arguments. (srg) [Entry date 07 /11/94)
Docket as of Februarj 12, 1996 3:34 pm Page l
C:00 31107~~HJ -l~noJ lJI~lSia sn
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i
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Proceedings include Jvents between 6/20/94 and 2/12/96. 3:93crl86-ALL USA v. ICherokee, et al MAG APPEAL
6/29/94
6/29/94 260
7 /21/94 261
8/31/94 262
8/31/94 263
9/12/94
10/11/94 264
10/11/94 265
CLOSED Jury trial as to Resources rnc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabe) Hartsell held/continues w/the Judge's CHARGE. The Jury retires to deliberate at 10:15 a. m. and returns to open Court w/VERDICTS of GUILTY as to all Defta at 11:29 a. m. (Defts to remain on bond and was ordered not to contact any of the wits. sentencing deferred to Oat. term.) Deft.#1, Guilty as to cts 1-6, & 8. Deft #2, Guilty as to Cts 1-6, & 8. Deft #3, Guilty as to (:ts 1-6. (erg) [Entry date 07/11/94]
JURY VERDICT as to Resources Inc. Cherokee, Keith Norland EidJon, Gene We!ll.ey (Gabe) Hartsell Guilty: Resources Inc. Cherokee (1) count(s) 1, 2-6, 8, Keith Norland Eidson (2) count(s) 1, 2-6, B, Gene Wesley (Gabe) Hartsell (3) count (s) 1, 2-6 (srg) [Entry date 07/11/94)
Sen~encing set for 9, 30 9/19/94 for Resou~·ces Inc. Che~ok~e, f.ot' Keith Norland Eidson, for Gene Wesley (Gabe) Hartlsell , Resources Inc. Cherokee (l) count(s) 1, 2-6, B, Keif,h Not'land Eidson (2) count(s) l, 2-6, 8, Gene Wesley (Gabe) Hartsell (3) count(s) 1, 2-6 (srg) [Entry date 07/11/94]
C,TA i:.o as to Theodore Karl Glauser Authorization to Pay H, M. Whitesl.des $ 16,604.58 Voucher# 0678181] ( Signed by Judge Robert D. Potter ) (mga) [Entry date 07 /21/94]
CJA ',21 as to Keith Not'land Eidson Ai1thorization to Pay Kris Turschmld $ l,.423. 03 for Expert Services voucher it 0161!140 ( Signed by Judge Robert D. Potter ) (mga) [En~ry date 09/01/94)
CJAi21 as to Theodore Karl Glauser Authorization to Pay Kris 'I'ursohmid $ 2,225.86 for Expert Services voucher# 0161140 ( Signed by Judge Robert D, Potter ) (mga) (Entry date 09/01/94)
Deadline updated as to Resources Inc. Cherokee, Keith Norl;and Eidson, Gene Wesley (Gabe) Hartsell, set Sentiencing for 4:00 9/21/94 for Resources Inc. Cherokee, for ,Keith Norland F.idson, for Gene Wesley (Gabe) Hartsell (ssJi) (Entry date 09/12/94]
' MOTION by Keith Norland Eidson, Gene Wesley (Gabe) Hartsell to Continue Sentencing Hearing (mga) [Entry date 10/12/94]
MOTJ;ON by Ke:ith Norland Eidson, Gene Wesley (Gabe) Hartsell for ',New Trial (mga) [Entry date 10/12/94]
Docket as of Februar~ 12, 1996 3:34 pm Page 2
£00 3110l~~HJ -l~noJ lJI~lSIU sn
ProcAAdings 1.nclude ~vents between 6/20/94 and 2/12/96. 3:93cr186-ALL USA v. !Cherokee, et al MAG hPPEAL
10/11/94 --
10/11/94 --
10/12/94 261'i
10/17/94 267
10/17/94 ?.68
10/17/94 269
10/1R/94 ?.70
10/18/94 271
10/18/94 272
10/19/94 273
I CLOSED ORAi, ORDER as to Keith Norland Eidson, Gene Wesley (Gabe) Har1j:lle11 denyi.ng [265-l] motion for New Trial as to Keith Norland Eidson (2), Gene Wesley (Gabe) Hartsell (3), denying (264-1] mot.i.on to Continue as to Keith Norland Eidson (2), Gene We~ley (Gabe) Hartsell (3) ( Entered by Judge Robert D. Potter ) (mga) [Entry date 10/12/94)
Sf'\nt.Ancing held Resources Inc. Cherokee (1) count (s) 1, 2-6; 8, Keith Norland Eidson (2) count(s) 1, 2-6, 81 Gene Wesley (Gabe) Hartsell (3) count(s) 1, 2-6 (srg) [En~ry date 10/14/94]
NOTICE OF APPEAL by Gene Wesley (Gabe) Hartsell (3) cou,:it(e) 1, 2-6 cc: Counsel, USM and USPO (mga) [En~ry date 10/18/94]
JtIDQMENT Reeourcee Inc. Cherokee (1) count(s) 1, 2 -6 1 B . FOUR (4) YEARS PROBATION, $50,000 FINE and $1,100 ASS~SSMENT ( Signed by Judge Robert D. Potter) ( Crim Judge Vol: 43 Page 1 65) (mga) [Entry date 10/18/94]
,JUDGMENT Keith Norland Eidson (2) ccunt (s) 1, 2 -6 1 8 FIFTY ONE (51) MONT~IS IMPRISONM2NT each count to run concurrently, THREE (3) YEARS SUPERVISED RELEASE, $5,000 FINE and $350 ASSESSMENT ( Si.gned by Judge Robert 0. Potter ) ( 'Crim Judge Vol: 46 Page: 66) (mga) [Entry date 10/18/94] ;
,JlJOOMF.NT Gene WP.\sley (Gabe) Hartsell (3) count (s) 1, FIFTY ONE ! ( 51) MONTHS IMPlHSONMENT, THREE ( 3) YEARS SUPERVISED RELEASE each ct. to ,cun concurrently, $10,000 FINE on all counts and $50 ASSESSMENT, Gene Wesley (Gabe) Ha,ctsell (3) count(e) 2-6. THIRTY SIX (36) MONTHS IMPRISONMENT ea ct to run concurrently with ct. 1, THREE (3) YEARS SUPERVISED RELSASE each ct. to run concurrently, $10,000 FINE on all counts and $250 ASSESSMENT ( Signed by Judge Robert D. Pottier ) ( Crim Judge Vol, 46 Page, 67) (mga) [Entry date 10/18/94]
MOTION by Keith Norland Eidson for Payment of Expert Feea (mg.\) [Entry date 10/18/94]
CJA 20 as to Gene Wesley (Gabe) Harteell Authorization to P.ay:Tlil"l'F.RTM PAYMENT Edward A. Fiorella$ 11,448.01 Voucher II 0619430 ( Signed by Judge Robert D. Potter ) (cat) [En~ry date 10/18/94]
C,TA :20 as to Gene Wesley (Gabe) Hartsell : Appointment of Attorney Edward A. Fi.orella (Fiorella has been paid interim payment, so new/final voucher prepared), voucher# 0619430 (cati) [Entry date 10/18/94]
NOTICE OF APPEi\.!. by Keith Norland Eidson (2) count(s) 1 1 2-6,i 8 cc, Counsel, USM and USPO (mga) [Enqry date 10/19/94]
Docket as of February 12, 1996 3:34 pm Page 3
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Proceedings include ~vents between 6/20/94 and 2/12/96.
3:93crl86-ALL USA v. ;Cherokee, et al MAG APPEAL
10/19/94 2?4
10/19/94 --
1.o/✓.1/g4 7.75
10/24/94 --
10/25/94 2?6
10/?.7 /94 ?.77
10/27/94 279
10/2?/94 280
10/2?/94 281
10/2?/94 --
10/27/g4 --
10/31/94 --
CLOSED
MOT!ON hy Ke.i.th Norland Eidson to be Released on Bond
Pending Appeal f.rom a Judgment of Conviction (mga)
[En~ry date 10/19/94]
Notice of appeal and certified copy of docket as to Keith
Norland F.idson, Gene Wesley (Gabe) Hartsell to USCA:
[27~-1] appeal, [266-1] appeal (mga) [Entry date 10/19/9<1]
NOTiCB
?.-6; 8
[Entry
OF APPEAL by Resources Inc. Cherokee
cc: Counsel, USM and USPO (mga)
date 10/24/94]
(1) count(s) 1,
Notice of appeal and certified copy of docket as to
Resources Inc. Cherokeo;, to !JSCA, (275-1] appeal (mga)
[Entry date 10/24/94)
ORDER as to Keith Norland Eidson granting (270-1) motion as
t::o !(.el.th Norland Eidson (2) ( Sig:ned by Judge Robert D.
Potter ) (mga) [Entry date 10/26/94)
PRESENTENCE INVESTIGATION REPORT (Sealed) as to Keith
Norland Eidson (mga) [Entry date 10/27/91]
P.RRSRN'l'ENCE INVESTIGATION' REPORT (Sealed) as to Gene Wesley
(C:labe) Hartsell (mga) [Entry date 10/27/94]
i
PRESENTENCE INVESTIGATION RRPORT (Sealed) as to Resources
Inc.' Cherokee (mga) [Entry date 10/27/94]
MOTION by Gene Wesley (Gabe) Hartsell to be Released
Pending Appeal from Judgment on Bond (mga)
[Entry date 10/31/94]
RES~ONSE by USA aa to Kelth Norland Eidson, Gene Wesley
(Gabe) Hartsell in opposition to [280-1] motion to be
Released Pending Appeal from Judgment on Bond, (274-1]
mot.{on to be Released on Bond (mga) [Entry date 10/31/94)
USCJ\. Case Number aa to Gene Wesley (Gabe) Hartsell Re,
(266-1] appeal USCA Number: 94-5796 (mga)
[Entjry date 10/31/94]
IJSCA Case Number as to Keith Norland Eidson Re: [273-l]
app,ial. USCA Number: 94-5797 consolidated w/94-5796 (mga) [Enqry date 10/31/94]
' USCA Case Number as to Resources Inc. Cherokee Re, (275-1]
appaal USCA Number, 94•5804 consolidated w/94-5796 (mga)
[Entry date 10/31/94)
Docket as of February 12, 1996 3:34 pm Page 4
500 31101~1:JH) -1~nm 1)1~1s1a sn
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Proceedings include ~vents between 6/20/94 and 2/12/96. 3:93cr186-ALL USA v. :cherokee, et al MAG APPE:AL
11/1/94 282
11/2/94 283
11/4/94 284
11/8/94 285
11/22/94 286
12/9/94
12/19/94 287
1/19/95 291
CLOSED ORDER a~ to Gene Wesley (Gabe) Hartsell denying (280-1] motion to be Released Pendl,ng Appeal from Judgment on Bond as to Gene Wesley (Gabe) Hai:-tsell (3) ( signed by Judge Rob'!'rt D. Potter l (mga) [Entry date 11/01/94]
MEMORANnT,JM by Gene Wesley (Gabe) Hartsell in support of their Motion for Release Pending Appeal (mga) [En¢ry date 11/03/94]
!
MOTION by Keith Norland Eidson and Gene Wesley (Gabe) Hartsell for Reconsideration of [282-1] order (mga) [En¢ry date 11/04/94]
ORDER as to Keith Norland Eidson, Gene Wesley (Gabe) Hartsell denying (284-1] motion for Reconsideration of [282-1) order as to Gene Wesley (Gabe) Hartsell (3), denying [274-1] motion to be Released on Bond as to Keith Norland Eidson (2) ( Signed by Judge Robert D. Potter l (mga) (Entry date 11/09/94)
MOT:tON by Theodore Karl Glauser for Payment of Expert Feei:i (mga) (Entry date 11/22/94]
TRANSCRIPT Trial fil,;d as to Resources Inc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabel Hartsell for dates of 6/16/94 thru 6/27/94 Re: [275-1] appeal, [273-1) appeal, (?.66-1] appeal (mga) [Entry date 12/12/94) [Edit date 12/12/94)
TRANSCRTPT Sentencing filed as to Resources Inc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabe) Hartsell for date of 10/12/94 Re: [275-1] appeal, [273-1] appeal, (266-1] app<1al (mgal [EntJ:y date 12/12/94] [Edit date 12/12/94]
Judgment Returned Executed as to Keith Norland Eidson; on ll/~9/94 (mga) [Entry date 12/19/94]
,Judgment Returned Executed as to Gene Wesley (Gabe) Hartsell ; on 11/30/94 (mga) [Entry date 12/19/94)
C,TA .20 as to K,;{th Norland Eidson Authorization to Pay Dale Morrison$ 12,464.05 Voucher# 0619435 ( Signed by Jud(l'e Robert D. Potter l (mga) (Entry date 01/04/95]
C,TA ;21 as to R"Rm1rces Inc, Cherokee, Keith Norland Eidson, Gene Wesley (Gab-,) Hartsell .Authorization to Pay Kris H. ·rurschmid $ 940. oo for Expert services Voucher ff 0161152 ( Sigl'\ed by Judge Robert D. Potter) (mga) [Entry date 01/04/95]
ORD~R as to Resources Inc. Cherokee, Keith Norland Eidson, GenA Wesley (Gabe) Hartsell, Theodore Karl Glauser granting [286-1] motion as to Theodore Karl Glauser (4) ( Signed by ,Judge Robert D. Potter ) (mga) [Entry date 01/19/95)
Docket as of Februar~ 12, 1996 3134 pm Page 5
900 3110ld~H) -ldnO) l)ldlSia sn 91 :91
t
l I ,,
• •
Proceedings include \"vents between 6/20/94 and 2/12/96, 3:93crl86-ALL USA v.:cherokee, et al MAG
CLOSED
Al?P!U\L
1/19/95 292
3/22/95 293
4/7/95 294
5/15/()5
2/2/96 296
C,TA: 21 as to Resources Inc. Cherokee, Keith Norland E:idson, Gene Wesley (Gabe) Hartsell, Theodore Karl Glauser , Appc;:d.ntment of Kris H. Turschmid as Expert. Voucher II 016:).16?, ( Signed by Judge Robert D. Potter ) (mga) (En~ry date 01/19/95)
ORD~R re: payment of expert services provided by Steve Hartness of Acumen Investigative 8vc as to Keith Norland Eidson, Gene Wesley (Gabe) Hartsell, Theodore Karl Glauser, Voucher #0161138 dated 11/5/93 for Oft. Glauser is null & void, Vour,her #01611.39 dated 11/23/93 for Oft. Hartsell is null & voi.d, Voucher #645155 dated 4/4/94 for Dft Eidson iA null & void, Voucher #0161158 dated 11/2/93 for Dft: Gl1meer .l.s APP.ROVED as amended and forwarded to Circuit: Judge subject to final approval ( Signed by Judge Robert D. ~otter ) (bsw) (Entry date 03/23/95)
CJA 21 as to Resources Inc. Cherokee Authorization to Pay Kris TUrschmid $ 4, 045. oo for Expert Services Voucher ti 0161162 ( Signed by Judge Robert D. Potter ) (jlk) [Entry date 04/10/95]
C,JA: ?.1 as to Theodore Karl Glauser Authori:!:ation to Pay s~.eve Har:t.ness $ 4104. 64 for Expert Services Voucher # Ot6i1.S8 ( Signed by Judge Robert D. Potter and Judge Sam Er.vin, III) (jlk) [Entry date 05/05/95]
'l'r..arismi.tt.sd Clerk' a Certificate to USCA certifying record is complete re: (275-1] appeal by Resources Inc. Cherokee, [273-1] appeal by Keith Norland Eidson, [266-1) appeal by Gfmt?. Wesley (Gabel Hartsell (chh) (Entry date 05/18/95]
MO'!'lON by Resources Inc. Cherokee, Keith Norland Eidson, Gene Wesley (Gabe) Hartsell for New Trial (jlk) (En~ry date 02/02/96]
Docket as of Februar~ 12, 1996 3:34 pm Page 6
'
l00 3110l~~HJ -l~noJ lJl~lSicr sn
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State of North Carolina
J\IICIIAEL F. EASLEY
ATTl>HNE\' GENEHAI,
Via Facsimile
Harriet Fisher
3304 Criminal Court Building
700 East 4th Street
Charlotte, NC 28202
l>t.'llilrlllH_'lll ()j .ltlSliCl'
1'.<). IH>Xti:!!l
Hr\! .El< iH
February 7, 1996
Reply to Robert R. Gelblum
Environmental Division
[phone]
Fax -[phone]
[e-mail]
Re: Administrative Search Warrant
120 I Berryhill Rd., Charlotte
Dea Ms. Fisher:
Faxed herewith, as you and I discussed my sending, is an affidavit my client Doug Moore,
of the state Superfund Section, and I have prepared, for Doug's signature, setting forth the basis for
the State's desire for an administrative search warrant to enter, and obtain environmental samples
from, the above-referenced property. As I stated, though Doug is still not precisely certain what day
in the near future he will be in a position to travel from Raleigh to Charlotte to see to this work, I am
faxing the draft affidavit in hopes someone there could review it for anything seen as deficiencies,
in order to expedite Doug's obtaining of a Superior Court judge's signature when he actually does
come down.
Thenk you for your help.
c: Doug Moore ,/
Yours truly, ,1, rrrn u~-----
Robert R. Gelblum
Assistant Attorney General
•
STA TE OF NORTH CAROLINA
In the General Court of Justice
Mecklenburg County
)
)
)
)
)
)
•
AFFIDAVIT TO OBTAIN
ADMINISTRATIVE
INSPECTION WARRANT
FOR PARTICULAR
CONDITION OR
·ACTIVITY
1. The undersigned is an Environmental Chemist with the CERCLA Branch of the
Superfund Section, Division of Solid Waste Management, North Carolina Department of
Environment, Health and Natural Resources appearing this day to request an administrative
search warrant for the Cherokee Oil Company Site ("site"), 1201 Berryhill Road, Charlotte,
Mecklenburg County, North Carolina.
2. The site is registered as parcel #16, block #51, tax map #71 at the Mecklenburg
County Tax Assessors office.
3. The site is owned by Gene Wesley Hartsell, as recorded in Deed Book #5828, Page
#0131 at the Mecklenburg County Register of Deeds.
4. The site was formerly operated by Cherokee Resources, Inc. ("Cherokee"), a
corporation incorporated under the laws of the State ofNorth Carolina with its principal place
of business at 1201 Berryhill Road, Charlotte, North Carolina.
5. Keith Norland Eidson was President and chief operating officer of Cherokee and had
a fifty percent (50%) ownership interest in Cherokee. Gene Wesley Hartsell was Vice
President of Cherokee and had a fifty ( 50%) ownership interest in Cherokee.
6. Cherokee was in the business of, among other things, reclaiming waste oil for energy
recovery and treating and disposing of oil-contaminated wastewaters, as well as treating other
industrial wastewaters at the site. Cherokee Resources used the site as a waste oil processing
facility.
7. · In July 1991, a criminal investigation was conducted by the EPA Hazardous Waste
Section, the EPA Criminal Investigation Division, the Office of the FBI, and several other
state and local authorities. A criminal search warrant was served on the owner of the site and
a criminal investigation was conducted at Cherokee Oil's 1201 Berryhill Road facility and at
a Cherokee Oil facility at 925 South Summit Avenue, Charlotte.
8. As a result of the criminal investigation, Keith Norland Eidson, Gene Wesley Hartsell
and Theodore Karl Glauser were indicted on charges of conspiracy to violate the federal
Clean Water Act by illegally disposing of and otherwise handling wastewaters in violation of
permit limitation.
•
Affidavit for 1201 Berryhill Road
Page2
•
9. In 1991, EPA detennined the Summit Avenue location posed an imminent and
substantial endangerment to public health, or welfare, or the environment. Between August
1991 and March 1993, the EPA Emergency Response and Removal Branch ("ERRB")
conducted an extensive emergency removal action at Cherokee Oil's 925 South Summit
Avenue location. The South Summit Avenue location was an unpennitted temporary storage
facility operated by Cherokee Resources from August 1990 to August 1991.
10. EPA identified approximately 6,096 drums, 13 roll-off containers of contaminated
soil, several tankers containing liquid waste and trailers containing drums stored at the
Summit Avenue site. The wastes stored at the Summit Avenue location included
polychlorinated biphenyls (PCB's), highly flammable solvents, cyanides, strong acids and
bases, hazardous organic compounds and hazardous inorganic substances.
1 I. In 1993, Keith Norland Eidson and Gene Wesley Hartsell were convicted of
conspiracy to violate the federal Clean Water Act. In 1994, Eidson and Hartsell were given
active sentences which they are currently serving at Seymour Johnson Air Force Base.
12. On Tuesday, January 30, 1996, I telephoned Gene Wesley Hartsell to seek his
authorization to enter the site for the purpose of collecting environmental samples. Mr.
Hartsell stated that before he allows anyone to enter his property, he wants to inspect the
property following EP A's removal action. He stated that he would be willing to allow us to
collect soil samples after he gets out of prison. When I asked him for a specific time, Mr.
Hartsell responded that his conviction was under appeal and that he could be released as soon
as Friday, February 2, 1996 or as late as August 1998.
13. I asked Mr. Hartsell if he could have a representative meet us at the site to observe
the sampling event. Mr. Hartsell stated that he wants to have a representative at the site when
any soil samples are taken from his property. We both agreed that he would attempt to locate
a representative and that I would contact him on Tuesday, February 6, 1996 in order to
discuss the sampling event.
14. I in fact telephoned Mr. Hartsell on February 6th, but was told by a Seymour Johnson
official named Robin Woodard, who left the phone to tell Mr. Hartsell ofmy call, that Mr.
Hartsell had said that he would not speak to me, that his attorney had told him he does not
have to assent to our going on the site, and that he will write me a letter. Based on a call to
the 4th Circuit Court of Appeals on February 5th, oral argument on Mr. Hartsell's appeal was
heard on February 2nd.
15. Cherokee used the site as an unpennitted temporary storage facility housing drums,
above-ground tanks, underground tanks, vats, tanker trailers and roll-offs containing
polychlorinated biphenyls, flammable solids and liquids, strong acids and bases, hazardous
organic compounds, hazardous inorganic compounds, waste oil and sludges.
•
Affidavit for 120 I Benyhill Road
Page 3
•
16. Many of the 2,856 drums found at the site were stacked both inside and outside the
warehouse with incompatible waste types stored adjacent to each other. A number of
containers had corroded causing the contents to leak onto the floor of the warehouse and to
the surface of the soil surrounding the warehouse. A large volume of free-standing oily liquid
and sludge covered the surface soils within three diked basin areas on the site. In September
1994, EPA determined the 1201 Benyhill Road site posed an imminent and substantial
endangerment to public health, or welfare, or the environment.
17. Between November 1994 and December 1995, EPA-ERRB conducted a second
extensive emergency removal action at the Cherokee Oil's 1201 Benyhill Road location to
remove the imminent threat.
18. In 1990, Mecklenburg County Department of Environmental Protection videotaped
a release of an oily material from the site onto a neighboring property at Suburban Propane.
The historic releases may have resulted in actual or potential exposure of workers to
hazardous substances.
19. The overland runoff release was intercepted by three storm sewer manholes where it
was directed south, underground, to an outlet on an unnamed tributary of Stewarts Creek
("UT"). The UT directs the runoff east to Stewarts Creek. Stewarts Creek is reportedly
used for recreational fishing. The historic release may pose an actual or potential threat of
exposure to hazardous substances on the part of nearby animals, food chain species and/or
human beings.
20. A limited number of samples collected by EPA during the removal action
demonstrates residual soil contamination at the site. Releases from the site may pose an
threat to nearby workers, food chain species and/or human health.
21. Due to the types of residual contamination remaining at the site, the potential threat
posed by historic releases and the inability to coordinate the sampling event with Mr. Hartsell,
the CERCLA Branch requests an administrative search warrant to collect additional
environmental samples from the site as part of an environmental assessment of 1201 Benyhill
Road. The samples will be used to determine the threat posed to human health and the
environment from historic releases. The assessment will also be used to determine the need
for additional investigation under CERCLA and/or other legal authorities.
Douglas B. Moore
Sworn and subscribed to before me.
Date Superior Court Judge
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•
Memo
Date: February 6, 1996
To:
From:
Re:
File
Douglas Moore
Environmental Chemist
NC Superfund Section
Site Access
Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg County, N.C.
US EPA ID: NCD 980 799 019
On Tuesday, January 30, 1996, I called Mr. Gary Miller, Seymour Johnson Air Force
Base -Federal Prison Center case manager [phone]. Mr. Miller is the case
manager for Mr. Gene W. Hartsell, inmate at the federal prison center. Mr. Hartsell is the
legal owner of the Cherokee Oil Company site. Mr. Miller arranged for me to have a
phone conversation with Mr. Hartsell to gain access to the subject site.
I identified myself and explained to Mr. Hartsell that I was conducting an environmetnal
assessment on behalf of the EPA for the subject site. The investigation includes
collection of environmental samples to address the long-term concerns related to historic
releases from the site. Mr. Hartsell stated that there were no releases from the site to any
neighboring properties. I recalled to Mr. Hartsell a videotape of a historic release from
the site to the neighboring Suburban Propane property. He stated that Cherokee
specifically constructed catch basins at the site to prevent runoff from leaving the site and
that the catch basins functioned as they were designed. Mr. Hartsell denied that the
release was a result of activities at the Cherokee Oil Company site. Mr. Hartsell claims
that the site does not pose an endangerment to the public health or the environment.
I told him that according to the Mecklenburg County Register of Deeds, he was the legal
property owner. He stated that technically the property was owned by a company named
"Centennial, Inc.", who in turn had sold the property to him. Since he had not paid for the
property, the property technically reverts back to Centennial. I asked him who owns
Centennial. He stated that he is one of the owners. I asked him if there were any other
owners of Centennial. He stated that there were not.
•
I told Mr. Hartsell that we wanted to collect three soil samples to further assess any
residual soil contamination that may remain at the site. He stated his opinion that we
were conducting a repetitive investigation and that EPA had already collected the samples
we needed to collect. I reminded him that EPA confined its removal action to the
immediate abatement of on-site threats and that we were collecting off-site samples as
well to address other potential environmental impacts.
Mr. Hartsell stated that before he allows anyone to enter his property, he wants to inspect
the property following EPA's removal action. He stated that he would be willing to allow
us to collect soil samples after he gets out of prison. I explained that I had a deadline to
meet and asked him for a specific time. Mr. Hartsell's responsed that his conviction was
under appeal and that he could be released as soon as Friday, February 2, 1996 or as late
as August 1998.
I asked Mr. Hartsell if he could have a representative meet us at the site to observe the
sampling event. Mr. Hartsell stated that he wants to have a representative at the site when
any soil samples are taken from his property. We both agreed that he would attempt to
locate a representative and that I would contact him on Tuesday, February 6, 1996 in
order to make arrangements for collecting the requested samples.
On Tuesday, February 6, 1996, I called Seymour Johnson AFB -FPC [phone] and
spoke with Mrs. Robin Woodard. Mr. Gary Miller, case manager for Gene W. Hartsell
was not present at the facility and would not be available until after 12:30 p.m .. Robert
Gelblum, assistant attourney general with the N.C. Attourney Generals office was present
as a witness to the conversation. I explained to Mrs. Woodard that I worked for the State
Division of Solid Waste Management, that I was conducting an environmental
investigation on a property in Charlotte owned by inmate Gene W. Hartsell, that I had
previously spoken with Mr. Hartsell to arrange to collect environmental samples from his
property and that Mr. Hartsell had agreed to speak with me on this day. Mrs. Woodard
stated that she would page Mr. Hartsell and that we could wait on the phone or call beack
in S minutes. We decided to call back. I called back Mrs. Woodard about 10 minutes
later.
