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HomeMy WebLinkAboutNCD095458527_20020718_FCX Inc. (Statesville)_FRBCERCLA LTAR_LTAR Semi-Annual Sampling Event Report November 2001 - April 2002 OU-1-OCRI I I I I I I II I I I I I I I I I I I Document Control No. RFW133-2A-ALIJ Revision 0 LONG TERM RESPONSE ACTION APRIL 2002 SEMI-ANNUAL SAMPLING EVENT REPORT (NOVEMBER 2001 THROUGH APRIL 2002) FCX-ST ATESVILLE OPERABLE UNIT 1 GROUNDWATER REMEDIATION STATESVILLE, NORTH CAROLINA Work Assignment No. 133-RALR-048M July 2002 REGION 5 U.S. EPA CONTRACT NO. 68-W7-0026 Weston Solutions, Inc. Suite 200 5405 Metric Place Norcross, Georgia 30092 WESTON W.O. No. 20064.133.100.0930 NOR/K:\WP\20064\133\Apr2002-2nd semi-annual rpt.doc I I I I I I I I I I I I I I I I I I I Prepared By: Approved By: Approved By: Approved By: LONG TERM RESPONSE ACTION APRIL 2002 SEMI-ANNUAL SAMPLING EVENT REPORT (NOVEMBER 2001 THROUGH APRIL 2002) REVISION0 FCX-ST A TESVILLE OPERABLE UNIT 1 STATESVILLE, NORTH CAROLINA U.S. EPA Contract No. 68-W?-0026 Work Assignment No. l 33-RALR-048M Document Control No. RFWl 33-2A-ALIJ July 2002 Date: _'7,_,/,_~! _r4-j__co-'2...=--/ N Site Manager ~~ ~alphP.McKeen, P.E. Date: ? k /2-2 ---,,~~---- WESTON Quality Assurance ~tf:tt£t¼ Program Manager Date: ~/2'+"~"'-1-/4~.J-__ Date: --------Ken Mallary EPA Region 4 Remedial Project Manager NOR/K:\ WP\20064\l 33\Apr2002 -2nd semi-annual rpt.doc RFWJ33-2A-ALU This document was pn..-pared by Weston Solutions, Inc., expressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Section 1 2 3 4 5 TABLE OF CONTENTS Title Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 Page INTRODUCTION .............................................................................................. 1-1 I. I 1.2 1.3 1.4 Purpose .................................................................................................... 1-1 Background ............................................................................................. 1-1 Lithology and Hydrogeology .................................................................. 1-5 Long-Term Response Action .................................................................. I-7 LONG TERM RESPONSE ACTION .............................................................. 2-1 2.1 2.2 Operation and Maintenance (O&M) ....................................................... 2-1 Groundwater Monitoring ......................................................................... 2-1 L TRA SUMMARY ............................................................................................ 3-1 3.1 Operation and Maintenance (O&M) Summary ....................................... 3-1 3.2 Second Semi-Annual Sampling Event -April 2002 ............................... 3-3 3.2.1 Groundwater Monitoring ................................................................... 3-3 3.2.1.1 3.2.1.2 Monitoring well Sample Results ........................................... 3-3 QA/QC Sample Results ......................................................... 3-6 3.2.2 Treatment System Monitoring ........................................................... 3-6 3.2.2.1 3.2.2.2 3.2.2.3 Water Level Elevations ......................................................... 3-7 Treatment System Results ..................................................... 3-9 POTW Discharge ................................................................ 3-10 CONCLUSIONS AND RECOMMENDATIONS ........................................... 4-1 REFERENCES ................................................................................................... 5-1 NOR/K:\WP\20064\133\Apr2002 -2nd semi-.annual rpt.doc RFW I 33·2A-ALIJ This document was prepared by Weston Solutions, Inc., expressly for EPA. It shall not be disclosed, in whole or in part, without the express written pennission of EPA. I I I I I I I I I I I I I I I I I I I Figure 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 TABLE OF CONTENTS (Continued) Title Site Location Map Site Map LIST OF FIGURES Shallow Aquifer Potentiometric Surface Map Alpha-BHC Concentration Map Beta-BHC Concentration Map Gamma-BHC Concentration Map Heptachlor Epoxide Concentration Map I, 1-Dichlorocthane (DCA) Concentration Map Chloroform Concentration Map Tctrachloroethene (PCE) Concentration Map Trichloroethene (TCE) Concentration Map Chromium Concentration Map Manganese Concentration Map Vanadium Concentration Map Quick Flow Model Results-November 2001 Quick Flow Model Results-December 2001 Quick Flow Model Results -January 2002 Quick Flow Model Results -February 2002 Quick Flow Model Results -March 2002 Quick Flow Model Results -April 2002 Quick Flow Model Results -November 2001 through April 2002 NOR/K:\WP'l200641133\J\pr2002 -2nd sc-mi-annual rpt.dtx: 11 RFW J 33-2A-ALIJ This document was prepared by Weston Solutions, Inc., expressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statcsvillc Operable Unit I Revision: 0 Date: July 2002 TABLE OF CONTENTS (Continued) Table 2 3 4 5 6 7 LIST OFT ABLES Title Groundwater Remediation Levels Summary of Monitoring Well Analytical Results Water Level Data Modeling Data Influent and Effluent Results Recovery Well Flow Meter Readings-Cubic Feet Recovery Well Flow Meter Readings-Gallons LIST OF APPENDICES APPENDIX A-City Discharge Permit APPENDIX B-System Check Forms APPENDIX C-Purge Forms APPENDIX D-Charts Traffic Reports and Chain of Custody APPENDIX E-Laboratory Analytical Reports APPENDIX F -Trend Analyses Charts APPENDIX G-Depth to Water Charts NOR/K:\WP..20064\133\Apr2002 -2nd semi-annual rpt.doc Ill RFW133-2A-ALIJ This document was prepared by Weston Solutions, Inc., c.iprcssly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I 1.1 PURPOSE SECTION 1 INTRODUCTION Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 EPA Region 4 tasked Weston Solutions, Inc., formerly Roy F. Weston, Inc., (WESTON@) to perform the Long Term Response Action (LTRA) at the Farmers Cooperative Exchange (FCX)- Statesville site, Operable Unit One (OU!) in Statesville, Iredell County, North Carolina The work is being performed under the Region 5 Response Action Contract (RAC) No. 68-W7-0026. The L TRA includes performing weekly operation and maintenance of a pump and treat system designed to capture and treat groundwater contaminated with pesticides and volatile organic compounds (VOCs) and semi-annual groundwater sampling of a network of 18 monitoring wells. 1.2 BACKGROUND The following information comes from the January 24, 2000 Statement of Work. The FCX- Statesville property is located at the intersection of Phoenix Street and West Front Street (Highway 90) approximately 1.5 miles west of downtown Statesville. The Site is approximately 5.5 acres in size. The coordinates of the Site are 35°47'11" north and 80°54'58" west. The Site is bound to the north by the Norfolk-Southern Railroad and Burlington Industries (formerly Beaunit Mills), to the west by the Carnation Milk Company property, to the south by residential and small businesses, and to the east by a prefabricated utility and sales lot (Figure I). Beginning around 1940, FCX began operations as an agricultural distribution center. These operations included the formulation, repackaging, warehousing, and distribution of farm chemicals, primarily pesticides and fertilizers, along with the milling and sale of feed grains. The repackaging of liquid pesticides was discontinued in 1966 and dust repackaging in 1969. NOIVK:\WP\20064\l33\Apr2002 -2nd snni-annual rpc.doc 1-1 RFWIJJ-2A-ALIJ This document was prepared by Wcslon Solutions, Inc., e,prcssly for EPA. It shall not be disclosed, in whole or in part, without the express wriucn pennission of EPA. I I I I I I I I I I I I I I I I I I I Second Scmi•Annual Sampling Event Report FCX-Statesvillc Operable Unit I Revision: 0 [hte: July 2002 The following information comes from the January 1999 Remedial Action Report. The site is currently abandoned. The dominant on-site structure is a warehouse located on the western half of the property. The warehouse consists of two attached structures: an upper building, constructed in 1968 or 1970, and a smaller, lower building constructed in I 982. The area south of the warehouse is paved except for a narrow grass strip along the sidewalk. The eastern half of the site is dominated by a large concrete pad, 6 inches to 7 inches thick, 62 feet wide, and 190 feet long, extending from the eastern end of the warehouse along the north property line. The area south of the pad is covered almost entirely with approximately 6 to 12 inches of crushed, compacted gravel. Several smaller areas within this area, mostly tractor-trailer pads and parking area, are paved with either concrete or asphalt. The area, except for the paved area between the warehouse and West Front Street, is completely fenced, mostly with chain-link fencing. The fence is in good condition and access is gained via Phoenix Street through a 36-foot-wide gate along the eastern end of the site. The gate is locked with a heavy chain and padlock. During the summer and early fall of 1991, U.S. EPA Region IV, conducted an in-house Phase I RI at FCX. The investigation involved extensive sampling (237 samples) of on-and off-site soil, groundwater, surface water, and sediment. Significant findings relating to groundwater contamination are summarized in this section. Samples from on-site monitoring wells indicated that both the surficial (saprolite) and bedrock portions of the groundwater system beneath the site are contaminated with pesticides, primarily lindane, BHC compounds, endrin ketone, and chlordane. A variety of chlorinated solvents were detected in groundwater samples from on-site monitoring wells, as well as the process well located on the Carnation property west of the site. The highest level of contaminant observed was tetrachloroethylene (PCE), with concentrations in excess of I 00 micrograms per liter (µg/L) being detected. Phase II of the FCXS RI was primarily an expanded investigation of grourrlwater quality and alleged trench location. Existing, on-site permanent monitoring wells and a network of 12 NOR/K:I WPl20064\133\Apr2002 -2nd semi-annual <pl.doc 1-2 RFW I JJ-2A-ALIJ This document was prepared by Weston Solutions, Inc., c:,>rcssly for EPA. It shall not be disclosed, in whole or in part, without the express written permission or EPA. I I I I I I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 temporary monitoring wells, located both on-site and off-site, were sampled to provide further groundwater characterization. The Phase II groundwater sampling program was designed primarily to evaluate the extent of pesticide contamination. Samples for purgeable organic compound analyses were also collected to obtain additional information on the extent of the chlorinated solvents. The pattern of contamination and groundwater flow patterns developed during Phase I of the investigation formed the basis for selection of the temporary monitoring well and permanent bedrock monitoring well locations chosen by EPA for Phase II. Most of the temporary monitoring wells were installed to provide additional data to be used to evaluate the lateral extent of contaminants in the overburden portion of the aquifer. One of the temporary wells, however, was installed to evaluate contamination previously identified m permanent well MW-3 that was higher than detected in any of the other permanent wells. In the saprolite, pesticides in groundwater arc restricted to the FCX property, with the exception of one detection of lindane. Lindane is one of the most mobile pesticides, and would therefore be expected to migrate farther than the other pesticides; however, the presence of lindane in the off- site well is difficult to explain. If the estimated movement of lindane in the saprolite is projected to be equal to the groundwater velocity, it would take over I 00 years for lindane to move through the saprolite from the closest area of lind:me groundwater contamination on the site to the off- site well. Also, the well is not directly downgradient of areas of pesticide contamination at the site. The modeled potential extent of pesticide contaminant plumes in the saprolite based on the observed lindane indicated that migration ranged from only a few feet from the source area for DDT and DOD to over I 00 feet from the source area for the most mobile pesticides. Contaminant migration rates in the bedrock are projected to be faster than contaminant migration rates in the saprolite. Only the more mobile pesticides (BHCs and endrin ketone) have been NOR/K:\WN0064\l 33\Apr2002. 2nd semi-annual rpt.doc 1-3 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e,prcssly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statcsville Operable Unit I Revision: 0 0-.itc: July 2002 found in samples from any bedrock wells, indicating that the vertical movement of the other, less mobile pesticides through the saprolite has not yet been detected in the bedrock groundwater. The results of soil transport modeling show that, potentially, the trichloroethene (TCE), PCE, and related contaminants detected in groundwater beneath the site may have been leached from soils along the northern side of the site at some time in the past. It is therefore possible that some of the VOC contamination now detected in groundwater beneath the site is the result of past leaching of VOC contaminated soils. The location of TCE and PCE contaminated soils beneath mostly impervious areas suggests that present soil leaching of these contaminants from FCX is likely to be insignificant. VOCs have generally been found in soils in concentrations of less than 10 µg/kg and arc mostly present in soil samples from less than 3 feet deep. Soil VOCs are primarily TCE and PCE. Groundwater samples indicated contamination by VOCs in excess of the Federal Maximum Contaminant Levels (MCLs) and the North Carolina Drinking Water Standards, both beneath the site and in a plume extending downgradient of the site. The distribution of the chlorinated VOCs in soils, groundwater, sediment, and surface water samples indicates that some of the VOC contamination may have originated from an off-site source to the north of the FCX property. Some groundwater samples also contain metals in excess of Federal or state 1,>roundwatcr or drinking water quality standards. According to the Phase II RI (EPA, 1992) these metals concentrations do not appear to be directly site-related. As part of OU3, additional monitoring wells were installed in the vicinity of FCX, and select wells were sampled in December 1995. Monitoring wells MW-Ss, MW-Sd, MW-11, W-22, W- 23, W-24, W-25, W-27, and W-29 were sampled for VOCs, SVOCs, metals, pesticides, and PCBs. It appears that in the saprolite, pesticides in the groundwater are restricted to the FCX property. Lindane and alpha-BHC were detected in MW-11. Lindane and the BHC compounds are some NOR/K:\Wl'\200641133\Apr2002 -2nd semi•annual rp1.doc 1-4 RFWIJJ-2A-ALIJ This document was prepared by Weston Solutions, Inc., e~ressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Scmi•Annual Sampling Event Report FCX•Statcsville Operable Unit I Revision: 0 Date: July 2002 of the more mobile pesticides and would therefore be expected to migrate farther than other pesticides. Also, contaminant migration rates in the bedrock are projected to be faster than contaminant migration rates in the saprolite. ROD cleanup goals were exceeded for alpha and beta BHC and lindane in three wells. Alpha- BHC and lindane concentrations exceeded cleanup goals in MW-5s and MW-5d (on-site saprolite and bedrock wells, respectively) and MW-I I. Beta-BHC exceeded cleanup goals in MW-5s and MW-5d. Groundwater samples indicated that contamination by VOCs in excess of the MCLs and North Carolina Drinking Water Standards, both beneath the site and downgradient of the site, exists. VOCs exceeding MCLs were detected in both saprolite and bedrock wells with the highest concentrations in bedrock wells. 1.3 LITHOLOGY AND HYDROGEOLOGY The following information comes from the September 1993 Declaration for the Record of Decision. The FCX site lies within the geologic belt known as the Blue Ridge-Inner Piedmont Belt. The soils at the site are primarily silts or clays. The Blue Ridge-Inner Piedmont Belt generally consists of metamorphic rocks including gneisses and schists, as well as gradations of the two types. Most of these rocks near the surface have weathered into a layer of overburden overlying the fractured, but relatively unweathered bedrock. The overburden ranges in thickness from 15 to 40 feet at the site, and consists of saprolite and residual soils interspersed with unweathered gneiss/schists. Granitic intrusions are also common in the area of the site. Soils in the general area of the site belong to the Lloyd Association. These soils are characterized as deep, well-drained soils with a subsoil of dark, red clay. Groundwater at the site occurs in an unconfined to semi-confined aquifer consisting of the overburden hydraulically interconnected with the underlying fractured bedrock. The saturated overburden serves as a groundwater reservoir that supplies water to the fractures, faults, and other secondary permeability features in the bedrock. The approximate depth to groundwater in NOR/K:IWl'l20064\133\Apt2002 -211dsrmi-annualrpt.doc 1-5 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., qnessly for EPA. II shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 the saturated overburden in the vicinity of the site generally ranges from 27 to 30 feet below land surface. During the wetter periods of the year, groundwater may intersect the ground surface and become overland or surface water flow. The following information comes from the January 1999 Remedial Action Report. FCX is located in a hilltop topographic setting. Such hilltop topographic locations are characteristically groundwater recharge zones. In groundwater recharge zones, groundwater flow usually has a downward component and the migration of contaminants into deeper parts of an aquifer may be enhanced in such areas. Water quality data suggest that this is the case at FCX. The soil permeability, or hydraulic conductivity, controls the amount of groundwater recharge, surface-water runoff and percolation, and rate of contaminant migration through the saturated zone. At FCX, the calculated hydraulic conductivity in the saprolite is approximately 1.62 x I o·6 ft/sec, which is indicative of a relatively low permeability unit. This thickness of the unsaturated zone should allow for substantial soil immobilization of many of the site-related contaminants. Measurements made at the site indicate that the hydraulic conductivity of the saprolite (weathered bedrock) is relatively low. The bedrock hydraulic conductivity is probably highly variable, with limited zones of high or moderate permeability along rock fractures, separated by substantial interfracture areas of extremely low or no permeability. The hydraulic conductivity contrast between the bedrock and saprolite may also cause groundwater to flow downward from the saprolite into the bedrock. The hydraulic gradient appears to steepen toward the south and east. The variations m the hydraulic gradient suggest that the site is near a groundwater divide. The high soil clay content reduces the mobility of both orgamc compounds and inorganic substances. In bedrock, fracture flow predominates, favoring increased contaminant mobility in the bedrock (EPA Phase II RI, 1992). NOR/K:\WPl2006411331Apr2002 -2nd semi-annual rpl.doc 1-6 RFW133-2A-ALIJ This document was prepared by Weston Solutions, Inc., e;,pressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I ii I 1.4 LONG-TERM RESPONSE ACTION Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 The following information comes from the January 24, 2000 Statement of Work and the January 1999 Remedial Action Report. EPA tasked WESTON under ARCS Contract 68-W9-0057 to install a ground water pump-and-treat system and to operate the system under work assignment no. 78-4RA8M. That work assignment provided for the operation and maintenance (O&M) of the LTRA from April 1998 through May 1999, at which time the work assignment was closed out because the ARCS contract expired. No L TRA was performed from May 1999 to April 2000. The Operable Unit I (OU!) ground water pump-and-treat system consists of ten (10) 4-inch vertical recovery wells (RW-1 through RW-10) and pneumatic submersible pumps for ground water extraction; four transfer pumps; a 300-gallon holding tank; a 1,200-gallon baffled holding tank; two (2) sand filters; and two (2) granular-activated carbon (GAC) units for treatment. The treatment system, powered by Duke Power, Inc., was transported to the site on April 25, 1998 and was installed by Envirosys, Inc. of Tampa, Florida on a level gravel pad that was prepared for the system at the site for treatment. Groundwater is extracted from the overburden materials beneath the FCX property using I 0 extraction wells and transported to an on-site treatment facility for treatment by filtration and carbon adsorption. Treated groundwater is discharged to the local publicly owned treatment works (POTW) under discharge permit T-43 issued by the City of Statesville (Appendix A). The ten recovery wells (RW-1 through RW-10) were installed and developed for the extraction system. Each of these wells was completed with four-inch outside diameter PVC casing and has 40 feet of 0.010-inch screen. Total depths ranged from 56.5 to 65 feet below ground surface. Pneumatically operated pumps were installed in each well and all wells were then permanently plumbed to the treatment system. Plumbing consisted of a ¾-inch diameter Schedule 80 PVC airline and a 2-inch Schedule 40 PVC water influent line. The airline supplies pressure to operate the pneumatic pumps while the influent line transports water pumped from the wells into the treatment system. These lines run parallel and are buried from 1.5 to 2.5 feet below ground NORIK:\WP\20064113J\Apr2002. 2nd semi-annual rptdoc 1-7 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e:,::iressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statesvillc Operable Unit I Revision: 0 Date: July 2002 surface. In areas necessitating aboveground installation (between RW-4 and RW-5 and at the treatment system entry), the water line was insulated with foam insulation. From April 1998 through May 1999 various activities were implemented as part of the O&M of the treatment system including: performing routine maintenance and repairs; weekly ground water level measurements from the existing monitoring wells and recovery wells; recording instrument readings; recording flow meter measurements from the recovery wells as well as effluent discharge, collecting influent and effluent samples from the system for analysis, and collecting ground water samples from the designated monitoring wells on a quarterly basis for analysis. Currently, there are twelve permanent groundwater-monitoring wells on the FCX property, as well as six wells further downgradient (Figure 2). Monitoring well W-22, located within the warehouse, was within the area that has been excavated and backfilled as part of the remedial action for OU2. During the remedial action, the well was destroyed. The previous work assignment, 047-RARA-048M, set the framework and requirements for WESTON to conduct the L TRA which included system start-up and diagnostic testing, O&M, performance monitoring, and sampling and reporting at the FCX -Statesville site. The Record of Decision (ROD) issued in September 1993, describes the RA selected for this site, and the RD documents provide the construction and implementation detail required to achieve the selected RA. The work assignment began April 2000; the completion date for the work assignment'was April 30, 2001. The current work assignment provides for the continuing implementation of the LTRA. NOR/K:\WP\200641133\Apr2002 -2ml semi.annual rpt doc 1-8 RFWI 33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e,pressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. . \ ,-.; ~ .. )11?Y ,,1·•. ,i:·, ,' ',,1_ ./f:.:\: i'.' ~::/.;: ;:.,:(,· ,;':. ~ ::•, : ;· _·~1' ~; ·, I I I I I I I I I I I I I I I I I I I SECTION 2 Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 LONG TERM RESPONSE ACTION 2.1 OPERATION AND MAINTENANCE {O&M) Applied Earth Sciences (AES) has been contracted by WESTON to perform O&M. O&M 1s performed on a weekly basis while additional site visits for non-routine maintenance are conducted on an "as needed" basis. In addition to performing maintenance to the system, the subcontractor records the system operating parameters such as recovery well flow meter readings, weekly discharge meter readings, pressure gauge readings, the time of the inspection and/or readings, and measures the groundwater elevation in the recovery wells. 2.2 GROUNDWATER MONITORING The subcontractor is required to perform semi-annual groundwater sampling. Groundwater from twelve on-site and six off-site monitoring wells and the influent and effluent to the OU I pump and treat system are sampled and analyzed for the contaminants of concern. The purpose of the monitoring is to verify: • that the pump and treat system is effective, • that cleanup standards for groundwater are achieved throughout the L TRA; and • that the system meets the effluent limits of the discharge permit. The contaminants of concern and the corresponding remediation levels and discharge limits are provided in Table I. The subcontractor is also required to record the water level in each of the extraction wells each week. The purpose for collecting groundwater elevations is to determine if the system is providing adequate capture of the contaminant plume beneath the site. NOR/K;\WP\20064\133\Apr2002 -2nd $erlli-arumal rpl doc 2-1 RFW 133-2A-ALIJ This document was prepared by Weston Solutions, Inc., q-,ressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 The samples are collected in accordance with the following documents: • Long Term Response Action Sampling And Analysis Plan, dated April 2000, and • U.S. Environmental Protection Agency Science and Ecosystem Support Division (EPA- SESD), Region 4, revised Environmental Investigation Standard Operating Procedure and Quality Assurance Manual (EISOPQAM), November 2001. Laboratories in the Contract Laboratory Program analyze all samples with the exception of the effluent sample. Prism Laboratories located in Charlotte, North Carolina analyzed the effluent sample. Samples are analyzed for volatile organic compounds (VOCs), base/neutral acids (BNAs), pesticides, polychlorinated biphenyls (PCBs), and total metals. NOR/K:\WN0064\133\Apr2002 -2nd semi-annual rp!.doc 2-2 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., c,pressly for EPA. It shall not be disclosed, in whole or in part. without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I SECTION 3 LTRA SUMMARY Second Semi-Annual Sampling Event Report FCX-Statcsville Operable Unit I Revision: 0 Date: July 2002 3.1 OPERATION AND MAINTENANCE (O&M) SUMMARY O&M activities were performed on a weekly basis from November 2001 through April 2002 and are summarized below. Weekly O&M reports are included in Appendix B. November 2001 • AES performed four weekly site visits for routine O&M. • Minor repairs were performed including replacing a recovery well air pressure regulator and leaky plumbing, and draining the secondary containment pond. • On 28 November 200 I, AES mobilized to the site to address a high alarm condition. The cause of the alarm was high water levels in the backwash tank and trickle filter sump due ,,, to a cracked union to a check val've. December 2001 • AES performed four weekly site visits for routine O&M. • Minor repairs were performed, including replacing a cracked check valve and leaky plumbing, changing the air compressor motor oil; and draining the secondary containment pond. January 2002 • AES performed five weekly site visits for routine O&M. • On 25 January 2002, recovery well pumps I and 3 were discovered to be pumping very little water. The pumps were pulled from the wells and disassembled to inspect for damage. AES contacted a technical representative of the pump manufacturer, Clean Environment Equipment, who stated that the pumps were in need of servicing due to the age and usage of the pumps. NOR/K:\V.W00641133\Apr2002 -2nd semi-annual rp1.doc 3-1 RFW I 33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e;,pressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I February 2002 • AES performed three weekly site visits for routine O&M. Second Semi-Annual Sampling Event Report FCX-Statesvillc Operable Unit I Revision: 0 Date: July 2002 • On 14 February 2002, the recovery well pump was removed from RW-3 and sent to the manufacturer for servicing; the manufacturer provided a temporary replacement pump. • Minor repairs were performed including replacing a faulty regulator at the recovery well 2 (RW-2). March 2002 • AES performed five weekly site visits for routine O&M. • On 12 March 2002, AES removed the pump from RW-1 and replaced it with the serviced pump originally in RW-3. The pump will be sent to the manufacturer for servicing. • Minor repairs were performed including replacing a faulty regulator at RW-1 and changing the air compressor motor oil. April 2002 • AES performed four weekly site visits for routine O&M. • On April 15, 2002, AES removed the manufacturer's temporary replacement pump from RW-3 and replaced it the serviced pump returned from the manufacturer. AES also removed the pump from RW-6 and replaced it with the manufacturer's temporary replacement pump. The pump from R W-6 was sent to the manufacturer for servicing. • Minor repairs were performed including repairing, on April 2, 2002, a ruptured air feed line coming from the compressor. • On 23 April 2002, the air compressor motor was discovered to have malfunctioned and ground faulted creating a failure in the compressor contactor in the control panel. An Ingersoll-Rand technician assisted AES in diagnosis of the problem. AES ordered a replacement motor. NOR/K:\WN0064\133\Apr2002 -2nd semi-annual ipt.doc 3-2 RFW133-2A-ALIJ This document was prepared by Weston Solutions, Inc., c~ressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I ·~ I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 3.2 SECOND SEMI-ANNUAL SAMPLING EVENT -APRIL 2002 3.2.1 Groundwater Monitoring WESTON and AES personnel mobilized to the site the week of 22 April 2002. AES personnel proceeded to purge and sample the 18 monitoring well network. Samples were collected on 23-24 April 2002. At least three well volumes were purged from each monitoring well using a submersible pump or dedicated disposable bailer. Water quality parameters (pH, specific conductance, temperature, and turbidity), water levels, and depth to bottom of the well were recorded during purging (Appendix C). Groundwater samples were collected using hailers, transferred into the appropriate containers, and preserved. Samples were labeled, tagged, and sealed with chain of custody seals and transported via FedEx to the assigned CLP laboratory (Appendix D). Organic samples were shipped to Ceimic Corporation or A4 Scientific and inorganic samples were shipped to Liberty Analytical Corp. Monitoring wells MW-9, MW-10 and MW-23 were not sampled due to the lack of water. Monitoring well MW-3 was not sampled due to damage to the riser, which obstructed and prevented access to the groundwater with a bailer. MW-I, MW-2, and MW-4 were analyzed for pesticides only. The remaining monitoring well samples were analyzed for VOCs, BNAs, pesticides, PCBs, and total metals. 3.2.1.1 Monitoring well Sample Results Groundwater samples collected from all of the monitoring wells, with the exception of MW-4, contained levels of VOCs, pesticides, BNAs, and metals that exceeded the remediation levels. The analytical results are summarized below: NOR/K:IWP'l20064\ 133\Apr2002 -2nd semi-annual rp1.doc 3-3 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e;,pressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I voes Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 I, 1-Dichloroethane (I, 1-DCA), chloroform, PCE, and TCE were detected at levels above the remediation levels in groundwater sampled from monitoring wells MW-SD, W-24, W-2S, W-27 and W-29. • 1,1-DCA was detected at S µg/L (estimated value) in W-29 and 6 µg/L (estimated value) in MW-SD. • Chloroform was detected at 0.42 µg/L (estimated value) in W-2S and I µg/L (estimated value) in W-29. • PCE was detected at concentrations ranging from 1.1 µg/L to~g/L in MW-SD, W-24, W-27, and W-29. • TCE was detected at S µg/L (estimated value) in MW-SD and 6 µg/L (estimated value) in W-29 . .,,,-----~-• Q,l:Qichloroethene ( 1,f:ocE), chloromethane, and bromodichloromethane were not . detected in~ftherri"6°nitoring wellsa15ove tne remediation·Ievels.__ ___ _ _ _ fJ o f.?,1 b? BNAs Bis (2-ethylhexyl) phthalate was detected at levels exceeding the remediation level in MW-SD, MW-6D, W-24, and W-29. • Bis (2-ethylhexyl) phthalate was detected in concentrations ranging from 7.3 µg/L t® µg/L in MW-SD, MW-6D, W-24, and W-29. Pesticides Alpha-BHC, beta-BHC, gamma-BHC (lindane), dieldrin, gamma-chlordane, alpha chlordane, and heptachlor epoxide were detected at levels exceeding the remediation levels in MW-I, MW- 2, MW-SD, MW-SS, MW-6S, MW-7, W-24, W-2S, and W-29. NOR/K:\Wl'\20064\133\Ap,-2002 -2nd =i-annual rpt.doc 3-4 RFW133-2A-ALIJ This document was prepared by Weston Solutions, Inc., c,pressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I • • • • Second Semi-Annual Sampling Event Report FCX-Statesvillc Operable Unit I Revision: 0 Date: July 2002 Alpha-BHC was detected in concentrations ranging from 0.017 (presumptive evidence) µg/L to9µg/L in MW-I, MW-2, MW-5D, MW-5S, MW-6S, and W-29. ~ Beta-BHC was detected in concentrations ranging from 0.060 µg/L toQ_jµg/L in MW-I, MW-2, MW-5D, and MW-5S. Dieldrin was detected at a concentration of0.32 (presumptive evidence) µg/L in MW-I. Gamma-BHC (lindane) was detected in concentrations ranging from 0.038 µg/L 10'3 µg/L in MW-I, MW-5D, MW-5S, MW-7, and W-29. • Heptachlor epoxide was detected in concentrations ranging from 0.045 (presumptive evidence) µg/L to 13 µg/L in MW-I, MW-2, MW-6S, MW-7, W-25, and W-29. • Gamma-chlordane and alpha chlordane were not detected in any monitoring wells. Metals Beryllium, chromium, manganese, and vanadium were detected in concentrations exceeding the remediation levels in groundwater collected from all of the monitoring wells sampled with the exception ofMW-5D and W-29. • Beryllium was detected at a concentration of 6.5 µg/L in MW-I I. • Chromium was detected in concentrations ranging from 68 (estimated value) µg/L to 170 µg/L in MW-5S, MW-I I, W-25, and W-27. • Manganese was detected in concentrations ranging from 110 (estimated value) µg/L to 3,000 µg/L in all of the monitoring well with the exception ofMW-5D and W-29. • Vanadium was detected at concentrations ranging from 110 (estimated value) µg/L to 210 (estimated value) µg/L in MW-11, W-25, and W-27. The laboratory results are summarized in Table 2; complete laboratory results can be found in Appendix E. A result of the trend analyses from April 2000 to April 2002 for wells that have consistently contained constituents of concern greater than the remediation levels indicates that levels or NORIK:\Wf'J:0064\\33\Apr2002. 2nd semi-annual rp1.doc 3-5 RFW I 33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e~ressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Semi•Annual Sampling Event Report FCX•Statesville Operable Unit I Revision: 0 Date: July 2002 concentrations of the majority of pesticides in the groundwater, notably alpha-BHC, beta-BHC, gamma-BHC (lindane), and heptachlor epoxide, tend to remain fairly stable or increase over time in monitoring wells MW-I, MW-2, MW-5S, MW-5D, and W-29 and decrease in MW-5S and MW-5D. A trend analyses from April 2000 to April 2002 indicates that the majority ofVOCs in the groundwater tend to decrease over time in monitoring wells MW-5D, MW-6D, MW-9, MW- ! I, W-24, and W-29. The trend charts can be found in Appendix F. WESTON has developed contaminant concentration contour maps for the VOCs, pesticides, BNAs, and metals exceeding the remediation levels. The contour maps illustrate the horizontal extent of groundwater contamination exceeding the remediation level for the shallow and deep portions of the aquifer below the site (see Figures 3 through 14). 3.2.1.2 QA/QC Sample Results The site-specific Sampling and Analysis Plan (SAP) requires quality assurance/quality control (QA/QC) samples to be collected as part of each groundwater sampling event. AES collected an equipment blank (EB-01), a field blank (FB-01), and a preservative blank (PB- 01) as required in the SAP. WESTON also submitted three trip blanks with the organic sample shipments. Duplicate ·samples were collected from monitoring wells MW-6D and W-24, and W- 29. Review of the duplicate analyses for monitoring well MW-6, W-24, and W-29 indicated unacceptable relative percent difference for bis (2-ethylhexyl) phthalate in MW-6 (33.52 per cent). This result has been flagged accordingly. 3.2.2 Treatment System Monitoring The treatment system monitoring performed from October 200 I through April 2002 1s summarized below. NOR/K:\WP\2006411331Ap12002 -2nd semi-annual rp1.doc 3-6 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., Cl)rcssly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I 3.2.2.1 Water Level Elevations Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 Water level elevations were recorded at each monitoring well during sampling events and weekly for each extraction well (Appendices B and C). The water level information is summarized in Table 3 and visually represented in Appendix G. In addition to water level measurements, flow meter discharge rates were recorded at each recovery well and at the system effluent. The data was used to model the groundwater elevation during operation of the system. By modeling the data, trends in changes in the groundwater elevations can be shown. During periods of pumping, the capture plume of the recovery wells should overlap the area of the plume indicating a hydraulic barrier to prevent further migration of contaminants off site. In order to determine if the contaminant plumes are being captured by the current recovery system, Weston utilized the groundwater model QuickFlow, Version 1.12. The following basic assumptions apply to this situation of simulating pumping in an unconfined aquifer: • The aquifer is unconfined. • The vadose zone has no influence on the drawdown. • Water initially pumped comes from the instantaneous release of water from elastic storage. • Eventually water comes from storage due to gravity drainage of interconnected pores and fractures. • The drawdown is negligible compared with the saturated aquifer thickness. • The specific yield is at least IO times the elastic storage. • All geological formations are horizontal and of infinite horizontal extent. • The potentiometric surface of the aquifer is horizontal and is not changing with time prior to the start of pumping. • The changes in the position of the potentiometric surface are due to the effect of the pumping wells alone. • The aquifer is homogeneous and isotropic. NORIK:IWP\20064\133\Ap,2002 -2nd semi-annual rpt.doc 3-7 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e:,prcssly for EPA. It shall not be disclosed, in whole or in part, without the express written pL'TTilission of EPA. I I I I I I I I I I I I • All flow is radial toward the well. • Groundwater flow is horizontal. • Groundwater has a constant density and viscosity. Second Semi-Annual Sampling Event Report FCX-Statesville Opernble Unit I Revision: 0 Date: July 2002 The hydrogeologic data was obtained from the Remedial Action Work Plan (OU I) prepared by Westinghouse Remediation Services, Inc. in December 1997. The potentiometric surface elevations and pumping rates were obtained during field sampling activities conducted m preparation for this Quarterly Monitoring Report. Table 4 shows all data used for the model. Figure 15 shows the model results for the pumpmg time of 29 days during the month of November. These results were calculated based on the average pumping rates from the flow meter readings taken from November 01 -November 29, 2001. Figure 16 shows the model results for the pumping time of 29 days during December (flow meter readings taken from November 30-December 28, 2001). Figure 17 shows the model results for the pumping time of 31 days during the month of January (flow meter readings December 29, 2001 -January 29, 2002). Figure I 8 shows the model results for the pumping time of 23 days during the month of February (flow meter readings January 30 -February 22, 2002). Figure 19 shows the model results for the pumping time of 33 days during the month of March (flow meter readings February 23 -March 25, 2002). Figure 20 shows the model results for the pumping time of 28 days during the month of April (flow meter readings March 26 -April 23, 2002). Figure 21 ,, show the model results based on the average flow meter data for the entire reporting period (November 200 I -April 2002) for the pumping time of 173 days. The model results indicate that I I I I I I the recovery system is capturing the greater part of the plume. However, the southeastern portion of the plumes, the area around monitoring wells W-25 and_W.