NCD003200383_19870305_Koppers Co. Inc._SERB C_Environmental Baseline Study-OCR

KEYSTONE_
ENVIRONMENTAL RF.SOL'RCf.S, lSC.
I
436 Seventh Avenue, Suite 1940, Pittsburgh. PA 15219
Dear Ms. DeRosa:
March 5, 1987
N.C. Department .of Human Resources
Division of Health Services
P. 0. Box 2091
Raleigh, N.C. 27602
ATTN: Pat DeRosa
Waste Management Specialist
Keystone Environmental Resources has been contracted by Koppers to
co~duct the environmental affairs associated with its former
Morrisville, N.C. Facility. In conjunction with the sale of this
property to Unit Structures Inc., an environmental base-line study was
conducted. This included a survey of the off-site groundwater used for
human consumption.
The off-site survey consisted of three rounds of samples, taken from
nlnc ~~l~~tc ~~tc~ ~211i, The first round was sampled on October 24,---
1986, and was analyzed by the Keystone Environmental Resources
Laboratory in Monroeville, Pa. The analysis included both conventional
water quality parameters; and volatile organics. The latter was done
.using gas chromatography (GC).
A second round of samples were taken on November 20, 1986. Duplicate
samples were analyzed by the Monroeville Lab and by Spectrix
Laboratory in Houston, Texas. The Houston laboratory utilized GC/MS
(gas chromatography/mass spectrophotometry) for organic analysis. The
Monroeville Lab used a modified procedure in the extraction step prior
to GC analysis, using four liters of sample instead of the normal one
liter .. A Koppers' method of analysis for pentachlorophenol was also
run in addition to the standard GC method.
The third round of sampling was conducted on January 14, 1987. The
samples were split between the Monroeville and Houston Laboratories,
and analyzed like the samples from round two. That is, 4L of sample
were extracted for organic analysis instead of the normal 1 L.
Both gas chromatography (GC) and gas chromatography/mass
spectrophotometry (GC/MS) are accepted methods of organic analysis
which can detect contamination at the ug/1 level (parts per billion).
Of the two methods, GC normally can detect organic compounds at lower
concentration levels, but does not positively identify the compound.
GC/MS provides a more positive identification of the compound but at a
slightly higher 1evel of detection.
Page 2
This· difference in lower detection levels, and the actual concentrations found, present some problems in the discussion of contamination levels. It appears inappropriate to state a definite concentration of a compound when the contamination levels are so low. Consequently we will present the ranges of contamination levels, noting -that in each case, at least one round of sampling exhibited no detectable contamination.
Based on the attached analytic data and interpretation, we feel that two of the off-site wells tested produce water·with trace levels of industrial chemicals. These are Wells 05-8 (The Shiloh Baptist Church) and Well 05-9 (William Barber Well). The range of constituent levels are:
Well 0S-8 (Shiloh Baptist Church)
Pentachlorophenol
Isopropylether
Well DS-9 (William Barber)
Isopropyl ether
8.8 to 28.8 ppb
(Avg. Detected 19.4 ppb)
26 to 85.5 ppb
(Avg. Detected 57.5 ppb)
13.3 to 17.5 ppb
(Avg. Detected 15.4 ppb)
1'( l'c'f' ;,
--? Please note that the average values do not include several "Not Detected" analytical results.
The constituents were found at low levels and not consistently detected in repeat sampling. The levels measured of these chemicals are not associated with adverse health effects. The highest concentrations found, 28 ppb pentachl orophenol, and 85 ppb isopropylether, are not considered dangerous to the health of jndividuals using the water on a daily basis for routine activities, i.e., drinking, cooking, bathing, and laundry. Regulatory standards have not been promulgated for either chemical in drinking water; . . \·{J/U\ . however, the U.S. EPA has issued~ lif7ti~e health advisory guideline J'-i)4 / t, ➔ of ?20 ppb f~r p~ntachloro~henol in drinking water. T~e mo~t . 1 • ! ,·.'\ stringent guideline establ ,shed for pentachlorophenol in drinking • i, :.•_,,,· water is that of the State of California which has set a level of 30 c--'-,, ppb on the basis of the taste and odor imparted by the contaminant on the water.
We have included the
for your inspection.
of custody documents
Page 3
analytical results
These include the
are available upon
from all the
QA/QC data.
request.
sampling rounds
The sample chain
We are looking forward to discussing this information with you next
week. Please call if you have anyquestions concerning this data.
Sincerely yours,
Martin M. Schlesinger, Assistant Program
Manager
Previously Operated Properties o--B0M~ J. H. Butala,·o.A.B.T.
Manager, Toxicology and Product Registration,
Koppers Company, Inc.
Page 4
ANALYTICAL INTERPRETATION
Wells 0s01 to OS-4
Round #1 -
ih'l "{\_
Route #2
Well OS-5
These samples were filtered in a room which contained sawdust contaminated with Pentachlorophenol. Because PCP was not found in the other samples these are to be disregarded. _ 1 f k "-~ (-' '-' VJ>\
The ~~contamination ,fo'und in Wells OS-1 to oS-~ 05-A' were below the~ concentrations in both the field and trip blanks and are therefore to be di scountea.
The only constituent identified was PCP in round #3 by the Monroeville Lab at 0.6 ppb, using GC. However, the Houston Laboratory did not find the compound at a higher detection limit. Because this trace level was found only once, this figure should be discounted.
Wel 1 0S-6
Unfortunately, the third sample round was destroyed in shipment. However, only a trace level of !PE was found by one lab during round #2. Based on the low level of !PE (1.46 ppb) and the lack of -confirmation,. this figure should be discounted.
Well 0S-7
A trace level (8.6 ppb) of PCP was found via GC by the Monroeville Laboratory during the third round. However, the same laboratory did not find PCP using the more sensitive Koppers' method, nor was PCP found by the Houston Lab using GC/MS. Based on the level of ~ontamination and the lack of confirmation in other rounds, this figure should be discounted.
Well 0S-8
Pentachlorophenol was found at trace levels (8.82-28.8), and confirmed by GC/MS in two rounds of sampling. Additionally, !PE was found at 26-85.5 ppb levels. Three phenolic compounds were identified in only one of the samples, but their presence was not confirmed.
Page 5
Wel 1 OS-9
Isopropylether was found in two samples, but not confirmed by the
GC/MS. Concentrations were 13.3 and 17.5 ppb.
✓
DEC 5 1986
KEYSTONE ENVIRONMENTAL RESOURCES
TABLE OF CONTENTS PRODUCED ON 10/24/86 AT 10:46 PAGE_
SAMPLE # SOURCE DESCRIPT DATE-COL DATE-REC -------------------------------------------------------------
RN860020 WELL OS-1-JOHN MEDLIN WELL ·09/10/86 09/11/86
RN860021 WELL OS-2 GEORGE HARDY WELL 09/10/86 09/11/86
RN860022 WE_LL_ OS-3 MRS. BAKER WELL 09/10/86 09/11/86
RN860023 WELL OS-4 ROY MEDLIN WELL 09/10/86 09/11/86
RN860024 WELL os-s TRIANGLE MATERIALS 09/10/86 09/11/86
RN860025 WELL OS-6 \II I LKERSON CONSTRUCT. 09/10/86 09/11/86
RN86002_6 WELL OS-7 JAMES CROWE WELL 09/10/86 09/11/86
RN860027 WELL os-e SHILOH BAPTIST CHRCH 09/10/86 09/11/-96
RN860029 WELL OS-9 \II I LL I AM BARBER WELL 09/10/86 09/11/86
KEYSTONE ENVIRONMENTAL RESOURCES
-------=-=.---------------------------------------
TABLE 1e SUMMARY OF ANALYTICAL DATA
SAMPLE# RSLT.LNE
CHEMICAL OXYGEN DEMAND.
RN860020 COD <Total>, ·mg/Le 12.0
RN860021 COD <Total>, mg/Le 12.0
RN860022 COD < Tota 1 > , mg/Le (10.0
RN860023 COD <Tota·,>, mg/Le 15.0
RN860024 COD <Total>, mg/Le 18.0
RN860025 COD <Total>, mg/Le (10.0
RN860026 COD <Total>, mg/Le (10.0
RN860027 COD <Total>, mg/Le 10.0
RN860028 COD <Total>, mg/Le (10.0
CONDUCTIVITY
~N860020
RN860021
RN860022
"'IN860023
.:..~i\!860024
.=iN,960025
.::,r-.1860026
::;:NS60027
=::--!S·S0028
=•HENOL
:.::i•:.::.r:.0021
.=:N860022
,9N360023
=(N860024
=:N860025
=:N8_00026
,C:N860027
cona. , umnos/cm
cona. , umhosicm
cona. ,umnos/cm
cona. ,umnosicm
con a. , umt;os/cm
cona. , umt;os/cm
cond. , umt1os1cm
con a. , umt1os /cm
cona. , umt;os/cm
520
925
1660
2210
2600
1 170
345
932
·532
mr:_n_ If"\ 005
Pneno1
Phenol
mg/Le <0.005
mg/Le <0.005
Phenol .mg/Le
Pher)OI mg/Le
Phenol, mg/Le
Pheno I, mg/Le
Phenol, mg/Le
RN860028 Phenol, mg/Le
TOTAL ORGANIC CARSON
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
RNS60020 TOC, mg/Le < 1 . 00
RN-960021 TOC, mg/Le 1 . 55
RN,960022 TOC, mg/Le. 1. 89
RN860023 TOC, mg/Le 3.22
RN860024 TOC, mg/Le 3.30
RN860025 TOC, mg/Le 1. 47
,9N960026 TOC, mg/Le < 1 '. 00
RN860027 TOC, mg/Le 1 . 25
=:N860028 TOC, mg/Le < 1 . 00
:JH
RN860020 pH, uni ts 7.5
?.N860021 pH, units 7 ·. 1
.:::::N,960022 pH, uni ts 7. 1
.9N860023 pH, uni ts 7.5
.',N860024 pH, uni ts 7. 1
RN860025 PH, uni ts 7.5
F<N860026 PH, units 7. 1
RN860027 OH, uni ts 7.4
RN860028 pH,. units 7.4
PRODUCED ON 10/24/86 AT 10 e 49 PAG.E
SOURCE ---------------
WELL 05-1
WELL OS-2
WELL 05-3
WELL 0S-4
WELL 0S-5
WELL 0S-6
WELL 05-7
WELL 05-8
WELL OS-9
WELL 0S-1
WELL OS-2
WELL 0S-3
WELL OS-4
WELL 05-5
WELL OS-6
WELL 05-7
WELL OS-8
WELL 0S-9
WELL OS-1
WELL OS-2
WELL 05-3
WELL OS-4
WELL OS-5
WELL 0S-6
WELL OS-7
WELL OS-8
WELL OS-9
WELL OS-1
WELL OS-2
WELL 0S-3
WELL OS-4
WELL OS-5
WELL OS-6
WELL OS-7
WELL OS-8
WELL OS-9
WELL OS-1
WELL OS-2
WELL OS-3
WELL 0S-4
WELL OS-5
WELL OS-6
WELL 05-7
WELL OS-8
WELL OS-9
1
KEYSTONE ENVIRONMENTAL RESOURCES
==============------------------------------------
TABLE 1: SUMMARY OF ANALYTICAL DATA PRODUCED ON 10/24/86 AT 10:49 PAGE 2
:;;:======
SAMPLE # RSL T. LNE SOURCE -----------------------------------------------------------------
TOTAL DISSOLVED SOLIDS
RN860020 mg/L, TDS @103 C 334 WELL OS-1
RN860021 mg_/L, 'TDS @103 C 572 WELL OS-2
RN860022 mg/L, TDS @103 C 1290 WELL OS-3
RN860023 mg/L, TDS· @103' C 1348 WELL OS-4
RN860024 mg/L, TDS @103 C 1772 WELL OS-5
RN86002_5 mg/L, TDS @103 C 722 WELL OS-6
RN860026 mg/L, TDS @103 C 266 WELL OS-7
RN860027 mg/L, TDS @103 C 732 WELL OS-8
RN860028 mg/L, TDS @103 C 340 WELL OS-9
KEYSTONE ENVIRONMENTAL RESOURCES
TABLE 2: SUMMARY OF ANALYTICAL DATA PRODUCED ON 10/24/86 AT 10:50 PAGE
'--·---.-----===---------------------------========
SAMP.LE # RSLT.LNE SOURCE -----------------------------------------------------------------
CHLORIDE
RN860020 en lor i ae, mg/L: 19.0 WELL OS-1
RN860021 cn.1oriae, mg/L: 29.0 WELL OS-2
RN860022 cn1oriae, mg/L: 350 WELL OS-3
RN860023 en lor i ae, · mg/L ·: 515 WELL OS-4
RN860024 en 1or i oe, mg/L: 699 WELL 05-5
RN860025 cn1oriae, mg/L: 126 WELL 05-6
RN860026 cn1oriae, mg/L: 9.70 WELL 05-7
RN860027 cn1oriae, mg/L: 68.0 WELL OS-8
RN860028 cn1orioe, mg/L: 37.0 WELL 05-9
FLUORIDE
RN860020 Fluoriae, mg/L: 0. 120 WELL 05-1
RN860021 FI uor i ae, mg/L: 0. 170 WELL OS-2
;c;N860022 Fluoriae, mg/L: 0. 150 WELL OS-3
RN860023 Fluoriae, mg/L: 0. 130 WELL 05-4
Ri·J860024 Fluoriae, mg/L: 0.290 WELL 05-5
~N,960025 Fluoriae, mg/L: 0.290 WELL 0S-6
.~;t✓.960026 FI uo r i ae, mg/L: 0.220 WELL OS-7
·0:Ne,60027 Fluoride, mg/L: 0.330 WELL OS-8
~:,J.960028 Fluoriae, mg/L: 0 .200 WELL OS-9
1·~1 I TR.A TE
::-iJ o Mr>r'l '.:l/"'i Nit!'"'AtA "'"' " mi: / I__ • 0. 12? WELL OS-1
:;r,:360021 Nitrate as N, mg/L: 0 .4,9 WELL OS-2
~r-!800022 Nitrate as N, mg/L: 3. 38 WELL OS-3
'<N860023 Nitrate as N, mg/L: <O. 100 WELL OS-4
==:i~-960024 Nitr:ate as N, mg/L: 0.922 WELL OS-5
.~NS.60025 Nitrate as N, mg/L: 0.552 WELL 0$-6
.=:N.S-30026 Nitrate as N, mg/L: 0.369 WELL OS-7
.=:t../860027 Nitrate as N' mg/L: 2. 1 5 WELL OS-8
RN860028 N.itrate as N, mg/L: <O. 100 WELL 03-9
NITRITE
RN86002.0 Nitrite as N, mg/L: <O .010 WELL OS-1
RN,860021 Nitrite as N, mg/L: <0.010 WELL ·os-2
RNS60022· Nitrite as. N, mg/L: (0.010 WELL OS-3
RN860023 Nitr:ite as N, mg/L: (0.010 WELL OS-4
RN.860024 Nitrite as N, mg/L: (0.010 WELL os-s
RN860025 Nitrite as N, mg/L: 0.049 WELL OS-6
RN860026 Nitrite as N, mg/L: <0.010 WELL OS-7
RN860027 Nitrite as N, mg/L: <0.010 WELL OS-8
RN-560028 Nitrite as N, mg/L, <0.010 WELL OS-9
3ULFATE
RN860020 Sulfate, mg/L: (10 .0 WELL 0S-1
=tN860'021 Sulfate. mg/L: < 1 0. 0 WELL OS-2
RN860022 ·Su I fate, mg/L: (10. 0 WELL OS-3
RN860023 Sulfate, mg/L: (10.0 WELL OS-4
RN860024 Sulfate, mg/L: 22. 7 WELL OS-5
RN860025 Sulfate, mg/L: 20: 6 WELL 05-6
=iN860026 Sulfate, m9/L: 19 .. 1 WELL OS-7.
RN860027 Sulfate, m9/L: 57. 1 WELL OS-8
=lN860028 Sulfate, mg/L: 1 1 . ,9 WELL OS-9
KEYSTONE ENVIRONMENTAL RESOURCES
TABLE 3: SUMMARY OF METALS DATA PRODUCED ON 10/24/86 AT 10:51 PAGE =================-=========-------------========
SAMPLE # RSLT.LNE SOURCE -----------------------------------------------------------------
ARSENIC
RNS60020 Arsenic, mg/L: <0.010 WELL OS-1
RNS60021 ArSet')iC, mg/L: <0.010 WELL OS-2
RNS60022 Arsenic, mg/L: <0.010 WELL OS-3
RNS60023 Arsenic, mg/L: (0.010 WELL OS-4
RN860024 Arsenic, mg/L: 0.014 s \)c,..IA .0 5' WELL OS-5 Tr;"'7\,, f'\s.M.
RN860025 Arsenic, mg/L: (0.010 WELL OS-6
RN860026 Arsenic, mg/L: <0.010 WELL OS-7
RN860027 Arsenic, mg/L: (0,010 WELL OS-8
RN860028 Arsenic, mg/L: <0.010 WELL OS-9
CALCIUM
RN860020 Calcium, mg/L: 33.6 WELL OS-1
RN860021 Calcium, mg/L: 76.8 WELL OS-2
=:NE'.60022 Calcium, mg/L: 134 WELL OS-3
=:N860023 Calcium, mg/L: 105 WELL OS-4
-=.US60024 Calcium, mg/L: 121 WELL OS-5-
:: ~,1860025 Calcium, mg/L: 46.6 WELL OS-6
:;--J860026 Calcium, mg/L: 20.8 WELL OS-7
.:'./J860027 ca I c i um, m9 IL : 38. 1 WELL OS-8
. '.J860028 Calcium, mg/L: 45.3 WELL OS-9
:.-.-ROM I UM
-rJ860020 cnromium, ma/L: (0.050 WELL OS-1
:: .. 350021 Ct1rom i um, mg/L: <0.050 WELL OS-2
-:-·:,1.-960022 cnromium, mg/L: <0.050 \l/EL L OS-3
~NS60023 Chromium, mg/L: <0.050 WELL OS-4
=:i·~-360024 Chromium, mg/L: <0.050 WELL OS-5
0.N.960025 Chromium, mg/L: <0.050 WELL OS-6
::!;·~360026 Chromium, mg/L: (0.050 WELL OS-7
=:N860027 Chromium; mg/L _: <0.050 WELL 0:3-8
=;N.'360028 Chromium, mg/L: (0.050 WELL OS-9
,·iAGNES I UM
=:N860020 Magnes i L,m, mg/L: 18.4 WELL OS-1
":NS60021 Magnesium, mg/L: 22.8 WELL 0S-2
=:NS60022 Magnesium, mg/L: 66.3 WELL OS-3
=:N860023. Magnesium, mg/L: 49.5 WELL OS-4
~N860024 Magnesium, mg/L: 70.9 WELL Q:5-5
=:N860025 Magnesium, mg/L: 34. 1 WELL OS-6
:::;NS60026 Magnesium, mg/L: 13. 1 WELL OS-7
=:N,960027 Ma9nesium, mg/L: 24 .4 WELL OS-8
::::r,J860028 Magnesium, mg/L: 16. 4 WELL OS-9
KEYSTONE ENVIRONMENTAL RESOURCES =============-------====----------====-----------= TABLE 3: SUMMARY OF METALS DATA ===================•==================== SAMPLE# RSLT.LNE ---------POTASSIUM RN860020 RN860021 RN860022 RN86002~ RN860024 RN860025 RN8600215 RN860027 RN860028 SODIUM RN860020 RN860021 ?.N860022 RN860023 RNS60024 i=:U8r.30025 i=;N.S60026 .~N860027 =.NE-•SO O 2 8 Potassium, mg/L: 1. 35 Potassium, ·mg/L: 1. 05 Potassium, mg/L: 1. 76 Potassium, mg/·L: 4.70 Potassium, mg/L: 5.21 Potassium. mg/L: 3.26 Potassium, mg/L: 1. 93 Potassium, mg/L: 1. 94 Potassium, mg/L: 1 . 5 1 Sodium, mg/L: 12.7 Sodium, mg/L: 27.7 :5od i um, mg/L: 27. Sodium, mg/L: 40.7 Sodium, mg/L: 190 Sodium, mg/L: 180 Sodium, mg/L: 70. Sodium, mg/L: 14.6 Sodium, mg/L: 4.S. 3 PRODUCED ON 10/24/86 AT 10:51 ===============~============= SOURCE ---------------WELL OS-1 WELL OS-2 WELL OS-3 WELL OS-4 WELL OS-5 WELL OS-6 \I/ELL OS-7 \I/ELL OS-8 WELL OS-9 WELL 0S-1 WELL OS-2 WELL OS-3 WELL 0S-4 ·wELL OS-5 WELL 0S-6 WELL OS-7 \I/ELL OS-8 WELL os.-9 PAGE 2 ========
KEYSTONE ENVIRONMENTAL RESOURCES
ABLE 4: SUMMARY OF ORGANIC COMPOUNDS ·PRODUCED ON 12/04/86 AT 11:46 PAGE
==-= ·===============================~== --------===================--========
AMPLE# RSLT.LNE
CID EXTRACTABLE PHE~OL.ICS
:N860020
:N.S'=,0021
2, 4, 6Tr i Ch I orophetlO I
2,4-D.ichlorophenol
2,4-Dimethylphenol
2,4-Dinitropnenol
2-Chlorophenol ... .
2-Nitrophehol .... .
< 1 . 00
< 1. 00
< 1. 00
< 1. 00
< 1 ·. 00
< 1. 00
4,6-Dinitro-o-cresol <1.00
4-Nitrophenol..... <1 .oo
Penta,:11 I oropheiio t". ·,e-•-f3: 9 -
Pheno t . < 1 . oo
Tetrach1or?pheno1
p-Chloro-m-creso1
2,4,6T(ict1:1oropneno1
2,4-Dicn10,ropneno1
2,4-DimethylphehOI
< 1 . 00
< 1 . 00
< 1 . 00
< 1 . 00
< 1. 00
2.4-Dinitr~pnenol <1 .co
2-ch1oropneno1 <1 .oo
2-Nitrop11e'r101 <1 .oo
4,6-Din-itrb-o-cresor <1.00
4-Nitropnenol. ,·1·.00
Pentach1oropheno1 15.3
Phenol
Tetracn1oropneno1
< 1 . 00
< 1 . 00
c-cn1oro-rn-creso1 <1.00
2,4,6Trichloropneno1 <1.00
2,4-Dicn1orooneno1
2,4-0imetny1pneno1
2,4-Dlnitr~onenoi
2-cn1oropnen01 .... ' 2-N i tropt1eno 1
·•,6-Dinitr6-o-creso1
4-Nitropnenol ....
< 1 . 00
< 1. 00
< 1 . 00
< 1 . 00
< 1 . 00
< 1. 00
< 1. 00
Pentachlorophenot ·,--·12.7
Pneno I . • • . • . . . . . < 1 . oo
Tetrachlorophenol
p-cn1oro-m-creso1
2,4,6Trichloropheno1
2,4-Dichl~ropnenol
2,4-Dirnethy1pneno1
2,4-Dinltropnenol
2-cn1oropheno1
2-N it rop·11eno 1 .
< 1. 00
·c 1 . oo
< 1 . 00
C 1 . 00
'· 1. 00
< 1 . 00
<.1. 00
< 1. 00
4,6-D,nitro-o-cresol <1.00
4-Nitropnenol. c1.oo
Pentacn I oropt1eno ,--,.·,-:· 15. s
P11eno I ' -·-<·;. oo
Tetracn1oropheno1 (1.00
p-cn1oro-m-creso1 c1.oo
,oove results are reportea in ug/L.
SOURCE ---------------
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
WELL OS-1
\I/ELL OS-2
WELL OS-2
WELL OS-2
WELL OS-2
w·ELL OS-2
WELL OS-2
WELL OS-2
WELL OS-2
WELL OS-2
\l./ELL OS-2
\l.'ELL ·OS-2
WELL OS-2
WELL OS-3
'J/ELL o:;-3
"WELL OS-3
ViE LL os-:3
WE~L OS-3
WELL OS-3
WELL OS-3
WELL OS-3
WELL OS-3
WELL OS-3
WELL os-:3
WELL OS-3
WELL 0S-4
WELL OS-4
WELL OS-4
WELL OS-4
WELL os~4
WELL OS-4
WELL OS-4
WELL OS-4
WELL OS-4
WELL OS-4
WELL OS-4
WELL OS-4
KEYSTONE ENVIRONMENTAL RESOURCES
.~8 :_ C: 4: SUMl\'lARY OF ORGANIC COMPOUNDS PRODUCED ON 12/04/86 AT 11•46
============-================
AMPLE# RSL T. LNE SOURCE
~--------.---------------------.---------------------------------
:•rn60024
N2,c30027
2,4,6Trichior9pheno1
2,4-Dicn1oropneno1
~,4-Dimetny1pneno1
2,4-Dinitropnenol
2-cn1oropn,no1 ...
2-N it rop11eno 1 ..
4,6-Dinitro-o-cresol
4~Nitropne~oJ ....
Pentacn1oropneno1
< 1 , 00
< 1 , 00
< 1. 00
< 1 , 00
<1.00
< 1 . 00
< 1, 00
< 1 . 00
<1.00
Pnenol < 1. 00
Tetracn1oropneno1
p-cn1oro-m-creso1
(1,00
< 1 . 00
2,4,6Trict1toropneno1 <1.00
2,4-Dicn1orophe~o1 ~, .oo
2,4-Dimetny1pner,or <1 .oo
2,4-D·initropr,enof <1.00
2-cn1oropneno1 <1 .oo
2-Nitropnehol <1 .oo
4,6-Dinitr6-o-creso1 <1 .oo
4-Nitropt1eno1 <1 .oo
Pentact11oropt1e110J <1 .00
Phenol < 1 . 00
<1.00 Tetrac111oropt1eno1
p-cn1oro-m-creso1
2,4,6Trichloropneno1
2,4-Dichloroc11eno1
2,4-Dimetny1p11e1~01
2~4-Dinitropner101
2-cn1oropneno1
2-N it :·opi-,eno I
4,6-Dinitro-0-creso1
4-N it r·ooneno I ..
Pentacn1or6pneno1
<1.00
<. 1 . 00
< 1 . 00
< 1 . 00
< 1 . 00
<.1 . 00
< 1 . 00
< 1 . 00
< 1 . 00
< 1 . 00
Pheno I ...... . < 1 . 00
Tetracn1oropneno1
p-cn1oro-m-creso1
2,4,6Tricn1oropneno1
2,4-DiChloropnenol
2,4-Dimetnylphenol
2,4-Dinitropnenol
2-cn1oropneno1
2-Nitropnenol
4,~-Dinitro-o-cresoi
4-Nitropne~ol ....
< 1 . 00
< 1 . 00
<1.00
< 1 . 00
< '1. 00
< 1 . 00
1. 00
< 1 . 00
< 1. 00
< 1 . 00
Pentacn1oropneno1
Pheno I ....... .
< 1 . 00
< 1 . 00
Tetracn1oropneno1
p-cn1oro-m~creso1
< 1 . 00
< 1 . 00 .
~eve results are reported _in ug/L.
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL OS-5
WELL 03-6
WELL OS-6
WELL OS-6
\1./E LL OS-6
WELL OS-6
WELL OS-6
WELL OS-6
1,1/ELL 0'3-6
\V~ LL OS-,5
';/ELL OS-6
WELL •,JS-6
WELL 0S-6
·••1/E LL o·;-1
WEL~ 0~--7
'I/ELL 0S-7
WELL OS-7
WELL c,s-7
\0EL L 03:...7
WELL OS-7
WEL.L ·o,3-7
WELL OS-7
WELL C>S-7
WELL 0::, - 7
WELL 1:1s-1
WELL OS-8
WELL 0'3-8
WELL os-s
WELL. OS-8
,WELi.. OS-'3
WELL OS-8
WELL 0'.3--9
WELL OS-8
WELL os-s
WELL 0~--8
WELL 0S-9
WELL OS-8
PAGE 2
========
KEYSTONE ENVIRONMENTAL RESOURCES
=====--========--------=-=---.-----------==========
.;BLE 4: SUMMARY OF ORGANIC COMPOUNDS PRODUCED ON 12/04/86 AT 11:46
AMPLE# RSLT.LNE SOURCE
,'1860028 2,4,6Tricn1oropneno1
2,4-Dicn1oropneno1·
2,4-Dimetny1pneno1
2,4-Dinitropnenol
< 1. 00
< 1. 00
•: 1 . 00
.( 1 . 00
2-cn1oropneno1... <1.00
2-Nitropnenol.. <1 .oo
4,6-Dinitro-o-cresoi <1.00
4-Nitropnenol c, .oo
Pentacn1oropneno1
Pl,eno I ..... .
Tetracn1oropneno1
p-cn1oro-m-creso1
< 1 . 00
< 1 . 00
< 1. 00
< 1 . 00
~ave results are reportea in ug/L.
WELL OS-9
WELL OS-9
\I/ELL OS-9
WELL OS-9
WELL OS-9
WELL OS-9
WELL OS-9
WELL OS-9
WELL OS-9
WELL C>S-9
\I/ELL OS-9
WELL OS-9
PAC•E 3
========
KEYSTONE ENVIRONMENTAL RESOURCES
~,,8t.E s, SUM!"1ARY OF ANALYTICAL DATA PRODUCED ON 10/28/86 AT 07, 11 PAGE
========
"3.P.MPLE # RSLT.LNE SOURCE -----------------------------------------------------------------,fr,860020 1sopropy1 Et11er ,ug/L, <100 \I/ELL OS-1
~;NB60021 1sopropy1 Etner,ug/L, < 100 WELL OS-2
::.:NS60022 1sopropy1 Et11er, ug/L, < 100 WELL OS-3
fiti860023 lsopropyl Etl1er, Ug/L, < 100 WELL OS-4
RNS60024 lsopropyl Etner,ug/L, < 100 WELL OS-5
,=.t>:860025 lsopropyl Etner,ug1L, (100 WELL OS-6
C:N860026 lsopropyl Etner,ug/L, < 100 \1/E LL OS-7
.=-:~✓860027 lsopropyl Etner,u91L, (100 WELL OS-8
fir,860028 1sopropy1 Etner,ug/L, (100 WELL OS-9
KEYSTONE ENVIRONMENTAL RESOURCES
TABLE OF CONTENTS PRODUCED ON 11/20/86 AT 13:24 PAGE --------=============. ================== ----------------------==-==== = = == = = = =
SAMPLE#
-RN860097
RN860098
RN660099
RN86010C
RN860101
RN860102
RN860103
RN860104
RN860105
RN860106
RN860107
· ,RN860 108
RN860109
SOURCE DESCRIPT -----------------------------------
OS-1 RIFS<GROUNDWATER)
OS-2 RIFSCGROUNDWATERl
OS-3 RIFS<GROUNDWATER)
OS-4 RIFSCGROUNDWATERl
OS-5 RIFS<GROUNDWATER)
OS-6 RIFS<GROUNDWATERl
OS-7 RIFSCGROUNDWATERl
OS-8 RIFSCGROUNDWATERl
··os-9 RIFS(GROUNDWATER)
os-10-0 ~ RIFS(GROUNDWATER)
OS-10A,(.--RIFS<GROUNDWATERl
OS-1 1 -') ~<,•\-RI FS <GROUNDWATER)
os-·12-?·0 "" R1Fs<GROUNDWATERl
J c,_,.:J__f
Jc,-.,1· ; _;.•_ . l
DATE-COL --------
11/06/86
11/06/86
11/06/85
11/06/86
11/06/86
11/06/86
11/06/86
11/06/86
11/06/86
11/06/86
11/06/86
11 /06/86
11/06/86
'DATE-REC --------
11/07/86
11/07/86
11/07/86
11/07/86
11/07/86
11/07/86
11 /07/86
11/07/86
11/07/86
11 /07 /861_ f \.-;_,.....,
11/07/86 j cv.01.ru.r---· /, 11/07/86 l ,-_, ..._.._
11/07/86 ~-, ··--el-"~
KEYSTONE ENVIRONMENTAL RESOURCES
TABLE 1: SUl'<'.MARY OF ANALYTICAL DATA, PRODUCED ON 11/20/86 AT 13:27 PAGE ------------------------=----========
SAMPLE # RSL T, LNE SOURCE -----------------------------------------------------------------I_SOPROPYL ETHER
RN860097 I sopropy'1 Etner,ug/L: < 1 , 00 OS-1
RN860098 1sopropy1 Etner,ug/L: < 1, 00 0S-2
RN860099 1sopropy1 Etner,ug/L: < 1, 00 OS-3
RN860100 1sopropy1 Etner,ug/L: < 1, 00 OS-4
RN860 10-1 lsopropyl Etner,ug/L: < 1 , 00 OS-5 RN860102 1sopropy1 Etner ,ug/L·: , 1, 46 OS-6
RN860103 I sopropy I Etner ,ug/_L: < 1 , 00 OS-7
RN860104 JsopropyJ Etner,ug/L: 85,5 0S-8
RN860105 1sopropy1 Etner,ug/L: 13,3 OS-9
RN860106 1sopropy1 Etner,ug/L: < 1 , 00 OS-10 . RN860 107 1sopropy1 Etner,ug/L: < 1 , 00 OS-10A
RN860108 1sopropy1 Etner,ug/L: < 1 ,00 OS-1 1 Rl,860109 1sopropy1 Etner,ug/L: < 1 , 00 OS-12
KEYSTONE ENVIRONMENTAL RESOURCES
TABLE 2: SUMMARY.OF ORGANIC COMPOUNDS PRODUCED ON 11/20/86 AT 13:27
SAMPLE# RSLT.LNE SOURCE
RN860097
Rl✓860098
c:r,s60099
.R/✓860 100
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
2,4-Dicn1oropneno1
2,4-Dimethylphenol
2,4-Dinitropnenol
2-cn1oropneno1 ... .
2-Nitrophenol ... .
_4,6-Dinitro-o-cresol
4-Nitropne~ol ....
4Chloro3metny1pneno1
Pentacn1oropneno1.
Pneno 1 ......... .
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
2,4-Dicn1oropHeno1
2,4-Dimetny1pneno1
.2,4-Dinitropne~ol
2-cn I oropneno I.
-2-Nitropnenol
4,6-Dinitro-o-cresol
4-Nitrophenol
4Cntoro3metny1pneno1
Pentacn1oropneno1
P11eno 1 .
2,3,5,6Tet-Cl-phenol
2,4,6Tricn1oropneno1
2,4-Dicn1oropneno1
2,4-Dimetny1pneno1
2,4-Dinitropnenol
2-cn1oropneno1
2-Nitrophenol ....
4,6-Dinitro-o-cresot
4-N it ropneno 1 ...
4Chloro3metnytpnenol
Pentacn1oropneno1
Pne·no 1.
2,3,5,6Tet-Cl-phenol
2,4,6Trichloropnenol
2,4-Dicnloropnenol
2,4-Dimetny1pneno1
2,4-Dinitropnenot
2-cn1oropneno1 ... .
2-Nitropnenol .... .
4,6-Dinitro-o-cresol
4-N it ropneno 1 ...
4Chloro3metny1pneno1
Pentacn1oropneno1.
< 1. 00
< 1 . 00
<0.50
<0.50
< 1. 00
(0.50
<0.50
< 1 . 00
< 1 . 00
<0.50
< 1 . 00
0.506
< 1 . 00
< 1 . 00
<0.50
(0.50
< 1 : 00
<0.50
<0.50
•: 1. 00
< 1 . 00
(0.50
(1.00
0.734
< 1 . 00
< 1 . 00
(0.50
(0.50
< 1 . 00
<0.50
<0.50
< 1 . 00
< 1 . 00
(0.50
< 1 . 00
0.516.
< 1 . 00
< 1 . 00
<0.50
<0.50
< 1 . 00
<0.50
<0.50
<·1 . 00
< 1. 00
<0.50
< 1. 00
Pl1eno1 <o.so
Above results are reportea in ug/L.
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-2
OS-2
OS-2
OS-2
OS-2
OS-2
0S-2
OS-2
0$-2
OS-2
OS-2
OS-2
OS-3
0:5-3
OS-3
OS-3
OS-3
OS-3
0S-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-4
OS-4
OS-4
OS-4
OS-4
OS-4
OS-4
c~S-4
OS-4
OS-4
OS-4
OS-4
PAGE 1
========
KEYSTONE ENVIRONMENTAL RESOURCES
==================================================
TABLE 2, SUMMARY.OF ORGANIC COMPOUNDS PRODUCED ON 11/20/86.AT 13,27
SAMPLE# RSLT.LNE SOURCE -----------------------------------------------------------------RN860101
RN860102
hi-.J°860 103
RN860104
2,3,5,6~et-c1-pneno1
2,4,6Tricn_·1oropheno1
2,4~Dicn1oropneno1
2,4-Dimetny1pneno1
2,4-Dinitropnenol
2-cn1oropneno1 ...
2-Nitropnenol
4,6-Dinitro-o-cresol
4-Nitropnenol ....
4cn1oro3metny1pneno1
Pentacn1oropneno1 ...
Pt1eno I ... · ..
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
2,4-DiChloropnenol
2,4-Dimetny1pneno1
2,4-Dinitropnenol
2-cn1oropneno1
· 2-N it ropneno r .
4,6-Dinitro-o-cresol
4-N; t ropneno 1 .
4cn1oro3metny1pneno1
Pentacn1oropneno1
Pneno 1.
2,3,5,6Tet-c1-pneno1
2,4;6Tricn1oropneno1
2,4-Dicn1oropneno1
2,4-Dimetny1pneno1
2,4-Dinitropnenoi
2-cn I oropneno I ••
2-Nitropne1101 ....
4,6-Dinitro-o-cresol
4-Nitropnenoi
4Cn1oro3metny1pneno1
Pentacn1oropneno1.
Pneno1 ........... .
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
2,4-Dicn1oropneno1
2,4-Dimetny1pneno1
2,4-Dinitropnenol
2-cn Io ropneno I .
2-N it ropneno 1 .
4,6-Dinitro-o-cresol
4-Nitropnenoi ...... .
4Cn1oro3metny1pneno1
Pentacn1oropneno1.
Pnenol
< 1 . 00
< 1 .·00
<0.50
<0:50
< 1. 00
.<0.50
<0.50
< 1 . 00
< 1 . 00
<0.50
< 1 . 00
<0.50
< 1 . 00
< 1 . 00
<0.50
<0.50
< 1 . 00
<0.50
(0.50
< 1. 00
<. 1 . 00
<0.50
< 1 . 00
<0.50
< 1 . 00
< 1 . 00
(0.50
<0.50
< 1 . 00
<0.50
<0.50
< 1 . 00
< 1 . 00
<0.50
< 1 . 00
<0.50-
< 1 . 00
< 1 . 00
<0.50
<0.50
< 1 . 00
<0.50
<0.50
< 1 . 00
< 1. 00
<0.50
8.82
. <O. 50
Above results are reportea in ug/L.
