NCD122263825_20010201_JFD Electronics - Channel Master_FRBCERCLA RA_Semiannual Groundwater Remediation Report April - October 2000-OCR

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Semiannual
Groundwater Remediation Report:
April -October 2000
JFD Electronics/Channel Master Site
Oxford, North Carolina
~
ARCADIS GERAGHTY&MILLER
February 2001
. PREPARED FOR
JFD Electronics Corporation and
CMSS, Inc
620 West Industry Drive
Oxford, North Carolina 27565
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Semiannual Groundwater
Remediation Report
JFD Electronics/Channel
Master Site
Oxford, North Carolina
Prepared for:
JFD Electronics CorPoration and
. CMSS, Inc.
620 West Industry Drive·
Oxford, North Carolina 27565
Prepared by:
ARCADIS Geraghty & Miller of North
Carolina, Inc
2301 Rexwoods Drive
Suite 102
Raleigh
North Carolina 27607
Tel 919 78i-551 i
Fax [phone]
Our Ref.:
NC000202.0170
Date:
.February 2001
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AR CAD IS GERAGHTY & MILLER
· SEMIANNUAL GROUNDWATER REMEDIATION REPORT
JFD ELECTRONICS/CHANNEL MASTER SITE
· OXFORD, NORTH CAROLINA
February 2001
Prepared by AR CAD IS Geraghty & Miller of North Carolina, Inc.
E: Nexa£idra Hartman, E.I.
Staff Engineer
Nanjun V. Shetty, P.E.
· Principal Engineer/Project Manager
\d1i%.t:!e, ~
Associate Vice President/Project Coordinator
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1. Introduction
1.1 Site History
1.2 Summary of Remedial System Construction and Startup
1.3 Monitoring and Reporting Requirements
2. Groundwater Monitoring
2.1 Water-Leve/ Measurement
2.2 Groundwater Sampling
2.2.1 Baseline
2.2.2 First Quarter
2.2.3 Second Quarter
2.3 Results and Discussion ,r
3. Remediation System Performance
3.1 Recovery System Performance
3.1.1 Capture Zone Evaluation
3.1.2 Assessment of Groundwater Quality
3.2 Treatment System Performance
3.3 Operation and Maintenance (O&M)
4. Summary
5. References
Tables
2-1 Groundwater Sample Quality VOC and Inorganic Data Summary-
September 1998.
2-2 Revised Monitoring Program.
2-3 Water-Leve/ Elevations April -October 2000.
2-4 Groundwater Quality Data Summary.
2-5 Comparison of Predicted and Actual Drawdown.
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Table of Contents
1-1
1 -1
1-1
1-2
2-1
2-1
2-1
2-2
2-2
2-3
2-3
3-1
3-1
3-1
3-1
3-2
3-2
4-1
5-1
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2-6 Summary of Recovery Well Analytical Results.
2-7 Air Stripper Influent Quality Data Summary.
2-8 Summary of Groundwater Remediation System Effluent Monitoring
Wells.
2-9 Summary of Extraction system Flow Rates.
Figures
1-1. Site Map.
2-1 Groundwater Potentiometric Surface, April 3, 2000.
2-2 Groundwater Potentiometric Surfce, July 24, 2000.
2-3 Groundwater Potentiometric Surface, october 9, 2000.
2-4 TCE and PCE Concentrations in Groundwater, April -October 2000.
Appendices
A. Analytical Reports.
B. Construction Document for Well CMMW22A.
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Table of Contents
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1. Introduction
ARCADIS Geraghty & Miller of North Carolina, Inc. (ARCADIS Geraghty & Miller)
prepared ·this report on behaif of JFD Electronics Corporation and CMSS, Inc. for the
JFD Electronics/Channel Master NPL site (the site) located in Oxford, North Carolina.
This report was prepared to meet the semiannual reporting requirements proposed in
the Final Design Report (FDR) (Geraghty & Miller, 1996). The purpose of tlus report
is to summarize groundwater-sampling results and operational 'information of the
groundwater remediation system, The remainder of this report is organized as follows:
Section I provides a brief history of the site and the remedial design information; . ' Section 2 discusses groundwater-sampling procedures and analytical results; Section 3
discusses the performance of the groundwater remediation system; Section 4
.summarizes the contents of this report; and Section 5 lists the references used in this
report.
1.1 · Site History
The JFD Electronics/Channel Master site is located in Oxford, Granville County,
North Carolina, and is approximately· 13 acres. A site map is included as Figure 1-1.
Television antennas were once manufactured at the site, a process that involved copper
and nickel electroplating and chrome conversion coating of antenna parts.
Manufacturing processes also involved the degreasing of parts using solvents,
including tetrachloroethene (PCE) and trichloroethene (TCE) (Geraghty & Miller,
1993).' Spent solvents reportedly were disposed of outside ofthe building near a •
loading dock. The site is currently owned by CMSS, Inc. (then Channel Master
. Satellite Systems). The main building is used as a packaging and distribution center of
electronic parts. The Bandag Warehouse is currently not in use. A.detailed
. operational history of the site is in~luded in the Remedial Investigation Report and
Feasibility Study completed by Bechtel Environmental, Inc. (Bechtel, 1992a and
1992b ). ARCAD!S Geraghty & Miller and GMCE, Inc. prepared the FDR in July
1996. The FDR was approved by the United States Environmental Protection Agency
(USEPA) in September 1996.
1.2 Summary of Remedial System Construction and Startup
The groundwater remediation system construction was initiated in May 1998 and was
completed in August 1998. The groundwater remediation system consists of four deep
saprolite recovery wells (up to 60 feet deep) and three shallow recovery wells (up to 25
feet deep), an air stripper for treatment of volatile organic compounds (VOCs) in
contaminated groundwater, and discharge of treated effluent to an unnamed tributary
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(intermittent stream)ofFishing Creek. The total depths of the recovery Wells PW-I,
PW-2, PW-3, and PW-4 are 60 feet, 37 feet, 24 feet, and 58 feet, respectively. The
recovery.well locations are presented in Figure 1-1. After an initial start-up period, the
remediation system began operation during the last week of August 1998. Details of
the remedial system construction could be found in the Final Construction Report -
Revision I {ARCADIS Geraghty & Miller, 2000).
Groundwater samples collected during the first week of operation (September 2, 1998)
indicated the presence of total and amenable cyanide in low concentrations in the
extracted groundwater. The total cyanide concentrations in the effluent exceeded the
substantive discharge requirements of 5 micrograms per liter {µg/L). The existing
remediation system is designed to treat only VOCs. Therefore, the groundwater
remediation system was immediately shut down. Table 1-1 summarizes analytical
results for VOCs and inorganic compounds in the recovery wells and treatment system
effluent. To address the disposal of the air stripper effluent containing low-
concentration cyanide, ARCADIS Geraghty & Miller negotiated a sewer usage permit
with the City of Oxford {the City). The City issued an Industrial User Permit in
September 1999. This permit has a maximum cyanide discharge limit of50 µg/L. A
design modification was ·proposed to the USEPA in a letter dated October 28, 1999.
Based. on verbal approval from the USEPA, the design modification was implemented·
in March 2000.
After implementing the design modifications, the groundwater system was returned to
operation on April 12, 2000. Pumping Wells PW-I, PW-2, PW-3, and PW-4 and the
air-stripper system were put into operation on that date. However, the PW-5 well
cluster (PW-SA, PW-SB, and PW-SC) was not put into operation as the Enhanced
Reductive Dechlorination {ERO) pilot test was in progress. This decision was based
on a request by the North Carolina Department of Environment and Natural Resources,
Underground Injection Control section to eliminate interference of the pumping wells
with the ongoing pilot test. The PW-5 well cluster was returned to operation on
November 17, 2000.
1.3 Monitoring and Reporting Requirements
An environmental monitoring program is required by the FDR to ensure that the
remedial efforts meet the design objectives. The groundwater monitoring Wells
CMMW05, CMMWIO, CMMW07, CMMW 15, CMMWI 7, CMMW19, CMMW 20,
CMMW21, CMMW22 (now CMMW22A), CMMW23, CMMW24, CMMW26, Mr.
Finch's water-supply well, the treatment system influent, and effluent must be sampled
periodically in accordance with the FDR. The frequency of monitoring and parameters
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for analysis, modified based on the sewer usage permit issued by the City, are listed on
Table 1-2.
Groundwater levels in the monitoring and recovery wells are to be monitored on a
monthly basis during the first year of remediation and semiannually thereafter:
However, due to miscommunications, ARCADIS Geraghty & Miller measured
groundwater levels on a quarterly, rather than monthly, basis during the first two·
quarters ofremediation. The water levels in the wells will be measured on a monthly
basis until the end of the first year of remediation. The purpose of the groundwater
measurements is to use the data to create potentiometric surface maps of the water
table and evaluate the· groundwater recovery system's effectiveness in containing the
dissolved contaminant plume.
As proposed in the FDR, reports on the monitoring results must be prepared and
submitted to the USEPA on a semiannual basis. These reports will include a
description of field activities, a summary of groundwater-quality data, and a summary
of water-level data. The results of the monitoring program will be used to optimize the
operation of the remediation system. A summary of the system operation and
maintenance program.must also be included in the report. Further.details of the
monitoring and reporting requirements can be found in the FDR.
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2. Groundwater Monitoring
As proposed in the FDR, groundwater samples were collected from the designated
monitor wells at the site on a quarterly basis. In addition, water levels in the monitor
and recovery wells were also collected. Section 2.1 briefly describes the water-level
measurement, and Section 2.2 describes quarterly monitor well sampling activities. . .
Analytical results of the quarterly monitoring are discussed in Section 2.3.
2.1 Water-Level Measurement
Prior to collecting groundwater samples, a round of groundwater levels was collected
from monitoring wells at the site using an electronic water-level meter. As discussed
in Section 1.3, water levels were collected on April 3, 2000, July 24, 2000, and
October 9, 2000 (quarterly). Depth to water levels and groundwater elevations in the
monitor and recovery wells collected during all three monitoring events are shown on
Table 2-1. Potentiometric surface maps of groundwater at the site were prepared based
on depth to groundwater measured during the quarterly sampling events. As shown on
Figure 2-1, groundwater at the site flows primarily to the east, which is consistent with
previously observed data. Figures 2-2_and.2-3 presents groundwater potentiometric
maps under pumping conditions at the site. Based on these maps, the general direction
of groundwater flow is primarily to the east. As shown on Figures 2-2 and 2-3,
groundwater drawdowns were observed in the vicinity of recovery wells due to
groundwater pumping.
2.2 . Grou~dwater Sampling
To date, three rounds of groundwater sampling have been conducted at the site. A
baseline sampling event was performed in April 2000, prior to starting the
groundwater remediation system. Subsequently, first quarter sampling was performed
in July 2000, and second quarter sampling was performed in October 2000. The
remainder of this section discusses the groundwater-elevation data and results of the
three sampling events. The extent and frequency_ of the monitoring program is
summarized in Table 1-2. The monitoring events were performed in general
accordance with the procedures described in the Performance Standard Verification
Plan (PSVP) which was included as Appendix I in the FDR (Geraghty & Miller,
1996). The sampling and analytical procedures are summarized below.
Prior to sampling, each well was purged and then sampled using low-flow techniques
as described in the PSVP. All field equipment was decontaminated according to the
PSVP after use at each well. The decontamination water and purge water was then
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transferred to the polyethylene tank located onsite, which contained development
water and decontamination water from the groundwater remediation system
construction for treatment and disposal.
As part of the quality control, trip blanks, equipment rinse blanks, and field blanks
were prepared and analyzed for voes. In addition, one duplicate sample was also
collected and analyzed for voes and total and amenable cyanide. All samples were
immediately preserved and placed in an ice chest after collection. The groundwater
samples were shipped to STL Savannah Laboratories in Savannah, Georgia, for
analysis. The following sections briefly discuss the various sampling events.
2.2.1 Baseline
AReADIS Geraghty & Miller personnel performed the baseline groundwater-
sampling activities between April 3 and April 6, 2000, at 12 monitoring wells. The ·
~ampling was performed to obtain baseline groundwater quality data at the site prior to
the start of the modified remedial system. Groundwater samples were collected from
the monitoring Wells eMMW04, eMMW05, eMMW07, eMMWI0, eMMWl5,
eMMW!7, eMMWl9, eMMW20, eMMW2l, eMMW23, eMMW24, and
eMMW26. eMMW22A, which replaced the destroyed Well eMMW22 on July 18,
2000, had not yet been installed. The locations of all wells are shown on Figure l -1.
As proposed in the FDR, one private water-supply well, located at the Finch residence,
was also sampled.
All groundwater samples collected at the site were analyzed for voes using lJSEPA
Method 8260. In addition, the groundwater sample from monitoring Well eMMW04
was analyzed for total and amenable cyanide (USEPA Method 90 I 0). The data was
validated by AReADIS Geraghty & Miller using Level II Data Quality objectives. A ·
summary of the laboratory analytical results is presented in Table 2-2. Analytical
reports are included as Appendix A.
2.2.2 First Quarter
On July 18, 2000, groundwater monitoring Well eMMW22A was installed in the
vicinity of the former Well eMMW22, as located by the AReADIS Geraghty &
· Miller surveyors. The well was installed to a depth of25 feet below land surface (ft
bis) with a screened interval from 15 ft bis to 25 ft bis. Borehole for the monitor well
was drilled using a hollow-stem auger drill rig. Tiris well was constructed of2-inch
diameter polyvinyl chloride casing and well screen with IO feet of 0.0 I 0-inc~ slotted
screen. The well construction document is included in Appendix B.
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The first quarter sampling event was performed on July 25, 2000, through July 27,
2000. A total of 13 monitoring Wells (eMMW04, eMMW05, eMMW07,
eMMWI0, eMMWJ5, eMMW17, eMMWl9, eMMW20, eMMW21, eMMW22A,
eMMW23, eMMW24, and eMMW26) were sampled and analyzed for VOCs by
US EPA Method 8260 and selected metals ( chromium, nickel, and copper) by US EPA
. Method 60 I 0. In addition, the sample obtained from eMMW04 was analyzed for total
and amenable cyanide by USEPA 9010. The data was validated by AReADIS
Geraghty & Miller using Level II Data Quality objectives. The analytical results are
summarized on Table 2-2.
2.2.3 Second Quarter
The second quarter sampling event was performed on October 9 through October 11, 2000.
A total of 13 monitoring Wells (eMMW 04, eMMW 05, eMMW07, eMMWI 0,
eMMW15, CMMWI 7, CMMW19, eMMW20, eMMW21, eMMW22A, eMMW23,
eMMW24, and eMMW26) and four recovery Wells (PW!, PW2, PW3, and PW4) were
sampled as well as the remedial system influent and discharge. All samples were analyzed
for voes using US EPA Method 8260. In addition, samples obtained from Well
eMMW04, the recovery wells, and the influent and discharge were analyzed for total and
amenable cyanide using USEPA Method 9010. The data was validated by AReADIS
Geraghty & Miller using Level II Data Quality objectives. The analytical results for
monitor wells are summarized on Table 2-2. The analytical results for the recovery wells
are discussed in Section 3.
2.3 Results and Discussion
Table 2-2 summarizes the analytical results for the groundwater samples collected in
_ April 2000, July 2000, and October 2000. Figure 2-4 presents the TeE and PeE
concentrations in groundwater samples collected during the baseline and quarterly
sampling events from the selected monitoring wells at the site. The following sections _
briefly discuss the sampling results.
Based on the analytical results summarized on Table 2-2, the voe concentrations in
the on-site monitoring wells vary only slightly from the previous sampling events, with
the exception of monitoring Well eMMWI0. This well had PeE and TCE
concentrations of 11,000 µg/L and 170,000 µg/L, respectively, in April 2000. These
concentrations are similar to those found in the March 1999 sampling event
(AReADIS Geraghty & Miller, 1999). The PeE and TeE concentrations declined to
3,400 µg/L and 83,000 µg/L in July 2000 and then to 2,000 µg/L and 42,000 µg/L in
October 2000, respectively. This significant decline in PeE and TeE concentrations is
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due to the ERD pilot test. This is supported by the increase in cis-1,2-dichloroethene
(cis-1,2-DCE) from 16,000 µg/L in April 2000 to 98,000 µg/L in October 2000.
The baseline concentration ofTCE in Well CMMW05 was slightly lower than that
observed in March 1999. The TCE concentration fluctuated between 140,000 µg/L
(baseline) to 200,000 µg/L in October 2000. Some fluctuations in PCE concentrations
were observed in this well. This type of fluctuations in contaminant concentrations is
common occurrence and is probably related to natural processes in the aquifer.
As presented in Table 2-2, VOC concentrations in monitoring Well CMMW04 varied
slightly over the sampling period. TCE concentrations decreased from 6,500 µg/L in
April 2000 to 5,500 µg/L in October 2000. PCE concentrations varied slightly during
the sampling period. These variations in VOC concentrations are probably due to ·
seasonal fluctuations in water levels. In March 1999, both total and amenable cyanide
were 250 µg/L in Well CMMW04. However, the total and amenable cyanide in this
well decreased to 170 µg/L and 12 µg/L, respectively, in April 2000. The total cyanide
concentrations remained at 170 µg/L during the first and second quarterly sampling
events,'but the amenable cyanide concentrations fluctuated from 12 µg/L to 50 µg/L.
The VOC concentrations in the groundwater samples collected from perimeter
monitoring Wells CMMW15, CMMW20, CMMW21, and CMMW26 varied slightly
from the previous sampling results. A slight decrease in PCE, TCE, and cis-1,2-DCE
concentrations were observed in Well CMMW15. Concentrations ofTCE and PCE in
Well CMMW20 began declining slightly from the baseline concentration. Low
concentrations ofTCE (1.1 µg/L to 1.7 µg/L) were observed in the downgradient Well
CMMW24 during the April 2000 and July 2000 monitoring periods. However, the
· October 2000 sampling event indicates that VOCs are below practical quantitation
limits (PQLs) in this well.
Monitoring Well CMMW23, located on Oxford Associates' property (Oak Ridge
housing), had not been sampled since February 1997 due to access restrictions. Low
concentrations ofTCE, PCE, and cis-1,2-DCE were detected in this well in February
1997. As shown on Figure2-4, monitoring Well CMMW23 had PCE concentrations ·
of 330 µg/L in April 2000 and 280 µg/L in October 2000. Similarly, TCE
concentrations varied from 42 µg/L (April 2000) and 38 µg/L (October ~000).
Low concentrations ofTCE and cis-1,2-DCE were detected in Well CMMW24
(downgradient well) at 1.7 µg/L and 1.2 µg/L, respectively, during the April 2000
sampling event. However, no VOCs were detected above PQLs in the first or second
quarterly sampling events.
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The VOC concentrations vary slightly in off-site monitoring Wells CMMW07,
CMMWI 9, and CMMWI 7 during the sampling period. A slight decrease in PCE,
TCE and cis-1,2-DCE concentrations were observed in Well CMMW07 over the
March 1999 sampling results. However, Well CMMW22A (replacement for well
CMMW22) did not contain VOCs above PQLs during the sampling period.
Consistent with the previous sampling events, no VOCs_were detected above PQLs in
. the groundwater sample collected from Finch's well in April 2000.
As presented in Table 2-2, none of the monitoring wells sampled in July 2000 had
metals (chromium, nickel, and copper) exceeding the PQLs, except for Well
CMMWI 5. Titis well contained chromium concentration of 14 µg/L in the July 2000
sampling event, which is below the Remediation Goal of 50 µg/L. This information
confirms that metals are not a concern at the site groundwater.
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3. Remediation System Performance
The extraction system was reactivated on April 12, 2000, after implementing the
design modifications (connection to sewer). The pumping Wells PW-I, PW-2, PW-3,
and PW-4 and the air stripper were put into operation. As indicated in Section 1.2, the
PW-5 well cluster was not returned to operation in this reporting period to reduce
interference with the ERD pilot test. This well cluster was returned to operation upon
completing of the pilot test in November 2000.
·rn accordance with the FDR, the performance of the recovery system was evaluated to
verify if the performance standards are being inet. The recovery system was evaluated
with respect to the capture zone and the groundwater quality. The remainder of this
section describes the recovery system evaluation.
3.1 Recovery System Performance
3.1.1 Capture Zone Evaluation
Potentiometric surfaces based on depth to groundwater measured are shown in Figures
2-1 through 2-3. The PSVP in the FDR proposed monitoring hydraulic parameters to
evaluate if the predicted capture zone is maintained during operation of the
groundwater recovery system. The approach proposed in.the PSVP is to compare the
predicted drawdown with actual drawdown in selected monitoring wells. A
comparison of predicted versus actual drawdown is presented in Table 3-1. Based on
the data in this table, actual drawdowns in selected wells are found to be greater than
the predicted drawdowns in the FDR. This is indicative oflikely establishment of
capture zones as predicted in the FDR.
3.1.2 Assessment of Groundwater Quality
As proposed in the FDR, groundwater samples were collected from the recovery Wells
PW-I, PW-2, PW-3, and PW-4 on April 18, 2000, and on October 11, 2000 (after 6
months of operation). The groundwater samples were analyzed for voes and total
and amenable cyanide. The recovery Well PW-5 cluster was not in operation and
therefore, it was not sampled. Table 3-2 presents a summary of the recovery well
analytical results. Based on the analytical results, the voe concentrations in Wells
PW-I and PW-3 increased slightly over the 6-month period. However, the voe
concentration slightly decreased in Well PW-2. voe concentrations were below PQL
for Well PW-4 in April 2000. However, low concentrations ofVOes were detected in
this recovery well in October 2000. Low concentrations of total cyanide were detected
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in the recovery Wells PW-I and PW-2, but the amenable cyanide co~centrations were
below PQL. Both total and amenable cyanide concentrations were below PQL in
Wells PW-3 and PW-4.
3.2 Treatment System Performance
As proposed in the FDR, treatment system influent and effluent were samp_led weekly
during the first month of operation and quarterly thereafter during the first year of
operation. Table 3-3 summarizes the analytical results for the air stripper influent. A
slight fluctuation in concentration ofVOCs is observed in the treatment system
influent. The results of the effluent sampling have been previously reported to the City
of Oxford. A summary of the analytical data for the effluent is included as Table 3-4.
The analytical results in this table indicate that the treatment system has been
consistently reducing VOCs to below their respective PQLs since the recovery system
began operation in April 2000. Total cyanide concentrations in the effluent fluctuate;
however, they are below the permit limit of 50 µg/L.
As part of the routine monitoring, totalizer data were collected from the recovery
Wells PW-I through PW-4. Using the totalizer data and the sampling dates,,average
flow rates·were calculated. Table 3-5 presents a summary of the recovery well flow
data and estimated extraction system flow rates. Based on data in this table, slight
seasonal fluctuations in the recovery rates were observed.
3.3 Operation and Maintenance (O&M)
O&M was performed in general accordance with the O&M_Manual in the FDR. Prior
to the start-up of the system (after design modifications), all flow meters, pumps, and
flow switches were cleaned. As part of the monitoring, pressru:e readings from the
individual recovery system headers and the combined influent to the air stripper were
routinely collected to monitor the recovery pumps' performance. In addition, pressure
readings were routinely monitored and recorded to evaluate the performance of the air
blower. The air stripper has been operating without major problems or breakdowns
since the start-up. No additional maintenance was performed during this period.
G:\E nv\JFDCHAN N\N (0202. 170\C&M REPORTS\Semi_Aiinua I_Report\T ext\!iemi-2000_Rev. DOC
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Performance
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4. Summary
Since operation of the recovery system began, the groundwater quality has changed
most significantly at Well CMMWI 0. However, the improvement in the groundwater
quality at CMMWI O is due to the enhanced reductive dechlorination pilot study in this
area. Overall, the monitoring wells show some fluctuations in VOC concentrations.
Concentrations ofTCE and PCE in downgradient monitoring Well CMMW24 have
declined. The trends in groundwater quality will be periodically evaluated. The
treatment system has been performing as excepted and has been successful in reducing
VOCs to below PQLs.
G:\Env\IFOCHAN N\N(D202. 170\0& M REPORTS\Semi_Ann ual_Report\T ext\seml-2000_Rev .DOC
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5. References
ARCADIS Geraghty & Miller of North Carolina, Inc., 2000. Final Construction
Report -Revision 1, Groundwater Remediation, JFD Electronics/Channel
Master Site, Oxford, North Carolina, December 2000.
Bechtel, 1992a. Remedial Investigation Report for the JFD Electronics/Channel ·
.Master Site, Oxford, Granville County, North Carolina. April.
Bechtel, 1992b. Feasibility Study Report for the JFD Electronics/Channel Master Site,
Oxford, Granville County, North Carolina. April.
Geraghty & Miller, Inc., 1993. Remedial Design Work Plan, JFD Electronics/Channel
· Master NPL Site, Oxford, North Carolina, November 30, 1993.
Geraghty & Miller, Inc., 1996. Final Design Report, JFD Electronics/Channel Master ·
Site, July 1996.
ARCADIS Geraghty & Miller, 1999. Annual Groundwater Sampling Results, JFD
Electronics/Channel Master NPL Site, Oxford, North Carolina, October 1999.
Semiannual
Groundwater
Remediation Report
References
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Groundwater
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Tables
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ARCADIS GERAGHTY&MILLER
Table 1-1. Groundwater Sample Quality VOC and Inorganic Data Summary, Groundwater Treatment System Operation -September 1998,
JFD Electronics/Cbannel Master Site, Oxford, North Carolina
Sample Name: PW-I PW-2 PW-3 PW-4 PW-5A,B,&C
Sample Date: 9/2/1998 9/2/1998 9/2/1998 9/2/1998 9/2/1998.
EF-1
9/2/1998
Sample Type: Recovery Well Recovery Well Recovery Well Recovery Well Recovery Well Treatment Effluent
Yolatilc Organic Compa1mds (11gll ,)
(USEPA Method 8260)
Vinyl Chloride <IO 3.6 <1.0 <1.0 <500 <1.0
I, I Dichloroethane <IO 1.4 <1.0 <1.0 <500 <1.0
l, 1-Dichloroethene <IO 2.0 <1.0 <1.0 <500 <1.0
cis-1,2-Dichloroethene 130 30 58D <25.0 1,400 1.3
trans 1,2 Dichloroethene <IO 2.0 <1.0 <1.0 <500 <1.0
Trichloroethene 5,400D 85D 330D 3.5 69,000D 11
Tetrachloroethene 380D 190D 280D <1.0 2,600 <1.0
C)!'.anidc (mga,)
(USEPA Method 335.2) ....
Total 0.053] 0.013] 0.017J <0.005 0.020J 0.022J
Amenable <0.005 <0.005 <0.005 <0.005 <0.005 <0.005
Metals (mgll )
(USEPA Method 6010)
Iron 0.39 0.1 0.28 <0.05 15 6.5
Manganese 0.084 0.22 0.025 <0.01 0,35 NA
Tumidity (NJ1 O 88 53 34 28 140 86
(USEPA Method 180.1)
µg/L Micrograms per liter.
mg/L Milligrams per liter
NTU Nephelometric Turbidity Unit
< Compound was not detected above the quantitation limit.
J Compound concentration is qualified as estimated because the batch sample matrix spike recovery was above the upper QC limit.
D Compound was quantitated using a secondary dilution factor.
NA Co!Dpound was not analyzed.
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Table 1-2 Revised Monitoring Program Groundwater Remediation System JFD Electronics/Channel Master Site, Oxford, North Carolina.
Groundwater Perimeter
Parameter Method Monitoring Wells' Monitoring Recovery Wells'
Wells'
1st Year 2nd Year 1st 3 Year 1st Year
Onward Only
pH Field Q s Q s
Temperature Field Q s Q s
Specific Conductivity Field Q s Q s
Trichloroethene Method 8260 Q s Q s
Tetrachloroethene Method 8260 Q s Q s
1,2-Dichloroethene (total) Method 8260 Q s Q s
I, 1-Dichloroethcne Method 8260 Q s Q s
1,2-Dichloroethane Method 8260 Q s Q s
Vinyl Chloride Method 8260 Q s Q s
Copper Method 6010 A
Nickel Method 6010 A
Chromium Method 6010 A
Cyanide (total) Method 335.2
Cyanide (amenable/total) Method 335.2 Q' Q' Q s
Water Table Elevation M s M
Flow
Weekly sampling for parameters indicated
Notes:
w
W-lffM
W-1/M
W-1/S
W-1/Q
M
Weekly sampling during 1st three months and monthly thereafter for the parameters indicated.
Weekly sampling during 1st moiith and monthly thereafter for the parameters indicated.
Weekly sampling during 1st month and semi-annually thereafter for the parameters indicated.
weekly sampling duru'ig 1st month and quarterly thereafter for the parameters indicated.
Monthly sampling for parameters indicated.
Q s
A
C
Quarterly sampling for parameters indicated.
Semi-annual sampling for parameters indicated.
Annual sampling for parameters indicated.
Continous flow monitoring per NPDES requirements
Not sampled/Not applicable
2nd Year
Onward
A
A
A
A
A
A
A
A
A
A
s
Treatment Influent
1st Year 2nd Year
Onward
W-1/Q s
W-1/Q s
W-1/Q s
W-1/Q s
W-1/Q s
W-1/Q s
---
Treatment Effluent
1st Year 2nd.Year
Onward
.. W-lfrM M
W-lffM M
W-lffM M
W-lffM M
W-lffM M
W-lffM M
W-lffM M
W-lffM M
W-lffM M
C C
1 Monitoring Wells: CMMW05, CMMW07, CMMWIO, CMMWl5, CMMW17, CMMW19, CMMCW20, CMMW21, CMMW22A, CMMW23, & CMMW26. Private water supply
well at the Finch fcsidence will be sampled annually for EPA Method 8260.
1 Recovery well samples will be collected from the recovery well headers 8.t startup, semi-annually during the 1st year and annually thereafter.
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3 Perimeter monitoring wells will be sampled quarterly during the first 3 years of remediation. These wells include CNIMW15, CMMW20, CMMW21, CMMW22A, CMMW23, CMMW24, & CMMW26
4 Monitoring Well CMMW04 will be sampled for total & amenable cyanide on a quarterly basis for the first 3 years of remediation.
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Table 2-1. Water Level Elevations, April-October 2000, JF1) Electronics/Channel Master Site, Oxford, Nonh earo·
I Measuring Point April 3, 2000 July 24, 2000 October 9, 2000
Monitor E:Ievation DTW GWE!vtn DTW GWE!vtn DTW GWElvtn
'
Well ID (ft ms!) (ft toe) (ft ms!) (ft toe) (ft ms!) (ft toe) (ft ms!)
CMMW0I 478.18 8.38 469.80 9.60 468.58 8.53 469.65
CMMW02 466.24 5.74 460.50 12.97 453.27 13.55 452.69
I CMMW03 466.23 3.22 463.01 NM 12.39 453.84
CMMW04 463.60 7.46 456.14 11.79 451.8 I 12.31 451.29
CMMW05 469.99 7.06 462.93 9.67 460.32 10.13 459.86
CMMW06 459.03 6.13 452.90 13.31 445.72 15.59 443.44
I CMMW07 463.60 4.72 458.88 6.99 456.61 8.34 455.26
CMMW08 476.74 7.23 469.51 8.41 468.33 8.09 468.65
CMMW09 472.68 4.46 468.22 5.33 467.35 5.74 466.94
CMMWI0 469.71 6.92 462.79 9.75 459.96 8.32 461.39
I CMMWII· 466.69 5.78 · 460.91 10.00 456.69 10.56 456.13
CMMW12 466.78 5.73 461.05 9.93 456.85 10.48 456.30
CMMW13 463.68 NM 10.92 452.76 11.55 452.13
CMMW14 468.40 9.11 459.29 14.56 453.84 15.22 453.18
I CMMWl5 468.17 8.88 459.29 14.51 453.66 15.22 452.95
CMMWI6 458.02 3.14 454.88 5.74 452.28 6.99 451.03
CMMW17 460.15 5.30 454.85 8.42 451.73 8.77 451.38
CMMWI8 455.58 3.89 451.69 8.51 447.07 8.72 446.86
I CMMW19 456.48 5.01 451.47 9.43 447.05 9.65 446.83
CMMW20 469.37 12.14 457.23 14.51 454.86 15.00 454.37
CMMW21 456.22 2.44 453.78 4.97. 451.25 5.43 450.79
CMMW221 456.12 NA NA NA I CMMW22A 460.45 NA 10.55 449.90 10.99 449.46
CMMW23 447.64 4.02 443.62 9.45 438.19 9.71 437.93
CMMW24 445.58 434 441.24 6.23 439.35 6.26 439.32
I CMMW25 466.96 6.91 460.05 10.57 456.39 11.54 455.42
CMMW26 468.44 6.40 462.04 9.80 458.64 10.30 458.14
TW-24 463.88 7.86 456.02 11.82 452.06 11.80 452.08
SME-01 477.80 6.67 471.13 7.90 469.90 9.62 468.18
I OW-I 466.14 5.28 460.86 NM 18.00 448.14
PW-1° 466.96 NM 18.41 448.55 9.59 457.37
PW-2° 458.36 NM 15.20 443.16 19.30 439.06
PW-3° 451.46 NM 15.60 435.86 16.59 434.87,
I PW-4° 459.29 NM 38.52 420.77 35.34 423.95
PW-5A0 470.17 NM 9.42 460.75 NM
PW-se· 469.64 NM NM NM
PW-sc· 469.24 NM NM NM
I Notes:
DTW Depth to Water
GWE!vtn Groundwater Elevation
I ft toe Feet below top of casing
ft msl Feet l!,bove mean sea level
NM Not Measured
Not Applicable
I NA Not Available
CMMW22 has been destroyed probably due to site clearing activites by the site owner. Therefore, a rep!
CMMW22A was installed in July 2000.
I Top of the well cOvers are used as measuring points for recovery wells. Where as the measuring point
elevations for monitoring wells are top of the casing.
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Table 2-2. Groundwater Quality Data Swmna,y, JFD Electronics/Channel Master Site, Oxford, North Carolin'!.
Sample Name: CMMW04' CMMW04 CMMW04 CMMW05' CMMW05 C:MMW05 CMMW07 / CMMW07 CMMW07 Sample Date: 4/5/2000 7/26/2000 10/11/2000 4/6/2000 7/27/2000 10/10/2000 4/5/2000 7/26/2000 10/10/2000
lab ID: 02218-12 05051-14 07009-1 02265-4 05051-1 07009-20 02218-7 05051-2 07009-22
Yolatilc O:reanic C-nmllOnDds BcmciUatian
(USFPA Method 8260) Goals
Acetone <1200 <1200 <1200 <25,000 <25,000 · <25,000 <50 <50 <50 Benzene 5 <50 <50 <50 <1,000 <1,000 <1,000 <2.0 <2.0 <2.0 Carbon disulfide <50 <50 <50 <1,000 <1,000 <l,000 <2.0 <2.0 <2.0 Carbon tetrachloride <50 <50 <50 <1,000 <1,000 <1,000 <2.0 <2.0 <2.0 Chlorobenzene <50 <50 <50 <1,000 <1,000 <1,000 <2.0 <2.0 <2.0
Chloroform <50 <50 <50 <1,000 <1,000 <1,000 <2.0 <2.0 <2.0 1,1-Dichloroethane <50 <50 <50 <1,000 <1;000 . <1,000 <2.0 <2.0 <2.0
I, 1-Dichloroethene 7 <50 <50 <50 <1,000 <1,000 <1,000 <2.0 <2.0 <2.0 cis-1,2-Dichloroethene 70 llOJ' 110 110 <l,000 650J <l,000 120 51 51 trans-1,2-Dichloroethene 70 <50 <50 <50 <1,000 <1,000 <1,000 <2.0 <2.0 <2.0 2-Hexanone <50 <50 <50 <10,000 <10,000 <10,000 <20 <20 <20 4-Methyl-2-pentanone <50 <50 <50 <10,000 <10,000 <10,000 <20 <20 <20
Tetrachloroethene 0.7 400J' 520 580 u,ooo 12,000 1s,ooo 41 29 30
1,1,1-Trichloroethane 200 <50 <50 <50 <l.!)00 <l.!)00 <1,000 <2.0 <2.0 <2.0
Trichloroethene 2.8 6JOO 6,200 SJOO 140,000 180,000 200,000 I 320 220 260
Vtnyl Chloride 0.015 <50 <50 <50 <l,000 <1,000" <l,000 <2.0 <2.0 <2.0
Molll.ls
(USFPA Method 6010)
Chromium 50 NA <20 NA NA <10 NA NA <10 NA
Nickel 100 NA <40 NA NA <40 NA NA <40 NA
Copper 1000 NA <10 NA NA <20 NA NA <20 NA
C=ide
(USFPA Method 9010)
Total 154 170 I 170 · I 170 NA NA NA NA NA NA, Amenable 12 29J so NA NA ·NA NA NA NA
Notes:
All results reported in microgTIIIDS per liter (/!g/L)
< Compound was not detected above the quantitation limit.
J Compound concentration is qualified as estimated.
D Compound was quantitated nsing a secondary dilution factor.
Compound concentration is qualified as estimated because the field replicate sample criteria were not met.
Compound concentration was qualified as non detected because of asstablished QC Blank sample contamination . • Field replicate of groundwater sample CMMW-04.
NA Compound was not analyzed.
!Constituents exceeding the remediation levels.
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Table 2-2. Groundwater Quality Data Summazy, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Sample Name: CMMWlOI CMMWlO CMMWlO CMMWIS I CMMWIS CMMWIS CMMW17 CMMWl7 CMMW17 Sample Date: 4/6/2000 7/26/2000 10/10/2000 4/5/2000 7/26/2000 10/11/2000 4/5/2000 7/26/2000 10/10/2000 lab ID: 02265-5 05051-3 07009-21 02218-9 05051-4 07009-23 02218-8 05051-5 07009-19
~latile Oxa:anh: Com12onnds Bcmediation
(USEPA Method 8260). Goals
Acetone <25,000 <25,000 <25,000 <62 <50 <62 57 <25 <25 Benzene 5 <l,000 <l,000 <1,000 <2.5 <2.0 <2.5 <1.0 <1.0 <1.0 Carbon disulfide <1,000 <1,000 <1,000 <2.5 <2.0 <2.5 2.3 <1.0 <1.0 Carbon tetrachloride <1,000 <1,000 <1,000 <2.5 <2.0 <2.5 <1.0 <1.0 <1.0 Chlorobenzene <1,000 <1,000 <1,000 <2.5 <2.0 <2.5 <1.0 <1.0 <1.0 Chloroform <l,000 · <1,000 . <1,000 <2.5 <2.0 <2.5 <1.0 <1.0. <1.0 1,1-Dichloroethane <1,000 <I 000 <1,000 <2.5 <2.0 <2.5 .<1.0 <1.0 <1.0 1,1-Dichloroethene 7 <I 000 480J <I 000 <2.5 <2.0 <2.5 <1.0. <1.0 <1.0 cis-1,2-Dichloroethene 70 16 000 87 000 98 000 13 4.2 <2.5 4.3 28 39 trans-1,2-Dichloroethene 70 <1,000 <l,000 <l,000 <2.5 <2.0 <2.5 <1.0 <1.0 <1.0 2-Hexanone <10,000 <10,000 ·<10,000 <25 <20 <25 <1.0 <10 <10 4-Methyl-2-pentanone <10,000 <10,000 <10,000 <25 <20 <25 <1.0 <10 <10 Tetrachloroethene 0.7 11,000 3,400 2,000 26 9.8 14 7.6 9.7 4.2 1,1,1-Trichloroethane 200 <l,000 <1:000 <I 000 . <2.5 <2.5 <2.5 <1.0 <1.0 <1.0
Trichloroeihene 2.8 110,000 83 000 42:000 390 180 230 14 27 24 I Vmyl Chloride 0.015 <1,000 <1,000 <1,000 <2.5 <2.5 <2.5 <1.0 <1.0 <1.0
Mc!ah
(USEPA Method 6010)
Chromium 50 NA <IO NA NA 14 NA NA _160 NA Nickel 100 NA <40 NA NA <40 NA NA 120 NA Copper 1000 NA <20 NA NA <20 NA NA <20 NA
{simido
(USEPA Method 9010)
Total 154 NA NA NA NA NA NA NA NA NA Amenable NA NA NA NA NA NA NA NA NA
Notes:
All results reported in micrograms per liter (Jlg/L) < Compound was not detected above the quantitation limit.
J Compound concentration is qualified as estimated.
D Compound was quantitated using a secondary dilution factor.
Compound concentration is qualified as estimated because the field replicate sample criteria were not met .
• Field replicate of groundwater sample CMMW-04.
NA Compound was not analy,.ed.
!Constituent, exceeding the remediation levels.
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Table 2-2. Groundwater Quality Data StlllllDllIY, JFD Electronics/Channel Master Site, Oxford, Nonh Carolina.
Sample Name: CMMW19 / CMMW19 CMMWl9 CMMW20' CMMW20 CMMW20 CMMW2J/ CMMW21 · CMMW21 Sample Date: 4/412000 7/25/2000 10/10/2000 4/412000 7/26/2000 10/10/2000 41412000 7/25/2000 10/9/2000
Lab ID: 02218-5 05051-6 07009-17 02218-4 05051-7 07009-16 02218-3 05051-8 07009-15
Yolatilt Oraanic Comnonnds · Bcmcdiation
(USEPA Method 8260) !lDals
Acetone <25 <25 <25 <250 <250 <250 <120 <125 <120 Benzene 5 <1.0 <1.0 <1.0 <10 <10 <10 <5.0 <5.0 <5.0
Carbon disulfide <1.0 <1.0 <1.0 <10 <10 <10 <5.0 <5.0 <5.0
Carbon tettach!oride <1.0 <1.0 <1.0 <10 4.8J <10 <5.0 <5.0 <5.0
Chlorobenzene <1.0 <1.0 <1.0 <10 <10 <10 8.0 83 <5.0
Chloroform <1.0 <1.0 <1.0 10 <10 <10 <5.0 <5.0 <5.0 1,1-Dichloroethane <1.0 <1.0 <1.0 <10 <10 <10 <5.0 <5.0 <5.0 1, 1-Dichloroethene · 7 <1.0 <1.0 <1.0 38 30 32 <5.0 <5.0 <5.0 cis-1,2-Dichloroethene 70 2.6 2.3 <1.0 36 26 27 300 270. 290
trans-1,2-Dichloroethene 70 <1.0 <1.0 <1.0 <10 <10 <10 <5.0 2.21 <5.0
2-HelOlllOne <10 <10 <10 <100 16J <100 <50 <50 <50
4-Methyl-2-pentanone <10 <10 <10 <100 16J <100 <50 <50 <50 Tetrachloroethene 0.7 · 67 62 31 lJOO 11!00 1,000 730 620 660
1,1,1-Trichloroethane 200 <1.0 <1.0 <1.0 <10 7.7J <10 <5.0 <5.0 <5.0
Trichloroethene 2.8 18 16 9.0 70 59 56 120 100 110
Vinyl Chloride 0.015 <1.0 <1.0 <1.0 <10 <10 <10 <5.0 <5.0 <5.0
Metah
(USEPA Method 6010)
Chromium 50 NA <10 NA NA <10 NA NA <10 NA Nickel 100 NA <40 NA NA <40 NA NA <40 NA Copper 1000 NA <20 NA NA <20 NA NA <20 NA
C=iJk
(USEPA Method 9010)
Total 154 NA NA NA NA NA NA NA NA NA
Amenable NA NA NA NA NA NA NA NA NA
Notes:
All results reported in micrograms per liter (µg/L)
< Compound was not detected above the quantitation limit.
I -Compound concentrD:tion is qualified as estimated.
D -Compound was quantitated nsing a secondary dilution factor.
' Compound concentration is qnalified as estimated becanse the field replicate sample criteria were not met.
• Field replicate of groundwater sample CMMW-04.
NA -Compound was not analyzed.
!Constituents exceeding the remediation levels.
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Table 2-2. Groundwater Quality Data Summary, JFD Electronics/Channel Master Site, Oxford, North Carolioa.
Sample Name: CMMW22A CMMW22A CMMW23 / CMMW23 CMMW23 CMMW24' CMMW24 CMMW24 Sample Date: 7/26/2000 10/9/2000 4/3/2000 7/25/2000 10/9/2000 4/3/2000 7/25/2000 . 10/11/2000 Lab ID: 05051-9 07009-14 02218-2 05051-10 07009-13 02218-1 05051-11 07009-12
Yolatilr: Oiaaoic Cnmixmods BemeiUaliDD
(USEPA Method 8260) · Gmlls
Acetone <25 <25 <25 <50 <25 <25 <25 <25 Benzene s <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 Carbon disulfide <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <LO <1.0 Carbon tetrachloride <LO <LO <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 Cblorobenzene <1.0 <LO <1.0 <2.0 <LO <1.0 <LO <1.0 . Chloroform <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <LO I, 1-Dichloroethane <1.0 <1.0 <1.0 <2.0 <1.0 <LO <1.0 <1.0 I, 1-Dichloroethene 7 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 cis-1,2-Dichloroethene 70 <1.0 . <1.0 68 80 69 1.2 <LO <1.0 trans-1,2-Dichloroethene 70 <LO <1.0 <1.0 <2.0 <1.0 <1.0 <LO <1.0 2-Hexanone <10 <10 <LO <20 <10 <1.0 <10 <1.0 4-Methyl-2-pentanone <10 <10 <1.0 <20 <10 <1.0. <10 <LO Tetrachloroethene · 0.7 <1.0 <LO 330D 320 280D 4.2 <1.0 <1.0 1,1,1-Trichloroethane 200 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <LO <1.0 Trichloroethene 2.8 <1.0 <LO 42 43 38 1.7 1.1 <LO Vmyl Chloride 0.015 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <LO <LO
Ml:lllh
(USEPA Method 6010)
Chromium so <10 NA NA <IO NA NA <10 NA Nickel 100 <40 NA NA <40 NA NA <40 NA Copper 1000 <20 NA NA <20 NA NA <20 NA
~
(USEPA Method 9010)
Total 154 NA NA NA NA NA NA NA NA Amenable NA NA NA NA NA NA NA NA
Notes:
All results reported in micrograms per liter (µg/L)
< Compound was not detected above the quantitation limit.
