NCD003200383_20020523_Koppers Co. Inc._FRBCERCLA RA_First Quarter 2002 Groundwater Monitoring Report-OCR

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May 23, 2002
Ms. Beverly Hudson
Remedial Project Manager
USEPA-Region IV
North Superfund Remedial Branch
Waste Management Division
100 Alabama Street
Atlanta, Georgia 30303
RE: First Quarter 2002 Groundwater Monitoring Report for the
Former Koppers Company Site, Morrisville, North Carolina
RETEC Project No.: BEAZ?-03624-103
Dear Ms. Hudson:
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The RETEC Group. Inc.
1822 E. NC Highway 54, Suite 100
Durtiam, NC 27713
[phone] Phone
[phone] fa,
www.retec.com
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MAY 2 4 2002
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'~ The RETEC Group, Inc. (RETEC), on behalf of Beazer East, Inc. (Beazer), hereby submits the
results of the first quarter 2002 groundwater monitoring event at the former Koppers Company Site
in Morrisville, North Carolina (Site). This report documents the field and laboratory results of the
groundwater monitoring event performed on February 18 and 19, 2002.
Groundwater Monitoring Program-First Quarter 2002
Based on Proposed Remedial Action Groundwater Monitoring Program requirements, the first
quarter 2002 monitoring event included the:
• Gauging of 50 monitoring wells (Figure 1 ): 35 on-site wells and 15 off-site wells
• Sampling of thirteen on-site wells: C-09B, C-I0A, C-1013, C-1 IB, C-12A, C-13B, C-
l4B, C-15B, C-27A, C-2713, C-28A, C-2913, and PW-01
RETEC found that wells C-01 B and M-04A (usually included in the program) were dry and could
not be sampled. In addition, although well C-l4A is usually included in the groundwater sampling
program, RETEC found that the volume of water present in this well was not sufficient to generate a
sample.
Groundwater Elevation and Direction of Flow
Groundwater elevations for the A-, B-, and C-zone wells, as measured on February 18, 2002, are
presented in Table I. Between 2000 and 2002, a temporary building was placed over well C-1 IA,
and RETEC was unable to gauge the well. However, this temporary building was recently removed
and (as shown on Table I and Figure 2) RETEC gauged the well during this sampling event.
Also during this first quarter sampling event, the depth to groundwater in well C-0 I B exceeded 100
feet. Since the water-gauging meter tape purchased for this project was l00 feet long, the depth to
water in this well was not measured. Should future measurements indicate that the depth to water in
this well continues to exceed l00 feet, RETEC will provide a water-gauging meter with a 150-foot
tape.
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Ms. Beverly Hudson
May 23, 2002
Page 2
Please note, however, that well C-01B and well C-I0B have historically had widely divergent
groundwater elevations compared to adjacent B-zone wells. These two wells are 35 to 95 feet deeper
than the deepest B-zone well. The intervals screened and the historic groundwater elevations
measured in these wells indicate that they are monitoring a zone that does not communicate with the
rest of the B-zone wells. Due to this lack of communication, well C-0IB and well C-I0B will
continue to be gauged, but will not be included in the dataset used to determine the potentiometric
surface for the B-zone (Figure 3).
The groundwater elevations presented in Table I were used to construct the A-B-and C-zone
groundwater potentiometric surface maps shown in Figures 2 through 4. Figures 2 and 3 show the
cone of depression that exists around the pumping well (PW-I) and indicate that, outside of the zone
of influence, groundwater flow is generally to the northeast and south-southwest. The high
variability in the C-zone groundwater elevations indicates that these wells are screened in isolated
fracture zones within the bedrock, as seen on Figure 4.
Phenolic Analytical Results
Each groundwater sample was analyzed for pentachlorophenol and 2,4-dichlorophenol using the
United States Environmental Protection Agency (USEPA) Method 8270C-Select Ion Monitoring.
RETEC personnel validated the groundwater analytical results and applied the necessary data
qualifiers, as summarized in Table 2. We also provide a complete copy of the laboratory analytical
results in Appendix A.
The record of decision for this Site requires that groundwater meet the following cleanup standards:
• I (microgram per liter) µg/L for pentachlorophenol
• 20 µg/L for 2,4-dichlorophenol
As shown in Table 2, pentachlorophenol was detected in groundwater sampled from wells C-29B and
PW-01. Both of these pentachlorophenol detections exceed the pentachlorophenol cleanup standard
of I µg/L; however, 2,4-dichlorophenol was not detected in any of the samples analyzed during this
event.
In accordance with the USEPA-approved Groundwater Monitoring Program, RETEC will continue
to collect quarterly samples from all wells with pentachlorophenol and/or 2,4-dichlorophenol results
above the specified cleanup levels. This sampling will continue until the concentrations of
pentachlorophenol and 2,4-dichlorophenol meet the cleanup levels for four consecutive sampling
events.
Since pentachlorophenol was detected in groundwater sampled from C-29B and PW-01, these wells
will be sampled as part of the second quarter monitoring event.
Pentachlorophenol was not detected in well C-14B for the third consecutive quarter. Well C-14B
will be sampled in the second quarter and will continue to be sampled until there are four consecutive
quarters with results reported below the specified cleanup levels.
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Ms. Beverly Hudson
May 23, 2002
Page 3
Also during the second quarter of 2002, RETEC will attempt to sample well C-14A. Although this
well is on the quarterly sampling schedule, it was dry, and RETEC was unable to sample it during the
last two monitoring events.