Mrs. Woodard stated that she had spoke with Mr. Hartsell and told him that someone
with the State Division of Solid Waste Management had contacted her and requested to
speak with him. Mrs. Woodard stated that Mr. Hartsell stated to her that he was not
interested in speaking with us on the phone. She stated that Mr. Hartsell asked her to get
my name and address and that Mr. Hartsell would write us a letter. She stated that he told
her that he had spoken with his lawyer and that his lawyer had advised him that he did
not have to let us onto his property, unless he was present. Mr. Gelblum interjected at
this point and stated to Mrs. Woodard that the property in question has been shown to
have contained hazardous wastes and that the State was investigated the property as a
potential human health threat. She advised that we sue Mr. Hartsell to gain access to the
site. She asked if this was a civil matter. Mr. Gel bl um indicated that at this time it was a
civil matter, but that Mr. Hartsell was placing himself at risk and could face possible
• •
criminal penalties for obstructing an investigation. She asked for our names and
addresses, which was given to her to transfer to Mr. Hartsell. Both I and Mr. Gelblum
asked her to request the name of Mr. Hartsell's attourney, in order to facilitate any future
negotiations on this matter. She stated that she would transmit this information to the
case manager, Gary Miller, and that she and Mr. Miller would talk with Mr. Hartsell this
afternoon and attempt to persuade him to speak with us on the phone.
.... OHM Remedialio,
, Services Corp. ~--==-A Subsidiary of OHM Corporation
January 24, 1996
Mr. Douglas Moore
North Carolina Dept. Of Environmental Health
and Natural Resources
Superfund Section
Division of Solid Waste Management
401 Oberlin Road, Suite 150
Raleigh, NC 27605
Dear Mr. Moore:
RECEIVED
JAN 251996
SUPERFUND SECTION
Enclosed please find a set of keys for the Cherokee Oil -Berryhill Road Site located in Charlotte,
North Carolina. In case you need to call me or page me, my numbers are as follows:
1/800/999-6710, Pin #997-6021 (Pager)
770-453-7722 (Office)
If you have any further questions or need anything else, please give me a call.
Sincerely,
OHM REMEDIATION SERVICES CORP. Im !It~ 1-t~td--
John A. Custance
Program Manager
JAC/lhw/0601.11r
pc: Steve Spurlin
Jack Kilbarger
5335 Triangle Parkway, Suite 450 c Norcross, Georgia 30092 D 404-729-3900
•
Memo
Date: December 22, 1995
To: File
From: Douglas Moore 4 f?>.,U,..,,____,
Environmental Chemist
NC Superfund Section
Re: Follow-Up On-Site Reconnaissance
Cherokee Oil Company Site
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCO 980 799 019
•
On Wednesday, December 20, 1995, Doug Moore of the NC Superfund Section travelled
to the subject site to conduct a follow-up on-site reconnaissance. At 10:45, I arrived at
the subject site and met with EPA federal on-scene coordinator Steve Spurlin. Mr.
Spurlin provided copies of analytical results from soil samples collected by EPA during
the removal action. He also presented a discussion of the analytical results in relation to
EPA's removal action.
At 11 :00, Jarrell Wootan of Mecklenburg County Department of Environmental
Protection (MCDEP) arrived at the site.
Mr. Spurlin provided a sampling grid map established for the drum staging area located
northwest of the site across Berryhill Road and analytical results that correspond to
sample points as outlined on the map. The sampling map and analytical results are
attached to the back of this memo. Mr. Spurlin indicated that Grids #I and #2 correspond
to the main staging areas for drums removed from the subject site. Grids #3 and #4
represent areas where materials removed from the drums were handled and transferred to
appropriate shipping containers prior to removal off-site to RCRA facilities. The
analytical results exhibit residual levels of BETX (benzene, ethylbenzene, toluene, and
xylene), chlorinated solvents and polynuclear aromatic hydrocarbons (PAH) in soil
samples removed from these locations. Mr. Spurlin believes the PAH's identified in the
soil samples originated from a layer of coal that was encountered under the staging area
when EPA scraped the surface of the site. He stated that the BETX and chlorinated
solvents may have resulted from leaking drums that were staged on the property.
He stated that EPA scraped surface soils from this location and removed visibly
contaminated soils from the staging area. He indicated that the levels found in the
I
• •
subsurface soils were well below regulatory levels for a removal action. EPA then
brought in clean backfill, applied a surface layer of clean soil to the drum staging area,
and reseeded the area.
Mr. Spurlin stated that EPA removed three underground storage tanks (UST) from a
refueling island located at the southwest corner of the site. In the process, EPA excavated
approximately 100 cubic yards of soil from around and under the UST's and stockpiled on
the site.
A soil sample (CO-WS-28) collected from the bottom of the excavation at UST #8
exhibited elevated concentrations of BETX compounds, tetrachloroethene and two
different phthalates in a tight red clay. Mr. Spurlin stated that the levels found at the base
of the excavation pit were below EPA regulatory concerns for a removal action and that
EPA backfilled the excavation with clean soil.
A soil sample (CO-WS-38) collected from the stockpile exhibited elevated concentrations
of ketones, BETX compounds, methylnaphthalene and several phthalates. Mr. Spurlin
indicated that the levels of contaminants found in the soils were below EPA regulatory
levels for a removal action. He stated that EPA plans to use the stockpile to regrade the
site to route the surface drainage towards the southeast corner of the site.
At 11:20, Jarrell Wootan, Steve Spurlin and Doug Moore toured the site. The site is
surrounded by a chain link fence topped with concertina wire. A former gap in the fence
at the southwest corner of the site has been fenced with a gate. There were several piles
of soil visible over the surface of the site: some with plastic tarpaulines, some uncovered.
In the center of the site is a rectangular warehouse. A muddy, open lot is located between
the warehouse and Berryhill Road. I took a panoramic photograph of the site from the
northwest corner entrance to the site.
We walked across the open lot to a soil pile covered by a plastic tarpauline, located near
the southwest corner of the site at the approximate location of the former refueling island.
Steve Spurlin stated that this was the area where the UST's were located. A large front
end loader was observed putting soil into a roll-off container at this location. Mr. Spurlin
stated that this is the soil stockpile that corresponds to soil sample CO-WS-38. Mr.
Spurlin said EPA removed three large, approximately 20,000 gallon underground storage
tanks from this location. There was a 1-1.5 foot thick concrete pad and two concrete
pyrimad shaped structures covering the UST's. The pyramid shaped structures had
several uncapped fill pipes running into the ground. EPA demolished the concrete
structures and pad in order to get to the UST's. Underneath the pad, they encountered a
layer of oil saturated gravel that was approximately I foot thick. EPA removed the oily
waste from the excavation, stockpiled, manifested and shipped it off-site. A red clay
layer was encountered below the gravel.
Mr. Spurlin stated that the UST's were aligned side by side in a direction parallel to
Berryhill Road (see figure in field notes). EPA labeled the three USTs #7, #8 and #9 in
2
• •
order of location descending from furthest away to nearest Berryhill Road. Mr. Spurlin
also stated that the oily layer was heaviest near UST #7 and believes that the material may
have originated from leaky distribution pipes that connected to a loading platform located
southeast of the UST's. He also indicated that a terra cotta pipe was encountered at this
location, which he thinks may be associated with a former sewer system drain field. He
suggested that the oily material may also have come from the terracotta pipe.
The depth to the base of the excavation was approximately 14 feet. The soil from the
excavation was stockpiled on site, sampled by EPA, and covered with a plastic tarpauline.
EPA also collected a soil sample from the base of the excavation under UST #8. Later,
EPA backfilled the excavation with clean soil. The materials contained inside the UST's
were pumped out, manifested and shipped off-site to RCRA disposal facilities. The
UST's were cut into pieces and removed from the site. Mr. Spurlin indicated that the
UST's contained waste oil and sludge. EPA plans to reuse the stockpiled soils from the
UST excavation to regrade the overland drainage towards the southeast corner of the site.
During the August 1995 on-site reconnaissance, an elevated concrete and wood loading
platform was observed at the south end of the warehouse. The platform was covered by a
tin roof and housed two large, steel-plated, square vats. At the east side of the loading
platform there were 6 large, approx. 20,000 gallon above-ground storage tanks (AST).
Under the AST's was a containment wall composed of cinderblocks, labeled
"containment area #2" by EPA. Another cinderblock wall was located at the south end of
the loading platform that was built to serve as a containment basin. This was labeled
"containment area #I" by EPA.
During the December 1995 on-site reconnaissance, the elevated platform and associated
steel plated vats, the 6 above-ground storage tanks and containment areas #I and #2 have
been demolished. One large stockpile of contaminated soil covered with a plastic
tarpauline, one stockpile of clean soil (uncovered) and one large stockpile of broken
concrete pieces (uncovered) was observed in the former location of these prior features.
Mr. Spurlin stated that EPA plans to remove the stockpile of contaminated soil and use
the stockpile of clean soil to grade the site. EPA plans to leave the concrete pile in place.
I took a panoramic photo of the site from the southeast corner of the site showing the
condition of the site and the general surface slope.
We inspected containment area #3, located at the northeast corner of the warehouse. The
containment area cinderblock wall was intact. There was residual stained soil in the
crawl space under the warehouse and at the northeast corner of the warehouse within
containment area #3. Mr. Spurlin indicated that EPA did not plan to remove any soil
from this area, because the levels were not above EPA regulatory levels and because it
would require EPA to demolish the warehouse in order to get to it. The northeast corner
was heavily vegetated and impassable. Mr. Spurlin stated that there are two empty square
cinderblock impoundments located in this area and a small diameter plastic pipe leading
from the warehouse to the impoundments. Mr. Spurlin did not know where the pipe
3
• •
originated within the warehouse nor it's purpose. I took several photos of the
containment area.
We inspected the warehouse. There was a open roll-off container outside at the south end
of the warehouse that was filled approx. halfway with metal debris. Mr. Spurlin stated
that the roll-off was present on the site prior to the removal and that EPA was using it to
store metal debris that could be salvaged. We inspected the inside of the warehouse.
There were two large, empty, cylindrical tanks at the south end inside the warehouse. Mr.
Spurlin said that these tanks were part of Cherokees wastewater treatment system. EPA
removed oily liquids and sludges from inside these tanks. There was also a device that
appeared to be stacked tubes. There were roughly 5 or 10 tubes, each about 3-5 inches in
diameter, roughly 10-12 feet long on each rack and stacked several racks high. The ends
of the tubes had a tapered fitting with a small 0.5 inch diameter plastic tube connecting
the larger tubes together, end to end fashion. Mr. Spurlin said this was some sort of
filtration system. I took a panoramic photo of the south end of the warehouse. There
were numerous old desks, chairs, and furniture scattered along the east wall of the
warehouse. There was a mens bathroom on the west wall. I observed a room through a
open door at the north end of the warehouse that had a desk and chair and appeared to be
a office. I did not see where the plastic pipe entered the warehouse from the previously
mentioned impoundments at containment area #3.
We walked outside the warehouse to the northwest entrance to the site. I walked down
Berryhill Road to the southwest corner of the site. I took a panoramic photo of the site
from Berryhill Road showing the new fence and gate and the south end of the warehouse.
At 12: 10, we walked back to the command trailer at Drum Street and discussed the bulk
analytical group data from the removal action. Mr. Spurlin pointed out that the majority
of contaminants found at the site were BETX and chlorinated solvents. He stated that
although PCB's were identified within the two vats located at the former loading
platform, no levels were found above the Toxic Substances Control Act regulatory level
of 50 ppm. Thus, they did not ship any bulk groups as PCB solids or PCB liquids from
the site.
I told Mr. Spurlin that our survey indicated that there were limited receptors that would
be affected by a release from the site. As a result, only highly toxic, highly
bioaccumulative and persistent contaminants would be capable of causing the site to
score greater than 28.5 on the Hazard Ranking System and asked him if any of these
contaminants were identified. Mr. Spurlin thought that some of the PCB data and PAH
data may be useful. He agreed to review the results and provide copies of bulk group
analytical results generated by EPA during the removal action to the NC Superfund
Section. I gave Mr. Spurlin my current business address. At 12:40, Jarrell Wootan and
Doug Moore departed the site. At 12:45, I broke for lunch. I arrived back at Raleigh at
16:30.
4
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'
. ' ... , State of North cc:llina
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
Mr. John Gibson
December 13, 1995
Solid and Hazardous Waste Program Manager
Mecklenburg County Department of Environmental Protection
700 North Tryon Street
Char1otte, NC 28202
RE: Site Inspection
On-Site Reconnaissance
Cherokee Oil Company
NCD 9611 198 Ei'l!J.
<J'il'om 011
Dear Mr. Gibson:
DEHNR
David Lilley of the NC Superfund Section spoke with Ms. Francis Duncan of your office today to notify
you that the NC Superfund Section will conduct a site reconnaissance of the subject site located In
Mecklenburg County, North Carolina The reconnaissance will be conducted on December 20, 1995 by Doug
Moore of the NC Superfund Section.
The purpose of the reconnaissance Is to determine tt the site poses a hazard to public health or the
environment because of releases of contaminants to soil, surface water, groundwater, or air. The
reconnaissance team will locate all nearby water supplies (surface and groundwater, community and private)
and any close sensitive environments, schools, and day care centers.
This reconnaissance is not an emergency situation but is a normal step in the evaluation of all
uncontrolled and unregulated potential hazardous waste sites in North Carolina. You may want to have your
representative meet the reconnaissance team at the site. If so, please contact Doug Moore at [phone],
ext. 315 and he will coordinate a meeting.
If the reconnaissance indicates the need for Mure study of the site, we will contact your office to
advise. If you have any questions, please dont hesitate to call David Lilley or me at [phone].
cc: Phil Prete
Doug Holyfield
Pat Williamson
Scott Ross
David Lilley
Donna Keith
1
sincerely,
Pat DeRosa, Head
CERCLA Branch
NC Superfund Section
P.O. Box 27687. Raleigh. North Carolina 27611-7687 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ l m'.. post-consumer paper
Federal • er.rip Notification & Authorization
Prepared by: ""D. {Y\<Jo/3e Today's Date: !)u ... I:!. I 9 'I~
• Use □lack Ink or Typewriter onJy.Staff to fill out fim 2 blocks only.
Site Trip-
Date of Trip: w~d,z~d"r, Dee;. :z.o,.('l"1.J
If trip date changed or cancelled note below:
Trip Date Changed To: _____ Cancelled:
NCO#: -4<j'c~9Jb1 f ~ I Site Name: ?/te.-n,h<:... CJ, (
City: (h4¥lo ft~ County: t/Au{,.lo.. J,u,,'1
Reason for Trip:
Name of Hotel (Overnight Trip): Hotel Telephone Number: ( ) ---------~ ----
Project Team Leader: /)0'0 /v),,.,r<e
Assistants: l&«f, {211,-,, 6-n,t. , __________________ _
Attach To Notification Form: 1 copy each:
Submit to the
Industrial Hygienist
Preliminary Assessment Form (First page only)
Site Map
PA Transmittal Letter
(Please lisl approprialc County Health DcpartmCnt contact person to call to advise of lrip) · ~j,),:i--1-/a.·c: · Environmental Supervisor or Health Director to call: fr)r, ]ck., 0<h>c"-Title: lu1,.fe A~,zr·i-
(Nole if Dr., M.I'., etc.) /Y1c_;-
Telephone Number: (;7,11)33,;'. -~,o0
1
'
Notes: Health Department Official Contacted:I/Jw5-1,nc,~ il"c:cv-
Back Up Letter Required: Yes X--No ~
1/;,o,-/t[;-{),j /)lh;, Ot_t,nc~ f':,. f;;;;,, (£/~,,.,_
~ /:2_-;3 -;:.:i-([):f3 c:'...,,)
Nole: Si pied original to Data Mana~cr
/
State of North callina
Department of Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
• AVA
DEHNR
December 13, 1995
Ms. Cindy Gurley
NC CERCLA Project Officer
EPA Region IV Waste Division, 6th Floor
345 Courtland Street, NE
Atlanta, Georgia 30365
Re: Integrated PA/SI Sampling Plan
Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg Co., N,C.
US EPA ID: NCD 980 799 019
Dear Ms Gurley:
Post-it' Fax Note 7671 Date1/.'" IS ,,,, _ # of ► -" 7.:, pages
Enclosed please find a copy of the proposed PA/SI sampling plan for the Cherokee Oil Company
site (NCD 980 799 019), tentatively scheduled for January 1996, located at 1201 Berryhill Road
in Charlotte, North Carolina,
1.0 Site Conditions
The site layout is indicated on Figure 1. The site consists of a former unperrnitted hazardous
waste storage facility, located on a 0.7 acre parcel in northwest Charlotte. The site is located in
an urban mixed residential/industrial area. Overland drainage from the site travels to the south
and southeast, where it is intercepted by storm sewers that direct the drainage for approximately
0.2 miles underground to an unnamed tributary (UT) to Stewarts Creek. The Mecklenburg
County Department of Environmental Protection (MCDEP) has received and investigated
numerous citizen complaints of materials discharged from the site to nearby propert!_,es and
ultimately to the UT to Stewarts Creek.
Two principals of Cherokee Resources have been convicted of violations of the Clean Water Act
and are currently serving active prison sentences.
Since November 1994, EPA, OHM Corporation and Roy Weston, Inc. Technical Assistance
Team (TAT) have been conducting a removal action at the Cherokee Oil Company site. Sources
found at the site at the time of the removal action include 2,851 drums, 12 large above ground
storage tanks, 3 large underground storage tanks and several diked containment areas containing
unknown liquids and sludges totaling over 300,000 gallons. To date, over 18 separate bulk waste
P.O. Box 27687, Raleigh, North Carolina 27611-7~87 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ l 0% post-consumer paper
•
Ms. Cindy Gurley
Cherokee Sampling Plan
Page 2
•
streams have been identified at the site requmng offsite treatment and disposal to RCRA
approved disposal facilities. Hazardous waste streams identified at the site include PCB solids
and liquids, flammable organic liquids, chlorinated liquids, strong acids and bases, and oxidizers
including peroxides. In addition, Cherokee Resources reportedly handled ethylene thiourea, a
RCRA Kl25 pesticide, at the Berryhill Road facility. Additional unspecified pesticides are
suspected to have been handled at this location.
2.0 Sources
2.1 Containment Area #1
In November 1994, EPA estimated that 17,842 gallons of free-standing liquid was contained
inside a diked containment area designated "Area #I", located at the south end of the loading
dock. In addition, EPA ERRB used area #I as a mixing basin to solidify site contaminants with
kiln dust. The containment area measures 26 feet wide by 61 feet long, or 1,586 square feet.
Following EPA's removal action, the soil will be scraped to a depth of 1-2 feet, sampled for
confirmation and backfilled with clean fill. EPA post-removal soil samples will be analysed for
volatile and semi-volatile organics and the 8 RCRA metals.
We propose to collect one vertical composite soil sample below the level of the backfill. The
soil sample will be collected using a hand auger. The borehole will be monitored using the HNu
or OVA. The soil sample will be submitted to the State Laboratory of Public Health for PCB's
and pesticide analyses.
2.2 Containment Area #2
In November 1994, EPA estimated that 30,108 gallons of free standing liquid was contained
inside a diked containment area designated "Area #2", located southeast of the loading dock.
The L-shaped containment area measured 40 feet wide by 81 feet long, or 3,088 square feet.
Following removal of the sludge and oily waste from Area #2, EPA removed contaminated soil
to 1-3 feet depth, depending on visual evidence of stained soil. EPA collected post-removal soil
samples from the base of area #2 at the surface and at 3 feet below the surface. Post-removal soil
samples from the base of the containment area identified elevated levels of acetone (420 ug/kg),
butanone (57 ug/kg), hexanone (140 ug/kg), methyl ethyl ketone (19 ug/kg), ethyl benzene (55
ug/kg), toluene (74 ug/kg), xylenes (480 ug/kg), naphthalene (3,900 ug/kg), methyl naphthalene
(19 ug/kg), phenanthrene (1,200 ug/kg) tetrachloroethylene (9.9 ug/kg est.) and bis (2-ethylhexyl)
phthalate (41,000 ug/kg) remaining in soils at containment aera #2. EPA later backfilled area #2
with clean fill.
We propose to collect one vertical composite soil samplebelow the level of backfill at this
location. The soil sample will be collected using a hand auger. The borehole will be monitored
using the HNu or OVA. The soil sample will be submitted to the State Laboratory of Public
Health for PCB's and pesticides analyses.
2
•
Ms. Cindy Gurley
Cherokee Sampling Plan
Page 3
2.3 Containment Area #3
•
In November 1994. EPA estimated that 21,600 gallons of free standing liquid was contained
inside a diked containment area designated "Area #3", located east of the loading dock. The L-
shaped containment area measured 40 feet wide by 6 I feet long, or 1,800 square feet. Following
removal of the sludge and oily waste from Area #3, EPA removed contaminated soil to 12
inches. EPA collected two 5-point composite surface soil samples under and adjacent to the
building and two vertical composite soil samples to 1.5 and 3.5 foot intervals.
Post-removal soil samples from the base of the containment area identified elevated levels of
acetone (1540 ug/kg), benzene (22 ug/kg), 2-butanone (I IO ug/kg), 1,1-Dichloroethane (19
ug/kg), ethylbenzene (44 ug/kg), 4-methyl-2-pentanone (75 ug/kg), tetrachloroethene (I IO
ug/kg), toluene (290 ug/kg), xylenes (500 ug/kg), bis(2-ethylhexyl)phthalate (87,000 ug/kg),
butylbenzyl phthalate (5,000 ug/kg est.), di-n-butylphthalate (I IO ug/kg est.), di-n-octylphthalate
(5,300 ug/kg est.), phenanthrene (3,900 ug/kg est.), pyrene (3,100 ug/kg est.), cadmium (17
mg/kg), chromium (130 mg/kg) and lead (290 mg/kg). The residual contaminated soil is located
in a crawlspace under the main building and is inaccessible. No PCB's were detected in any of
the four samples collected at area #3. As this area has been adequately characterized, no
additional soil samples will be collected at this location.
2.4 Underground Storage Tanks at Fuel Station
In November 1994, EPA removed three underground storage tanks (UST's) from a fuel station at
the southwest corner of the property. The three UST's contained oily waste and sludge
containing volatile and semi-volatile organics and metals. According to EPA OSC Steve Spurlin,
the tanks appeared to be in sound condition and the subsoil under the tanks was composed of a
tight red clay that was not stained, suggesting there had been no releases from the tanks. EPA
collected confirmatory soil samples from the subsoil under the tanks for volatile and semi-
volatile organics analyses. The analytical results of subsoil samples taken at this location were
unavailable prior to preparation of the sampling plan.
During our inspection of the refueling island, seeps of an oily material were observed south of
the pad that appeared to be originating from the refueling island. Mr. Spurlin indicated that a 1-
1.5 foot layer of oily material was encountered directly under the fuel station pad. The pad was
demolished to trace the extent of the oily layer. The oily layer was removed and stockpiled on
the site. The stockpiled soil was removed to a RCRA approved disposal facility. The UST pits
were backfilled with clean fill to a depth of approximately 14 feet.
We propose to collect one composite or grab soil sample from a ditch that recieves runoff from
both the seeps and Area #1. The soil sample may be collected using a hand auger. The borehole
will be monitored using the HNu or OVA. The soil sample will be submitted to the State
Laboratory of Public Health for volatile and semi-volatile organics, inorganics, PCB and
pesticides analyses.
3
•
Ms. Cindy Gurley
Cherokee Sampling Plan
Page4
3.0 Targets
•
The primary target identified at the site is a fishery located at the Freedom Road bridge over
Stewarts Creek, located approximately 0.3 mile downstream of the site PPE. A review of the
National Wetland Inventory maps for Charlotte indicated that a linear wetland existed along the
length of the UT to Stewarts Creek, beginning above the site PPE and extending downstream to
the confluence with Stewarts Creek. A physical survey conducted by Army Corps of Engineers
wetlands expert Steve Lund found no wetlands along this segment of the UT. There are no
terrestrial sensitive environments, endangered or threatened species along the entire 15 mile
surface water pathway.
A study of groundwater use within a 0.5 mile radius of the site was conducted by reviewing the
Charlotte-Mecklenburg Utility Department maps and a confirmatory windshield survey of the
plots that did not have a municipal tap record. No wells were identified within a 0.5 mile radius
of the site. Based on the surface topography, it is suspected that groundwater would flow south
and southeast towards Stewarts Creek and the UT to Stewarts Creek. The nearest suspected
wells are located northwest of the site in the vicinity of Paw Creek. As there are no known wells
within a 0.5 mile radius and downgradient of the site, the threat posed by the site to groundwater
use is minimal.
There are no workers on the site and no residents living on and within 200 feet of areas of soil
contamination. Historical site runoff across the adjacent Suburban Propane property southeast of
the site poses the only conceivable soil exposure threat associated with the site. The workers at
Suburban Propane located at work areas within 200 feet of contaminated soi I would be
considered targets. Soil samples CO-004-SL and CO-005-SL will determine the extent of soil
contamination remaining in these areas.
As all the above-ground storage tanks, underground storage tanks, drums, free-standing oils and
sludges have been removed from the site, the consequent air threat posed by these potential
sources has been removed. No current air releases are suspected at the site.
4
•
Ms. Cindy Gurley
Cherokee Sampling Plan
Page 5
•
Table I and Figures 2 and 3 identify the proposed sample points. The NC Superfund Section
plans to collect surface and subusrface soil, surface water and sediment samples at and near the
site. In order to achieve a site score > 28.5, a substance exhibiting a high human toxicity and
high bioaccumulation factor sufficient to result in a waste characteristics factor value of 320
would have to be found in site sources (for example, PCB's) and a site attributable release
exhibiting a bioaccumulation of 500 or greater must be found in sediments in the fishery. The
samples will be submitted to the N.C. State Laboratory of Public Health for volatile and semi-
volatile organics, inorganics, PCB's and pesticide analyses. If you have any questions, please
contact me at [phone], ext. 315.
attachments
Approved:
Cindy Gurley Date
NC CERCLA Project Officer
5
Sincerely,
Douglas Moore
Environmental Chemist
NC Superfund Section
Figure I.
Site I ,ayout ivlap
Cherokee Oil Company Site
EPA ID: NCD 980 799 019
Drawn by: Douglas Moo;.,
NC Superfund
November 1995
Map Not to Scale
c:::l Aboveground Storage Tank
t:: : l Underground Storage Tank
□ Storm Grate
~ Overland Runoff Direction
' ~ ~ .. ~
·•,
j
\
•
·\\ ~,r
~
Sample Id#
CO-001-SL
CO-001-SB
CO-002-SB
CO-003-SB
CO-004-SL
CO-005-SL
CO-OO!-SW/SD<11
-
CO-002-SW/SD<11
CO-003-SD111
CO-004-SW/SD11l
C0-005-SW/SDill
•
Table 1.
Sample Collection Information
Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCO 986 190 239
Location · Justification
Urban Soil near site Establish Background
(location to be determined
in field).
Urban Soil near site Establish Background
-at 3 feet below (location to be determined
surface. in field).
Area #1 -at 2 feet Potential Source
below surface.
Area #2 -at 3 feet Potential Source
below surface.
Soil in ditch outside Attribution
southwest corner of
Area#!
Soil in overland Attribution
runoff path from
Area #2
Upstream of Establish background in UT
drainage culvert -above PPE.