=22, is not being caP.tured. This is ------, likely due to location and depths of the recovery wells. The recover)'. wells are too remote from the uncaptured p_grtion_oLthe_plume. AdditionallY., the recovery wells_ ~lso do not extend to an adeql§te depth_to.capture-the-contaminatio11__.!!:!_at exists in the deep wells. The recovery system ---~ -·---::----c---------did not capture as large of an area_of th_e contaminant plume from February to April as was ------------captured earlier in the reporting period. This is attributed to poor performance of recovery wells one, two, and three (RW-1, RW-2, RW-3). ------ NORIK:\WP\200641133\Apr2002. 2nd scmi-1111nual rpl.doc 3-8 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., c;,prcssly for EPA. It shall not be disclosed, in whole or in part, without the express written pennission of EPA. I I II I I I I I I I I I I I I I I I I 3.2.2.2 Treatment System Results Second Semi-Annual Sampling Event Report FCX-Statcsville Operable Unit I Revision: 0 Date: July 2002 The purpose of collecting and analyzing the influent and effluent samples of the pump and treat system is to ensure compliance with the City of Statesville Discharge Permit, T-43 issued on 14 April 2000 and revised on 19 April 2000 and 8 August 2000. The effluent limits and monitoring requirements of the Permit are as follows: • Less than the Maximum Contaminant Level (MCL) (or the minimum quantitation limit (QL} if the MCL is less than the QL} for volatile hydrocarbons, and • Less than I µg/1 for pesticides. Metals, BN As, and PCBs are not covered under the discharge permit; therefore, the analytical results for these analyses for the influent and effluent samples will not be discussed. No other parameters arc required to be monitored. Samples were collected from the influent and effluent sample ports of the pump and treat system directly into the appropriate containers, and preserved. Samples were then labeled, tagged, and sealed with chain of custody seals and transported via FedEx to the appropriate laboratory. The influent sample was submitted to the CLP laboratories with the groundwater samples; the effluent sample, EF-01, was submitted to Prism Laboratories, Inc. The influent sample, IN-01, was analyzed for VOCs, BNAs, pesticides, PCBs, and total metals and the effluent sample was analyzed for VOCs and pesticides. Based on laboratory analytical results, the influent sample contained the following detectable levels of VOC and pesticide constituents of concern. • I, 1-DCA was detected at a concentration of 6.1 µg/L, • 1,1-DCE was detected at a concentration of3.2 µg/L, • Chloroform was detected at a concentration of 3.1 µg/L, • PCE was detected at a concentration of 130 µg/L, and • TCE was detected at a concentration of3.9 (estimated value) µg/L. NOR/K:\WN00641133\Apr2002 -2nd =i-annual rpl.doc 3-9 RFW133-2A-ALIJ This document was prepared by Weston Solutions, Inc., C,l)ressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I D IJ I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statcsville Opt.-rable Unit I Revision: 0 Date: July 2002 Other VOCs that were detected in the influent sample include 1,1,1-trichloroethane at a concentration of 0.81 µg/L; I, l ,2-trichloro-1,2,2-trifluoroethane at a concentration of 22 µg/L, carbon tetrachloride at a concentration of 0.37 (estimated value) µg/L, cis-1,2-Dichloroethene (cis-1,2-DCE) at a concentration of 21 µg/L, and methyl ethyl ketone at a concentration of 5.0 (estimated value) µg/L. • Alpha-BHC was detected at a concentration of0.26 µg/L, • Beta-BHC was detected at a concentration of0.40 µg/L, • Dieldrin was detected at a concentration of 0.034 µg/L, • Gamma-BHC (lindane) was detected at a concentration of0.18 µg/L, and • Heptachlor Epoxide was detected at a concentration of 1.4 µg/L. Other pesticides that were detected include delta-BHC at a concentration of 0.083 µg/L and endrin ketone at a concentration of 0.16 µg/L. The laboratory analytical results for the effluent sample indicate that no pesticides were detected above the laboratory-reporting limits. Three VOCs were detected in the effluent sample. I, 1- DCA, acetone, and cis-1,2-DCE were detected at concentrations of 7.3 µg/L, 240 µg/L, and 16 µg/L, respectively. The North Carolina groundwater quality standards for 1,1 DCA, acetone, and cis-1,2-DCE are 700 µg/L, 700 µg/L, and 70 µg/L, respectively. Consequently, the effluent from the pump and treat system meets the discharge criteria set forth in Discharge Permit T-43. The laboratory results are summarized in Table 5; complete laboratory reports can be found in Appendix E. 3.2.2.3 POTW Discharge After treatment, water is discharged to the City of Statesville sewer system under the conditions of City Discharge Permit, T-43. The permit was issued pursuant to the requirements of the City of Statesville Sewer Use Code. Permit conditions require that the discharge not exceed I 00 gpm. The effluent limits for pesticides and volatile hydrocarbons are required to be less than I NOR/K:I WN:00641133\Apr2002. 2nd se,ni-annual rpt.doc 3-10 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., e:,pressly for EPA. It shall nol he disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I I I I I I I I I I Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 microgram/liter (<l µg/1) and less than maximum contaminant level (MCL) (or the detection limit if none exists), respectively. The MCL is equivalent to the North Carolina Groundwater Quality Standards. Results are required to be submitted to the City of Statesville, Director of Water Resources Department within 30 days of the sampling event for each quarter of the year. AES recorded the discharge flow meters for each extraction well and the effluent meter on the treatment system. The flow meter readings and calculations can be found in Tables 6 and 7. Based on the effluent meter during the period of June 200 I through October 200 I; the total quantity of water the remediation system treated and discharged to the city sewer totaled 369,115.9 cubic feet or 2,760,986.93 gallons. Based on the laboratory analytical results for EFF-09260 I, the treatment system discharge was within the specified limits of the monitored effluent parameters. No analytes were detected above the discharge limits. NOR/K:\WP\200M\133\AP"2002 -2nd semi-annual rp(.doc 3-11 RFWl33-2A-ALIJ This document was prepared by Weston Solutions, Inc., Cl)TCSsly for EPA. II shall not be disclosed, in whole or in part, without the express written pennission of EPA. I I I I I I I I I I I I I I I I I I I SECTION 4 Second Semi-Annual Sampling Event Report FCX-Statcsville Operable Unit I Revision: 0 Date: July 2002 CONCLUSIONS AND RECOMMENDATIONS According to the laboratory results for FCX -OU I L TRA, a contaminant plume with VOC, BNA, pesticide, and metals concentrations greater than the remediation levels exists beneath the site and extends downgradient to the southeast towards monitoring well W-29. Review of the influent sample analytical results indicates that the mass of contaminants is being reduced through extraction by the pump and treat system. The operation of the treatment system's recovery wells contributes to an effective hydraulic barrier to inhibit the migration of the contaminant plume in the saprolite. The model results indicate that the recovery system is capturing the greater part of the plume. The recovery system did not capture as large an area of the contaminant plume from February to April as was captured earlier in the reporting period. This is attributed to poor performance of recovery wells one, two, and three, (R W-1, R W-2, RW-3), which have since been serviced by the manufacturer. Review of the effluent results indicates that the remediation system is effectively treating the groundwater prior to being discharged to the city sewer. Based upon the findings of the April 2002 sampling event, WESTON recommends continuing O&M and monitoring activities at FCX. NOR/K:\Wf'\20064\133\Apr2002 -2nd semi-annual rpt.doc 4-1 RFW 133-2A-ALIJ This document was prepared by Weston Solutions, Inc., Cl)ressly for EPA. It shall not be disclosed, in whole or in part. without the express written permission of EPA. I I I I I I I I I I I I I I I I I SECTION 5 REFERENCES Second Semi-Annual Sampling Event Report FCX-Statesville Operable Unit I Revision: 0 Date: July 2002 Freeze, R. Allen and Cherry, John A. Groundwater. Englewood Cliffs, NJ: Prentice Hall, Inc., 1979 Roy F. Weston, Inc.: Remedial Action Report, FCX Statesville Operable Unit One, Groundwater Remediation, Statesville, North Carolina. Norcross, Georgia: McKeen, 1999 U.S. EPA: Declaration for the Record of Decision. Atlanta, Georgia: 1993. U.S. EPA: Statement of Work for Long-Term Response Action. Atlanta, Georgia: January 2001. NOR/K:IWP\200641!33\Apr2002 -2nd semi-annual <pl.doc 5-1 RFWl33-2A-ALIJ This document was prepared by Wcslon Solutions, Inc., e:,pressly for EPA. It shall not be disclosed, in whole or in part, without the express written permission of EPA. I I I I I I I I I I FIGURES I 1~ I I I I I I I NOR/K:\WP\20064\t33\Apr2002-2nd semi-annual rpt.doc I I I I I I I I I I I I I I I I I I I FIGURE l SITE LOCATION MAP LONG TERM RESPONSE ACTION FCX -OUl STATESVILLE, NORTH CAROLINA I I I I I I I I I I I I I i I I I I Deep Wells Depth to Bottom Well (ft. BTOC} MW-5O 124 MW-6O 150 MW-11 77 W-29 98 Shallow Wells Depth to Bottom Well (ft. BTOC} MW-1 47 MW-2 51 MW-3 50 MW-4 54 MW-5S 39 MW-6S 54 MW-7 52 MW-8 57 MW-9 45 MW-10 47 W-23 23 W-24 20 W-25 24 W-27 40 BTOC = Below Top of Casing LEGEND A RW-1 Recovery Well ~-MW-1 Monitoring Well ~ W-23 Monitoring Well □ D Scale (feet) 0 100 200 0 W-23 FCX • OU1 0 MW-11 0 W-24 W-29 0 BURLINGTON INDUSTRIES ------/ STATESVILLE, !REDELL COUNTY, NORTH CAROLINA SITE MAP FIGURE 2 0 W-25 DKS DAJ'E DES. ENG. i 06/20/02 OATE Al'PllCMD ' I DAJE W.O.NO. 20064-133-100 DWG. NO. 0001.CDR I Shallow Wells I De12th to Bottom Well (ft. BTOC) I MW-1 47 MW-2 51 MW-3 50 I MW-4 54 MW-5S 39 I MW-6S 54 MW-7 52 I MW-8 57 MW-9 45 I MW-10 47 W-23 23 W-24 20 I W-25 24 W-27 40 I I I I I ; I LEGEND .A. RW-1 Recovery Well I 0-MW-1 Monitoring Well (OU1) · 912.65 Water Elevation (ft above msl) · W-23 Monitoring Well (OU3) I -0 916.60 Water Elevation (ft above msl) •. 924.0··· Water Elevation lsocontour I --+ Groundwater Flow Direction NA Not Applicable (Deep wells) I Scale (feet) □ D --~c::: ~-------, 0 100 200 Notes: (1) Water levels measured April 23, 2002. V D (2) NA= Not Applicable (Deep Wells) (3) Groundwater fiow patterns are inconsistent due to effects of pumping. MW-11 00 NA W-24 911.37 BURLINGTON INDUSTRIES --------1 I FCX-OU1 STATESVILLE, !REDELL COUNTY, NORTH CAROLINA SHALLOW AQUIFER POTENTIOMETRIC SURFACE MAP DRA'M< FIGURE 3 0 W-25 911.91 DKS D DATE DES. ENG. 06/20/02 DATE APl'RO>'EO DATE W.0.NO. 20064-133-100 fNIG.NO. 0002.CDR I I I I I I I I I I I I I I Shallow Wells Deep Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 ns nd A RW-1 0 MW-1 · 0.01 Degth to Bottom Degth to Bottom (ft. BTOC) Well (ft. BTOC) 47 MW-5D 124 51 MW-6D 150 50 MW-11 77 54 W-29 98 39 BTOC = Below Top of Casing 54 52 57 45 47 23 20 24 40 Scale (feet) C: ]~~~] 0 100 200 LEGEND Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Alpha-BHC Contaminant Concentration (ug/L) ~ W-23 Monitoring Well (OU3) I · 0.01 Alpha-BHC Contaminant Concentration (ug/L) N Presumptive Evidence of presence of material I t;;BJ.~lf;, ~b~~=dR:~:~'.a~io~'~:~r~~-~fn~;~inant (Shallow) D □ D / M 0 ~~ BURLINGTON INDUSTRIES nd ~ ~,., ri FCX M~SS MW'W ~7 d I nd D '--L.l.--~ CITY STORM SEWER ns FCX -OU1 STATESVILLE, !REDELL COUNTY, NORTH CAROLINA ALPHA-BHC CONCENTRATION MAP ---------7 f DRAWN 0 W-25 nd DATE DES. ENG. DATE W. O. NO. Inferred Extent of Alpha-BHC Contaminant (Deep) DKS i 06/25/02 20064-133-IOO IL ______ A_b_o_v_e_R_e_m_e_d_ia-tio_n_G_o_a1_o_f_o_.0_1_u_g_1L ______ _,_ _____ _,_ ____________ F_I_G_U_R_E_4 ____________ ...J_= ______ ...J_DATE ___ .1.Al'PflCNE ___ o ____ LoAJE ___ _,_DWG_::.:·NO:=.=c:._-1 0010.CDR I .--------.-------,----------.~----------------, I I I I I I I I I I I I I I I I I Shallow Wells Deep Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 ns nd ,A. RW-1 0-MW-1 · 0.01 ~-W-23 · 0.01 Degth to Bottom Degth to Bottom (ft. BTOC) Well (ft. BTOC) 47 MW-5D 124 51 MW-6D 150 50 MW-11 77 54 W-29 98 39 BTOC = Below Top of Casing 54 52 57 45 47 23 20 24 40 0 Scale (feet) 100 LEGEND 200 Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well {OU1) Beta-BHC Contaminant Concentration {ug/L) Monitoring Well {OU3) Beta-BHC Contaminant Concentration {ug/L) Inferred Extent of Beta-BHC Contaminant {Shallow) Above Remediation Goal of 0.01 ug/L D □ D BURLINGTON INDUSTRIES MW-8 ' _/ ~ ld FCX ~' ;- Rw10... D ~ yRWS :CM"',;d61] W-27 -j/J • R~9 0 / V ./ R~6RW7• RW8 / "11! V "'~<> ~-//ff •t? I/ 0 W-23 ns 0/) 0 V ~ ~J-!-+---~~CITY STORM SEWER o(;j FCX -OU1 MW-11 W-29 nd 0 STATESVILLE, !REDELL COUNTY, NORTH CAROLINA BETA-BHC CONCENTRATION MAP --------------1 I ORAv.!< 0 W-25 nd OAJ'E DES. ENG. DATE W. 0. NO. Inferred Extent of Beta-BHCContaminant {Deep) DKS ; 06/25/02 20064-I33-IOO II Above Remediation Goal of 0.01 ug/L FIGURE 5 O£O<ID DATE APPRCMD AJE CING. NO. II ~-----------------------~-----~----------------------------'--------'-'-----'-------'-----'---'-OOCCIC-'L-=-CD::..CR"---' I I I I I I I I I I Shallow Wells Deep Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 ns nd .A. RW-1 -0-MW-1 0.01 -0 W-23 · 0.01 J Degth to Bottom Degth to Bottom (ft. BTOC) Well (ft. BTOC) 47 MW-5D 124 51 MW-6D 150 50 MW-11 77 54 W-29 98 39 BTOC = Below Top of Casing 54 52 57 45 47 23 20 24 40 0 . Scale (feet) 100 LEGEND 200 Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Gamma-BHC Contaminant Concentration (ug/L) Monitoring Well (OU3) Gamma-BHC Contaminant Concentration (ug/L) Estimated Value Inferred Extent of Gamma-BHC Contaminant (Shallow) Above Remediation Goal of 0.027 ug/L D □ D ~----1+---1-----,,--'-r--TREATMENT SYSTEM 0 ~-1-1----CITY STORM SEWER ns FCX -OU1 STATESVILLE, !REDELL COUNTY, NORTH CAROLINA GAMMA-BHC CONCENTRATION MAP ORA"" CATE DES. ENG. DATI: W. O. NO. Inferred Extent of Gamma-BHC Contaminant (Deep) DKS 06/27/02 20064-133-100 II Above Remediation Goal of 0.027 ug/L FIGURE 6 OEaaD MJE APPRCMo ONG. NO. IJ ~-----------------------~-----~---------------------------~-------'-----'-------'-----.._-'-00:..:.1.::.2·.::.CD::.cR:.:.......J 1.-----.---------.-----~-------------- / 0~--~ I MWnd-4 . ¾~-BURLINGTON t 1/ ~, INDUSTRIES . . ~, I -' Shallow Wells Deep Wells Degth to Bottom Degth to Bottom Well (ft. BTOC) Well (fl. BTOC) MW-1 47 MW-5D 124 I I I I I I I I I I MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 ns nd • RW-1 I 0 MW-1 · 0.01 I I 0 W-23 · 0.01 N 51 MW-6D 150 50 MW-11 77 54 W-29 98 39 BTOC = Below Top of Casing 54 52 57 45 47 23 20 □ 24 40 D Scale (feet) c-~~~, 0 100 200 LEGEND Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Heptachlor Epoxide Contaminant Concentration (ug/L) Monitoring Well (OU3) Heptachlor Epoxide Contaminant Concentration (ug/L) Presumptive evidence of presence of materia_l Inferred Extent of Heptachlor Epoxide Contaminant (Shallow) Above Remediation Goal of 0.038 ug/L FCX D Cl [)~a,,.,- '-...__"' , RW1.. 1 W-1 ;.-· · . -·-..... ·"'~ -RW , /) M~s 0 \ 0 . -: ·04; .:-.. ~-:~:,~ \ loss ~ W-27 ~~ ~.t~ ·,c. · · · ... · 0 · I /'"\0 ~~-~~ 4,-· Rfa5~~r~ Rwi• Rt~ >~-"'{9M -d-c;P ,F V "ii'" _---.-RW6 . -·. · jf W ""~"b..,<t~---,• _---..__-,c : -'"~ ~ -,-~-~ ~~~ ~-ml Q '\ ;-;~;f' _/"~//'U ~ J \~\'•?;t/_x:-,.,, .. ~~ .rJ4 \~i{f.!i_:\, ... · , ( ;" . T TREATMENT SYSTEM -c-~1-7'~cc;:1"-CITY STORM SEWER -~::~I~~-: ns W-23 {) ......... C:J FCX -OU1 STATESVILLE, IREDELL COUNTY, NORTH CAROLINA HEPATCHLOR EPOXIDE CONCENTRATION MAP OAA'M-1 DATE DES. ENG. DATE W. O. NO. Inferred Extent of Heptachlor Epoxide Contaminant (Deep) DKS 06127/02 20064-133-100 l!!I Above Remediation Goal of 0.038 ug/L FIGURE 7 CHECl<ID DA1E APPRCMO ONG. NO. IJ ._ __________________________ _._ ____ _._ ____________________________ _._ ______ ___Jc__ ___ L--. ______ _,_ ___ _,__.::.:00:.:1.::.:3.::::C::::D.::.:R__J I I I I I I I I I I I I I I I I I Shallow Wells Deep Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 ns nd A RW-1 0 MW-1 0.01 0 W-23 · 0.01 J Der1th to Bottom Der1th to Bottom /ft. BTOC} Well /ft. BTOC} 47 MW-5D 124 51 MW-6D 150 50 MW-11 77 54 W-29 98 39 BTOC = Below Top of Casing 54 52 57 45 47 23 20 24 40 0 Scale (feet) 100 LEGEND 200 Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) 1, 1-Dichloroethane Contaminant Concentration (ug/L) Monitoring Well (OU3) 1, 1-Dichloroethane Contaminant Concentration (ug/L) Estimated Value Inferred Extent of 1, 1-Dichloroethane Contaminant (Shallow) Above Remediation Goal of 1 ug/L D □ D ns R~S 4 RW74 RW6 () MW-11 ------1 I FCX -OU1 STATESVILLE, IREDELL COUNTY, NORTH CAROLINA 1,1-DICHLOROETHANE (1,1-DCA) CONCENTRATION MAP OAAY,N 0 W-25 nd DATE DES. ENG. DATE W. 0. NO. Inferred Extent of 1,1-Dichlorethane Contaminant (Deep) DKS 06/28/02 20064-133-IOO I Above Remediation Goal of 1 ug/L FIGURE 8 O<ECl<ID <WE APPRCMO ATE DWG. NO. L----------------------,-------'------'------------------------------'---------'L----L--------'-----'---"OO:.:l_:.c4·..::C=.D:..cR__, 1.-----~---~---~---------------, / M • < """Gm, T I I I I I I I I I I I I I I I Shallow Wells Deep Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 ns nd A RW-1 -0 MW-1 · 0.01 0 W-23 · 0.01 J Der;1th to Bottom Der;1th to Bottom (ft. BTOC) Well (ft. BTOC) 47 MW-5D 124 51 MW-6D 150 50 MW-11 77 54 W-29 98 39 BTOC = Below Top of Casing 54 52 57 45 47 23 20 24 40 0 Scale (feet) 100 LEGEND Well was dry, not sampled 200 Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Chloroform Contaminant Concentration (ug/L) Monitoring Well (OU3) Chloroform Contaminant Concentration (ug/L) Estimated Value Inferred Extent of Chloroform Contaminant (Shallow) Above Remediation Goal of 0.19 ug/L D □ D ns INDUSTRIES £ 0 W-23 ns FCX -OU1 () STATESVILLE, IREDELL COUNTY, NORTH CAROLINA CHLOROFORM CONCENTRATION MAP DRA..,. ---- • ·: 042J ;·"' '~-~-jr-~;;;,, DAYE DES. ENG. DAJE W. 0. NO. Inferred Extent of Chloroform Contaminant (Deep) DKS : 06/28/02 20064-133-IOO ■ Above Remediation Goal of 0.19 ug/L FIGURE 9 CHEC1<ID DATE APPRCMO AJc DWG. NO. i) ~-------------------------~---~-----------------------------'--------L'-----'--------L----L--'-'00:.:.1:..:5 . .::CD.::R:.:.__, 1~-----~--------r---------~..,,....,,.-----------------------------, Shallow Wells Deep Wells ~ I Depth to Bottom Depth to Bottom BURLINGTON ! Well (ft. BTOC) Well (ft. BTOC) INDUSTRIES 1J MW-5D 124 ~ II MW-6D 150 ~-8 ~~ MW-1 47 I I I I I I I i I I MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24_ W-25 W-27 ns nd A RW-1 0 MW-1 · 0.01 0 W-23 · 0.01 51 50 MW-11 77 FCX r 54 39 54 52 57 45 47 23 20 - 24 40 0 -- Scale (feet) 100 LEGEND W-29 98 BTOC = Below Top of Casing 200 Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Tetrachloroethene Contaminant Concentration (ug/L) Monitoring Well (OU3) Tetrachloroethene Contaminant Concentration (ug/L) MW-9 ns D .. --□--. ---RW7A I,,. RWG-- D ~--i'-+-----CITY STORM SEWER 0 W-25 ~ ~ nd ~ C::J ---------/ f FCX -OU1 STATESVILLE, IREDELL COUNTY, NORTH CAROLINA -----_, __ _ I :'~:i°f,I;:;, Inferred Extent of Tetrachloroethene Contaminant (Shallow) ·----Above Remediation Goal of 0. 7 ug/L DA1E DES. ENG. DAJE W. 0. NO. TERTACHLOROETHENE (PCE) CONCENTRATION MAP WN Inferred Extent of Tetrachloroethene Contaminant (Deep) DKS 06/28/02 20064-133-100 ml L ______ A_b_o_v_e_R_e_m_e_d_ia_t_io_n_G_o_a_1_o_f_0._7_u_g_1L _________ .,__ ___ ~ _____________ F_IG_U_R_E_1_0 ____________ _._= ______ --''--CWE------'-APPRCM---o-----'-------'-DWG---NO--__ _, 1J 0016.CDR 1.-----------r--------.------~----------------, I I I I I I m I I I I I I il I I Sha!!ow V'/ells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 De1,1th to Bottom (ft. BTOC) 47 51 50 54 39 54 52 57 45 47 23 20 24 40 Scale (feet) Deep Wells De1,1th to Bottom Well (ft. BTOC) MW-5D 124 MW-6D 150 MW-11 77 W-29 98 BTOC = Below Top of Casing ~ 0 100 200 □ D f----------------------------, ns nd • RW-1 0 MW-1 · 0.01 ~ W-23 O.D1 J LEGEND Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Trichloroethene Contaminant Concentration (ug/L) Monitoring Well (OU3) Trichloroethene Contaminant Concentration (ug/L) Estimated Value Inferred Extent of Trichloroethene Contaminant (Shallow) Above Remediation Goal of 2.8 ug/L D MW-8 d FCX BURLINGTON INDUSTRIES ~ I ~-~ I MW-9 ---.,___J ns ', ns FCX -OU1 RW7A ,t,. RW6 ,t,. RW8 oo◊ oC) MW-11 -------1 f STATESVILLE, I REDELL COUNTY, NORTH CAROLINA TRICHLOROETHENE (TCE) CONCENTRATION MAP 0 W-25 nd DATE DES. ENG. OAJE W. 0. NO. Inferred Extent of Trichloroethene Contaminant (Deep) DKS 06/28/02 20064-133-J00 I Above Remediation Goal of 2.8 ug/L FIGURE 11 CHECl<Rl CWE APPRo,ED ATE r:mG. NO. ~----------------------,-------'------'-----------------------------'--------'----..__ _____ __J ___ __Jc___0:.:0..:_!7c:..C=.:D:..:R..:___J I I I I I I I I I I I Shallow Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 Degth to Bottom (ft. BTOC) 47 51 50 54 39 54 52 57 45 47 23 20 24 40 Scale (feet) Deep Wells Degth to Bottom Well (ft. BTOC) MW-5D 124 MW-6D 150 MW-11 77 W-29 98 BTOC = Below Top of Casing □ D 11--_____ 0 ____ 1_0_0 ___ 2_0_0 _________ -, I I I I ns nd .... RW-1 ~-MW-1 0.01 0-W-23 · 0.01 J LEGEND Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Chromium Contaminant Concentration (ug/L) Monitoring Well (OU3) Chromium Contaminant Concentration (ug/L) Estimated Value I :J;f.},ir~:• ~b~~=~;~:~:a~~o~h~~~/~7 5~o~~~tinant (Shallow) D 0 W-23 ns FCX -OU1 W-24 nd STATESVILLE, IREDELL COUNTY, NORTH CAROLINA CHROMIUM CONCENTRATION MAP BURLINGTON INDUSTRIES I '-----1+-1--+,.,_TREATMENTSYSTEM 0 ------------1 f WN DATE DES. ENG. DATE W. O. NO. Inferred Extent of Chromium Contaminant (Deep) DKS 06/28/02 20064-133-100 I L ______ A_b_o_ve_R_e_m_e_d_ia_u_o_n_G_o_a_1 _of_5_o_ug_1_L ___ ~-----'-------'--------------F-IG_u_R_E_1_2 ____________ __,_= ______ _____,_= ___ __,_Al'PllCMD ______ _,_DATE ____ ._DWG __ • NO:._ • ..,;_:.___J 0018.CDR I I I I I I I I I I I I Shallow Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 De12th to Bottom (ft. BTOC) 47 51 50 54 39 54 52 57 45 47 23 20 24 40 Scale (feet) Deep Wells De12th to Bottom Well (ft. BTOC) MW-5D 124 MW-6D 150 MW-11 77 W-29 98 BTOC = Below Top of Casing D □ D 0 M -4 ns BURLINGTON INDUSTRIES I I I I I I I I I I I I I I I I "-"-'+!"¥"'-'-,""-c-l-: TREATMENT SYSTEM I I J]~f "y STORM s,w,R I 11--_____ 0 ____ 1_0_0 ___ 2_0_0 _______ ~ I I I I ns nd ... RW-1 0· MW-1 · 0.01 0 W-23 . O.D1 J LEGEND Well was dry. not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Manganese Contaminant Concentration (ug/L) Monitoring Well (OU3) Manganese Contaminant Concentration (ug/L) Estimated Value Inferred Extent of Manganese Contaminant (Shallow) Above Remediation Goal of 50 ug/L FCX -OU1 W-29 nd 0 STATESVILLE, !REDELL COUNTY, NORTH CAROLINA MANGANESE CONCENTRATION MAP --------1 I C»AWN OAJE DES. ENG. DATE W. 0. NO. Inferred Extent of Manganese Contaminant (Deep) DKS 06/28102 20064-133-IOO I Above Remediation Goal of 50 ug/L FIGURE 13 CHECl<H) MTE Al'l'RO>'ED DATE CING. NO. L._ ______________________ ....;__ ___ ...,_ ______ ,__ ______________________________ .,__ ______ _Jl-___ ..L ______ _J ____ _i__.:.00::..:1.:.9:.::.C:::D:.:.R:_...J I~------~-----------------~ I I I I I I I I I I I I I I I I I I Shallow Wells Deep Wells Well MW-1 MW-2 MW-3 MW-4 MW-5S MW-6S MW-7 MW-8 MW-9 MW-10 W-23 W-24 W-25 W-27 ns nd A RW-1 ~ MW-1 0.01 ~ W-23 0.01 J Degth to Bottom Degth to Bottom /ft. BTOC) Well /ft. BTOC) 47 MW-5D 124 51 MW-6D 150 50 MW-11 77 54 W-29 98 39 BTOC = Below Top of Casing 54 52 57 45 47 23 20 24 40 0 Scale (feet) 100 LEGEND 200 Well was dry, not sampled Contaminant not detected above the remediation goal Recovery Well Monitoring Well (OU1) Vanadium Contaminant Concentration (ug/L) Monitoring Well (OU3) Vanadium Contaminant Concentration (ug/L) Estimated Value Inferred Extent of Vanadium Contaminant (Shallow) Above Remediation Goal of 98 ug/L Inferred Extent of Vanadium Contaminant (Deep) Above Remediation Goal of 98 ug/L D □ D ~-1 0Cfi ,---...... . BURLINGTON INDUSTRIES : .. ,:,. · ~-. 0M~ .a. j ns Jt;0W-27,;••,..•~~ W4R~5 RW7A ~.\s :\'."·~~~ ~ ~-. ,.-._;,:.:.:,-. ;~◊~ ~ 0 W-23 ns FCX -OU1 w n W-29 nd 0 STATESVILLE, IREDELL COUNTY, NORTH CAROLINA VANADIUM CONCENTRATION MAP FIGURE 14 D '-+----CITY STORM SEWER cs ------1 f DRAWN DATE DES. ENG. DKS 06/28/02 DATE APPRCMD DATE w.o.NO. 20064-133-100 r:tNG.NO. 0020.CDR l~------------c----------------------------i I I I I I I I I I I •1----- 1 I I I I .A. RW-1 ~ MW-1 ~ W-23 -----, . ... --...... -71.0 - LEGEND Recovery Well Monitoring Well (OU1) Monitoring Well (OU3) Inferred extent of total contamination in deep and shallow wells Water Level lsocontour Direction of Groundwater Flow D □ D Scale (feet) -= 0 100 200 • ~ \'-. .. -0 N 0 0 • • • • ,I' W-24 MW-11 / ------- FCX -OU1 O' ' W-25 / ,I' ~ o-,____,_____· , , , , STATESVILLE. IREDELL COUNTY, NORTH CAROLINA QuickFlow © Model Results Based on November 2001 Flow Meter Data FIGURE 15 ® ORA..,,. DAJ'E DES. ENG. OKS 06/24/02 CW'E APPllOJ'EO OAJE W.O.NO. 20064-133-100 r:mG. NO. 0003.CDR 1------------,-------------------------i I I I I I I I I I I I I I • '---------~ I I I I -"' RW-1 ·~ MW-1 ~· W-23 -... -, -71.0 - LEGEND Recovery Well Monitoring Well (OU1) Monitoring Well (OU3) Inferred extent of total contamination in deep and shallow wells Water Level lsocontour D □ D 0 o Scale (feet) 100 .c, _, .c, 0 200 \ \ \ BURLINGTON INDUSTRIES 919.0 ' ., -6S• ' ' D ' I ~ J ' • .o,, ~o~" W-24 FCX -OU1 STATESVILLE, !REDELL COUNTY, NORTH CAROLINA QuickFlow © Model Results Based on December 2001 Flow Meter Data ® ~ DATE DES. ENG. DA1E Direction of Groundwater FIGURE 16 OiECkB'.l DA1E APPRCMO DAJE ~-NO. I L _____ _.'.:F.'.'.lo~w:._ ______ _l ________________ _l _____________________________ L_ ______ ..1_ ___ _,_ ______ _,_ ___ --''--0_004_.c_o_R _ __, DKS 06/24/02 w.o.NO. 20064-133-100 1-------------,-----------------------~ I I I I I I I I I I I I I 11-----------, I I I I .A. RW-1 -0-MW-1 -0-W-23 ---... , -... ---... -71.0 - LEGEND Recovery Well Monitoring Well (OU1) Monitoring Well (OU3) Inferred extent of total contamination in deep and shallow wells Water Level lsocontour D □ D / -0 "' ~ 0 Scale (feet) -0 ..., -0 0 \ ~ 0 100 200 ' ' ' ' ' ., \ ', \, \• ' ' ' ' w-p BURLINGTON INDUSTRIES 919.0 FCX -OU1 ' ◊ ' W-25/~ STATESVILLE, !REDELL COUNTY, NORTH CAROLINA QuickFlow © Model Results Based on January 2002 Flow Meter Data ---------------- ® ClRA'Mj DATE DES. ENG. DKS 06/24/02 DATE w.o.NO. 20064-133-100 Direction of Groundwater FIGURE 17 O<EC1<1D DAlE APPRCMD CING. NO. I L _____ F'.:.'l~ow~ ______ _l__ _______________ ....1.. ___________________________ ..L_ ______ ..L_ ___ _.l_ ______ L_ ___ L_o_o_os_.c_o_R _ __, 1--------------,-----:------------------------i I I I I I I I I I I I 11------------, LEGEND I I I A RW-1 -0 MW-1 -0· W-23 ----, -............ -71.0 - Recovery Well Monitoring Well (OU1) Monitoring Well (OU3) Inferred extent of total contamination in deep and shallow wells Water Level lsocontour □ D D Scale (feet) _.MW ... .. .. - 0 ~ 0 100 200 ' ' ' ' .. W-23 -0 _, -0 0 _.._..MW-11 W-24 W-2s. BURLINGTON INDUSTRIES FCX -OU1 , , , ' 0 ' O' ' ' ' , STATESVILLE, IREDELL COUNTY, NORTH CAROLINA QuickFlow © Model Results Based on February 2002 Flow Meter Data I ® ORA\\N DATE DES. ENG. Ol'JE DKS 06/24/02 Direction of Groundwater FIGURE 18 CHEO<EO Ol'JE Al'l'llO,EO Ale ONG. NO. I L _____ ~Fl~o~w~ ______ L _____ _:_ _________ L __________________________ _J ______ -1 ___ -1 ______ --'------'--0_0_06_.c_o_R _ __, W.O. NO. 20064-133-100 I lffi I j I I I I I I m I I I I I E .... RW-1 I ~MW-1 ~-W-23 I .. ---, ' .. -....... I -71.0 - I □ D LEGEND Recovery Well Monitoring Well (OU1) Monitoring Well (OU3) Inferred extent of total contamination in deep and shallow wells Water Level lsocontour 0 Direction of Groundwater Flow / D Scale (feet) '100 i8 !" 0 • ' --+----a---t---a,\ ' 200 W-23 BURt!NG~T~O~N~-,--------ll_f----------lNDUST:ES ><-~~ ' ' ' ~ W-24 W-2~ ' ' ' ·;-~ FCX -OU1 , , -- , D' ~ W-25 ' ' STATESVILLE, !REDELL COUNTY, NORTH CAROLINA QuickFlow © Model Results Based on March 2002 Flow Meter Data FIGURE 19 OOAv.,< DKS CHEa<ED ® OAJE DES. ENG. 06124/02 DA1E APPRO'IEO DATE DATE W.O.NO. 20064-133-100 ONG.NO. 0007.CDR I lW I i I I I I I I I I I I I I I ,A. RW-1 I ·~ MW-1 ~ W-23 I .. ---... , -............ I -71.0 - I LEGEND Recovery Well Monitoring Well (OU1) Monitoring Well (OU3) Inferred extent of total contamination in deep and shallow weUs Water Level lsocontour Direction of Groundwater Flow □ D 0 V D Scale (feet) 100 • -~-1-c-••-+--~\--\-°"'1 -0 "' 0 200 • • • -0 _, -0 . . ,o • ' ' BURLINGTON INDUSTRIES~------7 '1 I ' ' 0 () MW-11 ~~ W-24 • FCX -OU1 I I STATESVILLE, !REDELL COUNTY, NORTH CAROLINA QuickFlow © Model Results Based on April 2002 Flow Meter Data FIGURE 20 ® DRAWN DAYE DES. ENG. DKS 06/25/02 CHECl<H) OAJE A1E W.O.NO. 20064-133-100 ONG.NO. 0008.CDR I I I I I I I I I I I I I 1--------. I I I I I A RW-1 0· MW-1 0 W-23 , -.... -... ....... -... -71.0 - LEGEND Recovery Well Monitoring Well (OU1) Monitoring Well (OU3) Inferred extent of total contamination in deep and shallow wells Water Level lsocontour Direction of Groundwater Flow D □ 0 200 . \ • -CJ . _, • -CJ ,o • • ' ' BURLINGTON INDUSTRIE,;:,Sc--- {) MW-11 ~~ W-24 FCX -OU1 -- ' ◊ ' , -- STATESVILLE, !REDELL COUNTY, NORTH CAROLINA QuickFlow © Model Results Based on Average Flow Meter Data from November 2001 to April 2002 FIGURE 21 ® OAAWN DATE DES. ENG. DKS 06/25/02 DATE APP1lO,IEI) DATE W.O.NO. 20064-133-100 OYIG.NO. 0009.CDR ··:•· I I I I I I ,, I I I I ,, ,, I I ' I I I· NOR/K:\WP\20064\133\Apr2002-2nd seml-imnual rpt.doc TABLES I I I I I I I I I I I I I I I Table I Groundwater Remediation Lelvels FCX -Statesville OUI Remediation Constituent Level (ug/L) I, 1-Dichloroethane I I, 1-Dichloroethene 7 Bromodich]oromethane 100 Chloroform 0.19 Chloromethane I Tetrachloroethene (PCE) 0.7 Trichloroethene 2.8 Bis(2-ethylhexyl) Phthalate 6 Aloha-Bl-IC 0.01 Aloha-chlordane 0.027 Beta-Bl-IC 0.01 Dieldrin 0.1 Gamma-Bl-IC (Lindanc) 0.027 Gamma-chlordane 0.027 1-leptachlor Epoxide 0.038 Bcrvllium 4 Chromium 50 Manganese 50 Vanadium 98 Notes: --No discharge limit required by pennit. Discharge Limit Inv/I.\ 700 7 10 0.19 I 0.7 2.8 -- I I I I I I I -- -- -- -- The remediation levels are defined in the Final ROD dated September 27, 1993; the discharge limits are set forth in the City of Statesville Discharge Permit No. T-43. k:lwp\20064\133\Apr2002-tbls.xls Table 1 -GW RGs -illil , .... -. Table 2 Groundwater Wells Analytical Data FCX-Statesville OUI April 2002 -- CAS Number Compound Remediation Station ID 1----~----,----=~-r---~=~..C..C-"',-'CC,----==-.--=~-,-,~~=-----r--=----i Level MW-I MW-2 MW-4 MW-SD MW-5S MW-6D MW-6D (Dup MW-6S MW-7 VOCs (ug/L) 75-34-3 I, 1-Dichloroethane 75-35-4 1,1-Dichloroethene 75-27-4 Bromodichloromethane 67-66-3 Chloroform 74-87-3 Chloromethane 127-18-4 Tetrachloroethene (PCE) 79-01-6 Trichloroethene BNAs (ug/L) 117-81-7 Bis(2-ethylhexyl) Phthalate 319-84-6 5103-71-9 3 I 9-85-7 60-57-1 58-89-9 12789-03-6 1024-57-3 7440-41-7 7440-47-3 7439-96-5 7440-62-2 Pesticides & PCBs (ug/L) Alpha-BHC Alpha-chlordane Beta-BHC Dieldrin Gamma-BHC (Lindane) Gamma-chlordane Heptachlor Epoxide lnorganics -Total (ug/L) Beryllium Chromium Manganese Vanadium (u L) I 7 100 0.19 0.7 2.8 6 0.01 0.027 0.01 0.1 0.027 0.027 0.038 4 50 50 98 0.010 U ~otowt,Nif.jl 0.010 U Wo7o6oAAII/~ 0.031 N 0.010 U 0.010 U 0.010 U 0.010 U 0.010 U 0.020 U 0.010 U 0.010 U Note: U = Compound analyzed for but not detected; value is the minimum quantitation limit. J -Estimated Value N = Presumptive evidence of presence of material. Shaded results exceed remediation level. The remediation levels are defined in the Final ROD dated September 27, 1993. k:\wp\20064\133\Apr2002-tbls.xls Table 2 · GW MW Data Page I of2 N6:f1iffi 5 J 10 U IOU IOU 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.40 J 0.50 U @"/r,!J\ore,:i l;,•$,t3(4\il§\11',i 0.010 U 0.010 U ij#o!r5/l:i§i@! ~tf J!o~:\ll/il 0.020 U 0.020 U !l~JH2)%:'l'I ll,1Pf4\IW,!(J 0.010 U 0.010 U 0.010 U 0.010 U 0.50 U 0.58 0.50 U 0.50 U 0.50 U 0.28 J 0.50 U 0.010 U 0.010 U 0.010 U 0.020 U 0.010 U 0.010 U 0.010 U 0.31 U 0.93 R 44 J 0.50 UJ 1.5 U 0.30 U ~~-0.64R ;0-0,L ltt'.40fJjlj 65 J 0.56 R 0.50 U 0.65 0.50 U 0.50 U 0.50 U 0.37 J 0.50 U 0.010 U 0.010 U 0.010 U 0.020 U 0.010 U 0.010 U 0.010 U 0.26 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 5.0 U 0:02~" "7 " 0.010 U 0.010 U 0.020 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 0.50 U 5.0 U 0.010 U 0.010 U 0.010 U 0.020 U - 111111 -.. -.. -iiijii) -liiiijJ liiiJ -4iillJ ---lliill Table 2 Groundwater Wells Analytical Data FCX-Statesville OU! April 2002 Remediation CAS Number Compound Level MW-8 MW-11 W-24 (u L) voes (ug/L) 75-34-3 U-Dichloroethane I 0.50 V 0.50 V 0.50 V 75-35-4 I, 1-Dichloroethene 7 0.50 V 0.50 V 0.50 V 75-27-4 Brornodichloromethane 100 0.50 V 0.50 V 0.50 V 67-66-3 Chloroform 0.19 0.50 V 0.50 V 0.50 V 74-87-3 Chloromethane I 0.50 V 0.50 V 0.50 V 127-18-4 T etrachloroethene (PCE) 0.7 0.50 V 0.34 J ~SH~ 79-01-6 Trichloroethene 2.8 0.50 V 0.50 V 2.3 BNAs (ug/L) 117-81-7 Bis(2-ethylhexyl) Phthalate 6 5.0 V 5.0 V Ri7t.6rJJ/l@i Pesticides & PCBs (ug/L) 3 I 9-84-6 Alpha-BHC 0.01 0.010 V 0.010 VJ 0.010 V 5103-71-9 Alpha-chlordane 0.027 0.010 V 0.010 VJ 0.010 V 319-85-7 Beta-BHC 0.01 0.010 V 0.010 VJ 0.008 J 60-57-1 Dieldrin 0.1 0.020 V 0.020 VJ 0.020 V 58-89-9 Gamma-BHC (Lindane) 0.027 0.010 V 0.010 VJ 0.010 V 12789-03-6 Gamma-chlordane 0.027 0.010 V 0.010 VJ 0.010 V 1024-57-3 Heptachlor Epoxide 0.038 0.010 V 0.010 J 0.039 V lnorganics • Total (ug/L) 7440-41-7 Beryllium 4 0.84 V 0.43 U 7440-4 7-3 Chromium 50 36 J 14 J 7439-96-5 Manganese 50 !!fl!l'lO!Jlffi 'timn:20IrSi 7440-62-2 Vanadium 98 20 J 1.5 R Note: U = Compound analyzed for but not detected; value is the minimum quantitation limit. J -Estimated Value N = Presumptive evidence of presence of material. Shaded results exceed remediation level. The remediation levels are defined in the Final ROD dated September 27, 1993. k:\wp\20064\133\Apr2002-tbls.xls Table 2 • GW MW Data Page 2 of2 Station ID W-24 (Dup W-25 W-27S W-29 0.23 J 0.50 V 0.50 V m-ns~~ 0.50 V 0.50 V 0.50 V 4 J 0.50 V 0.50 V 10 V 0.50 V 0.50 V ~lfJIIJ 0.50 V 0.50 V 0.50 V IO VJ •5:8-.J 0.30 J ~lli!Ih~ 2.7 0.50 V 0.50 V !li7 !G 11:i 5.0 V 5.0 V \illl!will 0.010 V 0.010 V 0.010 V {0!041~ 0.010 V 0.010 V 0.010 V 0.010 V 0.009 J 0.010 V 0.010 V 0.010 V 0.020 V 0.020 V 0.020 V 0.020 V 0.010 V 0.010 V 0.010 V fi0!038~J'ii 0.010 V 0.010 V 0.010 V 0.010 V Bo:o~SrNffl ij!0~76MNlli 0.010 V d1~•1U 0.42 V 3.1 V 4.2 V 0.24 V 15 J 1.6 VJ Rl30fJ~ 16 J 1.8 J 0.58 J -,lilllal - W-29 (Dup) ~s21~m 4 J 10 V -•fJl&'ll 10 V I I I I I ,, I I I I u Casing Elevation Well (ft msl) MW-I 949.5 MW-2 954.22 MW-3 954.51 MW-4 965.87 MW-5D 949.45 MW-5S 952.02 MW-6D 957.51 MW-6S 960.52 MW-7 950.69 MW-8 964.2 MW-9 959.42 MW-10 959.08 MW-II 920.5 W-23 934.23 W-24 919.62 W-25 930.01 W-27 947.48 W-29 913.18 • Measured on 23 April 2002 k: \wp\20064 \ 133\Apr2002-Jbls.xls Table 3 Water Level Data April 2002 FCX -Statesville OUI Depth to water* Depth to Bottom (ft) (ft BTOC) 39.24 47.00 44.57 51.00 39.16 50.00 44.25 54.00 35.75 124.00 37.77 39.00 44.13 150.00 48.82 54.00 38.95 52.00 42.90 57.00 41.35 45.00 47.40 47.00 7.75 20.00 20.55 23.00 8.25 99.00 18.10 24.00 33.01 40.00 2.00 98.00 Page I of I Water Table Elevation (ft msl) 910.26 909.65 915.35 921.62 913.70 914.25 913.38 911.70 911.74 921.30 918.07 911.68 912.75 913.68 911.37 911.91 914.47 911.18 I I I I I I I I I I I Cas Number 108-10-1 1634-04-4 I 08-87-2 75-09-2 104-51-8 103-65-1 91-20-3 99-87-6 135-98-8 I 00-42-5 98-06-6 127-18-4 108-88-3 I 330-20-7 156-60-5 10061-02-6 79-01-6 75-69-4 75-01-4 72-54-8 72.55.9 50-29-3 309-00-2 319-84-6 5103-71-9 3 19-85-7 57.74.9 319-86-8 60-57-1 959-98-8 33213-65-9 1031-07-8 72-20-8 7421-93-4 53494.70.5 58-89-9 12789-03-6 76-44-8 1024-57-3 72.43.5 8001-35-2 Table 5 Influent and Effluent Results FCX-Statesville OUl April 2002 Station ID Compound IN-01 EF-01 Methyl Isobutyl Ketone 5.0 U 10 U Methyl t-butyl ether (MTBE) 0.50 U 5.0 U Methylcyclohexane 0.50 UJ Methylene Chloride 0.50 U 5.0 U n-Butylbenzene 5.0 U n-Propylbenzene 5.0 U Naphthalene 5.0 U p-lsopropyltolucnc 5.0 U sec-butylbcnzcnc 5.0 U Styrene 0.50 UJ 5.0 U tcrt-Butylbenzcnc 5.0 U Tctrachloroctht-'Ilc (PCE) 130 5.0 U Toluene 0.50 UJ 5.0 U Total Xylenes 0.50 UJ 5.0 U Trans-1,2-Dichloroctht.-ne 0.50 U 5.0 U T rans-1,3-Dichloropmpcne 0.50 UJ 5.0 U T richlorocthcnc 3.9 J 5.0 U T richloro nuoromethanc 0.50 U 10 U Vinyl Chloride 0.50 U 10 U Pesticides (ug/L) 4,4'-DDD (p,p'-DDD) 0.020 U 0.1 U 4,4'-DDE (p,p'-DDE) 0.020 U 0.1 U 4,4'-DDT (p,p'-DDT) 0.020 U 0.1 U Aldrin 0.01 U 0.05 U Alpha-BHC 0.26 0.05 U Alpha-chlordane 0.010 U Bcta-BHC 0.40 0.05 U Chlordane 0.05 U Delta-BHC 0.083 0.05 U Dieldrin 0.034 0.1 U Endosulfan I (alpha) 0.01 U 0.05 U Endosulfan II (beta) 0.020 U 0.1 U Endosulfan Sulfate 0.020 U 0.1 U Endrin 0.020 U 0.1 U Endrin Aldehyde 0.020 U 0.1 U Endrin Ketone 0.16 Gamma-BHC (Lindane) 0.18 0.05 U Gamma-chlordane 0.010 U Heptachlor 0.01 U 0.05 U Heptachlor Epoxide 1.4 0.05 U Methoxychlor 0.10 UJ 0.1 U Toxaphene 1.0 U 5.0 U Discharge Effluent Limits (u!!'/U QL 200 QL 5 QL QL QL QL QL 100 QL 0.7 1000 530 70 QL 2.8 2100 0.0!5 I I I I I I I I I I I I I I I I I I I I I I Note: U = Compound analyLed for but not detected; value is the minimum quantitation limit. J = Estimated Value N = Presumptive evidence of presence of material. The discharge limits are set forth in the City of Statesville Discharge Permit No. T•43. k:\wp\20064\133\A.pr2002-tbls.;ds Table 5-IN & EF Data Page 2 of2 I I I I I 0 I I I I Cas Number 630-20-6 71-55-6 79-34-5 76-13-1 79-00-5 75-34-3 75-35-4 563-58-6 87-61-6 96-18-4 120-82-1 95-63-6 96-12-8 106-93-4 95-50-1 107-06-2 78-87-5 108-67-8 541-73-1 142-28-9 106-46-7 594-20-7 110-75-8 95-49-8 106-43-4 67-64-1 71-43-2 108-86-1 74-97-5 75-27-4 75-25-2 74-83-9 75-15-0 56-23-5 108-90-7 75-00-3 67-66-3 74-87-3 156-59-2 10061-01-5 110-82-7 124-48-1 74.95.3 75-71-8 100-41-4 87-68-3 109-59-1 98-82-8 79-20-9 591-78-6 78-93-3 Table 5 Influent and Effluent Results FCX-Slates,·ille OUl April 2002 Station ID Compound IN-01 EF-01 VOCs (ug/L) I, 1, 1,2-Tetrachloroethane 5.0 U 1, I, 1-T richloroethanc 0.81 5.0 U 1, 1,2,2-Tetrachloroethane 0.50 UJ 5.0 U 1, 1,2-T richloro-1,2,2-Tri fluoroethane 22 I, 1,2-T richlorocthane 0.50 UJ 5.0 U I, 1-Dichloroethane 6.1 7.3 I, 1-Dichloroethene 3.2 5.0 U I, 1-Dichloropropt.'Tle 5.0 U 1,2,3-T richlorobenzcne 5.0 U 1,2,3-Trichloropropane 5.0 U 1,2,4-T richlorobcnzcne 0.50 U 5.0 U 1,2,4-T rimethylbcrm.'Tle 5.0 U 1,2-Dihromo-3-chloropropane 0.50 UJ 10 U 1,2-Dihromocthane (EDB) 0.50 U 5.0 U 1,2-Dichlorobenzene 0.50 U 5.0 U 1,2-Dichlorocthane 0.50 U 5.0 U 1,2-Dichloropropane 0.50 UJ 5.0 U 1,3,5-T rimcthylht-'JlZene 5.0 U 1,3-Dichlorobenzene 0.50 U 5.0 U 1,3-Dichloropropane 5.0 U 1,4-Dichlorobenzene 0.50 U 5.0 U 2,2-Dichloropropane 5.0 U 2-Chlorocthylvinylether 10 U 2-Chlorotoluene 5.0 U 4-Chlorotoluene 5.0 U Acetone 5.0 U 240 Benzene 0.50 UJ 5.0 U Bromobenzene 5.0 U Bromochloromelhane 5.0 U Bnimodichloromethane 0.50 UJ 5.0 U Bromoform 0.50 U 5.0 U Bromomethane 0.50 U 10 U Carbon Disulfide 0.50 U 50 U Carbon T ctrachloride 0.37 J 5.0 U Chlorobenzcne 0.50 U 5.0 U Chlomethanc 0.50 U 10 U Chloroform 3.1 5.0 U Chloromethane 0.50 U 10 U cis-1,2-Dichlorocthenc 21 16 cis-1,3-Dichloropropene 0.50 UJ 5.0 U Cyclohexane 0.50 UJ Dibromochloromcthanc 0.50 U 5.0 U Dibromomethanc 5.0 U Dichloro<lifluoromethane 0.50 U 10 U Ethylbcnzenc 0.50 UJ 5.0 U Hcxachlorobutadicne 5.0 U IPE (lsopropyl Cellosolve) 5.0 U lsopropylbenzene 0.50 UJ 5.0 U Methyl Acetate 0.50 UR Methyl Butyl Ketone 5.0 U 10 U Methvl ethyl ketone {MEK) 5.0 J 10 U k:\wp\20064\133\Apr2002-tbfs.xts Table 5 -IN & EF Dala Pagelof2 Discharge Effluent Limits (ue/L) QL 200 QL QL QL 700 7 QL QL QL QL QL 0.025 0.0004 620 0.38 0.56 QL 620 QL 75 QL QL QL QL 700 I QL QL 10 0.19 QL QL 0.3 50 QL 0.19 I 70 QL QL QL QL 1400 29 QL QL QL QL QL 170 I I I I I, ff, I I. ·1 I I I Parameter Hydraulic Conductivitv (K\ Ton of Anuifer Bottom of Aquifer Reference Hvdraulic Head Porosity Well November RW-1 2.873 RW-2 0.467 RW-3 0.069 Pumping Rates RW-4 0.570 (gallons per RW-5 1.210 minute) RW-6 0.427 RW-7 1.095 RW-8 2.415 RW-9 0.379 RW-10 0.655 Pumping Time 29 ldavs\ Hydraulic Gradient Storage Table 4 Modeling Data November 2001 -April 2002 FCX -Statesville OUI Value 2.00 feet/day 925.0 feet msl 890.0 feet msl 911.91 feet(W-25) 0.2 December Januarv Februarv 1.009 0.016 0.120 4.594 5.849 0.757 0.040 0.028 0.399 0.677 0.855 0.907 1.448 1.419 1.291 0.998 1.044 1.098 1.217 1.26) 1.241 2.882 2.890 1.812 0.441 0.459 0.437 0.770 0.733 0.691 29 31 23 0.0159 ft/ft 0.001 ft3/ft3 k:lwp\200641133\Apr2002-tbls.xls Table 4 • Modeling Data Page I of I March Anril Averave 1.607 2.576 1.367 0.357 0.423 2.075 0.804 0.567 0.318 0.789 0.459 0.710 1.081 0.779 1.205 0.982 1.703 1.042 1.135 0.839 1.131 2.054 3.055 2.518 0.410 0.303 0.405 0.627 0.471 0.658 33 28 173 == Recovery Well ID Date: 31-0ct Effluent 236,270.65 RW-I 395 506,32 RW-2 68 337.00 RW-3 66.928.50 RW-4 135 026.23 RW-5 176 240.95 RW-6 165.454.48 RW-7 221422.12 RW-8 407 568.10 RW-9 73 108.21 RW-10 I 16,646.23 Effluent 236,270.65 RW-1 395 506.32 RW-2 68 337.00 RW-3 66 928.50 RW-4 135 026.23 RW-5 176 240.95 RW-6 165 454.48 RW-7 221422.12 RW-8 407 568. 