Dioxin and Furan Analytical Results
Dioxin and furan sampling occurs on a semiannual basis (in a subset of wells) and will occur during
the second and fourth quarters of 2002. RETEC will collect dioxin and furan samples from wells
that have concentrations of pentachlorophenol at or above the specified cleanup levels during the
previous sampling event, or wells with two or more quarterly pentachlorophenol detections in the
previous four quarters. Therefore, the next dioxin and furan sampling event (second quarter 2002)
will include wells C-l4A, C-29B, and PW-01.
Operational Summary
The groundwater extraction system is currently pumping at its optimum. The aquifer's low yield will
not support a pumping rate greater than 2 gallons per minute, nor will the low yield of the aquifer
support the "pulsing" of the system.
Quarterly review of the groundwater analytical results indicates that the concentrations of
constituents of interest are neither increasing nor decreasing in groundwater collected from the three
remaining wells with groundwater impact. Monitoring will continue in order to determine if and
when the levels of impact begin to decrease.
If you have any questions regarding these results, please call Michael Helbling of Beazer at (412)
208-8867 or Rita Bauer at [phone].
Sincerely,
RETEC North Carolina, Inc.
~o-D-~~
Stefanie D. Young U 0
Environmental Scientist
Enclosures
RETEC North Carolina, Inc.
Rita M. Bauer
Groundwater Sampling Program Manager
cc: D. Mattison-North Carolina Department of Natural Resources
M. Helbling-Beazer East, Inc.
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BEAZER EAST, INC.
BEAZ?-03624-103
OAT(: 5/7 /02 ORWN: P.0./UKN FILE: 3624CHC2
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LEGEND:
MONITORING WELL
RAILROAD TRACKS
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EAST, INC.
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SITE MAP
FORMER KOPPERS COMPANY
MORRISVILLE, NORTH CAROLINA
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BEAZER EAST, INC.
BEAZ?--03624-103
OAT£: 5/23/02 ORWN: P .0./0UR FILE: J624CHOI
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LEGEND:
.... MONITORING WELL
GROUNDWATER CONTOUR
368.53 GROUNDWATER ELEVATION
AT WELL (FEET MSL)
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A-ZONE GROUNDWATER CONTOURS
FEBRUARY 18, 2002
FORMER KOPPERS COMPANY
MORRISVILLE, NORTH CAROLINA "''°"'' C-ZONE FIGURE: 2
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GROUNDWATER MONITORING PROGRAM
BEAZER EAST, INC.
BEAV-03624-103
DATE: 5/7 /02 ORWN: P .0./0UR fllE: 3624CH04
/
LEGEND:
MONITORING WELL
GROUNDWATER CONTOUR
353.73 GROUNDWATER ELEVATION
AT WELL (FEET MSL)
NM NOT MEASURED
NOTE:
WELLS C-018 AND C-10B NOT USED IN CONTOURING.
Q
200 0 400
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SCALE: 1 "=400'
B-ZONE GROUNDWATER CONTOURS
FEBRUARY 18, 2002
FORMER KOPPERS COMPANY MORRISVILLE, NORTH CAROLINA
LAYOUT, B-ZONE. FIGURE: 3
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BEAZER EAST, INC.
BEAZ?-03624-103
04TE: '!,/7 /02 ORWN: P .0./DUR Fll[: 3624CH03
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LEGEND:
• MONITORING WELL
INFERRED GROUNDWATER CONTOUR
353.73 GROUNDWATER ELEVATION
AT WELL (FEET MSL)
NM NOT MEASURED
c 22'
200 0
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SCALE: 1 "=400'
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400
C.ZONE GROUNDWATER CONTOURS
FEBRUARY 18, 2002
FORMER KOPPERS COMPANY
MORRISVILLE, NORTH CAROLINA
LAYOUT: C-ZONE FIGURE: 4
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Tables
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Table 1 Groundwater Elevations
First Quarter 2002
Well ID Gauging Date
C-01A 16-Feb--02
C-02A 16-Feb-02
C-03A 16-Feb--02
C-04A 16-Feb-02
C-05A 16-Feb-02
C-06A 16-Feb--02
C-07A 16-Feb-02
C-OBA 16-Feb--02
C-OSA 16-Feb-02
C-10A 16-Feb-02
C-11A 16-Feb-02
C-12A 16-Feb-02
C-13A 16-Feb--02
C-14A 16-Feb-02
C-15A 16-Feb-02
C-25A 16-Feb-02
C-26A 16-Feb-02
C-27A 16-Feb-02
C-28A 16-Feb--02
C-30A 16-Feb-02
C-31A 16-Feb-02
C-33A 16-Feb-02
M-04 16-Feb-02
C-018 16-Feb-02
C-028 16-Feb-02
C-038 16-Feb-02
C-098 16-Feb-02
C-108 16-Feb-02
C-118 16-Feb-02
C-128 16-Feb--02
C-138 16-Feb--02
C-148 16-Feb-02
C-158 16-Feb-02
C-258 16-Feb-02
C-268 16-Feb-02
C-278 16-Feb-02
C-288 16-Feb-02
C-298 16-Feb-02
C-338 16-Feb-02
C-348 16-Feb-02
C-09C 16-Feb-02
C-12C 16-Feb-02
C-16C 16-Feb-02
C-19C 16-Feb-02
C-20C 16-Feb-02
C-21C 16-Feb-02
C-22C 16-Feb-02
C-32C 16-Feb-02
C-33C 16-Feb-02
C-34C 16-Feb-02
Notes:
ms! -mean sea level
NM -Not measured
Top of Casing
Elevation
(feet msl)
383.06
380.76
380.21
385.31
386.59
383.90
374.30
376.34
372.98