J -Compound concentration is qualified as estimated.
D. Compound was quantitated using a secondary dilution factor.
1 Compound concentration is qualified as estimated because the field replicate sample criteria were not met.
• Field replicate. of groundwater sample CMMW-04.
NA • Compound was not analy,.ed.
!Constituents exceeding the remediation levels.
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ARCADIS GERAGHTY&MILLER
Table 2-2. Groundwater Quality Data Summa,y,' JFD Electronics/Channel Master Site, Oxford, North Carolina.
Sample Name: CMMW26, CMMW26 CMMW26 REP-OJ• Duplicate• DUP-OJ• 'FINCH
Sample Date: 4/4/2000 7/26/2000 10/10/00 4/5/2000 7/26/2000 10/11/2000 4/25/2000
Lab ID: 02218-6 05051-12 07009-18 02218-13 05051-15 07009-2 02663-4
YoJatilc 0:t2aDic Comixmuds Remediation
(USEPA Method 8260) Gnala
Acetone <25 <25 <25 <1200 <1200 <1200 <25
Benzene 5 <1.0 <1.0 <1.0 <50 <50 <50 <LO
Carbon disulfide <1.0 <LO <1.0 <50 <50 <50 <1.0
Carbon tetrachloride <1.0 <1.0 <1.0 <50 <50 <50 <LO
Chlorobenzene <1.0 <1.0 <LO <50 <50 <50 <LO
Chloroform <1.0 1.2 <1.0 <50 <50 <50 <1.0
l , 1-Dichloroethane <1.0 <1.0 <1.0 <50 <50 <50 <LO
I, 1-Dichloroethene 7 <1.0 <1.0 <1.0 72 <50 <50 <1.0
cis-1,2-Dichloroethene 70 180 78 17 200 100 110 <LO
trans-1,2-Dichloroethene 70 5.0 1-5 <1.0 <50 <50 <50 <1.0
2-Hexanone <LO <10 <10 <50 <50 <500 <10
4-Methyl-2-pentanone <LO <10 <10 <50 <50 <500 <10
Tetrachloroethene 0.7 -180 180 36 650J' 430 450 <1.0
I, 1, I-Trichloroethane, 200 <LO <1.0 <1.0 <50 <50 <50 <1.0
Trichloroethene 2.8 12 14 · 3.1 1,000 5,!!00 51600 <1.0
Vinyl Chloride 0.o15 1-5 <1.0 <1.0 <50 <50 <50 <1.0
Ml:lllls
(USEPA Method 6010)
Chromium 50 NA <10 NA NA <20 NA NA
Nickel 100 NA <40 -NA NA <40 NA NA
Copper 1000 NA <20 NA NA <10 NA NA
C=ido
(USEPA Method 9010)
T_otal 154 NA NA NA 170 180 170 NA
Amenable NA NA NA ·8.9 57J 16 NA
Notes:
All results reported in micrograms per liter (µg/L)
< Compound was not detected above the quantitation limit.
J -Compound concentratiOn is qualified as estimated.
D -Compound was quantitated using a secondary dilution factor.
1 Compound concentration is qualified as estimated because the field replicate sample criteria were not met.
• Field replicate of groundwaier sample CMMW-04.
NA -Compound was not analyzed.
!Constituents exceeding the remediation levels.
G:1Env\lFOCfW..IN\NC0202. 170\0 REPORTS\Semi_Annual_RepOl'f\$arni-2000 _Rev.xi• Page 5 of5
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ARCADIS GERAGHTY&MILLER
Table 3-1. Comparison of Predicted and Actual Drawdown, JFD Electronics/Channel Mater, Oxford, North Carolina
Predicted Baseline First Quarter Second Quarter November
Location DrawdoMI1 4/3/2000 7/24/2000 10/9/2000 11/17/2000
· Groundwater Groundwater Drawdown2 Difference3 Groundwater Drawdown Difference Groundwater Drawdown Difference
Elevation Elevation Elevation Elevation
Shallow Wells
CMMW09 0.91 468.22 467.35 0.87 0.04 466.94 1.28 -0.37 466.31 1.91 . -1.00
CMMWIO 1.62 462.79 459.96 2.83 -1.21 461.39 1.4 0.22 459.03 3.76 -2.14
CMMWII 1.06 460.91 456.69 4.22 -3.16 456.13 4.78 -3.72
CMMWl3 1.40 NM 452.76 452.13 453.93
CMMWl4 1.25 459.29 453.84 5.45 -4.20 453.18 6_.11 -4.86 453.14 6.15 -4.90
CMMWl6 0.70 454.88 452.28 2.60 -1.90 451.03 3.85 -3.15 450.84 4.04 -3.34
CMMW20 0.56 457.23 454.86 2.37 -1.81 454.37 2.86 -2.30 453.49 3;74 -3.18
CMMW21 0.38 453.78 451.25 2.53 -2.15 450.79 2.99 -2.61 450.03 3.75 -3.37
CMMW22A' 0.55 NM 445.57 445.13 444.22
Intermediate Wells
CMMWOI 0.78 469.80 468.58 1.22 -0.44 469.65 0.15 0.63 467.68 2.12 -1.34
CMMW03 1.58 463.01 NM 453.84 9.17 -7.59 455.00 8.01 -6.43
CMMW05 1.44 462.93 460.32 2.61 -1.17 459.86 3.07 -1.63 459.38 3.55 -2.11
CMMW06 3.04 452.90 445.72 7.18 -4.14 443.44 9.46 -6.42 442.11 10.79 -7.75
CMMW19 1.04 451,47 447.05 4.42 -3.38 446.83 4.64 -3.60 445.98 5.49 -4.45
CMMW23 1.87 443.62 438.19 5.43 -3.56 437.93 5.69 -3.82 437.59 6.03 -4.16
CMMW24 0.32 441.24 439.35 1.89 -1.57 439.32 1.92 .-I.60
Notes:
' Druwdowns in monitor wells were predicted using the groundwater flow model in the Final Design Report.
' Drawdown = Baseline groundwater elevation -current groundwater elevation.
' Difference= Predicted drawdown -actual drawdown.
Difference in baseline and current groundwaler elevation.
' Replaced CMMW22 after the baseline water level readings
All values in feet
Groundwater elevations in feet above mean sea level
NM Not Measured
,
G:\Env\JFOCHANN\NC0202.17C10 REPORTS\Semt_Annual_Reportlseml-2000_Rev.xls
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ARCADIS GERAGHTY&MILLER
Table 3-2. Summary of Recovery Well Analytical Results, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Sample Name: PW! PW-I PW2 PW-2 PW3 PW-3 PW-4 PW-4
Sample Date: 4/18/2000 10/11/2000 4/18/2000 10/11/2000 4/18/2000 10/11/2000 4/18/2000 10/11/2000
Lab ID: 02502 07009-3 02502 07009-4 02502 07009-5 02502 07009-6
:!iolatile OrgaDh: Cowpmwds Bca:u:diatioD
(USEP A Me1hod 8260) Goals
Acetone <250 <250 2.9 <25 <50 <50 <25 <25
Benzene 5 <1.0 <10 <1.0 <1.0 0.30DJ <2.0 <1.0 <1.0
Carbon disulfide <1.0 <10 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0
Carbon tetrachloride <1.0 <10 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0
Chlorobenzcne <1.0 <10 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0
Chloroform <1.0 <10 <1.0 <1.0 <2.0 <2.0 <1.0 <1.0
1, 1-Dichloroethane <1.0 <10 1.3 <1.0 <2.0 <2.0 <1.0 <1.0
I ,'t-Dichloroethene 7 <10 <10 1.2 1.6 0.91DJ <2.0 <1.0 <1.0
.. cis-1,2-Dichloroethene 70 180 170 I 32· 26 72 93 I <1.0 5,8
trans-1,2-Dichloroethene 70 <1.0 <10 2.0 1.4 <2.0 <2.0 <1.0 <1.0
2-Hexanone <100 <100 <10 <1.0 <20 <2.0 <10 <1.0
4-Methyl-2-pentanone <100 <100 <10 <1.0 <20 <2.0 <10 <1.0
Tetrachloroethene 0.7 I 770 !,SOOD 2600 190 3900 4700 <1.0 27
I, I, !-Trichloroethane 200 <1.0 <10 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0
Trichloroethene 2.8 8,400D 13,000D 97 84 47 46 <1.0 3.4
Vinyl Chloride 0.015 18 <10 2.9 <1.0 <1.0 <2.0 <1.0 <1.0
~
(USEPA Method 9010)
Total 154 NS 20 NS 20 NS <5.0 NS <5.0
Amenable NS <5.0 NS <5.0 NS <5.0 NS <5.0
Notes:
All results reported in micrograms per liter (µg/L)
< Compound was not detected above the quantitation limit.
J Compound concentration is qualified as estimated.
D Compound was quantitated using a secondary dilution factor.
CompollllCl concentration is qualified as estimated because the field replicate sample criteria were not met. • Field replicate of groundwater sample CMMW-04 .
NS Wells not sampled for the indicated parameters.
G.\Env\JfDCHANNINC0202. 170\0 REPORTS\Semi_Mnual_Repolbeml-2000 _Rev .xis
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ARCADIS GERAGHTY&MILLER
Table 3-3. Air Stripper Influent Quality Data Summary, JFD Electronics/Channel Master Site, Oxford, North Carolina.
Sample Name:
Sample Date:
Lab ID:
Yolatile 0:rgaDic Qlmpmmds
(USEPA Method 8260)
Acetone
Benz.ene
Carbon disulfide
Carbon tetrachloride
Chlorobenz.ene
Chloroform
1, 1-Dichlorocthane
l, 1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichlorocthene
2-Hexanone
4-Methyl-2-pcntanone
Tetrachloroethene
I, I, I-Trichloroethane
Trichloroethene
Vinyl Chloride
Me!aJ.s
(USEPA Method 60 I 0)
Chromium
Nickel
Copper
~
(USEPA Method 9010)
Total
Amenable.
Notes:
Influent
4/18/2000
02502
<250
<IO
<10
<IO
<IO
<IO
<10
<IO
74
<10
<100
<100
410
<IO
3,400D
7.IDJ
NA
NA
NA
NA
NA
All results reported in micrograms per liter (µg/L)
Influent
4/25/2000
02663
<620
<25
<25
<25
<25
<25
<25
<25
48
<25
<250
<250
280
<25
3,600
<25
NA
NA
NA
NA
NA
< Compound was not detected above the qnantitation limit.
J Compound concentration is qnalified as estimated.
D Compound was qnantitated using a secondary dilution factor.
Influent
5/2/2000
02852
<620
<25
<25
<25
<25
<25
<25
<25
55
.<25
<250
<250
370
<25
5,100
<25
NA
NA
NA
NA
NA
Influent
5/9/2000
03010
<1,200
<50
<50
<50
<50
<50
<50
<50
69
<50
<500
<500
430
<50
4,600
<50
NA
NA
NA
NA
NA
Influent
7/25/2000
04927-3
<I,200
<50
<50
<50
<50
<50
<50
<50
82
<50
<500
• <500
590
<50
5,000
<50
NA
NA
NA
NA
NA
Compound concentration is qualified as estimated because the field replicate sample criteria were not met.
NA Compound was not analyzed.
G;\Env\JFDCHANNV-IC0202.170\0 REPORTS\Semi_Annual_R11pa,t\seml-2000_Rev .xis
Influent
10/11/2000
07009-7
<250
<10
<10
<10
<IO
<10
<10
<10 .
83
<10
<100
<100
620
<10
4,700D
<10
NA
NA
NA
7.7
<5.0
...
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ARCADIS GERAGHTY&MILLER
Table 3-4. Summary of Groundwater Remediation System Effluent Monitoring Results, JFO Electronics/Channel Master Site, Oxford, North Carolina.
PARAMETER Pl<:RMIT LIMITS SAMPLING DATES
DaUy Malimum
04/18/00 04/25/00 0S/02/00 OS/09/00 OS/16/00 05123/00 05/30/00 06/06/00 06/13/00
Yoh11ilc O[i:anii: Ccmiurnods (11 i:ll )
(USEPA Method 8260)
T etrachloroethy Jene <1.0 <1.0 <1.0 <LO <1.0 <LO <1.0 <1.0 <1.0 1,1 Dichloroclhane <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <LO <1.0 <1.0 Cis-1,2 Dichlorocthanc <1.0 <LO <l.0 <1.0 <l.0 <1.0 <1.0 <1.0 <1.0
Ch lorn benzene <l.0 <1.0. <1.0 <LO <1.0 <LO <1.0 <1.0 <LO Toluene <LO <1.0 <1.0 <1.0 <1.0 <LO <1.0 <1.0 <1.0
1,1-Dichlomethylene <1.0 <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Trans-1,2 Dichloroethylenc <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <LO <1.0 Trichloroethene <LO <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 Vinyl Chloride <LO <1.0 <1.0 <LO <LO <l.0 <1.0 <LO <1.0
Cvanidc frnra >
(USEPA Method 9010)
Total Cy'anidc: 0.0S 0.019 0.01S 0.0079 0.013 0.012 0.013 0.014 0.0081 0.011
Mctalsfrnitn\1
(US EPA Method 6010)
Barium NA NS NS 0.026 NS NS NS NS NS NS Chromium NA NS NS <O.Oto NS NS NS NS NS NS Lou! NA NS NS <0.00S0 NS NS NS NS NS NS Copper NA NS NS <0.020 NS NS NS NS NS NS Nickel NA NS NS <0.040 NS NS NS NS NS NS Zinc NA NS NS <0.020 NS NS NS NS NS NS
field Mcas:m:i::mcols
Daily Average Flow {MGD) 0.040 0.023 0.026 0.026 0.022 0.Q2S 0.027 0.02S 0.022 0.028 pH (SU) S.0 to l0.0 7.72 7.1S 6.34 6.36 6.41 8.10 7.66 8.20 6.88 Temperature ("C) 40 IS.4 14.8 16.S 17.7 19.0 21.6 17.8 19.2 20.9
Notes;
No Daily Maximum Indicated.
MGD Million Gallons per day.
µg/L Micrograms per liter.
mg/L Milligrams per liter.
SU Standard Units.
"C Degrees Centigrade.
< Compound was not detected above the quantitation limiL
YTD Year-to-date, YTD averages arc arithmetic averages.
J Qualified as estimated.
NA Not Applicable.
NS Not Sampled.
One time: metals analysis were based on a request by USEPA.
G~~C02J?.11'0\0 ftfl'ORTS\Sem_-~:ltal_Rw.>'.111 Page I or2
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ARCADIS GERAGHTY&MILLER
Table 3-4. Summary of Groundwater Remediation System Discharge Monitoring Results, JFD Electronics/Channel Master Site, Oxford, North Carolina.
PARAMETER PERMIT LIMITS SAMPLING DATES
Dally J\fn:imum
06/20/00 06(27/00 07/03/00 07/11/00 07118/00 07/25/00 08/16/00 09/11/00 10/J 1/00
~ola1ilc Quon ii:: Comgonads (ui;Q l
(USEPA Method 8260)
T ctrach lorocthylene <1.0 <1.0 <1.0 <1.0 <LO <LO <1.0 <1.0 <1.0 1,1 Dichloroetbane <1.0 <1.0 <1.0 <LO <1.0 <1.0 <1.0 <1.0 <LO Cis-1,2 Dichloroethanc <1.0 <1.0 <1.0 <LO <1.0 <1.0 <LO <1.0 <1.0
Chl9robenzene <LO <1.0 <1.0 <1.0 <1.0 <1.0· <LO <1.0 <1.0 Toluene <LO <LO <LO <1.0 <1.0 <1.0 <1.0 <l.0 <1.0
I, 1-Dichlorocthylenc <1.0 <1.0 <1.0 <l.0 <LO <LO <1.0 <1.0 <1.0 Trans-1,2 Dichloroethylene <l.0 <1.0 <1.0 <1.0 <1.0 <LO <LO <1.0 <1.0 Trichloroethene <1.0 <1.0 <LO <LO <1.0 <1.0 <LO <1.0 <1.0 Vinyl Chloride <LO <LO <1.0 <1.0 <LO <1.0 <1.0 <LO <1.0
Cyanide CrnvD l
(USEPA Method 9010)
Total Cyanide 0.0S 0.0089 o.01ru 0.012 0.011 0.0110 0.0099 0.011 0.0066 0.0068
Metals (mgD >
(USEPA Method 6010)
Barium NA NS NS NS NS NS NS NS NS NS Chromium NA NS NS NS NS NS NS NS NS NS L~d NA NS NS NS NS NS NS NS NS NS Copper NA NS NS NS NS NS NS NS NS NS Nickel NA NS NS NS NS NS NS NS NS NS Zinc NA NS NS NS NS NS NS NS NS NS
Field MeaSJU:cmenrs
Daily Average Flow (MGD) 0.040 O.D21 0,025 0.028 o.ozs 0.024 0.023 0.023 0.022 0.022 pH (SU) S.0 to 10.0 8.27 8.33 7.30 7.13 7.99 8.51 NA NA 6.63 Tempera~ ("C) 40 19.S 22.3 20.7 21.3 19.8 18.9 NA NA 17.8
Notes:
· No Daily Maximum Indicated.
MGD Million Gallons per day.
µg/L Micrograms per liter.
mg.IL Milligrams per liter.
SU Standard Units.
"C Degrees Centigrade.
< Compound was not detected above the quantitation limit.
YTD Year-to---date, YTD averages arc arilhmetic averages.
Qualified as estimated.
NA Not Applicable.
NS Not Sampled.
One time metals analysis were based on a request by USEPA.
0,1E.r.Nf'Dc:HANN'INC0202.170IO!IEPOOTS\Seml_"""""2_11_200Q_flo,i•la Page2of2
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ARCADIS GERAGHTY&MILLER
Table 3-5. Summary of Extraction System Flow Rates, JFD Electronics/Channel Master, Oxford, North Carolina.
PWI PW2 PW3 PW4 Influent
Total Reported Calculated Total Reported Calculated Total Reported Calculated Total Reported Calculated Total Reported Calculated
Date Gallons Flow Flow Gallons Flow Flow Gallons Flow Flow Gallons Flow Flow Gallons Flow Flow
4/18/2000 149898 5.8 39488 1.8 48535 1.8 154139 8 402987 17
4/25/2000 210140 6 6.0 55608 1.6 1.6 65516 1.6 1.7 232106 7.4 7.7 575432 17 17.1
51912000 323017. 6.0 5.6 83480 2.0 1.4 98481 2.0 1.6 386829 8.0 7.7 906854 18.0 16.4
5/16/2000 385837 6.0 6.2 83490 2.0 0.0 119721 2.0 2.1 466440 8.0 7.9 1088028 18.0 18.0
5/23/2000 445635 6.0 5.9 99228 2.0 1.6 138216 2.0 1.8 541074 8.0 7.4 1258679 18.0 16.9
6/6/2000 567254 6.0 6.0 130337 1.6 1.5 175194 2.0 1.8 692910 7.8 7.5 1604398 17.0 17.1
6/14/2000 634506 6.0 5.8 147050 2.0 1.5 196016 2.0 1.8 779165 8.0 7.5 1797755 18.0 16.8
6/20/2000 683328 6.0 5.7 159169 1.8 1.4 2111:45 2.0 1.8 842132 8.0 7.3 1939440 NM 16.4
6/27/2000 742755 6.0 5.9 176919 2.0 1.8 234235 1.8 2.3 918910 8.0 7.6 2117700 18.0 17.7
7/3/2000 792554 6.0 5.8 191060 2.0 1.6 253728 2.0 2.3 983500 8.0 7.5 2267510 18.0 17.3
7/11/2000 859371 6.0 5.8 209455 2.0 1.6 278865 1.8 2.2 1070482 7.9 7.6 2467292 17.0 17.3
. 7/18/2000 917334 6.0 5.8 224576 0.8 1.5 297427 2.0 1.8 1146122 7.2 7.5 2636749 16.0 16.8
7/25/2000 973737 6.0 5.6 230023 0.8 0.5 315564 1.9 1.8 1219384 7.6 7.3 2791610 16.0. 15.4
8/11/2000 1113800 NM 5.7 255490 NM 1.0 363120 NM 1.9 1397940 NM 7.3 3 I 88720 NM 16.2
8/16/2000 1155390 5.41 5.8 265290 1.26 1.4 3771 IO 1.89 1.9 1449630 6.79 7.2 3307310 . 16.53 16.5
8/25/2000 1222980 5.63 5.2 272590 NF 0.6 398750 1.67 1.7 1531660 6.04 6.3 3490170 15.0 14.1
9/11/2000 1367866 6.0 5.9 306115 1.5 1.4 442751 2.0 1.8 1686713 6.0 6.3 3873653 15.5 15.7
10/11/2000 1619389 NM 5.8 362833 NM 1.3 520440 NM 1.8 1952998 NM 6.2 4532943 15.5 15.3
Notes:
NM Not Measured.
NF No now registered,
Aow nitc in gallons pa day
Totalizer on the Recovery well PW-2 was not functioning on 5/J 6/00, but the pump was operating (low flow). The totalizer began registering flow ofter the pump was re,tartcd.
0:1Env'.!FDCHANN\NC0202. 170\0 REPORTS\Seml_Annuoll_ Roport\Mmi-2000_R.,.,.xls
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ARCADIS GERAGHTY&MILLER
Semiannual
Groundwater
· Remediation Report
Figures
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ARCADIS GERAGHTY & MILLER
OXFORD
PRINTING
2301 Re)(woods Drive of North Carolina, Inc.
Suite 102 RALEIGH, NC 27607
Tel: [phone] fax, 919/782-5905
PR.Ji MANAGER,
N. SHETTY
"
CHECKED BY•
A. HARTMAN
REFERENCE: BECHTEL FIGURE 1-3 FS REPORT, APRIL 1992.
0 IEIIEICE!l!H!l/iC:==::JI 200 FEET
0
CMMW20
DRAf"TER:
A. NORTON
DRAIJING,
G\./-PS-2000
DAT[,
OlFEBOI
(3CMMW21
-24
I@
CMMW22
0
CMMW22A
PROJECT NUMBER, NC000202.0170
JFD ELECTRONICS/CHANNEL MASTER
OXFORD, NORTH CAROLINA
I
. ---PW-41,.
,--,y ~'
PW-1 .A.
OW-1 [:.iii
N
0 CMMW21--,--
LEGEND
FENCE ~
FENCE 0
CULVERT 0
DRAINAGE CREEK • PROPERTY LINE --. TREE LINE 81
RAILROAD NM
PUMPING WELL CMMW01
OBSERVATION WELL
· SITE LAYOUT
SHALLOW WELL
INTERMEDIATE WELL
SHALLOW BEDROCK WELL
DEEP BEDROCK WELL
TOP OF ROCK WELL
ABANDONED WELL
NOT MEASURED
RI WELL/RD WELL
FIGURE;
1-1
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OXFORD
PRINTING
2301 Rnw0ods 0,-1..,. of North Carolina, Inc.
Sult• 102 RALtlGH, NC 2?i!i0?
l.t1 9191782·5511 fax[phone]·590,
CHECKED BY•
A. HARTMAN
REFERENCE: BECHTEL FIGURE 1-3
FS REPORT, APRIL 1992.
0 lmllllla:===:::i 200 FEET
"-
DRAFTER•
A. NORTON
DRA\JING,
G\./-PS-2000
DAT[,
Olf"EBOI
PROJECT NUMBER• NC000202.0170
JFO ELECTRONICS/CHANNEL MASTER
OXFORD, NORTH CAROLINA
PW-1
OW-1
458.14
N
~ ~
FENCE
FENCE
CULVERT
DRAINAGE CREEK
PROPERTY LINE
TREE LINE
RAILROAD
PUMPING WELL
OBSERVATION WELL
GROUNDWATER
ELEVATION (FT/MSL)
SHALLOW WELL
INTERMEDIATE WELL
SHALLOW BEDROCK WELL
DEEP BEDROCK WELL
TOP OF ROCK WELL
ABANDONED WELL
NM · NOT MEASURED
CMt,,1W01 RI WELURD WELL
_ 448 GROUNDWATER CONTOUR
-(FT/MSL)
GENERALIZED GROUNDWATER
FLOW DIRECTION
flGURE:
GROUNDWATER
POTENTIOMETRIC SURFACE
APRIL 3, 2000 2-1
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ARCADIS GERAGHTY & MILLER
2301 Rexwooels Dr!Ve of North Carolina,Jnc.
Suite 102 RALEIGH, NC 27607
Tet, 9!91782-5511 fo.x, 9191782-5905
PRJT MANAGER,
N. $HETTY
CHECKED BY,
A. HARTMAN
REFERENCE: BECHTEL FIGURE 1-3
FS REPORT, APRIL 1992.
0 •C!ia::::==::i 200 FEET
DRAFTER,
A. NORTON
DRA\JING,
GIJ-PS-2000
DATE,
0lFEB0I
PROJECT NUMBER: NC000202.01 70
JFD ELECTRONICS/CHANNEL MASTER
OXFORD, NORTH CAROLINA
OW-1 [;iii
458.14
TREE LINE
RAILROAD
PUMPING WELL
OBSERVATION WELL·
GROUNDWATER
ELEVATION (FT/MSL)
N
0
0
NM
SHALLOW WELL
·INTERMEDIATE WELL
SHALLOW BEDROCK WELL
DEEP BEDROCK WELL
TOP OF ROCK WELL
ABANDONED WELL
NOT MEASURED
CMMW01 RI WELURD WELL
_ 448 GROUNDWATER CONTOUR
-(FT/MSL) ..
GENERALIZED GROUNDWATER
FLOW DIRECTION
FIGURE:
GROUNDWATER
POTENTIOMETRIC SURFACE
JULY 24, 2000 2-2
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CONCRETE
PAD
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Cle'.
/ 0
>-Cle'.
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ti ::,
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} I
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~/
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ARCADIS GERAGHTY & MILLER
2301 Rexwoods Drive of North Carolina, Inc.
Suite 102 RALEIGH. NC 27607
Tel: 9!91782-5511 f"ox• 9191782-5905
'I
X I
PRJT MANAGER,
N. SHETTY
CHECKED BY,
A. HARTMAN
REFERENCE: BECHTEL FIGURE 1-3 FS REPORT, APRIL 1992.
0 •!l!Za:==:i 200 FEET
DRAFTER,
A. NORTON
DRAVING,
G\./-PS-2000
DATE:
OIF"EBOI
PROJECT NUMBER, NC000202.0170
JFD ELECTRONICS/CHANNEL MASTER
OXFORD, NORTH CAROLINA
,.._,y \---v-vY \
PW-1 ...
OW-1 I.iii
458.14
TREE LINE
RAILROAD
N
PUMPING WELL
OBSERVATION WELL
GROUNDWATER
ELEVATION (FT/MSL)
0
0
NM
SHALLOW WELL
INTERMEDIATE WELL
SHALLOW BEDROCK WELL
DEEP BEDROCK WELL
TOP OF ROCK WELL
ABANDONED WELL
NOT MEASURED
CMMW01 RI WELURD WELL
_ 448 _ GROUNDWATER CONTOUR
. (FT/MSL)
GENERALIZED GROUNDWATER
FLOW DIRECTION
FIGURE:
GROUNDWATER
POTENTIOMETRIC SURFACE
OCTOBER 9, 2000 2-3
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ARCADIS GERAGHTY&MILLER
Semiannual
Groundwater
Remediation Report
Appendix A
Analytical Reports
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com ·
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
OE(: 2 ' 1!100
STL Savannah
LOG NO: SB-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#18869
Sampl_ed By: Client
Code: 152501226
REPORT OF RESULTS Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
-----------------------------------------------------------------------------------
85311-1 EF-1 09-02-98/1330
-----------------------------------------------------------------------------------
PARAMETER 85311-1
·------------------------------------------------- ---------- --------------------
Cyanide (335.2)
Cyanide, mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cyanide (Amenable)
Cyanide (Amenable), mg/1
Preparation Date
Date Analyz!;d
Dilution factor
Batch ID
Iron (6010)
Iron, mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
· Dilution Factor
Analysis Date
Batch ID
0.022
09.04.98
09.04.98
1.0
0904S
<0.0050
09.04.98
09.04.98
1.0
0904S
6.5
09.03.98
09.05.98
1.0
0903H
1.0
09.05.98
0903H ----------------------------- ------ ---- ------ ---- ---------- -----.------------. --
STL Savannah is a part of Severn Trent Laboratories, Inc.
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • ~ax: 912 352 0165 • www.stl-inc.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
STL Savannah
LOG NO: S8-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#18869
Sampled By: Client
Code: 152501226
REPORT OF RESULTS Page 2
DATE/
Lo'G NO SAMPLE DESCRIPTIO_N , LIQUID SAMPLES TIME SAMPLED
---------- ------------ ----·------------------------ - - ---- ---------------------------
85311-1 EF-1 09-02-98/1330
---------- -------------------------- -- -------- -------------------------------------
PARAMETER 85311-1
--------------------------------------- ----------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Ac:etone, ug/1
Carbon disulfide, ug/1
1, 1-Dichloroethene, ug/1-
1, l-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Vinyl acetate, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1;3-Dichloropropene, ug/1
Trichloroethene, ug/1
STL Savan11ah is a part of Severn Trent Laboratories, Inc.
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
1.3
<l.0
<1.0
<1.0
<10
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
<1.0
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
~-
STL Savannah
LOG NO: SS-85311
Received: 03 SEP 98
·Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#18869
Sampled By: Client
Code: 152501226
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
-----------------------------------------------------------------------------------
85311-1 EF-1 09-02-98/1330
-----------------------------------------------------------------------------------
PARAMETER 85311-1
------------------------------------------------- -------------------- ----------
Dibromochloromethane, ug/1 <1.0
1,1,2-Trichloroethane, ug/1 <1.0
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
2-Chloroethylvinyl ether, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total,_ ug/1
Surrogate Toluene-de
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane.
Date Analyzed
<1.0
<1.0
<10
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
100 %
110 %-
100 %-
09.04.98
Dilution factor 1.0
Batch ID 1B0904
Dilution Factor 1.0
Analysis Date 09.04.98
Batch ID 1B0904
-------------------------------------------------------------------------------
STL Savannah is a part of Severn Trent Labora,tories, Inc.
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, ·Inc.
P.O. Box·31388
Raleigh, NC 27.612
~
STL Savannah
LOG NO: S8-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No;: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#18869
Sampled By: Client
Code: 152501226
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
------------------ -------------------- --·----------
DATE/
TIME SAMPLED
85311-1 EF-1 09-02-98/1330
Page 4
-----------------------------------------------------------------------------------
PARAMETER 85311-1
------------------------------------------------- -------------------- ----------
Turbidity (180.1)
Turbidity, NTU 86
Preparation Date
Date Analyzed
Dilution factor
Batch ID
09.11.98
09.11.98
10
0911A
------------------------------------------------- ------------------------------
STL Savannah is a part of Severn !rent ~boratories, Inc.
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
~~
STL Savannah
LOG NO: S8-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#18869
Sampled By: Client
Code: 152501226
REPORT OF RESULTS
LOG NO
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
85311-2
85311-3
85311-4
·PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
. -----------------------------
Cyanide (335.2)
Cyanide, mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Cyanide (Amenable)
Cyanide (Amenable), mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Iron (6010)
Iron, mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Dilution Factor
Analysis Date
Batch ID
85311-2
<0.0050
09.04.98
09.04.98
1.0
0904S
<0.0050
09.04.98
09.04.98
1.0
0904S
<0.050
09.03.98
09.05.98
1.0
0903H
1.0
09.05.98
0903H
----------
STL Savannah is a part of Severn Trent Laboratories, Inc.
85311-3
93 %
09.04.98
09.04.98
1.0
0904S
105'<
09.03.98
09.05.98
1.0
0903H
1.0
09.05.98
0903H
----------
Page 5
85311-4
85-115 %-
75-125 %
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com
Mr. Nanjun Shetty
,.ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
~
sn Savannah
LOG NO: S8·85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#18869
Sampled By: Client
·code: 152501226
REPORT OF RESULTS
LOG NO
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
--------- ---------------------------------------------------
85311·2 Method Blank
85311·3 Lab Control Standard% Recovery
85311·4 LCS Accuracy Control Limit (%R)
--------------------------------------------------
PARAMETER 85311·2 85311·3
Page 6
85311·4 --------------------------------------- ----------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide.;. ug/1
1,l·Dichloroethene, ug/1
1,l·Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans• 1, 2 ·_Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2·Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Vinyl acetate, ug/1
Bromodichlor_omethane, ug/1
l,1,2,2·Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
--------------------------------------- ----------
STL Savannah is a part of Severn Trent Laboratories, Inc.
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0 85 % 38·155 %
<1.0
<1. o
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<2.0
<1.0
<1.0
<1.0
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
p_o_ Box 31388
Raleigh, NC 27612
LOG NO: SS-85311
Received: 03 ·sEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO~l8869
Sampled By: Client
Code: 152501226
REPORT OF RESULTS
LOG NO
85311-2
85311-3
85311-4
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
2-Chloroethylvinyl·ether, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-de
Surrogate -4-Bromofluorobenzene
Surrogate -Dipromofluoromethane
Date Analyzed
Dilution factor
Batch ID
Dilution Factor
Analysis Date
Batch ID
85311-2
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<10
<10
<1.0
<1.0
<1.0
<l. 0
<1.0
<2.0
100 %
110 %
97 %
09.04.98
85311-3
100 %
95 %
100 %
98 %
93 %
100 %
87 %
09.04.98
1.0 1.0
1B0904 1B0904
1.0
09.04.98
1B0904
STL Savannah is a part of Severn Trent Laboratories, Inc.
Page 7
85311-4
10-213 %-
52-143 %
76-128 %
60-127 %-
67-134 %-
67-132 %-
64-142 %-
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
STL Savannah
LOG NO: S8-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/0xford/JFD Electronics»Channel Master/T0#18869
Sampled By: Client
Code: 152501226
REPORT OF RESULTS
LOG NO
DATE/
SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------
85311-2 Method Blank
, 85311-3 Lab Control Standard t Recovery
85311-4 LCS Accuracy Control Limit (tR)
-----------------------------·---------------------
PARAMETER 85311-2 85311-3
Page 8
85311-4 --------------------------------------- ------------------------------ ----------
Turbidity (180.1)
Turbidity, NTU
Preparation Date
D.ate Analyzed
Dilution factor
Batch ID
<0.10
09.11.98
09.11.98
1.0
0911A
100 t 90-110 t
----------------------------------------------------------- --------------------
STL Savannah is a part of Severn Trent Laboratories, Inc.
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
.Raleigh, NC 27612
~
STL Savannah
LOG NO: S8-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#l8869
Sampled By: Client
Code: 152501226
LOG NO
85311-5
85311-6
85311-7
85311-8
85311-9
REPORT OF RESULTS
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
Matrix Spike%-Recovery (Batch)
Matrix Spike Duplicate%-Recovery (Batch)
MS Accuracy Advisory Limit (%-R)
Precision (%-RPO) MS/MSD
MS Precision Advisory Limit (%-RPO)
Page 9
-·--------- ------------------------ ------------------- ------- -----------------------
PARAMETER
Cyanide (335.2)
Cyanide, mg/1
Preparation Date
Date Analyzed
Dilution factor
Batch ID
Iron (6010)
Iron,
Preparation Date
Date Analyzed
Dilution factor
Batch ID
85311-5
----------
91 %-
09.04.98
09.08.98
1.0
0904S -
109 %-
09.03.98
09.05.98
1.0
0903H
85311-6 85311-7
--------------------
128 %-75.-125 %-
09.04.98
09.08.98
1.0
0904S
110 % ?5-125 %-
09.03.98
09.05.98
1.0
0903H
STL Savannah is a part of Severn Trent Laboratories, Inc.
85311-8 85311-9
34 %-<30 %-
0.91 %-<20 ,\-
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com
Mr. ·Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
~
STL Savannah
LOG NO: SS-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202 .160/Oxford/JFD Electroni_cs»Channel Master /TO#18869
Sampled By: Client
Code: 152501226
LOG NO
REPORT OF RESULTS
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
Page 10
-----------------------------------------------------------------------------------
85311-5
85311-6
85311-7
85311-8
85311-9
Matrix Spike% Recovery (Batch)
Matrix Spike Duplicate% Recovery (Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
MS Precision Advisory Limit (%RPO)
-----------------------------------------------------------------------------------
PARAMETER 85311-5 85311-6 85311-7 85311-8 85311-9
--------------------------------------- ------------------------------ ----------
Volatiles by GC/MS (8260)
1,1-Dichloroethene
Trichloroethene
Benzene
Toluene
Chlorobenzene
Surrogate Toluene-dB
130 %
210 %
110 %
110%
120 %
100 %
Surrogate -4-Bromofluorobenzene 110 %
Surrogate -Dibromofluoromethane 110 %
Date Analyzed 09.04.98
Dilution factor 1.o"
Batch ID 1B0904
97 % 38-155
180 %-10-213
96 %-52-143
·100 %-76-128
100 % 60-127
100 %-67-134
110 %-67-132
100 %-64-142
09.04.98
1.0
1B0904
----------
STL Savannah is a part of Severn Trent Laboratories, Inc.
%-
%
%-
%
%
%
%-
%-
29 %-
35 %-
14 %-
10 %
18 %
<25 %-
<40 %-
<31 %-
<25 %-
<25 %-
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~
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
LOG NO
85311-5
85311-6
85311-7
85311-8
85311-9
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S8-85311
Received: 03 SEP 98
Reported: 08 SEP 98
Contract No.: JFD Channel Master
Project: NC000202.160/Oxford/JFD Electronics»Channel Master/TO#l8869
Sampled By: Client
Code: 152501226
REPORT OF RESULTS
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
.Matrix Spike% Recovery (Batch)
Matrix Spike Duplicate% Recovery (Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%RPD)
Page 11
---------- ------- - - ----------------------------------------- ---------------- - ------
PARAMETER 85311-5
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
85311-6 85311-7 85311-8 85311-9
Per client request, turbidity was performed on a sample aliquot preserved with
NaOH.
Batch MS/MSD for cyanide analysis was not performed on an ARCADIS sample. The
sample utilized was reported as 281 mg/1. MS result was 735 mg/1, MSD result
was 923 mg/1, and expected value for MS/MSD was 500 mg/1.
Amenable cyanide was analyzed by method 335.2.
STL Savannah is a part of Severn Trent Laboratories, Inc.
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RECRlVl{D
APR Z 4 2000 Sa v,a'n,n·a h
t.abar.itor:'ies .5102 LaRoche Avenue • Savannah, GA 31404 • (912) 354-.7858 '. Fax [phone] • www.stlsavlab.com
.. C.H..,,.~..,!~. :~--lue,HLj &Nti:tie.G NO: S0-02218
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
"P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------ --------------------------------------------------
02218-1 CMMW-24,;
02218-2 CMMW-23-
02218-2-DL CMMW-23
02218-3 CMMW-21-
02218-4 CMMW-20-
- - - - - - - -':' - - - - - --.= - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
04-_03-00/16:20
04-03-00/17:00
04-03-00/17:00
04-04-00/09:30
04-04-00/09:40
PARAMETER 02218-1 02218-2 02218-2-DL 02218-3 02218-4 ---------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <1.0
Bromomethane (Methyl <1. 0
bromide), ug/1
Vinyl chloride, ug/1 <1. 0
Chloroethane, ug/1 <1.0
Methylene chloride <5. O
(Dichloromethane), ug/1
Acetone, ug/1 <25
Carbon disulfide, ug/1 <1. 0
1,1-Dichloroethene, ug/1 <1.0
1,1-Dichloroethane, ug/1 <1.0
cis-1,2-Dichloroethene, ug/1 1.2
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <1.0
2 -Butanone (MEK) , ug/1 <10
1,1,1-Trichloroethane, ug/1 <1.0
Carbon tetrachloride, ug/1 <1.0
<1.0
<l_. 0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
68
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<2.0
<2.0
<2.0
<2.0
<10
<50
<2.0
<2.0
<2.0
71D
<2.0
<2.0
<2.0
<20
<2.0
<2.0
<5.0
<5.0
<5.0
<5.0
<25
<120
<5.0
<5. 0
<5.0
300
<5.0
<5.0
<5.0
<50
<5.0
<5.0
<10
<10
<10
<10
<50
<250
<10
38
<10
36
<10
10
<10
<100
<10
<10
s:a.v~a n,n·a· h
l!::abOr'atorit?s 51021..aRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] • www.sclsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr: Mark Radecke
REPORT OF RESULTS
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l90.000l
Sampled By: Client
Code: 121300419
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------ -------------------------------------------------- ----------------------
02218-l
02218-2
02218-2-DL
02218-3
02218-4
CMMW-24
CMMW-23
CMMW-23
CMMW-21
CMMW-20
PARAMETER 02218-l 02218-2 02218-2-DL
-------------------------------------------------
Brornodichlorornethane, ug/1
l,l,2,2-Tetrachloroethane, ug/1
l,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibrornochlorornethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Brornoforrn, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluorornethane
Dilution Factor
<l.0
<l.0
<l.0
<l.0
l. 7.
<l.0
<l.0
<l.0
<l.0
<l.0
<10
<10
4.2
<l.0
<l.0
<l.0
<l.0
<2.0
106 %
102 'Ir
108 %
<l.0
<l.0
<l.0
<l.0
42
<l.0
<l.0
<l.0
<l.0
<l.0
<10
<10
370E
<l.0
<l.0
<l.0
<l.0
<2.0
104 %
98 'Ir
106 %-
l l
Analysis Date
Batch ID
04.12.00 04.12.00
lA0412 lA0412
----------
<2.0
<2.0
<2.0
<2.0
40D
<2.0
<2.0
<2.0
<2.0
<2.0
<20
<20
330D
<2.0
<2.0
<2.0
<2.0
<4 .0
104 %
100 %
112 %
2
04.12.00
1A0412
----------
04-03-00/16:20
04-03-00/17:00
04-03-00/17:00
04-04-00/09:30
04-04-00/09:40
02218-3 02218-4
--------------------
<5.0 <10
<5.0 <10
<5.0 <10
<5.0 <10
120 70
<5.0 <10
<5.0 <10
<5.0 <10
<5.0 <10
<5.0 <10
<50 <100
<50 <100
730 1300
<5.0 <10
8.0 <10
<5.0 <10
<5.0 <10
<10 <20
.104 % 104 %
100 % 98 %
114 % 108 %
5 10
04.12.00 04.12.00
1A0412 1A0412
--------------------
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s,.:a~vJ_?i:n:ri:~a-h l:abor:atories 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
Received: 06 APR 00
Reported: 18 APR 00
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LT0#032800-C
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------ ------------------------------------------------ --
02218-5 CMMW-19-
02218-6 CMMW-26,,.-
02218-7 CMMW-07~·
02218-8 CMMW-17,
02218-9 CMMW-15,.