10 RW-9 73,108.21 RW-10 116 646.23 Toial Influent I 826,238.14 Variance I 589 967.49 Davs Elaoscd 36 661.00 A\·era<>e Dailv Effiuent 6.44 Aver.we Dailv Jnnuenl 49.81 AveraRe Oailv CFM 0.00 RW-1 DailvCFM 0.007 RW-2 DailvCFM 0.001 RW-3 Dailv CFM 0.001 RW-4 Dailv CFM 0.003 RW-5 Dailv CFM 0.003 RW-6 DailvCFM 0.003 RW-7 Dailv CFM 0.004 RW-8 Dailv CFM 0.008 RW-9 Dailv CFM 0.001 RW-I0DailvCFM 0.002 Total Daily Influent CFM 0.035 Variance is equal to Total lnfluent minus Effluent RW · Recovery Well 8-Nov 251 841.50 400 601.42 69 145.41 67.093.32 135 892.00 178 452.55 165.526.64 223 376.83 -- 73 782.19 117,846.81 15,570.85 5 095.10 808.4 I 164.82 865.77 2 211.60 72.16 I 954.71 ? 673.98 I 200.58 13 047.13 -2 523.72 8.00 I 946.36 1.630.89 1.35 0.442 0.070 0.014 0.D7S 0.192 0.006 0.170 lITC 0.059 0.104 1.133 13-Nov 21-Nov 261 834.7S 278 398.76 403 872.45 409 078.60 69 656.10 70421.98 67 175.65 67.260.30 136 608.12 137 552.65 179 874.98 181951.20 165 576.95 167 221.15 224 646.55 226 545.90 415 223.98 419 720.00 74215.15 74.870.70 118.608.84 I 19,745.20 9 993.25 16.564.01 3271.03 5206.15 510.69 765.88 82.33 84.65 716.12 944.53 1,422.43 2 076.22 50.31 1.644.20 I 269.72 I 899.35 7 655.88 4 496.02 432.96 655.55 762,03 I 136.36 16.173.50 18.908.91 6 180.25 2 344.90 5.00 8.00 I 998.65 2,070.50 3,234.70 2363.61 1.39 1.44 0.454 0.4.52 0.071 0.066 0.01 I 0.007 0.099 0.082 0.198 0.180 0.007 0.143 0.176 0.165 1.069 0.390 0.060 0.057 0.106 0.099 2.252 1.641 RW-2 RW-2 meter spinning conscanlly on 1/25/02. Meter reading was recorded as 133,999.05. RW-0 meter spinning conscandy on 4/15/02. Meter reading was recorded as 196,724.20. System down on 5/1/02 lITC • Unable to calculate k:\wpl20()64\133\Apr2002-tt:,tui. Table 6 -metot readings cu.It Table 6 Flow Meter Readings (cubic reel) October 2001 through April 2002 FCX-Statesvllle Operable Unit I Meter Readlm11 (cubic feeO 29-Nov 3-Dec 14-Dec 20-Dec 286,498.54 294,074.78 314 378.85 323,779.60 411484.25 413 890.S0 41S 768.25 415,780.40 70946.12 71,443.89 75 977.10 82 249.55 67.308.01 67,362.15 67 420.40 67.453.65 138 156.63 138 458.90 140 060.00 140 954.62 182 940.27 183 929.65 187 376.52 189 137.86 168.090.29 168,742.15 171 065.08 172.27!.85 227 496.09 228 352.98 231 II 1.15 232,527.72 421 822.88 423 925.76 430 523.46 433 835.10 75.215.35 75,508.32 76,556.02 77.078.20 120 279.59 120,813.97 122 225.20 123 390.17 8 099.78 7 576.24 20,304.07 9.400.75 2 405.65 2 406.25 I 877.75 12.15 524.14 497.77 4,533.21 6 272.45 47.71 54.]4 58.25 33.25 603.98 302.27 I 601.10 894.62 989.07 989.38 3,446.87 1.761.34 869.14 651.86 2.322.93 I 206.77 950.19 856.89 2 758.17 I 416.57 2.102.88 2 102.88 6 597.70 3.3 I 1.64 344.65 292.97 1,047.70 522.18 534.39 534.38 1411.23 I 164.97 9 371.80 8 688.79 25,654.91 16.595.94 I 272.02 1,112.55 5 350.84 7.195.19 8.00 4.00 11.00 6.00 1,012.47 1.894.06 1,845.82 1.566.79 I 171.48 2 172.20 2,332.26 2,765.99 0.70 1.32 1.28 1.09 0.209 0.418 0.119 0.001 0.045 0.086 0.286 0.726 0.004 0.009 0.004 0.004 0.052 0.052 0.101 0.104 0.086 0.172 0.218 0.204 0.D75 0.113 0.147 0.140 0.082 0.149 0.174 0.164 0.183 0.365 0.417 0.383 0.030 0.051 0.066 0.060 0.046 0.093 0.089 0.135 0.814 I.SOS 1.620 1.921 Page I of2 1!!1!11 - 28-Dec 4-Jan 9-Jan 14-Jan ZS-Jan 29-Jan 335 757.42 346 450.68 353 832.01 360 960.25 377 349.25 383 736.98 415,804.72 415 819.80 415 823.34 415 837.85 415 858.25 415 889.00 97 894,20 109 745.50 115503.70 121 449.01 ----134 691.50 67.507.96 67.539.75 67 560.21 67,577.01 67,630.00 67 667.20 142. 162.68 143 259.89 144,028.23 144,784.70 146,483.38 147 206.92 191 225.98 193 111.75 195,108.52 195 696.50 198,545.00 199 647.20 173 817.08 175 194.80 176 121.84 177 020.35 179115.32 179 994.65 234417.18 236,109.01 237 260.42 238,386.70 240,884.30 241 879.90 438 168.72 442 026.64 ..... 447 214.00 452.836.50 455.048.12 77 749.13 78 345.IO 78.945.97 79,176.50 80,093.35 80 463.15 124 486.25 125.444.82 126,134.61 126 781.25 128,189.13 128.791.15 11 977.82 10.693.26 7,381.33 7 128.24 16,389.00 6 387.73 24.32 15.08 3.54 14.5 ! 20.40 30.75 15 644.65 11 851.30 5 758.20 5 945.31 ? 13 242.49 54.31 31.79 20.46 16.80 52.99 37.20 1.208.06 I 097.21 768.34 756.47 1.698.68 723.54 2 088.12 I 885.77 1 996.77 587.98 2,848.50 I 102.20 I 545.23 1.3 77. 72 927.04 898.51 2 094.97 879.33 I 889.46 I 691.83 I 151.41 I 126.28 2.497.60 995.60 4 333.62 3 857.92 ? 5,187.36 5 622.50 2 211.62 670.93 595.97 600.87 230.53 916.85 369.80 I 096.08 958.57 689.79 646.64 1.407.88 602.02 28,554.78 23.363. 16 11,916.42 15,410.39 17.160.37 20 194.55 16,576.96 12 669.90 4 535.09 8 282.15 771.3 7 13 806.82 8.00 6.00 5.00 5.00 11.00 4.00 1,497.23 1.782.21 1,476.27 1,425.65 1.489.91 1,596.93 3,569.35 3,893.86 2 383.28 3.082.08 1.560.03 5 048.64 1.04 1.24 1.03 0.99 1.03 J.11 0.002 0.002 0.000 0.002 0.001 0.005 1.358 1.372 0.800 0.826 lITC 0.613 0.005 0.004 0.003 0.002 0.003 0.006 0.105 0.127 0.107 0.105 0. 107 0.126 0.181 0.218 0.277 0.082 0.180 0.191 0. 134 0.159 0. !29 0.125 0.132 0.153 0.164 0.196 0.160 0.156 0.158 0.173 0.376 0.447 lITC 0.360 0.355 0.384 0.058 0.069 0.083 0.032 0.058 0,064 0.095 0.111 0.096 0.090 0.089 0. 105 2.479 2.704 1.655 1.780 1.083 1.820 1[11111 --Table 6 Flow Meter Readlng5 (cubic feet) October 2001 through April 2002 FCX-Statesvllle Operable Unll I Recovny Meter Readln s (cubic (et?ll Well ID Date: 8-Feb Effluent 398 592.75 RW-1 4)6,]]3.(l() RW-2 136 339.60 RW-3 67 829.29 RW-4 148 917.37 RW-5 202 140.41 RW-6 182 019.62 RW-7 244 187.40 RW-8 -- RW-9 81247,54 RW-10 130057.12 Effiucn1 14 855.77 RW-1 224.00 RW-2 1,648.10 RW-3 162.09 RW-4 I 710.45 RW-S 2493.21 RW-6 2 024.97 RW-7 2 307.50 RW-8 ? RW-9 784.39 RW-10 I 265.97 Total Influent 12 620.68 Variance -2 235.09 Davs Elaoscd 9.00 Avera11e Dailv Effluent I 650.64 Avera11:e Dailv Influent 1 402.30 A veraize Dai Iv CFM 1.15 RW-1 DailvCFM 0.017 RW-2 Dailv CFM 0.127 RW-3 Dailv CFM 0.013 RW-4 Dailv CFM 0.132 RW-5 Dailv CFM 0.192 RW-6 Dailv CFM 0.156 RW-7 DailvCFM 0.178 RW-8 Daily CFM UTC RW-9 Dailv CFM 0.061 RW-IODailvCFM 0.098 Total Daily lnflllcnt CFM 0.974 Variance is eqt13.l 10 Total lnflllcnt minus Effiuent R W -Recovery Well 14-Feb 407 037.00 416.240.08 137 163.53 67,933.85 149 898.73 203 518.78 183.219.32 245 532.25 463.069.75 8 I 769.25 130 834.00 8 444.25 127.08 823.93 104.56 98 ! .36 1,378.37 I 199.70 I 344.85 8,021.63 521.71 776.88 IS 280.07 6.835.82 6.00 I 407.38 2 546.68 0.98 0.015 0.095 0.012 0.114 0.160 0.139 0.156 0.371 0.060 0.090 1.211 22-Feb 1-,\f&r 419 973.00 429.933.18 416,424.4] 416 597.85 138 096.48 138.235.77 69 495.90 70 725.77 151.258.42 152 433.47 205 430.37 207 031.75 184 894.88 186.304.25 247 422.80 249 049.14 ---- 82 394.50 82 936.12 131 865.03 132 725.36 12 936.00 9960,18 184.33 173.44 932.95 139.29 I 562.05 1.229.87 1.359.69 I 175.05 1911.59 I 60!.38 I 675.56 I 409.37 I 890.55 I 626.34 ' ? 625.25 541.62 I 031.03 860.33 II 173.00 8 756.69 -1 763.00 -1 203.49 8.00 9.00 I 617.00 I 106.69 I 396.62 972.97 1.12 0.77 0.016 0.013 0.081 0.011 0.136 0.095 0.118 0.091 0.166 0.124 0.145 0.109 0.164 0.125 UTC UTC 0.054 0.042 0.089 0.066 0.970 0.676 RW-2 R W-2 meter spinning constantly on J/25102. Meter reading was recorded as 133,999.05. R W-6 meter spinning constantly on 4/15/02. Meter reading was recorded as 196,724.20. System down on 5/1102 UTC -Unable to calculate k:lwpl200641133\Apr2002-lbls.xl1 Table 6 -meter readlr,g1 cu.n. 8-Mar 12-Mar 18-Mar 439 887.00 445,298.17 460,017.04 416034.12 4!5 916.30 421352.75 138 303.14 138.333.72 139 472.27 71 927.45 72 548.40 73 566.95 153 639.35 154.270.35 !55.260.56 208 619.36 209 436.02 210 839.04 187 709.10 188 437.95 189 732.65 250 653.15 25 I 506.90 252 993.24 ···-476 118.02 ..... 83 5 !4.34 SJ 806.90 84 372.00 133 635,40 134 088.72 !34 921.52 9 953.82 5411.17 14 718.87 -563.73 -I !7.82 5.436.45 67.37 30.58 I 138.55 1,201.68 620.95 1.018.55 I 205.88 631.00 990.21 1.587.61 8 !6.66 I 403.02 I 404.85 728.85 1.294.70 I 604.01 853.75 1.486.34 ' 13 048.27 ? 578.22 292.56 565.10 9\0.o4 453.32 832.80 7 995.93 17 358.12 14 165.72 -1.957.89 11 946.95 -553.15 7.00 4.00 6.00 I 421.97 I 352.79 2453.15 1.142.28 4 339.53 2 360.95 0.99 0.94 1.70 -0.056 -0.020 0.629 0.007 0.005 0.132 0.119 0.108 0.118 0.120 0.110 0.115 0.158 0. 142 0.162 0.139 0.127 0.150 0.159 0.148 0.172 UTC 0.324 UTC 0.057 0.051 0.065 0.090 0.079 0.096 0.793 1.072 1.640 Page 2 of2 .. -.. 2s-:-..1ar 2-Anr 12-Anr 15-Anr 2J-Anr 474.570.90 488,939.50 510 756.83 512 775.56 522,247.40 426,470.00 431.250.53 438.504.35 439 145.82 442 036.27 ]40.323.27 141.140.65 142 250.18 142 375.53 142,825.75 74,548.68 n 589.35 77,157.38 77 304.40 77 962.77 156 197.75 157 044.00 158.299.78 158419.13 158 958.15 212.221.50 213.552. 10 215.742.10 215.959.80 216,906.60 191 059.28 192311.25 194 213.87 ..... 197 568.87 254 543.33 256 069.92 258.392.40 258 623.92 259,571.56 -485 863.52 491.066.53 491 562.35 493.760.27 84,963.00 85J22.87 86 347.20 86 425.59 86 783.02 135 800.95 136644.15 137 938.50 138 062.35 138,637.02 14,553.86 14 368.60 21,817.33 2 018.73 9471.84 5 117.25 4 780.53 7 253.82 641.47 2 890.45 851.00 817.38 I 109.53 125.35 450.22 981.73 I 040.67 1.568.03 147.02 658.37 937.19 846.25 1,255.78 119.35 539.02 1,382.46 1.330.60 2 190.00 217.70 946.80 1 326.63 1.251.97 !,902.62 ' 3,355.00 I 550.09 1 526.59 2 322.48 231.52 947.64 ? 9.745.50 5 203.01 495.82 2 197.92 591.00 559.87 824.33 78.39 357.43 879.43 843.20 I 294.35 123.85 574.67 13 616.78 22 742.56 24 923.95 2 180.47 12 917.52 -937.08 8.373.96 3 106.62 161.74 3 445.68 7.00 7.00 !0.00 3.00 8.00 2 079.12 2 052.66 2 181.73 672.91 I, 183.98 I 945.25 3.248.94 2.492.39 726.82 I 614.69 1.44 1.43 1.52 0.47 0.82 0.508 0.474 0.504 0. 148 0.251 0.084 0.08 I 0.077 0.029 0.039 0.097 0. !03 0.109 0.034 0.057 0.093 0.084 0.087 0.028 0.047 0.137 0.132 0.152 0.050 0.082 0.132 0. !24 0.132 UTC 0.291 0.154 0.151 0.161 0.054 0.082 UTC 0.338 0.361 0. ! 15 0.191 0.059 0.056 0.057 0.018 0.031 0.087 0.084 0.090 0.029 0.050 1.351 1.628 1.731 0.505 1.121 -Illa Recovery Well ID Date: 31-0ct Effiuent I 767 304.46 RW-1 2.958J87.27 RW-2 511 160.76 RW-3 500 625. 18 RW-4 I 009.996.20 RW•S 1318,282.31 RW-6 1,237 599.51 RW-7 1.6S6.237.46 RW-8 3 048,609.39 RW-9 546 849.41 RW-10 872 513.80 Effiuent 76 095.91 RW-1 25 093.68 RW-2 4,153.27 RW-3 I 070.01 RW-4 4 576.86 RW-5 10 852.36 RW-6 173.39 RW-7 9 328,98 RW-8 22 606.06 RW-9 3,290.38 RW-IO 5 940.84 Total Influent 87 085.83 Variance 10 989.92 Davs Elansed #REF! Averal!e Daily Effiuent #REF! Avera11e Dailv Influent #REF! Averal!e Dailv Effluent GPM #REF! RW-1 DailvGPM #REF! RW-2 Dailv GPM #REF! RW-3 Daily GPM #REF! RW-4 Dailv GPM #REF! RW-5 Dai!vGPM #REF! RW-6 DailyGPM #REF! RW-7 Dai!vGPM #REF! RW-8 Dai!v GPM #REF! RW•9 Daily GPM #REF! RW-10 DailvGPM #REF! Total Dailv Influent GPM #REF! Variance is equal 10 Total Influent minus Effluent RW -Recovery Well RW - 2 meter spinning constantly on 1/25/02. RW-6 meter spinning constantly on 4/i 5/02. System down on 5/!/02 19 8-Nov I 883 774.42 2 996.498.62 517207.67 501 858.03 1 016.472.16 J 334 825.07 I 238 139.27 1,670,858.69 551890.78 88 ! 494.14 ! !6 469.96 38 111.35 6,046.91 I 232.85 6 475.96 16 542.77 539.76 14 62!.23 5 041.37 8 980.34 97 S92.53 -18 877.43 8.00 14.558,74 12 199.07 10.11 3.3083 0.5249 0. !070 0.5621 1.4360 0.0469 1.2692 0.4376 0.7795 8.4716 k:\wp\200641133\A.pr2002-~s.xl5 Table 7 • meter n,ad!ngs g.als 13-Nov I 958 523.93 3.020.965.93 52! 027.63 502 473.86 1.021.828.74 I 345 464,85 1,238 515.59 1.680.356.19 3,!05 875.37 555 129.32 887. 194.12 74 749.51 24.467.30 3 819,96 615.83 5.356.58 10,639.78 376.32 9 497.51 57 265.98 3 238.54 5 699.98 !20.977.78 46 228.27 5.00 14 949,90 24 195.56 10.38 3.3982 0.5306 0.0855 0.7440 1.4777 0.0523 1.3191 3.0591 0.4498 0.7917 11.9079 21-Nov 2 082 422.72 3.059,907.93 526 756.41 503 107.04 1.028.893.82 J 360994.98 1250814,20 1.694.563.33 3 139 505.60 560 032.84 895.694.10 123 898.79 38.942.00 5 728.78 633.18 7 065.08 15 530.13 12.298.62 14,207.14 33 630.23 4,903.51 8 499.97 !41.438.65 17,539.85 8.00 15 487.35 17 679.83 10.76 3.3804 0.4973 0.0550 0.6!33 !.348 ! l.0676 l.2333 2.9!93 0.42S7 0. 73 78 12.2777 --Table 7 Flow Meter Reading1 (gallons) October 2001 through Aprll 2002 FCX-State1vllle Operable Unit I Meter Readlno1 toatlonsl 29-Nov 3-Dec 14-Dec 2 143 009.08 2 199 679.35 2 35 l 553.80 3.077,902.!9 3,095,900.94 3 109,946.51 530 676.98 534,400.30 568,308.71 503,463.91 503 868.88 504 304.59 l.033 411.59 1.035,672.57 !,047,648.80 I 368 393.22 I 375,793.78 I 401 576.37 I 257,3!5.37 I 262,191.28 I 279 566.80 1.701 670.75 1,708,080.29 1,728 711.40 3 155 235.14 3,170964.68 3,220.315.48 562 610.82 564 802.23 572 639.03 899.691.33 903 688.50 914,244.50 60 586.35 56.670.28 15! 874.44 17 994.26 17 998.75 14 045.57 3 920.57 3 723.32 33,908.41 356.87 404.97 435.71 4517.77 2 260.98 I 1.976.23 7 398.24 7 400.56 25 782.59 6 501. !7 4,875.9! 17.375.S2 7,107.42 6,409.54 20,63 \.11 15 729.54 15,729.54 49 350.80 2,577.98 2,191.42 7.836.80 3 997.24 3.997. 16 JO 556.00 70 101.06 64992.15 191 898.73 9 514.71 8 321.87 40.024.28 8.00 4.00 11.00 7 573.29 14 !67.57 13 806.77 8 762.63 16 248.04 !7,445.34 5.26 9.84 9.59 1.5620 3.1248 0.8867 0.3403 0.6464 2.1407 0.0310 0.0703 0.0275 0.3922 0.3925 0.7561 0.6422 1.2848 1.6277 0.5643 0.8465 1.0969 0.6170 1.1128 1.3025 1.3654 2.7308 3.1156 0.2238 0.3805 0.4947 0.3470 0.6940 0.6664 6.0852 11.2834 12.1148 Page! of2 -.. - 20-Dec 28-Dec 4-Jan 9-Jan 14-Jan 25-Jiin 2 421 871.41 2 51! 465.50 2591451.09 2 646 663.43 2 699.982.67 2,822 572.39 3 110 037.39 3 110,2!9.31 3110.332.10 3,110,358.58 3,110,467.12 3 I 10 619.7! 6!5 226.63 732,248.62 820 896.34 863,967.68 908 438.59 504 553.30 504.959.54 505 !97.33 sos 350.3 7 505 476.03 505,872.40 1,054,340.56 1,063 376.85 1.071 583.98 1.077,331.16 1,082,989.56 1,095,695.68 1,414,751.19 1.430 370.33 1,444 475.89 !,459,411.73 1,463 809.82 I 485 116.60 1 288.593.44 1300 151.76 1,310,457.10 1317,391.36 1,324 112.22 1,339,782.59 1.739,307.35 1.753,440.51 1,766,095.39 1,774,707.94 1,783,132.52 I 801 814.56 3 245 086.55 3 277 502.03 3.306 359.27 3 345 160.72 3 387 217.02 576 544.94 58].563.49 586 021.35 590.515.86 592 240.22 599 098.26 922 958.47 931 !57.15 938 327.25 943 486.88 948 323.75 958 854.69 70,317.61 89.594.09 79.985.58 55 212.3S 53319.24 122,589.72 90.88 181.91 I 12.80 26.48 108.53 152.59 46 917.93 117,021.98 88,647.72 43 071.34 44 470.92 248.7! 406.24 237.79 153.04 125.66 396.37 6.691.76 9 036.29 8207.13 5747,18 5 658.40 12706.13 13 174,82 15 619.14 14 105.56 14,935.84 4 398.09 21 306.78 9,026.64 11,558.32 10,305.35 6 934.26 6 720.85 15 670.38 10 595.94 14133.16 12,654.89 8,6!2.55 8 424.57 18 682.05 24,771.07 32.415.48 28 857.24 38 801.45 42,056.30 3,905.91 5,018.56 4 457.86 4 494.5 l I 724.36 6 858.04 8 713.98 8 198.68 7 170. !O 5 159.63 4,836.87 JO 530.94 124,137.63 213 589.75 174 756.44 89 !34.82 115 269.72 128 359.57 53,820.02 123,995.66 94,770.85 33,922.47 6! 950.48 5 769.85 6.00 8.00 6.00 5.00 5.00 11.00 11 719.60 11 199.26 !3 330.93 l l 042.47 10 663.85 11 144.52 20,689.61 26 698.72 29 126.07 !7 826.96 23 053.94 11 669.05 8.14 7.78 9.26 7.67 7.41 7.74 0.0!05 0.0!58 0.0131 0.0037 0.015 ! 0.0096 5.4303 10.1582 10.2602 5.9821 6, 1765 0.0288 0.0353 0.0275 0.0213 0,0175 0.0250 0.7745 0.7844 0.9499 0.7982 0.7859 0.8022 1.5249 1.3558 1.6326 2.0744 0.6108 1.3451 1.0447 !.0033 1.1927 0.9631 0.9335 0.9893 1.2264 l.2268 1.4647 1.1962 1.1701 1.1794 2.8670 2.8 !38 3.3400 2.6945 2.6551 0.4521 0.4356 0.5160 0.6242 0.2395 0.4330 1.0086 0,7117 0.8299 0.7166 0.6718 0.6648 !4.3678 18.5408 20.2264 12.3798 13.3151 8.1035 -- Recovery Well ID Date: 29-Jan Effluent 2,870 352.61 RW-1 3 I IO 849.72 RW-2 I 007 492.42 RW-3 506 150.66 RW-4 I 101 107.76 RW-5 I 493 361.06 RW-6 I 346 359.98 RW-7 I.809 261.65 RW-8 3 403 759.94 RW-9 601 864.36 RW-10 963.357.80 Effluent 47 780.22 RW-1 230.01 RW-2 99 053.83 RW-3 278.26 RW-4 5 412.08 RW-5 8 244.46 RW-6 6 577.39 RW-7 7 447.09 RW-8 16 542.92 RW-9 2766.10 RW-10 4 503.11 Total Influent 151 055.23 Variance 103 275.01 Davs Elai,scd 4.00 Averal'e Dailv Effluent 11 945.06 Avcrn11:e Daily Influent 37 763.8 l Avcra1>e Dailv Effluent GPM 8.30 RW-l DailvGPM 0.0399 RW-2 Dailv GPM 4.5858 RW-3 Dailv GPM 0.0483 RW-4 Dailv GPM 0.9396 RW-5 Dailv GPM 1.4313 RW-6 Dailv GPM 1.1419 RW-7 DailvGPM 1.2929 RW-8 Dailv GPM 2.8720 RW-9 Dailv GPM 0.4802 RW-10 Dailv GPM 0.7818 Total Daily Influent GPM 13.6138 Variance is equal to Total Influent minus Effluent RW -Rc:covcry Well RW - 2 meter spinning constantly on 1/25/02. RW-6 meter spinning constantly on 4/15/02. System dO"Wn on 5/1/02 iiillll 8-Feb 2 981 473.77 3 112 525.24 1.019.820.21 507 363.09 1.113,901.93 1.512.010.27 I 361 506.76 I 826 521.75 607 731.60 972 827.26 11112l.16 I 675.52 12 327.79 I 212.43 12 794.17 18 649.21 15 146.78 17,260. JO 5 867.24 9 469.46 94 402.69 -16 718.47 9.00 12 346.80 10 489.19 8.57 0.1293 0,9512 0.0936 0.9872 1.4390 1.1687 1.3318 0.4527 0.7307 7.2842 k:\wp\2006A\13Jl,&.p(2002-lbll .• ll Table 7 • meter readings gall 14-Feb 22-Feb 3 044 636.76 3 141 398.04 3 I 13 475.80 3 114 854.59 1.025.983.20 1.032.961.67 508 145.20 519829.33 1.121 242.50 1.131412.98 1.522.320.47 1.536.619.17 I 370 480.51 1.383 013.70 I 836 581.23 I 850 722.54 3.463.761.73 611 633.99 616310.86 978 638.32 986 350.42 63 162.99 96 761.28 950.56 l 378.79 6163.00 6 978.47 782.11 11684.13 7 340.57 JO 170.48 10310.21 14 298.69 8973.76 12 533.19 10 059.48 14141.31 60 001.79 3 902.39 4 676.87 5811.06 7712.10 I 14 294.92 83 574.04 51 131.93 -13,187.24 6.00 8.00 10 527.17 12 095.16 19049.15 !0,446.75 7.31 8.40 0.1 JOO 0.1197 0.7133 0.6058 0.0905 1.0142 0.8496 0.8829 I.I 933 1.24 I 2 1.0386 1.0880 1.1643 1.2275 2.7779 0.4517 0.4060 0.6726 0.6695 9.0618 7.2547 Table 7 Flow Meter Re11dlngs (gallons) October 2001 lhrough April 2002 FCX-Sta1e1vllle Operable Unit I NIii - Meter Readin•s r~allons1 1-Mar 8-Mar 12-Mar 18-Mar 25-Mar 3215900.19 3 290 354.76 3 330 830.3 I 3 440 927.46 3 549,790.33 3 116151.92 3.11 I 935.22 3 111,053.92 J 151.71U7 3 189,995.60 1.034.003.56 I 034.507.49 I 034. 736.23 I 043 252.58 I 049 618.06 529 028.76 538 017.33 542 662.03 550 280.79 557 624.13 1 140 202.36 I 149,222.34 I 153 942.22 1,161.348.99 1-168-359.17 1.548.597.49 1.560472.81 I 566 581.43 I 577,076.02 I 587 416.82 I 393 555.79 I 404 064.07 I 409 515.87 I 419 200.22 I 429 123.41 1.862 887.57 1.874 885.56 1.881.271.61 1,892,389.44 \.903,984.11 3 561 362.79 620,362.18 624 687.26 626 875.61 63 I 102.56 635 523.24 992,78H9 999.592.79 1.002.983.63 l-009.212.97 l.015.791.l I 74 502. IS 74 454.57 40,475.55 110.097.15 108 862.87 l.297.33 -4216.70 -881.29 40,664.65 38,277.03 I 041.89 503.93 228.74 8 516.35 6 365.48 9 199.43 8 988.57 4 644.71 7618,75 7 343.34 8789.37 9 019.98 4 719.88 7.406.77 7 010.18 11 978.32 11 875.32 6 108.62 10.494.59 10,340.80 10 542.09 JO 508.28 5451.80 9 684.36 9 923.19 12,165.02 11 997.99 6 386.05 11,117.82 ! I 594.67 97,601.06 4 OS 1.32 4 325.09 2 188.35 4 226.95 4 420.68 6 435.27 6 807. !0 3 390.83 6 229.34 6 578. 14 65 500.04 59 809.56 129 838.74 105,959.59 JOI 853.51 -9,002.11 -14 645.02 89 363.19 -4,137.56 -7.009.36 9.00 7.00 4.00 6.00 7.00 8 278.02 JO 636.37 10,! 18.89 18,349.52 15.551.84 7,277.78 8,544.22 32,459.68 17,659.93 14,550.50 5.75 7.39 7.03 !2.74 10.80 0.1001 -0.4183 -0.1530 4,7066 3.7973 0.0804 0.0500 0.0397 0.9857 0.6315 0.7098 0.8917 0.8064 0.8818 0.7285 0.6782 0.8948 0.8194 0.8573 0.6955 0.9243 1.1781 1.0605 l.2147 1.0259 o.s 134 1.0425 0,9465 1.1209 0.9344 0.9387 1. 1903 1.1087 1.2868 !.I 503 2.4207 0.3126 0.4291 0.3799 0.4892 0.4386 0.4965 0.6753 0.5887 0.7210 0.6526 5.0540 5.9335 8.0175 12.2638 10.1045 Page 2 of2 -- 2-Anr 12-A~r 15-Anr 23-Anr 3 657 267.46 3 820 461.09 3 835 561.!9 3 906 410.55 3 225 753.96 J.280012.54 3,284 810.73 3 306 431.30 I 055 732.06 I 064031.35 I 064 96S.96 I 068 336.61 565 408.34 577 137.20 578 236.91 583 161.52 I 174 689.12 1.184.082.35 1 184,975.09 l,!89006.96 I 597 369.71 1613 750.91 1 615 379.30 I 622,461.37 I 438 488.15 1452 719.75 1,477 815.15 1,915.403.00 193277.5.15 I 934 506.92 1,941 595.27 3 634 259.13 3 673 177.64 3 676 886.38 3,693 326.82 639,711.07 645 877.06 646 463.4 I 649 136.99 1 022,098.24 I 03 l 779.98 I 032 706.38 I 037004.91 107477.13 163 193.63 15 JOO.JO 70 849.36 35 758.36 54 258.57 4 798.20 21 620.57 6,114.00 8.299.28 937.62 3 367.65 7 784.21 11 728.86 I 099.71 4 924.61 6 329.95 9 393.23 892.74 4031.87 9 952.89 16 381.20 I 628.40 7 082.06 9 364,74 14,23 !.60 25 095.40 11 418.89 17 372.15 I 73 l.77 7 088.35 72.896.34 38.918.51 3.708.73 16 440.44 4.187.83 6 165.99 586.36 2 673.58 6,307.14 9.681.74 926.40 4 298.53 170,114.35 186431.15 16 309.92 96 623.05 62,637.22 23,237.52 1,209.82 25.773.69 7.00 10,00 J 00 8.00 15 353.88 16.319.36 5 033.37 8.856.17 24 302.05 18643.11 5 436.64 12 077.88 10.66 11.33 3.50 6.15 3.5475 3.7680 1.1107 1.8768 0.6065 0.5763 0.2170 0.2923 0.7722 0.8145 0.2546 0.4275 0.6280 0.6523 0.2067 0.3500 0.9874 1.1376 0.3769 0.6148 0.9290 0.9883 1.5843 !.1328 1.2064 0.4009 0.6153 2.53 I I 1.1261 0.1288 0.5437 0.415S 0.4282 0.1357 0.2321 0.6257 0.6723 0.2144 0.3731 12.1758 11.3700 3.0457 6.9098 . ' _.,-.• .. ·-,. ':· , .. ,, ",.~ .. '\ ~--. :· .. ~-- :;.:; . ., . ~ '-" .-! .•: _._ ... ~ ... . ,-. . -.'.•\'. ·, .. ,'t ,, .. ,:·: -·-:'!·--, ,.,' ....... _; . ' -:' .... -,: ~: ~ ~-,-. . . ;: ~. ~·' f ·, -': • j ·-... . --. .. ,·· .,.,•""::"t .. ,: .• . •t'' ·•.· ,, ' .. •. •;: .• '; :-· j . •,· ', . . , ~ ., , ' .. :. :,.•'' . ... · ... ,. ,·s 4 '>· :· -::'-.. · ' _.,,: .. ' . : ; ~:,: . '\ ~.:: . ·~.,:·:/{·~<!( :·> . .. ;. ,<-~·_ ... ,., ._ ..... ·-. ~ . " .. '~-( .:~~ :.r:. './ ,-, . . . -_ ,\.•/' I I I I I I I I I I APPENDIX A CITY DISCHARGE PERMIT I I I I I I I I I I I I I I I I I I I I I I I I I I I I Qtitu nf ~tattnuillt ll). (IJ). l!!ux 1111 • %tatesuille. Nort~ Qlarolina 28687 August 8, 2000 OOCUMENTCONTHO~-~~!iu~, BF:W.£'.!Z,~z.f:?;_4 r:r 6r 1<---·--.... ' . Mr. Joseph Ferentz Roy F. Weston, Inc. Suite 200 5405 Metric Place Norcross, GA 30092-2550 Re: Modification to Permit No. T-43 FCX-Statesville Superfund Site Dear Mr. Ferentz: We have approved your request, stated in your letter of July 13, 2000, for the modification in language on your Effluent Limits page of Permit T-43. Enclosed is a revised copy of this page for your permit. 1bis change is effective as of the date of this letter. If you have any questions, please call at (704) 878-3438. Sincerely, . (2~-£ . Carol Rogers, ~nt Coordinator Water Resources Department Enclosure I I I I I I I I I I I I I I I I I I I ,,.;_ ,;., Am ~'-IUQ;;, AG.?K · Permit No, T-43 EFFLUENT LIMITS AND MONITORING REQUIREMENTS Parameter Permit Limit **F uency Volatile *<MCL I/quarter hydrocarbons Pesticides <1.0 ug/1 Grab I/quarter *MCL -North Carolina Groundwater Quality Standards or the minimum Quantitation Limit (QL) if the MCL is less than the QL, or if none exist, delimit to the QL. **Frequency-Quarters will start in January, Aprii July and October Collection of sample and analysis is the sole responsibility of the Permittee. Results should be submitted to the Director of Water Resources Department within 30 days of the sample event. I I I I I I I I I I I I I I I I I I C!titu of DOCUMENT CONTROL NUMBER . . ·.·.· · . ..~ '\= LU0Lj1-3/j:.:':~ :§tattn uillt lll-QI)_ i!,lox 1111 • §tatrsuillr. Nori~ (!]arolina 28687 April 19, 2000 Mr. Joseph Ferentz Roy F. Weston, Inc. Suite 200 5405 Metric Place Norcross, GA 30092-2550 Re: Revision to Permit T-43 FCX-Statesville Superfimd Site Dear Mr. Ferentz: Enclosed is a revised limit page to your permit, No. T-43. These revisions include: the addition of Pesticides monitoring; the phrase describing what limit applies if a parameter is not included in the North Carolina Groundwater Quality Standards; and, a clarification of who is responsible for sampling. Please insert this page in your permit and remove the old page. If you have any questions, please call me at (704) 878-3438. Sincerely, (}aJ. lo Carol Rogers, ~reatment Coordinator Water Resources Department I I I I I I I I I I I I I I I I I I I DOCUMENT CONTROL l·iUMBfR .... ,, , Rl=kJOtf7:::;0 ":~~ £-'( Permit No. T-43 EFFLUENT LIMITS AND MONITORING REQUIREMENTS Parameter Volatile hydrocarbons Pesticides Permit Limit *<MCL <1.0 ug/1 Sam leType °Frequency Grab I/quarter Grab I/quarter *MCL-North Carolina Groundwater Quality Standards or if none exist, default to Detection Limit. **Frequency-Quarters will start in January, Apri~ July and October Collection of sample and analysis is the sole responsibility of the Permittec. Resuhs should be submitted to the Director of Water Resources Department within 30 days of the sample event. I. I I I I I I I I I I I I I I I I I I Qtitu of §tatrnuill.e jp. @. l!lox Jill • matrsuillr. Nortl) <fuirolina 28687 April 14, 2000 Mr. Joseph Ferentz Roy F. Weston, Inc. Suite 200 5405 Metric Place Norcross, GA 30092-2550 Re: Transmittal of Permit T-43 FCX-Statesville Superfund Site Dear Mr. Ferentz: In accordance with your letter requesting the renewal of a discharge pennit, we arc forwarding herewith the subject City Discharge Permit. This pennit is issued pursuant to the requirements of the City of Statesville Sewer Use Code. If any parts, measurements, frequencies or sampling requirements contained in this permit arc unacceptable to you, you may request a modification by written request to the Director identifying the specific issues to be contended. Unless such a request is made within 30 days following receipt of this permit, this permit shall be final and binding. This permit does not effect or satisfy any requirements of the City of Statesville other than the above referenced. Please sign and return a copy of the receipt page of this permit to our office. If you have any questions, please contact Carol Rogers at (704) 878-3438. Sincerely, CON)_ tr;,w A L. F. "Joe" Hudson, Jr., Director Water Resources Department I I I I I I I I I I I I I I I I I I I CITY OF STATESVILLE, NORTH CAROLINA PERMIT NO. T-43 PERMIT TO DISCHARGE WASTEWATER UNDER THE SEWER USE ORDINANCE OF THE CITY OF STATESVILLE Pursuant to the City of Statesville Sewer Use Ordinance (here-after referred to as 'The Ordinance"), other lawful standards and regulations promulgated and adopted by the City of Statesville, as amended, and pursuant to the Permit Application (here-after referred to as 'The Application'') heretofore filed with the City of Statesville, FCX-Statesville Superfund Site, (here-after rererred to as "Permittee") is hereby authorized to discharge groundwater to sanitary sewers of the City of Statesville (here-after referred to as 'The City'') in accordance with effluent limitations, monitoring requirements, and special conditions contained herein.. All such discharges shall be made at discharge locations approved in advance by the City. This permit shall become effective on April 17, 2000. This permit and the authoriz.ation to discharge shall expire at midnight April 17, 2005. Signed this the Kdayof {Jpc; I I Jm . Water Resources Department I. I I I I I I I I I I I I I I I I I I Permit No. T-43 SPEOAL CONDffiONS I. Permittee shall discharge at a rate not to exceed I 00 gallons per minute (GPM). Flow must be monitored by a City approved meter, which is accessible to the meter reader. A billing account must be established with Collections at City Hall prior to discharge. 2. The Permittee shall operate and maintain an efficient pretreatment system. 3. The discharge is subject to all requirements of the City ofStatesville's Sewer Use Ordinance. Failure to meet these requirements and those listed in this permit will subject the Permittee lo fines and possible termination of the permit. I I I I I · Description of Discharges 01 Permit No. T-43 Description Treated groundwater I I I I I I I I I I I I I I The sampling point for Pipe O I is the sampling port off pretreatment system I I I I I I I I I I I I I I I I I I I Permit No. T-43 EFFLUENT LIMITS AND MONITORING REQUIREMENTS Parameter Volatile hydrocarbons Permit Limit *<MCL *MCL-North Carolina Groundwater Quality Standards * *Frequency -Quarters will start in January, Apri~ July and October I/quarter Results should be submitted to the Director of Water Resources Department within 30 days of the sample event. · I I I I I I I I I I I I I I I I I I I ➔A"' · '-'YIJMENT CGNTHO' ,•.iw; .. ,n ,,·,., -..... ~,...,,._~\ ~tiH,J3coN"t1-f~-;~n~-;ms e:::jft~ Receipt of the foregoing Permit is acknowledged. This the Ii day of A-'{)/2. \ L 2000. Name of Pennittee By~&1~ Ad ~5 Hzrfllt ~ SIE uX) I ~Uvss 6A: Jci:xi'2. :, I ; I I I I I I I I I I APPENDIXB SYSTEM CHECK FORMS I I I I I I I I I I I I I I I I I I I I I I I I I I I I November 16, 2001 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 Re: FCX Weekly System Check Forms Dear Mr. F crcntz; a, 19 2001 Enclosed are the FCX System Check Forms for the weeks ending November 9th and November 16'\ 2001. As noted on the form dated November 13, 2001, the regulator for RW-6 was replaced. If you have any questions please feel free to call 704-795-7075 at any time. s~~/- Brad Burdick 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • fox: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date: 11/8/01 Tessa Houck Was the system running upon arrival: Flow Meter Readings: Effluent 251,841.50 cit RW-1 400,601.42 cit RW-2 69,145.41 cit RW-3 67,093.32 cit RW-4 135,982.00 cit RW-5 178,452.55 cit RW-6 165,526.64 cit RW-7 223,376.83 cit RW-8 -cit RW-9 73,782.19 cit RW-10 117,846.81 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 57.05 Point 57.26 SF-1 37.41 SF-1 42.82 SF-2 50.41 SF-2 42.00 50.62 - 59.61 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 24 Effluent 22 Influent 22 Effluent 20 59.31 Any leaks observed: No ----------- I I I I I I I I I I I I I I I I I I I Date: 11/13/01 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 261,834.75 cit RW-1 403,872.45 cit RW-2 69,656.10 cit RW-3 67,175.65 cit RW-4 136,608.12 cit RW-5 179,874.98 cit RW-6 165,576.95 cit RW-7 224,646.55 cit RW-8 415,223.98 cit RW-9 74,215.15 cit RW-10 118,608.84 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes Nonroutine Hours 1.0 upon leaving: Yes Sand Filter Readings --While TP #2 is running. 59.45 Point Pressure (PSI) 57.45 SF-1 Influent 22 37.65 SF-1 Effluent 21 48.25 SF-2 Influent 21 53.40 SF-2 Effluent 20 54.77 51.00 51.68 59.69 56.30 Any leaks observed: No ----------- Upon arrival a submersible pump was placed in the retaining pond to begin draining the water. Replaced the regulator for RW-6 with a new regulator. RW-6 was running as designed upon departure. I I I I I I I I I I I I I I I I I I I December 17, 2001 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 ~~vt.DS'l,1>~ "Z' . . , 1- , . -- C/l u Q ~ ;\rcES;,: \8 re 1 r i~{(C 21 'lll\ . ·z;w 1 :.1-14-A\OT OOCUMENTCONTROLNUMl.1W..! I. .. " .. ' • ----.. Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed are the FCX System Check Forms for the weeks ending November 21, November 29, December 3, and December 14, 2001. All repair work performed during this time period is described in detail on the System Check Forms. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely; ~~ Brad Burdick 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • fax: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date· 11/21/01 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 278,398.76 cft RW-1 409,078.60 cft RW-2 70,421.98 cft RW-3 67,260.30 cft RW-4 137,552.65 cft RW-5 181,951.20 cft RW-6 167,221.15 cit RW-7 226,545.90 cft RW-8 419,720.00 cft RW-9 74,870.70 cft RW-10 119,745.20 cft Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes --- 59.95 Point 56.65 SF-1 37.80 SF-1 49.10 SF-2 56.50 SF-2 56.13 57.02 53.16 59.65 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 21 Effluent 20 Influent 20 Effluent 19 55.93 Any leaks observed: No ----------- DOCUMENT CONlROL NUMBER.._b.~ ... ,:;,;; I I I I I I I I I I I I I I I I I I I Date: 11129101 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 286,498.54 cft RW-1 411,484.25 cit RW-2 70,946.12 cft RW-3 67,308.01 cft RW-4 138,156.63 cft RW-5 182,940.27 cft RW-6 168,090.29 cft RW-7 227,496.09 cft RW-8 421,822.88 cft RW-9 75,215.35 cft RW-10 120,279.59 cft Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 No DEC 2 1 2001 Nonroutine Hours upon leaving: No Sand Filter Readings ----While TP #2 is running. 45.56 Point Pressure (PSI) 56.25 SF-1 Influent 20 37.65 SF-1 Effluent 19 47.34 SF-2 Influent 19 55.25 SF-2 Effluent 18 56.65 55.72 50.33 58.78 60.23 Any leaks observed: No ----------- Received page at 10:00 PM on 11-28-01. Arrived to site at 4:30 PM on 11-29-01. System was down upon arrival due to a high alarm in the backwash tank and trickle filter sump. Both tanks . were manually drained and the system was restarted. As soon as TP#2 turned on it began filling the backwash tank immediately. The system was shut off and the check valve on the _backwash tank was removed for inspection. The valve had a cracked section and was leaking. The part was not in stock at the plumbing store and was ordered. The system remained off upon leaving the site. I I I I I I I I I I I I I I 0 I I Date: · 12/3/01 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 294,074.78 cft RW-1 413,890.50 cft RW-2 71,443.89 cft RW-3 67,362.15 cft RW-4 138,458.90 cft . RW-5 183,929.65 cft RW-6 168,742.15 cft RW-7 228,352.98 cft RW-8 423,925.76 cft RW-9 75,508.32 cft RW-10 120,813.97 cft Pescdbe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 No -- 45.22 Point 57.21 SF-1 37.70 SF-1 47.25 SF-2 56.13 SF-2 56.63 55.54 49.80 59.76 · Nonroutine Hours 1.0 upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 18 Effluent 16 Influent 16 Effluent 16 62.42 Any leaks observed: ______ N_o.c_ ____ _ Replaced the broken union at the check valve on the backwash tank. Restarted system and noticed that the backwash tank was still filling when TP#2 turned on. System was turned off and the solenoid valve for the backwash tank was taken apart and cleaned. The valve was cleaned and replaced and the system turned back on. The system was monitored for 3 complete cycles and was running as designed. Next, the system was turned off to change the oil in the air compressor. One and a half fresh quarts of oil were added and then the system was restarted. I I I I I I I I I I I I I I I I I I I 12/14/01 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 314,378.85 cft RW-1 415,768.25 cft RW-2 75,977.10 cft RW-3 67,420.40 cft RW-4 140,060.00 cft RW-5 187,376.52 cft RW-6 171,065.08 cft RW-7 231,111.15 cft RW-8 430,523.46 cft RW-9 76,556.02 cft RW-10 L ~ -12,522.52-cft (/,sj 12.:z.., 2. z.s. ~ . ,..,...~n, ·-•--'· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes --- 35.65 Point 57.39 SF-1 37.29 SF-1 47.97 SF-2 52.10 SF-2 50.35 55.62 53.95 59.62 Nonroutine Hours 2.0 upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent Effluent Influent Effluent 60.65 Any leaks observed: ______ N.c.o ____ _ Upon arrival there was a leak in the plumbing effluent for TP#1. The plumbing was removed and replaced. Also, the pond outside the remediation shed was almost overflowing with water from the rain. A sump pump was placed in the pond and was allowed to drain. It took about two hours to get the pond drained to an acceptable level. DOCUMENT CONlROL NUMB~ I I I I I I I I I I I I I I I I I I I January 21, 2001 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed are the FCX System Check Forms for the period between December 14, 2001 and January 18, 2002. Any repair work performed during this time period is described in detail on the System Check Forms. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely· Brad Burdi 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • Fox: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date: 12/20/01 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 323,779.60 cit RW-1 415,780.40 cit RW-2 82,249.55 cit RW-3 67,453.65 cit RW-4 140,954.62 cit RW-5 189,137.86 cit RW-6 172,271.85 cit RW-7 232,527.72 cit RW-8 433,835.10 cit RW-9 77,078.20 cit RW-10 123,390.17 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes -- 35.83 Point 39.10 SF-1 37.57 SF-1 47.88 SF-2 55.66 SF-2 55.01 56.80 51.18 59.72 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 21 Effluent 20 Influent 19 Effluent 18 59.95 Any leaks observed: No ----------- I I I I I I I l I I I I I I I I I I I Date: 12/28/01 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 335,757.42 cft RW-1 415,804.72 cft RW-2 97,894.20 cft RW-3 67,507.96 cft RW-4 142,162.68 cft RW-5 191,225.98 cft RW-6 173,817.08 cft RW-7 234,417.18 cft RW-8 438,168.72 cft RW-9 77,749.13 cft RW-10 124,486.25 cft Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 35.50 Point 39.20 SF-1 37.35 SF-1 48.93 SF-2 54.55 SF-2 53.40 54.00 53.98 59.87 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 22 Effluent 21 Influent 20 Effluent 19 60.02 Any leaks observed: No ----------- I I I I I I I I I I I I I I Date: 1/4/02 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 346,450.68 cit RW-1 415,819.80 cit RW-2 109,745.50 cit RW-3 67,539.75 cit RW-4 143;259.89 cit RW-5 193,111.75 cit RW-6 175,194.80 cit RW-7 236,109.01 cit RW-8 442,026.64 cit RW-9 78,345.10 cit RW-10 125,444.82 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 35.52 Point 39.10 SF-1 37.66 SF-1 45.48 SF-2 53.25 SF-2 51.86 53.38 53.43 59.77 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 20 Effluent 20 Influent 19 Effluent 18 59.45 Any leaks observed: No -------=------ I I I I I I I I, I I I I I I I I I I I Date: 1/9/02 Jill Lemacks Was the system ronning upon arrival: Flow Meter Readings: Effluent 353,832.01 cit RW-1 415,823.34 cit RW-2 115,503.70 cit RW-3 67,560.21 cit RW-4 144,028.23 cit RW-5 195,108.52 cit RW-6 176,121.84 cit RW-7 237,260.42 cit RW-8 NM cit RW-9 78,945.97 cit RW-10 126,134.61 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 35.39 Point 39.14 SF-1 37.38 SF-1 46.61 SF-2 53.74 SF-2 56.56 56.40 NM 59.85 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 21 Effluent 20 Influent 18 Effluent 17 55.97 Any leaks observed: No ----------- I I I I I ,. I I I I I I I I I I I I I Date: 1/14/02 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 360,960.25 cf t RW-1 415,837.85 cft RW-2 121,449.01 cft RW-3 67,577.01 cft RW-4 144,784.70 cft RW-5 195,696.50 cft RW-6 177,020.35 cft RW-7 238,386.70 cft RW-8 447,214.00 cft 'RW-9 79,176.50 cft RW-10 126,781.25 cft Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes Nonroutine Hours upon leaving: Yes Sand Filter Readings --While TP #2 is running. 35.46 Point Pressure (PSI) 39.40 SF-1 Influent 21 37.57 SF-1 Effluent 20 50.95 SF-2 Influent 19 53.85 SF-2 Effluent 18 53.87 56.82 53.60 59.83 59.37 Any leaks observed: No ----------- I I I I I ,, I I I I I I I' I I I February 4, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 ·rrs o 7 20trl B~ l?:>3-'},f DOCUMENT CONTROL NUMBER., · • • 0 ' '""'~ A\-'-.S\ Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed are the FCX System Check Forms for January 25th and January 29'\ 2002. Any repair work performed during this time period is described in detail on the System Check Forms. The pump manufacturer stated they have only one loaner pump to send to me at this time. I am expecting the pump this week. As soon as I get the pump I will visit the site to remove one for service. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely; ~~~,~ Brad Burdick 434 Copperfield Blvd. N.E., Suite ll • Concord, North Carolina 28025 • Tel: (704) 795-7075 • fax: (704) 795-7076 I I I I I I I. I I I •· I I I I I Date· 1/25/02 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 377,349.25 cft RW-1 415,858.25 cft RW-2 133,999.05 cft RW-3 67,630.00 cft RW-4 146,483.38 cft RW-5 198,545.00 cft RW-6 179,115.32 cft RW-7 240,884.30 cft RW-8 452,836.50 cft RW-9 80,093.35 cft RW-10 128,189.13 cft Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 4.0 Yes Nonroutine Hours 6.0 upon leaving: Yes Sand Filter Readings -While TP #2 is running. 35.40 Point Pressure (PSI) 53.44 . SF-1 Influent 22 37.38 SF-1 Effluent 21 48.35 SF-2 Influent 20 51.60 SF-2 Effluent 19 55.82 56.00 53.85 59.60 58.05 Any leaks observed: No ------------ The pump for RW-2 appeared to be running continuously because the effluent meter was constantly spinning. Upon opening the sample port at the pump effluent it was noticed that there was some water being pumped, but it was mostly air coming through the line. The pump was pulled and inspected for any damages, leaks, etc. There were no leaks or visible damage on the pump. The pump was replaced and then the regulator for the pump was drained to bleed out any excess water. RW-2 appeared to be cycling normal now. After checking the flow readings for RW-1 and RW-3, they appeared to not be pumping much water. Both pumps were pulled and disassembled to look for any visible damage or scaling. Both pumps looked fine and they both were receiving the proper amount of air through the regulator. Next both regulators were bled to remove any excess water in the air lines. This still did not appear to cause either pump to function normally. After speaking with Ken Still ( a technical rep for the pump mfr.) he stated that due to the age and usage of the pumps, they probably are in need of service. He also said that they could service the pumps and provide a loaner rental while the pumps were being serviced. One replacement pump should be arriving on Februa,y 6th. (cont. on next page) 'I I I I I I I, I I I I I I I I I I I Pond Water Removal After traveling to 3 stores, there appeared to be no pump available that could perform the pumping job required to empty the retaining pond. An industrial size trash pump was then rented from a local rental facility. The remaining time on-site was spent pumping out the retention pond. The system was working fine upon site departure. I I I. I I I I I I I I I I I I I Date: 1/29/02 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 383,736.98 cit RW-1 415,889.00 cit RW-2 134,691.50 cit RW-3 67,667.20 cit RW-4 147,206.92 cit RW-5 199,647.20 cit RW-6 179,994.65 cit RW-7 241,879.90 cit RW-8 455,048.12 cit RW-9 80,463.15 cit RW-10 128,791.15 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes Nonroutine Hours upon leaving: Yes Sand Filter Readings -While TP #2 is running. . Point Pressure (PSI) • SF-1 Influent 20 . SF-1 Effluent 19 • SF-2 Influent 18 • SF-2 Effluent 17 • • . . • Any leaks observed: No ----------- *Water levels were not recorded during this visit due to a malfunction in the water level indicator during the weekly site visit. I I I I I I I I I I I I I I I I I I I FEB 19 2002 Date: 2-6-02 To: Joe Ferentz Roy F. Weston, Inc. From: Brad Burdick Staff Scientist CHANGE ORDER PROPOSAL FCX -ST A TESVILLE AES PROJECT NO. 153-92001-02 SUBCONTRACT AGREEMENT NO. 0012435 Phone: Fax: Phone: Fax: Applied Earth Sciences, Inc. Comments/Recommended Actions: Dear Mr. Ferentz; (770) 263-5452 (770) 263-5450 (704) 795-7075 (704) 795-7076 The following memo describes the out-of-scope activities conducted for the diagnosis and repair of the groundwater pump and treat system at the FCX facility. Specifically, this change order is for the additional time and materials used to drain the retention pond outside of the equipment compound. The attached costs is inclusive of project management time to purchase and pick-up the associated supplies and rental equipment. If you have any questions regarding the additional costs, please do not hesitate to contact me at the number above. I have included with this change order a description of the additional field activities associated with the repairs and I have also attached any receipts of items purchased or rented. January 25, 2002 Travel to pick-up supplies and rental equipment: Drain retention pond Rental of Industrial Trash Pump: Purchase of Garden Hose: ,f. Proposal Accepted: Sincerely, APPLIED EARTH SCIENCES, INC. Brad Burdick Project Scientist 2.0 hours @ 65/hour 4.0 hours @ 65/hour Lump Sum Lump Sum Total: $130.00 $260.00 $50.59 $16.78 $457.37 Date I I I I I I STATESVILLE RENTAL 905 Garner Bagnal Blvd. Slalesvllle, NC 28677 (704) 873-1951 /J'J,q11.o.,,vCt-1tV'/ ?u n .. ., ... ~--x ·-GOWE. "':S .. (7114)878-'!448 -SAl.