UT of Stewarts
Creek
Downstream of Establish current or historic
drainage culvert -release from site
UT of Stewarts
Creek
At drainage culvert Attribution
between PPE and
Stewarts Creek
On Stewarts Creek-Establish Background
upstream of
confluence of UT
and Stewarts Creek
On Stewarts Creek -Establish release impacting
downstream of nearest fishery.
confluence of UT
and Stewarts Creek
•
Matrix
Soil
Soil
Soil
Soil
Soil
Soil
Aq./Sed.
Aq./Sed.
Sed.
Aq./Sed.
Aq./Sed.
111 Note: Sediment samples will be collected within 0-12 inch profile using hand auger.
6
Analytical
Parameters
V,S,l,PCB,
Pesticides
V,S,I,PCB,
Pesticides
V,S,I,PCB,
Pesticides
V,S,I,PCB,
Pesticides
V,S,l,PCB,
Pesticides
V,S,I,PCB,
Pesticides
V,S,1-SW only
V,S,I,PCB,
Pesticides-Sed.
V,S,I -SW only
V,S,l,PCB,
Pesticides-Sed.
V,S,l,PCB,
Pesticides
V,S,I -SW only
V,S,l,PCB,
Pesticides-Sect.
V,S,I -SW only
V,S,I,PCB,
Pesticides-Sed.
Figure 2.
On·Site Sampling Locations
Cherokee Oil Company
EPA ID: NCO 980 799 019
Map Not to Scale
•
'··, •.,)
• •
C0-002-SI/_ :-[\.
CO-0(l4-S 1: -; \
\:
\
•
'\· ·< .. .'
/
\
\ \ _ ___,---------
\
\
\
__ \
••
STATE PROG. SECTION
•
I Ms. Cindy Gurley
I Cberokt.Q SamplillJI Plan
i Page 5
Table 1 and Figures 2 and 3 identify the proposed sample points. The NC Supommd S~tlon
plans to colloct surface and subu&rfiwe soil, siirtaco wator and sediment samples at and near the
site. In order to achieve a site score :> 28.5, a 111,1ba111nco oxlubui11B a blp human toxicit)' and
high bioaccumulatlon factor surt;icient t<t re.suit in " waslo cha....ctetlstic, factor value of 320
would have to be, found in site oourcos (for example. PCB's) and a &lte attributable release
cxbibltlng a bioacoumulatlon of 500 or greater must be found in sediments in the fishory. The
sampleg will b& submitted to the N.C. StaCf Laboratory of Public. Health Et1t volatik and se111i•
i volntile organics, inor,:anics, PCB 's and pesticide 111Wyse,;. If you have any questions, please
! contact mo at(lll9) 73]·2801, ML 315.
attacbments
Approved:
--'c£_..,~~-----"0-, .... ,o(...._, ...... o__,_~:re-J9 "9 u,
NC CBRCLA Project Officer
s
Sineerely,
¥/U,U,..,,_
Douglas Moore
Bnvirouo10nbll Chc,,nist
NC Superl'und Section
P.01
Memo
Date: December I 3, 1995
To: File
From: Douglas Moore
Environmental Chemist
NC Superfund Section
Re: December Removal Update
Cherokee Oil Company Site
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
•
On Wednesday, December 13, 1995, I spoke with EPA federal On-Scene Coordinator
Steve Spurlin [phone]. Mr. Spurlin projects that the removal will be complete by
the end of next week. I indicated that we would like to meet with him next week to get
copies of laboratory results to be used for HRS scoring purposes and tour the site. He
stated that he would be at the site next Tuesday and Wednesday, December 19-20. We
agreed to meet at the site around 11:00 a.m. on Wednesday, December 20, 1995.
I asked him about the analytical laboratory results for post-removal confirmatory soil
samples collected at the site. Mr. Spurlin provided the following summary information
for two soil samples collected at containment area #2 following excavation of the top 1-
2.5 feet of contaminated soil. EPA TAT collected a soil sample from the surface and at 3
feet below the surface at containment area #2, located under the aboveground storage
tanks. These samples were analyzed for volatile and semi-volatile organics and 8 RCRA
metals.
The surficial soil sample contained elevated levels of acetone ( 420 ug/kg), butanone (57
ug/kg), hexanone (140 ug/kg), ethylbenzene (55 ug/kg), methyl ethyl ketone (19 ug/kg
est.), toluene (74 ug/kg), xylenes (480 ug/kg), methyl naphthalene (3,900 ug/kg), bis (2-
ethylhexyl) phthalate (41,000 ug/kg), naphthalene (2,400 ug/kg) and phenanthrene (1,200
ug/kg). The acetone, butanone and hexanone were also found in the lab blank and could
be a laboratory artifact.
EPA had TAT excavate a pit to 3 feet deep in containment area #2 using a backhoe. A
single grab soil sample, collected at the base of this pit, exhibited elevated concentrations
of acetone, butanone and hexanone, ethylbenzene (150 ug/kg), methyl ethyl ketone (16
ug/kg), tetrachloroethylene (9.9 ug/kg est.), toluene (2,300 ug/kg est., xylene (1,350 ug/kg
•
est.), methyl naphthalene (930 ug/kg), bis (2-ethylhexyl) phthalate (16,000 ug/kg) and
naphthalene (1,000 ug/kg). The results show an increase in concentrations of
ethylbenzene, toluene, xylenes and tetrachloroethylene at three feet below the surface.
Mr. Spurlin stated that the UST's have been removed from the site. He was unable to
locate the post-removal confirmatory soil sample analytical results. However, he stated
that a layer of smelly stained soil was observed above UST #3. The material was located
adjacent to a series of distribution pipes from the loading dock, as well as a terra cotta
pipe which they believe may be associated with an old septic tank drain field. Mr.
Spurlin believes the material may have originated with leaks in the pipes. He stated that
TAT removed the approximately 1.5 foot thick layer, stockpiled, tested, manifested and
shipped the material off-site to a RCRA approved disposal facility. TAT collected post-
removal soil samples from the subsurface below the former UST#3 and placed them
inside a bag. OVA readings of the air inside the bag gave a positive reading. EPA had
TAT excavate several additional feet of material from the subsurface. Although the soil
was composed of a unstained tight clay, additional soil samples collected by TAT for
confirmation exhibited elevated OVA readings. Mr. Spurlin suspected the elevated
readings originate from vapors trapped in pore spaces in the soils.
I asked Mr. Spurlin about indications of any pesticides disposed at the site. Mr. Spurlin
indicated that no pesticides, other than small concentrations of PCB, were identified in
the wastestreams found at the site. He believes there may have been I or 2 hits for trace
quantities of pesticide. He stated that EPA recieved a document package from the
Department of Defense (DOD) detailing materials DOD gave to a federal contractor. The
contractor, in turn, had at least part of the materials manifested through Cherokee
Resources. EPA found some of these materials inside the warehouse at the site. The
document package included hazardous waste manifests which included waste oils, quart
jars of calcium hypochlorite (a strong oxidizer) and a small quantity of malathion. Mr.
Spurlin stated that EPA did not find malathion at the site.
' State of North Car.a Department of En nment,
Health and Natural Resources .
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
Mr. John Gibson
August 7, 1995
Solid and Hazardous Waste Program Manager
Mecklenburg County Department of Environmental Protection
700 North Tryon Street
Charlotte, NC 28202
RE: Preliminary Assessment: On-Site Reconnaissance
,Cherokee Oil Company
NCD 980 799 019
Dear Mr. Gibson:
NA
DEHNR
COP'{
David Lilley of the NC Superfund Section spoke with Ms. Sarah Edwards of your office today to notify
you that the NC Superfund Section will conduct a site reconnaissance of the subject site located In
Mecklenburg County, North Carolina. The reconnaissance will be conducted on August 7, 1995 by Doug
Moore of the NC Superfund Section.
The purpose of the reconnaissance Is to determine if the site poses a hazard to public health or the
environment because of contaminants to soil, surface water, groundwater, or air.
This reconnaissance is not an emergency situation but Is a normal step In the evaluation of all
uncontrolled and unregulated potential hazardous waste sites In North Carolina. You may want to have your
representative meet the reconnaissance team at the site. If so, please contact Doug Moore at [phone]
and he will coordinate a meeting. I am enclosing background data on the site for your information.
If the reconnaissance indicates the need for future study of the site, we will contact your office to
advise. If you have any questions, please dent hesitate to call David Lilley or me at [phone].
Enclosures
cc: Phil Prete
Doug Holyfield
Pat Williamson
Scott Ross
David LIiiey
Donna Keith
Sincerely,
, . ......._
Superfund Section
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone] FAX [phone]
An Equal Opportunity Affirmative Action Employer 50% recycled/ l 0% post-consumer paper
rc;uc:;1 c:11
.rip Notification & Authorizarw
Prepared by: Me--.....,_ I
Today's Date: l)y.4t 3/ '?.!
·Use Dlack Ink or Typewrite only•Staff to fill out fi~t 2 blocks only.
Site Trip.
Date of Trip: 77Jflr=-t:-1---'l.-<
If trip date changed or cancelled note below:
Trip Date Changed To: Cancelled: --
NCO#: c:;qo 199 0/9 Site Name: Cite.rake cJ,( Co/1,A~a'o/
City: //Adv lol-k County: /II .:.ek Let1. fz_., cq
/
Reason for Trip: fhu;_,.l-_ry ksl!'~n,et,v/ _. 0,-,-s-,k /<2k_ co;,"""', CS'~
Name of Hotel (Overnight Trip): Hotel Telephone Number: ( ) --. ;\ j( :? lfd·•.
Authorized by: J._ --J.,:,ie V-· '
Industrial HygieAi:,;t./
Project Team Leader: ftw~ . /nc,t,-,,<.
Assistants: ~f)~jt; {<v.,v,,(;,j ,
✓
Attach To Notification Form: 1 copy each: PrPliminarv Assessment Form (First page only)
Submit to the
Industrial Hygienist
C Site'M,,'rv
PA Tra~smittal Letter
(Please list appropriate County Hcallh Department contact person to ciill to advise of lrip) · Sf) /.J ~ Ha,C t'
Environmental Supervisor or Health Director to call: ,m r, JoA"-(:;;, b s,.,.___ Title: W:~k,. ()~1 .,.,..___
(Note 1f Dr., M.I ., etc.) _ /hp r:
Telephone Number: t;<11)3Y;, -> S-60
Notes: Health Department Official Contacted;1\ ~ar ,;:.,/\. · E;/.,1,,Jo..rJ<
Back Up Letter Required: Yes L No __
Note: SiJ!ncd oripnal to Data Manu:,.:cr
i1h£bed ,Jls.-r:Ji1-h,yb-'b-r ((/<' .6;h~v"r---
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.J'llflSTON-SALEM JOURNAL 5:/22Y; 0.C.mbe< 4, 19'4
STATII & LOCAL
._Toxic waste cleanup attracts EPA attention
■ Chemicals inside
company's barrels
;.-nay be poisonous
~I-£ ASSOaAIED PRESS ·
CHARLOTl'E
The problemB at an oil-recycling
i:ompany didn't end when the I-Op
two ex.ecullves were convicted in
Jw,e of .flushing toxic waste down the ciiy's sewers,
'. Taxpayers are cleaning up the $1
f1!illlon mess they left behind at
p~rotee Resources.
, Two thousand barrels, six
[15,000-gallon tanks, two tanker
lnillers and a· Dumpster-size bin at
Cherokre 's west. Charlotua proce-ss-
Ing plant are attracling the au.en-
Uon of lhe U.S. Environmental Pru-
lection Agency.
! The EPA believes that company
~,fficials had the containers packed
W'\vith chemicals that can poison,
borrode, bum or explode.
")L's· amazing how much they
packed ln there," said Steve Spur-
lln, the EPA cOQrdinator of a fe<ler-
.i S\lpeif\U\d cleallUP at the site.
1Toere's a little bit" of everything,
~dsome thlngll !hat there's no way
lt should be there."
North Carolina has 22 sites on
Superfund's list of long-term clean-ups. The Mecklenburg C-Ounty loca-
tion is getling rapid altenl.ion be--
cause U's on a list of sites deeml'<l
to be immediate threats (,o the envi-
ronment.
The cleanup began last month,
about the same time company Pres-
ident Keith Eidson and Vice Presi-
dent Gabe Hart.sell began their 5 l -
month prison 9entences.
Eidson and Hartsell are in prioon
ln Goldsboro. Both execulives are
appealing their convictions.
Spurlin beUeves that in addition
to recycling oil, Cherokre accepted
hazardous waste that it wasn't li-
censed l-0 handle. Some untreated
wast.es were flushed down a compa-
ny toilet, investigators said last
summer.
should have known they were en-
gaging in improper disposal, Spllr-
lin said.
"They could have called the stale
and checked the compliance or the
racility," he said.
An attorney representing Eidson
and Cherokee Resources contends
that there are no harmful pollutants
al the building and complained that
the government is persecuting his
client.
Federd.l Investigators couldn't
find hazardous wast.es when they
searched a Cherokee Resources
warehouse on Summit Avenue in
1991, said attorney Dale Morrison.
When government officials pad-
locked the warehouse, it neart)' put
the company out of business, he
said. EPA officials remember the
incident much ctiffereutly.
THE COMPANY mixed some
wastes into soil contaminated by
petroleum and had it trucked to a
landliU, Spurlin said. Hazardous
waste -cost.,; three or four times
more to dispost, of than petroleum,
whJch is not cJassilied as a hazard. 1 ous waste,
The b-uperfunct law, adopted in
1080, is supposed to make pollut-
ers pay the cost of serious clean-
ups.
Tht-y say 6,000 hanels ofhaz~mJ-
But because federal attorneys
think lhaL Cherokee Resources
doesn't have enough .remaining re-
sources, the EPA will try lo collect
rrom the businesses that sent w;iste
the Cherokee ·wasn't licensed to
handle.
The companies that sent waste (,o
Cherokee Resources could be n-
na11cially responsibll' because they
ous wa.s1e -including drums of
deadly so<lium cyanide -were tak-
en from the warehouse.
That cleanup cost lru<payers
•bout $ 2 million.
Preliminary samples identiried
wastes at the Berryhill Road proc-
essing plant as solvents, caustic
m•terials, plat.ing wastes, paints
and a.sbestos.
Many were mixed toget.her and
unlabeled.
A portable Jab stands ready to
tentalively identify what each bar-
rel holds, a process that is only now
beginning.
Once the waste is identified, the
EPA will know how to dispose or
the barrels.
Workers are expected to be at
U1e site another two months. The
EPA has budgeted $1 mJUion for
ch·anup and disposal
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DEC-l:l'::!-l':::!':::14 .:11::1:4'=' ri-<u1·1 uc.ru'1r<; 1·1Uur;.c.=ivJL ... w:. ,u ...... ,,, '.._...,...,,,.
2, :1f]\'l ., Si)■ I i!t] f_i] I? I I 7:111 re,
Photot br Q.UIY O'BRIEH/SLAlf
lrokee Resourc8s, Sn oll-ra·cycllng Ur~ In wast Chartotta, is convicted of flushing toxic wastes down sewers. NeighbOrs of
silo of a Supgrfund cloanup. Two• tc,p e~ecutlves were the Berryhill Road business go about their daily routines..
1 ¥aste .r~movu} begins; neighbors wary.
Barrels in west Charlotte'
>se unknown hazards to
)rkers, nearby residents.
BRUCE HENDERSON W-.ike astronauts in training, ihe people in
white suits and oxygen masks out . on
ryhill Road move Warily across a moon·
pe of rusted barrels, tall fences and
blackened ground. ·
'rison sentences didn't end the-case Of
irokee Resources, an oil-recycling firm
:>s.e lop two executives were convicted ln
e of flushing toxic wastes down Char.
e's sewers. · · ·
·axpayers are cleaning up the $1 million
ss they left behind.·
wo thousand barrels, six 1S,0.00-g311on
<S, two tanker I.Jailers and a Dumpster-size
at Cherokee's west Charlotte processing
1t are filled with chemicals that can
;on, corrode, burn or explode. the Envi•
menlal Protection Agency believes.
It's a.mazirig howl riluch they packed in
re." said Steve Spurlin, the EPA coordina.·
of a federal Superfund cleanup. "l11ere·s a
e bit of everything, aod some things that
re's no way it should be there."
he cleanup began last month, as com-
1y President Keith Eidson and vice presi-
it Gabe Hartsell began their SI-month
~n sentenc;e,; -a n;;tional record for
Wearing protective suits, workers from
OHM Remed!atlon Services investigate
Spurlin believes Cherokee did much ffiore
than recycle oil, accepting hazardous wastes
that it wasn't licensed to handle. Some
untreated wastes were !lushed down a com-
pany loilet. investigators said last summer.
the hundreds of abandoned barrels at
Cherokee Resources.
petroleum and had it trucked to a landfill.
Haundous waste costs three or lour times
more to dispose of than petroleum. Petro·
leum is not categorized as a hazardous waste.
Other substances apparently accumulated
in and around the weary-lookin~ metal
DEC-09-1994 08:52 FROM DEHNr;: 1•11.JUK.t:.~VILLt:. ,u .1.-.,n r-'-LJU1'-Surprise: Worker~ never knciw what they wm !Ind Some barrel& are bulging. indicating some sort of whQn thuy op9n barTola at Cherokee Ruources. roac\ion has occurred with tturlr C"Ont9nu.. Cleanup to take 2 more months 1 · Wastes Contlnuocl lrom pega 1C building. which sltJ :.cross from a neighborhood ol small homes. rhe S11perlul'ld law. adopted in 1980. is i:utiposed lo make pollut• er., ~y for clnnups like this. but often WI,. North (aroliru. ha, 22 Lites on Svperlund".s i;st o( lorn<· !erm cleanup&. including one !n Mtcklenburg County. Cherokee Re,ourccs ls get.ling faster ,11en--tion be<cause It's on a IMgl:1' li$.l of ,i1e, deemed lo be a mon! imrnedl• at,i: thrcal 10 the envfronmenL Scu,lln. s.a.id that ~nee· federi,1 •homey, think Cherol<et Re• ,ourcea lsn"t wonh muc;h ;wy more. lhe EPA will uy lo c-ol• lecl from the businessc, lhal ,ef'lt wut.CI thet Cherokee co11ldn·1 legally hindle. · The compa-niu .. should have known." Spml!n uld, "They could Spurlin h4vc c:.a!Jed the ~le al'\d chc,c;ked the compl>am;e of the l•dllty, ~ · An attorney retircsenllng Eidson and Cherokc-c, who complained of governmrnt peuecutlon, say~ th::Tt'0l no1hl<>S h:irmlul at the. buikllng. Eidson and Hartsell are in prlson In Gold,boro. Chero. '" Roourecs no longer operates Attorney Dale Morriron UY$ federal lnves1lgaton c.ou!dn't (ind· h1z.erdou, waste, ,when they ..searched a Oierol<~ · Resources warehou,,e on Summit Avenue in 1991. When the government o.,d. loclr.ed the warehow.c. he said. it r>eatly put Ch~kee out or bw.i• '=· EPA olfic[al, remember !t much d,rrercntly. They s:.y they remQ",ed i:ibout 6,000 bo.rr-cl., of h.uudous w~tc -1ncludin& d11.1ms or deadly ood!um cyantde -trnm Summit Avenue. Th;it c!e.:inu? c~t tupaycrs SOrrn? S2 million. ~Any1hlng he could get_~id to di..,~ of, h.i w;u 1.:iklng 11," ~Id I~ £PA·, Doro AnnJohruon, who helped conduct \h~I cle1nup. .. When you o~ Up a watch= and you flel exp105lve re~dingll from a llle.llity lh.11', svppoocd to be proc:escina w.utc oU, somc--th.ing', wrong:· Moni~n. Eid.son's .11tomey. at• lributed the BerryhUI Ro.ad cleMUD 10 "l:al'!ldy polilia, lo justify the indictment ol two bust• nu"<rnen .and basically the d=· tion of a company ... To OHM Remed~1lon Services, the At!anU en.,.;ronmental !inn the EPA hired, all 1ho~ barreb hold a m)'Sttry brew. Much of the w;utu -Spurlin S.'.l.i-:1 pn!liminaiy Sllrnple, ldcntllicd u,tv-ent~. 0:-..!lllShc ni.:,!eri.~ls, platin,,g w11,1es. paints ~nd asbe,10, -were mixed together and unl.:i• bc:lcd. OHM".s la.sk i..~ 10 move the b.irrcls trom lht pl.lnl site to .J fenc«l lot ll<:TO~ Berryhill Road. A neighborhood street has been bar• ricaded while the barrels a.re movf!d. Then the worlrers, each clad In l""'0 protc,c;tlve suits and LID to 10 glove Iii.yen;. gin!erty pry open e.Jch banet 1.11d l.'.I. e a =pie. A portable lbb sLand5 ready 10 \entatr,,cly tdenti!y what each b11,r· rel hold,, a proce:r, that's only now bcgmnlng. Once Lhe waste ii; Identified, the £PA will k.now h0"" 10 dispose ol the barrels. Won::trs .!Ire e~peeted to be 111 the site another two ""0nlhs. The EPA ha.s b1Jdseted SI million for cleanup and d"pos.al. Folks on Ringwood Street. a few !«1 horn the st:.ging area, ho!)(, they don't chok.e on l1Jmes or go up in Ila.mes before thl" job is flnbhed. 'They 5hould hi,ve come and .1.$kl:O the l'tlght>ortlood 1ir5t -they ju.st came and close<l o!! th~ £.tree\ ,nd starting moving lho..«e blirrels MOUOO," s.aid BlMche For• man, who hu asthma.. ·'Tho~ men -ere out there in thoi;e whi1e $U!l!I I ,md here I am inhaling that stuU on; my way to the bus slop:· · The:e·s lillle chance fumes wll! hurt anybody, Spur!ln s.iid. -The , eoniractor monitot.'I the air !our· times a day 10 detect twmf1JI tmissions.. an.Q none have been , dete{;ted. . But !Mcau,c the deanup crew doe~11·1 yet know what il'6 dealing with. he added. "the potenllaf is there .. for fire or ev,cn explosion. Btlorc they"re moved. torrodcd bam:ds a.re packed In \.1f'Rtr drums or 1helr contcnls pvmpe,d, 1nm 5«.Ure b.lnels. The danger comes lrom unl(nown W11Stti mixed. to· scther or "inc:omp.itible .. maieri-als stored loo close 10 each other. '"Thst'd be~ I'll""""-" Sporlin ~Id, "You"d have 11 I minimum a !ire and PO!..~ibly a11 expl0,1,ion. ·• ,0,.., • 0.,, ,_..L_. ~ ~ ', :.~.:i--1'\ :.;:;t~· :':~~-Ol!icia~ don't know how much soil is tontaminaled at !he Jile. or whetMr ~roundwotcf Is t~lntcd. They do k'now that dikn under thi, sh: abovci.round tank, hold 20,000 to 30.000 es.lions of unidentified liquM th.Ill =rnow, during hctvy ram,;, ··rm afrllld lhe d~mage h.» been done :.lr11:.1dy, lo the waler lines Of wmc1hin3;: ~id Ringwood Sin~et resident Don Gr~nw;:iy. "Wr>. don't k.now for ,u~ lh"t everybody over here i.s not .:i.lrcady contaminated,'• r-• ..,_, • TOTHL P.l:J3
•EPA: ComPany's
• to:x1c waste poses
immediate threat
f 8 The EPA says Cherokee Resources'· plant in west Charlotte is packed with containers of chemicals that can poison, corrode,
burn or explode . ..JJ~ Miwo'Y~ · 11Jfr/
CHARLOTTE -The ~. '."'.'"7«.n_i~11'.~. k.~i whicli is not classified as a problems at an oil-rei;y-i;;:@T,he!e'J! !IJ! hazardous waste. · cling company didn't end t<little bit of.~ The Superfund law, when top two executives -~1;-"'Jt.&,\'fJi_Ji•"1·'1':'t;,% .. adopted in 1980, is sup-were convicted in June of 1:--e~e ,n ,-•,,..-~!j posed to make polluters flushing ~oxic wastes :i~,~~u;,~~~-~l,,; pay the cost of seriOus down the city's sewers. .. p,;,thmp t_hat ,~: cleanups. But because fed-. Taxpayers are cleaning rl'there's nci"S! era! attorneys think Cher-I up the $1 million mess ·f·1!!W2i,,1•.'"'t+ka:i;..,~Jdi · okee Resources doesn't they left behind at Chero-!lway I ,SIJOU . 'i have enough remaining
1
kee Resources. ,be there;a), resources, the EPA will -:Two thousand barrels, ~-:;S'/41i;;}jfj-\~:~iJJ try to collect from the six JS,000-.gallon tanks, I Steve S~urlm, ;i businesses that sent I two tanker trailers and a {,,EPA__c,l,ecinup,d wastes the Cherokee ! waste bin at Cherokee's /:':.·'.C~ainat~T'·\\\i wasn't licensed to handle. I west Charlotte processing i-c· '•"' • · ·1 The companies that sent piant are attracting" the attention of · waste to Cherokee Resources could tlie U.S. Environmental Protection be financially responsible ·because Agency. The EPA believes com-they should have known they were pany officials had the containers . engaging in improper disposal, , p8cked with chemicals that cari Spurlin said. pOison, corrode, burn or explode. "They could have called the.state ' ""It's amazing ho~ much they and checked the compliance of the packed in there," said Steve Spur-facility,'' he said. · lin, the EPA coordinator of a fed-An lawyer representing Eidson eral Superfund cleanup at the site. and Cherokee Resources says there "There's a little bit of everything, are no harmful pollutants at the and ·soine things that there's no way building and complained that the it should· be· there." government is persecuting his cli-North Carolina has 22 sites on Superfund's list of long-term clean-ups. The Mecklenburg County lo-cation is getting rapid attention because it's on ii list of sites
deemed to be immediate threats to the environment.
The cleanup began last month, about the same time company President Keith Eidson and Vice President Gabe Hartsell began their Sl~month prison sentences.
Eidson and Hartsell are in prison in Goldsboro. Both are appealing their convictions. ·
Spurlin believes that in addition to recycling oil, Cherokee accepted
hazardous wastes that it wasn't Ii-I censed. to handle. Some Untreated ' wastes· were flushed down a com-pany toilet, investigators said last summer.
·The-~\\:::ompany miXed som·e
wastes into soil contaminated by
ent.
Federal investigators couldn't
find hazardous wastes when they searched a Cherokee Resources warehouse on Summit Avenue in
1991, said attorney Dale Morrison.
When the government padlocked the warehouse, it nearly put the company out of business, he said.
EPA officials remember the inci-dent much differently.
They say 6,000 barrels of hazard-ous waste -

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drums of deadly sodium cyanide -were taken from the warehouse. That cleanup cost taxpayers about $2 million.
Preliminary samples identified wastes at the Berryhill Road pro-cessing plant as solvents, caustic materials, plating wastes, paints and asbestos.· Many were mixed together and unlabeled.
petroleum and had it trucked to a A portable lab stands ready to landfill, Spurlin said. Hazardous tentatively identify.what each bar-1 . waste costs three or four times rel holds, a process that is only now , more to dispose of than petroleum, b~ginning.