04-04-00/12:40
04-04-00/15:45
04-05-00/09:45
04-05-00/10:10
04-05-00/11:15
------------------------------------------------------------------------------------------
PARAMETER 02218-5
---------------------------------------
Volatiles by GC/MS (8260)
·chloromethane, ug/1 <1.0
Bromomethane (Methyl <l.O
bromide) , ug/1
Vinyl chloride, ug/1 <l. O
Chloroethane, ug/1 <1.0
Methylene chloride <5.0
(Dichloromethane), ug/1
-Acetone, ug/1 <25
Carbon disulfide, ug/1 <l. o
1,1-Dichloroethene, ug/1 <l.O
1,1-Dichloroethane, ug/1 <l.0
cis-1,2-Dichloroethene, ug/1 2.6
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <l.O
2 -Butanone (MEK) , ug/1 <10
02218-6
<l.0
<1.0
1.5
<1.0
<5.0
<25
<1.0
<1.0
<1.0
180
5.0
<1.0
<l.O
<10
02218-7
<2.0
<2.0
<2.0
<2.0
<10
<50
<2.0
<2.0
<2.0
120
<2.0
<2.0
<2.0
<20
02218-8
<l.0
<l.0
<1.0
<l.0
<5.0
57
2.3
<1.0
<1.0
4.3
<1.0
<1.0
<l.0
<10
02218-9
<2.5
<2.5
<2.5
<2.5
<12
<62
<2 .5
<2.5
<2.5
13
<2.5
<2.5
<2.5
<25
1,1,l-Trichloroethane, ug/1 <1.0 <l.O <2.0 <l.0 <2.5
Carbon tetrachloride, ug/1 <1.0 <1.0 <2.0 <1.0 <2.5
Sa v1.i1n·1n a•h ~abo~ratCJri'eS ................. , .... ..__. .... 5102 I.a.Roche Avenue • Savannah, GA 31404 • [phone] • Fa..'C [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LT0#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
Page 4
DATE/
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
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-------------------------------------- ------------ ------------------ -- --------------------
02218-5
02218-6
02218-7
02218-8
02218-9
CMMW-19
CMMW-26
CMMW-07
CMMW-17
CMMW-15
04-04-00/12:40
04-04-00/15:45
04-05-00/09:45
04-05-00/10:10
04-05-00/11:15
I
I ------------------ ---------- ------------- --------------------------- ----------------------
PARAMETER 02218-5
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-de
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<1.0
<1.0
<1.0
<1.0
18
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
67
<1.0
<1.0
<1.0
<1.0
. <2. 0
. 104 %
100 '!r
108 '!r
1
Analysis Date
Batch ID
04.12.00
1A0412
02218-6 02218-7
--------------------
<1.0 <2.0
<l.0 <2.0
<l.O <2.0
<1.0 <2.0
12 320
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<10 <20
<10 <20
180 41
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<1.0 <2.0
<2.0 <4. 0
104 %-106 %-
100 %-102 %-
104 %-106 %-
1 2
04.12.00 04.12.00
1A0412 1A0412
--------------------
02218-8
----------
<1.0
<1.0
<1.0
<1.0
14
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
7.6
<1.0
<1.0
<1.0
<1.0
<2.0
104 %-
100 %-
108 %-
1
04.12.00
1A0412
----------
02218-9
----------
<2. 5
<2.5
<2. 5
<2.5
390
<2.5
<2.5
<2. 5
<2. 5
<2. 5
<25
<25
26
<2. 5
<2.5
<2.5
<2.5
<5.0
106 %-
98 %-
108 %-
2.5
04.12.00
1A0412
----------
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s·a·v~a'n n,a-h
C'aliarafOries 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fa..'! [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
G NO: S0-02218
Received: 06 APR 00
Reported: 18 APR 00
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LT0#032800-C
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sample9 By: Client
Code: 121300419
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------ -------------------------------------------------- ----- -----------------
02218-10 FIELD BLANK-1 -04-04-00/14 :45
02218-11 TRIP BLANK-1 , 04-03-00
---- ------------------------------ --------------------------------------------------------
PARAMETER 02218-10 02218-11
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroet_hene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<l. o
1,1,2,2-Tetrachloroethane, ug/1 <1.0
1,2-Dichloropropane, ug/1 <1.0
<1.0
<l.0·
<l.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
Savannah
t:.abOr"atCiri'es 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LTO~032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------- ----- ------------------------------------------------------------------------
02218-10
02218-11
FIELD BLANK-1
TRIP BLANK-1
04-04-00/14:45
04-03-00 ------------------------------------- ------------------------------- ----------------------
· PARAMETER 02218-10
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene,. ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
104 %
102 'lr
108 'lr
1
Analysis Date
Batch ID
04.12.00
1A0412
02218-11
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<l.0
<1.0
<1.0
<1.0
<2.0
106 'lr
-100 'lr
110 'lr
1
04.13.00
1A0413
-------------------------------------------------
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S,_a:v1a,.n/~;~ f! t.abor,ata~1es •-o1-r-,~ ..... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LT0#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------------------------ -- ------------------------------ ----------------------
02218-12 CMMW-04 04-05-00/13:20
02218-13 REP-01 04-05-00
------------------ ---------- --------------------------------- ------- ----------- -----------
PARAMETER
Cyanide, Total (9010), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02218-12
----------
170
1
04.12.00
04.12.00
0412S
12
1
04.12.00
04.12.00
0412S
02218-13
----------
170
1
04.12.00
04.12.00
0412S
8.9
1
04.12.00
04.12.00
0412S
S afv•a1n,n a•h
l!.'abor'citories 5102 uRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------------------------ ---------------------------------- --------------------
02218-12
02218-13
CMMW-04
REP-01
04-05-00/13:20
04-05-00
-------------------------------------------------------------------- ----------------------
PARAMETER 02218-12
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <50
Bromomethane (Methyl bromide), ug/1 <50
Vinyl chloride, ug/1 <50
Chloroethane, ug/1 <50
Methylene chloride <250
(Dichloromethane), ug/1
Acetone, ug/1 <1200
Carbon disulfide, ug/1 <50
1,1-Dichloroethene, ug/1 <50
1, 1-Dichloroethane, ug/1 <50
cis-1,2-Dichloroethene, ug/1 110
trans-1,2-Dichloroethene, ug/1 <50
Chloroform, ug/1 <50
1,2-Dichloroethane, ug/1 <50
2-Butanone (MEK) , ug/1 <500
1,1,1-Trichloroethane, ug/1 <50
Carbon tetrachloride, ug/1 <50
Bromodichloromethane, ug/1 <50
1,1,2,2-Tetrachloroethane, ug/1 <50
1,2-Dichloropropane, ug/1 <SO
trans-1,3-Dichloropropene, ug/1 <50
02218-13
<50
<50
<50
<50
<250
<1200
<50
72
<50
200
<50
<50
<50
<500
<50
<50
<50
<50
<50
<50
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·---,-~ .... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fa..x [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LTO#032800-C
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------------
02218-12 CMMW-04 04-05-00/13:20
02218-13 REP-01 04-05-00
------------------ --------- ---------------- -----------------------------------------------
PARAMETER 02218-12 02218-13
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromofonn, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene ,. ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-da·
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluqromethane
Dilution Factor.
6500 7000
<50 <50
<50 <50
<50 <50
<50
<50
<500
<500
400
<50
<50
<50
<50
<100
106 %-
100 %
108 %
50
<50
<50
<500
<500
650
<50
<50
<50
<50
<100
106 %-
100 %
108 %-
Analysis Date
Batch ID
04.12.00
1A0412
50
04.12.00
1A0412
Sa,va'nn-a-h
L'abOiatades 5102 LJ!Roche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LT0#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l90.0001
Sampled By: Client
Code: 121300419
REPORT OF RESULTS Page 10
DATE/
LOG NO
02218-14
02218-15
02218-16
02218-22
02218-23
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
--------------------------------------------------
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate Result
Precision (%RFD) of LCS/LCSD
PARAMETER 02218-14 02218-15 02218-16 02218-22
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <1.0
Bromomethane (Methyl <1.0
bromide), ug/1
Vinyl chloride, ug/1 <l. O
Chloroethane, ug/1 <1.0
Methylene chloride <5.0
(Dichloromethane), ug/1
Acetone, ug/1 <25
Carbon disulfide, ug/1 <1.0
1,1-Dichloroethene, ug/1 <1.0 94 % 46-147 %
1,1-Dichloroethane, ug/1 <1.0
cis-1,2-Dichloroethene, ug/1 <1.0
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <1.0
2-Butanone (MEK), ug/1 <10
1,1,1-Trichloroethane, ug/1 <1.0
Carbon tetrachloride, ug/1 <1.0
02218-23
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S a·v a•n.n ah
Labo·ratOi'ieS 5102 LaRocheAvenue • Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com
G" NO: S0-02218
Received: 06 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Reported: 18 APR 00
Client PO. No.: LT0#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202,0190.0001
Sampled By: Client
Code: 121300419
Page :u
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02218-14
02218-15
02218-16
02218-22
02218-23
--------------------------------------------------
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate Result
Precision (%-RPD) of LCS/LCSD
------------------------------------ ----------------------------------------·---------------PARAMETER 02218-14
----------------------------- ----------
Brornodichlorornethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibrornochlorornethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Brornoforrn, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Brornofluorobenzene
Surrogate -Dibrornofluorornethane
Dilution Factor
<1.0
<1.0
<1.0
<l .O
<1.0
<1.0
<1.0
<l .O
<l.0
<1.0
<10
<10
<1.0
<1.0
<l.O
<1.0
<1.0
<2. 0
104 %
100 %
108 %
1
Analysis Date
Batch ID
04.12.00
1A0412
---------------------------------------
02218-15
100 %
100 %
104 %-
106 %-
106 %-
102 'Ir
108 %-
1
04.12.00
1A0412
----------
02218-16
56-143 %
62-135 %-
68-131 %-
72-127 'Ir
77-122 %
74-126 %-
70-130 %-
1
04.12.00
1A0412
----------
02218-22 02218-23
----------
~ a v }l\n in~_a h
l:aboratories 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LT0#032800-C
Requisition: SQ98·0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
REPORT OF RESULTS Page 12
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------ --------------- -- --------------------------------------- -- --------------
02218-14 Method Blank
02218-15 Lab Control Standard% Recovery
02218-16 LCS Accuracy Control Limit (%R)
02218-22 Lab Control Standard Duplicate Result
02218-23 Precision (%RPO) of LCS/LCSD
------------------ ------·-------------------------------------------- ----------------------
PARAMETER
Cyanide, Total (9010), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010), ug/1
-Dilution Factor
Prep Date
Analysis Date
Batch ID
02218-14
<5.0
1
04.12.00
04.12.00
0412S
<5 .0
l
04.12.00
04.12.00
0412S
02218-15
101 %
2
04.12.00
04.12.00
0412S
02218-16
85·115 %
02218·22 02218-23
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•-•s..-r,.,..,.___..,,_ 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LT0#032800-C
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
REPORT OF RESULTS Page 13
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------ -------------------------------------------------- ----------------------
02218-24 LCS Precision Control Limit (Advisory) %RPD
------------------ ------- -- ---------------------------------------------------------------
PARAMETER 02218-24
---------------------------------------
Volatiles by GC/MS (8260)
1,1-Dichloroethene,
Trichloroethene,
Benzene,
Toluene,
Chlorobenzene,
Surrogate Toluene-d8
Surrogate 4-Bromofluorobenzene
Surrogate Dibromofluoromethane
Cyanide, Total (9010), ug/1
Cyanide, Amenable (9010), mg/1
S,a ~:f';n·Jl .c! ,h
t!abar.atoraes 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
Received: 06 APR 00
Reported: 18 APR 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
REPORT OF RESULTS Page 14
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------ ---- ---------------- ------------------------------
. 02218-17 MS % Recovery (Batch)
02218-18 MSD % Recovery(Batch)
02218·19 ·MS Accuracy Advisory Limit (%R)
02218-20 Precision (%RPD) MS/MSD
02218-21 MS Precision Advisory Limit (%RPD)
---- -------------- ---------------------------------------------------
PARAMETER 02218-17 02218-18 02218-19 02218-20 02218-21
------------------------------------------------- ---------- --------------------
Volatiles by GC/MS (8260)
1,1-Dichloroethene, .. 104 %
Trichloroethene, 'Is 108 %
Benzene, % 106 %
Toluene, 'Is 112 ..
Chlorobenzene, 'Is 114 ..
Surrogate Toluene-as 104 %
Surrogate . 4-Bromofluorobenzene 100 ..
Surrogate . Dibromofluoromethane 108 %
Dilution Factor 1
Analysis Date
Batch ID 1A0412
Cyanide, Total (9010), ug/1 101 'Is
Dilution Factor 2
Prep Date 04.12.00
Analysis Date 04.12.00
Batch ID 0412S
Cyanide, Amenable (9010), mg/1
96 ..
106 'Is
104 %
110 ..
110 %
106 ..
102 'Is
106 'Is
1
04.12.00
1A0412
107 ..
2
04.12.00
04.12.00
0412S
46-147 ..
56-143 ..
62-135 'Is
68-131 ..
72-127 ..
77-122 %
74-126 %
70-130 ..
1
1A0412
85-115 %
8 'Is < 30 %
2 'Is
2 'Is
< 35 %
< 37 %
2 'Is < 33 %
4 %
1
04.12.00
1A0412
5.9 %
< 22 'Is
NA
NA
NA
1
04.12.00
1A0412
<30 %
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S'a'.,.1ia n n;a h t.citiOra'tor:te-s •-•-T-~ ..... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
Received: 06 APR_00
Reported: 18 APR 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 121300419
REPORT OF RESULTS Page 15
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------------ ------------------------------------------------------------------
PARAMETER
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality coritrol
requirements.
J = Estimated result between the reporting limit (RL) and the method detection
limit (MDL) .
E = Result is above the upper calibration limit; therefore, dilution is
required.
Final Page Of Report
-----------A~R"c'JADIS Laboratory Task Order No./P.O. No. 03:Z.eix:.>· <-. GERAGHTY&MILLER
Project Number/Name ~<""'°~"'2-.,,,,,,, I
Project Location °'1~.,.J, ,v <-
LaboratoryS-.t-,-,~-I,_ l,,b 'l,l ~t' t-:.}
Project Manager ~"-;~-"'\L ff-,, ~ J .v '1-...·V ,,v , I ,,,, ~ . .
Sampler(s)/Affiliation 4-1--i-.:.s;;•-'-/ J? 6,,..-!I...,,~ I\ , 'v
' 0 '--' "\ . . -t "l,.
Date/Time ~ :r c--f~o _o Sample ID/Location Matrix Sampled Lab ID J:~ V ~
C..HKw · Z 'i L 41,3/'7-? ~,a,.;, s
( ,'.,(I'-, w · <'. 3 L '{/._-yr~,:, '/t"?o!> .3
Cr>/'-Jl<--'-2. I (. W¥/%"t ?o 3
C1'7,,t.rt-v --2. o L rrf(o o/o yti, 3
C/'7/2 ..,/ -I c, L. 'il,ui r,;_"D s
C/7/Ji.v-·,G /,-rfl% {) /, 5"/ J .3
C ,vfl---tu--1 -o 7-L 1//-"/,,. / 1-'[ . /69'-I .3
,(__f'--f H t,-0 • I r / 171,.-v°h . J~/'O -)
<:::.1---11'-1 \.)0 -/,5 L. '-/IN//!//, 5
(._ /vpLf l,v -0 '-f L l<ltn,1o,._, ? ' ,320 ..)
h:S -Of l. 'f/J!,/'7; 1J.2~ 3 I
/vlSu · o I l. '-I ,,f..,-;r,, -, _
/_Jt:,(,) 3 I
l<'.-,.,,.-.01 L '//1!3/a:.) 3. i
P.e (J 1'5 l,v,k-f L. '1/'//<J <Y,~-;s-3
fr;? 61~-k · I L '! I j/c.e. -3
Sample Matrix: L = ~uid· c --<olid; A = Air . 1 /] ,r ,;
Relinquished~: / / ~ / / t' -.,,_ "' ,.anization: / f re.,,/'.·,
Received by: -'7~ • . · Organization: 5 f(,; ~ 5/11( V , '
Relinquished by: Organization:
Received by: Organization:
Special Instructions/Remarks: /\I 1,1V"-f...,'"',,/1,.,-~ ·, C q I ( 'V.• ,,_) {..cR ·n-~-<,'"I
'
Delivery Method: □ In Person ~ommon Carrier /-(.~i Gr1
--- - -CHAIN-OF-CUSTODY RECORD
ANALYSIS/ METHOD/ SIZE
- - -Page __ / __ of_i_
I
Remarks Total
J
J
>
.3
>
3
;>
..::i
3
.3
l/
'1
'-1
I-(
3' :s
Total No. of Bottles/ 11 Containers
Date '1 ; 5 9h 72» Time (-;?'~ I ~ Intact? Date Time f·sec No NIA
Date I I Time Seal Intact?
Date I I Time Yes No NIA
117, ~P2-4..:Jr/
□ Lab Courier
so-02--2-JZ
□Other
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L,, ;1301 REXWDODS DR
RALEIGH
!ntemal Billing Refarence /VC c)t::; () ;,:_-·~ · ;.·
Wa ARCADIS GERAGHTY&MILLER
/._:>,:,.Vea~.-.~ h_ £_...,:. ~
60 ,,_ '?"'. "-1 p I
·Laboratory Task Order Task Order No.; 032cP?--,C:....
ARCADIS Geraghty & Mi!Jer Office:.,,; c.. h· 1 "<.. Phone: ':J.ff• 'l.e;.l. -.£511 Date: ::ll.28/"'=) -
Address: Project Number: ~C<Zo ZO?. 011-c,. tJ. i_D I I
Laboratory Reporting Level: C=:::J1 c:::K=i11 C=:::J II C=:::J1v c=! NJOEP Reduced C=:::J GJSKEY Disks
Project Na'me: {ri) fl«t=-·, ~ I(.~ •. .., l "-1,d,r Location: o,£.~J ,>...I(.
Lab Provides Sample Containers? ~Yes C=:::J No Dat_e Required: ::,{.-3, t.= Ship To: /.c.tr.1.A.A. ~ A-f c.--~~ ......__
A. or: r 7 JI,, ,:;•e1~ Estimated Date Of Sample Receipt By Laboratory: L/. 2 <X>.e> Report Due: Z ;,AS
ReportsDeliveredTo: /-Je::l .',!:. ... SLtf't' Number Of Reports: 2. ' . 'I T Work Description: Lni: .... ). · JJr:{hr , S:~ -.z/>,
Send Invoice To: r \ -' · ")l .r: tf.,
1
I
I
I • Det. ' Oet. ' Oet. # Det. PHYSICAL PROPERTIES Water Method Limit Soil Method Limit NON-METALLICS Water Method Limit Soil Method Limit
pH Acidity
Spec. Cond. Alkalinity (Total) I
Hardness (total) Carbonate
TDS Bicarbonate
TSS Bromide
Temperature Chloride I
Turbidity Cyanide -/-f-,. / l1 ::,. I"", o o o..£ • i
lgnitability -A _LL,_ Jj,i -1c/t) .o•Ji..._ fl,
Corrosivity Ammonia "
7
r' I
Reactivity Nitrate /'i ,.f<. ~ -• h. I Ii. :J. ~ 1 /./., • f-
TCLP Extraction TKN -' '' I lf:..A_ u ~:, /J I ,.,
Nitrite ~ TCLP Complete
METALS" Phosphorus I
Aluminum Silica
Antimony Sulfate
Arsenic Sulfide I
Barium Surfactants (MBAS)
Beryllium ORGANICS
Cadmium BOD I
Calcium COD
Chromium TOC
Hex Chromium TR.PH
Copper Phenols"
Iron Pesticides/PCBs"
lead PNAs"
Maonesium Org. Phos. Pest." I
Manganese Dio~ins
MerCU"' Chlor. Herb? -z.;;..,t .. ,x...
Nickel Volatile Organics" zo 9-ZL;.o IU,//4-
Potassium Semi Volati!e Organics" I
Selenium APPENDIX IX"
Sliver RAOJONUCLIOES
Sodium Gross Alpha . I
Thallium Gross Beta
Tin Radium 226
Vanadium Radium 22B
Zinc I
Priority Pollutant Metals"
TAL Metals,,
"Metals are Total Metals Unless Specifie · ·
Special Instructions Or Other:,_-~/ ~"''-'.!.,':.,=:S._-!.:'::;~~~,-li°-'fLCJ.:C..,,i,,l:,.,--a,,:;!.~~ps,~L~~•<,J,"'1/l-"'--~'..5e!<!.1""-.!~0,.-.---------~ efi-c:::> •
•Includes All Organic and Inorganic Compounds. I
AG&M Project Manager Signature: r7 ::z;lJ------
/ Laboratory Acceptance: _________________ Qate: _____ _
Date: '3::2,r-c..g.
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•---T--lno. ;102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
02265-1
. 02265-2
02265-3
02265-4
02265-5
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller,. Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
POW-1
POW-2
IW-1
CMMW-05
CMMW-10 .
LOG NO: S0-02265
Received: 07 APR 00
Reported: 24 APR 00
o ■».o ■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.000S
Sampled By: Client
Code: 161500425
Page 1
DATE/
TIME SAMPLED
04-06-00/11:55
04-06-00/09:10
04-06-00/15:00
· 04-06-00/13 :40
04-06-00/10:50 -~------------------------------------------------
PARAMETER 02265-1 02265-2 02265-3 02265-4 02265-5
-------------------------------------------------------------------------------
Bromide (300.0), mg/1 160 0.12B 2000 0.23B 4.6
Dilution Factor 100 1 1000 1 2
Prep Date 04.17.00 04.17.00 04.17.00 04.17.00 04.17.00
Analysis Dat_e 04.19.00 04.18.00 04.19.00 04.18.00 04.19.00
Batch ID 0417C 0417C 0417C 0417C 0417C
Sulfate as S04 (375.4), mg/1 <5.0 6.2 1100 <5.0 <5.0
Dilution Factor 1 1 so 1 1
Prep Date 04.12.00 04.12.00 04.12.00 04.12.00 04.12.00
Analysis Date 04.12.00 04.12.00 04.12.00 04.12.00 04.12.00
Batch ID 0412A 0412A 0412A 0412A 0412A
Nitrite-N (353.2), mg/1 0.058 '<0. 050 0.55 <0.050 0.24
Dilution Factor 1 1 1 1 1
Prep Date 04.10.00 04.10.00 04.10.00 04.10.00 04_1·0.oo
Analysis Date 04.10.00 04.10.00 04.10.00 04.10.00 04.10.00
Batch ID 0410A 0410A 0410A 0410A 0410A
-------------------------------------------------------------------------------
S .a~v._al ,n~~ a ~ taboratories 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
0: so :-0-2265
Received: 07 APR 00
Reported: 24 APR 00
o ■~. o ■
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 2 REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
02265-1 POW-1
02265-2 POW-2
02265-3 IW·l
02265-4 CMMW-05
02265-5 CMMW-10
PARAMETER
Nitrate-N (353.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chloride (325.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Alkalinity (to pH 4.5) as
CaC03 _(310.1), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02265-1 02265-2 02265-3
<0.050 3.0 <5.0*F65
1 5 100
04.07.00 04.07.00 04.07.00
04.07.00 04.07.00 04.07.00
0412A 0412B 0412C
220
5
04.12.00
04.12.00
0412E
900
1
04.13.00
04.13.00
0413A
----------
29
1
04.12.00
04.12.00
0412E
73
1
04.13.00
04.13.00
0413A ----------
1600
100
04.12.00
04.12.00
0412E
<1.0
1
04.13.00
04.13.00
0413A
----------
DATE/
TIME SAMPLED
04-06-00/11:55
04-06-00/09:10
04-06-00/15:00
04-06-00/13:40
04-06-00/10:50
02265-4 02265-5
--------------------
1.4 3.2
1 5
04.07.00 04.07.00
04.07.00 04.07.00
041_2A 0412B
14 35
1 1
04.12.00 04.12.00
04.12.00 04.12.00
0412C 0412C
72 99
1 l
04.13.00 04.13.00
04.13.00 04.13.00
0413A 0413A
--------------------
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
C,NO; S0-02265
Received: 07 APR 00
Reported: 24 APR 00
Mr. Nanjun Shetty 0 ■».o ■
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
LOG NO
02265-1
02265-2
02265-3
02265-4
02265-5
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
REPORT OF RESULTS Page 3
DATE/
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
-------------------------------------------------------------------------
POW-1 04-06-00/11:55
POW-2 04-06-00/09:10
IW-1 04-06-00/15:00
CMMW-05 04-06-00/13:40
CMMW-10 04-06-00/10:50
------------------------------------------------------------------------------------
PARAMETER
Biochemical Oxygen Demand
(5 Day) (405. l/5210B), mg/1
_Dilution Factor
Prep Date
Analysis Date
Batch ID
Ammonia (as N) (350.1), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
02265-1
----------
1700
04.07.00
04.07.00
0407A
0.061
1
04 .11. 00
04 .11.00
0411D
----------
02265-2 02265-3 02265-4 02265-5
----------------------------------------
<2.0 25000 <2.0 11
04.07.00 04.07.00 04.07.00 04.07.00
04.07.00 04.07.00 04.07.00 04.07.00
0407A 0407A 0407A 0407A
0.037 1.4 0.077 <0_030
1 1 1 1
04 .11. 00 04.11.00 04 .11. 00 04.11.00
04.11.00 04.11.00 04.11.00 04.11.00
0411D 0411C 0411D 0411C ----------------------------------------
S ~:~v1.'!1irt .i:a~~1~1J l!abar:atar;1es 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
02265-1
02265-2
02265-3
02265-4
02265-5
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
POW-1
POW-2
IW-1
CMMW-05
CMMW-10
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
02265-1 02265-2
<1000
<1000
<1000
<1000
<5000
<25000
<1000
<1000
<1000
90000
<1000
<1000
<1000
<10000
<1000
<1000
<1000
<1000
<1000
<1000
<5000
<25000
<1000
<1000
<1000
5900
<1000
<1000
<1000
<10000
<1000
<1000
G NO: $0-02265
Received: 07 APR 00
Reported: 24 APR oo
o■>. "■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 4
02265-3
<4.0
<4 .0
<4 .o
<4. 0
<20
<100
<4.0
<4.0
<4.0
<4 .0
<4 .o
13
<4. 0
<40
<4.0
<4.0
DATE/
TIME SAMPLED
04-06-00/11:55
04-06-00/09:10
04-06-00/15:00
04-06-00/13:40
04-06-00/10:50
02265-4
<1000
<1000
<1000
<1000
<5000
<25000
<1000
<1000
<1000
<1000
<1000
<1000
<1000
<10000
<1000
<1000
02265-5
<1000
<1000
<1000
<1000
<5000
<25000
<1000
<1000
<1000
16000
<1000
<1000
<1000
<10000
<1000
<1000
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51021..aRocheAvenue · Savannah,GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
0: so -U2T&S----
Received: 07 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 3,1388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
02265-1
02265-2
02265-3
02265-4
02265-5
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
POW-1
POW-2
IW-1
CMMW-05
CMMW-10
PARAMETER
Brornodichlorornethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibrornochlorornethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Brornoforrn, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone
(MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
·styrene, ug/1
Xylenes, Total, ug/1
02265-1
<1000
<1000
<1000
<1000
<1000
<1000
<1000
<1000
<1000
<1000
<10000
<10000
<1000
<1000
<1000
<1000
<1000
<2000
02265-2
<1000
<1000
<1000
<1000
90000
<1000
<1000
<1000
<1000
<1000
<10000
<10000
11000
<1000
<1000
<1000
<1000
<2000
Reported: 24 APR 00
oa». o ■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
02265-3
<4.0
<4.0
<4.0
<4 .0
360
<4.0
<4 .0
<4 .0
<4 .o
<4 .o
<40
<40
13
<4 .0
<4.0
<4.0
4.5
<8.0
Page 5
DATE/
TIME SAMPLED
04-06-00/11:55
04-06-00/09:10
04-06-00/15:00
04-06-00/13 :40
04-06-00/10:50
02265-4
<1000
<1000
<1000
<1000
140000
<1000
<1000
<1000,
<1000
<1000
<10000
<10000
14000
<1000
<1000
<1000
<1000
<2000
02265-5
<1000
<1000
<1000
<1000
170000
<1000
<1000
<1000
<1000
<1000
<10000
<10000
11000
<1000
<1000
<1000
<1000
<2000
S ;a(.v'a.jn~nta~h
l::'abo"r:at'orieS 5!02LaRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
G NO: S0-02265
Received: 07 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Reported: 24 APR 00
o ■». o ■
R~quisition: SQ98-0553
Contract No.: JFD Channel"Master
Project: NC000202.0160.0005
_Sampled By: Client
Code: 161500425
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
02265-1
02265-2
02265-3
02265-4
02265-5
POW-1 04-06-00/11:55
POW-2 04-06-00/09:10
IW-1 04-06-00/15:00
CMMW-05 04-06-00/13:40
CMMW-10 04-06-00/10:50
------------------------------------------------------------------------------------
PARAMETER 02265-1 02265-2 02265-3 02265-4 02265-5 -------------------------------------------------------------------------------
Surrogate Toluene-dB 104 %-104 %-104 % 104 %-104 %-
Surrogate -4-Bromofluorobenzene 98 %-98 %-96 % 96 % 98 %-
Surrogate -Dibromofluoromethane 104 %-104 % 104 % 104 % 102 %-
Dilution Ji'.actor 1000 1000 4 1000 1000
Analysis Date 04.12.00 04.12.00 04.12.00 04.12.00 04.12.00
Batch ID 1B0412 1B0412 1B0412 1B0412 1B0412
Iron (Dissolved) (200.7)
Iron, mg/1 67 0.094 140 0.32 0.20
Dilution Factor 2 1 1 1 1
Prep Date 04.10.00 04:10.00 04.10.00 04.10.00 04.10.00
Analysis Date 04.20.00 04.19:00 04.19.00 04.19.00 04.19.00
Batch ID 0410H 0410H 0410H 0410H 0410H
Iron (200. 7)
Iron, mg/1 54 10 130 1.1 2.0
Dilution Factor 1 1 1 1 1
Prep Date 04.20.00 04.20.00 04.20.00 04.20.00 04.20.00
Analysis Date 04.20.00 04.20.00 04.20.00 04.20.00 04.20.00
Batch ID 0420G 0420G 0420G 0420G 0420G
-------- -------------- - - - - - ----------------------------------------------------
)
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OG NO: S0-02265
Received: 07 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC-: Mr. Mark Radecke
Reported: 24 APR 00
o ■».oll
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l60.0005
Sampled By: Client
Code: 161500425
REPORT OF RESULTS Page 7
DATE/
LOG NO
02265-l
02265-2
02265-3
02265-4
02265-5
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
POW•l· 04-06-00/ll:55
POW-2 04-06-00/09:10
IW-l 04-06-00/15:00
CMMW-05 04-06-00/13:40
CMMW-10 04-06-00/10:50
PARAMETER
Manganese (Dissolved) (200. 7)
Manganese, mg/1
Dilution FaCtor
Prep Date
Analysis Date
Batch ID
Manganese (200. 7)
Manganese, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Total Organic Carbon (415.l),
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
02265-l
----------
37
2
04.10.00
04.20.00
0410H
26
l
04.20.00
04.20.00
0420G
mg/1 900
10
04.12.00
04.12.00
0412A
----------
02265-2 02265-3 02265-4 02265-5
-------------------- --------------------
0.043 7.5 0.045 0.31
l l l l
04.10.00 04.10.00 04.10.00 04.10.00
04.19.00 04.19.00 04.19.00 04.19.00
04lOH 0410H 0410H 04lOH
0.ll 7.3 0.081 0.26
l l l l
04.20.00 04.20.00 04.20.00 04.20.00
04.20.00 04.20.00 04.20.00 04.20.00
0420G 0420G 0420G. 0420G
l.l 13000 <l.0 7.0
l 100 l l
04.12.00 9.4. ll. 00 04.ll.OO 04.ll.OO
04.12.00 04.ll.OO 04. ll. 00 04.ll.00
0412A 04llC 04llC 04llC
----------------------------------------
r
s;a v·a n•n•a:h
Lab Q {a tci"r:) e'.S 5102LaRocheAvenue • Savannah,GA31404 · [phone] • Fax[phone] • www.stlsavlab.com
CC.NO: $0-02265
Received: 07 APR 00
LOG NO
02265-1
02265-2
02265-3
02265-4
02265-5
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
POW-l
POW-2
IW-l
CMMW-05
CMMW-10
Reported: 24 APR 00
o■».o ■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 8
DATE/
TIME SAMPLED
04-06-00/ll:55
04-06.c00/09 :10
0_4-06-00/15:00
04-06-00/13:40
04-06-00/10:50
PARAMETER 02265-l 02265-2 02265-3 02265-4 02265-5
Dissolved Organic Carbon 840 7.7 13000 2.5 9.3
(415. l), mg/1·
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chemical Oxygen Demand
(410 .1), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
10
04.12.00
04.12.00
0412A
1300
1
04.12.00
04.13.00
0412A
----------
1
04.12.00
04.12.00
0412A
23
1
04.12.00
04.13.00
0412A
----------
100 l 1
04". ll. 00 04.ll.00 04.11.00
04.11.00 04.11.00 04.ll.OO
04llC 04llC 04llC
8800 36 53
100 1 l
04.12.00 04.12.00 04.12.00
04 .13. 00 04.13.00 04.13.00
0412A 0412A 0412A
------------------------------
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
L N : -02265
Received: 07 APR 00
Reported: 24 APR 00
0151». 011
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l60.0005
Sampled By: Client
Code: 161500425
Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
02265-6 TB-2 04-06-00
02265-7 RB-l 04-06-00
PARAMETER 02265-6 02265-7
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
l,l-Dichloroethene, ug/1
l,l-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-l,2-Dichloroethene, ug/1
_Chloroform, ug/1
l,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
l,l,l-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1, 1, 2, 2-TetraChloro·ethane, ug/1
l,2-Dichloropropane, ug/1
trans-l,3-Dichloropropene, ug/1
Trichloroethene, ug/1
<l.0 <l.0
<l.0 <l.O
<l.0 <l.0
<l.0 <l.0
<5.0 <5.0
<25 <25
<l.0 <l.0
<l.0 <l.0
<l.O <l.0
<l.0 <l.0
<l.0 <l.0
<l,0 <l.0
<l.0 <l.0
<10 <10
<1.0 <1.0
<l.0 <1.0
<l.0 <1.0
<l.O <l.O
<1.0 <l.0
<l.O <1.0
<l.0 <l.O
------------------------------
•-<'S.-T,...,._,,_,.._111<. 5102LaRocheAvenue • Savannah,GA31404 • [phone] · Fax[phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
,P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
-276S---
Received: 07 APR 00
Reported: 24 APR 00
o ■».011
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 10
DATE/
TIME SAMPLED
02265-6 TB-2 04-06-00
02265-7 RB-1 04-06-00
PARAMETER 02265-6 02265-7
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
------------------------------
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<10 <10
<10 <10
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<2.0 <2.0
104 'Ir 102 'Ir
98 'Ir 98 %-
106 'Ir 102 'Ir
1 1
04.12.00 04.12.00
1B0412 1B0412
----------
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5102 La.Roche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
265
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Received: 07 APR 00
Reported: 24 APR 00
o ■».011
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l60.0005
Sampled By: Client
Code: 161500425
Page 11
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
--------------------------------------------------
Method Blank
Lab Control Standard 'Ir Recovery
LCS Accuracy Control Limit ('lrR)
02265-8
02265-9
02265-10
02265-11
02265-12
Lab Control Standard Duplicate 'Ir Recovery
Precision ('lrRPD) of LCS/LCSD
PARAMETER
Bromide (300.0), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID·
Sulfate as S04 (375 .4),
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nitrite-N (353.2), mg/1
Dilution Factor
Prep Date
Analysis Da\;e
Batch ID
mg/1
02265-8
<1.0
1
04.17.00
04.18.00
0417C
<5.0
1
04.12.00
04.12.00
_ 0412A
<0.050
1
04.iO.OO
04.10.00
0410A
02265-9
104 'Ir
1
04.17.00
04.18.00
0417C
118 'Ir
1
04.12.00
04.12.00
0412A
99 'Ir
1
04.10.00
04.10.00
0410A
02265-10
90-110 'Ir
75-125 'Ir
80-120 'Ir
-----------------------------------------------------------
02265-11
2.07
1
04.17.00
04.18.00
0417C
21.5
1
04.12.00
04.12.00
0412A
----------
02265-12
0 'Ir
4.3 'Ir
----------
5102l.aRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
-cnns----
Received: 07 APR 00
Reported: 24 APR 00
011». o ■
Requisition: SQ98-0553
Contract No.: JFD.Channel Master
Project: NC000202. 0160. 0005
Sampled By: Client
Code: 161500425
Page 12
DATE/
LOG NO
02265'8
02265-9
02265,10
02265-11
02265-12·
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RPO) of LCS/LCSD
PARAMETER
Nitrate-N (353.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chloride (325.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Alkalinity (to pH 4.5)
CaC03 (310.1), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
as
02265-8
<0.050
1
04.07.00
04.07.00
0412A
<LO
1
04.12.00
04.12.00
0412E
<1.0
1
04.13.00
04.13.00
0413A
02265-9
105 %
1
04.07.00
04.07.00
0412A
106 %
1
04.12.00
04.12.00
0412E
99 'Ir
1
04.13.00
04.13.00
0413A
02265-10
80-120 %
85-115 "'
80-120 %
-----------------------------------------------------------
02265-11 02265-12
98 % 1.0 %
1
04.13.00
04.13.00
0413A
--------------------
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LOG NO: S0-02265
Received: 07 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC _27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Reported: 24 APR 00
o ■».o ■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 13
DATE/
LOG NO
02265-8
02265-9
02265-10
02265-11
02265-12
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
TIME SAMPLED
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RPD) of LCS/LCSD
PARAMETER
Biochemical Oxygen Demand
(5 Day) (405. l/5210B), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Ammonia (as N) (350 .1), mg/1
Dilution Factor
Prep Date
Analysis_Date
Batch ID
02265-8
<2.0
04.07.00
04.07.00
0407A
<0.030
1
04.11.00
04 .11. 00
0411C ----------
02265-9
101 %
04.07.00
04.07.00
0407A
110 %
1
04 .11. 00
04.11.00.
0411C
----------
02265-10
85-115 %
85-115 %
02265-11
97 %
04.07.00
04.07.00
0407A
02265-12
4.0 %
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCl\DIS Geraghty & Miller:, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
: 6S-
Received: 07 APR 00
Reported: 24 APR 00
o ■». o ■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 14
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-8
02265-9
02265-10
02265-11
02265-12
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
_Precision (%RPD) of LCS/LCSD
PARAMETER 02265-8 02265-9 02265-10
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide) , ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25 ·
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<l.0
<1.0
94 % 46-147 %
02265-11 02265-12
48 2 %
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S a•.wa-:n:1n11a.'h C.8bci(iatO-r.i~fs 5102LaRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: ·Mr. Mark Radecke
REPORT OF RESULTS
So-"lr2"2"6S
Received: 07 APR 00
Reported: 24 APR 00
o ■». 011
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l60.0005
Sampled By: Client
Code: 161500425
Page 15
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
02265-8
02265-9
02265-10
02265-11
02265-12
Lab Control Standard Duplicate% Recovery
Precision (%RPO) of LCS/LCSD
PARAMETER 02265-8
Bromodichloromethane, ug/1 <1.0
1,1,2,2-Tetrachloroethane, ug/1 <1.0
1,2-Dichloropropane, ug/1 <1.0
trans-1,3-Dichloropropene, ug/1
Trichloroethane, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<1.0
<1.0
<1.0
"<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
102 %
98 %
104 %
l
Analysis Date
Batch ID
04.12.00
lB0412
02265-9
106 %
108 %
106 %
108 %
104 %
98 %
102 %
l
04.12.00
1B0412
02265-10
56-143 %
62-135 %
68-131 %
72-127 %
77-122 %
74-126 %
70-130 %
02265-11 02265-12
52 2 %
53 2 %
52 2 %
54 0 %
52
50
53
l
04.12.00
lB0412
5102 LaRocheAvenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
G NO: S0-02265
Received: 07 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
Reported: 24' APR 00
o ■». o ■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
REPORT OF RESULTS Page 16
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-8
02265·9
02265-10
02265-11
02265-12
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (tR)
Lab Control Standard Duplicate t Recovery
Precision (tRPD) of LCS/LCSD
PARAMETER 02265-8 02265-9 02265-10
Iron (Dissolved) (200. 7)
Iron, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Iron (200.7)
Iron, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Manganese (Dissolved)
Manganese, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
(200.7)
-----------------------------
<0.050 108 t 85-115 %
l l
04.10.00 04.10.00
04.19.00 04.19.00
0410H 0410H
<0.050 97 'Ir 85-115 'Ir
1 1
04.20.00 04.20.00
04.20.00 04.20.00
0420G 0420G
<0.010 106 t 85-115 t
l l
04.10.00 04.10.00
04.19.00 04.19.00
0410H 0410H
------------------------------
02265-11 02265-12
104 'Ir 3. 8 'Ir
1
04.10.00
04.19.00
0410H
96 t 1.0 'Ir
1
04.20.00
04.20.00
0420G
102 t 3.8 'Ir
1
04.10.00
04.19.00
0410H --------------------
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Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC .27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
265
Received: 07 APR 00
Reported: 24 APR 00
011». 011
Requisition: SQ98-0553
Contract No.: JFD Channel Master·
Project: NC000202.0160.0005
Sampled By: Clfent
Code: 161500425
Page 17
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-8
02265-9
02265-10
02265-11
02265-12
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Lab Control Standard Duplicate% Recovery
Precision (%RFD) of LCS/LCSD
PARAMETER 02265-8 02265-9 02265-10
Manganese (200.7)
Manganese, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<0.010
1
04.20.00
04.20.00
0420G
Total o'rganic Carbon (415.1), mg/1
Dilution Factor
<1.0
1
Prep Date
Analysis Date
Batch ID
04 .11.00
04.11.00
0411C
Dissolved Organic Carbon <1.0
(415 .1), mg/1 ·
Dilution Factor 1
Prep Date 04.11.00
Analysis Date 04.11.00
Batch ID 0411C
95 \-
1
04.20.00
04.20.00
0420G
106 \-
1
04.11.00
04.11.00
0411C
106 %
1
04.11.00
04.11.00
0411C
85-115 \-
80-120 %
80-120 %
02265-11 02265-12
__ .,._,_.___,,.,__ 5102 I.aRocheAvenue • Savannah, GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
G7ID: S0-02265
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Received: 07 APR 00
Reported: 24 APR 00
oa».o ■
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
REPORT OF RESULTS Page 18
DATE/
L_OG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-8 Method Blank
02265-9 Lab Control Standard%' Recovery
02265-10 LCS Accuracy Control Limit (%-R)
02265-11 Lab Control Standard Duplicate%' Recovery
02265-12 Precision (%-RPD) of LCS/LCSD
PARAMETER 02265-8
Chemical Oxygen Demand (410.1), mg/1 <20
Dilution Factor 1
Prep Date 04·. 12. 00
Analysis Date 04.13.00
Batch ID 0412A
02265-9
80 %'
1
04.12.00
04.13.00
0412A
02265-10
60-140 %'
02265-11
82 %'
1
04.12.00
04.13.00
0412B
02265-12
2. 5 %'
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;102 La.Roche Avenue • Sa~, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.coin
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
u-=u2.65
Received: 07 APR 00
Reported: 24 APR 00
o ■,. oa
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 19
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED . ------------------------------------------------------------- -----------------------
02265-13 LCS Precision Control Limit (Advisory) %RPD
PARAMETER 02265-13
Bromide (300.0), mg/1 <30 %
Sulfate as S04 (375.4), mg/1 <30 %
Nitrite-N (353.2), mg/1
Nitrate-N (353.2), mg/1
Chloride (325.2), mg/1
Alkalinity (to pH 4.5) as CaC03 (310.1), mg/1
Dilution Factor
Batch ID
Biochemical Oxygen Demand (5 Day) (405 .1/52iOB) , mg/1
Ammonia (as N) (350 .1) , mg/1
<30 %
<30 %
S ai.1v.,'Eii'n1nta: h
't::iHfO'titcirJeS' 5102 laRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
65
Received: 07 APR 00
Reported: 24 APR 00
Mr. Nanjun Shetty 0 ■».0 ■
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
REPORT OF RESULTS Page 20
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-13 LCS Precision Control Limit (Advisory) %RPD
PARAMETER
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %
Toluene, %'
Chlorobenzene, %
Surrogate -Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Iron (Dissolved) (200. 7)_
Iron, %'
Iron (200. 7)
Iron, %'
Manganese (Dissolved) (200. 7)
Manganese, %
Manganese (200.7)
Manganese, %
Total Organic Carbon (415.1), mg/1
Dissolved Organic Carbon ·(415.1), mg/1
02265-13
< 30 %
< 35 %
< 37 %
< 33 %
< 22 'Ir
<NA%
< NA 'Ir
< NA 'Ir
<20 %
<20 'Ir
<20 %
<20 %
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Mr. Nanjun.Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
. REPORT OF RESULTS
: - 0 ZZ6 S-----
Received: 07 APR 00
Reported: 24 APR 00
o ■ ». o ■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client ·
Code: 161500425
Page 21
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR.LIQUID SAMPLES TIME SAMPLED
02265-13 LCS Precision Control Limit (Advisory) tRPD
PARAMETER 02265-13
Chemical Oxygen Demand (410.1), mg/1 60-140 t
------------------------------------------------- -------------------- ----------
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
-02265
Received: 07 APR 00
Reported: 24 APR 00
o ■».o ■
Requisi.tion: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 22
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
,MS% Recovery(Batch)
MSD % Recovery(Batch)
02265-14
02265-15
02265-16
02265-17
02265-18
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
MS Precision.Advisory Limit (%RPO)
PARAMETER
Bromide (300.0), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Sulfate as S04 (375.4), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nitrite-N (353.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02265-14 ----------
101 %
1
04.17.00
04.18.00
0417C
139 %*F73
1
04.12.00
04.12.00
0412A
99 %
1
04.10.00
04.10.00
0410A
02265-15
----------
102 %
1
04.17.00
04.18.00
0417C
139 %*F73
1
04.12.00
04 .12·. 00
0412A
97 %
1
04.10.00
04.10.00
0410A
02265-16 02265-17 02265-18
----------
90-110 % 0.99 % <30 %
75-125 % 0 % <30 %
80-120 % 2.0 % <30 %
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L NO: SD-02265
Received: 07 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Reported:. 24 APR 00
o ■:t>. 011
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 23
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-14 MS% Recovery(Batch)
02265-15 MSD % Recovery(Batch)
02265-16 MS Accuracy Advisory Limit (%R)
02265-17 Precision (%RPO) MS/MSD
02265-18 MS Precision Advisory Limit (%RPO)
PARAMETER
Nitrate-N (353.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chloride (325.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Alkalinity (to pH 4 .5)
CaC03 (310.1), mg/1
as
Biochemical Oxygen Demand·
(5 Day) (405. l/5210B), mg/1
-----------------------------
02265-14 02265-15
--------------------
89 % 89 %
1 1
04.07.00 04.07.00
04.07.00 04.07.00
0412B 0412B
103 % 104 %
5 5
04.12.00 04.12.00
04.12.00 04.12.00
0412E 0412E
--------------------
02265-16 02265-17 02265-18
80-120 % 0 % <30 %
85-115 % 0.97 % <30 %
------------------------------
S'a v•ain"n,a h t;.i bo'i:ittO ii e"S 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
a:---50""'17276 5
Received: 07 APR 00
Reported: 24 APR 00
Mr. Nanjun Shetty •■».• ■
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
REPORT OF RESULTS Page 24
LOG NO
DATE/
SAMPLE.DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-14 MS% Recovery(Batch)
02265-15 MSD % Recovery(Batch)
02265-16 MS Accuracy Advisory Limit (%-R)
02265-17 Precision {%RPO) MS/MSD
02265-18 MS Precision Advisory Limit (%RPO)
PARAMETER
Ammonia {as N) (350 .1), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, t
Benzene, %
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
02265-14
----------
94 \-
1
04.11.00
04.11.00
0411C
3l'lr*F73
80 \-
110 \-
110 %
115 %
105 \-
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
100
100
%
\-
4
Analysis Date
Batch ID
Iron· (Dissolved) (200. 7)
Iron, mg/1
04.12.00
1B0412
02265-15
- -- -----·--
98 %
1
04.11.00
04.11.00
0411C
26%*F73
80 %
100· %
100 %-
100 %-
105 %-
100 %-
105 %-
4
04.12.00
1B0412
02265-16 02265-17 02265-18
85-115 % 4.2 % <30 %
46-147 % 18 % < 30 %
56-143 % 0 %-< 35 %-
62-135 %-10 %-c 37 \-
68-131 \-10 %-< 33 %-
72-127 %-14 %-c 22 %
77-122 %-< NA \-
74-126 % c NA %
70-130 %-< NA %
75-125 %-<20 %
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OG NO: S0-02265
Received: 07 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0.-Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Reported: 24 APR 00
011». om
Requisition: SQ9.8-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 25
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02265-14
02265-15
02265-16
02265 · 17
02265-18
MS%-Recovery(Batch)
MSD %-Recovery(Batch)
MS Accuracy Advisory Limit (%-R)
Precision (%-RPD) MS/MSD
MS Precision Advisory Limit (%RPO)
------------------------------------------------------------------------------------
PARAMETER
Iron (200. 7)
Iron, mg/1
Manganese (Dissolved) (200.7)
Manganese, mg/1
Manganese (200.7)
Manganese, %-
-Dilution Factor
Prep Date
Analysis Date
Batch ID
Total Organic Carbon
Dilution Factor
Prep Date.