£- RENTAL SAI.ES I: S8458JV1 17934 81-25-112 92359 FAIRUIWH 5/8 X 5 2 @ 7.88 SUBTOTAi.: TAX 38192 : IH'IOIC£ 24518 TOTAi.: 15.n 15. 76 1.112 16. 78 BPJJlltCEIIUE:~-- AIIEX:~ MEX XXIDXXXXXXX1888 8383 515164 AIUllJIT: .16.78 8458 Tml!HAI.: 24 81/25/112 11:81:34 THllHX rDII B BURDICK FOIi SIIOPPIH6 LOW(' S REC£IPT REllUIREO FOR CASH REFUND. CHECK PURCHASE REFIJWS REOUIRE 15 oor WAIT PERIOD FOR CASH BAO(. STORE "GR: DALE YOUHGER WE HAVE TH£ LOWEST PRICESi GUAAAHTEEO' IF rou FINO A LINER Pf<IL[ W[ Will ' BEAT IT Br 10%. SEE STORE FOR DETAILS. ADVANCE RENTAL CHARGE ADDITIONAL CHARGE REFUND CONTRACT NO. 6 8131 '{] HOMEOWNER RENTED OUT I I ':\... j ·.:-.\. ,,;,. . 0 CONTRACTOR 7 ,; /.'-' DUE ► -5 I''{ , .. ~OMMERCIAL , -··. RETURNED JOO NO P.O.NO. CHARGE ADVANCE FINAL RENTAL CHARGE DESCRIPTION CHARGES ,_..I· RENT -'-f.. / !) J SUB TOTAL SALES TAX ·sue TI>TAL ,. :.,,CC AOOITIONAL CHARGES ,;. I I I I I I I I I I I I I I I I I I I Date· 1/25/02 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 377,349.25 cit RW-1 415,858.25 cit RW-2 133,999.05 cit RW-3 67,630.00 cit RW-4 146,483.38 cit RW-5 198,545.00 cit RW-6 179,115.32 cit RW-7 240,884.30 cit RW-8 452,836.50 cit RW-9 80,093.35 cit RW-10 128,189.13 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 4.0 Yes Nonroutine Hours 6.0 upon leaving: Yes Sand Filter Readings -While TP #2 is running. 35.40 Point Pressure (PSI) 53.44 SF-1 Influent 22 37.38 SF-1 Effluent 21 48.35 SF-2 Influent 20 51.60 SF-2 Effluent 19 55.82 56.00 53.85 59.60 58.05 Any leaks observed: No ------------ The pump for RW-2 appeared to be running continuously because the effluent meter was constantly spinning. Upon opening the sample port at the pump effluent it was noticed that there was some water being pumped, but it was mostly air coming through the line. The pump was pulled and inspected for any damages, leaks, etc. There were no leaks or visible damage on the pump. The pump was replaced and then the regulator for the pump was drained to bleed out any excess water. RW-2 appeared to be cycling normal now. After checking the flow readings for RW-1 and RW-3, they appeared to not be pumping much water. Both pumps were pulled and disassembled to look for any visible damage or scaling. Both pumps looked fine and they both were receiving the proper amount of air through the regulator. Nex1 both regulators were bled to remove any excess water in the air lines. This still did not appear to cause either pump to function normally. After speaking with Ken Still ( a technical rep for the pump mfr.) he stated that due to the age and usage of the pumps, they probably are in need of service. He also said that they could service the pumps and provide a loaner rental while the pumps were being serviced. One replacement pump should be arriving on February 6th. (cont. on next page) I I I I I I I I I I I I I I I I I I I pond Water Removal After traveling to 3 stores, there appeared to be no pump available that could perform the pumping job required to empty the retaining pond. An industrial size trash pump was then rented from a local rental facility. The remaining time on-site was spent pumping out the retention pond. The system was working fine upon site departure. I I I I I I I I I I I I I I I I I I I February 12, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 fEB 1 9 20112 DOCUMENT CONTROL NUM&J( RR,.i IT3 ~::, 1 A1<.5J Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed is the FCX System Check Form for February 8th , 2002. Any repair work performed during this time period is described in detail on the System Check Form. If you have any questions please feel free to call 704-795-7075 at any time. Brad Burdick 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • Fox: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date: 2/8/02 Amy Icenhour Was the system running upon arrival: Flow Meter Readings: Effluent 398,592.75 cit RW-1 · 416,113.00 cit RW-2 136,339.60 cit RW-3 67,829.29 cit RW-4 148,917.37 cit RW-5 202,140.41 cit RW-6 182,019.62 cit RW-7 244,187.40 cit RW-8 --cit RW-9 81,247.54 cit RW-10 130,057.12 cit Describe reoairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes -- 35.2 Point 57.27 SF-1 37.48 SF-1 44.65 SF-2 56.56 SF-2 53.1 55.5 - 59.6 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 20 Effluent 20 Influent 20 Effluent 20 55.85 Any leaks observed: No ----------- No repair work.was conducted, however the regulators for RW-1 and RW-6 are going to have to be replaced soon. They are leaking a small amount of air right now which may be an indication of a futur problem with the regulators. I I I I I I I I I I I I I I I I I I I February 18, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed is the FCX System Check Form for February 14th , 2002. Any repair work performed during this time period is described in detail on the System Check Form. If you have any questions please feel free to call 704-795-7075 at any time. ~~ Brad Burdick 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • fax: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date: 2/14/02 Brad Burdick Steve lrrninqer Was the system running upon arrival: Flow Meter Readinas: Effluent 407,037.00 cit RW-1 416,240.08 cit RW-2 137,163.53 cit RW-3 67,933.85 cit RW-4 149,898.73 cit RW-5 203,518.78 cit RW-6 183 219.32 cit RW-7 245,532.25 cit RW-8 463,069.75 cit RW-9 81,769.25 cit RW-10 130,834.00 cit Describe repairs conducted: SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 35.4 Point 57.46 SF-1 37.8 SF-1 45.7 SF-2 56.65 SF-2 53.56 53.5 53.55 59.64 Nonroutine Hours 4.5 upon leaving: Yes Sand Fitter Readinas While TP #2 is runnlna. Pressure IPSll Influent 22 Effluent 22 Influent 20 Effluent 20 60.99 Any leaks observed: ____ __:N..:;o:_ ___ _ Removed pump from RW-3 and installed the loaner pump in RW-3. Turned pump back on and ij was pumping well. Removed old regulator from RW-2 and installed a new regulator for RW-2. Turned RW-3 back on and there was no leaks observed from the new regulator. Returned to office and shipped the pump for RW-3 lo the manufacturer to be serviced. I I I I I I I I I I I I I I I I I I I March 4, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 HAR O 8 2002 DOCUMENT CONTROL NUt.WER RfW f:?3-31 . -AktL ="' Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed is the FCX System Check Form for February 22, 2002 and March I, 200 I. Any repair work performed during this time period is described in detail on the System Check Form. I am expecting the serviced pump to be here on Wednesday March 6, 2002. As soon as it arrives I will remove the other pump for RW-1 to be serviced. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely; _ _✓,;, //'L.-.,,.., ~~ Brad Burdick 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • Fox: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date: 2/22/02 Amy Icenhour Was the system running upon arrival: Flow Meter Readings: Effluent 419,973.00 cit RW-1 416,424.41 cit RW-2 138,096.48 cit RW-3 69,495.90 cit RW-4 151,258.42 cit RW-5 205,430.37 cit RW-6 184,894.88 cit RW-7 247,422.80 cit RW-8 NS cit RW-9 82,394.50 cit RW-10 131,865.03 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 34.85 Point 34.97 SF-1 60.75 SF-1 46.76 SF-2 56.6 SF-2 55.9 56.35 NS 59.55 58.38 Any leaks observed: MAR O 8 2lll12 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 18 Effluent 18 Influent 19 Effluent 19 No I drained the water out of the air regulators in the following wells: RW-1, -2, 3, 4, 5, 7, & 9. I I I I I I I I I I I I I I I I I I I Date: 3/1/02 SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina MAR O 8 20112 Routine Hours Nonroutine Hours Amy Icenhour 3.0 . Was the system running upon arrival: Yes upon leaving: Yes Flow Meter Readings: Sand Filter Readings Effluent 429,993.18 cft -While TP #2 is running. RW-1 416,597.85 cf! 33.8 Point Pressure (PSI) RW-2 138,235.77 cft 35.7 SF-1 Influent RW-3 70,725.77 cft 60.9 SF-1 Effluent RW-4 152,443.47 cft 45.2 SF-2 Influent RW-5 207,031.75 cf! 56.75 SF-2 Effluent RW-6 186,304.25 cf! 53.3 RW-7 249,049.14 cf! 51.35 RW-8 NS cft NS RW-9 82,936.12 cf! 59.6 RW-10 132,725.36 cf! 60.35 Any leaks observed: No Describe repairs conducted· I drained the water out of the air regulators in the following wells: RW-1, 2, 3, 5, 7, & 9. I was unable to close the air regulator valves on RW-1 and RW-3. This produced a slow hiss of air. These regulators have most likely gone bad. They will be replaced as soon as new regulators are ordered. 16 18 18 19 I I I I I I I I I I I I I I I I I I I March 12, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 ffW13")-3,4-DOCUMENT CONTROL NUMBER ~ a~ A-\<}!(Q Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed is the FCX System Check Form for March 81h and March I 2'h, 2002. Any repair work performed during this time period is described in detail on the System Check Form. If you have any questions please feel free to call 704-795-7075 at any time. s~~ Brad Burdick 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • Fax: (704) 795-707~ I I I I I I I I I I I I I I I I I I I .. NV'l lUJ:"NT CONTROLNUNRfR A-K )('~ SYSTEMeRECK'FORm -,-_--- Date: 3/8/02 Amy Icenhour Was the system running upon arrival: Flow Meter Readings: Effluent 439,887.00 cft RW-1 416,034.12 cft RW-2 138,303.14 cft RW-3 71,927.45 cft RW-4 153,639.35 cft RW-5 208,619.36 cft RW-6 187,709.10 cft RW-7 250,653.15 cft RW-8 NS cft RW-9 83,514.34 cft RW-10 133,635.40 cft Describe repairs conducted· FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 33.85 Point 35.38 SF-1 60.90 SF-1 47.90 SF-2 55.25 SF-2 53.90 55.00 NS 59.55 60.05 Any leaks observed: Nonrouline Hours upon leaving: Yes Sand Filter Readings _ While TP #2 is running. Pressure (PSI) Influent 17 Effluent 18 Influent 18 Effluent 19 No We are still waiting on the serviced pump to be delivered. Once it is delivered we will proceed with the replacement and servicing of the pump from RW-1. Also, the meter reading from RW-1 has a lower number reading from the previous week. I believed the meter for RW-1 is spinning backwards from effluent water tt is receiving from RW-2 and RW-3. This is most likely because a check valve in the pump for RW-1 has gone bad. This problem should be eliminated when RW-1 · is serviced and replaced. I I I I I I I I I I I I I I I I I I I I DOCUMENT CONTROL HUMBER. AKiG ;,a''-, Date· 3/12/02 SYSTEM CHECK FORM FCX 1620 W. F rant Street Statesville, North Carolina Routine Hours Nonroutine Hours Brad Burdick 3.0 4.5 Amy Icenhour Was the system running upon arrival: Yes upon leaving: Yes Flow Meter Readings: Sand Filter Readings Effluent 445,298.17 cit -While TP #2 is running. RW-1 415,916.30 cit 33.85 Point Pressure (PSI) RW-2 138,333.72 cit 35.45 SF-1 Influent RW-3 72,548.40 cit 60.55 SF-1 Effluent RW-4 154,270.35 cit 50.00 SF-2 . Influent RW-5 209,436.02 cit 54.43 SF-2 Effluent RW-<'i 188,437.95 cit 52.96 RW-7 251,506.90 cit 52.20 RW-8 476,118.02 cit 54.20 RW-9 83,806.90 cit 59.75 RW-10 134,088.72 cit 62.10 Any leaks observed: No Describe repairs conducted· Arrived on site and took weekly readings first. RW-2 was not pumping properly, so it was removed for inspection. The inspection did not reveal any noticeable damage or non-functioning parts. The pump was replaced in to the well. Upon placing the pump back into the well it began pumping properly. After returning two hours. later the pump was still pumping as designed. The pump for RW-2 may be in need of servicing like pumps.RW-1 and RW-3. It is recommended that it be serviced soon. Next, the pump from RW-1 was removed io replace with the serviced pump from Clean Environment Equipment. While replacing the pump the barb fitting for the air line cracked. I Traveled to the nearest hardware store to find a new fitting. Once the fitting was replaced, the pump was placed back in to the well. Also, a new regulator for RW-1 was installed. RW-1 was then turned back on and the pump was functioning as designed. Finally, the oil was changed in the air compressor. 21 20 19 18 I I I I I I I I I I I I I I I I I I I March 26, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed are the FCX System Check Forms for March I 8th and March 25th , 2002. Any repair work performed during this time period is described in detail on the System Check Form. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely; Brad Burdick 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • fax: (704) 795-7076 I I I I I I I I I I I I I I I I I Date· 3/18/02 Amy Icenhour Was the system running upon arrival: Flow Meter Readings: Effluent 460,017.04 cit RW-1 421,352.75 cit RW-2 139,472.27 cit RW-3 73,566.95 cit RW-4 155,260.56 cit RW-5 210,839.04 cit RW-6 189,732.65 cit RW-7 252,993.24 cit RW-8 ns cit RW-9 84,372.00 cit RVv-10 134,921.52 cit Describe repairs conducted· .AKXP DOCUMENTCONTROLNUMBERr__~~~~~-. SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 49.84 Point 56.10 SF-1 60.30 SF-1 46.46 SF-2 56.65 SF-2 55.50 53.70 ns 59.60 55.25 Any leaks observed: Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 16 Effluent 17 Influent 17 Effluent 18 No I I I I I I I I I I I I I I I I I I I Date: 3/25/02 I !Amy Icenhour Was the system running upon arrival: Flow Meter Readings: Effluent 474,570.90 cit RW-1 426,470.00 cit RW-2 140,323.27 cit RW-3 74,548.68 cit RW-4 156,197.75 cit RW-5 212,221.50 cit RW-6 191,059.28 cit RW-7 254,543.33 cit RW-8 NS cit RW-9 84,963.00 cit RW-10 135,800.95 cit Describe repairs conducted· . .. . ·1·0N gil,jW)~-Af_il,;...;;.s..; SYSTEM ct-rt:Ci~¥\'Jif~T CON o\h --_·. . FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 57.76 Point 57.50 SF-1 60.35 SF-1 49.45 SF-2 55.70 SF-2 54.30 56.90 NS 59.65 58.60 Any leaks observed: Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 15 Effluent 15 Influent 14 Effluent 14 No I I I I I I I I I I I I I I I I I I CHANGE ORDER PROPOSAL FCX -STATESVILLE AES PROJECT NO. 153-92001-02 SUBCONTRACT AGREEMENT NO. 0012435 Date: 3/26/02 To: Joe Ferentz Roy F. Weston, Inc. From: Brad Burdick Staff Scientist Applied Earth Sciences, Inc. Comments/Recommended Actions: Dear Mr. Ferentz; Phone: (770) 263-5452 Fax: (770) 263-5450 Phone: (704) 795-7075 Fax: (704) 795-7076 The following memo is a recommendation for the FCX-Statesville site. Due to the down time associated with the repair and maintenance of the pumps for RW-1 and RW-3, AES is providing the following recommendation. AES will purchase the remanufactured AP-4 pump from Clean Environment Equipment. This pump will remain on-site in case of any future pump failure. This pump can also be used to replace existing pumps that may be in need of servicing. Project Management Purchase of AP-4 Pump AES Markup: Proposal Accepted: 1.0 hours@ 65/hour Lump Sum 10% mark-up Total: Roy. F. Weston, Inc. Sincerely, APPLIED EARTH SCIENCES, INC. Brad Burdick Project Scientist $65.00 $1,447.50 $144.75 $1,657.25 Date I I I I I I I I I I I I I I I I I I CHANGE ORDER PROPOSAL #4 FCX -ST A TESVILLE AES PROJECT NO. 153-12001-02 SUBCONTRACT AGREEMENT NO. 0012435 Date: 3/27 /02 To: Joe Ferentz Roy F. Weston, Inc. From: Brad Burdick Staff Scientist Applied Earth Sciences, Inc. Comments/Recommended Actions: Dear Mr. Ferentz; Phone: (770) 263-5452 Fax: (770) 263-5450 Phone: (704) 795-7075 Fax: (704)795-7076 The following details the costs associated with out-of-scope work, requested by you, for the FCX site. On 3(25/02 and 3(26/02 AES personnel collected the data you requested for the pump efficiency test. AES traveled to the site to on 3(25/02 to collect the weekly groundwater data for the site, along with the groundwater level readings for monitoring wells MW-I, MW-2, MW-3, MW-5S, MW-6S, MW-7, MW-10 and MW-27S. After these readings were collected, the pump-and-treat-system was turned off at approximately 11 :38 AM. On 3(26/02 AES again mobilized to the site to continue the test. Groundwater levels were measured from all the recovery wells and from the above-listed monitoring wells. The system was then turned back on at approximately 11 :00 AM on 3(26/02. A three (3) hour time period elapsed before AES recorded the final groundwater readings from the monitoring and recovery wells. During the pump test it was also noted that a number of the monitoring wells were in need of new padlocks. Some of the pad locks were either damaged or rusted to the point that they could no longer be used. The costs below also reflect the price of replacing these locks. Project Management: Padlock Replacement (MW-I, MW-2, MW-3, MW-5S, MW-6S, MW-7 And MW-10): 3/25/02 Collect Groundwater Data from Monitoring Wells: 3 .0 hours @ 65/hour $195.00 Lump Sum $45.00 .50 hours @ 65/hour $32.50 I I I I I I I I I I I I I I I I I I I Mr. Joseph Ferentz October 2, 200 I Page 2 3/26/02 Travel To/From Site: Collect Data from Monitoring And Recovery Wells: Travel to Store for Padlocks Truck Mileage Proposal Accepted: Sincerely, Brad Burdick Project Scientist 2.0 hours@ 65/hour 5.0 hours@ 65/hour 1.0 hour@ 65/hour 130 miles@ .40/mile Total: Roy. F. Weston, Inc. $130.00 $325.00 $65.00 $52.00 $ 844.50 Y/2.slo1- Date I I I I I I I I I I I I I I I I I April 8, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 Re: FCX Change Orders Dear Mr. Ferentz; Enclosed are the weekly system check forms for the FCX-Statesville Site. These forms cover the weeks of March 25 th and April 2nd, 2002. Any work performed during the weekly visit is explained in detail on the system check form. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely; Applied Earth Sciences, Inc. Brad Burdick Project Scientist 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • Fox: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date: 3/25/02 I !Amy Icenhour Was the system running upon arrival: Flow Meter Readings: Effluent 474,570.90 cft RW-1 426,470.00 cft RW-2 140,323.27 cft RW-3 74,548.68 cft RW-4 156,197.75 cft RW-5 212,221.50 cft RW-6 191,059.28 cft RW-7 254,543.33 cft RW-8 NS cft RW-9 84,963.00 cft RW-10 135,800.95 cft Describe repairs cqnducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes ---- 57.76 Point 57.50 SF-1 60.35 SF-1 49.45 SF-2 55.70 SF-2 54.30 56.90 NS 59.65 58.60 Any leaks observed: Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure {PSI) Influent 15 Effluent 15 Influent 14 Effluent 14 No I I I I I I I I I I I I I I I I I I Date: 412/02 SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours Nonroutine Hours Brad Burdick 3.0 4.0 Was the system running upon arrival: No upon leaving: Yes Flow Meter Readings: Sand Filter Readings Effluent 488,939.50 cft ·-While TP #2 is running. RW-1 431,250.53 cft 46.45 Point Pressure (PSI) RW-2 141,140.65 cft 57.45 SF-1 Influent 24 RW-3 75,589.35 cft 60.70 SF-1 Effluent 24 RW-4 157,044.00 cft 51.00 SF-2 Influent 22 RW-5 213,552.10 cft 52.70 SF-2 Effluent 22 RW-6 192,311.25 cft 55.70 RW-7 256,069.92 cft 57.10 RW-8 485,863.52 cft 53.15 /58.98-5.80) New pipe extension is 5.80 ft. RW-9 85,522.87 cft 59.55 RW-10 136,644.15 cft 56.60 Any leaks observed: No Describe repairs conducted· During the site visit it was observed that the main air feed line from the compressor had burst. It appears that the pipe had burst as a result of temperature changes over an extended period of time. An.inventory.o_f the plumbing part necessary for the repair was taken and then AES personell traveled off-site lei pick up the needed parts. The plumbing above ground could not be adapted to due to the fact that it was swollen too large to union the PVC to. Therefore, the plumbing below ground had to be dug up to locate a section of pipe in which to adapt the new plumbing too. After digging approximately two feet outside the remediation shed a section of pipe was found that could be used and the new plumbing was installed. A 30 minute time period was allowed to elapse to insure the plumbing was dry and ready for use. The system was then turned back on and monitored. Everything appeared to be in working order and there were no air leaks noticed in the new section of plumbing. The plumbing was then once again buried. Also, a new section of plumbing was added to RW-8. Since RW-8 in in a confined space, groundwater readings have not been collected lately. A section of pipe 5.80 ft. long was added so that these readings could once again be collected during the weekly site visits. After this work was done the weekly readings were collected. I I I I I I I I I I I I I I April 22, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 Re: FCX Change Orders Dear Mr. Ferentz; DOCUMOOCOHTROl.MUMBER"R~W t~3 -3t" A~-:z.y Enclosed are the weekly system check forms for the FCX-Statesville Site. These forms cover the weeks of April 12th and April 15th , 2002. Any work performed during the weekly visit is explained in detail on the system check form. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely; Applied Earth Sciences, Inc. Brad Burdick Project Scientist 434 Copperfield Blvd. N.E .. Suite B • Concord, North Carolina 28025 • Tel: (704) 795-707S • Fax: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date: 4115102 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 512,775.56 cit RW-1 439,145.82 cit RW-2 142,375.53 cit RW-3 77,304.40 cit RW-4 158,419.13 cit RW-5 215,959.80 cit RW-6 196,724.20 cit RW-7 258,623.92 cit RW-8 491,562.35 cit RW-9 86,425.59 cit RW-10 138,062.35 cit Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 No - 45.00 Point 57.22 SF-1 60.13 SF-1 50.92 SF-2 56.55 SF-2 54.86 55.74 Nonroutine Hours 3.0 upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 20 Effluent 20 Influent 19 Effluent 19 52.35 (58.15-5.80) New pipe extension is 5.80 fl. 59.72 61.42 Any leaks observed: No Arrived on site and the air compressor was not running. The breaker had been tripped. Reset the breaker and then the air compressor started up. After restarting the system the loaner pump from RW-3 was removed and replace with the newly service pump from Clean Environment Equipment During the reading of RW-6 ii was observed that the effluent meter was spinning constantly. This was due to an air leakage in the recovery pump. The pump for RW-6 was not pumping water like it should. The pump was removed and examined. No visible damage was noticed, however ii was determined that the air line check valve in the pump was in need of replacement. The pump was removed and the loaner pump was installed in its place. The loaner pump was then pumping as designed. The pump for RW-6 was then shipped to Clean Environment Equipment for servicing. I I I I I I I I I I I I I I I I I I I Date: 4/12102 Brad Burdick Was the system ronning upon arrival: Flow Meter Readings: Effluent 510,756.83 cf\ RW-1 438,504.35 cfl RW-2 142,250.18 cf\ RW-3 77,157.38 cfl RW-4 158,299.78 cf\ RW-5 215,742.10 cf\ RW-6 194,213.87 cfl RW-7 258,392.40 cf\ RW-8 491,066.53 cf\ RW-9 86,347.20 cfl RW-10 137,938.50 cf\ Describe repairs conducted· SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 Yes - 58.25 Point 58.00 SF-1 60.40 SF-1 46.40 SF-2 56.77 SF-2 54.21 51.33 Nonroutine Hours upon leaving: Yes Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent 20 Effluent 20 Influent 19 Effluent 19 51.28 /57.18-5.80) New pipe extension is 5.80 ft. 59.72 58.35 Any leaks observed: No IApr-25-02 ll:14A Applied Earth Sciences 704 795-7076 I I I I DOCUMENT CONTROL NUW;)i;.t( Qh,'J 1'3 '3-34 A'KZX CHANGE ORDER PROPOSAL 116 FCX -ST AT ES VILLI! AES PROJECT NO. 153-92001-02 SUBCONTRACT AGREEMENT NO. 0012435 I Date, 4/25/02 I I I I I I I I I I I I I To: Joe Ferentz Roy F. We,ton, Inc. From: Brad Burdick Staff Scientist Applied Earth Sciences, Inc. Comments/Recommended Action,: Dear Mr. Ferentz; Phone: (770} 263-5452 Fax: (770} 263-5450 Phone: (704) 795-7075 Fax: (704)795-7076 During the Semi-Annual Sampling event of April 23-24, 2002, the pump-and-treat system was not running due to a malfunction of the air compressor. AES contacted Ingersoll-Rand. the manufacrurer, to send out a field technician lo troubleshoot the problem. After approximately two hours, it was determined that the motor on the compressor had gone bad and ground faulted. This ground fault created a power surge which also damaged the air compressor contact in the control panel. Both the motor and the contact will both need to be replaced in order to re-start the system. The following details the work scope necessary to replace these components. According to Ingersoll Rand the new motor weighs approximately 350-400 pounds. As a result this will require some ne.cessary preparation and additional equipment to complete the work. Removing this motor through the doors of the shed will not be possible due to the weight and space constriction, therefore a section oflhe building will have to be disassembled in order to reach the motor_ After this section is removed. AES intends to have a smal1 crane on si1e. This crane will be used to remove the old motor and set the new one in place. Once the motor is in place a technician from Ingersoll Rand will install the new motor. After the motor is installed a certified electrician will replace the contacts in the control panel and check all the wiring before turning the system on. The electrician will also check the PLC to ensure it is operating properly. The following is an estimation of the cost breakdown for this projecl Any unexpected additional costs incum:d during this project will be submitted under a separate proposal letter. Project Management (sub-contractor Bidding and coordination, Parts tracking elc. } Equipment and Materials Explosion Proof Motor Motor Starter Contact Crane Rental 4 .0 hours @ 65/hour Lump Sum Lump Sum 4.0 hours@ 85/hour $260.00 $1,200.00 $275.00 $340.00 P.02 I Apr-25-02 Il:14A Applied Earth Sciences 704 795-7076 I I I I I I I I I I I I I I I I I I Mr. Joseph Ferentz October 2, 200 I Page 2 Electrician/PLC Programmer Ingersoll Rand Technician A ES Personnel Proposal Accepted: Sincerely, APPLIED EARTH SCIENCES, INC. Brad Burdick Project Scientist 8 hours@ 120/hour 8 hours @ 65/hour IO hours @ 65/hour Total: $960.00 $520.00 $650.00 $4,205.00 Date P.03 I Apr-25-02 OB:39A Applied Earth Sciences 704 795-7076 I I I I I I I I I I I I I I I I I I UY~RR,J l?,1.-::3A oocuMENT coNTROL N A I< iv' ,, CHANGE ORDER PROPOSAL #4 FCX • STATESVILLE AES PROJECT NO. 153-12001-02 SUBCONTRACT AGREEMENT NO. 0012435 Date: 4/25/02 To: Joe Ferentz Roy F. Weslon, In<. From: Brad Burdick Staff Scientist Applied Earth Sciences, Inc. Comment,/Recommended Actions: Dear Mr. Ferentz; Phone: (770) 263-5452 Fax: (770) l63-S4SO Phone: (704) 795-7075 Fax: (704) 795-7076 The following details the costs associated wilh out-of-scope work, requested by you, for the FCX site. On 3/25/02 and J/26/02 AES personnel collecled lhc data you requested for the pump efficiency test. A ES traveled to the site to on 3/25/02 to collect the weekly groundwater data for the site. along with the groundwater level readings for monitoring wells MW-I. MW-2, MW-3. MW-5S, MW-6S, MW-7, MW-IO and MW-27S. After these readings were collected, the pump-and-treat-system was turned offal approximately I I :38 AM. On 3/26/02 AES again mobilized to the site to continue the test Groundwater levels were measured from all the recovery wells and from the above-listed monitoring wells. The system was then turned back on al approximately I I :00 AM on 3/26/02. A three (3) hour time period elapsed before AES recorded lhc final groundwater readings ti-om the monitoring and recovery wells. During ihe pump test it was also noted that a number of the monitoring wells were in need of new padlocks. Some of the pad locks were either damaged or rusted to lhe point that they could no longer be used. The _costs below also reflect the price of replacing these locks. Project Management: Padlock Replacement (MW-I, MW-2, MW-3, MW-5S, MW-6S, MW-7 And MW-JO): 3125/0l Collect Groundwater Data from Monitoring Wells: 3.0 hours@ 65/hour $195.00 Lump Sum $45.00 .50 hours @ 65/hour $32.50 P.02 I Apr-25-02 08:39A Applied Earth Sciences Mr. Joseph Ferentz October 2, 200 I Page2 3/26/02 Travel To/From Site: Collect Data from Monitoring And Recovery Wells: Travel to Store for Padlocks 2.0 hours@ 65/hour 5.0 hours@ 65/hour 1.0 hour@ 65/hour 704 795-7076 $130.00 $325.00 $65.00 I I I I I I I I I I I I I I I I I Total: S 792.50 I Proposal Accepted: Roy. F. Weslon. Inc. Sincerely, APPLIED EARTH SCIENCES, INC. Brad Burdick Projec-t Scientist f?.goz_ Date P.03 I I I I I I I I I I I I I I I I I I May 8, 2002 Mr. Joseph Ferentz Roy F. Weston, Inc. 5405 Metric Place -Suite 200 Norcross, Georgia 30092-2550 -R.~(33-"34-DOCUMENT CONTROL NlJMl;,1,t:W 1 _ . _ ? "'l"' Au=.--J Re: FCX Weekly System Check Forms Dear Mr. Ferentz; Enclosed are the weekly system check forms for the FCX-Statesville Site. These forms cover the dates; April 23rd, May I st and May 71\ 2002 Any work performed during the weekly visit is explained in detail on the system check form. If you have any questions please feel free to call 704-795-7075 at any time. Sincerely; Applied Earth Sciences, Inc. /~~ Brad Burdick Project Scientist I 434 Copperfield Blvd. N.E., Suite B • Concord, North Carolina 28025 • Tel: (704) 795-7075 • Fox: (704) 795-7076 I I I I I I I I I I I I I I I I I I I Date· 4/23/02 Brad Burdick Was the system running upon arrival: Flow Meter Readings: Effluent 522,247.40 cit RW-1 442,036.27 cit RW-2 142,825.75 cit RW-3 77,962.77 cit RW-4 158,958.15 cit RW-5 216,906.60 cit RW-6 197,568.87 cit RW-7 259,571.56 cit RW-8 493,760.27 cit RW-9 86,783.02 cit RW-10 138,637.02 cit Describe repairs conducted· -- SYSTEM CHECK FORM FCX 1620 W. Front Street Statesville, North Carolina Routine Hours 3.0 No 37.33 Point 36.99 SF-1 39.50 SF-1 36.65 SF-2 40.35 SF-2 42.10 41.18 Nonroutine Hours upon leaving: No Sand Filter Readings While TP #2 is running. Pressure (PSI) Influent -- Effluent - Influent -- Effluent - 40.87 (46.67-5.80) New pipe extension is 5.80 ft. 46.53 44.57 Any leaks observed: No Upon arrival for the semi-annual sampling event the compressor was not running. The breaker had been tripped. The breaker was reset and the system was re-started. The compressor ran for about 5 minutes before the breaker tripped again. Ingersoll Rand was called to come out and troubleshoot the compressor. The Ingersoll Rand technician determined that the compressormotor had gone bad. The motor had also ground faulted which created a failure of the compressor contactor in the control panel. The faulty motor was an explosion proof type which would have to be special ordered. Also, an electrician would have to be called to replace the contact and diagnose the control panel to make sure there were no other problems. I I I I I I I I I I APPENDIXC PURGE FORMS I I I I I I I I I I I I I I I I I I I I I I I I I I I DOCUMENT CONTROL NUMBER P..fW r~·1-;>1)-AL-i!.Q· FUlng Information Job No. Job File ----::F,-ield:--:-:Fi::-le-11 Punch No Punch Description: FCX Fluid Level Measurements No. 150-92002--01 ---------------,------------ Well Ga&iAS Time Depth Depth Product Corrected Comments Ele•,·etion To To Thickness Ground Water TtJTl/lDEl'I Product Water Elevation MW-1 Ul ,:S( ) IY'f, z.,4 MW-2 if ,, I/"\ l/l/.~7 MW-3 1:Jd ,( :H, /fn MW-4 ?5,0 .. LI l/,25 MW-5D >IOit . s 'l, MW-5S ·, " /,· I '. . ~D •/{, Ill'• '• }• MW-6S IZJl8,0n / • MW-7 ~~.rn I~ ,c ) ., MW-8 '?I/ .oo ~ ,. ,o ' MW-9 15,50 ~ ,,,5' MW-10 qr){) I -J MW-11 "I ,ctu 7,-.. W-22S· ~ W-23 2tJ.7S t..:Jo, .5 ~ W-24S l/5.~Jt-8. '7 C:,J!L W-255 2S,d /?.Id -,· .. W-27S 1..0.so 33,0/. , , • , W-29I c;,y,o 2-oo RW-1 3·1, ;-'.'.:< t/42,Cf2.ln,27 RW-2 ;") 0 I' r< Ll;,.c,/,•~-::J'S"7S RW-3 3 ,c;(\ p7· · I I, v (g'Z.,77 RW-4 '"> '• rE::, l'5 [j, \ 'o~,I <..., RW-5 '? z 0, ( I/?,{~ RW-6 l ' !U l I._ ,n } _p,- RW-7 {.. • ,IQ 9 .5, /,er_ zc. RW-8 - RW-9 I ~-r 1--J'j ,. 7fJ3.CJl RW-10 I ,.j Ji In~-,02. . ... • I /P = -J.·tJo ,.,;-.n __. -? J' I .,("" I I I I I I I I I I I I I I I I D Site: Well ID: Water Level Indicator: pH/fempcrature Meter: Conductivity Meter: Borehole diameter: Total depth of wcU: Depth to water: Water column: Date Time ll/ :,--' I/ ,J 3:3'7f/11 3'.~00 ~;Cfflrn Form reviewed by: 2 ,, Water Level I Purge Well Purging Record FCX Statesville, North Carolina UJLLf CIT:D SR-fTlf{£ lt-T 4.'20Prn Volume ~Comments(Clarity, color, odor) Removed 0 o,'10 .~.n r; Z0,3 qc ") I.BO o. I -::7 -z_j,fJ'J (, 'V 'J 7,/n~ n. 7 -Jii.~ l °J() • ' -. Date: Page 1 • I I I I I I I I I I I I I I I I I I I Sile: Well ID: Water Level Indicator: pH/rempcrarure Meler: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Waler column: Date Time ~2 Form reviewed by: Water Level Purge Well Purging Record -FCX Statesville, North Carolina to!kl~~ J jfl;D'J Volume ~Comm~"'Cl•i,y, ,a~.-) Removed 0 :i~ •? Q(k) // L J L • I, S ,~5 Ir ;:;., ? L/eJ"J ?" -/4, .s-./'~,L· :J. 1 £..> /7 /Y,/ -<Jrp J ,__;t.l. .·/: ·. JS }.,( .. · . ' : .·-•·· · . . . :.·, . '.! :,i."::. :; . : . ; <•, ' ~ · .. . -.. . . · . . ·. Date: • I I I I I I I I I I I I I I I I I I I Site: FCX Well ID: fill{; ~ 3 Water Level Indicator: pH/femperature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time , . ~/?2l5Z, I I Fonn reviewed by: 2 I/ Water Level . Purge Well Purging Record . FCX n~ Statesville, North Carolina , ~~~ viii is ~ Jji,/r1 ,,-/-o (a~nd »ei vtll Removed - Volume ~Comments(Clarity, color, odor) o f\1n N6f SAmPui lr.L - . . Date: Page 1 I I I I I I I I I I I I I I I I I I I Site: F(X Well ID: nwJ~q Water Level Indicator: pH/femperature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time If /7_;1,/r,.7 I I Form reviewed by: Water Level II/V \ll;;D IT 5' Purge Well Purging Record FCX Statesville, North Carolina col)fdXo .0r1)f 6-½ )7:?D Volume ~Comments(Clarity, color, odor) Removed 0 1,9.3 'q 14 )".'?> }' In 3,loln (,' 14 'fl.1 (._ I( I,{) t;', YR l.b \ '-1 11.i I ,t\ () . • - Date: Page 1 • I I I I I I I I I I I I I I I I I I I . Sile: Fe~ Well ID: Mm~ Water Level Indicator: pH/fempcrature Meter: Conductivity Meler: Borehole diameter: Total deplh of well: Deplh to water: Water column: Date Time ' ---~ --- 41/.0/ 3Z77 (p,Z3 Water Level Fonn reviewed by: Purge Well Purging Record FCX Statesville, North Carolina v,...,, ~•~)'(cr.;ry,wl~,..,,, ,,.-;;-r.•J Removed . 14 ' 0 1 ..... ," Is::.£.""-' k?~·~. ~K) ') ·76 ~ -J.!J,00 -,4C .\.., io,J /11 71). ;;,o UC(rQ .I, ;IiJ;. '-1--,< :Jn.t~o C 'C/D ' Date: Page 1 . I I I I I I I I I I I I I I I I I I I Sile: Well ID: Waler Level lndicalor: pHffemperature Meler: Conduclivily Meler: Borehole diameter: Tola] depth of well: Depth to waler: Water column: Date Time ,\· -~ 11./lU \'\'J: () /jJl ~ f,{ ;,:Jo Form reviewed by: Waler Level ~o ~o ld.0 Purge Well Purging Record FCX Statesville, North Carolina l27J7 /4 J-0 jD )~l"f /(/JO Volume ~C.mmm•(CJ.,;O,<ol&, ""'l Removed 0 L-~ :1 ~ 9<>i0 /.~b-7 ;Jt2 /Jl,-J 1"10 t•• 7 :24 'J.l'J t. fq(_) . . • Date: Page 1 • I I I I I I I I I I I I I I I I I I I Site: Well ID: Water Level Indicator: p!Vfemperature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time . 4121/ldl ti,'/!t 11 , tl,'/ ,,,., ll. ·,<i , , ,1,1 .Form reviewed by: Water Level Purge Well Purging Record FCX Statesville, North Carolina v,rum, ~Cruruooo"'Cl'"'Y, oolM, ""'' Removed 0 l ' 2 2 "' ~ 1 L 7, d C,l 10 2,li~ 10, , /1 l I £1 :J C. /C-/17 3, iP(p 5': ,? . l/ I! tJ,;) ', CJ(') .c,• ··-~ AT '1.'l/5111v1 • Date: o ...... ,.,,, 1 -.. · • I I I I I I I ' I I I I I I I I I I I . Site: £()( Well ID: mw -lo D Water Level Indicator: pH/femperarw-e Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time Y,LJ;fbl. ,,,ow . Form reviewed by: 4 /f Water Level . Purge Well Purging Record FCX Statesville, North Carolina Vol=• ~;;1p1~.f -"(aorizy, ~•,. 000,) Removed 0 ~6 / 12 ·100 ·10 Jt/ I J ,,,., t.3'00 \\0 1. '/ IY 1', {,, F-.+,,:-0 !Th AT )/ '{)'°M_ n,.01 ir~P,~ A,,;_ 12 :zz. .. . . , . · ......... __ _. ... _ .. . . · .. c, _.'l . .. . !:) -L,) ... I I I I I I I I I I I I I I I I I I I Site: Well JD: Water Level Indicator: pWfemperature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time -- Water Level 10::)1 A 1 • /'\'S( 'i I\ I ./J5A 1 I , l/ • I • /t'I \ I's 1i' " IZ'. ,rff ~' Ptv t-, ·&:Vf'I i"\ • . Form reviewed by: i Purge Well Purging Record .FCX Statesville, North Carolina v,,.,,, ~C.mmrn .. Cl>rify, ro_,, _,.,, Removed 0 1.1,9 I,.. CJ ·:::; /,7(; Cl. ?'l 5.c, 21 I I (1 (,~ . 1. It,. Cj,J 2-lv I~ , i Si.J-n lt£T ,fhl /(l.M --.7 a3 ;(, ~ 5/(~~ ~-i1 -I ,, l?,nc'i 5,·; Z·Y IC -. ~ Oi "\; . I • . ') I 1 • ,c;.r I 5: I,, ?Pi I C L 3 ') f?,, O I' J:"h (Y!t • 17.~ ~ ,5. (o 2~ J} I (.. I ,, ') "'' c;; .TI) i.!~ -I' 'lf'),(Y c;; ( A 7F, Ir i,C--(. '7 111P ~ ,1) iTI, ~A{, 1.:~r1-,, .A:f"-1~~ . . . . .. .•.• > _ .. • Date: • -· L ~ ) It b I I I I I I I I. I I I I I I I I I Site: Well ID: Water Level Indicator: p!Vrcmperaturc Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time . @J/Jz ~ Form reviewed by: 511.m- 42 I 'JOI II, IQ' Water Level /J'.:?J 17:.).o Purge Well Purging Record FCX Statesville, North Carolina rodJtJ ~,1lr ~ IJ<JO v,...,, ~C.=mH(Cl•IO, col~, OOill) Removed 0 I ,8?) . ~ 1 _ 10. 5-rD -S. nln /,7. II? 2. ;Jo. -z__ /4'-fo 17:tp 5 . • { /1 I •. :,, ? t.o c;r;z,o ' . . ·.· '.' :-.. , :·-.: : .. ' ... . • Date: Page 1 I I I I I I I I I I I I I I I Site: Well ID: Water Level Indicator: pH/fempcrature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time I ' Y/7JJ/07, ·1:7il/f 7 ., Form reviewed by: 2." Water Level n . · Purge Well Purging Record FCX Statesville, North Carolina KJ/LL-fuff5E 2,/2 G/HLONS Vo..,, ~C-eo«(C .. ri<,, ro,~. 000<) Removed 0 O.lJ5 io; · I .' >CJO!O <,nOf'FD Pup:: i"r,y,,, n,, . 77) L-\IR 1 . {;f'i iN d'..J . n,n 11.\AT 5) Lr'H.Pt,P( A-L'• ' .. . . .. I - • - Date: Page 1 r1 , I I I I I I I I I I I I I I D D Sile: f[X We II ID: M,W ::-}( ) Water Level Indicator: pWfempcraturc Meter: Conductivity Meter: Borehole diameter: Total depth of well: 2 I/ Purge Well Purging Record FCX Stalcsvillc, North Carolina Depth to water: Water columo: 'ft ,0' )~01/? IIJ,·u Ptd'IJ£ 0,8z. G,ftlWNS Date Time Water Volume ~Conunents(Clarity, color, odor) Level Removed ' 0 I.ff) u 'iZ,, 3:':f) o. 05 -· --Klar 8' \I'll) C.-H Tu I Fh IA )WTT. J r:',I.AA-II LW..Jfli 1<.:& Of'..:i, ~ F A lv}\.1 ~ T:e,t. • ) j I "-."I ""!Sj\" / '"'--" 1Y\ll '>Tl I j {,lr ~ .. • . . Form reviewed by: Date: Page 1 i , I (! I I I I I I I I I Site: Well ID: Water Level Indicator: pH/fcmperaturc Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time Y/~('f). 1 /.;J-:J::) Form reviewed by: Water Level Purge Well Purging Record FCX Statesville, North Carolina ( cJ)PrW _snt{t{ @r ;}',00 v,,=, ~c"T.J'c,mo. ~•~ .• ,,,, Removed '/ /. 0 . ~ 7f7 0 Cj~<J '-I (,_(\ 0.. ,1.0. (\(\C) (, {,.~ °' \;.O q<\\) • .. Date: Page 1 • • I I I I I I I I I I I I I I I Site: Well ID: . Water Level Indicator: pH/fempcrature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time Form reviewed by: Water Level Purge Well Purging Record FCX Statesville, North Carolina Volume ~Comments(Clarity, color, odor) Removed 0 ;· . .:::.;:i:i}'.· . .. '' . • .. · .. c:r~: ,, '' .·. ',• ,, • - Date: Page 1 _. . ty:;_; _.-I·. . :-· - 1:. I I I I I I I I ·1, I I I· I I· I ., I I I Purge Well Purging Record .FCX Statesville, North Carolina Site: __._fi...,CX-~-- Well ID: 2LIS f~9" i../ 6rlJ()b 1 ~ r-'J'/3 H1-. {oJ/d~~I ob p:oo tp/e~ Ot-pJ i,1, 1:i:J~ - Water Level Indicator: pH/fempcraturc Meter: Conductivity Meter: Borehole diameter: Total depth of well: · Depth to water: Water column: Date Time '-ll,3lo') \~:>,O f;)~so f/:1JO '!;;so '/:'Is Form reviewed by: 4 ,, (t5,5' -M£ ~1 wiu PwPie I I/, lfi fjklWNS Water Voh,m, ~~"\~,w•~•"'°'' Level Removed t,. : , ~ -~ 0 ','.31\ '/, -,. 11. !IA . 1£\ ;,_ ).~ •. l IY-q~o ' . ;Po~ 79' ~< t,f?:J 100 1()0~ 7.4 L15 ,~ '., J7.{0 II I,..