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3 Cn-w<.-:i~ Jl-Y-/i/~o X ,a:\-r •.. ('' I ' () ""-(. "'-M , I , l-Yo-z.. ,x X y_ 1, , ... ,;, ,' J. / .,',/ # '> -<;.I ~·~-LI' ·1-<1 "' 1~-4 '-": I-( --f~,-.. ../...:"'"' <., ..... n I, . /·'-J o-Z.' X )< X . 4 :..o-1.0r si. : LJc.-o )< a~ ),, .• ',/A' r.. '.,./# Lj -,__, ,,f, { 1·'1--nz. !l-'-l-\4~ X <;;c,' .. /-'-/oz., X 'X X 5 CO-'wS-c, 7 QC-D, .• "· L .lrl .... J~,.,. t' ... r I l.411 ..... nl, \-<L.._,
/ l-LJ-IS')D X ~-' --~ .,•LI t:-.0 ,.l ,,,,,.-JJ--,11 11 _ /-Yn. X X 6 fri-l,..jt....-14-. 4,:-IT. ~· , I -4. • ..,
7
8
9
10
ffi. REMARKS lll~ ITEM TRANSFERS TRANSFERS ~~i h~~ .. T4T re9,.,.,jQf i~ NUMBER RELINQUISHED BY ACCEPTED BY DATE TIME
01 -Of:, I ,,1, UA r, ~ rel tx /d-<j· ticiv
-no f;ese,v,. i1.,1 1
i)~ ... 5~;f(~ ~ it•L. ,
2
3
SAMP C~JIGNr,uv; A
4
, . .
LAB COPY
Form 0019
Field Technical Services 1614 2 8 Rev. 08/89
REMARKS •
CEC-07-1995 17:34 FROM SAV~NAH LABS • TO • 917043911147 P,02
SAVANNAH LABORATORIES
I ENVIRONMWNTAL SERVICA, INC. SL
) 5102 LaRoche Avenue• Savsnnah, GA 31404 • [phone] • Fsx [phone]
l'.r. John Rhyne
OHM Corporacion
S335 Triangle Pkwy, Suite 450
Norcross, GA. ~0091
CC: Jack Kilbarger
•.·•,,.-: P.BPORT OF P.ESOLTS
LOG NO: S5·56748
Received: 05 CiC 95
Reported: 07 DEC 95
Purchase 0%"der: 1016477
Project: 16817 Cherokee Oil
Sa.mp!ed By: ~lient
DATE/
LOG NO
56748•1
5'70-2
56748-3
S6748·4
56748·5
SAMPLE DESCRIPT.ON, SOLID OR SEMISOLID SAMPLES TIME SAMPUD
\\ .... ·co-ws-33 y,,1...: ,._
CO-WS-li ,, ,,.)..__
CO•WS-3S " " -"
CO·WS-36 •' '• A
CO•WS-37
..................... ........ ............. ---------------------
PARAMETER 50748-1 ............................................................
1,2-Dichloropropane, ug/kg dw
trans·l,3-Dichloropropene,
ug/kg dw
Trichloroethene, ug/kg dw
Dibromochlorometha.ne, ug/kg dw
1,1,2-Trichloroethane, ug/kg dw
Benzene, ug/kg dw
cis-1,3-Dichloropropene, ug/kg dw
Bretn0:o:m, ug/xg ow
•·Hexanone, ug/kg dv
<5.7
<~.7
<5.7
<5.7
<5,7
<5.7
<5.7
<5.7
<28
4 -MP.t:hyl .. ?. -l")Prit::tnrnio, c-7. A
(MIBK), ug/kg dw
Tetrachloroethene, ug/kg dw 15
Toluene, ug/kg dw 7. 6
Chlorobenzene, ug/kg dw <5.7
KthylbQn~QnQ, ~g/;.g dw 6.9
Styrene, ug/kg dw <5.7
Xylene~, ug/kg dw 52
Surrogate Toluene-dB 96 t
Surrogate• 4-Brcxnofluorobenzene 95 t
Surrogate• 1,~-Dichloroethano-d~ ~5 \
Data Analy:od 12.06.95
:;G748-2 !jG74-8-J -------------... -----
<6.0 <750
<6.0 <750
<6.0 <7S0
<6.0 <750
<6.0 <750
<6.0 <750
<6.0 <750
<6,0 <7~U
<3C <3800
c~O <3300
<6 .0 <750
<6,0 <750
<6.0 <750
-:, . 0 ,:750
<6.0 <750
:. 6 <750
96 t 100 t
100 t 99 " 102 ' 88 .,
12.06.95 12.07.95
----------... -.. ---.. -..
12•04·95/1500
12-04-~5/1440
12·04•95/1420
12·04-95/1450
12·04-95/1430 .............................
SC740-4 SG748 5
-------------------· <6.1
<6 .1
<5,1
<6.1
<6.l
<6.1
<6.1
<i;. l
<30
<30
<6,l
<6.1
<6.1 <' .1
<6.l
c6.l
1:0 " 122 t
1:.6 "' 12.07.95 ·---------
<7.S
<7.5
c;.7.5
<7,5
<7.5
<7.5
<7.S
<7.S
<37
<37
<7.5
<7.5
<7.5
c:7. !i
<7.5
<7.5
98 t
94 t
H "' 12.07.95 ----. -......
ubo,.torlH In S•v•nn•h, GA • T•llahaeuo, Fl. • T•mp•, l'I. • Oeerlleld Beach, Fl. • Mob/le, Al. • New Orle•nt, LA
J:EC-07-1995 17:35 FROM SAV~ LABS • TO • 9: 7043911147 P.03
SL SAVANNAH LABORATORIES
& ENVIRONMENTAL SERVICES, INC.
5102 LaAoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] \
)
1".r. John R.'lyne
OHM Corporation
5335 Triangle Pkwy. Suite 4S0
Norcrose, GA 30092
CC: Jack Kilbarger
REPORT OF RESULTS
LOG NO: S5•!6748
Received: OS DEC 95
Reported: 07 DEC 95
Project: 16817 Cherokee Oil
Sa.mp1=d By: Clier.t
Paqe 3
DAI'E/
LOG ~O
56748-l
56748-2
56749·3
56748·4
56748·5
SJIMPLE DESCRIPTION, SOLID OR SEMISOLID SJIMPLES TIME SJWPL!!D
CO-WS-33
CO-WS-34
CO·WS-35
CO·WS-36
CO·WS-37
TCL Semivolatiles (8270)
Phenol, ug/kg dw
bis(2·Chloroethyl)ether,
~-Chlorophonol, ug/kg dw
ug/kg
1,3-Dichlorobenzene, ug/kg dw
l,4-Dichlorobenzene, ug/kg dw
1,2-Dichlorobenzene, ug/kg dw
2·Methylphenol (o-cresol),
ug/ks-dw
2,2'-0xybis(l·Chloropropane
) (bis-2-chloroiseprepyl
ether), ug/kg dw
3·Methylphenol/4·Methylphen
0l {m&p-cres0l) , ug/kg d.,,
N-Nitroso-di-n-propylamine,
ug/kg dw
Hexachloroethane, ug/kg dw
Nitrobenzene, ug/kg dw
lsopl'lorone, ug/kg c;lv
2-Nitro,;henol, ug/kg dw
<380
dw <380
<380
<380
420
<380
<380
<380
<380
<:380
<380
<380
<380
<380 .. ·---... -----... --------------....... ----..
<400 <400
<400 <400
<400 <400
<400 <400
.,·400 c400
<400 c400
<400 <400
<400 <400
<400 <400
c400 c400
<400 <400
<400 <400
<400 c400
<400 <400 --.. --..... ------------
-----------------------12-04-95/1500
12 • 04 • 95/1440
12·04•95/1420
12-04-95/1450
12·04·95/1430
<400
<400
<4.00
<400
<400
<400
<400
<400
<400
<400
<400
<400
<400
<400
<430
<430
<-UO
<430
<430
<430
d30
dlO
<430
<43C
<430
<430
<430
<430 ----..... -.. -... -.. ---.. -
L.aboratorl•• In S..v11nn•h, GA • Te//11h11ssee, FL • Tampa, FL • 0.•rll•ld S..Ch, FL • Mob/IA .. AL • New Orluna. U
CEC-07-1995 17:35 FROM SAV~ LABS TO 917043911147 P.04
SL. SAVA~NAH LAt!ORATORIES.
& l!NVIRONMENTAL Sl!RVICES. INC.
•
) 5102 LaRoche Avenue• Savannah, GA 31404 • (912) 354·7858 • Fax [phone]
Mr. John Rhyr.e
0~ C'ori;,orAtion
5335 Triangle Pkwy. Suite 4S0
Norcro&&, GA 30092
LOG NO: S5·!6748
Received: OS DEC 9S
Reported: 07 DBC 95
Purchaao Oi:'dor, 101'477
CC: Jack Kilcarger ?reject: 16817 Cherokee Oil
S""'f'led By: Client:
REPORT CF RESULTS
LOG NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES -.. -. -. . . . ----------------------------........ -..................... .
56748•1 CO·WS-33
56748-~ CO·WS-34
56748·3 CO·WS-35
56748·4 CO-WS-36
56748·5 CO•WS•37
PARAMETER 5674B·l
2,4•Dimethylphenol, ug/kg dw
0is(2-cn1oroetho,cy)111etnane,
) ug/kg dw
2,4•Dichlorox,hPnnl, u51/l<51" dv
l,2,4·Trichlorobeozene, ug/kg dw
Naphthalene, ug/kg dw
4•Chloroa.niline, ug/kg dv
Hexachlorobutadieoe, ug/kg dw
4-Chloro-3--thylphonol, ug/kg dw
2-Methylnaphthalene, ug/kg dw
Hexaohloroc:yclopentadiene,
ug/kg c!.'lt
2,4,6-Trichlorophenol, ug/k~ dw
~,1,S-Triehlcrophcnol, u9/kg dw
2·Chloronaphthalene, ug/kg dw
2-Nitro-.~iline, ug/kg dw
Oimethylphthalate, ug/kg c!.w
Acenaphthylene, ug/kg dw
3-Nitroa.•ili.ne, ug/kif r.lw '
Acanaphchena, ug/kg dw
c3ao
<380
d80
<380
<380
<750
<380
<390
560
<380
<380
-<380
<380
<1900
<380
<380
<HOO
<380
56748•2 56748•3
·----------. ----... --
<400 <400
<400 <400
,:400 r:400
<400 <400
<400 <400
<800 <800
<400 <400
dOO <'100
440 <400
<:400 <400
<400 <400
..;:100 ..:4CO
<400 <400
<2000 <2000
<400 <400
<400 <400
<2000 <2000
<400 <400 ··---------··--------
OATE/
T.IME SAMPLED
l2·04•9S/lSCO
12·04·95/1440
12·04·95/1420
12-04-95/HSO
l2·04·95/.L4.l0
56748•'
Page 4
56748-5 ------........ ----·-----<400 <430
<400 <430
,.,oo ,,.430
<400 <430
<400 <430
<800 <860
<400 <430
<100 <130
<400 <430
<400 <430
<400 <430
..:400 -:430
<400 <430
<2100 <2200
<400 <430
<400 <:430
<2l00 <2200
<400 <430 ---.... --.... ----...... -.
Laboratorl11 In S11r11nn1h, GA • T11/1h111te, FL • Tampa, FL • DHrlltld S.11ch, FL • Mob/le, AL • New Orleana, LA
I:EC-07-1995 :7:36 FROM SAVi:NNAH LABS TO 9, 7043911147 P.05
SL SAVA~NAH tfsoRATORIES
& ENVIRONMENTAL SERVICES, INC.
•
} 5102 LaRoche A~enue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: S!·!6748
OS O!C 9!
07 DEC 95
,)
)
LCG ,o
Mr. John R.'iyne
OHM Co=Poracion
5335 Triangle Pkwy. Suite 450
Norcross, GA 30092
CC: Jack Kilbarger
REPORT OF RESULTS
SAMPLE DESCRI~TION • SOLID OR SEMISOLID
Received:
Reportec1:
Project: l68l7 Cherokee Oil
Sampled Hy: ~lient
P,!lgA !
DATE/
SA.'!PLSS TIME SAMPLl!.D ....... - • ■ .... -

•
·-------·········--------·--------·-·----·------------------------·-····· 56749 ·l CO-WS•33 l2•04·SS/l500 56749·2 CO-WS-34 12-o,-ss/1uo 56748·3 CO·WS·35 l2·04·SS/l420 56749•4 CO-WS-36 l2•04 •9S/l4S0 56745-5 CO•WS-37 12-04-95/1430 ---.... --... --.... -------........... ------------------... -..... ---------------------·-····· P :.l>.AMETEJa. 567'19-l SG718-:l 56748-3 56748-4 SG?48-S .......................................... ......... ---.... ----------------------------------------2,4-Dinitrophenol, ug/kg dw <lSIOO ciooo <2000 <2100 <2200 4•Nitrophenol, ug/kg clw c:1900 <2000 c2000 <2100 c2200 Diben~oturan, ug/kg dw <380 <400 <400 <400 <430 ~,1-Dinitrotoluane, '-'9/l<g dw .;JSO ,iOO .... oo .... oo c.i30 2,6-Dinitrotoluene, ug/kg dw <380 <400 <400 <400 <430 Diethylphthalate, ug/kg dw <380 <400 <400 <400 <430 4•Chlorophenylphenyl <380 <400 <400 <400 <430 ether, ug/kg dw
Fluorene, u,1/ls.1,1 uw <380 <400 <400 <400 <430 4•Nitroaniline, ug/kg c1w <1900 <2000 <2000 <2100 <2200 4,6·Dinitro•2·methylphenol, <1900 c2000 <2000 <2100 <2200 ug/kg dw
N•Nitrosodiphenylamine/Diph <380 <400 c400 <400 <430 enylamine, ug/kg aw
4-Bromophenyl phenyl <380 <400 <400 <400 <430 ether. ug/kg c1w
Hexachlorober.zene, ug/kg dw <380 <400 <400 <400 <430 Pen~achlorophenol, u9/k9 dw <1900 c2COO <2000 <2100 <2200 Phenanthrene, u9/Jc9 dw 890 <400 <400 <400 <BO Anthracene, ug/kg dw <380 <400 c400 <400 <430 -----------------------------···------· ------------------------------. ---------
I:EC-07-1995 :7:37 FROM SAVl'N-lAH LABS TO 9: 704391114?
SL SAVANNAH tfsoRATORIES
I tNVIRONMENTAL SERVICES, INC. •
.) 5102 LaRod1e Avenue• Savannah. GA 31404 • [phone] • Fax [phone]
LOG NO: SS·S6748
Received: 03 DE: 95
Reported: 07 DE: 95
)
l!!r. John Rhyne
Ol!M C'~rporAtion
S33S Trianil• Pkwy. suite 450
Norcross, GA 30092
CC: Jack Kilbarger
REPORT OF R.ESOLTS
Project: 16817 Cherokee 0:1
Ge.,:,pled Oy: Client
DATE/ LOG NO
56748•1
S6748-2
56748-3
56748-4
56748·5
SA.'!PLE DESCRIPTION, SOLID OR SEMISOLID SA."U'LES
CO-WS-33
TIME SAMPLl!:l
l2·04•9S/l5v0
12·04-95/lU0
12·04-95/1420
12-04-95/1450
l,·04•35/lUO
CO-WS-34
CO•'IIS•JS
CO•WS•36
C0-WS-J7
P ARAMETF.l< 56748-1
Oi-n-butylphthalate, ug/kg dw
•·luoranthene, ug/~g Ow
Pyrene, ug/kg dw
Bur.ylhP.nxylphth!'ht,o, wr/k(I dw
3,3'-0ichloroben%idine, ug/kg dw
Ben.zo(a)anthraeene, u9/kg dw
bis(2·Bthylhexyl)phthalate,
ug/kg dw
<380
820
600 ,;o
<750
<380
5600
Ch:cy,;vn<>, ug/l<g dw 380
Oi•n-oetylphthalate, ug/kg dw <380
Benzo(b)fl-Jora.nthene, ug/kg dw s10 !enzo(k)fluoranthene, ug/kg dw <380
Benzo(a)pyrene, ug/kg dw <380 Indeno(l,2,J-cd)pyrene, ug/kg aw <380
Dibenso(a,h)anthracene, ug/ki dw <380
Benzo(g,h,i)perylene, ug/kg dw <380 Carba:ole, ug/kg dw <380
Surrogate • Phenol dS 92 t Surrogate,• 2-Fluu~,ophenol
Surrogate 2,4,6-Tribromophenol
Surrogate· Nitrobenzene • dS
Surrogate 2-Fluorobiphanyl
Surrogate Terphenyl • dl4
1, t
79 t
79 t
10!1 t
74 t tlace Ex,:ra-,,:eo
Date ~lyHd
1:LoS.95
12.06,llS
S~74R-~
----... -. --
<,00
<400
<400
-,400
<800
<400
4400
•·~oo
<400
<:400
<400
<400
<400
<400
<400
<400
n t
6~ \'
6S t
240 '-
66 t
60 t
12.05.95
12.06.95 . .. .. --. -. -.
%748-3 5,S748-4 SP48-~ .. .. -.. -..... --.. --..... ---. ---. -. -...
<400 <400 <430
<400 <400 <430
<400 <400 <430
<400 <400 c4:l0
<800 <800 <860
<400 <400 d30
2300 <1700 <2200
<iOO <iOO •430
<400 <400 <430
<400 <400 <430
<400 <400 <430
<400 <400 <430
<400 <400 <430
<400 <400 <430
<400 <400 <430
<400 <400 <430
75 t 66 t 77 ' ~J \' ,a t Sl t
56 t 44 t 32 t ~n .. 5• tr !:4 • 78 t 72 t 64 ' 58 t 52 t 45 %
12.05.95 12.05.95 12.05,95
12,06.95 12.06.95 12.06.95 ----------.. . --. ----. --.. ----.....
Laboratorltt In Sevannah, GA • Ta//thacaee, FL • Tampa, Fl. • O.erf/tld BHCh. FL • Mobile. AL • New Orl111n1, LA I
::EC-07-1995 ,7:38 FROM SAVF'NNAH LABS TO 917043911147 P.07 • • SL SAVANNAH LABORATORIES
& eNV/fllONMt:NTAL 3t:RVICD, INC.
'') 5102 LaRoche Avenue• Savannah. GA 31404 • (9 12) 354-7858 • F11x (ll1:>) ~:'l;>.()1fl5
Mr. John Rhyna
OHM Corporation
5335 Triangla PkW"/. Suitt 450
Norcro~~. QA ~0093
CC: Jack Kilbarger
REPORT OF RESUI,TS
100 NO: S5·56748
Rac:oivod: 05 DEC 95
Reported: 07 D!C 95
Purchase Order: 1016477
Project: 16817 Cherokee Oil
Sampled By: Cl:.ent •
DATE/
LOG NO SAMPL! DESCRIPTION, SOLID OR SEMISOLID SAMl'LES TIMI! SAMPLED
55748·1 CO·WS-33
SG7~0-2 CO·WS•3~
56748·3 CO•WS-35
56748-4 CO·WS-36
56748·5 CO·WS-37 ............ __ ---.......................................................... -............. .
12-04·95/lS00
l:i•04·95/J.U0
12·04·95/1420
12·04·95/1450
12·04·95/1430
PARAMBTl!:R 56"/48·1 5~748·2 56748·3 56748·4 5(;748·5
Arsenic
·.) Arsenic (6010), mg/kg dw
Date Analyzed
15
12.06.95
18
12.06.95
17 22 17
12.06.95 12.06.95 12.06.95
)
.t1arium (G0l0)
Barium (60:0), mg/kg dw llO 'n 110 130 Dllt" . ., J>.naly,<>d l:l .o, .95 1J.OG.95 12.06.SS 12.06.95 Cadmium (6010)
Cacl!:li\lll\ (6010), mg/kg dw l.l <0.60 <0.60 <0.61 Data Analyzed -:.2 .06 .95 12.06.95 12.06.95 12.06.95 Chromium (6010)
C~romium (,010), mg/kg dv Sl 46 38 u Date Analysed 12 .06 .95 12.05.95 l:1.06.95 12.06.95 Mercury
Mereur-, (7470/7471), mg/kg dw 0.12 O.ll 0.071 0 .077 Date Analysed 12. 06. 95 12.06.9S 12.06.95 12.06.9S !':ilve:i: (GOlO)
Silver (6010), mg/kg dw <l.l <.l.2 <l.2 <1.2 Date Anal:,,:ed 12.06.95 U.06.95 12.06.95, 12.06.95 Selenium
Selenium (6010), mg/kg dw <ll <12 <12 <•4*F65 Da.te Allaly•,.<l !,l.06.5'~ l.Z.Q~.95 l.i.06.95 l2.06,9S
77
:i.a.06.ss
<0.75
12.06.95
2,
12.06.95
0.091
12.06.95
<l.S
12.06.95
<30*F65
12. 06 .95
ubor•toriea In SoYonnoll, OA • T•//•honn, f'L • T•mp•, l'L • Defllfleld fleacfl, l'I. • Mobile, Al. • New Orle11ns, LA
rEC-07-1995 17:39 FROM ~ LABS
SL SAVA~NAH tloRATORIES -
& l!NVIRONlll!NTAL SERVICES, INC.
TO 917043911147 • P.03
-) 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: SS•SS748
05 DEC 35
07 DEC 35 Mr. John Rhyne
OHM Co"l)O>:':>t:ion
533S Trianil• Pkwy. suite 450
Norcross, GA 30092
CC: Jack Kill:>arger
REPORT OF RESULTS
Received:
Reported:
Pi.irchaae Order: 1015•77
Project: 16817 Cherokee Oil
SampleO Hy: Client
DATE/ LOG NO
56748-1
56748•2
56748·3
56748-4
,,6-l4ij •5
SAMPLE DBSCRIPTZON, SOLID OR SEMISOLID SAMPLES
CO•WS•33
TIME $1,MPLJi:D
12·04•95/lSOO
12-o,-9s/1uo
12•04•95/1420
12·04•95/USO
l2·04-9S/l430
CO-WS-34
CO•WS•3S
CO•WS•36
CO•WS-37
Lead (6010)
_ Lead (6010), mg/kg dw
·) Date Analyzed
PG>:'Cant Solidc c1,o.J), ~
)
110
12.06.9S
OQ
140
12.06.95
83
75 62 150
12,06.95 12.06.95 12.06.95
83 82 67 -. -----... -

-
-
-
-
-
-
-
. -.. ----------
'--bon,torles In Savannah. GA • Tal/ahnn•. FL • Tamp,,, FL • DHrfleld "-"""· l'l • Mohl/ft, AL • NttW Ot/lUlnll, LA
)
!:EC-07-1 995 l 7: 39 FROM SAVFN-IAH LABS TO 917043911147 P.09
SL SAVA~NAH ifeoRATORIES
& INVIRONM!NTAL SaRVIC~I:, INC.
•
5102 LaRoche Avenue • Savannah, GI>. 31404 • [phone] • Fax [phone]
Mr. John Rhyne
OHM Corpo.i:a.t..l1.1u
S335 Triangle PkV/. Suite 450
Norcross, GA 30092
CC: Jack Kilbarger
P.EPOP.T Oi" P.ESULTS
LOG NO: S5•56748
Received: 05 Die 95
Reported: 07 DEC 95
.Purchase order: 1016477
Project: l6817 Cherokee Oil
Sampled By, Client
Paga 9
DATE./ LOO NO SAMPLE DESCRZ?TION, SOLID OP. SEMISOLID SAMPLES TIMI! SAMPLED
PARAMETER
Volatiles by GC/MS (8240)
Chloromethane, ug/kg d·#
BrQ~Ofllceho.12.a, ~g/kg dY
Vinyl chloride, ug/kg dw
Chloroetha.ne, u0/kg dw
Methylene chloride (Dichloromethar.e), ug/kg dw Acetor.e, ug/kg dw
C~rbor. c:lisul!l~•, ug/kg dw
l,l•Dichloroethene, ug/kg dw
1,1-Dichloroethane, ug/kg cw
Cis/Trans•l,2-Dichloroethene, ug/kg dw
Chloroform, ug/kg dw
~,~•DichlO:rQCCn:ino, ~g/kg dw
2-Butanone (MEK), ug/kg dw
l,l,l·Trichloro1>thru,A, 119/kg dw
Carbon tetrachloride, ug/kg dw
Bromodichlorcmethane, ug/kg dw l,l,2,2-Tetrachloroethane, ug/kg dw
1,2-Dichloropropane, ug/kg dw
trans-1,l-Dichlorop:opane, ug/kg dw
Trichloroethene, u9/k9 dw
Dibro:r.oc:,loromeehane, ug/kg d· .. l,l,2-Trichloroethane, ug/kg dw
Benzene, ug/kg dw
56748-6
<1700
<~700
<1700
<l 700
<840
<8400
<840
<840
<840
<840
<840
..:840
20000 \_./".
,:9,40
<840
<840
<840
<840
<840
<840
<840
<840
<840
Lal:,or,toriH In S.t,::innolt, OA • T1//ah,usaa, FL • Tampa, FL • Deerlfeld 8eaeh, FL • Mob/la, AL • New Or/eana, LA
I:EC-07-1995 17:40 FROM SAV~ LABS
S. L SAVA~NAH tloRATORIES
& !!NVIRONMtNTAL SEJIVICES, INC.