Analysis Date
Batch ID
(415.1),
-----------------------------
02265-14
----------
96 %
1
04.20.00
04.20.00
0420G
mg/1 104 'Is
1
04.11.00
04.11.00
0411C
----------
02265-15 02265-16 02265-17 02265-18
-------------------- --------------------
75-125 % <20 %-
75-125 % <20 %
101 %-75-125 'Is 5.1 %-<20 'Is
1
04.20.00
04.20.00
0420G
104 'Is 80-120 'Is 0 % <25 %
1
04.11.00
04.11.00
0411C
----------------------------------------
Sa v:a mma':h
t[3 lfciifit(fii eS 5102 LaRoche Avenue• Savannah, GA 31404 • (912)-354-7858 • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
-2265
Received: 07 APR 00
Reported: 24 APR 00
o ■».o ■
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
REPORT OF RESULTS Page 26
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
MS\-Recovery(Batch)
MSD \-Recovery(Batch)
02265-14
02265-15
02265-16
02265-17
02265-18
MS Accuracy Advisory Limit (\-R)
Precision (\-RPD) MS/MSD
MS Precision Advisory Limit (\-RPD)
PARAMETER
Dissolved Organic Carbon
(415.1), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chemical Oxygen Demand
(410 .1), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02265-14
----------
101 %
1
04.11.00·
04.11.00
0411C
103 %
1
04.12.00
04 .13. 00
0412A
----------
02265-15
----------
101· \-
1
04.11.00
04.11.00
0411C
105 \-
1
04.12.00
04.13.00
0412A
----------
02265-16 02265-17 02265-18
------------------------------
80-120 % 0 % <25 %
60-140 % 2.0 \-<30 \-
------------------------------
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•-.. -y_._..., 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] · www.stlsavlab.com
NO: S0-02265
,_ Received: 07 APR 00
Reported: 24 APR 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 161500425
Page 27
DATE/
LOG NO I ._ 02265-14
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
TIME SAMPLED
I
I
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I
I
02265-15
02265-16
02265-17
02265-18
PARAMETER
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%RPD)
02265-14 02265-15
NC DEHNR Cert. #269
02265-16
Methods: EPA SW-846, Update III and 40 CFR Part 136.
02265-17
All assocated QA/QC samples were within STL-SL QA/QC criteria.
All associated Inorganic ICV's & CCV's met STL-SL QA/QC criteria.
Where MS/MSD was unavailable or inappropriate, an LCS/LCSD has been
provided for precision.
Due to sample concentration, it was determined that lower dilutions
could not be performed without possible detremental impact on
instrumentation. Where possible, "J" values have been provided in order
to better assess degradation products.
Batch MS/MSD's failed· to meet advisory criteria for dissolved iron and
dissolved manganese due to the abundance of analyte present in the
sample. The dissolved iron concentration was 67mg/L and the dissolved
manganese was 37mg/L. MS/MSD spike levels were lmg/L and 0.50mg/L
respectively.
Batch MS/MSD failed advisory criteria for total iron due to _the
abundance of analyte. The total iron concentration in the sample was
10mg/L and the spike level was lmg/L. ·
02265-18
LOG NO
02265-14
02265-15
02265-16
02265-17
02265-18
5102 La.Roche Avenue • Savannah, GA 31404 • [phone] • Fa..'< [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
-2-zo~
Received: 07 APR 00
Reported: 24 APR 00
011». "■
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l60.0005
Sampled By: Client
Code: 161500425
Page 28
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
MS Precision Advisory Limit (%RPO)
PARAMETER 02265-14 02265-15 02265-16 02265-17 02265-18
Batch MS/MSD failed advisory criteria for sulfate due to a suspected
matrix interference. The sample concentration was <5.0 mg/L, and the
spike level was 20mg/L.
Batch MS/MSD failed advisory criteria for l,l-Dichloroethene due to the
abundance of analyte. The sample concentration was 250ug/L and the spike
level was SOug/L.
*F65 = Elevated detection limits were reported due to sample matrix
interference which required sample or extract dilution.
*F73 = Matrix spike recoveries were· outside advisory limits due to matrix
interference present in the sample.
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~--·--·-~ - - -~ k 072-?a-.o-A ----... -.. -Page-~-ofZ__ -ARCADIS GERAGHTY&MILLER Laboratory Tas Order No./P.O. No. ,, <C.CJ-· rT CHAIN-OF-CUSTODY RECORD
Project Number/Name A)ccco 2.c::>Z c,1Go. =~
Project Location _O~~~{L_J)~. ~,..:S_<. _______ _
I ANALYSIS/ METHOD/ SIZE I
Laboratory "S.T7 · .SovG .,.,. l
Project Manager "-.).,. ": --.s;L._-fr,1
Sample r(s)/ A ffi Ii ation -'''i-(..:.'. !:./v::j~c:c::c:S.~:$~~===--~-
Datemme
Sample ID/Location Matrix Sampled Lab ID Remarks Total
?oc> -2., l 1,fl//U'ftc:J ( I z.
,:__I--\'"' \...l -10 L /1050
pow -I L 1/(i~.t;
<'... !'--\ M v-l , cT L /1"3'r.D 2.
1 \,) -I L ,,-/jj-.rj z.. .
L .
(_
Sample Matrix: L. = ';!_qui~ S = Solid;.. A = Air , Total No. of Bottles/ /a Containers
Relinquished by: I////--;.-_;-····· Organization:_,,7rt/ . ..ulc-'-'"""'.:..J. "":..s.,_~~-----
Received by: /T /}/ -. Organization: $n --'\ ti V
/ . ./ ./
Date ql~ l~ Time /rc<:Q Seal Intact?
Date '-/ I :r / O i) nme r •q•t:,D ~) No N/A .
Relinquished by: __________ Organization: __________ _ Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Specral lnstruct1ons/Remarks: ____________ __c_-'------------------------'-------
Delivery Method: □ In Person ~-Common Carrier~F_,_,_J~~""~'c=-,----
sPEc1FY
□ Lab Courier □Other ______ _
SPECIFY
CHAIN-OF-CUSTODY RECORD Page -~7~. -of ___L
.
Datemme
Sample ID/Location Matrix Sampled Lab ID Remarks Total
~.:.)u-.} .. -;J' L. 'i/61'%~ (C, 3 I ( t /1 I '
Ci'--1 !--(c,.l -( D L /; 0.5-0
?c.:,L.:, -I l., /,i?S-3 1 1 '1 /1 , .
(_/'--1 MW .o.5 L /i$1<-9
I:?.:, , I l 'V /1::,ot, ."': f , J/t l
s
Sample Matrix: L = Liquid; S = Solid; A = Air , <Jf!: ~) Total No. ~~!~f~'=~ f:(
Relinquished by: _;,,~·L.· /L'.-'~/.;:;;j~==-=-· ___ Organization:_,L/., /7.',-:'"<"s..:r=~·J/.:..'.-<..~-=--,.----Date <',:11 G / o;:::J Time 1Kiti Seal Intact?
Received by: //7 '!/ ~ , , ; Organization: c .r, -<" LI ~ Date 3/l 7: l O O Time tf: {.l D ~·No N/A
Relinquished by: ______ -_____ Organization: ___ ~-------Date_~'-~'--Time ____ _ Seal Intact?
Received by: Organization: Date ' ' Time Yes No N/A
Special Instructions/Remarks: ___________________________________________ _
Delivery_l\t'Lethod: □ In Person
111!1111!!!!1:1 ----
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. · Nanjun Shetty
ARCADIS Geraghty_& Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l70.
Sampled By:.Client
Code: 095600512
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
02502-1 DISCHARGE 04-18-00/10:40
PARAMETER 02502-1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1;2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
<l.0
<l.0
<l.0
<l.0
<l.0
<l.0
<10
<10
<1.0
<l.0
<l.0
<l.0
<l.0
<2 .0
102 %-
-Surrogate -4-Bromofluorobenzene 94 %-
Surrogate -Dibromofluoromethane 106 %-
Dilution Factor l
Analysis Date 04.25.00
Batch ID 1B0424
Cyanide (335.2), ug/1 19
Dilution Factor 1
Prep Date 04.25.00
Analysis Date 04.25.00
Batch ID 0425S
•Ol>hllooolS...mT"<t-.1.., 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
. Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02502
Received: 19 APR 00
Reported:27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0i70
Sampled By: Client
Code: 095600512
Page 1
DATE/
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
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025 02 -l DISCHARGE 04-18-00/10,40 I
----------------------
PARAMETER 02502-1
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <1,0
Bromomethane (Methyl <l. o
bromide) , ug/1
Vinyl chloride, ug/1 <l. o
Chloroethane, ug/1 <l. 0
Methylene chloride <5.0
(Dichloromethane), ug/1
Acetone, ug/1 <25
Carbon disulfide, ug/1 <l. O
1,1-Dichloroethene, ug/1 <1.0
1·, 1-Dichloroethane, ug/1 <l. 0
cis-l,2~Dichloroethene, ug/1 <1.0
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2·-Dichloroethane, ug/1 <1.0
2-Butanone (MEK) , ug/1 <10
1,1,1-Trichloroethane, ug/1 <1.0
Carbon tetrachloride, ug/1. <1.0
Bromodichloromethane, ug/1 <l. 0
1,1,2,2-Tetrachloroet~ane,.ug/l <1.0
1,2-Dichloropropane, ug/1 <1.0
trans-1,3-Dichloropropene, ug/1 <1.0
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,_d_,,_,,.___..,_ 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27.APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 095600512
Page 4
DATE/
LOG NO
02502-2
02502-2-DL
02502-3
02502-3-DL
02502-4
SAMPLE DESCRIPTION, LIQUID SAMPLES
PW•l
TIME SAMPLED
04-18-00/09:50
04-18-00/09:50
04-18-00/10:00
04-18-00/10:00
04-18-00/10:10
PW·l·
PW-2
PW-2
PW-3
---------------------------------------------------
PARAMETER 02502-2 02502-2-DL
1,1,2,2-Tetrachloroethane, ug/1
1, 2-Dichloropropane·, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibrornochlorornethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Brornoforrn, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachlor9e~hene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluorornethane
<10
<10
<10
5800E
<10
<10
<10
<10
<10
<100'
<100
770
<10
<10
<10
<10
<20
104 %'
96 %'
106 %'
Dilution Factor 10
Analysis Date 04.26.00
Batch ID 1B0426
<50
<50
<50
8400D
<50
<50
<50
<50
<50
<500
<500
830D
<50
<50
<50
<50
<100
100. %'
94 %'
102 %'
50
04.26.00
1B0426
02502·3 02502-3-DL 02502-4
<1.0
<1.0
<1.0
97
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
250E
<1.0
<1.0
<1.0
<1.0
<2.0
104 %'
94 %'
104 %'
1
04.25.00
1B0424
<2.0
<2.0
<2.0
98D
<2.0
<2.0
<2.0
<2.0
<2.0
<20
<20
260D
<2.0
<2.0
<2.0
<2.0
<4 .0
102 %'
96 %'
106 %'
2
04.25.00
1B0425
<2.0
<2.0·
<2.0
47
<2.0
<2.0
<2.0
<2.0
<2.0
<20
<20
410E
<2.0
<2.0
<2.0
<2.0
<4.0
104 %'
96 %'
104 %
2
04.25.00
1B0425
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC : . Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02502
Received·: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Requisition: SQ98-0553
Contract.No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 095600512
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION_, LIQUID SAMPLES TIME SAMPLED
02502-2
02502-2-DL
02502-3
02502-3-DL
02502-4
PW-1
PW-1
Pw-2·
PW-2
PW-3
PARAMETER 02502-2 02502-2-DL
Volatiles by GC/MS (8260)
Chloromethane, ug/1. <10
Bromomethane (Methyl bromide), ug/1 <10
Vinyl chloride, ug/1 18
Chloroethane, ug/1
Methylene chloride'
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
<10
<50
<250
<10
<10
<10
180
<10
<10
<10
<100
<10
<10
<10
<50
<50
<50
<50
<250
<1200
<50
<50
<50
180D
<50
<50
<50
<500
<50
<50
<50
04-18-00/09:50
04-18-00/09:50
04-18-00/10:00
04-18-00/10:00
04-18-00/10:10
02502-3 02502-3-DL 02502-4
<1.0
<1.0
2.9
<1.0
.<5 .0
<25
<1.0
1.2
1.3
32
2.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<2.0
<2.0
2.9D
<2.0
<10
<50
<2.0
l.5DJ
1.4DJ
32D
2.2D
<2.0
<2.0
<20
<2. 0
<2.0
<2.0
<2. o
<2.0
<2.0
<2.0
<10
<50
<2 .0
<2.0
<2.0
72
<2.0
<2.0
<2. o.
<20
<2.0
<2.0
<2.0
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•-ol-T..,.,-lr>t 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02502
· Received: 19 APR 00
Reported: 27 APR 00
Revi·sed: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 095600512
REPORT OF RESULTS Page 6
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
02502-4-DL PW-3
02502-5 PW-4
02502-6 INFLUENT
02502-6-DL INFLUENT
02502-7 TRIP BLANK
PARAMETER 02502 -4-DL .
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
·Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
<2.5
<2.5
<2.5
<2.5
45D
<2.5
<2.5
0.30DJ
<2 .5
<2.5
<25
<25
390D
<2 .5
<2.5
<2.5
<2.5
<5.0
102 %-
94 %-
104 'I-
.Dilution-Factor
Analysis Date
Batch ID
,2 .5
04.25.00
1B0425
02502-5 02502-6
--------------------
<1.0 <10
<1.0 <10
<1.0 <10
<1.0 <10
<1.0 2900E
<1.0 <10
<1.0 <10
<1.0 <10
<1.0 <10
<1.0 <10
<10 <100
<10 <100
<1.0 410
<1.0 <10
<1.0 <10
<1.0 <10
<1.0 <10
<2.0 <20
104 'I-104 'I-
94 'I-96 .%-
106 'I-104 'I-
1 10
04.25.00 04.25.00
1B0424 1B0424
--------------------
DATE/
TIME SAMPLED
04-18-00/10:10
04-18-00/10:20
04-18-00/10:30
04-18-00/10:30
04-18-00
~--------------------~
02502-6-DL 02502-7
--------------------
<25 <1.0
<25· <1.0
<25 <1.0
<25 <1.0
3400D <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<250 <10
<250 <10
430D <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<50 <2.0
102 % 100 %
96 'I-94 'I-
106 % 108 %-
25 1
04.25.00 04.25.00
1B0425 1B0425
--------------------
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box ·31388
Raleigh, NC 27612·
CC: Mr. · Mark Radecke
REPORT OF RESULTS
WG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. N6.: LT0#041300-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 095600512
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------ ---------------------------------------------------------·---------------
02502-4-DL
02502-5
02502-6
02502-6-DL
02502:1
PW-3
PW-4
INFLUENT.
INFLUENT
TRIP BLANK
04-18-00/10:10
04-iS-00/10:20
04·-10-00/10:30
04-18-00/10:30
04-18-00
-- -- ------------------------------- ------------- -- ---------------- -- ------------------ ----
PARAMETER 02502-4-DL
Volatiles by GC/MS (8260)
Chlorornethane, ug/1
Brornornethane (Methyl
bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichlorornethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<2.5
<2.5
<2 .5
<2.5
<12
<62
<2. 5 ·
0.91DJ
<2.5
72D
<2. 5
<2.5
<2.5
<25
<2.5
<2.5
02502-5
<l ;o
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
02502-6 02502-6-DL
<10 <25
<10 <25
<10 7. lDJ
<10 <25
<50 <120
<250 <620
· <10 <25
<10 <25
<10 <25
74 76D
<10 <25
<10 <25
<10 <25
<100 <250
<10 <25
<10 <25
02502-7
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
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·---,--. ..,.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LT0#041300-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: ·Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client.
Code: 095600512
REPORT OF RESULTS Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02502-8 Method Blank
02502-9 Lab Control Standard % Recovery
02502-10 LCS Accuracy _Control Limit (%R)
02502-11 Lab Control Standard Duplicate% Recovery
02502-12 Precision (%RFD) of LCS/LCSD
PARAMETER 02502-8 02502-9 02502-10 02502-11 02502-12
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <1.0
Bromomethane , (Methyl <1. O
bromide), ug/1
Vinyl chloride, ug/1 <1. O
Chloroethane, ug/1 <1.0
Methylene chloride <5.0
(Dichloromethane), ug/1
Acetone, ug/1 <25
Carbon disulfide, ug/1 <1. o
1,1-Dichloroethene, ug/1 <1.0 110 % 46-147 % 106 % 4 %
1,1-Dichloroethane, ug/1 <1.0
cis-1,2-Dichloroethene, ug/1 <1.0
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <1.0
2-Butanone (MEK) , ug/1 <10
1,1,1-Trichloroethane, ug/1 <1.0
Carbon tetrachloride, ug/1 <1.0
LOG NO
5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1) ·
Client PO. No.: LT0#041300-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 095600512
Page 7
DATE/
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
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PARAMETER
------__ : _ -- ----------1
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5102 LaRciche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com •-Ol_,,T_.__ ....
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 095600512
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------ ---------------------------- ----- -------------------------------- -- -----
02502 -8 Method Blank
02502-9 Lab Control Standard \-Recovery
02502-10 LCS Accuracy Control Limit (\-R)
02502-11 Lab Control Standard Duplicate\-Recovery
02502-12 Precision (\-RPD) of LCS/LCSD
-----------------.-----~---------------------------
PARAMETER 02502-8
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
.1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
"Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1.
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
. <10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
104 \-
96 \-
106 \-
1
Analysis Date
Batch ID
04.24.00
1B0424
02502-9
112 \-
116 \-
112 %-
112 \-
104 %-
96 %-
l:04 %-
1
04.24.00
·1B0424
02502-10
56-143 \-
62-135 %-
68-131 %-
72-127 %-
77-122 \-
74-126 \-
70-130 \-
1
02502-11
108 \-
112 %-
108 \-
108 %-
102 \-
94 \-
106 \-
1
04.25.00
1B0424
----------
02502-12
4 \-
4 %-
4 %-
4 \-
---
NA
NA
NA
1
04.24.00
1B0424
----------
5102 LaRocheAvenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Raleigh, NC 27612 Requisition: SQ98-0553
_Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 101700512
REPORT OF RESULTS Page 10
DATE/
LOG NO SAMPLE DESCRIPTION , QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
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-------- -------------------------------------- ----- -----------------
02502-8 Method Blank
----------------------1
02502-9 Lab Control Standard%' Recovery
02502-10 LCS Accuracy Control Limit (\'R)
02502-11 Lab Control Standard Duplicate%' Recovery
02502-12 Precision (\'RPD) of LCS/LCSD
PARAMETER
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02502-8
----------
<5.0
1
04.25.00
04.25.00
0425S
----------
02502-9
----------
104 %'
1
04.25.00
04.25·.oo
0425S
----------
02502-10
----------
85-115 %'
----------
02502-11
----------
101 %'
1
04.25.00
04.25.00
0425S
----------
02502-12
----------
2.9 %'
----------
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 095600512
Page 12
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02502-14 MS %-. Recovery (Batch)
02502-15 MSD %-Recovery (Batch) ·
02502-16 .MS Accuracy Advisory Limit (%-R)
02502-17 Precision (%-RPD) MS/MSD
02502-18 MS Precision Advisory Limit (%-RPD)
PARAMETER 02502-14 02502-15 02502 -16 _02502-17 02502-18
Volatiles by GC/MS (8260)
1,1-Dichloroethene, t
Trichloroethene, \-
Benzene, %
Toluene, %
Chlorobenzene, %-
Surrogate Toluene-dB
99 %-
84 %-
110 %-
108 %-
106 %-
104 %-
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
96 %-
104 %-
1
Analysis Date
Batch ID
Cyanide (335.2),
Dilution Factor
Prep Date
Analysis Date
Batch ID
ug/1
-------------------.----------
04.24.00
1B0424
94 %-
1
04.25.00
04.25.00
0425S
----------
10_1 %-46-147 %-2 %-<30 %-
84 %-56-143 %-0 %-<35 %-
110 %-62-135 %-0 %-<37 %-
108 %-68-131 %-0 % <33 %-
106 %-72-127 %-0 % <22 %-
104 %-77-122 %-NA NA
96 %-74-126 %-NA NA
104 %-70-130 %-NA NA
1
04.24.00
1B0424
90 %-85-115 %-4.3 %-<20 %-
1
04.25.00
04.25.00
0425S
-------------------- --------------------
LOG NO
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02502
Received: 19 APR 00
Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041300-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No·. : JFD Channel Master
· CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 095600512
REPORT OF RESULTS Page 11
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
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02502-13 LCS Precision Control Limit (Advisory) %RPO
----------------------•
PARAMETER 02502-13
Volatiles by GC/MS (8260)
1, 1-Dichloroethene, %' <30 %
Trichloroethene, % <35%
Benzene, % <37%
Toluene, % <33 %
Chlorobenzene, %
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<22 %
NA
NA
NA
1
Analysis Date
Batch ID
04.24.00
1B0424
Cyanide (335. 2), ug/1 <20 %
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- - - - - - - - - - - - - - - -;-- -'2 AR(ADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. CHI 5~-/1-CHAIN-OF-CUSTODY RECORD Page _L of---L.-
Project Number/Name .--.) ~=2-""Z. ct 7"'
Project Location nx {!...,.£ d '-
Laboratory 2ll /Oo v'a., "" I,
Pro1·ect Manager i'J,, ~ ; -.,_ · SL.~ ff 't 7 · · I
Sampler(s)/Affiliation J,,.._""7 k,,:;.,.
Dateffime
Sample ID/Location Matrix Sampled
vW ·· I I-i/1€1--;z; -1.'lt.1
,')w · z l /;=
?w . .3 l 7010
PlA.} -'i L /1020
~ ,, ,+-(_ /;oJcl ...&-.-;,., :·1._,_<..,..,
1--:',~,c : ., .. ,..,_.,.. L ~ /io'-fD -
. i,;::-" ;i--L _ k L 'i //8/Cf.:J
'
I ANALYSIS/ METHOD/ SIZE
Lab ID
3
.3
3
Sample Matrix: L -LiquiM = Solid; A = A~ •
Relinquished bv: / f.// /~ --Organization:~~-=~cso-.1,.,,,'~.,-~L_------Date '/ 1/e, l = Time . ·~ ... .,,,-.· ..• "/./ t -r_/ c:--/_,· a le,, c"' Received b/ --"'~ ,_,. ~ Organization: ~ , ,,__ -,14....)~ Date r I LI . .., Time
" A ,
I
Remarks Total
3
3
Total No. of Bottles/ .:_ z..
Containers
I? <:5'".J Seal Intact?
9;• tZ> ~o N/A
Relinquished by: ____ •• ______ Organization: ___________ Date_~'-~'--Time ____ _
Received by: Organization: Date 1 1 Time ____ _
Seal Intact?
Yes No N/A
Special lnstruct,ons/Remarks: ___________________________ ~----------------
5V (!')2-50:Z....
Delivery Method: □ In Person ~ommon Carrier &J. EA
f SPECIFY
□ Lab Courier □Other _______ _
SPECIFY
•-"'-T....t-.~ · 5102 LaRocheAvenue · Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun·Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02502
Received: 19 APR 00
. Reported: 27 APR 00
Revised: 12 MAY 00 (1)
Client PO. No.: LT0#041300-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 095600512
Page 13
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
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PARAMETER
----------------------1
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the_SL quality control
requirements.
Final Page Of Report
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5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT .OF RESULTS
.SAMPLE DESCRIPTION, LIQUID SAMPLES
02663-1 DISCHARGE_ (14:15)
LOG NO: S0-02663
Received: 26 APR 00
Reported: 03 MAY 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
·code: 100100512
Page 1
DATE/
TIME SAMPLED
04-25-00/14:15
PARAMETER 02663-1
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
15
1
05.02.00
05.02.00
0502T
5102 LaRoche Avenue • Savannah, GA 31404 • (912).354-7858 • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Mi.Iler, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO: S0-02663
Received: 26 APR 00
Reported: 03 MAY 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041900-A
LOG NO
02663-2
02663-3
02663-4
02663-5
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID·SAMPLES
INFLUENT
Requisition: SQ98-0553
Contract No.:_JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 100100512
Page 2
DATE/
TIME SAMPLED
04-25-00/13:40
04-25-00/13:55
04-25-00/16:10
04-25-00
DISCHARGE (13:55)
FINCH
TRIP BLANK
PARAMETER
Volatiles by GC/MS ( 82 60) ·
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, .ug/1
1, 1-Dic.hlaroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
·1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
02663-2 02663-3 02663-4 02663-5
<25 <1.0 <1.0 <1.0
<25 <1.0 <1.0 <1.0
<25 <1.0 <1.0 <1.0
<25 <1.0 <1.0 <1.0
<120
<620
<25
<25
<25
48
<25
<25
<25
<250
<25
<25
<25
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<25 <1.0
<25 <1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
.<1.0
<1.0
<1.0
<10
<1.0
<1.0
<l.O
<l. 0 <l. o·
<l. 0 <l. 0
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02663
Received: 26 APR 00
Reported: 03 MAY 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041900-A
Raleigh, NC 27612' Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202."0170
Sampled By: Client
Code: 100100512
REPORT OF RESULTS Page 3
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
02663'2 INFLUENT
02663-3 DISCHARGE (13:55)
02663-4 FINCH
02663-5 TRIP BLANK
PARAMETER
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Di'chloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1·
Styrene, ug/1
Xyleries, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
-02663-2
----------
<25
3600
<25
<25
<25
<25
<25
<250
<250
280
<25
<25
<25
<25
<50
116 %-
102 %-
108 %-
25
05.02.00
100502
02663-3
----------
<1.0
<1.0
<l .·O
<1.0
<1.0
<1.0
<1.0
<10
<10
<l.0
<1.0
<_1.0
<1.0
<1.0
<2.0
116 %-
102 %-
110 %-
l
05.02.00
100502
DATE/
TIME SAMPLED
04-25-00/13:40
04-25-00/13:55
04-25-00/16:10
04-25-00
02663-4 02663-5
--------------------
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<10 <10
<10 <10
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0'
<1.0 <1.0
<2.0 ·<2.0
116 %-118 %-
102 %-104 'Ir
108 %-110 %-
-1 l
05.02.00 05.02.00
100502 .100502
·'"'"'""'~f<onll.obonol""90.lno. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388.
Raleigh, NC .27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02663
Received: 26 APR oo
Reported: 03 MAY 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 100100512
Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------- -------------------------------------------------------------------------
02663-6 Method Blank
02663-7 Lab Control Standard% Recovery
02663-8 LCS Accuracy Control Limit (%R)
02663 -11 LCS Precision Control .Limit (Advisory) %RPD
---------------------------------.---------------------------------------------------
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene·, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
·2-Butanone · (MEK) , ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
02663-6
<1.0
<l.0
<1.0
<1.0
<5.0
·<25
<LO
<1.0
<l.0
<l.0
<1.0
<l.0
<l.0
<10
<l.0
<l.0
<1.0
02663-7
106 %
1., 1, 2, 2-Tetrachloroethane, ug/1 <l. 0 ---
1,2-Dichloropropane, ug/1 <1.0
02663-8 02663-11
~6-147 %
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02663
Received: 26 APR 00
Reported: 03 MAY 00
Revised: 12 MAY 00 (1) ·
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project:·NC000202.0170
Sampled By:_ Client
Code: 100100512·
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
Method Blank
Lab Control Standard t Recovery
LCS Accuracy Control Limit (tR)
02663-6
02663-7
_02663-8
02663-11 LCS Precision Control Limit (Advisory) tRPD
PARAMETER
trans-1,3-Dichloroprapene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
02663-6 02663-7 02663-8 02663-11
<1.0
<1.0 92 %-56-143 %-
<1.0
<1.0
<1.0 96 t 62-135 %-
<1.0
<1.0
<10
<10
<1.0
<1 .. 0
<1.0
<1.0
<1.0
<2.0
114 t
104 t
110%
1
05.02.00
100502
94 t
96 t
112-%-
106 %-
110 t
1
05.02.00
100502
68-131 %-
72-127 %-
77-122 %-
_74-126 %-
70-130 t
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0~02663
Received: 26 APR 00
Reported: 03 MAY 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.:_JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 101700512
REPORT--OF RESULTS Page 6
LOG NO
02663-6
02663-7
02663-8
02663-11
SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Lirni t ( %R).
LCS Precision Control Limit (Advisory) %RPD
PARAMETER
Cyanide (335.2) ,· ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
----------
----------
02663-6 02663-7
--------------------
<5.0 99 %
1 1
05.02.00 05.02.00
05.02.00 05.02.00
0502T 0502T
---------- ----------
DATE/
TIME SAMPLED
02663-8· 02663-11
---------------------
85-115 %
--------------------
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5102 LaRoche Avenue• Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02663
Received: 26 AP_R 00
Reported: 03 MAY 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke· Project: NC000202.0170
Sampled By: Client
Code: 100100512
REPORT OF RESULTS Page 1
LOG NO
02663-12
02663-13
02663-14
02663-15
02663-16
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
MS Precision Advisory Limit (%RPO)
PARAMETER 02663-12 02663-13 02663-14
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
B~n·zene, % .
Toluene, %'
Chlorobenzene, %
Surrogate Toluene-de
96 %
100 %
104 %
108 %
104 %
106 %
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
104
98
%
%
Dilution Factor 1
Analysis Date 04.28.00
Batch ID 100428
Cyanide (335. 2), mg/1 93 %
Dilution Factor 1
Prep Date 05.02.00
Analysis Date 05.02.00·
Batch ID 0502T
---------------------------------------
98 % 46-147 %.
98 % 56-143 %
104 % 62-135 %
104 .% 68-131 %
102 % 72-127 %
106 % 77-122 %
100 % 74-126 %
96 % 70-130 %
1 1
04.28.00
100428
98 % 85-115 %
1
05.02.00
05.02.00
0502T --------------------
DATE/
TIME SAMPLED
02663-15 02663-16
2 % < 30 %
2 % < 35 %
0 % < 37 %
4 % < 33 %
2 % < 22 %
. NA NA
NA NA
NA NA
1 1
5.2 % <30 %
--------------------
5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC. 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-_02663
Received: 26 APR 00
Reported: 03 MAY 00
Revised: 12 MAY 00 (1)
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 100100512
Page 8
DATE/
LOG NO
02663 · 12·
02663-.13
02663-14
02663-15
02663-16
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
MS t'Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%RPD).
PARAMETER 02663-12
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
02663-13 02663-14 02663-15 02663-16
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Angie W irnerskirk, Project Manager
Final Page Of Report
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Datemine Sample ID/Location Matrix Sampled Lab ID 1~l/11t' .... + l-eJ/2.~/,, n 13.''f, /; s C, J.:.,,-,:;, I-I I I J .'§S°
cl,' < ,,./j,, .,;,,, 8 . I 14:15 ;:,·A, L (I I Jt-:,:10
/J/"?:,1:> I -f\ I/
'
. '
Sam_ pie Matrix: L = Liquid..:_;--,;_S,=,..,1-S..:_ol__:id-.:___; ___ A..:_=_A_ir ____ ___:__,.---,.~-=-·.:.j. ~,-,r,-t,----,.-~-:---c--c-----c,,.Tort.,al_N_o_. '::'.of~B~o~tt~le:'.s/~/::'.':::: ~=; ~ ,s : ,:¥ Containers Relinquished by: .,,,'7,/;;_J-'' ' Organization: Wrc-.d.i,1. " '" 1L./~ ate '-', 7e-, r.n Time,/S -'"b Seallntact? Received by: (I Jf"Y.V ~ •= Organization: $[I. -Sd f ' r Date?' LU I, a Time _____ Yes No N/A Relinquished by: __________ Organization:_· __________ Date _ __,_,'-. _ _,_, __ Time _____ J Seal Intact? Received by: Organization: ... Date 1 1 Time Yes No NIA Special lnstruct1ons/Remarks:~. --------,~-----------"---------------------------&z e f,A.J~<'! k. -C, r /I &2.., .... J
-Delivery Method:·· □ In Person □Lab Courier □Other ______ _
SPEOFY AG DS.OS97
rm
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O.,No 1')£// '100 .I/-CHAIN-OF-CUSTODY RECORD Page _f_ of_{_ .
Project Number/Name All'..@ 2oz •DI 7 b I ANALYSIS I METHOD I SIZE . ·.
Project Location 0-fr,-J , JUL . &'(_ t;-v
1
/
Laboratory sn/ s t;J -;J ~'1. ~h . l_ . -'1)
0
• IL
. :::::::~,;,:"°~J/.~·s i j-' ,, j,} '
. <;i (..J ~,J IQ
Datemme r/,;. ~ l,O Sample ID/Location Matrix Sampled Lab ID Q:i · f\J '' Remarks Total
I I
/J/?.D
w ~ Jf--------+-------+----1
_ J Containers Sample Matrix: L = Liqu;id;t; ':J.'sS ~=i.~,o~li;d;==A==CA~igr ~~;;;;;=~~~~z;:;:.;;UiJ.gbj·t'1=o-;;;--:3_~~=::z:j~~~;:;zT~o:taf;il ~N~o.=o=frB~ott~l;es!~/~~~ Relinquished by: ~ .JI ' ~ Organization: 'Fire,.. -,.,L,-,, /'.: ''' .f J.,/L. ate 4 1 zc' "D Time /:S -'Db Seal Intact? Received by: /l. 1~, -~ Organization: S 11 ~ > '~ .a ;T ·' 1 Date 1/ I?£ I , 1J · Time ____ Yes No N/A
Relinquished by: __________ Organization: ___________ Date __ ~I_,__,_ Time ___ _ Seal Intact? Received by: Organization: Date ' ' Time Yes No N/A
Special lnstruct,ons/Remarks:-;-----,---------,,-------• ------------------'----------f),,, e. w,z ~tc . u ,.,., ace ... .,.,J.
Delivery Method: D In Person - - ---p:t:common Carrier t'.,d ~.K 8LB'/·~7'1)-. □ Lab Courier
---.;. .. ECIFY~',l&>---
□Other ___ -,-___ _
SPECIFY
----•cos, ..
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S,a ,v;a n n-a.h lia'bor·a10,Jes 5102 LaRocheAvenue • Savannah, GA31404·:··c9i2)·354-7s5s • Fax[phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty &
P.O. Box 31388
Raleigh, NC 27612
Miller, Inc.
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LT0#042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 125500512
Page 1
DATE/
TIME SAMPLED
-- ------------------------------- -- -- ---------------------------------------- -------
02852-1 DISCHARGE .05-02-00/1·1:00
----------- ----------------------- ------- ------------------------- ------------------
PARAMETER
Volatiles by GC/Ms· (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1, 1-Dichlo_roethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1·
1,2-Dichloroethane, ug/1
2-Butanone-(MEK) ·, ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
02852-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
s~ a Vrn1 n,,n-'arh l!a bO r.a t 6~r,i e's 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Natijun Shetty
ARCADIS Geraghty & Miller, Inc.
P·.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID. SAMPLES
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 125500512
Page 2
DATE/
TIME SAMPLED
----------- ------------------------- ------------------------------------------------
02852-1 DISCHARGE 05-02-00/11:00
----------- -------------------------------------------------------------------------
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl~2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromof~uorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor·
Analysis Date
Batch ID
02852-1
----·------
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
104 'Ir
98 'Ir
102 'Ir
1
05.08.00
100508
Cyanide (335.2), ug/1 7.9
Dilution Factor . 1
Prep Date 05.11.00
Analysis Date 05.11.00
Batch ID 0511S
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I.:. a b'Or at Or i'e s •-al-Tw<.....,._, ..... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02852
Received: 03 MAY 00
·Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Raleigh, NC 27612 Reguisition:·SQ98-0553
Contra·ct No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 125500512
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
02852-1 DISCHARGE 05-02-00/11:00
---------------------------------------·---------------------------------------------
PARAMETER
Barium (6010)
Barium, mg/1
Dilution Factor
Prep Date
-Analysis Date
Batch ID
Chromium (6010)
Chromium, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Lead (6010)
Lead, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02852-1
0.026
1
05.05.00
05.10.00
0505J
<0.010
1
05.05.00
05.10.00
0505J
<0.0050
1
05:05.00
05.10.00
0505J
S;,?l v \~~m !1.,~a.\h. laborator,1es 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202 .. 0170 ·
Sampled By: Client
Code: 125500512
~age 4
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
--------------------------------------------------------------------------- ---------
02852-1 DISCHARGE 05-02-00/11:00
------------ -------------------------- ----- --------------------- ----------- ----- ----
PARAMETER
Copper (6010)
Copper, mg/1
Dilution Factor
Prep Date.
Analysis Date
Batch ID
Nickel (6010)
Nickel, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Zinc (6010)
Zinc, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02852-1
<0.020
1
05.05.oo·
05.10.00
0505J
<0.040
1
05.05.00
05.10.00
0505J
<0.020
1
05.05.00
05.10.00
0505J
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S,a•Via•in~n a~h
~aboi-at6r'.ies 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 125500512
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
02852-2 INFLUENT 05-02-00/10:30
02852-3 TRIP BLANK 05-02-00
PARAMETER 02852-2 02852-3
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone,· ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-·1, 2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,i-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichioromethane, ugil
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
<25 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<120 <5.0
<620 <25
<25 <1.0
<25 <1.0
<25 <1.0
55 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<250 <10
<25 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
<25 <1.0
5100 <1.0
------------------------------
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
02852-2
02852-3
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
INFLUENT
TRIP BLANK
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 125500512
Page 6
DATE/
TIME SAMPLED
05-02-00/10:30
05-02-00
----------- ------------------------------ -------------------------------------------
PARAMETER
Dibromochioromethane, ug/1
1,1,2-Trichloroethane, ug/1
senzerie, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
02852-2
<25
<25
<25
<25
<25
<250
<250
370
<25
<25
<25
<25
<50
106 'Ir
98 'Ir
102 'Ir
25
05.08.00
100508
02852-3
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
106 'Ir
100 'Ir
102 'Ir
1
05.08.00
100508
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S,ar..v•al n, n,a~h
IE'abO'r.ilt(i'r.ieS 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 125500512
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT_FOR LIQUID SAMPLES TIME SAMPLED
02852-4 Method Blank
02852-5 Lab Control Standard% Recovery
02852-6 LCS Accuracy Control Limit (%R)
PARAMETER 02852-4
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
02852-5 02852-6
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloioethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2:Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1.
trans-1,3-Dichloropropene, ug/1
<1.0 98 t 46-147 %
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
5102 I.aRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Ger.aghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO~042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC0.00202. 0170
Sampled By: Client
Code: 125500512
Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
02852-4 Method Blank
02852-5 Lab Control Standard 'Ir Recovery
02852-6 LCS Accuracy Control Limit ('lrR)
PARAMETER
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluoromethane
Dilution Factor
Anal}'"sis Date
Batch ID
02852-4
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2 .o
104 'Ir
100 'Ir
104 %
1
05.08.00
100508
02852-5
88 'Ir
88 %-
88 %
88 %-
106 'Ir
98 %-
102 %-
1
05.08.00
100508
----------
02852-6
56-143 %-
62-135 'Ir
68-131 %-
72-127 'Ir
77-122 %-
74-126 %-
70-130 %-
1
04 .. 08.00
100408
----------
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98-0553
Contract No. : JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 125500512
REPORT OF RESULTS Page 9
LOG NO
02852-4
02852-5
02852-6
SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES
PARAMETER
Method Blank
Lab Control Standard%-Recovery
LCS Accuracy Control Limit (%-R)
Cyanide (335.2), ug/1
Dilution Factor
Prep'Date
Analysis Date
Batch ID
Barium (6010)
Barium, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chromium (6010)
Chromium, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02852-4
<5.0
1
05.11.00
05.11.00
0511S
<0.010
1
05.05.00
05.10.00
0505J
<0.010
1
·o5.05.oo
05.10.00
0505J
DATE/
TIME SAMPLED
02852-5
97 %
1
05.11.00
05.11.00
0511S
106 1r
1
05.05.00
05.10.00
0505J
104 %-
1
05.05.00
05.10.00
0505J
02852-6
85-115 %-
75-125 1r
75-125 1r
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: _ 125500512
Page 10
DATE/
LOG NO. SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------- ----------------------------- --------------------- ------------------- -- --
02852-4
02852-5
02852-6
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
------ -----. --- -----------------------------------------------
PARAMETER
Lead (6010)
Lead, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Copper ( 6010)
Copper, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010)
Nickel, mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02852-4
----------
<0.0050
1
05.05.00
05.10.00
0505J
<0.020
1
05.05.00
05.10.00
0505J
<0.040
1
05.05.00
05.10.00
0505J
02852-5
----------
102 %
1
05.05.00
05.10.00
0505J
105 %
1
05.05.00
05.10.00
0505J
103 %
1
05.05.00
05.10.00
0505J
02852-6
----------
75-125 %
75-125 %
75-125 %
--------------------------·------------- -------------------- --------------------
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sza ·v,·a~n•n~alh 11abciflttir,i~S 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LT0#042800-A
Contract
Requisition: SQ98-0553
No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 125500512
Page 11
DATE/
LOG NO
02852-4
02852-5
02852-6
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
TIME SAMPLED
PARAMETER
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Zinc (6010)
Zinc, rng/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
02852-4
<0.020
1
05.05.00
05.10.00
0505J
02852-5
102 %
1
05.05.00
05.10.00
0505J
02852-6
75-125 %-
• ......, .. -..rrn.....,_,..,"10. 5102LaRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 125500512
Page 12
DATE/
LOG NO
02852-10
02852-11 .
02852-12
02852-13
02852-14
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED --------------------------------------------------
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%-RPD)
--------------------------------------------------
PARAMETER 02852-10 02852-11 02852-12
--------------------------------------- ---------- ----------
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
92 %
84 %
86 %
86 %
84 %
104 %
96 %
100 %
1
82 %
76 %
78 %
80 %
80 %-
106 %
96 %-
102 %-
1
Analysis Date
Batch ID
04.08.00 04.08.00
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
100408 100408
93 %-88 %
1 1
05.11.00 05.11.00
05.11.00 05.11.00
0511S 0511S
46-147 %-
56-143 %-
62-135 %
68-131 %
72-127 %-
77-122 %-
74-126 %
70-130 %
1
04.08.00
100408
85-115 %
-----------------------
02852-13
----------
11 %-
10 %
10 %
7 %-
5 %
1
04.08.00
100408
5.5 %-
02852-14
----------
< 30 %
< 35 %-
< 37 %-
< 33 %-
< 22 %-
1
04.08.00
100408
<20 %
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr._ Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Rale_igh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
. Client PO. No.: LT0#042800-A
Requisition:" SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 125500512
Page 13
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
02852-10
02852-11
02852-12
02852-13
02852-14 '
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%-RPD)
PARAMETER 02852-10 02852-11 02852-12 02852-13 02852-14
Barium (6010)
Barium, %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chromium (6010)
Chromium, %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Lead (6010)
Lead, %-
Dilution Factor
Prep_Date
Analysis Date
Batch ID
107 %-
1
05.05.00
05.10.00
0505J
108 %-
1
05.05.00
05.10.00
0505J
104 %-
1
05.05.00
05.10.00
0505J
109 %
1
05.05.00
05.10.00
0505J
108 %
1
05.05.00
05.10.00
0505J
105 %-
1
05.05.00
05.10.00
0505J
75-125 %-1. 9 %-<20 %-
75-125 %-0 %-<20 %-
75-125 %-0.96 %-<20 %-
•-"'-T_,_..,_ 5102 LaRocheAvenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO: S0-02852
Received:. 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client.
Code: 125500512
REPORT OF RESULTS Page 14
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
-------------------------------------- -------------------------------------- ----- ---
02852-10 MS 'Ir Recovery(Batch)
02852-11 MSD 'Ir Recovery(Batch)
02852-12 MS Accuracy Advisory Limit ('lrR)
02852-13 Precision ('lrRPD) MS/MSD
02852:14 MS Precision Advisory Limit ('lrRPD)
------------------------------------------------------------- -- ----- ----------------
PARAMETER 02852-13 02852-14 02852-10 02852-11 02852°12
-------------------------------------------------------------------------------
Copper (6010)
Copper, %-
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010)
Nickel, 'Ir
Dilution Factor
Prep Date
Analysis Date
Batch ID
Zinc (6010)
Zinc, 'Ir
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
106 'Ir
1
05.05.00
05.10.00
0505J
106 'Ir
' 1
05.05.00
05.10.00
0505J
104 'Ir
1
05.05.00
05.10.00
0505J
----------
105 % 75-125 'Ir · 0 .95 'Ir
1
05.05.00
05.10.00
0505J
105 'Ir 75-125 'Ir 0.95 % <20 %
1
05.05.00
05.10.00
0505J
104 'Ir 75-125 'Ir 0 % <20 %
1
05.05.00
05.10.00
0505J
----------------------------------------
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5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P,O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-02852
Received: 03 MAY 00
Reported: 11 MAY 00
Client PO. No.: LTO#042800-A
Requisition: SQ98·-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By:'Client
Code: 125500512
Page 15
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
MS 'Ir Recovery (Batch) .
MSD 'Ir Recovery(Batch)
MS Accuracy Advisory Limit (%-R)
Precision (%-RPD) MS/MSD.