-7.P l,;)f I'✓-< . ' f:J<JO v Dale: Page 1 . I I I I I I I I I I I Site: Well ID: »l-26S: Water Level Indicator: pH/femperarure Meter: Conductivity Meter: Borehole diameter: :J.5,DO Purge Well Purging Record FCX Statesville, North Carolina td/ed,IJ #· /}t J/;r:Jo Total depth ofweH: Depth to water: Water column: ~.r7" 1.34 "" ~,O:J. Date Time Water Volume ~"7'<,(ClariO,rol~.-) Level Removed 0 YPP2 II ·-1 7 ff, 7';V }/41'1#/ :}. "J l5.? 6-17-£ WV 7 J"1.. ~ .I , 'l,o 5.,p 7 /7,Y C/C/,,f} J ♦L ' I - . . ,· .. · . • . ., "• F. ·':::>: I,:"'·. < ... ., ,. ·.· -.,. . -~ -, > ... ,::~, ,, , . ·. ... -~· .. ,· . . 't',- : ·, . • . . . . -. Form reviewed by: Date: Page 1 \ / I I I, I I I I I I: .1 I :I I ., I, I I I I Site: Well ID: Water Level Indicator: pH/femperature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time ' . i//mfl ,,q: '.2{"\ I I ~.:t/{ ~:> Form reviewed by: Water Level Purge Well Purging Record FCX Statesville, North Carolina 1oltt11J ot L~ 00 ~::;, I Vol=o ~""""""'C"'"', ro_,, """l Removed 77,(f!g TU'tf t? 0 ~ I <1J .B 1 lo I CJ. 7° z. 7,:;., U', ~ x' '1' JO 1q, c;o ·~ :A 8 7 LY q '1t70 Jq. :.3 . .. ''• . ,-)75 It' /• '. , .. , ·-., .. . ':: ·::',_:' .··· ;. '·· : - Date: Page 1 .. • I I I I I I I I 'I I I, I I I I, I I I I I Site: Well ID: Water Level Indicator: pl-Vfemperature Meter: Conductivity Meter: Borehole diameter: Total depth of well: Depth to water: Water column: Date Time . . 1//J'/fr2. , Form reviewed by: Water Level 15 3D Lf? Purge Well Purging Record FCX Statesville, North Carolina Vol=, ~Commoo .. CoriO, oo•,. odo) Removed 0 . t. /J /:_.., ; vvo c; 1 l'J l~•.6 '-4~.:b.!J 5,7 IJ !S.t po .. .. ' ' ! .• .. ,c: .. . .. ··;:-,.· . .. . r' - Dale: Page 1 .; . . . ·□·' ,", ' '• ·-· .. ',;. I• ·:=~·:! :· :::{'· ::::·. ., .•• 'Ji • :' ,_.,,-, _,, ,_, '. l. ·, :_ -:•.' /:· ·-. ; :·_/:·~~--~: _?'~ -.'· . ·-; ·~ .-:~ '\ ., '. ·:. ! . ~ ...... ~ ·: ... : '1·· ·., '' ··, .. ·_..,-': .. ·· . ..,• ,, ,, ~-. . \. -· ... , ., ,::5., .::\ :/~;-i· })·' 'f. ::--,•: ·r: ·,) ... •: . . ',_ . .... •·· -~·--: . ;: :. ! . ,' '.;_\·: . '' .-.. , . •·• . .. . •'' ' . •:-J..;-'' ., ·, .•·- I I I I I I ' I I ff I n I I ,, ' : I I I I APPENDIXD TRAFFIC REPORTS AND CHAIN OF CUSTODY ---,.-.-..., ·~I --, Organic Traffic R"':;rt -....,. ........ --......, ......, _, --C EPA United States Environmental Protection Agency Case No, ~a, Contract Laboratory Program & Chain of Custody Record JtPI,/ ~ (For Organic CLP Analysis) 1. Project Code tJ,!J.,.-ot/C, 3 2. Reg2to·1 Sampw§.$7bA/ \2~ ~¼~arrierh;a~ ~-o~C 6. Matrix 7. Preservative > (Enter in (Entsrln Account Code S~Name) hJ. Air6~1:9n berg~.::J-t, '(/}~/ 6134 Column A) ColumnD) 'ZMMirJf!..I,4 1/2.f) 1. Surtace Water 1. HCI 2. Ground Water 2. HN03 Site Name Sampler Zinnair,r• / L/ 3. Leachate 3. NaHS04 '.7/. 4. Field QC 4. H2S04 , -/ -r 5. Soil/Sediment 5. Ice only 5. Ship To: CiF ~A1ze, ~t>MT~lv kX / 5f IF{es//a~ /t> PE,'J-N NA-ti>~ .t),,e. I f'i',jr )OSe•" Eariy~loo 6. PE-water 6. CH30H • ' ~IA Long-Temi )v A-/!/f!Jl6rlrtV'%TTj,££ ~B;i.. 7. PE-soil 7. Other /specify ~ PA """' 8. Other /specify in in Column D) Site Spill ID Op Unit • REM ~ N. Not Preserved -City, Slate Column A) ST RI !"c4,eG;il ~/US6N '5f m~ lit"~ ;t,t.-, -FED SI -BZ ESI ATTN: M CLP A B C D E F G H I J K Sample Matrix Cone.: Sample Preser-RAS Analysis Regional Specific Station Mo/Day/ Corresponding Sampler Field QC Numbers (from Type: vative TA TA TA Tracking Number Location Year/Time CLP Inorganic Initials Qualifier (from labels) Box 6) (from I""" :;:jp' (circle one) (ciftje one) or Tag Numbers Identifier Sample Sample No. B • Blank S • Reid Spi:,e Other. Low Comp./ Box 7) nn* 7 1 ..,,..,. 7 14 ,, pR*71421 Collection O•FioklOuplea , . .,,,_ Med Grab Other. -Pesv PE • Pertorm Eval. VOA BNA PCB /)/"IT t,J I)-L,... ,Gr I >< I.; '1,1{)/)q4/ /l'/W-5,1) V.z. ·/4., · l.6~ '-•A --;7t,t 7P /)l'JWb .a...,, L... (; ,.. I ><--M-1/~.1~/tli/cr /J1a;-~q ,_ 'bd·/7t!7 /n/)/"f /, I ✓? V h/"Jt11? ~ L,... l-,r / '><" if _,+:-@t'Jt) /tJ 1,/,;2. Rk.P-~ t1 /tJ. /,,,t, AA, ,7,C:. 1>1'11,V/3 .:;... [,,-1,,,,-I '...c" WS~dtJt1tl I tJ i/l'J 7A-o~ ,,/. i'O•/"l!Zr, .7):::: T,e.rP n., •• , , -, ./ r--I ,-, -, _ .... A l'V'lN • ::TCONTR JL. - Al<.Z-T' Shipment fod?ase _l.~;e/ VOA MSIMSD Required? c;fN Sample#: D/ ,, Additional Sampler Signatures Chain of Custody Seal Number(s) Complete? N) BNA MSIMSD Required? YIN Sample#: Pes~CB Msn.tSD R~uired? Y/N Samole#: *PR orovldes 7-day 9;3!a turnaround in addition to preliminary results. Requests for Cha'in of Custod Record prehmmary results will increase analytical costs. Relinqui ed b (Signature) Date I Time Received by: (Signature) Relinquished by: (Signature) Date/ Time Received by: (Signature) ff Jil',ji ~" 0 Date /Time Received by: (Signature) Relinquished by: (Signature) Date/ Time Received by: (Signature) Relinquished by: (Signature) Date/Time Received for Laboratory by: .(Signature) Date/Time Remarks: Is custody seal intact? YIN/none IMtribulioll: Blue· Region Copy Pink· SMO Copy 'Mtile • Lab Copy for Retum lo SMO Yellow• Lab Copy for Retum to Region EPA Form 9110-2 (2199) See Reverse for Additional Standard Instructions **See Reverse for Purpose Code Definitions 404488 ClASS-!lS-001 iiiil /J - 1. Project C~e:J-tJ Account Code 'Pfl orovides 7-dav Qata turnaround lo addition (o preliminary results. Requests for preilmma resultsw,11,ncrease anal ,cal costs. Chain of Custod Record Relin e Received by: (Signature) Relinquished by: (Signature) Date/ Time ptJ e Received by: (Signature) Relinquished by: (Signature) Date/Time 6. Matrix (Enter in Column A) 7. Preservative (Enter in CotumnD) :,I 1. Surtace Water 2. Ground Water 3. Leachate 4. Field QC 5. Soil/Sediment 6. PE-water 7. PE-soil 8. Other (specify in Column A) I Corresponding CLP Inorganic Sample No. J Sampler Initials Received by: (Signature) Received by: (Signature) 1. HCI 2. HN03 3. NaHS04 4. H2S04 5. Ice only 6. CH30H 7. 01/ler /specify in Column D) N. Nol Preserved K Field QC Qualifier a • Blank s • Field Spike D • Fleld OuplicaU R•Rinuta PE• Pw1orm e~■- 0 Relinquished by: (Signature) Date/Time Received for Labcratory by: (Signature) Date /Time Remarks: Is custody seal intact? YIN/none Distribution: Blue • Region Copy Pink. SMC Copy White -lab Copy lot Return lo SMC Yellow • Lab Copy for Return to Regi:m EPA Form 9110-2 (2/99) See Reverse ror Additional Standard Instructions "See Reverse for Purpose Code Definlilons 404486 CLASS-!>". liiiil Cit State M CLP A Sample Matrix Numbers (from (from labels) Box 6) Other: Site Spill ID Op Unit '~"":""' PA REM RI SI ESI Long-Term AcrlOII ~: hipTo/ff, '=746/VT.CA /5ff $Aa;O',(_q-,.e"~ ~, So /2W /1/oPJ)ll)Nj~ 7X 77 3& o ATTN: /:El}/) F Regional Specific Tracking Number or Tag Numbers G Station Location Identifier Mo/Day/ Year/Time Sample Collection 6. Matrix (£nterln Column A) 7. Preservative (Enter In Column D) 1. Surlace Water 2. Ground Water 3. Leachate 4. Field QC 5. Soil/Sediment 6. PE-water 7. PE-soil 8. Other (specify in Column A) I Corresponding CLP Inorganic Sample No. J Sampler Initials 1. HCI 2. HNO3 3. NaHS04 4. H2S04 5. Ice only 6. CH3OH 7. Other (specify in Column DJ N. Not Preserved K Field QC Qualifier B•Blri S•Fleld59lt 0 • Field 014)1c .. •·-PE • Perfoml ev.. Shipment !~ase Complete '(YIN) Page/ VOAMSIMSD Required? y __L of -BNA MSIMSD Required? y Sample#: Additional Sampler Signatures Chain of Custody Seal Number(s) Sample#: Pest/PCB MSIMSO R uired? ~ Sam le#: •pf! provides 7-day da!a turnaround in addition to prelim'1nary results. Requests for prehrtirna results Will increase an 1ca! costs. Chain of Custody Record Relinquished by: (Signature) Date/Time Received by: (Signature) Received for Laboratory by: {Slgneture) Distribution: Blue • Region Copy Pink· SMO Copy . White. Lab Copy for Return lo SMO Yeller#. Lab Copy fol Return 10 Region Relinquished by: (Signature) Date I Time Received by: (Signature) Relinquished by: (Signature) Date/Time Received by: (Signature) Date /Time Remarks: Is custody seal intact? YIN/none EPA Form 9110-2 (2199) See Reverse for Additional Standard Instructions .. See Reverne for Purpose Code DeflniUons CLASS-99-001 404487 liiiil -------......, W~ ~ ----le cR -Case NO. c,i, ~ United States Environmental Protection Agency & Ch · f C t d R d 3tP///8 ~ Contract Laboratory Program a,n O · US O Y ecor (For Organic CLP Analysis) 1. ProjectC~~-t?~93 2. Regffo·\ Sampl~$/O,,{/ 4. Date Shipped \ Carrier/;€£.)e=,RA'.'.; fu /?£5':.. 6. Matrix 7. Preservative (Enter in (Enter in Account Code ~Name) h, Airbill Numberb',;h "7/?:, -, _ ,;~1~6/f'-;) Column~) Column DJ MZ.Tl2J:A-,,ep 1. Surtace Water 1. HCI fi/::/1,'5/f'tJ )5"1~ )(,/J?:&1 2. Ground Water 2. HN03 Site Name Samplerrn~ _ / V 5. Ship To: If f 5qfiA17Z:rZ:,.C/ 3. Leachate 3. NaHS04 pc,)< /7fAfESVJ.Uif' -4. Field QC 4. H2S04 '<-/ I /~# .5At,,V/,XA~ Ro) :}l; ,SbS 5. Soil/Sediment 5. Ice only ,r·· ,~, ' 6. PE-water 6. CH30H " _IA Long.Term 7l-!e /AIClltJUi-/llP>_;7X 77 38 CJ 7. PE-soil 7. Other (specify SF PA Action 8. Other /specify in in Column OJ Site Spill ID Op un·,1 RP -REM Mis City, State ST -RI ATTN ,k'.i:; PP y h M/11 lifZ- Column A) N. Not Preserved 7{A1~~/i/C, FEO -ii BZ -SI M CLP A B C D E F I G H I J K Sample Matrix Cone.: Sample Preser-RAS Analysis Regional Specific Station Mo/Day/ Corresponding Sampler Field QC Numbers (from Type: vative TA TA TA Trackin~ Number Location Year/Time CLP Inorganic Initials Qualifier (from labels) Box 6) (from 1-7.1 I-~ (ciltle~ or Tag umbers Identifier Sample Sample No. B•Blri. S•Flc!h!Spb Other: Low Comp.I Box 7) oo• 7 '21 loo• 7 21 oo* 7 '21 Collection O•FllldOupk-. Pesv •·-Med Grab Othe, VOA BNA. PCB PE • Penom,_ Ev,..& /),7,.,. a. L-~ I ~ I~ X /«-Q .,.,.,,v~f" '=,&?-o I l,fj!.>4,6~: MPO Upl'?T9 ---.:-:L':'·-.. • ... OA"/~t.f ,JI 11<1WLL _,,,_ '-~ ,r I ><' ~ >< t,,5-d P<J CV/,!;:~ Ou/J-tP~ II,_ .., -,.,.,,/, vf/J/'9W:t-:7r" /) 'J/(Jbt// ~ L /'..r I ----.e "><'.:'_ __,,,. /41.>-Lf ~~ ~o/ 74 Utv-/?1>· ,,, ,l tJ~:IUF. U~/qtv/ -::7F /)f1W3 ~ L ty / --:::,..:::... '>C X ws--=4 g '2~~{,. Mlt/-h< , ;;""" U/J/'1W3 'r r ' l Mt/I~ ,;2._ L-Gr I .....___,_,,-IY:S'...; {/ -• IP.!!. p., Tl!, tJ/ W,;~ ~.15!.S' '-' 'F . / Shipment for Case _J~i~ VOA MS/MSD Required? N Samole #: 0/ ?lf/.5 Additional Sampler Signatures Chain of Custody Seal Number(s) Complete? (Y/NA/ BNA MS/MSD Required? h-1 Samole#: 0/, ,IA,),:/ PestlPCB MS/MSO R~~-IN Samole#: n,/&1/~/ 2 •p~ orovides 7-day data turnaround in addition to preliminary results. Requests tor Cha'in of Custod Record prehrtunary results will increase analytical costs, Relinquished by: (Signature) Date/ Time Received by: (Signature) Received for Laboratory by: (Signature) Dislribulion; Blue • Region Copy Pink· SMO Copy White • Lab ~PY for Retum to SMO Yellow• Lab Copy for Re tum to Regbrl Date/ Time Received by: (Signature) Relinquished by: (Signature) Date/Time Received by: (Signature) Date/Time Remarks: Is custody seal intact? YIN/none EPA Form 9110-2 (2/99) See Reverse for Additional Standard Instructions "See Reverse for Purpose Code Definitions CLASS-9~1 404489 =------._, --iillJ -liilll -- - -.., -Inorganic Traffic Report Case No. Q EPA United Slates Envlronmenlal Protedlon Agency ~J' Contrad Laboratcry Program If Ujo:Y' & Chain of Custody Record (For Inorganic CLP Analysls) ~~/6 ; 1. Project Code I 2. Account Code 3. R"?t No. Sa~~ PAI 5. ,9ae '"I"""" 1 Canter ~ 7. Matrix 8. Pneservatlve P.P-t'.;:.-1:; : .k~c£Al-~Bs imrlrt =:DJ 1111t1AJ Regional information ~(Name/ ~ -Ai'rlllll wr ~q ~~/~I 111-1. Surface Water 1. HCI '.J:MMZr,eJ:A-~ 2. Ground Water 2, HN03 Non-Superfund Program Sampler )lgnabjpr ,/ f/ 6. Ship To: Ul!E..vY ~ If? ln:a4l-,,- 3. Leachate 3. NaOH 4. Aeld 4, H~04 / I , I 5. Soll/Sediment 5. K~R 0, Slte~/4 VtJrpo,e' """T'"" ~ M-9,p.t:;S.?/il /2VE, 8. OIi (High only) 8. Ice onr, ,k)t, ~&v'/:Uc CLEM _._, 7. Waste (High only) 7. Other sp&CI/-/ ~ ._ PA -FS --;Y1.IV~ ~7J7 3 8. OOler (spec/ft In In Column DJ ~~Nd -REM .:ii i Column A/ N. Not Prasetved Site Spill IQ -Rl At.~Ct E/1' ,f#..S -SI -ATTN: ESI CLP A B C D E RAS Ana MIS F G H I J K Sample Matrix Cone.: Sample Presar-Low ~~ Regional Specific Station Mo/Day/ Corres~dlng Sampler Aeld QC Numbeni (from Low Type: vatlve J 11 On• Tracldn~ Number LocaUon Yearmme CLP rganlc Initials Qualifier (from labels) Box 7) Med Comp./ (from fl li I or Tag umbers ldenUfier Sample Sample No. B•Blri: S•si,ic;• Ollie,: High Grab Box8) ~ Collectlon D•-R•-01hr. PE• Ptrtrm Eval, -■ Not i ,;.;.-s.-·· . lnnleJ? n .::i---l-6T .1-/f-lS-41 t't't>/t1/,,2...., '!~A "<tJ / 7~/4 ~/,U,,' -;~ b • I I 1'/b/<17.' ~ '-~ ,.. .!1--NG-• ~ <JOO/Rt:'~ A-1A-t-~d ';fplt.'17 !)--6'---'-/2 -~ A/,~--• t i1tl CJ/t'tJ6 IX/,,P-tJ/ Molerl' , ..!L, '--;;'r· ~ .:t--W.5-, t ~t'CJ/t:>/e, //1'1,I .er: MO ''r/' ::> ~ t.-(; r .;!-U/S,--4 /)(J/) qq ., /4w-J/ /)11}/' n, {)-. L-t ... /J.-Y/~..!., ~M~t i&j t. C ~-, . -,' I ~ 1t101q,-, ~ L, ,r ~ M-~~tJoCJ"?<J'q ,l,f,W-)' MIJ!iJWP ~ L C. ,-~ K ws-'1-ot11Jlt'J~o /l'JW-55 -.,,v,7Wb ~ L ... ~ ~ w5-,!t<J1Jt1/t>39i /i1tt1-~q 'MIJ/~Y/ a,, L :;_ X , .,,. / t?t?t? /tJP-4 fA;-tJJ ' .,.. Shipment ~se :omplete? ) Per~ ..Lot Sample(s) to be Used for Laboratay QC 'tf1Pl9AIP -M~jM$[> I Additional Sampler Slgnaturaa Chain of Custody Record Received by: (Signature) Relinquished by: (Signsture) Received by: (Signature J Relinquished by: (S/gnsture) ' J (.,~ Dl4TI vP :N L -,.-Pl'1T.#-, .::JP D J, .,.M.:IJl. /)/. '/ ""T z::: ~7' •/ ,,--;;~ /J/• 1rs. \ c::---. I .~.;~ , /.)p "/6;, -rp ~' /4i:~ 17 /.J / '1'T .:;z.. ,Tl=- [Lj/~3/,'J{. Jt;,, 't>Jc,WtJ JP- ,/_ ,,L:. •l'H , Ol'!/A/6 ' ·r-. ,, /4:~ , t>l'!X I ,-rp- , , ,,,, Chain of Custody Seal Number(s) Date/ Time 12,H;,I I 3 3 -3A Received by: (Signature} Akzs Received by: (Signatura) !e6nqulshed by: (Signature) Date I Time Received for Laboratory by: (Signature/ Date /Time Remarks: Is custody seal Intact? YIN/none llltrlbuUon: 8-. Rogian Copy Pink, CUS8 Copy WIINI • Lab Copy ro, Rotum lo Ra;loo Yollow • Lab Copy lor Rotum lo CI.A88 EPA Form 9110-1 (8/99) a..-.rorAddJllonal atandardl- '9• -for p.._. Code Dlftnlllont 399850 ft EA~ Inorganic Traffic Report Case No . .._._.. United ~~~i,:,~~ ~~~ Agency & Chain of Custody Record / L ..... (For Inorganic CLP Analysis) So-// B 1. Project Code ,2. Account Code 3. Rei io No. Sem9l\ng,Co. 5._.9~ ~~ I Carrier /-. C:: t~>t:¥/f3 '-Wt:-S7l)IV w~ IP~ rE/Jc/e,ft_ c5Cf'l!E>5 Regional lnfomlallon Se~!!" (Name) r Alrblll ~ber 7. Matrix (Enter In o,,.,,,,, ,<) 6. Preservative (Enlerln 0,,.,,,,, DJ VI/,fMCftaA 17J)l/),, p~9"6tj$.P-/~// ti- Non-Superfund Program Sempler;;ignatu~ / 6. Ship To: L -t / JI 1 , L -I ~ -, , I:U.J! TJ MNAL-v rz Cl!- CLP A B C D E RASAna Is F G Semple Matrix Cone.: Semple Preser-~ : , Regional Specific Station Number, (from Low Type: vatlve t.. :I Tracking Number Location (from labels) Box 7) Med Comp./ (from :I :I f f f j or Tag Numbeni Identifier Olher: High Grab Box 8) ~ ~ _; l i. Other. H Mo/Day/ Yearmme Sample Collection 1. Surface Water 2. Ground Water 3. Leachate 4. Field 5. Soll/Sediment 6. Oil (High only) 7. Waste (High only) 6. other (specify in Column A) I Com>spondlng CLP Organic Semple No. J Sampler Initials 1. HCI 2. HNO3 3. NaOH 4. H~"04 5. K~R 0? 6. lceont 7. Other (specify In Column DJ N.NotPrese<ved K Field QC Qualifier e • Blltit s • Spb O•-R•-PE•PwbmE'tll. -•Not ~ ... '·-V,1 ti-L ,,,,.,.. ~ } 11/)/' ~~ :;..✓ I _... ,P.-I) w£ :t,t. OtJ/JliP~ r · WG-/1-oo;; 1~4'-3 /?11P-t:J.S ,n. ~ ,✓-.,.&" 0/~)l,;J.-, I,_,... Shipment foi_£a_se Complete? [91N) ,._P•~ ,1 • Sample(s) to be Used for Laboratory QC -F of ...sc MI) 19 t,(,I $ -"'4 f /,11,ts p Jl?u/-.::j-V, ·• :~ • ./}Jqt(/$ ,Jf- Additional Sampler Slgnaturas Chain of Custody Seal Number(s) Chain of Custody Record , ~e0nQ1Jlshed by: (Signature) Received by: (Signature) '/) Received by: (Signature) Date/ Tune Received for Laboratory by: (Signature) Clnon•RooianCopy Plnk•CUl8Copy Whllo • I.ab Copy lor _,,, o, R,glGn Yollow•UbC"1'f lat Rotum o, CUSS Relinquished by: (S/gnsture) Date /Time Received by: (Signature) Relinquished by: (Slgnsture) Date /Time Received by: (Signature) Date/ Tune Remarl<s: la custody seal Intact? YIN/none EPA Form 9110·1 (8/99) ... _.., __ ,_ ,_ '8• -for PUIIIOU C4de Doflnltlonl 399854 .. , . : .... .. • .. ., ;,,_, ~,, . . ,-. :, . i'. •,l: •• ... '· '• .·' -.. :,_1 .-~' .. ·,:,f••. . .._ "· ~-: :,.~·-.:··->:-. ~~:; -;•,. '~~-' -; • ,· --,.1 r,·{·.: ... .':-.... •:• ' . ::~;··~-•,: ' ~ ~ t '•, ' :. ' ~---( .. . ·-..... , . 'i-_; "· , :. .. • ,~ ~ > • -~. :•::.•: ··•.,,, '' .,.~ ,i' r • ~ • -. I • • ! e ~,..., ' "·, i ·. \, ... ·\i-::t·; .. ' ' .. ·-'• ~:~x-.. .-. ·, / ~'. .,:, __ ._ .... ,· ~ \ ~ !-: •• ? ., I I I I I I I I I I I I I I I I I I I APPENDIXE LABORATORY ANALYTICAL REPORTS I I I I I I MEMORANDUM UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division 980 College Station Road Athens, Georgia 30605-2720 Date: 06/03/2002 I Subject: Results of VOLATILES Sample Analysis I I I 02-0493 FCX, Inc. (Statesville Plant) Statesville, NC From: Mcconney, John ~'c c..5 To: Mallary, Ken CC: Ralph McKeen RACSNJ I Thru: QA Office DOCUMENT CONTROL NUMBER ].,H.>h ~ 1, - ::A--lJ.U:,, p I Attached are the results of analysis of samples collected as part of the subject project. If you have any questions, please contact me. I I I I ATTACHMENT I I I I I I I Case Number: Site ID. I Date: I Affected Samples VOA I 4378,4379,4381- 4384,43 86-4394, 14399,4400 4378,4381-4385, 14387-4390,4399 4379 14380,4395,4396 4380,4385,4395, 14396 14380 • 4381,~384,4388, 389 -· 4385 I 11'385 lt386 4386 I I 30418 ORGANIC DATA QUALIFIER REPORT Project Number 02-0493 FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Compound or Fraction methyl acetate 1,2-dibromo-3-chloropropane I, 1-dichloroethane bromomethane, chloroethane I ,2-dibromo-3-chloropropane I, 1-dichloroethene, I, I -dichloroethane, cis-1,2- dichloroethene, trichloroethene, xylene(total) tetrachloroethene chloromethane, bromomethane, chloroethane, trichlorofluoromethane, I, I -dichloroethene, I, I ,2-trichloro-I ,2,2-trifluoroethane, acetone I, I -dichloroethene, I, I ,2-trichloro-I ,2,2- trifluoroethane, I, 1-dichloroethane, cis-1 ,2- dichloroethene, chloroform, trichloroethene carbon tetrachloride, trichloroethene cyclohexane, benzene, trichloroethene, methylcyclohexane, I ,2-dichloropropane, bromodichloromethane, cis-I ,3-dichloropropene, toluene, trans-I ,3-dichloropropene, I, 1,2- trichloroethane, ethylbenzene, xylene(total), styrene, isopropylbenzene, I, I ,2,2- tetrachloroethane, I ,2-dibromo-3-chloropropane Flag Used R J J J R J J J J J J SAS Number NIA Reason erratic initial & continuing calibration relative response factors erratic continuing calibration response factor < quantitation limit erratic continuing calibration response factor erratic initial & continuing calibration relative response factors < quantitation limit < quantitation limit erratic continuing calibration response factor < quantitation· limit < quantitation limit low deuterated monitoring compound recovery I I I I Case Number: Site ID. I Date: I Affected Samples 4386 I 4390 14391 4391,4393 14393 14393 14395 14400 14378,4384,4386 0 m 4378-4393 I I I I 30418 ORGANIC DATA QUALIFIER REPORT Project Number FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Compound or Fraction methylcyclohexane, l ,2-<libromo-3- chloropropane methylene chloride chloroform, tetrachloroethene I, 1,2,2-tetrachloroethane, 1,2-<libromo-3- chloropropane ethylbenzene xylene(total) I, 1-<lichloroethene, I, l ,2-trichloro-1,2,2- trifluoroethane, I, 1-<lichloroethane, cis-1,2- dichloroethene, chloroform, trichloroethene I, 1-<lichloroethane, bromochloromethane, chloroform, cis-1,3-<lichloropropene, I, 1,2- trichloroethane 2,4-<lichlorophenol, hexachlorobutadiene, caprolactam, 4-chloro-3-methylphenol, 2,4,6- trichlorophenol, 2,4,5-trichlorophenol, 1,1'- biphenyl, dimethylphthalate, diethylphthalate, 4,6-<linitro-2-methylphenol, 1,2,4,5- tetrachlorobenzene, pentachlorophenol, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate 02-0493 SAS Number NIA Flag Used J J J J J J J J J Reason erratic continuing calibration response factor contaminated storage blank < quantitation limit low deuterated monitoring compound recovery < quantitation limit warning high in low concentration PE sample < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery 3,3'-<lichlorobenzdine J erratic continuing calibration response factor I I I I Case Number: Site ID. I Date: I Affected Samples 14379 I I 4381,4385 14382 I I 4387 14388 I "389 D I I ORGANIC DATA QUALIFIER REPORT Project 30418 Number 02-0493 FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Flag Compound or Fraction Used 2,4-dichlorophenol, hexachlorobutadiene, 4-J chloro-3-methylphenol, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 4,6-dinitro-2- methylphenol, 1,2,4,5-tetrachlorobenzene, pentachlorophenol, benzo(b )fluoranthene, benzo(k)fluoranthene, benzo( a)pyrene, indeno(l,2,3-cd)pyrene, dibenzo(a,h)anthracene, benzo(g,h,i)perylene caprolactam J 2,4-dichlorophenol, 4-chloro-3-methylphenol, J 1,1'-biphenyl, acenaphthylene, acenaphthene, 4,6- dinitro-2-methylphenol, hexachlorobenzene, atrazine, phenanthrene, anthracene, benzo(b )fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, indeno(l,2)-cd)pyrene, dibenzo( a,h)anthracene, benzo(g,h,i)perylene 4,6-dinitro-2-methylphenol J 2,4-dichlorophenol, hexachlorobutadiene, 4-J chloro-3-methylphenol, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 1,2,4,5-tetrachlorobenzene, pentachlorophenol 2-methylphenol, 4-methylphenol, 2,4-J dimethylphenol, 2,4-dichlorophenol, naphthalene, hexachlorobutadiene, caprolactam, 4-chloro-3- methylphenol, 2-methylnaphthalene, 2,4,6- trichlorophenol, 2,4,5-trichlorophenol, I, 1 '- biphenyl, 2-chloronaphthalene, dimethylphthalate, acenaphthylene, acenaphthene, diethylphtha!ate, 1,2,4,5- tetrachlorobenzene, pentachlorophenol, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate SAS Number NIA Reason low deuterated monitoring compound recovery < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery low deuterated monitoring compound recovery low deuterated monitoring compound recovery I I I I Case Number: Site ID. I Date: I Affected Samples 4389 14390 I 4390 I 14391 I 4393 '4393 ~ -_ t394 I ll'EST 4378-4394,4397, lf398,440! 4378,4379 I 30418 ORGANIC DATA QUALIFIER REPORT Project Number 02-0493 SAS Number NIA FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Flag Compound or Fraction Used acetophenone J caprolactam, 1,1'-biphenyl, dimethylphthalate, J diethylphthalate, 4,6-dinitro-2-methylphenol, di- n-butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate, atrazine J . 4,6-dinitro-2-methylphenol, J benzo(b )fl uoranthene, benzo(k)fluoranthene, benzo(a)pyrene, indeno( I ,2,3-cd)pyrene, dibenzo(a,h)anthracene, benzo(g,h,i)perylene 2-nitroaniline, 3-nitroaniline, 2,4-dinitrophenol, J 4-nitrophenol, 4-nitroarriline, 4,6-dinitro-2- methylphenol benzaldehyde J 2-methylphenol, 4-methylphenol, 2,4-J dimethylphenol naphthalene, caprolactam, 2-methylnaphthalene, J I, 1 '-biphenyl, 2-chloronaphthalene, dimethylphthalate, acenaphthylene, acenaphthene, diethylphthalate, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate caprolactam, atrazine, 3,3'-dichlorobenzidine J methoxychlor J beta-BHC J Reason < quantitation limit low deuterated monitoring compound recovery < quantitation limit, erratic initial calibration response factor low deuterated monitoring compound recovery low deuterated monitoring compound recovery < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery erratic continuing calibration response factor erratic initial calibration response factor < quantitation limit I I I I I I I I I I I I I I I I I Case Number: Site ID. Date: Affected Samples 4379,4391 4381 4384 4392 4397 4401 I 30418 ORGANIC DATA QUALIFIER REPORT Project Number FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Compound or Fraction heptachlor epoxide all compounds endrin ketone gamma-BHC heptachlor epoxide, dieldrin, methoxychlor alpha-BHC, dieldrin 02-0493 SAS Number NIA Flag Used Reason N difference in columns J low surrogate recovery N difference in columns J < quantitation limit N difference in columns N difference in columns mple 4378 FY 2002 Project: 02-0493 ,LATILES SCAN :ility: FCX, Inc. (Statesville Plant) ,gram;.SF Statesville, NC 3tation: MW24 I dia: GROUNDWATER Case No: 30418 MD No: 19T1 D No: 19T1 lnorg Contractor: LIBRTY Org Contractor: A4 SUL TS .sou .sou .sou .sou .sou .sou .sou .sou S.OU .sou .SOUR .sou .SOU .sou .sou 1.3 .sou .sou .sou .sou .sou .sou .68 2.3 .sou .sou .sou .sou S.OU .sou .sou .sou 5.1 S.OU .sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS . O.SOU o.sou o.sou O.SOU o.sou o.sou O.SOU o.sou o.sou O.SOU o.sou O.SOUJ o.sou Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 12:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDS) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE· BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE e value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptlve evidence ot presence of material. ll'alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling and reanalysls is necessary for verification. Page 1 of 1 Tlt.a;AM11!!!!9ANtllll1S == liiill 1mple 4378 FY 2002 Project: 02-0493 SCELLANEOUS COMPOUNDS 1cility: FCX, Inc. (Statesville Plant) ogram;. SF 'Station: MW24 I 3dia:GROUNDWATER Statesville, NC Case No: 30418 MD No: 19T1 D No: 19T1 :SUL TS l.SOU l.SOU l.60J UNITS UG/L UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 REPORTED AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED OCHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES 1ge value. NA•not analyzed. NAl•interferences. J-estlmated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project leader: KMALLARY Beginning: 04123/2002 12:00 Ending: ti value is known to be less than value given, L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ::Hcates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 Tiple 4379 FY 2002 Project: 02-0493 LATILES SCAN ;ility:. FCX, Inc. (Statesville Plant) ,grani:--SF Statesville, NC Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 Ending: ,tation: DUP01 / dia: GROUNDWATER Case No: 30418 MD No: 19T2 D No: 19T2 lnorg Contractor: LI BRTY Org Contractor: A4 iULTS .sou .SOU .sou .sou .sou .SOU .sou .sou 5.0U . sou .SOUR .sou .sou .sou .23J 1.6 5.0U .sou .sou .sou .sou .sou .sou 2.7 .sou sou sou .sou 5.0U sou sou sou 5.8 5.0U sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/l UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE . METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE . 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS UNITS a.sou uGtL 0.SOU UG/L a.sou UG/L 0.SOU UG/L a.sou UG/L 0.50U UG/L 0.SOU UG/L 0.50U UG/L O.SOU UG/L 0.SOU UG/L O.SOU UG/L 0.SOU UG/L 0.SOU UG/L e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive eVidence of presence of material. ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE ,alue is known to be less than value given. L-actual value is known to be greater than yalue given. U-material was analyzed for but not detected. the numbef is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling and reanalysis is necessaiy for verification. Page 1 of 1 1111!!!1 mple 4379 FY 2002 Project: 02-0493 SCELLANEOUS COMPOUNDS cility: FCX, Inc. (Statesville Plant) igramc SF Station: DUP01 / ,dia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19T2 D No: 19T2 SULTS UNITS •.SOU UG/L •.SOU UG/L I.S1J UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 tEPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED lCHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES -liill -lilll -.. Production Date: 06/03/2002 07:49 Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 Ending: 1e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quanlitation limit. icates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification. Page 1 of 1 11ple 4380 FY 2002 Project: 02-0493 LATILES SCAN :ility: FCX, Inc. (Slatesville Plant) ,gram:-SF Statesville, NC 3tation: MW5D I dia: GROUNDWATER Case No: 30418 MD No: 19T4 DNo:19T4 lnorg Contractor: LIBRTY Org Contractor: CEIMIC SULTS UNITS 10U UGIL 10U UGIL 10U UGIL 10UJ UGIL 10UJ UG/L 10U UGIL 5J UGIL 10U UGIL 10U UGIL 10U UG/L 10U UGIL 10U UG/L 10U UGIL 10U UG/L 6J UG/L 9J UG/L 10U UGIL 10U UGIL 10U UG/L 10U UGIL 10U UGIL 10U UG/L 10U UGIL 5J UG/L 10U UG/L 10U UGIL 10U UG/L 10U UGIL 10U UGIL 10U UGIL 10U UG/L 10U UGIL . 39 UGIL 10U UG/L 10U UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 10U 10U 10U 4J 10U 10U 10U 10U 10U 10U 10U 10UR 10U Je value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. liiil-----Product1on Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/2312002 16:30 Ending: UNITS UG/L UG/L UG/L UGIL UGIL UG/L UG/L UGIL UGIL UGIL UGIL UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed tor but not detected. the number is the minimum quantitation limit. iicate& that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 .. nple 4381 FY 2002 Project: 02-0493 LATILES SCAN :ility: FCX, Inc. (Statesville Plant) ,gram:. SF Statesville, NC ,talion: MW11 / dia: GROUNDWATER Case No: 30418 MD No: 19TS D No: 19TS lnorg Contractor: LIBRTY Org Contractor: A4 SULTS .SOU .sou .sou .sou .SOU .sou .sou .sou S.OU .sou .SOUR .SOU .SOU .sou .sou .sou S.OU .sou .SOU •.SOU ,.sou ,.sou •.SOU •.SOU ,.sou ,.sou I.SOU I.SOU S.OU I.SOU ,.sou ,.sou l.34J S.OU ,.sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE . CARBON DISULFIDE· METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS o.sou 0.SOU o.sou o.sou o.sou o.sou o.sou O.SOU 0.50U 0.SOU o.sou 0.SOUJ o.sou ~e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. ------Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 16:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDS) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known lo be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 iiiiil nple 4381 FY 2002 Project: 02-0493 iCELLANEOUS COMPOUNDS :ilily:. FCX, Inc. (Statesville Plant) grarri:,,SF Hation: MW11 / jia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19TS D No: 19TS lULTS sou sou UNITS UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE lnorg Contractor: LIBRTY Org Contractor: A4 1CHLOROMETHANE AND 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES e value. NA-not analyZed. NAl-interfere.nces. J-estimated value. N-presumptive evidence of presence of material. iiiillial ___ _ Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 16:00 Ending: value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. cates that data unusable: compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 liiiil nple 4382 FY 2002 Project: 02-0493 LATILES SCAN :ility: FCX, Inc. (Statesville Plant) grani~-SF Statesville, NC aation: MW27S / fa: GROUNDWATER Case No: 30418 MD No: 19T6 D No: 19T6 lnorg Contractor: LIBRTY Org Contractor: A4 lULTS sou .SOU .SOU .SOU .SOU .sou .SOU .SOU S.OU .SOU .SOUR .SOU .SOU .sou .sou .sou S.OU .SOU .SOU .sou .sou .sou .sou .sou .sou .sou .sou .sou S.OU :SOU .sou •.SOU 1.1 S.OU ,.sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE. METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS a.sou a.sou 0.S0U a.sou a.sou O.SOU a.sou a.sou a.sou O.SOU a.sou O.S0UJ a.sou Je value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 1 S:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDS) CHLOROBENZENE ETHYL BENZENE TOT AL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the mlnirtlum quantitation limit. lcates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 nple 4382 FY 2002 Project: 02-0493 !CELLANEOUS COMPOUNDS :ility: FCX, Inc. (Statesville Plant) ,gram:. SF ,talion: MW27S / dia:GROUNDWATER Statesville, NC Case No: 30418 MD No: 19T6 D No: 19T6 ,ULTS .sou .sou UNITS UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE lnorg Contractor: LIBRTY Org Contractor: A4 )CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES liiill Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 1 S:00 Ending: JB value. NA-not analyzed. NAl-interterences. J-estlmated value. N-presumptive evidence of presence of material. value is known to be less th3n value given. L-aciual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ,icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 liiiil ople 4383 FY 2002 Project: 02-0493 _ATILES SCAN ility: FCX, Inc. (Statesville Plant) grarri>-SF Statesville, NC ,tation: MW8 / Jia:GROUNDWATER Case No: 30418 MD No: 19T7 D No: 19T7 lnorg Contractor: LIBRTY Org Contractor: A4 ,ULTS sou sou sou sou sou sou sou sou i.OU sou SOUR sou sou sou sou sou ;.au sou sou sou sou .sou .sou .sou sou .sou .sou .sou 5.0U .sou .sou .sou .sou 5.0U .sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L. UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1,1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE. METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-0\CHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1,1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-0\CHLOROPROPENE 1, 1,2-TR\CHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS a.sou a.sou a.sou a.sou a.sou a.sou a.sou a.sou a.sou 0.SOU O.SOU O.SOUJ 0.SOU e value. NA•not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 17:40 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE . 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value ls known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quanutation limit. cates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification. Page 1 of 1 11111 iilil nple 4383 FY 2002 Project: 02-0493 lCELLANEOUS COMPOUNDS :ility:. FCX, Inc. (Statesville Plant) grams.SF ,talion: MW8 I dia:GROUNDWATER. Statesville, NC Case No: 30418 MD No: 19T7 D No: 19T7 lULTS .sou .sou UNITS UGIL UGIL ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE lnorg Contractor: LIBRTY Org Contractor: A4 lCHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES ie value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. liiil iiiil-----Product1on Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04123/2002 17:40 Ending: value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable, compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 liiiiiii E~E-V s11! AT., G,--llilll liiliil liiil -.. -Production Date: 06/03/2002 07:49 nple 4384 FY 2002 Project: 02-0493 LATILES SCAN :ility:. FCX, Inc. (Statesville Plant) 1grami .. SF Statesville, NC Produced by: Mcconney, John Requester: ,talion: MWSS / dia: GROUNDWATER Case No: 30418 MD No: 19WO D No: 19WO lnorg Contractor: LIBRTY Org Contractor: A4 Project Leader: KMALLARY Beginning: 04/23/2002 1 S:00 Ending: SULTS .sou .sou .sou .sou .sou .sou .SOU .SOU S.OU . SOU .SOUR .sou .sou .sou •.SOU ,.sou S.OU •.SOU ·.SOU •.SOU ,.sou ,.sou ,.sou ,.sou ,.sou •.SOU ,.sou I.SOU S.OU ,.sou I.SOU ,.sou l.40J S.OU I.SOU UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE . METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1,1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS UNITS a.sou UG/L a.sou UG/L a.sou UG/L a.sou UG/L a.sou UG/L a.sou UG/L a.sou UG/L a.sou UG/L O.SOU UG/L a.sou uGJL a.sou UG/L O.SOUJ UG/L 0.50U UG/L ~e value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptlve evidence of presence of material. ANALYTE 1,2-DIBROMOETHANE (EDS) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 liiiiil nple 4384 FY 2002 Project: 02-0493 ,CELLANEOUS COMPOUNDS ility:_ FCX, Inc. (Statesville Plant) grarri:-.SF ;talion: MW5S / jia: GROUNOWATER Statesville, NC Case No: 30418 MD No: 19W0 D No: 19WO lULTS 50U 50U l.5J UNITS UG/L UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 •CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES EPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. iiiiiil ------Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: value is known to be less than value given. L-actual value is known lo be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. cates that data unusable. compound may or may not be present. resampling and reanalysis is necessar; for verification. Page 1 of 1 nple 4385 FY 2002 Project: 02-0493 -A Tl LES SCAN ility:. FCX, Inc. (Statesville Plant) gram:_ SF Statesville, NC :tation: MW29 / Jia: GROUNDWATER Case No: 30418 MD No: 19W6 D No: 19W6 lnorg Contractor: LIBRTY Org Contractor: CEIMIC iULTS 10U 10UJ 10U 10UJ 10UJ 10UJ 4J 2J 10UJ 10U 10U 10U 10U 10U SJ 9J 10U 1J 10U 10U 10U 10U 10U 6J 10U 10U 10U 10U 10U 10U 10U 10U 47 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1,1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10UR 10U e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. ------liiil Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 17:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE ,alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 nple 4386 FY 2002 Project: 02-0493 LATILES SCAN :ility:. FCX, Inc. (Statesville Plant) grani:-SF Statesville, NC Hation: IN01 I dia: GROUNDWATER Case No: 30418 MD No: 19X1 D No: 19X1 lnorg Contractor: LIBRTY Org Contractor: A4 ,ULTS sou .sou .SOU .SOU .sou .SOU 3.2 22 S.0U .sou .SOUR .sou .sou .SOU 6.1 21 S.0J 3.1 1,81 ,.S0UJ l.37J 1.SQUJ ,.sou 3.9J I.SQUJ l,S0UJ I.S0UJ I.S0UJ S.0U I.S0UJ I.S0UJ i.S0UJ 130 S.0U I.SOU UNITS UGIL UG/L UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UG/L UG/L UG/L UGIL UG/L UGIL UG/L UGIL UGIL UG/L UGIL UGIL UGIL UG/L UGIL UGIL UGIL UGIL UGIL UGIL UG/L UG/L UGIL ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS a.sou a.sou 0.S0UJ 0.S0UJ 0.S0UJ a.sou 0.S0UJ 0.S0UJ a.sou a.sou a.sou 0.S0UJ a.sou ;e value. NA-not analyzed. NAl-lnterferences. J-estlmaled value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/2412002 1 S:30 Ending: UNITS UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UG/L UGIL UGIL UG/L UGIL ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE l value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitatlon limit. licates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,,pie 4386 FY 2002 Project: 02-0493 ;CELLANEOUS COMPOUNDS ility:_ FCX, Inc. (Statesville Plant) grani:-.SF ;talion: IN01 I Jia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19X1 D No: 19X1 iULTS 50U 50U 19J UNITS UGIL UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZNE 2 UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 >CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES tEPORTEO AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED ie value. NA-not analyzed. NAHnterferences. J-estimated value. N-presumptlve evidence of presence of material. llllilil ~duct1oh Date: os!fflooffl:49ai Produced by: McConney, John · Requester: Project Leader: KMALLARY Beginning: 0412412002 15:30 Ending: value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 IL~MP~AL'9i liiil - 1ple 4387 FY 2002 Project: 02-0493 .ATILES SCAN lity:_ FCX, Inc: (Statesville Plant) irani:-.SF Statesville, NC tation: EB01 I lia:GROUNDWATER Case No: 30418 MD No: 19T9 D No: 19T9 lnorg Contractor: LIBRTY Org Contractor: A4 ULTS 50U sou sou sou sou sou sou sou i.0U sou SOUR sou sou sou sou sou i.0U sou sou sou sou sou sou sou 50U 50U 50U 50U i.0U 1.4 sou sou 50U i.0U 50U UNITS UGIL UGIL UG/L UGIL UG/L UGIL UGIL UGIL UGIL UGIL UG/L UG/L UGIL UGIL UGIL UG/L UGIL UGIL UG/L UGIL UG/L UG/L UG/L UGIL UGIL UG/L UGIL UG/L UGIL UGIL UG/L UGIL UG/L UGIL UGIL ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE . METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 0.S0U 0.50U 0.50U 0.50U 0.50U 0.50U 0.50U 0.50U 0.S0U 0.50U 0.50U 0.50UJ 0.50U , value. NA-not analyzed. NAl-interferences. J-estimated value, N-presumptive evidence of presence of material. Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 0412412002 09:00 Ending: UNITS UGIL UG/L UGIL UG/L UG/L UG/L UG/L UG/L UGIL UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE ,alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 1111 nple 4387 FY 2002 Project: 02-0493 ,CELLANEOUS COMPOUNDS ;ility: FCX, Inc. (Statesville Plant) ,grams SF 3tation: EB01 / dia:GROUNDWATER Statesville, NC Case No: 30418 MD No: 19T9 D No: 19T9 SULTS .sou .SOU 3.5J UNITS UG/L UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 )CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES iEPORTED AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED Je value. NA-not analyzed. NAl-interferences. J-eslimated value. N-presumptive evidence of presence of material. liiil Produced by: Mcconney, John Requestor: • Project Leader: KMALLARY Beginning: 04/24/2002 09:00 Ending: : value is known to be less than value given. L-actual value is known to be greater thar1 value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. licates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 nple 4388 FY 2002 Project: 02-0493 ..A TILES SCAN ility: FCX, Inc. (Statesville Plant) gram:-.SF Statesville, NC ;talion: DUP02 / jia:GROUNDWATER Case No: 30418 MD No: 19W2 D No: 19W2 lnorg Contractor: LIBRTY Org Contractor: A4 iULTS sou sou sou sou sou sou 65 sou 49 sou SOUR .SOU .SOU sou sou 7.6 5.0U .SOU .SOU .sou .sou .SOU .SOU .SOU .SOU .SOU .SOU .SOU s.ou .SOU .SOU .SOU .37J 5.0U .sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UG/L UG/L UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UGIL UGIL ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1,1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS a.sou a.sou o.sou a.sou a.sou O.SOU 0.SOU a.sou o.sou O.SOU o.sou O.SOUJ a.sou 1e value. NA-not analyzed. NAl-lnterferences. J.estimated value. N-presumptive evidence of presence of material. ---.. --·-Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDS) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. cates that data unusable. compound may or may not be present. resampling and reanalysis ts. necessary for verification. Page 1 of 1 liiiil nple 4388 FY 2002 Project: 02-0493 ;CELLANEOUS COMPOUNDS :ility: FCX, Inc. (Statesville Plant) gram:, SF itation: DUP02 / dia:GROUNDWATER Statesville, NC Case No: 30418 MD No: 19W2 D No: 19W2 ,ULTS .sou .sou 30J UNITS UG/L UGIL UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 )CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES lEPORTED AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED ~e value. NA•not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material. liiiJ Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 Ending: value is known to be less then value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. licates that data unusable. compound may or may not be present. resampling and teanalysis is necessary for verification. Page 1 of 1 1ple 4389 FY 2002 Project: 02-0493 _ATILES SCAN ility:. FCX, Inc. (Statesville Plant) irani:,SF Statesville, NC talion: MW6D / lia:GROUNDWATER Case No: 30418 MD No: 19W1 D No: 19W1 lnorg Contractor: LIBRTY Org Contractor: A4 iULTS UNITS SOU UG/L SOU UG/L 50U UG/L 50U UG/L 50U UG/L 50U UG/L 58 UG/L 50U UG/L 38 UG/L 50U UG/L SOUR UG/L SOU UG/L SOU UG/L SOU UG/L SOU UG/L '.6 UG/L i.OU UG/L SOU UG/L SOU UG/L SOU UG/L 50U UG/L SOU UG/L SOU UG/L SOU UG/L SOU UG/L · SOU UG/L SOU UG/L SOU UG/L 5.0U UG/L SOU UG/L SOU UG/L SOU UG/L 28J UG/L 5.0U UG/L SOU UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE . METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE . DIBROMOCHLOROMETHANE RESULTS 0.SOU 0.50U 0.50U O.SOU 0.SOU 0.50U 0.SOU O.SOU O.SOU 0.SOU O.SOU O.SOUJ 0.SOU e value. NA-not analyzed. NAl-interferences. J..estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 12:09 Ending: UNITS UG/L UG/L UG/L UGiL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. Cates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 -pie 4389 FY 2002 Project: 02-0493 :ELLANEOUS COMPOUNDS lity: . FCX, Inc. (Statesville Plant) iram' -SF ation: MW6D / ia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19W1 D No: 19W1 ULTS UNITS ;au UG/L ;au UG/L ,5J UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES :PORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED , value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 12:09 Ending: ,alue is known to be less·than value given. L-actual value is known to be greater than value given, U-material was analyzed for but not detected. the number is the mini~um quantitation limit. :ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 lliil iple 4390 FY 2002 Project: 02-0493 .A TILES SCAN ility: FCX, Inc. (Statesville Plant) Jram:-SF Statesville, NC talion: MW6S / lia: GROUNDWATER Case No: 30418 MD No: 19W3 D No: 19W3 lnorg Contractor: LIBRTY Org Contractor: A4 ,ULTS sou sou 50U 50U 50U 50U 50U 50U i.OU 50U 50UR 71J 50U 50U 50U 50U 5.0U .50U .sou .sou .50U .50U .sou .sou .sou .50U .50U .50U S.OU .sou .sou .sou .sou 5.0U .50U UNITS UG/L UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE. METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1,1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 0.50U a.sou 0.50U a.sou 0.50U a.sou O.SOU a.sou a.sou a.sou a.sou 0.50UJ O.SOU Je value. NA.not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/2412002 10:00 Ending: UNITS UGIL UG/L UG/L UG/L UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value Is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitatlon limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 L~M P iWNAL-.. pie 4390 FY 2002 Project: 02-0493 :ELLANEOUS COMPOUNDS lily:. FCX, Inc. (Statesville Plant) 1rani:,SF :ation: MW6S / ia:GROUNDWATER Statesville, NC Case No: 30418 MD No: 19W3 D No: 19W3 ULTS UNITS ;ou UG/L ;ou UG/L \OJ UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES ::PORTED AS IDENTIFIED BY CLP LAB . IDS NOT VERIFIED :t value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. -Produced by: McConney, John . Requester: Project Leader: KMALLARY Beginning: 04/24/2002 10:00 Ending: ,atue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ;ates that data unusable. compound may or may not be present. resampling and re~nalysis is necessary for verification. Page 1 of 1 1ple 4391 FY 2002 Project: 02-0493 .ATILES SCAN ility:. FCX, Inc. (Statesville Plant) iram,. SF Statesville, NC talion: MW2S / lia: GROUNDWATER Case No: 30418 MD No: 19X2 D No: 19X2 lnorg Contractor: LIBRTY Org Contractor: A4 ;ULTS sou sou sou sou sou sou sou sou ;.ou sou SOUR sou sou sou sou sou ;.OU 42J sou .SOU .SOU .SOU .SOU .sou .sou .sou .SOU .SOU S.OU .sou .SOU .sou .30J S.OU .SOU UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1,1,1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE(TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 0.50U O.SOU 0,50U 0.SOU 0.SOU 0.SOU O.SOU 0.SOUJ 0.SOU O.SOU 0.SOU O.SOUJ 0.SOU 1e value. NA-not analyzed. NAl-inlerferences. J-estimated value. N-presumptive evidence of presence of material. -~ducflo~ Date: os!fflooffl:49W · liiil Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 16:30 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given, l-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,pie 4391 FY 2002 Project: 02-0493 CELLANEOUS COMPOUNDS ility:. FCX, Inc. (Statesville Plant) irarri:,,SF talion: MW25 / lia:GROUNDWATER Statesville, NC Case No: 30418 MD No: 19X2 D No: 19X2 iULTS 50U 50U UNITS UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE I norg Contractor: LI BRTY Org .Contractor: A4 tCHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES 1e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. -·-·-· ---Production Date: 06/W2002 07:49 Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 16:30 Ending: value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. cates that data unusable. compound may or may not be present. resampling and reanalysls is necessary for verification. Page 1 of 1 nple 4392 FY 2002 Project: 02-0493 LATILES SCAN ,ility:. FCX, Inc. (Statesville Plant) gram:. SF Statesville, NC aation: MW7 / jia: GROUNOWATER Case No: 30418 MD No: 19WS D No: 19WS lnorg Contractor: LIBRTY Org Contractor: A4 iULTS sou sou .sou .SOU. .SOU .sou .SOU .sou S.OU .sou .SOUR .sou .sou .sou .sou .sou S.OU .sou .sou .SOU .SOU .sou .sou ·.SOU ,.sou ,.sou . ,.sou ,.sou S.OU ,.sou ,.sou ,.sou I.SOU S.OU I.SOU UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L. UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1,1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1,1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS a.sou 0.SOU a.sou a.sou O.SOU a.sou a.sou 0.50U a.sou a.sou a.sou 0.50U a.sou ~e value. NA-not analyzed. NAl-lnterferences. J..estlmated value. N-presumptive evidence of presence of material. ------Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 14:30 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDS) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given. L-actual value is known to be greater than value given. U-materia1 was analyzed for but not detected. the number is the minimum quantitation limit. licates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 liliJ >le 4392 FY 2002 Project: 02-0493 :ELLANEOUS COMPOUNDS ty: . FCX, Inc. (Statesville Plant) ·am' --SF Statesville, NC Case No: 30418 MD No: 19W5 D No: 19W5 1tion:MW7 / a: GROUNDWATER JLTS OU OU 6J 4JN 5JN 8JN 2JN UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE 22 UNKNOWN COMPOUNDS 1 H-INDENE, 2,3-DIHYDRO-1, 1,3 BENZENE, (1,3-DIMETHYL-2-BUT NAPHTHALENE, 1,2,3.4-TETRAHY NAPHTHALENE, 1-METHYL- lnorg Contractor: LIBRTY Org Contractor: A4 :HLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES :PORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 14:30 Ending: 1 value. NA-not analyzed. NAl-interferences. J--estimated value. N-presumptive evidence of presence of material. . ·alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit :ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 -.. - - ~ES SAMPLE ANALYSIS ------EPA -REGION IV SESD, ATHENS, GA 1111 -.. -.. --Production Date: 06/03/2002 07:49 ,le 4393 FY 2002 Project: 02-0493 ._TILES SCAN ity: FCX, Inc. (Statesville Plant) ram:--SF Statesville, NC alien: FB01 / a: GROUNDWATER Case No: 30418 MD No: 19X3 D No: 19X3 lnorg Contractor: LIBRTY Org Contractor: A4 JLTS OU OU OU ,OU :ou :ou :ou :au .OU :ou ,OUR :ou i0U i0U :ou i0U .OU iOU iOU iOU iOU i0U iOU i0U 50U 50U 50U 50U :.ou .9 50U sou sou :.au sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE . METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 0.50U 0.50U 0.15J 0.76J 0.50U 0.50U 0.50U 0.50UJ 0.50U 0.50U 0.50U 0.50UJ 0.50U , value, NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:15 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENE$ STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE .1,2-DICHLOROBENZENE 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE 1alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ;ates that data unusable. compound may or may not be present. resampHng and reanalysis is necessary for verification. Page 1 of 1 liliJ -1ple 4393 FY 2002 Project: 02-0493 CELLANEOUS COMPOUNDS ilitv.: FCX, Inc. (Statesville Plant) ,rams SF ,tation: FB01 / Jia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19X3 D No: 19X3 ;uL TS sou sou l.4J UNITS UG/L UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZNE UNKNOWN COMPOUND lnorg Contractor: LIBRTY Org Contractor: A4 )CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES lEPORTED AS IDENTIFIED BY CLP LAB • IDS NOT VERIFIED 1e value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material. ----.. -·-Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 1 S:1 S Ending: value is known to be less than value given. l-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. lcates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 pie 4394 FY 2002 Project: 02-0493 ATILES SCAN ity:. FCX, Inc. (Statesville Plant) rani:--SF Statesville, NC ation: PB01 / a: GROUNDWATER Case No: 30418 MD No: 19X4 D No: 19X4 lnorg Contractor: LIBRTY Org Contractor: A4 JLTS ,OU ,OU ,OU i0U i0U i0U i0U i0U .OU i0U i0UR ;ou ;ou ;ou i0U i0U .OU ;ou ;ou ;ou ;ou ;ou ;ou 50U 50U 50U sou sou i.0U .7 sou sou sou i.0U sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L · UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE . METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 0.50U 0.S0U a.sou 0.50U 0.S0U o.sou 0.S0U o.sou 0.50U 0.50U a.sou 0.S0U a.sou e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 1S:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE ,alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 --,le 4394 FY 2002 Project: 02-0493 :ELLANEOUS COMPOUNDS ity:. FCX, Inc. (Statesville Plant) ram:,,SF ation: PB01 / a: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19X4 D No: 19X4 JLTS UNITS OU UG/L OU UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE lnorg Contractor: LIBRTY Org Contractor: A4 :HLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES 1 value. NA•not analyzed. NAl-interferences. J--estlmated value. N-presumptive evidence of presence of material. .. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:00 Ending: ·alue is known to be less than value given. L-actual value is kr'lown to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling and re.analysis is necessary for verification. Page 1 of 1 1ple 4395 FY 2002 Project: 02-0493 ..ATILES SCAN ility: FCX, Inc. (Statesville Plant) gram~ SF ,tation: DUP03 / Statesville, NC Case No: 30418 Jia: GROUNDWATER D No: 19W7 Org Contractor: CEIMIC ,ULTS 10U 10U 10U 10UJ 10UJ 10U 4J 3J 10U 10U 10U 10U 10U 10U SJ BJ 10U 1J 10U 10U 10U 10U 10U 6J 10U 10U 10U 10U 10U 10U 10U 10U 49 10U 10U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE . CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 10U ,au 10U ,au ,au 10U 10U 10U ,au ,au 10U 10UR 10U Je value. NA•not analyzed, NAl•interferences. J-eslimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 Ending: UNITS UG/L UG/L UG/e UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,pie 4396 FY 2002 Project: 02-0493 .ATILES SCAN lily: FCX, Inc. (Statesville Plant) Iramc SF Statesville, NC Case No: 30418 lation: TB02 I iia:GROUNDWATER D No: 19W8 Org Contractor: CEIMIC ULTS IOU IOU IOU \OUJ \OUJ IOU IOU ,ou 10U 10U 10U 10U ,ou 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U UNITS UG/L UG/L UGIL UGIL UGIL UGIL UGIL UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UGIL . UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1,1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE . 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10U 10UR 10U e value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 17:30 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENE$ STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitatlon limit. eates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,pie 4399 FY 2002 Project: 02-0493 .ATILES SCAN lily: FCX, Inc. (Statesville Plant) 1ramc SF Statesville, NC Case No: 30418 talion: TB01 / lia: TRIP BLANK -WATER D No: 19W4 Org Contractor: A4 ULTS ;au ;au ;au sou sou sou sou sou i.OU sou SOUR sou sou sou sou sou ;.au sou sou sou sou sou .sou .sou .sou .sou .SOU .SOU 5.0U .SOU .sou .sou .sou S.OU .sou UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLOR0-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2-DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) METHYL BUTYL KETONE DIBROMOCHLOROMETHANE RESULTS a.sou a.sou a.sou a.sou a.sou a.sou a.sou a.sou a.sou a.sou a.sou O.SOUJ a.sou Je value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 1S:1S Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROM0-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 1ple 4399 FY 2002 Project: CELLANEOUS COMPOUNDS ility: FCX, Inc. (Statesville Plant) iram; SF talion: TB01 / lia:TRIP BLANK· WATER 02-0493 Statesville, NC Case No: 30418 D No: 19W4 ;ULTS sou sou UNITS UG/L UG/L ANALYTE BROMOCHLOROMETHANE 1,2,3-TRICHLOROBENZENE Org Contractor: A4 lCHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES Je value. NA-not analyzed. NAl-interferences. J--estlmated value. N-presumptive evidence of presence of material. --.. - ---·-Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 1S:1S Ending: value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,pie 4400 FY 2002 Project: 02-0493 .A TILES SCAN ility: FCX, Inc. (Statesville Plant) iram~ SF Statesville, NC Case No: 30418 talion: TB03 / lia:TRIP BLANK· WATER D No: 19W9 Org Contractor: A4 ,ULTS 50U 50U 50U 50U 50U 50U 50U 50U ;.OU 50U 50UR 50U 50U 50U 50UJ 50U ;.ou .50UJ .50U .50U .50U .50U .50U .50U .50U .50U .50U .50UJ 5.0U .50U .50UJ .50UJ .50U 5.0U .50U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DICHLORODIFLUOROMETHANE CHLOROMETHANE VINYL CHLORIDE BROMOMETHANE CHLOROETHANE TRICHLOROFLUOROMETHANE (FREON 11) 1, 1-DICHLOROETHENE (1, 1-DICHLOROETHYLENE) 1, 1,2-TRICHLORO-1,2,2-TRIFLUOROETHANE (FREON 113) ACETONE CARBON DISULFIDE METHYL ACETATE METHYLENE CHLORIDE TRANS-1,2-DICHLOROETHENE METHYL T-BUTYL ETHER (MTBE) 1, 1-DICHLOROETHANE CIS-1,2-DICHLOROETHENE METHYL ETHYL KETONE CHLOROFORM 1, 1, 1-TRICHLOROETHANE CYCLOHEXANE CARBON TETRACHLORIDE BENZENE 1,2,DICHLOROETHANE TRICHLOROETHENE (TRICHLOROETHYLENE) METHYLCYCLOHEXANE 1,2-DICHLOROPROPANE BROMODICHLOROMETHANE CIS-1,3-DICHLOROPROPENE METHYL ISOBUTYL KETONE TOLUENE TRANS-1,3-DICHLOROPROPENE 1, 1,2-TRICHLOROETHANE TETRACHLOROETHENE (TETRACHLOROETHYLENE) .METHYL BUTYL KETONE DIBROMOCHLOROMETHANE Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 17:35 Ending: RES UL TS UNITS 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L 0.50U UG/L ANALYTE 1,2-DIBROMOETHANE (EDB) CHLOROBENZENE ETHYL BENZENE TOTAL XYLENES STYRENE BROMOFORM ISOPROPYLBENZENE 1, 1,2,2-TETRACHLOROETHANE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,2-DICHLOROBENZENE 1,2-DIBROMO-3-CHLOROPROPANE (DBCP) 1,2,4-TRICHLOROBENZENE Je value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification. · Page 1 of 1 -,pie 4400 FY 2002 Project: 02-0493 CELLANEOUS COMPOUNDS ility: FCX, Inc. (Statesville Plant} gram~ SF ;talion: TB03 / Jia:TRIP BLANK· WATER Statesville, NC Case No: 30418 D No: 19W9 iULTS sou sou l.6J UNITS UG/L UG/L UG/L ANALYTE BROMOCHLOROMETHANE c, 1,2,3-TRICHLOROBENZENE 4 UNKNOWN COMPOUNDS Org Contractor: A4 )CHLOROMETHANE & 1,2,3-TRICHLOROBENZENE ARE TARGET ANAL YTES !EPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED . Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 17:3S Ending: ~e value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. . value is known to be less than value given. L-actual value Is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. licates that data unusable. compound may or may not be present. resampling·and reanalysis is necessary for verification. Page 1 of 1 I I I I I I I I I I I :;,'-"£0 ST,1,-~,5' . ft . l~J .,. "It PR~C,. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 MEMORANDUM Date: 06/03/2002 Science and Ecosystem Support Division 980 College Station Road Athens, Georgia 30605-2720 Subject: Results of PESTICIDES/PCB Sample Analysis 02-0493 FCX, Inc. (Statesville Plant) Statesville, NC From: Mcconney, John To: Mallary, Ken CC: Ralph McKeen RACS/W Thru: QA Office .Attached are the results of analysis of samples collected as part of the subject project. If you have any questions, please contact me. I I I .ATTACHMENT I I I I I I I Case Number: .1 Site ID. Date: I Affected Samples VOA I 4378,4379,4381- 4384,4386-4394, 14399,4400 4378,4381-4385, 14387-4390,4399 4379 14380,4395,4396 14380,4385,4395, 4396 t380 !14381,4~84,4388, IIB89 :- 14385 ,385 1386 4386 I I I ORGANIC DATA QUALIFIER REPORT 30418 Project Number 02-0493 . SAS Number NIA ------------ FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Flag Compound or Fraction Used methyl acetate R 1,2-dibromo-3-chloropropane J 1, 1-dichloroethane J bromomethane, chloroethane J 1,2-dibromo-3-chloropropane R 1, 1-dichloroethene, 1, 1-dicWoroethane, cis-1,2-J dichloroethene, trichloroethene, xylene(total) tetrachloroethene J chloromethane, bromomethane, cWoroethane, J trichlorofluoromethane, 1, 1-dicWoroethene, 1, l ,2-trichloro-1,2,2-trifluoroethane, acetone 1, 1-dichloroethene, 1, l ,2-trichloro-1,2,2-J trifluoroethane, 1, 1-dichloroethane, cis-1,2- dicWoroethene, chloroform, trichloroethene carbon tetrachloride, tricWoroethene J cyclohexane, benzene, trichloroethene, J methylcyclohexane, 1,2-dichloropropane, bromodicWoromethane, cis-1,3-dichloropropene, toluene, trans-1,3-dichloropropene, I, 1,2- trichloroethane, ethylbenzene, xylene(total), styrene, isopropylbenzene, l, 1,2,2- tetrachloroethane, 1,2-dibromo-3-chloropropane Reason erratic initial & continuing calibration relative response factors erratic continuing calibration response factor < quantitation limit erratic continuing calibration response factor erratic initial & continuing calibration relative response factors < quantitation•limit < quantitation limit erratic continuing calibration response factor < quantitation limit < quantitation limit low deuterated monitoring compound recovery I I I I Case Number: Site ID. I Date: I Affected Samples 4386 I 4390 14391 4391,4393 I 4393 14393 14395 ,378,4384,4386 I I 4378-4393 I I I 30418 ORGANIC DATA QUALIFIER REPORT Project Number FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Compound or Fraction methylcyclohexane, 1,2-dibromo-3- chloropropane methylene chloride chloroform, tetrachloroethene 1, 1,2,2-tetrachloroethane, 1,2-dibromo-3- chloropropane ethylbenzene xylene(total) 1, 1-dichloroethene, 1, l ,2-trichloro-1,2,2- trifluoroethane, 1, 1-dichloroethane, cis-1,2- dichloroethene, chloroform, trichloroethene 1, 1-dichloroethane, bromochloromethane, chloroform, cis-1,3-dichloropropene, 1, 1,2- trichloroethane 2,4-dichlorophenol, hexachlorobutadiene, caprolactam, 4-chloro-3-methylphenol, 2,4,6- trichlorophenol, 2,4,5-trichlorophenol, 1,1 '- biphenyl, dimethylphthalate, diethylphthalate, 4,6-dinitro-2-methylphenol, 1,2,4,5- tetrachlorobenzene, pentachlorophenol, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate 3,3'-dichlorobenzdine 02-0493 SAS Number NIA Flag Used J J J J J J J J J J Reason erratic continuing calibration response factor contaminated storage blank < quantitation limit low deuterated monitoring compound recovery < quantitation limit warning high in low concentration PE sample < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery erratic continuing calibration response factor I I I I Case Number: I Site ID. Date: I Affected Samples 14379 I 4381,4385 14382 I I 4387 I 4388 I 1389 I I I I I 30418 ORGANIC DATA QUALIFIER REPORT Project Number 02-0493 SAS Number NIA FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Flag Compound or Fraction Used 2,4-dichlorophenol, hexachlorobutadiene, 4-J chloro-3-methylphenol, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 4,6-dinitro-2- methylphenol, 1,2,4,5-tetrachlorobenzene, pentachlorophenol, benzo(b )fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, indeno( 1,2,3-cd)pyrene, dibenzo( a,h)anthracene, benzo(g,h,i)perylene caprolactam J 2,4-dichlorophenol, 4-chloro-3-methylphenol, . J I, 1'-biphenyl, acenaphthylene, acenaphthene, 4,6- dinitro-2-methylphenol, hexachlorobenzene, atrazine, phenanthrene, anthracene, benzo(b )fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, indeno(l,2,3-cd)pyrene, dibenzo( a,h )anthracene, benzo(g,h,i)perylene 4,6-dinitro-2-methylphenol J 2,4-dichlorophenol, hexachlorobutadiene, 4-J chloro-3-methylphenol, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 1,2,4,5-tetrachlorobenzene, pentachlorophenol 2-methylphenol, 4-methylphenol, 2,4-J dimethylphenol, 2,4-dichlorophenol, naphthalene, hexachlorobutadiene, caprolactam, 4-chloro-3- methylphenol, 2-methylnaphthalene, 2,4,6- trichlorophenol, 2,4,5-trichlorophenol, 1,1 '- biphenyl, 2-chloronaphthalene, dimethylphthalate, acenaphthylene, acenaphthene, diethylphthalate, 1,2,4,5- tetrachlorobenzene, pentach!orophenol, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate Reason low deuterated monitoring compound recovery < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery low deuterated monitoring compound recovery low deuterated monitoring compound recovery I I I I Case Number: I Site ID. Date: I Affected Samples 4389 I 4390 I I 4390 I 4391 I 4392 I 4393 14393 -:. 14394 I IPEST 4378-4394,4397, 14398,4401 4378,4379 I , 30418 ORGANIC DATA QUALIFIER REPORT- Project Number 02-0493 FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Compound or Fraction acetophenone caprolactam, I, 1 '-biphenyl, dimethylphthalate, diethylphthalate, 4,6-dinitro-2-methylphenol, di- n-butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate, atrazine 4,6-dinitro-2-methylphenol, benzo(b )fluoranthene, benzo(k)fluoranthene, benzo( a)pyrene, indeno( 1,2,3-cd)pyrene, dibenzo(a,h)anthracene, benzo(g,h,i)perylene 2-nitroaniline, 3-nitroaniline, 2,4-dinitrophenol, 4-nitrophenol, 4-nitroaniline, 4,6-dinitro-2- methylphenol benzaldehyde 2-methylphenol, 4-methylphenol, 2,4- dimethylphenol naphthalene, caprolactam, 2-methylnaphthalene, I, 1 '-biphenyl, 2-chloronaphthalene, dimethylphthalate, acenaphthylene, acenaphthene, diethylphthalate, di-n- butylphtha]ate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate caprolactam, atrazine, 3,3'-dichlorobenzidine methoxychlor beta-BHC Flag Used J J J J J J J J J J J SAS Number NIA Reason < quantitation limit low deuterated monitoring compound recovery < quantitation limit, erratic initial calibration response factor low deuterated monitoring compound recovery low deuterated monitoring compound recovery < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery erratic continuing calibration response factor erratic initial calibration response factor < quantitation limit I I I I Case Number: I Site ID. Date: I Affected Samples 14379,4391 4381 14384 4392 14397 4401 I I I I I I I I D I ORGANIC DATA QUALIFIER REPORT Project 304 I 8 Number 02-0493 SAS Number NIA FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Flag Compound or Fraction Used Reason heptachlor epoxide N difference in columns all compounds J low surrogate recovery endrin ketone N difference in columns gamma-BHC J < quantitation limit heptachlor epoxide, dieldrin, methoxychlor N difference in columns alpha-BHC, dieldrin N difference in columns 1ple 4378 FY 2002 Project: 02-0493 ,TICIDES SCAN ility: FCX, Inc. (Statesville Plant) Jram:-.SF Statesville, NC Case No: 30418 MD No: 19T1 tation: MW24 I lia: GROUNDWATER D No: 19T1 -ULTS IOU )BJ 10U 10U 10U 10U 39U 10U 20U 20U 20U 20U 20U 20U 20U 10UJ 20U 20U 10U 10U I.OU 20U 40U 20U 20U 20U 20U 20U UNITS UGIL UGIL UG/L UGIL UG/L UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UG/L UG/L UGIL UGIL UGIL UGIL UGIL UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4.4'-DDT (P,P'-DDD METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 a value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptlve evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 0412312002 12:00 Ending: 1alue is known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ;ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. 1ed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 ,pie 4379 FY 2002 Project: 02-0493 TICIDES SCAN lily: FCX, Inc. (Statesville Plant} Iram;,.SF Statesville, NC Case No: 30418 MD No: 19T2 talion: DUP01 / ia: GROUNDWATER D No: 19T2 ULTS IOU )9J IOU IOU IOU IOU 15N IOU !OU !OU !OU !OU wu· !OU !OU IOUJ 20U 20U 10U 10U .OU 20U 40U 20U 20U 20U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE} HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA} DIELDRIN 4,4'-DDE (P,P'-DDE} ENDRIN ENDOSULFAN II (BETA} 4,4'-DDD (P,P'-DDD} ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDl) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) · PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 , value. NA-not analyzed. NAl-interferences. J-estimaled value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 Ending: ·alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. ed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 ,le 4380 FY 2002 Project: 02-0493 rlCIDES SCAN ily:_ FCX, Inc. (Statesville Plant) ram~SF Statesville, NC Case No: 30418 MD No: 19T4 ation: MW5D / a: GROUNDWATER D No: 19T4 JLTS UNITS 0 UG/L 5 UG/L 8 UG/L 2 UG/L 2U UG/L OU UG/L OU UG/L OU UG/L OU UG/L :OU UG/L :au UG/L :au UG/L :au UG/L :au UG/L :au UG/L IOUJ UG/L !OU UG/L ?OU UG/L IOU UG/L IOU UG/L .OU UG/L WU UG/L IOU UG/L ?OU UG/L WU UG/L !OU UG/L WU UG/L WU UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: CEIMIC Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 16:30 Ending: , value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material. 1alue is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. :ates that data unusable. compound may or may not be present. resampling an9 reanalysis ls necessary for verification. 1ed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane ~age 1 of 1 -ample 4381 FY 2002 Project: 02-0493 ESTICIDES SCAN acility:. FCX, Inc. (Statesville Plant) rograms.SF Statesville, NC ;/Station: MW11 / edia:GROUNOWATER Case No: 30418 MD No: 19T5 D No: 19T5 cSULTS UNITS .010UJ UG/L .010UJ UG/L ·.010UJ UG/L •.010UJ UG/L •.010UJ UG/L 1.010UJ UG/L I.010J UG/L I.01 OUJ UG/L I.020UJ UG/L I.020UJ UG/L I.020UJ UG/L I.020UJ UG/L l.020UJ UG/L I.020UJ UG/L l.020UJ UG/L 0.10UJ UG/L 1.020UJ UG/L l.020UJ UG/L 1.010UJ UG/L l.010UJ UG/L 1.0UJ UG/L 0.20UJ UG/L 0.40UJ UG/L 0.20UJ UG/L 0.20UJ UG/L 0.20UJ UG/L 0.20UJ UG/L 0.20UJ UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4.4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4.4'-DDD (P.P'-DDD) ENDOSULFAN SULFATE 4.4'-DDT (P.P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 ·age value. NA-not analyzed. NAl-lnterferences. J.estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 16:00 Ending: al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantilation limit. 1dicates that data unusable. compound may or may not be present. resamp1ing and reanalysis Is necessary for verification. firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 -ample 4382 FY 2002 Project: 02-0493 ESTICIDES SCAN acility:. FCX, Inc. (Statesville Plant) rogram: .• SF Statesville, NC Case No: 30418 MD No: 19T6 I/Station: MW27S I ledia: GROUNDWATER D No: 19T6 ESULTS •.010U ,.01ou ,.o,ou I,010U l,010U l.010U l,010U l,010U l.020U l.020U l.020U l.020U l,020U l,020U I.020U 0.10UJ l.020U I.020U l.010U l.010U 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UGIL UG/L UGIL UGIL UG/L UGIL UG/L UGIL UG/L UG/L UGIL UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDl) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE 12 GAMMA-CHLORDANE 12 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 ·age value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: al value is known to be less than value given. L-aclual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. 1dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 ra.J:Sif9aAMIIIIIIIAN.talls -- ,ample 4383 FY 2002 Project: 02-0493 'ESTICIDES SCAN 'acility: FCX, Inc. (Statesville Plant) •rogram~ SF Statesville, NC Case No: 30418 MD No: 19T7 d/Station: MW8 / Aedia: GROUNDWATER D No: 19T7 :ESULTS J.010U ).010U ).010U ).010U ).013 ).010U ).010U J.010U ).020U ).020U ).020U ).020U J.020U J.020U J.020U 0.10UJ 0.020U 0.020U 0.010U 0.010U 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN. HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA-not analyzed. NAl-inter1erences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 17:40 Ending: 1al value is known to be less than value given. L-actual value is known to be greater than value given, LI-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 ample 4384 FY 2002 Project: 02-0493 ESTICIDES SCAN ~cility: FCX, Inc. (Statesville Plant) rograni;, SF Statesville, NC Case No: 30418 MD No: 19W0 :/Station: MWSS I edia:GROUNDWATER D No: 19W0 cSULTS 3.4 3.0 2.1 7.4 .010U .010U .010U .010U ·.020U .020U •.020U •.020U ,.02ou ,.02ou •.020U 0.10UJ 3.4N l.020U l.010U l,010U 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L · UG/L UG/L UG/L UG/L UG/L UG/L UGIL UGIL UGIL UGIL UG/L UG/L UG/L UGIL UG/L UG/L UG/L UG/L UGIL UG/L UGIL UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDTI METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE 12 GAMMA-CHLORDANE 12 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) . PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04123/2002 15:00 Ending: al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. 1dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. irmed by gems: 1.when no value is reported, see chlordane constituents 2.constiluents or metabolites of technical chlordane Page 1 of 1 iiiil -ample 4385 FY 2002 Project: 02-0493 ESTICIDES SCAN 3cility: FCX, Inc. (Statesville Plant) rograni;_ SF Statesville, NC Case No: 30418 MD No: 19W6 /Station: MW29 / ,edia: GROUNDWATER D No: 19W6 :SUL TS .041 .010U ·.010U •.038 •.010U •.010U 1.1 ,.01ou l.020U l.020U l.020U l.020U l.020U I.020U J.020U 0.10UJ 1.052 J.020U l.010U l.010U 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: CEIMIC ·age value. NA•not analyzed. NAl-interferences. Jo-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Lead_er: KMALLARY Beginning: 04/24/2002 17:00 Ending: 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. 1dicates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification. firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 1 -,mple 4386 FY 2002 Project: 02-0493 :STICIOES SCAN ,cility:. FCX, Inc. (Statesville Plant) ograni: .• SF Statesville, NC Case No: 30418 MD No: 19X1 DNo: 19X1 'Station: IN01 / adia: GROUNDWATER :SUL TS J.26 J.40 083 l 18 ).01U ).01U 1.4 ).01U .034 .020U .020U .020U .020U .020U .020U D.10UJ 0.16 .020U .010U .010U 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT {P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 15:30 Ending: al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. Idica1es that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification, irmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 iiiil 1cllll;/P~M Piiili!NALliiilit; --1mple 4387 FY 2002 Project: 02-0493 ,STICIDES SCAN 1cility:. FCX, Inc. (Statesville Plant) ograrri:-.SF Statesville, NC /Station: EB01 / edia:GROUNDWATER Case No: 30418 MD No: 19T9 D No: 19T9 :SUL TS UNITS 010U UG/L 010U UG/L 010U UG/L .010U UG/L .010U UG/L .010U UG/L .010U UG/L .010U UG/L .020U UG/L .020U UG/L . 020U UG/L .020U UG/L .020U UG/L .020U UG/L .020U UG/L 0.10UJ UG/L .020U UG/L .020U UG/L .010U UG/L .010U UG/L 1.0U UG/L 0.20U UG/L 0.40U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN . ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 1ge value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumplive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 09:00 Ending: 11 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification . . rmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 1aJs1PcJNhMFiMl.NAM!, -.. ample 4388 FY 2002 Project: 02-0493 ::STICIOES SCAN acility: FCX, Inc. (Statesville Plant) ·ogramc,SF Statesville, NC /Station: OUP02 / Case No: 30418 MD No: 19W2 edia: GROUNDWATER D No: 19W2 :SUL TS .010U .010U .016 .010U .010U .010U .010U .010U .020U .020U .020U .020U .020U .020U ·.020U 0.10UJ •.020U ,.02ou ,.01ou ,.01ou 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P.P'·DDD METHOXYCHLOR ENDRtN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254). PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 age value, NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 Ending: al value is known to be less than value given. L-actual value is known lo be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitatfon HmiL 1dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. irmed by gems·. 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 iiiil 11ple 4389 FY 2002 Project: 02-0493 STICIDES SCAN :ility:. FCX, Inc. (Statesville Plant) ,gram·: -SF Statesville, NC Case No: 30418 MD No: 19W1 ,talion: MW6D / dia: GROUNDWATER D No: 19W1 SULTS UNITS l10U UG/L l10U UG/L l10U UG/L l10U UG/L l10U UG/L l10U UG/L l10U UG/L l10U UG/L l20U UG/L l20U UG/L nou uGtL nou uGtL 020U UG/L 020U UG/L 020U UG/L 1.1 0UJ UG/L 020U UG/L 020U UG/L 010U UG/L 010U UG/L 1.0U UG/L l.20U UG/L l.40U UG/L l.20U UG/L l.20U UG/L l.20U UG/L l.20U UG/L l.20U UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) . 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 19e value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 12:09 Ending: I value is known to be less than value given. L-actua1 valUe is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. jicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. rmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 liiiil mple 4390 FY 2002 Project: 02-0493 :STICIDES SCAN cility: FCX, Inc. (Statesville Plant) ogram:-.SF Statesville, NC Case No: 30418 MD No: 19W3. D No: 19W3 ·station: MW6S / idia: GROUNDWATER 'SULTS UNITS 024 UG/L 010U UG/L 010U UG/L 010U UG/L 010U UG/L 010U UG/L 3.0 UG/L 010U UG/L 020U UG/L 020U UG/L 020U UG/L .020U UG/L .020U UG/L .020U UG/L .020U UG/L ).10UJ UG/L .020U UG/L .020U UG/L .010U UG/L .010U UG/L 1.0U UG/L 0.20U UG/L 0.40U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P.P'-DDD METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 ige value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. l!BI llllplrocmon~: ~/2~7:~ Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 10:00 Ending: ii value is known to be less than value given. L-actual value is known to be greater th3n value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. -Oicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. irmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 1<WstP~M~NA-- ,mple 4391 FY 2002 Project: 02-0493 :STICIDES SCAN 1cility: FCX, Inc. (Statesville Plant) ·ograrri:-.SF Statesville, NC Case No: 30418 MD No: 19X2 /Station: MW25 I edia: GROUNDWATER D No: 19X2 :SUL TS UNITS .010U UG/L .010U UG/L .010U UG/L .010U UGIL .010U UG/L .010U UG/L 0.76N UG/L .010U UG/L .020U UG/L .020U UG/L .020U UG/L .020U UG/L .020U UG/L .020U UG/L .020U UGIL 0.10UJ UG/L •.020U UG/L 1,020U UG/L 1.010U UG/L 1.010U UGIL 1.0U UG/L 0.20U UG/L 0.40U UGIL 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE · ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE} ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD} ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE 12 GAMMA-CHLORDANE 12 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/2412002 16:30 Ending: al value is known to be less than value given. L-actual value is known to be greater than value given. U-material waS analyzed for but not detected. the number is the minimum quantitation limit. ldicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. 1rmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 -,mple 4392 FY 2002 Project: 02-0493 :STICIDES SCAN 1cility:. FCX, Inc. (Statesville Plant) ograni:-,SF Statesville, NC 'Station: MW? / edia:GROUNDWATER Case No: 30418 MD No: 19W5 D No: 19W5 :SUL TS 010U 010U 010U ).33J .010U .010U 13 .010U .020U .020U .020U .020U .020U .020U .020U 0.10UJ .020U .020U .010U .010U 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4.4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4.4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE . 4,4'-DDT (P,P'-DDT) METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 14:30 Ending: al value is known to be less than value given. L-actual value is known to be greater than value given. U-materia1 was analyzed for but not detected. the number is the minimum quantitation limit. 1dicates that data unusable. compound may or may not be present. resampHng and reanalysis is necessary for verification. irmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 C.-1PcwillMPlilliflNALJla ----R--..i ,_..o, ..-NS,. .. .,ro-onBe: cM,2cM1:., liiil mple 4393 FY 2002 Project: 02-0493 STICIDES SCAN cility: FCX, Inc. (Statesville Plant) >gram: ,.SF Statesville, NC Case No: 30418 MD No: 19X3 Station: FB01 / ,dia:GROUNDWATER. D No: 19X3 SULTS UNITS J10U UG/L D10U UG/L 010U UG/L 010U UG/L 010U UG/L 010U UG/L 010U UG/L 010U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L J.10UJ UG/L 020U UG/L 020U UG/L 010U UG/L 010U UG/L 1.0U UG/L J.20U UG/L ).40U UG/L J.20U UG/L J.20U UG/L J.20U UG/L l.20U UG/L J.20U UGIL ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT {P,P'-DDD METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE 12 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 1ge value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:15 Ending: 11 value ls known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. jicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. rmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 mple 4394 FY 2002 Project: 02-0493 STICIOES SCAN cility: FCX, Inc. (Statesville Plant) igram:,SF Statesville, NC Case No: 30418 MO No: 19X4 Station: PB01 / ,dia: GROUNDWATER 0 No: 19X4 SULTS UNITS )10U UG/L )10U UG/L )10U UG/L J10U UG/L 010U UG/L 010U UG/L 010U UG/L 010U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L 020U UG/L l.10UJ UG/L 020U UG/L 020U UG/L 010U UG/L 010U UG/L 1.0U UG/L l.20U UG/L ).40U UG/L l.20U UG/L l.20U UG/L l.20U UG/L l.20U UG/L l20U UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIOE ENOOSULFAN I (ALPHA) OIELORIN 4,4'-00E (P,P'-OOE) ENORIN ENOOSULFAN II (BETA) 4,4'-000 (P,P'-000) ENOOSULFAN SULFATE 4,4'-00T (P,P'-DDD METHOXYCHLOR ENORIN KETONE ENORIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) lnorg Contractor: LIBRTY Org Contractor: A4 1ge value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:00 Ending: 11 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. jicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. rmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 --Re-. 1vWn,AWNs.• .. nple 4397 FY 2002 Project: 02-0493 STICIDES SCAN :ility: FCX, Inc. (Statesville Plant) 1gram:._$F Statesville, NC Case No: 30418 ,talion: MW1 / dia: GROUNDWATER D No: 19T3 SULTS 2.1 .31 .14 .96 l10U l10U 3.2N l10U ·.32N l20U l20U l20U l20U l20U l20U >.10NJ 1.51 nou 010U J10U 1.0U I.20U l.40U I.20U l.20U l.20U l.20U l.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDD METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) Org Contractor: A4 ~e value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 16:30 Ending: value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. icates that data unusable. compound may or may not be present. resampling and· reanalysis is necessary for verification. :ned by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 1mple 4398 FY 2002 Project: 02-0493 :STICIDES SCAN 1cility: FCX, Inc. (Statesville Plant) ·ogram~ SF Statesville, NC Case No: 30418 /Station: MW4 I edia: GROUNDWATER D No: 19T8 :SUL TS UNITS .010U UG/L .010U UG/L .010U UG/L .010U UG/L .010U UG/L .010U UG/L .010U UG/L .010U UG/L .020U UG/L .020U UG/L .020U UG/L .020U UG/L •.020U UG/L •.020U UG/L ,.02ou UG/L 0.10UJ UG/L I.020U UG/L I.020U UG/L ,.01ou UG/L I.010U UG/L 1.0U UG/L 0.20U UG/L 0.40U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L 0.20U UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4.4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHLORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) Org Contractor: A4 ·age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 17:30 Ending: al value is known to be less than value given. L-actual value Is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. ,dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 of 1 ,mple 4401 FY 2002 Project: 02-0493 :STICIDES SCAN ,cility: FCX, Inc. (Statesville Plant) ogram~ SF Statesville, NC Case No: 30418 'Station: MW2 / adia: GROUNDWATER D No: 19XO :SUL TS 017N .060 .010U .010U .010U .010U 0.47 .010U .031N .020U ,050 .020U .020U .020U .020U 0.10UJ 1.0 ,.02ou l.010U l.010U 1.0U 0.20U 0.40U 0.20U 0.20U 0.20U 0.20U 0.20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALPHA-BHC BETA-BHC DELTA-BHC GAMMA-BHC (LINDANE) HEPTACHLOR ALDRIN HEPTACHLOR EPOXIDE ENDOSULFAN I (ALPHA) DIELDRIN 4,4'-DDE (P,P'-DDE) ENDRIN ENDOSULFAN II (BETA) 4,4'-DDD (P,P'-DDD) ENDOSULFAN SULFATE 4,4'-DDT (P,P'-DDn METHOXYCHLOR ENDRIN KETONE ENDRIN ALDEHYDE ALPHA-CHLORDANE /2 GAMMA-CHlORDANE /2 TOXAPHENE PCB-1016 (AROCLOR 1016) PCB-1221 (AROCLOR 1221) PCB-1232 (AROCLOR 1232) PCB-1242 (AROCLOR 1242) PCB-1248 (AROCLOR 1248) PCB-1254 (AROCLOR 1254) PCB-1260 (AROCLOR 1260) Org Contractor: A4 Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 15:00 Ending: rage value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimi.Jm quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. firmed by gems: 1.when no value is reported, see chlordane constituents 2.constituents or metabolites of technical chlordane Page 1 ot 1 I I ::-,,i,tED Sr,4r~_, . ft . i~J I \:,,_.