OS-5
OS-5
OS-5
OS-5
OS-5
OS-5
OS-5
OS-5
OS-5
0S-5
OS-5
OS-5
OS-6
OS-6
OS-6
OS-6
OS-6
OS-6
OS-6
OS-6
OS-6
OS-6
OS-6
OS-_6
0S-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-8
OS-8
OS-9
·os-s
OS-8
OS-8
0S-8
OS-8
OS-8
0S-8
0S-8
OS-8
PAGE 2
========
KEYSTONE ENVIRONMENTAL RESOURCES
TABLE 2, SUfv\MARY OF QRGANIC COMPOUNDS PRODUCED ON 11/20/86 AT 13,27 -------=----======-----=----------------
SAMPLE# RSLT.LNE SOURCE -----------------------------------------------------------------RN860105
RNS60106
c<!,860107
RN860108
2,3,5,6Tet-Cl-phenol
2,4,6Trichloropnenol
2,4-DiChlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2-Chlorophenol ...
2-N; tropheno 1 ..
4,6-Dinitro-o-cresol
4-N it ropnerio I .
4Chloro3methylphenol
Pentach1oropneno1 .. .
Phenol ........ .
2,3,5,6Tet-Cl-phenol
2,4,6Trichloropneno1
2,4-Dicn1oroprieno1
2,4-Dimetnylphenol
2, 4-D in i t rophe·no 1
2-Ch I oropheno I .
·2-N i tropheno I.
4,6-Dinitro-o-cresoi
4-N it ropheno 1.
4Chloro3metny1pneno1
Pencachlorophenol
Phenol
2,3,5,6Tet-Cl-phenol
2,4,6Trichloropnenol
2,4-Dichlorophenoi
2,4-Dimetnylphenol
2,4-Dinltrop11eno1
2-Ch I oropheno I .
2-N; t ropheno 1 .
4,6-Dinitro-o-cresol
4-N it ropheno I .
4Chloro3methy1pneno1
Pentach1oropheno1
Pheno I ..
2,3,5,6Tet-Cl-phenol
2,4,6Tricn1oropneno1
2,4-Dichloropnenol.
2,4-Dimetny1pneno1
2,4-Dinitrophenol
2-c111 oropheno I
2-N it ropneno I.
4,6-Dinitro-o-cresol
4-Nitrophenol ..... .
4Chloro3metny1pneno1
Pentach Io ropheno I : ..
Pheno I.. . .
< 1 . 00
< 1 . 00
(0.50
<O c50
< 1 . 00
(0.50
<0.50
< 1 . 00
< 1 . 00
(0.50
< 1 . 00
(0.50
< 1 . 00
< 1 . 00
<0.50
(0.50
(1 .00
<0.50
<0.50
< 1 . 00
< 1 . 00
<0.50
< 1 . 00
0.632
< 1 . 00
< 1 . 00
<0.50
<0.50
< 1 . 00
(0.50
(0.50
. < 1 . 00
< 1 . 00
(0.50
< 1 . 00
0.823.
< 1 . 00
< 1 . 00
<.0.50
<0.50
< 1 . 00
(0.50
<0.50
< 1 . 00
< 1 . 00
(0.50
< 1 . 00
(0.50
Above results are reportea in ug/L.
05-9
05-9
05-9
05-9
05-9
OS-9
05-9
OS-9
05-9
OS-9
05-9
OS-9
OS-10
OS-10
OS-10
OS-10
OS-10
OS-10
OS-10
OS-10
os-10
OS-10
OS-10
OS -1 0 ::.., c, r .~-·
OS-10A
OS-10A
o·5-10A
OS-10A
OS-10A
OS-10A
OS-10A
os-10A
OS-10A
OS-10A
OS-10A
OS-10A
os-11
OS-11
os-11
Os-1 1
OS-1 1
OS-1 1
OS-11
0S-11
0S-11
0S-11
0S-11
OS-11
PAGE 3
========
f:EYSTONE ENVIRONMENTAL RESOURCES ----------------------------.---------------------
°"7".'\BLE 2, SUMMARY_ OF ORGANIC COMPOUNDS PRODUCED ON 11/20/86 AT 13,27
SAMPLE# RSLT.LNE SOURCE
ciN860109 2,3,5,6Tet-c1-pneno1
2, 4, 6Tr icn.1 o ropt1_eno I
2,4-Dicnioropnenot
2,4~Dimetny1pneno1
2,4-Dinitropnenol
2~cn1oropneno1 .. .
2-Nitropnenol ... .
4,6-Dinitro-o-cresol
4-Nitropnenol ...... .
4Cn1oro3metny1pneno1
Pentacn1oropneno1 ...
Pneno 1.
< 1 . 00
< 1 . 00
<0.50
<0.50
< 1. 00
<0.50
<0.50
< 1. 00
< 1. 00
<0.50
< 1. 00
<0.50
~cove results are reportea in ug/L.
0S-12
05-12
OS-12
OS-12
os-12
os-12
OS-12
OS-12
OS-12
os-12
OS-12
OS-12
PAGE 4
========
.... ·.,•••''·""-•'•··•·••· ·:···•···•••• .. • .. •···•••••••···••·· ............ ,.•••-•·········--····-·-·•····· .. ·,, ...... ,,,·-.-· l \ L.J" UI\ I WU/'K UJ'Ut'I' lf tJo-11-v1t1 Received: 11/07/86
REPORT Keystone Env. Resource Inc.
TO Water Quality Enaineerino
440 College Park Prive
Monroeville, Pa. 15146-1536
ATTEN R. D. Hepner
CLIENT KEYSTONE ENV SAMPLES 20 COMPANY Keystone Env. Resource Inc. FACILITY
WORK ID Water/Sediment
TAKEN Client
TRANS Federal
TYPE Water/Sediment
P. D. # R~6_-=2-'4~1~5 ___________ _
INVOICE under separ~tg cover
SAMPLE IDENTIFICATION
Q.!_ OS-1
02 OS-2
03 OS-3
04 OS-4
Q;i_ OS-5
Q6 OS-6
07 OS-7
08 OS-8
09 OS-8 MS
!Q OS-8 MSD
ll OS-9
12·DS-10
ll OS-11
1.1. OS-12
12 Inlet Medlin Pond <LLS) .LJ? Dtsc~~rge Medlin Pond (LLS
1..Z. Sa!f' ',o.,_....,K~i,._t=--------1.!1 !>' '""ti~i~t ______ _
1 9 · "'-c' t=--------~~ ·, ,
11/21/86 16:24:31
PRE-'ARED !:l.P-.!li .. .t.r.-1 .. x Corporation
DY ;3c111 Fondre
Syi te 100
Houston, Texas 77063-5821
ATTEN Sample Control
PHONE [phone]
CERTIFIED BY
CONTACTC ~~B~v~z ___ _
Please call the aboye number if you have ani1 questions. NOT_E: ALL SAMPLES WILL BE RETAINED FOR 90 DAYS AND THEN DISCARDED. IF YOU WISH YOUR SAMPLES RETURNED TO YOUR FACILITY CALL SAMPLE CONTROL AT THE ABOVE NUMBER. .
r,111 I '-'1-' -..v," ,.,, • I
11/\IER 1-111rn1x SPIKE/ IIIIIIUX SPIKE UUPLICAI[ RECOVERY
1/ork Order#: 86-11-010 Contractor·: SP£CTl!IX CORl1JRATION Sile: _KenJ.o~□=e~----
FRACT !UN
VUA
SN-IPL[ NU.
NA
. U/ N
SAMPLE NO.
NA
ACID
SA11PL E NU.
OS-8
PEST.
SAMPLE NU.
Nil
COI-IPUUNO
1,1-0fchloroethene
Tr1chl oroethene
Chlorobenzene
Toluene
Benzene
1,2,4-Trfchlorobenzene
Acenaphthene
2.4-0fnltrotoluene
Pyrene
N-Nltroso-Ul-n-Propylamlne
1,4-0fc11lorol,~nzene
Pentachloropl1enol
Phenol
2-Chlorophenol
4-Chloro-J-Methylphenol
4-111 trophenol
LI ndane
lleptachlor •
Aldrin
Uleldrln
Endrln
4 ,4' -OUT
• ASTEl!ISKEO VALUES ARE UUTSIIJE l)C LIM] rs
CONC. SPIKE
ADDEO (ug/L)
NA -Rr ----__/j!!_ __ NL
NA
100 =r@= 100 =1og=
_!00 __
11/1
NII -Nil--Nii __ _
NII
Nil
SAMPLE
II ESULf
NI\ -nr
_UL
_li!!_
_ill)_
Ill\ -ri/i-
_JJ/L_
__ Jlfl_
__ CT!!_
__ )'I[\_
_Q__ __ o_
_Q_
_Q_
0
COIJC.
MS
NI\ -nr ---
NII
_NII_ _w:x _
NII
NII -Nii-
i
REC.
NII NA
__JJ{L_
Ill\
NA
NII ---1111
_ /UL
NI\
NII
N/1
COIIC.
11S0
NII
NII
_ljtl__
_ljtl__
NA
NI\
.JUL_
_ljtl__
_JJ/L__
_M __
NI\
_]J_
_J_z_
_Ji9__
__!i.L_
02
NII
NII
_NIL_
NI\
NII
NA
i
REC.
NII
7i11-
_N8 _
_NL
NA
NII
J[L_
_NfL_
_fl/\_.
_ NiL_
J/L_
__ 23 __
_]2 _
-1,9 _
__5.9__
02
~[!__
NII
J{L_
NII
__!!LI_
NA
ltPU: VUAs N/1 out or s·; outside QC llrnfts RECOVERY: VOAs NII out of 10; outside QC limits
U/N --w.-out of 7T; outside QC 1 lmits
ACIO ---U out ur 711; outside QC I lmlts
PEST -llA out of 7T; outside QC 1 lmfts
B/N NA out or --i;-; outside QC 1 l111l ts·
ACID ---u-out or -Y-; outside QC limits
PEST 7171 out of -.;-;· outside QC ·l lml ts
Canments: Nil• Not Applicable
RPO
NII
NI\
__l/8._
_/j/L....
__l/8._
NII
_/j/L._
_N/L..
_Jj/L_
_NIL_
NA
Jq
QC LIMITS•
RPO REC-REC
14
14
13
13
11
28
JI
38
31
JO
28
61-145
71-120
75-130
76-125
76-127
39-98
46-118
24-96
26-127
41-116
36-97
50 · 9-103
42 12-89
40 27-123
42 23-97
50 · 10-80
NI\ 15 56-123
40-13 I
40-120
52-126
56-121
38-127
. JL · 20
_tl.8__ 22
NA 10
NII 21
N/1 27
pl<'(• I":
/'" (.)\ /1 l' \ , I .-----·
ORGANICS ANALYSIS DATA SHEET
ACIDS
Laoora tory Na.me: Spee tri x Sample Number: OS-I
Lao Sar.ipl e ID No.: Jb//o/8"CJ/
Data Rel ease Authorized By~~
Concentration: Low·
Samp 1 e Matrix: Wa. ter
Date Sample Received:
Units: ug/L
Date Extracted: // /7/.P-£ Cone/Oil Factor: / ---'--------'--,£, '--.J....C....:..=..--
D ate Analyzed: // ,//;.../J>b ----,1., :.....:.~L-~--Canpounds Detected:
NPDES #
10A
IA
oA
3A
2A
dA
lJ.A .. .OA
IA
4A
9A
CAS #
108-95-2
10:,-01-':,
i 20-83-2
88-0o-Z
ol-28-o
100-02-1
534-oZ-I
81-36-:,
COMPOUND
P heno 1
2-l..nloropnenoi
t.-Nl tropneno 1
c,4-01metnypneno1
2 ,4-D,cn1 oropneno1
p-l..n1oro-m-cresol
t.,4,o-1r1cn1oropneno1
2,4-D1n1tropnenol
4-Ni tropneno I
4 ,0-D1 n1 tro-2-/1,ethy I pneno I
?entacnloropnenol
U = Undetected at the 1 i sted detection 1 imit
J = CCC:Jpound is present, but below the listed detection limit
8 = Compound also found in blank
0
10 u zu 0
10 0
10 U
10 0
iu u
50 U
:,0 0
:,J u
50 u
5,.:.;-,F L~ : :
CALI3 STD ~ATE
SPECTRIX DC # ----1~
SE~IVGLAr!LE WATER ·RE?0RT
SS-1
11/12/86 17: 55: 00
11/7/86
INST ID.
ANALYST
VERIFIED BY
CORR. FACTOR
4530
YPH
1. 00
---------------· ----------------------------------------------------------------SCAN# SE:-1I '/OLA T IL£ COMPOUNDS AMOUNT RRT --------------------------------------------------------------------------------497 CIJO 1, 4-DICHLORCBENZEND-C4 *" IS1 ** 152 40 UG/L 1. 000 3513~
711 CI 40 N,',PHTHALENE:...oa ..... IS2 ** 136 40 UG/L 1. 000 122.;:,J.: 1005 CI 5.J ACEN,',?HTHENE-D10 , .... IS3 ** 164 40 UG/L 1. 000 6383: 1244 -: r 6,J ?HENANTHRENE-DlO ** IS-+ ** 1S8 40 UG/L 1. 000 6.lC,2•: .. ,..., . -:r7o -:HRYSE~/E-D 12 ...... •-c .:. cio .. .i,. =-...,. ... .. 240 40 UG/L 1. 000 1 ss-s;;
..!. ·"OC,C· -: I 75 ?E:iYLENE-D!2, ...... ·c . l~O "* 264 40 UG/L 1. 000 ';4:5( .:;:so ---c., 2-:'"l... 'JO?.CP HEN CL *~ ·3L'" ...... :2 36 ., 0. 581 .. ::;;c 51: ~ --=-\.; ' ,. , . -,: 3.15 ?HENCL-DS ** SV2 -<-,c 99 ~-., 0. 936 1 ·J: :;: . ..1:: "'!'C;:) .'0 , .
:36 ,: S 5:; " 4, ,',-TR I 3RC'~CPHEclCL ** SU5 ** 330 J6 . , 1. 130 64-=-.. ~, ,.
'5~7 ·,:s21:• \l: ·:RC.I3£NZ~l'iE-D5 <H· Si,_;3 """ 22 34 ., 0. 840 Jc2;.;.:
'7 () :3 -:s2s 2-~LUUORDBI?HENYL ... .,, SU4 ** 1 7'1 77 1/. 0. 899 .. -..-,,-,. , ~ J.. "'1' -:e.. = ~ =·1 '7 =:SJO 7~R?HENY~-D14 ,:S..-~ SU6 <>-> 244 160 1/. 0. 904 1 ..... _, --"'1-.:...~/ :,723 1:7:35 3!S(2-~T~YLHEXYL)~H7~A~ATE :':.49 ! . UG/L 1. 025 6?;::
~-,//} !.:.u~ .-
.----\----
-· I
I I
I
#
u
0
Y,
0
fl.
'" rl
100.0
PIC:
RIC
11112/86 17:55:00
SAMPLE: 05-1 cot IDS. : ---
RAtlGE: G 1,2400
onrn: 4Ull018A01 ttl
CALI: 4U11018AOI tt3
SCfltlS 200 l f.l 1350
LhP.EL: M 0, ,1. 0 p1_1n11: A 0, L 0 .J O BASE: U 20., 3 903
,I I
465
497
l
1005
1000
lio:'1 1)
1244
113G
I
I 1 o,t \ __ ,_.,.....-J...:,,..-,.--
1200
2i}: 00
148224.
SCAll
TIME
..
u
C-l
X
H
n:
I-
'·' IJJ
CL
UJ
() ..
100. 0
F'IC
RIC UAl/1: 4U11018A01 ttl
cnLI: 4U!l01Bn01 HJ
5CA1i5 1350 Tll 24(11)
ll/12.-86 17:55:00
Si1t1PLE: 05-1
(01105.: ---
Rf➔I IGE: G 1, 2480 LABEL: ti IJ .. 11. 0 QUAIi: A 0, 1. 0 .J O BASE: U 20, 3
40896 1519
I
I J:::0 l ·153 \ I 1320 -· -1~· ·---,·-· ... ·---T--.
1400 1600
23:20· 26,40
1681
1300
J \\_J _ELc~ _J __ _,_3j-;...04_· ~-}~!!2 .. ~---2-!?.L.~,.:;c.;-.::"""e.;.3~~2_35~6;.... .... _
.. . .----·,· ............ -.. --T·------~---,---------.~---~---"-,
1er,o . 2800
33:20
2:00
31:-: ,10
2400 SCAH
40: 00 T IIIE
ORGANICS ANALYSIS DATA SHEET
AC!OS
Laoora tory Name: Spectri x Samp 1 e Number: OS-2.....
Lao Sar.ip1e ID No.: ,?t//o/?o::i-
Data Release Authorized
Concentration: Low
Date Extracted:
Samp1 e i-tatrix: Water
Date Sample Received:
Units: ug/l
Cone/Oil Factor:
Canpounds Detee ted:
I
Q
NPOES # CAS 4 COMP<JUND RESULT
lOA
IA
oA
JA
2A
dA
u.A
oA
IA
.,.;i:
:, A
108-95-2
1uo-o, -9
Ic0-83-2
08-0o-Z
~1-28-5
100-02-)
o34-o2-l
8)-36-o
? he no 1
<'.-L.n I oropne~o I
,-tn :.ropneno 1
2 ,4-01 en I oropneno I
p-Ln!oro-m-creso·1
2,4-01n1tropneno1
4.-t-tl tropnenot
~.o-01n1tro-Z-Metny1pneno1
?en tac n Io ropneno 1
U = Undetected at the listed detection l irnit
J = Canpound is present, but below the listed detection 1imit a = Compound al so found in til ank
10/8S ( 1,AnAW?\
10 U
Io u zo u
10 0
10 U
10 0
10 u
50 U
50 u
SAMPLE ~=· F:L:::NAl".':E CLIENJ DATE I:l~'E-:"TED C~IB S"TD ~ATE SPECTRIX DC# ----14 SE~:VCLAT!LE WA7E2 ·RE?CRT ·os-2 4Ul 1018.'102 )..(_EYSJCNE 11/12/86 18:46:00 11/7/86 INST ID. 4~30 AN.'ILYST YPH VERIFIED BY ';Jf7?/ CORR. FACTOR 1.00 ----~---------·-----------------------------------------------------------------SCAN# SEMIVOLATILE COMPOUNDS M/E AMOUNT RRT ARE . .; ------------------------------------------------------------------------------·· 498 Cl30 1,4-DICHLOROBENZEND-04 ** IS! ** 152 40 UG/L 1. 000 3762~ 712 C140 NAPHTHALE:NE-DS ** IS2 ** 136 40 UG/L 1. 000 1360 =·" 1005 CI 50 ACENAPHTHENE-DlO ** IS3 ** 164 40 UG/L 1. 000 7024...: 1244 CI60 PHENANTHRENE-DlO ** !S4 ** 188 40 UG/L 1.000 7550~ !682 c:;o CHR YSENE--cD 12 ** IS5 *" 240 40 UG/L 1. 000 12~8~ ! 9C1J -":"-:-,;;: ._,_,_; PE',YLENE-D!2. ** ,-· • :io ..... 264 4G UG/L 1. 000 ~ec.:: 293 -.::se,) 2-Fl..UORCPC.:ENOL """ SUl ~-1-1 ! 2 83 Z. 0. 588 62,'57'C 4-67 cs .. 1,s PHENOL-05 •• SU2 *·+ 99 75 'l. 0. 938 1 :)3c; 5: 1 ~ ., . ,:s=5 2, 4,6-TRIBROMOPHENOL ... * SUS 4* 3:30 45 'l. 1. 13G ·=':.-;;• -..L...:0 59S . :-::::::-r1 ,'Ji Ti'<OBENZENE-D5 ** SU:J ...... ~~ 72 i: 0.840 3457'. :::.:;.;. 903 •= s:;: s 2-FLUUOROBIPHENYL ,...,, SU4 ** 172 6 7 'l. .o. 899 "T -: ;' "':'--: -... _,, -· ....... ~ 51 9 CS:30 TEi'<P!-iENYL-014 *-.} SL;6 ...... .., , ' e.~"1' 136 :~ 0.903 33C~-:
.x
" er f-u
lll
IL
UJ
100.0
PIC Dilrh: 4IJ11018fi02 ff!
COLI: 4U11018h02 tt3
SCAHS 200 TO 13:,0
11112186 18:46:00
5(lMPLE: 05-2
COIID5. : ---
PAI IGE:. G 1, 2400 LABEL: tl 0, 4. 0 @JAIi: i1 0, 1. 0 ._I 0 BASE: U 20, 3 903
293
4f.7
438
= ~ ~l-=--~-:-=-;:,~1=,_1,_.:::,.-'.:::o•'-=>-r-~ ~··:'.'.:=. --.~·y l,_J
200 400 i::oo :J;:20 6;,JO l(l;(HJ
.. I
81Jl)
13:20
87'0 · I ,_
1000.
t[.:•10
1136
1244
I
1200
20:00
1320
I
16742•
SCAt1
TIME
#
u
Q
(l'.
f-u
~I n.
l/1
0 · r1 ,,
'1
100.0
RIC
11,12186 18:46:00
51)I1f'LE: 05-2
COIIOS.: ---
P.AIIGE: G 1, 2400 1513
onrn: 4u11010no2 ttl
C(tl.l: •IUl 1018i"l02 H3
SCAMS 1350 TO :2400
LABEL: II 0., 4. fJ (11./flll: 11 0, I. 0 J O . BASE: U 20, 3 ·
2857E
ORGANICS ANALYS[S DATA SHE~T
AC ros
Laooratory N~ne: Spectrix Samp1 e Number: OS-3
Lao Sar.ipl e ID No.: ,?b//o/?tl3
Data Release Authorized ay~-c::~ r-
Concentration: Low
Date Extracted:
Date Analyzed:
Sample Matrix: Water
Date Samp1 e Received:
Units: ug/L
Cone/Oil Factor:
Ccmpounds Detected:
I
o·
NPDES "-,r COMPOUND RESULT
lOA
LA
cA
jA
2A
Of\
uA
~A
IA
4A
9A
108-95-2
.!.V~-o,-9
l 2u-d3-2
88::Uo-Z
100-02-1
534-~2-1
di-36-~
?heno l
2-\..n I oropneno i
t..-N1 :ro\:)neno 1
c.. ,4-Q, en t or'.)pneno I
2,4,o-1r1cn1oropneno1
2,4-D1n1tropneno\
il-Nl -cr·opneno 1
4,o-J1n1:ro-Z-Metny1pneno1
?entacnioropnenol
U = Undetected at the listed detection limit
J = Coopound is present, but below the listed detection limit a = Compo_und al ~o found in :il anic.
,n,~c: /1"'1,'\n.,.,,,..,,
10 U
1.0 u
20 0
10 0
10 U
10 0
to u
50 U ~co ~o a
50 u
S;..r--.PL.£ : : FILSN~i~E CLIENI S?ECTRIX DC W ----1-1 SE~IVCLATILE WATER .REPORT ·•:JS-3 4Ul 1018A03 i-'.EYSTONE INST ID. ANALYST 4530 '<PH L'ATE j;",_,:E.:JED 11/12/86 !C:38:QQ VERIFIED BY pn CORR. FACTOR CAL!E 37:) DATE 1~/7/86 1. 00 ----------------------------------------.--SCAN# SE~IVOLATILE COMPO~NDS M/E AMOUNT RRT AR~ . .:, ----------------------------------------------------------498 -:r30 1,4-DICHLOROBENZEND-D4 ** ISl ** 152 40 UG/L 1. 000 4-:,0.:1~ 711 •: I 40 NAPHTHALENE-DB .... IS2 ** 136 40 UG/L 1. 000 1-lB::::J:: 1004 C!50 ACENAPHTHENE-D10 ** 1S3 ** 164 40 UG/L 1. 000 75565 1.., . '""I ~.,__, CI60 ?HENANTHRENE-D10 ** !S4 ** 188 40 UG/L 1. 000 99141 1680· ,: I 70 •:HRYSENE-_D12 ** IS5 ** 240 40 UG/L 1. 000 .., ...... , .. .... ...;i"'!-t::...~ 12~9 C"I75 ?E.~YL..S:'JE-D.12 ** l'SC ..... 264 40 VG/L 1. 000 ~ ,-..-. --.1.~,~~ 'r-:::' c:. ~," ,:=:=0 2-FLUORGPHENbL ** SU! *·~ 112 82 t. 0. 592 774::5~ .;.::;o 1:=.4 5 ?HEl~CL-DS ** SU2 44 99 74 1/. 0.936 1 ! • ..,. -~ ..,_,1,.0✓_,.. • , --:.c:; -~S55 2, 4,6-TRIBROhGPHENGL ,H> SLJS ** 330 53 1/. 1. 130 ! : 7~c >-----c~~ . ,:s:;:,J N!TROEEN:ENE-05 •• 3U'.3 *~ 82 75 1/. 0.840 ..,,... __ .-. -7 ' ~ 7.:::. ::,, .... 7c,.;:: .,: s~ s· 2-FLUUORGBlPHENYL ~~ SU4 ** 1 --, 68 1/. 0.898 15507: 1~ ~-:. ~ 8 ~S:JO TERPHENYL-D14 ~4 SU6 <H> 244 135 1/. 0. 904 5-::;90( ..... ,.........., C7::.":5 BISl2-ETHYLHEXYL:PHTHALATE 149 1 UG/L 1. 025 1 .J,:;~ -, =..::::. '
1" ....
I
I
I
I
#
u 0
>< -rt'. ,_
u w
"-[0
rl •-•
1--
1/l 7.
100.0
RIC
RIC
11,,12,,86 19:38:00
SAMPLE: 05-3 cot ms. : ---
RAt!GE: G 1, 2400
DAiA: 4ll!IOIBA03 NI
CALI: 4Ul1018A03 #3
SChtlS 200 TO 13':,0 ·
UlBEL: H 0, 4. 0 l_jlJ11tl: A 0, !. 0 J IJ BhSE: 1J 20, 3 902
71 I
466
537
t243
1135
295
__ Jl_ =-----'7;',=c.~-=-cL::.'.:,_'::::·--:--0= ==1..;'··::..::-'·., ___ · ... ~,-l·~A==··.,.. ~---8_b':l"-I .:::c--4~»------,.-_.t._-""'---,---'...:,l_...-_
liJOO
16:40
1200
2f): 00 200
31 jl;)
foi.1(1
lf:l:(H.\
8(1')
I:) I ,:1)
174592,
SCAtl
TIME
#
u
Q
X -Ct: I-
fJ w
CL
(n
C> n •• ~
I -
UI
''
1(10. 0
RIC
P.IC Dnrn: '1Ull018fl03 lll SCAIIS 1350 TO ,:400
11,12186 19:38:00 cnL!: 4Ul!Ol8A03 tt3
SA~lPLE: 05-3
COIIOS.: ---P.f!IIGE: _ G I, 2400 LABEL: II 0, •1. 0 Ol/(lll: A 0, !. 0 J O BASE: U 20, 3 ·
1518
lf.80
( _ 16-1() I?/.<
1-1~. I '· I r,:n l \ J I ::<ij:3
f.c-e-c_-_ ~, ~--~~c=-r,,c-,c_ .:ec--c.~-<~-~------:.r' -~=--·------(·"'•'-""'-
1-l(ll) lf:-00 I :,:(nf
?:-:; : ,:O ;:-1;-,.10 :f1 I I.,,
1899
;-oi:,ri
n: ;:o
--,-----
?:?(tf)
:}(~: ,p)
5408(
2•100 SCAII
•10: 00 T lilE
ORGANICS ANALYSIS DATA SHEET
ACIDS
Laoora tory Nairie: Spectri x Sample Number: OS-t.f
Sample i-latrix: Water Lao Salilple ID No.: J£//o/?P,;L
Data Rel ease Authorized By~~ Date Sarll?l e Received: 11 /7/2(
7
Concentration: Low
Date Extracted:
Date Analyzed:
NP!) C:S "ff
lOA
i.A
oA
~A
2A
On
UA .. :,,;
IA
-+A-
9A
CAS #
108-95-2
9:,-:,/-d
od-/5-:i
1uS-o,-~
Izu-83-2
88-0o-L
:,1-28-~
100-02~1
:,34-:iZ-J.
d/-36-:i
COMPOUND
?he no 1
2-1...ntoropnenot
~-Ni ~ropneno 1
Units: ug/L
Cone/Oil Factor:
Ccmpounds Detected:
c,~-J1metnypneno1
2 ,4-0icn t oropneno I
µ-1..n I oro-m-creso J
Z,4,o-1r1cnloropneno1
2,4-0initropnenol
4-ili tropneno I
4,o-il1n1 cro-2-Metnyipnenal
?encacnloropneno1
U = Undetected at the listed detection limit
J = Ccrnpound is present, but belc1>1 tl1e listed detection limit
B = Compound al so found in blank
I
0
RESULT
10 U
10 u
20 0
lG 0
10 U
10 0
10 u
50 u
50 0
:,0 u
50 u
', "' ,~ ... -Ill I 0 tJ n 11 in
'-I rn ·lJ Ul .. /• l•J (IJ O· f'J <.) '4 4• n I ~ ]> r· H l>
ri ,_ 0 "' l,J O· -1) ·-0 (/) .,. 0 .... -J) ), I -l H r· :I
l•J [J) ... u--" U1 r•.1 m 0 rJ w o '4 2 I H n1 in Ill 1)
# I' t.1 z z· ,-
I r• ··l J> ,n .-, t-> Cl .. , ~-, f") c, \·;, CJ tJ \-> () ,, I u, .. , 3 ,.
'I ff) (J) (JJ rn {rl IJ I H ..... J-f •-1 ~-◄ ... I ··I C IT1
IJ l,l r.J l•J ln ,.. '" ·• l ·.J r,-en -~ L.l I 0 IT1 I)
IJ, 0 Ui (J {fl (11 0 Ul l) (J 0 0 0 I ()
I t:) -l
I :t, in
w -i h..1 .• (•.) "f, j,j u .-. ,_, :r, 2 .... I -I tJ
H ill I ... T I Ill 1: I O J, I Ill
Ill :.u 11 ·-I .Jc, rn 11 ;o :u rn n1 " .,. I.
.--. .1) 1--:u . ::: r·• -< -< L 2 I I I
ru :i: en (I· Q C: r (/) l, l> -l 0 (I) I
I fll C "' I 1-· 0 fll 111 z " I H IT1 I
Iii 'L. 0 /fl -i I ::n L. z -I :i: :r, n :1 I •• , .. :,.: ... Cl ~, -< ::0 z :o t:J O IT1 ITJ I --i r :r: H I •• , . n, C: U1
:r: ,-a ,., ,., ,_n " I J :u I 1n r .::: I ., .. -< .... I
-~ I tJ ITI w :c O tJ ITJ fll z a L7 ·1 ·-.J .... (fl ·-+>
r· (:J ... z :u .. n1 , ......... z 2 ITl :U r I ' IU -~ 0
I , .. 11 fll Cl •• z IJ l'.J ITl fTl I 0 :r, I . (ll ' (] ....
ITJ t.. I I ::I 0 I I 0 lO ., ()'-ID •;, (J)
X fll tJ 0 u·, r *· * OOCDfTI •• ()'-iii ], u.,
-: 2 tn ·o C * * .... .... z r 0 Ill ,-• ·• . :I: ;\J ,. 00 1-J IIJ l<l t-:.<
.\ ,--~·-rrl .--:-. H ... ,, Tl] 0 . H ,_, .,. ~:.: *· l.fJ U) * z n
:r. o1 * r:i * ti, O· ,.n * * tJ 0 l<J 0
•·l C *· "' r C * * H I ::I ·O r
I O· C .... * * Ul 0 " ],
). 1/1 U • 4 H H ftj .l,:. L1 0 -j
r * C * * UJ l/l C 0 .l·f
}> * +> * .;. t. .J. l.l * * z 1-
··i 4 * * tJ ill n, * lll * * lll
~' C * * H £
U1 [/) )> .... I -j
* I rn
* * . I ;o
* I
I :u
I ill
I 1J .... I\J,... lJ ... 11J 11J ~· ,. .... ... ::I I n (lj .,:. "' '·J (JJ (.l -0 H (l-.pOJO·WUI '• I ;rJ 11
•I] t.. ~) PJ O ·-0 rJ ./-0 CO .I> 0-IU I~ I -l Ill
I n < ]> H n
I CJ fTI 2 z -l
I :u :o ]> (I) ~)
I ;o H r -I ,.
I 11 ., ,<
], I ,_, Ul H .... 3: I Tl Ill -l tJ tJ
r,. -..,m ,.. ri) -.0 .t, .,. .i,. -1, .,. .,. 0 I :r, l:) .-,
.i,. O· U1 r.i ··-J -f~ .... 00 0000 C I n z I -l tl:J ,.
C :...: ;-~ ,. ;-.!~~:---:CCC CCC --i I 0 -< " 0 O')<i)G)G:)00 ::0
----
'· .............. ,,
----) r r rrrrr I' ... ..
-. 0 0 0 ....... 0 0 •-... .... ... ... ... -< .J>
::0 " U1
o -{) rn u:, ... -JJ U1 0 0 0 0 0 0 ;o :r: LJ
~J0'1JWWWCOOOOOOO -l ... 0
U1 +' ro --0 .... Q,(0000000 0 I) ... ... ... ~-,.n l-11.1 W ._... IU '-J •..J ..J.;. .i.,. :,.
ru u1 -o (1 ·O ;_n f.) () 0 CJ 11.J O 0 )]
r.n (.J f.,l 11) 1.11 1,)•1010· ... ()'-,.1 [.) Ill
/1_1 r1:1 ,;; c, (.J '" .i .. PJ I•• ·{) .l:. J:.._C, J, I.
'. .. ' ,. , .. " '" ·I,-·, ltl, n ,, ... "
't ...
I I
I I
#
u
Q
>< ...
c,:
I-
IJ w n.
1/l
'I
I·
Ul ,_ ...
100.0
F'IC
RIC
I l/12,•86 20:2:3:00
S{1MPLE: 05-4
cot 1Ds. : ---
p11t !GE: G 1, 2400
292
D1ilh: .-11.Jt 1018(104 ff!
CALI: 4Ull01Bn04 ff3
SCAIIS 200 TO 1350
LA8EL: ti O .. 4.0 (l!Jf)tl: h 0, 1.0 J O BliSE: IJ 20., 3 301
110 10(.1.3
1S5
43i'
1242
JI 1.-1
I
;,,._l-~1=~ I,,. l. . 11:,,•.~· ... ~. ,1,L-T' __ __;,~1.:, =----1-·0o,··-.........;1.:..:1,o..:..J3 ILl''---,,,_.---Jj~~--
1000 1200
20:00 2,,0 ,1011 i;nn 1)00
6:-10 l•):11,:, .1 J:}.l) .3: 20 I 6: ,10
195072.
SCAH
TIME
\1·
~
I I
I I
#
,_,
0
,,: ..
ll'.
f-
IJ
Lil
(l_
lJl
0
(')
"' -r
'. u,
2 ··•
100.0
F:lt:
Jl-!2,8G 20:29:00
S1~MPLE: 05-4
COIIDS.: ---
P.1\tlGE: G I, 2400 1518
UllJEL: t·I
1680
un1n: 41111010no4 ttl
Cflll: <IIJ!!Ol8110 1I U3
Ul_lfitl: A 0, 1. 0 .J O B1,SE: IJ 20, 3
2000
:fJ:20
22ru3
.3~~: ,10
45120.
2400 SUitl
40:(10 TIME
ORGANICS ANALYSIS DATA SHEET
ACIDS
Laooratory Name: Spectrix Sample ~umber: OS-S-
Sample i~atrix: Water
. -.
Lao Sar.;pl e ID No.: Jb//o/? "S°
Data Release Authorized By~~ Date Sample Received: -11/,/2t: ;
Concentration: Low
Date Extracted:
Date Analyzed:
NPDES #
lOA
1A
oA
Ji-\
2A .. ,,,
Uri
~A
IA
4A-
9A
108-95-2
120-83-2.
68-06-Z
100-02-1
~34-,2-1
81-36-,
COMPOUND
? heno 1
z-,~n I oropneno 1
Z-N1 tropneno 1
Units: ug/L
Cone/Di l Factor:
Ccr.,pounds De tee ted:
2,4-01c~1or~pneno1
2,4-01n1trcpnenol
4-N1trooneno1
4,o-J1n1 :ro-,-Metny1pnenol
?entacn I c rcpneno,
U = Undetected at the listed detection limit
J = Ccr.,pound is present, but below the listed detection limit a = Compo_und also found in blank
1 O /::l~ I ,,Antu?\
I
a
RESULT
10 U Io u
2.0 U lo 0
10 U
10 0 lo u
50 U
:,0 0
50 u
CS-5
· ..llj 1~018A05;3
ll/12/86 23:03:00
11/7/8_6
·SPECTR!X DC~ ----14
INST ID.
ANALYST
4530
YPH
VERIFIED l3Y ~
CORR. FACTOR 1. 00
-------------------------------------------------------------------------------··
SE~lVOLATlLE COMPOUNDS M/E AMOUNT RRT -------------------------------·-------------------------------------------------=!5 CI.JO 1, 4-DICHLOROI3ENZEND-D4 ** IS! ...... 152 40 UG/L .1. 000 41~>> 716 CI40 NAPHTHAL!::NE-D8 ** IS2 ...... 136 40 UG/L 1. 000 1..:.60'.:··~ 1004 CI50 ACENAPHTHENE-D10 ** !53 ** 164 40 UG/L 1. 000 754..;.: , ..,,.,,....
-.:;.. ""t..) CI60 PHENANTHRENE-D10 ...... IS4 ...... 188 40 UG/L l. 000 ~'"'.;"1 -, ·-· .',: 1682 CI70 CHR YSE~IE-D 12 ...... !S5 ... ... 240 40 UG/L l. 000 ..!.26.!,:
~901 CI75 ?EflYLE~IE-D12 •* IS6 ** 264 40 UG/L 1. 000 _;;~4~:~ -;i...-,c:. -:S5C: 2-;::-i__UORCPHENOL ..... 3U1. *" 112 35 1/. 0. 650 l 1 ---:--....;._-.., -... c-.. = .:126 c:;..15 i=+:E~mL-D5 ...... SU2 *~ 99 58 1/. 0. 944 -~S4~:..: . ::s c-~== ..., 4. 6-TRIBROMCPHENCL ..... SUS ....,, 330 .., ' 1/. l. 130 ! 5: :;·: . ~-' . =.01 •:s~c, NITKOI3ENZENE-D5 ~* SU3 ...... 82 76 ., 0. 848 ==~c-~~ ,.