02852-10
02852-11
02852-12
02852-13
02852-14 MS Precision Advisory Limit (%-RPD)
PARAMETER 02852-10
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
02852-11 02852-12 02852-13 02852-14
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
~
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No o</28 Ck>-,1-. CHAIN-OF-CUSTODY RECORD Page ----L-. 0 f__i_
Project Number/Name t,k <'.YY2Za2'.. 01-z.n I ANALYSIS/ METHOD/ SIZE I
Project Location ~Fvt:6,,..~-~ L<../,.-k.,<L 1---, • .,-h.-{ nJ ' Laboratory .S:,.(. -3:a {9~-• l. t-.c-l,:;. v" "
Project Manager JJ.,...,t_ ~b~ ' ·'-',V IV V, ~i '-V . ',;, • ~~ . J(I\: -{kf ~ Sampler(s)/Affiliation ,J:;i,..,..::...lS_
'-' \.J if; v:,..
\g J' '-<"'? .! ' :f 0~ Date/Time A_V O ~ ~ D,i?(! El <l Sample ID/Location Matrix Sampled Lab ID * •V~,v ~ /:j Remarks Total
c;:::::,(lf _ -1-. L. p/=· s -~ /?o,o
17\-c_l. (., ~~. ~ I I 5 r•<. //«:> , .
~
/-.•c-, f.._! ¥/; L £/~ ~
.
Sample Matrix: L =,,.Li~= Solid; ~ Total No. of Bottles/ LL. Containers
Relinquished by: · Organization: Date Time Seal Intact?
Received by: c.~ Organization: S-q -),:lv' £A6~ Date ..-1 l Cl!:::.~ Time g_:c,: Yes No N/A ~
Relinquished by: Organization: Date Time Seal Intact?
Received by: Organization:· Date Time Yes No N/A
0
Delivery Method: □ In Person __ , ___ , __ ... -h Gx SPECIFY ---□ Lab Courier □Other ___ -c==----
i.....:..:z..c 5'2_ SPECIFY \---•-,iiiis5----AGO> ..
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~ ARCADIS GERAGHTY&MILLER
Laboratory Task Order Task o,dec No.: DL/28 oo-1/
ARCADIS Geraghty & Miller Office: K,:i /'---//4 "1. • ,v C... Phone: &/('J, ]!N.., 55 I ( Date: '-1-28-o O
Address: /.e;c, \ fl> • J 5 br, , £, '.£/() 7 4 &, ',1 /1.J {., Pcoject Numbec: _,.,N,._,t..,:c_,.b,.bc.ch,_,,Z.ee<>"--'Z~·~O~l _7~"--
r---, I ~/ r---1 II 1---------, 1
1v 27 I, o,b Laboratory Reporting Level: L____J ~ L____J L____J ~ NJDEP Reduced c::::::::::J GISKEY Disks
P,ojectName: :tF-J> z-/, ,+-lb"'-LJ,S ob :,-,M,j /4.u,<;;-tr-Location: Oc/:rd. ~ ,
Lab Pmvides Sample Containecs? ~ Yes
I
c::::::::::J No Date Requi,ed: 5 -/ --12 0 Ship T: kai;,{ f J '1os-:o '1
Estimated Date Of Sample Receipt By Labocatory: 5""~ J-o O Report Due: / t,.,,./4.,, ,:;f:k.r;.
Reports Delivered To: A)o 1, /~1 ).<,_ ,ti:._,., Number Of R:: .... -a::.c.e,/
Work Description: ___ .>,=-\,P'"-'~1,.':-'':.:='---'$,,_="'":'::.ri_c_,'..,__/,-'-;",l.;-=---------------------------------
IIJ,. -,~.,. 51 .IL ' {I Send Invoice To:
• Oet. #
PHYSICAL PROPERTIES Water Method Limit , Soil
pH
Spec. Cond.
Hardness (total)
TOS
TSS
Temperature
Turbidity
1gnitability
Corrosivity
Reactivity
TCLP Extraction
TCLP Complete
METALSU
Aluminum
Antimony
Arsenic
Barium I {,b/O
Beryllium
Cadmium
Calcium
Chromium I l/J ft,
Hex Chromium
Copper I 1,,, I o
Iron
lead I t.n io
Maqnesium
Manoanese
Oet.
Method Limit NON-METALLICS
Acidity
Alkalinity (Total)
Carbonate
Bicarbonate
Bromide
Chloride
Cyanide
Fluoride
Ammonia
Nitrate
TKN
Nitrite
Phosphorus
Silica
Sulfate
Sulfide
Surfactants (MBAS)
ORGANICS
BOO
COD
TOC
TRPH
Phenols"
Pesticides/PCBs"
PNAs"
Org. Phos. Pest."
Dioxins
• Water Method
Oet .
Limit
#
Soil Method
Det.
Limit
Mercurv Chier. Herb."
~N~k,,,,,,_1 ------+_,_l_41LJlnuf_(J!<.j. __ -l---+----l---+V"'o"''":::;'o.•::,0:,'9e,'"c:;,:,a" ___ -1~~"1,U.JF("--'Z"'' t,..o""--"l.).-~'cs'-'::1--~e----+---~
Semi Volatile Organics" 7..,-L '-~· Potassium
Selenium APPENDIX IX" ' Cl
Silver RADIONUCLIDES
Sodium Gross Alpha
Thallium Gross Beta
Radium 226
Vanadium Radium 228
Zinc I f,0/ 0
Priority Pollutant Metals"
TAL Metals"
"Metals are Total Metals Unless Specified as Dissolved Under Special lnnructions. "Attach Table of Elements or Compounds to be Analyzed. "Includes All Organic and Inorganic Compounds.
Special Instructions Or Other: ____________________________________________________ _
AG&M Project Manager Signature: ______________ Date: ______ AG&M QA Officer Signature: ____________ Date: _____ _
laboratory Acceptance: Date:------
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l!a bO l'.-a tO r,ie 'S 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
03010-1 DISCHARGE
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 121100517
Page 1
DATE/
TIME SAMPLED
05-09-00/11:40
PARAMETER 03010-1
Cyanide (335.2), ug/1 13
Dilution Factor 1
·Prep Date 05 .16. 00
Analysis Date 05.16.00
Batch ID 0516S
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 121100517
Page 2
DATE/
TIME SAMPLED
----------- -------------------------------------- ------------
03010-1 DISCHARGE
----------- --------------------------------------------------
PARAMETER 03010-1
-----------------------------------------------------------
Volatiles by GC/MS (8260)
· Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1 ·
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
·sromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.0
<10
<1.0
<1.0
<1.0
<1.0
<l.·O
<1.0
<1.0
<1.0
--------------------------------------- --------------------
05-09-00/11:40 11
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P,O. Box 31388
Raleigh, NC 27612
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 121100517
REPORT OF RESULTS Page 3
LOG NO SAMPLE DESCRIPTION LIQUID SAMPLES
·03010-1 DISCHARGE
PARAMETER 03010-1
1,1,2-Trichloroethane, ug/1
Ben~ene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1_
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene,. ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<l. 0
<1.0
<2.0
102 %
96 %
102 %-
1
05.16.00
1A0516
DATE/
TIME SAMPLED
05-09-00/11:40
S·a~vtaf n~niarh llabOr.'a'tctr/e's 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] , www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 121100517
Page 4
DATE/
TIME SAMPLED
----------- ----------------------------- -- ------ - - ----------- ----- ------------------
03010-2 INFLUENT 05-09-00/11:20
03010-3 TRIP BLANK 05-09-00
----------- ------------- ---------------- -------- - ------------------ -----------------
PARAMETER 03010-2 03010-3
-------------------------------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
l,i,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
<50
<50
<50
<50
<250
<1200
<50
<50
<50
69
<50
<50
<50
<500
<50
<50
<50
<50
<50
<50
4600
----------
<1.0
<1.0
<l.0·
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<l.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
--------------------
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,_ .. _1 ___ .., 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr .. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 121100517
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03010-2 INFLUENT 05-09-00/11:20
03010-3 TRIP BLANK 05-09-00
PARAMETER 03010-2 03010-3
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Sllrrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
,Batch ID
--------------------
<50 <1.0
<50 <1.0
<50 <1.0
<50 <1.0
<50 <1.0
<500 <10
<500 <10
430 <1.0
<50 <1.0
<50 <1.0
<50 <1.0
<50 <1.0
<100 <2.0
100 %-100 %-
94 %-96 %-
102 %-102 %-
50 1
05.16.00 05.16.00
1A0516 1A0516
----------
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 121100517.
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID·SAMPLES TIME SAMPLED --------------------------------------------------
03010-4
03010-5
03010-6
Method Blank
Lab Control Standard I Recovery
LCS Accuracy Control Limit (IR)
--------------------------------------------------
PARAMETER 03010-4 -----------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
ci~·-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<l.0
<1.0
<1.0
--------------------------------------- --------------------
03010-5 03010-6
104 % 46-147 I
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•-.,.....,,r,.,,.~..._ 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#04l900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l70
Sampled By: Client
Code: 121100517
Page 7
DATE/
LOG NO SAMPLE DESCRIPTION,· QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------- --------------------------------------- ----------------------------------
03010-4 Method Blank
03010-5 Lab Control Standard% Recovery
03010-6 LCS Accuracy Control Limit (%R)
PARAMETER 03010-4
Trichloroethene, ug/1
Dibromochloromethane, ug/1
l,l,2-Trichloroethane, ug/1
Benzene, ug/1
cis~l,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<l.0
"<l.0
<l.0
<l.0
<l.0
<l.0
<10
<10
<1.0
<l.0
<l.0
<l.0
<l.0
<2.0
102 %
96 %
100 \-
l
05.16.00
lA05l6
03010-5 03010-6
100 \-56-143 %
106 %-
106 %-
108 \-
100 \-
94 \-
102 \-
l
05.16.00
lA05l6
62-135 \-
68-131 %
72-127 \-
77-122 %-
74-126 %-
70--130 %-
-------------------------------------------------------------------------------
•-.. a~T,.noL>oororon•.lno. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 121100517
Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03010-4 Method Blank
03010-5 Lab Control Standard% Recovery
03010-6 LCS Accuracy Control Limit (%R)
PARAMETER 03010-4
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<5.0
1
05.16.00
05.16.00
0516S
03010-5 03010-6
94 % 85-115 %
1
05.16.00
05.16.00
1516S
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5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 121100517
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03010-10 MS% Recovery(Batch)
03010-11 MSD % Recovery(Batch)
03010-12 MS Accuracy Advisory Limit (%-R)
03010,.13 Precision (%'RPO) MS/MSD
03010-14 MS Precision Advisory Limit (%RPD)
PARAMETER 03010-10 03010-11 · 03010-12
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %-
Toluene, %
ChlorObenzene, %
Surrogate Toluene-dB
106 %'
100 %
108 %
108 %
108 %
100 %
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
96 %
100 %'
1
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution-Factor
Prep Date
Analysis Date
Batch ID
05.16.00
1A0516
95 %
1
05.16.00
05.16.00
0516S
114 %
106 %
112 %-
114 ,.
114 Ir
100 Ir
98 Ir
102 Ir
1
05.16.00
1A0516
89 %
1
05.16.00
05.16.00
0516S
46-147 ,.
56-143 %
62 -135 %'
68 -131 %'
72-127 %'
77-122 Ir
74-126 %'
70-130, Ir
85-115 %'
03010-13 03010-14
7 ,. < 30 %
6 % < 35 %'
4 % < 37 ,.
5 % < 33 ,.
5 Ir < 22 Ir
6.5 Ir <20 %-
--------------------------------------- -------------------- --------------------
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03010
Received: 10 MAY 00
Reported: 17 MAY 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 121100517
Page 10
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03010-10
03010-11
03010-12
03010-13
03010-14
PARAMETER
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R).
Precision (%RPO) MS/MSD
MS Precision Advisory Limit (%RPO)
03010_-10 03010-11
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
03010-12 03010-13 03010-14
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
,, .,,
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~ ,.. ., ·, -~· , ... ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. ____ _ ,_ CHAIN-OF-CUSTODY RECORD Page ___L_ of_/_
Project Number/Name l\'k-?--?2o?. co;; 1-c,. ~--...,,.x;.
Project Location _C~'llc;\b1~1 =~-J<)::..~--------
Laboratory~ ·~ .ra.-,-1-/,._ l.jzs
ANALYSIS/ METHOD/ SIZE I
Project Manager /-Jc.":~~-S,~f[1
Sampl~r(s)/Affiliation {. M <--:':i'S.,;__
Sample ID/Location
/
Matrix
l
L
Datemme
Sampled Lab ID Remarks Total
3
3 ;
f----· -----+---+-----l--1---+----+---+-------l----lR LJ!5-f!
Sample Matrix: L ; ~qu~S ; Solid; A ; Air , Total No. of Bottles/ J Containers
Relinquished by: I / // /-. ----Organization: ft----f, •, -:..--J' V,tl ,,,V , ~·,/ ,.,_ - , Received by: ·'-' --? ,-/,,, Organization: --' r II I>
Date '"i L 1 l ~J Time l'2~ ~I Intact?
Date -S:uo l ,:, o Time 'ff'; ~-5 No N/A
Relinquished by: ____ f __ v· ______ Organization: ___________ _ Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Delivery Method: □ In Person ~o_ mmon Carrier j;J,c.,,.,.-
.....__ SPECIFY
□ Lab Courier □ Other __ ----c=---srEc1Fv AG 05--0597
,,;
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•-.. -T,.,.,._,,_,.., 5102 LaRoche Avenue , Savannah, GA 31404 •· [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 172500530
Pagel
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03240-1 DISCHARGE 05-16-00/15:40
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-l,2°Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane; ug/1
2-Butanone (MEK), ug/1
1,1,l-Trichloroethane,·ug/l
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
03240-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
S B•N' a.ninra,h
t!aOO r:ato r,re·s ·-.. -·-~...,_ 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty.
ARCADIS Geraghty. & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 172500530
Page 2
DATE'/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03240-1 DISCHARGE 05-16-00/15:40
---------------------------------------------------------------------- --------------
PARAMETER 03240-1
-------------------------------------------------------------------------------
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<l.0
<10
<10
<1.0
<1.0
. <1.0.
<1.0
<1.0
<2.0
96 %-
9 2 %-
96 %-
1
05.24.00
1B0524
Cyanide (335.2), mg/1 0.012
Dilution Factor· 1
Prep Date 05.23.00
Analysis Date_ 05.23.00
Batch ID 0523S
-------------------------------------------------------------------------------
,,
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY oo
Client PO. No.: LTO#032800-C
Raleigh, NC 27612 ·Requisition:-SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke. Project: NC000202.0190.0001
Sampled By: Client
Code:· 172500530
REPORT OF RESULTS Page"3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03240-2 TRIP BLANK 05-16-00
.PARAMETER
Volatiles by GC/MS (8260)
Chlorornethane, ug/1
Brornornethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichlorornethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1, 2_-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride; ug/1
Brornodichlorornethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibrornochlorornethane, ug/1
03240-2
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
5102 LaRocheAvenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LTO#032800-C
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD.Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 172500530
REPORT OF RESULTS Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03240-2 TRIP BLANK 05-16-.00
PARAMETER
1,1,2-Trichloroethane, ug/1
, Benzene, ug /1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluorornethane
Dilution Factor
Analy.sis Date
Batch ID
03240-2
<1.0
<1.0
<1.0
<1.0
<10·
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
94 \-
. 92 \-
94 %-
1
05.24.00
1B0524
I\
.1,
,,)
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
Client PO. No.: LTO#032800-C
_Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD·Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 172500530
REPORT OF RESULTS Page 5
LOG NO SAMPLE DESCRIPTION ; QC REPORT FOR LIQUID SAMPLES
03240-3 Method-Blank
03240-4 Lab Control Standard% Recovery
03240-5 LCS Accuracy Control Limit (%-R)
PARAMETER 03240-3
Volatiles by GC/MS (8260).
Chlorornethane, ug/1
Brornornethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichlorornethane), ug/1
Aceto1:1e, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Brornodichlorornethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<LO
<1.0
<1.0
DATE/
TIME SAMPLED
03240-4 03240-5
104 % 46-147 %
•-ol-T..r11ution-.no. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr_. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 172500530
Page 6
DATE/
LOG NO
03240-3
03240-4
03240-5
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
PARAMETER
-------------------·----------~--------------------
Method Blank
Lab.Control Standard Ir Recovery
LCS Accuracy Control Limit (%-R)
03240-3 03240-4 03240-5
-------------------------------------------------------------------------------
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK) ,· ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ·ug/1
Surrogate Toluene-dB
·surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
94 %-
92 %-
94 %-
1
05.24.00
1B0524
94 Ir 56-143 Ir
96 'Ir 62-135 %-
92 'Ir 68-131 %-
94 %-72-127 %-
94 %-77-122 %-
92 %-74-126 %-
94 %-70-130 %-
1
05.24.00
1B0524
I'. ,·
rf
<,
1
'I
:!I
I
,1
!II
11\
I
11
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I·
1J!
I
1·
I
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab:com
Mr. Nanjun Shetty
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LTO#032800-C
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 172500530
REPORT OF RESULTS Page 7
LOG NO
03240-3
03240-4
03240-5
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
PARAMETER
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Cyanide (335.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
03240-3
<0.010
1
05.23.00
05.23.00
0523S
DATE/
TIME SAMPLED
03240-4 03240-5
102 % 85-115 %
1
05.23.00
05.23.00
0523S
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box.31388
Raleigh, "NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
Client PO. No.: LTO#.032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client.
.DATE/
Code', 172500530
Page 8
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
--------------------------------- - ----------------------- ---- ---------------- -- -- ---
03240-9
03.240-10
03240-11
03240-12
03240-13
MS 'Ir Recovery(Batch)
MSD 'Ir Recovery(Batch)
MS Accuracy Advisory Limit ('lrR)
Precision ('lrRPD) MS/MSD
MS Precision Advisory Limit ('lrRPD)
--- ----- ---------------------------------------------------------------------- ------
PARAMETER 03240-9 03240-10 03240-11 03240-12 03240-13
--------------------------------------- ---------- ------------------------------
Volatiles by GC/MS (8260)
1,1-Dichloroethene, 'Ir 100 % 108 .,.. 46-147 % 8 'Ir < 30 %
Trichloroethene, 'Ir 92 % 102 'Ir 56-143 'Ir 10 'Ir < 35 %
Benzene, 'Ir 94 % 104 'Ir 62-135 'Ir 10 % <" 37 %
Toluen~, 'Ir 90 'Ir 100 'Ir 68-131 'Ir 10 'Ir < 33 'Ir
Chlorobenzene, %-92 %-100 'Ir. 72-127 %-8 %-< 22 'Ir
Surrogate Toluene-dB 94 'Ir 94 'Ir 77-122 %-< NA 'Ir
Surrogate -4-Brornofluorobenzene 92 'Ir 92 %-74-126 'Ir < NA %-
Surrogate -Dibromofluoromethane 92 'Ir 92 %-70-130 %-< NA 'Ir
Dilution Factor 1 1
Analysis Date 05.24.00 05.24.00
Batch ID 1B0S24 1B0S24
Cyanide (335 .2), 98 'Ir 96 'Ir 85-115 %-2.1 %-<20 'Ir
Dilution Factor 1 1
Prep Date 05.23.00 05.23.00
Analysis Date 05.23.00 05.23.00
Batch ID 0523S 0523S
----------------------·---------------------------------------------------------
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s:ai v~a1n4n\a h wa1ro r,Btor.re·s 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O." Box 31388
LOG NO: S0-03240
Received: 19 MAY 00
Reported: 30 MAY 00
Client PO. No.: LTO#032800-C
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 172500530
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03240-9 MS% Recovery(Batch)
03240-10 MSD % Recovery(Batch)
03240-11 MS Accuracy Advisory Limit (%R)
03240-12 Precision (%RPD) MS/MSD
03240-13 MS Precision Advisory Limit (%RPD)
PARAMETER 03240-9 03240-10 03240-11 03240-12 03240-13
These test results meet all the requirements of NELAC. All. questions·
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
)m,1!
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. ____ _ CHAIN-OF-CUSTODY RECORD Page _I_ of--1_
Project Number/Name NC-=zoz:. ~ 110. <:>cooc;
Project Location _,c'.>=A=fu~"'J,,--J.Ct,l",,.,(~-------
LaboratorySTL /s;,<@.,., .. l, L,.b_,
I ANALYSIS/ METHOD/ SIZE
Project Manager AJ....,:.,.. ~ SI, ~11-y 1 Sampler(s)/Affiliation "\/ere,,,;..,_.:,. f-11... ~ [a,..._...-1
Datemme
Sample ID/Location Matrix, ,Sampled Lab ID
.1 i),-.l J.. .-G-L '?t'-1/,e,110
I
'Tr: ., 1.. ;_ ., 1,, I ,!//C:100
Sample Matrix: L = Liquid· S = Solid; A _, A = Air
..3 I
Relinquished y: __________ Organization: __________ _
Received by: Organization:
Date s·1 Ir: I cro
Date ;it (f IO 6
Date
Date
I
Remarks Total
Total No. of Bottles/ -Z..
Containers ~'~~
Time ?,~ s I Intact?
Time No N/A
Time Seal Intact?
Time Yes No N/A
Special lnstructions/~arks: ___ -.-------m~---,.=---c-----s-----r--------------------
l(t:..1"' /71, Vu< / kkc-6 ,_,,p;.</" '-~U-fL Kee c.r/--. . ., I'\,, c_c/;0
Delivery Method: □ In Person 12'!--Common Carrier ,.....,,_J EJ<.. □ Lab Courier □Other ---SPECIFY --•-~----------.----,SccPEccCIFY=-c----
_:~ --(Jl!II AGOS-
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
LOG NO: S0-03334
Received: 24 MAY 00
Reported: 05 JUN 00
Mr. Nanjun Shetty
ARCADIS Geraghty &
P.O. Box 31388
Raleigh, NC 27612
Miller, Inc. ':1 Client PO. No.: LTO#032800-C
LOG NO
\\·~.
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: .NC000202. 0190. 0001
Sampled By: Client
Code: 11270065
Page 1
_DATE/
TIME SAMPLED
03334-1 DISCHARGE 05-23-00/14:00
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1·, 1.-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1·, 1, 2, 2 -Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
03334-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0"
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
S~a~v-~a. ntma~h lfEibor,a·fol".iffs· 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARO\DIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03334
Received: 24 MAY 00.
Reported: 05 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 11270065
Page 2
DATE/
TIME SAMPLED
------------------------------------- ----------------------------------------- ------
03334-1 DIS.CHARGE 05-23-00/14 :00
------- - - - ------------------------------------ --------------- ------------------ -- ---
PARAMETER 03334-1
----------------------------------------------------------- ---------- ----------
1;1,2-Trichloroethane, ug/1 <1.0
Benzene, ug/1 <1.0
cis-1,3-Dichloropropene, ug/1
Bromofonn, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
·chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate -Toluene-dB
Surrogate -·4-Bromofluorobenzene
Surrogate -Dibromofluoromet~ane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
.Analysis Date
Batch ID
<l. 0
<1.0
<10
<10
<1.0
"<1.0
<1.0
<1.0
<1.0
<2.0
98 'Ir
90 'I;
84 'I;
1
05.26.00
1B0526
13
1
06. 01. 00
06.01.00
0601T
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Ma_rk Radecke
REPORT OF RESULTS
.
LOG NO: S0-03334
Received: 24 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract ·No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 11270065
Page 3
DATE/
LOG NO SAMPLE DES~RIPTION, LIQUID SAMPLES TIME SAMPLED
03334-2 TRIP BLANK 05-23-00
PARAMETER 03334-2
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyi bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1 ·
Carbon disulfide·, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
BrornOdichloromethane, ug/1
l,1,2,2-1"etrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochioromethane, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<l.0
<1.0
<1.0
<1. 0
<10
<1.0
<1.0
<1.0
<1. 0 ·
<1.0
<1.0-
<1.0
<1.0
•-"'s...n,r,...uoo,a.,.....n,. 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty'& Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03334
Received: 24 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code·, 11270065
Page 4
DATE/
TIME SAMPLED
03334-2 TRIP BLANK 05-23-00
--------------------------------------------------------------------------- ----- ----
PARAMETER
----- ----------------------·-- ---------- ----------
1,1,2-Trichloroet~ane,'ug/1
Benzene, ug/1
cis-1,3-Dichloropropene; ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Brornofluorobenzene
Surrogate -Dibrornofluorornethane
Dilution Factor
Analysis Date·
Batch ID
. 03334-2
<1.0
<1.0
<1.-0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
96 %-
90 %-
84 %-
1
05.26.00
1B0526
--------------------------------------- ---------- ---------- --------------------
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
_Mr. Nanjun Shetty .
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO: S0-03334
Received: 24 MAY 00
Reported: 05 JUN 00,
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No. : JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 11270065
REPORT OF RESULTS Page 5
DATE/
LOG NO
03334-3
03334-4
03334-5
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bro;.omethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane; ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/i
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1, 1, 2 ,·2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
03334-3
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0'
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
trans-1,3-Dichloropropene, ug/1 <1.0
03334-4
94%
03334-5
46-147 %
5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller·, Inc.
P.O. Bcix 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03334
Received: 24 MAY. 00
Reported: 05 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 11270065
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03334-3 Method Blank
03334-4 Lab Control-Standard%-Recovery
03334-5 LCS Accuracy Control Limit (%-R)
PARAMETER 03334-3
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene,· ug/1
·xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10_
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
96 %-
90 %-
86 %-
1
05.26.00
1B0526
03334-4
94%-
102%-
94%
90%-
96%-
90%-
84%-
1
05.26.00
1B0526
03334-5.
56-143 %-
62-135 %-
68-131 %-
72-127 %-
77-122 %-
74-126 %-
70-130 %-
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St~• .. v~~~nrtn~_~th tabo,;ator.1es 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty.
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03334
Received: 24 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampied By: Client
Code: 11270065
Page 7
. DATE/
LOG NO SAMPLE DESCRIPTION; QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03334-3 Method Blank
03334-4 Lab Control Standard% Recovery
03334-5 LCS Accuracy Control Limit' (%R)
PARAMETER 03334-3
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<5.0.
1
06.01.00
06.01.00
0601T
03334-4 03334-5
96 % 85-115 %
1
'06. 01. 00
06.01.00
0601T
5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03334
Received: 24 MAY 00
Reported: 05 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 11270065
Page 8
DATE/
LOG NO
03334-9
03334-10
03334-11
03334-12
03334-13
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED --------------------.---------------------------c --
MS %-Recovery (Batch)
MSD %-Recovery(Batch)
MS Accuracy Advisory Limit (%-R)
Precision (%-RPD) MS/MSD
MS Precision Advisory Limit (%-RPD)
----------- -------------------------- --------------------------------------------- --
PARAMETER '03334.9 03334-10 03334-11 03334-12 03334-13
--------------------------------------- ----------------------------------------
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %-
Trichloroethene, %
Benzene, %-
Toluene, % .
Chlorobenzene, %-
Surrogate Toluene-dB
104%-
100%
108%-
102%-
96%
98%
92%
84%-
Surrogate -4-Bromofl~orobenzene
Surrogate -Dibromofluoromethane
Dilution Factor 1
05.29.00 Analysis Date
Batch ID
Cyanide (335.2),
Dilution Factor
Prep Date
Anaiysis Date
Batch ID
ug/1
---~-----·--------------------
1B0529
99 \-
1
06.01.00
06.01.00
0601T
----------
9 8%-46-147%-6% <30%-
96%-56-143%-4%-<35%-
104% 62-135%-4% <37%-
98% 68-131\-4%' <33%
92 Ir 72-127%-4%-<22%-
96%-77-122\-N/A N/A
90% 74-126\-N/A N/A
84% 70-130\-N/A N/A
1 1 1 1
05.29.00 05.29.00 05.29.00 05.29.00
1B0529
90 \-85-115 %-9.5 %-<30 %
1
06.01.00
06.01.00
0601T
---------- ------------------------------
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LOG NO
03334-9
03334-10
0_3334-11
03334-12
03334-13
51021.aRocheAvenue • Savannah, GA31404 · [phone] • Fax[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03334
Received: 24 MAY 00
Reported: 05 JUN 00
Client PO. No.: LT0#032800-C
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project:.NC000202.0190.0001
Sampled By: Client . ' Code: 11270065
REPORT OF RESULTS Page 9
SAMPLE DESCRIPTION
MS% Recovery(Batch)
MSD % Recovery(Batch)
Q~ REPORT FOR LIQUID SAMPLES
MS Accuracy_Advisory Limit (%R)
Precision (%RPD)· MS/MSD
MS Precision Advisory Limit (%RPD)
DATE/
TIME SAMPLED
~----;------~----------
PARAMETER 03334-9 · 03334-10 -03334-11 03334-12 03334-13
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEIINR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Angie We' erskirk, Project Manager
Final Page Of Report
Pi.:!
ARCADIS GERAGHTY & MILLER Laboratory Task Order No.IP.a. No. ____ _
Project Number/Name 1k<Z::io.,i::<1Z. c1?0 • ~ I ANALYSIS/ METHOD/ SIZE I
Project Location O(Jt,j 1 )JC
. ,f ;,~ Lab~ratory -:S.TL {~v0 .,.,,, L. _ ~-~
Project Manager. N?J:~ ~ . "-·. .
"' q -1' ~ ,,v -~ ~· ,v3 ':-.J
Sampler(s)/Affiliation: .~ = :/i"~t/-".t, Date/Time
Sample ID/Location Matrix Sampled Lab ID 0£J: ~ . Remarks Total
::i:>, \ r(,_ • ~ <.. L ~2~/7<"" "') I 4 ,, .
i--N., /J.. L 9'z~ ~ '\ . 1--:-:\fj ........
" ,
.
!
-.,.
. 1'lrP fl ~ ~1 ~¥Tl . . . . ~
') CL ~ .. , . -
.
Sample Matrix: L = Liquid;' ~ Solid; A = Air Total No. of Bottles/ ?--, / ·--·· Contciiners
Relinquished by: Organization: Date -512 lc;i::J Time
Received by: _--.-<---__.=c'il-""""2"-~,----Organization:_:c::..L.f==c..::::::._,~=:::_ __ _ Date '>1211<>0 Time
Relinquished by: Organization:~----------Date Time Seal Intact?
Received by: Organization: Date Time Yes No N/A
Delivery Method: · □ In Person ~ommon Carrier_--"~,,...,~_J!~-=;r::::,..x_· __ _
SPECIFY
□ Lab Courier-□Other __ --,--:=:=,----
, SPECIFY ------------- - -- -
AG 0S-0597 - - -
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SiaLyJa 1n: n1,aJ!1 L::aborator,1es 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty_& Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
-i
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
"}\)ij8
Client PO'. No.: LTO#041900-A
Contract
Requisition:_ SQ00-0265
No.: JFD Channel Master
Project:·NC000202.0170
Sampled By: Client
Code: 13400067
Pagel
DATE/
TIME SAMPLED
03488-1 DISCHARGE 05-30-00/14:45
PARAMETER
Cyanide (3·35. 2) , ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
03488-1
14
l
06.01.00
06.01.00
0601T
S,a\ __ v' a:n:mai h
l!""abo•r.at0f.i85' __ .,_,,,,.,.~---= 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION,' LIQUID SAMPLES
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 13400067
Page 2
DATE/
TIME SAMPLED
---------------------------------------------------------------------------- --------
03488-1 DISCHARGE 05-30-00/14:45
----- --------------------------------------- -------------------------- --------------
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromid_e) , ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride. (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1.
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ~g/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
03488-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
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;102 LaRocheAvenue • Savannah, GA 31404 • (912) 3;4-7858 · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO. No.: LT0#041900-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 13400067
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03488-1 DISCHARGE 05-30-00/14:45
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromofoi::m, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
03488-1
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
102 %
98 %
98 %
1
06.06.00
100606
,......,,,,.s.-.r .... _rnc. 5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 13400067
Page 4
DATE/
TIME SAMPLED
---- ------- -------------------------- -- ---------------------------- -------------- ---
03488-2 TRIP BLANK 05-30-00
--------------------------.----------------------------------------------------------
PARAMETER 03488-2
-------------------------------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
<1.0
<1 .. 0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
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S, a\'!}?_tn;il),!~1. h l!abor,atories 5102 L~Roche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No. :.JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 13400067
Page 5
DATE/
TIME SAMPLED
03488-2 TRIP BLANK 05-30-00
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromofonn, ug/1.
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ·ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
03488-2
<l.0
<l.0
<l.0
<l.0
<10
<10
<l.0
<l.0
<l.0
<l.0
<l.0
<2.0
102 %
100 %
96 %
1
06.06.00
100606
5102 LaRocheAvenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab'.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00 ·
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.:·JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 13400067
Page _6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------- ----------------------------- ---------------------
03488-3 Method Blank
03488-4 Lab Control Standard%-Recovery
03488-5 LCS Accuracy Control Limit (%-R)
---------- ------------------- ---------------- ----------------
PARAMETER 03488-3 03488-4 03488-5 --------------------------------------- ---------- ---------- --------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
<1.0
<1.0
<1.0
<1.0
<5. 0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<l. 0
<1.0
<10
<1.0
<l.0
<1.0
<1.0
<1.0
trans-1,3-Dichloropropene, ug/1 <1.0
98% 46-147%-
--------------------------------------- ----------------------------------------)
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5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com •-oJ._,,T,_IMXI<_...,_
Mr_ Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO_ No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 13400067
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03488-3 Method Blank
03488-4 Lab Control Standard%-Recovery
03488-5 LCS Accuracy Control Limit (%-R)
PARAMETER 03488-3
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane,. ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surroga_te Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factqr
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
102 %-
100 %-
98 %-
1
06.06.00
100606
03488-4
98%-
104%-
106%-
108%-
102%-
96%-
98%-
1
06.06.00
03488-5
56-143%-
. 62-135%-
68-131%-
72-127%-
77-122%-
74-126%-
70-130%-
1
06.06.00
5102 LaRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke ·
REPORT OF RESULTS
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 13400067
Page 8
DATE/
LOG NO
03488-3
03488-4
03488-5
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
03488-3 03488-4 03488-5 --------------------------------------- ----------------------------------------
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<5.0 96 % 85-115 %
1 1
06.01.00 06.01.00
06.01.00 06.01.00
0601T 0601T
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s:a,v~a:n) nfa, h lfa'bO r.iito·~ies 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com
.Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 13400067
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03488-9 MS%-Recovery(Batch)
03488-10 MSD %-Recovery(Batch)
03488-11 MS Accuracy Advisory Limit (%-R)
03488-12 Precision (%-RPD) MS/MSD
03488-13 MS Precision Advisory Limit (%-RPD)
.,._ -------------------------------------------------
PARAMETER 03488-9
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %-102%-
Trichloroethene, %-102%-
Benzene, %-106%-
Toluene, %-108%-
Chlorobenzene, % 108%
Surrogate Toluene-dB 102%-
Surrogate -4-Bromofluorobenzene 96%-
Surrogate -Dibromofluoromethane 100%
Dilution Factor
Analysis Date
Cyanide (335 .2),
Dilution Factor
Prep Date
Analysis Date
Batch ID
ug/1
------ -----------------------
1
06.06.00
99 %
1
06.01.00
06.01.00
0601T
----------
03488-10
94%
96%
100%
102%
104%
102%-
96%-
98%
1
06.06.00
90 %
1
06.01.00
06.01.00
0601T
----------
03488-11
46-147%-
56-143%
62-135%-
68-131%
72-127%-
70-130%-
74-126%
70-130%
1
06.06.00
85-115 %
03488-12
8%-
6%
6%-
6%-
4%
0 %-
0 %-
2 %
1
06:06.00
9.5 %
.03488-13
0-30 %-
0-35 %
0-37 %
0-33 %-
0-22 %
N/A
N/A
N/A
1
06.06.00
<30 %-
5102 LaRoche Avenue · Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr_ Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03488
Received: 31 MAY 00
Reported: 07 JUN 00
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No_: JFD.Channel Master
Project: NC000202_0170
Sampled By: Client.
DATE/
Code: 13400067
Page 10
LOG NO SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03488-9 MS% Recovery(Batch)
03488-10 MSD % Recovery(Batch)
03488-11 MS Accuracy Advisory_ Limit (%R)
03488-12 Precision (%RPD) MS/MSD
03488-13 MS Precision Advisory Limit (%RPD)
-------------------------------------- ----------------------------------- --------- --
PARAMETER 03488-9 03488-10 03488-11 03488-12 03488-13 -------------------------------------------------------------------------------
These ·test results meet all the requirements of NELAC. All questions...-
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
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lntersul Billing Reference /\J I., {)OQ ,:;i:i) l,. , J J 7 CJ
----------~ - ---ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. ___ _ CHAIN-OF-CUSTODY RECORD
Project Number/Name IJt., CLX) ·2,f) 2-, u 1 7 Q lr--------:;A-:-N:--:A:-:-L:--:Y-:cSlc::-S-c/-:M-:-:Ecc:Tc.--H:-::O:-::Dc-/.,-S:ccl=cZE=-----------,1
Project Location_ C)-g ii .r cL) N L-JJ(
-·--Page __!,f_L
Laboratory <;,;TI_ S;;i...1~-'\"le 4, 'i.
Project Manager I\\,;" i'v " ~-'eit~ , / ,;i ,, :1' 1-\ A .J,_ r;, .:\ti ... ~ \J'..1 Sampler(s)/Affiliation r .;;I ( ! -rc:.-.J.d.1 Sr 'i,l.... V .._ ...._ / Q ;J / ~._ ,/:'O _ 'l
/<:c,"I -7 ::t ,0 0 Date/Time
Sample ID/Location Matrix Sampled Lab ID
I J I
I .
I
Remarks Total
4
1--t--t-----+-----+-----+---+---------+-----------+--,~ I
'
Sample Matrix: L ; Liquid; S -Solid· ~ :J-I , A ; Air
A , , J • , ,,1
Total No. of Bottles/ "'--7
Containers ·'?""'
Relinquished by~~..,, -'. ·_
Received by: P;>.~ -.
Organization: ~,~L:.'.{ /4~_,...,,J.,,_,r I,. /11, Date;:, t 3.:i I ,...
Organization: -...-;-/ . -c,...-z. Date -S-I ?U I Ou
Time //,.' ,!F> Seal Intact?
Time 9 .' CO Yes · o N/A
Relinquished by: __________ Organization: ___________ Date __ ,__,_c__,_ Time ____ _
Received by: Organization: Date ' I Time ____ _
Seal Intact?
Yes No N/A
Speoal Instructions/Remarks.----:,--,----=,._--------+-' ------------------~d/'---~~..-rf-e#-U"'-'~· '---
One vJ"'ew hcJ_,,.,,, <Jr.,,,~d ?5fl)-a3iii ~
Delivery Method: □ In Person □ Lab Courier □Other __ ----:=cc---
sPEc1Fv
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sra•-v;a ntma~h
L:a b'C>"ra to r,i es 5102 LaRocheAvenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com __ .,_,_,___""'-
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: _LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
_Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03679-1 DISCHARGE
PARAMETER 03679-1
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane,. ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
06-06-00/16:00
•-ot-•-~""'-5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03679-1 DISCHARGE 06-06-00/16:00
------------------------------------------------------------------------------------
PARAMETER 03679-1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
96 1r
90 %-
84 %-
1
06.08.00
2B0607
8.1
1
06.12.00
06.13.00
0612T
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com •-0,-T,.,.-,"'<.
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN oo
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 3
DATE/
LOG ·NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03679-2 TRIP BLANK
PARAMETER 03679-2
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
06-06-00
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 4
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03679-2 TRIP BLANK 06-06-00
------------------------------------------------------------------------------------
PARAMETER 03679-2
--------------------------------------- -------------------- --------------------
1,1,2-Trichloroethane,·ug/l
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
94 %-
90 %-
82 %
1
06.08.00
2B0607
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03679-3 Method Blank
03679-4 Lab Control Standard% Recovery
03679-5 LCS Accuracy Control Limit (%R)
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
03679-3 03679-4 03679-5
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0 108 % 46-147 %
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
__ .,_,_.____..,_ 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN oo
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------------------------------------------------------------------------------------
03679-3 Method Blank
03679-4 Lab Control Standard 'Ir Recovery
03679-5 LCS Accuracy Control Limit ('lrR)
------------------------------------------------------------------------------------
PARAMETER
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene ,-ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
03679-3 03679-4
<1.0 104 'Ir
<1.0
<1.0
<1.0
<l.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
96 'Ir
92 'Ir
84 'Ir
1
06.07.00
2B0607
108 'Ir
102 'Ir
98 'Ir
96 %-
90 %-
84 %
1
06.07.00
2B0607
03679-5
56-143 'Ir
62-135 'Ir
68-131 'Ir
72-127 %
77-122 'Ir
74-126 'Ir
70-130 'Ir
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S!ar.vJatn·n~·a,h
~abo-r;atbr,i'e .. s 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03679-3
03679-4
03679-5
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
03679-3 03679-4 03679-5
<5.0 98 % 85-115 %
1 1
06.12.00 06.12.00
06.13.00 06.13.00
0612T 0612T
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03679
Received: 07 JUN 00
Reported: 15 JUN oo
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0l70.0001
Sampled By: Client
Code: 133300615
Page 8
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
03679-9 MS% Recovery(Batch)
03679-10 MSD % Recovery(Batch)
03679-11 MS Accuracy Advisory Limit (%-R)
03679-12 Precision (%RPO) MS/MSD
,03679-13 MS Precision Advisory Limit (%RPD)
PARAMETER 03679-9 03679-10 03679-11
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %-
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
98 %
98 %
102 %
100 %
96 %
98 %
92 %
82 %
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor 1
06.09.00 Analysis Date
Batch ID
Cyanide (335.2),
Dilution Factor
Prep Date
Analysis Date
Batch ID
ug/1
----------------------- ------
1B0609
102 %-
1
06.12.00
06.13.00
0612T
----------
96 % 46-147 %
92 % 56-143 %
96 %-62-135 %
94 %-68-131 %
90 %-72-127 %
98 % 77-122 %
92 % 74-126 %
84 % 70-130 %
1
06.09.00
1B0609
93 % 85-115 %
1
06.12.00
06.13.00
0612T,
--------------------
03679-12 03679-13
2 % 0-30 %
6 % 0-35 %
6 %-0-3 7 %
6 % 0-33 %
6 % 0-22 %
0 % NA
0 % NA
2 % NA
9.2 %-<20 %
--------------------
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S,alviatnfo)a:h
L!.8b"ar3toiiieS 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stJsavlab.com ••-olS.-.mT,..,..___,,nc.
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: ,S0-03679
Received: 07 JUN 00
Reported: 15 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 133300615
Page 9
LOG NO
03679-9
03679-10
03679-11
03679-12
03679-13
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
PARAMETER
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
MS Precision Advisory Limit (%RPO)
03679-9 03679-10 03679-11 03679-12 03679-13
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Angie we· erskirk, Project Manager
Final Page Of Report
,' I nromoy Can De remO'JeDTOr nec1prnrns reCOtOS:
·-fl--{;, ,_, r'7 0 FedEx Tracking Number
:'' .:& /'I., !ltu L
8169114380'
ZIP ;2 7 ,.':··, Q 7
Internal Billing Reference /,,} t, ,';l,:V 2 i) Zr , () / 7 0, I} ,') () O /
.. --·:---· .... --1111!!1 !---· ·-,. ·--,_ r AR(ADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No.____ CHAIN-OF-CUSTODY RECORD Page __L of--
Project Number/Name JlOvo 7-a z OI 76 I lbo::, I lr------A-c-:Nc:-Ac--cLc:-YccScclS...,/..,.M"'"'E=Tcc-HccOccD-/=s=1z=E~-----1
Project Location IJ K·fu_rcf , /\J:L
Laboratory ::!,-f; ,/ t; c,1vb.-i,-i a,~ .J....)(. "(:,/
. "" V.
Project Manager bJ .3...., 1,J-, S; k#J · , f .f' • .J ~f ·f >-
Sampler(s)/Affiliation ~4=-/-Li/] .,-ftrr~t4:s C:!V-•~., ,., J'-/ :t-
Sample ID/Location Matrix
I
Sample Matrix: L = LiCJJidj
Date/Time
SampJed
I I
i :.i .r ./ ;:; ()
'>I,, .11;5 1•> ,,,., ,;j ~v'::f;-v_ ,:f~ Lab ID "'U
I •
A = Air . ,
Relinquished by: ' ·"' Organization: .LL.., '/I) ,l / .,_,. · LZ., ~M .f l,/bate
Organization:~--"'-T,L. ::1f:u.X/ · l Date
Relinquished by: ____ /_/ ______ _ Organization: Date
Received by: Organization: Date
''::.>v..J "'OA /2, _; /.,./ C ;;,:,,. ~ .,,-;;,,,.,,,_,,.,,,,,+--,"f'}
~ ,, , b
•
t-, 1 l, 1 rr, Time
·· ' '.l ' ,o O Time C
I I Time
I I Time
)> ~--./.,, ,
Remarks Total
---,
Total No. of Bottles/ 7
Containers
Seal Intact?
~No N/A
Seal Intact?