373.88
363.28
375.00
367.31
371.13
357.08
365.52
382.12
372.10
372.40
379.11
379.98
354.37
368.83
383.35
381.72
380.69
374.76
373.58
363.28
375.75
367.02
371.66
357.62
364.85
382.21
372.01
373.07
369.00
352.84
376.31
374.34
376.11
368.37
365.84
378.17
361.04
355.24
368.88
353.54
376.39
Depth to Groundwater
Groundwater Elevation
(feet) (feet msl)
25.88 357.18
26.80 353.96
21.12 359.09
19.81 365.50
19.95 366.64
16.41 367.49
10.85 363.45
32.47 343.87
14.09 358.89
19.82 354.06
10.84 352.44
17.73 357.27
11.44 355.87
29.40 341.73
3.97 353.11
21.03 344.49
Orv On,
21.68 350.42
13.96 358.44
· 27.18 351.93
23.57 356.41
9.21 345.16
Orv Orv
>100• NM
12.03 369.69
24.98 355.71
20.54 354.22
73.78 299.80
11.90 351.38
17.27 358.48
7.55 359.47
28.86 342.80
3.12 354.50
20.91 343.94
33.11 349.10
37.10 334.91
10.50 362.57
37.27 331.73
7.60 345.24
17.68 358.63
14.61 359.73
81.34 294.77
17.38 350.99
12.70 353.14
28.97 349.20
31.33 329.71
4.98 350.26
. 28.58 340.30
14.95 338.59
18.34 358.05
Water elevations >100 feet were not measured due to gauging meter being 100 feet
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Table 2 Groundwater Sampling Analytical Results
First Quarter 2002
Cleanup
Parameter Units Standard C-098
2/18/02
2,4-0ichloroohenol "n/L 20 0.2 U
Pentachloroohenol ua/L I 1 U
Cleanup Parameter Units C-27A Standard 2/19/02
2,4-Dichloroohenol ua/L 20 0.2 U
Pentachloroohenol ua/L I 1 U
Notes:
Bold font indicates exceedance of cleanup standard
U indicates compound was analyzed for, but not detected.
J indicates an estimate result.
C-10A
2/18/02
0.2 U
1 U
C-278
2/19/02
0.2 U
1 U
D Indicates that the result was taken from the analysis of a secondary dilution.
Sample Location
C-108 C-118 C-12A C-138 C-148
2/18/02 2/18/02 2/19/02 2/18/02 2/19/02
0.2 U 0.2 U 0.2 U 0.2 U 0.23 U
1 U 1 U 1 U 1 U 1.2 U
Sample Location
C-28A C-298 PW-01 PW-01 OUP EB-01
2/19/02 2/19/02 2/18/02 2/19/02 2/19/02
0.2 U 2 U 0.2 U 0.2 U 0.22 U
1 U 27 4.2 D 7.6 1.1 U
-

-

-
C-158
2/18/02
0.2 U
1 U
FB-01
2/18/02
0.2 U
1 U
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Appendix A
First Quarter 2002 Analytical Results
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Draft Data Evaluation Report
Site: Beazer/Raleigh
Program/Event: CERCLA Groundwater Monitoring/ Q1-02
Laboratory: Severn Trent Laboratories, Inc. -Pittsburgh
Laboratory Project Number: C2B200218
Analyses: Pentachlorophenol and 2,4-Dichlorophenol by SW-
846 method 8270C SIM
Evaluator: Gretchen A. Phipps
Date: March 5, 2002
The Raleigh Q 1-02 data report from Severn Trent Laboratories, Inc. -Pittsburgh was
evaluated using USEPA National Functional Guidelines and USEPA method
specifications. Each issue requiring comment and/or data qualification is addressed
below. All results were accepted without qualification.
II
Sample Collection, Receipt, and Log-In
1.
2.
Sample Collection: Wells C-OIB, C-14A, and M-04 were dry. Samples
could not be collected for these wells.
Sample Receipt: Samples were received by the laboratory in good
condition and within the optimal temperature range of 2-6° C.
Pentachlorophenol and 2,4-Dichlorophenol by SW-846 method
8270C SIM
Dilutions/Reporting Limits: Sample C-29B was analyzed at a I 0-fold dilution due
to the high concentration ofpentachlorophenol. This caused the reporting limit
of 2,4-dichlorophenol to be elevated.
Sample PW-01 was analyzed at a secondary two-fold dilution because
pentachlorophenol exceeded the calibration range of the instrnment. For this
reason, the pentachlorophenol result from the original analyses was qualified "E"
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Beazer/Raleigh
Ql-02
Client Work Product
Private and Co,~{idential
Ill
by the laboratory. The pentachlorophenol result from the secondary dilution was
acceptable and must be used.
Due to insufficient sample volume, sample C-14B and the equipment blank (EB)
were extracted using smaller sample aliquots. This caused the reporting limits to
be slightly elevated. There were no positive hits (no signal) between the required
method detection and the elevated reporting limits.
Field Duplicate Samples
Samples PW-01 and DUPO! were the primary and field duplicate samples
collected for this round. All positive results are presented in the table below. No
data qualifications are required based on the relative percent difference (¾RPD)
of field duplicate sample data. However, the results are presented in the table
below to evaluate precision and sample homogeneity. A ¾RPD greater than the
advisory limit of 50% is an indication of sample heterogeneity with respect to
that compound, poor field precision and/or poor laboratory precision.