903 cs~s 2-FLUUOROBIPHENYL ** SU4 * ... 172 70 1/. 0. 899 15466 : S~·J •:S:J0 TE:rsPi-!ENYL-014 A-~ 3U6 ..... 244 101 1/. 0. 904 .ss..:.3; 1725 C735 BISC2-~THYLHEXYL)PHTHALATE 149 99 UG/L l. 026 1 c:; -;-,.., .c::.
.J.I =--~
#
IJ
Cl
X ••
1'(
i· u
ltl
11.
IJl
0 (']
'" .,
RIC
11/12/86 23:03:00
SAMPLE: 05-5 cmms.: ---
RAtlGE: G I, 2400
DATA: 4U11018A05B ff!
CALI: 4U11018A05B #3
SCAtJS 200 TO 1350
U)BEL: N O, 4. 0 QUAIi: A O, 1. 0 J 0 BASE: U 20, 3 '.303
100.0
PIC
345
515
486
t.07
._, ___ ~•-·'-· ____ jJ_L l, \, ..... ~--Jt t._--.J .-=.:.::::::::=..:=;..::::=__.::.:::::::;===i_..;.:.:.-2'.:== i --·. ·-··-i-
',:'.(H) .
:?,: ;::n
4~1l)
6:40
r;oo
\ (1; 1.)IJ
741
1()04
788 l
·..:::·-~--..!'.=L::=•""===·• ....:..:~,..;..~:~-,:.;;10:31
800
. J:3i '20
1000
lfi:411
1136
1243
L:00
20:00
1B688e
SCAN
THIE
•t
rl
I I
I
I
#
u
0
X •·· 11:
f··
'-' w
11.
lfJ
0 n
" .,
'.
1(10.0-
RIC
11'12,,86 2.3:03:00
5At1PLE: 05-5
COMDS.: ---.
Rf1IIGE: G I, 2400
l '320
DATA: 4U11018A05B ttl
CALI: 4Ul1018A058 tt3
SCAIIS 1350 TO 2400
LhBEL: M 13 .. 4.~3 OUA11: r~ 0, 1.0 J 0 8i~5E: U 2CJ., 3
1643
1725
168.,
474112,
· ·_ L I lO"i5 l'.-\°l I. ~
1
_ _}_~ ·-,--1 '.i:?_~4 ~"-'--.LL,.,,· ~d':~f, 10~ .:.1 ---'/1,:..,-__,l.::.:3'.;.;1, __ 1.--...::2.:.0;:;,;'.iO.:-...;f;.;.' l.,_1 c"-_; _.::.2 :.;;18:.;.f-. _.:2.:a.26:;,;;6'--""~a:.3.:,.;19;;...._...,1
I ,j ,:,<) I 600 I ;::nn · 2000 2200 24 00 SC At I
,~::!IJ ,G140 °:n:nn 33:20 :3.G:'10 40;00 THIE
ORGANICS ANALYSIS DATA SHE~T
ACIDS
Laooratory Nfilne: Spectrix Sample Number: OS_£ -.=.:=----=---
Lao Sample ID No.: Jt//o/? t1.f Sample Matrix: Water
Data Rel ease Authorized By~--::::~
. /.
Date Sample Received:· 11/7/4/{
)
Concentration: Low
Date Extracted:
Date Analyzed:
~PDES "ff
lOA
IA
oA
~A
2A
8A
uA -· ~,...
IA
:+A
9A
CAS #
108-95-2
oo-1~-~
.!.V.'.J-0/-'j
1 20-83-2
08-0o-Z
~1-28-~
lu0-02-J
COMPOUND
? he no 1
c-l'.nloropneno1
L-N1 tropneno 1
Units: ug/l
Cone/Oil Factor:
Ccrnpounds Detected:
2,4-J11netnypneno1
2 ,4-01 en I oropneno I
c,4,o-1r1cn1oropneno1
2,4-Dinitropnenol
4-Nitropnenol
4,o-01n1 cro-2-Metnylpnenol
?en tac n Io ropneno 1
U = Undetected at the listed detection limit
J = CCC:Jpound is ~res<:!nt, but below the listed det<:!ction limit
8 = Compound also found in blank
I
0
RESULT
10 U
lu u
20 0 ro o
10 U ro a
10 u
50 U ~o o
5d 0
. OS-6 . ~ ...
AU l l O l 3AO.:,
·!l/12/96 23: 54:00
11/7/86
. .
.SPECTR!X DC~ ----l~
INST ID. 4530
A/"·JAL 'tST '(PH
VERIFIED BY~
CORR. FACTOR 1. 00
----------------------------·----------------------------------------------------
SEMIVOLATIL~ COMPOLNDS i"l/E AMOUNT RRT --------------------------------------------------------------------------------498
711
1003
,242
!680
!399
~S'S-
90 l
=: ! 30
-: I 40
•: I 5·J
-: ! :S0
•: T70
,: :75
-:s..is
,:s2s
•:S30
1,4-DICHLOROBENZEND-D4 ** ISl **
NAPHTHALENE-DB ** IS2 **
ACENAPHTHENE-D10 ** IS3 **
?HENANTHRENE-D10 ** !S4 **
C~RYSENE-D12 ** ISS *~
P£RYLENE-D12 ~* lS6 **
2-~LUCRCPHENOL ~~SUI••
P~E~JOL-D~ •• SU2 *·•
2, ~, 67TR!EROMCPHENOL **SUS~~
NITROE~NZ£NE-D5 44 SUJ *4
2-F~UUOROBIPHEN.t'L ~~ SU4 **
fERPHENYL-014 4~ 3U6 ~•
3!5(2-~THYLHEXYL~PHTHALATE
152
136
164
188
240
264
1, 2
99
330
32
172.
1 ..:10 ..
40 UG/L
40 UG/L
40 UG/L
40 UG/L
40 UG/L
40 UG/L
8'7 'l.
77 ¼
57 :~
92 i:
78 1/.
1 •)2 ¼
1 UG/L
l. 000
1.000
1. 000
1. 000
1. 000
1. 000
0. SQ'.:'
0. 938
1. 131
0. 840
0. 898
0. 904
1. 026
36:J5:'
13274G
62312
81297
1 ·J32b::
99~:=
..:29:=.;:
1..::. 1 ~~~
X -Cl'. >--u
lJ.I a..
1/J
I· Ul ;:
"
100.0
P.IC
RIC
11 <'I 2/86 23: 54: 00
Sf1MPLE: 05-6
COtlOS.: ---
RAl~E: G 1,2400
Df, rn: 41_111 o 181106 tt 1
CALI: 4Ull018A06 ff3
SCAHS 200 TO 1:350
LABEL: ti 0, 4 . 0 [•Ufil I: !1 0, 1. 0 .J O Bf1SE: U 20 , 3 901
736
1003
467
597
1242
1134
. 2/:1'
;::r; ,: I 358 ~. 11 r.:::::::".=,,~·'.:::~~"'_::_·::::____J~~'-':::·~'---~=='-::.··-::.,_:::-''.!:~==::· __ T-.... ½.~.
I
\ . ...___.._, -.;,, 1~----t\c~_,.-.L::,--,--
1
(,I)()
I 1:1: 1:11.1
,·oo ,ion
3: 20 f;:40
800
· 13:20
1000
16:•10
1200
?0:00
171520
SC At I
TIME
'T ....
I
I I
I
tic
(.J
Q
X
H
Cl'. I-
I) ,,,
[L
lfl
i I
t -
U)
,'..
100.0
P!C
RIC
11 / 12186 2:3: 54: 00
snMF'LE: 05-6
COtlD5. : ---
PAIIGE: G 1, 2400 1518
! ·100
?31 /0
DATA: 4U11018A06 ttl
CALI: 4U11018A06 tt3
. 5CAll5 1350 TO 2400
LABEL: II 0, 4. 0 Qlf(ll I: () 0, I. 0 .J 0 Bf'l5E: IJ 20, 3
1899
2000
0'3:20
?200
3f;: •10
68096
2400 SCAIJ
40: 00 TIME
ORGANICS ANALYSIS DATA SHEET
AC:DS
Laoora tory Name: Spectri x Sample !-lumber: os-7
Lao Sample ID No.: J6//o/?tl 7 Sample Hatrix: Water
'
Data Release Authorized By:~
Concentration: Low
Date Sample Received: 11/7/21;-
7
Units: ug/L
Date Extracted: // / 7 /p-..6 Cone/Oil Factor: / __ ....:,_ ___ _
---. :_._,__....:..c..::,. __
Ccrnpounds Det~ted: O · -~---
NPOES ii
l0A
J.A
oA
.:iA -, . -" . ' un
liA
oA
IA
.... A.
9A
CAS #
108-95-2
08-10-0
1uo-01-9
120-83-2
38-Jo-Z
dl-36-o
COMP<J UNO
? heno 1
2-l.n I oropne~o 1
2,4-u11netnypneno1
2 ,4-01 en\ oropneno \
2,4-01n1trophenol
4-Nl tropneno1
_4,o-J1n1 tro-L-Metny1pnenal
U = Undetected at the listed detection 1 imit
J = Ccrnpound -is present, but below the listed det~tion limit
B = Compound also found in ~lank
10/85 (l1AnAW?)
RESULT
10 U
iO u
20 u
iO 0
10 U
10 0
10 0
50 U
~o o
50 u
SA~PL~ lD ;:-! L::'.i'lr\~E -:i_ I ::N7 DAT£ It'l,..iE•:TED CAL1l3 S,D DA':°E _SPECTRIX DC~ ----14 SE~:~JOLAT:L~ W~7~~ R~?SR7 ,QS-7 41Jl!013A07 >'.C:"iSTCNE 11/13/86 0:46:00 11/7/86 HlST ID. ANALYST 4530 YPH VERIFIED IlY ~ CORR. FACTOR 1. 00 -~ -----------------------------------------------------SCAN# SEMIVDLATILE COMPOUNDS M/E AMOUNT RRT AREA --------------------------------------------------------------------------------498 C .. ~,, 1, 4-DICHLOROilENZEND-D4 ** ISl ** 152 40 UG/L 1. 000 33C2S' •-'-' 710 C!40 NAPHTHALENE-DB ** IS2 ** 136 40 UG/L 1. 000 1069'"1'.; 1003 CI 50 ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000 55075 1242 CI60 PHENANTHRENE-010 .... IS4 ** 188 40 UG/L 1. 000 71096 1681 CI70 CHR"SENE-012 ** IS5 -1$-4 240 40 UG/L 1. 000 ' .. ---~ J. .:. ; ' .. • !.899 Cl7S PER'(LE,',IE-012 *..,. ISO ** 264 40 UG/L 1. 000 -.242::= 293 CSSO:l 2-FL:UCRGP,-,ENOL ~~ 3U1 ** 1 ! 2 1 ·)2 ;~ 0. 588 -.. ---... -+ .... ..;. 406 CS45 F!-:~NOL-D5 ** SU2 •-4-99 88 'l. 0. 936 10/Q..!1:· .! 134 CS55 2,4,6-TR!3ROMOPHENOL *~ SU5 ** 320 56 Y. 1. 131 ss-~.c 597 · ·2S2·J :'i I'" OGEN ::ENE -D 5 II;'* 51,_r:3 *" 82 '70 Y. 0. 841 ...,,_ __ -..J...:i.· ::::.:..: 7'01 ,'""c-;i::; 2-FLUUOROBIPHEN(L •• SU4 ** 172 85 Y. .0. 898 13691:: -.... c. _, l. 51 S CS:JO T:C:.'lPHE>IYL-D14 ..s-~ SU6 ** 244 122 Y. 0. 903 6677--:-~ -...., . .-, ! ,' C...:, C7'.25 3:S!2-ETHYLHEXYLlPHTHALATE 1 .,o J...,. .· 1 UG/L 1. 025 1 ;:,-•• -,;. ..,J...)~
<t ...
I I I I
#
u
0
X -ft'. ~ u
ltl
[L
!fl
0
fl
J ' .
·t
I
Ul -, ,_ ,,
RIC
I 1/13/86 0: •16: 00
SflMPLE: OS-7
COHOS.: ---
RAI IGE: G I, 2400
DnTn: 4Ull01Bn07 ff!
CALI: 4Ul1018A07 tt3
5CAll5 200 TO 1350
LABEL: ti 0, 4.0. QIJAII: (l 0, 1.0 .J O B(1SE: U 20, 3 901
100.0
101)3
P. IC 71•)
466
498 1242
,r
::..:..:::·~--~\'--.:::::=-=· ~-~~-c-,!_\_:___J....::'=-·=·=!;-,=Jt. ______ l, _ _;8..._,6R;;_-~=-;..._~--,-1_'.:~~=,.___,,-L:l '~:,..__,.-
~-,:u) •IC:l!J ,,,i.:, :300 1()01~ 1200
3:;::o 6:40 lt):tll) .lJ:20 !G:40 20:00
11:35
152576
SCAM
TIME
#
u C,
><
H
l'.l:: >-I.I lll n.
lfJ
0 n
U) .,
n
H
JOO. 0
PIC
RIC
11,13/86 0:46:00
SAMPLE: 05-7
COtl05.: ---
RflllGE: G I, 2400 1518
[1(1 Hl: 4U 1 10181)07 ff 1
CALI: 4U11018r107 #3
5CAtl5 1350 TO 240~1
LABEL: ti O _, 4. 0 0Ur111: A O, 1. 0 J O BASE: U 20, 3 ·
1681
189:3
172:3
i'110 \ -1640 1 I ··~,_!}]l.. f'.Q}}. ____ 21?X,_., ... _~ff1.L, 2310 ~~
604IE
fn,.-,~,r-......, .................... _ _';,.-=o,,,.,, ' ......... "-"""'--;---~ l.,-.,M"'· "·-, =---~ ==1.;:::::::::::=-::::;::::::::::::::::'::::::;:=:::::=:~·.:::::~:::::::::::::.=:;::~::::::::::::;
I lu:io 1 f.0() 180(1 2000 2;-,_10 2400 SCAI l
2!?,:•10 °:rqni1 33:20 :;:f;:40 40:00 TIME
ORGANICS ANALYS!S DATA SHE~T
ACIOS
Laooratory Name: Spectri x Sample Number: os-r
Sample Hatrix: Water Lao Sample ID No.: Jb//o/?o,?'
Data Re 1 ease Authorized By :.-.,-W~ /)
Date Sample Received: 11/7/J,t: ;
Concentration: Low
Date Extracted:
Date Ana 1 yzed:
NPOES #'
lOA
1A
--oA
jA
2A
o,-.
uA
~A
I A
4A
9A
CAS #
108-95-2
ll.J~-o/-9
120-83-2
08-iJo-Z
liJ0-02-7
534-~2-I
81-36-~
COMP<JUND
?her.a i
2-l-n I oropneno;
Z-N1t.ro\:)ne:101
Units: ug/L
Cone/Oil Factor:
Ccmpounds Detected:
Z ,4-01 en I oropneno 1
p-\,,n I uro-m-creso l
2,4,o-1r1c~1crcpneno1
2,4-01n1tropnenol
<+-N,tropnenol
r'en tac n Io ropneno I
U = Undetected at the listed detection limit
J = Ccmpound is present, but below the listed detection limit a = Compound also found in blank
,n1o:Jc: t,"'l,'\nA1,,,,
I
0
RESULT
10 U
10 u
LO u
10 0
10 U
10 0
50 U ~ca ~o a
50 u
4Ul1018A08
11/13/86 1:37:00
11/7/86
5?ECTR!X DC ~ ----1~
INST ID.
ANALYST
4530
YPH
VERIFIED BY '7??/
CORR. FACTOR l. 00
------------------------------------------------------------------------------·-·· . '
SEMIVOLATILE CCMPGUNDS M/E AMOUNT RRT
4"' • C, CI30 L 4-DICHLORDBENZEND-D4 ** ISl ** 152 40 UG/L 1. 000 3134,:,: 710 CI40 N.;PHTHAL!::NE-D8 ** IS2 ** 136 40 UG/L 1. 000 1 OCc: ":; 1003 ,: r 50 .;CEN.;PHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000 5!a,s..: .... ,,.,...,
.1 ,:;.-, c:.. Cle:•) PHENANTHRENE-010 ** IS4 .... 188 40 UG/L 1. 000 6706.: 1620 ,::i/:J 1:HRYSENE-D12 ** IS5 ** 240 40 UG/L l. 000 .,....,c,--,-..J, 0 /-= ! 399 c:1s PZ~YLENE-·012 ...... T-· ~ ::o ..... 264 40 UG/L 1. 000 -2407·: 2~.·J -,..... ,: -2-FL.UGRGPHENOL *"' 3l•l "'* 11 ~ 90 1/. 0. 585 s..i=·-;·: '-=-•'..J ·-.:;05 •:S45 P!"'iENOL-D5 ... ,. SU2 ... 99 66 1/. 0. 937 7.:J52C ; : '.;4 -,... C: ·-.., 4, 6-TR!BROMCPH!::NOL ** SUS ...... 330 42 ., 1. 131 70~.~ ;_. :::; ,../::, ~-,. 5=:.~. ,: ;;:o N: TR OBE:~i:E::'JE-D5 *" SUJ *" 82 68 ., 0 . 839 24C-S: ,.
~•J 1 ,:s2s 2-FLUUOROBIPHENYL ..... SU4 ... ... 172 63 1/. 0. 898 0 c:_ -i •.
--·c_ -.:. :-. 5: S c="Jo TE"PHENYL-014 ** SU6 ..... 244 o~ • I 1/. 0. 904 514~-17~3 ,:7::;5 3IS(2-ETHYLHEXYL)PHTHALATE 149 4 UG/L 1. 026 .cl 75-:
cit
u
Q
X ....
fl'.
f-u 1,1
n. UI
I) ..
I·
UJ ,:
"'
I 00. O·
-
-
RIC
ll/13/86 1:37:00
Sf'l11PLE: 05-8
COIIDS.: ---
RAI IGE: G 1, 2400
230
DATf): 4UIIOl8A08 Ml
CALI: 4Ull01BA08 #3
SCAMS 200 TO 1350
LABEL: fl 0, 4. 0 OIJAI l: A O, I. 0 J O BASE: U 20, 3 901
710
Hl03
4S5
595
1242
1134
L•-_. ·:_:'--:=:_-''_::·~:::..,., ".~-::-:::-=::::38'.:::4~· 1· =:::::...::...", \.-==· =~ ~'= •·•~ _l _ '.:::...::..:::'.( ?-""~;=· =-=c~u,-\.-\~~~~c:==,...!.1,::.0 •:..;;".3:.,., _.ll~\I =---...-,..eclt.~..,., -
20~)
3: ,;o
~0() l,l1,J [!1)1.l 1000 I ,:(JI)
6: 40 In: 1JO . 1.3: 20 16: •lfJ 20: 00
107392
SCAM
T !ME
·,i-...
I I
I . I
1t
V
Cl
>< ...
r>:
I-
f.l
ltl n. (I)
. (.1 r,
" -t
''
lOIJ.0
R.I (
F:IC [1(1l11: ,11_1110181108 ff! SUlllS J:350 TO 2480
ll>IJ/t:G 1:3i':OO U\Ll: ·1UIIOl8D08 HJ
SMIPLE: 05-8
COIJOS.: ---
~:i'll!GE: G L2•W1) LABEL: 11 0, 4.0 OU11II: A 0, 1.0 J O BASE: IJ 20, 3
1518
I·''·' I 1-1·.i,· • _......._...,,< ___ , ... , r
I
1:11)(\
~.); 21)
16413
160Cl
,·6: ,10
1681
J ,:o,-, .
)ii l f11i .
18:39
2000
3:31 20
2bJrJ
:31;, ,10
46784
2400 SCAfl
40: 00 T Il'lE
ORGANICS ANALYSIS DATA SHEET
Laoora tory Name:· Spectri x Sample Number: OS-f:MS
Lao S.i.r.ipl e ID No.: Jb//o/?O[
J
Data Release Authorized By:_,,:~
~
Sample i-latrix: Water
Date·.Sampl e R~eived:
Concentration: Low Uni ts: ug/L
Date Extracted: 1//7/,?-£ Cone/Oil Factor: / ---, --J-.-----------
D.i.te Analyzed: Ccrnpounds Detected:· 0 _c._ __ _
NPDES #
10A
IA
Ci\
JA
2A
..! .\
11A
5A
IA
4A
9A
CAS #
108-95-2
9:,-J/-d
120-83-2
38-0o-Z
100-0Z-/
81-db-:,
COMPDUNO
?heno 1
2-L.n I oropneno 1
,-,l1 ::.ropnenol
L,4-U1metnypneno1
· Z,4-□1cnloropnenol
2,4,o-1r1c~1oropneno1
2,4-D1n1tropneno\
4-Nl tropneno 1
4,o-J1n1tro-Z-Metny1onenoi
?enc.i.cn,oropnenol
U = Undetected at the listed detection limit
J = CCC:lpound is present, but below the listed detection 1 imit
B = Compou_nd al so found in blank
10/85 ( OADAW?l
RESULT
10 U
10 u
20 u
10 a
10 U
10 a
10 u
50 U
:,O a
:,0 u sou
SCAN#
497 ,::30
7 1 I •: I 40
1003 ,:r5o
1243 CI60
.:.. 621 C ~ 7:)
291 · ... -=::u
586
707
827
~GOB
~049
105_0
1228
1477
1723
C:340
C37·J
CS60
C57.J
C635
C715
C735
:-<-C.YSiONE
ll/13/86 2:29:00
l!:'7/96
SE.'1: 'iOLAT:L.:C: CCMFOUNDS
1,4-DICHLOROBENZEND-D4 •• 1S1 ••
NAPHTHALENE-CS •• !S2 ••
ACENAPHTHENE-D10 •• 1S3 **
?HENANTHRENE-D10 •• IS4 **
~HRYSENE-012 ** ISS **
:.JS:~YL==NE-D.!.2 ** IS6 **
~-F~~CRCP~ENCL ~4 5U1 *4
?HE~iGL-D5 ** SU2 *6
~-~.6-TRIBRGMCP~E~JOL **SUS~•
N:TRGBE~IZENE-D5 ~~ SU3 **
2-=LUUGROB!PHENYL •• SU4 **
TERP~ENYL-D14 ~~ SU6 *•
?~ENCL.
~-.~~1 _..,!'."i.-.r"!1 • .-... !~) --· ,._,_,, ...... '·-· ~,_, ....
1, 4-DICHL □ROEENZENE
N-N!TR □S □D!PRGFYLAM:NE
1, 2,4--rRICHLOROBENZENE
~~CHLGRG-M-CRESOL
~.: E>JAPHTHENE
4-NITROPHENOL
2, 4-DINITROTOLUENE
?ENTACHLDROPHENOL
PYRENE
B:S(2-ETHYLHEXYLlPHTHALATE
INST ID. 4'530
ANALYST. YPH
VERirIED llY ---p7i
CORR. FACTOR l. oc
M/E
152
136
164
188
240
264
'7 ... .:. .::.. .
82
94
128
146
70
180
!07
153
139
165
266
202
149
AMOUNT
40 UG/L
40 UG/L
40 VG/L
40 VG/L
40 VG/L
40 UG/L
:20 ¼
S::? ¼
83 :~ .,
I ✓ '• 11 9 .,
69
66
UG/L
IJG/L
31 IJG/L
33
60
35
94
43
14
54
VG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
7 UG/L
RRT
1. 000
1. 000
1. 000
1. 000
1. 000
1. 000
0. 586
0. 940
1. 13 l
o. 840
o. 898
0. 904
0. 944
0. 944
l. 006
1. 1 79
0. 994
1. 163
1. 005
1. 046
1. 047
0. 988
0.879
1. 025
34.1-::,;;
1221C.3
63072
........... ..,_ -, C: ..J....: _:
-.c ..,; ... :c .·
306.:·:
-.. ,J -..:,~-· .. ,
as.i:.4:
98,:::7"
X
P.'. 1--u
~I
IL
U)
. '
I·
Ol
PIC DrHfl: 4UI 1018(10'3 ff! SUIIIS 2013 TO 1350
11.··L::,'86 2:28:00 COLI: 4UII\Jl81~03 tt:~
rno.o
Sflt-lPLE: 05-81-15
COi iDS. : __ .:
P.hl!GE: G L24013 LhBEL: H 0, 4.0 QIJf)II: r1 0, 1.0 J O 8A5E: U 20, 3
469
0
901
711
PIC 1003
827
1243
51)0
585 1135
1050
292
\~---l-L_'.':\,,...-~, __,_I\ :--1•--'-'.:I.(->-' ~~-
3:2D
~l)t)
f,: 40 I t1 1 1_111
IOO•J
If.: •If)
1200
20;00
191744.
SCAii .
TIME
'"' H
f(
t-u w
0.. IJJ
()
(')
"' ,,
r,
100.0
PIC
PIC
11113·86 2:28:00
SAMPLE: OS-8MS
COtlDS.: ---
RA!IGE: G I, 2400
1477
DATA: 4UIIOl8A09 HI
CALI: 4UIIUIBA09 ff3
SCAIIS 1350 TO 2400 .
LABEL: tl 0., 4. 0 QIJhll: n 0, I. 0 .J 0 BASE: U 20, 3
1641
1631
1 ':)00
127488.
1. . l 'l
1I, "7' 1m, l 10,2 "" 21c; "" 231' "" ---r ·--·-·......-Lo--~·-r--~~' -'"-i--~-J~-====='===7c;===:;::;==;=,-=-·""--""·· ""-·-""-·""-·-cc,1;2-. =-=. ====;:===="==
2000 ,.c:,1O
33:20 3Gl·l0
2400 SCAtl
-101 00 T H1E
ORGANICS ANALYSIS DATA SHE~T
ACIDS
Ldoora tory Name: Spect:-i x Sc1.mpl e ~umber:. OS -J: MSZ>
Ldo Sc1.1i1pl e iD No.: Jb//o/? / o Samp 1 e i~ atri x: Water
Data Release Author~zed By~ Date Sample Received: 11/,/2t'
7
Concentrc1.tion: Low
Date utracted:
Date Analyzed:
NPOES " ,,.
10A
1A
oA
jA
2A
dA
UA
"· :>A
iA
-+A
9A
CAS #
108-95-2
i20-d.J-2
:,9-:,0-,
:,l-28-5
100-02-)
:,34-:,2-1
27-30-:,
?heno 1
~-\..n I oropneno 1
.:::.-th tropneno 1
Units.: ug/l
Cone/Oil Factor:
Ccrnpounds Detected:
2,4-Jimethypnenol
2 ,4-01 en Io rooneno 1
c,4,o-1r1cn,oropneno1
2,l-D1n1tropneno1
4-N 1 tropne no I
4,o-J1n1tro-2-Metny1pneno1
?entacnioropnenoi
U = Undetected at the listed detection limit
J = CCl:lpound is present, but beicw :he listed detection 1 imit
8 = Compound also found in blank
10/85 (OADAW2)
I
0
RESULT
10 U
10 u
20 0
Io 0
10 U
10 D
10 u
50 U :io D
:,0 u
50 u
4U !. l O 18A 1 ·J
11./1:::3/86 3:19:DO
1.1/7/86
INST ID. 4530
YPH
VERIFIED !lY ~
CORR. FACTOR 1. 00
--------------------------------------------------------------------------~------
SEMIVGLATILE COMPOUNDS AMOUNT RRT A?.E.-\
497 C!30 1, 4-DICHLORO!lENZEND-D4 ** ISl ...... 1 52 40 UG/L 1. 000 34322 -' I • 1 ,:I40 NAPciTHALENE-DS ** 1S2 ** 136 40 UG/L 1. 000 1206!3 1003 C!50 ACENAPciTHENE-DlO ...... 1S3 ** 164 40 UG/L 1. 000 634·;-~ 12~3 ,: !o•J PHENANTHRENE-DlO ** 154 ** 188 40 UG/L l. 000 7S2:::~ 1681 C!70 .:HRYSEf·IE-D 12 ...... r-c . ::, .., ** 240 40 UG/L l. 000 430~..! 1 "'C0 ,... T' ;c:; ·-. ., -?=R "(LS>IE-D .!. 2 ** ,56 ** 264 40 UG/L 1. 000 27t?-+S 2S'·J c==o 2-i='L 1...JCP.CP ~EN~L *~ SUl ** l 12 9~· :. 0. 584 -:-~=-=-'= . ~ ..... -.... =·= ,:S45 ?!-:Ei\iGL-2'2 ...... SU2 *~ 99 87 1/. 0. 928 l >J=-as '-c -:s~ s .,
~-' --r~: 3R !:JMG? '-IE:'·~CL.. ,. .. SUS ** J~O 74 :. 1. . --, l 32 S1:,
J.~-., "'' J. ...l,:::. =~= c::~0 N: T~CGE>~Z~:'·JE-~5 .. ~~ ,-, 1, ** .---, ·7·c• 0. 838 22::c:s ::,\.,_ c~ .. -l :~25 2-FLUUORCB!PHEN'f~ ** SU4 ** . i.c:..'. 73 :. 0. 898 1 J:;c;::: :· : 9 •.:s20 TE::RPHE>fYL-D 14 .... Sl'6 *+ 2~~ .~-1/. 0. 904 :::.-, --..-. . -:-c:;. ..,c;.;.:-=..;c ' --::::; l 5 PHENOL S4 72 UG/L 0. 942 1. :.::c-2::: ..... ==-
-:,o ·::;30 2-C i-il OR GP L.:,ENOL 1~-"'"' ::, ', UG/L 0. 942 3:3C0 .. co -' , C34•J 1, 4-Di~HLORO!lENZENE 146 34 !JG/L 1. 004 44:J23 ~•=6 ,:270 N-N!~ROSGDIPROPYLAM!NE 70 JS UG/L 1. 179 31 ·---i::..:::. • o ... -..., -~-I:_, I ,: -1-4 5 1, ""' 4-TRICHLOR03ENZENE 180 J6 UG/L 0. 994 G3~88 E27 ,:465 P-CHLORG-M-CRES□L 107 59 UG/L 1. 163 524.\ . .:,. lC•C2 ,:550 ~C:::::>IAPH7HENE 153 35 UG/L 1. 005 '5460":0 1050 •:560 4-NITROPHENCL 139 82 UG/L 1. 047 14007 1c::-o s=-7o 2. 4-DINTTROTDLUENE 165 43 UG/L 1. 047 .. c:-, !. o-.,: ""'!' 1 .... -,,:J C635 ?ENTACHLOROPHENOL 266 23 UG/L 0. 988 51 ' . .:.e...c..--.. 1477 C71S PYRENE 202 45 UG/L 0. 879 755E5 1724 C735 3:5<2-~THYLHEXYL)PHTHALATE 149 2 UG/L 1. 026 3092
u <-1
X -~
[".
f-
'·' L1/
lL lfl
0 n
UJ
-1·
IJ!
100. 0
PIC
F:IC
ll/13/86 3:19:00
51\MPLE: 05-8 1150
COtlOS.: ---
R(111,~E: G I, 2400
I
\ I • . . -~...,.___•'.,___
,1,_1
: ?O
40()
6: •IIJ
OAfA: 4Utt018At0 #I
CALI: 4Ull018AIO #3
5CAll5 200 TO 1350
LABEL: 11 0, 4. 0 QU(sll: (l 0, 1. 0 .J O 8ASE: U 20., 3
468
71 I
4'.39
o--,-,
'·' i,, I
eou
1··{: zo
901
I fJO 3
1000
11:::40
1243
1135
I 0'30
~1c,..,..... ..... 1.~-r....L"-""-•~-
, ?00
,'.O: IJO
194048.
SCAll .
THIE
tic
(.)
0
)(
H
((
1-u
UJ
[L
lll
''
I·
IJ) :<
PIC
RIC ll/13/86 3:19:oo·
SAMPLE: 05-8 11S0 cot IDS. i ---
F:flt lGE: G I, 2400 1477
DMri: 11111 l0l8AIO Ill
CALI: 4Ull018AIO tt3
SCAll5 1350 TO 2400 •
LABEL: M 0, 4.0 OUAtl: A 0, 1.0 J O BASE: IJ 20, 3
1681
1980
2000
:3): 20
2200
3S!4'.:l
53248.
2400 SCAM
40:00 TIME
ORGANICS ANALYSIS DATA SHEET
ACrDS
Laooratory Name:· Spectrix Sample Number: os-1
Lao Sample ID No.: Jlt//o/?I/ Sample Hatrix:. Water
Data Release Authorized 6y~~
. /
Date Sample Received: 11/;/2t' ;
Concentration: Low
Date Extracted: ///7/?°£
---· -~-c...=;,. __
iJnits: ug/L
Cone/Oil Factor:
Date Analyzed: Car.pounds Detected:
NPDES #: CAS # CGM?DUND
10A ?henoi
!.A Z-l.nl aropnenol
oA 2-N, :.:-opneno 1 ~A 105-o,-9 Z,4-01metnypneno1 ., .0. 2. ,4-0·~ c Ci\ o ropne no i
ol'. p-l.h Io ro-m-creso 1 u.A 38-0o-Z
' 01\ 2,~-D1n1trapneno\ 7 ;,. 100-02-7 4-Nitrapnenol .. 4,o-u1n1 tro-2-Mecnytpnenol
9A ?entacn1oropneno1
U = Undetected at the listed detection limit
.J = Ccmpound is present, but bel cw the listed detection 1 imit a = Compound also found in blank
I
0
RESULT
10 U
10 u
20 u
10 u
10 U
10 u
10 u
50 U
CALil3 STD DATE
GS-9
4Ul1018Al:
11/.1_3/86
11/7/86
4: 10: .JO
SPECTR!X DC I ----1~
INST ID.
ANALYST
VERIFIED BY
CORR. FACTOR
4530
Y?H
1. 00
--------------------------------------------------------------------------------
SCAN# SEMIVGL~rILE COMPOUNDS AMOUNT RRT AREA --------------------------------------------------------------------------------
498 cr30· 1, 4-DICHLOROBENZEND-D4 * ... ISl ** 152 40 UG/L 1. 000 39806 711 CI40 NAPHTHALENE-OS ** IS2 ** 136 40 UG/L 1. 000 125288 1004 CI50 ACENAPHTHENE-D10 ** !S3 ** 164 40 UG/L 1. 000 65816 1243 CI60 PHENANTHRENE-D10 ** IS4 ** 188 40 UG/L 1. 000 83866 1682 C:i:70 CHRYSENE-D12 ** IS5 ...... 240 40 UG/L 1. 000 5165E :~01 C:I75 PER'r'LENE-D!2 ** r~· • ::,o ...... 264 40 UG/L 1. 000 3235~ :;:94 cseo 2-Fl.UORCF'-iENCL ... ~ , .... 1 : 1 ::, -. 4• 112 75 'Y. 0. 590 . ,... ..... C:::.c.:' •~ 467 •:S45 . "HENGL-OS ...... su:;: *-V 99 56 'Y. 0 . 938 316-l-C :. :35 CS5·S .·, ~-~,-6-rR!3RCMC?~ENOL ~* SUS ** 330 42 1/. 1. 130 :ca-; 597 ,:s21.) 1.Jl TriCBE>E.£NE-G5 ** SliJ ** 82 65 'Y. 0. 840 2S5J...: 902 ,:s~s ~-FLUUCRCB!PHENVL 1-* SU4 ** 172 61 1/. 0. 898 11762: j__'.:19. 1:s20 iC:RPHE>iYL-D 14 -,.,; SC:6 ~ ... 244 76 'l. 0. 903 5224:
31Hl
HUJS
"800£?:T
.(i(J: (1.7.
(.10i: l
UI' :~, I
0081
_ __._ ,--,..-L..c_; ·,-::-J.,I ..,--..;; t-..-<=ca::
'i \ 00 I I -----.,
l I •,
9fll
t,(JOJ
uu:uJ
lJlJ:j (llJ9
(J 1, : :J
[i(J 1,
o.~. :c~ ooz.
...... ~----•-•-. __ •. 1 ... _ __.....~, .•• :·L .............. ==~--;==:::::=:=--'-:::::--I I 1 --~I -v~--
L££ \
h,l
0·001
Z.(16 E 'OZ (I :3sua O r 0' 1 '0 U :1wnu 0 ·i, 'O fl ll38Ul 00PZ: · 1 '.l =3~Jll1Ji:I ---: • SOll1}.)
6-50 : 31.:Jl·ltJS
EH TIU810JJ(I~ :11UJ 00:01:p 98/EJ/JJ
OSU 01 003 SfRl)S 1H I JIJ8 WI JnP :tJ1 IJO Jia
•·• l.J
I
I
I I -.i.
n .. ,
I·· tr) .,
100. 0
PIC
ll/13✓86 4:10:00.
SflMPLE: 05-9
COIIOS.: ---
RAIIGE: G L 241)0 U\8EL: 11
1519
1 icOO
/i~1 ·lD
0, 4, 0
1682
orrr,1: ,11.111otsAt t ff!
U1LI: 4Ul 1018hl I U3
SCfll 15 1350 Tl) 2400 ,
1~1_1r,11: n 0, 1. 0 _I O E:f'.6E: IJ 20, :1
18n1,
·.;i-1: i-1n
?001)
?? : _;~n
44608.
24'10 SCAII
40:00 TIME
ORGAlHCS ANALYSIS DATA SHEET
ACIDS
Laoora tory Narne:-Spectri x
Lao Salilple.ID No.: £b//o/?/;2.
Samp 1 e Number: -=O_,,S"----L/_'7 __
Sample rlatrix: Water
Data Release Authorized By~~ Date Sample Received: 11/7/J,t'
7
Concentration: Low Units: ug/L
Date Extracted: Cone/Di 1 Factor: / -------
Date Analyzed: Ccmpounds Detected: ___,t:2"'-----
NP DES -~r CAS # COMPOUND
lOA 108-95-2 ?henol
lA
oA
~A 10~-o,-9 ~.4-Dimethypnenol
2A 120-83-2.. 2,4-D1cnloropneno\
,.( l
uA 08-0o-Z 2,4,o-1r1cnloropneno1
►. ~A ~l-28-~ 2,4-0,nitrophenol
IA 100-02-/ ~-N1tropnenol
4A ~~4-~Z-l 4,a-u1n1tro-Z-Metnylpneno1
:I A -----~a-1--3~5---~-----?-e_n_t_a_c_~loropneno1
U = Undetected at t.he 1 i sted detection 1 imi t
J = Ccmpound is present, but belcw the listed detection limit a = Compound also found in blank
10/85 (OADAW2l
RESULT
10 U
Io u
20 U
10 0
10 U lo U
J.0 u
50 U
~o u
50 u
CALIB STD DA7C::
SCAN#
_4U11018Al2
'-'.EYSTONE
ll/!3/86
11/7/86
SE:-1IVGLATIL:::'.