Yes No N/A
Delivery Method: □ In Person ~ommon Carrier J0!4 ftlf 11(3 8Pt9 □ Lab Courier
SPECIFY ;
□Other _______ _
SPECIFY AG 05,0597
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S~a.,.v~·a·,ntnl_a,.h
l!aborator,1es 5102 LaRocheAvenue · Savannah, GA31404 · [phone] · Fax[phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03845
Received: 14 JUN 00
Reported: 21 JUN 00
Client PO. No.: LTO#032800-C
:.'\ Requisition: SQ98-0553
Contract No.: ~FD Channel Master
·, Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
Page 1
DATE/
TIME SAMPLED
03845-1 DISCHARGE 06-13-00/13:30
----------- ----------------------------------------------.---- -------- - - - ---- - --- ----
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
·1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloraethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
03845-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
••""""'"s.-nr,.,......,,. ........ ,00. 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
SAMPLE DESCRIPTION
REPORT OF RESULTS
LIQUID SAMPLES
03845-1 DISCHARGE
LOG NO: S0-03845
Received: 14 JUN 00
Reported: 21 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-05.53
Contract No.: JFD Channei Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
Page 2
DATE/
TIME SAMPLED
06-13-00/13 :30
PARAMETER 03845-1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Brornoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
102 %
90 %
88 %
1
06.15.00
1L0615
11
l
06.16.00
06.i6.00
0616T
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5102 La.Roche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab0com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-03845
Received: 14 JUN 00
Reported: 21 JUN oo
Client PO. No·.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
03845-2 TRIP BLANK 06-13-00
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroetharle, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
03845-2
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<l. 0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
•-"'-r"""'-"'-5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-03845
Received: 14 JUN 00 ·
Reported: 21 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
Page 4
DATE/
TIME SAMPLED
------------------------------------------------------------------------------------
03845-2 TRIP BLANK 06-13-00
----------- -- - ---------------------- ------------------------- ------------ -- ----- -- --
PARAMETER
-------------------------------------------------
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene; ug/1 ·
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID C
03845-2
<l. 0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
102 %
·94 %-
88 %-
1
06.15.00
1L0615
--------------------------------------- -------------------- --------------------
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5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
·REPORT OF RESULTS
LOG NO: S0-03845
Received: 14 JUN 00
Reported: 21 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03845-3 Method Blank
03845-4 Lab Contr_ol Standard % Recovery
03845-5 LCS Accuracy Control Limit (%R)
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichlaroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
03845-3
<1.0
<l. 0
<1.0
<1.0
<5.0
<25
<l. 0
03845-4 03845-5
<1.0 96 % 46-147 %
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-03845
Received: 14 JUN 00
Reported: 21 JUN oo
Client PO. No.: LT0#032800-C
Requisition: SQ98--0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke · Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
REPORT OF RESULTS Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC_ REPORT FOR LIQUID SAMPLES TIME SAMPLED
----------- ---------------------------------- ---------------------.;. --------------- --
03845-3 Method Blank
03845-4 Lab Control Standard% Recovery
03845-5 LCS Accuracy Control Limit ('lrR)
--------------------------------- ----------------------------
PARAMETER 03845-3 03845-4 03845-5
--------------------------------------- ----------------------------------------
Trichloroethene, ug/1·
Dibromochloromethane, ug/1 ·
1, 1·, 2 -Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloroproperie, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ·ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromafluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0.
<1.0
<1.0
<1.0
<1.0
<10
<10
'<l _O
<1.0
<1.0
<1.0
<1.0
<2 ·. 0
106 'Ir
96 %
86 'Ir
1
06.15.00
1L0615
94 'Ir
104 'Ir
102 %
100 %
104 'Ir
94 'Ir
88 %
1
06.15.00
1L0615
56-143 'Ir
62-135 %
68-131 %
72-127 %-
77-122 %
74-126 'Ir
70-130 'Ir
------ ----------------------- --------------------. - - - --·----- ---------- ----------
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5102 LaRoche Avenue • Savannah, GA 31404 , [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty·
ARCADIS Geraghty & Miller, Inc.
P.O. ·Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO: S0-03845
Received: 14 JUN 00
Reported: 21 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
03845-3 Method Blank
03845-4
03845-5
PARAMETER
.Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
03845-3
<5.0
l
06.16.00
06.16.00
0616T
03845-4
96 %
l
06.16.00
06.16.00
0616T
03845-5
85-115 %
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Mille_r, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-03845
Received: 14 JUN 00
Reported: 21 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract 'No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
Page 8
LOG NO
03845-9
03845-10
03845-11
03845-12
03845-13
SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES
MS%-Recovery(Batch)
MSD %-Recovery(Batch)
MS Accuracy Advisory Limit (%-R)
Precision (%-RPD) MS/MSD
MS Precision Advisory Limit (%RPD)
---- ------- ------------------------ ------------ --------- ----- -------------------- - -
PARAMETER 03845-9 03845-10 03845-11 03845-12 03845-13
------------------------------------------------- ---------- --------------------
Volatiles by GC/MS (8260)
1,1-bichloroethene, %-98 %-
Trichloroethene, -%-110 %
Benzene, %-116 %-
Toluene, %-110 %
Chlorobenzene, %-110 %
Surrogate Toluene-dB 100 %-
Surrogate -4-Bromofluorobenzene 96 %
Surrogate -Dibromofluoromethane 86 %
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
1
06.15.00
1L0615
108 %-
1
06.16.00
06 .16 ._00
0616T
100 %
102 %
110 %
110 %
104 %
104 %-
96 %
86 %
1
06.15.00
1L0615
91 %
1
06.16.00
06.16.00
0616T
46-147 %-
56-143 %
62-135 %
68-131 %
72-127 %
77-122 %
74-126 %
70-130 %
75-125 %
2 %-
8 %-
5 %-
0 %-
6 %-
NA
NA
NA
1
06.15.00
1L0615
17 %
·< 30 %
< 35 %
< 37 %-
< 33 %
< 22 %
< NA %
< NA %-
< NA %
<30 %
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Ska"fvla:ni[l:a}h
lfa bo i-,8to rii'e'S · 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
03845-9
03845-10
03845-11
03845-12
03845-13
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: so-03"945
Received: 14 JUN 00
Reported: 21 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0190.0001
Sampled By: Client
Code: 092700622
Page 9
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precjsion (%RPD) MS/MSD
MS Precision Advisory Limit (%RPD)
PARAMETER 03845-9-03845-10 03845-11 03845-12 03845-13
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
-~-- - - - - -_, ----------CHAIN-OF-CUSTODY RECORD Page _I_ 0 f_i AR(ADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. ___ _
Project Number/Name ~c.t6?o.:> 17 -. ,. = -c I 'c.,:_,,1.,:r..:..c~--':-..:i ANALYSIS/ METHOD/ SIZE I c.Jb ' 'C Project Location , ·, n,,I ;-.J
--;:· . I ic-£ ... 'x"' Laboratory, "(CH)<• --" ~ 'jY·,(,1 ,
.~\:., V: .,' ._,. ,_ ~""'~ <Tr~ ' ~ •. IV
Project Manager -~ J' \. ,1 \./ L' .• ,
i ir'fYIM •, {,1 ,.._. ·--.:, ' ··\ 'v \
-,_ I " Sampler(s)/Affi I iation } ,.., -~-L'-....-.,. __ 'v ,~, __,; ~--;i:: ,. I ,:f:--..''"O !
Date/fime ,, t_; :t" './,y \; :£ ),._ 1'/ . (.; -,_ Sample ID/Location Matrix Sampled Lab ID '° . '·t ' 'v""I~ Remarks Total ' ( .1 J,-,...:....,..-"' < r·1 e l I "I'/..::/'-=-5a'U-:; § I L/ ---.-,/. I, I / /,<J/"'-~ ·"' -,. ; r->p t'--J" ,. (1., '-"' ,._;,
' I
.
Total No. of Bottles/ -Sample Matrix: L :✓~-~d;.77s = Solid; A = Air r --./ . Containers
Relinquished by: ' / _..,;.// /·_,%?,,--Organization: /' I (1'! ·..,-c-I• ~ Date C~ I ;-:-.·s L c,r~ Time I i.. 'Cf~:::) Seal Intact? ",x· ,. /, .__,;/ Organization: SV-=5;:.u,!. i, 1/f/ tc?C) &_·',LO / " Received by:· · . ·· Date Time Yes )No N/A / I •• '--~,,.
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date I . I Time Yes No N/A
Special lnstruct,ons/Remarks: -------------------,--,--,---------------------------
/ / ;
Delivery Method: □ In Person /, -Common Carrier F~ ·, ,£,-'c.
SPECIFY
□ Lab Courier □ Other __ ---:=c----
sPEc1Fv
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5102 LaRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, ·NC 27612 ));::;.,·>· .,
CC: Mr .. Mark Radecke
.j
REPORT OF RESULTS
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED
04031-1 DISCHARGE 06-20-00/11:45
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroe~hene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
04031-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
.<1.0
<1.0
<1.0
<10
<1.0
<1.0
<l. 0
<1 ·. 0
<1.0
<1.0
<1.0
<1.0
5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] · www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller; Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO~032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
Page 2
DATE/
TIME SAMPLED
04031-1 DISCHARGE 06-20-00/11:45
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl.-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene; ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
.Dilution Factor
Prep Date
Analysis Date
Batch ID
04031-1
<1.0
<1.0
<1.0
<1.0
<10
<10
<l. 0
<1.0
<1.0
<1.0
<l. 0
<2.0
96 ..
78 'k
76 'k
1
06.22.00
1A0622
8.9
1
06.26.00
06.27.00
0626T
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5102 LaRocheAvenue • Savannah, GA31404 • [phone] • Fax[phone] · www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
Page 3
DATE/
TIME SAMPLED
04031-2 TRIP BLANK 06-20-00
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
04031-2
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
04031-2
PARAMETER
SAMPLE DESCRIPTION
TRIP BLANK
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
REPORT OF RESULTS
LIQUID SAMPLES
2,Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
· Page 4
04031-2
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2'. 0
88 %
80 %
72 'Ir
1
06.22.00
1A0622
DATE/
TIME SAMPLED
06-20-00
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__ .,,__,,..,._,,_,.., 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04031-3 Method Blank
04031-4 Lab Control Standard% Recovery
04031-5 LCS Accuracy Control Limit (%R)
PARAMETER 04031-3
Volatiles by GC/MS (8260)
Chloromethane, ug/1
------------~-----~-
Bromomethane (Methyl bromide), ug/1
Vinyl chloride,· ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
04031-4 04031-5
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene,-ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1.0 108 'Ir 46-147 'Ir
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty·& Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800·C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04031-3 Method Blank
04031·4 Lab Control Standard%-Recovery
04031·5 LCS Accuracy Control Limit (%-R)
PARAMETER 04031·3
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene·, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate· Dibromofl'uoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
88 %-
82 %-
76 %-
1
06.22.00
1A0622
04031-4
104 %-
106 %
90 %
106 %-
88 %-
78 %-
76 %-
1
06.22.00
1A0622
04031-5
56·143 %-
62-135 '<
68-131 %
72-127 %
77-122 %-
74-126 ,..
70-130 %-
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._,ooa.-,,r_,,._,...,,,.. ..... 5102LaRocheAvenue • Savannah,GA31404 • [phone] · Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES "TIME SAMPLED
04031-3 Method Blank
04031-4 Lab Control Standard% Recovery
04031-5 LCS Accuracy Control Limit (%R)
PARAMETER 04031-3
Cyanide (335.2), ug/1
-Dilution Factor
Prep Date
Analysis Date
Batch ID
<5.0
1
06.26.00
06.27.00
0626T
04031-4
96 %
1
06.26.00
06.27.00
0626T
04031-5
Silatv!a1'1n1n[a.h l(cibOl'.'a-ta~r.iE!S
•-<11-T .... ~.""-5102 LaRoche Avenue• Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04031
Received: 21 JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
Page 8
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
04031-8 MS%-Recovery(Batch)
04031-9 MSD %-Recovery(Batch)
04031-10 MS Accuracy Advisory Limit (%R)
04031-11 Precision (%-RPD) MS/MSD
04031-12 MS Precision Advisory Limit (%-RPD)
PARAMETER 04031-8
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %-
Benzen~, %
Toluene, %
Chlorobenzene, %-
Surrogate -Toluene-dB
98 %
98 %-
100 %-
92 %-
98 %-
96 %
76 %-
76 %-
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor 1
06.22.00 Analysis Date
Batch ID
Cyanide (335 .2),
Dilution Factor
Prep Date
Analysis Date
Batch ID
ug/1
------ -----------------------
1A0622
96 %-
1
06.26.00
06.27.00
0626T
----------
04031-9
100 " 120 " 116 %
112 " 112 %
94 %-
90 %-
84 %-
1
06.22.00
1A0622
94 %-
1
06.26.00
06.27.00
0626T ----------
04031-10 04031-11 04031-12
46-147 % 2 % < 30 %-
56-143 %-20 %-< 35 %-
62-135 % 15 % < 37 %
68-131 % 20 % < 33 %-
72-127 %-13 " < ·22 %-
77-122 %-NA NA
74-126 %-NA NA
70-130 %-NA NA
75-125 %-2.1 %-<30 %-
-------------------- ----------
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LOG NO-
04031-8
04031-9
04031-10
04031-11
04031-12
5102 LaRocheAvenue • Savannah, GA31404 · [phone] · Fax[phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P_O_ Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04031
Received: 21·JUN 00
Reported: 30 JUN 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 104200630
Page 9
SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
MS Precision Advisory Limit (%RPD)
PARAMETER 04031-8 04031-9 04031-10 04031-11 04031-12
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report_
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
1/f.l\l
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. ____ _ CHAIN-OF-CUSTODY RECORD Page __L of_f_
f Project Number/Name /Vt,. o,,o 2.0 L. u ( 7o, {)DO'" l I ANALYSIS/ METHOD/ SIZE
Project Location /) X .fr,._ d. , Ill" L-;~ .,J ,/ £Tl _:<:.-.~ • .)~ ,,.., 2-l-... ~ .'C J, Laboratory . -'
A I 2>hc,llu J __, r . .., -·i
Project Manager ( .,i ,1\J .,, ~
I. • ::;.
Sampler(s)/Affiliation :.::t', llA-( ,!_ ---Ar¢...~d:JJ 'J':a:--. J--,; ..., \J r-',I.
.:J._/ ''(j -.J-1 ~o
Date/Time ~'\J~ ~ ,~ -SamQle ID/Location Matrix Sampled Lab ID ' J. -;) , ,✓:1,r1.'J L.., (; ✓ 2,;.; . i>i>/; p( ? I --r.' ... L-. i 'z.,./4_ L . A) , L,-· .,..., 3
I
-
Sample Matrix: L = Liquid; s = oli ; A = Air i ,i
Relinquished b · Organization:
Received by: __ +-,If-'-.,__ _______ Organization: ______ ~~---
Relinquished by: ~---Organization: -'>u-S '\,.; ~
Received by: Organization:
,,
,:?J t.,
CZ.• I alt Date~"~~~~-
Date_~-~--
I
'
Remarks Total
'-f-
>
tJ~
Total No. of Bottles/ ·7 Containers
Time 2£iJo ,,::,, I Seal Intact?
Time Yes No N/A
Time ::l<>s Seal Intact?
Time Yes No N/A
Delivery Method: □ In Person Common Carrier_,____,,~r.-;a;;,,p,.---□ Lab Courier □Other _______ _ ---------------<-•• .. '3j-SPECI-ACO ...
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5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
'. '
REPORT OF RESULTS
LOG NO: S0-04227
Received: 28 JUN 00 -.;} Reported: 06 JUL 00
-:' /!\~
Client PO. No.: LT0#021199-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 16030076
. Page 1
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED
04227-1 DISCHARGE 06-27-00/14:00
PARAMETER 04227-1
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <1.0
Bromomethane (Methyl <l ;o
bromide), ug/1
Vinyl chloride, ug/1 <l. 0
Chloroethane, ug/1 <1.0
Methylene chloride <5.0
(Dichloromethane), ug/1-
Acetone·, ug/1 <25
Carbon disulfide, ug/1 <1.0
1,1-Dichloroethene, ug/1 <1.0
1,1-Dichloroethane, ug/1 <1.0
cis-1,2-Dichloroethene, ug/1 <1.0
trans-1,2~nichloroethene: ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <1.0
2 -Butanone (MEK) , ug/1 <10
1,1,1-Trichloroethane, ug/1 <1.0
Carbon tetrachloride, ug/1 <.l. 0
Bromodichloromethane, ug/1 <1.0
1,1,2,2-Tetrachloroethane, ug/1 <1.0
1,2-Dichloropropane, ug/1 <1.0
trans-1,3-Dichloropropene, ug/1 <1.0
s;aiv:ai'n;n~a h
L:'aDOfiit'o'rieS 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
LOG NO: S0-04227
Received: 28 JUN 00
Reported: 06 JUL 00
ARCADIS Geraghty & Miller, Inc. Client PO. No.: LTO#021199-A
P.O. Box 31388
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.0005
Sampled By: Client
Code: 16030076
REPORT OF RESULTS Page 2
DATE/
TIME SAMPLED
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04227-1
SAMPLE DESCRIPTION, LIQUID SAMPLES
DISCHARGE 06-27-00/14:00 I ------- ---------------
PARAMETER 04227-1
Trichloroethene, ug/1 <l. 0
DibromoChloromethane, ug/1
1,1,2-Trichloroethane, ug/1
B_enzene, ug/1
cis-1,3-Dichloropropene, ug/1
Brornoform, ug/1'
<1. 0
<1.0
<1.0
<1.0
<1.0
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
96 %-
94 %-
96 %-
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate -Toluene-dB
S~rrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluorornethane
Dilution Factor 1
06.30.00 Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution ·Factor
Prep Date
Analysis Date
Batch ID
1B0630
10
1
07.05.00
07.05.00
0705S
1
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com •-ol-1,_.~..,_
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04227
Received: 28 JUN 00
Reported: 06 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ00~0265
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 16030076
Page 3
DATE/
LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED
04227-2 TRIP BLANK 06-27-00
PARAMETER 04227-2
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide) , ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1.0
<1.0
<1.0.
<1.0
<5.0
<25
<1.0
<LO
<1.0
<1.0
<1.0
<1:0
<1.0
<10
<1.0
<1.0
<1.0
<l. 0
<1.0
<1.0
LOG NO
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS ·Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04227
Received: 28 JUN oo·
Reported: 06 JUL 00
Client PO. No.: LT0#021199-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Crient
Code: 16030076
Page 4
DATE/
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
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04227-2 TRIP BLANK 06-27-00 I
----------------------
-PARAMETER 04227-2
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1 ·
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1 .
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
98 %-
96 %-
100 %-
DilutiOn·Factor
Analysis Date
Batch ID
1
06.30.00
1B0630
1
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5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] ; www.stlsavlab.com __ .,_,_.___""-
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC ·27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04227
Received: 28 JUN 00
Reported: 06 JUL 00
Client PO. No.: LTO#021199-A
Requisition:.SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 16030076
Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04227-3 Method Blank
Lab Control Standard%-Recovery 04227-4
04227-11
04227-5
04227-12
Lab Control Standard Duplicate%-Recovery
LCS Accuracy Control Limit (%R)
Precision (%RPO) of LCS/LCSD
PARAMETER
Volatiles by.GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
04227-3
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10 .
<1.0
<1.0
04227-4
92 %-
04227-11 04227-5 04227-12
46-147 %
S,a~vraqn,nYB.h
lab-Orato'r.ie"s 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com • ....,..,..,_,,,r,...,~ . ...,
Mr. Nanjun ·shetty
ARCADIS Geraghty & Miller, Inc. '
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04227
Received: 28 JUN 00
Reported: 06 JUL 00
Client PO. No.: LT0#021199-A
Requisition: SQ00-0265
Contract No. : JFD Channel Master
Project: NC000202.0160.0005
Sampled.By: Client
Code: 16030076
Page 6
LOG NO
DATE/
SAMPLE.DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04227-3
04227-4
04227-11
04227-5
04227-12
-----------------------------------------·---------
Method Blank
Lab Control Standard% Recovery
Lab Control Standard Duplicate% Recovery
LCS Accuracy Control Limit (%R)
Precision .(%RPD) of LCS/LCSD
----------------------------------------------------- ---- ----------- ----------------------
PARAMETER 04227-3
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
.1,2-Dichloropropane, ·ug/1
trans-1; 3·-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
<1.0
<l. 0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
100 %
100 %
100 %
Dilution Factor
Analysis Date
Batch ID
1
06.30.00
1B0630
04227-4
86 %
88 %
92 %
90 %
98 %
104 %
100 %
1
06.30.00
1B0630
04227-11
-----------------------------------------------------------
04227-5
56-143 %-
62-135 %
68-131 t
72-127 %
77-122 %
74-126 %
70-130 %
04227-12
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,_.,a....,r..,.........,,...,.., 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04227
Received: 28 JUN 00
Reported: 06 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 16030076
Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04227-3 Method Blank
Lab Control Standard% Recovery 04227-4
04227-11
04227-5
04227-12
Lab Control Standard-Duplicate% Recovery
LCS Accuracy Control Limit (%R)
Precis_ion (%RPD) of LCS/LCSD
PARAMETER
Cyanide (335.2), ug/1
Dilution Factor
Prep Date.
Analysis Date
Batch ID
04227-3
----------
<5.0
1
07.05.00
07.05.00
0705S
----------
04227-4
----------
100 %
1
. 07.05.00
07.05.00
0705S
----------
04227-11
----------
110 %-
1
07.05.00
07.05.00
0705S
----------
04227-5 04227-12
--------------------
85-115 %-9.5 %-
---------- ----------
S ·a7v~a··n~m at,h ll'SbO~Bto·ires· 51021.aRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04227
Received: 28 JUN 00
Reported: 06 JUL 00
Client PO. No.: LTO#021199-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.0005
Sampled By: Client
Code: 16030076
Page 8
LOG NO
04227-6
04227-7
04227-8
04227-9
04227-i0
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS 'Ir Recovery(Batch)
MSD 'Ir Recovery(Batch)
MS Accuracy Advisory Limit ('irR)
Precision (%RPO) MS/MSD
MS Precision Advisory Limit ('lrRPD)
PARAMETER 04227-6
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
Benzene, %
Toluene, %
Chlorobenzene, 'Ir
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluorometharie
Oilution Factor
96 'Ir
88 'Ir
92 'Ir
90 'Ir
92 'Ir
96 'Ir
90 'Ir
102 %
l
Anal:,,sis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
06.30.00
1B0630
70 'Ir
l
07.05.00
07.05.00
0705S
04227-7
104 'Ir
96 'Ir
96 'Ir
100 'Ir
100 %
100 %
98 %
100 'Ir
l
06.30.00
1B0630
55 'Ir
l
07.05.00
07.05.00
0,705S
04227-8 04227-9 04227-10
46-147 'Ir 8 'Ir < 30 %-
56-143 %-9 %-< 35 %-
62-135 %-4 %-< 37 'Ir
68-131 'Ir 10 %-< 33 'Ir
72-127 'Ir 8 %-< 22 %-
77-122 'Ir < NA %-
74-126 'Ir < NA %-
70-130. %-< NA 'Ir•
---
75-125 %-24 'Ir <30 %-
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5102 LaRoche Avenue , Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com __ ,,_,_,__..._
LOG NO
Mr .. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04227
Received: 28 JUN 00
Reported: 06 JUL 00
Client PO. No.: LTO#021199-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0160.000S
Sampled By: Client.
Code: 16030076
REPORT.OF RESULTS Page 9
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
PAR.l\METER
These test results.meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Cyanide MS/MSD percent recoveries failed to meet advisory limits due to
matrix interference in the sample. The sample result was <10 ppb and
the spike level was 100 ppb.
Project Manager
Final Page Of Report
~
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No., ____ _ CHAIN-OF-CUSTODY RECORD Page-. --ot-· -
i2 ...
iS)
N !I) /'1
N ...
()\
&]
~
Project Number/Name 1'\-:.<>Q:::,<.02 .<>/Co
I
Project Location OK/7,,,J.AJ '-
Laboratory ::ST/,. /_..5=,1L•"~,l j
"" Project Manager N. <.,L._-lfv ,,v
.~,V .i: ~f
Sampler(s)/Affiliation J N·<-: .,.._:___ ~f IV~ v V .f" 0
DatefTime ' { ' '-I!) 1,
Sample ID/Location Matrix Sampled Lab ID JJ £ ~,If-!-~/to;,
,l ·~ cL an<.. L I c.;z!f:t';-= ~ I
I
'--r,-.-,-, l:J .... ~ L < I 2 rfa<, .:s
'
Sample Matrix: L = Liquid; s = Solid; A = Air /
Relinquished by: "' "//-~s----Organization: />lr., '., Received by. • =I ,i;~ ~ ·' d · Organizatior,"i'U---fisd , ' .
Relinquished by: I Organization:
Received by; Organization: tSl ...
1 Speclal lnstructron!i/Remar: ~ I l.,),;,<. I<, /=.,.,._ r..,,
Delivery Method: □ In Person r.¢£ommon Carrier k J G6.
SPECIFV
ANALYSIS/ METHOD/ SIZE 7
_/'
Remarks Total
4
3
~
--~--
Total No. of Bottles/
Containers
Date I".. ,z;z,~ Time,~ al Intact?
Date {p I Z'! l""o Time IJ.. '.:, 0 ~eh_No NIA
Date I I Time Seal Intact?
Date I I Time Yes No N/A
□ Lab Courier □Other ______ _
SPECIFY AG OS,Q.;!1 - --..... --------------
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.JUL l ~ 2000
5102 LaRoche Avenue • Savannah, GA 31404 · [phone] J,.fax (912);3,?2;(,ll6_5;;1i;>YWW.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
04421-1 DISCHARGE 07-03-00/13:55
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (D_ichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1, 1-Dichloroethene, ·ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichlo_roethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1;2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
04421-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
S1ra~,v ,'a~nt'!J!aih I.Fa Do ·r·ato r i es· 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#032800·C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
·sampled By: Client
Code: 112300714
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
04421-1 DISCHARGE 07-03-00/13:55
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
04421-1
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1. 0
<1.0
<2.0
88 %-
96 %-
90 %-
1
07.11.00
1B0711
12
1
Prep Date 07.13.00
Analysis Date 07.13.00
Batch ID 0713S
----~------·----------
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5102LaRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
Page 3
DATE/
TIME SAMPLED
04421-2 TRIP BLANK 07-03-00
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1 ·
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1, 1-Dichlo.roethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1_, 1, 1-Trichloroethane, ug/1
carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
04421-2
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<l. 0
<l. 0 ·
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
Dibromochloromethane, ug/f <1.0
5 a"':v' atntn~a~h lliib·o·r=atOr1ieS 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF.RESULTS
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
04421-2 TRIP BLANK
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total·, ug/1·
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14 JUL 00
Client PO', No.: LTOJI032800·C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
·Page 4
DATE/,
04421-2
<1.0
<1.0
·<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<l. 0
<2.0
80 tr
90 tr
92 tr
1
07.10.00
1B0710
TIME SAMPLED
07-03-00
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,_o,S...mT ... .--.ln<. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14-JUL 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
Page 5
LOG NO ·SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
04421-3
04421-4
04421-5
PARAMETER
Method Blank
Lab Control Standard%-Recovery
LCS Accuracy Control Limit (%-R)
04421-3 04421-4 04421-5
-------------------------------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<l.0
<1.0
<1.0
<1.0
trans-1,3-Dichloropropene, ug/1 <1.0
90 %-46-147 %-
Sia v•a,n,n,a~h
e:a·b'O 'r,a"to f.i e ... s 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr: Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
Page 6
LOG NO
04421-3
04421-4
04421-5
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
PARAMETER
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -bibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
04421-3
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
84 %
92 %
100 %
1
07.10.00
1B0710
04421-4
88 %
86 %
72 %
86 %
84. %
92 %
100 %
1
07.10.00
1B0710
04421-5
56-143 %
62-135 %
68-131 %
72-127 %
77-122 %
74-126 %
70-130 %
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-04421
Received:·06 JUL 00
Reported: 14 JUL 00
Client PO. No.: LT0#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
REPORT OF RESULTS Page 7
LOG NO
04421-3
04421-4
04421-5
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
PARAMETER
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Cyanide (335.2), ug/1
Dilution Factor ,
_Prep Date
Analysis Date
Batch ID
04421-3
----------
<5.0
1
07.13.00
07.13.00
0713S
04421-4 04421-5
--------------------
102 ,. 85 -115 ,.
1
07.13.00
07.13.00
0713S
5102 LaRoche Ave!}ue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
Page 8
LOG NO
04421-6
04421-7
. 04421-8
04421-9
04421-10
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS%-Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%-R)
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%RPD)
PARAMETER 04421-6 04421-7 04421-8 04421-9 04421-10
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %-
Trichloroethene, %
Benzene, %
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
Surrogate --4 -Bromofluorobenzene
Surrogate -Dibromofluoromethane
_Dilution Factor
98 %-
96 %-
96 %-
80 %-
92 %
84 %
92 %-
92 %
1
Analysis Date
Batch ID
Cyanide (335.2),
Dilution Factor
Prep Date
Analysis Date
Batch ID
mg/1
-----------------------------
_07.10.00
1B0710
107 %-
1
07.13.00
07.13.00
0713S
----------
100 % 46-147 % 2 %-< 30 %
96 % 56-143 %-0 %-< 35 %-
98 % 62-135 % 2 %-< 37 %-
78 %-68-131 %-2 %-< 33 %-
92 % 72-127 % 0 %-< 22 %-
84 %-77-122 %-< NA %-
92 %-74-126 %-< NA %-
92 %-70-130 %-< NA %-
1
07.10.00
1B0710
96 %-85-115 %-11 %-<20 %-
1
07.13.00
07.13.00
0713S
-------------------- --------------------
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__ .,_,,,r...,,....,.__,oe. 5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
.cc: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04421
Received: 06 JUL 00
Reported: 14 JUL 00
Client PO. No.: LTO#032800·C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 112300714
Page 9
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES.
04421-6 MS% Recovery(Batch)
04421-7 MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPD) MS/MSD'
04421-8
04421-9
04421-10 MS Precision Advisory Limit (%RPD)
PARAMETER 04421-6 04421-7 04421-8 04421-9 04421-10
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples· were within the SL quality control
requirements.
Angie We merskirk, Project Manager
Final Page Of Report
ti'.i«
ARCADIS GERAGHTY & MILLER Laborat<?ry Task Order No./P.O. No_/)/, zBQ o-'4CHAIN-OF-CUSTODY RECORD Page _j_ of~
Project Number/Name /l;L ~ Z.'D,_ · O I 10 0oDO I I ANALYSIS/ METHOD/ SIZE I
Project Location Ox-(;cd( Nz
Laboratory < _:,J ~ --~ h ,
Project Manager /1. 1. <;/._.A,,
Sampler(s)/Affiliation 7' c/..k II
1 /,A ~}. / .
Datemme
Sample ID/Location Matrix Sampled Lab ID
,
Sample Matrix: L ; :!9i'id~ S ""/ S?lf A ; Air
3, \
,/
Relinquished by) L /.J~ '
Received by: C .. 1/.-1-llt., I,_,: . ,
Organization: :,<v,,_, ., r .... IC A--
Organization: c--•:,,, _ -<; 0 "/'
Remarks Total
rst r'------t----,
Date / , 3. 160
Date 7 / G /tdJ
Total No. of Bottles/
Containers
Time s,o .. •
"""t!" .... ·•J Time _ •. t:1
Seal Intact?
Yes No N/A
Relinquished by: __________ Organization: ___________ Date_~'-~'--Time ____ _ Seal Intact?
Received by: Organization: Date / / Time Yes No N/A
Special lnstruct,ons/R::rks: I t--ee 'L -£ c--1
Delivery Method: □ In Person □Other ___ ~~---
sPEcrFv
□ Lab Courier ___ , __ _
~ -• •-----, .. •GOS-
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.1 u L 3 1 2Dao
5102 LaRoche Avenue · Savannah, GA 31--4,04,; 0)12) 354-7858 • Fax [phone] • www.stlsavlab.com
" ._...,,~z-;ig_!'.t)' & :Hiller
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION·, LIQUID SAMPLES
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1)
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 125600727
Pagel
DATE/
TIME-SAMPLED
04575-1 DISCHARGE 07-11-00/14:45
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
C_arbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
04575-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<l. 0
<1.0
1,1,2,2-Tetrachloroethane, ug/1 <1.0
1,2-Dichloropropane, ug/1 <1.0
trans-1,3-Dichloropropene, ug/1 <1.0
Trichloroethene, ug/1 <1.0
Dibromochloromethane, ,ug/1 <l. O
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com .-.. -r, .... i.-....
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
. Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1)
Client PO. No.: LT0#032800-C
Requisition: SQ00-0265
Contract No.:·JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 125600727
Page 2
DATE/
TIME SAMPLED
04575-1 DISCHARGE 07-11-00/14:45
PARAMETER 04575-1
1,1,2-Trichloroethane, ug/1 <1.0
-Benzene, ug/1 ·<1.0
cis-1,3-Dichloropropene, ug/1
Brornoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluorornethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
100 %
'98 %
100 %
1
07.15.00
100715
11
1
07.17.00
07.18.00
0717U
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·-.. -,-~ .... 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised:' 27 JUL 00 (1)
Client PO. No.: LTO#032800-C
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170.0001
Sampled By: Client
Code: 125600727
REPORT OF RESULTS Page 3
DP.TE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
04575-2 TRIP BLANK 07-11-00
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane; ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
04575-2
<1.0
<1.0
<1.0
<1.0
<5. 0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
. CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1)
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 125600727
Page 4
DATE/
TIME SAMPLED
04575-2 TRIP BLANK 07-11-00
------------------------------------------------------------------------------------
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
.Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
E_thylbenzene, ug/1
'Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
04575-2
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<l.0
<1.0
<1.0
<2.0
102 %-
96 ,.
102 %-
1
07.14.00
100714
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5102 LaRoche Avenue , Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1)
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 125600727
Page 5
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
04575-3 Method Blank
04575-4 Lab Control Standard% Recovery
04575-5 LCS Accuracy Control Limit (%R)
PARAMETER 04575 0 3 04575-4 04575-5
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride,· ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0 104 % 46-147 %-
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<l.0
<1.0
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty. & Miller, Inc.
P.O. Box 31388
Raleigh, NC ·27512
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1)
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 125600727
Page 6
LOG NO
04575-3
04575-4
04575-5·
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
PARAMETER
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Trichlor6ethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate·-Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
04575-3
<1.0
<1.0
<1.0
<1.0
<1.0
. <1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
. <1.0
<2.0
100 %
98 %
104 %
l
07.14.00
100714
04575-4
96 %
108 %
104 %
100 %-
94 %-
100 %-
1
07.14.00
100714
04575-5
56-143 %
62-135 %
68-131 %-
72-127 'Ir
77-122 'Ir
74-126 'Ir
70-130 %
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51021..aRocheAvenue • Savannah,GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1)
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001·
Sampled By: Client
Code: 125600727
Page 7
LOG NO
04575-3
04575-4
04575-5
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
PARAMETER
Lab Control Standard 'Ir Recovery
LCS Accuracy Control Limit ('lrR)
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
04575-3
<5.0
l
07.17.00
07.18.00
0717U
04575-4
9 0 'Ir
l
07.17.00
07.18.00
0717U
04575-5
85-115 'Ir
•~OIS-T_,L.allcmonH,n,.
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0 .. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1) ·
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 125600727
Page 8
LOG NO
04575-6
04575-7
04575-8
04575-9
04575-10
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS%-Recovery(Batch)
.MSD %-Recovery(Batch)
MS Accuracy Advisory Limit (%-R).
Precision (%-RPD) MS/MSD
MS Precision Advisory Limit (%-RPD)
PARAMETER 04575-6 04575-7 04575-8 04575-9 04575-10
Volatiles by GC/MS (8260)
1,1-Dichloroethene, 'Ir
Trichloroethene, %
Benzene, %
Toluene, %-
Chlorobenzene, %
Surrogate Toluene-dB
104 %-
96 'Ir
102 %
108 %
104 %-
100 %-
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
94 %-
100 'Ir
1
Analysis Date
Batch ID
Cyanide (335.2),
Dilution Factor
Prep Date
Analysis Date
Batch ID
ug/1
-----------------------------
07.17.00
100717
108 %-
1
07.17.00
07.18.00
07170
----------
106 %-46-147 %-2 %-< 30 %-
96 %-56-143 %-0 %-< 35 %-
104 %-62-135 % 2 %-< 37 %
110 %-68-131 %-2 %-< 33 %-
106 'Ir 72-127 %-2 'Ir < 22 %-
100 % 77-122 % < NA 'Ir
92 %-74-126 'Ir < NA 'Ir
98. %-70-130 %-< NA 'Ir
1
07.17.00
100717
87 %-85-115 'Ir 22 %-<30 %-
1
07.17.00
07.18.00
07170
----------------------------------------
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5102 LaRoche Avenue · Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04575
Received: 12 JUL 00
Reported: 19 JUL 00
Revised: 27 JUL 00 (1)
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: · 125600727
Page 9
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
04575-6 MS% Recovery(Batch)
04575-7 MSD % Recovery(Batch)
MS Accuracy Advisory Limit (\R)
Precision (\RPD) MS/MSD
04575-8
04575-9
04575-10 MS Precision Advisory Limit (\RPD)
PARAMETER 04575-6 04575-7 04575-8 04575-9 04575-10
These test results meet all the requirements of·NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
~
ARCADIS GERAGHTY & MILLER Laboratory Task Order No.IP.a. No. ____ _ CHAIN-OF-CUSTODY RECORD Page-+-of~.i-
Project Number/Name N<'C:Z.J:l.Zc:,7, 012-" I ANALYSIS/ METHOD/ SIZE
Project Location c:»: {l:.J, JJ '-
Laboratory ~ I Z. _/Sc-.,~..,~, h L -b.:. V ·-
"--·, ~c"
Project Manager ,/IJ"' ..,-; •~ " _:s:; ~ #-z ~-.",v .r ~ .-\/ \
Sampler(s)/Affiliation i , f'---f ,....-:55-'v ~ ·-·v "
0-! ~ -i
Date/fime
\j 9 \j O .o
Sample ID/Location Matrix Sampled Lab ID a)~'(./ J".;!';
--.. l I }., ';( C c .'1 .__ L -_, f/u..:....~
I -1'-i-'--1' ~ I -,
-:7.,~ ~le.,..~ L 7-/11/,,'"?.:. ~~
'
Sample Matrix: L = ~uid; __,J-;f Solid; ~r , .
Relinquished by:,--,,--,,-_,,,,,..,_.,..------Organization:-/-'.\Ll'--'-=-'-'-="-c------
Received by: Organization:-~~~=~------
Relinquished by: Organization: ___________ _
Received by: Organization:
Special lnstrnions/Remarks:/ I (J_ (?.(_, b r:, • C\
~ommon Carrie r-1'-::.-'..:"'--""'"-----
Date 21'.,_ I
Date -z II t.. I ,Jtl
Date
Date
□ Lab Courier Delivery Method: □ In Person -------- ---- - -
I
Remarks Total
<{
s
Total No. of Bottles/ t Containers
Time lb:. <> Seal Intact?
Time -;f'; l,t-: ~No NIA
Time Seal Intact?
Time Yes No N/A
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s:a:)y:~/nfn(_~•h Labor.ator,1es
'""'"""'"s...,,,r-,uo..,.,,,..,tnc
RECEIVED
AUG O 7 2000
5102 LaRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
ARCAD!S Geraghtyf<. Miller
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
REPORT OF RESULTS Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
-_,_ -------- -------------------------------------------------- -----------------------
04821-1 DISCHARGE 07-18-00
----------- --------------------------- ----------------------- ------------ -----------
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichlaroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
04821-i
<1.0
<1.0
<1.0
<1.0
<5. 0
<25
<1.0
-<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<l. 0
<1.0
<1.0
<1.0
<1.0
C
. ..._.,_r,..-,m 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www_stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc_
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
04821-1 DISCHARGE
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromofm:m, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofltiorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO_ No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
Page 2
DATE/
04821-1
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
108 %
88 %
86 %
1
07.24.00
1L0724·
0.011
1
07.28.00
07.31.00
0728T
TIME SAMPLED
07-18-00
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""''"'°"°'S.V.mT,ont[.obo,a1o,~o.0.: 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
Page 3
DATE_!
TIME SAMPLED
------------ ------------------------- ----- ----- ----------- --- -------------------- ---
04821-2 TRIP BLANK 07-18-00
------------------------------------------------------------------------------------
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1·
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
04821-2
<1.0
<1.0
<1.0
<1.0"
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
1,1,2,2-Tetrachloroethane, ug/1. <1.0
1,2-Dichloropropane, ug/1 <1.0
trans-1,3-Dichloropropene, ug/1 <1.0
Trichloroethene, ug/1 <1.0
Dibromochloromethane, ug/1 <1.0
------------------------------------------------- ------------------------------.
5102 LaRoche Avenue • Savannah, GA 31404 • (912) 35+7858 • Fax [phone] • www.stlsavlab.com •""""""orS.,omT""1L&oo<ao, ... ,..,
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
. CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
Page 4
DATE/
TIME SAMPLED
04821-2 TRIP BLANK 07-18-00
PARAMETER
1,1,2-Tiichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene,·ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
.Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilutio'n Factor
Analysis Date
Batch ID.
04821-2
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0,
<1.0
<1.0
<1.0
<2.0
110%-
90 %-
88 %-
1
07.24.00
1L0724
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sra;v ~a ,n':n,a 1h
l!'a bo fil tci'r,i tis 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04821
• Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
REPORT OF RESULTS Page 5
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
04821-3 Method Blank
04821-4 Lab-Control Standard t Recovery
04821-5 LCS Accuracy Control Limit (tR)
PARAMETER 04821-3
Volatiles by GC/MS (8260)
Chloromethane, ug/1 ·
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dic~loroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1, 2 -Dichloropropane, -ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<l. 0-
<l. 0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
trans-1,3-Dichloropropene, ug/1 <1.0
04821-4 · 04821-5
84 t 46-147 t
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
Page 6
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
04821-3 Method Blank
04821-4 Lab Control Standard·% Recovery.·
04821-5 LCS Accuracy Control Limit (%R)
PARAMETER 04821-3
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Tolue,:,e, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
. <l. 0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
106 %
88 %
92 %
1
07:24.00
1L0724
04821-4
90.%
108 %
98 %
88 %
106 %
92 %
94 ·%
1
07.24,00
1L0724
04821-5
56-143 %
62-135 %
68-131 %
72-127 %
77-122 %-
74-126 %-
70-130·%.
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5102 LaRocheAvenue • Savannah, GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
Page 7
LOG NO SAMPLE DESCRIPTION, QC -REPORT FOR LIQUID SAMPLES
-- - --.---- - - -------·-------------------------- --- - ------------- --- - - -----------------
04821-3 Method Blank
04821-4 Lab Control Standard% Recovery
04821-5 LCS Accuracy Control Limit (%R)
PARAMETER
Cyanide (335.2), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
04821-3
<0.010
1
07.28_00
07.31.00
0728T
04821-4
100 %
1
07.28.00
07.31:00
0728T
04821-5
85-115 %
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
Page 8
LOG NO
04821-6
04821-7
04821-8
04821-9
04821-10
SAMPLE DESCRIPTION, QC. REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%-RPD) MS/MSD
MS Precision Advisory Limit (%-RPD)
PARAMETER 04821-6 04821-7 04821-8 04821-9 04821-10
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %
Trichloroethene, %
, Benzene,_ %
Toluene, %
Chlorobenzene, %
Surrogate Toluene-dB
70 %
82 %
100 %
90 %-
80 %
108 %
86 %-
84 %-
Surrogate_-4-B~omofluorobenzene
Surrog~te -Dibr~mofluoromethane
Dilution Factor 1
07.24.00 Analysis Date
Batch ID
Cyanide (335.2), mg/1
Dilutiori Factor
Prep Date
Analysis Date
Batch ID
1L0724
105 %-
1
07.28.00
07. 31. 00
0728T
80 %-
88 %-
104 %
96 %
84 %-
108 %-
88 %-
88 %-
1
07.24.00
1L0724
98 %-
1
07.28.00
07.31.00,
0728T
46-147 % 13 % < 30 %
56-143 % 7 %-< 35 %
62-135 % 4 %-< 37 %
68-131 % 6 % < 33 %-
72-127 % 5 %-< 22 %
77-122 % NA NA
74-126 %-NA NA
70-130 %-NA NA
1
07.24.00
1L0724
85-115 'Ir 6 .9 %-<20 %
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LOG NO
04821-6
. 04821-7
04821-8
04821-9
04821-10
5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04821
Received: 20 JUL 00
Reported: 02 AUG 00
Client PO. No.: LTO#032800-C
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170.0001
Sampled By: Client
Code: 15060082
Page 9
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (tR)
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%RPD)
PARAMETER 04821-6 04821-7 04821-8 04821-9 04821-10
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL Project Manager
who signed this test report.
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
t;,'it.!
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. ____ _ CHAIN-OF-CUSTODY RECORD Page
Project Number/Name ~c.<2'..D,;:'.o ? . c 1 ?0 I ANALYSIS/ METHOD/ SIZE I
Project Location OX~,~ -~-
Laboratory-Si{_ {-SerJ,..,_,~L._ / ,,,L:s ,:-\j ,
..J I "-y\v.v
Project Manager ,..la~ : "' ~ -SL-fq i', i'" i ~"-"\ ~-.v ~ ~\
Sampler(s)/Affiliation ~ · T f-\ "",'.:l$~~ ._')' v'\'.\. 0' ;' '()
0 cl " '-.. ·=--;
Date/Time 1' \J i),' 0
Sample ID/Location Matrix ~ampled Lab ID do :f 1 /:()~ Remarks Total
J);:-s,l l ,.. ,, , . I r/ r-~-~ I 1
/
I r'.C7 -;z_;~ ,, Y\ L ?-llc1~ 3. .)
' -
~~ ~ • . ""'°'·
.
·•
Sample Matrix: L = Liquid; .,..--57= Solid; A = Air Total No. ofBottles/ r Containers /'7 ..--, _,; . -,/ F1
Relinquished by/ / ./ / / ?_,. Organization: /f'r,.,,,,.c.,t ·S Date T / /;,; <)':I, Time In ,c-~al Intact? I •
, A.,/?---; 1 ~"co/'\,_cr Organization: '_:3·(L-~ 7 1Zo I O c> Time <"),"/ () .¥~½o N/ A Received by: -, • Date ' / I II
Relinquished by:
, V Organization: Date I I Time iS"eal Intact?