Beazer/ Raleigh
Q1 -02 Field Duplicate Comparison
Parameter PW-01 DUP01 RPD (%)
Pentachloro□henol 4.2 ,on/L 7.6 ua/L 57
Attachments:
Qualifications Summary
F:BEAZ7-03 624/DataEva/Report _ 2002/RA _QI -02 2
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Sample
C-10A
C-10A
C-10B
C-10B
C-13B
C-13B
C-29B
C-29B
C-28A
C-28A
C-14B
C-14B
C-27A
C-27A
C-12A
C-12A
C-27B
C-27B
EB
EB
OUP01
OUP01
C-09B
C-09B
C-15B
C-15B
PW-01 --PW-01
FB
FB
C-11B
C-11B
Analyte
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-OICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-OICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
2,4-OICHLOROPHENOL
2,l QIGMbGRGPMENGb
PENTAGMbOROPME~IOb
PENTACHLOROPHENOL
2,4-OICHLOROPHENOL
PENTACHLOROPHENOL
2,4-DICHLOROPHENOL
PENTACHLOROPHENOL
Qualifications Summary
Beazer, Raleigh
Q1-02
Result Units Lab Qualifier
0.2 UG/L u
1 UGIL u
0.2 UG/L u
1 UG/L u
0.2 UG/L u
1 UG/L u
2 UG/L u
27 UG/L
0.2 UG/L u
1 UGIL u
0.23 UG/L u
1.2 UG/L u
0.2 UG/L u
1 UG/L u
0.2 UGIL u
1 UGIL u
0.2 UG/L u
1 UGIL u
0.22 UG/L u
1.1 UG/L u
0.2 UGIL u
7.6 UG/L
0.2 UG/L u
1 UGIL u
0.2 UGIL u
1 UG/L u
0.2 UGIL u
(h4 YGlb y
44 YGlb I,
4.2 UGIL
0.2 UGIL u
1 UG/L u
0.2 UGIL u
1 UGIL u
Validation Detection
Qualifier Limit Dilution
0.2 1
1 1
0.2 1
1 1
0.2 1
1 1
2 10
10 10
0.2 1
1 1
0.23 1
1.2 1
0.2 1
1 1
0.2 1
1 1
0.2 1
1 1
0.22 1
1.1 1
0.2 1
1 1
0.2 1
1 1
0.2 1
1 1
0.2 1
(h4 2
4 4
2 2
0.2 1
1 1
0.2 1
1 1
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ANALYTICAL REPORT
PROJECl' NO. BEAZER
Raleigh, Morrisville
Lot ff, C2B200218
Gregory Malzone
ThermoRetec Corporation
SEVERN TRENT LABORATORIES, INC.
~~,t-
Veronica Bertot
Project Manager
February 27, 2002
STL P1t1sburgl1 1s ;1 part of Sf~Vern lre11\ Laboratorie:;, Inc.
SE V E:R N
SERVICES
I
STL Pittsburgh
450 William Pit1 Way
flittsburgh, PA 15238-1330
Tel: [phone]
fax 4 I 2 820 2080
www.stl-inc.com
Sample Receiving:
CASE NARRATIVE
THE RETEC GROUP
Raleigh, Morrisville
STL Lot # C2B2002 I 8
STL Pittsburgh, PA received samples on February 20, 2002 in good condition. The
cooler was within the proper temperature range.
GC/MS Semivolatiles SIM:
Due to the concentration ofpentachlorophenol detected, sample PW-01 was analyzed
undiluted and at a 2X dilution. Both sets of results are reported.
Samples C-l 4B and EB had the reporting levels elevated due to the insufficient amount
of sample provided for extraction.
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METHODS SUMMARY
C2B200218
ANALYTICAL PREPARATION
~P~ARAM==E~T~E~R~---------------------METHOD ~M~E~T~H~O~D ____ _
8270C (SIM) SW846 8270C SIM SW846 3520C
I References:
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SW846 "Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods", Third Edition, November 1986 and its updates.
SAMPLE SUMMARY
C2B2002l8
_l:!Q_J!_ SAMPLE# CLIENT SAMPLE ID
EVDPC 001 C-lOA
EVDPH 002 C-lOB
EVDPK 003 C-13B
EVDPM 004 C-29B
EVDPP 005 C-28A
EVDPQ 006 C-14B
EVDPR 007 C-27A
EVDPT 008 C-12A
EVDPW 009 C-27B
EVDPO 010 EB
EVDP6 011 DUPOl
EVDP7 012 C-09B
EVDP9 013 C-15B
EVDQA 014 PW-Ol
EVDQD 015 FB
EVDQF 016 C-llB
NOTE(S)
-The analytical results of the samples listed above are presented on the fol!owing'pages.
-All calculations arc performed before rounding to avoid rouud·off errors in calculaccd results
-Results noted as "ND" were noc detecced at or above the staced limit.
• This report muse not be reproduced, except in full, witl10uc the written approval of the laboratory.
-Results for the following parameters are never reported on a dry weight basis: color, corrosivity, density, flashpoint, ignitabilicy, layers, odor,
paint filter 1es1, pH, porosity pressure, reactivity, redox pO!cntial, specific gravity, spot tests, solids, soluhility, temperature, viscosity, and weighc.