5:02:00
/
C::3MF!JUNDS
INST ID.
AN,',LYST
4530
YPH
VERIFIED l3Y~
CORR. FACTOR 1. 00
M/E AMOUNT RRT Ar\E;:; -----------------------------------.--------------------------------------498 ,: 120 1. 4-DICHLOROBENZEND-D4 ** ISl ** 152 40 UG/L 1. 000 3c39~ 711 C!40 NAPHTHALENE-D8 ** IS2 ** 136 40 UG/L 1. 000 1101 ----: ... ._.~, 1003 CISO ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000 6.:.C6.:: !242 CI60 ?hENANTHRENE-DlO ** IS4 ** 188 40 UG/L 1. 000 7738C 1681 C!70 -:hRYSENE-D12 ** !S5 ** 240 40 UG/L 1. 000 ~,:..'":QC .............. !9CO c:75 ?ER.fLENE-0!2 ** . -. ** 264 40 UG/L 1. 000 ---ic, ...,,_ .... ~~ .::.. , ... ,-:..:. :,c, a -... •.:s5o 2-;::-'-. ')CR_CP :-1ENOL ~~ SU! ** 1. ~ . "'-110 'l. 0. 590 :3S2:Ji ~-= 7 ,: '.3 4 5 ::, ciE:✓CL -D 5 ...... SU2 ....... 4 99 91 1/. 0. 938 1226-~~ 1.!.~4 CS55 -.1' ~-TR!BROMCPhENOL ** SU5 ** 330 -:S6 1/. 1 . 131 1 !32, .:.,'.;
~C--:" ". , C ::2•J ,\J: JRC5ENZi:':NE-D5 .... Sl.i3 ** ·~""'! -"'-98 1/. 0. 840 406~: .:;c,1 CS25 2-FLUU □RCBiPHENVL ,H> SU4 ** 172 91 'l. 0. 898 1 . -•.. Cc. l. ,;. -!. :: :. 9 r--.....,,-. ..,,::...:,v 7:C:;;:PHE:•YL-Dl 4 ~-;,} 3U6 ...... 24~ 130 1/. 0. 904 79c;.:4:
It
u
0
X ...
rr 1-u
Ill
IL
[I)
0 1·1 ,,., ...
1-
Ul ;:
1(10.0
r--rc
,10
F:IC DnTn: 1UIIOl8Al2 ff! uiu: ,1u1101sn12 113
SC hi IS 200 TO I :?,:.:oiJ
11 ✓13•86 5:02:00
SMIPLE: 05-10
COIIDS, : ---
P111 H;[: G I, 2400 LABEL: ti 0, 4.0 G1IJf)II: A 0, 1.0 .J O BASE: U 20, 3 901
100:?.
71 I
4G7
4"38
l_ "J~_, \. --,-··---··T--··-·--L.::::...::::=.=-· =--""-~T --..,,.,.
4(H) 601_1
. : ?O G:40 10:no
800
1:-:1:c!J
10130
IG:40
1134
1200
20:00
178688.
SCAtl
T!l'IE
u
Cl
o:
f-u
lll
(L
lll
r.,
H
,_rJ
;:
''
l 00. 0
RIC
11 ✓13 ✓86 5:02:00 ·
SAMPLE: OS-10
onTn: 4UIIOIBAl2 ttl
U1Ll: ,tlfl 10181\12 lt3
scn11s 1350 rn 24CJ0
CO! 11)5. : ---
Rfit lGE: G 1,2400 LP8EL: M 0, 4.0 01.1,)11: Ii 0, I.CJ J CJ BASE: IJ 20, 3
1519
1 i;oo
7G:•10
1 !::or:i
~,1·1: (i(;
2or10
:J?: 20
2200
:}G~ •10
87936.
2400 SCAII
40:00 TI11E
ORGANICS ANALYSIS DATA SHEEi
ACIDS
Laoora tory Name: Spectri x
Lao Sample. ID No.: Jb//o/?/3
Sample Number: _.::.O..,,S<e.--__,_!.,_I __
Sample i~ atri x: Water
Data Release Authorized By~-__,,~
✓-~
Date Sample Rec;:ived: 11/7/2?
7
Conc.entra ti on: Low
Date Extracted:
Date Analyzed:
NPDES #
lOA
oA
JA
2A
dA
IA
CAS if
108-95-2
i.uS-o,-3
120-83-2_
38-0o-Z
Jl-28-J
J.00-02-,
dl-36-J
COMP<JUIW
?heno 1
Z-l..nloropneno1
2-N1 tropneno 1
Units: ug/L
Cone/Oil Factor:
Ccx:ipounds Detected:
2,~-01cn1oropneno1
Z,4,o-1r1cn1crcpneno1
4-ih tropneno I
4,o-01n1 tro-Z-Metny1pneno1
?entacn\oropneno1
U = Undetected at the listed detection limit
J = Ccmpound is present, but below the listed detection limit a = Compound al so found in blank
10/85 (OADAW2)
I
a
RESULT
10 U
LO u
20 0 ra o
10 U
10 u
10 u
50 U
JO u ~o u
GS-11
41Jl 10l8A13
~EYSTONE
l: / 1.3/86 5: 5:3: ·JO
ll/7/86
S?ECTR!~ DC I ----14
INST ID.
ANALYST
4530
YPH
VERIFIED BY -;J1'7?t
CORR. FACTOR. l. 00
---------------------------------------------------------------------------------
SCAN# ·3Ei1 ! \/OLA T :i L~ CC:"'1POUNDS M/E AMOUNT RRT --------------------------------------------------------------------------------498 CI30 1,4-D!CHL□ROBENZEND-D4 ** ISl ••
710 CI40 NAPHTHALENE-OS •• IS2 ••
1003 cr~o ACENAPHTHENE-D10 •• IS3 ~·
!242 CI60 PHENANTHRENE-D10 •• IS4 **
~621 er:--:, Cr.R'(SE:SIE-D!.2 ** !55 .....
!qOO CI75 ?ERVL£~JE-D12 •• IS6 ••
294 CS50 2-FL~ORCFhENOL ** 3L! **
?hENCL-DS •• SU2 *~
~~ ~, 6-fR!JRCMGF~E~#OL
5~7 CS~•J ;-.J:7ROBEi"l:ZE::NE-D5 ~~ 3U:3 *4
~01 C5~S 2-F~GUORCBIPHEN'(L ~~ su~ **
-~13 CS30 TERP~ENYL-D!4 ❖~ S~6 ❖~
152
136
164
188
240
264
112
::;9
330
82
172
244
14?
40 UG/L
40 UG/L
40 UG/L
40 UG/L
40 UG/L
40 UG/L
·:;> ! 1/.
i , ,.
48 Y.
75 1/.
7 1 'l.
78 1/.
15 UG/L
1. 000
1.000
1. 000
1. 000
1. 000
1. 000
0. 590
0. 938
1. 131
0. 841
0.898
0. 903
1. 025
419JC
13908"
7159:
9125E
540:::C
]407'.:
84:~:
1 ~ -~4,:-::
~601
36631
1424 s:
'1" ....
I
I
I
I
1t
u r.J
X ...,
c,:
1--u
UI n.
lfl
0 r, ,n ...
rl •·•
f(JO.O
P. IC
11 ii 3/86 5: 5:3: 00
SAMPLE: 05-11
COIIOS.: ---
RAIIGE: G 1, 2400
29·1
200
:!: 20
•100
6:•18
DATA: 4Ul1018A13 ff!
CALI: 4Ul101BAJ3 ff3
SCAMS 200 TO 1350
L()BEL: fl 0, 4. 0 Ql_l()II: A 0, I. 0 J O BASE: LI 20, 3 901
i;no
In: 1)C\
710
l"'
800
~.J:-2()
!()03
I Of)n
IS: •10
1134
11 l):J '.
1
. 1242
I .
1~00
_:-r1: nn
I
177920.
SCAII.
TIME
no
u
Cl
,, -fl:: t-u
UI n.
llJ
0
(')
U l
ct
! -
'!! ,. ,.,
100.0
RIC
PIC onrn: 4Ull018Al3 ttl
CALI: 4U1101Bnl3 ff3
SCAtlS 1350. TO 2'100 •
11/ I 3/86 5: 53: 00
SAMF'LE: 05-11
COttOS.: ---
RAtft~E: G I, 2401) U'\BEL: ti 0, 4. I) 91Jf\tt: A 0, I. 0 J O BASE: U 20, 3
1518
15':12 -T! 4 ~~-.:.xc.», ,.__"1,,J.,,.1J,_~ _ __.,
1480 1600
1681
!---.·, ( L,,_•
47104,
l '.100
1993 207? 2145 220 I 2282 2338 •""-. ...,>&.• ...... ,J_.,•.,,.,_,...,._..,._. ____ .. ,_ ._.,( ...... , ........ -•••·••Ll._"1'.J•••-• . ...-..... ..-... ...-, ............................ _...~ .. ,~
2400 SCAtl .
40:00 TltlE
ORGANICS ANALYSIS DAiA SHE~T AC[OS Laooratory Name:. Spectrix Sample ~umber: OS - / .2.. Lao Sarapl e .ID No.:· ,?b//o/?/,j. Sample i-latrix: Water Data Rel ease Authorized By~ Date Sample Rec~ived: _ 1#t' Concentration: Low Units: ug/L Date Extracted: ///7/4-£ Cone/Di 1 Factor: / __ ...;.._ __ _ ' Date Analyzed: // //::,./J'b Ccmpounds Detected: 0 > NPOES #· CAS # COMPOUND lOA 108-95-2 ? heno l J.A 9:,-:,/-8 2-Ln I ord_oneno i OA oo-, :i-:i L-N1 ';;ro\)neno 1 ~;r, l \T:,-o T7:g ~,~-0,methypnenol 2A J. 20-83-2 . 2 ,4-u,cnloropneno\ ,:s;I" :-iY-;jO-i p-~nioro-m-creso! .u.A 28-Do-Z Z,4,o-1r1cnioropneno1 :,A :ir:7B"-:i Z,l-u1n1t~opnenol T:I. ,D0-02-1 l-N1 tropileno 1 :+A_ :,34-:iZ-I l,o-J1n1cro-Z-Mecnylpnenol ilT-3"6-:i ,encacn1oro9nenol U = Undetected at the 1 i sted detection limit J = Ccmpound i.s present, but below the listed detection limit a.= Compound also found in blank 10/85 (OADAWZl -----RESULT 10 U Iu u N7J rtJ7]' 10 U rtJ7]' rtJ7]' 50 U :,ui]' SulJ ;TI u
FiLCNAME
CALI3 STD DATE
~S-12
4U11018A14
:.<.EYSTONE
11/13/96 6:44:00
11/7/86
SPECTR!X DC ~ ----14
INST ID.
'ANALYST
4530
YPH
VERirIED BY fr?!
CORR. FACTOR 1. 00
--------------------------------------------------------------------------------
4'?8
7:0
10,:,2
1242
1621
:co,:.o
.2'° 4
cr30·
C!40
CI50
CI60
CI70
CI75
-:S50
CS45
C35S
CS25
CS::?O
C7J5
SEMIVOLATILE COMPOUNDS
l,4-DICHLOROBENZEND-04 •• ISl ••
NAPHTHALENE-OS •• IS2 **
ACENAPHTHENE-010 ** IS3 **
PHENP..NTHRENE-D10 ** IS4 **
CHRYSENE-D12 ** IS5 **
?ERYL~NE-012 ** IS6 **
2-rL.UOROPHENOL *.,. SUl -s-•
?hENCL-05 ** SU2 4~
2, 4,6-TR!3ROMGPHENOL ••SUS**
NITR08ENZENE~D5 .... SU3 ••
2-~LUUCROBIPHENYL •• SU4 •*
T~~?HEN'(L-D14 ~* SU6 •~
s:sc2-£THYLHEXYL)PHTHALATE
152
136
164
188
240
264
112
99·
330
92
172
244
149
AMOUNT
40 VG/L
40 UG/L
40 VG/L
40 VG/L
40 VG/L
40 VG/L
103 :r.
75 1/.
94 1/.
85 7.
81 1/.
76 :r.
3 UG/L
RRT
1. 000
1.000
1.000
1.000
1. 000
1. 000
0. 590
o. 938
1. 132
0. 841
o. 898
0. 903
1. 026
335~:;
111872
56817
695•)7
3456'7
17734
! SO~(
J:6·77
13340.J
3..;9s.;
3:37C
,.
u u
X
H
r>:: f-
Ll
IJI n. trJ
(.l
I') ,,
<t
.. r.,
H
RIC DIH(1: 4IJ110181H4 #1
ll/13/86 6:44:00 cnLI: 4IJII018A14 H3
5(1MPLE: 05-12
COHOS.: ---
RAt!GE: G 1,2400 LA8EL: ti 0, 4.0 QIJ(lll: Ii 0, 1.0 J 0
100:0-
\
PJC
-
-
f:00
:~: 28
294
467
498
710
SCAI 15 200 TO I ~':i(l
8~1SE: IJ 21), 3
901
1002
1242
1134
-~,_,_1.1£ l~1:. .,_ 1305 -·r-----·-----·-,-~.:::::~:;'.:.::=--~~'.::,::~
1000 120')
tG: 40 20: 00
136704.
SCAIJ
TIME .
,.
u
0
X
H
O'. ,-u w
{L
Lil
(J
[')
"' ,,.
1-
'l'
,-:
100. 0
RIC
P.IC
11,13,86 6:44:00
SAMPLE: 05-12
COJIOS.: ---
P.llflGE: G l, 2400
I •l•JO
2:J: 20
1518
DnTA: 41Jll0181H4 ff!
CALI: 4UJIOIBAl4 tt3
5Udl5 1350 TO 2400.
LABEL: H 0, 4.0 QUAN: n 0, 1.0 J 0 BASE: IJ 20, 3
11))0
2f.1•lfJ
1681
I. 724
1817
I (:(l(l
J(t: (11.i
1900
)(H)l)
:?,,?,: 20
t;'i1<J
:':P:: ·10
32096
2400 SCAtl.
•11J: OCJ TI ME
ORGANICS ANALYSIS DATA SHEET
ACIDS
Laboratory Name: Spectrix .
Lab Sample II) tio.: ~6//~/t?' IS-
Data Release Authorized.By:~
Sample Number: Inlet HeJ[;a Ponci
Sample Matrix: Soil
Date Sample Received: // /1/4f ~,
Concentration: Low Units: ug/Kg
Date Extracted: I/ /7 /a.b ---'~,..__L ____ _
Date Analyzed: // /( 3 /? f --;--,L---...,_--'---':,__--
Cone/Oil Factor: ---T=i--={)'--_
Compounds Detected: __ 0=---
MPDES II
lOA
iA
6A
3A
2A
3A
llA
SA
7A
4A
9A
CAS ~
108-95-2
"5-57-8
88-15-5
105-67-9
120-83-2
~9-50-1
88-06-2
100-02-7
534-52-1
S/-Sli-5
CCf.lPOUND
Phenol
2-Chior::ipnenol
2-Nltropnenol
2,4-Dimetnyphenol
2,4-Dichlorophenol
p-Chloro-m-cresol
2,4,6-Trichlorophenol
2,4-01n1trophenol
4-Nitroohenol
4, 6-Di n i tro-2-Methy]pheno 1
Pentachlorophenol
U = Undetected at the 1 isted detection 1 imit
J = Compound is present, but below the listed detection limit
B = Compound al so found in blank
RESULT
<100 U
400 U
400 u
400 U
4D0 U
400 u
400 U
2000 U
2000 U
2000 U
2000 U
:)ATE IN.JEC,ED
C,:>LIB STD DATE
DC # ----14
3E~IVOLA,!LE sor~ REPORT
INLET ME~LlN POND
;.<,EYSTONE
11/13/86 3:27:00
l·! /7 /86
!NST ID.
ANALYST
4530
YPH
VERIFIED BY~
CORR. FACTOR 44, 00
--------------------------------------------------------------------------------SCAN# SE~!VOLAT!L~ CG~POUNDS M/E AMOIJNT RRT --------------------------------------------------------------------------------497 CI30 1, 4-DICHLOROBENZEND-D4 ** !S1 ** 152 1760 UG/KG 1. 000 43673 710 CI40 NAP'-/TH,'\LENE-D8 ** IS2 ** 136 1760 UG/KG 1. 000 161 !07 !002 crso ACENAP'-/THENE-D10 ** !S3 ** 164 1760 UG/KG 1. 000 78585 !242 C:i'.60 PHENANTHRENE-D10 ** !S4 ** 188 1760 UG/KG 1. 000 9026! 1630 C!70 c:~R-..tSE>IE-D 12 ** !S5 ** 240 1760 UG/KG 1. 000 351?.: :3c;q C!75 P£RYLE!\JE-D12 ** ~ ,-' .... J, ='0 264 1760 UG/KG 1. 000 27S6l 298 C.S50 2-F:_lJCRGP\.JENOL ;H-·3u1 ** 1 . :,· "-74 1/. 0. 600 67971 .:!67 CS45 ::;~E'.'IGL-DS ** SU2 _, * 99 68 1/. 0. 940 1042·3S ~:~4--,-c:;-7 ·+-6-TRI3ROMCPHENCL ..... SUS ** 330 61. 1/. 1. 132 ! ~~-?•:: L..::, .... :, =-·'
596 •:.S2·) 'I: TRCl3E/•iZSi'IE-D5 .,..,, Sl'3 ...... 82 -S7 1/. 0, 839 3:;q1,.:
'?C! ,:s2s 2-FLUUORGBIPHENYL ...... SU4 ... ... 172 66 1/. 0. 899 14357(
151'8 ,: S:JO TER?~ENYL-D14 ** 3U6 ** 244 106 1/. 0. 904 , -~ -,-4 ,' .I.-);
,t ...
I
I I
I
#
LI
0
X
H
n:
f-u
L• I n.
OJ
0
11
U!
-1·
..
0 -
f·
lf] ;,: ...
100.0
PIC
\
RIC
ll/13✓86 8:27:00
DATA: 4U!l018Al5 ff!
CALI: 4Ull018A15 ff3
SCAHS 200 TO 1350
Sl'ltfPLE: HILET MEDLifl POflO
COIIOS.: ---Rf~IIGE: G I, 2400 LABEL: H . 0., 4. 0 QUAIi: A 0, 1. 0 J 0 BASE: U 20, 3
251
298
437
467
?DI
1003
1 ~qr; 113,1
1242
1281 \; \ ~~~J~-~~~-'~J -32Jl,.~-·~__,I,,~ 7'r_~ 1072 ~ 1 I 82 _T ____ ·····. --,--=a==---~~=~-.i,:~~=~=~lc!!.:4-!<===
2DO 400 c-00 800 IDOO
:~: 2(t 6:~0 IIJ1fH) .1:i:)(1 lf.:4(1
1200 :·n, nn ... . ' ...
416256
SCAfl
TIME
<t ...
I
I
I
I ,.
u
Cl
X
~
n:
1--
()
UI n. LO
1-
Ul ;,~ , ..
100.0
PIC
RIC O(iTf): 4IJ11018(115 Ul SCAl/5 1350 TO 24(H),
11/1:3,86 8:27:00 Clill: 4IJ1Wl81H5 113
SAMPLE: JHLET MEDLHI POIID cc,,,os.: ---
PAI/GE: G 1,2400 Lr1BEL: H 0, 4.0 Ql_l1~JI: A 0, 1.0 J 0 8(l5E: U 20, :3
1518
1424
1'100
~:: ): 28.
1614
1600
26140
1680
1831
1899
;,ooo
33: 20
22(H)
:,:r,: ·10
23~3
53632
2400 SCAJl
40100 TIME
ORGANICS ANALYSIS DATA SHEET
ACIDS
Laboratory Name: Spectrix .
Lab Sample IIJ '!o,: 16//c;,/tf /6
Data Release Authorized By:~
Concentration: Low
Date Extracted: 11/7µ£.
Date Analyzed: // /2.:s /rl J J
HPDES If CAS ii
lOA 108-95-2
IA 95-57-8
oA 88-15-~
3A 105-67-9
2A 120-83-2
8A 59-50-1
llA 88-06-2 SA 51-28-5
7A 100-02-7
4A 534~52-l
9A 87-8ii-5
_Sample Number: ]);sci, 4 'Je Hedbn Pond
Sample Matrix: Soil
Date Sample _Received:_ 1/ /7/,y,t
'
Units: ug/Kg
Cone/Oil Factor: 4-:o
Compounds Detected: ---""O __ _
Ca-lPOUND RESULT
Phenol 400 U 2-Chloropnenol 400 U
2-Nitroonenol
2 '4-Dl methyphenol
800 U
2,4-0ichlorophenol 400 U 400 U
p-Chloro-m-cresol 400 U
2,4,5-Trichloroohenol 400 U
2 ,4-D1n1 trophenol 2000 U
4-Ni trooheno 1 2000 0
4,6-0in\tro-2-Methylphenol
Pentachlorophenol 2000 II
2000 U
U = Undetected at the listed detection limit
J = Compound is present, but below the listed detection limit
· B = Compound al so found in blank
CLIENT
CALI3 STD iJATE
;:;c it ----1 ..
:.3EM!','.CL"-TILE SOIL REPORT
DISCHARGE MEDLIN POND
4Ull018A16
:<.SYSTONE
,l/13/36 9:19:00
ll/'.1/86
INST IO. 4530
ANALYST YPH
VERIFIED BY ;;t'P7'f
CORR. FACTOR 43.00
--------------------------------------------------------------------------------
SE.~ I ','CLA TI LE C DMPGUNDS M/E AMOUNT RRT --------------------------------------------------------------------------------
681 C I30
959 CI40
1270 CI50
l 51 1 •:: I 60
:950 CI71J
2:7,:, CI75
315 CS50
-S46 ,: 34j
: ...:,.03 CS55
s2J c~;;:o
: :66 ,:s2s
• 7:3-/ ,: s::o
1,4-DICHLOROBENZEND-04 ** ISl **
NAPHTHALENE-OS ** IS2 **
ACENAPHTHENE-010 ** IS3 **
PHENANTHRENE-D10 ** IS4 **
CHRYSE~E-012 ** ISS **
?~~'(!....='.NE-012 ** :so <-~
2-~LUGRCPHE~iOL ~• 3C! •4
PHENGL-03 ** SU2 ••
2, 4,6-TR!JROMGPHENCL **SUS**
N!TRGBE~JZENE-05 •~ SU3 **
2-FLUUORCGIPHENYL ** SU4 **
T2RPHEN~'L-D14 ~~ SU6 ~*
152
136
164
188
240
264
112·
99
330
S2
172
244
1720 UG/KG
1720 UG/KG
1720 UG/KG
1720 UG/KG
1720 UG/KG
1720 UG/KG
103 1/.
98 'l.
60 1/.
105 1/.
83 1/.
92 1/.
1. 000
1. 000
1.000
1. 000
1. 000
1. 000
0. 463
0. 949
1. 105
0. 858
0. 918
0. 916
46568
175766
82835
~5650
-l664S
3847:
10025;5
1 oC-6-!-C
l 33 i ..i
6307:
18940,::
5668;;:
,t ...
I
I
I I ,.
u 0
X ..
r,_:
I-u
Lt!
(L
I~
(.) n .,
•I
I··
f/1
P.J(: OAHl: 4Ul 1018f)16 ff! SUlllS 200 TO t:350
l l / I 3,--~:6 9: I 9: 00 ((ll! : 4 LI I IO I 8n I 6 H 3
SAMPLE: DISCHARGE MEDLI II POHD
COIIOS. : ---Rril lGE: G 1,240Cl LABEL: 11 0, 4.0 ,;i1x,t1: n 0, 1.0 J O 8f~5E: U 28, :3
100.0 21;2
PIC 11 t.G
960 1270
316
G1G
823
---.,..-'.=-...r:_·~•'-,~~-" '~. ·-r _·, '·1'-··-'".--... ,,...-1 __ /._,, __ ._ \_,. 0~ l~ '. "'---. '.,J .. <',c::,Lc-/..:.:!'•V~o,c: ---'="-' -~ ----=--'--------···--------"-'-----'r--·-----'--r·"'•='·····r~~~,----r.~
;::,10 400 GOlJ :300 1000 1201)
:3:i•r, io:•11) 111:11:1 ; ,1: ,0 IG:·10 Zi.1:f)Q
395264
SCAll
TlllE
;t
u
Cl
>< •·· cr.:
f-u ~,
(L tn
,_,
n ' . . ,.
I··
Ul . ::
100.0
PIC
lJ/[3/86 9:19:00
S(lMPLE: DISCHARGE MEOLltl POHD
DATA: 4Ull018Al5 ttl
CALI: 4Ull01BAl6 #3
SCAtlS 1350 TO 24rJO.
f)JIIDS.: ---
PAIIGE: G I, 2400 Ul!3EL: II 0, 4.(1 QIJrdl: fl 0, I. 0 J O BASE: U 2@, :3
I •1[13
14()0
?'?: :-~IJ
1511
IGIJ!J
i.'6: 4Q
1645
1788
------,--·----
! 8(1(1
::ii: no
1930
13:34
2088
JJ:20
2077 2163
--·,-·---,--.
22ftD
]>,: ·10
2273 75392
2352
l
2400 SCAii .
4'3100 TIME
L.Lw 3L.C(.
4B11018C01
CLIENT
il/.12/86 15: 12:00
CALIO STD DAT~ 11/7/86
S?~CTRIX DC# ----1-l
INST ID.
AN,',LYST
4530
YPH
VERIFIED llY ~
CORR. FACTOR 1. 00
--------------------------------------------------------------------------------SCANlt SE'1 I '✓OLA TI L:C: CGMP-□UNDS M/E AMOUNT RRT MREA --------------------------------------------------------------------------------525 CI30 • 4-DICHLOROBENZEND-D4 ..... IS1 ** 152 40 UG/L 1. 000 2258:J " 731 CI40 NAPHTHAL::NE-D8 ..... IS2 ** 136 40 UG/L 1. 000 74823 1024 CI 50 ACENAPHTHENE-D10 .... IS3 ** 164 40 UG/L 1. 000 43673
1268 CI60 PHENANTHRENE-D10 ** IS4 ** 188 40 UG/L 1. 000 4851C 1713 CI70 CHRYSENE-D12 ** !S5 ** 240 40 UG/L 1. 000 2151:: .t q36 rT-,,9 .., -I -?ERYLENE-012 ..... IS6 ..... 264 40 UG/L 1. 000 1297~
33'? ,:sso .2-;::-;_'JCRCPHENOL .::;.4 SU! .... 1 1 """! -~ 35 1/. 0. 646 • "7 C:,"\ • ! , ·.J ... -495 ,:54.5 ? !-;~;--.ICL -D 5 ** SIJ2 ,. .. 99 61 1/. 0. 943 SG-36,;: : : se CS:55 ' ,l, ~-fR!JROMOPHENDL ** SUS ~-<H> 330 53 1/. 1. 131 65]~
. ---=.::::.. '.J •=~2r] >JI 7ROBE~IZ~NE-D5 ,..,. SUJ ** 82 91 1/. 0. 848 24():3C
'7·21 CS25 2-=LUUCRGBI?HENYL ..... ;u.; ** 172 76 1/. 0. 899 0. - - -. ..::) ::J :;i._
~::~8 CS30 :'C:RPl-iENYL-D14 .. ,. SU6 .,,. .. 244 1 ~,., G~ :~ 0. 904 3.19,~
~.; 7 C61S ~-N:TR □SODI?HENYLAMINE 169 2 UG/L 0. 905 1 ""') ., .-:;:.--,.,_
~ ...
I
I I I
"' u
Q
X
~
c,:
f-u
UJ n. II)
0 n
" .,
RIC
11 1 12✓86 15:12:00
SAMPLE: LLH BLK
COt105.: ---
RAIIGE: G L 2400
DrH(I: 4BI l018C01 Ill
CALI: 4811018COI #3
SCAIJS 200 TO 1350
LABEL: t·I O, 4. 0 Ql_lf~H: A 0, 1. 0 J 0 BASE: IJ 20, 3 921
100. 0-
PIC
-348
1025
731
495
1268
_.
1153 620
"'---.~_;__,..-, ,____-\. ... ( " \1, I\. \ . I~ 1234 ' ~_:::=::=;:'..:=:''.._~:;:,==d~ .~==1,,.!·--1~:::,,,,.-.--,-_...J __ ..,. '--•-r==-·,,,. ..... ._,..L...=,,.....,1--L·~---,.--...c!~~.,...!;l~..l..::"'"-,-
?'10
·~: 2D
tf 0[) f;C)I) 808 l 000 1700
~.: •10 I 0: t:H1 I-~: 20 16: 40 20: 00
104448.
SCAfl.
TIME
'1" ....
I
I
I
I
#
u
Cl
X .....
r,:
f-u LL!
IL
1/J
0
{1
~' ....
100.0
P. IC
RIC
ll/12/86 15:12:00
snMPLE: LLH BLK
onrn: 4e1101sc01 1t1
cnLI: 4811018C01 #3
SCAtlS 1350 TO 24()0
COHOS.: ---
RflflGE: G 1,2400 L"1BEL: ft 0, 4.0 Ql_lf1li: A 0, 1.0 J 0 BASE: U 20, :3
1548
1713
.1936
32352.
14A3 I I 1 ;,sr. 2031 2112 2227 2317 _,.J,~~-.;.;.. \ 1672 \. r-1835 19_~2 "~-~~--~··-··---, .... ~-~~-·~~~----~~--
----7. ------,:=~~==~-""',-. ~-"· ---i-·-·_.___,.,c.."'-,-----.-----.-----,----~--~
1400 1600 1800
23:20 26:40 ~n:nn
2001}
'33:20
24013 SCAH .
40:00 Tlt1E
sr.MPL:=: .z D. :-"iLE:N;;~t= ·-,::LI ::'.NT :JMTE IN.JE•:""'.""ED CAL!B STD DAT~ S? ZC:~~ .: -~ cc~----!.➔ SE~iVpLAT:~E SO!L RE?ORT c..L3 3LK 4Il1l018A02 ;.t.EYSTONE l!/13/86 7: 36:00 11/7,'86 INST ID. ANALYST 4530 YPH VERIFIED BY ~ CORR. FACTOR 33.00 -----------------------------------------------SCAN# SE,'1I','OLATIL::'. CG,''.FOUNDS M/E AMOUNT RRT Ar'.SA -----------------------------------------------------500 CI30 1,4-DICHLOROBENZEND-D4 ** ISl ** 152 1320 UG/KG 1. 000 4,---... ::,, _; 711 CI40 NAPHTHALENE-DB ...... !S2 ** 136 1320 UG/KG 1. 000 153353 1003 crso ACENAPYTHENE-D10 ..... IS3 ** 164 1320 UG/KG 1. 000 75-1 s:;: 1243 CI6V PHENANTHRENE-D10 ..... IS4 . ... 188 1320 UG/KG 1. 000 97656 .:. £:32 CI7iJ Cl~F.YSE:'.JE-D 12 ** ISS ** 240 · 1320 UG/KG 1. 000 5755: ~ :=c 1 -r--? ER YLE:SIE -D 12 ** ,56 ** 264 1320 UG/KG 1. 000 3-::;:c;-. I..., .. ' :i , --. -· :o·s csso 2-FLUCRCPHENOL *<E-3U1 ..... 112-108 1/. 0.610 ·?soi:=~ 4-70 CS~5 . :J~ENGL-D'.: -cf--1'.f SU2 44-·-:,9 ·:;>4 ✓~ 0.940 l JEc2: :,35 CS55 2. 4, 6-TR!JROMCPHENOL ~4 SUS ** 330 48 1/. 1. 132 ;5~; e--~-.-::i CS20 NITRGEE~lZ~NE-DS •~ SU3 *• 82 1oJ1 :r. 0. 841 5~7.2: ~02 C·:325 ~-F"i_l_it.)IJRCB ! PHENYL *4-SU4 ..... 172 83 1/. . 0. 899 1-·--/ ! ::, .' :: : ==~:) -,: SJO TE"?f-iEiiYL-Dl '+ ** SLi6 ~ .. 244 1 02 1/. 0. 904 741 ;.:
<t ..,
I .
I
I
I
c!t
u
Q
X
~ ~: ,_
u UI n..
l~
L' l'I
~)
•t·
.. n ,.,
, ..
trJ ,.
RIC Dn T!l: 4 B 110 I 8A02 ff I SCAtlS 200 TO 1350
11/13/86 7:36:00 CALI: 4B11018f102 ff3
SAMPLE: LLS BLK
COtlOS.: ---PhllGE: G 1, 2400 LABEL: H 0, 4. 0 QIJ(III: A 0, I. 0 ,I O BASE: U 20, 3
100.0 26>)
Rl.C
305 470
500
~ ~\ Jr,, .
',~J~,~_J
~·i)lJ ,11_1n
-?:21? G: ~ri
i 11
'.302
1004
1243
11:3s I
863 \ 1n_51 -A 1207 \ 1~83
""-----1-"'-__:...;.;;.; _ __,__11,.,~ . '-&T
j 1_il_1()
Jf:-: ·10
I /01)
20:00
453120.
scn11 .
TltlE
#
u
Cl
X ~· 11:
I··
'-' UI n. "'
Q
('I
ifl ..,.
100. 0
pre
RIC
11/1:3/86 ,:'.36:00
S()MPLE: LLS BLK cm,os.: ---rn,~E: G 1,2400 1520
onrn: 4e1101en02 n1
CALI: 4B11018A02 flJ
semis 1350 ro 241}@.
l(18EL: N 0, 4.0 Q.UAtl: () 0, 1.0 J O BASE: U 20, 3
1682
1901
2026 2129 ___,,._....__ . ...._._
71552
22·16 2362 __ .::.::,;.,;......._._..-..------...._._.._,_ _J,1?l,.__....J l.-=......,.-1..,,6.___22......,,.,JL"' ----_ L __ . -r···---------··, l ,---··---···-·· · ··-,-··· -------,-----~,-----.------..-----~--~
I ,100 I GOO l 80tJ 2000
33:20
2200
3ft 40
2400 SCAIJ
40:01) TIME /~170 26140 30:Qtl
SPECTRIX MOl✓ROEVILLE
>2LE OF CONTENTS PRODUCED ON 02/02/87 AT 09:28 PAGE
;r.-iPL E # SOURCE DESCRIPT DAT-COL RATE-REC
------------------------------------------------------------
70,10197 05-1 JOHN MEDLIN \I/ELL 01/14/87 01/ 15/87
7010198 05-2 . GEORGE HARDY \1/E LL 01/14/87 01/15/87
7010199 05-3 MR_S. BAKER WELL 01/14/87 01/15/87
7010200 · 05-4 ROY MEDLIN \1/E LL 01/14/87 01/15/87
7010201 05-5 TRIANGLE MATERIALS 01/14/87 01/15/87
7010202 05-7 JAMES CRO\1/E \1/E LL 01/14/87 01/15/87
7010203 OS-8 SH I LOH BAPTIST CHRCH 01/14/87 01/15/87
7010204 05-9 \II I LL I AM BARBER \I/ELL 01/14/87 01/15/87
7010205 05-10 RIFS 01/14/87 01/15/87'\ p\ c:.~--"-
7010206 OS-10A RIFS 01/14/87 01/15/87 ( " c"eto.J.."\
7010207 05-11 RIFS 01/14/87 01/15/87 I
io 1020a 05-12 RIFS 01/14/87 01/15/87 I I
7010209 05-13 RIFS 01/14/87 01/15/87 -· )
SPECTRIX MONROEVILLE 2
=-======---=======------------------====----------·
3LE 1: SUMMARY OF ·ORGAN I_C COMPOUNDS PRODUCED ON 02/02/87 AT 09:30 PAGE
::,PLE ll TEST # RSLT.LNE SOURCE
----------------
OPROPYL ETHER
·010197 IPE lsopropyl Ether , u g /_L :
'010196 IPE I sopropy 1 · _Ether ,ug/L:
'010199 IPE 1sopropy1 Etner,ug/L:
'0 10200 IPE 1sopropy1 Ether,ug/L:
'010201· IPE 1sopropy1 Ether,ug/L:
'0 1 0202 IPE 1sopropy1 Ether,ug/L:
'0 10203 IPE ,1sopropy1 Etner,ug/L:
'0 10204 lPE .. 1 sopropy I Ether,ug/L:
'010205 IPE 1sopropy1 Ether ,Llg/L:
'01 0206 IPE lsopropyl Ether,ug/L:
·010207 IPE 1sopropy1 Et11er ,ug/L:
'0 10·208 IPE 1sopropy1 Ether,ug/L:
·,) 10209 IPE lsopropyl Ether,ug/L:
-~TACHLOROPHENOL ~.
:i0197 PCP\/,,~PCP, ug/L: 1. 07
)10196 PCP PCP, ug/L: < 1 . 00
. ,, 0 19·;; PCP PCP, ug/L: < 1 . 00
: ,0200 PCP PCP, ug/L: < 1 . 00
: , 020 \ PCP PCP, ug/L: < 1. 00
. 10202 PCP PCP, ug/L: 8.68
)10203 PCP PCP, ug/L: 20 :•6'
)~0204 PCP PCP, ug/L: 14.0
'G'.0205 PCP PCP, ug/L: 5.47 ½ ~o 10206 PCP PCP, Ug/L: 7.50 .J
',) 10207 PCP PCP, ug/L: 2. 15
')~0206 PCP PCP, ug/L: < 1 . 00
0~0209 PCP PCP, ·ug/L: 5.71
.Lf '{ . 7 ,, ,{_,/, ..
V ,J /:::..U..(J~rr / -/! (?"'(;_'7_,,_' l.l .. •·' /
< 1. 00
< 1. 00
< 1. 00
<1.00
<1.00
< 1. 00
6_0. 9
17.5
< 1. 00
<1.00
< 1. 00
< 1 . 00
< 1 . 00
~-:..
OS-1
OS-2
OS-3
0S-4
OS-5
OS-7
OS-8
·OS-9
OS-10
OS-10A
OS-11
OS-12
OS-13
OS-1
0S-2
OS-3
0S-4
OS-5 ·
OS-7
OS-8
0S-9
OS-10 I i\,rj;.c.5
OS-10AJ
os-11
os-12
OS-13
o'.,c_/-C.....,j) ::er-~ >r~c)· ....£~ 'i /_,~ 7,_,,, ~
;:,
G-C 0 0 er ,r-0-{,,_r....d.