Received by: Organization: Date I ., Time Yes No N/A
S~ec1a~ lnstr~ct1on51emarks:
/ 1,X-<-I'> , ,,,, C..,
Delivery Method: D In Person - - - - -
d¾:ommon Carrier_~r_·t_._)_.~Z=-~>< ___ _ - - - -
SPECIFY -- -
D Lab Courier □Other ___ ~~--spec1Fv - - - -
AG 0S-0597 - - -
-----------------
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P·.o. Box 31388
Raleigh, NC 27612 ' .
LOG NO: S0-04972
Received: 26 JUL 00
Reported: 04 AUG·oo
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled.By: Client
Code: 11060084
REPORT OF RESULTS Page 1
LOG NO
04972-1
SAMPLE DESCRIPTION
DISCHARGE
DATE/
LIQUID SAMPLES TIME SAMPLED
07-25-00/08:30
PARAMETER 04972-1
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
-1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
· 1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<l. 0
<LO
<1.0
<1.0
<1.0
<1.0
· ,1, c i n r_.,,,'1 ,,,._ "" .• j,,_
5102 LaRoche Avenue · Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
DISCHARGE
LOG NO: S0-04972
Received: 26"JUL 00
Reported: 04 AUG 00
Client PO. No.: LTO#041900~A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
·sampled By: Client
Code: 11060084
Page 2
DATE/·
TIME SAMPLED
07-25-00/08:30
LOG NO
04972-1
PARAMETER
----------------------------------------------.----
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -· 4 -Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide· (335. 2), · ug/1
Dilut~on Factor
Prep Date
Analysis Date
Batch ID
04972-1
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
94 %
116 %
80 %
1
07.29.00
1B0729
9.9
1
08.02.00
08.02.00
0802S
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04972
Received: 26 JUL 00
Reported: 04 AUG 00.
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 .Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 11060084
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------- ---- -------------------------------------------------- ----------- ------------
04972-·2 INFLUENT 07-_25-00/08: 45
04972-3 TRIP BLANK 07-25-00
------------------------------------------------------------------------------------
PARAMETER 04972-2 04972-3
--------------------------------------- ---------- ------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1, 2-Dichloroethene, "ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
· Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene\ ug/1
Trichloroethene, ug/1
<50 <1.0
<50 <1.0
<50 <1.0
<50 <1.0
<250 <5.0
<1200 <25
<50 <1.0
<50 <1.0
<50 <1.0
82 <1.0
<50 <1.0
<50 <1.0
<50 <1.0
<500 <10
<50 <1.0
<SO <1.0
<50 <1.0
<50 <1.0
<50 · <1.0
<50 <1.0
5000 <1.0
------------------------------
•-OIS.-.T..,,utiota,onao,n:. 5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-04972
.Received: 26 JUL 00
Reported: 04 AUG 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 11060084
Page 4
DATE/
TIME SAMPLED
----------- ------------------------------ -------------------- ---------- ----- ------ --
04972-2 INFLUENT 07-25-00/08:45
04972-3 TRIP BLANK 07-25-00
PARAMETER
Dibromochloromethane, ug/1
l,_1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene; ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibr_omofluoromethane
Dilution Factor
Analysis Date
Batch ID
----------
04972-2 04972-3
--------.------------
<50 ~1.0
<50 <1.0
<50 <1.0
<50 <1.0
<50 <1.0
<500 <10
<500 <10
590 <1.0
<50 <1.0
<50. <1.0
<50 "<1.0
<50 <1.0
<100 <2.0
96 \-92 \-
116 \-.116 \-
80 \-80 \-
50 1
07.29.00 07.29.00
1B0729 1B0729
----------
--------------------------------------- -------------------- --------------------
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5102 LaRoche Avenue • Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr·. Nanjun Bhetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04972
Received: 26 JUL 00
Reported: 04 AUG 00
Client PO. No.: LTO#04l900-A
Contract
Requisition: SQ98-0553
No.: JFD Channel Master
Project: NC000292.0170
Sampled By: Client
Code: 11060084
Page 5
DATE/
LOG. NO
04972-4
04972-5
04972-6
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
Method Blank
TIME SAMPLED
PARAMETER.
Lab Control Standard t Recovery
LCS Accuracy Control Limit (tR)
04972-4 04972-5 04972-6
----------------- - ----------------------------.---· -------------------- ----------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), .ug/1
Acetone, ug/1
Carbon disulfide, ug/1
l,l-Dichloroethene, ug/1
l,l-Dichloroethane, ug/1
cis-l,2-Dichloroethene, ug/1
trans-1,2-oichloroethene, ug/1
Chloroform, ug/1
l,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,-1, 1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
l,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<l.0
<1.0 130 % 46-147 %
<1.0
<1.0
. <l. 0
<l.0
<1.0
<l0
<1.0
<1.0
<1.0
<l.0
<1.0
<1.0
5102 LaRoche Avenue· Savannah, GA 31404 · [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjuri Shetty·
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO: S0-04972
Received: 26 JUL 00
Reported: 04 AUG 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 11060084
REPORT OF RESULTS" .Page 6
DATE/
LOG NO "SAMPLE.DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04972-4 Method Blank
04972-5 Lab Control Standard%-Recovery
04972-6 LCS Accuracy Control Limit (%-R)
----- ------ ---------------------------------- ----------------
PARAMETER 04972-4 04972-5 04972-6
-------·-------------------------------- ----------------------------------------
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichlo~oethane, ug/1
_Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1·
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<l.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
94 %-
116 'Ir
70 %-
1
07.29.00
1B0729
110 %-
70 %-
102 %-
110 %-
92 %-
118 %-
82 %-
1
07.29.00
1B0729
56-143 %-
62-135 %-
68-131 %-
72-127 %-
77~122 %-
74-126 %-
70-130 %-
------------------------------------------------- ---------- --------------------
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5102 LaRocheAvenue • Savannah, GA 31404 · [phone] · Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-04972
Received: 26 JUL 00
Reported: 04 AUG 00
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 11060084
REPORT OF RESULTS Page ·7
DATE/ LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
04972-4 Method Blank
04972-5 Lab Control Standard% Recovery
04972-6 LCS Accuracy Control Limit (%R)
PARAMETER 04972-4
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<5.0
1
08.02.00
08.02.00
0802S
----------.
04972-5
104 %
1
08.02.00
08.02.00
0802S
04972-6
85-115 %
S1a1lV)i1!nl1ii~afh
tta'bOf.atOFiies 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nan:iun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O .. Box 31388
Raleigh, NC 27612
CC: Mr. Mark·Radecke
REPORT OF RESULTS
LOG NO: S0-04972
Received: 26 JUL 00
Reported: 04 AUG 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC00.0202.0170
Sampled By: Client
Code: 11060084
Page 8
LOG NO
04972-10
04972-11
04972-12
04972-13
04972-14
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS Ir Recovery(Batch)
MSD Ir Recovery(Batch)
MS Accuracy Advisory Limit (lrR)
Precision (lrRPD) MS/MSD
MS Precision Advisory Limit (%RPO)
PARAMETER 04972-10 04972-11 04972-12 04972-13 04972-14
Volatiles by GC/MS (8260)
1,1-Dichloroethene, Ir 118 Ir 118 % 46-147 %-o Ir < 30 1r·
Trichloroethene, Ir 106 Ir 106 % 56-143 Ir 0 Ir < 35 Ir
Benzene, Ir 70 % 70 %-62-135 %-o % < 37 %
Toluene, Ir 100 Ir 100 'Ir 68-131 Ir 0 Ir < 33 Ir
Chlorobenzene, Ir 108 Ir 106 Ir 72-127 'Ir 2 Ir < 22 Ir
Surrogate -Toluene-dB 94 Ir 94 'Ir 77-122 Ir < NA 'Ir
Surrogate -4-Bromofluorobenzene 118 Ir 116 'Ir 74-126 Ir < NA Ir
Surrogate -Dibromofluoromethane 78 Ir 80 Ir 70-130 Ir < NA Ir
Dilution Factor 1 l·
Analysis Date· 07.29.00 07.29.00
Batch ID 1B0729 1B0729
Cyanide (335.2), mg/1 100 Ir 95 Ir 85-115 Ir 5.1%-<20 Ir
Dilution Factor 1 1
Prep Date 08.02.00 08.02.00
Analysis Date 08.02.00 08.02.00
Batch ID 0802S 0802S
---------------------------- ----------- ----------------------------------------
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5102 LaRoche Avenue · Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
·P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-04972
Received: 26 JUL 00
Reported: 04 AUG 00
Client PO. No.: LTO#041900-A
Contract
Requisition: SQ98-0553
No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 11060084
Page 9
LOG NO
04972-10
04972-11
04972-12
04972-13
SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES
MS% Recovery(Batch)
MSD % Recovery(Batch)
·MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
04972-14 MS Precision Advisory Li~it (%RPO)
PARAMETER 04972-10
Methods: EPA SW-846, ·update III.
NC DEHNR Cert. #269
04972-11 04972-12 04972-13 04972-14
Comment: All associated QA/QC samples were within the SL quality control
requirements.
~l!illl"VtKAVnl I A11Jf& MILLER, INC.
.A11lJ/Environmental Services
Laboratory Task Order No. __ _
Project Number .Jco= 202.. c, 16 •<~ao,
Project Location ..,,C"'')·.,.\',,.~e.:J:,,.:.:/J=-<..=.· ____ _
Laboratory0,; ,r<;...,,~.t.. (_6 ~
Sampler(s)/Affiliation ~ · H "..:SJ""'-:-
Date/Tme
SAMPLE IDENTITY Code Sampled
?:>·0,l.a~.:.. L =,./ 2!)/~ ce.~c.
('' 1' ..L ., I "· l. ·1-,•c:e1.:.
Lab ID
Sample Code: · L = Liquid; . S = Solid; A = Air
Relinquished by: / / · / / I _..,..._-
Received by: /f;!. L-,
I
V
S\. "
..-s
Organization: /.J .--, f.-,
Organization: ~r, •-5 8'-' v..l.~
CHAIN-OF-CUSTODY RECORD Page,_~_ ot_j_ .
· SAMPLE BOTTLE / CONTAINER .DESCRIPTION
Total No. of Bottles/
Containers
Date, 7: (2:5 I ~ime i 7 3 s::>
Date, ·7 /2' I"' Time 6''{c,
I
TOTAL
J
~al Intact?
~ No N/A
Relinquished·by: ______ .:.._ ____ Organization: ___________ Date ' ' Time,______ Seal Intact?
Received by: --------;::-;;-;-;-:::-=-=-=--,'.:0'.'..:rg~a~n~iza'.'.'.t'.::io~n::....::===========--=D~a::le'.==='== '=-'..T'.'..'.im~e'.::===========-:..1~%&>'.'.::'.'.~N~o::__'.N~l:AJ
Special lnstructions/Re~a ·· n.o/-·, ·rf:· .. , / Ir, 'l-e 11 t(,. · · _,____ !/.. · .e11.c.. · / _ I r ~.1 ! -<! <'_;)-~ .-P.. -~, -_ 3 ~ft~.
Delivery 'Method: D In Perso'n ()vf Comm6n Carner ..1.;;;._,-=-_l_,6,.,,___ ____ _ •• , SPECIFY -·--·---

-

-

-
-· i--D Lab Courier --·-D Other----~---
--,.FYs..411111768-
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RECEIVED
JAN 26 2001 5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
ARCADIS Geraghty & Milter. LOG NO: S0·05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
PO. No.: LT0#071700
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Client
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
05051·1 CMMW05 07-27-00/09:15
05051·2 CMMW07 07-26-00/08:45 05051-3 CMMWlO 07-26-00/15:20
05051-4 CMMW15 07-26-00/17:00
05051-5 CMMW17 07-26-00/16:50
PARAMETER 05051-1 05051-2 05051-3 05051-4 05051-5
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide) , ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
l,1-Dichloroethene, ug/1
l,l·Dichloroethane; ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<1000
<1000
<1000
<1000
<5000
<25000
<1000
<1000
<1000
650J
<1000
<1000
<1000
<10000
<1000
<1000
<2.0
<2.0
<2.0
<2.0
<10
<50
<2.0
<2.0
<2 .0
51
<2.0
<2,0
<2.0
<20
<2.0
<2.0
<1000
<1000
<1000
<1000
<5000
<25000
<1000
480J
<1000
87000
<1000
<1000
<1000
<10000
<1000
<1000
STL Savannah is a part of Severn Trent Laboratories. 1nc.
<2.0
<2.0
<2 .o
<2.0
<10
<50
<2.0
<2.0
<2.0
4.2
<2.0
<2 .o
<2.b
<20
.<2 .0
<2.0
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1; ,1
28
<1.0
<1.0
<1.0
<10
<1.0
<1.0
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051
Received: 28 JUL oo
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 2
DATE/
LOG NO
05051-1
05051-2
05051-3
05051-4
05051-5
SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
CMMW05 07-27-00/09:15
CMMW07 07-26-00/08:45
CMMWlO 07-26-00/15:20
CMMW15 _07-26-00/17:00
CMMW17 07-26-00/16:50 -----------------------------------------------------------------------------------
PARAMETER
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone
(MIBK) , ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
05051-1
<1000
<1000
<1000
<1000
180000
<1000
<1000
<1000
<1000
<1000
<10000
<10000
12000 ·
<1000
<1000
<1000
<1000
<2000
----------
05051-2 05051-3 --------------------
<2.0 <1000
<2.0 <1000
<2 .0 <1000
<2.0 <1000
220 83000
<2.0 <1000
<2.0 <1000
<2.0 <1000
<2.0 <1000
<2.0 <1000
<20 <10000
<20 <10000
29 3400
<2.0 <1000
<2.0 <1000
<2. 0 <1000
<2.0 <1000
<4 .0 <2000 ----,----------------
STL Savannah is a part of Severn Trent Laboratories, Inc.
05051-4 05051-5
--------------------
<2.0 <1.0
<2 .0 <1.0
<2.0 <1.0
<2.0 <1.0
180 27
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
<20 <10
<20 <10
9.8 9.7
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
<2.0 <1.0
<4 .0 <2.0
--------------------
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5102 L..aRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.s~nc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: .Mr. Mark Radecke
LOG NO
05051-1
05051-2
05051-3
05051-4
05051-5
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
PARAMETER
CMMW05
CMMW07
CMMWl0
CMMW15
CMMW17
-----------------------------
Surrogate Toluene-dB
05051-1
----------
92 %
Surrogate -4-Bromofluarobenzene 90 %
Surrogate -Dibromofluoromethane 110 %
Dilution Factor 1000
Analysis Date 08.03.00
Batch ID 100803
Chromium (6010), mg/1 <0.010
Dilution Factor 1
Prep Date 07.31.00
Analysis Date 08.03.00
Batch ID 0731I
Nickel (6010), mg/1 <0. 040
Dilution Factor 1
Prep Date 07.31.00
Analysis Date 08.03.00
Batch ID 0731I ---------------------------------------
05051-2
----------
94 %-
92 \-
112 'Ir
2
08.03.00
100803
<0.010
1
07.31.00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I ----------
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 3
05051-3
----------
94 %-
92 'Ir
110 'Ir
1000
08.03.00
100803
<0.010
1
07.31.00
08.03.00
0731I
<0.040
l
07.31.00
08.03.00
0731I ----------
DATE/
TIME SAMPLED
07-27-00/09:15
07-26-00/08:45
07-26-00/15:20
07-26-00/17:00
07-26-00/16:50
05051-4
----------
94 %-
90 %-
114 'Ir
2
08.03.00
100803
0.014
1
07.31.00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
05051-5
94 'Ir
92 %-
ll.O %
1
08.02.00
100802
0.16
1
07.31.00
08.03.00
0731I
0.12
1
07.31.00
08.03.00
0731I
--------------------
STL Savannah is a part of Severn Trent laboratories, Inc.
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-lnc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
05051-1 CMMW05
05051-2 CMMW07
05051-3' CMMWlO
05051-4 CMMW15
05051-5 CMMW17
PARAMETER 05051-1 05051-2 -------------------------------------------------
Copper (6010), mg/l <0.020 <0.020
Dilution Factor 1 1
Prep Date 07.31.00 07.31.00
Analysis Date 08.03.00 08.03.00
Batch ID 0731I 0731I -------------------------------------------------
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 4
05051-3 ----------
<0.020
1
07.31.00
08.03.00
0731I
----------
DATE/
TIME SAMPLED
07-27-00/09:15
07-26-00/08:45
07-26-00/.15 :20
07-26-00/17:00
07-26-00/16:50
05051-4 05051-5
----------
<0.020
1
07 .31.00
08.03.00
0731I
----------
<0.020
1
07.31.00
08.03.00
0731I
STL Savannah is a part of Severn Trent Laboratories, Inc.
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr.-Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box,31388
.Ralei.gh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO
05051-6
05051-7
05051-8
05051-9
·05051-10
SAMPLE DESCRIPTION, LIQUID SAMPLES
CMMW19
CMMW20 ·
CMMW21
CMMW22A
CMMW23
PARAMETER 05051-6
I Volatiles by GC/MS (8260)
Chloromethane, ug/1 <l. O
Bromomethane (Methyl <1.0
bromide) , ug/1
Vinyl chloride, ug/1 <1.0
Chloroethane, ug/1 <1.0
Methylene chloride <5.0
(Dichloromethane), ug/1
Acetone, ug/1 <25
Carbon disulfide, ug/1 <1.0
1,1-Dichloroethene, ug/1 <1.0
1,1-Dichloroethane, ug/1 <1.0
cis-1,2-Dichloroethene,. ug/1 2.3
trans-1,2-Dichloroethene, ug/1 <1.0
Chloroform, ug/1 <1.0
1,2-Dichloroethane, ug/1 <1.0
2-Butanone (MEK) , ug/1 <10
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<1.0
<1.0
05051-7
<10
<10
<10
<10
<50
<250
<10
30
<10
26
<10
10
<10
<100
7.7J
4.8J
----------
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 5
DATE/
TIME SAMPLED
05051-8
<5.0
07-25-00/16:15
07-26-00/09:45
07-25-00/17:30
07-26-09/16:00
07-25-00/14:45
05051-9
<1.0
<5 .0 .. <1.0
<5.0 <1.0
<5.0 <l.0
<25 <5.0
<120 <25
<5.0 <1.0
<5.0 <1.0
<5.0 <1.0
270 <l.0
2.2J <1.0
<5.0 <1.0
<5.0 <1.0
<50 <10
c5.0 <1.0
<5.0 <1.0
05051-10
<2.0
<2.0
<2. 0
<2 .0
<10
<50
<2.0
<2.0
<2 .0
80
<2.0
<2 .0
<2 .o
<20
<2.0
<2 .0
------------------------------
STL Savannah is a part of Severn Trent Laboratories. Inc.
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • WW\•Y.stl-lnc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
05051·6
05051-7
05051·8
05051·9
05051·10
REPORT OF RESULTS ·
SAMPLE DESCRIPTION, LIQUID SAMPLES
CMMW19
CMMW20
CMMW2l
CMMW22A
CMMW23
PARAMETER 05051-6 ---------------------------------------
Bromodichloromethane, ug/1
l,l,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
l,l,2·Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4'Methyl•2·pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate· Dibromofluoromethane
Dilution Factor
<l.0
<l.0
<l.0
<l.0
16
<1.0 ·
<l.0
<l.0
<l.0
<l.0
<10
<10
62
<l.0
<l.0
<l.0
<l.0
<2.0
92 'Ir
92 %-
112 'Ir
1
Analysis Date
Batch ID
08.02.00
100802
05051-7
<10
<10
<10
<10
59
<10
<10
<10
<10
,<10
16J
16J
1200
<10
<10
<10
<10
<20
94 'Ir
92 %
112 'Ir
10
08.03.00
100803
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Requisition: SQ98·0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 6
05051-8
<5;o
<5.0
<5.0
<5.0
100
<5.0
<5.0
<5.0
<5. o
<5.0
<50
<50
620
DATE/
TIME SAMPLED
07·25·00/16:15
07•26-00/09:45
07·25·00/17:30
07-26-00/16:00
07-25-00/14:45
05051·9
<l.0
<l.0
<l.0
<l.0
<1.0
<l.0
<l.0
<l.0
<1.0
<1.0
<10
<10
<l.0
<l.0
<l.0
<l.0
<l.0
<2.0
94 'Ir
92 'Ir
05051·10
<2.0
<2.0
<2.0
<2.0
43
<2.0
<2.0
<2.0
<2.0
<2.0
<20
<20
320
<2.0
<2.0
<2.0
<2.0
<4 .o
92 \-
90 %-
<5 .o
8 .3 ·
<5 .o
<5 .o
<10
94 'Ir
90 'Ir
110\-
5
08.02.00
100802
112 'Ir
1
08.02.00
100802
112 \-
2
08.03.00
100803
STL Savannah is a part of Severn Trent Laboratories, Inc.
I
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax; 912 352 0165 • www.sll-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
·05051-6
05051-7
05051-8
05051-9
05051-10
REPORT OF, RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
CMMW19
CMMW20
CMMW21
CMMW22A
CMMW23 ,
PARAMETER
Chromium (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
. Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Copper (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
-- ---------------------------
05051-6 05051-7
--------------------
<0.010 <0.010
1 1
07.31.00 07.31.00
08.03.00 08.03.00
0731I 0731I
<0.040 <0.040
l 1
07.31.00 07.31.00
08.03.00 08.03.00
0731I 0731I
<0.020 <0.020
1 1
07.31.00· 07.31.00
08.03.00 08.03.00
0731I 0731I
--------------------
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25, JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 7
05051-8
----------
<0.010
1
07.31.00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
<0.020
1
07.31.00
08.03.00
0731I ----------
DATE/
TIME SAMPLED
07-25-.00/16:15
07-26-00/09:45
07-25-00/17:30
07-26-00/16:00
07-25-00/14:45
05051-9
<0.010
1
07 .31. 00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
<0.020
1
07.31.00
08.03.00
0731I
05051-10
<0.010
1
07 .31. 00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
<0.020
1
07.31. 00
08.03.00
0731I
--------------------
STL Savannah is a part of Severn Trent Laboratories, Inc.
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.sti.inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc:
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master.
Project: NC000202.0170.0000
·sampled By: Client
Code: 161810125
Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
05051-11 CMMW24 07-25-00/13:30
05051-12 CMMW26 01-26-00/13:10
05051-13 EB-1 07-26-00
--------------------------------------------------
PARAMETER 05051-11 05051-12 05051-13 -------------------------------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1, 1, 2, 2·-Tetrachloro8thane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
----------
STL Savannah is a part of Severn Trent LaboratorieS, Inc.
<1.0 <1.0
<1.0 <1.0
2.0 <1.0
<1.0 <1.0
<5.0 <5.0
<25 <25
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
78 <1.0
1.5 <1,0
1.2 <1.0
<1.0 <1,0
<10 <10
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
--------------------
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
LOG NO
05051-11
05051-12
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
CMMW24
CMMW26.
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98·0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 9
DATE/
TIME SAMPLED
07-25-00/13:30
07-26-00/13:10
05051·13 EB·l 07-26·00
PARAMETER
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate ·.Toluene-dB
Surrogate· 4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis _Date
Batch ID
05051·11
----------
1.1
<1.0
<l.0
<1.0
<l.0
<1.0
<10
<10
<l.0
<1.0
<1.0
<1.0
<1.0
<2.0
94 %
92 %
112 %
1
08.03.00
100803 ----------
STL Savannah is a part of Severn Trent laboratories, Inc.
05051-12 05051-13
--------------------
14 2.0
<l.0 <l.0
<1.0 <l.0
<1.0 <l.0
<1.0 <1.0
<1.0 <1.0
<10 <10
<10 <10
180 <1.0
<1.0 <l.0
<1.0 <l.0
<1.0 <1.0
<1.0 <1.0
<2. 0 <2.0
94 % 94 %
90 % 88 %
112 % 112 %
1 1
08.02.00 08.02.00
100802 100802
--------------------
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
REPORT. OF RESULTS Page 10
LOG NO
05051-11
05051-12
05051-13
SAMPLE DESCRIPTION, LIQUID SAMPLES
CMMW24
CMMW26
EB-1
PARAMETER
·----------------------· ----------------·----------
Chromium (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Copper (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
-------------------------------------------------
05051-11
----------
<0.010
1
07 .31.00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
<0.020
l
07.31.00
08.03.00
0731I
----------
STL Savannah is a part of Severn Trent Laboratories, Inc.
DATE/
TIME SAMPLED
07-25-00/13: 30
07-26-00/13:10
07-26-00
05051-12 05051-13
--------------------
<0.010 <0.010
1 1
07.31.00 07.31.00
08.03.00 08.03.00
0731I 0731I
<0.040 <0.040
1 1
07.31.00 07.31.00
08.03.00 08.03.00
0731I .0731I.
<0.020 <0.020
1 l
07.31.00 07 .31.00
08.03.00 08.03.00
0731I 0731I
---------- ----------
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5102 laRoche Avenue • Savannah. GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 0l
Client PO. No.: LTO#07l700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0l70.0000
Sampled By: Client
Code: 161810125
Page ll
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
05051-14 CMMW04 07-26-00/15:55
05051-15 DUPLICATE 07-26-00
PARAMETER 05051-14 05051-15
--------------------------------------- ------------------------------ ----------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
l,l-Dichloroethene, ug/1
l,l-Dichloroethane, ug/1
cis-l,2-Dichloroethene, ug/1
trans-l,2-Dichloroethene, ug/1
Chloroform, ug/1
l,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
l,l,l-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
l,l,2,2-Tetrachloroethane, ug/1
l,2-Dichloropropane, ug/1
trans-l,3-Dichloropropene, ug/1
Trichloroethene, ug/1
<50
<50
<50
<50
<250
<1200
<50
<50
<50
ll0
<50
<50
<50
<500
<50
<50
<50
<50
<50
<50
6900 ----------
STL Savannah is a oart of SP.Vern TrPnt I ;iht'lr;itnripc;__ lni-
<50
<50
<50
<50
<250
<1200
<50
<50
<50
100
<50
<50
<50
<500
<50
<50
<50
<50.
<50
<50
5800
--------------------
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stt-inc.com STL Savannah
LOG NO
Mr. Nanjun Shetty
AR.CADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 12
DATE/.
TIME SAMPLED
-----------------------------------------------------------------------------------
05051-14 CMMW04 07-26-00/15:55
05051-15 DUPLICATE 07-26-00
PARAMETER 05051-14 05051-15
-------------------------------------------------
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide, Total (9010), ug/1
Dilution Factor
Prep Date
Analysis Date·
Batch ID
----------
<50
<50
<50
<50
<50
<500
<500
520
<50
<50
<50
<50
<100
94 'Ir
90 %-
112 'Ir
so
08.03.00
100803
170
1
08.02.00
08.03.00
0802'1'
STL Savannah is a part of Severn Trent Laboratories, Inc.
----------
<50
<50
<50
<50
<50
<500
<500
430
<50
<50
<50
<50
<100
94 %-
94 'Ir
114 \-
50
08.03.00
100803
180
1
08.02.00
08.03.00
0802T
----------
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. ·Box 3_1388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 13
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
05051-14 CMMW04 07-26-00/15:55
05051-15 DUPLICATE 07-26-00
PARAMETER 05051-14 05051-15
Cyanide, Amenable (9010), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Copper (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chromium (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
29
1
08.02.00
08.03.00
0802T
<0.020
1
07.31.00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
<0.010
1
07.31.00
08.03.00
0731I
57
1
08.02.00
08.03.00
0802T
<0.020
1
07.31.00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
<0.010
1
07.31.00.
08.03.00
0731I
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.sll-inc.com STL Savannah
I
I
LOG NO: S0-05051
Received: 28 JUL 00 ·1
Reported: 07 AUG 00
Mr. Nanjun Shetty.
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 14
LOG NO
'05051-16
05051-17
05051-18
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
PARAMETER
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
. 1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
------------------·-------------------------------
05051-16
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
05051-17 05051-18
<1.0 76 % 46-147 %
<1.0 ---
<1.0
<1.0
<1.0
<1.0.
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
STL Savannah is a part of Severn Trent Laboratories. Inc.
I
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.sU-inc.com STL Savannah
Mr. Nanjun Shetty
ARCAD.IS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 15
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
-----------------------------------------------------------------------------------
05051-16 Method Blank
05051-17 Lab Control Standard% Recovery
05051-18 LCS Accuracy Control Limit (%R)
PARAMETER
Trichloroethane, ug/1
Dibrornochlorornethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Brornoforrn, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1·
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate. -Toluene-dB
Surrogate -4-Brornofluorobenzene
Surrogate -Dibrornofluorornethane
Dilution Factor
Analysis Date
Batch ID
05051-16 05051-17
<l. 0 86 %
<1.0
<1.0
<1.0 86 %
<1.0
<1.0
<10
<10
<l. 0.
<l. 0 94 %
<1.0 96 %
<1.0
<1.0
<2.0
92 %
94 %
114 %
1
08.02.00
100802
92 %
96 %
116 %
1
08.02.00
100802
----------
STL Savannah is a oart of Severn Trent Laboratories. Inc.
05051-18
56-143 %
62-135 %
68-131 %
72-127 %
77-122 %
74-126 %
70-130 %
1
08.02.00
----------
5102 LaRoche Avenue • Savannah, GA 31404 • Te!: 912 354 7858 • Fax: [phone] • www.stHnc.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Client
STL Savannah
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
PO. No.: LTO#071700
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
REPORT OF RESULTS Page 16
DATE/
LOG NO
05051-16
05051-17
05051,18
SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES TIME SAMPLED --------------------------------------------------
PARAMETER
Method Blank
Lab Control Standard 'Ir Recovery
LCS Accuracy Control Limit ('lrR)
Cyanide, Total (9010), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide, Amenable (9010), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chromium (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Nickel (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
05051-16
<5.0
1
08.02.00
08.03.00
0802T
<5.0
1
08.02.00
08.03.00
0802T
<0.010
1
07.31.00
08.03.00
0731I
<0.040
1
07.31.00
08.03.00
0731I
STL Savannah is a part of Severn Trent laboratories, lnc.
05051-17
96 %
1
08.02.00
08.03.00
0802T
106 'Ir
1
07 .31.00
08.03.00
0731I
104 'Ir
1
07 .31.00
08.03.00
0731I
05051-18
85-115 %-
75-125 %-
75-125 'Ir
I
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I.
I
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I
5102 L..aRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O .. Box ·31399
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
Client
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Clien.t
Code: 161810125
Page 17
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
05051-16 Method Blank
05051-17 Lab Control Standard% Recovery
05051-18 LCS Accuracy.Control Limit (\R)
---------------------------------------------------·-------------------------------
PARAMETER
Copper (6010), mg/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
-----------------------------
05051-16
<0.020
1
07 .31.00
08.03.00
0731I
STL Savannah is a oart of Severn Trent Laboratories. Inc.
05051-17
105 %
1
07 .31.00
08.03.00
0731!
05051-18
75-125 %
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com · STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LT0#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 18
DATE/
LOG NO SAMPLE DESCRIPTION QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
05051-24 Matrix Spike 'Ir Recovery (CMMW04)
05051-25 Matrix Spike Duplicate%, Recovery (CMMW04)
PARAMETER 05051-24 05051-25
Volatiles by GC/MS (8260)
1,1-Dichloroethene, ug/1
Trichloroethene, ug/1
Benzene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Surrogate Toluene-de
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Cyanide, Total (9010), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Chromium (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
88 'I-
68 'Ir
104 'Ir
112 %
116 'Ir
92 'Ir
92 'Ir
116 'Ir
50
08.03.00
96 'Ir
1
08.02.00
08.03.00
0802T
105 %-
1
07.31.00
08.03.00
0731I
STL Savannah is a part of Severn Trent laboratories, Inc.
88 'Ir
64 'Ir
108 'Ir
116 'Ir
120 'I-
92 'I-
92 'Ir
112 'I-
so
08.03.00
96 'Ir
1
08.02.00
08.03.00
0802T
104 %-
1
07.31.00
08.03.00
0731I
I
I
I
I
I
I
I
I
I
I
I
1:,
I
I
I
I
I
I
I.
I
I
I
I
I
I
I
I
I
I
I
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.sll-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Raleigh, NC 27612 Requisition: SQ98·0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
REPORT OF RESULTS Page 19
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
05051·24 Matrix Spike% Recovery (CMMW04)
05051-25 Matrix Spike Duplicate% Recovery (CMMW04)
-----------------------------------·------------------------------------------------
·PARAMETER 05051·24 05051·25
Nickel (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
Copper (6010), %
Dilution Factor
Prep Date
Analysis Date
Batch ID
102 %
1
07.31.00
08.03.00
07311
101 %
1
07.31.00
08.03.00
07311
107 % 109 %
1 1
07.31.00 07.31.00
08.03.00 08.03.00
07311 07311
STL Savannah is a □art nf SevPrn Tri=>nt I ::ihnr::itnriP<: !nr
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller' Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Requisition: SQ98·0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 20
DATE/
LOG NO
05051·21
05051·22
05051·23
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED --------------------------------------------------
MS Accuracy Advisory Limit (%-R)
Precision (%-RPD) MS/MSD
MS Precision Advisory Limit (%-RPD)
--------------------------------.------------------
PARAMETER
Volatiles by GC/MS (8260)
l,l·Dichloroethene, ug/1
Trichloroethene, ug/1
Benzene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Surrogate Toluene·d8
Surrogate -4-Bromofluorobenzene.
Surrogate -Dibromofluoromethane
Analysis Date
Cyanide, Total (9010), mg/1
Cyanide, Amenable (9010), mg/1
Chromium (6010), 'Ir
Nickel (6010), 'Ir
Copper (6010), 'Ir
05051·21
46·147 'Ir
56·143 'Ir
62·135 'Ir
68·131 'Ir
72·127 'Ir
77·122 'Ir
74·126 'Ir
70-130 'Ir
08.03.00
85·115 'Ir
75·125 'Ir
75·125 'Ir
75·125 'Ir
STL Savannah is a part of Severn Trent Laboratories, Inc.'
05051·22
0 'Ir
1 'Ir
4 'Ir
4 'Ir
3 'Ir
08.03.0_0
0 'Ir
0.96 'Ir
0. 99 %-
1. 9 'Ir
05051·23
<30 'Ir
<35 'Ir
<37 'Ir
<33 %-
<22 'Ir
<30 'Ir
<20 'Ir
<20 'Ir
<20 'Ir
I
I
I
I
••
I
I
I
I y
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
LOG NO
05051·21
05051·22
05051·23
Mr. Nanjun Shetty
ARCADIS Geraghty &'Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05051.
Received: 28 JUL 00
Reported: 07 AUG 00
Revised: 25 JAN 01
Client PO. No.: LTO#071700
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170.0000
Sampled By: Client
Code: 161810125
Page 21
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
MS Accuracy Advisory Limit (%R)
TIME SAMPLED
Precision (%RPD) MS/MSD
MS Precision Advisory Limit (%RPD)
PARAMETER 05051·21 05051-22 05051-23
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
Comment: All associated QA/QC samples were within the SL quality control reqtlirements.
Final Page Of Report
STL Savannah is a part of Severn Trent laboratories, Inc.
ARCADIS GERAGHTY & MILLER Laboratory Task Order No.IP.a. No. Of/-,OC CHAIN-OF-CUSTODY RECORD Page _L_ of___:c_
N Project Number/Name , ta:CZoZ. ~-l ]<.> • C-<o"= I ANALYSIS/ METHOD/ SIZE . I
Project Location c,K{b-Jl Al<... (v
Laboratory St L/Sc,.Jo,,, ~,, ~ I "'l.,, . V -~ '-:I ,:..,,_.
Project Manager !0,,,...., /~ -,5. L. rf7. '-. '? Y,v ..,·, ~;,·
·!' .J ~,; VI. ._. ~" u.~ '-
Sampler(s)/Affiliation ,/rec 1,u. ·1 h -:s.~ ,,_,,_ ~ • < ' l -~"' ~ ~ (.;v \Jv. '-' r 0 \,,'\ ~-' .f -j .::!X: j .f ±-
Dateffime "\i) -f '-,J -l>_ SJ O ~,f 0
Sample ID/Location Matrix Sampled Lab ID ·V'§? 'I. \J J (V \ 1(,/IJi -J. {!" -:" Remarks Total
c ,t..-i 1--1w o</ L 7-,,r., ~
le>:5~ :3 I I I ~
(.. M ,-.... W 05 .,,. .t:.. ,_ f --
O?/ft 3 I 4
<...•~MW◊ f 7/Z"''"° cB'l5 ~ I t/
C"4h (,) to 'f/Ul<rO /,., Le 3 I '{
/ M H W ,5 I rt Z, G I"""'-
I 7-"'"" ~ I '1
<._ "4 Mv.J Ir r(2.Gr~..:. 3 I '-f ,✓---,I; c-
(_ht-,_ W 19 r/Z:,t<-= 3 r 'i /¢,I:!,
<'.,MM(>J ?C 7/2.'-t~~ -~ I '1 -C:,',4',;
(_<'--1 MW z { ()~-' 11' 1-, .. ,,1= /"f,,a ~ I '1
( t'--1 1--11..J 2. <..ft :.--.,..,·~?1---0 I '-I /600 -:.:
C,...i'-1w ~-3 I ?,1.!5/~--0
I "('f'> 3 I '-I
(... .--, M ._J c.1 i I, , r1~•~~ ,_ ~ ~ I i../
c_ f-1 MW ·c.r ..... .,,.,~r-;;: ..._°.:;! I
. ;; I /c.
Sample Matrix: L = Liqui~ S = Solid; A= Air Total No. of Bottles/ 5-I . :,.-, Containers
Relinquished by:/ // / / / -~-Organization: n-~.-./ ·, Date 7'-12r.1 <"•Cl Time /e,50 Seal Intact?
Received by: t'/ /1,/' -' · Organization: •;'71:, -S,,</ I Date ? l-Z-1' 1t>V Time <z , ., · I @ No N/A cl ' / • I -,
Relinquished by: Organization: Date I I Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Spec,al Instructions/Remarks: ___________________________________________ _
Delivery Method: -- -
□ In Person .. -~ommon Carrier t= <:c.,( £x
..-_, •'-1111111 W"FY-
□ Lab Courier □Other~--------- -"'-.. _,rn,_,,,, ..
II!!!! .. _, .. -.. _, --...
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No.oH"f:P ----·------CHAIN-OF-CUSTODY RECORD Page -l-otL
Project Number/Name ;.}cc-.scz_o·;: er?<::-· oc-c:,ez._ I ANALYSIS/ METHOD/ SIZE [
Project Location Ox/1-J, 0<... ;----r,,,.---,-------,-----r---_-~----1
Laboratory :STl, .lx, Uo. <-< ,-, • L [J.:, ~ t,~"..,.;"'
(,
,;;_.J ;-, ':v ~ I) • ~ ..JI ...._ ,, .,,,-• 1i v· ~
Project Manager .., , ~ -U /2> '''t . , ~ ·.v ->/"\~ u" · V. .f ~ -.'.)' I\/ J 'v ~ t• "'--\j;_ \Y V
Sampler(s)/Affiliation 'VCrc,,v./ ,-1 ~..ls«------...., , ~ .;_,,, !! ,.., v'\y ~ 'v.., ,t '('-
ci" ·,' 'I'" o 1J ~ -0 0 ,r XJ 0
Sample ID/Location
__.1 I ' r , ~, -, J I,
Matrix
L
Datemme
Sampled
....
Lab ID ~ ~ r',:J, 1/,1 ig<o '{ .g "?;
~ I I /
3 I I I
3 I I I
j
Remarks Total
G
~
(
~ .
3 ,,;
-
@
Sample Matrix: L = Liquid; S = Solid; A = Air -~
Total No. of Bottles/ 2_'3 "Z.f"
Containers ---
Relinquished by: · -Organization:..pl.li""'-=~~-----Date~~-="-'---Time ;e;To
Received by:--!..;1~·-:.;·,:z.'"'-"'•e;LJ""'------Organization: 5C(., ✓ 56''1 Date r:✓11(IV Time q., cl
Relinquished by: Organization: Date_~-~--Time ____ _
Received by: Organization: Date Time
Seal Intact?
~-No N/A
Seal Intact?
Yes No N/A
Special Instructions/Remarks: ___________________________________________ _
Delivery Method: □ In Person , Common Carrier re.,) ::-. ----"<-----□ Lab Courier □Other _______ _
SPEC I FY SPECIFY
◄
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S _\a:~, a~ nz.. 11{.~;h Labor;atories
•-.. -.r .... i.-a-.1n<. 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
RECEIVED
SEP !'lS i:uu1J
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP oo.
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, IiMCADTS Geraghly & Miller Client PO. No. : LTO#041900-A
P.O. Box 31388
LOG NO
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 104100912
Page 1
DATE/
TIME SAMPLED
------------------------------------------------------------------------------------
05643-1 DISCHARGE 08-16-00/15:45
----------- -------------------------------------------------- ---·--------------------
PARAMETER
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
05643-1
---------- ------------------------------ ----------
11
1
08.27.00
08.28.00
0827S
---------- ----------------------------------------
S afv~a;,n.n,a,h taboiatOri'eS 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 104100912
Page 2
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
05643-1 DISCHARGE 08-16-00/15:45
PARAMETER
Volatiles by GC/MS (8260)
Chlo.romethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1;2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
05643-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
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I
I
I
5102 LaRoche Avenue · Savannah, GA 31404 • [phone] · Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTOi041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 104100912
REPORT OF RESULTS Page 3
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
------ --------------------------- ----- ----------------------- ----------------- -- ----
05643-1 DISCHARGE 08-16-00/15:45
-------- --- -------------------------- ----- ------------------- ------- ---------- -- -- --
PARAMETER 05643-1
-------------------------------------------------------------------------------
1,1,2-Trichloroethane, ug/1 <1.0
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluoromethane
Dilution Factor
Analysis Date
Batch ID
<l.0
<l.0
<l.0
<10
<10
<l.0
<l.0
<l.0
<l.0
<l.0
<2.0
100 %-
92 %-
98 %-
1
08.24.00
1B0824
s:a:v•'aimnVa, h
1.::abor1atCfrfes 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
C.ode: 104100912
Page 4
DATE/
TIME SAMPLED
----------------------------------------------- ----------------------------- ----- ---
05643-2 TRIP BLANK 08-16-00
----------- ------------------------------------------------------------------- ------
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1, 2-Di_chloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
05643-2
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
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5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] · www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 104100912
REPORT OF RESULTS Page 5
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
--- ------------------------------------- --------------------- ------------------- ----
05643-2 TRIP BLANK '08-16-00
- - ----------------------------------------------------------- --- ----------- ----- ----
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluoromethane
Dilution Factor
Analysis Date
Batch ID
05643-2
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
100 'Ir
94 'Ir
110 'Ir
1
08.24.00
1B0824
------------------------------------------------- ---------- --------------------
~,a•,y.~a: n~nr_a11'!_
t:abor,ator,1es 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 104100912
Page 6
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
05643-3 Method Blank
05643-4 Lab Control Standard% Recovery
05643-5 LCS Accuracy Control Limit (%R)
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
05643-3
<1.0
<l.0
<1.0
<1.0
<5.0
<25
<1.0
05643-4 05643-5
<1.0 108 % 46-147 %
<1.0
<l:0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
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5102 I.aRoche Avenue• Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 104100912.
REPORT OF RESULTS Page 7
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
05643-3 Method Blank
05643-4 Lab Control Standard% Recovery
05643-5 LCS Accuracy Control Limit (%R)
_PARAMETER 05643-3
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<LO
<1.0
<1.0
<2.0
100 %
92 %
112 %
1
08.24.00
1B0824
05643-4
98 %
112 %-
96 %-
96 %
104 %-
96 %-
112 %
1
08.24.00
1B0824
05643-5
56-143 %-
62-135 %-
68-131 %-
72-127 %-
77-122 %
74-126 %-
70-130 %
S; ~~ta1 m!',;_~~.h ~aborator,res •-ol-y,........_,..,_ 5102 LaRocheAvenue • Savannah, GA31404 • [phone] • Fax[phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS'
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 104100912
Page 8
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
05643-3 Method Blank
05643-4 Lab Control Standard% Recovery
05643-5 LCS Accuracy Control.Limit (%R)
PARAMETER
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
05643-3
<5.0
1
08.27.00
08.28.00
0827S
05643-4
105 %
1
08.27.00
08.28.00
0827S
05643-5
85-115 %
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Sta~v;am,;ii/a.'h tfa bCfri:l'tOi-,ies· 5102 LaRoche Avenue • Savannah, GA 31404 • [phone] • Fax [phone] • www.stlsavlab.com
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Raleigh, NC 27612 Requisition: SQ98-0553
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code·: 104100912
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
------- ---- ------------------------- -- -- --------------------- ------- --------- -------
05643-9 MS%-Recovery(Batch)
05643-10 MSD % Recovery(Batch)
05643-11 MS Accuracy Advisory Limit (%R)
05643-12 Precision (%RPD) MS/MSD
05643-13 MS Precision Advisory Limit (%-RPD)
--------------------------------------------------- ------ ---- --------------- -- ------
PARAMETER 05643-9 05643-10 05643-11 05643-12 05643-13
----------------------------------------------------------- --------------------
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %-
Trichloroethene, \
Benzene, %-
Toluene, %'
Chlorobenzene, %-
Surrogate Toluene-dB
112 %
98 %
116%
98 %
96 %-
100 %
92 %-
102 %
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor 1
08.24.00 Analysis Date
Batch ID 1B0824
Cyanide (335.2), mg/1 104 %-
Dilution Factor 1
Prep Date 08.27.00
Analysis Date 08.28.00
Batch ID 0827S
---------------------------------------
112 %-46-147 % 0 % < 30 %
106 % 56-143 %-8 % < 35 %
122 % 62-135 % 5 % < 37 %
106 % 68-131 % 8 % < 33 %
104 % 72-127 %-8 %-< 22 %
102 % 77-122 %-< NA %
92 % 74-126 %-< NA %
110 % 70-130 %-< NA %-
1
08.24.00
180824
95 % 75-125 % 9.0 % <20 %
1
08.27.00
08.28.00
0827S
----------------------------------------
S,a~v a.n·tn,a h
l!abcrf,atCfr,ieS 5!02LaRocheAvenue, Savannah, GA31404 • [phone] · Fax[phone] • www.stlsavlab.com •-o!S.-,,T...,,l,,b<n-.ln<
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark·Radecke
REPORT OF RESULTS
LOG NO: S0-05643
Received: 18 AUG 00
Reported: 12 SEP 00
Client PO. No.: LTO#041900-A
Requisition: SQ98-0553
Contract No.: JFD Channel Master
Project: NC00.0202.0170
Sampled By: Client
Code: 104100912
Page 10
DATE/
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
05643-9
05643-10
05643-11
05643-12
05643-13 MS Precision Advisory Limit (%RPO)
PARAMETER 05643-9
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
05643-10 05643-11 05643-12 05643-13
Comment: All associated QA/QC samples were within the SL quality control
requirements.