TO 9, 7043911147 P.10 •
-) 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. John Rhyn•
OHM Cnrror,.hon
5335 Triangle Pkwy. Suite 450
Norcross, GA 30092
CC: Jack Kilbarger
REPORT OF RESOl..TS
1.-0G NO: S5•55748
Received: OS DEC 95
Reported: 07 DBC 95
Project, 16817 Cherokee Oil
Sampled By: Cll,;,n~
Paqe lO
DATB/ LOG NO SAMPLB DESCRIPTION, SOLID OR SBMISOLID SAMPLBS TIMi SAMPLED
56748-6 CO•WS-38 12-04-95/1530
eis-J., J ·Dichloz:o,p..-vpt:,uu, ug/kg <:iw
Bromofor:n, ug/kg dw
2-Hexancne. ug/kg dw
4•Methyl-2-pentanone (MIBK), ug/kg dw
Tetrachloroethene, ug/kg dw
Toluene, ug /kg dw ·
) Chlorobenzene, ug/kg dw
EthylbenzP.nA, ug/'.cg dw
Styrene, ug/kg dw
Xylenes, ug/kg dw
surrogate Toluene•d8
Surrogate• 4·BrOIIIOfluorobenzene
Surrogato -1,2-Diohloroeeh~e d4
!late Analyzed
<ij40
<840
<g400
<8400
<8'0
7400
<840
2800
<840
1700
109 4-
109 t
:z.03 1-
12. 06, 95
Llboratorlet In Savannah, GA • T1l/1hl .. ff, FL • Tampa, FL • Detrlftld Bffch, FL • Mob/It, Al. • New Orleans, LA
)
rEC-07-1 995 17: 40 FROM SAVA'-i!'IAH LABS TO 917043911147 P.11
SL SAVA~NAH ~ORATORIES
& ENVIRONMENTAL SERVIC!S. INC. •
5102 LaRoche Avenue • Savannah, GA 31404 • (9:2) 354•785a • Fax [phone]
Mr. John Rhyne
OHM Corpo~~tion
5335 Triangle Pkwy. suite 450
Norcross, GA 30092
CC: Jack Kilbarger
REPORT OF RESULTS
LOG NO: SS-56748
Received: 05 OEC 9S
Reported: 07 DEC 95
?roject: 16817 Cherokee Oil
Sampled 5y: Client
DATE/ LOG NO SAMPLE DESCRIPTION, SOLID OR SE:ilSOLID SAMPLES TIME SAMPLED
56748·6 CO-WS-38 l2•04·95/l530
PJ>.AAM!!TBR
·1-c1.o ~ernivola.ti.1.es 18270)
Phenol, ·~g/kg d•,1
hi~(?.-~h1o~o~thyl)ether, ug/kg dw
2-Chlorophencl, ug/kg dw
1,3-Dichlorobenzene, ug/kg dw 1,4-Dichlorobenzene, ug/kg dw
1,2•Dichlorobenzene, ug/kg dw
2•Methylphenol (o-orosol), ug/kg dw
2,2'-Cxybis(l•Chlorcpropane)
(bis-2-chloroisopropyl ether), ug/kg dw 3·Methylphenoll•·Methylphenol(m&p•cr,;,sol), ug/kg dw N-N~troso-di•n·propylainine, ug/kg dw Hexaohlor0<0tho.ne, ug/kg dw
Nitrobenzene, ug/kg dw
Isophcrone, ug/k~ dw
~-Nitrophenol, ug/kg dw
2,4•Di:ne:hylphenol, ug/kg dw bis(2•Chloroechoxy)methane, ug/~g aw
2,4-Dichlorophenol, ug/kg dw
l,2,4•TrichlcrobenzanA, 119/kg dw Naphthalene, ug/kg dw
4-Chloroaniline, ug/kg dw
Kexaoh10:-00utadiene, ug/kg dw '
4•Chloro•3·methylphenol, ug/kg dw
S6748-6
<8900
, <8~00
<8900
<8.900
<8900
<8.900
~uco
<8900
<8.900
<8900
<3900
<8900
<8900
<8900
<8900
<8.900
<8900
~8900
<8.900
<18000
<8900
<8900 ............................ ___ --------·· .. -------------------
Liboratories In S1v1nn1h, GA • Ta//ahauGD, FL • T•mp11, FL • O.•rflold S.a<!h, FL • Mobil•. AL • New OrlHns, I.A
CEC-07-1995 ,7:41 FROM SAUi'tiNAH LABS TO 9, 7043911147 P.12 • • SL SAVANNAH LABORATORIES
& l!NVlltONMENTAL 31:/tV/CES, INC,
5102 LaRoche Avenue• Savannah. GA 31404 • (912) 354-7R!'iR • l"a• [phone]
Mr. John Rhyne
OHM Corporation
5335 Triangle Pk,,.,. suite 450 Noreros£, GJ\ l0092
CC: Jack Kilbarger
P.EPORT OF R3Sl.7LTS
1,0G NO: SS-56748
Received: os csc s~
Reported: 07 DSC 95
Purchase Order: 1016477
Project: 16817 Cherokee Oil Sampled By: Client
Page 12
DATE/ l,00 NO SAMPLE DESCRIPTION, SOLID OR SEMISOLID SAMPLES TIME s»l:i'LSD
56748•6 CO·WS-38 12-04-jS/lSJO
PARAMETER
2-Methylnaphthalene, ug/kg dw Hexachlorocyclopentadiene, ug/kg dw 2, 4, 6 ··rrichloropnenol, ug/kg aw 2,4,S•Trichlorophenol, ug/kg dw 2-Chlor~n~~hth~l~ne, u~/kg dw 2-Nitroanilir.e, ug/kg dw _) Dimethylphthalate, ug/kg c:lw Acenaphthycene, ug/kg dw
3-Nitroaniline, ug/kg dv A<,gnaphthene, ug/kg dw
2,4-Dinitrophenol, ug/kg dw 4-Nitrophenol, ug/kg dw Dioenzofura.n, ug/kg dw
~.4-Dinitrotoluene, ug/kg dw ~,~.ninitrotoluene, u~/k~ dw Diethylphthalate, ug/kg dw 4·Chlorophenylphenyl ether, ug/kg dw Fluorene, ug/kg dw
4-Nitroani:ine, ug/kg dv 4,6-Diz,it;Lo·2·met:hylpheno1, ug/kg aw N-Nit:osod~phenylamine/Oiphenyla.~ine, ug/kg dw 4-Bromophenyl phenyl ether. ug/kg dw Hexacr.lorobenzene, ug/kg dw
Pentachlorophenol, ug/kg dw
10000
<8900
<8900
<8900
<9900
<46000
<8900
<8j00
<46000
,a,o o
<45000
<46000
<8900
<8900
.a,oo
18000
<8900
<8900
<46000
<4bOCO
<8900
.. ~~co
<8900
<46000 -----------------------------·---~----· ······-----------------------· -----·-·--
)
Labor•tories in Se,annah, GA • T1//1hassee, FL • Tampa, FL • Dffl1/e/t1 EUIICII, FL • MODi/1, AL • New Or/tan,, LA
CEC-07-1995 :,:.i2 FROM SAVl'N-A-I LABS TO 9: 7043911147 P.13 ·s L SAVANNAH ifsoRATORIES
& l!NVIRONMl!NTAL SERVICES, INC. •
) 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
LOG NO: SS-5'748
05 DiC 55
07 DEC g5
)
Mr. John R.'1yne
C"!HM Cni,;:o,..l'..tion
5335 Triangle Pkwy. Suite 450
Norcross, GA 30092
CC: Jack Kilbarger
R.sPORT OF RESULTS
Receivvd:
Reported:
Project: 16817 Cherokee Oil
Sampled B1: Cll,;,<ll.
Pa9e 13 DATE/ LOG NO SAMPLE DESCRI?TION, SOLm OR SEMISOLID SAMPLES TIMB SAMPLED
S6748·6 CO·WS-38 12·04·9S/1S30 ----·····---------·•·········---------··················-----------·----------------' P.M.AMETER
Plii:,ucu1thre.1e, ug/k'J dw
A.~thracene, ug/kg dw
Di•n•butylphthalate. ug/kg dw Fluoranthene, ug/kg dw
Pyrene, ug/kg dw
Bu~ylbenzylphthalate, ug/kg dw
3,3'-Dichlorobenzidine, ug/kg dw
!!An«>(,.) Anthr,.c,,n", tt!;l/k17 dw
bis(2·Bthylhexyl)phthalate, ug/kg dw Chrysene, ug/kg dw
Di-n-octylphthalate, ug/kg dw
Benzo(b)fluoranthene, ug/kg dw San•o(k)fl\.lo:ro.nthcne, u9/l<g '1><
Ben:o(a)pyrene, ug/kg dw
Indeno(l,2,3•cd)pyrene, ug/kg dw Oibenzo(a,h)a.nthracene, ug/kg dw
Benzo(g,h,i)perylene, ug/kg dw
Carbazole, ug/kg dw
Surrogate Phenol dS
Sur=ogate 2·Fluorophenol
Surrogate 2,4,6-Tribromophenol
Surrogate Nitrobenzene • dS
Su.:~u~O.Lw Z•ll'l,UQ:C-Obiphenyl
Sur=ogate Terphenyl • dl4
Date Bxtracted
Date Analyzed
56748-6
<8~00
c9900
'loOOO
<8900
<8900
93000
<18000
<9goo
120000
<8900
<8900
<8900
,e,oo
<8900
<8900
<8900
<8900
ca,oo
•p33
•F33
*F33
•F33
•F~:S
*Fll
11.0'i.~'i
12.07,95
Lllboratorlea In Su1nnah, QA • Ta/lah11-. FL • Tampa, FL • Dflflrlleld Beach, FL • Mob/le, AL • New Orleans, LA
J:EC-07-1995 17:42 FROM SAVA'-INAH LABS TO 917043911147 P.14 • • SL SAVANNAH LABORATORIES
t ENVIRONMl:NTAL 3BIVICO, INC.
', 5102 LaRoche Avenue •Savannah.GA 31404 • [phone] • F11x (91::!) 352-0185
)
Mr. John Rhyne
OIIM Corporation
5335 Triangle Pkwy. Suite 450
Norcro••, Cl.71. l009~
CC: Jack Kilbarger
REPORT 01' RES'Ol.TS
LOG HO: SS·S674i
Rccoivod, OS PSC 95
Reported: 07 DSC 95
Purchase Order: 1016477
Project: 16817 Cherokee Oil
Sampled By: Client
Page 14
DA.TB/ LOG HO S-?.MPLB DESCRIPTION, SOLID OR SEMISOLID ~LES Til!lB SAMPLED
56748•6 CO·WS-38 il-04·95/1530
PARAMETBR 56748-6
Percent solids (160.3), t 74
LAl>oretorlH In SaY11nn111h, QA • Ta/lahasser,, l'L • Tampa, l'I. •·DHr1flltl SNcn, Fl.• Mob/It, Al.• NtW o,,.,n,, I.A
r:EC-07-1995 17:43 FROM SAUFNsAH LABS TO 917043911147 P.15
SL SAVA~NAH ~ORATORIES
& ENVIRONMENTAL SERVICES, INC. •
) 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
)
LOG NO
Mr. John Rhyne
OUM Co:i:poration
5335 TrillJlgle Pkwy. Suite 450
Norcross, GA 30092
CC: Jack Kilbarger
REPORT OF RESULTS
LOG NO: S5·56748
Received: 05 DEC 95
Reportad: 07 DRC PS
Purchasu 0.-der: 10Ui77
Project: 16817 Cherokee Oil
~ampled By: ~lient
P._l)'fl 15
SAMPLE DSSCRIPTlON, QC REPORT FOR SOLID/SEMISOLID
Method Blank 56748 • i
56748-8
56748-9
Lah Cnnr.rnl St~ndto.rd (LCS) • Reeovery/Duplieate
LCS t RPD
PARAMETER
Vol~tilea by CC/MS (8240)
Chloromethane, ug/kg dw
Bro1110111ethane, ug/kg dw
Vinyl chloride, ug/kg dw
Chloroethane, ug/kg aw
M.::thylene ehloride (Dieh:oromethar.e), u9/k9 dw
.Acetone, ug/kg dw
Carl)on disulfide, ug/kg dw
l,l·Dichloroethene, ug/kg dw
l,l-Dichloroethane, ug/kg dw
Cie/Trans•l,2-Di<.:hl<.>;i;,;,uthene, ug-/kg dw
Chloroform, ug/kg dw
1,2·Dichloroethane, ug/kg dw
2•Butanone (MEK), ug/kg dw
l,l,l-Trichloroeth&r.e, ug/kg dw
car~on tetrachloride, ug/kg dw
Bromodic:hloroznethane, ug/kg dw
l.1.2.2•Tetrachloroatha.n11, ug/kg tlw
l,2•Dichloropropane, ug/kg dw
trans-1,3-Dichloropropene, ug/kg dw
•Trichloroetnene, ug/kg dv
Dibromoc.~loromethane, ug/kg dw
56748•7
<10
<10
<10
<10
~!1.0
<25
<5.0
56748·8
<5.0 134/136 t
<5 .o
<5.0
<5.0
<5.0
<25
<5.0
<5.0
<5,0
~s.o
c5.0
<5.0
<5 .0 ll4/l20 t
<5.0
56748•9
l t
3 t
LabontorlH in S,ovannah, GA • Ta/lahatffe, FL • Tampa, FL • O.erll-1d /ieaoh, FL • Mob/lo, AL • Now Orla.,,,, LA
&
CEC-07-1995 17:44 FROM SAVl'N'm LABS
. SAVANNAH !soRATORIES s L & INVIRONIIINTAL. 11/ilW/Cff, INC.
TO 917043911147 P.16 •
, 5102 L&Roche Avenue• Savannah. GA 31404 • [phone] • Fax [phone] I
Mr. John Rhyne
OHM C<><pun.l;ion
5335 Triangle Pkwy, Suite 450
Norcross. GA 30092
LOG KO: SS-56748
Received: OS OEC 9S
Reported: 07 OBC 95
Purchase order: 1016477
CC: Jack Kilbarger Project: 16817 Cherokee Oil
Sampled Sy: CHent
LOG NO
S6748-7
56748-8
S6748-9
PAAAM!.TER
IUPORT OV IU~Ol.TS
S.Ai.'!PLE DESCRIPTION, QC REPORT POI>. SOLIO/SB~ISOLID
Method Slank
Lab Control Sc:u:,d.:lrd (LCS) t Recovery/Duplicate
LCS \ RPD
56748-7
l,l,~ Trichlo=~thane, Ui/kg dw
Benzene, ug/kg dw
c:is•l,3-Dichloroproper.e, ug/kg dw Bromo!ot111, ug/kg dw
.. i,. 0
<S.O
<5.0
<S.O
p.,,gc 16
·56748-8 56748•9
128/128 \ 0 t
J 2 • Hexa.none , ug/kg dw
4•Me:Lh;rl-2·J,,1•mtanone (IUB!C), usr/kg dw Tetrac:hloroethene, ug/kg dw
<25
<l!>
<5.0
<~.o
<S.O
<5.0
c5.0
cS.O
)
./
Toluene. ug/kg dw
Chlorobensene, ug/kg dw
Ethylber.:ene, ug/kg dw
scyrene, ug/kg dw
Xylenes, ug/kg dw
Surrog,111':A -T~,\l~ne-d8
Surrogate• 4-Bromotluorobenzene
Surrogate• l,2·Dichloroethane•d4
Dat!!! Analyzed
aa "' 104 t
94 \
12.06.95
\20/1 '~ 't
132/130 \
a,;s,"
100/96 t
92/94 \
12.04.95
5 t
2 '
Lllboratorle1 In Sav:tnnah, QA • Tallah///tlHe, FL. • Tampa, FL. • Deerll•ld Soeolt, Ft. • Mob/le, AL. • New Ot/Hne, L.A
I:EC-07-1995 17:44 FROM SAVA'INAH LABS
SL SAVA~NAH iloRATORIES
& ~NV/FIONM~TAL SERVICES, INC.
TO •
) 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone]
9: 7043911147 P.17
LOG NO:
Recei~d:
Reported:
SS•S6748
OS OS:C 95
07 os:c 95 Mr. John RhYDe
OUM Co:a.-por~ti0rt Purchase o,.-ae.c: 1015477 5335 Triangle Pkwy. Suite 450 Norcross, GA 30092
CC: Jack Kilbarger Project: 16817 Cherokee Oil
Sampled :By: Client
LOG NO
S6748•7
S6748·8
56748·9
REPORT OF RESULTS
SAMPLE OESCRIPTION, QC REPORT FOR $0LID/SEMISOLIO
Method Blank
Lab Control Standard (LC:S) t R"'mv,i,ry/T>up1ic-~t<> LCS 't RPO
56748·7 56748·8 56748-9 .... --..... ·----. -... -.-.... -------. -.. -. ----... --·------

-
-------............ -----.. --------. TC".T, i;~m:tvol~t.ileG (8270)
Phenol, ug/kg dw
bis(2·Chloroethyl)ether, ug/kg dw 2·Chlorophenol, ug/kg dw
) 1, 3-Dichlorobenzene, ug/1::g dw .. -· 1,4-Dichlorobenacnc, ug/i<g dw
1,2-Dichlorobensene, ug/kg dw
2•Methylphenol (o-cresol), ug/kg dw 2,2'•0xybis(l·Chloropropane)
)
(bis-2-chloroisopropyl ether), ug/kg dw 3-Methylphenol/-lo·Methylphenol(m&i:,•c.i::""vl), ,..y/l<y uw N·Nitroso-di-n•propylamine, ug/kg dw Hexachloroethane, ug/kg dw Nitroberu:ene, ug/kg dw
Isophorone, ug/kg dw
2•N1Lz:v1,1hvur.,l, ug/l<g mr
2,4•0imethylphenol, ug/kg dw bis(2-Chloroethox;r)~etha.ne, ug/kg dw 2,4-0ichlorophenol, ug/kg dw
l,2,4-Trichlorobenzene, ug/kg dw Naphth~lene, ug/kg dw
4·Chloroaniline, ug/kg dw
<330
<330
<330
<330
~330
<330
<330
<330
<330
c330
<330
<330
<330
<.3.30
<330
cun
<330
<330
<330
<660
67/76 t
67/73 t
70/70 ~
70/76 t
65/70 t
12 t
8 t
0 '
Llboralorlea In Savannah, QA • Ta/111h11SSH, FL • Tampa, FL • Doorllo/d Beach, FL • Mobti.. AL • Now Or/oana, LA
)
CEC-07-1995 ,7:45 FROM SAV~ LABS TO 917043911147 P. 18
SL SAVANNAH ~ORATORIES
& lNVIRONlttl!NTAL SERVICES, INC. •
5102 LaRocht Avenue •Savannah.GA 31404 • [phone] • Fax [phone]
Mr. John R.'lyn@
CHM Corpor~t:inn
5335 Triangle Pkwy. Suite 450
Norcross, GA 30092
CC: Jack Kilbarger
REPORT OF RBS'CiLTS
LOG NO: S5·55748
Received: 05 DEC 95
Re00rtad: 07 DBC 95
Purchaao Ordor, 1016477
Project: l68l7 Cheroku Oil
Eompled By: Client
Page 1a
LOG NO
56743·7
56748•8
56749-9
SAMPLE DESCRI?TION, QC REPORT FOR SOLID/SEMISOLID
Method Blank
Lab Control Standard (LCS) t Recover,-/DUDlic:ate LCS t RPO .
P;>.RAMETSR
Hexachlorobutadiene, u9/kg dw
4-Chloro-3-methylphencl, ug/kg dw
2-Methylnaphthalene, ug/kg dw
Hexachloroc:yc:lopencadiene, ug/kg ~w
2,~,6-Trichlorophenol, ug/kg dw
2 . 4, 5 -TrichlorO[>h"'nn l , ,,g /kcr dw
2-Chloronaphthalene, ug/kg dw
2-Nitroaniline, ug/kg dw
Dimethylphthalate, ug/kg dw
Acenaphthylene, ug/kg dw
3-Nitroanilir.o, ug/kg dw
Acenaphthene, ug/kg dw
2,4-Dinitrophenol, ug/kg dw
4-Nitrophenol, ug/kg dw
Dibensofuran, ug/kg dw
~,t·Dinitrotol1.1ene, ug/kg dw
2,6-Dinitrotoluene, ug/kg dw
Die:hylphthalate, ug/kg dw
4-Chlorophenylphenyl ether, ug/kg dw
Fluorene, ug/kg dw
~-Nitroeniline, ~g/~9 dw
(,6·Dinitro-~•methylphenol, ug/kg dw
<330
<330
<330
<330
<330
,.330
<330
<1700
<330
<330
<1700
<330
<1700
<1700
<330
d30
<llO
<330
<330
<llO
<1700
<1700
73/79 t
70/76 t
73/76 t
82/&8 \
8 I
7 '
Lil'boratoriH In S1v1nn1h, GA • T1//1hnna, FL • Tampa, FL • O..rll_,d Beach, FL • Mob/le, Al. • New Or/Nns, LA
CEC-07-1995 17:45 FROM SAV~H LABS • TO • 917043911147 P.19
SAVANNAH LABORATORIES
& ~NVIRONMliNTAL SERVICQ, INC, SL
--1 5102 l.4Roche Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. John Rhyne
OHM Coq,oration
5335 Triangle Pkwy; Suit• ,so
Norcrose, ClA 30092
CC: Jack Kilbarger
Rli:PORT OF RE.llTJLTS
LOG NO: SS·S67t8
Received: OS D~C 9S
Reported: 07 DEC 95
Purchase orcier: 101~477
Project: 16817 Cherokee Oil
Sampled By: Client
LOO NO si.MPLE DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
SG;48•7
s,1H-8
56748·9
Method Blank
L"1> Codtrol Ctanclard (~CS) ~ Recovery/1:>\iplicate
LCS !I-RPO
PJ\RA.'JETER 56748•7 55748•8 56748•9 --·········--··----•··-·-···-----........ ------------------------------.......... . N-Nitrosod.iphenylAmine/D.i.pht!:uyl~iuw, ug/k.g dw
4•Bromophenyl phenyl ether, ug/kg dw
Hexachlorobenzene, uq/kq dw
Pentachlorophenol, ug/kg dw
<330
<330
<330
48/48 t 0 t
1 Phenanthrene, U9'/k9' dw
<1700
<330
<J30
<330
d)O
<330
<330
<660
<330
cno
<330
<330
<330
<330
~no
<330
<330
<330
<330
)
Anthracene, U9'/kg C,.w
Di·n·butylphthalate, ug/kg dw
Fluoranthene, ug/kg dw
Pyrene, ug/kg dw
Butylbenzylphthalate, ug/kg dw
3,J'•Dien~orobenzicline, ug/k9 dw
Benzo(a)anthracene, ug/kg dw
bis(2-Kthylh•xyl)phth•late, ug/kg dw
Chrysene, ug/kg dw
Di•n-octyll)hthalate, Ui,/kg dw Benzo{b)fluoranthena, u9/kg dw
Benzo(k)fluoranthene, ug/kg dw
Bcnao{~)pyronQ, ug/kg dw
Indeno{l,2,3•cd)pyrane, ug/kg d~
Diben,o(a,h)anthracene, ug/kg dw ienzo(g,h,i)perylene, u9'/kg dw
Carbazole, ug/kg dw
65/65 t 0 t
Labor.ttories In S•v■nnah, QA • TollohnaH, FL • Tampa, FL • Oeerlie/d BeKh, FL • Mob/le, AL • New Or/Hna, LA
CEC-07-1995 :7:45 FROM SAVA'ffiH LABS • TO • SL SAVANNAH LABORATORIES
& 5NVIRONlll/iNTAL $IAV/Cft, INC,
, 5102 LaAOChe Avenue • Savannah, GA 31404 • (912) 354•7858 • Fax [phone] '
9: 7043911147 P.20
LCG NO: S5-56748
Received: OS DBC 95
Reported: 07 DiC 95 Mr. John Rhyne
OHM C:orpor11t:ion li'Urchase orcer: 1016477 533S Triangle Pkwy. Suite 450
Norcross, GA 30092
CC: Jack Kilbarger Project: 16817 Cherokee Oil
Sampled By: Client
~POP.':' OV !Ui:Stn.TS
LOG NO SJ\MPLE DESCRIPTION, QC REPORT FOR SOLID/Sl!MISOLID
Method Blank 56748-7
s,,o. s
56748-9
, Lab Co~trol Stan&>.rd (LCS) t naeovery/Duplicate
LCS t RPO
PARAMETER
Surrosate Phenol cl:;
surrogate 2-Fluorophenol
Surrogate 2,4,6-Tribromophenol
Surrogate Nitrobensene • dS
') s·~rrogate 2•P'luorobiphenyl
Swci:'-'\l"t" Terphenyl • dl4
Date Extracted
Date Analysed
Arsenic
Arsenic (6010), mg/kg dw
uat:e Analysed
Barium (6010)
)
Barium (~010), mg/kg dv
Date Analyzed
Cadmium (6010)
cac,m1\ll!\ (6010), mg/kg dw
Date Analyzed
Chromi,..,, (i0l0)
Ch,:-omium (6010), mg/kg dv
Date J\nalyzed
Mercury
Mercury (7470/7471), mg/kg dw
I>o.to An<1,lyoed
56748•7
82 t
73 t
est
70 t
76 %
7U t
12.0S.9S
P.06.95
<l. .0
12.06.95
<0.50
12.06.95
<l.0
12.06.95
<0.010
12.os.,~
56748•8
73/7, t
70/73 t
82/85 t
65/70 t
70/76 \-
7U/7~ \'
12.05.95
l:l.06.95
103/99 t
12.06.95
96/92 t
12.06.95
101/98 t
12.06.95
99/96 \-
l2. 06 .95
96/10, t 12.os.,s
S6748·9
4.0 t
3. 0 t
3.l t
6. l l-
I:EC-07-l 995 17: 47 FROM SAUFNNAH LABS TO 9: 7043911147 P,21
• • • -5 L SAVANNAH LABORATORIES
& liNVIRONN!NTAL S5RVICff, INC.
•
51021.ARoct,e Avenue• Savannah, GA 31404 • [phone] • Fax [phone]
Mr. John Rhyne
OHM Cv•1,1vr•ticm
5335 hiangl• Pkwy. Suit• 450
Norcross, GA 30092
U)G NO:
Received:
Reported.:
s~-,~74~
OS Dli:C: 95
07 DEC 95
c~-Jack ~ilbarger Project: 16817 Cherokee Oil
Sampled By: Clie~t
P.EPORT 011 R!i!SULTS
LOG NO
5G7O·7
s,7,a-a
56743•9
SAMPLi DESCRIPTION, QC REPORT FOR SOLID/SEMISOLID
M• 1.hw !1lt11,l,;
Lab Ce>ntrol Standard (LC.S) \-Reoov,:zy/rluplic:,.t0
LCS t RPO
PARAMiTBR
Silvc>:' (60l.0)
Silver (6010), mg-/kg-dv
Date lu:lalyzed
Selen~um
Selenium {6010), mg/kg dv
) Date Analy•e<l
L"lld ('010)
Lead. (6010), mq/kq dw
Date 1..rlaly:ecl ---· .... --------------.. ----.....
Met:hods: E~A SW·84b
56748•7 ........ ---.. -..
•1.0
12.06.95
<10 12.os.,s
<5.0
12.06.95 ...... --..
Page ~l
56748•8 56748·3 .......... --.... -.... --.. --. -
99/96 • 3., • 12.06.95
96/94 ' 2.1 ' l.2.0~.,5
99/98 ' l.O ' 12.06.95
----------. . ----... -
•F33 ~ Cont~ol lim:i.es a~e eata.bli5hed only to• surrogate concentration lev-els specifi11d J:,y 11:PA mP.1':hnt!,., 111.,c,mse ~h .. sample was diluted prior to analysia, s~rrogate recoverie5 are not reported.
•F65 • Eleva-:ed detection limite were :reported due to sample matrix
interfe:ii.-e:nce '#hl.c.:h L·•"iu..i.z.vd 1:1ample or ex1=.ract dilution.
Steven J. White, Project Mar.ag,,r 41"1 .
Final Pag9 Of Report
· Uoboratorl•a Jn Savenneh, GA • Ta//ah .. too, FL • Tampa, FL • DHrll•lrJ BHch, FL • Mob/le, A~ • New Orlean•, U
TOTAL P.21
CHAIN OF CUSTODY
· Fll1l,d pH·, .· :J},i\'t.f,
· Result_;_·:_·''-'. "c..' '-'-~'-'--c·
, Analyst .c.· ---'--'--'--
:.:Time/Date ....
· · (QA/QC Separate) O: ;,
;
·s ~· . ·~-~ . . .
Please sign and return the white.~ndyellow copie~
to·the Laboratory ... ·. · ~t" .. : .. :·' '.i:'·. :.
··,f":.r·· . .. • ... :::5ft~~Wi,-
DEC 14 '95 15:12 TO 3911147
Qm!!i
Environme11tal
Consultants. Inc
• FROM AquaChem Enu\r. Lab T-810 P.02 •
OEC
Certificate of Analysis
Client: OHM Corporation North Carolina Certlflcadon Number: 305
2401 Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 381 Receipt Date: 30-Nov-95
Contact: Jack Kilbarger Report Date: 14-Dec-95
Sample Date: 30-Nov-95 ill ill ffi ~
SDG#: SDG-000502
Approved By:
Lall Sample ID:LSID-001951 Kenneth R. Richardoon
Sample ID: CO-WS-31 Project Manager
Reporting.