/JL(./t~ () cf ;j,,-("·{c-f'r_.!-&::, · -" I ./ c-f C (I,,~ ,.__
,:,..,,n_.f, 1,£. /! .
1·
f/ ,t -L,,v ;:·-(_:/ i'-,11'"~.
/~..,!
! • I SPECTRIX MONROEVILLE '-'
3LE 2: SU!v"MARY OF ·ORGAN 1.C COMPOUNDS PRODUCED ON 02/02/87 AT 09: 30 PAGE
TEST# RSLT.LNE SOURCE
-----------------------------------------------------------------------
ENOLS CBY EPA METHOD 604)
010197
"010199
7010200
GC604
GC604
· GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604.
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
Pheno I ............. .
2-cn1oropneno1 ..... .
Pentacn1oropheno1 .. .
4,6-Dinltro-o-cresoi
2,3,5,6Tet-Cl-pnenol
2,4,6Trichloropnenol
4-Nitrophenol ...... .
2,4-Dinitrophenol .. .
4Cnloro3metny1pneno1
2,4-Dichlorophenol ..
2;4-Dirnetny1pneno1 ..
2-N it ropheno I ••••••
2-cn1oropneno1 .....
Pheno I.-.•..•••
2-Nitropnenol ..... .
2,4-Dirnetny1pneno1 ..
2,4-Dichloropnenol.
4Chloro3rnetny1pneno1
2,4-Dinitropnenol .. .
4-Nitropnenol ...... .
2,4,6Tricn1oropneno1
2,3,5,6Tet-c1-pneno1
4,6-Dinitro-o-cresol
Pentacn1oropneno1 .. .
Pentacn1oropneno1 .. .
4,6-Dinitro-o-cresol
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
4-Nltropnenol ..... :.
2,4-Dinitrophenol .. .
4Chloro3metny1pneno1
2,4-Dichlorophenol ..
2,4-Dlrnethylphenol
2-Nitrophenol ... .
Phenol ........... .
2-cn1oropneno1 ... .
2,4-Dirnetny1pneno1.
2-N it ropheno I .
2-Chloropnenol ... .
Phenol ............ .
Pentacn1oropneno1 ..
4,6-Dinitro-o~cresol
2,3,5,6Tet-Cl-pneno1
2,4,6Trlchloropnenol
4-Nitropnenol ...... .
2,4:Dinitropnenol .. ·.
4cn1oro3rnetny1pneno1
2,4-Dlchloropnenol.
ne acove results are reportea in ug/L.
· <O. 1·25
< 0, 125
<0.250
(0.250
<0.250
(0.250
(0,250
<0.250
< 0. 125
< 0 . 1 25
< 0. 125
< 0 . 125
< 0, 125
-(0,125
< 0. 125
< 0 . 1 25
< 0. 125
< 0 . 1 25
(0.250
(0.250
.(0.250
(0.250
<0.250
(0. 250
<0.250
(0. 250
(0.250
<0.250
(0,250
<0.250
(0. 125
< 0 . 1 25
< 0, 125
(0. 125
(0. 125
< 0 . 125
< 0. 125
< 0 . 1 25
(0. 125
(0.125
(0.250
(0.250
<0.250
(0,250
<0.250
(0.250
< 0 . 125
<0.125
0S-1
OS-1
os-1
OS-1
OS-1
os-1
OS-1
OS-1
OS-1
OS-1
os-1
0S-1
0S-2
OS-2
OS-2
0S-2
OS-2
OS-2
OS-2
OS-2
0S-2
0S-2
OS-2
0S-2
0S-3
0S-3
os-::;
0S-3
OS-3
0S-3
05-3
OS-3
OS-3
0S-3
05-3
0S-3
05-4·
0S-4
OS-4
OS-4
OS-4
0S-4
05-4
0S-4
05-4
OS-4
OS-4
0S-4
SPECTRIX MONROEVILLE
3LE 2: SUM\1ARY OF ORGAN I_C COMPOUNDS PRODUCED ON 02/02/87 AT 09: 30 PAGE
-.,PLE # TEST # RSL T. LNE SOURCE
-----------------------------------------------------------------------
010201
010202
·.)~0203
1010204
GC604
GC604
GC604-
·oc604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604.
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
·2-cn1oropneno1 ..... .
Pneno I ............. .
2-Nitropneno1 ...... .
2,4-Dimetny1pneno1 ..
._P':)_ntacl1 ro.ropti~.no 1· ...
4,6-Dinitro-o-cresol
2,3,5,6Tet-Cl-phenol
2,4,6Tricnloropnenol
4-Ni~ropnenol ...... .
2,4-Dinltropnenot .. .
4Chloro3methylpnenol
2,4-Dicn1oropneno1 ..
4-N it ropneno I ..... .
2,4-Dinitropnenoi.
2-cn I or-opneno 1 ..
Pneno I. . .... .
2-Nitropnenol ... .
2,4-Dimetny1pneno1
2,4-Dicn1oropneno1 .'
4Cnloro3mecny1pneno1
Pentacn1oropneno1 ...
4,6-Dinitro-o-cresol
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
2-cn1oropneno1 ..
Phenol ............ .
2-Nitropnenol ..... .
2,4-Dimetr,y1pneno1 ..
2,4-Dichloropnenol ..
4Cntoro3metny1pneno1
2,4-Dinltropnenol ...
< 0 . 125
<O. 125
< 0 . 125
< 0. 125
,_o·. 650
<0.250
(0. 250
<0.250
<0.250
<0.250
< 0. 125
<O. 125
<0.250
<0.250
<O. 125
<O. 125
<O. 125
<O. 125
< 0 . 1 25
<O. 125
<0.250
<0.250
<0.250
(0.250
(0. 125
< 0 . 1 25
(0. 125
< 0 . 125
< 0. 125
0.442
<0.250
GC604 4-N it ropneno I. . . . . . . o. 840
GC_<30"!.._ ____ P_t,ntacn_1_oropneno1 ·.• .. •---'-28.8
GC604 4,6-Dinltro-o-cresol <0.250
GC604 2,3,5,6Tet-Cl-pnenol 8.53
GC604·
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
2,4,6Trtcn1oropneno1
Pentacn1oropneno1 ..
4,6-Dlnitro~o-cresol
2-cn I oropneno 1 .. .
Pt;eno I ............. .
2-Nitropnenot ...... .
2,4-Dimetnytpnenol.
2,4-0icnloropnenol ..
4Cntoro3metny1pneno1
2,4-Dinitropnenol .. .
4-Nitropnenol ...... .
2,4,6Tricn1oropneno1
2,3,5,6Tet-c1-pneno1
<0.250
0.392
<0.250
< 0 . 125
< 0. 125
< 0 . 125
< 0. 125
< 0. 125
0.290
(0.250
0.271
<0.250
<0.250
ne above results are reported in u~/L.
OS-5
OS-5
OS-5
OS-5
/.OS-5
OS-5
OS-5
OS-5
OS-5
OS-5
0S-5
OS-5
OS-7
OS-7
OS-7
0S-7
OS-7
OS-7
OS-7
0S-7
0S-7
OS-7
OS-7
0S-7
0S-8
OS-8
OS-8
0S-8
OS-8
OS-8
OS-8
.OS-8
0S::c 8 ____ _
os-a
OS-8
OS-8
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
. OS-9
OS-9
OS-9
SPECTRIX MONROEVILLE
.~LE 2: SUrtMARY OF.ORGANIC CQV,POUNDS PRODUCED ON 02/02/87 AT 09:30 PAGE
,.,,\PLE # TEST # RSL T. LNE SOURCE
------------------------------------------------------------------------
'0 10205
70 10206
·010207
'010208
GC604
GC604
GC604
.GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
Gc'604
GC604
GC604
GC604
GC604
GC604
GC604
GC604·
GC604
GC604
GC604
.GC604
GC604
GC604
GC604
GC604
GC604
GC604
GC604
c2-Chlorophenol .... .
Phenol ............ .
2-Nitrophenol ..... .
2,4-DimethyiphenoJ.
2,4-Dich1oropheno1:.
.'4Ch' Io ro3me t h)l°J"pheno·1.
2,4-Dinitropnenol, ..
4-Nitrophenol ...... .
2,4,6Trichlorophenol
2,3,5,6Tet-Cl-phenol
4~6-Dlnltro-o-cresol
Pentachlorophenol ...
Pheno I •••••••••••••
2-Chlorophenol ..... .
Pentacn1oropheno1 .. .
4,6-Dinitro-o-cresol
2,3,5,6Tet-c1-pneno1
2,4,6Tricnloropnenol
4-Nitropnenol ...... .
2,4-Dinitrophenol .. .
4Chloro3methylphenol
2,4-Dlcnlorophenol
2;4-Dimetny1pneno1 ..
2-Nitropnenol ...... .
2-Chloropheno1 ..... .
Phenol ............. .
Pentachloropnenol .. ,
4,6-Dinitro-o-cresol
2,3,5,6Tet-Cl-phenol
2,4,6Trlchlorophenol
◄-Nitropnenol ...... .
2,4-Dlnltropnenol .. .
4Chloro3metny1pheno1
2,4-Dichlorophenol ..
2,4-Dimetnylphenol ..
2-N It ropneno I.
2-Chlorophenol
Pneno I ....... .
2-N It ropheno 1 .
2,4-Dimethylpnenol.
Pentacn1oropheno1 ..
4,6-Dlnitro-o-cresol
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1or6pneno1
4-N it ropneno I •••••••
2,4-Dinitropnenol ...
4Chloro3methylphenol
GC604 2, 4 .:o i Ch I oropheno I .
1e above results are reported in ug/L.
< 0. 125
<0.125
< 0. 125
< 0. 125
< 0. 125
0.609
<0.250
0.767
(0,250
<0.250
0.526
1. 24
< 0. 125
< 0. 125
<0.250
(0,250
<0.250
(0.250
1. 00
(0.250
0.539
.<0.125
(0.125
(0, 125
2.44
< 0. 125
1. 22
0.746
<0.250
<0.250
0.584
<0.250
0.622
<O. 125
<0.125
<O. 125
<O. 125
<0.125
< 0 . 1 25
<O. 125
(0,250
6.74
(0.250
<0.250
0.574
<0.250
0.424
(0. 125
OS-10
05-10
05-10
05-10
OS-10
.os-10 ./
OS-10
05-10
OS-10
OS-10
OS-10
os-10
OS-10A
OS-10A
OS-10A
OS-10A
OS-10A
OS-10A
OS-10A
OS-10A
OS-10A
OS-10A
OS-10A
0S-10A
os-11
os-11
OS-11
OS-1 \
OS-11
OS-11
OS-11
OS-11
OS-11
OS-11
OS-11
os-11
os-12
OS-1·2
OS-12
os-12
os-12
05-12
05-12
OS-12
05-12
OS-12
os-12
os-12
SPECTRIX MONROEVILLE
,3LE 2: SUr.","1ARY OF-ORGAN 1.C COMPOUNDS PRODUCED ON 02/02/87 AT 09:30 PAGE
---------------------.----===
;;:,;:,LE # TEST # RS LT. LNE SOURCE
------------------------------------------------------------------------
;Q'\0209 GC604 ···.2-cn I oropneno 1
GC604 Pneno 1 ............
GC604 2-Nitropnenol .....
.GC604. 2,4-Dimetny1pneno1
GC604 2,4-Dlcn1oropneno1
GC604 iCn 1 o ro3me t ny I _pt1eno I
GC604 Pentacn1oropneno1 ...
GC604 ~~6-Dihitro-o:cresol
GC604 2,3,5,6Tet-Cl-pnenol
GC604 2,4,6Tricn1oropneno1
GC604 _4·:::-N i t rop-heno 1·:-'. : ...
GC604 2,4-DinitropnenoJ ..
1e above resu I ts are reported in ug/L.
< 0. 1 25
<O. 125
< 0. 125
< 0. 1 25
<O. 125
0.482
(0.250
0.719
(0.250
(0.250
Q.549
<0.250
'-
OS-13
OS-13
OS-13
OS-13
OS-13
.os~13
OS-13
OS-13
OS-13
OS-13
OS-13
OS-13
CX1p I e NO.:
escr.iption:
cote Collected:
-=.te Received:
SPECTRIX MONROEVILLE
870 1.0 197
Jonn Medi in .Wei I
01/14/87
01/15/87
A~PL~ # RSLT.LNE SOURCE
SOPROPYL ETHER
7010197 lsopropyl Etner ..
C:NTACHLOROPHENOL
7010197 PCP ..... 1.07
HENOLS IBY EPA METHOD ~04)
7010197
7010197
7010197
.7010197
-0~0197
··,:,10197
-:,,0197
-::~0197
:·,0197
:,·,0197
~ ~ 0 197
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
2,4-Dicn1oropneno1 ..
2,4-Dimetny1pneno1 ..
2,4-Dinitropnenol.
2-cn1oropneno1 ..... .
2-Nitropnenol ...... .
4,6-Dinitro-o-cresol
4-Nitropnenol ...... .
4.Ch Io ro3me tt,y I pneno I
Pencacn1oropneno1 ...
< 1 . 00
<0.250
<0.250
< 0. 125
< 0. 1 25
<0.250
< 0. 125
<0.125
<0.250
<0.250
< 0. 1 25
<0.250
: ·,0197' Phenol.. .. .. .. .. .. <0. 125
_ acove results are reported in. ug/L.
OS-1
.'OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
OS-1
,mp I e NO. :
,script ion:
,te co11ected:
,te Received:
SPECTRI X MONROEVILLE
87010198
•George·_Hardy \,1e1 I
_01/14/87
01/15/87
;MPLE # RSL T .-LNE SOURCE
,OPROPYL ETHER
1010198 1sopro~y1 Etner ....
~NTACHLOROPHENOL
7010198 PCP ..... (1.00
~ENOLS (BY-EPA METHOD 6041
7010198
7010198
7010198
7010198
7010198
"·)10198
-::~10198
)10198
;10198
. )10198
2,3,5,6Tet-Cl-phenol
2,4,6Tricn1oropneno1
2,4-Dicn1oropneno1.
2,4-Dimetny1pneno1.
2,4-Dinitropnenol.
2-cn1oropneno1 .... .
2-Nitropnenol ...... .
4,6-Dlnitro-o-cresol
4-Nitropnenol .....
4Chloro3metny1pneno1
Pentacn1oropneno1 ...
(1.00
(0.250
<0.250
< 0. 125
< 0. 1 25
(0.250
< 0. 125
< 0. 125
<0.250
(0.250
< 0. 125
<0.250
:, 1 o 1·9 8 · P n e no I . .. . . . .. . . . . . . < o . 1 2 s
a aoove results are reported ;n·ug/L.
OS-2
OS-2
OS-2
OS-2
OS-2
OS-2
OS-2
OS-2
0S-2
OS-2
OS-2
OS-2
OS-2
OS-2
SPECTR I X MON ROE·V I LL E
-----~===-=-=-------------------------------------
~nple NO.:
script ion:
te col 1ectea:
te Receivea:
87010199
Mrs, BaKer we'I 1
01/14/87
01/15/87
;,',PLE # RSL T. LNE SOURCE
.OPROPYL ETHER
010199 lsopropyl Ether ..
:NTACHLOROPHENOL
'010199 PCP..... <1.00
IENOLS (BY EPA METHOD 604)
'010199
'0\0199
'010199
:, 10199
)10199
~,10199
:-10199
J"i0199
: \0199
:,10199
~0199
. '. 0 199
2,3,5,6Tet-Cl-phenot
2,4,6Trichlorophenol
2,4-Dichtorophenol.
2,4-Dimethylphenol
2,4-Dinitrophenol.
2-cn1oropheno1 .•.
2-Nitropheno1 .....
4,6-Dinitro-o-cresol
4-Nitropnenol ..... .
4Chloro3methylphenol
Pentachloropnenol ..
Phenol..... . .
(1.00
(0.250
(0,250
< 0. 1 25
<0. 125
<0.250
< 0. 125
<0. 125
<0.250
<0.250
<0. 125
<0.250
<0. 125
! aoove results are reportea in ug/L.
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
OS-3
SPECTRIX MONROEVILLE
,;--,;) l e NO. :
~er ;_pt ion:
te co11ected:
te Received:
87010200 ··-•--Roy Med .. 1 in Vie I I
01/f4/87
·01/15/87
MPLE # RSLT.LNE ------------------------------------------
OPROPYL ETHER
010200 lsopropyl Ether .. ,
NTACHLOROPHENOL
010200 PCP..... (1.00
ENOLS (SY EPA METHOD 6-041
2,3,5,6Tet-c1-pneno1
2,4,6Trichloropnenol
2,4-Dicnloropnenol ..
2,4-Dimethylpnenol.
2,4-Dinitropnenol.
2-cn1oropneno1 ... .
2-Nitropnenol .... .
4,6-Dinitro-o-cresol
4-Nitrophenol ..... .
4cn1oro3metny1pneno1
Pentachloropnenol ...
< 1. 00
<0:250
<0.250
< 0. 1 25
< 0. 1 25
<0.250
< 0. 125
<0.125
<O. 2_50
<0.250
< 0. 1 25
.<0. 250
010200
010200
010200
010200
·)10200
,:,10200
: 1·0200
:'10200
:i 10200
: 1 0200
·,10200
. ',0200 Phenol ............ <0.\25
_ aoove results are reported in·ug/L.
SOURCE
0S-4
OS-4
OS-4
OS-4
OS-4
OS-4
OS-4
OS-4
0S-4
OS-4
0S-4
OS-4
OS-4
OS-4
SPECTR IX MONROEVILLE
=-------------------------------------------------
mp I e NO.:
script ion:
te co11ected:
te Receivea:
87010201
Trlang1a.Mater1a1~
01/14/87
01/15/87
MPLE # R~LT.LNE SOURCE --------· -------------------------------------------------------
,QPROPYL ETHER
·010201 lsopropyl Etner ...
:NTACHLOROPHENOL
·010201 PCP ..... (1.00
!ENOLS (BY EPA METHOD 604)
·010201
·010201
010201
·010201
".)f0201
)10201
)~0201
) ~ 0 20 1
:,10201
:,·,0201
:· '10ZO 1
~',0201
2,3,5,6Tet-c1-pneno1
2,4,6Tricn1oropneno1
2,4-Dicn1oropneno1 ..
2,4-Dimetny1pneno1 ..
2,4-Dinitropnenol
2-cn1oropneno1 ...... .
2-Nitropnenol .... .
4, 6-D in it ro-o-cr-eso I
4-Nitropnenol ...... .
4Cnloro3metny1pneno1
Pentacn1oropneno1 .. .
Pnenol ........... .
< 1. 00
(0.250
(0.250
(O. 125
< 0. 1 25
<0.250
< 0. 125
(0. 125
<0.250
(0.250
< 0 . 1 25
0.650
< 0. 1 25
_ e~ove results are reported in-ug/L.
OS-5
OS-5
OS-5
OS-5
OS-5
0S-5
0S-5
0S-5
0S-5
os-s
OS-5
OS-5
OS-5
OS-5
~illp I e NO. :
,script ion:
~te Col tected:
~te Received:
SPECTR IX l<ONROEV ILLE
87010202
,James crowe we I r-~ . . ·•.
01/14/87
01/15/87
\t,l;:>LE # RSL T .. LNE SOURCE
---------. -----.-------------------------------------------------
30;:>ROPYL ETHER
7010202 lsopropyl Ether ..
:NTACHLOROPHENOL
1010202 PCP;; ... : 8.68
iENOLS IBY-EPA METHOD 6041
'010202 2,3,5,6Tet-Cl-phenol
1010202 2,4,6Trlchlorophenol
1010202 2,4-Dichloropnenol.
1010202 2,4-Dlmethylphenol.
1010202 2,4-Dlnltropnenol.
•1)10202 2-Chlor.ophenol .... .
-)10202 2-Nltropnenol ...... .
·0,0202 4,6-Dinltro-o-cresol
:10202 4-Nltropnenol ...... .
:10202 4Chloro3methylphenol
:10202 Pentachlorophenol .. .
:,0202 · Phenol ............. .
: (1.00
<0.250
<0.250
< 0. 125
<O. 125
<0.250
< 0. 125
< 0 . 1 25
<0.250
<0.250
< 0. 125
(0.250
(0. 125
~ a~ove results are reported in·ug/L.
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
OS-7
0S-7
OS-7
OS-7
OS-7
0S-7
OS-7
0S-7
SPECTRIX MONROEVILLE
---===============================================
:;;1p I e NO. :
,scr .!Pt ion:
:::~e collected:
cte Received:
67010203
.sh1.·1oh 8apt)_st Church
01/14/87
01/15/87
:.:,1PLE: It RSL T. LNE SOURCE ----------------------------------------------------------------
3OPROPYL ETHER
1010203 ,1sopropy1. Ether ... :·::".'.': 60 .. 9-
~rlTACHLOROPHENOL
7010203 PCP ... :·. : 20.6
"ENOLS <BY EPA METHOD 604)
1010203 _2,3,5,6Tet-Cl-phehol
7010203 2,4,6Trichlorophenol
7010203 2,4-Dichlorophenol.
7010203 2,4-Dimethylphenol.
7010203 2,4-Dlnitrophenol.
1010203 2-Chloropheno1 .....
-·J10203 2-Nitropneno/. . ..
7010203 4,6-Dinitro-o-c~esol
-~10203 4-Nitropnenof. . ..
-~10203 4Chloro3methylpnenol
·010203 Pentachlorophenol .. .
·:10~03· Phenol ............ .
8.53
<0.250
< 0. 125
< 0. 125
<0.250
< 0. 125
<0. 125
<0.250
0.840
0.442
28.8
<0. 125
·,c aoove results are reportea .. in.ug/L.
, 05-8
05-8
05-8
OS-8
05-6
OS-8
05-8
OS-8
05-8
OS-8
05-8
OS-8
05-8
0S-8
·, ! I
SPECTRIX MONROEVILLE
--==----=--===-------=-----------------------=----
,mp I e NO.:
,script ion:
,;:e co11ected:
:te Received:
87(>°10204
. w I 1,1 I aJY\".Barber .. we 1 ·1:
01 ("14/87
01/15/87
-.MPLE # RSL T. LNE SOURCE ----------------------------------------------------------------;oPROPYL ETHER
,010204 · rs6pr6p-yT· Et."rfor~··:-:-~-··,--17: s·
,NTACHLOROPHENOL
7010204 PCP., ... 14.0
iENOLS CBY -~PA METHOD 604)
'010204
1010204
'010204
'0 1 0·204
·010204
,:, 10204
~';0204
010204
102·04.
i0204
10204
: ', 0204
2,3,5,6Tet-Cl-pnenol
2,4,6Tricn1oropneno1
2,4-Dicn1o~opneno1 ..
2,4-Dimetny1pneno1 ..
2,4-Dinitropnenol
2-cn1oropneno1 .....
2-Nitropnenol. . ..
4,6-Dinitro-o-c~esol
4-Nitropnenol ...... .
4Chloro3metnylphenol
Pentacn1oropneno1 .. .
Phenol ........... .
<0.250
<0.250
< 0 . 125
< 0. 125
<0.250
<0.125
<O. 125
(0.250
0. 271 ·
0.290'·
0.392
< 0. 125
_ aoove results are reported in ug/L.
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
OS-9
0S-9
0S-9
0S-9
0S-9
OS-9
eived: 01/16/87
EPORT §pectrix-Monro~yi·l=J=e ____ _
TO 440 College Park Drive
Monroeville, PA l;:)146-1:336
ATTEN R. D. Hgpner
SPECTRIX MON SAMPLES lQ I_ IENT
MPANY
ILITY
Spectrix-Monroeyille
RK ID 179277
TAKEN Client
TRANS Fed. Ex.
TYPE-Water
. 0. n R6-2415
VOICE under s~p~ratg coyer
SAMPLE IDENTIFICATION
DS-1
DS-2
DS-3
DS-4
DS-5
DS-7
ps-s
JS-8
DS-8
JS-9
MS ACID ONLY
MSD ACID ONLY
PREP~RED Spectrix Corporation
DY 3911 Fq-'-'n-"'d-'--"e-"nc.._________ . , _ ~~ ..
Syite oo· ~==:f:-~
Houston, Jex as 77063-5821 . ~&v · · ·
ATTEN Sample Control
PHONE [phone] CONTACT ~C~R=U=Z ___ _
Please call the above nurnbgr if '12.\/ have any ·questions.
NOTE: ALL SAMPLES WILL OE RETAINED FOR 90 DAYS AND THEN
DISCAllDED. IF YOU WISH YOUR SAMPLES RETURNED TO YOUR FACILITY
CALL SAMPLE CONTROL AT THE AOOVE N=U~M~Il=E~R~·------------
SPECTRIX DC#-----8
SAMPLE NUMBER: OS-1
ORGANICS ANAL~SIS DATA SHEET (PACE 11
L~AT~Y rJAME: SPECTRIX
L~A~ ID rw. : 27,0104501
E-""-t:E ,;,>.TRIX: WATER _·
C;.,_~S:ASE AUTHORIZED 8Y: ·'llV
CASE NO.: ----
QC REPORT NO. : ---:_--
CONTRACT NO. : ----
DATE. SAl'IPLE RECEIVED:///~ /q,'1
VOLATILES
C%-°EN1-;:.t-TION: LOW
D '•§ EXl'i'~CTED/PREPARED: 01./23/87
0,•~rANA.}ZED: 01/23/87
DATAFILE:. 4U01045V01
DILUTION FACTOR:./ ... : ... ·.
--::,-----. -----.-----------------------------------------------. -----------
.:AS# COMPOUND UC/L --=-~--..:---------------------------------------------------------------------
('31:t CHLOROMETHANE
CG~ 8ROM0~1ETHANE
C~ VIl·.JYL CHLORIDE
.C~ CHLOROETHANE
C03t METHYLErJE CHLORIDE
C04:· C ARE:ON DISULFIDE
co~ .1., 1-DICHLOROETHENE
Ces( j_, i-UICi-ii_UKVE.:THANE
C0:.:""!:: TRANS-1, 2-DIC HLOROETHENE
C~ CHLOROFORM
Ce&:.. 1, 2-DICHLOROETHANE
. Cl..3£ 2-E:UTANONE
CU:5 1, 1, 1-TRICHLOROETHANE
Cl.i~t CARBON TETRACHLORIDE
Cl.3:: VU.JYL ACETATE
CL~ 8ROMODICHLOROMETHANE
Ci~ 1., 2-DICHLOROPROPANE
Ci~ TRANS-1,3-DICHLOROPROPENE
Cl.~ TRICHLOROETHENE
C~ DI8ROMOCHLOROMETHANE
C~ 1, 1: 2-TRICHLOROETHANE
C 1 E<: E:ENZENE
Cl.~ CIS-1., 3-DICHLOROPROPENE
C1 ~-2-(HLOROETHYLVINYLETHER
C~ E:ROHOFORM
C2.K 2-HEXANONE
C2~ 4-METHYL-2-PENTANONE
C~-TETRACHLOROETHENE
C23':' 1, 1, 2, 2-TETRACHLOROETHANE
C2.$. TOLUENE
C2~ CHLOROE:ENZENE
C2~-ETHYL8ENZEN!::
C2~ STYRENE
C~ TOTAL XYLENES
U • u~CTED AT THE LISTED DETECTION LIMIT
10 U
. 10 U
HlU
1.0 U
5 U
1.0 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
5 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5· U
10 U
5 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
.) • t~ND IS PRESENT, BUT 8ELOW THE LISTED DETECTION LIMIT
8 7 c~ND ALSO FOUND IN BLANK
i_A80RATORY NAME:
1)C REPORT NO. :
SPECTRIX oc· # -----8
SAMPLE NlJME:ER: OS-l.
'ORGANICS ANALYSIS DATA SHEET -PAGE 4
SPECTRIX CORPORATION CASE NO. : ----
ANALYST: CKT DATAFILE: 4UGl.G45V0l.
8. TENTATIVELY IDENTIFIED COMPOUNDS
-------------------------------------------------------------------------------·
CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT ------------------------------------------------------------------------------
UGi
NO NON-HSL COMPOUNDS FOUND> l.0% OF NEAREST INT.STD.
J -ESTIMATED VALUE -A l.:1 RESPONSE FACTOR IS ASSUMED
SPECTRIX DC# -----14
SAMPLE ID.
F'ILENAME
CLIENT
DATE INJECTED
CALI8 STD DATE
VOA QUANTITATION REPORT
4U01045V0.1.
SPEC-MON
01/23/87 ~9•05:00
01-13-87
INST
ANALYST
·VERIFIED 8Y
CORR. FACTOR
4000
CKT
.1.. 00
-------------------------------------------------------------------------------
SCAN# VOA COMPOUNDS M/E AMOUNT RRT AREA. -----------------------------------------------------------------------------
177 CI0.1. 8ROMOCHLOROMETHANE **IS1.** .1.28 50 UC/L 1.. 000 45451.
370 CI.1.0 1,4-DIFLUOROBENZENE **IS2** 114 50 UC/L 1.. 000 187264
463 CI20 D5-CHLOR08ENZENE **IS3** .1..1. 7 50 UC/L .1.. 000 155987
229 CS15 D4-.1., 2-DICHLOROETHANE **SU.1.** 65 84 'l. 1.. 294 25621.
L40 CS05 D8-TOLUENE **SU2** 98 99 'l. 0. 950 :1.13.1.96
535 CS.1.0 P-BROMOFLUOROBENZENE *"SU3** 95 107 'l. .1.. .156 82306
116 C030 METHYLENE CHLORIDE ;f-84 7 UC/L 0. 655 12258
264 C125 VINYL ACETATE f-43 .1 UC/L 0. 714 1.242
443 ·C230 TOLUENE ,f-92 .1. UC/L 0. 957 148.1.
=rLENAME
CLIENT
S?ECTRIX DC# ---14
SEHIVOLATILE WATER REPORT
051
4U0104!5C01
SPEC-HON
INST ID.
ANALYST
4!530
CEB
DATE INJECTED
CAL!B STD DATE.
02/02/87 21:23:00
02/02/87
VERIFIED BY~
CORR. FACTOR 1.00
---------------------------------------------------
SCAN# SEMI VOLATILE COMPOUNDS HIE AMOUNT RRT --------------------------------·-----------------------541 CI30 1,4-DICHLOROBENZEND-D4 ** ISl· ** 1 !52 40 UO/L 1. 000
7!52 CI40 NAPHTHALENE-DB ** IS2 ** 136 40 UG/L 1. 000
1046 CI50 ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000
1287 CI60 PHENANTHRENE-DlO ** IS4 ** 188 40 UG/L 1. 000
1729 CI70 CHRYSENE-012 ** IS5 ** 240 40 UG/L 1. 000
1950 CI75 PERYLENE-012 ** 156 ** 264 40 UG/L 1. 000
341 cs:so 2-FLUOROPHENOL ** SU1 ** 112 31 X O.b30
504 C545 PHENOL-D!5 ** SU2 ** 99 18 :c 0.932
~i78 CS55 2,4,6-TRIBROMOPHENOL ** SU!5 -330 96 X 1. 126
638 · CS20 NITROBENZENE-D5 ** SU3 ** 82 65 X 0.848
943 . CS25 2-FLUUOROBIPHENYL ** SU4 -172 74 X 0.902
:. 364 CS30 TERPHENYL-D14 ** SU6 ** 24-4 80 ~ 0.905
------
AREA
2242;;
9652A
!5396E
7495E
2942::
1492E
2064l
1652(
926E
2294:
11218'.
34181
SF'ECTRIX DCM-----8
SAMPLE NUMBER: OS-2
ORGANICS ANALYSIS DATA SHEET IPAGE 1)
~~~-ORA70RY ~lAME: SPECTRIX
~A3 SAMPLE ID NO.: 870104502
~~MPLE MATRIX: WATER
:J.:. TA ;;:ELEASE AUTHOFUZED E:Y: 170
CASE NO. : ----
QC REPORT NO. :
CONTRACT NO.: ----
DATE SAMPLE RECEI'.IED: / / /& /q,_7
VOLATILES
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 01/23/87
DATE ANALYZED: 01/23/87
DATAFILE: 4U01045V02
DILUTION FACTOR: .. l ..... :~
-------------------~-----------------------------------------------------------
CAS # COMPOUND UC/L -------------------------------------------------------------------------------
.--r.... c-
\.,. ·-· ...,_..,_J
CC:20
. C <J25
C (~)·30
C:035
.,::::4·0
C(:;45
c\~so
C055
C060
C065
C.1 . .1.0
Cll5
Cl20
· Cl25
Cl30
Cl40
Cl45
Cl50
-. 1 -=:: ',,., ... :,-..J
Clt-0
Cl-S5
Cl7Q
C.L75
-C180
C210
C205
C220
C225
C2:30
C2:~5
C240
C245
C250
CHLOROMETHANE
E:S:1JMOMETHANE
VINYL CHLORIDE.
C HLOROETHA/'~E
METHYLENE CHLORIDE
ACETONE
C AR':::ON DISULFIDE
1, 1-DICHLOROETHENE
1, 1-DICHLOROETHANE
TRANS-i, 2-DICHLOROETHENE
CHLOROFORM
1, 2-DICHLOROETHANE
2-f:UTANONE
i, 1, i-TRICHLOROETHANE
CARBON ~ETRACHLORIDE
VINYL ACETATE
BROMODICHLOROMETHANE
i,2-DICHLOROPROPANE
TRANS-i, 3-DICHLOROPROPENE
TRICHLOROETHENE
DISROMOCHLOROMETHANE
1, 1;2-TRICHLOROETHANE
8EN::ENE
CIS-1, 3-DICHLOROPROPENE
2-CHLOROETHYLVINYLETHER
E:RrJMOFORM
2-'-HEXANONE
4-METHYL-2-PENTANONE
TETRACHLOROETHENE
i, 1, 2, 2-TETRACHLOROETHANE
T•)LUENE
CHLOROBE~JZEt✓E
ETHYL8ENZEN.E
STYRENE
TOTAL XYLENES
U = UNDETECTED AT THE LISTED DETECTION LIMIT
10 U
10 U
10 U
10 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
5 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5' U
10 U
5 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
J = COMPOUND IS PRESENT, BUT BELOW THE LISTED DETECTION LIMIT
B = COMPOUND ALSO FOUND IN BLANK
ORGANICS ANALYSIS DATA SHEET
AC:DS
Laoora tory Name: Spectri x. Sar.? 1 e Number:
Samp1 e Hatrix.: Water Lao Sample ID No.: ~701oys:02...
Data Release Authorizea By~ Date Sample Received: t-11o-1:>7
Concentration: Low Units: ug/L
Date Extracted: Conc/Dil Factor: \ .o
Date Analyzed: 2-2 -'S7 Ccr.ipounds Detected: __ Q,_,_ __ _
NPOES ij CAS ~ CQMP0UND "
10A 108-95-2 P he no 1
1A ,~-:,/-8 ,:-1.,n I oropneno 1
OA 00-/::,-:, c.-Nl ':.ropneno 1
JA lu:i-o,-9 ,::,~-01metnypneno1
2A lLU-8.J-2 2 , 4 -il, c n I a ro p n en o 1
dA ~:i-:iU-1 p-~n,oro-m-creso,
IIA 08-uo-Z c.,4,o-1r1cn1oropneno1
SA :il-28-5 2,4-0~nitropneno\
IA !00-02-1 4-N 1 ':.ropneno I
"" :iJ4-:iZ-I 4,o-01n1tro-Z-Metny1pnenal
9A 81-30-:i ?en cacn I a ropneno 1
U = Undetected at the listed detection 1imit
J = Ccmpound is presi!nt, but below the listed det<:C':.ion 1imit a= Compou~d a1so found in ~1an~
RESULT
10 u
10 u
,:0 u
10 u
10 u Io u lo u
50 u
:,0 u ~o o.
50 u
SPECTRIX DC 8 -----8
SAMPLE NUMBER: OS-2
ORGANICS ANALYSIS DATA SHEET -PAGE 4
LABORATORY NAME: SPECTRIX CORPORATION CASE NO.: ----
C!C REPORT NO. :. ----ANALYST: CKT DATAFILE: 4UGiG45V(r2
8. TENTATIVELY IDENTIFIED COMPOUNDS
-------------------------------------------------------------------------------
CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT -------------------------------------------------------------------------------
METHANAMINE, .N-METHYL-ii2
J = ESTIMATED VALUE - A i:1 RESPONSE FACTOR IS ASSUMED
•
UC/
5 J
SAMPLE ID.
FILE~JAME
CLIENT
SFECTRIX DC~ -----14
VOA QUANTITATION REPORT
0S-2
4UG.1.045V02
SF·E.C-MON
INST 4000
CKT
J/01 DATE INJECTED
U,LI8 STD DATE
01/23/87 .1.9:49:00
01-.1.3-87
ANALYST
VERIFIED 8Y
CORR. FACTOR 1.00
------------------------.---------------.-------------.-----------------------
SCAN# VOA COMPOUNDS M/E AMOUNT RRT AREA ------------------------------------------------------------------------------
.1.80 CI0.1. BROMOCHLOROMETHANE **IS1** .1.28 50 UC/L l.. 000 41470
370 CI10 1, 4-DIFLUOROBENZENE **IS2** 114 50 UG/L l.. 000 .166282
4.S4 CI20 D5-CHLOROE:EN:Z:ENE **IS3** 117 50 UC/L i. 000 1.38374
230 CS15 D4-1, 2-DICHLOROETHANE **SU1** 65 86 1/. 1.. 278 240<)9
440. CS05 DB-TOLUENE **SU2** 98 97 1/. 0. 948 98746
535 CS10 P-BROMOFLUOROBENZENE **SU3** 95 109 1/. 1.. .1.53 74481
l-2 .l . C030 METHYLENE CHLORIDE -)f-84 6 UC/L 0. 6 72. 10073
·* BLANK CORRECTED ON DATA SHEET
S?ECTRIX DC# ---14
SEHIVOLATILE ~ATER REPORT
3"'-!✓.?LE ID.· OS2
:=rLENAME 4uo·1045C02 INST ID. 4530
CLIENT SPEC-MON ANALYST CEB
CATE INJECTED 02/02/87 22: 14:00 VERIFIED BY~
CA!...IB STD DATE 02/02/87 CORR. FACTOR 1. CO
-------
SCAN~ SEMIVOLATILE COMPQUNDS M/E AMOUNT RRT ------------
:541 CI30 1,4-DICHLOROBENZEND-D4 ** IS1 ** 1 :l2 40 UG/L 1.000
7:l2 CI4-0 NAPHTHALENE-DB -IS2 ** 136 40 UG/L 1. 000
1046 CISO ACENAPHTHENE-DlO -IS3 -164 40 UG/L 1. 000
:!.288 CI60 PHENANTHRENE-D10 -IS4 -188 40 UG/L 1. 000
1729 CI70 CHRYSENE-012 ** IS5 ** 240 40 UG/L 1. 000 1.950 CI75 PERYLENE-012 ** IS6 ** 264 40 UG/L 1. 000
341 CS50 2-FLUOROPHENOL ** SU1 ** 112 29 ,: 0. 630 · 504 CS45 PHENOL-05 ++·SU2 ** 99 15 ,: 0.932
.. 178 CS55 2,4,6-TRIBROHOPHENOL ++ SUS -330 113 ,: 1. 126
b38 CS20 NITROBENZENE~D:l ** SU3 +:+ 82 80,: 0. 84B
9~-3 CS25 2-FLUUOROBIPHENYL ** SU4 <HI-172 87,: 0.902
: 564 CS30 · TERPHENYL-014 ** SU6 ** 244 76,: 0.905
AREA
21379
89599
5058:3
6973E
3054:3
13217
1855~
12991
1023c
2613!