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SAMPLED SAMI
DATE TIME
02/18/02 16,I
02/18/02 17,10
02/18/02 131 02/19/02 l2,
02/19/02 lL 5
02/19/02 131 02/19/02 0 9, I
02/19/02 10,
02/19/02 09,30
02/19/02 lO I 02/18/02 11,
02/18/02 15,35
02/18/02 14,, 02/18/02 ll,
02/18/02 lO,
02/18/02 15,00
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Chain of
Custody Record
STL--4124 (1200)
Cliep r;:,--r p:_ (_.,
Ad~s~~~ A,1
- -
5-k.-3,oZ c,,ce,v\,~ ~I ZioJ°'74 z. ~p;_;;z;;a:n (~ Lo·~
Con~urchase Order/Quote No. ..__,
,P .£<.Z.. r · 0 3 Ip 2-L./ · o°Jc
Sample f.D. No. and Description Date (Containers for each sample may be combined on one line)
- -- --
p~t,. fx.~
r~7 gmb3:; r°""r:; ;":Z" I ~ z 3q I s,sn:a\/~, Lab Cont; (1 V, ~ ' cg:£'7~3b~ I 3~ 4~ I\J
Q)
Containers & \t Matrix Preservatives
! . 0 "' ' 0' Time ~ ~ a. "' 0 G 0 ,o I
~ i .5l § ~ , • ~~ ~ ' ' ,
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v/3 lo'Zh
C I rr3 L5lro
.
(J,
~~le Hazard ldent1ficat1on
on~Hazard D Flammable 0 Skin Irritant D Poison B
I Sample Disposal
D Unknown D Return To Client txf'.oisposal By Lab D Archive For
Tbm Around Time Required
\l7f 0/he, ~.
QC Requirements (Specify)
D 24 Hours 0 48 Hours D 7 Days D 14 Days 0 21 Days
- ---Severn Trent Laboratories, Inc.
oaz,/;q/ oz_ Chain of lt]d6N89 6
Lab Number (_ Page of \
Analysis (Attach fist if
more s Jace is needed
Speciaf Instructions/
Conditions of Receipt
(A tee may be assessed d samples are retained
Months longer than 3 months)
f. Relrnquished By 5z:;,~1•t-1,100) 1 Recei,ed~th, _ ,j /} a. A,,/--l
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"'r.P.e//nquisf.'.jd By (,
1
Date
1
Time 2. Received /Jy -
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Dale
1
Time
.1 R•illl!r/111',/lt7r/ ny 10,1/r>
1
rimn .1 R<'crivrd nv ("'' 1
r,me
Comments
OISTRfRUrtON; WHITF. · Sr,1ys with lh~ Sample; CANARY· Returned to Client with Report: PINK· Field Copy
SEVERN
TRENT Chain of
Custody Record SERVICES . Severn Trent Laboratories, Inc.
STL-4124 (POOJ .
Client Pro~~ f2c,_c.,,J:,J,-DZ-ft Ci(c>Z Cha;n of lso"Ef 89 7 1Z6rl:x
Address 2J/e. 3oz: Te0°7e/•:(~:t1~a,74zz I 3Zf3Ci Lab Number I ,2xro ~/av /_ ,. Page ( of
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C ~ ~ . =-----, V-JI;;,,..,,,.(-+ more soace is needed
" Project Name and Location (State) Carrier/Waytft!I Number-~ .
(Pr/' z:_o,,--7Zc..le-, -./4... &-7.:S.34 7 . .:y::; 4 G::,5" Special Instructions/
Contract/Purchase Order/Quote No I,.,' Containers & ·f Conditions of Receipt
'Px.c.z 7-CC:>02.4 -c::,t:::f_ ( Matrix Preservatives
Sample I. D. No. and Description i . 0 ~ , "' ~ Date Time ll I ~ 0 0 ~o I (Containers for each sample may be combined on one line) ~ • ~ ~ 2 G '1 ~~ • ~ , , ,
rnsa v/tR/o? I /(11) y, X t-
~fJJ 1026'
OuPd I I ifD
C. oe,a., 1535
C · 156 I 4tt::;
\
'
Possible Hazaro ldentitication I Sample Disposal (A tee may be assessed if samples are retained ' ClYNon.Hazard D Flammable D Skin lrntant 0 Poison B D Unknown D Return To Client ~isposal By Lab 0 Archive For Months longer than J months)
Turn Around Time Required • QC Re uirements (Spec, )
D 24 Hours D 48 Hours D 7 Days D 14 Days D 21 Days ther~ •
q fy
Time 1. Receive Datr. Time
l4tf'D :;, oJu ~,2u
Time 2. Received By Dale Time
T/fl)(I j Rocoivod EJy 0,l!r) r,m,,
Commt?nts
Chain of
Custody Record
STL-4124 (1200)
Clie~
Address
3(50 ~b.v ~
--
o)c_~
c,ry ·;--, ~.,.{ ~ lz;o7e7.e1z
Project Name and Location (State) Exe,~ VZ=/.2-,' 0-,.
Cong;;;~e7~'~3~~-bGz /
Sample I. 0. No. and Description Date (Containers for each sample may be comb_ined on one line)
C-7,A 2-1,,o;
C· /2-4
C · Z""76
~s,ble Hazard lden/J!Jcation
Non-Hazard D Flammable D Skin lrntant D PoisonB . Tum Around Time Requ,red
- -- --
Pro~ac;,;_ D=tu.ei.--
Tq'7n8,u:b2A7 ?~7:::r~m; / 5c .5 g
S1teConta~ ::S-;:;:,,-.. ILa~oni. I. ;-t-
CarrierMlay/Ji/1 Number -.J
827534 755"</~S-CJ
Containers & ~ Matrix Preservatives
l ~ 0 "' , ~~ tl Time ti ~ a "' 0 G 0
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1co6 .