Final Page Of Report
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Serial Number Ui:::'.~Ui:::'.U
-ANALYSIS REQUEST AND CHAIN OF CUSTODY RECORD ~ 5102 LaRoche Avenue, Savannah, GA 31404 Phone: {912) 354-7858 Fax: [phone]
0 2846 Industrial Plaza Drive, Tallahassee, FL 32301 Phone: [phone] Fax: [phone]
~ 0 900 Lakeside Drive, Mobile, Al 36693 Phone: (334) 666·6633 Fax: [phone] -== 0 6712 Benjamin Rd .. Suite 100. Tampa, FL 33634 Phone: [phone] Fax: [phone] a dl\1Cr<:n ol Sos~,n Tre"t l...,b<>r3lo"',s, l,,c.
PROJECT REFERENCE PROJECT NO. PROJECT LOCATION MATRIX PAGE I OF
.JF'D /(}/la.nf"JP 1 ,Mar J.. •-• il!OOO;Jl):J.. / 70 (STATE) ),/,C, TYPE REQUIRED ANALYSES I I -
TL (lA8J PROJECT MANAGER P.O. NUMBER CONTRACT NO. 0 0 ~· STANDARD REPORT ~
[?.1.,y_e .. ~ e~s f.., ,,,/G ,-...J DELIVERY w ~ OATEOUE_el___l,(lUA.,.4 ~ >--' ~ UENT (SITE) PM CLIE~J:;;~E CLIENT FAX z ~ ,/) .t-1/,'fffj' NI ct
., 'W'i ':J -_,;5 H " 'J/_ q· ' -S,o• ~i w :-§ ] > s;;: EXPEDITED REPORT J VI CLJE~r NA11,. I CLIE1't"1 EMAIL . 0 0 DELIVERY , 0 ~ "' C 1 A-,ee.A1)1S~tl,fAM1lk j '::$ '<:.) 0 (SURCHARGE) ... m £ ~ .,c -:s-~ ~ 0 " "' DATE DUE CLIENT ADDRESS ol30~ ~IA.lood~ »~·vc.. suik 5 /02.. ~ ir a ~ 0 w ~ OA~,--:.·,. &fr> z--,, '<'. u ~ "' i ~ 1,.i
1
\~!~t ~;1ttf ;z1il\ii:a1·
1
:1· 114,i'1;: NUMBER OF COOLERS SUBMJTTED PEA
1.,QMPANY CONTRACTlNG THIS W"""'K (il'applicable): ~~ ~ SHIPMENT: 0 la "' w I i . .-1·1 -ft ' . t ~1 ' . ·1 m ~ ~ ::t , , .1 •• , "(• -~ ~ i' •,. · , •t j· ·
0 0 0 SAMPLE ~ w .,c
SAMPLE IDENTIFICATION ~ ~ z NUMBER OF CONTAINERS SUBMITTED REMARKS DATE TIME 0 a ~ 0 u .,c ~ z
W~/no /SLiS D ,'<I./' ha r-tu v I ; -
1.r,·h R/o,1,,/t:_ '1' 3
I
-
.
RELINQUISHED BY: (SIGNATURE) f}E% TIME RELINQUISHED BY: (SIGNATURE) 3/17/lll TIME RELINQUISHED BY: (SIGNATURE) DATE TIME
liJ_(¼f} ,, 1~(i;}fiV'Wfftfllmm!t~ffi /J1fl,<{j'~ I'S"/ o ,,
RECEIVED BY: (SsGNATUR{) DATE TIME AECEl~Y: (SIGNATURE) uAT!f TIME RECEIVED BY: (SIGNATURE) DATE TIME
l'ef.:c~•·i:"jj' ,\;\!(nill1i",¼!ll/llrnUR.!JI
LABORATORY USE ONLY
RECEIVED FOR LABORATORY BY: 1%, TIME CUSTODY INTACT CUSTODY STL-SL LOG NO. LABORATORY REMARKS:
(SIGNATURE) )4 4 ~ SEAL NO.
'16'o5°'(:,t./3 '-;£v&,u "'lJ·· i¼o c,:zo -- - - ----. ----- - -
---
~ (!j
ii: 0
PLEASE FOLD THIS SHIPPING DOCUMENT IN HALF AND PLACE IT IN A WAYBILL POUCH AFFIXED
TO YOUR SHIPMENT SO THAT THE BAR-CODE PORTION OF THE LABEL CAN BE READ AND SCANNED.
--WARNING: USE ONLY THE PRINTED ORIGINAL LABEL FOR SHIPPING. USING A PHOTOCOPY OF
THIS LABEL FOR SHIPPING PURPOSES IS FRAUDULENT AND COULD RESULT IN ADDITIONAL
BILLING CHARGES, ALONG WITH THE CANCELLATION OF YOUR FEDEX ACCOUNT NUMBER.
FROM: Michele Rapp [phone]
arcadis geraghty & miller
2301 rexwoods drive SHIPPER'S FEDEX ACCOUNT NUMBER
102 ,
raleigh, NC 27607
TO: ANGI Weimerskirk [phone]
Savannah Laboratories
5102 La Roche Avenue
Savannah, GA 31404-
REF: nc000202.0170.00001
OEI.JI/ERY ADDRESS BARCODE fFEDEX-EDR)
CAD# 3942852 PRIORITY OVERNIGHT
TRK # 7926 3619 2550 FORM 0201
Deliver By:
SAV lBAUGOO
Federal Express
SHIP DATE: 17AUG00
MAN-WGT: 3 LBS
,J; D o5 J:; t.,/ -~
·-.
FRI
AA
31404-GA-US XH SAVA
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RECEIVED
JAN 2 6 2001
w~
MMUN
5102 LaRoche Aven~!S.hltll"llmll!Jl'.~llgf2 354 7858 • Fax: [phone] • www.stl-inc.com
~
STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke Project:
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
LOG NO SAMPLE DESCRIPTION
REPORT OF RESULTS
LIQUID SAMPLES
Page 1
DATE/
TIME SAMPLED
---------------------------------------- --- ----------------- ---------- -- -----------
06187-1 DISCHARGE 09-11-00/15:15
---------- --------------------------- -- ------- --------------------- -- -- ------- -- ---
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1,
1,2-Dichloroethane, ug/1
2-Butanone (MEK) , ug/1
1,1,1~Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
--------------------------------------- ----------
06187-1
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
STL Savannah is a part of Severn Trent Laboratories, Inc.
lfl1RiW --5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.st!-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC:. Mr. Mark Radecke Project:
LOG NO: S0-06187
Received: 12 .SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
Page 2
DATE/
TIME SAMPLED
-----------------------------------------------------------------------------------
06187-1 DISCHARGE 09-11-00/15:15
------------------------------- - ---------------------------------------------------
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
Analysis Date ,
Batch ID
06187-1
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
90 %
98 %
108 %
1
09.14.00
1A0914
6.6
1
09.15.00
09.15.00
0915S
STL Savannah is a part of Severn Trent laboratories, Inc.
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~ ~Jl-
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Raleigh, NC 27612
CC: Mr. Mark Radecke
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
LOG NO
06187-2
06187-3
06187-4
PARAMETER
REPORT OF-RESULTS
SAMPLE. DESCRIPTION, LIQUID SAMPLES
CMMW-10
POW-1
TRIP BLANK
-------------------------------------------------.-
06187-2
DATE/
TIME SAMPLED
09-11-00/11 :25
09-11-00/12:10
09-11-00
06187-3
Page 3
06187-4
.-------------------------------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide) ,.ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK) ,' ug/1
1,1,l-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ,ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<1000
<1000
<1000
<1000
<5000
<25000
·<1000
<1000
<1000
140000
<1000
<1000
<1000
<10000
<1000
<1000
<1000
<1000
<1000
<1000
----------
STL Savannah is a part of Severn Trent Labo.ratories, Inc.
<250 <1.0
<250 <1.0
<250 . <l·.o
<250 <1.0
<1200 <5.0.
<6200 <25
<250 <1.0
<250 <1.0
<250 <1.0
50000 <1.0
<250 <1.0
. <250 <1.0
<250 <1.0
<2500 <10
<250 <1.0
<250 <1.0
<250 <1.0
<250 <1.0
<250 <1.0
<250 <1.0
--------------------
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stHnc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke Project:
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTOj041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
Page 4
DATE/
TIME SAMPLED
---------- ------------------------- ------------------------------------- ----- -- -- --
06187-2 CMMW-10 . 09-11-00/11:25
06187-3 POW-1 09-11-00/12:10
0.6187-4 TRIP BLANK
PARAMETER
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1 ·
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes,.Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Brornofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
09-11-00.
06187-2 06187-3
--------------------
48000 9200
<1000 <250
<1000 <250
<1000 <250
<1000 <25o·
<1000 <250
<10000 <2500
<10000 <2500
2400 540
<1000 · <250
<1000 <250
<1000 <250
<1000 <250
<2000 <500
94 % 90 %
98 % 98 %
130 % 110 %
1000 250
09.14.00 09.18.00
1A0914 1A0918
---------- ----------
STL Savannah is a part of Severn Trent Laboratories, Inc.
06187-4
----------
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<l. 0
<1.0
<1.0
<1.0
<1.0
<2.0
92 %
98 %
104 %
1
09.14.00
1A0914
----------
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&It~ ~-. ~
5102 laRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com $TL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke Project:
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
REPORT OF RESULTS Page 5
LOG NO
06187-5
06187-6
06187-7
PARAMETER
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
Method Blank
Lab Control Standard% Recovery
LCS Accuracy Control Limit (%R)
06187-5 06187-6 06187-7 --------------------------------------- -------------------- ---------- ----------
. Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
--------------------------------------- ----------
STL Savannah is a part of Severn TrE!nt Laboratories, Inc.
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<l.0
<1.0
<l. 0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<l.0·
116 % 46-147 %
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke Project:
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
REPORT OF RESULTS Page 6
LOG.NO
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
06187-5
06187-6
0.6187-7
PARAMETER
Method Blank
Lab Control Standard%-Recovery
LCS Accuracy Control Limit (%-R)
06187-5 06187-6
--------------------------------------- ------------------------------
Trichloroethane, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ·ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibrornofluoromethane
Dilution Factor
Analysis Date
Batch ID
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
90 %-
100 %-
110 %-
1
09.14.00
1A0914
STL Savannah is a part of Severn Trent Laboratories, Inc.
·102 %-
106 %-
96 %-
114 %-
90 %-
100 %-
112 " 1
09.14.00
1A0914
----------
06187-7
56-143 %-
62-135 %-
68-131 %-
72-127 %-
77-122 %-
74-126 %-
70-130 %-
1
09.14.00
1A0914
----------
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~f1ffl~
~ II'~
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
LOG NO
06187-5
06187-6
·06187-7
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Raleigh, NC 27612
CC: Mr. Mark Radecke
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
REPORT OF RESULTS
DATE/
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES TIME SAMPLED
--------------------------------------------------
Method Blank
Lab Control Standard 'I-Recovery
LCS Accuracy Control Limit ('1-R)
--------------------------------------------------
Page 7
PARAMETER 06187-5 06187-6 06187-7 -------------------------------------------------
Cyanide (335. 2), ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
----------
<5.0
1
09.15.00
09.15.00
0915S
--------------------
97 'I-85-115 'I-
1
09.15.00
09.15.00
0915S
-------------------------------------------------------------------------------
STL Savannah is a part of Severn Trent Labora_tories, Inc.
--5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl.inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Requisition: SQ00-0265
CC: Mr. Mark Radecke
Contract No.: JFD Channel Master
Project: NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: 113710125
REPORT OF RESULTS
LOG NO SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES
06187-11 MS%-Recovery(Batch)
06187-12 MSD %-Recovery(Batch)
06187-13 MS Accuracy Advisory Limit (%-R)
06187-14 Precision (%-RPD) MS/MSD
06187-15 MS Precision Advisory Limit (%-RPD)
Page a.
PARAMETER 06187-11 06187-12 06187-13 06187-14 06187-15
Volatiles by GC/MS (8260)
1,1-Dichloroethene, %-
Trichloroethene, %
Benzene, %-
Toluene, %-
Chlorobenzene, %
Surrogate Toluene-dB
122
108
118
106
122
90
%-
%-
%-
%-.
%-
%-
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
98
108
%-
%-
Dilution Factor l.
Analysis Date 09.14.00
Batch ID 1A0914
Cyanide (335.2), ug/1
Dilution Factor
Prep Date
.Analysis Date
Batch ID
100 %-
1
09.15.00
09.15.00
0915S
120 %-
106 %-
116 %-
104 . %-
114 %-
-94 %-
.100 %-
110 %-
l.
09.14.00
l.A0914
101 %-
1
09.15.00
09.15.00
09l.5S
46-147 %-
56-143 %-
62-135 %-
68-131 %-
72-127 %-
77-122 %-
74-126 %-
70-130 %-
l.
09'.14.00
l.A09l.4
STL Savanna~ is a part of Severn Trent Laboratories, Inc.
2 %-< 30 %-
2 %-< 35 %-
2 %-< 37 %-
2 %-< 33 %-
7 %-. < 22 %-
NA NA
NA NA
NA NA
l. l.
09.14.00 09.14.00
l.A0914 l.A09 l.4
1.0 % <20 %-
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li*lf.lffli
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl~nc.com STL Savannah
LOG NO
-06187-11
06187-12
06187-13
06187-14
06187-15
Mr. Nanjun Shetty
ARC.ADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-06187
Received: 12 SEP 00
Reported: 19 SEP 00
Revised: 25 JAN 01
Client PO. No.: LTO#041900-A
Raleigh, NC 27612
CC: Mr. Mark Radecke
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0160.00005/NC000202.0170.00006
Sampled By: Client
Code: ·113710125
REPORT OF RESULTS Page 9
SAMPLE DESCRIPTION, QC REPORT FOR LIQUID SAMPLES'
MS% Recovery(Batch)
MSD % Recovery(Batch)
MS Accuracy Advisory Limit (%R)
Precision (%RPO) MS/MSD
MS Precision Advisory Limit (%RPO)
-- -- ------------------------------- ------------------------------------------------
PARAMETER 06187-11
Methods: EPA SW-846, Update III.
NC DEHNR Cert. #269
06187-12 06187-13 06187-14 06187-15
Comment: All associated QA/QC samples were within the SL qu_ality control
requirements.
These test results meet all the requirements of NELAC. All questions
regarding this test report should be directed to the STL project manager
who signed this test report.
Ilk·. >-&zi/J~ .
,v,Ailgie Weirn~irk, Project Manager
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Final Page Of Report
STL Savannah is a part of Severn Trent Laboratories, Inc.
)i1l(l
ARCADIS GERAGHTY & MILLER Laboratory Task Order No./P.O. No. ____ _ CHAIN-OF-CUSTODY RECORD Page_·_\_ of_1_
Project Number/NamP 1'¥51'.nZ:02. """'4(;; o=:,05"": I ANALYSIS/ METHOD/ SIZE I ,,h = ·z.::. Z . <> I <! ,
Project Location OK/ke ~ <..
Laboratory S:"72. ..:X, t/o,..,.~ l.. \,:''
emJ,ct M,.,;., iJ.J:. • : ff ·, ' :-1., ' \J ,y
~',v f '<-: ::;..._
Sampler(s}/AffiliatiC:: ~rr,.;, /-7 -.:.S~ 0 ;--.:::.." 0\: ~
' Q Datemme ,. -;~ f ~t'~ Sample ID/Location Matrix Sampled Lab ID Remarks Total
CH1'1W -/o L.. ,11•.f.~ 1/Z !> ·'3 3
r<)tJ -I I '!/I•/-'~ 3 :s 1?/u
,_ (I/ I d"\....t l 1/111~ ~ I 1 .. I ,; . ., .. Ul''• ,
-
~r,,,'1-J,,,~i,_ L j-/Jt Jov ~
I
..)
'
i
Sample Matrix: L = ~id0= Solid; A= Air Total No. of Bottles/ f-0, ,,.,-, , ""'-' . Containers
Relinquished by: f / 1/ / / .. / Organization: v -~ / _.,,<rr /£-"\ ,.. ~' r~ \ Date 7 I II I~ Time I -f d.cJ · ~I Intact? ~ /, ''../ •r Organization: STL-£~ Date 't 117 1oi> Time fJ.'f'i) s No N/A Received by:'c ~ / , .
Relinquished b{ Organization: Date I I. Time Seal Intact?
Received by: Organization: Date I I Time Yes No N/A
Special lnstruct,ons/Remarks: -----------------'--------------------------------~
Delivery Method: □ In Person ---------□ Lab Courier □Other ___ ~~---
sPEc1Fv SPECIFY
---111111 -----t"~-
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RECEIVED
NOi/ 0-1 7.000
ARCADlS Geraghty & Miller
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax; 912 352 0165 • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Ral~igh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTO~092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
.Code: 155501027
Page 1
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
07009-1
07009-2
07009-3
07009-3-DL
07009-4
PARAMETER
CMMW-04
DUPLICATE
PW-1
PW-1
PW-2
07009-1 07009-2
10-11-00/11:45
10-11-00
10-11-00/15:00
10-11-00/15:00
10-11-00/15:05
07009-3 07009-3-DL 07009-4
-------------------------------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1 <50
Bromomethane (Methyl bromide), ug/1 <50
Vinyl chloride, ug/1 <50
Chloroethane, ug/1 <50
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-_l, 2-Dichloroethene, ug/1
Chloroform, ug/1
1_, 2 -Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1·
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
<250
<1200
<50
<50
<50
110
<50
<50
<50
<500
<50
<50
<50
<50
<50
<50
<50
<250
<1200
<50
<50
<50
110
<50
<50
<50
<500
<50
<50
<50
<10
<10
<10
<10
<50
<250
<10
<10
<10
170
<10
<10
<10
<100
<10
<10
<10
STL Savannah Is a part of Severn Trent Laboratories, Inc.
<100
<100
<100
<100
<500
.<2500
<100
<100
<100
150D
<100
<100
<100
<1000
<100
<100
<100
<1.0
<1.0
<1.0
<l.0
<5.0
<25
<1.0
1.6
<1.0
26
1.4
<1.0
<1.0
<10
<1.0
<1.0
<1.0
5102 LaRoche Avenue • Savann~h, GA 31404 • Tel: [phone] .• Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
.ARC.ADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
07009-1
07009-2.
07009-3
07009-3-DL
07009-4
SAMPLE DESCRIPTION
REPORT OF RESULTS
LIQUID SAMPLES
CMMW-04
DUPLICATE
PW-1
PW-1
PW-2
PARAMETER 07009-1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1 ·
1,1,2-Trichloroethane, ug/1
Benzerie, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate -Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<50
<50
<50
5500
<50
<50
<50
<50
<50
<500
<500
580
<50
<50
<50
<50
<100
94 %-
92 't
102 %-
50
Analysis Date
Batch ID
10.16.00
201016
07009-2
----------
<50
<50
<50
5600
<50
<50
<50
<50
<50
<500
<500
450
<50
<50
<50
<50
<100
94 %-
94 %-
98 %-
so
10.16.00
201016
----------
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LT0#092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 155501027
07009-3
----------
<10
<10
<10
9200E
<10
<10
<10
<10
<10
<100
<100
1400
<10
<10
<10
<10
<20
94 %-
92 %-
100 %-
10
10.16.00
201016
----------
Page 2
DATE/
TIME SAMPLED
10-11-00/11 :45
10-11-00
10-11-00/15:00
10-11-00/15: 00
10-11-00/15:05
07009-3-DL 07009-4
--------------------
<100 <l.0
<100 <l.0
<100 <l.0
13000D 84
<100 <l.0
<100 <l.0
<100 <l.0
<100 <1.0
<100 <1.0
<1000 <10
<1000 <10
1500D 190
<100 <l.0
<100 <l.0
<100 <l.0
<100 <l.0
<200 <2.0
98 %-96 %-
86 %-90 %
92 %-96 %-
100 l
10.17.00 10.17.00
101017 101017
--------------------
S'.l Savannah is a part of Severn Trent Laboratories, lnc.
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5102 LaRoche Avenue • Savannah, GA 31404 • Te!: 912 354 7858 • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTO#092900-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0l70
Sampled By: Client
Code: 155501027
REPORT OF RESULTS Page 3
·oATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
10-11-00/11 :45
10-11-00
10-11-00/15:00
10-11-00/15:00
10-11-00/15:05
07009-1 CMMW-04
07009-2 DUPLICATE
07009-3 PW-1
07009-3-DL PW-1
07009-4. PW-2
PARAMETER
Cyanide (9010)
Cyanide, Total, ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide (Amenabie) (9010)
Cyanide, Amenable, ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
07009-1 07009-2 07009-3
------------------------------
170 170 20
5 1 1
10.17.00 10.17.00 10.17.00
10.18.00 10.18.00 10.18.00
1017T 1017T 1017T
so 16 <5.0
5 1 1
10.17.00· 10.17.00 10.17.00
10.18.00 10.18.00 10.18.00
1017T 1017T 1017T
------------------------------
STL Savannah is a part of Severn Trent Laboratories, Inc.
07009-3-DL
----------
----------
07009-4
----------
20
1
10.17.00
10.18.00
1017T
<5 .0
1
10.17.00
10.18.00
1017T
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] ~ Fax: [phone] • www.stl-inc.~om STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTO#092900-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark .Radecke Project: NC000202.0170
Sampled By: Client
Code: 155501027
REPORT OF RESULTS Page 4
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
. 07009-5 PW-3
07009-5-DL PW-3
07009-6 PW-4
07009-7 INFLUENT
07009-7-DL INFLUENT
DATE/.
TIME SAMPLED
10-11-00/15:10
10-11-00/15:10
10-11-00/15:15
10-11-00/15 :20
10-11-00/15:20
PARAMETER 07009-5 07009-5-DL 07009-6 07009-7 07009-7-DL
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide) , ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<2.0
<2.0
<2.0
<2.0
<10
<50
<2 .0
<2.0
<2.0
93
<2.0
<2.0
<2.0
<20
<2.0
<2.0
<4.0
<4.0
<4. 0
<4.0
<20
<100
<4.0
<4. 0
<4.0
85D
<4. 0
<4.0
<4 .0
<40
<4.0
<4.0 ----------
<1.0
<1.0
<1.0
<1.0
<5 .0
<25
<1.0
<1.0
<1.0
5.8
<1.0
<1.0
<1.0
<10
<1.0
<1.0
----------
STL Savannah is a part of Severn Trent laboratories, Inc.
<10
<10
<10
<10
<50
<250
<10
<10
<10
83
<10
<10
<10
<100
<10
<10
----------
<40
<40
<40
<40
<200
<1000
<40
<40
<40 ·
74D
<40
<40
<40
<400
<40
<40
----------
I
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5102 laRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCJ\DIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
07009-5
07009-5-DL
07009-6
07009-7
07009-7-DL
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
PW-3
PW-3
PW-4
INFLUENT
INFLUENT
PARAMETER 07009-5 07009-5-DL
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<2.0
<2.0
<2 .0
<2.0
46
<2.0
<2.0
<2.0
<2 .o·
<2.0
<20
<20
470E
<2.0
<2 .0
<2 .0
<2.0
<4 .0
96 %
92 %
100 '1r
2
Analysis Date
Batch ID
10.17.00
'201016
<4 .0
<4.0
<4.0
<4.0
44D
<4.0
<4 .0
<4.0
<4.0
<4 .0
<40
<40
470D
<4 .0
<4.0
<4.0
<4 .0
<8.0
100 %
90 '1r
96 %
4
10.17,00
101017
LOG NO: ·so-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTO#092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 155501027
07009-6
<1.0
<1.0
<1. 0
<1.0
3.4
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
27
<1.0
<1.0
<1.0
<1.0
<2.0
96 %
88 %
,94 %
1
10.17.00
101017
Page 5
DATE/
TIME SAMPLED
10-11-00/15:10
10-11-00/15 :10
10-11-00/15:15
10,11-00/15:20
10-11-00/15 :20
07009-7 07009-7-DL
<10
<10
<10
<10'
4900E
<10
<10
<10
<10
<10
<100
<100
620
<10
<10
<10
<10
<20
94 %
88 %
96 %
10
10.17.00
201016
<40
<40
<40
<40
4700D
<40
<40
<40
<40
<40
<400
<400
560D
<40
<40
<40
<40
<80
98 %
90 %
96 " 40
10.17.00
101017
STL Savannah is a part of Severn Trent laboratories, Inc.
--·
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO
07009-5
07009-5-DL
07009-6
07009-7
07009-7-DL
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
PW-3
PW-3"
PW-4
INFLUENT
INFLUENT
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTOij092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 155501027
Page 6
DATE/
TIME SAMPLED
10-11-00/15:10
10-11-00/15:10
10-11-00/15:15
10-11-00/15:20
10-11-00/15:20
PARAMETER 07009-5 07009-5-DL 07009-6 07009-7 07009-7-DL
Cyanide (9010)
Cyanide, Total, ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
Cyanide (Amenable) (9010)
Cyanide, Amenable, ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
<5.0
1
10.17.00
10.18.00
1017T
<5.0
1
10.17.00
10.18.00
1017T
<5.0
1
10.17.00
10.18.00
1017T
<5,0
1
10.17.00
10~18.00
1017T
STL Savannah is a part of Severn Trent laboratories, Inc.
7.7
1
10.17.00
10.18.00
1017T
<5. o
1
10.17.00
10.18.00
1017T
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5102 laRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTO#092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By:·Client
Code: 155501027
Page 7
DATE/
TIME SAMPLED
07009-8 DISCHARGE 10-11-00/15:25
PARAMETER
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromoniethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
l,l;'l-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
07009-8
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<1.0
1,1,2,2-Tetrachloroethane, ug/1 <1.0
1,2-Dichloropropane, ug/1 <1.0
trans-1,3-Dichloropropene, ug/1 <1.0
Trichloroethene, ug/1 <1.0
Dibromochloromethane, ug/1 <1.0
STL Savannah is a part of Severn Trent Laboratories, Inc.
5102 LaRoche Avenue • Savannah, GA 31404 • Tel; 912 354 7858 • Fax: [phone] • www.stl-inc.com STL Savannah
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTO#092900·A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 155501027
Page 8
DATE/
TIME SAMPLED
07009·8 DISCHARGE 10·11·00/15:25
PARAMETER
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ·ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene,· ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate· 4-Bromofluorobenzene
Surrogate· Dibromofluoromethane
Dilution Factor
Analysis Date
Batch ID
Cyanide (9010)
Cyanide, Total, ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
07009·8
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2,0
96 %-
88 %-
96 %-
1
10.17.00
201016
6.8
1
10.17.00
10.18.00
1017T
STL Savannah is a part of Severn Trent Laboratories, Inc.
I
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5102 laRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LT0#092900-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel ·Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 155501027
REPORT OF RESULTS Page 9
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
07009-8 . DISCHARGE 10-11-.00/15:25
----------------------------------~-------------------------------------------------
PARAMETER
Cyanide (Amenable) (9010)
Cyanide, Amenable, ug/1
Dilution Factor
Prep Date
Analysis Date
Batch ID
07009-8.
<5.0
1
10.17.00
10.18.00
1017T
STL Savannah is a part of Severn Trent Laboratories, Inc.
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl•inC.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
LOG NO
07009-9
07009-10
07009-11
07009-12
07009-13.
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
TRIP BLANK 10/09/00
TRIP BLANK 10/10/00
TRIP BLANK 10/11/00
CMMW-24
CMMW-23
LOG NO: S0-07009
Received: 12 OCT 00
Reported·: 26 OCT 00
Client PO. No.: LTO#092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0l70
Sampled By: Client
Code: 155501027
Page 10
DATE/
TIME SAMPLED
10-09-00
10-10-00
10-11-00
10-11-00/13 :20
10-09-00/12:15
PARAMETER 07009-9 07009-10 07009-11 07009-12 07009-13
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide) , ug/1
Vinyi chloride, ug/1
Chloroethane, ug/1
Methyl~ne chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
l,l-Dichloroethene, ug/1
l,l-Dichloroethane, ug/1
cis-l,2-Dichloroethene, -ug/1
trans-l,2-Dichloroethene, ug/1
Chloroform, ug/1
l,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
l,l,l·Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<1.0
<1.0
<l.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<l.0
<l.0
<1.0
<1.0
<10
<l.0
<l.0
<1.0
<1.0
<1.0
<l.0
<5.0
<25
<1.0
<1.0
<l.0
<1.0
<l.0
<l.0
<l.0
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
STL Savannah is a part of.Severn Trent laboratories, Inc.
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<l.0
<1.0
<1.0
<l.0
<l.0
<10
<1.0
<l.0
<1.0
<1.0
<l.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
69
<1.0
<1.0
<l.0
<10
<1.0
<1.0
I
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
Mr, Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LT0#092900-A
Raleigh, NC 27612 Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 155501027
REPORT OF RESULTS Page 11
DATE/
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES TIME SAMPLED
07009-9
07009-10
07009-11
07009-12
07009-13
TRIP BLANK 10/09/00
. TRIP BLANK 10/10/00
TRIP BLANK 10/11/00
CMMW-24
CMMW-23
PARAMETER 07009-9
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/1
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
Trichloroethene, ug/1
Dibromochl~romethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ugil
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<10
<1.0
<1.0
<1.0
<1.0
<1.0
<2.0
96 %-
88 %-
98 ·"
1
Analysis Date
Batch ID
10.17.00
201016
07009-10 07009-11
--------------------
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<i'.o <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<10 <10
<10 <10
<1.0 <1.0
. <1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<2 .. 0 <2.0
94 %-96 'Ir
96 %-90 %-
96 %-96 %-
1 1
10.17.00 10.17.00
201016 201016
--------------------
STL Savannah is a part of Severn Trent Laboratories, Inc.
10-09-00
1·0-10-00
10-11-00
10-11-00/13 :20
10-09-00/12:15
07009-12 07009-13
--------------------
<1.0 <l.O
<1.0 <1.0
<1.0 <1.0
<l.O <1.0
<1.0 38
<1.0 <1.0
<l.O <l.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<10 <10
<10 <10
<1.0 270E
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<2 .0 <2.0
96 " 98 " 92 %-88 " 96 %-96 ..
1 1
10.17.00 10.17.00
201016 201016
--------------------
5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.st!-inc.com STL Savannah
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LTOi092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 155501027
Page 12
DATE/
TIME SAMPLED
07009-13-D CMMW-23 10-09-00/12:15
07009-14 CMMW-22A 10-09-00/14:45
07009-15 CMMW-21 10-09-00/14:50
07009-16 CMMW-20 10-l0'00/16:00
07009-17 . CMMW-19 10-10-00/10 :20
PARAMETER 07009-13-DL 07009-14 07009-15 07009-16 07009'17
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide) , ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1.
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<2.0
<2.0
<2.0
<2.0
<10
<50
<2.0
<2.0
<2 .o
68D
<2.0
<2.0
<2 .0
<20
<2.0
<2.0
<1.0
<1.0
<1.0
<1.0
<5 .0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<10
<1.0
<1.0
<5.0 <10
<5.0 <10
<5. 0 <10
<5 .0 <10
<25 <50
<120 <250
<5. 0 <10
<5.0 32
<5. 0 <10
290 27
<5.0 <10
<5. 0 <10
<5. 0 <10
<50. <100
<5.0 <10
<5.0 <10
STL Savannah Js a part of Severn Trent Laboratories, Inc.
<1.0
<1.0
<1.0
<1.0
<5.0
<25
<1.0
<1.0
<1.0
<1.0
<1.0
<l.0
<1.0
<10
<l.0
<1.0
I
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5102 LaRoche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax; 912 352 0165 • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client ·Po. No.: LT0#092900-A
Raleigh, NC 27612 , Requisition: SQ00-0265
Contract No.: JFD Channel Master
CC: Mr. Mark Radecke Project: NC000202.0170
Sampled By: Client
Code: 155501027
REPORT OF RESULTS Page 13
LOG NO SAMPLE DESCRIPTION, LIQUID SAMPLES
07009-13-D CMMW-23
07009-14 CMMW-22A
07009-15 CMMW-21
07009-16 CMMW-20
07009-17 CMMW-19
PARAMETER 07009-13-DL
----------------------------------------
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane,
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene,
Trichloroethene, ug/1
Dibromochloromethane, ug/1
1,1,2-Trichloroethane, ug/1
Benzene, ug/1
cis-1,3-Dichloropropene, ug/1
Bromoform, ug/1
ug/1
ug/1
2-Hexanone, ug/1
4-Methyl-2-pentanone (MIBK), ug/1
Tetrachloroethene, ug/1
Toluene, ug/1
Chlorobenzene, ug/1
Ethylbenzene, ug/1
Styrene, ug/1
Xylenes, Total, ug/1
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
Dilution Factor
<2.0
<2.0
<2.0
<2.0
37D
<2.0
<2.0
<2.0
<2.0
<2.0
<20
<20
280D
<2.0
<2.0
<2.0
<2.0
<4 .0
98 %-
86 %-
92 %-
2
Analysis Date 10.17.00
Batch ID 101017
07009-14
----------
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<l.0
<1.0
<10
<10
<1.0
<l.0
<1.0
<1.0
<l.0
<2.0
96 't
88 %-
96 %-
1
10.17.00
201016 ----------
07009-15
----------
<5.0
<5.0
<5.0
<5.0
110
<5.0
<5.0
<5.0
<5.0
<5.0
<50
<50
660
<5.0
<5.0
<5.0
<5.0
<10
94 %-
88 %-
92 %-
5
10.17.00
201016
----------
STL Savannah is a part of Severn Trent laboratories, Inc.
DATE/
TIME SAMPLED
10-09-00/12:15
10-09-00/14:45
10-09-00/14:50
10-10-00/16:00
10-10-00/10:20
07009-16 07009-17 --------------------
<10 <1.0
<10 <1.0
<10 <l.0
<10 <1.0
56 8.7
<10· <1.0
<10 <1.0
<10 <1.0
<10 <1.0
<10 <1.0
<100 <10
<100 <10
1000 31
<10 <1.0.
<10 <1.0
<10 <1.0
<10 <1.0
<20 <2.0
96 %-96 %-
86 %-88 %-
98 %-98 %-
10 l
10.17.00 10.17.00
201016 201016
5102 LaRoche Avenue • Savannah, GA 31404 •. Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
LOG NO
07009-18
07009-19
07009-20
07009-21
07009-22
Mr. Nanj un She tty·
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
CMMW-26
CMMW-17
CMMW-05
CMMW-10
CMMW-07
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LT0#092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0l70
Sampled By: Client
Code: 155501027
Page 14
DATE/
TIME SAMPLED
10-10-00/11:40
10-10-00/14:25
10-10-00/15:05
10-10-00/15:00
10-10-00/17:00
PARAMETER 07009-18 07009-19 07009-20 07009-21 07009-22
-----------------------------------------------------------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl
bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride
(Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
l,l-Dichloroethene, ug/1
l,l-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
<l.0
<l.0
<l.0
<l.0
<5.0
<25
<l.O
<l.0
<l.O
17
<l.0
<l.0
<l.0
<10
<l.0
<l.0
<l.0
<l.0
<l.0
<l.0
<5.0
<25
<l.0
<l.0
<l.0
39
<l.0
<l.O
<l.0
<10
<l.O
<l.0
<1000
<1000
<1000
<1000
<5000
<25000
<1000
<1000
<1000
<1000
<1000
<1000
<1000
<10000
<1000
<1000
STL ~avannah is a part of Severn Trent Laboratories, Inc.
<1000
<1000
<1000
<1000
<5000
<25000
<1000
<1000
<1000
98000
<1000
<1000
<1000
<10000
<1000
<1000
<2 .0
<2.0
<2.0
<2.0
<10
<50
<2 .0
<2.0
<2.0
51
<2.0
<2.0
<2.0
<20
<2.0
<2.0
I
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5102 LaRoche Avenue • Savannah, GA 31404 • Te!: 912 354 7858 • Fax: [phone] • www.stl-inc.com STL Savannah
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P .0. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
LOG NO
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
07009-18 CMMW-26
07009-19 CMMW-17
07009-20 CMMW-05
07009-21 CMMW-10
07009-22 CMMW-07
PARAMETER 07009-18
Bromodichloromethane, ug/l <l.0
1,1,2,2-Tetrachloroethane, ug/l <l.O
1,2-Dichloropropane, ug/l <1.0
trans-1,3-Dichloropropene, ug/l
Trichloroethene, ug/l
Dibromochloromethane, ug/l
1,1,2-Trichloroethane, ug/l
Benzene, ug/l
cis-1,3-Dichloropropene, ug/l
Bromoform, ug/l
2-Hexanone, ug/l
4-Methyl-2-pentanone (MIBK), ug/l
Tetrachloroethene, ug/l
Toluene, ug/l
Chlorobenzene, ug/l
Ethylbenzene, ug/l
Styrene, ug/l
Xylenes, Total, ug/l
Surrogate Toluene-dB
Surrogate -4-Bromofluorobenzene
Surrogate -Dibromofluoromethane
<l.O
3.1
<l.0
<1.0
<1.0
<l.0
<1.0
<10
<10
36
<l.O
<l.O
<l .O
<l.O
<2. 0
96 %-
88 %-
92 %-
1 Dilution.Factor
Analysis Date
Batch ID
10.17.00
201016
07009-19
----------
<l.0
<l.O
<l.0
<l.0
24
<l.0
<l.0
<l.0
<l.0
<l.O
<10
<10
4.2
<l.0
<l.0
<l.0
<l.0
<2.0
96 %-
94 'Ir
94 %-
l
10.17.00
201016
----------
LOG NO: S0-07009
Received: 12 OCT 00
Reported: 26 OCT 00
Client PO. No.: LT0#092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0l70
Sampled By: Cli_ent
Code: 155501027
07009-20 ----------
<1000
<1000
<1000
<1000
200000
<1000
<1000
<1000
<1000
<1000
<10000
<10000
15000
<1000
<1000
<1000
<1000
<2000
96 'Ir
86 %-
96 %-
1000
10.17.00
201016 ----------
Page 15
DATE/
TIME SAMPLED
10-10-00/11:40
10-10-00/14:25
10-10-00/15:05
10-10-00/15:00
10-10-00/17:00
07009-21 07009-22
--------------------
<1000 . <2 .0
<1000 <2.0
<1000 <2 .0
<1000 <2.0
42000 260
<1000 <2 .0
<1000 <2 .0
<1000 <2.0
<1000 <2.0
<1000 .<2 .0
<10000 <20
<10000 <20
2000 30
<1000 <2.0
<1000 <2.0
<1000 <2.0
<1000 <2.0
<2000 <4.0
96 %-98 'Ir
88 %-88 'Ir
94 %-96 %-
1000 2
10.17.00 10.17.00
101017 101017
--------------------
STL Savannah is a pa~ of Severn Trent laboratories, Inc.
\
5102 laR.oche Avenue • Savannah, GA 31404 • Tel: [phone] • Fax: [phone] • www.stl-inc.com STL Savannah
I
I
LOG NO: S0-07009
Received: 12 OCT 00 1·
Reported: 26 OCT 00
LOG NO
Mr. Nanjun Shetty
ARCADIS Geraghty & Miller, Inc.
P.O. Box 31388
Raleigh, NC 27612
CC: Mr. Mark Radecke
REPORT OF RESULTS
SAMPLE DESCRIPTION, LIQUID SAMPLES
Client PO. No.: LTO#092900-A
Requisition: SQ00-0265
Contract No.: JFD Channel Master
Project: NC000202.0170
Sampled By: Client
Code: 155501027
Page 16
DATE/
TIME SAMPLED
----------------------------- --------------------------------
07009-23 CMMW-15
· 07009-24 EQUIPMENT BLANK
07009-25 FIELD BLANK
PARAMETER 07009-23
10-11-00/11:15
10-10-00/17:40
10-10-00/16:00
07009-24 07009-25
------------------------------------------------- ---------- ---------- ----------
Volatiles by GC/MS (8260)
Chloromethane, ug/1
Bromomethane (Methyl bromide), ug/1
Vinyl chloride, ug/1
Chloroethane, ug/1
Methylene chloride (Dichloromethane), ug/1
Acetone, ug/1
Carbon disulfide, ug/1
·. 1,1-Dichloroethene, ug/1
1,1-Dichloroethane, ug/1
cis-1,2-Dichloroethene, ug/1
trans-1,2-Dichloroethene, ug/1
Chloroform, ug/1
1,2-Dichloroethane, ug/1
2-Butanone (MEK), ug/1
1,1,1-Trichloroethane, ug/1
Carbon tetrachloride, ug/1
Bromodichloromethane, ug/1
1,1,2,2-Tetrachloroethane, ug/i
1,2-Dichloropropane, ug/1
trans-1,3-Dichloropropene, ug/1
<2.5
<2.5
<2.5
<2.5
<12
<62
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5
<25
<2.5
<2.5
<2.5
<2.5
<2.5
<2.5 ----------
STL Savannah Is a part of Severn Trent Laboratories, Inc.
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<5.0 <5.0
<25 <25
<1.0 <1.0
<1.0 <1.0
<l.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1 .. 0 <1.0
<1.0 <1.0
<10 <10
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0
<1.0 <1.0 --------------------
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ARCADIS GERAGHTY&MILLER
Semiannual
Groundwater
Remediation Report
Appendix 8
Construction Document
for Well CMMW22A
I
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1:
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01-15-2001 09:32AM PARRATTWOLFF HILLSBOROUGH [phone]
North Carolina • Oepar1:ment of Environment and Natura.I Resource$ -Division or Watll!r Quality• Groundwa1er Section
1636 Mail Service Centet • Raleigh. N.C. 27699-1636-Phona [phone]
WELL CONTRACTOR: PARRA TT-WOLFF, INC.
P.02
WELL CONSTRUCTION RECORD
MW22A WELLCONIRACTOR CERTIFICATION#: 2973/K, WHITE
STATE WELL CONSTRUCTION PERMIT#:
1. WELL USE (Chock Applicable aox): Residential D
Recovery O Hea• Purnp Waler lnjeclion 0 Municipal D lndustrtal 0
Other O II Other, list_Use:
Agricultural D Monitoring K»
2. WELL LOCATION: (Show sketch of the localion below)
Nea,eSI Town: OXFORD County: _......;G:cR=Ac:.N:..;Vc.;I:.;L::;L=E'-------
PINE TREE ROAD
(Flo.ad Name Md Numtien;, Community, or Subdivl&ion andJ.DI No.) DRILLING LOG DEPTH
3. OWNER JFD ELECTRONICS/CHANNEL MASTER From To Formation Doset'lption
Address PINE TREE ROAD
(Street or Roule No.) OXFORD NC 27565
City or Town Stare Zip Coao
4. DATE DRIL.L.EO 7 /18/00 NO S ~MPJ. T"'-"'----------
S. TOTAL DEPTH 25, 0'
6, · CUTTINGS COLLECTED YES(!] NO□
7. DOES WEL.L REPLACE EXISTING WELL? YES [!) NO□
8, STATIC WATER LEVEL. Below Top of Casing: 13. 0 FT.
(Use••· U AOOve Top OI CaoinQ)
9. TOP OF CASING IS 3. 0 FT. Above Land Surface•
"'Top of cuing totmlnated at/or below l.ltf\d surfac• nqulrH • vartar1ee In accor----------
danco with 15A NCAC 2C .0118
10. YIEL.D (gpm): __ METHOD OF TEST ______________ _
11. WATER ZONES (depth): ____________________ _
12. CHL.ORINATION: Type ------Amount ___ _ II &ddltlol'\af apace Is needed use back of lorm
13. CASING: -==---------==-==
Depth Diameter.
From--'□"--TO --1.2..._ Ft. 2"
Wall Thlel<nes,
or Waight/Ft,
SCH40 Material
'PVC
From To---Ft.---
From To---Fl.---
14. GROUT:
Depth Material
. From __ o_ To ...2..:2...Ft. PORTLAND
From __lL_2_ To ....!LFt. BENTONITE
1S.' SCREEN:
Method
TREMIE
TREMIE
Depth Diameter Slol Size Material
From --l2_ To --1..2... Ft _2_ In. ...:..2l.9In, PVC
From __ To __ Ft. __ In. __ In. ___ _
From __ To __ Ft. __ In, __ In. ___ _
16. SANO/GRAVEL PACK:
Depth
From 13 · To 25
Size Material
Ft . .....:,#"'l.___ _....,S-..A,_.N~D::.._ __
From ___ To ___ Ft. ___ _
LOCATION SKETCH
(ShoW direction and distance 1,001 at least two S1ate
Roads, or other map reference points) ,
'f\'1.-".
'f...
17. REMARKS: __________________________________ _
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE Wl'Tl-i 1SA NCAC 2C, WEL.L.
CONSTRUCTION ST AN DAROS, ANO THAT A COPY. OF THIS RECORD AS BEEN PROVIDED TO THE WELL OWNER.
FOR OFFICE use ONLY
O\Jad No:
Serial No,
I I;/ di
SIGNATURE OF PERSON CONSTAUCTJNQ THE WELl DATE
5'.tbml orlgfnaJ to Oivf.SOn 01 W1tor Quality. Orol.ll'\dwatot S6¢tion wllhln 30 days
GW-1 REV, 12199
TOTAL P.02