123011
33591
SF~CTRIX DC~-----8
ORGANICS A~ALYSIS DATA SHEET (PAGE 1)
LABORATORY NAME: SPECTRIX
LA8 SAMPLE ID NO.; 570.1.04503
SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED
CASE NO.: ----
QC REF·ORT NO. :
CONTRACT NO.: ----
DATE SAMPLE RECEIVED: / / /(; /<i1
VOLATILES
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 0.1./23/87
DATE ANALYZED: 01/23/87
DATAFILE: 4U01045V03
bILUTION FACTOR:. f:. , .....
.----------------------------------------------------------------------CAS #. COMPOUND UC/L -------------------------------------------------------------------------------
C0.1.5
CO2(,
c-:r2s
CC30
C035
.C04·0
C,j45
C050
C055
C060
C065
Cl.1.0
C.1.15
C.1.2O
C125
C.130
· C140
C.1.45
C.1.50
C155
C .1.6.)
1:165
Cl 70
C175
_1:.1.sc
c210·
C205
(220
C225
C230
C235
C240
C245
C25O
CHLOF:OMETHANE
E:ROMOMETHA~JE
VINYL CHLORIDE
CHLOR·JETHANE
METHYLENE CHLORIDE
ACETONE
C ARE:O~J DISULFIDE
l, 1-DICHLOROETHENE
.1., 1-DICHLOROETHANE
TRANS-1, 2-DICHLOROETHENE
CHLOROFORM
.1, 2-DICHLOROETHANE
2-E:UTANONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
VINYL ACETATE
8ROMODICHLOROMETHANE
1, 2-DICHLOROPROPANE
TRANS-.1., 3-DICHLOROPROPENE
TRICHLOROETHENE
D!BROMOCHLORCMETHANE
1, 1,_2-TRICHLOROETHANE
i::ErJZENE
CIS-i, 3-DICHLOROPROPENE.
2-CHLOROETHYLVINYLETHER
C::F:OMCFORM
2-HEXA~•GNE
4-METHYL-2-PENTANONE
TETRACHLOROETHENE
1, 1, 2, 2-TETRACHLOROETHANE
TCLUENE
C HL 0~:(;E:ENZE~JE
ETHYLE:ENZENI::
STYRENE
.TOTAL XYLENES
U = UNDETECTED AT THE LISTED DETECTION LIMIT
10 U
10 U
10 U
10 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
.1.0 U
5 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
5 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
J = COMPOUND IS PRESENT, BUT BELOW THE LISTED DETECTION LIMIT
8 = COMPOUND ALSO FO_UND IN 8LANK
ORGANICS ANALYSIS DATA SHEET
AC'.OS
Lacoratory Naine: Spectrix SaITT?l e Number: OS:3
Lao Sa..ipl e ID No.: s:z O J Q'JS-03
Data Release Authorizea By:~
Sample Matrix: Water
Date Sample Received: 1-11s>-B7
Concentration: L<l'ff Units: ug/L
Date Extracted: -1B-B7 Cone/Oil Factor: \. o
Date Analyzed: 2 -z -81 Ccr.ipounds Detected: o -----
NPDES 'if CAS it COMPOUND RESULT
10A 108-95-2 Phenol 10 u
iA 9:,-:,/-8 L-1.,n I oropneno 1 10 u
oA 00-/:,-:, L 1n ~ropneno I 20 u
~A iv~-o,-9 L,4-01metnypneno1 10 u
2A Ui.J-83-2 2 ,4-u1 en I oropneno 1 10 u
dA :i9-:,0-1 p-~n,oro-m-creso, iO D
UA Cb-I.JO-<'.. ·Z,4,o-1r1cn1crcpneno1 10 u
5A :il-28-5 2,4-D1n1 tropnenoi 50 u
,A. lUU-02-1 4-N 1 ;:ropne no 1 :,0 u
4A :,34-:iZ-l 4,o-01n1tro-Z-Me:nylpnenol :,Q a.
9A <Jl-30-:, ?entacn\oropneno1 5b u
U = Undetected at the 1 i sted detec'.ion 1 imi t
J = CCXTipound is present, but below the listed detection limit
3 = Compou;id a_lso found in blani:.
:;::is, IO: . 4000
LABORATORY NAME:
QC REPORT NO.: ----
SPECTRIX DC~-----8
SAMPLE NUMBER: 0S-3
ORGANICS ANALYSIS DATA SHEET -PAGE 4
SPECTRIX CORPORATION CASE NO.: ----
'ANALYST: CKT DATAFILE: 4UOi045V03
B. TENTATIVtLY IDENTIFIED COMPOUNDS
------------------------------------------------------------------------------
VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT ----------------------------------------------------------------------------
I-, LJ _uo -:.3 1,:-..7.-1
METHANAMINE, N-METHYL-. ii1.
J = ESTIMATED VALUE - A i:i RESPONSE FACTOR IS ASSUMED
UC/
5 J
SAM?LE ID.
CLISNT
SPECTRIX DC# -----14
VOA QUANTITATION REPORT
OS-3
4U01045V03 INST
SPEC-MON
4000
CKT
1)V
CALIB STD DATE
01/23/87 20:44:00
01-13-87
ANALYST
VERIFIED E:Y
CORR. FACTOR 1.. 00
-------------------------------------------------------------------------------SCAN# VOA COMPOUNDS M/E AMOUNT RRT AREA ------------------------------------------------------------------------------179 CI01. BROMOCHLOROMETHANE **IS1** 128 50 UG/L 1. 000 44396 370 CI10 L 4-DIFLUOROE:ENZENE **IS2** 114 50 LJG/L 1. 000 193652
463 CI20 D5-CHLOR08ENZENE **IS3** 1.1. 7 50 UG/L 1. 000 165995
220 CS15 D4-1., 2-DICHLOROETHANE **SU1.** 65 90 'l. 1.. 285 26884
4:: 9 CS05 DB-TOLUENE **SU2** 98 95 'l. 0. 948 116640 s:s CS10 P-8ROMOFLUOR08ENZENE **SU3** 95 107 'l. 1. 156 88100 1-::, ~-C030 METHYLENE CHLORIDE -;f-84 ·6 UG/L 0. 676 10785
* BLANK CORRECTED ON DATA SHEET
A:PLE ID_.
ILENAME
LIENT
0
>ATE INJECTED
:ALIB STD DATE
SEMIVOLATILE ~ATER REPORT
OS3
4U01045C03
SPEC-MON
02/02/87 23:05:00
0.2/02/87
-------------------------------------------
SFECTRIX DC#----8
INST ID.
ANALYST
4530
CEB
VERIFIED BY~
CORR. FACTOR 1.00
---------------
SEMIVOLATILE COMPOUNDS HIE AMOUNT RRT AREA ----------------------------------------------------------------~1 CI30 1,4-DICHLDROBENZEND-04 ** IS1 ** 1:52 40 UG/L 1. 000. 2069C
7:53 CI40 NAPHTHALENE-DB -IS2 ** 136 40 UQ/L 1. 000 8867~
l047 CI :50. ACENAPHTHENE-010 ** IS3 ** 164 40 UO/L 1.000 :5086!:
[288 CI60 PHENANTHRENE-010 ... 154 -188 40 UO/L 1.000 6816:::
l730 CI70 CHRYSENE-D12 ** IS5 iHI-240 40 UO/L · 1. 000 28:50:
l 9:x) CI7:5 PERYLENE-:-D12 ** 156 ** 264 40 UO/L 1.000 1445t
341 csso 2-FLUOROPHENOL ** SU1 ** 112 32 X 0.630 198S:::
504 CS45 PHENOL-D:5 -1Ht SU2 *-* 99 17 X 0.932 1451l
:78 CS55 2,4,6-TRIBROHOPHENOL ** SUS <Ht 330 123 Z 1. 125 1119]
:::.;9 CS20 NITROBENZENE-05 ** SU3 -82 78 Z 0.847 25211
-;-.~-3 . CS25 2-FLUUOROBIPHENYL ** SU4 -172 85 Z 0.901 121671
:65 CS30 TERPHENYL-Dl4 ** SU6 ii-¼ 244 94 Z 0.90:5 3999;
SPECTRIX DC~-----8
Ii'~ST ID 4606 SAMPLE NUMBER: 0S-4
ORGANICS ANALYSIS DATA SHEET <PAGE 1.l
LABORATORY NAME: SPECTRIX
LAB SAMPLE ID NO. : 87:).1.04504
~AMPLE MATRIX: WATER.
DA TA RELEASE AUTHORIZED E:Y: . p-o
CASE NO.: ----
QC REPORT NO.: ----
CONTRACT NO.: --~-
DATE SAMPLE RECEIVED: f/lv/<&t
VOLATILES
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 01./24/87
DATE ANALYZED: 01/24/87
DATAFILE: 4U01045V04
DILUTION FACTOR:./.: .. · ....
----------------------------------------------------------------------------CAS # COMPOUND UC/L -------------------------------------------------------------------------------
COlO
C015
C020
co·2s
C030
C035
. C048
C045
\.,V-..J~
C055
C06Q
C065
C110
C115
C120
· C125
C130
C140
C145
C150
C155
CibO
C.l.65
C.l. 70
C175
.C180
C210
C205
.C220
C225
C230
C235
C240
C245
C250
CHLOROMETHANE
E:ROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARSON.DISULFIDE
1, 1-DICHLOROETHENE
J.., .i.-U3:Ci-ii....Vr\0C:7i-iMi~C:
TRANS-1, 2-DICHLOROETHENE
CHLOROFORM
1, 2-DICHLOROETHANE
2-E:UT ANO NE
1, 1, 1-TRICHLOROETHANE
CARSON TETRACHLORIDE
VINYL ACETATE
8ROMODICHLOROMETHANE
1.,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
Dii::ROMOCHLOROMETHANE
1, 1,2-TRICHLOROETHANE
i::ENZENE
CIS-L3-DICHLOROPROPENE
2-CHLOROETHYLVINYLETHER
E:RQMOFORM
2:--HEXANONE
4-METHYL-2-PENTANONE
TETRACHLOROETHENE
1, 1, 2, 2-TETRACHLOROETHANE
TOLUENE
CHLOROE:ENZENE
ETHYL8ENZE~JF
STYRENE
TOTAL XYLENES
U = UNDETECTED AT THE LISTED DETECTION LIMIT
10 U
10 U
10 U
10 U
5 Ll
10 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
5 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5· U
10 U
5 U
10 U
10 U
5 U
s u
5 U
s u
s u
s u
s u
J = C0!1POUND IS PRESENT, 8UT BELOW THE LISTED DETECTION LIMIT
8 = COMPOUND ALSO FOUND IN BLANK
ORGANICS ANALYSIS DATA SHEET,
AC;OS
laoora tory Nai.1e: · Spectri x Samp1 e Humber: oS'i
Lao Sar;;ple IO No.: 6,0!0t..\50'-\
Dat.i Release Authorized 3y:~
Samp1 e i-\atrix: \.later
Date Sample RecJ?ived: \-1&::.-'2,7
Concentration: low Units: ug/l
Date Extracted: - I '2:, -'o'7 Cone/Oil Factor: \ . O
Date Analyz:ed: c3 -3 -B 7 CCI:J!lOUnds Detected: O ---'=-----
NP<JE:S j CAS " COMr'JUND RESULT TT
lOA 108-95-2 P he ~o 1 10 u
1A ~::i-01-d 2-i.n, oropneno I 10 u
oA co-1::i-o _L-,·-n ;:ropneno 1 20 u
.)A .1.v::i-0, -';J Z1 +-J1metnypneno1 10 u
2A l20-d3-2 2 ,4-u1cn I oropneno l 10 u
oA ;~-00-, p-~~1oro-m-creso1 l\J u
llA cd-vo-, Z,+,o-,r1cn1oropneno1 Io u
::iA ::il-b3-::i 2,4-01n1-cropneno\ 50 u
IA 1uu-iJc:-, :+-.~, ;:ropneno1 ::,0 u
"'" ::i.H-;Z-1 -+,o-01n1tro-~-Mecnylpneno1 ~iJ □-
9A ol-.Jo-::i ?en;:acn1oropnenol 50 u
U = Undete-::ted at the 1 i sted detection 1 imi t
J = C:::mpound is ;>resent, but belcw the lis:ed detection limit
3 = Compound a1 so found in bl ani(.
LAE:ORATORY NAME:
OC REPORT NO.: ----
SPECTRIX DC~-----8
SAMPLE NUMBER: OS-4
ORGANICS ANALYSIS DATA SHEET -PAGE 4
SPECTRIX CORPORATION CASE NO.: ----
ANALYST: CKT DATAFILE: 4U0i045V04
8. TENTATIVELY IDENTIFIED COMPOUNDS
-------------------------------------------------------------------------------CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT -------------------------------------------------------------------------------
UGI
NO NON-HSL COMPOUNDS FOUND> i0% OF NEAREST INT. STD.
J = ESTIMATED VALUE -A 1:1 RESPONSE FACTOR IS ASSUMED
FILENAME
CLIENT
DATE INJECTED
CALIB STD DATE
VOA O.UANTITATION REF'ORT
0S-4
4U01045V04
SPEC-MON
01/24/87 i2:26:00
01-13-87
. .
SCAN# VOA COMPOUNDS M/E
INST 4000
ANALYST CKT
VERIFIED 8Y i_// 61
_CORR. FACTOR i.00
AMOUNT RRT AREA ------------------------------------------------------------------------------179 CI01 BROMOCHLOROMETHANE **IS1** 128 50 UC/L 1.. 000 46447 370 CI10 1,4-DIFLUOROBENZENE **IS2** 114 50 UC/L 1.. 000 182925
464 CI20 D5-CHLOROBENZENE **IS3** 117 50 UC/L L 000 137409
230 CS15 D4-1, 2-DICHLOROETHANE **SU1** 65 84 I, 1. 285 27949
440 csos D8-TOLUENE **SlJ2** 98 101 I, 0. 948 108912
535 CS10 P-BROMOFLUOROBENZENE_ **SU3** 95 89 I, 1.. 153 68761
~ ,::, 1 C030 METHYLENE CHLORIDE -f 84 -5 UC/L 0. 676 6086 -~-
* BLANK CORRECTED ON DATA SHEET
FILENAME
CLIENT
MIT INJECTI::D
CALIB STD DATE
SPECTRIX DC# ----14
SEMIVOLATILE ls/ATER REPORT
OS4
4U01045C04
SPEC-MON
02/03/87 18:30:00
02/02/87
INST ID.
ANALYST
4530
CEB
VERIFIED BY~
CORR. FACTOR 1. 00
--------------------------------------------
SCAN# SEMIVOLATILE COMPOUNDS HIE AMOUNT RRT AREA ------------------------------·----------------------------------------------
537
7:l0
1045
1286
1727
1947
334
!:-00.
:177
636
942
.. 5,:::,2
CI30
CI40.
CI50
CI60 ·
CI70
Cl75
csso
CS45
CS55
CS20
CS2:l
CS30
** 1,4-DICHLOROBENZEND-D4 ** IS1
NAPHTHALENE-DB ** IS2 **
ACENAPHTHENE-D10 ** IS3 **
PHENANTHRENE-D10 ** 154 4-¼
CHRYSENE-D12 ** 155 **
PERYLENE-D12 ** 156 **
2-FLUOROPHENOL ** SU1 **
PHENOL-D5 ** SU2 **
2,4,6-TRIBROMOPHENOL ** SU5 **
NITROBENZENE-D5 ** SU3 -IHl-
2-FLUUOROBIPHENYL ** SU4 <H>
TERPHENYL-D14 ** SU6 **
152
136
164
188
240
264
112
99
330.
82
172
244 ·
40 UQ/L
40 UG/L
40 UG/L
40 UG/L
40 UO/L
40 UG/L
35 X
19 X
119 X
97X
95 X
92 X
1. 000
1. 000
1. 000
1. 000
1. 000
1.000
0.622
0. 931.
1. 126
0.848
o. 901
0.904
23037
9872C
5292C
6757(
2736~
16081
2313]
1658!
10351
3364'
14062:
3545•
EPECTRIX DC~----~ 8
SAMPLE NUMBER: OS-5
ORGANICS ANALYSIS DATA SHEET (PACE 11
~ABORATORY ~~AME: SPECTRIX
LA8 SAMPLE ID NO. : 879104505
SAt-',F"LE MATRIX: WAT:cR -.7/)
DATA RELEASE AUTHORIZED BY:~~
CASE NO. : ----
CYC REPORT NO. :
CONTRACT NO.: ----
DATE SAMPLE RECEIVED: t / f /; /<"61
VOLATILES
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 01/24/87
DATE ANALYZED: 01/24/87
DATAFILE: 4U01045V05
bILUTION FACTOR: ... ( .. : ...
-------------------------------------------------------------------------------CAS # COMPOUND UC/L -------------------------------------------------------------------------------C,)10
C'.;}15
C020
C025
C030
C035
C040
C045 .,..I"\=, ...
"' ..., _, ',J
C055
C060
C065
C110
C115
Cl.20
Cl.25
Cl.30
Cl.40
C145
C150
Cl.55
C160
c1.::.s
C170
Cl.75
Cl.80
C210
C205
C220
C225
C230
C235
C240
C245
C250
CHLOROMETHANE
E:S:OMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE
~ ~ "_nTl"'LJI l"\!•r'l.=-TUAldC" ......... ...., ........ ,._._,, ,...,_''" "~---
TRANS-1, 2-DICHLOROETHENE
CHLOROFORM
1, 2-DICHLOROETHANE
2-i::UT ANONE
1, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
VINYL ACETATE
8ROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
DI8ROMOCHLOROMETHANE
1, i, 2-TRICHLOROETHANE
E:ENZENE
CIS-1, 3-0ICHLOROPROPENE
2-CHLOROETHYLVINYLETHER
E:i:;:OMOFORM
2:--HEXANONE
4-METHYL-2-PENTANONE
TETRACHLOROETHENE
1,1, 2, 2-TETRACHLOROETHANE
TOLUENE
CHLOR08ENZENE
ETHYL8ENZENF:
STYRENE
TOTAL XYLENES
U = UNDETECTED AT THE LISTED DETECTION LIMIT
10 U
10 U
10 U
10 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
Hl U
5 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
5 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
J = COMPOUND IS PRESENT, BUT BELOW THE LISTED DETECTION LIMIT
8 = COMPOUND ALSO FbUND IN BLANK.
ORGAN!CS ANALYSlS DATA SHEET
. ACIDS
Laoora tory Harne: Spec tri x Sample Number:
Lao Sc.r.;ple ID No.: P,7 o I OL)SOS-
Data Release Authoriz.ed ay:_~
Sc.mpl e Hatrix: Water
Date Sample Received: J-\y,-B"l
Concentration: Low Uni ts: ug/L
Date utracted: \ -I 'i3 -07 Cone/Oil Factor: \ . O _..:..._....:::::,_ __ _
Date Analyz.i:d: ~ -3 -6 7 Ccrnpounds Deteeted: O -~~---
NFQES ij CAS .,_ COMPOUND RESULT ,,.
10A 108-95-2 Pheno 1 10 u
~A ~:>-'J/-b 2-t..n I oropneno I 10 u
oA ca-, :,-:i . ,-,·n ;:r1Jpni2no 1 20 a
..\A 10:0-01 -'j c.~-J1metnypneno1 10 a
2A lZU-d..1-2 2,4-01cn1oropneno\ 10 u
dA :.'::-'JU-I p-~n1oro-m-cresa1 Io a
u.A l:lb-Jo-2 L,+,o-,r1cn1oropnena1 10 u
:,A :il-28-5 2,4-01n1tropneno\ 50 u
IA 1UU-vL-1 -+-,~ ~ srooneno I :,Q u
4.-1 :0..\4-:0l-l 4,o-J1n1:ra-Z-Mecny1pnenol :,i) 0-
9A di-do-:, ?en:acn,oropnenol 50 u
u = Undetected at the 1 i sted detection 1 imi t
J
3
..
=
C0:1pound is ~resent, but be1cw t!1e 1is::d detection limit
Compound a1 so found in ~l ani<
Ii,ST ID: 4000
LA80RATORY NAME:
QC REPORT NO.: ----
SPECTRIX DC~-~---8
SAMPLE NUME:ER: OS-5
ORGANICS ANALYSIS DATA SHEET -PAGE 4
SPECTRIX tORPORATION CASE NO.
ANALYST: CKT DATAFILE: 4U01045V05
a TENTATIVELY IDENTIFIED COMPOUNDS
CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT -----------------------------------.----------------------------.-----------
UG/
NO NON-HSL COMPOUNDS F00ND > 10% OF NEAREST INT.STD.
J = ESTIMATED VALUE - A 1:1 RESPONSE FACTOR IS ASSUMED
SAMF·LE ID.
FILC::i'JAME
CLIC::NT
DATE: IN.JECTED
CALIE: STD DATE
SPECTRIX DC tt -----14.
VOA QUANTITATION REPORT
4U01045V05
SPEC-MON
01/24/87 13:06:00
01-13-87
INST
ANALYST
VERIFIED 8Y
CORR. FACTOR
4000
CKT
------------------------------------------------------------------------·----
SCAN# VOA COMPOUNDS M/E AMOUNT RRT AREA -------------------------------------------------------------------------------
179 CI01 8ROMOCHLOROMETHANE **ISl** 128 50 UG/L 1. 000 46216
371 CI10 1,4-DIFLUOROBENZENE **IS2** 114 50 UG/L 1. 000 186433
465 CI20 DS-CHLOR08ENZENE **IS3** 117 50 UG/L 1, 000 144690
220 CS15 D4-1, 2-DICHLOROETHANE **SU1** 65 86 I. 1. 285 28625
441. csos DB-TOLUENE **SU2** 98 97 ,. 0, 948 111169
5::::.-:, CS10 P-8ROMOFLUOROBENZENE **SU3** 95 89 I. 1. 153 72181
.1.l9 C030 METHYLENE CHLORIDE * 84 9 UC/L 0. 665 10062
* BLANK CORRECTED ON DATA SHEET
"ILENAME
:L!ENT
S?ECTRIX DC I ----14
SEMIVOLATILE WATER REPORT
4U01045C05
SPEC-MON
INST ID.
ANALYST
4530
CEB
)ATE INJECTED
:ALIB STD DATE
02/03/87 19:20:00
02/02/87
VERIFIED BY --;::tP7f -
CORR. FACTOR 1. 00
------------------------------------------------------3CAN# SEMIVOLATILE COMPOUNDS M/E AMOUNT RRT -AREA -------------------------------------------------------------------------535 CI30-1,4-DICHLOROBENZEND-D4 ** IS1 ** 152 40 UG/L 1.000 2373t
750 CI4-0 NAPHTHALENE-DB ** IS2 ** -136 40 UG/L 1. 000 10038E
!.045 CISO ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000 5404::0
1286 CI60 PHENANTHRENE-D 10 ** 1S4 ** 188 40 UG/L 1. 000 6940E
1727 CI70 CKRYSENE-D12 ** 1S5 ** 240 40 UG/L 1.000 3193:
:947 CI75 PERYLENE-D12 ** IS6 ** :264 40 UG/L 1. 000 1737C
329 CS50 2-FLUOROPHENOL ** SU1 ** 112 44 'Z 0.615 2955:
'c98 CS45 PHENOL-D5 ** SV2 *"* 99 24 'Z 0.931 2221;
: 77 csss 2,4,6-TRIBROMOPHENOL ** SUS ** 330 123 'Z 1. 126 1094( 634 CS20 N!TROBENZENE-D5 ** SU3 ** 82 97 'Z 0.845 3413:
0 42 CS25 2-FLUUOROB!PHENYL ** SU4 -11--11-172 92 'Z 0.901 14016]
. ::,3 CS30 TERPHENYL-D14 -SU6 ** 244 88,: 0.905 3970,
.. • ......
•
SPECTRIX DC#-----8
SAMPLE NUMBER: OS-7
ORGANICS ANALYSIS DATA SHEET <PAGE .1.)
LABORATORY NAME: SPECTRIX
LAS SAMPLE ID NO.: 870.1.04506
SAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED E:Y: 77V
CASE NO.: ----
QC REPORT NO.: ----
~ONTRACT NO.: ----/
DATE SAMPLE RECEIVED: / /t,/'61
VOLATILES
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 01/24/87
DATE ANALYZED: 01/24/87
DATAFILE: 4U01045V06
DILUTION FACTOR:./ .. :.:: ..
-------------------------------------------------------------------------------
GAS# COMPOUND UC/L ------------·------------------------------------------------------------------
COiO
C0.1.5
C020
C025
COJO
COJ5
C040
-C045
r.~s~
C055
C060
C065
CliO
Cii5
C120
· . C125
C130
C140
C.1.45
C.1.50
C.1.55
C.1.60
Ci65
C.'..70
CJ..75
Cl80
C2.1.0
C205
C220
C225
C230
,..,~•JC:: \., ._._,._J
C240
C245
C250
CHLOROMETHANE
BF:OMOMETHANE
VINYL CHLORIDE
CHLORCETHANE
METHYLENE CHLORIDE
,ACETONE
CARE',ON DISULFIDE
.1., 1-DICHLOROETHENE
1, 1-nTCHI.OROETHAN~
TRANS-1, 2-DICHLOROETHENE
CHLOROFORM
.1., 2-DICHLOROETHANE
2-SUTANONE
.1., .1., 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
VINYL ACETATE
BROMODICHLOROMETHANE
1, 2-DICHLOROPROPANE
TRANS-1,3-DICHLOROPROPENE
TRICHLOROETHENE
DIBROMOCHLOROMETHANE
.1., 1,2-TRICHLOROETHANE
BENZENE
CIS-1,3-DICHLOROPROPENE
2-.C HLOROETHYL VINYLETHER
E:ROMOFORM
2-HEXANONE
4-METHYL-2-PE~lT ANONE
TETRACHLOROETHENE
1, 1, 2, 2-TETRACHLOROETHANE
TOLUENE
CHLOROE:ENZENE
ETHYLE:ENZENE
STYRENE
TOTAL XYLENES
U = UNDETECTED AT THE LISTED DETECTION LIMIT
.1.0 U
.1.0 U
. .1.0 U
.1.0 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
5 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
.5 U
10 U
.1.0 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
J = COMPOUND IS PRESENT, BUT BELOW THE LISTED DETECTION LIMIT
B = COMPOUND ALSO FOUND IN BLANK
ORGANICS ANALYSIS DATA SHEET
AC:::is
laboratory Name: Spec tri x Samp1 e Humber: os 7 __ -.::;_:_ ___ _
Lao Samp1 e I_D No.: B?ol o~SO(p
Data Rel ease Authori z.ed By:
• Coricentration: Low
Date Extracted: t -le -Bl
Date Analyzed:
NPQES ij CAS if
lOA 108-95-2
lA 9o-:i7-d
oA 00-1:i-o
.jj-\ l\J0-0 i -9
ZA 1.20-83-2
::u. J'j-jo-,
IIA ob-06-2
oA oi-28-5
IA 100-02-i
4A :i.J4-:i2-1
9A di-30-0
Samp 1 e i~atri x: '.ia ter
Date Sample Received:
Uni ts: ug/L
Cone/Oil Factor: \ D __ .....;;;;. ___ _
Ccr.ipounds Detected: O -----
COMP<JUND RESULT
P he no 1 10 u
2-L.n I oropneno I 10 u
i::-m ;:ropneno 1 zo 0
Z,+-01metnypneno1 10 u
2 ,:1--01 en I oropneno l 10 u
o-~n1oro-m-creso1 lo u
Z,+,o-1r1cn1oropneno1 10 u
2,➔-D1n1 trcphenol 50 u
.\-,~, 1:ropneno I oo u
-1,o-J1n1 tro-2-Meuiylpnencli tiO 0-
?entacn1oropnenol 50 u
U = Undetected at the 1 i sted detection 1 imi t
J = Coopound is present, but below the listed detection limit
3 = Compound al so found in :il ani<.
:::r·,ST ID: 400,)
LABORATORY NAME:
QC REPORT NO.: ----
SPECTRIX DCM-----8
SAMPLE NUMBER: OS-7
ORGANICS ANALYSIS DATA SHEET -PAGE 4
SPECTRIX CORPORATION CASE NO. :
ANALYST: CKT DATAFILE: 4UOi045V06
8. TENTATIVELY IDENTIFIED COMPOUNDS
-----------------------------------------------------------------------------
CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT ------------------------------------------------------------------------------
UC/
NO NON-HSL COMPOUNDS FOUND> 10% OF NEAREST INT.STD.
J = ESTIMATED VALUE - A 1:1 RESPONSE FACTOR IS ASSUMED
SPECTRIX DC# -----14
SAMPLE ID.
r l.Lt:.NAMC.
CLIENT
DATE IN.JECTEO
CALIB STD DATE
VOA QUANTiTATION REPORT
0S-7
4U0l045V06
SPEC-MON
01/24/87 14:00:00
01-13-87
INST
ANALYST
VERIFIED 8Y
CORR. FACTOR
4000
CKT
J.[01
1 .. 00
--------------------.----------------------------------------------------------SCAN# VOA COMPOUNDS M/E AMOUNT RRT AREA ------------------------------------------------------------------------------181 CI01 8ROMOCHLOROMETHANE **IS1** 128 50 UC/L 1. 000 52931 371 CI10 1, 4-DIFLUOROBENZENE **IS2** 114 50 UC/L 1. 000 215413 464 CI20 D5-CHLOROE:ENZENE **IS3** 1.17 50 UC/L 1. 000 174075 231 CS.15 D4-1, 2-DICHLOROETHANE **SU1** 65 87 'l. 1. 276 33193 441. CS05 DB-TOLUENE **SU2** 98 99 'l. 0. 950 135428 5::6 CS.Hl P-BROMOFLUOR08ENZENE **SU3** 95 95 'l. 1. 155 93170 123 C030 i'IETHYLENE CHLORIDE f 84 12 UC/L 0. 680 15370
* BLANK CORRECTED ON DATA_SHEET
3A!"'rPLE ID .. :
:LI ENT
SEMIVOLATILE ~ATER REPORT
OS7
4U0104:SC06
SPEC-MON
INST ID.
ANALYST
4530
CEB
)ATE INJECTED
:ALIB STD DATE
02/03/87 20: 12:00
02/02/87
VERIFIED BY~
CORR. FACTOR 1.00
------------------------------------
SCAN# SEMIVOLATILE COM?OUNDS 11/E AMOUNT RRT AREA -------------------------------------------------------------------
:S39 CI30 1,4-DICHLOROBENZEND-04 .... IS1
751 CI40 . NAPHTHALENE-DB ** IS2 ....
1045 CISO ACENAPHTHENE-D10 .... IS3 ** 1286 CI60 PHENANTHRENE-D10 ** IS4 -1727 CI70 CHRYSENE-D12 .... IS5 **
194-7 CI75 PERYLENE-012 ** IS6 **
339 csso 2-FLUOROPHENOL ** SU1 ....
C:--03 CS45 PHENDL-D5 ...... SU2 **
. l.76 CS55 2,4,6-TRIBROMOPHENOL ** SUS
636 CS20 NITROBENZENE-D:S ** SU3 **
c'.'.'.-1 CS25 2-FLUUOROBIPHENYL ** SU4 ....
561 ·cs30 TERPHENYL-D14 ** SU6 ....
.. .. 152
136
164
188
240
264
112
99
** 330
82
172
244
40 \JG/L
40 UG/L
40 UO/L
40 UO/L
40UG/L
40 UO/L
17 Z
11 z
52 Z
39·z
41 z
18 z
1.000
1.000
1. 000
1. 000
1. 000
1. 000
0.629
0. 933 .
1. 125
0.847
0.900
0.904
35508
157221
7934C
114057
4542:;
2414:.
1761E
144Ti
685c
2175~
9178]
1170]
SPECTRIX DC tt ---~-8
SAMPLE NUMBER: 0S-8
ORGANICS ANAL_YSIS DATA SHEET (PAGE 1)
LABORATORY NAME: SPECTRIX
L.-'18 · SAMPLE ID NO. : 8.7,)1.04507
SAMPL::'. MATRIX: WATER /j7"[7j
DATA RELEASE AUTHORIZED BY=-/;v-
CASE NO. : ----
QC REPORT NO. :
CONTRACT NO. : ----
DATE_ SAMPLE RECEIVED: t/t&/«.J
VOLATILES
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 01./24/87
DATE ANALYZED: 01./24/87
DATAFILE: 4U01.045V07
bILUTION FACTOR:./.: .... ~.
------------------------------------------------------------------------------CAS ~ COMPOUND UC/L -------------------------------------------------------------------------------C01.0
C015
C020
C025
C030
C035
C040
C045
\,.,V,.J't;J
C055
C060
C065
C 1.1. 0
C 1.1.5
C1.20
C1.25
C1.30
-C1.40
C1.45
CJ.50
C155
C1.60
C165
Cl 70
Cl 75
C180
C21.0
C205
.C220·
C225
C230
C235
C240
C245
C25G
CHLOROMETHANE
E:ROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETONE
CARE:ON DISULFIDE
1., 1.-DICHLOROETHENE
TRANS-L 2-DICHLOROETHENE
CHLOROFORM
J., 2-DICHLOROETHANE
2-8UTANONE
J., J., J.-TRICHLOROETHANE
CARBON TETRACHLORIDE
VINYL ACETATE
BROMOOICHLOROMETHANE
J.,2-DICHLOROPROPANE
TRA~JS-L 3-0ICHLOROPROPENE
TRICHLOROETHENE
DIBROMOCHLOROMETHANE
1., J., 2-TRICHLOROETHANE
E:ENZENE
CIS-1, 3-0ICHLOROPROPENE
2-•: HLOROETHYL VINYLETHER
E:ROMOFORM
2:--HEXANONE
4-METHYL-2-PENTANONE
TETRACHLOROETHENE
1., 1, 2, 2-TETRACHLOROETHANE
TOLUENE
CHLOR08ENZE~JE
ETHYL8ENZENE
STYRENE
TOTAL XYLENES
U = UNDETECTED AT THE LISTED DETECTION LIMIT
10 U
10 U
· 10 U
10 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
J.0 U
5 U
5 U
J.0 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5. U
10 U
5 U
10 U
1.0 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
J = COMPOUND IS PRESENT, BUT BELOW THE LISTED DETECTION Lit:,IT
8 = COMPOUND ALSO FOUND IN BLANK_
ORLlNlCS ANALYSIS DATA S~E~T . -··
Laoora tory Naioe: Spectri x Satnp1e Number: .. OS~ --=-'"-------
Lao Sar;;p1 e ID No.: '2,7o\o'-t507 Samp1e i-latrix: \.later
Data Re1ease Authorized :ly:-<f;17?Y Date Samp1e Received: l-\&>-87
Concentration: Lew
Date Extracted: l -l 'a-07
Date Ana1yzed: ,.'.l -3 -8,7
NP DES 'ff CAS " ,r
10A 103-95-2
lA 'j:,-:,1-8
, oA oo-, ::i-~
.;.r-, !.V~-0.I -~
2A 12\J-dj-Z
dA :;-;:-':Ju-,
i.LA oo-uo-Z
:,,\ :, l.-2:8-:,
I .-\ J.VU-IJZ-1
➔.-1 :,..14-:,2-1 ---g-,,; -=3o-:,
COM?SUND
?he:101
Z-1...n I or,:,;nenc 1
Z-tn ;:ropner.o 1
Units: ug/L
Cone/Di 1 Fae tor:
Ca:ipounds Detected:
, ,+-J1me:nypneno 1
Z ,{-::i1cri I or-opr,,:no !
y-\.,.1,oro-m--creso 1
L,+,o-Ir1c~Ioropneno1
Z,4-01n1-c.ropnenol
:+-,ii -c.ropneno 1
-+,o-u1n1-c.ro-Z-Metny1pnenol
?en -c.ac:, 1 o ropneno I
U = Undete-:ted at the 1isted detectio:i 1imit
J= Cc:mpound is preser.t, but be1cw ::Ile 1is:ed detection 1imit
3 = Cor:ipcund a1 so found in ::>1 ani:.
\ .o
RESULT
10 u
10 u za iJ
IO a
10 u
ri:l a
H! 0
50 u
:,0 a ~a iJ. / nm ~
~NSI IO: ·. 4000
LAE:ORATORY NAME:
SPECTRIX DC~-----8
SAMPLE NUMBER: OS-8
. ORGANICS ANALYSIS DATA SHEET -PAGE 4
SPECTRIX ·CORPORATION CASE NO. : ----
QC REPORT NO. : ANALYST: CKT DATAFILE: 4U01045V07
8. TENTATIVELY IDENTIFIED COMPOUNDS
-------------------------------------------------------------------------------·
CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT -----------------------------------------------------------------------------·
UGI
.· D q, -~0 -3 DIISOPROPYL ETHER (DOT) · 343 26 J
J = ESTIMATED VALUE -A 1:1 RESPONSE FACTOR IS ASSUMED
I
SPECTRIX DC 8 -----14
VOA QUANTITATION REPORT
SAMPLE ID.