-oq3z
I Sample Disposal
D Unknown O Re;urn To Client OCoisposat By Lab D Archive For
0 QC Requlfements (Sp_c1ty)
D 24 Hours D 48 Hours D 7 Days D /4 Days D 21 Days
Date ~J:, I? /Z ;q/4 (JV
Date 2. Received By
n.,1,, .1 Rr>1:r>1,·r>d fl\'
DISTRIBUTION: WHITE. Stay$ \Vl/h th~ Sarnole. CANARY. Returned lo Client with Report: PINK. Field Copy
--- -
Severn Trent Laboratories, Inc.
oz/;9,/b C
Chain of Custody Number 106898
Lab Number
Page I of (
Analysis (Attach fist if
more soace is neededJ
Special Instructions/
Conditions of Receipt
(A fee may be assessed if samples are retained
Months longer than 3 months)
Time
/0 ·O . JU
Time
Tim~
Chain of
Custody Record
STL-4124 (1200)
Client
"/Z.£,r~ C
Address &c.3Dz c3oD f.ibob-A-v,
City i;a~!z;vt"; .qz c.,...,,.,~
Pro1g_ame and Location (Stat~
.J7 r, -Z: ev -e, . r:<1,,, Contrgz;;_or;;~uo0~ /c;Z L( • c)Ci'.-{
Sample f.D. No. and Description Date (Contamers tor each sample may be combined on one line)
C· toA 2· (~-cR.
C-t or:z,
C . 100
C -Z-4'3 -z_. ('1-0
C~z.8LL I
r ---L 4p., I
Possible Hazard Identification
~Non-Hazard D Flammable D Skin Im/ant D Poison B
Turn Around Time Re uired q
SEVERN
TRENT
· SERVICES Severn Trent Laboratories, Inc.
Proje(~/k l:2.U£i---Date Ii ( z_ (Ci 15~ Chain of 1s cr 689 9
Te/~78~b3A7 t"•;::r U I a'Z3 Lab Number
"' Page I of I
Site Conta\j Lab Contact 1 Analysis (Attach fist if \ 6, --::,.__,,___ V.:61..v"-k+ more s ace is needed ) tiz.:f'33";{ 7 o'5 4 to5 I) Special Instructions/
Matrix Containers & ~-
Conditions of Receipt
·Preservatives
1 " 0 "' " "" ~ • Time ll ii ! "' 0 G 0 sO . ~ ~ ~ ~~ ' "' " " /{.,4D Ix; Y-1.2
' 1110
13/v
/2~-D
1/25"
000
l Sample Disposal
D Unknown D Return To Client ~isposal By Lab D Archive For
(A fee may be assessed ,t samples are retained
Months longer /han 3 months)
QC Re uirements S ec1 ( p /y) q
D 24 Hours D 48 Hours D 7 Days D 14 Days D 21 Days
Dale ,1 Time
,;J ::.J.o/o8. lo ::>,o
Date Time
.1 Rnr.Aivf'd Ry Trme
Commtmls -- --
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Lot-Sample# ... , C2B200218-001
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-d5
Terphenyl-d14
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID, C-l0A
GC/MS Semivolatiles
Work Order# ... , EVDPClAA
Date Received .. , 02/20/02
Analysis Date .. , 02/25/02
Matrix. - . - -.. - . : WJ..TER
MS Run# ....... , 2052100
Method ......... , SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
58 (32 -112)
44 (10 -144)
56 (30 -llO)
55 (13 -110)
59 (10 -113)
72 (21 -122)
Lot-Sample# ... , C2B200218-002
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
. Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID, C-10B
GC/MS Semivolatiles
work Order# ... , EVDPHlAA
Date Received .. , 02/20/02
Analysis Date .. , 02/25/02
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Matrix ......... , WATER I
MS Run # ....... , 2052100
Method ......... , SW846 8270C SIM I
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REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1. 0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
50 (32 . 112)
57 (10 . 144)
53 (30 . 110)
45 (13 . llO)
55 (10 . 113)
72 (21 . 122)
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Lot-Sample# ... : C2B200218-003
Date Sampled ... : 02/18/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-ds
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: C-13B
GC/MS Semivolatiles
Work Order# ... : EVDPKlAA
Date Received .. : 02/20/02
Analysis Date .. : 02/25/02
Matrix ......... : WJ..TER
MS Run# ....... : 2l•o2l00
Method ......... : SWB46 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
42 (32 -112)
50 (10 -l44)
42 ( 30 -110)
26 (13 -110)
19 (10 -113)
51 (21 -122)
Lot-Sample# ... : C2B200218-004
Date Sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 10
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: C-29B
GC/MS Semivolatiles
Work Order # ... : EVDPMlAJ'.