#' I I MEMORANDUM I Date: 06/03/2002 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and E_cosystem Support Division 980 College Station Road Athens, Georgia 30605-2720 DOCUMENTCO."fTRot NUMBER RJ;...)1'33-3A- A-L-~..J Subject: Results of E CT ABLES Sample Analysis I 02-0493 FCX, Inc. (Statesville Plant) Statesville, NC I I I I From: Mcconney, John To: Mallary, Ken CC: Ralph McKeen RACS/W Thru: QA Office cs Attached are the results of analysis of samples collected as part of the subject project. If you have any luestions, please contact me. I I lnAcHMENT I I I I I I I I Case Number: .Site ID. Date: I Affected Samples ~ 4378,4379,4381- lf'384,4386-4394, '4399,4400 14378,4381-4385, 387-4390,4399 4379 1380,4395,4396 1380,4385,4395, 396 ,381,4384,4388, 389 _ - 1385 I I I I 30418 ORGANIC DATA QUALIFIER REPORT Project Number FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 02-0493 Flag Compound or Fraction Used methyl acetate R 1,2-dibromo-3-<:hloropropane J 1,1-dichloroethane J bromomethane, chloroethane J 1,2-dibromo-3-chloropropane R I, 1-dichloroethene, I, 1-dichloroethane, cis-1,2-J dichloroethene, trichloroethene, xylene(total) tetrachloroethene J chloromethane, bromomethane, chloroethane, J trichlorofluoromethane, I, 1-dichloroethene, I, I ,2-trichloro-1,2,2-trifluoroethane, acetone I, 1-dichloroethene, I, I ,2-trichloro-1,2,2-J trifluoroethane, I, 1-dichloroethane, cis-1,2- dichloroethene, chloroform, trichloroethene carbon tetrachloride, trichloroethene J cyclohexane, benzene, trichloroethene, J methylcyclohexane, 1,2-dichloropropane, bromodichloromethane, cis-1,3-dichloropropene, toluene, trans-1,3-dichloropropene, 1,1,2- trichloroethane, ethylbenzene, xylene(total), styrene, isopropylbenzene, 1,1,2,2- tetrachloroethane, 1,2-dibromo-3-<:hloropropane SAS Number NIA Reason erratic initial & continuing calibration relative response factors erratic continuing calibration response factor < quantitation limit erratic continuing calibration response factor erratic initial & continuing calibration relative response factors < quantitation limit < quantitation limit erratic continuing calibration response factor < quantitation limit < quantitation limit low deuterated monitoring compound recovery a 0 I Case Number: (Fite ID. Date: u Affected Samples lr386 r.390 ll391 ,391,4393 if393 IJi393 1.395 loo I BNA 1378,4384,4386 I I 178-4393 I I I I 30418 ORGANIC DATA QUALIFIER REPORT Project Number FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Compound or Fraction methylcyclohexane, 1,2-dibromo-3- chloropropane methylene chloride chloroform, tetrachloroethene I, 1,2,2-tetrachloroethane, 1,2-dibromo-3- chloropropane ethylbenzene xylene(total) I, 1-dichloroethene, 1,l ,2-trichloro-1,2,2- trifluoroethane, I, 1-dichloroethane, cis-1,2- dichloroethene, chloroform, trichloroethene I, 1-dichloroethane, bromochloromethane, chloroform, cis-1,3-dichloropropene, I, 1,2- trichloroethane 2,4-dichlorophenol, hexachlorobutadiene, caprolactam, 4-chloro-3-methylphenol, 2,4,6- trichlorophenol, 2,4,5-trichlorophenol, I, l '- biphenyl, dimethylphthalate, diethylphthalate, 4,6-dinitro-2-methylphenol, 1,2,4,5- tetrachlorobenzene, pentachlorophenol, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate 3,3'-dichlorobenzdine 02-0493 SAS Number NIA Flag Used J J J J J J J J J J Reason erratic continuing calibration response factor contaminated storage blank < quantitation limit low deuterated monitoring compound recovery < quantitation limit warning high in low concentration PE sample < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery erratic continuing calibration response factor I I I Case Number: I Site ID. Date: I Affected Samples 14379 I I i4381,4385 "4382 I I 1387 i388 I I I I I 30418 ORGANIC DATA QUALIFIER REPORT Project Number 02-0493 SAS Number NIA FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Flag Compound or Fraction Used 2,4-dichlorophenol, hexachlorobutadiene, 4-J chloro-3-methylphenol, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 4,6-dinitro-2- methylphenol, 1,2,4,5-tetrachlorobenzene, pentachlorophenol, benzo(b )fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, indeno( 1,2,3-cd)pyrene, dibenzo( a,h)anthracene, benzo(g,h,i)perylene caprolactam J 2,4-dichlorophenol, 4-chloro-3-methylphenol, J 1, 1 '-biphenyl, acenaphthylene, acenaphthene, 4,6- dinitro-2-methylphenol, hexachlorobenzene, atrazine, phenanthrene, anthracene, benzo(b )fluoranthene, benzo(k)fluoranthene, benzo( a)pyrene, indeno(l ,2,3-cd)pyrene, dibenzo{a,h)anthracene, benzo(g,h,i)perylene 4,6-dinitro-2-methylphenol J 2,4-dichlorophenol, hexachlorobutadiene, 4-J chloro-3-methylphenol, 2,4,6-trichlorophenol, 2,4,5-trichlorophenol, 1,2, 4,5-tetrachlorobenzene, pentachlorophenol 2-methylphenol, 4-methylphenol, 2,4-J dimethylphenol, 2,4-dichlorophenol, naphthalene, hexachlorobutadiene,. caprolactam, 4-chloro-3- methylphenol, 2-methylnaphthalene, 2,4,6- trichlorophenol, 2,4,5-trichlorophenol, 1,1 '- biphenyl, 2-chloronaphthalene, dimethylphthalate, acenaphthylene, acenaphthene, diethylphthalate, 1,2,4,5- tetrachlorobenzene, pentachlorophenol, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate Reason low deuterated monitoring compound recovery < quantitation limit low deuterated monitoring compound recovery low deuterate.d monitoring compound recovery low deuterated monitoring compound recovery low deuterated.monitoring compound recovery I I I Case Number: .Site ID. Date: I Affected Samples ,389 4390 I t390 I 1393 '!393 1394 I I 4394 lsT 178-4394,4397, 98,4401 178,4379 } I 30418 ORGANIC DATA QUALIFIER REPORT Project Number 02-0493 SAS Number NIA FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Flag Compound or Fraction Used acetophenone J caprolactam, I, I '-biphenyl, dimethylphthalate, J diethylphthalate, 4,6-dinitro-2-methylphenol, di- n-butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate, atrazine J 4,6-dinitro-2-methylphenol, J benzo(b )fluoranthene, benzo(k)fluoranthene, benzo(a)pyrene, indeno( I ,2,3-cd)pyrene, dibenzo(a,h)anthracene, benzo(g,h,i)perylene 2-nitroaniline, 3-nitroaniline, 2,4--dinitrophenol, J 4-nitrophenol, 4-nitroaniline, 4,6-dinitro-2- methylphenol benzaldehyde J 2-methylphenol, 4-methylphenol, 2,4-J dimethylphenol naphthalene, caprolactam, 2-methylnaphthalene, J I, l '-biphenyl, 2-chloronaphthalene, dimethylphthalate, acenaphthylene, acenaphthene, diethylphthalate, di-n- butylphthalate, butylbenzylphthalate, bis(2- ethylhexyl)phthalate, di-n-octylphthalate caprolactam, atrazine, 3,3'--dichlorobenzidine J methoxychlor J beta-BHC J Reason < quantitation limit low deuterated monitoring compound recovery < quantitation limit, erratic initial calibration response factor low deuterated monitoring compound recovery low deuterated monitoring compound recovery < quantitation limit low deuterated monitoring compound recovery low deuterated monitoring compound recovery erratic continuing calibration response factor erratic initial calibration response factor < quantitation limit I I I Case Number: .Site ID. Date: I Affected Samples 14379,4391 4381 t384 4392 fn97 4401 I I I I I I I I I I I 30418 ORGANIC DATA QUALIFJER REPORT Project Number FCX. Inc. (Statesville Plant), Statesville, NC 5/24/02 Compound or Fraction heptachlor epoxide aJI compounds endrin ketone gamma-BHC heptachlor epoxide, dieldrin, methoxychlor alpha-BHC, dieldrin 02-0493 SAS Number NIA Flag Used Reason N difference in columns J low surrogate recovery N difference in columns J < quantitation limit N difference in columns N difference in columns Sample 4378 FY 2002 Project: 02-0493 EXTRACT ABLES SCAN Facility: FCX, Inc. (Statesville Plant) Programs.SF Statesville, NC Case No: 30418 MD No: 19T1 Id/Station: MW24 I Media: GROUNDWATER D No: 19T1 ~ESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5:0UJ 5.0U 5.0U 5.0UJ 5.0UJ. 5.0UJ 5.0U 5.0U 5.0UJ 20UJ 5.0UJ 5.0U 20U 5.0UJ 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UGIL UG/L UG/L UG/L UG/L UG/L UGIL UG/L UG/L UGIL UGIL UGIL UGIL ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-ANDIOR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2.4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0UJ 5.0U 5.0U 20U 20UJ 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U NA 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 7.6J 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U ,rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 0412312002 12:00 Ending: UNITS UG/L UG/L UGIL UG/L UG/L UG/L UGIL UG/L UGIL UGIL UGIL UG/L UGIL UGIL UGIL UG/L UGIL UGIL UG/L UGIL UGIL UGIL UG/L UGIL UGIL UG/L UGIL UGIL UGIL UGIL ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE 0I-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1.2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE ual value is known to be less than value given. l-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ttiiiAt:iLIIIIJiA~ANWll)IS -.. -A -.-ON-.iESctllllJE~ - Sample 4378 FY 2002 Project: 02-0493 MISCELLANEOUS COMPOUNDS Facility: FCX, Inc. (Statesville Plant) Program: .• SF Statesville, NC Case No: 30418 MD No: 19T1 Id/Station: MW24 / Media: GROUNDWATER D No: 19T1 tESULTS 5.0UJ 9.6JN 2.0JN 9.7J UNITS UG/L UG/L UG/L UG/L ANALYTE 1,2,4,5-TETRACHLOROBENZENE CYCLOPENTENE, 1,2,3,4,5,-PENT 3.ALPHA., 11.ALPHA.-DIAMINO-P 3 UNKNOWN COMPOUNDS \ REPORTED AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED ,5-TETRACHLOROBENZENE IS TARGET ANAL YTE lnorg Contractor: LIBRTY Org Contractor: A4 Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 12:00 Ending: rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 liiil ·--AB-.aA~AN-1S -liill -A --IO~ES~-iE~ .. -Pr-tic""1ate.03-o'-R - Sample 4379 FY 2002 Project: 02-0493 EXTRACT ABLES SCAN Facility:_ FCX, Inc. (Statesville Plant) Program;. SF Statesville, NC Case No: 30418 MD No: 19T2 Id/Station: DUP01 / Media: GROUNDWATER D No: 19T2 ,ESUL TS UNITS 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 20UJ UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 20U UG/L 20U UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILJNE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL Produced by: Mcconney, John Requester: lnorg Contractor: LIBRTY Org Contractor: A4 Project Leader: KMALLARY Beginning: 04/23/2002 Ending: RESULTS UNITS 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 20UJ UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L NA UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U. UG/L 7.3 UG/L 5.0U UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILJNE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A.H)ANTHRACENE BENZO(GHl)PERYLENE uage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. ual value is known to be less than value given. L-actual value Is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 -At:l~A~ ANliil)llS -..,A--101'-a.!ES~E~A all Sample 4379 FY 2002 Project: 02-0493 MISCELLANEOUS COMPOUNDS Facility: FCX, Inc. (Statesville Plant) Program;_ SF Id/Station: DUP01 / Media: GROUNDWATER RESULTS UNITS ANALYTE Statesville, NC Case No: 30418 MD No: 19T2 D No: 19T2 5.0UJ UG/L 13JN UG/L 22J UG/L 1,2,4,5-TETRACHLOROBENZENE CYCLOPENTENE, 1,2,3,4,5-PENT (2 ISOMERS) 6 UNKNOWN COMPOUNDS I,5-TETRACHLOROBENZENE IS TARGET ANAL YTE A REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: A4 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 Ending: ,rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. ual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification, Page 1 of 1 Sample 4380 FY 2002 Project: 02-0493 EXTRACTABLESSCAN Facility: FCX, Inc. (Statesville Plant) Program; SF Statesville, NC Case No: 30418 MD No: 19T4 Id/Station: MW5D I Media: GROUNDWATER D No: 19T4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20U 5.0U 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: CEIMIC RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 87 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U erage value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptlve evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 16:30 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L · UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE tual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis ls necessary for verification. Page 1 of 1 1-IA8iilJSAl'llliii ANIIIJ51S -.-,A .-IOl96ES-HE~A - Sample 4380 FY 2002 Project: 02-0493 MISCELLANEOUS COMPOUNDS Facility_: FCX, Inc. (Statesville Plant) Program; SF Statesville, NC Case No: 30418 MD No: 19T4 DNo: 19T4 Id/Station: MW5D / Media: GROUNDWATER RESULTS UNITS 5.0U UG/L. 15J UG/L 12JN UG/L 3.6JN UG/L ANALYTE 1,2,4,5-TRICHLOROBENZENE 5 UNKNOWN COMPOUNDS CYCLOPENTENE, 1,2,3,4,5-PENT OCTADECANOIC ACID, 2-METHYL- 1,5-TETRACHLOROBENZENE IS TARGET ANALYTE A REPORTED AS IDENTIFIED BY CLP LAB • IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: CEIMIC :1rage value. NA-not analyzed. NAJ-interferences. J-eslimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 16:30 Ending: lual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 -AC...,A~AN-IS - Sample 4381 FY 2002 Project: 02-0493 EXTRACTABLES SCAN Facility: FCX, Inc. (Statesville Plant) Program~ SF Statesville, NC Case No: 30418 MD No: 19T5 Id/Station: MW11 / Media: GROUNDWATER D No: 19T5 RES UL TS UNITS 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 1.0J UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 20U UG/L 20U UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 1rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumpf1ve evidence of presence of material. Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 16:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CO) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE ual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 .. r--AB..isAr.-ANaillts --Sample 4381 FY 2002 Project: 02-0493 MISCELLANEOUS COMPOUNDS Facility.: FCX, Inc. (Statesville Plant) Program:, SF Statesville, NC Id/Station: MW11 / Case No: 30418 MD No: 19T5 Media: GROUNDWATER D No: 19T5 RESULTS 5.0U 52J UNITS UG/L UG/L ANALYTE 1,2,4,5-TRICHLOROBENZENE 3 UNKNOWN COMPOUNDS 1,5-TETRACHLOROBENZENE IS TARGET ANAL YTE A REPORTED AS IDENTIFIED BY CLP LAB • IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: A4 erage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evlde,:ice of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 16:00 Ending: lual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,ample 4382 FY 2002 Project 02-0493 :XTRACT ABLES SCAN 'acility:. FCX, Inc. (Statesville Plant) 'rogram:-.SF Statesville, NC Case No: 30418 MD No: 19T6 d/Station: MW27S / ~edia: GROUNDWATER D No: 19T6 iESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 20U 5.0U 5.0UJ 20U 5.0U 5.0U 5.0UJ 20U 5.0UJ 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2.4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0UJ 5.0UJ u 5.0U 5.0U s.ou 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0UJ 5.0UJ 5.0UJ 5.0UJ 5.0UJ Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE 6IS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-materiat was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 -Sample 4382 FY 2002 Project: 02-0493 MISCELLANEOUS COMPOUNDS Facility: FCX, Inc. (Statesville Plant) Program~ SF Id/Station: MW27S / Media: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19T6 D No: 19T6 ~ESUL TS UNITS 5.0U UG/L 6.7J UG/L ANALYTE 1,2,4,5-TRICHLOROBENZENE 2 UNKNOWN COMPOUNDS !,5-TETRACHLOROBENZENE IS TARGET ANAL YTE 'A REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: A4 srage value. NA-not analyzed. NAl-interlerences. J.estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: tual value is known to be less than value given. L-actual value Is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification. Page 1 of 1 --------- ,....o.._AM~N.._S --.aJA--ON..,SD-EN .... --Pr-tio~te:Wo3,.0~ - ,ample 4383 FY 2002 Project: 02-0493 ,XTRACTABLES SCAN 'acility: FCX, Inc. (Statesville Plant) 'rogram:_ SF Statesville, NC Case No: 30418 MD No: 19T7 d/Station: MWS I Aedia: GROUNDWATER D No: 19T7 :ESULTS s.ou s.ou s.ou 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5,0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20U 5.0U 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE · 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1,1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2.6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U sou 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U u 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U s.ou ·age value. NA-not analyzed. NAl-interterences. J-estimated value. N-presumptlve evidence of presence of material. Produced by: Mcconney, John Requester·. Project Leader: KMALLARY Beginning: 04/23/2002 17:40 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4.6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER . HEXACHLOROBENZENE (HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3.3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A.H)ANTHRACENE BENZO(GHl)PERYLENE 1at value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit. :-idicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 Sample 4383 FY 2002 Project: 02-0493 ..,ISCELLANEOUS COMPOUNDS =acility:. FCX, Inc. (Statesville Plant) "rograriK. SF Statesville, NC Case No: 30418 MD No: 19T7 Id/Station: MW8 / Media: GROUNDWATER D No: 19T7 lESUL TS UNITS 5.0U UG/L 10JN UG/L 820J UG/L 60JN UG/L 5.6JN UG/L 20JN UG/L 11JN UG/L ANALYTE 1,2,4,5-TRICHLOROBENZENE TRIDECANOIC ACID 10 UNKNOWN COMPOUNDS PHENOL, 4,4'-BUlYLIDENEBIS [2 ERUCYLAMIDE 1,2-BENZISOSELENAZOLE 9-OCTAOECENOIC ACID, (E) - ,5-TETRACHLOROBENZENE IS TARGET ANAL YTE ~ REPORTED AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: A4 irage value. NA-not analyzed.' NAl-interferences. J..astimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 17:40 Ending: ual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quanlitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,ample 4384 FY 2002 Project: 02-0493 :XTRACTABLES SCAN 'acility: FCX, Inc. (Statesville Plant) 'rogram: .• SF Statesville, NC Case No: 30418 MD No: 19WO D No: 19WO d/Station: MWSS I Jedia: GROUNDWATER :ESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0UJ 5.0U 5.0U 5.0UJ 20UJ 5.0UJ 5.0U 20U 5.0UJ 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UG/L UGIL UG/L UG/L UG/L UG/L UGIL UGIL UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1,1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE· 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: L/BRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0UJ 5.0U 5.0U 20U 20UJ 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U NA 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U ge value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of p_resence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: UNITS UG/L UG/L UG/L UG/L UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2.4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE I value is known to be Jess than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. licates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 al '------"'''lliir'',_,;, --,ample 4384 FY 2002 Project: 02-0493 ~ISCELLANEOUS COMPOUNDS 'acility: FCX, Inc. (Statesville Plant) 'rograni;. SF Statesville, NC Case No: 30418 MD No: 19W0 D No: 19W0 d/Station: MW5S / i.1edia: GROUNDWATER IESULTS 5.0UJ 2.3JN 2.3JN 4.8JN 7.0J 3.2JN UNITS UG/L UG/L UG/L UG/L UGIL UGIL ANALYTE 1,2,4,5-TETRACHLOROBENZENE .ALPHA.-LINDANE CYCLOHEXANE, 1,2,3,4,5,6-HEX CYCLOHEXANE, 1,2,3,4,5,6-HEX UNKNOWN COMPOUND ENDRIN KETONE ;-TETRACHLOROBENZENE IS TARGET ANAL YTE REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: A4 11ge value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: ii value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. dlcates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 Sample 4385 FY 2002 Project: 02-0493 EXTRACT ABLES SCAN Facility: FCX, Inc. (Statesville Planl) Program:. SF Statesville, NC Case No: 30418 MD No: 19W6 Id/Station: MW29 / Media: GROUNDWATER D No: 19W6 ~ESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 1.7J 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20U 5.0U 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2 ,4-DIMETHYLPH ENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: CEIMIC RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 17 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. -- -----Production Date: 06/03/2002 07:49 Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 17:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE . PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE Jal value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 Sample 4385 FY 2002 Project: 02-0493 MISCELLANEOUS COMPOUNDS Facility: FCX, Inc. (Statesville Plant) Program~ SF Statesville, NC Case No: 30418 MD No: 19W6 Id/Station: MW29 / Media: GROUNDWATER D No: 19W6 ~ESULTS 5.0U 230J 5.6JN 6.2JN 2.3JN 2.4JN 11JN 3.8JN UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE 1,2.4,5-TETRACHLOROBENZENE 14 UNKNOWN COMPOUNDS BROMACIL PHENOL, 4.4'·(1-METHYLETHYLI OCTADECANAL NONADECANE 1-EICOSANOL PENTADECANE, 8-HEXYL- I,5-TETRACHLOROBENZENE IS TARGET ANALYTE A REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: CEIMIC ,rage value. NA-not analyzed. NAl-interferences. J•estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 17:00 Ending: ual value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,ample 4386 FY 2002 Project: 02-0493 ,XTRACT ABLES SCAN =acility: FCX, Inc. (Statesville Plant) 'rogram:. SF Statesville, NC Case No: 30418 MD No: 19X1 d/Station: IN01 I ~edia:GROUNDWATER D No: 19X1 IESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0UJ 5.0U 5.0U 5.0UJ 20UJ 5.0UJ 5.0U 20U 5.0UJ 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITRO BENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHEN!: 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0UJ 5.0U 5.0U 20U 20UJ 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U NA 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U age value. NA-not analyzed. NAl-lnterferences. J-eslimated value. N-presumplive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:30 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quanlitation limit. 1dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 -,ample 4386 FY 2002 Project: 02-0493 AISCELLANEOUS COMPOUNDS 'acility: FCX, Inc. (Statesville Plant) 'rogram:, SF d/Station: IN01 / Aedia: GROUNDWATER ANALYTE Statesville, NC Case No: 30418 MD No: 19X1 · D No: 19X1 :ESULTS 5.0JN 330J 21JN 5.0U UNITS UG/L UG/L UG/L UG/L HEMANTHAMINE P-BROMOBENZOATE 2 UNKNOWN COMPOUNDS DODECANOIC ACID, 1,2,3-PROPA 1,2,4,5-TETRACHLOROBENZENE ,5-TETRACHLOROBENZENE IS TARGET ANALYTE I REPORTED AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA•not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:30 Ending: Jal value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation fimil. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 R ,ample 4387 FY 2002 Project: 02-0493 :XTRACTABLES SCAN =acility:. FCX, Inc. (Statesville Plant) >rogram:_ SF Statesville, NC Case No: 30418 MD No: 19T9 d/Station: EB01 / 14edia: GROUNDWATER D No: 19T9 tESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20U 5.0U 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROtSOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U irage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 09:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE 0I-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE 0I-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE ual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantilation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 -:ample 4387 FY 2002 Project: 02-0493 IISCELLANEOUS COMPOUNDS ·acility: FCX, Inc. (Statesville Plant) •rogram;_ SF Statesville, NC Case No: 30418 MD No: 19T9 j/Station: EB01 / 1edia: GROUNDWATER D No: 19T9 ESULTS UNITS 2.3JN UG/L 2.4JN UG/L 4.SJN UG/L 5.0U UG/L 10J UG/L ANALYTE ALPHA.-LINDANE CYCLOHEXANE, 1,2,3,4,5,6-HEX CYCLOHEXANE, 1,2,3,4,5,6-HEX 1,2,4,5-TETRACHLOROBENZENE 2 UNKNOWN COMPOUNOS 5-TETRACHLOROBENZENE IS TARGET ANALYTE , REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED lnorg Contractor: LIBRTY Org Contractor: A4 ·age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. -Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 09:00 Ending: 1al value is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. re~ampling and reanalysis ls necessary for verification. Page 1 of 1 .ample 4388 FY 2002 Project: 02-0493 :XTRACT ABLES SCAN acility: FCX, Inc. (Statesville Plant) 'rogram:_ SF Statesville, NC Case No: 30418 MD No: 19W2 J/Station: DUP02 / 1edia: GROUNDWATER D No: 19W2 ESUL TS UNITS 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 3.0J UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 20UJ UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 20U UG/L 20U UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2.4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 37 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U rage value. NA.not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ,ample 4388 FY 2002 Project: 02-0493 !ISCELLANEOUS COMPOUNDS ·acility: FCX, Inc. (Statesville Plant) 1rogram:-~SF J/Station: DUP02 / Aedia:GROUNDWATER .ESUL TS UNITS ANALYTE Statesville, NC Case No: 30418 MD No: 19W2 D No: 19W2 28J UG/L 5.7JN UG/L 2.1JN UG/L 5.0UJ UG/L 6 UNKNOWN COMPOUNDS BENZENEMETHANOL, .ALPHA.,.AL OXYBENZONE 1,2,4,5-TETRACHLOROBENZENE \ REPORTED AS IDENTIFIED BY CLP LAB • IDS NOT VERIFIED ,5-TETRACHLOROBENZENE IS TARGET ANAL YTE lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumptive evidence of presence of material. Produced by: Mcconney; John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 Ending: 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ;ample 4389 FY 2002 Project: 02-0493 :XTRACT ABLES SCAN 'acility: FCX, Inc. (Statesville Plant) 'rogram: .• SF Statesville, NC Case No: 30418 MD No: 19W1 J/Station: MW6D / ~edia: GROUNDWATER D No: 19W1 .ESULTS UNITS 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 3.3J UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0U UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0U UG/L 5.0UJ UG/L 20UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 20U UG/L 5.0UJ UG/L 5.0U UG/L 5.0UJ UG/L 20U UG/L 5.0UJ UG/L 20U UG/L 20U UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE: 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0UJ 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U NA 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 7.3J 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 1ge value. NA-not analyzed. NAl-interferences. J-estimaled value. N-presumptive evidence of pr8sence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 12:09 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE 11 value is known to be less than value gtven. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ;ample 4389 FY 2002 Project: 02-0493 ~ISCELLANEOUS COMPOUNDS 'acility: FCX, Inc. (Statesville Plant) •rogram:-. SF j/Station: MW6D / ~edia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19W1 D No: 19W1 .ESULTS 5.0UJ 17J UNITS UG/L UG/L ANALYTE 1,2,4,5-TETRACHLOROBENZENE 5 UNKNOWN COMPOUNDS \ REPORTED AS IDENTIFIED BY CLP LAB -IDS NOT VERIFIED ,5-TETRACHLOROBENZENE IS TARGET ANALYTE lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 12:09 Ending: Jal value Is known to be less than value given. L-actual value is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resamplin9 and_ reanalysis is necessary for verification, Page 1 of 1 ample 4390 FY 2002 Project: 02-0493 XTRACTABLES SCAN acility:. FCX, Inc. (Statesville Plant) 'rogram;, SF Statesville, NC Case No: 30418 MD No: 19W3 j/Station: MW6S / ledia: GROUNDWATER D No: 19W3 ESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 3.3J 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U ZOU 5.0UJ 5.0U ZOU 5.0UJ 5.0U 5.0U 20U 5.0U ZOU 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UGIL UGIL UGIL UGIL UG/L UGIL UG/L UGIL UGIL UGIL UGIL UGIL UG/L UG/L UGIL UG/L UGIL UGIL UGIL ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-ANDIOR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LI BRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0UJ 5.0U 5.0U ZOU 20UJ 5.0U 5.0U 5.0U 1.8J 5.0U 5.0U 5.0U NA 5.0UJ 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 10:00 Ending: UNITS UG/L UGIL UG/L UG/L UGIL UGIL UG/L UG/L UGIL UG/L UGIL UGIL UG/L UG/L UG/L UG/L UGIL UGIL UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) .ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE 0I-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE 8IS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE Jal value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ample 4390 FY 2002 Project: 02-0493 IISCELLANEOUS COMPOUNDS acility:. FCX, Inc. (Statesville Plant) rograni;, SF I/Station: MW6S / ledia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19W3 D No: 19W3 ESULTS 5.0U 28J 3.9JN UNITS UG/L UG/L UG/L ANALYTE 1,2,4,5-TETRACHLOROBENZENE 4 UNKNOWN COMPOUNDS BROMACIL , REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED 5-TETRACHLOROBENZENE IS TARGET ANALYTE lnorg Contractor: LIBRTY Org Contractor: A4 -Produced by: McConney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 10:00 Ending: ·age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptlve evidence of presence of material. 1a1 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 llllll ample 4391 FY 2002 Project: 02-0493 KTRACT ABLES SCAN acility:. FCX, Inc. (Statesville Plant} rogranLSF Statesville, NC Case No: 30418 MD No: 19X2 /Station: MW25 / edia: GROUNDWATER D No: 19X2 :SUL TS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20U 5.0U 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL} ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL} ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL. 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE. ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL Produced by: Mcconney, John Requester: lnorg Contractor: LIBRTY Org Contractor: A4 Project Leader: KMALLARY Beginning: 04/24/2002 16:30 Ending: RES UL TS UNITS 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 20UJ UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L NA UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L 5.0UJ UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALATE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE :1ge value, NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. :11 value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected, the number is the minimum quantitation limit. dicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary tor verification. Page 1 of 1 (iiiiiif\BL;a;AMfiliiS\NAllll]S -~. ~N aalso,lililEN~ ample 4391 FY 2002 Project: 02-0493 IISCELLANEOUS COMPOUNDS acility: FCX, Inc. (Statesville Plant) ·rogram~ SF l/Station: MW25 / 1edia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19X2 D No: 19X2 ESULTS 5.0U 7.9J UNITS UG/L UG/L ANALYTE 1,2,4,5-TETRACHLOROBENZENE UNKNOWN COMPOUND , REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED 5-TETRACHLOROBENZENE IS TARGET ANAL YTE lnorg Contractor:.LIBRTY Org Contractor: A4 iiiil Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04124/2002 16:30 Ending: age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ldicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 iiiiiil ample 4392 FY 2002 Project: 02-0493 XTRACT ABLES SCAN acility: FCX, Inc. (Statesville Plant) rogram~ SF Statesville, NC Case No: 30418 MD No: 19W5 D No: 19W5 I/Station: MW7 / ledia: GROUNDWATER ESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20UJ 5.0U 5.0U 5.0U 20UJ 5.0U 20UJ 20UJ UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE . 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20UJ 20UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U rage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 14:30 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYL BUTYL PHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantilation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 11!!!!1 ;ample 4392 FY 2002 Project: 02-0493 ~ISCELLANEOUS COMPOUNDS 'acility.: FCX, Inc. (Statesville Plant) 'rograrn:. SF ct/Station: MW7 I Aedia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19W5 D No: 19W5 :ESULTS 5.0U 200J 16JN UNITS UG/L UGIL UG/L · ANALYTE 1,2,4,5-TETRACLOROBENZENE 29 UNKNOWN COMPOUNDS BROMACIL \ REPORTED AS IDENTIFIED BY CLP LAB • IDS NOT VERIFIED ,5-TETRACHLOROBENZENE IS TARGET ANAL YTE lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 14:30 Ending: Jal value is known to be less than value given. L-actual value is known to be greater than value given. Li-material was analyzed for but not detected. the number is the minimum quantilation limit. ,ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ample 4393 FY 2002 Project: 02-0493 XTRACTABLES SCAN acility: FCX, Inc. (Statesville Plant) rogram:, SF Statesville, NC Case No: 30418 MD No: 19X3 I/Station: FB01 / ledia: GROUNDWATER D No: 19X3 ESULTS 2.1J 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20U 5.0U 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:15 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2.4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE :age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material waS analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ample 4393 FY 2002 Project: 02-0493 IISCELLANEOUS COMPOUNDS acility: FCX, Inc. (Statesville Plant) rograril~ SF I/Station: FB01 / \edia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19X3 D No: 19X3 ESUL TS UNITS 5.0U UG/L 9.3JN UG/L ANALYTE 1,2,4,5-TETRACHLOROBENZENE BENZOPHENONE , REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED 5-TETRACHLOROBENZENE IS TARGET ANALYTE lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA-not analyzed. NAl-interferences. J-estimated value, N-presumptive evidence of presence of material. Produced by: Mcconney, John Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:15 Ending: 1al value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ;ample 4394 FY 2002 Project: 02-0493 :XTRACT ABLES SCAN 'acility: FCX, Inc. (Statesville Plant) 'rogram; SF Statesville, NC Case No: 30418 MD No: 19X4 d/Station: PB01 / Aedia: GROUNDWATER D No: 19X4 :ESULTS 3.5J 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0UJ 5.0U 5.0UJ 5.0U 5.0U 20U 5.0UJ 5.0UJ 20U 5.0UJ 5.0U 5.0UJ 20U 5.0UJ 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0UJ 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U NA 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U uage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 15:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALA TE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CO) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE :ual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 :ample 4394 FY 2002 Project: 02-0493 IISCELLANEOUS COMPOUNDS 'acility: FCX, Inc. (Statesville Plant) 'rogram; SF j/Station: PB01 I Aedia: GROUNDWATER Statesville, NC Case No: 30418 MD No: 19X4 D No: 19X4 :ESULTS 5.0U 4.3J 8.0JN UNITS UG/L UG/L UG/L ANALYTE 1,2,4,5-TETRACHLOROBENZENE UNKNOWN COMPOUND BENZOPHENONE .,_ REPORTED AS IDENTIFIED BY CLP LAB· IDS NOT VERIFIED •,5-TETRACHLOROBENZENE IS TARGET ANAL YTE lnorg Contractor: LIBRTY Org Contractor: A4 irage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requestor: Project Leader: KMALLARY Beginning: 0412412002 15:00 Ending: ual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number Is the minimum quantitatlon limit. indi~tes that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 - I I I I I I I I I I I • ,_.,c, MEMORANDUM Date: 06/11/2002 UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division 980 College Station Road Athens, Georgia 30605-2720 NT. CONTROL NUMBER~ 1~3 -?:...4 Subject: Results of EXTRACT ABLES Sample Analysis 02-0493 FCX, Inc. (Statesville Plant) Statesville, NC DOCUME AL-'=l"" From: Mcconney, John To: Mallary, Ken CC: Ralph McKeen RACS/W Thru: QA Office Please substitute these results for those previously reported. If you have any questions, please contact me. I I I tACHMENT I I I I -liiiiiiil -. -~-~·-~,__.,., ---l'A llliJ310lilli)5ESliiilifHEiiiiil,A -liiiilil PMctillf'batP.lli11 A2 A alll. Sample 4382 FY 2002 Project: 02-0493 EXTRACTABLES SCAN Facility: FCX, Inc. (Statesville Plant) Program; SF Statesville, NC Case No: 30418 MD No: 19T6 Id/Station: MW27S / Media: GROUNDWATER D No: 19T6 RESULTS UNITS 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 5.0U UG/L 5.0U UG/L 20U UG/L 5.0U UG/L 5.0UJ UG/L 20U UG/L 5.0U UG/L 5.0U UG/L 5.0UJ UG/L 20U UG/L 5.0UJ UG/L 20U UG/L 20U UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACT AM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2.4,5-TRICHLOROPHENOL 1, 1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20UJ 5.0U 5.0U 5.0UJ 5.0UJ 5.0U 5.0UJ 5.0UJ NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0UJ 5.0UJ 5.0UJ 5.0UJ 5.0UJ erage value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: McConney, John Requester: Projecl Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4.6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE(HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALA TE DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO·A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE tual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. : indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 Sample 4383 FY 2002 Project: 02-0493 EXTRACTABLES SCAN Facility: FCX, Inc. (Statesville Plant) Program~ SF Statesville, NC Case No: 30418 MD No: 19T7 Id/Station: MWB I Media:GROUNDWATER D No: 19T7 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 20U 5.0U 5.0U 20U 5.0U 5.0U 5.0U 20U 5.0U 20U 20U UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L · UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE BENZALDEHYDE PHENOL BIS(2-CHLOROETHYL) ETHER 2-CHLOROPHENOL 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL) ETHER ACETOPHENONE (3-AND/OR 4-)METHYLPHENOL N-NITROSODI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BIS(2-CHLOROETHOXY)METHANE . 2,4-DICHLOROPHENOL NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE CAPROLACTAM 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE (HCCP) 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 1,1-BIPHENYL 2-CHLORONAPHTHALENE 2-NITROANILINE DIMETHYL PHTHALATE 2,6-DINITROTOLUENE ACENAPHTHYLENE 3-NITROANILINE · ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL lnorg Contractor: LIBRTY Org Contractor: A4 RESULTS 5.0U 5.0U 5.0U 5.0U 5.0U 20U 20U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U NA 5.0U 5.0U 5.0U 5.0U 5.0UJ 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U 5.0U erage value. NA-not analyzed. NAl-interlerences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Mcconney, John Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 17:40 Ending: UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE DIBENZOFURAN 2,4-DINITROTOLUENE DIETHYL PHTHALATE FLUORENE 4-CHLOROPHENYL PHENYL ETHER 4-NITROANILINE 2-METHYL-4,6-DINITROPHENOL N-NITROSODIPHENYLAMINE/DIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE (HCB) ATRAZINE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE CARBAZOLE DI-N-BUTYLPHTHALA TE : FLUORANTHENE PYRENE BENZYLBUTYLPHTHALATE 3,3'-DICHLOROBENZIDINE: BENZO(A)ANTHRACENE CHRYSENE BIS(2-ETHYLHEXYL) PHTHALATE DI-N-OCTYLPHTHALATE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE BENZO-A-PYRENE INDENO (1,2,3-CD) PYRENE DIBENZO(A,H)ANTHRACENE BENZO(GHl)PERYLENE tual value is known to be less than value given. L-actual value is known to be greater than value given. U-materia1 was analyzed tor but not detected. the number is the minimum quantitation limit. . indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 I I I I UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 4 Science and Ecosystem Support Division 980 College Station Road Athens, Georgia 30605-2720 I MEMORANDUM tfAY z 8 2002 I I I I I I Date: 05116/2002 Subject: Results of METALS Sample Analysis 02-0493 FCX, Inc. (Statesville Plant) Statesville, NC From: Goddard, Denise To: Mallary, Ken CC: Ralph McKeen RACS/W Thru: QA Office DOCUMENT CONTROLNUMBE'tl}FyJ trs-}A; -.AwJ Attached are the results of analysis of samples collected as part of the subject project. If you have any f uestio.ns, please contact me. I J.nACHMENT I I I I I I I I I I I I I I I I I I D I I I Page 1 of 6 May 10, 2002 INORGANIC DATA QUALIFIERS REPORT Case Number:~3~0~4~1~8"-------------- Project Number:__,0~2~-~0~4.,_,,_9~3---,--------,---- Site: FCX, Inc. (Statesville Plant), Statesville, NC Sam:gle No. Element Flag Reason 4378 Al J Serial d.ilution percent difference = 14.S't As R Analyte reported as potential false positive Ba J Serial dilution percent difference = 12.S't Be u Baseline instability in cal, prep, and blind Cr J Serial dilution percent difference lS't Cu u Baseline instability in cal blanks Fe J PE sample recovery > warning limit Serial dilution percent difference = 14.9\ Mg J Serial dilution percent difference 13. 