FILENAME
CLIENT
DATE INjECTED
CALI8 STD DATE
OS-8
4U0i045V07
SPEC-MON
0i/24/87 i4:41.:00
01.-13-87
INST
ANALYST
VERIFIED BY
CORR. FACTOR
4000
CKT
t_/V01
L 00
------------------------------------------------------------------------------
SCi'.N# VOA COMPOUNDS M/E AMOUNT. RRT AREA
----------------------------------------------------.--------------------------
180 CI01. BROMOCHLOROMETHANE **IS1** 128 50 UC/L .L 000 49446
37 1. CI10 1., 4-DIFLUOROBENZENE **IS2** 1.14 50 UC/L .L 000 206169
464 CI20 D5-CHLOR08ENZENE **IS3** 1.17 50 UC/L 1.: 000 1.6 7 661.
231. CS.1.5 D4-1.,2-DICHLOROETHANE **SU.1.** 65 85 'l. L 283 30414
..::4 l CS05 DB-TOLUENE **SU2** 98 98 'l. 0. 950 f30013
536 CS.1.0 P-BROMOFLUOROBENZENE **SU3** 95 95 1/, 1.. 1.55 89870
.:.20 C030 METHYLENE CHLORIDE T 84 11. UG/L 0. 667 1.2724
* BLANK CORRECTED ON DATA SHEET
S<~IPLE ID.
FILENAME
CLIENT
DATE INJECTED
CALIB STD DATE
SCAN#
SPECTRIX DC tt ----14
SEMIVOLATILE WATER REPORT
OS8
4U01045C07
SPEC-MON
02/03/87 21:02:00
02/02/87
SEMIVOLATILE COMPOUNDS
INST ID.
ANALYST
VERIFIED BY
CORR. FACTOR
H/E AMOUNT
4530
CEB
1. 00
RRT AREA -------------------------------------------------------------------------
:;33 CI30 1,4-DICHLORDBENZEND-D4 ** IS1-** 1~2 40 UG/L 1.000 1998(
749 CI 4-0· NAPHTHALENE-DB ** I52 ** 136 40 UG/L 1. 000 8~09t
1044 CI:)0 ACENAPHTHENE-DlO ** IS3 *"* 164 40 UG/L 1.000 4555E
12136 CI60 PHENANTHRENE-D10 ** 154 ** 188 40UG/L 1. 000 5887:
1726 CI70 CHRYSENE-D12 ** 155 ** 240 40 UG/L 1.000 2534(
1947 CI75 PERYLENE-D12 ** IS6 ** 264 40 UG/L 1.000 1334~
326 CS:)0 2-FLUORDPHENOL ** SU1 ** 112 26 X 0.612 1494:
.C..-96 CS45 PKENOL-DS ** SU2 ** 99 16 X 0.931 1217(
:· 176 CS55 2,4,6-TRIBROMOPHENOL ** SUS ** 330 98 X 1. 126 732•
633 . CS20 NITROBENZENE-D:) ** SU3 ** 82 69 X 0.845 2059(
';'..;-O CS25 2-FLWOROBIPHENYL ** SU4 ** 172 72 X 0.900 9239(
: 561 CS30 TERPHENYL-D14 ** SU6 ** 244 64 X 0.904 2288:
270 C635 PENTACHLOROPHENOL 266 102 UG/L 0.988 1309•
ORGAN!CS ANALYStS DATA S~EET
Laoora tory Nalile: Spectri x Sdmp1 e Numtier:
Lao Sa.fi'lple ID No.: B"1QIO'-t50P, Samp1 e i~atrix: Water
Data Release Authorized Date Samp1 e Received: \-H,,-'o7
Cor.centration: Low Units: ug/L
Date Extracted: (-I e, -f',7 Cone/Oil Factor: l. o __ _.;:::;_ __ _
Date ,\na1:;z.ed: .;2 -3 -87 Ca:-:pounds Detected: _..,,~5""----
NPOES :f CAS " COMP'JUND RESULT ,r
10A 103-95-2 ?r.e:101 40
rA ~::,-::, I -3 Z-1..n I orcpneno I 80
oA oo-, :>-:> l-N1 ~ropric:no 1 20 u
jA lV:>-O I-~ ,,4-01rnetnypneno1 10 u
2A t 2.U-d..1-2. i.,4-D1cn1orooneno\ 10 u
oA :l~-:>1.J-/ p-~~1or~-~-cresol 84
uA 08-uo-~ L,4,~-1r1cn1orc~neno1 10 u .. :il-28-:i Z,~-D1n1cropneno1 50 u ::,11,
IA 1.u0-v"-' -+-,x1 ;:ropneno1 80
4;,. ::,j4-::i<.-l ~.o-01n1 ;:ro-Z-Metny1pnenal ::,Q Q.
9A ol-do-:i ?en cac n I oropneno 1 120
U = Undetec;:ed at the listed detection limit
J = CC0pound is pr2sent, but belc-..i t!1e listed det~:ion limit
3 = Compc·und a1 ;o found in bl anic.
Ali?LE ID.:
"lLENAr:E
:LIENT
)ATE INJECTED
:ALIB STD DATE·
SEMIVOLATILE ~ATER .REPORT
OSSMS
4U01045C08
SPEC-MON
02/03/87 21:52:00
02/02/87
INST ID.
ANALYST
4530
CEB
VERIFIED BY~/
CORR. FACTOR 1.00
--------------------------------------------------
3CAN# SEMIVOLATILE COMPOUNDS M/E AMOUNT RRT AREA_ -------------------------------------------------------------------------------534
749
1045
1287
L727
~947
227
1.,.·?'9
:77
~-34
.·::-4
.. ::33
. ::7 !
CI30
c140·
CI:50
CI60
CI70
CI75 . cs:,o
CS45
CS55
CS20
CS25
CS30
C315
C330
C465
C560
C635
1,4-DICHLOROBENZEND-D4 ** IS1-**
NAPHTI-lALENE-D8 ** IS2 **
ACENAPHTHENE-D10 ** !S3 **
PHENANTHRENE-D10 ** 1S4 **
CHRYSENE-D12 ** 1S5 **
PERYLENE-D12 ** IS6 **
2-FLUOROPHENOL ** SU1 **
PHENOL-D5 ** SU2 **
2,4,6-TRIBROMOPHENOL **
NITROBENZENE-D5 ** SU3 **
2-FLUUOROB I PHENYL ** SU4 -!HI-f•· TERPHENYL-D14 *"'° S116 ,.__.., ___ _
SUS**
PHENOL
2-CHLOROPHENOL
P-CHLDRD-M-CRESOL ·
4-NITROPHENOL
PENTACHLOROPHENOL
152
136
164
188
240
264
112
99
330
82
172
244
94
128
107
139
266
40 UO/L 1.000
40 UO/L 1. 000
40 UO/L 1.000
40 UG/L 1. 000
40 UO/L 1.000
40 UO/L 1. 000
64 :C o. 612
41 'Z 0.933
120 Z 1 1. 126
95 Z '\ 0. 846 92 'Z 0.900
98 'Z-1 0. 905
40 UG/L1,,, 0. 936
80 UG/L 1f/ 0. 948
84 UG/L '-' 1. 154
80 UG/L I/ 1. 036
120 UG/L]/ 0.988
20:592
89247
47095
60177
2434E
1276C
3719C
32631
934~
2981:
12Z33,
3383:
3826:
6265E
5175]
1067<.
l :57 6 l
ORGAH!CS ANALYSIS DATA SHEET
AC'.OS
LaDoratory Harne: Spectrix
Lao Sample ID No.: B7D\Qll.509
Samp1 e ~umber: 0$ 8 t-J\S. \:>
Samp1 e Hatrix: Water
Data Re1ease Authorized 3y:~ D_a te Sample Receivec!:
Concentration: low Units: ug/l
Date Extracted: l-/5-~7
Date Analyzed: :2 -3 -B7
Cone/Oil Factor: \ . 0
Cc:rnpounds Detected: S -=-----
NPIJES " CAS " CJMPSUND ., T
10A 108-95-2 ?he:101
lA ~::,-:,/-0 C:::-1..,n I orcpner:o I
oA oo-, :,-::, c-,'c, ~;-opr.eno 1
~A .J.V::l-0 I-~ c:. ,..\.-u1wet.:-,:1~:1eno t
V. l .c0-dJ-2 2. ,4-Jl en I oropneno l
:;Si·--sv-1 p-.... n1c,o-;n-creso I
uA b<i-vo-.::. Z,+,o-,r1cn1oropneno1 .. ::il-28-5 2,~-D1n1-.:ropnena\ ::,A
IA wU-vZ-1 4-i'C ~ropoeno I
::i:;,; :,,j4-::Z-l ::i:,o-J1n1 -.:ro-2-Mecnylpnenol
9A dl-Jo-:i ?en :Jc., 1 o ropneno I
U -= Undetected at the 1 i s-.:ed de:ection 1 imi ".:
J = CO:!jJound is.present, but be1Gw_ t:1e lis-:ed detection limit
3 = Compcund also fvund in ~lan(
RESULT
34
73
20 u
10 u
10 u
7!:i
1d u
50 u
b9
!::id 0-
'-
:LI ENT
;ATE INJECTED.
:i'.L I B STD DATE ·
3CANit
=?ECTRIX UC~----8
SEMIVOLATILE WATER REPORT
OSSMSD
4U01045C09
SPEC-MON
02/03/87 22:42:00
02/02/87
SEMIVOLATILE COMPOUNDS
INST ID.
ANALYST
VERIFIED BY
CORR. FACTOR
M/E AMOUNT
------------
4530
CEB
1.00
RRT AREA
5 =<4 CI30 1,4-DICHLOROBENZEND-D4 ** IS1 ** 152 40 UG/L\ 1.000 20458
749 CI4-0· NAPHTHALENE-DB ** IS2 ** . 136 40 UG/L \ 1. 000 87550
!.045 crso ACENAPHTHENE-010 ** IS3 ** 164 40 UG/L l 1. ooo 4682;;
1256 CI60 PHENANTHRENE-010 ** IS4 ** 188 40 UG/L ' 1.000 60413
:727 CI70 CKRYSENE-D12 4-4 ISS ** 240 40 UG/L 1. 000 23543
~91",7 CI75 PERYLENE-D12 ** IS6 ** 264 40 UG/L 1. 000 1288!:
-:;::-:7. CSSO 2-FLUOROPHENOL ** SU1 4-4 112 55 Z 0.612 3202,
.'?·2 CS45 PHENDL-05 ** SU2 ** 99 34 Z 0. 933 2719E
-;,, CS55 2, 4, 6-TRIBROM,OPHENOL 4-4 SUS ** 330. 121 Z 1. 125 930,
·.33 CS20 NITROBENZENE-D5 ** SU3 ** 82 87 Z 0. 845 267H
·.:1 CS25 2-FLUVOROBIPHENYL+4SU4** 172 .84Z 0.900 1099H
J CS30 TERPHENYL-014 ** SU6 ** 2~ 110 Z 0. 904 367H
~) C315 PHENOL ,I· 94 -34UG/L) 0.936 3173(
-·•5. C330 2-CHLOROPHENOL 128 73 UG/L .. 0. 946 5688~
a3 C465 P-CHLORO-M--CRESOL 107 78 UG/L.' 1. 152 4706;
, -~,'c3 C560 4--NITROPHENOL 139 69 UG/L i_ 1. 036 ', 909E
C635 PENTACHLOROPHENOL 266 116 UG/Lj 0. 988 ·' 1530;
'··
ORGAN!CS ANALYSIS DATA SHEET AC :os Lacoratory Nar.ie: Spectrix Sample Humber: o::iC:.. Lao Sar;;pl e ID No.: f:,]O\ Ol..\5 10 Data Release Authorized :ly:~ Concentration: Low Samp 1 e i~atri x: Water Date Sample Received: ,-,(q-8] Date Extracted: \_-..li2_ -__'g] Units: ug/l Cone/Oil Factor: I. o Date Analyzed: i2:. -3 f.?_1 Ca:ljlOUnds Oetec ted: NP!JES ffe CAS iF COMP'JUNO lOA 108-95-Z Pheo101 L'-1 :1~-::::i I -0 L-c.n1oropneno1 OA co-1 ::-::::i .. t...-,'n c.ro9ncno t .) ,:... ..l.lJ::)-0 J -';J t... ,+-u1rueEnypneno 1 2A 120-3.l-Z z.~-~1cn1oropnenol oA :i::-,U-7 p-\,,:i I or"J-.n-creso 1 l.LA oo-uo-L L,~,o-1r1cn1oropnenc1 c,A :il>ZS-5 z.~-D1n1;:ropnenol IA J.U0-0Z-1 .!,-.~ ~ :ropneno I '+A ~..i:+-~z-I .!, , o-u, n 1 :ro-Z-,1erny I pneno 1 J .\ -" 31-do-:, ?en ;:.:c ,11 a ropneno I U = Undetected at the 1 i sted detection 1 imit J = Ccopound is present, but belcw t!1e listed det.ection limit 3 = Cor:ipcund al so found in :Jl ~ni(. Q RESULT 10 U 10 u zu a HJ a 10 U 1u a .LiJ iJ 50 U ::iu a ~u _u. so u
'ILENAME
:LI ENT
)ATE INJECTED
:Af_IB STD DATE·
· SPECTRIX DC•----8
SEJ1IVDLATILE WATER.REPORT
OS9
4U01045C10
SPEC-MON
02/03/87 23:33:00
02/02/87
INST ID.
ANALYST
4530
CEB
VERIFIED BY~
CORR. FACTOR 1.00
---------------------------------------------
3CAN~ SEMIVOLATILE COMPOUNDS HIE AMOUNT RRT AREA ----------------------------------------------------------------------------
534 CI3D 1,4-DICHLOROBENZEND-D4 ** IS1 ** 152 40 UG/L 1. 000 20331
749 CI4o· NAPHTHALENE-DB ** IS2 ** 136 40 UG/L 1. 000 8764E
;~~5 CI50 ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1.000 4537!:
1236 CI60 PHENANTHRENE-D10 ** IS4 -188 40 UO/L 1. 000 58337
c727 CI70 CHRYSENE-D12 ** ISS ** 240 40 UO/L 1. 000 22524
:·.-:;47 CI75 PERYLENE-D12 ** IS6 ** 264 40 UO/L 1. 000 1171:;
229 csso 2-FLUOROPHENOL ...... SU1 ** 112 32 'Z 0.614 18351
"17 CS45 PHENOL-D5 -Ht ,SU2 ** 99 16 z 0.931 1283~
·76 CS55 2,4,6-TRIBROMOPHENOL ** SUS ...... 330. 131 'Z 1. 125 980~
.34 CS20 NITROBENZENE-05 ** SU3 ..... 82 103 X 0.846 3166t
. ~ ! . CS25 2-FLUUOROBIPHENYL ** SU4 ** 172 99 z 0.900 12569:
:':2 CS30 TERPHENYL-D14 ** SU6 ** 244 58 ,:; 0.904 1835~
SPECTRIX DC~-----8
SAMPLE NUMBER: LLW 8LK
ORGANICS ANAL.YSIS DATA SHEET (F·AGE 1)
LABORATORY NAME: SPECTRIX
LA8 SAMPLE ID NO. : 8Jo/o1~
~AMPLE MATRIX: WATER
CASE ~JO. : ----
DATA RELEASE AUTHORIZED
QC REPORT NO.: ----
_CONTRACT NO.: ----
DATE SAMPLE RECEIVED: E:Y:_~
VOLATILES
CONCENTRATION: LOW DATAFILE: E80i23V0.1.
DATE EXTRACTED/PREPARED: 01/23/87
DATE ANALYZED: 0.1./23/87 . I DILUTION FACTOR:.: ....... .
. -------------------
CAS # ·coMPOUND VG/L ----------------------------------------------------------------------------
C010
COiS
C020
CC125
C030
C035
C040
C045
coso
COSS
C060
C065
Ci10
C1.i5
·c120
C125
C130
C1.40
C1.45
C1.50
C.1.55
· C.1.60
C165
C1.70
.C175
· Cl.80
C210
C205
C220
C225
C230
C2·35
C240
C245
C250
CHLOROMETHANE
E:ROMOMETHANE
VINYL CHLORIDE
CHLOROETHANE
METHYLENE CHLORIDE
ACETO~E
CARBON DISULFIDE
1, 1-DICHLOROETHENE
.1., .1.-DICHLOROETHANE
TRANS-.1., 2-DICHLOROETHENE
CHLOROFORM
.1.,2-DICHLOROETHANE
2-8UTANO~lE
.1., 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
VINYL ACETATE
BROMODICHLOROMETHANE
.1.,2-DICHLOROPROPANE
TRANS-.1., 3-DICHLOROPROPENE
TRICHLOROETHENE
DIBROMOCHLOROMETHANE
.1., L2-TRICHLOROETHANE
BENZENE
Cis-.1.;3-DICHLOROPROPENE
2-CHLOROETHYLVINYLETHER
E:ROMOFORM
'2-HEXANOl,E
4-METHYL-2-PENTANONE
TETRACHLOROETHENE
i, .1.,2, 2-TETRACHLOROETHANE
TOLUENE
CHLORQE,ENZENE
ETHYL8ENZEI\JE.
STYRENE
-TOTAL XYLENES
U = UNDETECTED AT THE LIST~D DETECTION LIMIT
H) U
10 U
.1.0 U
iO U
6
iO U
5 U
5 U
5 U
5 U
5 U
5 U
7 J
5 U
5 U
iO U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
10 U
5 U
iO U
iO U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
J = COMPOUND IS PRESENT, BUT BELOW THE LISTED DETECTION LIMIT
. 8 = COMPOUND ALSO FOUND IN BLANK
ORGANICS ANALYSIS DATA SHEET
ACIDS
L.:.cvratory Name: · Spectrix Sample Number: LLW I::>~
Lao Sample lD No.: 8701045" Sample Hatrix: Water
Gata Rel ease Authorize a By·:.~
Concen·tration: Low
Date Sample Received: 1-1c.·e,7
Units: ug/L
Date Extracted: 1-1e,-1:,7 ----'---'--=-------"'-'-----
Cone/Oil Factor: , ----'~-o"""----
Date Analyzed: 2.-2.-57 C CXTI])ounds Detected: --~O"---
NPDES # CAS " COMPOUND "
10A 108-95-2 Pheno 1
lA 9:i-:i/-o 2-L.n I oropneno I
oA oo-1 :,-:, 2-Nl tropneno 1
.oA lV:J-0 I -9 Z,4-D1met~ypneno1
ZA lLU-1:i.l-2 2 ,4-Di en l oropneno !.
cA ~~-:i0-J p-L.n1oro-m-cresol
I.LA od-uo-.:: Z,+,o-1r1cn1oropneno1
:,A :il-28-5 2,4-01n1tropheno\
IA 100-02-1 +-Fii tropneno I
4A :,~4-:,2-1 4,o-J1n1tro-Z-Metny1pnenal
9A 81-3b-5 ?entacnloropnenoi
U = Undetected at the 1 i sted detection 1 imit
J = Ccnpound is present, but below the listed deteetion limit
a= Compound also found in blani(
RESULT
10 U
10 u
20 U
10 U
10 U
10 U
10 u
50 U
50 u
::c6T ID: 4COO SPECTRIX DC~-----8
SAMPLE NUMBER: LLW BLK
ORGANICS ANALYSIS DATA SHEET -PAGE 4
LABORATORY NAME: SPECTRIX CORPORATION CASE NO. : ----
QC REPORT NO.: ----ANALYST: NOT DATAFILE: E80123V01
8. TENTATIVELY IDENTIFIED COMPOUNDS
-------------------------------------------------------------------------------·
CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT -------------------------------------------------------------------------------·
UGi
NO NON-HSL COMPOUNDS FOUND> 10½ OF NEAREST INT. ST~
I
J = ESTIMATED VALUE - A 1:1 RESPONSE FACTOR IS ASSUMED
SPECTRIX DC# -----.14
VOA QUANTITATION REPORT
t="ILE:NAME
CLIENT
DA,E IN.JECTED
CALI8 STD DATE
EE:0123V0.l
SPECTRIX
01/23/87 10:59:00
01-13-87
INST 4000
ANALYST NOT
VERIFIED BY J/ c1
CORR. FACTOR .1. 00
-------------------------------------------------------------------------------SCAN# VOA COMPOUNDS M/E AMOUNT RRT AREA ------------------------------------------------------------------------------.179 CI0.l BROMOCHLOROMETHANE **IS.l** .128 50 UC/L .1. 000 40773
370 CI.10 .1, 4-DIFLUOROE:ENZENE **IS2** 1.14 50· UC/L .1. 000 177684
4-~3 CI20 D5-CHLOROBENZENE **IS3** 1.17 50 UC/L .l.000 144864
2:::0 -CS.15 D4-.1,2-DICHLOROETHANE **SU.1.** 65 87 'l. 1. 285 23970
• ~ ,':I ·-~ ..... CS05 D8-TOLUENE **SU2** 98 96 'l. 0. 950 102632
": 3::'r CS10 P-8ROMOFLUOR08ENZENE **SU3** 95 106 'l. .1 . .156 75646
_-_.:_9 C030 Mi::THYLENE CHLORIDE 84 6 UC/L 0, 665 10092
~~7--c1.10 2-E:UT A NONE 72 7 UC/L 0. 619 1.284
,
i<'-.:S0 LE ID .. :
"ILE.NAME
:LI ENT
)ATE INJECTED
:ALIB STD DATE
LLW ELK
SPECTRIX DC# ----14
SEMIVOLATILE WATER,RE?ORT
INST ID.
ANALYST
4530
CEB
4B01045C01
SPEC-HON
02/02/87 20:31:00
02/02/87
VERIFIED BY~
CORR. FACTOR . 1. 00
----------------------------------------------------------------------,CAN# SEMIVOLATILE COMPOUNDS M/E AMOUNT RRT AREA -------------------------------------------------------------
:5-41 cr:ro 1,4-DICHLOROBENZEND-D4 ** ISl ** 152 40 UG/L 1. 000 2083.!
7:52 CI40 -NAPHTHALENE-DB ** IS2 ** 136 40 UG/L 1,000 8855E
1046 CI50 ACENAPHTHENE-D10 ** IS3 .. 164 40 UO/L 1. 000 5049i
l2S7 CI60 PHENANTHRENE-D10 ** IS4 .. 188 40 UO/L 1. 000 6845i
',;729 CI70 CHRYSENE-D12 ** IS5 ** 240 40 UO/L .1. 000 2425€
i.949 CI75 PERYLENE-D12 -IS6 ** 264 40 UG/L 1. 000 1195!
3-41 CS50 :2-FLUOROPHENOL ** SU1 ** 112 50 ,: 0.630 3104]
' ...... .,, ..... ._•"T CS45 PHENOL-D5 ¼¼ ,SU2 ** 99 31 ,:; 0.932 2609~
~ ':70 •·, _, CS:55 2,4,6-TRIBROMOPHENOL ** SU:3 ** 330 109 '%, 1. 126 985:
~.23 CS20 NITROBENZENE-D:3 ii-+ SU3 +¼ 82 82 ,: 0.848 26:33:
=--~-3-CS25 2-FLUUOROBIPHENYL ** SU4 ¼¼ 172 88 ,: 0.902 12520(
-· I. ~ ' ..:-'"'t CS30 TERPHENYL-D14 -SU6 ii-+ 244 119 ,:; 0.905 4205(
SPECTRIX CC#-----8
SAMPLE NUMBER: BLANK
ORGANICS ANA~YSIS DATA SHEET (PAGE i)
LABORATORY NAME: SPECTRIX
LAB SAMPLE ID NO.: 86--
EAMPLE MATRIX: WATER
DATA RELEASE AUTHORIZED BY:
CASE NO. : ----
QC REPORT NO.:.----
CONTRACT NO.: ----
DATE SAMPLE RECEIVED: !/t~[~t
VOLATILES
CONCENTRATION: LOW
DATE EXTRACTED/PREPARED: 01/24/87
DATE ANALYZED: 01/24/87
DATAFILE: 480124V01
DILUTION FACTOR: .1.:. J:<?.°. ..
·-------------------. -------------------------------------------
CAS # COMPOUND UC/L ----------------------------------------------------------------------------COi•)
C015
C020
C030
C035 . c ,3t~·o
C045
C050
C055
C060
C065
CiiO
C115
Ci20
Ci25
Ci30
"C140
C145
Ci50
C155
C160
Ci65
C170
t.;175
-Ci80
C210.
C205
<:220
C225
C230
C235
C240
C245
C250
CHLOROMETHANE
E:RQMOMETHANE
VINYL CHLORIDE.
CHLOROETHA~JE
METHYLENE CHLORIDE
ACETONE
CARBON DISULFIDE
1, 1-DICHLOROETHENE ..
1, i-DICHLOROETHANE
TRANS-i,2-DICHLOROETHENE
CHLOROFORM
1, 2-DICHLOROETHANE
2-BUTANONE
i, 1, 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
VINYL ACETATE
BROMODICHLOROMETHANE
1,2-DICHLOROPROPANE
TRANS-1, 3-DICHLOROPROPENE
TRICHLOROETHENE
DIBROMOCHLOROMETHANE
i, i, 2-TRICHLOROETHANE
E:ENZENE
crs-1; 3-DICHLOROPROPENE
2-CHLOROETHYLVINYLETHER
E:ROMOFORM
2~HEXANO~JE
4-METHYL-2-PENTANONE
TEYRACHLOROETHENE
1, 1, 2, 2-TETRACHLOROETHANE
TOLUENE
CHLOROE:ENZENE
ETHYL BENZENE
STYF:ENE
TOTAL XYLENES
U = UNDETECTED AT THE LISTED DETECTION LIMIT
10 U
10 U
· 10 U
10 U
5 J
10 U
5 U
5 U
5 U
5 U
5 U
5 U
9 J
5 U
5 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
5. U
10 U
5 U
10 U
10 U
5 U
5 U
5 U
5 U
5 U
5 U
5 U
J = COMPOUND IS PRESENT, BUT BELOW THE LISTED DETECTION LIMIT
9 = COMPOUND ALSO FOUND IN BLANK.
::·,ST ID.: 4C00 SPECTRIX DC~-----8
SAMPLE NVME:ER: E:LANK
ORGANICS ANALYSIS D~TA SHEET -PAGE 4
LABORATORY NAME: SPECTRIX. CORPORATION CASE NO. : ----
<)C REPORT NO. : ----ANALYST: CKT DATAFILE: 48Gi24V0i
8. TENTATIVELY IDENTIFIED COMPOUNDS
-------------------------------------------------------------------------------·
VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT -------------------------------------------------------------------------------·
UGI
NO NON-HSL COMPOUNDS FOUND> i0% OF NEAREST INT. STD.
J = ESTIMATED VALUE -A i:i RESPONSE FACTO~ IS ASSUMED
SAi·iPLE ID.
r=ILENAME
CLIEl-sT
SPECTRIX DC~ -----.1.4
VOA QUANTITATION REPORT
480124V01
SPEC-MON
INST 4000
ANALYST CKT
VERIFIED 8Y Jvo1 DATE IN-.JECTED .
CALI8 STD DATE
01/24/87 ·11:41:00 .
01-13-87 CORR. FACTOR 1.00
--------------------------------.----------------------------------------------
SCAN# VOA COMPOUNDS M/E AMOUNT RRT AREA ----------·------------. -------------------------------------------------------
1:76 CI01 BROMOCHLOROMETHANE **IS1** 128 50 UG/L 1. 000 51501.
370 CI10 1, 4-DIFLUOROBENZENE **IS2** 114 50 UG/L 1.000 216938
464 CI20 D5-CHLOR08ENZENE **IS3** 117 50 UG/L 1. 000 175476
228 CS15 D4-1, 2-DICHLOROETHANE **SUl ** 65 91 '1/. 1.295 33949
4 .11 CS05 OS-TOLUENE ~*SU2** 98 100 '1/. 0. 950 138275
536 CS10 P-8ROMOFLUOR08ENZENE **SU3** 95 98 '1/. 1. 155 96658
1.J.3 CO30 METHYLENE CHLORIDE 84 5 UG/L 0. 642 5935 -::-::io _C110 ,_ ..... __, 2-8UTANONE --:, ,~ 9 u·c1L 0. 616 .1.728
~~tLIKlA ncruR1 V'/ 1..1 / f·, '-' I \.J '.. I II •-· ', \.' .i. V r ·..1
l'F.r'OPT !].P ec lr i. x -Monro ev ii 1 e~. ____ _
TD 'I/JO ColleCJJ' Park Drive,__ __ _
11onroeville, PA 15146-1536
ATTEtJ R. D. Hep~~e~r _________ _
,;1.TENT SPECTRIX MON SAMPLES_;)_
.,_ I 1MPf,tJY Svpc.tr i x-Monroevi 1·1~e,,__ ___ _
! . (,•:.: TL IT'(
1.,; .;~1-: J () _1_77277
11,1< FN C~l~i ~e~n~t. _____________ _
H!N•IS f:J?_<L...,E~,o..··~------------
TYPE l~ater =--"~-------------1'. 1.1. tt B4-2'11~5 ___________ _
INVOI•::E uuder separate cover
SAMPLE IDENTIFICATION
"1 P.S::.J.O~-----------
Q.S-1 Ot, BL~A~N~K~-------
. 0:l l}':i_-_,__1.o.1 ___________ _
f'li ~J~::J_Z:_~' -----------
t':, LJ!;j-13 ·~~-----------
02/19/87 11:24: 56
PREPARED $.rr.ctri x Corporation _ · 'i70
DY 3911 Fondren Ii
Suite 100 H~~o~u~s~t~o~n~,~T_e_x_a_s __ 7_7_0_6_3 ___ 5_8_2_1__ CERT IF I D Il Y ·
ATTEN Sample Control
rHONE 1713) 266-6800 CONTACT CRUZ, ____ _
Please cal 1 the above number if lLCUJ-1l.;ave anu_CJ.fil1U;.i.Q.fl_<;.
!:fOTs_: ALL SAMPLES WILL DE RETAI~D _f0fl-2._0_J2,AYS AND THEN
DISCARDED. IF YOU WISH YOUR SAMf_l,._E';g_ RETURNED TO YOUR FACILITY
CALL SAMPLE CO_NTROL AT THE ABOVE _NUMBE=·R~·~----------
S~·~CTRIX DC~-----8 .:. '-.. SAMPL~ ~iU~!SE~: ~5~102·-QRGANICS ANALYSIS DATA SHE~T CF·AGE 1) · ~~~--~~T0~·{· ~=A~£: SF·ECTRIX -.:. ·.: .. :\f••:= t.:=. lC-NO. E-7:~.:i.04-S0.1. S,~:·~~·L~-i~~--T~IX: WAT~R --, --,-···-A'JT'"--~--n E" 71TJ •_1~ ! '""' ~-•:::..:.....:::.~:::-:-:-_ ,..,, -~• . .)t-;.J..-4-t:.!..... : 'I: //·V CASE NO.: ----DC REF·ORT NO. CONTRACT NO. DATE SAMPLE RECEIVED: f/1&{~1 VOLATILES C0~JCENTRA7:~i~-Low· C-~TE EXTRA~TED/PREPARED: 01/24/87 DAl"E A!~~LYI~D: 01/24/87 CAS # COi'1F·OUt✓D DATAFILE:_ 4U01046V01 DILUTION FACTOR:. ) : _/_-_D_O. \JG/L ------·-------------------------------------------------------------------------c.:!.:..i:\ c~:1i::. C::120 _c.:~21:, ,::: J·J::~ -'~ .)·JS t ::·, ., --v~l.:) C-34::", C iJs~:, r-r4.:::::: C06\) C\)6::":1 ci:10 C:115 Cl20 Cl25 C130 C140 C1.45 Ci5(• Ci55 (~6\:; -.... :.:::, ::; C~70 Cl75 Cl20 C2~0 C~05 C~20 C?.~5 ~~·-· :~ -~J::'1 l~ _"::_j. ,:, C2.:+5 C250 C~!LOROMETHANE E:ROMOMETHANE 'J!NYL. CHLORIDE CHLOROETHANE ~ETHYLE~!E CHLORIDE ACETONE C~RBON DISULFIDE l, 1-DICHLOROETHENE 1, 1-DICHLOROETHANE ~~.\~!S-!, 2-8:C~LC~CETHENE CHLOROFORM 1, 2-DICHLOROETHANE 2-E:UT ArWNE 1, 1, 1-TRICHLOROETHANE CARBON TETRACHLORIDE VHNL ACETATE BROMODICHLOROMETHANE 1, 2-DICHLOROPROPANE TRANS-1, 3-DICHLOROPROPENE TfiICHLOF:OETHENE DIBROMOCHLOROMETHANE 1, i, 2-TRICHLOROETHANE ,=::=:i'"JZENE CIS-i,.3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER ~:F-:8i'-10FD~:M 2-~E :-< A~JONE A-M~THYL-2-PENTANONE ~ETR~CHLOR0ETHENE l, .i, 2, 2-TETRACHLOROETHArJE ·:-~,;_ t_,:Ei~E I~:--'.;_ :jF,••::~:t]-~Z~!-lE . E.Th'v'LE:!::}iZE:"iE STYREl\iE TOTAL XYLEr,ES U = l'NOETECTEb AT THE LISTED DETECTION LIMIT 10 U 10 U 10 U 10 U 5 U 31 5 U 5 U 5 U 5 U 5 U 5 U 10 U 5 U 5 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 \J 10 U 5 U 1,::, U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U J = ~2MPQ0~: IS PRESE~IT, BUT BELOW THE LISTED DETECTION LIMIT ::..-.:..: ··:·· .. -~~;~ F(·U~lS I!~ E'.LANK
ORGANICS ANALYSIS DATA SHEET AC r:,s · L~baratory Name: Spectrix Sample Number: __ _f)_~_LD ____ _ Lab Sa.mp le ID No. : __ g_]_D_LQ_t{~RJ_ Dat3. Rel_ease AuthcJrized By: -11J72i Concentration: Lew Cate E:<tracted: _____ ,_/1'1 [g 1 ____ _ Sample Matri:<: Water Date Sample Received: Units: UG/L Q1Dil Factor: -~L~J1_7 3, O Da:te An a. l yz ed: _____ _;,j'{b._2 ____ _ Compounds Detected: ____ [ __ _ NFDC.S # CAS # COMF-'D!JND 10a 108-95-2 F'her1cil 1A 95-57-8 ::-Ch l or,::::p henol 6A 88-75-5 2-Nitrophenol 3A 105-67-9 2,4-Dimethylphenol 2A 120-83-2 2,4-dichlorophenol BA 59-50-7 p-Chloro-m-cresol 11A 68-06-2 2;4,6-Trichlorophen□l 5A 51-28-5 214-Dinitrophenol 7A 100-02-7 4-Nitrophenol 4A 534-52-1 4,6--Dinitro-2-Methylphenol 91'4 87-86-5 Pentachlorophenol U = Undetected at the listed detectiQn -limit J ='Compound is present, but below the listed detection limit B = Compound also found in blank RESULT 1. 7 J 3.3 U 6.7 U 3.3 U 3.3 U 3.3 U 3.3 U 17.0 U 17. 0 U t7.0 U 17.0 U
5Al1PLE NUME:ER: OS-10
-ORGANICS ANALYSIS DATA SHEET -PAGE 4
CASE NO. : ----
OC R[?ORT tJO.: ----.A~ALYST~ CKT DATAFILE: 4U01046V01
8. TENTATIVELY IDENTIFIED COMPOUNDS
VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT
NO NON-HSL COMPOUNDS FOUND 10% OF NEAREST INT: STD.
J = ESTIMATED VALUE - A 1:1 RESPONSE FACTOR IS ASSUMED
INST
At'JALYSJ CKT
\iERIFIED E:Y
CORR. FACTOR
--------------------·------------------------------------------------------~ ------
VOA COMF·OUNOS M/E AMOUNT RRT -------------------------------------------------------------------------------
l75 CIOi BROMOCHLOROMETHANE **IS.1** .128 50 UG/L 1. 000 481)54
369 CI10 1, 4-DIFLUOROBENZENE **IS2** 114 50 UG/L .1. 000 195~0?
.:c3 .:I20 C•S-C HLOROE:E~JZE::NE *i!:·J::53** 1.17 50 UG/L 1. 00C, 1524.::_:;_~
-=,-:.-;, CS15 04'-1, 2-DI,:HLOROETHANE *~·SU.l** 65 84 1/. 1. 297 29•J=:.::. :.... ._ I
~4:7, :: SO::'· D8--TOL!JEi'JE *~·SU2** 98 99 •1 c,_ 950 11. :::• -;: '7 ,:: ..
:. ..;: :., C:S.1.0 F'--~:ROMO~~U0R08ENZEN~ **SU3~* '?::, 97 1/. 1. 156 8.::::: .. =.:..
il2 '2 (::: c~ ~i'::THYLE~JE CHLORIDE ,f 84 1.1 UG/L 0. 640 < . . . .. --. --.:..2 :;· ,: !: :,=:. ;,,:CTDNE 43 3.1. UG/L 0. 703 -:.: :.:: ,::. ·==·
* BLANK CORRECTED ON DATA SHEET
S~,:1PLE ID.
;:=JLENAME
CLIENT
DATE INJECTED
CALIB STD DATE
._; r 1.:... \., l I\ .I. ,-,. 1-"~
SEMIVOLATILE ~ATER REPORT
OS10
·4U01046C01
SPEC-MON
02/04/87 20: 59:00
02/02/87
INST ID.
ANALYST
VERIFIED BY
CORR. FACTOR
4530
CEB
b(J
1.00
-------------------------------------------------------------------------------SCAN# SEMI VOLATILE COMPOUNDS M/E AMOUNT RRT AREA --------------------------------------------------------------------------------540 CI30 1,4-DICHLOROBENZEND-D4 ** IS1 ** 152 40 UG/L 1. 000 18127 751 CI40 NAPHTHALENE-DB ** IS2 **· 136 40 UG/L 1. 000 76541
1045 CI50 ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000 40451 1287 CI60 PHENANTHRENE-D10 ** IS4 ** 188 40 UG/L 1.000 51382
1729 CI70 CHRYSENE-Dl2 ** ISS ** 240 40 UG/L 1. 000 22297 1950 CI75 PERYLENE-Dl2 ** IS6 ** 264 40 UG/L 1. 000 10801
340 CS50 2-FLUOROPHENOL ** SUl ** 112 73 X 0.630 40747 505 CS45 PHENOL-D5 ** SU2 ** 99 71 '7. 0.935 52560
: "77 CS55 2,4,6-TRIBRO~OPHENOL ** SUS ** 330 95 X 1. 126 7892
637 CS20 NITROBENZENE-D5 ** SU3 ** 82 81 . Y. 0.848 21672
·?42 · CS25 2-FLUUOROBIPHENYL ** SU4 ** 172 78 I. 0.901 90880
: ~,.S4 CS30 TERPHENYL-D14 ** SU6 ..... 244 11 B X 0.905 37521
'..:-06 C3 l 5. PHENOL 94 /•7 -5--ll4/L 0.937 432<;
~
0
-=.. :~_\,.'i= _::_ :•:: !'•lt). ~-1~=~~_;:~4::,,)2
s~.t-;F::._~. i'~~ 7RI >:.: ~.A. TE:;;:
SF'CCTl~IX DC ~ ------8
CA'=-E NO.