Parameter Result Limit Unit Method Time Date
1,1, 1-Trichloroelliane u 5 ppb EPA 80 I 0/8020 20:31 12/4/95
I .1,2,2-Tetrachloroethane u s ppb EPA 8010/8020 20:31 12/4/95
I, 1,2-Tichloethane u 5 ppb EPA 801018020 20:31 12/4/95
I, 1-Dichloroethane u 5 ppb EPA 8010/8020 20:31 12/4/95
1.1-Dichloroethene u 5 ppb EPA 8010/8020 20:31 12/4/95
1,2-Dichloropropane u 5 ppb EPA 8010/8020 20:31 12/4/95
1,2-Dichlorobenzene 15 5 ppb EPA 80 I 0/8020 20:31 12/4/95
1,2-Dichloroethane u s ppb EPA 8010/8020 20:3 I 1214/95
1,3-Dichlo!Obenzcne LT 5 ppb EPA 801018020 20:31 12/4195
1,4-Dichlorobenzcne u 5 ppb EPA 8010/8020 20:31 12/4/95
2-chloroethyl vinyl ether u 5 ppb EPA 8010/8020 20:31 12/4/95
Benzene u s ppb EPA 8010/8020 20:31 12/4/95
Bromodichloromethane u 5 ppb EPA 801018020 20:31 12/4/95
Bromoform u s . ppb EPA 8010/8020 20:31 12/4/95
Bromomethane u 5 ppb EPA 8010/8020 20:31 12/4/95
Carbon tetrachloride u 5 ppb EPA 8010/8020 20:31 12/4/95
Chlorobenzene u 5 ppb EPA 80 I 0/8020 20:31 12/4/95
Chloroethane u 5 ppb EPA 8010/8020 20:31 12/4/95
Chloroform u s ppb EPA 80 I 018020 20:31 1214/95
Chloromethane u 5 ppb EPA 8010/8020 20:31 12/4/95
Dibromochloromethane u 5 ppb EPA 8010/8020 20:31 1214195
11176 Do,ms Ro .. -PlnovW., NC 28134 Phone: (704)!88-5076 -FAX: ~04)588-24M
Page I
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Analyst
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DEC 14 '95 15:12 TO 3911147
Qmni.
Environmental
Consultants. Inc
• FROM AquaChem Enu\r. Lab T-810 P.03 •
OEC
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 381 Receipt Date: 30-Nov-95
Contact: Jack Kilbarger Report Date: 14-Dec-95
Sample Date: 30-Nov-95 ill) ill &~
SDG#: SDG-000502 Approved By:
Lab Sample ID:LSID-001951 Kenneth R. Richardson
Sample ID: CO-WS-31 Project Manager
Reporting
Parameter Result Limit Unit Method Time Date
Ethylbenzene 44 5 ppb EPA 80 l0/8020 20:31 12/4/95
Methylene chloride u 5 ppb EPA 80 I 0/8020 20:31 12/4/95
Tetrachloroothene u 5 ppb EPA 801018020 20:31 12/4/95
Toluene 19 5 ppb EPA 801018020 20:31 12/4/95
Total Xylcnes 226 5 ppb EPA 801018020 20:31 ll/4/95
trans-1,2-Dichloroethcne u 5 ppb EPA 80 l018020 20:31 12/4/95
trans-1,3-Dichloropropene u 5 J>pb EPA 8010/8020 20:31 12/4/95
Trichloroethene u 5 ppb EPA 801018020 20:31 12/4/95
Trichlorofluorornethane u 5 ppb EPA 801018020 20:31 12/4/95
Vinyl chloride u 5 ppb EPA 8010/8020 20:31 12/4/95
1.2,4-Trichlorobenzene u 20 ppb EPA 8270 12/12/95
1,2-Dichlorobenzene u 20 ppb EPA 8270 12/12195
1,3-Dichlorobcnzenc u 20 ppb EPA 8270 12/12195
1,4-Dichlorobenzene u 20 ppb EPA8270 12/12195
2,4,5-Trichlorophenol u 20 ppb EPA 8270 12/12195
2,4,6-Trichlorophenol u 20 ppb EPA8270 12/12195
2,4-Dichlorophcnol u 20 ppb EPA 8270 12/12/95
2.4-Dirnethylphenol u 20 ppb EPA8270 12/12/9S
2,4-Dinitrophenol u 20 ppb EPA8270 12112/9S
2,4-Dinitrotoluene u 20 ppb EPA 8270 12/12/95
2,6-Dinitrotoluene u 20 ppb EPA 8270 12112195
1117' llowu Road . Pln••llle, NC 2813-4 Phone, (704) 588-50?6 FAX, (704) !88-24!4
Page 2
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Analyst
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SJ
SJ
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SJ
SJ
SJ
SJ
DEC 14 '95 15:13 TO 3911147
Qm!li.
Environmental
consultants-Inc
• FROM AquaChem Enuir. Lab •
OEC
Certificate of Analysis
T-810 P.04
Client: OHM Corporation North Carolina Certification Number: 305
240 l Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 381 Receipt Date: 30-Nov-95
Contact: Jack Kilbarger Report Date: 14-Dec-95
Sample Date: 30-Nov-95 rn rn ~ ~
SDG#: SDG--000502
Approved By:
Lab Sample ID:LSJD-001951 Kenneth R. Richardson
Sample ID: CO-WS-31 Project Manager
Reporting
Parameter Result Limit Unit Method Time · Date
2-Cbloronaphthalene u 20 ppb EPA 8270 12/12/95
2-Chlorophcnol u 20 ppb EPA 8270 12/12/95
2-Methlyphenol (o-cresol) u 20 ppb EPA 8270 12112195
2-Methylnaphthalene u 20 ppb EPA 8270 12112/95
2-Nitroaniline u 20 ppb EPA 8270 12/12/95
2-Nitrophenol u 20 ppb EPA 8270 IVl2/95
3,3-Dichlorobenzidine u 20 ppb EPA8270 12/12/95
3-Nitroaniline u 20 ppb EPA 8270 lVl2/95
4,6-Dinitro-2-methylphenol u 20 ppb EPA 8270 12/12/95
4-Bromophenyl phenyl ether u 20 ppb EPA8270 12/IV95
4-Chloraniline u 20 ppb EPA8270 12/12/95
4-Chloro-3-rncthylphenol u 20 ppb EPA 8270 12/12/95
4-Chlorophenyl phenyl ether u 20 ppb EPA 8270 12/12/95
4-Methylphenol (p-cresol) u 20 ppb EPA 8270 12/12/95
4-Nitroaniline u 20 ppb EPA 8270 12/12/95
4-Nitrophenol u 20 ppb EPA 8270 12/12/95
Acenaphthene u 2U ppb EPA 8270 12/12/95
Acenaphthylene u 20 ppb EPA 8270 12/12/95
Anthmcene u 20 JJPb EPA 8270 12/12/95
Benzo (a) anthmcene u 20 ppb EPA 8270 12/12/95
Benzo (a) pyrene u 20 ppb EPA 8270 12/12/95
11176 llowns Road. Plnevllle, NC 281l4 Phone: [phone] -FA.X: (704) 588-l4SI
Page 3
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Analylt
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SJ
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SJ
DEC 14 '95 15:14 TO 3911147
Qmni
Environmental
Consultants. lnc
• FROM AqeaChem Enu\r. Lob T-810 P. 05 •
OEC
Certificate of Analysis
Client: OHM Corporation North Carolina Certification Number: 305
240 I Tuckaseegee Road South Carolina Certification Number: 99032
Charlotte, NC
Client#: 381 Receipt Date: 30-No,·-95
Contact: Jack Kilbarger Report Date: 14-Dec-95
Sample Date: 30-Nov-95 00 Uct ffi ~ u
Approved By:
SDG#: SDG-000502
Lab Sample ID:LSID--001951
Kenneth R. Richardson
Sample ID: CO-WS-31
Project Manager
Reporting
Parameter Result Limit Unit Method Time Uate
Benzo (b) fluoranlhene u 20 ppb EPA8270 12/12/95
Ben1.o (ghi) perylene u 20 ppb EPA 8270 12112195
Benzo (k) fluoranthene u 20 ppb EPA8270 12112/95
Benzoic acid u 20 ppb EPA 8270 12/12/95
Benzyl alcohol u 20 ppb EPA 8270 12112/95
Bis (2-chloroethoxy) methane u 20 ppb EPA 8270 12112/95
Bis (2-chloroethyl) ether u 20 ppb EPA 8270 12112/95
Bis (2-chloroiscprobyl) ether u 20 ppb EPA 8270 12112/95
Bis (2-ethylbexyl) phthalate 38541 20 ppb EPA 8270 12/12195
Butyl benzyl phthalate 24568 20 ppb EPA 8270 12112/95
Chrysene u 20 ppb EPA 8270 12112195
Di-n-bulyl phthalate 9754 20 ppb EPA 8270 12/12/95
Di-n-octylphthalate u 20 ppb EPA8270 12/12/95
Dibenzo (ah) anthraccne u 20 ppb EPA 8270 12112/95
Dibenzofuran u 20 ppb EPA 8270 12112/95
Diethylphthalate u 20 ppb EPA 8270 12/12195
Dimethylphthalate u 20 ppb EPA8270 12/12/95
Fluoranthene u 20 ppb EPA8270 12/12195
Fluoreoe u 20 ppb EPA 8270 12/12/95
Hcxachlorobenzene u 20 ppb EPA 8270 12/12/95
Hexachlorobutadicne u 20 ppb EPA 8270 12112/95
11176 Downs Road. Pineville. NC 28134 Phone: (104)!1118-5076. FAX: [phone]
Page 4
Analyst
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DEC 14 '95 15;14 TO 3911147
Qml1i.
· E,wironmental
Consultants, Inc
•
Client: OHM Corporation
FROM HquaChem E~vir. LJb T-810 P.06 •
OEC
Certificate of Analysis
North Carolina Certification Number: 305 240 I Tuckaseegee Road Soulb Carolina Certification Number: 99032 Charlotte, NC
Client#: 381 Receipt Date: 30-Nov-95 Contact: Jack Kilbarger
Repor1 Date: 14-Dec-95
Sample Date: 30-Nov-95 ® [2 ~ ~ u Approved By: SDG#: SDG-000502
Lab Sample ID: LSID-001951 Kenneth R. Richardson Sample ID: CO-WS-31 Project Manager
Reporting
Parameter Remit Limit Unit Method Time Date Hexachlorocyclopentadiene u 20 ppb EPA 8270 12112195 Hexachloroethane u 20 ppb EPA 8270 12/12/95 lndeno (1,2,3-cd) pyrenc u 20 ppb EPA 8270 12112195 lsophoronc u 20 ppb EPA 8270 12112/95 N-Nitroso-di-n-propylamine u 20 ppb EPA 8270 12/12/95 N-Nitrosodipbenylaminc u 20 ppb EPA8270 12/12/95 Naphthalene u 20 ppb EPA 8270 12/12/95 Nitrobenzene u 20 ppb EPA8270 12/12/95 Pentachlorophenol u 20 ppb EPA8270 12/12/95 Phenanlhrene u 20 ppb EPA8270 !2/!2/95 Phenol u 20 ppb EPA8270 12/!2/95 Pyrene u 20 ppb EPA8270 12/!2195
lll76 °"""" Road-Plrumll,,,NC 28134 Phone; [phone]-FAX: [phone]
Page 5
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Analyst
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LAq~hem
ENVIRONMENTAL LABORATORIES, INC,
CHAIN c;;:. CUSTODY
11178 DOWNS ROAD 7041588--5076 PIN'f':ILLE, NC 28134 FAX 704/58&-2454
Phone Number: ,70 '-j ) )J )-01] 7 Client: Dali) Core,
Fax Number: <70'1 l__:1-__,_9:l~-~.ul-l:Y:7:~~~~~~~~~~~~~-Address: UoQ n,t.,.."' S-1:
Purchase Order Number: \DI 001,', City C kM /Jj e State: f} / · Zip: d 1, ; O 1, Certification Requirement:-----~~~~-------Contact Person IJ J,,, K k)b4,f;
Project Name:-=L'-'h_,.,_c-'-'Co"'k'-'-'n"--__,Dcc.,w· ! ________ _ Sampled By: J. k, / & a,1.,l . Rush C~arges Authorized O zes /81 No ./ I JI (J4'{ TAT tfq.,,')\l'
By relinqu1sh1ng this sample(s) to laboratory Personnel, I warram tha1 I am author1zed to enter rnto thrs agreemenr ror the Clj'nr named above and that I authOnze thep,elow analysis subr,ct 10 !He I rms and cond1oons on Che reve,se hereof
This agreement 1s gover by the 1erms d cond11JOns on the reverse Side hereol. AnalystS charges shall be as mcfuded m the Laboratones tee sdledule 1n effect at the time or the analysis. Relinquished 13y;f, -ai-F"'-'---'-}_,_, .,·==+-''-"'-'--"'----------------
.eceived By:_, 1;-' _· '=cLJ,,.~'-'-----JL-"-!-·--_)_,r::'-'f"'.
1
"')"'_(:_=· _"-------------
Date: _1_0_-__ ; 1_1-_9_-; _____ _
Date: /r:i · > r;. ·'/
Time: ~/l~O~D __ _
~ \ Time: ~/~------Relinquished By: ___ ~--------------------Date: ____________ _ Time: _______ _ Received By: ____ ~--------------------Date: ____________ _ Time: _______ _
I!! ~ fJi f li 88Eifl1111'/iiJ1!i11JJ!illi Samples received on ice? Yes □ No □ ~, Dale & Time . QJ U • tf "(' 0 -.J ~ ....... ,;c f .J:" Sample ID Samoled lab ID ""3 ,oo ;E: ... e:
Olher Analys~ Preseivative l0-\,/5-_ I/.. X Io-~•1-1,;
Ii ID " f,~.) Vol.tt -h, ik"'l 'bllO v.,, )L/O I
. :it · 1 t'-t/<J,11 tJ ,-,<,,tfatf' ~.LI ( . "•I JI. -111,1h,./ q)Jv .k ~5"00
T,,, I( t; )l J p tJ. le"
q., _Re~ A "'A J,, ! l>~o0 . .. ' «-\Js-17 /CJ-~~~J', .
T ,LI Vo),,f /c,, -h,iuf ~'l'i! 1/o,[ l~O~
~ -, i lh \ I
TA~ t .tilj ~ j ,\: i,. p /)/ ""(J\ f}/111 '\ -· d ,c l -J (L" T,.JJ <,_; I/cl.JI,, -~,.-11,"'/'l,~~ '~)Olli ----./ .
J l~l 'O 1-, · fr ~A .,,. tic.
. '
I
T.kl A ., '+ R,· 11 t IV YLJ.0?
AutosampJer Sampler Location ___ _ Field pH Date Installed ____ Time Installed ____ _ Flow ____ CF/GPD Result ____ _ Please sign and return the white and yellow copies to the Laboratory.
Date Picked Up Time Picked Up ___ _ Flow ___ _ Analyst ____ _ Composite Type: D Flow D Time D Hand Time/Date ___ _
(ONOC Seoaratp\
)
)
NOV 28 '95 15:02 TO 3911147
Qm/Ji
Enylrqnnuntal
Co"!H®R,. Inc
• FROM AquaChem Enuir, Lab
•• •
OEC
Certificate of Analysis
T-715 P.02
'
Oient: OHM ColJ)Ot'allon
240 I Tuckaseegee Road
Charlotte, NC
North Carolina Certification Number: 305
South Carolina Certlflcatioo Number: 99032
Oient#:
Contact:
Sample Date:
SDG#:
381
Jack Kilbarger
24-0ct-95
SDG-000285
Receipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Lab Sample ID:LSID--001095 Kenneth R. Richardson
Sample ID: CO-WS-16
Parameter
Cadmium
Chromium
Lead
Silver
MertUiy
Selenium
Project Mllllager
Reponln2
Result Umit Unit Method Time
1.50 0.25 ppm EPA6010 23:17
8.25 1.25 ppm EPA6010 23:17
G.50 1.25 ppm EPA6010 23:17
u 0.25 ppm EPA6010 23:17
0.010 0,003 ppm EPA 7470 15:35
u 0.125 ppm EPA 7740 10:10
11l7'Downo a...i -P!amllo,l!C 211.U _,(704) 511a.51l7' -FAX, ("/04)51S.2~
Page 1
Date
10/30/9S
10/30/9S
10/30/95
10/30/9S
10/27/9S
10l2i/9S
Analy.a
RCD
RCD
RCD
RCD
DRW
RCD
NQU 28 '95 15:0:l TD ~11147
Qmll1
Environmental
• FRDM AquoChem Envir, Lab T-7:5 P.0:l •
) Consultants. Inc OEC
)
J
Certificate of Analysis
Client#:
Contact:
Sample Dale:
SDG#:
OHM Corporation
240 I Tuckaseegee Road
Charlollc, NC
381
Jack Kilbarger
24-0ct-9S
SDO-000285
Lab Sample ID:LSID-001096
Sample ID: CO-WS-16
Parameter Result
1,1, I-Trichloroethane u
I, 1, I-Trichloroethane u
1, 1,2,2-Tetrachlorocthanc: u
1, 1,2,2-Tetrachloroethane u
1, 1,2-Trichloroethane u
I, 1.2-Trichloroelhane u
1,1-Dichloroethane u
I, 1-Dichloroethane u
1, 1-Dichlorocthcnc u
I, 1-Dichloroethcne u
1,2-Dichlorobenzcnc u
1,2-Dichlorobenzcne u
1,2-Dichlorocthane u
1.2-Dichloroethane u
1,2-Dichlomcthcne u
1,2-Dichloropropane u
1,2-Dichloropropane u
1,3-Dichlorobenzene u
1,3-Dichlorobenzene u
1,4-Dichlorobenzene u
1,4-Dichlorobcnznc . u
Reporting
Limit Unit
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
3] ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
North Carolina Certification Number: 305
South Carolina Certification Number. 119032
Re<.eipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. Richardson
Project Manager
Method Time Date
EPA8240 1112195
EPA8240 11/2195
EPA 8240 11/2195
EPA8240 1112195
EPA 8240 1112/95
EPA 8240 11/2195
EPA 8240 11/2195
EPA8240 1112195
EPA8240 1112195
EPA8240 1112195
EPA8240 1112195
EPA 8240 11/2195
EPA8240 11/2195
EPA 8240 11/2195
EPA8240 11/2/95
EPA8240 11/2/95
EPA 8240 11/2/95
EPA8240 11/2/95
EPA 8240 11/2195
EPA 8240 1112195
EPA8240 1112195
Analyst
1117' Dowm Rood --._ NC 28134 Phcao, (7CM) !118-5016 -FAX: (7CM) aa.2'64
Paac 2
)
NOV 28 '95 15:03 TO 3911147
J1mni
Enl'ironmental
ConsullanU, /nc
• FROM AquaChem Enuir. L•b •
OEC
Certificate of Analysis
T-715 P. 04
Client: OHM Corporatlon
2401 Tucka.secgee Road
Charlotte, NC
North Carolina Certlllcatlon Number. 305
South Carolina Certification Number: 99032
Oien!#: 381
Contact: Jack Kilbarger
Sample Date: 24-0ct-95
SDG#: SDG-000285
Lab Sample ID:LSID--001096
Sample ID: CO-WS-16
Reporting
Parameter Result Limit
2-Butanone 57BJ 62
2-Butanonc 57BJ 62
2-Chlorocthcylvinylcthcr u 120
2-Chloroethylvinylclhcr u 120
2-Hexanonc 140B JI
2-Hcxanonc 1'4P"t;..,.6 31
4-Mcthyl-2-pcntanone u 62
4-Methyle-2-pcmanonc u 62
Acetone 4208 62
Acetone 420B 62
Benzene u 31
Bc:nzcnc u 31
Bromodichloromcthanc u 31
Bromodichloromc:tluwc u 31
Bromoform u 31
Bromofonn u 31
Bromomethane u 31
Bromornethane u 31
Carbon disulfide u 31
Carbon Disulfide u 31
Carbon ICIJ8Chloridc u 31
Unlt
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
Receipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. Richardson
Project Manager
Method Time Date
EPA8240 1112/95
EPA 8240 11/2/95
EPA8240 1112/95
EPA8240 1112195
EPA 8240 1112195
EPA 8240 11/2195
EPA 8240 1112195
EPA8240 1112195
EPA 8240 1112195
EPA8240 1112'95
EPA8240 11/2/95
EPA8240 111219S
EPA8240 11/2/95
EPA 8240 11/2/95
. EPA 8240 1112195 '
EPA 8240 1112'9S
EPA 8240 11/2/95
EPA8240 11/2/95
EPAR240 ll/2/95
EPA 8240 1112195
EPA 8240 11/2/95
1117' n.,,.,. Rood --..m.. NC 211:M Piton,: (71M) ffl.5076 -FAX: (NM) 588-2454
Pap: 3
Analyst
' '
QmnJ.
Environmental
-,,consultanq. Inc I
• FROM AquaChem Enuir. Lab T-7;5 P. 05 •
OEC
Certificate of Analysis
Client: OHM Corporation
240 l Tuclcasccgee Road
Charlotte, NC
Client II: 381
Contact: Jack Kilbarger
Sample Date: 24-0:t-95
SDG#: SDG-000285
Lab Sample ID:LSID-001096
Sample ID: CO-WS-16
Parameter Rc!lllt
Carbon Tetrachloride u
, Chlorobcnz,:nc u I • Chlorobc=nc u
Chlorocthane u
Chlorae\hant u
Chlorofonn u
Chlorofonn u
Chloromethane u
Chloromethane u
cis-1,2, -Dichloroethcnc u
cis-1,3-Dichloropropcne u
cis•l.3·Dichloropropcnc u
Dibromochloromctllanc u
Dibrornochlorometllanc u
Ethyl benzene S.5°4i-
Ethylbcnzne 55
Methylene Chloride 191
Methylene chloride 191
Styrene u
Styrene u
Tctrachloroctllcne u
)
Reporting
Limit Unit
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Receipt Date: 24-0ct-95
Report Date; 28-Nov-95
Approved By:
Kenneth R Richardson
Project Manager
Method Time Date
EPA8240 11/2/95
EPA8240 11/2/95
EPA8240 1112/95
EPA8240 11/2195
EPA 8240 1112195
EPA 8240 111219S
EPA 8240 11/2/9-'
EPA8240 11/2/95
EPA8240 11/2/95
EPA 8240 11/2/95
EPA8240 11/2/95
EPA8240 11/2/95
EPA8240 1112/95
EPA 8240 11/2/95
. EPA8240 11/2/95
EPA 8240 1112195
EPA8240 lll2/95
EPA8240 Jl/2/95
EPA 8240 11/2195
EPA 8240 11/2/95
EPA 8240 11/2/95
Analyst
111~6 Do,,m Ro..l . ---., NC 211~ Ph..,., (71M) !li-5076 -FAX: (71M) Sll&-2454
Paae 4
!lmn1
Enyjrqnmentgl
1 Consultants. Inc
•
FROl1 AquaCnom Enuir. Lab T-715 P. 06 •
OEC
Certificate of Analysis
)
Client:
Client#:
ContaC1:
Sample Datt:
SDG II:
OHM Corporation
2401 Tuckas: cgoe Road
Cltarlotte. NC
381
Jack Kilbarger
24-0ct-95
SDG--000285
Lab Sample ID: LSID-OOI096
Sample ID: CO-WS-16
Parameter Bault
Tetrachlorocthcnc u
Toluene 74
Toluene 74
Total Xylenes 480
Total Xylenes 480
trans-1,2-<lichloroethene u
trans-1,3-Dichloropropcnc u
irans-1,3-Dichloropropene u
Trichloroethene u
Trichloroelbcne u
Trichlorofluoromctlumc u
Trichlorofluoromcthanc u
Vinyl acetate u
Vinyl Acetate u
Vinyl chloride u
Vinyl Chloride u
1,2,4-Trichlorobenzcnc u
1,2-Dichlorobenzene u
1,3-Dichlorobcnzene u
1,4-Dichlorobem.enc u
2,4,5-Trichlorophcnol u
Reporting
Limit Unit
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
62 ppb
62 ppb
31 ppb
31 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
North Carolina Certification l'iumber: 305
South Carolina Certification Number: 99032
Rec,,ipt Date: 24-0ct-95
Report Date: 28-Nov-95
Appro,·ed By:
Kenneth R. Richardson
Project Mana~r
Method Time Dale
EPA8240 ll/V95
EPA 8240 IIIV95
EPA 8240 1112195
EPA 8240 11/2195
EPA 8240 11/2195
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 1112/95
EPA8240 1112/95
EPA 8240 11/2/95
EPA 8240 1112195
EPA 8240 11/2/95
EPA 8240 ll/2195
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 1112195
EPA 8270 llnt9S
EPA8270 lln/95
EPA 8270 lln/95
EPA8270 lln/95
EPA 8270 lln/95
Analy1t
1117' -lloa,I. Plrr,mlle, NC 1813, Pbou: (71)C) S18-S076 -FAX: (78') !lli-:WS.
Pap S
}
Qmni
Enyjronmental
Consu1tana. lac
FROM AquaChem Enuir, Lab • •
OEC
Certificate of Analysis
T-715 P,07
Client: OHM Corporation
240 I Tuckascc:gce Road
Charlotte, NC
North Carolina Certification Number: 305
South Carolioa CertlOcatloo Number: 99032
Client#: 381
Contact: Jack Kilbarger
Sample Date: 24-0ct-95
SDG#: SDG--000285
Lab Sample ID: LSID-001096
Sample ID: CO-WS-16
Parameter Result
2,4,6-Trichlorophcnol u
2,4-Dicblorophenol u
2,4-Diruelhylphcnol u
2,4-Dinitropbenol u
2,4-Dinitrotolucne u
2,6-Dinitrotolucne u
2-Chloronaphthalene u
2-Chlorophenol u
2-Methlyphenol (o-cresol) u
2-Melhylnaphthalene 3900
2-Nitroaniline u
2-!,1trophenol u
3,3-Dichlorobcll:lidine u
3-Nitroanilinc u
4,6-Dinitro-2-mcthylphenol u
4-Bromophcnyl phenyl ether u
4-Chloraniline u
4-Chloro-3-melhylphcnol u
4-Chlorophenyl phenyl ether u
4-Mcthylphenol (p-crosol) u
4-Niuoanilinc u
Reporting
Limit Unit
830 ppb
830 ppb
830 ppb
4200 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
4200 ppb
4200 ppb
1600 ppb
4200 ppb
4200 ppb
830 ppb
1600 ppb
1600 ppb
830 ppb
830 ppb
4200 ppb
Receipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. Rlchanlson
Project Manazer
Method Time Date
EPA 8270 llnt95
EPA 8270 lln/95
EPA 8270 lln/95
EPA 8270 Jlnt95
EPA 8270 Jlnt95
EPA 8270 11n19s
EPA 8270 Jln/95
EPA 8270 llnt95
EPA 8270 lln/95
EPA 8270 lln/95
EPA 8270 I 1/7/95
EPA 8270 Jln/95
EPA 8270 llnt9!1
EPA 8270 lln/95
EPA 8270 lln/95
EPA 8270 lln/95
EPA 8270 lin/95
EPA 8270 lln/95
EPA 8270 lint95
EPA8270 lln/95
EPA 8270 11n19s
II 176 Dowm llood -1'1-NC Zlll:14 Phoac: (704) 588-!!076-FA.'<: (704) 918-2-
Page 6
Analyst
NOU 28 '95 15:00 TO 3911147
Qmni
Environmentgl • FR0'1 AquaChem Envir. Lab T-715 P.08 •
) Consultants, Inc OEC
)
Certificate of Analysis
---·--------------------------------
Client: OHM C-orporatlon
240 l Tuckaseegee Road
Charlotte, NC
Client#: 381
Contact: Jack K ilbarger
Sample Date: 24-0ct-95
SDG#: SDG-000285
Lab Sample ID:LSID-001096
Sample ID: CO-WS-16
Parameter Result
4-Nitrophenol u
Accnaphthcnc u
Accnapbthylcnc u
AnthraceDc u
Benzo(a)anthracenc u
Benzo (a) pyrenc u
Benzo (b) lluoranthcne u
Ben10 (ghi) pcrylenc u
Benzo (k) fluoranthene u
Benzoic: acid u
Bcnzyl alcohol u
Bis (2-chloroethoxy) methane u
Bis (2-chloroethyl) ether u
Bis (2-chloroisoprobyl) ether u
Bis (2-ethylhexyl) phthalatc 4IOOOE
Butyl benzyl phthalale u
Chrysene u
Di-n-bWyl phthalate u
Di-n-octylphthalate u
Diben2o (ah) anthracene u
Dibenzofumn u
Reportin&
Limit Unit
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
4200 ppb
1600 ppb
830 ppb
830 ppb
830 ppb
830 ppb,.