Date Received .. : 02/20/02
Analysis Date .. : 02/25/02
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Matrix ... _ ..... : w.:.TE:Z I
MS Run # ....... : 2·c52l00
Method ......... : SW846 8270C SIM I
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RESULT
ND
27
PERCENT
RECOVERY
65
52
61
53
58
70
REPORTING
LIMIT
2.0
10
RECOVERY
LIMITS
(32 -112)
(10 -144)
(30 -110)
(13 -110)
(10 -113)
(21 -122)
UNITS
ug/L
ug/L
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L()t-Sample # ••. : C2B200218-005
Date Sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-ds
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2 1 4 1 6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: C-28A
GC/MS Semivolatiles
Work Order# ... : EVDPPlAA
Date Received .. : 02/20/02
Analysis Date .. : 02/25/02
Matrix ......... : WATER
MS Run# ....... : 2052100
Method ......... : SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
64 (32 -112)
53 (10 -144)
61 (30 -110)
59 (13 -110)
59 (10 -113)
73 (21 -122)
Lot-Sample# ... : C2B200218-006
Date Sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: C-14B
GC/MS Semivolatiles
Work Order# ... : EVDPQlAA
Date Received .. : 02/20/02
Analysis Date .. : 02/25/02
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Matrix ......... : W.Z..TE;. I
MS Run# ....... : 2052100
Method ......... : SW846 8270C SIM I
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RESULT
ND
ND
PERCENT
RECOVERY
56
30
53
49
53
73
REPORTING
LIMIT
0.23
1.2
RECOVERY
LIMITS
(32 -112)
(10 -144)
(30 -110)
(13 -110)
(10 -113)
(21 -122)
UNITS
ug/L
ug/L
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Lot-Sample# ... : C2B200218-007
Date sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: l
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-ds
Terphenyl -d14
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: C-27A
GC/MS Semivolatiles
Work Order# ... : EVDPRlAA
Date Received .. : 02/20/02
Analysis Date .. : 02/26/02
Matrix ......... : WATER
MS Rrm # ....... : 2052100
Method ......... : SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND l.O ug/L
PERCENT RECOVERY
RECOVERY LIMITS
49 (32 -112)
60 (10 -144)
46 (30 -110)
43 (13 -110)
50 (10 -113)
47 (21 -122)
Lot-Sample# ... : C2B200218-00B
Date Sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: C-12A
GC/MS semivolatiles
Work Order# ... : EVDPTlAA
Date Received .. : 02/20/02
Analysis Date .. : 02/25/02
Matrix ......... :
MS Run 1/ ....... :
Method ......... : SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
55 (32 -112)
39 (10 -144)
55 (30 -110)
48 (13 -110)
52 (10 -113)
65 ( 21 -122)
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2C·S2i00
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Lot-Sample# ... : C2B200218-009
Date Sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-d14
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: C-278
GC/MS Semivolatiles
Work Order# ... : EVDPWlAA
Date Received .. : 02/20/02
Analysis Date .. : 02/25/02
Matrix ......... : wr.TE:<
MS Run# ....... : 2052100
Method ......... : SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
59 (32 -112)
50 (10 -144)
54 (30 -110)
53 (13 -110)
57 (10 -113)
65 (21 -122)
Lot-Sample# ... : C2B200218-010
Date Sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID: EB
GC/MS Semivolatiles
Work Order# ... : EVDP0lAA
Date Received .. : 02/20/02
Analysis Date .. : 02/25/02
Matrix ......... :
MS Run# ....... :
Method ......... : SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.22 ug/L
ND 1.1 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
73 (32 -112)
65 (10 -144)
64 (30 -110)
67 (13 -110)
60 (10 -113)
73 (21 -122)
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wr.TE:=:. I
2Cc2l00
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Lot-Sample# ... , C2B200218-011
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
_ Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-d5
Terphenyl-d14
2-Fluorobiphenyl
2-Fluorophenol
Phenol-dS
2,4,6-Tribrornophenol
THE RETEC GROUP INC
Client Sample ID, DUP0l
GC/MS Sernivolatiles
Work Order# ... , EVDP61AA
Date Received .. , 02/20/02
Analysis Date .. , 02/25/02
Matrix ......... : \\·.; T~?.
MS Run # ....... , 20S,lQ.0
Method ......... , SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
7.6 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
62 ( 32 -112)
63 (10 144)
58 ( 30 -110)
55 (13 110)
60 (10 -113)
71 (21 -122)
Lot-Sample# ... , C2B200218-012
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID, C-09B
GC/MS Semivolatiles
Work Order# ... , EVDP71AA
Date Received .. , 02/20/02
Analysis Date .. , 02/25/02
Matrix ......... : w.r:::-~?.
MS Run# ....... : 20S2100
Method ......... , SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND l.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
65 ( 32 -112)
62 (10 -144)
60 (30 -110)
59 (13 -ll0)
56 (10 -ll3)
67 (21 -122)
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Lot-Sample# ... , C2B200218-013
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
TifE RETEC GROUP INC
Client Sample ID, C-15B
GC/MS Semivolatiles
Work Order# ... , EVDP91AA
Date Received .. , 02/20/02
Analysis Date .. , 02/25/02
Matrix ......... : \\ATE?..
MS Run U ....... : 20S21O0
Method ......... , SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
47 ( 32 -112)
41 (10 -144)
45 (30 110)
37 (13 -110)
32 (10 113)
53 (21 122)
Lot-Sample# ... , C2B200218-014
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlor?phenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
NOTE (S) ,
THE RETEC GROUP INC
Client Sample ID, PW-01
GC/MS Semivolatiles
Work Order# ... , EVDQAlAA
Date Received .. , 02/20/02
Analysis Date .. , 02/26/02
Matrix ......... : w..n.T::::?.
MS Run # ....... : 2os21c,o
Method ......... , SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
14 E 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
62 (32 -112)
65 (10 -144)
59 (30 -110)
54 (13 -110)
61 (10 -113)
70 (21 -122)
E Estimated resull. Result conccutration exceeds the calihratio11 range.