C!C F.:Et=·ORT NO. :
CONTRACT NO.: ----
·DATE SAMPLE RECEIVED:
VOLATILES
CONCENTRATION: LOW·
C~TE EX-~R~CT~D,PRE~·~RED: 01/24/87
OA Tee ANAL"{:ZEO: 01. / 24 /87
c.:~:..s E;S:1)r·\Or-1CTHAi'JE
C020 ~JINYL-CHL0RIDE
~025 C~ii_OROETHANE
,_ •Y.::u t·1:::1;-ry·L'.::NE 1:HLOF:IDE
C040 C~P80~l DISULFIDE
c .:,4 ':, .L i-DICHLOF:OETHENE
C0~10 1, 1-DICHLORC'ETHANE
C055 TRANS-1., 2-DICHLOROETHENE
CC60 CHLOROFORM
C065 1., 2-DICHLOROETHANE
C 1.1.0 2-E:IJT ANONE
C1.1.5 1., 1., 1.-TRICHLOROETHANE
Cl20 CA~BON TETRACHLORIDE
Cl25 VINYL ACETATE
Cl30 BROMODICHLOROMETHANE
Cl40 1., 2-DICHLOROPROPANE
Cl.45 TRANS-1., 3-DICHLOROPROPENE
Cl.50 TRICHLOROETHENE
Cl.55 DI8ROMOCHL0RCMETHANE
Ci60 1, l, 2-TRIC~LGROETHANE
·._ .:._.::::. =-=.:;;iZE;•-JE
C170 cis~1. 3-DICHLOROPROF'ENE
(l:~ 2---:HLOR0ET~YLVI~JYLETHER
C205 4--r~ETHYL-2-PENTANONE
C220 TETR~CHLQF.OETHENE
C2~S __ l, 2, 2-T~7~PCHLOROETl~A~JE
(:35 C~iL08QE:ENI~~JE
C240 ETHYLSE~JZENE
C245 STYRENE
C250 TOTAL ~iLENES
DATAFILE: 4U0i046V02
DILUTION FACTOR'· / : ·'· ._oo.
. UG/L
1.0 U
1.0 U
1.() u
1.0 U
5 U
1.0 U
5 U
5 U
5 U
5 U
5 U
5 U
1.0 U
5 U
5 U
1.0 U
5 U
5 U
5 U
5 lj
5 U
5 U
5 U
5 U
1.0, U
5 U
1.0 U
1.0 U
5 U
5 LI
5 U
5 U
5 U
5 LI
-5 U
U = UNDETECTED AT THE LISTED DETECTION LIMIT
J = C0~~00ND IS PRESENT, BUT BELOW THE LISTED DETECTION I_IMIT
::: -1~ -~· ... 1i· ·: =_.:r..:c· :.\L.;.-:: ;::,_~;t_:tJC1 IN E:Lt-r-H<
I n ~.::1 r·
I J> l) ),
I lfJ ,:T:I
I J) 0
(_ I # ['l J":i
I -o )..·
. II I 0 _, I}
I ;::, C•
rn I -l ;,:,
Ul I -.. ;.:
-l I ~ ,·
H I 0 2··
::r z I <: ! 1· ,·:,
J.' 0 I 0 I
-l I r-I rri
fll z I J> I
0 0 I -l I z I H I
<: I I r I
J> I I rn I [JI
r 1.n I I 7·, (,
C r-I 0 I IJJ . ·rfi · 7-1
rn I 0 I c, (")
n ! ::r I -I ::,
0 I 7) I -l J:I z
::r I 0 I rn H H
J> 71 C I z >< r,
0 z I -l lfJ
.... C 0 I J> r,
z I -; J> 0 ),
.... 0 z I H ~-:J:t z: ·-lfi J> I < )► 7:, J;,
J) ::r I rn r-0 r-·
ffJ 71 rn I r· -( J) -<
UJ 0 lfJ I -< lO J•· (/]
7) C I -; -I H
0 z. I H H lfJ
z 0 I CJ 0
IJJ I ffJ n z 0
r~ I z :;c J•
I -l -l -)
-ri .... I H );•
)> Ci I -ri
n •' I H Ul
-·I I I 111 :r.
0 0 I I 0 fll
J_l -q I I rn
I I () -;
H z I I 0
(I] rri I I :'.I
J;, I I 7)
J:• :,1 I I 0 7_1
(J) fl) I . I C J> (Q f!1
(fl UJ I (0 I z C'J J> -:)
C -➔ I () I 0 11·1 3 1n
3: I J> I (0 . 7) n
rn H I z I 0 ~ r--·1
0 z I # I J> rn _,._,
:-:I I I -l H
I I J> -Z ),:
(/] I I -ri C
-l I 71 I H () ::r . 0
0 I c I r J> I)) ()
I J) I rn (J) ['l
I H I fll JJ ,i
I -l I
I -< I ./> z
I I C !=' 0
I I 0 lJJ
I J> I .... I
I 3: I C, f-•
I 0 I ./> 0
I C I c,-(jj
I z I <: (I']
I -l I (;I s;.
I I rd
C I I '2_
I I " I I
'
Ci/24/87 16:00:00
O.!.-l.3-87
Ii'~ST
Ar!ALYST CKT
i/ERIFIED E:Y i_flOI
CORR. FACTOR
-------------------------------------------------------------------------------
SCAN# VOA COMPOUrJDS M/E_ AMOUNT RRT ----------·-------------------------·-----------------------------------------·-
178 CI01 BROMOCHLOROMETHANE *~·IS1** 128 50 UG/L 1. 000 50512
37c, CI10 1, 4-DIFLUOROBENZENE *it·IS2** 114 50 UG/L 1. 000 2062:32
4:;:.4 CI20 D5-CHLOROBENZENE **IS3** 117 50 UG/L 1. 000 168"7S::·
22.9 C.Sl5 c,.:-1, 2-DICHLGF:OETHANE *{i•SUl** 65· 89 1/. 1. 287 32·~2.::;.
4-2(:: C.S05 Di3-TOLUE~JE *~·SU2** 00 100 'I 0. 948 1327 :;.2 • u ,.
;:,JS cs·i~~: t=·-E:ROMUFLUOROE:ENZEi\!E *1::·SUJ::·-* o~ q , 1/. 1, 153 9.12-~:; ,_, .0
11-9 C030 t"-'1ETH'r'LENE CHLORIDE jC 84 12 UG/L 0. 663 14:;,;2
* BLANK CORRECTED ON DATA SHEET
C:A3E f·JO. : ----
(!C F:EF'OFT ND. :
CC,NIFAC T NO.
D,'Tc: ~AMF'LE F:ECEIVED: I jt&./<,,7
VOLATILES
C1~flC~~T~ATIC!~: LOW DATAFILE: 4U010461,,'03
GA"fE ~XTRACT~2.IPR~?ARED: 01/24/87·
C-,c..TE AHALY:::::;:,: 01/24.187 DILUTION FACTOR: . /.: _/. _oo
i"'::·,-:.:::-. ~-· \..' -,_,
C:045
C050
C'-360
C065
C.l.1<3
C115
Cj_2Q
C125
Cl30
C140
Ci45
(i~()
::.24(:
C245
:::r:.: C r1 Cll'1C:: TH Al'~ E
~..:It-.J'(L. C.HLOF:IDE
,: hl_ :::JF-:G C.T ~,.:. t-JC
~. l-DICHLOROETHENE
1, 1-DICHLOROETHANE
CHLOROFOR:M
1, 2-DICHLOROETHANE
2-E:UT AN ONE
1, L 1-TRICHLOROETHANE
CARBON TETRACHLORIDE
'✓INYL ACETATE
BROMODICHLOROMETHANE
1, 2-0ICHLOROPROPANE
TRANS-1, 3-DICHLOROPROPENE
-~R!CHLOROETHENE
DIBROMOCHLOROMETHANE
1, !, 2-~R:C~LOROETHANE
=:==:~j::EhiE
CIS~~, 3-0ICHLOROPROF·ENE
2-C~LOROETH'{L~'INYLETHER
'.::;=·,:: :v1~:: F .:; F·:--:
~--:~;:: X .~i'-iC,~·JE
u-0ET~YL-2-PENTANONE
7~~PACHLC~~ETHENE
,:.. :., 2.-2-T~~1:=:.--~Cr.LO:=:-C:ETH1-\~·JE
: --~-;_ :_; E:-;,J E.
ST'r'RE:\iE
TOTAL XYLnit:s
U = UNDETECT~O AT THE LISTED DETECTION LIMIT
UG/L
1c,
10
10
10
5
10
5
5
5
5
5
5
10
5
5
10 = • ..J
5 = ..J
5
5
:::,
= ·...I
5
10 = . ..J
10
10
5
5
5
5
5
5
5
.) = ,: ·)r-iFC!.iH:: r::, F'S:!,"_;-,un, BUT E:ELOW THE l..ISTEC> [,ETECTION LIMIT
u
u
u
u
u u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
u
lJ
u
u
u
u
u
u
u
u
u
u
u
u
OSG,C,N I CS ANAL't'S IS :)ATA '::-i-'EET
L~.b .Sc>.mpl e ID No. : _.l_2fJj)_tj/J__()3_
Dat~ Re\ease ~uthorized By:~
Concentration: Low
D~.te E:<tracted: _____ lj}"IJJ.J __ _
De. t e Ana 1 yo: ed: ______ ,2:/j}i_J ____ _
Nr'DES # CAS # COMPOUND
S2.mp le Mumber: ___ f2.5 fj . __ _
Sample Matrix: Water
Date Sample Received:
Units: UG/L
~Dil Factor:
Compounds Detected: ____ () __ _
RESULT ------------------------------------------------------------------------
10-:?. 108-95-2 F'hen,::,l
1A 95-57-8 2-Ch l ,::Jrc;phenol
6A 8,9-75-5 2-Nitrophenol
3A 105-67-9 2,4-Dimethylphenol
2A 120-8.3-2 2:4-dichlorophenol
SA 59-50-7 p-Chloro-m-cresol
11A 88-06-2 2,4,6-Trichlorophenol
SA 51-28-5 2,4-Dinitrophenol
7A 100-02-7 4-Nitrophenol
4A 534-52-1 4,6-Dinitro-2-Meth1/lphenol
9A 87-86-5 Pentachlorophenol
U = Undetect2d at the listed detection limit
J = Compound is present, but below the listed detection limit
B = tompound also found in blank
5.1) !J
5.0 IJ
10.0 u
5.0 IJ
5.0 u
5.0 IJ
5.0 IJ
25.0 u
25.0 u
25 .. 0 u
25.0 u
0 I f) 1-. ,-·
l> I \ • .I -~-
(J) I Q.I
I ;,, 0
(._ # I ri ::r·;
I -) J;-
II I 0 -I
I Jl Ci
rn I ..., ::r.i
(fl I < ..., I -, ,_
H I 0 2.
::r z < I l:. -· -
J)-0 0 I .:..
-I r I l'I
rn z l> I
CJ 0 ..., I z H I
< I r· I
],-I [Tl I (fl
r U) I ,_I . ,-)
C r-n I TI_I rr1· ~-(1
[Tl 0 I 1·.1 C.1
n ::r I -I ").-
0 ,:1 I -I .J) 2:
::r 0 I rrr H t·I
]> ,) C I z :•< 0
0 z I -I u·1
I-C 0 I ]> C.1 z I -; l• ("t .:r,
I-() z I H z J_I z:
Ul ]> I < l>· IJ l>·
)) :I I rri r 0 1-·
rri ,1 rn I r -< .:-1.1 -(
(_(j (J Cf) I ~ lO J:· r.n
,) C -i -I H
0 z I H H Iii
z CJ I 0 (.'
CfJ I rr1 () Cl
fll I z ~< J;·
I -, --l --1
'"fl t--· I H :;-,,
]> (j I ,1
r., :--: I H ((I
-I I 111 :.1:
0 0 I Cl rri
)) ,1 I I 'I
I 0 --1
H z I 0
CfJ fll I 3:
]", I ,)
]> ;,, I Ci ·r:1
Cf) Pl I C :r-rJi (!)
I.fl IJJ I (I) z ,;, );. ,_I
C -i I n Cl r·1 3 r:·1
:I I ]> Ul -,:, CJ
rn H I z 0 -.., r ··!
0 z # ]> fll ;r_1 ..., -i H
l• -, X ~-
lO '"fl C ..., ,) H 0 3: Cl
0 C r J:• ~IJ (")
)) rn Cfl fTI
H rn )) ;; ...,
-< .i,. z: .c ~· 0
0 ff)
]> I-I
:I 0 t •
0 ~> I-
C O·· l)j
z <
-I ~~· 0
,-.c,_, i
>J ._, ........
01/24187"16-48:00
;)i-13~87
INST
ArMLYST
CORR. FACTOR
4000
CKT
J/01
i. 00
--·------------------------------·----------------------------------------------
'JOA COMPOUNDS M/E AMOUNT RRT -------------------------------------------------------------------------------
179 CI0.1. BROMOCHLOROMETHANE **IS.1.** .1.28 50 UC/L i. 000 5033.l
370 CI.1.0 1, 4-DIFLUOROBENZENE *~·IS2** .1..1.4 50 UC/L i. 000 200.1.~S'
4-t,:J CI20 DS-CHLOROBENZENE **IS3** .1..1. 7 50 UC/L i. 000 1627'.=':J
230 CS1.5 D4-1, 2-DICHLOROETHANE *-tt·SU.1. ** . "" bJ 85 1/. i. 285 3092.1.
44 \:) CS05 US-TOLUENE **SU2** 98 99 i'. 0. 950 1267~.:
s:::::1:", C:3i0 P-8ROMOFLUOR08ENZENF **·SU3** 9"" . J
.:..21. C030 METHYLENE CHLORIDE/-84
97 1/. .1. . 156 8t::89 c:
12 UG/L 0. 676 14oq7
* BLAIH'. CORRECTED ON DATA SHEET
SEMIVOLATILE WATER REPORT
S,,:~PLE ID. OSl 1
r!LENAME 4U01046C03 INST ID. 4530
CLIENT SPEC-MON. ANALYS.T CEB
DATE INJECTED 02/04/87 21:51:00 VERIFIED DY G4
CALIB STD DATE 02/02/87 CORR. FACTOR 1. 00
SCAN# SEMIVOLATILE COMPOUNDS M/E AMOUNT RRT AREA
540 CI30 1,4-DICHLOROBENZEND-D4 ** ISl ** 152 40 UG/L 1. 000 18111
752 CI40 NAPHTHALENE-DB ** IS2 **· 136 40 UG/L 1.000 75800
1046 CI50 ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000 40900
1287 CI60 PHENANTHRENE-D10 ** IS4 ** 188 40 UG/L 1. 000 50796
1728 CI70 CHRYSENE-D12 ** IS5 ** 240 40 UG/L 1. 000 2329.:
19-,9 CI75 PERYLENE-D12 ** IS6 ** 264 40 UG/L 1. 000 10767
2-40 CS50 2-FLUOROPHENOL ** SU1 ** 112 24 t. 0.630 13374
505 CS45 PHENOL-D5 ** SU2 ** 99 37 t. 0.935 27206
1177 CS55 2,4,6-TRIBROMOPHENOL ** SUS ** 330 96 7. 1. 125 8062
637 CS20 NITROBENZENE-D5 ** SU3 ** 82 BB 'l. 0.847 23294
?t",-2 CS25 2-FLUUOROBIPHENYL ** SU4 ** 172 79 7. 0. 901 92895
1 !:a.64 -CS30 TERPHENYL-D14 ** SU6 ** 244 124 t. 0.905 41424
CC:tiTR,;c T N0.
DATE SAl~F·LE RECEIVED:
VOLATILES
DATAFILE: 4U0i046V04
~~7-~ ~XTR~CY~~/PR~F·ARED: 01/2~/87·
C:HT:: ~N.4LY::E:.:.•: (.1_\../24/97 DILUTION FACTOR: . /_:. / · O(?_
UG/L
-------------·---·---·-·-----·------------------------------------------------------··-·
-.-, -: -,
·-·-· -·-
CC,60
C110
C115
Cl:20
C..!.25
c.13~=,
C1.;l0
C1-i5
.• 1 =.-. --._,
·-· --·-·
.. -·-· -·
-·-·-
~1: ~:,,:1,~E
•:· _: ... =.c:,:i;,j DI::-\..)LFIDE
l, i-DIC-HLC1F,CiE:THEi•J~
l, 1-DICHLOROETHArJ~ ..
"' -' --.-.-., ... -....... -.. -...-,,.-~,,-• 0 . ..-.•-i~-..1.., ..:.-u.L\..•r11_vr-. ... ,c:. 1 r.c.1,;C.
Ci-lLOROFORM
1, 2-0ICHLOROETHANE
2-:::UT ANO~JE
1, i, 1-TRICHLOROETHANE
CARSON TETRACHLORIDE
VIcNL ACETATE
BROMODICHLOROMETHANE
1, 2-DICHLOROPROPANE
TRA~fS-l, 3-DICHLOROPROPENE
· ;~::::;-',LC)RC!ETHENE
or;~·GM0CHL~ROMETt~Ai~E
·~·~4 ~: ·::. T"Y F,·Ei\iE
C2SO TOTAL ~YLE!~ES
U = UNDETECT:~ AT THE LISTED DETECTION LIMIT
1,:,
10
10
. 10
5
10
5
5
5
5
'\23
~ . .J
1Q
5
5
10
~ . '"'
5
5
5
~ . .J
5
5
~ . .J
10
5
1<)
10
5
5
5
~ .J
5
5
5
= ,~<-~-:-;:•(;t..,:i -~-: .T.~, 1-=•;.:•::=:~.:.:'ifT, E:UT BELCl.J THE LIS,T~D Ct::.7ECTI 1JN LIMIT
u
u
u
u
u u
u
u
u
u
u
u
u
i.J
u
u
u
u
u
u
u
u
u
u
u
u
u
I_/
u
lJ
u
u
u
u
ORGANICS ANALYSIS DATA 5hEET
ACE>S
~~_,=,.me: Spectri :<
Lab S-:='.mple ID No. : __ g]_QlD_ilQJl/
D~t-3. Release Authorized By: ~
Concentration: Low
Sample Matrix: Water
Date Sample Received:
Units: UG/L
Ex~racted: _____ 1)J~ls1 ___ _
Ana.l y::ed: -----~}s}J_] ____ _
~Dil .Factor: ______ t/. ____ _
Compounds Detect~d: ___ .J. ___ _
NPDES # CAS #
103 10S-95-2 'i...Phenol
lA 95-57-8 2-Ch 1 :~ropt-,enol
.SA 88-75-5 2-~~i tri~phen•~l
3A 105-67-9 2,4-Dimethylphenol
2A 120-83-'.2 2,4-dichlorophenol
8A 59-:50-7 p-Chloro-m-cresol
11A 88-06-2 2,4,6-Trichlcrophenol
5A 51-28-5 2,4-Dinitrophenol
7A 100-02-7 4-Nitrophenol
4A 534-52-1 4,6-Dinitro-2-Methylphenol
9A 87-·86-5 Pentachlorcphenol
U = Undetected at t~~ listet detecticn limit
J = Compound is pre~ent, but bel □~J the listed detection limit
B = Compound also found in blani~
RESULT
·1. 5
-, e ..:... -..J
5.0
-, e .,;_. ,J
.2.5
2.5
2.5
13.0
13.0
13.0
13.0
.]
JJ
lj
JJ
JJ
JJ
JJ
u
u
u
u
CAS #
ORGANICS ANALYSIS DATA SHEET -PAGE 4
. ANALYST:· Cf<T
CASE NO. : ----
DATAFILE: 4U0i046'/;)2
8. TENTATIVELY IDENTIFIED COMPOUNDS
VOLATILE COMPOUND NAMES SCAN# F·URITY AMOUNT
NO NOtJ-~iSL COMPOUNDS FOUND 10% OF NEAREST INT. STD.
J = ESTIMATED VALUE - A 1:1 RESPONSE FACTOR IS ASSUMED
.. -· -·-:....·. .. -· ·-.: .:'.
CKT
CORR. FACTOR .1. 00
VOA COMPOUNDS M/E AMOUNT RRT
174 CI0.1 BROMOCHLOROMETHANE **IS.l** .1.28 50 UG/L .1. 000 4~2C:2,
370 Cii.O i, 4-DIFLUOROBENZENE **IS2** 1.14 50 UG/L .1. 000 2026.1'7
4,::_,4 CI20 05-CHLOROBENZENE **IS3** 1.17 50 UG/L L 000 it.=°•SE:-1:•
227 CSi5 04-.1, 2-DICHLOROETHANE **SU.l** 65 83 •t .1. 305 2'7·J71 " . .:j .-l \~~ C = 1::•::, [".;2-TC:Ll..!E~JE -~*SU2*~ o-98 •t 0, 948 12E:?::-:, :;_ ,t ,.
s:.Q cs:.~:, F·-8ROMOFLUOR08ENZENE -~*:;U3:<·* ,:.. 97 •t L i=,s •:; ::,:::-,,7;:: ,.
.1.2.C! ::.~:;::o METH\'LENE CHLORIDE ¥-84 10 UG/L 0. 6"'"".J'J 11.:::2.·-:-~~
21.:=:, CObO CHI_ORCFOF:M 83 -23 UG/L .1. 236 3 ~; ~_:) ..
* BLANK CORRECTED ON DATA SHEET
~(•,hPLE ID.
rlLENAME
C:LIENT
DATE INJECTED
CALIB.STD DATE
SEMIVOLATILE WATER REPORT
OS12
4U01046C04
SPEC-MON
02/04/87 22:42:00
02/02/87
INST ID.
ANALYST
VERIFIED BY
CORR. FACTOR
4530
CEB
1.00
-------------------------------------------------------------------------------SCAN# SEMI VOLATILE COMPOUNDS M/E AMOUNT RRT AREA --------------------------------------------------------------------------------541 CI30 1,4-DICHLOROBENZEND-D4 ** ISl ** 152 40 UG/L 1. 000 18620
752 CI40 NAPHTHALENE-DB ** IS2 ** 136 40 UG/L 1.000 77834
1045 CI50 ACENAPHTHENE-D10 ** IS3 ** 164 40 UG/L 1. 000 41798
1287 CI60 PHENANTHRENE-D10 ** IS4 ** 189 40 UG/L 1. 000 48514
1728 CI70 CHRYSENE-012 ** !S5 ** 240 40 UG/L 1. 000 14327
1949 CI75 PERYLENE-D12 ** !S6 ** 264 40 UG/L .1. 000 12687
346 csso 2-FLUOROPHENOL ** SUl ** 112 45 'l. 0.640 25594
506 CS45 PHENOL-OS ** SU2 ** 99 76 7.. 0.935 5790~
1177 CS55 2,4,6-TRIBROMOPHENOL ** SUS ** 330 105 'l. 1. 126 899E
638 CS20 NITROBENZENE-05 ** SU3 ** 82 92 ;,: 0.848 25105
942 CS25 2-FLUUOROBIPHENYL ** SU4 ** 172 84 'l. 0.901 100014
1563 . CS30 TERPHENYL-D14 ** SU6 ** 244 99 ;,: 0.905 2020;;:
508 C315 PHENOL 94 /,S -b-UG/L 0.939 5638
7f'71
r.1.1 (_ C
II II II
,·, C. .:·., .-' ( .• ,-.. ' ,,-·1 1·.1 ,, ,-:1 n 0 ("_1 n 0
,·;1 7· fl< fl\. : I I t" ,! ! ~I r 11 Id r:.1 t•.I I I' I·· I • f· I·-'· ,... ,... I·' ,... 1-· , .. .-r Cl L'I-Jo -I'• ,., r.·1 r ,·1 ~ I
01 ,•:, ,. ff• --I ··•I (t. (r· !JI u; Jo .IS t.:< rt.:1 f(I
" I! rr1 i::, UI G· , __ ;• ;1; 1.11 (__, ,:! l_q •.:..' (.ll (., (11 Ci Ct UI 0
' .-:·, -I
C fl I ·-I_[ I 111 ,:·1 ,,, 11_, i•_i i'":1 i_J• I. 1:r ·--1 -I ,... III C n
• I .. , .;: .. ·I !"1 I I -,, : . ~ I 'i H ·1:1 Jl :J:1 H J>
rri -I .... .-· :1· i . ' I. ' ' J i_!,I .. :-·· i-• ;_i:1 H :v h) C, 2. ;i:1
H r_:_1 1, Jl '· i ::.1 11! !Tl r I 'H :1_1 C) 2. I -:-;. -< l)"_l
(.0 r fTl ,-J• iT! I l• ·I _:,. ' .. I I· : II t1l 1::1 :r: (fJ ,::, C• r ,:., ., .I> l_t~ ,: J. ]. ·11 ' ..! I :~ r I H i:.:i z
·' ,) -I )<' fTI I II •II :11 ,,, r , . '·' L,"1 /11 --1 (J () ,... n H J>
. 71 -< i"I! r· ' ' ·:r1 ' -).1 () :J_t I (J 0 -I
" 11'1 -I r· l·I --i ,:) I ;, "?,. rri ,: ' l·I T 0 w r· I rri fTI
(I) :r rn ,,, J··l (l! 'Jl J"LI Pl .. , l··I '· ' [" JTJ ' 0 r -I --1
1'1 Ill z ~:". t (j .. , C• I r f". T ,-, -I Cl ;,:i 0 J> :J!
X IT/ rq ·:.1 rq ·1_1 C: T r :J1 I H 0 ;r_, -I J;,·
1 -; r· :_II ! r; ··I rr1 1··· r ,:-J () fTI n 7) 0 fTI c,
~ (', T .J! 3: 7-I ;r_, ::i: :c
H . rs.i ::: /ri --1 I·/ J:"1 ,-, fTI fTI r 0 fTI r
' cl) -I r z J;, -·J· C• fTJ -I 0 7) -I 0
C rr, () ;,1 --,-·< -o -I I ;r_, J> I ;r_, .. -1 Cl ;,:, 0 , .. :Cl T 'v C, z J> H ' .-' ;:'.'. ;r1 G l:· z 7) fTI z 0 .. .:.• J_l) Cl rri rri .. , ·r:1 7:'.'. f'l :J1 fTI fTI
fTI iTl -I T rn /11 0 ,---I :r: :ri z 'I!
() n1 1'· :ti 1ri rn
~ c, z
-I /Ci fTl
'" H :r: 0 rri z
r r I-' H
lD 3 --1 H . ':I -I Cl
Cl ,,,
-I rr,
("1 _,
H
(_ I z ,-
r-1 :,
H
-I ,... ... I"· ,...
UI UI lij UI Lil UI 1.n C, (,) L'I _o UI [II r_ij UI rJ! UI (.fl (.ij Cl rn
C C C C C C C C C C C C C C C C C C C C C
(') ,-., c, ,c, ,-, ,-~ ,·. ' .. ' •: I ' -' ,... I·• Cl C, ,::, 1:~• r:::.· ,-:, ,',1 ,::, ,.... ,.... <}'-o-01 rJI J;:. /a /., (~I r,' r (I
UI 0 (II 0 en (., ( II i::., '·' 1_11 0
.... 1\1 ... (") ·-I I·• I C., L• ··i 1:·, ,,
I T :~r 1· r, rn J" H .... 0) 10 r J> ,. I-· J:• ,r, --1 ,-·
C I C'.I .,. I I •:(i ... , :r. ,:-_, < •-· ,... ··-! 0 ;r_, f.ll Cl c.1 C.1 C -< :,:i ,--
I J> H C, I H H ·~ 2. ,-c·1 L
-I 2. " Ti ,... r, n rr1 II/ Pl c,
:,:1 0 I 0 T :r: Cl z --1 :c
H 7.: r ::u r., ,-,-H ,,, T r--
0 fTI 0 :I I 0 0 (f_l 1, C, :r: .J".:1 Cl J'! ;,:i '--· 1'".• -, <. .-i:., r 0 H 0 u ,-:L n1 f-1
0 fTI () rri ['l •1 r-Cl
;r_, -I I ·-i -I H 0. fTI·
0 I ,· I :r: Cl .::r:1
fTI J> 0 :t-,n Ill H
-I z ;r_, 7 , z Cl
I f'l 0 rn ff] ['"I
J:• I'll z -I
fTI I
fTI z
fTI
,... 1-f·' ,...
UI 0 Ul Ul (ij (.ij rn UI i:;:i (J1 Ci (.)
C C C C C C C C c<= C C
I I Cl Cl
. I I l> l·
I I -I ··/
I Ill Fl
•. ' ' I I ::-.1 I I I> I" I·• I··• I I ? ,, ..
I.II .::1 I I ]> --1
I ,-.. I i'" ,1_1
I ·1~ I -<. J•
~I I C ' I (/) I l··I .-:·.1
_:1_! T I I I'! -' 1-· I '" I i"_I j?j
-' i::, I I ,.: t
I. ,I 7.: I I
0 I I c_;, .. ,_:
j[j :i I I I• -;:1
-I P"I I I ·,. ['l :r: ... , I I rt, ·1_1
)> :i: I (") I ,, J,
::1_ J• I c, I ....... .JJ
ITl ,_ I 3· I (;) rn
rn. I ,) I --J Cl
I 0 I
I C I
I z I (,)
I 0 I I-·
I I .,_
I I ru
I I .(.,
I I
, __
I I Ill
I I -.J
I I
I I
I I
I I
I I
I I
I I
I I ·o
I I H
I I r
I I C:
I I -I
I I H
I 0
I -Z I
I 'Tl
I J>
I n
I -I
I 0
I :1.1
I
I
I ---I
C
)-• I-· C, -1::1 0 ' r : C) C C Q
' ·-.i
•.:1 z (',
rr1 .. 7. , ..
-I ·1.1 --··I
!· I
r· .-.:.,
'£.
<: C• r
J;, -I
H r· rn
Cl (/J
J>
-I J>· 'TJ
H r
fTI
,,
C:
(:1 ,...
Ci
+-'
I)'-
< 0 UI
!_-, 1J1 t I
I· j, I .
: ~ i::. 1:-'. )... .,.
I (l I:'! 1·
ii.!·:• I
i-• .•I
. f"! ·.1.1
1·1! I! ,.
I•
.j;., :-,(·
1),
•.•.:,
UI
Cl C'> :!) (":I
1.-.. () C.1 J;.
-~ Z lfl
fll ·-i ::n fii
)_l l"rt rn J, !_1
"J:, Ct C• C•
? -·I ·_1:i i::i ·--I ,--z
In q z
•.') !-1
rn
QRGANICS ANALYSIS DATA SHEET
ACIDS
Saa.:nple N'..cmber: ___ Q,5 /.,3 ___ _
La.b Sa.mple ID No. :_tfJ(2/01t'.ft_05 Sample MatriM: Water
Data Relea.se Authorized By:---1/Pi
Concentration: Low·
Da.te. Sa.mpl e f;:ecei ved: ···-_Ju/J:;
Units: IJG/L
Da.te Extracted: ____ / htzir1 ____ _
D2 te An2 l y:: ed: ____ _d:l!/lt.J... ____ _
~Dil Fa.ctor: ______ 3 ___ _
Compounds Detected: ____ (! __ _
CAS # C:JMPOUND
10a 108-95-2 F'henol
1A '7'5-57-,S 2-Chlorophen □l
bA 88-75-5 2-Ni trophen,:il
3A 105-67-9 2,4-Dimethylphenol
2A 120-83-2 2~4-dichlorophenol
8A 59-50-7 p-Chloro-m-cresol
11 A 88-06-2 2,4,6-Trichlorophenol
5A 51-28-5 2,4-Dinitrophenol
7A 100-02-7 4-Nitrophenol
4A 534-52-1 4,6-Dinitro-2-Hethylphenol
9/0! 87-86-5 Pentachlorophenol
U = Undetected at the li5ted detection limit
·J ='Compound is present, but below the listed detection limit
B = Compound also f~und in blank
RESULT
3.3
3.3
6.7
-, ~ •.J. •.:>
3.3
3.3
3.3
17.0
17.0
17.0
17.0
u
u
u
IJ
u
u
u
u
u
u
u
1-__ ,_.: 3FECTRI:< DC~ ----·-·-
SAMPLE NUMBER: OS-i3
CRC~NICS ANALYSIS CATA SHEET -PACE 4
b~~Clk~X CORPORATION
ArJ~LYST:. CKT
~-TENTATIVELY IDENTIFIED COMPOUNDS
CASE NO. : ----
DATAFILE: 4UGi046VOS
------------------------------------------------------------------------------·-·
CAS # VOLATILE COMPOUND NAMES SCAN# PURITY AMOUNT --------------------------------------------------------------------------------
NO NON-HSL COMPOUNDS FOUND 101/. OF NEAREST INT. STD.
J = ESTIMATED VALUE -A 1:1 RESPONSE FACTOR IS ASSUMED
UJ () r::1 ,. ' " ' , .. 1..'l .r~, I ,l .js (,) ,, c, l> 1' r· I· I
fd-LJ t, r ... :i 0 -1 (D J, r-·-1 H
I-' (l 1.:.• 0 "' C, C, z I 1-1 rr~ [Tl Fi ,, ' "'' I (~I z '
0 c, ,·-:1 ,-, 0 0 n I I I· I --1 }:· lq
c, ,r, (rt (fl H H "'' i I (J~t :::· .:.-:
(._) /-• i:;i I-' r,, I-' c:1 I I -I (.__ j"f1 l·"I
* C, (,', Ul (.'I (:1 C, f;"-/. I 0 r1 (!
• I I ._.-,
co I I r_:I -I ,-..,. 7_! i::.1 0 CJ /-" IJ:! I I )>· "' :,, iii i.:-; :z I ((I .,,, Lil -J:1 I I ·-I
7' --l m I I I .., C, I I r:1
n I j_1 -·/ I_-' n I .3 .. I I
-<'() () :r: Q C, I I
·O r :r ,-· f,J r H Ci I I ;o ;o rn (J C I 0 ·n I: -1 I
rn z ,, fl) Cl J:I r r· I I .r;, ,•~1 '" ., .. :.:,
n rr, ,. .. -~:: H'O C 0 I C I I•· I--u C 1_q
-t C nt C:i IJ:I 0 ::r.1 I c, I iTI ,:;, I ,,,
c:, () 0 I rn ::JJ 0 I J> I , .. 1',.1 C• , _ I -
:r: J:.1 r z 0 ::r I I l,l .,i::. ·; ,:.1 I',·,
0 r 0 () ~J I:) rn I () I . / ry·
2 0 ((I ;,:, fTI rn --l I 0 I (0 /JI c, (I-
c:, ;o n·, () z z I I ::r 1· -J · I z '•-
:,, H z rn rn ~I J>· I ,, I ·:?:• ()
-t r_1 f 1 -l rn z I 0 I ·1--UI l•
:,, fT/ fll 1: z rn I C I 'J)
~~ :r,, n, I ., z: I ,·,
V, ~-I Cl 1.· 1\J :c· ..:: ..
rn rn I rf1 I 1" >
rn I ;:
-t ' I 0 .. ,
* * * * * * I ,; ,..:.1 ·H
* '~ "' * * * I I .. ,
(0 (f J (Jj H H H I. ;·
C: --c: [j) (JJ u:, I -·! '-· r,1 r.) I-' (J ru I-' I !"·I ~->) * * * * I ,··,
* * * * * * I ;-~
I I .,.,
I :1'!
I
.,,
/-" ,. /-" I ::;:: ;,d
CO, . .J'J -0 0-· /-" /-" ru I '-J,1 i.,-i .., UI (0 ln -~ -I> I]) I rn ·I 1•·.
I Ci
I --1
I (") <" J> H :1.1
I 0 iii z -z: H
I ;o J:1 l> rJ1 : .. :
I l> ;o H r· -➔
/-" /-" ::r •I ~-i::i
/-" C, 0 ..:, ll/ rn ln 0 H IJI () .., C, ru l,) 0 C, 0 C ·11 n1 -I z l> C:J .,,,
C ;-.: -. ;-.: C C C -l () •' 0 0 0 ,;-, •➔ ,:,:, I
' -,, ' ' C, -:.: I
r r r r ;o I
I
I ....
0 ... 0 ! ... /-" ! ~
.,,
J:I
0-I-' -0 ru G• 0 0 :0 C'> .i,.
-.J rn -I> -.J C, 0 G> --l 0 7:. 0
ru en OJ (0 0 C, C, \ -I 0
t· 0
•· ,_. I)) .o
/-" -0 LJ Ll 1)--C, r..n .:-;,
(I· -I> .I; ,t, .. , rn ,:1 l•
(I" ul di , .. 1·,) I, I -~• :11 I
'" ' ,, i' ,:, t'. 11 (I· .. , !'I !
.-;:', -~ t
,_ ; ,. •', 1!! I. !I ,(I i::• !• ' -./
'ILENAME
:LI ENT
)ATE INJECTED
:ALIB STD DATE
SEMIVOLATILE WATER REPORT
OS13
4U01046C05
SPEC-MON
02/04/87 23:34:00
02/02/87
INST ID.
.ANALYST
VERIFIED BY
CORR. FACTOR
4530
CEB
1.00
:. '.-
--------.. ----------------------------------------------------------------------
;;CAN# SEMIVOLATILE COMPOUNDS AMOUNT RRT AREA.: -------------------------------------------------·------------------------------
:;41
752
1046
1287
1729
1950
349
509
1178
638
942
1564 ·
CI30 1, 4-DICHLOROBENZEND-~D4 ** ISl **
CI40 NAPHTHALENE-DB -1S2 **
c{:fo'" ACENAPHTHENE-Dto;:··** Ts3 **
CI60 PHENANTHRENE-D10.''fi1-IS4 **
CI70 CHRYSENE-D12 ** IS5 **
CI75 PERYLENE-D12 ** 1S6 **
CS50 2-FLUOROPHENOL ** SUl **
CS45. _PHENOL-D5 fil-SU2 **
CS55 2, 4,·6-TR IBROMOPHENOL ** sus· **
CS20 NITROBENZENE-D5 ** SU3 **
CS25 2-FLUUORDBIPHENYL ** SU4 **
CS30 TERPHENYL-D14 ** SU6 fil-
152
136
164
188
240
264
112
99
330
82
172
244
40 UG/L
40 UG/L
4o··uG1L:
40 UG/L
40 UG/L
40 UG/L
72 X
69 X
98 X
83 7.
74 X
69 'l.
1. 000
1. 000
1. 000
1. 000
1.000
1. 000
0.645
0.941
1. 126
0.848
0.901
0.905
18408
76364
42279
5162',
19:,2::
15C2~
40406
5199(
8454
2225<;
8987:
1924<;