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
North Carolina Certification Number: 305
South Carolina Certlflcatioa Number: 99032
Receipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. Richardson
Project Man•~•
Method Time Date
EPA 8270 I 1/7/95
EPA 8270 ll/i/95
EPA 8270 11/7/95
EPA 8270 lln/95
EPA 8270 1 ln/95
EPA 8270 lln/95
EPA8270 lln/95
EPA 8270 11/7/95
EPA 8270 11/7/95
EPA8270 llnt9S
EPA8270 lln/95
EPA8270 11/7/95
EPA8270 11/7/95
EPA8270 I 1/7/95
EPA 8270 11/7/95
EPA8270 11/7195
EPA8270 11/7195
EPA8270 11/7195
EPA8270 11/7195
EPA8270 11/7195
EPAH270 11/7195
Analyll
11116 Do!nu Road . Plnn'lla. NC 2813-4 I'll..,.: [phone] • FA..'C: (704) 588-1"5<
Paae 7
)
!11llD1
Environmmtql
Comultantr, Inc
• •
OEC
Certificate of Analysis
1-r::, F.1)9
Client: OHM Corporation
2401 Tuckaseegce Road
Charlotte. NC
North CaroHna Certification Number: · 30S
Soutb Carolina Certification Number: 99032
Client#: 381
Contact: Jack Kilbarger
Sample Date: 24-0ct-9,
SDG#: SDG--000285
Lab Sample ID:LSID--001096
Sample ID: CO-WS-16
Parameter Result
Dietbylphthalate u
Dimethylphthalate u
Flwiranthene u
Fluorenc u
Hcxachlorobcru:enc u
Hcxachl=butadicnc u
Hexachlorocyclopcntadicnc u
Hcxachlorccthane u
lndcno (1,2,3~) pyrene u
lsophorone u
N-Nitroso-di-n-propylamine u
N-Nitrosodiphenylaminc u
Naphthalcnc 2400
Nitro~c u
Pcntachlorophcnol u
Pbcnaruhrenc 1700
Phenol u
Pyrenc u
Reponlag
Umlt Unit
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
830 ppb
4200 ppb
830 ppb
830 ppb
830 ppb
Receipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. Richardson
Project Manager
Method 'lime Date
EPA8270 llnt9S
EPA 8270 lln/95
EPA8270 llnt9S
EPA8270 lln/95
EPA 8270 llnt9S
EPA8270 lln/95
EPA 8270 llnt9,
EPA8270 lln/95
EPA 8270 lln/95
EPA 8270 I ln/95
EPA 8270 llnt9S
EPA 8270 lln/95
EPA 8270 lln/95
EPA 8270 11,7/95
EPA 8270 11,7/95
EPA 8270 llnt95
EPA 8270 lln/95
EPA 8270 llnt9S
111?60.-Rood ..... n-11-. NC: 111134 Pb,_, ('70C) Sllll.3076-F.U: ~) S88-I~
Paae 8
Analyst
. ··-' '., .... ._ .... ,., ..... ,.., '' ....... ., I •.J [, ,LIQ
Qmm • • "°~
I ) _~_:_"_=_~_=tql_,oc ______ o __ E __ c __________ ~=i
)
)
CUcnl:
Clienl #:
Conlaci:
Sample Date:
SDGN:
Certificate of Analysis
OHM Corporation
240 l Tuckascegcc Road
Charlotte. NC
381
Jack Kilbarger
24-0c:t-95
SDG--000285
Norlb Carolina Certification Number: 305
Soath Carolina Certification Number: 99032
Receipt Dale: 24-0ct-95
Report Date: 28-Nov-95
Appro,-ed By:
Lab Sample ID:LSID--001097 Kenneth R. Rlcbardaon
Sample ID:
Parameter
Arsenic
Bariwn
Cadmium
Chromium
Lead
Silver
Mercwy
Selenium
CO-WS-17 Project Manager
Reporting
Rcault Limit Un.ii MClbod Time
0.350 0.125 ppm EPA 7060 9:15
25.5 D 2.5 ppm EPA 6010 10:25
1.50 0.25 ppm EPA 6010 23:22
17.3 1.25 ppm EPA 6010 23:22
3.00 1.25 ppm EPA6010 23:22
u 0.25 ppm EPA 6010 23:22
0.016 0.003 ppm EPA 7470 15:50
u 0.125 ppm EPA TI40 10:10
11176-Rood · Plaevlle. NC lll:14 ,._, (704J !III-W!6• FAX: (704) l!A-1454
P•ae 9
Date
10/27/95
10/26/95
10/30/95
10/30/95
10/30/95
10/30/95
10/27/95
10/21195
Analyst
RCD
RCD
RCD
RCD
RCD
RCD
DRW
RCD
Qmni
E11riro11me111at
) Consultant1. Inc
•
OEC
Certificate of Analysis
' .. ,.,, ' .... •
Client: OHM CoipOration
240 I Tuckaseegee Road
Charlotte, NC
North Carolilla Ccruf'icatioo Number: 305
South Carolina Certification Nnmber: 99032
)
Client#: 381
Cuotact: Jack Kilbarger
Sample Date: 24-0ct-95
SDG#: SDG--000285
Lab Sample ID:LSID-001098
Sample ID: CO-WS-17
Parameter Result
I, 1, 1-Trichloroet.hane u
I, 1,1-Trichlorocthanc u
I, 1,2,2-Tctrachloroctbanc u
I, 1,2,2-Tetrachloroelhanc u
I .1.2-Trichloroetbane u
l,1,2-Trichloroetbanc u
I, 1-Dichlorocthanc u
l, 1-Dichloroethane u
1,1-Dicbloroethene u
I, 1-Dichloroethene u
1,2-Dichlorobenzcne u
1,2-Dichlorobcnzcne u
1,2-Dichlorocthane u
1,2-Dichloroetbanc u
I ,2-Dichloroethene u
1,2-Dichloropropane u
1,2-Dichloropropane u
1,3-Dichlorobcnzene u
1,3-Dichlorobcnzene u
1,4-Dichlorobcnzene u
1,4-Dicblorobcnzne u
Reporting
Limit Unit
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
~ipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Ke•netb R. Richardson
Project Manalll'r
Method Time Date
EPA 8240 1112/95
EPA 8240 11/2195
EPA 8240 11/2195
EPA8240 1112/95
EPA 8240 11/2/95
EPA 8240 1112195
EPA 8240 11/2195
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 1112/95
EPA 8240 11/2195
EPA 8240 11/2/95
EPA 8240 11/2/95
. EPA 8240 11/2/95
EPA 8240 I 1/2195
EPA 8240 11/2195
EPA 8240 11/2195
EPA8240 11/2195
EPA 8240 11/2/95
EPA 8240 11/2/95
11176 -Raad-PlacYtle, !<C 28134 P .. ac: (70.) !188-l0:6-FAX: (7M) -.l454
Page 10
Analyst
NOU 28 '95 15:00 TO 3911147
Qmai
EnyiromnentgJ
'"pnsu1tana. Inc
• FROM AquoChom Enuir. lob T-7l5 P. 12
,P~ •
OEC I~.
-------------------------~<;' 0 Certificate of Analysis
Ctient:
Client#:
Contact:
Sample Date:
SDG#:
OHM Col1)0ralion
240 I Tockaseegee Road
Charlotte, NC
381
Jack Kilbarger
24-0ct-95
SDG--000285
Lab Sample ID:LSID-001098
Sample ID: CO-WS-17
Parameter Result
2-Butanonc 37BJ
)2-Butanonc 37BJ
2·Chlorocthcylvinylethcr u
2-Chloroctbylvioylether u
2-Hexanone u
2-Hexanone u
4-Methyl-2-pcntanone u
4-Methylo-2-pentanooe u
Acetone 320B
Acetone 320B
Benzene u
Benzene u
Bromodichloromctbanc u
Bromodichloromethanc u
Bromofonn u
Bromoform u
Bromomethane u
Bromomethane u
Calbon Disulfide u
Caibon disulfide u
Carbon Tetrachloride u
)
Reportlng
Llmlt Unit
63 ppb
63 ppb
130 ppb
130 ppb
63 ppb
63 ppb
63 ppb
31 ppb
63 ppb
. 63 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
North Carolina Cenlflcatlo11 Number. 30S
South Carolina Certilicadon Number: 99032
Recl,ipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. Rkbardson
Project Manager
Method Time Date
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/9S
EPA 8240 11/2195
EPA8240 ll/2195
EPA 8240 1112/95
EPA8240 1112/95
EPA 8240 1112/9S
EPA8240 11/2195
EPA 8240 1112195
EPA8240 1112195
EPA 8240 1112195
EPA8240 11/2/95
EPA8240 1112/95 ·
EPA8240 1112195
EPA 8240 ll/2M
EPA 8240 11/2195
Analyst
1117" Down• Road. Ptnn11k. NC 28134 1'!•11•0: (71M) 581-5016-F.U:: (71M) 5118-J454
Paae ll
NUV a:, ·-:r::, 1~:1::19 TO 3911147
Qm.aJ.
Environmental
) consultanu, Inc
• FROM AquaChem Enuir, Lab T-71:5 P. lJ •
OEC
Certificate of Analysis
)
)
Clieot:
Client#:
Contact:
S11111ple Date:
SDG#:
OHM Corporation
240 I Tuckaseegcc Road
Charlotte, NC
381
Jack Kilbarger
24-0ct-95
SDG--000285
Lab Sample ID:LSID--001098
Sample ID: CO-WS-17
Parameter Result
CarlJon tetrachloride u
Chlorobcnane u
Cblorobenzenc u
Chloroethane u
Chloroethanc u
Chloroform u
Chloroform u
Chloromethane u
Chlorornethano u
cis-1,2,-Dichloroethcnc u
cis-1,3-Dichloropropcnc u
cis-1,3-0ichloropropenc u
Dibromochloromcthanc u
Dibromochloromethane u
Etbyfbenz.enc ISO
Etbylbcnzne 150
Methylene Chloride 16J
Mcthyleno chloride 161
Slyrenc u
Styrene u
Tetrachlorocthcnc 9.91
Reportini
Limit Unit
31 ppb
31 ppb
31 ppb
63 ppb
31 ppb
31 ppb
31 ppb
63 ppb
63 ppb
31 ppb
JI ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
31 ppb
JI ppb
31 ppb
North Camllna Certlficallon Number: 30!1
South Carolina Certification Number: 99032
Receipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. llicbard,on
Project Manager
Method Time Dale
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 1112/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 1112/95
EPA 8240 11/2/95
EPAS240 11/2/95
EPA 8240 11/2/95
EPA 8240 1112/9S
EPA8240 11/2/95
EPA8240 11/2/95
EPA8240 11/2/95
EPA 8240 11/2/95
EPA8240 11/2195
EPA8240 11/2195
EPA8240 1112/95
EPA 8240 11/2/95
EPA8240 11/2/95
EPA8240 11/219S
EPA8240 1112/95
Analyst
1117'-Rood. Plne¥llle, NC 11u, Phou: (71M) B-5076 • PAX, (704) B-2454
Pap 12
NOU 28 '95 15:09 TO 3911147
Qnmi
Enyironmental
l consulta,m. Inc
• FROM AquaChem Enuir. Lab •
OEC
Certificate of Analysis
T-715 P. 14
Client: OHM Corporation
240 I Tuckascegcc Read
Charlotte, NC
North Carolina Certlflcadon N11mber: 305
South Carolina Certlficadon Number: 99032
·i
)
Client#: 381
Contact: Jack Kilbarger
Sample Date: 24-0ct-95
SDG II: SDG--000285
Lab Sample ID:LSID-001098
Sample ID: CO-WS-17
Parameter
Tetracbloroethene
Toluene
Toluene
Total Xylencs
Total Xylenes
trans-1,2-dichloroethene
trans-1,3-Dichloropropenc
trans-1,3-Dichloropropenc
Tricbloroethene
Trichloroelbcn•
Trichlorolluoromcthane
Trichlorolluorometbanc
Vinyl Acetate
Vinyl acetate
Y½IYI chloride
Vinyl Chloride
1,2 ,4-Tricblorobcn,..ene
1,2-Dichlorobenzene
1,3-Dichlorobenzcne
I, 4-Dicblorobenvmc
2, 4 ,5-Trichlorophenol
Reporting
Result Limit
9.91 31
2300E 31
2~/i" 31
1350 31
1350 31
u 31
u 31
u 31
u 63
u 31
u 63
u 31
u 63
u 63
u 63
u 63
u 860
u 860
u 860
u 860
u 860
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
?pb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
Receipt Date: 24-0ct-95
Report Date: 28-~ov-95
Approved By:
Kenneth R. Richardson
Project Manager
Me!hod Time Date
EPA 8240 11/2/95
EPA 8240 l 1/2/95
EPA 824/l I l/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA 8240 11/2/95
EPA8240 1112/95
EPA8240 11/2/95
EPA 8240 1!/2195
EPA 8240 11/2/9-'
EPA R240 1112195
EPA8240 l 1/2/95
. EPA 8240 !l/2/95
EPA8240 1112195
EPA 8270 1116195
EPA8270 11/6/95
EPA8270 l l/6/9S
EPA 8270 !l/6/95
EPA8270 11/6/95
11176 Dcmu Rood. l'tnmllc, NC Z8134 Pbom: ('704) 58S-5076. YAX: ('704) 51111-J.464
Paae 13
Analyst
NUV ~~ '95 15:10 TO 3911147
Qmni
Environmental
',) Consultants. Inc
• FROM AquaCoem E.iv\r. Lab T-715 P, 15
•
OEC
Certificate of Analysis
·1
)
Client:
Client#:
Coo1111:1:
Sample Date:
SDG#:
OHM Corporation
2401 Tuckasccgcc Road
Charlo!1e, NC
381
Jack Kilbarger.
24-0ct-95
SDG-000285
Lab Sample ID:LSID--001098
Sample ID: CO-WS-17
Parameter Result
2,4,6-Trichlorophenol u
2,4-Dichlorophc:nol u
2, 4-0imethylphcnol u
2,4-Dlnitrophenol u
2,4-Dinitrotolucnc u
2.6-Dinitrotolucnc u
2-Chloronaphthalene u
2-Chlorophcnol u
2-Methl}t>henol (o-cresol) u
2-Methylnaphthalene 930
2-Nitroaniline u
2·Nitrophcnol u
3,3-Dichlorobenzidinc u
3-Nitroaniline u
4,6-Dinitro-2-mcthylphcnol u
4-Bromophenyl pbcnyl etllcr u
4-Chloraniline u
4-Chloro-3-methylphcnol u
4-Chlorophenyl phenyl ether u
4-Mcthylphenol (p-aa;ol) u
4-Nitroanilinc u
Reporting
Limit Unh
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
4300 ppb
860 ppb
1700 ppb
4300 ppb
4300 ppb
860 ppb
1700 ppb
1700 ppb
860 ppb
860 ppb
4300 ppb
North Carolina Certification Number: 30S
South Carolina Certltlcadon Nnmber: 99032
Receipt Date: 24-0ct-95
Report Dale: 28-Nav-95
Approved By:
Kenneth IL Richardson
Project Manaeer
Method Time Date
EPA 8270 11/6/95
EPA 8270 111619S
EPA 8270 11/6.'9S
EPA 8270 1116195
EPA 8270 11/6.'9S
EPA 8270 11/6/95
EPA 8270 11/6,195
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6195
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
· EPA 8270 11/6/95
EPA8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA8270 11/6/95
EPA 8270 11/6/95
Analyst
1117' 0-. R .... Plmmllo, !'iC 28134 P_, (')04) Sllh5076 . FAX: (')04) !88-24S4
Page 14
•
QmnJ.
Environmental , · -1 Consultants. Inc
• T-7:5 P. 16
•
OEC
Certificate of Analysis
)
)
Client: OHM Corporation
240 I Tuckaseegee Road
Cbartottc, NC
Oient#: 3~1
Contact: Jack Kilbarger
Sample Date: 24-0ct-95
SDG#: SDG--00028S
Lab Sample ID:LSID--001098
Sample ID: CO-WS-17
Parameter Result
4-Nitrophenol u
Accnaphtheue u
Acenaphthyleue u
Anthraccne u
Bcnzo (a) anthraca,c u
Bcnzo (a) pyrcllC u
Bcnzo (b) tluorantheue u
Bcnzo (ghi) pc1ylenc u
Bcnzo (k) fluorantheue u
Benzoic acid u
Benzyl alcohol u
Bis (2-<:hloroethoxy) methane u
Bi• (2-<:hlomcthyl) ether u
Bis (2-<:hloroisoprobyl) ether u
Bis (2-<:thylhcxyl) phthalalc 16000E
Butyl bcnzyl phthalatc u
Cluysenc u
Di-n-butyl phthalatc u
Di-u-octylphthalate u
Dibcnzo (ah) anthraccne u
Dibenzofurau u
Reporting
Lbnlt Unit
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
4300 ppb
1700 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
North Carolina Certification Number: JOS
South Carolina Certification Number: 99032
Rttelpt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kenneth R. Rlchanhon
Project Manager
Method Time Date
EPA 8270 11/6/95
EPA8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 1 l/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 l l/6/95
EPA8270
EPA8270 11/6/95
EPA 8270 11/6/95
EPA8270 l l/6/95
EPA8270 11/6/95
EPA8270 l l/6/95
EPA8270 11/6/95
EPA8270 11/6/95
EPA8270 11/6/95
EPA 8270 1116195
EPA 8270 11/6/95
EPA 8270 11/6/95
Analyst
IJJ76Jlawnallood-Ptnnllle.:-IC 281:M ""-•(704)AAll-~~-FAX,('704)!'Jl8.l-
Pap 15
flm.ni
Envtronmentql
) Conmltants, Inc
• OEC
Certificate of Analysis
Client: OHM Corporation
2401 Tuckaseegee Road
Charlone, NC
North Carolina Certification Number: 305
South Carolina Certification Number: 99032
Client#: 381
Connet: Jack Kilbarger
Sample Date: 24-0ct-95
SDG#: SDG-000285
ub Sample ID: LSID-00 I 098
Sample ID: CO-WS-17
Parameter Result
Diethylphthalate u
) Dimethylphthalate u
· Fluorantbcne u
Fluorene u
Hcxachlorobenune u
Hexachlorobutadiene u
Hc:xachlorocyclopentadicne u
Hexachloroetllane u
lndeno ( 1,2,3~) pyrene u
Jsophorone u
N-Nitroso-di-n-propylamine u
N-Nitrosodiphenylamine u
Naphthalene 1000
Nitrobenzcne u
Pcn:ach!oropbcnol u
Phcnanihrene u
Phenol u
Pyrcnc u
Report1o11
Limit Unit
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
860 ppb
4300 ppb
860 ppb
860 ppb
860 ppb
Receipt Date: 24-0ct-95
Report Date: 28-Nov-95
Approved By:
Kennetb R. Richardson
Project Manager
Metbod Time Date
EPA 8270 11/6/95
EPA 8270 1116/95
EPA 8270 1116195
EPA 8270 11/6/95
EPA 8270 l 1/6/95
EPA 8270 I 1/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA8270 I 1/6/95
EPA8270 I 1/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 11/6/95
EPA 8270 I J/6/95
EPA 8270 11/6/95
EPA8270 I J/6/95
EPA 8270 I 1/6/95
11176 Dow,u a...t. -.. NC Zlll:W Pho•: ("704) !lfl-5076. FAX: (ilM) !II-~
Pap 16
..
Analyst
LAquaChem
ENVIRONMENTAL LABORATORIES, INC. CHAIN OF CUSTODY j _ • 11178 OOWNS ROAD 704/588-5076 PINEVILLE, NC 2s134 FAX 10415es-2454
Phone Number: <Jo 'j l_3_,_'J,.,.I_-_.._O_,,q,_,'7~7 ________ _
Client: 01:/:M (~~
Fax Number: 17o'-{ l >J/-1\':{7
Address: I ~00 DL: s+
Purchase Order Numb...,.e~r:-'--;'(o~,~D~o-'b_s= ______ _
Ctty (Lt lg ~ c
State: /J' l Zip: J b d Oy, Certification Requireme')t:-""-'-"'-"--'-'-'---------
Contact Person ,J.J:, /,:,')bgt)f.f
Project Name: C/,e~•"te. D!) ,
Sampled By: ,l,\'.,1
1/~,u,fr
RushCh~rges~'!,~rized D Yes \2l'No
By relinquishing !his s.ample(s) ro la!oraiory Personnel, I warrant rhar I am authorized ro enter inlo !his agreement for !he Clienr nam~ abo\1'8 and thal I author~~~~/~ Trfal.J.sis sub;ect to lhe terms and conditions on the reverse hereof.
This agreement is governed by the terms and conditions on the reverse side hereof. Analysis charges shall be as included in !he laborafo,ies fee schedule in effect al lhe lime or the analysis.
Relinquished By:
Date: I\-drl ~'1 Time:
Received By:
Dale:
Time:
Relinquished By:
Date:
Time:
~eivedBy:
Date:
Time: I!!
ii"
& "' },Ji g $ f§Ea//JiJiJiJ1Ji1JJJJ,fff Samples received on ice? Yes □ No □
Dale & Time J " Sample ID Samoled lab ID ,,.a o ~r::r::f!:
Other Analysis Prese-rvatrve
CD-w--~i X I l -i.J-9:; I)
T.-1-~I V I.J!/6( ,..;ALI 2ilyo) 14,:)':i'
17fw
r,o;,, .
q U~T#-1, 1 o~f:,.__.,: :, ~
r.L 1 <.,.,_; ~n 1,,1 I I.,, ( ... A( j '1,f7r \ ,iL:;'o'o .
sa.,,,,,l,-1-{,.1.,,,,, H -, I-
I
'
(
\ it\ Awi, + Bil( l'fl~qoc" l'l
/ •
Autosampler Sampler Location. ___ _
Field pH
Date lns;..,,lled____ Time Installed. ____ _ Flow CF/GPO Result ____ _ Please sign and return the white and yellow copies to the Laboratory_
Date Pic~ed Up Time Picked Up ___ _ Composite Type: O Flow O Time O Hand
----Flow. ___ _ Analyst ____ _
Time/0ate __ -c_ (QNQC Separate)
1 r,UJJ M'-{Ud\.. .. lf:'111 c::iutr. Lat) ---- --·------., ------------
0.!lllll '
Enviro11menta1
Consultants, Inc
Client: OHM Corporation
•
OEC
Certificate of Analysis
North Carolina Certification Nwnber: J05 240 I Tucka&eegee Road South Carolina Certification Number: 99032 Charlotte. NC
Client#: 381 Receipt Date: 22-Nov-95 Contact: Jack Kilbarger
Report Date: 07-Dec-95
Sample Date: 21-Nov·9~ ... -.,,~ SDG#: SDG-000477 ~--Lab Sample ID:LSID-001875 obert Curry Sample ID: CO-WS-28 ( '-'-s-c-~% er-co=""'-''-""' j Project Manager
Parameter
1,U•Trichloroewme
I, 1,2,2 • T etrachloroethar.e
I, 1,2-Trichloroethrule
I, 1-Dichloroethanc
1,1-Dichloroethcnc
l,2•Dichlorobenzcnc
1,2-Dichlorocthane
1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichlorobcnzene
1,4-Dichlorcbenzcne
2-Butanono
2-Hexanone
4-Mcthyl-1-pentanone
Acetone
3enzene
a romodichloromethanc
Brcmofcrm
Brome methane
Carbon Disulfide
Caioon T etraehlcride
Reportina
Result Limit Unit Method Time
u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34 u s ppb EPA 8240 18:34
u 5 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34
u 5 ppb EPA 8240 18 34 u s ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34
u s ppb EPA 8240 18:34 u 10 ppb EPA 8240 18:34 u 10 ppb EPA 8240 18:34
u 10 ppb EPA 8240 18:34 u 5 ppb EPA 8240 18:34
95 s ppb EPA 8240 18:34
u s ppb EPA 8240 18:34
u 5 ppb EPA 8240 18:34
u 10 ppb EPA 8240 18:34 u s ppb EPA 8240 18:34
u s ppb EPA 8240 18:34
l1176 0.-. R•d-Plnmllo. SC 28134 Phon.: ("IIM) -6-FAX: (71M) 58a-%454
Page I
Date
12/4/95
12!4/95
!2!4195
12/~95
12/4/95
12/4/95
12/4/95
12!4!9S
12/4/95
12/4/95
12/4!95
12/4/95
12/4/95
12/4/95
12/4/95
l2i4/95
12/4/95
12/4/95
12/4/95
12/4/95
12/4/95
Analyn
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
, .Qnmi'
Environmental
Consultants. Inc
• •
OEC
Certificate of Analysis
Client:
Client#:
Contact:
OHM Corporation
240 I Tuckasecgcc ii.cad
Charlotte, NC
381
Jack Kilbarger
Sample Date: 21-Nov-95
SDG-OJ0477
Lab Sample ID: LSID-001875
Sample ID: CO•WS-28
Parllllleter Result
Chlorcbenzene
Chlorcethane
Chloroform
Chlorcmethanc
cis-1,J-Dichlorcpropene
Oibrcmochloromethane
Ethylbcnzene
¼thylenc Chloride
Styrene
Tetrachlorocthcne
Toluene
Total Xylenos
o:ans-1,3-Dichloroprcpene
Trichloroetbene
Vinyl Acetate
Vinyl Chloride
1,2, 4-Trichlorobenzene
2,4,S-Trichlorophcnol
2, 4,6-Trichlorophcnol
2,4-Dichlorophenol
2.4-Dimethylphenol
u
u
u
u
u
u
170
u
u
175
45
500
u
u
u
u
u
u
u
u
u
Reportinz
Limit
5
10
5
10
5
5
5
5
5
5
5
5
5
' 10
s
20
20
20
20
20
Unit
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
ppb
North Carolina Certification Number: J~
South Carolina Certification Number: 99032
Receipt Date: 22-Nov-95
Report Date: 07-De<:-95
Approved By:
crfL.Cu~7
Method
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8240
EPA 8270
EPA 8270
EPA 8270
EPA 8270
EPA 8270
Project Manager
Time
18;34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
18:34
10:00
10:00
10:00
10:00
10:00
Daie
12/4195
12/4195
12/4195
12/4195
12/4195
12/4195
12/4195
12/4/95
12/4/95
12/4195
12/4/95
12/4/95
12/4/95
12/4/95
12/4195
12/4/95
12/1195
12/1/95
12/1195
12/L195
12/1/95
Analyst
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
11116 Do,nu Rood -PlnmJU. ~C 28134 Pbono, [phone] -FAX, (704) <""-24"4
Page 2
!JJmli.·
Environmental
Consullants. ln c
Client: OHM Corporation
1 '~".'"''' n'1'-<>'-'•1<.III '-''"'' • L..<IIU
• •
OEC
Certificate of Analysis
North Carolina Certification Number: 305 240 I Tuckaseegce Road South Carolina Certification NllDlbcr: 99032 Charloite, NC
Client#: 3RI &ceipt Date: 22-Nov-95
Contact: Jack Kilbargcr
Report Date: 07-Dec-95
Sample Date: 2!-Nov-95
SDG#: SDG--000477 Approved By:
Lab Sample ID:LSID--001875
Sample ID: CO-WS-28
Reporting
Parameter &!Ult Limit Unit Method Time
2, 4-Dinitrophenol u 20 ppb EPA 8270 10:00
2,4-Dinitrotolucne u 20 ppb EPA 8270 10:00
2,6-Dinitrotolucnc u 20 ppb EPA 8270 10:00
2-Chloronaphlhalcnc u 20 ppb =PA 8270 10:00
2-Chlorophenol u 20 ppb · EPA 8270 10:00
2-Mcthlyphenol (<Kresal) u 20 ppb EPA 8270 10:00
2•Mcthylnaphthalcne u 20 ppb EPA 8270 10:00
2-Nitroaniline u 20 ppb EPA 8270 10:00
2-Nitrophcnol u 20 ppb EPA 8270 10:00
3,3-Dichlorobell2idinc u 20 ppb EPA 8270 10:00
3-Nitroanilinc u 20 ppb EPA 8270 10:00
4,6-Dinitro-2-methylphcnol u 20 ppb EPA 8270 10:00
4-Bromophcnyl phenyl ether u 20 ppb EPA 8270 10:00
4-Chloranilinc u 20 ppb EPA 8270 10:00
4-Chloro-3-methylphcnol u 20 ppb EPA 8270 10:00
4-Chlorophcnylphenyl:thcr u 10 ppb EPA 8270 10:00
4-Mcthylphcnol (p-crcsol) u 20 ppb EPA 8270 10:00
4.Nitroaniline u 20 ppb EPA 8270 10:00
4-Nit.rophonol u 50 ppb EPA 8270 10:00
Acenapbthcne u 20 ppb EPA 8270 10:00
Acenapbthylenc u 20 ppb EPA 8270 l0:00
1117' l>owna Road -Pto..we. NC 281.14 PIM>no, ("IIM) 5111-~7• -FAX, ('IW) sn.2=
Page 3
Date Analyn
1211/9.l DRW
1211/95 DRW
12/1/95 DRW
1211/95 DRW
1211/95 DRW
12/1/95 DRW
12/1/95 DRW
1211195 DRW
1211195 DRW
1211195 DRW
1211/95 DRW
1211/95 DRW
1211/95 DRW
1211/95 DRW
12/1/95 DRW
12/1/95 DRW
12/1/95 DRW
12/1/95 DRW
12/1/95 DRW
12/1/95 DRW
12/1/95 DRW
•
Qmai '
Environmental,
Consultants, Inc
Client: OHM Corporation
• •
OEC
Certificate of Analysis
North Carolina Certification Number: 305 240 I Tucka.seegee Road South Carolina Certification Number: 99032 Charlotte, NC
Client#: 381 Receipt Date: 22-Nov-95
Contact: Jack Kilbargc:
Report Date: 07-Dcc-95
Sample Date: 21-Nov-95 tfilf:F?'-SDG#: SDG--000477 Approved By:
Lab Sample ID: LSID-001875
Sample ID: CO-WS-28 Project Manager
Reporting
Parameter Result Limit Unit Method Time
Anthracene u 20 ppb EPA 8270 10:00 Benzi.dine u 50 ppb EPA 8270 10:00
Be=(a}anthraceno u 20 ppb EPA 8270 10:00
Benzo (a} pyrene u 20 ppb EPA 8270 10:00
Benzo (b) fluoranthenc u 20 ppb EPA 8270 10:00
Bcnzo (ghi) perylene u 20 ppb EPA 8270 10:00
Bonzo (k) fluoranthenc u 20 ppb EPA 8270 10:00
Benzoic acid u 20 ppb EPA 8270 10:00
Benzyl alcohol u 20 ppb EPA 8270 10:00
Bis (2-cttloroetho,cy) methane u 20 ppb EPA 8270 J0:00
Bis (2-dlloroethyl) ether u 20 ppb EPA 8270 10:00
Bis (2-cttloroisoprobyl} ether u 20 ppb EPA8270 10:00
Bis (2-,,thylhexyl} phthalate 3592 20 ppb EPA 8270 10:00
Butyl benzyl phthalate 3355 20 ppb EPA 8270 10:00
Chryscne u 20 ppb EPA 8270 10:00
Di-a-butyl phtllalalC u 20 ppb EPA 8270 10:00
Di-n-occylphthalatc u 20 ppb EPA 8270 10:00
Dtbenzo (ah) anthracene u 20 ppb EPA 8270 10:00
Dibenzofuran u 20 ppb EPA 8270 10:00
Dicthylphthalate u 20 ppb EPA 8270 ]0:00
Dimethylphlhalate u 20 ppb EPA 8270 10:00
11176 llowm Row -Plnffllle. NC lll:M Phont: (70.) _, -FAX: [phone]
Page 4
Date
12/1/95
12/1/95
12/1/95
12/1/95
12/1/95
12/1/95
12/1/95
12/1/95
12/1/95
12/1/9S
12/1/95
12/1/95
12/1/95
12!1/95
1211/95
12/1/95
12/1/95
12/1/95
12/1/95
12/1/95
12/1/95
Analytt
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRW
DRIV
DRW
DRW
DRW
DRW
DRW
DRW
DRW
..,..._._ ,.... .. ... ,...., . ...,... ,..., ....... ,.,. ... ,
·Qmfil.