3't Mn J Serial dilution percent difference 13.4\ Ni J Serial dilution percent difference = 11. 6't Se J Matrix spike recovery= 56.1% Tl J Matrix spike recovery = 37.G't V R Analyte reported as potential false positive 4379 Al J Serial dilution percent difference 14. S't Ba J Serial dilution percent difference = 12.S't Be u Baseline instability in cal, prep, and blind Cr J Serial dilution percent difference lS't Cu u Baseline instability in cal blanks Fe J PE sample recovery> warning limit Serial dilution percent difference 14.9\ Mg J Serial dilutiOn percent difference 13.J't Mn J Serial dilution percent difference 13.H Hg UJ PE sample recovery > action limit Baseline instability in blind blank Ni J Serial dilution percent difference 11.G't Se J Matrix spike recovery = 56.1% Tl J Matrix spike recovery= 37.6\ V J Serial dilution percent difference lH 4380 Al UJ Serial dilution percent difference = 14 .st Positives in cal blanks As R Analyte reported as potential false positive Ba J Serial dilution percent difference = 12. 5 't Be u Baseline instability in cal, prep,· and blind Cr R Analyte reported as potential false positive cu u Baseline instability in cal blanks Fe J PE sample recovery > warning limit Serial dilution percent difference 14.9\ Mg J Serial dilution percent difference 13.H Mn J Serial dilution percent difference = 13.H Ni R Analyte reported as potential false positive Se J Matrix spike recovery= 56.1% Tl J Matrix spike recovery= 37.6\ V J Serial dilution percent difference lH blanks blanks blanks I I Page 2 of 6 I May l.0, 2002 INORGANIC DATA QUALIFIERS REPORT (continued) I Case Number: 30-4~l.~8~~~-----------Project Number: 02-0493 Site: FCX, Inc. (Statesville Plant), Statesville, NC I Sam2le No. Element Flag Reason 4381 Al J Serial dilution percent difference 14. 5% Sb u Baseline instability in cal blanks Ba J Serial dilution percent difference = 12.5% I Cr J Serial dilution percent difference 15% Fe J PE sample recovery > warning lirriit• Serial dilution percent difference 14.9% I Mg J Serial dilution percent difference 13. 3% Mn J Serial dilution percent difference 13 .4% Hg UJ PE sample recovery > action limit Baseline instability in blind blank I Ni J Serial dilution percent difference = 11. 6% Se R Analyte reported as potential false positive Tl J Matrix spike recovery = 37.6% V J Serial dilution percent difference 14% I 4382 Al J Serial dilution percent difference 14 .5% As R Analyte reported as potential false positive Ba J Serial dilution percent difference 12.5% I Be u Baseline instability in cal, prep, and blind Cr J Serial dilution percent difference 15% Fe J PE sample recovery > warning limit Serial dilution percent difference 14.9% I Mg J Serial dilution percent difference = 13 .3% Mn J Serial dilution percent difference = 13.4% Hg UJ PE sample recovery > action limit I Baseline instability in blind blank Ni J Serial dilution· percent difference 11. 6% Se J Matrix spike recovery= 56.1% Tl J Matrix spike recovery = 37.6% I V J Serial dilution percent difference 14% 4383 Al J Serial dilution percent difference 14. 5% As J % RSD > 20% for ICP multiple exposures I Ba J Serial dilution percent difference 12.5% Be u Baseline instability in cal, prep, and blind Cr J Serial dilution percent difference 15% cu u Baseline instability in cal blanks I Fe J PE sample recovery > warning limit Serial dilution percent difference 14.9% Mg J Serial dilution percent difference 13 .3% Mn J Serial dilution percent differerice 13.4% • Ni J Serial dilution percent difference = 11. 6% Se J Matrix spike recovery= 56. 1% Tl J Matrix spike recovery= 37.6% I V J Serial dilution percent difference 14% I I blanks blanks I I Page 3 of 6 I May 10, 2002 INORGANIC DATA QUALIFIERS REPORT (continued) Case NUmber:~3~o~·4"1"-"8 _____________ _ I Project Number ,_,0,.,2:.:-:.,0~4,.,9'"3'----------- Si te: FCX, Inc. (Statesville Plant), Statesville, NC I Sa!!!];!le No. Element Flag Reason 4384 Al J Serial dilution percent difference 14.5% Ba J Serial dilution percent difference = 12.5% Be u Baseline instability in cal, prep, and blind I Cr J Serial dilution percent difference 15% Fe J PE sample recovery > warning limit· Serial dilution percent difference = 14.9% I Mg J Serial dilution percent difference 13. 3% Mn J Serial dilution percent difference 13 .4% Hg UJ PE sample recovery > action limit Baseline instability in blind blank I Ni J Serial dilution percent difference = 11.6% Se R Analyte reported as potential false positive Na u Positive in prep blank Tl J Matrix spike recovery= 37.6% I V J Serial dilution percent difference 14% 4385 Al UJ Serial dilution percent difference 14 .5% Positives in cal, prep, and blind blanks I Sb u Baseline instability in cal blanks Ba J Serial dilution percent difference = 12.5% Be u Baseline instability in cal, prep, and blind Cd R Analyte reported as potential false positive I Cr UJ Serial dilution percent difference 15% Baseline instability in cal blanks cu u Baseline instability in cal blanks I Fe J PE sample recovery > warning limit · Serial dilution percent difference 14. 9% Pb R Analyte reported as potential false positive Mg J Serial dilution percent difference 13. 3% I Mn J Serial dilution percent difference 13.4% Ni J Serial dilution percent difference 11.6% Se J Matrix spike recovery= 56.1% Tl J Matrix spike recovery= 37.6% 14386 V J Serial dilution percent difference 14% Al J Serial dilution percent difference 14.5% Ba J Serial dilution percent difference = 12.5% I Be u Baseline instability in cal, prep, and blind Cr UJ Serial dilution percent difference 15% Baseline instability in cal blanks Fe J PE sample recovery> warning limit I Serial dilution percent difference 14. 9% Pb R Analyte reported as potential false positive Mg J Serial dilution percent difference 13. 3% I Mn J Serial dilution percent difference 13. 4% Ni J Serial dilution percent difference 11. 6% Se J Matrix spike recovery = 56.1% Tl J Matrix spike recovery= 37.6% I V J Serial dilution percent difference = 14% I blanks blanks blanks I I Page 4 of 6 I May 10, 2002 INORGANIC DATA QUALIFIERS REPORT (continued) I Case Number,~3~0~4~1~8,,_ ____________ _ Project Number,~0~2~-~0~4~9=3 __________ _ Site: FCX, Inc. (Statesville Plant), Statesville, NC I SamQ:le No. Element Flag Reason 4387 Al J Serial dilution percent difference 14 .5% Ba UJ Serial dilution percent difference 12.5% Positives cal and blind blanks I Cr J Serial dilution percent difference 15% Cu u Baseline instability in cal blanks Fe UJ PE sample recovery > warnin9 limit I Serial dilution percent difference 14. 9% Positive in blind blank Mg J Serial dilution percent difference 13 .3% Mn UJ Serial dilution percent difference 13 .4% I Baseline instability in cal and blind banks Ni J Serial dilution percent difference 11. 6% K u Positives in cal and prep blanks Se J Matrix spike recovery= 56.1% I Na u Positive in prep blank Tl J Matrix spike recovery = 37.6% V J Serial dilution percent difference 14% I 4388 Al UJ Serial dilution percent difference = 14 .5% Positives in cal, prep, and blind blanks Ba J Serial dilution percent difference = 12.5% Be u Baseline instability in cal, prep, and blind blanks I Cd R Analyte reported as potential false positive Cr R Analyte reported as potential false positive Cu u Baseline instability in cal blanks I Fe J PE sample recovery > warning limit Serial dilution percent difference = 14. 9% Mg J Serial dilution percent difference = 13 .3% Mn J Serial dilution percent difference = 13 .4% I Ni R Analyte reported as potential false positive Se J Matrix spike recovery= 56 .1% Tl J Matrix spike recovery= 37.6% V J Serial dilution percent difference 14% I 4389 Al UJ Serial dilution percent difference 14.5% Positives in cal, prep, and blind.blanks Ba J Serial dilution percent difference = 12.5% I Be u Baseline instability in cal, prep, and blind blanks Cd R Analyte reported as potential false positive Cr R Analyte reported as potential false positive Cu u Baseline instability in cal blanks I Fe J PE sample recovery > warning limit serial dilution percent difference = 14.9% Mg J Serial dilution percent difference = 13.3% I Mn J Serial dilution percent difference = 13.4% Ni R Analyte reported as potential false positive Se R Analyte reported as potential false positive Tl J Matrix spike recovery= 37.6% I V R Analyte reported as potential false positive I I I I I I I I I I I I I I I I I I I I Page 5 of 6 May 10, 2002 INORGANIC DATA QUALIFIERS REPORT (continued) Case Number:--"3~0~4~1~8~-------------Project Number,_,0~2~-~0~4'.!.z:923 __________ _ Site: FCX, Inc. (Statesville Plant), Statesville, NC Sam11le No. Element Flag Reason 4390 Al J Serial dilution percent difference 14.5% Ba J Serial dilution percent difference = 12.5% Be u Baseline instability in cal, prep, and blind blanks Cr J Serial dilution percent difference 15% Cu u Baseline instability in cal blanks· Fe J PE sample recovery > warning limit Serial dilution percent difference 14. 9% Mg J Serial dilution percent difference 13 .3% Mn J Serial dilution percent difference = 13 .4% Hg J PE sample recovery > action limit Ni J Serial dilution percent difference 11.6% Se J Matrix spike recovery= 56.1% Tl J Matrix spike recovery= 37.6% V J Serial dilution percent difference 14% 4391 Al J Serial dilution percent difference 14.5% Ba J Serial dilution percent difference = 12.5% Be u Baseline instability in cal, prep, and blind blanks Cr J Serial dilution percent difference 15% Fe J PE sample recovery > warning limit Serial dilution percent difference 14. 9\ Mg J Serial dilution percent difference 13.3% Mn J Serial dilution percent difference 13.4% Hg UJ PE sample recovery > action limit Baseline instability in blind blank Ni J Serial dilution percent difference = 11.6% Se J Matrix spike recovery = 56.1% Tl J Matrix spike recovery= 37.6% V J Serial dilution percent difference = 14% 4392 Al J Serial dilution percent difference = 14.5% Ba J Serial dilution percent difference = 12.St Be u Baseline instability in cal, prep, and blind blanks Cr UJ Serial dilution percent difference = 15\ Baseline instability in cal blanks Cu u Baseline instability in cal blanks Fe J PE sample recovery > warning limit Serial dilution percent difference = 14. 9% Mg J Serial dilution percent difference = 13 .3% Mn J Serial dilution percent difference = 13 .4% Ni J Serial dilution percent difference = 11. 6\ Se J Matrix spike recovery= 56.1% Tl J Matrix spike recovery= 37.6% V J Serial dilution percent difference 14% I I I I Page 6 of 6 May 10, 2002 INORGANIC DATA QUALIFIERS REPORT (continued) I Case NUmber:~3~0~4~1~8~------------- Project NUmber:___,,0~2~-~0~4~9~3'------------Site: FCX, Inc. ·(Statesville Plant), Statesville, NC I Sample No. Element 4393 Al Ba I Cr Fe I Mg Mn Ni I Se Na Tl I V 4394 Al I As Ba Cr Fe I Mg Mn I Ni Se Na I Tl V I I I I I I Flag UJ J J UJ J UJ J J u J J Reason Serial dilution percent difference= 14.5% Positives in cal, prep, and blind blanks Serial dilution percent difference= 12.5% Serial dilution percent difference= 15% PE sample recovery> warning limit• Serial dilution percent difference= 14.9% Positive in blind blank Serial dilution percent Serial dilution percent Baseline instability in Serial dilution percent Matrix spike recovery= Positive in prep blank Matrix spike recovery= Serial dilution percent difference difference cal and blind difference 56.1% 37.6% difference= 13.3% 13.4% blanks 11.6% 14% UJ Serial dilution percent difference 14.5% Positives in cal, prep, and blind blanks R Analyte reported as potential false positive J Serial dilution percent difference 12.5% J Serial dilution percent difference= 15% UJ PE sample recovery> warning limit Serial dilution percent difference 14.9% J UJ J J u J J Positive in blind blank Serial dilution percent Serial .dilution percent Baseline instability in Serial dilution percent Matrix spike recovery= Positive in prep blank Matrix spike recovery= Serial dilution percent difference= difference= cal and blind difference= 56.1% 37 .6% difference= 13.3% 13.4% blanks 11.6% 14% -Sample 4377 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program~ SF Id/Station: MDRS01 / Media: GROUNDWATER RES UL TS UNITS 53 UG/L 1.6U UG/L 4.2U UG/L 0.13 UG/L 0.31 UG/L 0.30U UG/L 17U .UG/L a.sou UG/L 0.60U UG/L 0.70U UG/L 14 UG/L 1.3U UG/L 12U UG/L 0.36 UG/L 0.14 UG/L a.sou UGJL 13U UG/L 2.2U UG/L 0.70U UG/L 1SOU UG/L 3.3U UG/L a.sou UGJL 1.4U UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE -~IDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19TO lnorg Contractor: LIBRTY rage value. NA•not analyzed. NAl•lnterferences. J--estlmated value. N.presumptlve evidence of presence of material. Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/18/2002 12:00 Ending: Jal value is known to be less than value given. L-actual value 18 known to be greater than value given. U-materlal was analyzed for but not detected. the number is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 --Sample 4378 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program:,SF Statesville, NC Id/Station: MW24 / Media: GROUNDWATER RESULTS 620J 1.6U 9.3R 26 0.43U 0.30U 23000 14J 0.60U 3.5U 1000J 1.3U 5500J 120J 0.10U 4.0J 3100 2.2UJ 0.70U 9100 3.3UJ 1.5R 23 NA UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE llDE ANALYSIS NOT REQUESTED Case No: 30418 MD No: 19T1 D No: 19T1 lnorg Contractor: LIBRTY Org Contractor: A4 ·age value. NA-not analyzed. NAl-interferences. J-estimated value. N-presumptive evidence of presence of material. Produced by: Goddard, Denise Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 12:00 Ending: al value Is known to be less than value given. L-actual value Is known to be greater than value given. U.n,aterial was analyzed for but not detected. the number is the minimum quantitatlon limit. 1dlcates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification. Page 1 of 1 iiil -Sample 4379 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Programc SF Id/Station: DUP01 / Media: GROUNDWATER RESULTS UNITS 630J UG/L 1.6U UG/L 4.2U UG/L 28J UG/L 0.42U UG/L 0.30U UG/L 25000 UG/L 15J UG/L 0.60U UG/L 3.8U UG/L 1000J UG/L 1.3U UG/L 5900J UG/L 130J UG/L 0.11UJ UG/L 4.3J UG/L 3400 UG/L 2.2UJ UG/L 0.70U UG/L 9800 UG/L 3.3UJ UG/L 1.8J UG/L 20 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL . POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE \NIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19T2 D No: 19T2 lnorg Contractor: LIBRTY Org Contractor: A4 erage value. NA-not analyzed. NAl-lnterferences. J-estlmated value. N-presumptive evidence of presence of material. Produced by: Goddard, Denise Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 Ending: tual value Is known to be leas than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitatlon limit. : Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 Sample 4380 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Programs SF Id/Station: MW5D / Media: GROUNDWATER RESULTS UNITS 120UJ UG/L 1.6U UG/L 4.4R UG/L 29J UG/L 0.31U UG/L 0.30U UG/L 27000 UG/L 0.93R UG/L 0.60U UG/L 0.70U UG/L 100J UG/L 1.3U UG/L SO00J UG/L 44J UG/L 0.10U UG/L 1.2R UG/L 2900 UG/L 2.2UJ UG/L 0.70U UG/L 11000 UG/L 3.3UJ UG/L 0.S0UJ UG/L 1.4U UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE INIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19T4 D No: 19T4 lnorg Contractor: LIBRTY Org Contractor: CEIMIC erage value. NA-not analyzed. NAl-lnterferences. J--estlmated value·. N-presumptlve evidence of presence of material. Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/23/2002 16:30 Ending: tual value is known to be less than value given. L-actual value Is known to be greater than value given. U-materlal was analyzed for but not detected. the number is the minimum quantitation limit. : Indicates that data unusable, compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 ".@!!!!liAMm!IAN,e;;alS liiiiiil liiiiil -lii&A -lliiONiiilil:S~EN..... --PrMbtid,! bate!111!!1!hs1"'21f!if!l iiil Sample 4381 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program:. SF Id/Station: MW11 / Media: GROUNDWATER ~ESULTS UNITS 34000J UG/L 1.8U UG/L 4.2U UG/L 720J UG/L 6.5 UG/L 0.30U UG/L 6900 UG/L 95J UG/L 34 UG/L 92 UG/L 79000J UG/L 42 UG/L 12000J UG/L 1900J UG/L 0.18UJ UG/L 41J UG/L 7900 UG/L 2.5R UG/L 0.70U UG/L 12000 UG/L 3.3UJ UG/L 200J UG/L 250 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE NIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19T5 D No: 19T5 lnorg Contractor: LIBRTY Org Contractor: A4 ,rage value. NA•not analyzed. NAl-lnterferences. J-estlmated value. N-presumpUve evidence of presence of material. Produced by: Goddard, Denise Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 16:00 Ending: ual value Is known to be lesa than value given. L-actual value is known to be greater than value gtven. U-material was analyzed for but not detected. the number is the minimum quantitation limit. Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 r.lllitAi';lallANallS ll!ml 1111 ~ample 4382 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program:, SF Statesville, NC Id/Station: MW27S / Media: GROUNDWATER ~ESULTS UNITS 43000J UG/L 1.6U UG/L 6.0R UG/L 940J UG/L 4.2U UG/L 0.30U UG/L 2000 UG/L 97J UG/L 88 UG/L 130 UG/L 82000J UG/L 26 UG/L 24000J UG/L 3000J UG/L 0.13UJ UG/L 110J UG/L 21000 UG/L 2.2UJ UG/L 0.70U UG/L 7500 UG/L 3.3UJ UG/L 110J UG/L 350 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE NIDE ANALYSIS NOT REQUESTED Case No: 30418 MD No: 19T6 D No: 19T6 lnorg Contractor: LIBRTY Org Contractor: A4 !lrage value. NA-not analyzed. NAl-lnterferences. J--estimated value. N;,resumptlve evidence of presence of material. Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: tual value is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number Is the minimum quantitatlon limit. Indicates that data unusable. compound may or may not be present. resampllng and reanalysis is necessary for verification. Page 1 of 1 --A ... 1otliiiiiiesd, Iii LE-A .. Sample 4383 FY 2002 Project: 02-0493 Produced by: Goddard, Denise Requeslor: METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program~ SF Id/Station: MW8 / Media: GROUNDWATER RESULTS UNITS 3300J UG/L 1.6U UG/L 14J UG/L 63J UG/L 0.84U UG/L 0.30U UG/L 1400 UG/L 36J UG/L 3.4 UG/L 11U UG/L 8200J UG/L 3.0 UG/L 2000J UG/L 110J UG/L 0.10U UG/L 13J UG/L 1600U UG/L 2.2UJ UG/L 0.70U UG/L 1100U UG/L 3.3UJ UG/L 20J UG/L 50 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE NIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19TT D No: 19TT lnorg Contractor: LIBRTY Org Contractor: A4 Project Leader: KMALLARY Beginning: 04/23/2002 17:40 Ending: arage value. NA.not analyzed. NAl-lnterferences. J-estimated value. N-presumptiv8 evidence of presence of material. tual value Is known to be less than value given. L-actual value Is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minimum quantitatlon limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 iiil -Sample 4384 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program~ SF Id/Station: MW5S / Media: GROUNDWATER ~ESULTS UNITS 16000J UG/L 1.6U UG/L 4.2U UG/L 340J UG/L 1.5U UG/L 0.30U UG/L 2000 UG/L 68J UG/L 24 UG/L 55 UG/L 47000J UG/L 16 UG/L 10000J UG/L 1000J UG/L 0.10UJ UG/L 59J UG/L 9700 UG/L 2.3R UG/L 0.70U UG/L 3700U UG/L 3.3UJ UG/L 65J UG/L 110 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE ~JOE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19W0 D No: 19W0 lnorg Contractor: LIBRTY Org Contractor: A4 1rage value. NA-not analyzed. NAl-lnterferences. J--estimated value. N-presumptive evidence of presence of material. Produced by: Goddard, Denise Requestor: Project Leader: KMALLARY Beginning: 04/23/2002 15:00 Ending: ual value Is known to be less than value given. L-actual value is known to be greater than value given. U-materlal was analyzed for but not detected. the number is the minimum quantitation limit. Indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 liiiil lllfA -18110r-illilES~Et-llllliA - Sample 4385 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program:, SF Id/Station: MW29 / Media: GROUNDWATER RESULTS UNITS 92UJ UG/l 1.9U UG/l 4.2U UG/L 73J UG/l 0.24U UG/l 0.60R UG/L 4900 UG/L 1.6UJ UG/L 0.60U UG/l 2.2U UG/L 110J UG/l 1.6R UG/l 3400J UG/l 16J UG/l 0.10U UG/l 2.6J UG/l 2200 UG/l 2.2UJ UG/L 0.70U UG/L 13000 UG/L 3.3UJ UG/L 0.58J UG/L 32 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE IIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MO No: 19W6 D No: 19W6 lnorg Contractor: LIBRTY Org Contractor: CEIMIC age value. NA-not analyzed. NAl-interferences. J-estlmated value. N-presumpllve evidence of presence of material. Produced by: Goddard, Denise Requester: Project leader: KMALLARY Beginning: 04/24/2002 17:00 Ending: al value Is known to be less then value given. l-actual value Is known to be greater than value given. LI-material was analyzed for but not detected. the number is the minlmum quantitation limit. 1dicates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification. Page 1 of 1 liiil Sample 4386 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program~ SF Id/Station: IN01 / Media: GROUNDWATER ~ESULTS UNITS 250J UG/L 1.6U UG/L 4.2U UG/L 86J UG/L 0.30U UG/L 0.30U UG/L 4300 UG/L 1.6UJ UG/L 0.90 UG/L 32 UG/L 380J UG/L 2.0R UG/L 3700J UG/L 42J UG/L 0.10U UG/L 1.9J UG/L 1600 UG/L 2.2UJ UG/L 0.70U UG/L 11000 UG/L 3.3UJ UG/L 0.88R UG/L 18 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE ~IDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19X1 D No: 19X1 lnorg Contractor: LIBRTY Org Contractor: A4 Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:30 Ending: rage value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptlve evidence of presence of material. Jal value ls known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number Is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reBnalysls is necessary for verification. Page 1 of 1 liii.i ,.._,AMl!IIIANJIIIIIS --,ample 4387 FY 2002 Project: 02-0493 IIET ALS SCAN 'acility: FCX, Inc. (Statesville Plant) 'rogramc SF d/Station: EB01 / \ledia: GROUNDWATER tESULTS UNITS 40UJ UG/L 1.6U UG/L 4.2U UG/L 0.32UJ UG/L 0.20U UG/L 0.30U UG/L 17U UG/L 0.50UJ UG/L 0.60IJ' UG/L 1.4U UG/L 22UJ UG/L 1.3U UG/L 12UJ UG/L 1.2UJ UG/L 0.10U UG/L 0.50UJ UG/L 21U UG/L 2.2UJ UG/L 0.70U UG/L 600U UG/L 3.3UJ UG/L 0.50UJ UG/L 16 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE -IIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19T9 D No: 19T9 lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA•not analyzed. NAl-lnterferences. J--estlmated value. N•presumptlve evidence of presence of material. Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/24/2002 09:00 Ending: Jal value ls known to be less than value given. l•actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitation limit. ndlcates that data unusable. compound may or may not be present. resampling and reanalysls Is necessary for verification. Page 1 of 1 ,ample 4388 FY 2002 Project: 02-0493 nETALS SCAN 'acility:. FCX, Inc. (Statesville Plant) 'rogram:·-SF d/Station: DUP02 / nedia: GROUNDWATER :ESULTS UNITS 78UJ UG/L 1.6U UG/L 4.2U UG/L 9.9J UG/L 0.26U UG/L 0.63R UG/L 4300 UG/L 0.89R UG/L 0.60U UG/L 2.8U UG/L 440J UG/L 1.3U UG/L 1400J UG/L 140J UG/L 0.10U UG/L 2.0R UG/L 1200U UG/L 2.2UJ UG/L 0.70U UG/L 6100 UG/L 3.3UJ UG/L a.sou UG/L 49 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE IIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19W2 D No: 19W2 lnorg Contractor: LIBRTY Org Contractor: A4 rage value. NA•not analyzed. NAl•interferences. Jo.estimated value. N-presumptive evidence of presence of material. Produced by: Goddard, Denise Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 Ending: Jal value Is known to be less than value given. L-actual value ls known to be greater than value gtven. U-materlal was analyzed for but not detected. the number is the minimum quantitatlon limlt. ndleates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification. Page 1 of 1 ..... AMIB!ANJlll!!IS lllill _Sample 4389 FY 2002 Project: 02-0493 "1ETALS SCAN =acility: FCX, Inc. (Statesville Plant) 0 rogram~ SF d/Station: MW6D / vledia: GROUNDWATER IESUL TS UNITS 85UJ UG/L 1.6U UG/L 4.2U UG/L 11J UG/L 0.30U UG/L 0.44R UG/L 4400 UG/L 0.64R UG/L 0.60U UG/L 1.5U UG/L 460J UG/L 1.3U UG/L 1500J UG/L 140J UG/L 0.10U UG/L 1.4R UG/L 1100 UG/L 2.6R UG/L 0.70U UG/L 6200 UG/L 3.3UJ UG/L 0.56R UG/L 34 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE •IDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19W1 D No: 19W1 lnorg Contractor: LIBRTY Org Contractor: A4 Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/24/2002 12:09 Ending: rage value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material. Jal value is known to be less than value given. L-actual value Is known to be greater than value given. LI-material was analyzed for but not detected. the number Is the minimum quantitation limit. ndicates that data unusable. compound may or may not be present. resampllng and ~eanalysis is necessary for verification. Page 1 of 1 Sample 4390 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program: SF Id/Station: MW6S / Media: GROUNDWATER ~ESULTS UNITS 5000J UG/L 1.6U UG/L 4.2U UG/L 170J UG/L 0.61U UG/L 0.30U UG/L 110 UG/L 15J UG/L 14 UG/L 14U UG/L 12000J UG/L 9.9 UG/L 2800J UG/L 500J UG/L 0.40J UG/L 13J UG/L 2900 UG/L 2.2UJ UG/L 0.70U UG/L 17000 UG/L 3.3UJ UG/L 16J UG/L 47 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE ~IDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19W3 D No: 19W3 lnorg Contractor: LIBRTY Org Contractor: A4 Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/24/2002 10:00 Ending: rage value. NA-not analyzed. NAl-lnterferences. J-estimated value. N-presumptive evidence of presence of material. Jal value Is known to be less than value given. L-actual value Is known to be greater than value given. U-materlal was analyzed for but not detected. the number is the minimum quantitation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis Is necessary for verification. Page 1 of 1 iiiiil . ~AIVBI AN-IS -liliiil Sample 4391 FY 2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Programs SF Statesville, NC Id/Station: MW25 I Media: GROUNDWATER {ESUL TS UNITS !4000J UG/L 1.6U UGIL 4.2U UG/L 530J UG/L 3.1U UGIL 0.30U UG/L 1200 UGIL 170J UG/L 60 UGIL 150 UG/L 18000J UGIL 21 UG/L 3600J UGIL 1700J UG/L 0.11UJ UG/L 29J UGIL 2600 UG/L 2.2UJ UGIL 0.70U UG/L 6600 UG/L 3.3UJ UGIL 210J UG/L 77 UGIL NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM "COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE 'IIDE ANALYSIS NOT REQUESTED Case No: 30418 MD No: 19X2 D No: 19X2 lnorg Contractor: L/BRTY Org Contractor. A4 rage value. NA.not analyzed. NAJ.interferences. J--estlmated value. N•presumptive evidence of presence of material. Produced by: Goddard, Denise Requestor: Project Leader: KMALLARY Beginning: 04/24/2002 16:30 Ending: Jal value Is known to be less than value giyen. l•actual value ls known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantitatlon limit. ndicates that data unusable. compound may or may not be present. resampling and reanalysis ls necessary for verification. Page 1 of 1 - iiiil .... AMilaAN ..... IS l!!I! ,ample 4392 . FY 2002 Project: 02-0493 AETALS SCAN 'acility: FCX, Inc. (Statesville Plant) 'rogram;_ SF cl/Station: MW7 / Aedia: GROUNDWATER :ESULTS UNITS 1200J UG/L 1.6U UG/L 4.2U UG/L 270J UG/L 0.86U UG/L 0.30U UG/L 540 UG/L 6.8UJ UG/L 15 UG/L 9.5U UG/L 2600J UG/L 2.7 UG/L 4200J UG/L 280J UG/L 0.10U UG/L 15J UG/L 2500 UG/L 2.2UJ UG/L 0.70U UG/L ·0000 UG/L 3.3UJ UG/L 2.8J UG/L 74 UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE IIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19W5 D No: 19W5 lnorg Contractor: LIBRTY Org Contractor: A4 Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/24/2002 14:30 Ending: age value. NA-not analyzed. NAl•lnterferences. J-estimated value. N-presumptlve evidence of presence of material. al value Is known to be less than value given. L-actual value Is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quanlitation limit. 1dlcates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 iiiil ,ample 4393 FY 2002 Project: 02-0493 \1ETALS SCAN =acility: FCX, Inc. (Statesville Plant) 0rogramc SF d/Station: FB01 / \1edia: GROUNDWATER tESULTS UNITS 38UJ UG/L 1.6U UG/L 4.2U UG/L 0.10UJ UG/L 0.20U UG/L 0.30U UG/L 17U UG/L O,SOUJ UG/L 0.60U UG/L 0.70U UG/L 14UJ UG/L 1.3U UG/L 12UJ UG/L 0.30UJ UG/L 0.10U UG/L 0.50UJ UG/L 13U . UG/L 2.2UJ UG/L 0.70U UG/L 210U UG/L 3.3UJ UG/L 0.50UJ UG/L 1.4U UG/L NA UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON. LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE ~IDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19X3 D No: 19X3 lnorg Contractor: LIBRTY Org Contractor: A4 Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:15 Ending: rage value. NA-not analyzed. NAl-lnterferences. J-estlmated value. N-presumptive evidence of presence of material. J&I value la known to be less than value given. L-actual value Is known to be greater than value given. U-materlal was analyzed for but not detected. the number is the minimum quantitation limit. ndleates that data unusable. compound may or may not be present. resampllng and reanalysis Is necessary for verification. Page 1 of 1 iiiil Sample -~~.:.;--'rr'-'=2002 Project: 02-0493 METALS SCAN Facility: FCX, Inc. (Statesville Plant) Program;, SF Id/Station: PB01 / Media: GROUNDWATER ~ESULTS 23UJ 1.6U 4.7R 0.10UJ 0.20U 0.30U 17U 0.50UJ 0.60U 0.70U 17UJ 1.3U 12UJ 0.45UJ 0.10U O.SOUJ 13U 2.2UJ 0.70U 280U 3.3UJ 0.50UJ 1.4U NA UNITS UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L ANALYTE ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COPPER IRON LEAD MAGNESIUM MANGANESE TOTAL MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM VANADIUM ZINC CYANIDE NIDE ANALYSIS NOT REQUESTED Statesville, NC Case No: 30418 MD No: 19X4 D No: 19X4 lnorg Contractor: LIBRTY Org Coniractor: A4 ,rage value. NA-not analyzed. NAl-lnterferences. J-estlmated value. N-presumptlve evidence of presence of materl_aL Produced by: Goddard, Denise Requester: Project Leader: KMALLARY Beginning: 04/24/2002 15:00 Ending: ual value Is known to be less than value given. L-actual value is known to be greater than value given. U-material was analyzed for but not detected. the number is the minimum quantltation limit. indicates that data unusable. compound may or may not be present. resampling and reanalysis is necessary for verification. Page 1 of 1 I I I I I I I I I I APPENDIXF TREND ANALYSES CHARTS I I I I .I I I I I liiiiil ---l!!!l!!I -----liiiil --.. .. --iiill liiil Pesticide Trends in MW-I 3.500 - . . .. -·· . --· --·-. ~ -l 'an 3.000 ---•· 2.500 2-2.000 1 ----==· ..:.-:...,,,; C 0 ~ ~ -,. ~ 1.500 C 0 u 1.000 -i ----• ___ -==!,._-___ .:._ ·_ 0.500 -i----~~ 0.000 0 0 C. 0. < 0 0 ' C ::, ~ 0 0 ' oI) ::, < • .<. _, -1 ----. --==-=----=--=-=-=· -~ _ __.__=---=----~ -~-~ -------=·•-:---::.·_-=...i:;-='::·,;;;· 0 0 ' u 0 0 0 ' (.) 0.) 0 0 ' ..D Cl µ.., :,tt _ __,,_ ..:,---=-::· 0 0 ' ' B.. C ::, < ~ Sample Date 0 OJ) ::, < 0 ' u 0 0 ' u " 0 ., ·,:, /J •. ~...! N 0 ' ..D <l) µ.., N 0 C. 0. < --Alpha-BHC -o-Beta-BHC Dieldrin , . .., --Gamma-BHC (Lindane) -o-Heptachlor Epoxide - ------.. - - Pesticide Trends in MW-2 0.500 ' --,.-". ---.--,,.--,-.-; - . .., .... -7.; 0 .400 -r·-·--""· ~=-'='· ~~s,,~-~ss·~~----~."s-. ~--""· ·=·===-·e,e·=· -'=-"=-"'="-="··-==-=-· -='-c-.s=, s.a. __ as,· cc-see--aca·=·=-"'"'·=-:.:~;;...,..~. =·-· eec.~.ces..··=-.--ea,-.<e_-_=-~-"":c';-':: .=e;,=-,a._.-_es=.I -,'>.•.•••a••,;;''(:, •• ,-• • •••• > ,•'t•;' f ,- 3 . •·'"" -~9!' 0.1 00 1:-:::-=~=~:::::~:=-=:-:-:·-:· ::-:::::-:-~-=-~:·:·~~~:;·-;;;:;-~:;-~;;--~;,::-::;-r~;:~~-;:;-;g·;;· ~-;::-~----,J .---. , --_---------------r---~ . :---c-=~,,.,,....---: ·_ ,: -~ .... "' . -:=:-: .... :· ,~--:-q '' --~=-----:--··...:~_~--:-~:..:--~ _ _;__~_-_. ~ -· -_,:;:_-:;-1 " 0 -:c:__ 0.250 -l-~~~-:ce,c_:=~e:-ae_-~-c-e·-'=·~--~-~-~-=cec"~-'=. =-='-"=--~-=-'-~--~-"=-=". c-S=---='--e==S='='~--="b-a~~===='=~""'-=· °"'-~-::.'::'. ' . '. , ' ~ /! j ."!. •• '1) <..) § u 0 000 0 0 ' ,... 0. < 0 0 ' " ::, ~ 0 0 0 0 0 0 ' ' ' bi) ti ::, < 0 <..) V 0 0 0 0 0 0 ' ' ' ' ' .D ,... " bi) ti '1) 0. ::, ::, LL. < ~ < 0 Sample Date N N 0 0 0 ' ' ' <..) .D ,... '1) '-' 0. 0 LL. < Bil liiliil lliiil -Alpha-BHC ---Beta-BHC -<)--Heptachlor Epoxide -- 8.00 6.00 5.00 ;,; 4.00 '--C (I) u s u 2.00 1.00 -----.. -.. - - Pesticide trends in MW-5S --·~~ . - • ' • '. • . ' ., ._.., . ' i . . I _____ :J ------, ............. __ _._______· __ . __ __.__· ___ , ------·-------------------1 I I -----------.. -_.'.... ..:__· _,_ --__j -. ' . . . . . . ' ~ - ----. ---' -------y ------~ -~- . . . ~ • J" .,,,.. -- "'-~¾~--~=3/~cs'""ce-o-'.-=.=a-=-=-"'--s=s-=c...es-c:-e,;::sa-aa_,s_;e,,_s== --=---~--~_.:__=-::._-_=._-_-_=:-_-_-_____ ___;_-~-~ :_.··-~---'.. 0.00 -.. --__ ·: ---:_, ___ :'__ "-----· ---~--- 0 0 0 0 0 N N 0 0 0 0 0 0 0 0 0 0 0 0 0 ' ' ' ' ' ' ' ' ' ' ' ' ' '-C 00 0 u .0 '-C 00 0 u .0 '-0. :, :, V ,;-' 0. :, :, <1) V 0. < ~ < 0 0 < ~ < 0 0 "-< Sample Dates -llii} -+-Alpha-BHC Beta-BHC ---Jl(---Gamma-BHC (Lindane) liill liiii iiiil -liilll -.. 4.50 ( ' 4.00 3.50 ~ 3.00 ....) -01) ::, ~ 2.50 8 cl ~ ~ 2.00 (.) C: ' 0 u 1.50 1.00 L' 0.50 0.00 0 0 0 0 0 0 0 0 0 0 ' ' ' ' ' ~ C: 01) u (.) 0. ::, ::, '1) <( ~ <( 0 0 --.. .., Pesticide Trends in MW-5D ~'~-------~-· ~- ------------- 0 0 0 ' ' ' .D ~ C: " 0. ::, LL. <( ~ Sample Dates 0 ' 01) ::, <( .. 0 ' u 0 0 ' (.) " 0 N 0 ' .D <l) LL. .. tiilil --Alpha-BHC Beta-BHC ---¼-Gamma-BHC (Lindane) liiiil C 0 liilil'I 1.20 1.00 0.80 -~ 0.60 5 0 ~ 0 u 0.40 0.20 0.00 I. I: i '- 0 0 ' '-a. <( iiiil liiiJ ---'------'- 0 0 0 0 0 0 0 0 ' ' ' ' C OJj u 0 ;:J ;:J C) ~ <( 0 Q --=i Pesticde Trends in W-29 < ~ •• ' . . \. ~,. ·L - , -· •.-.. .·· --+--Alpha-BHC --Gamma-BHC (Lindane) --+-Heptachlor Epoxide --.---.,-7 • I ',..____ _____ -~------ N N 0 0 0 0 0 0 0 0 ' ' ' ' ' ' ' ' ..0 '-C OJj u 0 ..0 '-0 a. ;:J ;:J u V a. '-', < ~ <( 0 Q '-', <( Sample Dates --iiiiil liiiil iiiil iiiil iill -l!!l!!!l VOC Trends in MW-5D 45 40 ,~-~"=--=_c~~~-~~=-~-~-~~--~~~:---~-~-e=--,=--~=ec-=''S'"~C=-~=-"'~~--~--~-=-="=· ·=•-=-~-~--=-~-~--~--=~-~-=-=--=•-=-=-·-"'---' ,-: -------, ~ :<· 1 35 30 15 10 5 0 , _ __:_. _' ·, ---_, _ _, . 0 0 ~ 0. < 0 0 ' OI) ::l < ----·----- 0 0 0 0 ' ' u u 0 V Ci ---' -1 -----~------ --------------- • -1 --____ _____J N N 0 0 0 0 0 0 0 0 ' ' ' ' ' ' ' ' .D ... ,::: Oil u u .D ... <l) 0. ::l ::l u "' 0. c,.. < ~ < 0 Ci c,.. < Sample Dates e:51 ---I, 1-Dichloroethane ---o---Tetrachloroethene (PCE) -+-Trichloroethene § ;; h " '1) 0 " 0 u liiiii VOC Trends in MW-6D .- 14 ·," 12 ,--C----.~--~-~~~~-~.~~~---~.-·~,~~--~#-=-=~-~-~--=-~-='='==-~--aa===""'-<~~====~-~=-~--=--~-~-·~-,-i -' .,. ' 8 6 '-, ~-_______ ....... ~----·--- -. 4 2 ______ -0--.,...-- ~. - 0 ----------------___ ....:....:. ....... __ 0 0 0 0 0 N N 0 0 0 0 0 0 0 0 0 0 9 0 0 ' ' ' ' ' ' ' ' ' ' ' "-h " O!) u 0 ..0 h " O!) u 0 ..0 Q. :, :, V V Q. :, :, 0) V Q. <I'. ~ <I'. 0 0 u.. <I'. ~ <I'. 0 0 u.. <I'. Sample Dates liiil -o-1, 1-Dichloroethene ---Chloroform -o-Tetrachloroethene (PCE) --t-Trichloroethene iiiil -iiilil liil YOC Trends in MW-9 I 250 ._, _,_, ____ ..u ... ,~7","---. -::-, .... ,! . ,. ~ '.;I I 'I , I 200 _j --+---I, 1-Dichloroethane --o--I, 1-Dichloroethene -¼--Chloromethane '\,. -O-Tetrachloroethene (PCE) -+-Trichloroethene 0 ' 0 0 0 0 0 N N 0 0 0 0 0 0 0 0 0 0 0 0 0 ' ' ' ' ' ' ' ' ' ' ' ' ' ,_ C 01) u u ,D ,_ C 01) u u ,D ,_ 0. ::J ::J V V 0. ::J ::J u C) 0. < ~ < 0 0 "-< ~ < 0 0 "-< Sample Dates -llliE 50 40 20 10 0 0 0 0 0 0 0 0 0 0 0 0 ' ' ' ' ' ' '-" oJJ u u n 0. ;::, ;::, V V -< ~ -< 0 0 Cl. iiiil iiiiii) liil I!!!!!] VOC Trends in MW-I I 0 0 0 ' ' ' '-~ oJJ 0. ;::, ::, -< ~ -< Sample Dates 0 ' u 0 . . -----------~ -- 0 ' u V 0 ,. --~---:---=-1 N 0 ' n a, Cl. ' i ' --........i !!!!!!I -+-I, 1-Dichloroethane -O-Tetrachloroethene (PCE) -+-Trichloroethene VJ '" a 'O ii'" tJ '" ;; V, Apr-00 .lun-00 Aug-00 Oct-00 -0 V, 0 Concentration (ug/L) -v, tv 0 tv V, ' <.,; 0 w V, 1----, -·,:_-··-----:--;~-:,-;c--_ --··:;,--· ----1~-----.·:1 •. II > 11· . ·!I ' !i . Ii,:·· : )1·· -.. 1::.. . • I I •. I . • . 't ' L I I . . 1 . I _2_J_'il~-. ~-··t!i •~-j! ': 7[ · i,:' .: I .... I ' ' [!·: iii ,-i .·.(::~ii· ·I· ·_1:1, • 1 · · · I' · 1 · · · · I · I 1 • I I,,-·. . . , ;i I · · .'. I '.. . · I• .. · • ' · 11--..:.0-II , I • ' • , 1 . ·,. It ' ,I •, ' :j:' '.J ! . -4 0 !l 'I . ·1, ,11 ·· < .. ·11 . ' 11 I. . I, j ,t .'· o·!i ;'1· I . . Ii '-I • . - ' :· . -1 f : ' < ' -~"'. 1 ~ Dec-00 -11-' ·. . '1 . • ... II r :: ' i: ' . : • . ,· : : : . . ;II:,:: .•.. l I . I . . I •• I · 1 ·· . . ' '! ' I. i. I . Feb-01 f .... 11. :··: [ ·, ·.:Ji . ·. · , I . ·,il-· · . ~-· Apr-01 .lun-01 Aug-01 Oct-01 Dec-01 Feb-02 J\pr-02 . ·'· : ': ; .. . , . :,; • ; ' : . : ' ! •• . : . • . ~ I I . . . 1 I · ·, :· I· . . . I ' . . . ·1 ' . . . 1 · . . j ' . ' ' I , . _ . i_ .. . . If _;_ ~----· --., -1 ·_··· .. > . ,. 1· ·, ''i . _;:::: i ._ . : I . 1· · -· ii : .· · . . f . . . I ·. 111· ·,··. ·1': · ·; .. ·1 .-. ·. 11_· ·: ,-: .. ·• 1·1 · -, .. ·• ·. "· .· :•. . . . ~ ' I ;-I " ',; ·, ._· . . I • · 1 -. ;. i d' · 1 ·, -1 -Ii. ! ' . :I\ ·~ .~j . ! I, , 11 . i ·. ·: l ':· ·11 :f: , .. ii . :j1 . ill'' . ' I · .· 1 I:· · -1 · .· . · : ' _ : ; I_ ; · . :··i r . : . · . · , ,.· ·J,' w .· . ii .':: :I .·. ::i, ··\ 1i ·. ·.°Ji· . ,' II::.·. i· · . 11 , . i 1 : . . 1 · .. ··1 ~ . · ·. · -i , . , ·i I . , · 1 . . : : . , lL ·::1L· ,, ·, ,· ,:· ··::. ,i. ·1. '. L.~ ..... J -~-J ___ :_Jl ,c.cJ:_ · .. ,:1·, .• :. IL.· _:_, __ ,_j t ? ..., ..., ..., (I) n· :; ;:," '" -(') 0 ;:," ..., -0 0 (1) ..., ~ 0 ;:," (1) (1) ~ " ;:," (1) (I) " (1) ~ >-t) () c I I I I I I I I < ' I ~ I (I) I " ~ I ::;:: I ' ';: I I I i ~ ~ ~ a D C 0 60 50 40 30 2 5 u g u 20 IO 0 91 . ---.. -·' . ' . . -----~ i !, ___ --------------.,. --,--:--.' T -----,-.--.;, • ,, ----.---- .. , ,, VOC Trends in W-29 •,t, ·--------1.~ --~-·-------- : ... -·-----"--1 __ .,_ ' ,, ----·;, I --~-----·....: ·-----· . -.. ----. ---.. --· ____ _:_____ -. ---. -_.-----...:...... . .,_ -. -1 0 0 0 0 0 N N 0 0 0 0 0 0 0 0 0 0 0 0 0 ' ' ' ' ' ' ' ' ' ' ' ' ' Cl.. C oJJ u u .D ~ C oJJ u u .D ~ ;::J ;::J 0 0 V 0. ;::J ;::J V V 0. <!'. -. <!'. Cl u... <!'. -. <!'. 0 Cl u... <!'. Sample Dates el ---+--I, 1-Dichloroethane -¾--Chloroform --o---Tetrachloroethene (PCE) -t-Trichloroethene I I I I I I I I I I APPENDIXG DEPTH TOW ATER CHARTS H D I I I I I I I 70.00 60.00 50.00 2 i 30.00 "' 0 20.00 10.00 0.00 11/01/2001 . ... ./ -~ / . 12/01/2001 Depth to Water RW-10 November 200 l through April 2002 .. . A --___/ ' ' 01/01/2002 02/01/2002 03/01/2002 Dates • V -. A\ \ 04/01/2002 05/01/2002 - - - - - -----&iii _, iiil illll --.. -liill· ~ a:: ~ ~ (U "' 3: 0 .c 0. a) Cl · 70.00 60.00 . 50.00 40.00 30.00 20.00 10.00 0.00 11/01/2001 . • ' 12/01/2001 Depth to Water RW-9 November 2001 through April 2002 ' 0 l /0 l /2002 ' 02/01/2002 Dates -, 03/01/2002 ~ . ~\ \ 04/01/2002 05/01/2002 ~ a:: ~ '-cu cii 60.00 50.00 40.00 :3: 30.00 2 ..c: 0. "' 0 20.00 10.00 0.00 11/01/2001 Depth to Water RW-8 November 200 I through April 2002 /V. ~ ~- ~ 12/0 I /200 I 01/01/2002 • • 02/01/2002 Dates ♦ ' 03/01/2002 ♦ . ..... , \ ' 04/01/2002 05/01/2002 ~ ,;:: ~ '-<l) '" Depth to Water RW-7 November 200 l through April 2002 ~ 30.00 -i-------------------------------------------j ..c 0. <l) 0 0.00 -t--------,-------,----------,-------,--------,---------,J l 1/01/2001 12/0 l /200 I 01/01/2002 02/01/2002 03/01/2002 04/01/2002 05/01/2002 Dates ~ ,;:: ~ i, ;; Depth to Water RW-6 November 2001 through April 2002 :$ 30.00 -j--------------------------------------_J 2 .<:: 0-" 0 0.00 -j--------~-----------~-----------------_J 11/01/2001 12/01/200 l 01/01/2002 02/01/2002 03/01/2002 04/01/2002 05/0 l /2002 Dates ~ a:: ~ '-a) ;;; Depth to Water RW-5 November 201 through April 2002 ;3: 30.00 -+--------------------------------------__j 3 0.00 -+-------------~------------------------__j 11/01/2001 12/01/2001 01/01/2002 02/01/2002 03/0 l /2002 04/01/2002 05/01/2002 Dates -= --&ill! lliliil -._, .. --liiil liiil -----illil - ~ c;:: ~ '-v "' Depth to Water RW-4 November 200 I through April 2002 40.00 -i-----------------------------------\-------c :$ 30.00 -i-----------------------------------------j 0 -..c: 0. "' Cl 0.00 -t-------,---------,---------,-------,--------,--------,J 11/01/2001 12/01/200 I 01/01/2002 02/01/2002 03/01/2002 04/01/2002 05/01/2002 Dates ~ <;:: ~ .... '-' cl ~ 0 ..c: 0. <l.) Cl 70.00 60.00 50.00 40.00 30.00 20.00 10.00 0.00 11/01/200 I . . . . . ' 12/0 I /200 I Depth to Water RW-3 November 200 I through April 2002 . . . ' 01/01/2002 ' 02/01/2002 Dates I I 1 ' 03/01/2002 \ \ • 7 ' 04/01/2002 05/01/2002 ~ q:: ~ ~ 'ci ~ 0 ..c 0. " Cl 50.00 40.00 30.00 20.00 Depth to Water RW-2 November 200 l through April 2002 0.00 +-------------~------------------------~ l 1/0 l/200 l 12/01/200 I 0l/01/2002 02/01/2002 03/01/2002 04/01/2002 05/01/2002 Dates ---- 70.00 60.00 50.00 ;, 40.00 '" "' 0 li 30.00 <l) 0 20.00 10.00 0.00 l---/ I 1/01/2001 - -- - - l!!!!!l!!!I 9:1 Depth to Water RW-1 November 200 I through April 2002 \ ~ ~ . - ' I 2/01/2001 . . -- ' 01/01/2002 . - 02/01/2002 Dates 03/01/2002 liiiill l!iiiil iiiil iiliil . I\ I I V \ I ". ' 04/01/2002 05/01/2002