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Lot-Sample# ... , C2B200218-014
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
Dilution Factor: 2
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
Tiffi RETEC GROUP INC
Client Sample ID, PW-01
GC/MS Semivolatiles
Work Order# ... , EVDQA2AA
Date Received .. , 02/20/02
Analysis Date .. , 02/26/02
Matrix ......... : W . .:\T2R
MS Run If ....... , 20521C"O
Method ......... , SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.40 ug/L
4.2 2.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
55 ( 32 -112)
60 (10 144)
54 (30 110)
48 (13 -110)
55 (10 113)
59 (21 122)
Lot-Sample f/ ... , C2B200218-015
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch f/ ... , 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-dS
2,4,6-Tribrornophenol
THE RETEC GROUP INC
Client Sample ID, FB
GC/MS Semivolatiles
Work Order# ... , EVDQDlAA
Date Received .. , 02/20/02
Analysis Date .. , 02/26/02
Method ......... , SW846 8270C
REPORTING
RESULT LIMIT
ND 0.20
ND 1.0
PERCENT RECOVERY
RECOVERY LIMITS
67 ( 32 -112)
67 (10 -144)
60 (30 110)
61 (13 110)
64 (10 -113)
66 (21 122)
Matrix ......... : WAT~R
MS Run ll. ...... , 2002100
SIM
UNITS
ug/L
ug/L
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Lot-Sample# ... , C2B200218-016
Date Sampled ... , 02/18/02
Prep Date ...... , 02/21/02
Prep Batch# ... , 2052220
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-d5
Terphenyl'dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-dS
2,4,6-Tribromophenol
THE RETEC GROUP INC
Client Sample ID, C-llll
GC/MS Semivolatiles
Work Order# ... ' EVDQFlAA
Date Received .. , 02/20/02
Analysis Date .. , 02/26/02
Matrix ......... : w.::..T:::?.
MS Run # ....... : 205L.1c, Cl
Method ......... , SW846 8270C SIM
REPORTING
RESULT LIMIT UNITS
ND 0.20 ug/L
ND 1.0 ug/L
PERCENT RECOVERY
RECOVERY LIMITS
59 (32 112)
54 (10 -144)
53 (30 110)
56 (13 110)
57 (10 -113)
61 ( 21 -122)
METHOD BLANK REPORT
GC/MS Semivolatiles
Client Lot# ... : C2B200218 Work Order# ... : EVEPPlAA
MB Lot-Sample#: C2B210000-220
Analysis Date .. : 02/25/02
Dilution Factor: 1
PARAMETER
2,4-Dichlorophenol
Pentachlorophenol
SURROGATE
Nitrobenzene-d5
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-dS
2,4,6-Tribromophenol
NOTE(S):
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
REPORTING
RESULT LIMIT
ND 0.20
ND l.0
PERCENT RECOVERY
RECOVERY LIMITS
61 ( 32 -112)
60 (10 -144)
53 (30 -110)
58 (13 -110)
60 (10 -113)
61 (21 -122)
Calculations are performed before rounding to avoid round-off errors in calculated results.
UNITS
ug/L
ug/L
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Matrix ......... : WATER I
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METHOD
SW846 8270C SIM I
SW846 8270C SIM
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LABORATORY CONTROL SAMPLE EVALUATION REPORT
GC/MS Semivolatiles
Client Lot# ... : C2B200218 Work Order# ... : EVEPPlAC Matrix ......... : WAT~R
LCS Lot-Sample#: C2B210000-220
Prep Date ...... : 02/21/02 Analysis Date .. : 02/25/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PERCENT RECOVERY
PARAMETER RECOVERY LIMITS METHOD
Pentachlorophenol 53 (10 -140) SW846 8270C SIM
2,4-Dichlorophenol 58 (42 -ll5) SW846 8270C SIM
PERCENT RECOVERY
SURROGATE RECOVERY LIMITS
Nitrobenzene-dS 60 (32 -ll2)
Terphenyl-dl4 63 (10 -144)
2-Fluorobiphenyl 55 (30 -ll0)
2-Fluorophenol 55 (13 -ll0)
Phenol-d5 57 (10 -ll3)
2,4,6-Tribromophenol 67 (21 -122)
NOTE (S) :
Calcula1ions are performed before rounding to avoid round-off errors in calculated results.
MATRIX SPIKE SAMPLE EVALUATION REPORT
GC/MS Semivolatiles
Client Lot# ... : C2B200218 Work Order# ... : EVDQAlAC-MS
EVDQAlAD-MSD
Date Received .. : 02/20/02
Analysis Date .. : 02/26/02
Matrix ......... : WATER
MS Lot-Sample#: C2B200218-014
Date Sampled ... : 02/19/02
Prep Date ...... : 02/21/02
Prep Batch# ... : 2052220
Dilution Factor: 1
PARAMETER
Pentachlorophenol
2,4-Dichlorophenol
SURROGATE
Nitrobenzene-dS
Terphenyl-dl4
2-Fluorobiphenyl
2-Fluorophenol
Phenol-d5
2,4,6-Tribromophenol
NOTE (S):
PERCENT
RECOVERY
130
133
59
61
RECOVERY
LIMITS
(10 -140)
(10 -140)
(42 -ll5)
(42 -ll5)
PERCENT
RECOVERY
62
65
57
58
55
57
57
61
57
60
68
70
Calculations are performed before rounding to avoid round-off errors in calculalcd results.
MS Run# ....... : 20521GO
RPD
RPD LIMITS METHOD
SW846 8270C SIM
0.88 (0-56) SW846 8270C SIM
SW846 8270C SIM
3.9 (0-44) SW846 8270C SIM
RECOVERY
LIMITS
(32 -· ll2)
(32 -ll2)
(10 -144)
(10 144)
(30 -llO)
(30 -llO)
(13 -llO)
(13 -llO)
(10 ll3)
(10 -113)
(21 -122)
( 21 -122)
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