Environmental
Consultants. Inc
• •
OEC
Certificate of Analysis
Olent: OHM Corporation North Carolina Certification Number: 305 240 l Tuckasecgcc Road South Carolina Certification Number: 99032
Charlene, NC
Client#: 381 Receipt Date: 22-Nov-95
Contact; Jaclc Kilbarger Repon Date: 07-Dec-95
Sample Date: 21-Nov-95 ~--SDG#: SDG--0004 77 Approved By:
Lab Sample ID:LSID--001875 bert k'curry 0
Sample ID: CO-WS-28 Project Manager
Reportinf
Par:lmeter Result Limit Unit Method Time Date Analyst
Fluoranthene u 20 ppb EPA 8270 10:00 12/1/95 DRW
Fluorenc u 20 ppb EPA 8270 10:00 12/1/95 DRW HcxachlorobeI12enc u 20 ppb EPA 8270 10:00 12/1/95 DRW
Hcxachlorobutadienc u 20 ppb EPA 8270 10:00 12/1/95 DRW
Hexachlorocyclopeniadicnc u 20 ppb EPA 8270 10:00 12/1195 DRW
Hcxachloroethanc u 20 ppb EPA 8270 10:00 12/li9S DRW
lndeno (1,2,3-cd) pyrenc u 20 ppb EPA 8270 10:00 12/1195 DRW
Isophoronc u 20 ppb EPA 8270 10:00 12/1/95 DRW
N-Nitroso-di-n-propylamine u 20 ppb EPA 8270 10:00 1211/95 DRW
N-Nitrosodiphcnylaminc u 20 ppb EPA 8270 10:00 1211195 DRW
Naphlhalcne u 20 ppb EPA 8270 10:00 12il/95 DRW
NitrobeI12cne u 20 ppb EPA 8270 10:00 12il/9S DRW
Pcntachloropbcnol u 20 ppb EPA 8270 10:00 12/1/95 DRW
Phcnantlmru: u 20 ppb EPA 8270 10.00 12/1/95 DRW
Phenol u 20 ppb EPA 8270 10:00 12/1195 DRW
Pyrene u 20 ppb EPA 8270 10:00 1211/95 DRW
11176 Dowm Rod. Pln<Yilk. ~c zatJ.4 l'llone: (71M) 588-5(176. FAX: [phone]
P1ge 5
• • U.S. ARMY CORPS OF ENGINEERS
Wilmington District
Action ID: / 99 b O C, 3 b ~ County: /'A ECK 1-£.A) E,i.:, K6--
Notification of Jurisdictional Determination
Property owner/Authorized Agent ,Jc., D rvr.sto,J ol=
Address Su pJ!.gJ=.vtJD 51.!..c.'rt.o,,,J . A n--;J :
l
J.{o I o 13£./'...l.."r/lJ P..oA.JJ
Telephone Number 919 -7.33 -~O / X 31 r:{'
I
Size and Location of Property(waterbody, Highway name/number, town, etc.)
A 0."'/ -Ml::.L.£. Lo,J(,., .Sl!..6-M£Ni Oc AN UNNAMl!D H?.'r/3urA/'..y' '[b ,
5 'rcvJ Af.. rs c.~ux B E!...'11.JE.E.v e, !!. j1.$ Y If -r.u l?oAD /\ AJD TH I!. Co.Al 1=ll.)£.Nc.E.
wrnt .S';1:.WAl-r,S cl;uJ( .SovrH AAlrl PAe.ALJ..El.. I[) Ff_EE.DoNI J?.IY,,.D A., Indicate Whicli of the following apply: C.-HA f!..Lo r, I!,..
• There arc wetlands on the above described property which we strongly suggest should be delineated and
surveyed. The surveyed wetland lines must be verified by our staff before the Corps will make a final
jurisdictional determination on your property.
• Because of the size of your property and our present workload, our identification and delineation of your
wetlands cannot be accomplished in a timely manner. You may wish to employ a consultant to obtain a
more timely delineation of the wetlands. Once your consultant has flagged a wetland line on the property,
Corps staff will review it, and, if it is accurate, we strongly recommend that you have the line surveyed for
final approval by the Corps. The Corps will not make a final jurisdictional determination on your property
without an approved survey.
• The wetlands on your lot have been delineated, and the limits of Corps jurisdiction have been explained
to you. Unless there is a change in the law or our published regulations, this determination may be relied
upon for a period not to exceed three years from the date of this notification.
CT)rhere are no wetlands present on the above described property which are subject lo the permit
, requirements of Section 404 of the Clean Water Act (33 USC 1344). Unless there is a change in the law
"-·.. or our published regulations, this determination may be relied upon for a period not to exceed three years
·. from the date of this notification. "Tl+E c.i-JA,v.\lE.l. r .S A /?,.E.Wi..A nED WA~P-. o-,:. Tflt U.S ,
• The project is located in one of the 20 Coastal Counties. You should contact the nearest State Office of
Coastal Management to determine their requirements.
Placement of dredged or fill material in wetlands on this property without a Department of the Army
permit is in most cases a violation of Section 301 of the Clean Water Act (33 USC 1311). A permit is
not required for work on the property restricted entirely to existing high ground. If you have any
questions regarding the Corps of Engineers regulatory program, please contact
S'rE.v'L!,,IJ Lu>J.D at 7o'/-:i.. 7 /-~!rS-7
Property owner/ Authorized Agent Signature _::=::===::,...._:=====---======--====-
Project Manager Signature __.,/2c....,cfu....__..,,..,.,., • ..__"'IA.,.l,,__.J.~"""'=¥------------------
Date 11 / o 7 / 95"' Expiration Date // / C '/ 9~ I ' ~-'+.~~,,-,.~-------
SURVEY PLAT OR FIELD SKETCH OF DESCRIBED PROPERTY AND THE WETLAND
DELINEATION FORM MUST BE ATTACHED TO THE YELLOW (FILE) COPY OF THIS FORM.
CESA W Form 51>6
I OCT92
U5 AR~.Y CORPSIENGRS
To:
·=1-704-252-1721
The United States Army
Corps of Engineers
Asheville Regulatory Field Office
g 1 !>anon Avenue, llooin 143, Asheville, NC 28801-5006
(704) ?.71-4854 • (lax) [phone]
FaxNtunber: q1q-7 .. 33 -'/ff!/
From: L\JJJD
Telephone:
Number of Pages (including this pag<!): .
Remarks:
14:02 No.DOS P.01
US ~8~Y CORPSIENGRS TD:1-704-252-1721 • NOV i '95 14:02 No .005 P.02
U.S. ARMY CORPS OF ENGINEERS
Wilmington District
Action JD: I ?96 Oc, 36 'c('" C.ounty: /v\ECKl.J!.IJBuK6-,-
Notification of Jurisdictional Determination
l'ropcrtyowncr/AullmrizcdAg<:nt NC--o.t=Vr.$u,.,J ol= Sot.-Z:L) WA:S>:J!:. MAA!A6-i;,1,HrA.J1
Address s UPl!./?l=-vAJD ~l[.c.rco.J ; A rr,J : Do oJH,A..S ;'J..co /?..E .
J../o/ ol';t;:,<.L):A} /!o4.D f.;t'\t.Jr£<rlf ,Jc_, ;2.7£,c,S-1
Tukphonc Number 9 / 9 -7 ~"' '3 -~ t, I )( :31 2$"
Size and Localion of l'roperty(waterhody. Highway namc/numher. town, c,tc.)
A 6,"t -Ml:L£ L,•,,.JIY .Sr!.6:Mf.JJC oF A,J uA1AIAMED )1?rBur-A/t\l__ n, r ~~--
:lrEVIA{tr5 e.gux t'J.fb.n,J,E E.•,l t,'f. i--it-Y /-f'C.Ll-f::oAp AA.ID TH£. C¢A.l~LOE.NCL
t•n:ni 6'rt:'4./At.'J"S cR.,rL.J{ .$c,vrf-i AAl'6 PAP-A~ei-nl P/?.lf E.Dor.l\ /ts:;,o, D I'\ 'r Indicate Which of the following ap(l"ly: c.. I-IA £..1-c i-r J!_
• ThcH: arc wcllamls un lhc above described property which we slrongly suggest <hould be delineated and
surveyed. The surveyed wclland lines must he verified by our staff before the Corps will make a final
jurisdiclional tlelermination on your properly.
• BL:causc of lhl: si,c of your properly and our present workload, our idenlificalion and delineation of your
wetlands cannot he ac<.:omplished in a timely manner. You may wish to employ a consultant to obtain a
more timely delineation of the wetlands. Once your consultant has flagged a w,:1laml line on the propcny,
Cnrp< <laff will re.view it, ~nd, if ii is accur:,lc, we strongly recommend that you have the line survi;sycd for
[in al approval by the Corps. The Corps will no1 make a final juri.,dictional dcterminalion on your property
without an approved survey.
• The wcllands on your Joi have heen delineated, and the limils of c~,rps jurisdiction have been explained
to you. Unless there is a change in the law or our published regulations, lhis dctcrminalion may he relied
__ upon 1hr a period nm m exceed three years from the date Df this normcation.
0:·hcre arc no wetlands present on the above described properly which flre subject IO lhc permit
._ requirements ofSecticm 404 of the Clcnn Water Act (33 USC 1344). Unlc:.ss thc1\: i~ • change in the law
or our published regulations, this determination may he relied upon for n period nol to cxcc<:t.l three ye.ir~
Crom the date of this notifiealion. ,lie CAAI\JA.l!-L-r.s A P-..E./;,ol.ATED WA~:?. o>! Jflt U.5,
• The projccl is localed in one of the 20 Oiaslal O,untics. You should con1ac1 lhc nearest State Office of
O,astnl Management to delermine their requirem(:nts.
Placement of dredged or fill material in wetlands on this properly without a Department of the /\rmy
permit is in most cases a violation of Section 301 of the Clean W:1ter Act (33 USC 1J 11 ). A permit is
not required for work on the property reMric!etl entirely to existing high ground. If you have any
que,tions regardlng the Corps of Engineers regulatory program, please cnntacl
snve--Al L-u,JD ~1 7o4-;;., 1_1-_J.(~ll'.-~~7 ____ _
Properly nwncr/Aulhorizcd AgL:nl Sigm1tuu: -=-=====:,._....======--======::__-===:=..
Project Manager Signalurc /2.J-;';., A IAL .i»:.J _______ _
Date 11/07/ 9,S-Expirati<,nD~to ll/0·7/ff;' r ' _ __,., -~.-~-~-----
SURVEY PLAT OR FIELD SKETCH OF DESCRIBED PROPERTY AND THIC WETLAND
DELINEATION FORM MUST DE ATTACHED TO THE YELLOW (FILE) COPY OF THIS FORM,
CK'il\ W l'n:"r'II !it.6
1 ocrrn.
• •
August 1, 1995
Attn: Mr. Steve Lund
Army Corps of Engineers
Regulatory Branch
Re: Wetland Identification -Charlotte, NC
Cherokee Oil Company Site
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
Dear Mr. Lund:
Per our phone conversation today, enclosed is a copy of the NWI map for
northwest Charlotte near the site. The potential wetland to be identified is circled on the
map, just south of Freedom Road (Highway 27). It appears to border an unnamed
tributary of Stewarts Creek, south of and parallel to Freedom Road. The segment of
concern begins at the Berryhill Road bridge flows southeast for approx. 0.4 miles to the
confluence with Stewarts Creek. The NWI map identifies it as palustrins scrub-shrub.
I would like to request a letter discussing the results of your survey when it is
completed. My address is: Attn: Douglas Moore
Division of Solid Waste Management
NC Superfund Section
401 Oberlin Road
Raleigh, NC 27605
If I can be of further assistance, please contact me at [phone], ext. 318.
Sincerely,
¥~
Douglas Moore
Environmental Chemist
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•
Memo
Date: August I, 1995
To: File
From: Douglas Moore
Environmental Chemist
NC Superfund Section
Topic: Tax Office Information
Cherokee Oil Company
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
•
On this day, I spoke with Mrs. Deborah Potts, Office Assistant ID -Mecklenburg County
Real Estate Office [phone]. Mrs. Potts provided the following information over
the phone. They have no listing for 1201 Berryhill Road. However, there is a warehouse
located on 0.71 acres at 1225 Berryhill Road. The owner is listed as Gene W. Hartsell,
1208 Berryhill Road, Charlotte, NC. 28208. The taxes are sent to "Spurrier Oil", 1225
Berryhill Road, Charlotte, NC. On May 25, 1988, the property was transferred to Mr.
Hartsell (Deed Book 5828, Page 131 ). Prior to 1988, a company listed as "Centennial,
Inc." was registered as the site owner. The I 986 and 1987 taxes owed by Centennial, Inc.
have not been paid.
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• •
4
RIIFS upcoming at Five . n Iron
A state cleanup contractor is in the middle of a
$ 1.5 million removal effort at the Fivenson Iron and
Metal site in Alpena, Mich. An RI/FS will be
launched next spring.
The Michigan Dept. of Natural Resources
(MDNR) plans to conduct a state-funded RI/FS and
will decide this winter whether to bid the study or
have one of the state's three in-place, investigative
contractors do the work. One of the three contrac-
tors will develop an RI/FS work plan and, if the
work is bid. prepare specifications. The state hasn't
decided which of its three contractors will prepare
the work plan.
Studies will be needed across the 7-acre former
scrap metal yard between residential and commer-
cial sections of Alpena. Also, the extent to which
adjacent wetlands are contaminated will be studied.
There has been some off-site migration of contami-
nation into the wetlands.
Meanwhile, Northern A-1 Services of Kalkaska,
Mich., is removing 70 drums of waste, 27 trans-
formers and capacitors, compressed gas cylinders,
metal and wood scrap. and is scraping 2.5 feet of
soil from 40% of the site. The soil has PCBs, heavy
metals, low levels of dioxins, oil and other contami-
nants. Some wastes are being shipped off-site for
incineration. others to recyclers.
Site work started Sept. 12 under a state-bid
contract awarded Aug. 3. The state hopes to have
the removal completed by Dec. 15.
The property was seized for non-payment of
taxes and is now state-owned. The land is one of the
state's highest ranked abandoned sites, but isn't on
EPA's NPL.
Contact: John Vick, state project manager,
MDNR Gaylord District Office. 517-732-3541, ext.
5305.
Cherokee Oil removal launched
EPA began an emergency cleanup Nov. 8 at the
Cherokee Oil-Mecklenburg Road site in Charlotte,
N.C .. to secure and sample drums, tanks and other
bulk containers recently found there.
The containers of toxics will eventually be
treated on-site and/or disposed off-site. EPA found
numerous drums in various stages of deterioration,
above-ground tanks and tanker trailers.
Ethylbenzene, 1, 1, 1 trichloroethane, styrene,
chlorobenzene and corrosive liquids have been
found in initial samples. Leaks will be plugged and
non-compatible liquids separated. Drums will be
overpacked.
Sampling and the securing of containers will
take about four months and may cost more than $1.8
million.
Cherokee Oil Co. processed and shipped waste
oil and other substances to other facilities from the
site at 1201 Berryhill Road in Mecklenburg County.
Contac_t: Steve Spurlin, EPA on-scene coordina-
tor, 404-347-3931, ext. 6135.
Superfund Week -November 11, 1994
' Allied-Signal and Dom-ia.-e PRPs because their predecessors
were among companies that r-d tar from iron plants to make tar
paper and shingles.
Interlake, a maker of aerospace components, packaging systems
and other engineered materials, had Retec Inc. of St. Paul, Minn., do
remedial studies. Allied Signal and Dom-Tar had ENSR of Acton,
Mass., do other RI work. Interlake submitted a study of its areas of OU-
3 and the other PRPs submitted their own studies of areas of the St.
Louis River site where their predecessors had businesses.
The groundwater will be monitored but probably won't be
remediated because nobody uses it.
Sediment samples to be drilled through ice
In OU-4, river sediment of the St. Louis River, especially
embayments near the peninsulas, will be subject of remedial studies.
Interlake is looking for third-party PRPs, but so far is preparing to do
the sediment study alone.
The Stryker embayment appears to have the bulk of the sediment
contamination (70,000 to 140,000 cubic yards), but other areas of
contamination include the Keane Creek embayment (no estimate
available), where a creek enters the river, a boat slip between the
peninsula loading docks (20,000 to 40,000 cubic yards), and an area
around an outfall (15,000 to 30,000 cubic yards).
Interlake intends to submit an RI work plan soon so that its
contractor can begin taking sediment samples in February when the
river is frozen. Samplers will be able to take samples from fixed
locations more easily by boring through ice than by floating around in a
boat.
Malcolm Pirnie Inc. did a site-wide RI for the state, so that the
state could issue enforcement actions. But more in-depth studies are
needed before PRPs can come up with feasibility studies.
Contact: Deborah Seibers, EPA project manager, 312-353-9299;
Ann Bidwell, state project manager for lnterlake site, 612-296-7827;
Frank Wallner, state project manager, U.S. Steel, 612-296-7443; Dan
Talsma, lnterlake' s director of environmental control, Lisle, lll., 708-
852-8800; Mark Kami/ow, Allied Signal's environmental manager,
201-455-2119; Marcel Sylvestre, environmental manager, Dom-Tar of
Montreal, 514-457-8269.
Minnesota wants USX to fix Duluth steel site
The Minnesota Pollution Control Agency is trying to get USX
Corp. of Pittsburgh to address contaminated sediment, a large glob of
coal tar and other problems at its former steel plant on the St. Louis
River near Lake Superior.
The 300-acre U.S. Steel plant site in Morgan Park, a south suburb of
Duluth, Minn., is pan of the St. Louis River NPL site (see story, p. 3).
For reasons unknown to the present state and federal project managers.
EPA named the former steel plant location as part of the same NPL site
as that of former pig iron and tar plant locations on the St. Louis River
about four nautical miles downstream. There isn't any other connection
between the Interlake site detailed in the previous story and this U.S.
Steel Duluth Works plant site.
The U.S. Steel site has 18 state-defined operable units (OUs,
classified by letters A-R) but only a few could become major cleanup
efforts. EPA hasn't divided this site into OUs, but the state is taking the
cleanup enforcementlead.
OU-J consists of a glob of perhaps I 0,000 cubic yards of coal tar
buried in the bed of an unnamed creek, and is releasing contaminants
Pasha Publications, 1616 N. Fort Myer Drive, Suite 1000, Arlington, Va. 22209
State of NorthArolina Department o~vironment, Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes, Secretary
William L. Meyer, Director
November 2, 1994
Memo
To: Mike Kelly
Deputy Director
Division of Solid Waste Management
Thru: PatDeRosa ~/~
Head, CERCLKB~ '
From: Douglas Moore J:k.,f-,, /5.,,lJ.) ____,
Environmental Chemist
NC Superfund Section
Subj.: Cherokee Oil Company Site
1201 Berryhill Road
Charlotte, Mecklenburg Co., NC
US EPA ID: NCD 980 799 019
DEHNR
On this day, I received a phone call from EPA Emergency Response and Removal Branch (ERRB), On-Scene Coordinator Steve Spurlin [phone] x 6135. Mr. Spurlin stated that beginning on Thursday, November 3, 1994, ERRB plans to conduct an emergency removal at the subject site. The site currently contains over 1000 drums, 6 above ground tanks which are full, 1 rolloff container, several diked areas containing free liquid and possible underground storage tanks. He stated there is little room to stage the drums on the site and ERRB negotiated an access agreement with the landowner across the street to stage drums on a fenced lot. He stated that EPA has worked out an agreement with the Department of Transportation to close off an adjacent side street, "Drum Avenue", to through traffic for the duration of the removal action. He estimates that the first phase of the removal action (hazardous catergorization of onsite wastes) should take between 1-1.5 months. He stated that there appears to be free standing oil on the site and that there has been documented releases from the site to offsite adjacent properties. Mr. Spurlin is currently on call, but plans to visit the site next week. The site phone numbers are: [phone] and [phone].
I gave Mr. Spurlin the phone numbers for John Gibson, Solid and Hazardous Waste Section at Mecklenburg County Environmental Protection Department and Jesse Wells,
P.O.-Box 27687. Raleigh, North Carolina 27611-7687 Telephone [phone] FAX [phone] An Equal Opportunity Affirmative Action Employer sat recycled/ l 0% post-consumer paper
• •
Hazardous Waste Section at the Mooresville Regional Office. He stated that he would notify these people on EPA's future removal action at the subject site.
cc: Jack Butler
Bruce Nicholson
Doug Holyfield
File
State of Nort&arolina
Department~Environment,
Health and Natural Resources
Division of Solid Waste Management
James B. Hunt, Jr., Governor
Jonathan B. Howes. Secretary
William L. Meyer. Director
January 4, 199_Y
Mr. Doug Lair, Chief
Emergency Response and Removal Branch
Waste Management Division
.--=;;RE:;-;;C~IEUITTVE~D'\
1 J~N O 51994 \
us EPA Region IV
345 Courtland Street, N.E.
Atlanta, Georgia 30365
RE: Cherokee Resources, Inc./Cherokee Oil Company
1201 Berryhill Road, Charlotte, NC
Dear Mr. Lair: IJGD 1'30 7qq o /1
suPERfUND SECTION ·.
The North Carolina Hazardous Waste Section, Solid Waste Management
Division, requests that the Region IV Emergency Response and Removal
Branch inspect the Cherokee Resources facility (Berryhill Road site)
in Charlotte for a possible removal action. This site is owned by
the same company that operated the Cherokee Oil site at 725 South
Summit Avenue and is the site where waste processing occurred.
Based on observations by our staff and comments by other state and
federal offices, it appears that Cherokee has ceased operations at
the Berryhill Road site. This agency sent an NOV (copy enclosed) to
Cherokee on October 18, 1993, which (among other things) contained a
request for an inventory of the contents of all tanks and containers
on the site. About this same time we received notice that Defense
Reutilization and Marketing Service had improperly shipped hazardous
material/waste to Cherokee (attached memo).
Cherokee's reply was that they have not ceased operation (attached).
However, we were recently informed by the FBI that Cherokee is not
processing and their sewer connection has been cut off.
Thank you for any assistance you can give us.
Sincerely,
./-'-'· •·"'·'• ;{', J.. . .f?I.~,-. _::,~--
/
Jerome H. Rhodes, Chief
Hazardous Waste Section
JHR/ppb
Attachments
P.O. Box 27687. Raleigh. North Carolina 27611-7687 Telephone 919-73.'-~996 JAX 919-715-3605
An Equ~I Opportunify Affirmative Acti6n Employer 50% recycled/ rm'., Post-consumer paper